MO-29128_48312_CA_IAR_20220303_Initial Abatement Action Report

hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS
Via Email
March 3, 2022
NC DEQ Division of Waste Management
UST Section
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Attention: Ms. Beverly Trudy
RE: IAA Report
Puckett/Nash Assemblage
Charlotte, NC
H&H Job No. WIT-019
Dear Beverly,
On behalf of Withrow Capital, Inc, Hart & Hickman is submitting the attached Initial Abetment
Action (IAA) Report for the above referenced property located in Charlotte, Mecklenburg County,
North Carolina.
If you have any questions or comments, please do not hesitate to contact me.
Sincerely,
Hart & Hickman, PC
Stephen R. Libbey, P.G.
Project Manager
Enclosures
cc: Withrow Capital, Inc (via email)
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

Initial Abatement Action Report
Puckett/Nash Assemblage
Puckett Road
Charlotte, North Carolina
H&H Job No. WIT-019
March 3, 2022
hart � hickman
SMARTER ENVIRONMENTAL SOLUTIONS
#C-1269 Engineering
#245 Geology
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

Initial Abatement Action Report
A. Site Information
1. Site Identification
Date of Report: March 3, 2022
Facility ID: N/A UST Incident Number: N/A
Site Name: Puckett/Nash Assemblage
Site Street Address: 10219 and 10200 Puckett Road
City, Town: Charlotte, NC Zip Code: 28216 County: Mecklenburg
Description of Geographical Data Point: UST Basin
Location Method: Internet GIS Mapping
Latitude: 35.214028 Longitude:-80.504156
2a. Information about Contacts Associated with the Leaking UST System
UST Owner: James Geoffrev Nash
Address: 19306 Wildcat Trail, Davidson, NC, 28036 Tel.: [phone]
UST Operator: Unknown
Address: N/A Tel.: N/A
Property Owner: James Geoffrey Nash
Address: 19306 Wildcat Trail, Davidson, NC, 29036 Tel.:
Property Occupant: vacant
Address: 10200 Puckett Road (Parcel No. 02507204) Tel.: N/A
Consultant/Contractor: Hart & Hickman, PC
Address: 2923 South Tryon Street, Ste 100, Charlotte, NC 28203
Tel.: [phone]
Analytical Laboratory: Waypoint Analytical, LLC State Cert. No. 402
Address: 449 Springbrook Road, Charlotte, North Carolina Tel.: [phone]
2b. Information about Contacts Associated with the Leaking UST System
UST Owner: Joe Lee. Mack Vance Puckett. and James Geoffrev Nash
Address: 19306 Wildcat Trail, Davidson, NC, 28036 Tel.: [phone]
UST Operator: Unknown
Address: N/A Tel.: N/A
Property Owner: Joe Lee and Mack Vance Puckett and James Geoffrey Nash
Address: 19306 Wildcat Trail, Davidson, NC, 29036 Tel.:
Property Occupant: vacant
Address: 10219 Puckett Road (Parcel No. 02508102) Tel.: N/A
Consultant/Contractor: Hart & Hickman, PC
Address: 2923 South Tryon Street, Ste 100, Charlotte, NC 28203
Tel.: [phone]
Analytical Laboratory: WMToint Analytical, LLC State Cert. No. 402
Address: 449 Springbrook Road, Charlotte, North Carolina Tel.: [phone]
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3. Information About Release
Date Discovered: March 2, 2020
Estimated Quantity of Release: Unknown
Cause of Release: Leakingheating eating oil USTs
Source of Release: Out of use heating oil USTs
Sizes and contents of UST system: two (2) 550-gallon heating oil USTs
4. Certification
I, Stephen Libbey, PG, a Professional Geologist for Hart & Hickman, PC, do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
NSg6 ���
SEAL
1658 _ 03/03/22
Hart & Hickman, PC is licensed to practice geology/engineering in North Carolina. The
certification numbers of the company are C-245/C-1269.
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B. Site History and Characterization
1. UST Owner and Operator Information:
UST ID Number UST-1
Facility ID Number
N/A
Name of Owner
Dates of Ownership
James Geoffrey Nash
prior to 1990-present
Street Address
19306 Wildcat Trail
City
State
Zip
Telephone Number
Davidson
NC
28036
336-722-0885
Name of Operator
Dates of Operation
Unknown
Unknown
Street Address
City
State
Zip
Telephone Number
UST ID Number
UST-2
Facility ID Number
N/A
Name of Owners
Dates of Ownership
Joe Lee, Mack Vance Puckett, and James
Geoffrey Nash
prior to 1990-present
Street Address
19306 Wildcat Trail
City
State
Zip
Telephone Number
Davidson
NC
28036
336-722-0885
Name of Operator
Dates of Operation
Unknown
Unknown
Street Address
City
State
Zip
Telephone Number
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2. UST Information:
Description
Was
release
UST ID
Current/Last
Previous
Capacity
Construction
Tank
of
Date
Status of
associated
Number
Contents
Contents
(gallons)
Details
Dimensions
Associated
Tank
UST
with the
Piping and
Installed
UST
Pumps
System?
UST-1
Heating Oil
None
550
Single -walled
42" x 6'6"
N/A
Unknown
Removed
Yes
steel
UST-2
Heating Oil
None
550
Single -walled
42" x 6'6"
N/A
Unknown
Removed
Yes
steel
4 hart hickman
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3. Non -UST spills at the site:
No non -UST spills are known to exist at the subject site.
4. Description of release:
On March 2, 2020, EVO Environmental and Industrial Resources (EVO) of Winston-
Salem, NC removed two inactive residential 550-gallon heating oil USTs at the subject
site. Following removal of the USTs, field screening of soils using a photoionization
detector (PID) indicated elevated readings in the UST basins soils. Soil was excavated
from the UST basins until the field screening indicated impacted soils were removed.
UST removal activities are discussed further in Section D.
5. Site characteristics:
The site is comprised of four contiguous residential parcels of land (Parcel IDs:
02508101, 02508102, 02507201, and 02507204) that total approximately 21 acres. The
site was formerly developed with four single-family residences, two agricultural
buildings, and a detached garage. The site is located southwest of the intersection of
Interstate-485 and Interstate-77 and along former Puckett Road. A Site location map is
presented as Figure 1 and a Site layout is depicted on Figure 2.
The subject site is located in the Piedmont Physiographic Province of North Carolina.
According to the Geologic Map of North Carolina dated 1985, the subject property lies
within the Charlotte Belt. In the site area, underlying bedrock is composed of granitic
rock. The land surface of the area is generally characterized as gently sloping, which
may become moderately steep where intersected by streams.
In the Piedmont, the bedrock is overlain by a mantle of weathered rock termed saprolite
or residuum. The saprolite consists of unconsolidated clay, silt, and sand with lesser
amounts of rock fragments. Due to the range of parent rock types and their variable
susceptibility to weathering, the saprolite ranges widely in color, texture, and thickness.
Generally, the saprolite is thickest near interstream divides and thins toward streambeds.
In profile, the saprolite normally grades from clayey soils near the land surface to highly
weathered rock above the competent bedrock.
The occurrence and movement of groundwater in the Piedmont is typically within two
separate but interconnected water -bearing zones. A shallow water -bearing zone occurs
within the saprolite, and a deeper water -bearing zone occurs within the underlying
bedrock.
Groundwater in the shallow saprolite zone occurs in the interstitial pore spaces between
the grains comprising the saprolite soils. Groundwater in this zone is typically under
water table or unconfined conditions. Groundwater movement is generally lateral from
recharge areas to small streams that serve as localized discharge points.
The UST parcels are located at an approximate elevation of 790 ft to 810 ft above mean
sea level. The site is located on a topographic high, therefore, the eastern portion of the
site slopes to the east, the western portion of the site slopes to the west, and the southern
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portion of the site slopes to the south. Dixon Branch is located approximately 2,000
southeast of the UST basins, and Vances Twin Lakes Stream, a tributary of Dixon
Branch, is located approximately 1,010 feet east of the UST-1 basin. Based on
topography, H&H anticipates that the groundwater flow direction in the vicinity of the
UST basins is to east-southeast towards Vances Twin Lakes Stream (Figure 1).
Visual observations during the removal of the USTs indicate that the soil in the area of
the USTs consists of reddish clayey silt. Groundwater was not encountered during the
excavation activities. The maximum depths observed during the excavation activities
were 7 feet below ground surface (ft bgs) in the UST-1 excavation and 5 ft bgs in the
UST-2 excavation.
The site has been vacant since the early 2000s. Electricity was previously provided to the
site by Duke Energy. The residences were connected to private water supply wells and
septic systems when occupied. The water supply wells and septic systems will be
abandoned prior to redevelopment of the site.
6. Initial abatement actions, assessment activities, and corrective actions performed to
date:
No other known assessment or corrective actions have been conducted at the site.
C. Site Check Report
Not Applicable
D. UST Closure Report following UST-12 format and Site Investigation Report for
Permanent Closure or Change -in -Service of UST (UST-2 Form)
1. Preparations for closure including the steps taken to notify authorities, permits
obtained and the steps taken to clean and purge the tanks:
The UST removal activities were conducted by EVO of Winston-Salem, North Carolina
on March 2, 2020 and October 19, 2021. A permit to remove the USTs was not required
from the local fire department because the USTs were non -regulated heating oil tanks.
Prior to removal activities, approximately 30 gallons of residual fluid and sludge were
pumped from UST-1 by EVO into a 55-gallon drum. UST-2 did not contain any
measurable fluids. The USTs were then rinsed with water by EVO. Following removal
of the residual fluids and rinse water, the USTs were tested with a combustible gas
indicator to ensure that potentially combustible vapors had dissipated.
2. Closure procedures:
Initially, soil was removed from the top and sides of the USTs with a track hoe so that the
tanks could be removed from the ground. Soils encountered during the excavations were
evaluated in the field for the presence of odors and staining, and for the presence of
organic vapor with a PID. The PID was calibrated prior to its use against an isobutylene
standard.
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Following removal, the USTs were inspected for holes, scaling, and pitting. The tanks
were constructed of single -walled steel. No holes were observed on the tanks. However,
the tanks were observed with large scale rust.
3. Note the amount of residual material pumped from the tank and describe the
storage, sampling and disposal of the residual material and the disposal of the tank,
pumps and piping:
As stated above, approximately 30 total gallons of residual fluid, sludge, and rinse water
were removed from the USTs. The liquids were disposed of at EVO's treatment facility
in Winston-Salem, NC. The disposal manifest is included in Appendix A.
The USTs were transported off -site by EVO for disposal at EVO's facility in Winston-
Salem, NC. The tank disposal certificates are included in Appendix B.
4. Initial response actions and initial abatement actions:
Initial response and abatement actions are discussed in the following section.
5. Soil excavation and site investigation activities:
After removal of the USTs, one closure soil sample was collected below UST-1 and one
closure soil sample was collected below UST-2. The closure samples were collected
using a track -hoe bucket and a nitrile glove -covered hand, placed in a Ziploc bag, and
screened with a PID for organic vapors. PID readings as high as 70.4 parts per million
(ppm) were recorded from the base of the UST-1 basin and as high as 72.1 ppm along the
western sidewall of the UST-2 basin.
Approximately 8.3 tons of impacted soil was excavated from the UST-1 basin and
approximately 9 tons of impacted soil was excavated from the UST-2 basin as part of the
UST removal activities. The stockpiled soil was placed on plastic sheeting and covered
with plastic sheeting for long term storage. Groundwater was not encountered in the
excavation basins. The approximate dimensions of the UST-1 excavation were 8 feet
long by 5 feet wide and 7 feet deep. The approximate dimensions of the UST-2
excavation were 8 feet long by 4 feet wide and 5 feet deep. Following soil removal and
soil sample collection, the UST excavations were backfilled with native soils from on -
site.
It is important to note that due to limited site accessibility, EVO was unable to remove
the stockpiled soils from the site during the UST removal activities in April 2020. The
stockpiles were hauled off -site and additional impacted soils were excavated and hauled
off -site in October 2021 as discussed below.
Following soil excavation, five post -excavation confirmation soil samples (UST-1 Basin,
and UST-1 Sidewall N, E, S, and W) were collected from the UST-1 basin and five post -
excavation soil samples (UST-2 Basin, and UST-2 Sidewall N, E, S, and W) were
collected from the UST-2 basin. In accordance with DEQ guidance, the soil samples
were analyzed for volatile organic compounds (VOCs) by EPA Method 8260, semi-
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VOCs by EPA Method 8270, and volatile petroleum hydrocarbons (VPH) and extractable
petroleum hydrocarbons (EPH) by the Massachusetts Department of Environmental
Protection (MADEP) Methods.
The results of analyses of the post -excavation samples indicated that samples collected
from UST-1 basin did not contain compound concentrations above DEQ Maximum Soil
Contaminant Concentrations (MSCCs). C11-C22 Aromatics were detected at a
concentration in UST-2 basin sample UST-2 Sidewall N above its respective Soil -to -
Groundwater MSCC, but below Residential and Commercial/Industrial MSCCs.
Due to the slight exceedance of the Soil -to -Groundwater MSCC in soil sample UST-2
Sidewall N, H&H re -visited the site on March 18, 2020 and sampled approximately 5 feet
north of the previous UST-2 Sidewall N sample location. Based on the analytical results
for subsequent soil sample UST-2 Sidewall N2, no target compounds were detected
above laboratory detection limits.
As part of UST closure sampling, composite soil samples Stockpile-1 and Stockpile-2
were collected from the soil stockpiles. The soil samples were analyzed for gasoline -
range total petroleum hydrocarbons (TPH-GRO) by EPA Method 5030/8015M and
diesel -range total petroleum hydrocarbons (TPH-DRO) by EPA Method 3550/8015M.
TPH-GRO and TPH-DRO were not detected above laboratory detection limits in soil
sample Stockpile-1. The analytical results for soil sample Stockpile-2 indicated TPH-
GRO (410 mg/kg) and TPH-DRO (860 mg/kg) concentrations above the action levels of
50 mg/kg and 100 mg/kg, respectively.
On October 19, 2021, following the installation of access roads to the site, the previously
stockpiled soils were hauled off -site by EVO. In addition, an additional approximately
5.5 tons of impacted soils were excavated from the former basin sidewall up to the
location of former soil sample UST-2 Sidewall N2. Following soil removal, the
excavation was backfilled with native soils from on -site. Copies of the certificates of
disposal, non -hazardous waste manifests, and certified weight tickets for the excavated
soil are provided in Appendix C.
The approximate footprints of the UST-1 and UST-2 basin excavations are depicted in
Figure 3. The soil sample analytical results, analytical methods, and sample depths are
summarized in Table 1. The laboratory analytical data report and chain -of -custody
record are provided in Appendix D.
E. Free Product Investigation and Recovery Report
No free product has been detected at the site.
F. Groundwater and Surface Water Investigation
No groundwater or surface water samples were collected during UST closure activities.
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G. Initial Response and Abatement Activities
See Section B.
H. Excavation of Contaminated Soil
See Section D.
I. Conclusions and Recommendations:
On March 2, 2020, two inactive residential 550-gallon heating oil USTs were removed from
the site. Approximately 23 tons of impacted soils were excavated for off -site disposal from
the UST-1 and UST-2 basins. Analytical results of confirmation soil samples collected from
the UST-1 and UST-2 basins do not indicate the presence of VOCs, SVOCs, VPH, or EPH at
concentrations above DEQ MSCCs.
Based on the results of the initial abatement action activities, H&H recommends that DEQ
issue a no further action (NFA) letter for the UST incident.
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Table 1
Summary of Soil Sampling Results
Puckett/Nash Assemblage
Puckett Road
Charlotte, North Carolina
H&H Job No. WIT-019
5030/
3550/
8260
8270
MADEP VPH
MADEP EPH
Analytical Method
8015M
8015M
Contaminant of Concern
CD
E
O
rn
E
O
N
O
O>
o
O
a
U
m
o
"
U
ccU
°"
00
U
U
Co
M
O U
L)
U
N
N
�? U
m
U E
W
0�
>
¢
o
¢
N
a
as
a
=,Q
=LQ
Date
Source
Sample
Incident
=
=
O
ul
w
w
Sample ID
Collected
Area
Depth (ft)
Phase
F
F
U
U
U
UST 1 Basin
03/02/20
UST
7
IA
NA
NA
BRL
BRL
BRL
BRL
BRL
<32
<32
<32
UST 1 Sidewall E
03/02/20
UST
5.5
IA
NA
NA
BRL
BRL
BRL
BRL
BRL
<33
<33
<33
UST 1 Sidewall N
03/02/20
UST
5.5
IA
NA
NA
BRL
BRL
BRL
BRL
BRL
<32
<32
<32
UST 1 Sidewall S
03/02/20
UST
5.5
IA
NA
NA
BRL
BRL
BRL
BRL
BRL
<32
<32
<32
UST 1 Sidewall W
03/02/20
UST
5.5
IA
NA
NA
BRL
BRL
BRL
BRL
BRL
<32
<32
<32
Stockpile-1
03/02/20
UST
NA
IA
<9.1
<9.0
BRL
BRL
BRL
BRL
BRL
NA
NA
NA
UST 2 Basin
03/02/20
UST
5
IA
NA
NA
BRL
BRL
BRL
BRL
BRL
<35
<35
<35
UST 2 Sidewall E
03/02/20
UST
4.5
IA
NA
NA
BRL
BRL
BRL
BRL
BRL
<32
<32
<32
UST 2 Sidewall N
03/02/20
UST
4.5
IA
NA
NA
BRL
BRL
BRL
BRL
BRL
160
49
64
UST 2 Sidewall N2
03/18/20
UST
5
IA
NA
NA
BRL
BRL
BRL
BRL
BRL
<1.6
<5.4
<8.8
UST 2 Sidewall S
03/02/20
UST
4.5
IA
NA
NA
BRL
BRL
BRL
BRL
BRL
<31
<31
<31
UST 2 Sidewall W
03/02/20
UST
UST
4.5
IA
NA
NA
BRL
BRL
BRL
BRL
BRL
<32
<32
<32
Stockpile-2
03/02/20
NA
IA
410
860
BRL
BRL
BRL
BRL
BRL
NA
NA
NA
Action Level (mg/kg)
50
100
Soil to Ground Water MSCC (mg/kg)
540
#
31
Residential MSCC (mg/kg)
1500
31000
469
VL
Industrial/Commercial MSCC (mg/kg)
40000
810000
12,264
Notes:
North Carolina Department of Environmental Quality (DEQ) Soil to Groundwater Maximum Soil Contaminant Concentrations (MSCCs)
DEQ Residential Cleanup MSCCs
DEQ Industrial/Commercial Cleanup MSCCs
Bold indicates concentration exceeds Soil to Groundwater MSCCs
UST = underground storage tank basin; EPH = Extractable Petroleum Hydrocarbon; NA = Not Analyzed/Not Applicable; '-- = Not Established
mg/kg = milligrams per kilograms; TPH = Total Petroleum Hydrocarbons; DRO = Diesel Range Organics; GRO = Gasoline Range Organics
BRL = below reporting limits; VOCs volatile organic compounds; SVOCs = semi -volatile organic compounds; # = health based level >100%
File: UST Soil Table, Table 1
Date: 4/24/2020

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' COUNTY GIS, 2020.
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SITE MAP
PROJECT PUCKETT/NASH ASSEMBLAGE
PUCKETT ROAD
CHARLOTTE, NORTH CAROLINA
2923 South Tryon Street -Suite 100
hart hickman Charlotte, North Carolina28203
w 704-586-0007(p) 704-586-0373(E)
SMARTER ENVIRONMENTAL SOLUTIONS License # C-1269 / #C-245 Geology
DATE: 1-28-20 REVISION NO. 0
JOB NO. WIT-019 FIGURE NO. 2

Appendix A
Fluid Disposal Manifest
19
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No. 09975
GENERATOR INFORMATION
Generator: Lan et, LLC and A O 'Phone:
Site Address: 10219. Packett Rd
City/State: C lharlck te'_ ('_ 29216 Contact: MI,;.,.,n
MATERIAL DESCRIPTION /QUANTITY 1 WEIGHT
Gross Weight (Ibs): Material: Product
Empty Weight (lbs): Contaminant: Eud,,.,(;J1, tHoatin fly,
Net Weight (Ibs):
Quantity ' Tons Drums Pails Sacs Yards Other:
TRANSPORTER- INFORMATION
Transporter: Evo CratioR Phone: [phone]
Truck #: r—
�. Contact: Tom* Dishe_
4
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
t� 1
Driver Signature: ! v 1 h Date:
FACILITY INFORMATION
x .s a
L.;703 Vargirave
Evo Project #: 02a007
Phone:
Contact:
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or Olspa*I in a man
,Der that has been authorized by the State of North Carolina.
1=acilit 5i nature: ' Date: '
White/Facility Canary/Invoice Pink/Carrier
Lvo Carporation, 2008

Appendix B
Tank Disposal Certificates
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

1 550 Gallons #2 Fuel Oil
Transporter: Eva Corporation
EC Project #: 032007
Disposal Certification:
Evo Corporation does hereby certify that the above named storage tank was
transported to Foss Recycling, 3459 Thomasville Road, Winston-Salem, NC for
proper disposal and recycling.

Tank Owner: LandNet, LLC and Assigns
Site Address: 10219 Puckett Road
Charlotte, NC
Description of Tanks:
Tank Size of Tank Contents
Number
i 550 Gallons #2 Fuel Oil
Transporter: Evo Corporation
EC Project #: 032008
Disposal Certification:
Evo Corporation does hereby certify that the above named storage tank was
transported to Foss Recycling, 3459 Thomasville Road, Winston-Salem, NC for
proper disposal and recycling.
/a
Signature

Appendix C
Certificate of Disposal and Non -Hazardous Waste Manifests
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

Iwo
CORPORATION
1703 Vargrave Street
Winston-Salem, NC 27107
ph 336-725-5844
fax [phone]
CERTIFICATE OF DISPOSAL
Evo Corporation does hereby certify that 8.31 tons of non -hazardous
contaminated material received on 10/19/2021 from:
Generator: Withrow Capital, Inc.
Originating at: 10109 Puckett Road
Charlotte, NC
EC Waste ID #: 102109
has been disposed of by Evo Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
C
Signature
Thomas W. Hammett
CEO
Eva Corporation
www.evocorp.net H NEX®i LEVEL

'CORPORATION
1703 Vargrave►:: -
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Lead # Manifest No. 7
��.. .. .-GENERATOR INFORMATION-
Site Address:
City/State, Contact: n
MATERIAL DESCRIPTION / QUANTITY / WEIGHT
Contaminant: Met -QV fleaumg UR
Orurns Fails Sacs Yards Other:
Transporter: Phone:
Tack : Contact:
As rr
..terials manifest are pro p "condition transport
applicablein commerce under the o
delivery to the facility designate.
r
Evo Project #-
....1703 Vargrave Street 336-725-5844
Phone:
Wnaton-Salem IC 27107 er
Contact:
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal In a manner that has beets authorized by the State of Forth Carolina.
Facility Signature:
Gate:-/l Cr / Z--&
ity
€MI Corpo"Ition,?008
Canary/Invoice

TICKET NUMBER
IL96521292440
A
CERTIFIED
AUTOMATED
TRUCK
SCALE
CAT SCALE COMPANY
P.O. BOX 630
WALCOTT IA 52T73
(877)22B-7225
www.catscale.com
THE CAT SCALE GUARANTEE
The CAT Scale Company guarantees that our scales will give an accurate weight. What makes
us different from other scale companies Is that we back up our guarantee with cash o
WEIGH WHAT WE SAY OR WE PAYe Iq
If you get an overweight fine from the state AFTER, one of our CAT Scales showed a legal weight, we will
immediately check our scale and we will:
(1) Reimburse you for the cost of the overweight fine if our scale is wrong, OR
(2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness it we
believe our scale was correct.
IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD PO THE FOLLOWING TO GETTHE PROBLEM RESOLVED:
1) Post bond and request a court date.
2) Cell CAT Scale Company direct 24 hours a day at 1-877-CATSCALE, ext. 7 (Toll Free) or visit www.catscaleguarantee.com
for instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn: Guarantee Department.
The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT
and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale.
5�8/0 -2 !O
DATE: 10-19-21 Z17 _339 STEER AXLE
DRIVE AXLE
09 : 26 SCALE: 1965
LOCATION: LOVES COUNTRY STORES TRAILER AY1F
PU UE WEIGHMASTEVS I 40 EXIT 154
CERTIFICATE OF STATE5V I LLE NC : GROSS WEIGHT
WCTERTA, UPAKIIIIr
r �
r :` i'IJBLIC i
4 :VMGHMASTER= J
t _ !
WEIGH NUMBER
2431
99C7C] 1 b
2014U 1 b
1. 738O 1 b
4--7420 1 b
This is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy welghmaster, and when properly signed and sealed shall be prima facla evidence of the
accuracy of the weight shown as prescribed by law.
LIVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED
COMPANY EVO
rr r • •y - 02121W -
FREIGHT ALL KINDS
TRACTOR #217, TRAILER k 339
FUULL$$ 1196521292431
(IF REWEIGH)
MEFI COPY 0CAT ScaWeReg W75521

r- 1vv
CORPORATION
1703 Vargrave Street
Winston-Salem, NC 27107
ph 336-725-5844
fax [phone]
CERTIFICATE OF DISPOSAL
Evo Corporation does hereby certify that 14.51 tons of non -hazardous
contaminated material received on 10/19/2021 from:
Generator: Withrow Capital, Inc.
Originating at: 10200 Puckett Road
Charlotte, NC
EC Waste ID #: 102108
has been disposed of by Evo Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
Signature
Thomas W. Hammett
CEO
Evo Corporation
www.evocorp.net NEXT L VE

Transporter: Phone:
Truck : 1L Ise, Contact:
As the transporter, I certify that the Materials described above being shipped under this non -hazardous
Materials Manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Evo Project M
i e 1 4 1 al C 1
I certify that the carrier has delivered the Materials described above to this facility, and I hereby adept this
Material for treatment and/car disposal in a manner that has been authorized by the State of North Carolina.
MMMINSIMM
tir
White/Facility
ink/Carrier

TICKET NUMDER
1196521292464
SCALE
CERTIFIED
AUTOMATED
TRUCK
SCALE
CAT SCALE COMPANY
P.O. BOX 630
WALCOTT, IA 52773
[phone]
www.catscale.com
THE CAT SCALE GUARANTEE
The CAT Scale Company guarantees that our scales will give an accurate weight. What makes
us different from other scale companies is that we back up our guarantee with cash.°
WEIGH WHAT WE SAY OR WE PAY®
If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will
Immediately check our scale and we will:
(1) Reimburse you for the cost of the overweight fine if our scale Is wrong, OR
(2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness V we
believe our scale was correct.
IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED:
1) Post bond and request a court date,
2) Call CAT Scale Company direct 24 hours a day at 1-B77-CATSCALE, exL 7 (Tall Free) or visit www.catscaleguarantee.com
for instructions.
3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to
CAT Scale Company Attn: Guarantee Department.
"The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT
and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale.
Sc8to2-1 d 9"
DATE: } 0-19-21 z17 3� � STEER AXLE
SANE AXLE
13:27 SCALE; 1965
L.00ATiON: LOVES COUNTRY STORES TRALM AXLE
PUBLIC WEICHMASTWS I 40 EXIT 154
CERTIFICATE OF
WEIGHT I! MEASURE
t CAO,
1
rLA3LiG #
# :WEJGHMASTER. #
1 �
_ !
WEIGH NUMBER
2431
STATESV I LLE NC t GROSS WEIGHT
c? E3 2 0 1 b
2fb0O0 1 b
24000 1 b
5C9020 1 b
This is to certify that the following described merchandise was weighed, counted, or measured by a
public or deputy welghmaster, and when property signed and sealed shell be prima facie evidence of the
accuracy of the weight shown as prescribed by law.
LIVESTOCK, PRODUCE, PROPERTY. COMMODITY, OR ARTICLE WEIGHED FREIGHT ALL KINDS
COMPANY O V O R 217 339
TRAILER #
WEIGHMASTER OR TICKET # FEE $3.00 WEIGHER SIGNATU_ - r FULL REWEIGH 1146521292431
` (IF REWEIGH)
ER COPY 0CAT scaW&Reg 3MM21

Appendix D
Laboratory Analytical Data and Chain -of -Custody
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

Case Narrative
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte)
Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: WIT-019
Lab Submittal Date: 03/03/2020
Work Order: 0030027
3/10/20 11:50
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
a,j
Angela D. Overcash
Senior Project Manager
Data Qualifiers Key Reference:
CCVH CCV result is above control limits but within method parameters. Result is considered estimated.
M Matrix spike outside of the control limits.
SM Surrogate is outside of the QC limits due to matrix.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Way� nt
poiAICAL
NALYT
Sample Receipt Summary
03/10/2020
Work Order: 0030027
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
UST-1 Basin
0030027-01
Solid
03/02/20
12:40
03/03/20
11:55
UST-1 Sidewall-N
0030027-02
Solid
03/02/20
12:50
03/03/20
11:55
UST-1 Sidewall-E
0030027-03
Solid
03/02/20
13:00
03/03/20
11:55
UST-1 Sidewall-S
0030027-04
Solid
03/02/20
13:05
03/03/20
11:55
UST-1 Sidewall-W
0030027-05
Solid
03/02/20
13:10
03/03/20
11:55
UST-2 Basin
0030027-06
Solid
03/02/20
14:10
03/03/20
11:55
UST-2 Sidewall-N
0030027-07
Solid
03/02/20
14:15
03/03/20
11:55
UST-2 Sidewall-E
0030027-08
Solid
03/02/20
14:20
03/03/20
11:55
UST-2 Sidewall-S
0030027-09
Solid
03/02/20
14:30
03/03/20
11:55
UST-2 Sidewall-W
0030027-10
Solid
03/02/20
14:30
03/03/20
11:55
Stockpile-1
0030027-11
Solid
03/02/20
15:00
03/03/20
11:55
Stockpile-2
0030027-12
Solid
03/02/20
14:45
03/03/20
11:55
Samples were received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Summary of Detections
WayPAoi
03/10/2
nt .
Work Order: 0030027
NALYTICAL
Waypoint ID
Client ID
Parameter
Method
Result Units
0030027-07
UST-2 Sidewall-N
C9-CI8 Aliphatics
'MADEP EPH
160 mg/kg dry
0030027-07
UST-2 Sidewall-N
C19-C36 Aliphatics
*MADEP EPH
49 mg/kg dry
0030027-07
UST-2 Sidewall-N
C11-C22 Aromatics
"MADEP EPH
64 mg/kg dry
0030027-12
Stockpile-2
Diesel Range Organics
`8015C
860 mg/kg dry
0030027-12
Stockpile-2
Gasoline Range Organics
`8015C
410 mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waynt.�
03/10/2020
PA
ANALYTICAL
Hart & Hickman (Charlotte)
Project: WIT-019
Client Sample ID: UST-1 Basin
Attn: Matt Ingalls
Sample ID: 0030027-01
2923 South Tryon St. Ste 100
Work
Order: 0030027
Charlotte, NC 28203
Sample Matrix: Solid
Time
Collected: 03/02/20 12:40
Time
Submitted: 03/03/20 11:55
Parameter
Result Units
Report
MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
BRL
mg/kg dry
32
1.6
1
*MADEP EPH 3/9/20 11:08
ZRC
P000104
C19-C36 Aliphatics
BRL
mg/kg dry
32
5.3
1
*MADEP EPH 3/9/20 11:08
ZRC
P000104
C11-C22Aromatics
BRL
mg/kg dry
32
8.6
1
*MADEP EPH 3/9/20 11:08
ZRC
P000104
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
55 %
40-140
o-Terphenyl
61 %
40-140
2-Fluorobiphenyl
75 %
40-140
2-Bromonaphthalene
88 %
40-140
General Chemistry Parameters
% Solids
78.4
% by
0.100
0.100
1
*SM2540 G 316120 8:56
EDV
P000098
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.84
0.15
1
*8270E 3/5/20 19:22
JMV
P000087
1,2-Dichlorobenzene
BRL
mg/kg dry
0.84
0.14
1
*8270E 3/5/20 19:22
JMV
P000087
1,3-Dichlorobenzene
BRL
mg/kg dry
0.84
0.12
1
*8270E 3/5/20 19:22
JMV
P000087
1,4-Dichlorobenzene
BRL
mg/kg dry
0.42
0.13
1
*8270E 3/5/20 19:22
JMV
P000087
1-Methyl naphthalene
BRL
mg/kg dry
0.84
0.013
1
*8270E 3/5/20 19:22
JMV
P000087
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.84
0.18
1
*8270E 3/5/20 19:22
JMV
P000087
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.84
0.20
1
*8270E 3/5/20 19:22
JMV
P000087
2,4-Dichlorophenol
BRL
mg/kg dry
0.84
0.16
1
*8270E 3/5/20 19:22
JMV
P000087
2,4-Dimethylphenol
BRL
mg/kg dry
0.42
0.17
1
*8270E 3/5/20 19:22
JMV
P000087
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.49
1
*8270E 3/5/20 19:22
JMV
P000087
2,4-Dinitrotoluene
BRL
mg/kg dry
0.84
0.22
1
*8270E 3/5/20 19:22
JMV
P000087
2,6-Dinitrotoluene
BRL
mg/kg dry
0.84
0.22
1
*8270E 3/5/20 19:22
JMV
P000087
2-Chloronaphthalene
BRL
mg/kg dry
0.84
0.21
1
*8270E 3/5/20 19:22
JMV
P000087
2-Chlorophenol
BRL
mg/kg dry
0.84
0.16
1
*8270E 3/5/20 19:22
JMV
P000087
2-Methyl naphthalene
BRL
mg/kg dry
0.84
0.016
1
*8270E 3/5/20 19:22
JMV
P000087
2-Methylphenol
BRL
mg/kg dry
0.84
0.16
1
*8270E 3/5/20 19:22
JMV
P000087
2-Nitrophenol
BRL
mg/kg dry
0.84
0.14
1
*8270E 3/5/20 19:22
JMV
P000087
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.84
0.17
1
*8270E 3/5/20 19:22
JMV
P000087
3/4-Methyl phenol
BRL
mg/kg dry
0.84
0.18
1
*8270E 3/5/20 19:22
JMV
P000087
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.46
1
*8270E 3/5/20 19:22
JMV
P000087
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.84
0.20
1
*8270E 3/5/20 19:22
JMV
P000087
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.84
0.16
1
*8270E 3/5/20 19:22
JMV
P000087
4-Chloroaniline
BRL
mg/kg dry
0.42
0.10
1
*8270E 3/5/20 19:22
JMV
P000087
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
*8270E 3/5/20 19:22
JMV
P000087
4-Nitrophenol
BRL
mg/kg dry
0.84
0.21
1
*8270E 3/5/20 19:22
JMV
P000087
Acenaphthene
BRL
mg/kg dry
0.84
0.019
1
*8270E 3/5/20 19:22
JMV
P000087
Acenaphthylene
BRL
mg/kg dry
0.84
0.017
1
*8270E 3/5/20 19:22
JMV
P000087
Anthracene
BRL
mg/kg dry
0.84
0.0093
1
*8270E 3/5/20 19:22
JMV
P000087
Azobenzene
BRL
mg/kg dry
0.84
0.18
1
*8270E 3/5/20 19:22
JMV
P000087
Benzo(a)anthracene
BRL
mg/kg dry
0.84
0.010
1
*8270E 3/5/20 19:22
JMV
P000087
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Basin
Attn: Matt Ingalls Sample ID: 0030027-01
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 12:40
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.84
0.0075
1
*8270E
3/5/20 19:22
JMV
P000087
Benzo(b)fluoranthene
BRL
mg/kg dry
0.84
0.0078
1
*8270E
3/5/20 19:22
JMV
P000087
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.84
0.0083
1
*8270E
3/5/20 19:22
JMV
P000087
Benzo(k)fluoranthene
BRL
mg/kg dry
0.84
0.0089
1
*8270E
3/5/20 19:22
JMV
P000087
Benzoic Acid
BRL
mg/kg dry
2.6
0.70
1
*8270E
3/5/20 19:22
JMV
P000087
Benzyl alcohol
BRL
mg/kg dry
0.84
0.16
1
*8270E
3/5/20 19:22
JMV
P000087
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.84
0.16
1
*8270E
3/5/20 19:22
JMV
P000087
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.84
0.14
1
*8270E
3/5/20 19:22
JMV
P000087
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.42
0.15
1
*8270E
3/5/20 19:22
JMV
P000087
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.84
0.19
1
*8270E
3/5/20 19:22
JMV
P000087
Butyl benzyl phthalate
BRL
mg/kg dry
0.42
0.15
1
*8270E
3/5/20 19:22
JMV
P000087
Chrysene
BRL
mg/kg dry
0.84
0.010
1
*8270E
3/5/20 19:22
JMV
P000087
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.84
0.024
1
*8270E
3/5/20 19:22
JMV
P000087
Dibenzofuran
BRL
mg/kg dry
0.84
0.23
1
*8270E
3/5/20 19:22
JMV
P000087
Diethyl phthalate
BRL
mg/kg dry
0.84
0.22
1
*8270E
3/5/20 19:22
JMV
P000087
Dimethyl phthalate
BRL
mg/kg dry
0.84
0.20
1
*8270E
3/5/20 19:22
JMV
P000087
Di-n-butyl phthalate
BRL
mg/kg dry
0.84
0.21
1
*8270E
3/5/20 19:22
JMV
P000087
Di-n-octyl phthalate
BRL
mg/kg dry
0.42
0.22
1
*8270E
3/5/20 19:22
JMV
P000087
Fluoranthene
BRL
mg/kg dry
0.84
0.0096
1
*8270E
3/5/20 19:22
JMV
P000087
Fluorene
BRL
mg/kg dry
0.84
0.015
1
*8270E
3/5/20 19:22
JMV
P000087
Hexachlorobenzene
BRL
mg/kg dry
0.84
0.18
1
*8270E
3/5/20 19:22
JMV
P000087
Hexachlorobutadiene
BRL
mg/kg dry
0.84
0.19
1
*8270E
3/5/20 19:22
JMV
P000087
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.84
0.29
1
*8270E
3/5/20 19:22
JMV
P000087
Hexachloroethane
BRL
mg/kg dry
0.84
0.13
1
*8270E
3/5/20 19:22
JMV
P000087
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.84
0.024
1
*8270E
3/5/20 19:22
JMV
P000087
Isophorone
BRL
mg/kg dry
0.84
0.18
1
*8270E
3/5/20 19:22
JMV
P000087
Naphthalene
BRL
mg/kg dry
0.84
0.018
1
*8270E
3/5/20 19:22
JMV
P000087
Nitrobenzene
BRL
mg/kg dry
0.42
0.18
1
*8270E
3/5/20 19:22
JMV
P000087
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.84
0.19
1
*8270E
3/5/20 19:22
JMV
P000087
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.84
0.23
1
*8270E
3/5/20 19:22
JMV
P000087
Pentachlorophenol
BRL
mg/kg dry
1.3
0.54
1
*8270E
3/5/20 19:22
JMV
P000087
Phenanthrene
BRL
mg/kg dry
0.84
0.0092
1
*8270E
3/5/20 19:22
JMV
P000087
Phenol
BRL
mg/kg dry
0.84
0.14
1
*8270E
3/5/20 19:22
JMV
P000087
Pyrene
BRL
mg/kg dry
0.84
0.012
1
*8270E
3/5/20 19:22
JMV
P000087
Pyridine
BRL
mg/kg dry
0.42
0.080
1
*8270E
3/5/20 19:22
JMV
P000087
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
74 %
39-132
2-Fluorobiphenyl
66 %
44-115
2-Fluorophenol
68 %
35-115
Nitrobenzene-d5
64 %
37-122
Phenol-d5
67 %
34-121
Terphenyl-d14
65 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Basin
Attn: Matt Ingalls Sample ID: 0030027-01
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 12:40
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0057
0.00069
1
*8260D
3/5/20 17:43
TLB
P000102
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0057
0.00084
1
*8260D
3/5/20 17:43
TLB
P000102
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0057
0.00041
1
*8260D
3/5/20 17:43
TLB
P000102
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0057
0.00061
1
*8260D
3/5/20 17:43
TLB
P000102
1,1-Dichloroethane
BRL
mg/kg dry
0.0057
0.0010
1
*8260D
3/5/20 17:43
TLB
P000102
1,1-Dichloroethylene
BRL
mg/kg dry
0.0057
0.0010
1
*8260D
3/5/20 17:43
TLB
P000102
1,1-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00088
1
*8260D
3/5/20 17:43
TLB
P000102
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00081
1
*8260D
3/5/20 17:43
TLB
P000102
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0057
0.00065
1
*8260D
3/5/20 17:43
TLB
P000102
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00054
1
*8260D
3/5/20 17:43
TLB
P000102
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0057
0.00060
1
*8260D
3/5/20 17:43
TLB
P000102
1,2-Dibromoethane
BRL
mg/kg dry
0.0057
0.00051
1
*8260D
3/5/20 17:43
TLB
P000102
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00063
1
*8260D
3/5/20 17:43
TLB
P000102
1,2-Dichloroethane
BRL
mg/kg dry
0.0057
0.00068
1
*8260D
3/5/20 17:43
TLB
P000102
1,2-Dichloropropane
BRL
mg/kg dry
0.0057
0.00086
1
*8260D
3/5/20 17:43
TLB
P000102
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0057
0.00071
1
*8260D
3/5/20 17:43
TLB
P000102
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00071
1
*8260D
3/5/20 17:43
TLB
P000102
1,3-Dichloropropane
BRL
mg/kg dry
0.0057
0.00048
1
*8260D
3/5/20 17:43
TLB
P000102
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0057
0.00072
1
*8260D
3/5/20 17:43
TLB
P000102
2,2-Dichloropropane
BRL
mg/kg dry
0.0057
0.00071
1
*8260D
3/5/20 17:43
TLB
P000102
2-Chlorotoluene
BRL
mg/kg dry
0.0057
0.00076
1
*8260D
3/5/20 17:43
TLB
P000102
4-Chlorotoluene
BRL
mg/kg dry
0.0057
0.00065
1
*8260D
3/5/20 17:43
TLB
P000102
4-Isopropyltoluene
BRL
mg/kg dry
0.0057
0.0014
1
*8260D
3/5/20 17:43
TLB
P000102
Acetone
BRL CCVH
mg/kg dry
0.023
0.0015
1
*8260D
3/5/20 17:43
TLB
P000102
Benzene
BRL
mg/kg dry
0.0057
0.00089
1
*8260D
3/5/20 17:43
TLB
P000102
Bromobenzene
BRL
mg/kg dry
0.0057
0.00079
1
*8260D
3/5/20 17:43
TLB
P000102
Bromochloromethane
BRL
mg/kg dry
0.0057
0.00093
1
*8260D
3/5/20 17:43
TLB
P000102
Bromodichloromethane
BRL
mg/kg dry
0.0057
0.00054
1
*8260D
3/5/20 17:43
TLB
P000102
Bromoform
BRL
mg/kg dry
0.0057
0.00044
1
*8260D
3/5/20 17:43
TLB
P000102
Bromomethane
BRL
mg/kg dry
0.011
0.0028
1
*8260D
3/5/20 17:43
TLB
P000102
Carbon Tetrachloride
BRL
mg/kg dry
0.0057
0.0011
1
*8260D
3/5/20 17:43
TLB
P000102
Chlorobenzene
BRL
mg/kg dry
0.0057
0.00089
1
*8260D
3/5/20 17:43
TLB
P000102
Chloroethane
BRL
mg/kg dry
0.011
0.0011
1
*8260D
3/5/20 17:43
TLB
P000102
Chloroform
BRL
mg/kg dry
0.0057
0.00070
1
*8260D
3/5/20 17:43
TLB
P000102
Chloromethane
BRL
mg/kg dry
0.011
0.0017
1
*8260D
3/5/20 17:43
TLB
P000102
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0057
0.00089
1
*8260D
3/5/20 17:43
TLB
P000102
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00056
1
*8260D
3/5/20 17:43
TLB
P000102
Dibromochloromethane
BRL
mg/kg dry
0.0057
0.00038
1
*8260D
3/5/20 17:43
TLB
P000102
Dichlorodifluoromethane
BRL
mg/kg dry
0.011
0.0016
1
*8260D
3/5/20 17:43
TLB
P000102
Ethylbenzene
BRL
mg/kg dry
0.0057
0.00086
1
*8260D
3/5/20 17:43
TLB
P000102
Isopropyl Ether
BRL
mg/kg dry
0.0057
0.00083
1
*8260D
3/5/20 17:43
TLB
P000102
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0057
0.00066
1
*8260D
3/5/20 17:43
TLB
P000102
m,p-Xylenes
BRL
mg/kg dry
0.011
0.0015
1
*8260D
3/5/20 17:43
TLB
P000102
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Basin
Attn: Matt Ingalls Sample ID: 0030027-01
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 12:40
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.023
0.00039
1
*8260D
3/5/20 17:43
TLB
P000102
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.023
0.0013
1
*8260D
3/5/20 17:43
TLB
P000102
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.023
0.00046
1
*8260D
3/5/20 17:43
TLB
P000102
Methylene Chloride
BRL
mg/kg dry
0.0057
0.00092
1
*8260D
3/5/20 17:43
TLB
P000102
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0057
0.00080
1
*8260D
3/5/20 17:43
TLB
P000102
Naphthalene
BRL
mg/kg dry
0.011
0.00057
1
*8260D
3/5/20 17:43
TLB
P000102
n-Butylbenzene
BRL
mg/kg dry
0.0057
0.00053
1
*8260D
3/5/20 17:43
TLB
P000102
n-Propylbenzene
BRL
mg/kg dry
0.0057
0.00082
1
*8260D
3/5/20 17:43
TLB
P000102
o-Xylene
BRL
mg/kg dry
0.0057
0.00061
1
*8260D
3/5/20 17:43
TLB
P000102
sec-Butylbenzene
BRL
mg/kg dry
0.0057
0.00061
1
*8260D
3/5/20 17:43
TLB
P000102
Styrene
BRL
mg/kg dry
0.0057
0.00055
1
*8260D
3/5/20 17:43
TLB
P000102
tert-Butylbenzene
BRL
mg/kg dry
0.0057
0.00068
1
*8260D
3/5/20 17:43
TLB
P000102
Tetrachloroethylene
BRL
mg/kg dry
0.0057
0.0010
1
*8260D
3/5/20 17:43
TLB
P000102
Toluene
BRL
mg/kg dry
0.0057
0.00091
1
*8260D
3/5/20 17:43
TLB
P000102
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0057
0.0011
1
*8260D
3/5/20 17:43
TLB
P000102
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0057
0.00049
1
*8260D
3/5/20 17:43
TLB
P000102
Trichloroethylene
BRL
mg/kg dry
0.0057
0.0011
1
*8260D
3/5/20 17:43
TLB
P000102
Trichlorofluoromethane
BRL
mg/kg dry
0.011
0.0015
1
*8260D
3/5/20 17:43
TLB
P000102
Vinyl acetate
BRL
mg/kg dry
0.011
0.00062
1
*8260D
3/5/20 17:43
TLB
P000102
Vinyl chloride
BRL
mg/kg dry
0.011
0.0011
1
*8260D
3/5/20 17:43
TLB
P000102
Xylenes, total
BRL
mg/kg dry
0.017
0.0020
1
*8260D
3/5/20 17:43
TLB
P000102
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99 %
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
92 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
25
5.0
100
*MADEP VPH
3/5/20 15:58
TBL
P000106
C9-C12 Aliphatics
BRL
mg/kg dry
25
2.2
100
*MADEP VPH
3/5/20 15:58
TBL
P000106
C9-Cl0 Aromatics
BRL
mg/kg dry
25
2.4
100
*MADEP VPH
3/5/20 15:58
TBL
P000106
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
113 %
70-130
2,5-Dibromotoluene (FID)
119 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waynt.�
03/10/2020
PA
ANALYTICAL
Hart & Hickman (Charlotte)
Project: WIT-019
Client Sample ID: UST-1 Sidewall-N
Attn: Matt Ingalls
Sample ID: 0030027-02
2923 South Tryon St. Ste 100
Work
Order: 0030027
Charlotte, NC 28203
Sample Matrix: Solid
Time
Collected: 03/02/20 12:50
Time
Submitted: 03/03/20 11:55
Parameter
Result Units
Report
MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
BRL
mg/kg dry
32
1.6
1
*MADEP EPH 3/7/20 2:07
ZRC
P000104
C19-C36 Aliphatics
BRL
mg/kg dry
32
5.4
1
*MADEP EPH 3/7/20 2:07
ZRC
P000104
C11-C22Aromatics
BRL
mg/kg dry
32
8.7
1
*MADEP EPH 3/7/20 2:07
ZRC
P000104
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
82 %
40-140
o-Terphenyl
79 %
40-140
2-Fluorobiphenyl
72 %
40-140
2-Bromonaphthalene
43 %
40-140
General Chemistry Parameters
% Solids
76.9
% by
0.100
0.100
1
*SM2540 G 316120 8:56
EDV
P000098
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.86
0.15
1
*8270E 3/5/20 19:44
JMV
P000087
1,2-Dichlorobenzene
BRL
mg/kg dry
0.86
0.14
1
*8270E 3/5/20 19:44
JMV
P000087
1,3-Dichlorobenzene
BRL
mg/kg dry
0.86
0.13
1
*8270E 3/5/20 19:44
JMV
P000087
1,4-Dichlorobenzene
BRL
mg/kg dry
0.43
0.14
1
*8270E 3/5/20 19:44
JMV
P000087
1-Methyl naphthalene
BRL
mg/kg dry
0.86
0.013
1
*8270E 3/5/20 19:44
JMV
P000087
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.86
0.18
1
*8270E 3/5/20 19:44
JMV
P000087
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.86
0.21
1
*8270E 3/5/20 19:44
JMV
P000087
2,4-Dichlorophenol
BRL
mg/kg dry
0.86
0.17
1
*8270E 3/5/20 19:44
JMV
P000087
2,4-Dimethylphenol
BRL
mg/kg dry
0.43
0.18
1
*8270E 3/5/20 19:44
JMV
P000087
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.50
1
*8270E 3/5/20 19:44
JMV
P000087
2,4-Dinitrotoluene
BRL
mg/kg dry
0.86
0.23
1
*8270E 3/5/20 19:44
JMV
P000087
2,6-Dinitrotoluene
BRL
mg/kg dry
0.86
0.22
1
*8270E 3/5/20 19:44
JMV
P000087
2-Chloronaphthalene
BRL
mg/kg dry
0.86
0.21
1
*8270E 3/5/20 19:44
JMV
P000087
2-Chlorophenol
BRL
mg/kg dry
0.86
0.16
1
*8270E 3/5/20 19:44
JMV
P000087
2-Methyl naphthalene
BRL
mg/kg dry
0.86
0.017
1
*8270E 3/5/20 19:44
JMV
P000087
2-Methylphenol
BRL
mg/kg dry
0.86
0.16
1
*8270E 3/5/20 19:44
JMV
P000087
2-Nitrophenol
BRL
mg/kg dry
0.86
0.14
1
*8270E 3/5/20 19:44
JMV
P000087
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.86
0.17
1
*8270E 3/5/20 19:44
JMV
P000087
3/4-Methyl phenol
BRL
mg/kg dry
0.86
0.19
1
*8270E 3/5/20 19:44
JMV
P000087
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.47
1
*8270E 3/5/20 19:44
JMV
P000087
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.86
0.20
1
*8270E 3/5/20 19:44
JMV
P000087
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.86
0.16
1
*8270E 3/5/20 19:44
JMV
P000087
4-Chloroaniline
BRL
mg/kg dry
0.43
0.10
1
*8270E 3/5/20 19:44
JMV
P000087
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
*8270E 3/5/20 19:44
JMV
P000087
4-Nitrophenol
BRL
mg/kg dry
0.86
0.21
1
*8270E 3/5/20 19:44
JMV
P000087
Acenaphthene
BRL
mg/kg dry
0.86
0.020
1
*8270E 3/5/20 19:44
JMV
P000087
Acenaphthylene
BRL
mg/kg dry
0.86
0.017
1
*8270E 3/5/20 19:44
JMV
P000087
Anthracene
BRL
mg/kg dry
0.86
0.0095
1
*8270E 3/5/20 19:44
JMV
P000087
Azobenzene
BRL
mg/kg dry
0.86
0.18
1
*8270E 3/5/20 19:44
JMV
P000087
Benzo(a)anthracene
BRL
mg/kg dry
0.86
0.010
1
*8270E 3/5/20 19:44
JMV
P000087
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-N
Attn: Matt Ingalls Sample ID: 0030027-02
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 12:50
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.86
0.0077
1
*8270E
3/5/20 19:44
JMV
P000087
Benzo(b)fluoranthene
BRL
mg/kg dry
0.86
0.0079
1
*8270E
3/5/20 19:44
JMV
P000087
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.86
0.0084
1
*8270E
3/5/20 19:44
JMV
P000087
Benzo(k)fluoranthene
BRL
mg/kg dry
0.86
0.0091
1
*8270E
3/5/20 19:44
JMV
P000087
Benzoic Acid
BRL
mg/kg dry
2.6
0.71
1
*8270E
3/5/20 19:44
JMV
P000087
Benzyl alcohol
BRL
mg/kg dry
0.86
0.16
1
*8270E
3/5/20 19:44
JMV
P000087
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.86
0.16
1
*8270E
3/5/20 19:44
JMV
P000087
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.86
0.14
1
*8270E
3/5/20 19:44
JMV
P000087
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 19:44
JMV
P000087
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.86
0.19
1
*8270E
3/5/20 19:44
JMV
P000087
Butyl benzyl phthalate
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 19:44
JMV
P000087
Chrysene
BRL
mg/kg dry
0.86
0.010
1
*8270E
3/5/20 19:44
JMV
P000087
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.86
0.025
1
*8270E
3/5/20 19:44
JMV
P000087
Dibenzofuran
BRL
mg/kg dry
0.86
0.23
1
*8270E
3/5/20 19:44
JMV
P000087
Diethyl phthalate
BRL
mg/kg dry
0.86
0.22
1
*8270E
3/5/20 19:44
JMV
P000087
Dimethyl phthalate
BRL
mg/kg dry
0.86
0.21
1
*8270E
3/5/20 19:44
JMV
P000087
Di-n-butyl phthalate
BRL
mg/kg dry
0.86
0.21
1
*8270E
3/5/20 19:44
JMV
P000087
Di-n-octyl phthalate
BRL
mg/kg dry
0.43
0.22
1
*8270E
3/5/20 19:44
JMV
P000087
Fluoranthene
BRL
mg/kg dry
0.86
0.0097
1
*8270E
3/5/20 19:44
JMV
P000087
Fluorene
BRL
mg/kg dry
0.86
0.015
1
*8270E
3/5/20 19:44
JMV
P000087
Hexachlorobenzene
BRL
mg/kg dry
0.86
0.19
1
*8270E
3/5/20 19:44
JMV
P000087
Hexachlorobutadiene
BRL
mg/kg dry
0.86
0.19
1
*8270E
3/5/20 19:44
JMV
P000087
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.86
0.30
1
*8270E
3/5/20 19:44
JMV
P000087
Hexachloroethane
BRL
mg/kg dry
0.86
0.14
1
*8270E
3/5/20 19:44
JMV
P000087
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.86
0.024
1
*8270E
3/5/20 19:44
JMV
P000087
Isophorone
BRL
mg/kg dry
0.86
0.18
1
*8270E
3/5/20 19:44
JMV
P000087
Naphthalene
BRL
mg/kg dry
0.86
0.018
1
*8270E
3/5/20 19:44
JMV
P000087
Nitrobenzene
BRL
mg/kg dry
0.43
0.18
1
*8270E
3/5/20 19:44
JMV
P000087
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.86
0.20
1
*8270E
3/5/20 19:44
JMV
P000087
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.86
0.24
1
*8270E
3/5/20 19:44
JMV
P000087
Pentachlorophenol
BRL
mg/kg dry
1.3
0.55
1
*8270E
3/5/20 19:44
JMV
P000087
Phenanthrene
BRL
mg/kg dry
0.86
0.0094
1
*8270E
3/5/20 19:44
JMV
P000087
Phenol
BRL
mg/kg dry
0.86
0.14
1
*8270E
3/5/20 19:44
JMV
P000087
Pyrene
BRL
mg/kg dry
0.86
0.012
1
*8270E
3/5/20 19:44
JMV
P000087
Pyridine
BRL
mg/kg dry
0.43
0.082
1
*8270E
3/5/20 19:44
JMV
P000087
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
79 %
39-132
2-Fluorobiphenyl
71 %
44-115
2-Fluorophenol
74 %
35-115
Nitrobenzene-d5
66 %
37-122
Phenol-d5
72 %
34-121
Terphenyl-d14
67 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-N
Attn: Matt Ingalls Sample ID: 0030027-02
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 12:50
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0092
0.0011
1
*8260D
3/5/20 11:40
TLB
P000102
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0092
0.0013
1
*8260D
3/5/20 11:40
TLB
P000102
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0092
0.00067
1
*8260D
3/5/20 11:40
TLB
P000102
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0092
0.00099
1
*8260D
3/5/20 11:40
TLB
P000102
1,1-Dichloroethane
BRL
mg/kg dry
0.0092
0.0017
1
*8260D
3/5/20 11:40
TLB
P000102
1,1-Dichloroethylene
BRL
mg/kg dry
0.0092
0.0017
1
*8260D
3/5/20 11:40
TLB
P000102
1,1-Dichloropropylene
BRL
mg/kg dry
0.0092
0.0014
1
*8260D
3/5/20 11:40
TLB
P000102
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.018
0.0013
1
*8260D
3/5/20 11:40
TLB
P000102
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0092
0.0010
1
*8260D
3/5/20 11:40
TLB
P000102
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.018
0.00088
1
*8260D
3/5/20 11:40
TLB
P000102
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0092
0.00097
1
*8260D
3/5/20 11:40
TLB
P000102
1,2-Dibromoethane
BRL
mg/kg dry
0.0092
0.00082
1
*8260D
3/5/20 11:40
TLB
P000102
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0092
0.0010
1
*8260D
3/5/20 11:40
TLB
P000102
1,2-Dichloroethane
BRL
mg/kg dry
0.0092
0.0011
1
*8260D
3/5/20 11:40
TLB
P000102
1,2-Dichloropropane
BRL
mg/kg dry
0.0092
0.0014
1
*8260D
3/5/20 11:40
TLB
P000102
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0092
0.0012
1
*8260D
3/5/20 11:40
TLB
P000102
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0092
0.0011
1
*8260D
3/5/20 11:40
TLB
P000102
1,3-Dichloropropane
BRL
mg/kg dry
0.0092
0.00077
1
*8260D
3/5/20 11:40
TLB
P000102
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0092
0.0012
1
*8260D
3/5/20 11:40
TLB
P000102
2,2-Dichloropropane
BRL
mg/kg dry
0.0092
0.0011
1
*8260D
3/5/20 11:40
TLB
P000102
2-Chlorotoluene
BRL
mg/kg dry
0.0092
0.0012
1
*8260D
3/5/20 11:40
TLB
P000102
4-Chlorotoluene
BRL
mg/kg dry
0.0092
0.0010
1
*8260D
3/5/20 11:40
TLB
P000102
4-Isopropyltoluene
BRL
mg/kg dry
0.0092
0.0023
1
*8260D
3/5/20 11:40
TLB
P000102
Acetone
BRL CCVH
mg/kg dry
0.037
0.0023
1
*8260D
3/5/20 11:40
TLB
P000102
Benzene
BRL
mg/kg dry
0.0092
0.0014
1
*8260D
3/5/20 11:40
TLB
P000102
Bromobenzene
BRL
mg/kg dry
0.0092
0.0013
1
*8260D
3/5/20 11:40
TLB
P000102
Bromochloromethane
BRL
mg/kg dry
0.0092
0.0015
1
*8260D
3/5/20 11:40
TLB
P000102
Bromodichloromethane
BRL
mg/kg dry
0.0092
0.00087
1
*8260D
3/5/20 11:40
TLB
P000102
Bromoform
BRL
mg/kg dry
0.0092
0.00071
1
*8260D
3/5/20 11:40
TLB
P000102
Bromomethane
BRL
mg/kg dry
0.018
0.0045
1
*8260D
3/5/20 11:40
TLB
P000102
Carbon Tetrachloride
BRL
mg/kg dry
0.0092
0.0018
1
*8260D
3/5/20 11:40
TLB
P000102
Chlorobenzene
BRL
mg/kg dry
0.0092
0.0014
1
*8260D
3/5/20 11:40
TLB
P000102
Chloroethane
BRL
mg/kg dry
0.018
0.0017
1
*8260D
3/5/20 11:40
TLB
P000102
Chloroform
BRL
mg/kg dry
0.0092
0.0011
1
*8260D
3/5/20 11:40
TLB
P000102
Chloromethane
BRL
mg/kg dry
0.018
0.0028
1
*8260D
3/5/20 11:40
TLB
P000102
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0092
0.0014
1
*8260D
3/5/20 11:40
TLB
P000102
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0092
0.00091
1
*8260D
3/5/20 11:40
TLB
P000102
Dibromochloromethane
BRL
mg/kg dry
0.0092
0.00061
1
*8260D
3/5/20 11:40
TLB
P000102
Dichlorodifluoromethane
BRL
mg/kg dry
0.018
0.0026
1
*8260D
3/5/20 11:40
TLB
P000102
Ethylbenzene
BRL
mg/kg dry
0.0092
0.0014
1
*8260D
3/5/20 11:40
TLB
P000102
Isopropyl Ether
BRL
mg/kg dry
0.0092
0.0013
1
*8260D
3/5/20 11:40
TLB
P000102
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0092
0.0011
1
*8260D
3/5/20 11:40
TLB
P000102
m,p-Xylenes
BRL
mg/kg dry
0.018
0.0023
1
*8260D
3/5/20 11:40
TLB
P000102
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-N
Attn: Matt Ingalls Sample ID: 0030027-02
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 12:50
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.037
0.00064
1
*8260D
3/5/20 11:40
TLB
P000102
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.037
0.0021
1
*8260D
3/5/20 11:40
TLB
P000102
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.037
0.00075
1
*8260D
3/5/20 11:40
TLB
P000102
Methylene Chloride
BRL
mg/kg dry
0.0092
0.0015
1
*8260D
3/5/20 11:40
TLB
P000102
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0092
0.0013
1
*8260D
3/5/20 11:40
TLB
P000102
Naphthalene
BRL
mg/kg dry
0.018
0.00093
1
*8260D
3/5/20 11:40
TLB
P000102
n-Butylbenzene
BRL
mg/kg dry
0.0092
0.00086
1
*8260D
3/5/20 11:40
TLB
P000102
n-Propylbenzene
BRL
mg/kg dry
0.0092
0.0013
1
*8260D
3/5/20 11:40
TLB
P000102
o-Xylene
BRL
mg/kg dry
0.0092
0.00098
1
*8260D
3/5/20 11:40
TLB
P000102
sec-Butylbenzene
BRL
mg/kg dry
0.0092
0.00099
1
*8260D
3/5/20 11:40
TLB
P000102
Styrene
BRL
mg/kg dry
0.0092
0.00089
1
*8260D
3/5/20 11:40
TLB
P000102
tert-Butylbenzene
BRL
mg/kg dry
0.0092
0.0011
1
*8260D
3/5/20 11:40
TLB
P000102
Tetrachloroethylene
BRL
mg/kg dry
0.0092
0.0017
1
*8260D
3/5/20 11:40
TLB
P000102
Toluene
BRL
mg/kg dry
0.0092
0.0015
1
*8260D
3/5/20 11:40
TLB
P000102
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0092
0.0018
1
*8260D
3/5/20 11:40
TLB
P000102
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0092
0.00079
1
*8260D
3/5/20 11:40
TLB
P000102
Trichloroethylene
BRL
mg/kg dry
0.0092
0.0018
1
*8260D
3/5/20 11:40
TLB
P000102
Trichlorofluoromethane
BRL
mg/kg dry
0.018
0.0025
1
*8260D
3/5/20 11:40
TLB
P000102
Vinyl acetate
BRL
mg/kg dry
0.018
0.00099
1
*8260D
3/5/20 11:40
TLB
P000102
Vinyl chloride
BRL
mg/kg dry
0.018
0.0018
1
*8260D
3/5/20 11:40
TLB
P000102
Xylenes, total
BRL
mg/kg dry
0.028
0.0033
1
*8260D
3/5/20 11:40
TLB
P000102
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
92 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
25
4.9
100
*MADEP VPH
3/5/20 16:27
TBL
P000106
C9-C12 Aliphatics
BRL
mg/kg dry
25
2.2
100
*MADEP VPH
3/5/20 16:27
TBL
P000106
C9-Cl0 Aromatics
BRL
mg/kg dry
25
2.3
100
*MADEP VPH
3/5/20 16:27
TBL
P000106
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
114 %
70-130
2,5-Dibromotoluene (FID)
121 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waynt.�
03/10/2020
PA
ANALYTICAL
Hart & Hickman (Charlotte)
Project: WIT-019
Client Sample ID: UST-1 Sidewall-E
Attn: Matt Ingalls
Sample ID: 0030027-03
2923 South Tryon St. Ste 100
Work
Order: 0030027
Charlotte, NC 28203
Sample Matrix: Solid
Time
Collected: 03/02/20 13:00
Time
Submitted: 03/03/20 11:55
Parameter
Result Units
Report
MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
BRL
mg/kg dry
33
1.6
1
*MADEP EPH 3/7/20 2:44
ZRC
P000104
C19-C36 Aliphatics
BRL
mg/kg dry
33
5.5
1
*MADEP EPH 3/7/20 2:44
ZRC
P000104
C11-C22Aromatics
BRL
mg/kg dry
33
8.9
1
*MADEP EPH 3/7/20 2:44
ZRC
P000104
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
83 %
40-140
o-Terphenyl
84 %
40-140
2-Fluorobiphenyl
70 %
40-140
2-Bromonaphthalene
53 %
40-140
General Chemistry Parameters
% Solids
76.3
% by
0.100
0.100
1
*SM2540 G 316120 8:56
EDV
P000098
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.87
0.15
1
*8270E 3/5/20 20:07
JMV
P000087
1,2-Dichlorobenzene
BRL
mg/kg dry
0.87
0.14
1
*8270E 3/5/20 20:07
JMV
P000087
1,3-Dichlorobenzene
BRL
mg/kg dry
0.87
0.13
1
*8270E 3/5/20 20:07
JMV
P000087
1,4-Dichlorobenzene
BRL
mg/kg dry
0.43
0.14
1
*8270E 3/5/20 20:07
JMV
P000087
1-Methyl naphthalene
BRL
mg/kg dry
0.87
0.013
1
*8270E 3/5/20 20:07
JMV
P000087
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.87
0.18
1
*8270E 3/5/20 20:07
JMV
P000087
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.87
0.21
1
*8270E 3/5/20 20:07
JMV
P000087
2,4-Dichlorophenol
BRL
mg/kg dry
0.87
0.17
1
*8270E 3/5/20 20:07
JMV
P000087
2,4-Dimethylphenol
BRL
mg/kg dry
0.43
0.18
1
*8270E 3/5/20 20:07
JMV
P000087
2,4-Dinitrophenol
BRL
mg/kg dry
2.0
0.51
1
*8270E 3/5/20 20:07
JMV
P000087
2,4-Dinitrotoluene
BRL
mg/kg dry
0.87
0.23
1
*8270E 3/5/20 20:07
JMV
P000087
2,6-Dinitrotoluene
BRL
mg/kg dry
0.87
0.22
1
*8270E 3/5/20 20:07
JMV
P000087
2-Chloronaphthalene
BRL
mg/kg dry
0.87
0.21
1
*8270E 3/5/20 20:07
JMV
P000087
2-Chlorophenol
BRL
mg/kg dry
0.87
0.17
1
*8270E 3/5/20 20:07
JMV
P000087
2-Methyl naphthalene
BRL
mg/kg dry
0.87
0.017
1
*8270E 3/5/20 20:07
JMV
P000087
2-Methylphenol
BRL
mg/kg dry
0.87
0.17
1
*8270E 3/5/20 20:07
JMV
P000087
2-Nitrophenol
BRL
mg/kg dry
0.87
0.14
1
*8270E 3/5/20 20:07
JMV
P000087
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.87
0.17
1
*8270E 3/5/20 20:07
JMV
P000087
3/4-Methyl phenol
BRL
mg/kg dry
0.87
0.19
1
*8270E 3/5/20 20:07
JMV
P000087
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.0
0.48
1
*8270E 3/5/20 20:07
JMV
P000087
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.87
0.20
1
*8270E 3/5/20 20:07
JMV
P000087
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.87
0.17
1
*8270E 3/5/20 20:07
JMV
P000087
4-Chloroaniline
BRL
mg/kg dry
0.43
0.10
1
*8270E 3/5/20 20:07
JMV
P000087
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
*8270E 3/5/20 20:07
JMV
P000087
4-Nitrophenol
BRL
mg/kg dry
0.87
0.21
1
*8270E 3/5/20 20:07
JMV
P000087
Acenaphthene
BRL
mg/kg dry
0.87
0.020
1
*8270E 3/5/20 20:07
JMV
P000087
Acenaphthylene
BRL
mg/kg dry
0.87
0.017
1
*8270E 3/5/20 20:07
JMV
P000087
Anthracene
BRL
mg/kg dry
0.87
0.0096
1
*8270E 3/5/20 20:07
JMV
P000087
Azobenzene
BRL
mg/kg dry
0.87
0.18
1
*8270E 3/5/20 20:07
JMV
P000087
Benzo(a)anthracene
BRL
mg/kg dry
0.87
0.010
1
*8270E 3/5/20 20:07
JMV
P000087
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-E
Attn: Matt Ingalls Sample ID: 0030027-03
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 13:00
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.87
0.0077
1
*8270E
3/5/20 20:07
JMV
P000087
Benzo(b)fluoranthene
BRL
mg/kg dry
0.87
0.0080
1
*8270E
3/5/20 20:07
JMV
P000087
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.87
0.0085
1
*8270E
3/5/20 20:07
JMV
P000087
Benzo(k)fluoranthene
BRL
mg/kg dry
0.87
0.0092
1
*8270E
3/5/20 20:07
JMV
P000087
Benzoic Acid
BRL
mg/kg dry
2.6
0.72
1
*8270E
3/5/20 20:07
JMV
P000087
Benzyl alcohol
BRL
mg/kg dry
0.87
0.16
1
*8270E
3/5/20 20:07
JMV
P000087
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.87
0.17
1
*8270E
3/5/20 20:07
JMV
P000087
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.87
0.14
1
*8270E
3/5/20 20:07
JMV
P000087
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 20:07
JMV
P000087
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.87
0.20
1
*8270E
3/5/20 20:07
JMV
P000087
Butyl benzyl phthalate
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 20:07
JMV
P000087
Chrysene
BRL
mg/kg dry
0.87
0.010
1
*8270E
3/5/20 20:07
JMV
P000087
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.87
0.025
1
*8270E
3/5/20 20:07
JMV
P000087
Dibenzofuran
BRL
mg/kg dry
0.87
0.23
1
*8270E
3/5/20 20:07
JMV
P000087
Diethyl phthalate
BRL
mg/kg dry
0.87
0.22
1
*8270E
3/5/20 20:07
JMV
P000087
Dimethyl phthalate
BRL
mg/kg dry
0.87
0.21
1
*8270E
3/5/20 20:07
JMV
P000087
Di-n-butyl phthalate
BRL
mg/kg dry
0.87
0.22
1
*8270E
3/5/20 20:07
JMV
P000087
Di-n-octyl phthalate
BRL
mg/kg dry
0.43
0.22
1
*8270E
3/5/20 20:07
JMV
P000087
Fluoranthene
BRL
mg/kg dry
0.87
0.0098
1
*8270E
3/5/20 20:07
JMV
P000087
Fluorene
BRL
mg/kg dry
0.87
0.015
1
*8270E
3/5/20 20:07
JMV
P000087
Hexachlorobenzene
BRL
mg/kg dry
0.87
0.19
1
*8270E
3/5/20 20:07
JMV
P000087
Hexachlorobutadiene
BRL
mg/kg dry
0.87
0.20
1
*8270E
3/5/20 20:07
JMV
P000087
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.87
0.30
1
*8270E
3/5/20 20:07
JMV
P000087
Hexachloroethane
BRL
mg/kg dry
0.87
0.14
1
*8270E
3/5/20 20:07
JMV
P000087
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.87
0.024
1
*8270E
3/5/20 20:07
JMV
P000087
Isophorone
BRL
mg/kg dry
0.87
0.19
1
*8270E
3/5/20 20:07
JMV
P000087
Naphthalene
BRL
mg/kg dry
0.87
0.018
1
*8270E
3/5/20 20:07
JMV
P000087
Nitrobenzene
BRL
mg/kg dry
0.43
0.18
1
*8270E
3/5/20 20:07
JMV
P000087
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.87
0.20
1
*8270E
3/5/20 20:07
JMV
P000087
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.87
0.24
1
*8270E
3/5/20 20:07
JMV
P000087
Pentachlorophenol
BRL
mg/kg dry
1.3
0.55
1
*8270E
3/5/20 20:07
JMV
P000087
Phenanthrene
BRL
mg/kg dry
0.87
0.0094
1
*8270E
3/5/20 20:07
JMV
P000087
Phenol
BRL
mg/kg dry
0.87
0.14
1
*8270E
3/5/20 20:07
JMV
P000087
Pyrene
BRL
mg/kg dry
0.87
0.013
1
*8270E
3/5/20 20:07
JMV
P000087
Pyridine
BRL
mg/kg dry
0.43
0.083
1
*8270E
3/5/20 20:07
JMV
P000087
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
79 %
39-132
2-Fluorobiphenyl
74 %
44-115
2-Fluorophenol
72 %
35-115
Nitrobenzene-d5
62 %
37-122
Phenol-d5
69 %
34-121
Terphenyl-d14
74 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-E
Attn: Matt Ingalls Sample ID: 0030027-03
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 13:00
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0064
0.00078
1
*8260D
3/5/20 12:10
TLB
P000102
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0064
0.00094
1
*8260D
3/5/20 12:10
TLB
P000102
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0064
0.00047
1
*8260D
3/5/20 12:10
TLB
P000102
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0064
0.00069
1
*8260D
3/5/20 12:10
TLB
P000102
1,1-Dichloroethane
BRL
mg/kg dry
0.0064
0.0012
1
*8260D
3/5/20 12:10
TLB
P000102
1,1-Dichloroethylene
BRL
mg/kg dry
0.0064
0.0012
1
*8260D
3/5/20 12:10
TLB
P000102
1,1-Dichloropropylene
BRL
mg/kg dry
0.0064
0.00099
1
*8260D
3/5/20 12:10
TLB
P000102
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00092
1
*8260D
3/5/20 12:10
TLB
P000102
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0064
0.00073
1
*8260D
3/5/20 12:10
TLB
P000102
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00061
1
*8260D
3/5/20 12:10
TLB
P000102
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0064
0.00068
1
*8260D
3/5/20 12:10
TLB
P000102
1,2-Dibromoethane
BRL
mg/kg dry
0.0064
0.00057
1
*8260D
3/5/20 12:10
TLB
P000102
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0064
0.00072
1
*8260D
3/5/20 12:10
TLB
P000102
1,2-Dichloroethane
BRL
mg/kg dry
0.0064
0.00076
1
*8260D
3/5/20 12:10
TLB
P000102
1,2-Dichloropropane
BRL
mg/kg dry
0.0064
0.00096
1
*8260D
3/5/20 12:10
TLB
P000102
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0064
0.00081
1
*8260D
3/5/20 12:10
TLB
P000102
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0064
0.00080
1
*8260D
3/5/20 12:10
TLB
P000102
1,3-Dichloropropane
BRL
mg/kg dry
0.0064
0.00054
1
*8260D
3/5/20 12:10
TLB
P000102
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0064
0.00081
1
*8260D
3/5/20 12:10
TLB
P000102
2,2-Dichloropropane
BRL
mg/kg dry
0.0064
0.00080
1
*8260D
3/5/20 12:10
TLB
P000102
2-Chlorotoluene
BRL
mg/kg dry
0.0064
0.00086
1
*8260D
3/5/20 12:10
TLB
P000102
4-Chlorotoluene
BRL
mg/kg dry
0.0064
0.00073
1
*8260D
3/5/20 12:10
TLB
P000102
4-Isopropyltoluene
BRL
mg/kg dry
0.0064
0.0016
1
*8260D
3/5/20 12:10
TLB
P000102
Acetone
BRL CCVH
mg/kg dry
0.026
0.0016
1
*8260D
3/5/20 12:10
TLB
P000102
Benzene
BRL
mg/kg dry
0.0064
0.0010
1
*8260D
3/5/20 12:10
TLB
P000102
Bromobenzene
BRL
mg/kg dry
0.0064
0.00089
1
*8260D
3/5/20 12:10
TLB
P000102
Bromochloromethane
BRL
mg/kg dry
0.0064
0.0011
1
*8260D
3/5/20 12:10
TLB
P000102
Bromodichloromethane
BRL
mg/kg dry
0.0064
0.00061
1
*8260D
3/5/20 12:10
TLB
P000102
Bromoform
BRL
mg/kg dry
0.0064
0.00050
1
*8260D
3/5/20 12:10
TLB
P000102
Bromomethane
BRL
mg/kg dry
0.013
0.0031
1
*8260D
3/5/20 12:10
TLB
P000102
Carbon Tetrachloride
BRL
mg/kg dry
0.0064
0.0013
1
*8260D
3/5/20 12:10
TLB
P000102
Chlorobenzene
BRL
mg/kg dry
0.0064
0.0010
1
*8260D
3/5/20 12:10
TLB
P000102
Chloroethane
BRL
mg/kg dry
0.013
0.0012
1
*8260D
3/5/20 12:10
TLB
P000102
Chloroform
BRL
mg/kg dry
0.0064
0.00079
1
*8260D
3/5/20 12:10
TLB
P000102
Chloromethane
BRL
mg/kg dry
0.013
0.0019
1
*8260D
3/5/20 12:10
TLB
P000102
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0064
0.0010
1
*8260D
3/5/20 12:10
TLB
P000102
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0064
0.00063
1
*8260D
3/5/20 12:10
TLB
P000102
Dibromochloromethane
BRL
mg/kg dry
0.0064
0.00043
1
*8260D
3/5/20 12:10
TLB
P000102
Dichlorodifluoromethane
BRL
mg/kg dry
0.013
0.0018
1
*8260D
3/5/20 12:10
TLB
P000102
Ethylbenzene
BRL
mg/kg dry
0.0064
0.00096
1
*8260D
3/5/20 12:10
TLB
P000102
Isopropyl Ether
BRL
mg/kg dry
0.0064
0.00094
1
*8260D
3/5/20 12:10
TLB
P000102
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0064
0.00075
1
*8260D
3/5/20 12:10
TLB
P000102
m,p-Xylenes
BRL
mg/kg dry
0.013
0.0016
1
*8260D
3/5/20 12:10
TLB
P000102
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-E
Attn: Matt Ingalls Sample ID: 0030027-03
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 13:00
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.026
0.00044
1
*8260D
3/5/20 12:10
TLB
P000102
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.026
0.0015
1
*8260D
3/5/20 12:10
TLB
P000102
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.026
0.00052
1
*8260D
3/5/20 12:10
TLB
P000102
Methylene Chloride
BRL
mg/kg dry
0.0064
0.0010
1
*8260D
3/5/20 12:10
TLB
P000102
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0064
0.00090
1
*8260D
3/5/20 12:10
TLB
P000102
Naphthalene
BRL
mg/kg dry
0.013
0.00065
1
*8260D
3/5/20 12:10
TLB
P000102
n-Butylbenzene
BRL
mg/kg dry
0.0064
0.00060
1
*8260D
3/5/20 12:10
TLB
P000102
n-Propylbenzene
BRL
mg/kg dry
0.0064
0.00093
1
*8260D
3/5/20 12:10
TLB
P000102
o-Xylene
BRL
mg/kg dry
0.0064
0.00068
1
*8260D
3/5/20 12:10
TLB
P000102
sec-Butylbenzene
BRL
mg/kg dry
0.0064
0.00069
1
*8260D
3/5/20 12:10
TLB
P000102
Styrene
BRL
mg/kg dry
0.0064
0.00062
1
*8260D
3/5/20 12:10
TLB
P000102
tert-Butylbenzene
BRL
mg/kg dry
0.0064
0.00076
1
*8260D
3/5/20 12:10
TLB
P000102
Tetrachloroethylene
BRL
mg/kg dry
0.0064
0.0012
1
*8260D
3/5/20 12:10
TLB
P000102
Toluene
BRL
mg/kg dry
0.0064
0.0010
1
*8260D
3/5/20 12:10
TLB
P000102
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0064
0.0012
1
*8260D
3/5/20 12:10
TLB
P000102
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0064
0.00055
1
*8260D
3/5/20 12:10
TLB
P000102
Trichloroethylene
BRL
mg/kg dry
0.0064
0.0012
1
*8260D
3/5/20 12:10
TLB
P000102
Trichlorofluoromethane
BRL
mg/kg dry
0.013
0.0017
1
*8260D
3/5/20 12:10
TLB
P000102
Vinyl acetate
BRL
mg/kg dry
0.013
0.00070
1
*8260D
3/5/20 12:10
TLB
P000102
Vinyl chloride
BRL
mg/kg dry
0.013
0.0013
1
*8260D
3/5/20 12:10
TLB
P000102
Xylenes, total
BRL
mg/kg dry
0.019
0.0023
1
*8260D
3/5/20 12:10
TLB
P000102
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
93 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
22
4.3
100
*MADEP VPH
3/5/20 16:56
TBL
P000106
C9-C12 Aliphatics
BRL
mg/kg dry
22
1.9
100
*MADEP VPH
3/5/20 16:56
TBL
P000106
C9-Cl0 Aromatics
BRL
mg/kg dry
22
2.1
100
*MADEP VPH
3/5/20 16:56
TBL
P000106
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
115 %
70-130
2,5-Dibromotoluene (FID)
121 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waynt.�
03/10/2020
PA
ANALYTICAL
Hart & Hickman (Charlotte)
Project: WIT-019
Client Sample ID: UST-1 Sidewall-S
Attn: Matt Ingalls
Sample ID: 0030027-04
2923 South Tryon St. Ste 100
Work
Order: 0030027
Charlotte, NC 28203
Sample Matrix: Solid
Time
Collected: 03/02/20 13:05
Time
Submitted: 03/03/20 11:55
Parameter
Result Units
Report
MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
BRL
mg/kg dry
32
1.6
1
*MADEP EPH 3/7/20 3:20
ZRC
P000104
C19-C36 Aliphatics
BRL
mg/kg dry
32
5.3
1
*MADEP EPH 3/7/20 3:20
ZRC
P000104
C11-C22Aromatics
BRL
mg/kg dry
32
8.6
1
*MADEP EPH 3/7/20 3:20
ZRC
P000104
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
71 %
40-140
o-Terphenyl
65 %
40-140
2-Fluorobiphenyl
71 %
40-140
2-Bromonaphthalene
65 %
40-140
General Chemistry Parameters
% Solids
78.9
% by
0.100
0.100
1
*SM2540 G 316120 8:56
EDV
P000098
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.84
0.15
1
*8270E 3/5/20 20:30
JMV
P000087
1,2-Dichlorobenzene
BRL
mg/kg dry
0.84
0.14
1
*8270E 3/5/20 20:30
JMV
P000087
1,3-Dichlorobenzene
BRL
mg/kg dry
0.84
0.12
1
*8270E 3/5/20 20:30
JMV
P000087
1,4-Dichlorobenzene
BRL
mg/kg dry
0.42
0.13
1
*8270E 3/5/20 20:30
JMV
P000087
1-Methyl naphthalene
BRL
mg/kg dry
0.84
0.013
1
*8270E 3/5/20 20:30
JMV
P000087
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.84
0.18
1
*8270E 3/5/20 20:30
JMV
P000087
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.84
0.20
1
*8270E 3/5/20 20:30
JMV
P000087
2,4-Dichlorophenol
BRL
mg/kg dry
0.84
0.16
1
*8270E 3/5/20 20:30
JMV
P000087
2,4-Dimethylphenol
BRL
mg/kg dry
0.42
0.17
1
*8270E 3/5/20 20:30
JMV
P000087
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.49
1
*8270E 3/5/20 20:30
JMV
P000087
2,4-Dinitrotoluene
BRL
mg/kg dry
0.84
0.22
1
*8270E 3/5/20 20:30
JMV
P000087
2,6-Dinitrotoluene
BRL
mg/kg dry
0.84
0.22
1
*8270E 3/5/20 20:30
JMV
P000087
2-Chloronaphthalene
BRL
mg/kg dry
0.84
0.20
1
*8270E 3/5/20 20:30
JMV
P000087
2-Chlorophenol
BRL
mg/kg dry
0.84
0.16
1
*8270E 3/5/20 20:30
JMV
P000087
2-Methyl naphthalene
BRL
mg/kg dry
0.84
0.016
1
*8270E 3/5/20 20:30
JMV
P000087
2-Methylphenol
BRL
mg/kg dry
0.84
0.16
1
*8270E 3/5/20 20:30
JMV
P000087
2-Nitrophenol
BRL
mg/kg dry
0.84
0.14
1
*8270E 3/5/20 20:30
JMV
P000087
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.84
0.17
1
*8270E 3/5/20 20:30
JMV
P000087
3/4-Methyl phenol
BRL
mg/kg dry
0.84
0.18
1
*8270E 3/5/20 20:30
JMV
P000087
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.46
1
*8270E 3/5/20 20:30
JMV
P000087
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.84
0.20
1
*8270E 3/5/20 20:30
JMV
P000087
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.84
0.16
1
*8270E 3/5/20 20:30
JMV
P000087
4-Chloroaniline
BRL
mg/kg dry
0.42
0.10
1
*8270E 3/5/20 20:30
JMV
P000087
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
*8270E 3/5/20 20:30
JMV
P000087
4-Nitrophenol
BRL
mg/kg dry
0.84
0.21
1
*8270E 3/5/20 20:30
JMV
P000087
Acenaphthene
BRL
mg/kg dry
0.84
0.019
1
*8270E 3/5/20 20:30
JMV
P000087
Acenaphthylene
BRL
mg/kg dry
0.84
0.016
1
*8270E 3/5/20 20:30
JMV
P000087
Anthracene
BRL
mg/kg dry
0.84
0.0092
1
*8270E 3/5/20 20:30
JMV
P000087
Azobenzene
BRL
mg/kg dry
0.84
0.18
1
*8270E 3/5/20 20:30
JMV
P000087
Benzo(a)anthracene
BRL
mg/kg dry
0.84
0.010
1
*8270E 3/5/20 20:30
JMV
P000087
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-S
Attn: Matt Ingalls Sample ID: 0030027-04
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 13:05
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.84
0.0075
1
*8270E
3/5/20 20:30
JMV
P000087
Benzo(b)fluoranthene
BRL
mg/kg dry
0.84
0.0077
1
*8270E
3/5/20 20:30
JMV
P000087
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.84
0.0082
1
*8270E
3/5/20 20:30
JMV
P000087
Benzo(k)fluoranthene
BRL
mg/kg dry
0.84
0.0089
1
*8270E
3/5/20 20:30
JMV
P000087
Benzoic Acid
BRL
mg/kg dry
2.5
0.69
1
*8270E
3/5/20 20:30
JMV
P000087
Benzyl alcohol
BRL
mg/kg dry
0.84
0.16
1
*8270E
3/5/20 20:30
JMV
P000087
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.84
0.16
1
*8270E
3/5/20 20:30
JMV
P000087
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.84
0.13
1
*8270E
3/5/20 20:30
JMV
P000087
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.42
0.15
1
*8270E
3/5/20 20:30
JMV
P000087
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.84
0.19
1
*8270E
3/5/20 20:30
JMV
P000087
Butyl benzyl phthalate
BRL
mg/kg dry
0.42
0.14
1
*8270E
3/5/20 20:30
JMV
P000087
Chrysene
BRL
mg/kg dry
0.84
0.0099
1
*8270E
3/5/20 20:30
JMV
P000087
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.84
0.024
1
*8270E
3/5/20 20:30
JMV
P000087
Dibenzofuran
BRL
mg/kg dry
0.84
0.23
1
*8270E
3/5/20 20:30
JMV
P000087
Diethyl phthalate
BRL
mg/kg dry
0.84
0.22
1
*8270E
3/5/20 20:30
JMV
P000087
Dimethyl phthalate
BRL
mg/kg dry
0.84
0.20
1
*8270E
3/5/20 20:30
JMV
P000087
Di-n-butyl phthalate
BRL
mg/kg dry
0.84
0.21
1
*8270E
3/5/20 20:30
JMV
P000087
Di-n-octyl phthalate
BRL
mg/kg dry
0.42
0.22
1
*8270E
3/5/20 20:30
JMV
P000087
Fluoranthene
BRL
mg/kg dry
0.84
0.0095
1
*8270E
3/5/20 20:30
JMV
P000087
Fluorene
BRL
mg/kg dry
0.84
0.014
1
*8270E
3/5/20 20:30
JMV
P000087
Hexachlorobenzene
BRL
mg/kg dry
0.84
0.18
1
*8270E
3/5/20 20:30
JMV
P000087
Hexachlorobutadiene
BRL
mg/kg dry
0.84
0.19
1
*8270E
3/5/20 20:30
JMV
P000087
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.84
0.29
1
*8270E
3/5/20 20:30
JMV
P000087
Hexachloroethane
BRL
mg/kg dry
0.84
0.13
1
*8270E
3/5/20 20:30
JMV
P000087
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.84
0.024
1
*8270E
3/5/20 20:30
JMV
P000087
Isophorone
BRL
mg/kg dry
0.84
0.18
1
*8270E
3/5/20 20:30
JMV
P000087
Naphthalene
BRL
mg/kg dry
0.84
0.018
1
*8270E
3/5/20 20:30
JMV
P000087
Nitrobenzene
BRL
mg/kg dry
0.42
0.18
1
*8270E
3/5/20 20:30
JMV
P000087
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.84
0.19
1
*8270E
3/5/20 20:30
JMV
P000087
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.84
0.23
1
*8270E
3/5/20 20:30
JMV
P000087
Pentachlorophenol
BRL
mg/kg dry
1.3
0.53
1
*8270E
3/5/20 20:30
JMV
P000087
Phenanthrene
BRL
mg/kg dry
0.84
0.0091
1
*8270E
3/5/20 20:30
JMV
P000087
Phenol
BRL
mg/kg dry
0.84
0.14
1
*8270E
3/5/20 20:30
JMV
P000087
Pyrene
BRL
mg/kg dry
0.84
0.012
1
*8270E
3/5/20 20:30
JMV
P000087
Pyridine
BRL
mg/kg dry
0.42
0.080
1
*8270E
3/5/20 20:30
JMV
P000087
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
69 %
39-132
2-Fluorobiphenyl
59 %
44-115
2-Fluorophenol
63 %
35-115
Nitrobenzene-d5
55 %
37-122
Phenol-d5
61 %
34-121
Terphenyl-d14
62 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-S
Attn: Matt Ingalls Sample ID: 0030027-04
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 13:05
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0065
0.00079
1
*8260D
3/5/20 12:40
TLB
P000102
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0065
0.00095
1
*8260D
3/5/20 12:40
TLB
P000102
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0065
0.00047
1
*8260D
3/5/20 12:40
TLB
P000102
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0065
0.00070
1
*8260D
3/5/20 12:40
TLB
P000102
1,1-Dichloroethane
BRL
mg/kg dry
0.0065
0.0012
1
*8260D
3/5/20 12:40
TLB
P000102
1,1-Dichloroethylene
BRL
mg/kg dry
0.0065
0.0012
1
*8260D
3/5/20 12:40
TLB
P000102
1,1-Dichloropropylene
BRL
mg/kg dry
0.0065
0.0010
1
*8260D
3/5/20 12:40
TLB
P000102
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00093
1
*8260D
3/5/20 12:40
TLB
P000102
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0065
0.00073
1
*8260D
3/5/20 12:40
TLB
P000102
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00062
1
*8260D
3/5/20 12:40
TLB
P000102
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0065
0.00069
1
*8260D
3/5/20 12:40
TLB
P000102
1,2-Dibromoethane
BRL
mg/kg dry
0.0065
0.00058
1
*8260D
3/5/20 12:40
TLB
P000102
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0065
0.00072
1
*8260D
3/5/20 12:40
TLB
P000102
1,2-Dichloroethane
BRL
mg/kg dry
0.0065
0.00077
1
*8260D
3/5/20 12:40
TLB
P000102
1,2-Dichloropropane
BRL
mg/kg dry
0.0065
0.00097
1
*8260D
3/5/20 12:40
TLB
P000102
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0065
0.00081
1
*8260D
3/5/20 12:40
TLB
P000102
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0065
0.00080
1
*8260D
3/5/20 12:40
TLB
P000102
1,3-Dichloropropane
BRL
mg/kg dry
0.0065
0.00054
1
*8260D
3/5/20 12:40
TLB
P000102
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0065
0.00082
1
*8260D
3/5/20 12:40
TLB
P000102
2,2-Dichloropropane
BRL
mg/kg dry
0.0065
0.00081
1
*8260D
3/5/20 12:40
TLB
P000102
2-Chlorotoluene
BRL
mg/kg dry
0.0065
0.00087
1
*8260D
3/5/20 12:40
TLB
P000102
4-Chlorotoluene
BRL
mg/kg dry
0.0065
0.00074
1
*8260D
3/5/20 12:40
TLB
P000102
4-Isopropyltoluene
BRL
mg/kg dry
0.0065
0.0016
1
*8260D
3/5/20 12:40
TLB
P000102
Acetone
BRL CCVH
mg/kg dry
0.026
0.0017
1
*8260D
3/5/20 12:40
TLB
P000102
Benzene
BRL
mg/kg dry
0.0065
0.0010
1
*8260D
3/5/20 12:40
TLB
P000102
Bromobenzene
BRL
mg/kg dry
0.0065
0.00090
1
*8260D
3/5/20 12:40
TLB
P000102
Bromochloromethane
BRL
mg/kg dry
0.0065
0.0011
1
*8260D
3/5/20 12:40
TLB
P000102
Bromodichloromethane
BRL
mg/kg dry
0.0065
0.00061
1
*8260D
3/5/20 12:40
TLB
P000102
Bromoform
BRL
mg/kg dry
0.0065
0.00050
1
*8260D
3/5/20 12:40
TLB
P000102
Bromomethane
BRL
mg/kg dry
0.013
0.0032
1
*8260D
3/5/20 12:40
TLB
P000102
Carbon Tetrachloride
BRL
mg/kg dry
0.0065
0.0013
1
*8260D
3/5/20 12:40
TLB
P000102
Chlorobenzene
BRL
mg/kg dry
0.0065
0.0010
1
*8260D
3/5/20 12:40
TLB
P000102
Chloroethane
BRL
mg/kg dry
0.013
0.0012
1
*8260D
3/5/20 12:40
TLB
P000102
Chloroform
BRL
mg/kg dry
0.0065
0.00079
1
*8260D
3/5/20 12:40
TLB
P000102
Chloromethane
BRL
mg/kg dry
0.013
0.0020
1
*8260D
3/5/20 12:40
TLB
P000102
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0065
0.0010
1
*8260D
3/5/20 12:40
TLB
P000102
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0065
0.00064
1
*8260D
3/5/20 12:40
TLB
P000102
Dibromochloromethane
BRL
mg/kg dry
0.0065
0.00043
1
*8260D
3/5/20 12:40
TLB
P000102
Dichlorodifluoromethane
BRL
mg/kg dry
0.013
0.0018
1
*8260D
3/5/20 12:40
TLB
P000102
Ethylbenzene
BRL
mg/kg dry
0.0065
0.00097
1
*8260D
3/5/20 12:40
TLB
P000102
Isopropyl Ether
BRL
mg/kg dry
0.0065
0.00095
1
*8260D
3/5/20 12:40
TLB
P000102
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0065
0.00075
1
*8260D
3/5/20 12:40
TLB
P000102
m,p-Xylenes
BRL
mg/kg dry
0.013
0.0017
1
*8260D
3/5/20 12:40
TLB
P000102
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-S
Attn: Matt Ingalls Sample ID: 0030027-04
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 13:05
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.026
0.00045
1
*8260D
3/5/20 12:40
TLB
P000102
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.026
0.0015
1
*8260D
3/5/20 12:40
TLB
P000102
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.026
0.00053
1
*8260D
3/5/20 12:40
TLB
P000102
Methylene Chloride
BRL
mg/kg dry
0.0065
0.0010
1
*8260D
3/5/20 12:40
TLB
P000102
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0065
0.00091
1
*8260D
3/5/20 12:40
TLB
P000102
Naphthalene
BRL
mg/kg dry
0.013
0.00065
1
*8260D
3/5/20 12:40
TLB
P000102
n-Butylbenzene
BRL
mg/kg dry
0.0065
0.00061
1
*8260D
3/5/20 12:40
TLB
P000102
n-Propylbenzene
BRL
mg/kg dry
0.0065
0.00094
1
*8260D
3/5/20 12:40
TLB
P000102
o-Xylene
BRL
mg/kg dry
0.0065
0.00069
1
*8260D
3/5/20 12:40
TLB
P000102
sec-Butylbenzene
BRL
mg/kg dry
0.0065
0.00070
1
*8260D
3/5/20 12:40
TLB
P000102
Styrene
BRL
mg/kg dry
0.0065
0.00063
1
*8260D
3/5/20 12:40
TLB
P000102
tert-Butylbenzene
BRL
mg/kg dry
0.0065
0.00077
1
*8260D
3/5/20 12:40
TLB
P000102
Tetrachloroethylene
BRL
mg/kg dry
0.0065
0.0012
1
*8260D
3/5/20 12:40
TLB
P000102
Toluene
BRL
mg/kg dry
0.0065
0.0010
1
*8260D
3/5/20 12:40
TLB
P000102
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0065
0.0012
1
*8260D
3/5/20 12:40
TLB
P000102
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0065
0.00055
1
*8260D
3/5/20 12:40
TLB
P000102
Trichloroethylene
BRL
mg/kg dry
0.0065
0.0013
1
*8260D
3/5/20 12:40
TLB
P000102
Trichlorofluoromethane
BRL
mg/kg dry
0.013
0.0017
1
*8260D
3/5/20 12:40
TLB
P000102
Vinyl acetate
BRL
mg/kg dry
0.013
0.00070
1
*8260D
3/5/20 12:40
TLB
P000102
Vinyl chloride
BRL
mg/kg dry
0.013
0.0013
1
*8260D
3/5/20 12:40
TLB
P000102
Xylenes, total
BRL
mg/kg dry
0.019
0.0023
1
*8260D
3/5/20 12:40
TLB
P000102
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
92 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
17
3.4
100
*MADEP VPH
3/5/20 17:26
TBL
P000106
C9-C12 Aliphatics
BRL
mg/kg dry
17
1.5
100
*MADEP VPH
3/5/20 17:26
TBL
P000106
C9-Cl0 Aromatics
BRL
mg/kg dry
17
1.6
100
*MADEP VPH
3/5/20 17:26
TBL
P000106
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
114 %
70-130
2,5-Dibromotoluene (FID)
121 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waynt.�
03/10/2020
PA
ANALYTICAL
Hart & Hickman (Charlotte)
Project: WIT-019
Client Sample ID: UST-1 Sidewall-W
Attn: Matt Ingalls
Sample ID: 0030027-05
2923 South Tryon St. Ste 100
Work
Order: 0030027
Charlotte, NC 28203
Sample Matrix: Solid
Time
Collected: 03/02/20 13:10
Time
Submitted: 03/03/20 11:55
Parameter
Result Units
Report
MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
BRL
mg/kg dry
32
1.6
1
*MADEP EPH 3/7/20 3:56
ZRC
P000104
C19-C36 Aliphatics
BRL
mg/kg dry
32
5.4
1
*MADEP EPH 3/7/20 3:56
ZRC
P000104
C11-C22Aromatics
BRL
mg/kg dry
32
8.7
1
*MADEP EPH 3/7/20 3:56
ZRC
P000104
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
77 %
40-140
o-Terphenyl
76 %
40-140
2-Fluorobiphenyl
71 %
40-140
2-Bromonaphthalene
47 %
40-140
General Chemistry Parameters
% Solids
78.1
% by
0.100
0.100
1
*SM2540 G 316120 8:56
EDV
P000098
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.85
0.15
1
*8270E 3/5/20 20:53
JMV
P000087
1,2-Dichlorobenzene
BRL
mg/kg dry
0.85
0.14
1
*8270E 3/5/20 20:53
JMV
P000087
1,3-Dichlorobenzene
BRL
mg/kg dry
0.85
0.12
1
*8270E 3/5/20 20:53
JMV
P000087
1,4-Dichlorobenzene
BRL
mg/kg dry
0.42
0.13
1
*8270E 3/5/20 20:53
JMV
P000087
1-Methyl naphthalene
BRL
mg/kg dry
0.85
0.013
1
*8270E 3/5/20 20:53
JMV
P000087
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.85
0.18
1
*8270E 3/5/20 20:53
JMV
P000087
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.85
0.20
1
*8270E 3/5/20 20:53
JMV
P000087
2,4-Dichlorophenol
BRL
mg/kg dry
0.85
0.17
1
*8270E 3/5/20 20:53
JMV
P000087
2,4-Dimethylphenol
BRL
mg/kg dry
0.42
0.18
1
*8270E 3/5/20 20:53
JMV
P000087
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.50
1
*8270E 3/5/20 20:53
JMV
P000087
2,4-Dinitrotoluene
BRL
mg/kg dry
0.85
0.22
1
*8270E 3/5/20 20:53
JMV
P000087
2,6-Dinitrotoluene
BRL
mg/kg dry
0.85
0.22
1
*8270E 3/5/20 20:53
JMV
P000087
2-Chloronaphthalene
BRL
mg/kg dry
0.85
0.21
1
*8270E 3/5/20 20:53
JMV
P000087
2-Chlorophenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/5/20 20:53
JMV
P000087
2-Methyl naphthalene
BRL
mg/kg dry
0.85
0.016
1
*8270E 3/5/20 20:53
JMV
P000087
2-Methylphenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/5/20 20:53
JMV
P000087
2-Nitrophenol
BRL
mg/kg dry
0.85
0.14
1
*8270E 3/5/20 20:53
JMV
P000087
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.85
0.17
1
*8270E 3/5/20 20:53
JMV
P000087
3/4-Methyl phenol
BRL
mg/kg dry
0.85
0.18
1
*8270E 3/5/20 20:53
JMV
P000087
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.47
1
*8270E 3/5/20 20:53
JMV
P000087
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.85
0.20
1
*8270E 3/5/20 20:53
JMV
P000087
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/5/20 20:53
JMV
P000087
4-Chloroaniline
BRL
mg/kg dry
0.42
0.10
1
*8270E 3/5/20 20:53
JMV
P000087
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
*8270E 3/5/20 20:53
JMV
P000087
4-Nitrophenol
BRL
mg/kg dry
0.85
0.21
1
*8270E 3/5/20 20:53
JMV
P000087
Acenaphthene
BRL
mg/kg dry
0.85
0.019
1
*8270E 3/5/20 20:53
JMV
P000087
Acenaphthylene
BRL
mg/kg dry
0.85
0.017
1
*8270E 3/5/20 20:53
JMV
P000087
Anthracene
BRL
mg/kg dry
0.85
0.0094
1
*8270E 3/5/20 20:53
JMV
P000087
Azobenzene
BRL
mg/kg dry
0.85
0.18
1
*8270E 3/5/20 20:53
JMV
P000087
Benzo(a)anthracene
BRL
mg/kg dry
0.85
0.010
1
*8270E 3/5/20 20:53
JMV
P000087
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-W
Attn: Matt Ingalls Sample ID: 0030027-05
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 13:10
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.85
0.0076
1
*8270E
3/5/20 20:53
JMV
P000087
Benzo(b)fluoranthene
BRL
mg/kg dry
0.85
0.0078
1
*8270E
3/5/20 20:53
JMV
P000087
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.85
0.0083
1
*8270E
3/5/20 20:53
JMV
P000087
Benzo(k)fluoranthene
BRL
mg/kg dry
0.85
0.0090
1
*8270E
3/5/20 20:53
JMV
P000087
Benzoic Acid
BRL
mg/kg dry
2.6
0.70
1
*8270E
3/5/20 20:53
JMV
P000087
Benzyl alcohol
BRL
mg/kg dry
0.85
0.16
1
*8270E
3/5/20 20:53
JMV
P000087
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.85
0.16
1
*8270E
3/5/20 20:53
JMV
P000087
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.85
0.14
1
*8270E
3/5/20 20:53
JMV
P000087
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.42
0.15
1
*8270E
3/5/20 20:53
JMV
P000087
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/5/20 20:53
JMV
P000087
Butyl benzyl phthalate
BRL
mg/kg dry
0.42
0.15
1
*8270E
3/5/20 20:53
JMV
P000087
Chrysene
BRL
mg/kg dry
0.85
0.010
1
*8270E
3/5/20 20:53
JMV
P000087
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.85
0.024
1
*8270E
3/5/20 20:53
JMV
P000087
Dibenzofuran
BRL
mg/kg dry
0.85
0.23
1
*8270E
3/5/20 20:53
JMV
P000087
Diethyl phthalate
BRL
mg/kg dry
0.85
0.22
1
*8270E
3/5/20 20:53
JMV
P000087
Dimethyl phthalate
BRL
mg/kg dry
0.85
0.20
1
*8270E
3/5/20 20:53
JMV
P000087
Di-n-butyl phthalate
BRL
mg/kg dry
0.85
0.21
1
*8270E
3/5/20 20:53
JMV
P000087
Di-n-octyl phthalate
BRL
mg/kg dry
0.42
0.22
1
*8270E
3/5/20 20:53
JMV
P000087
Fluoranthene
BRL
mg/kg dry
0.85
0.0096
1
*8270E
3/5/20 20:53
JMV
P000087
Fluorene
BRL
mg/kg dry
0.85
0.015
1
*8270E
3/5/20 20:53
JMV
P000087
Hexachlorobenzene
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/5/20 20:53
JMV
P000087
Hexachlorobutadiene
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/5/20 20:53
JMV
P000087
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.85
0.29
1
*8270E
3/5/20 20:53
JMV
P000087
Hexachloroethane
BRL
mg/kg dry
0.85
0.13
1
*8270E
3/5/20 20:53
JMV
P000087
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.85
0.024
1
*8270E
3/5/20 20:53
JMV
P000087
Isophorone
BRL
mg/kg dry
0.85
0.18
1
*8270E
3/5/20 20:53
JMV
P000087
Naphthalene
BRL
mg/kg dry
0.85
0.018
1
*8270E
3/5/20 20:53
JMV
P000087
Nitrobenzene
BRL
mg/kg dry
0.42
0.18
1
*8270E
3/5/20 20:53
JMV
P000087
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/5/20 20:53
JMV
P000087
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.85
0.23
1
*8270E
3/5/20 20:53
JMV
P000087
Pentachlorophenol
BRL
mg/kg dry
1.3
0.54
1
*8270E
3/5/20 20:53
JMV
P000087
Phenanthrene
BRL
mg/kg dry
0.85
0.0092
1
*8270E
3/5/20 20:53
JMV
P000087
Phenol
BRL
mg/kg dry
0.85
0.14
1
*8270E
3/5/20 20:53
JMV
P000087
Pyrene
BRL
mg/kg dry
0.85
0.012
1
*8270E
3/5/20 20:53
JMV
P000087
Pyridine
BRL
mg/kg dry
0.42
0.081
1
*8270E
3/5/20 20:53
JMV
P000087
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
84 %
39-132
2-Fluorobiphenyl
75 %
44-115
2-Fluorophenol
80 %
35-115
Nitrobenzene-d5
72 %
37-122
Phenol-d5
78 %
34-121
Terphenyl-d14
76 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-W
Attn: Matt Ingalls Sample ID: 0030027-05
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 13:10
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0079
0.00096
1
*8260D
3/5/20 13:10
TLB
P000102
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0079
0.0012
1
*8260D
3/5/20 13:10
TLB
P000102
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0079
0.00057
1
*8260D
3/5/20 13:10
TLB
P000102
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0079
0.00085
1
*8260D
3/5/20 13:10
TLB
P000102
1,1-Dichloroethane
BRL
mg/kg dry
0.0079
0.0014
1
*8260D
3/5/20 13:10
TLB
P000102
1,1-Dichloroethylene
BRL
mg/kg dry
0.0079
0.0014
1
*8260D
3/5/20 13:10
TLB
P000102
1,1-Dichloropropylene
BRL
mg/kg dry
0.0079
0.0012
1
*8260D
3/5/20 13:10
TLB
P000102
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.016
0.0011
1
*8260D
3/5/20 13:10
TLB
P000102
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0079
0.00089
1
*8260D
3/5/20 13:10
TLB
P000102
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.016
0.00075
1
*8260D
3/5/20 13:10
TLB
P000102
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0079
0.00083
1
*8260D
3/5/20 13:10
TLB
P000102
1,2-Dibromoethane
BRL
mg/kg dry
0.0079
0.00070
1
*8260D
3/5/20 13:10
TLB
P000102
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0079
0.00088
1
*8260D
3/5/20 13:10
TLB
P000102
1,2-Dichloroethane
BRL
mg/kg dry
0.0079
0.00094
1
*8260D
3/5/20 13:10
TLB
P000102
1,2-Dichloropropane
BRL
mg/kg dry
0.0079
0.0012
1
*8260D
3/5/20 13:10
TLB
P000102
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0079
0.00099
1
*8260D
3/5/20 13:10
TLB
P000102
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0079
0.00098
1
*8260D
3/5/20 13:10
TLB
P000102
1,3-Dichloropropane
BRL
mg/kg dry
0.0079
0.00066
1
*8260D
3/5/20 13:10
TLB
P000102
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0079
0.0010
1
*8260D
3/5/20 13:10
TLB
P000102
2,2-Dichloropropane
BRL
mg/kg dry
0.0079
0.00098
1
*8260D
3/5/20 13:10
TLB
P000102
2-Chlorotoluene
BRL
mg/kg dry
0.0079
0.0011
1
*8260D
3/5/20 13:10
TLB
P000102
4-Chlorotoluene
BRL
mg/kg dry
0.0079
0.00090
1
*8260D
3/5/20 13:10
TLB
P000102
4-Isopropyltoluene
BRL
mg/kg dry
0.0079
0.0020
1
*8260D
3/5/20 13:10
TLB
P000102
Acetone
BRL CCVH
mg/kg dry
0.031
0.0020
1
*8260D
3/5/20 13:10
TLB
P000102
Benzene
BRL
mg/kg dry
0.0079
0.0012
1
*8260D
3/5/20 13:10
TLB
P000102
Bromobenzene
BRL
mg/kg dry
0.0079
0.0011
1
*8260D
3/5/20 13:10
TLB
P000102
Bromochloromethane
BRL
mg/kg dry
0.0079
0.0013
1
*8260D
3/5/20 13:10
TLB
P000102
Bromodichloromethane
BRL
mg/kg dry
0.0079
0.00075
1
*8260D
3/5/20 13:10
TLB
P000102
Bromoform
BRL
mg/kg dry
0.0079
0.00061
1
*8260D
3/5/20 13:10
TLB
P000102
Bromomethane
BRL
mg/kg dry
0.016
0.0039
1
*8260D
3/5/20 13:10
TLB
P000102
Carbon Tetrachloride
BRL
mg/kg dry
0.0079
0.0015
1
*8260D
3/5/20 13:10
TLB
P000102
Chlorobenzene
BRL
mg/kg dry
0.0079
0.0012
1
*8260D
3/5/20 13:10
TLB
P000102
Chloroethane
BRL
mg/kg dry
0.016
0.0015
1
*8260D
3/5/20 13:10
TLB
P000102
Chloroform
BRL
mg/kg dry
0.0079
0.00096
1
*8260D
3/5/20 13:10
TLB
P000102
Chloromethane
BRL
mg/kg dry
0.016
0.0024
1
*8260D
3/5/20 13:10
TLB
P000102
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0079
0.0012
1
*8260D
3/5/20 13:10
TLB
P000102
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0079
0.00078
1
*8260D
3/5/20 13:10
TLB
P000102
Dibromochloromethane
BRL
mg/kg dry
0.0079
0.00053
1
*8260D
3/5/20 13:10
TLB
P000102
Dichlorodifluoromethane
BRL
mg/kg dry
0.016
0.0022
1
*8260D
3/5/20 13:10
TLB
P000102
Ethylbenzene
BRL
mg/kg dry
0.0079
0.0012
1
*8260D
3/5/20 13:10
TLB
P000102
Isopropyl Ether
BRL
mg/kg dry
0.0079
0.0012
1
*8260D
3/5/20 13:10
TLB
P000102
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0079
0.00092
1
*8260D
3/5/20 13:10
TLB
P000102
m,p-Xylenes
BRL
mg/kg dry
0.016
0.0020
1
*8260D
3/5/20 13:10
TLB
P000102
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-1 Sidewall-W
Attn: Matt Ingalls Sample ID: 0030027-05
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 13:10
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.031
0.00054
1
*8260D
3/5/20 13:10
TLB
P000102
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.031
0.0018
1
*8260D
3/5/20 13:10
TLB
P000102
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.031
0.00064
1
*8260D
3/5/20 13:10
TLB
P000102
Methylene Chloride
BRL
mg/kg dry
0.0079
0.0013
1
*8260D
3/5/20 13:10
TLB
P000102
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0079
0.0011
1
*8260D
3/5/20 13:10
TLB
P000102
Naphthalene
BRL
mg/kg dry
0.016
0.00079
1
*8260D
3/5/20 13:10
TLB
P000102
n-Butylbenzene
BRL
mg/kg dry
0.0079
0.00074
1
*8260D
3/5/20 13:10
TLB
P000102
n-Propylbenzene
BRL
mg/kg dry
0.0079
0.0011
1
*8260D
3/5/20 13:10
TLB
P000102
o-Xylene
BRL
mg/kg dry
0.0079
0.00084
1
*8260D
3/5/20 13:10
TLB
P000102
sec-Butylbenzene
BRL
mg/kg dry
0.0079
0.00085
1
*8260D
3/5/20 13:10
TLB
P000102
Styrene
BRL
mg/kg dry
0.0079
0.00076
1
*8260D
3/5/20 13:10
TLB
P000102
tert-Butylbenzene
BRL
mg/kg dry
0.0079
0.00093
1
*8260D
3/5/20 13:10
TLB
P000102
Tetrachloroethylene
BRL
mg/kg dry
0.0079
0.0014
1
*8260D
3/5/20 13:10
TLB
P000102
Toluene
BRL
mg/kg dry
0.0079
0.0013
1
*8260D
3/5/20 13:10
TLB
P000102
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0079
0.0015
1
*8260D
3/5/20 13:10
TLB
P000102
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0079
0.00067
1
*8260D
3/5/20 13:10
TLB
P000102
Trichloroethylene
BRL
mg/kg dry
0.0079
0.0015
1
*8260D
3/5/20 13:10
TLB
P000102
Trichlorofluoromethane
BRL
mg/kg dry
0.016
0.0021
1
*8260D
3/5/20 13:10
TLB
P000102
Vinyl acetate
BRL
mg/kg dry
0.016
0.00085
1
*8260D
3/5/20 13:10
TLB
P000102
Vinyl chloride
BRL
mg/kg dry
0.016
0.0016
1
*8260D
3/5/20 13:10
TLB
P000102
Xylenes, total
BRL
mg/kg dry
0.024
0.0028
1
*8260D
3/5/20 13:10
TLB
P000102
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
104 %
84-123
Toluene-d8
92 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
21
4.2
100
*MADEP VPH
3/5/20 17:55
TBL
P000106
C9-C12 Aliphatics
BRL
mg/kg dry
21
1.8
100
*MADEP VPH
3/5/20 17:55
TBL
P000106
C9-Cl0 Aromatics
BRL
mg/kg dry
21
2.0
100
*MADEP VPH
3/5/20 17:55
TBL
P000106
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
109 %
70-130
2,5-Dibromotoluene (FID)
116 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waynt.�
03/10/2020
PA
ANALYTICAL
Hart & Hickman (Charlotte)
Project: WIT-019
Client Sample ID: UST-2 Basin
Attn: Matt Ingalls
Sample ID: 0030027-06
2923 South Tryon St. Ste 100
Work
Order: 0030027
Charlotte, NC 28203
Sample Matrix: Solid
Time
Collected: 03/02/20 14:10
Time
Submitted: 03/03/20 11:55
Parameter
Result Units
Report
MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
BRL
mg/kg dry
35
1.7
1
*MADEP EPH 3/7/20 4:33
ZRC
P000104
C19-C36 Aliphatics
BRL
mg/kg dry
35
5.8
1
*MADEP EPH 3/7/20 4:33
ZRC
P000104
C11-C22Aromatics
BRL
mg/kg dry
35
9.4
1
*MADEP EPH 3/7/20 4:33
ZRC
P000104
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
76 %
40-140
o-Terphenyl
77 %
40-140
2-Fluorobiphenyl
73 %
40-140
2-Bromonaphthalene
59 %
40-140
General Chemistry Parameters
% Solids
71.4
% by
0.100
0.100
1
*SM2540 G 316120 8:56
EDV
P000098
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.93
0.16
1
*8270E 3/5/20 21:16
JMV
P000087
1,2-Dichlorobenzene
BRL
mg/kg dry
0.93
0.15
1
*8270E 3/5/20 21:16
JMV
P000087
1,3-Dichlorobenzene
BRL
mg/kg dry
0.93
0.14
1
*8270E 3/5/20 21:16
JMV
P000087
1,4-Dichlorobenzene
BRL
mg/kg dry
0.46
0.15
1
*8270E 3/5/20 21:16
JMV
P000087
1-Methyl naphthalene
BRL
mg/kg dry
0.93
0.014
1
*8270E 3/5/20 21:16
JMV
P000087
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.93
0.20
1
*8270E 3/5/20 21:16
JMV
P000087
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.93
0.22
1
*8270E 3/5/20 21:16
JMV
P000087
2,4-Dichlorophenol
BRL
mg/kg dry
0.93
0.18
1
*8270E 3/5/20 21:16
JMV
P000087
2,4-Dimethylphenol
BRL
mg/kg dry
0.46
0.19
1
*8270E 3/5/20 21:16
JMV
P000087
2,4-Dinitrophenol
BRL
mg/kg dry
2.1
0.54
1
*8270E 3/5/20 21:16
JMV
P000087
2,4-Dinitrotoluene
BRL
mg/kg dry
0.93
0.25
1
*8270E 3/5/20 21:16
JMV
P000087
2,6-Dinitrotoluene
BRL
mg/kg dry
0.93
0.24
1
*8270E 3/5/20 21:16
JMV
P000087
2-Chloronaphthalene
BRL
mg/kg dry
0.93
0.23
1
*8270E 3/5/20 21:16
JMV
P000087
2-Chlorophenol
BRL
mg/kg dry
0.93
0.18
1
*8270E 3/5/20 21:16
JMV
P000087
2-Methyl naphthalene
BRL
mg/kg dry
0.93
0.018
1
*8270E 3/5/20 21:16
JMV
P000087
2-Methylphenol
BRL
mg/kg dry
0.93
0.18
1
*8270E 3/5/20 21:16
JMV
P000087
2-Nitrophenol
BRL
mg/kg dry
0.93
0.15
1
*8270E 3/5/20 21:16
JMV
P000087
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.93
0.18
1
*8270E 3/5/20 21:16
JMV
P000087
3/4-Methyl phenol
BRL
mg/kg dry
0.93
0.20
1
*8270E 3/5/20 21:16
JMV
P000087
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.1
0.51
1
*8270E 3/5/20 21:16
JMV
P000087
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.93
0.22
1
*8270E 3/5/20 21:16
JMV
P000087
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.93
0.18
1
*8270E 3/5/20 21:16
JMV
P000087
4-Chloroaniline
BRL
mg/kg dry
0.46
0.11
1
*8270E 3/5/20 21:16
JMV
P000087
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.4
0.28
1
*8270E 3/5/20 21:16
JMV
P000087
4-Nitrophenol
BRL
mg/kg dry
0.93
0.23
1
*8270E 3/5/20 21:16
JMV
P000087
Acenaphthene
BRL
mg/kg dry
0.93
0.021
1
*8270E 3/5/20 21:16
JMV
P000087
Acenaphthylene
BRL
mg/kg dry
0.93
0.018
1
*8270E 3/5/20 21:16
JMV
P000087
Anthracene
BRL
mg/kg dry
0.93
0.010
1
*8270E 3/5/20 21:16
JMV
P000087
Azobenzene
BRL
mg/kg dry
0.93
0.20
1
*8270E 3/5/20 21:16
JMV
P000087
Benzo(a)anthracene
BRL
mg/kg dry
0.93
0.011
1
*8270E 3/5/20 21:16
JMV
P000087
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Basin
Attn: Matt Ingalls Sample ID: 0030027-06
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:10
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.93
0.0083
1
*8270E
3/5/20 21:16
JMV
P000087
Benzo(b)fluoranthene
BRL
mg/kg dry
0.93
0.0086
1
*8270E
3/5/20 21:16
JMV
P000087
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.93
0.0091
1
*8270E
3/5/20 21:16
JMV
P000087
Benzo(k)fluoranthene
BRL
mg/kg dry
0.93
0.0098
1
*8270E
3/5/20 21:16
JMV
P000087
Benzoic Acid
BRL
mg/kg dry
2.8
0.77
1
*8270E
3/5/20 21:16
JMV
P000087
Benzyl alcohol
BRL
mg/kg dry
0.93
0.17
1
*8270E
3/5/20 21:16
JMV
P000087
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.93
0.18
1
*8270E
3/5/20 21:16
JMV
P000087
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.93
0.15
1
*8270E
3/5/20 21:16
JMV
P000087
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.46
0.17
1
*8270E
3/5/20 21:16
JMV
P000087
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.93
0.21
1
*8270E
3/5/20 21:16
JMV
P000087
Butyl benzyl phthalate
BRL
mg/kg dry
0.46
0.16
1
*8270E
3/5/20 21:16
JMV
P000087
Chrysene
BRL
mg/kg dry
0.93
0.011
1
*8270E
3/5/20 21:16
JMV
P000087
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.93
0.027
1
*8270E
3/5/20 21:16
JMV
P000087
Dibenzofuran
BRL
mg/kg dry
0.93
0.25
1
*8270E
3/5/20 21:16
JMV
P000087
Diethyl phthalate
BRL
mg/kg dry
0.93
0.24
1
*8270E
3/5/20 21:16
JMV
P000087
Dimethyl phthalate
BRL
mg/kg dry
0.93
0.22
1
*8270E
3/5/20 21:16
JMV
P000087
Di-n-butyl phthalate
BRL
mg/kg dry
0.93
0.23
1
*8270E
3/5/20 21:16
JMV
P000087
Di-n-octyl phthalate
BRL
mg/kg dry
0.46
0.24
1
*8270E
3/5/20 21:16
JMV
P000087
Fluoranthene
BRL
mg/kg dry
0.93
0.011
1
*8270E
3/5/20 21:16
JMV
P000087
Fluorene
BRL
mg/kg dry
0.93
0.016
1
*8270E
3/5/20 21:16
JMV
P000087
Hexachlorobenzene
BRL
mg/kg dry
0.93
0.20
1
*8270E
3/5/20 21:16
JMV
P000087
Hexachlorobutadiene
BRL
mg/kg dry
0.93
0.21
1
*8270E
3/5/20 21:16
JMV
P000087
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.93
0.32
1
*8270E
3/5/20 21:16
JMV
P000087
Hexachloroethane
BRL
mg/kg dry
0.93
0.15
1
*8270E
3/5/20 21:16
JMV
P000087
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.93
0.026
1
*8270E
3/5/20 21:16
JMV
P000087
Isophorone
BRL
mg/kg dry
0.93
0.20
1
*8270E
3/5/20 21:16
JMV
P000087
Naphthalene
BRL
mg/kg dry
0.93
0.020
1
*8270E
3/5/20 21:16
JMV
P000087
Nitrobenzene
BRL
mg/kg dry
0.46
0.20
1
*8270E
3/5/20 21:16
JMV
P000087
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.93
0.21
1
*8270E
3/5/20 21:16
JMV
P000087
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.93
0.25
1
*8270E
3/5/20 21:16
JMV
P000087
Pentachlorophenol
BRL
mg/kg dry
1.4
0.59
1
*8270E
3/5/20 21:16
JMV
P000087
Phenanthrene
BRL
mg/kg dry
0.93
0.010
1
*8270E
3/5/20 21:16
JMV
P000087
Phenol
BRL
mg/kg dry
0.93
0.15
1
*8270E
3/5/20 21:16
JMV
P000087
Pyrene
BRL
mg/kg dry
0.93
0.013
1
*8270E
3/5/20 21:16
JMV
P000087
Pyridine
BRL
mg/kg dry
0.46
0.088
1
*8270E
3/5/20 21:16
JMV
P000087
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
74 %
39-132
2-Fluorobiphenyl
64 %
44-115
2-Fluorophenol
65 %
35-115
Nitrobenzene-d5
56 %
37-122
Phenol-d5
65 %
34-121
Terphenyl-d14
62 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Basin
Attn: Matt Ingalls Sample ID: 0030027-06
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:10
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0084
0.0010
1
*8260D
3/5/20 13:41
TLB
P000102
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0084
0.0012
1
*8260D
3/5/20 13:41
TLB
P000102
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0084
0.00061
1
*8260D
3/5/20 13:41
TLB
P000102
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0084
0.00090
1
*8260D
3/5/20 13:41
TLB
P000102
1,1-Dichloroethane
BRL
mg/kg dry
0.0084
0.0015
1
*8260D
3/5/20 13:41
TLB
P000102
1,1-Dichloroethylene
BRL
mg/kg dry
0.0084
0.0015
1
*8260D
3/5/20 13:41
TLB
P000102
1,1-Dichloropropylene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 13:41
TLB
P000102
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.017
0.0012
1
*8260D
3/5/20 13:41
TLB
P000102
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0084
0.00095
1
*8260D
3/5/20 13:41
TLB
P000102
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.017
0.00080
1
*8260D
3/5/20 13:41
TLB
P000102
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0084
0.00089
1
*8260D
3/5/20 13:41
TLB
P000102
1,2-Dibromoethane
BRL
mg/kg dry
0.0084
0.00075
1
*8260D
3/5/20 13:41
TLB
P000102
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0084
0.00093
1
*8260D
3/5/20 13:41
TLB
P000102
1,2-Dichloroethane
BRL
mg/kg dry
0.0084
0.00099
1
*8260D
3/5/20 13:41
TLB
P000102
1,2-Dichloropropane
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 13:41
TLB
P000102
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0084
0.0011
1
*8260D
3/5/20 13:41
TLB
P000102
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0084
0.0010
1
*8260D
3/5/20 13:41
TLB
P000102
1,3-Dichloropropane
BRL
mg/kg dry
0.0084
0.00070
1
*8260D
3/5/20 13:41
TLB
P000102
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0084
0.0011
1
*8260D
3/5/20 13:41
TLB
P000102
2,2-Dichloropropane
BRL
mg/kg dry
0.0084
0.0010
1
*8260D
3/5/20 13:41
TLB
P000102
2-Chlorotoluene
BRL
mg/kg dry
0.0084
0.0011
1
*8260D
3/5/20 13:41
TLB
P000102
4-Chlorotoluene
BRL
mg/kg dry
0.0084
0.00095
1
*8260D
3/5/20 13:41
TLB
P000102
4-Isopropyltoluene
BRL
mg/kg dry
0.0084
0.0021
1
*8260D
3/5/20 13:41
TLB
P000102
Acetone
BRL CCVH
mg/kg dry
0.033
0.0021
1
*8260D
3/5/20 13:41
TLB
P000102
Benzene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 13:41
TLB
P000102
Bromobenzene
BRL
mg/kg dry
0.0084
0.0012
1
*8260D
3/5/20 13:41
TLB
P000102
Bromochloromethane
BRL
mg/kg dry
0.0084
0.0014
1
*8260D
3/5/20 13:41
TLB
P000102
Bromodichloromethane
BRL
mg/kg dry
0.0084
0.00079
1
*8260D
3/5/20 13:41
TLB
P000102
Bromoform
BRL
mg/kg dry
0.0084
0.00065
1
*8260D
3/5/20 13:41
TLB
P000102
Bromomethane
BRL
mg/kg dry
0.017
0.0041
1
*8260D
3/5/20 13:41
TLB
P000102
Carbon Tetrachloride
BRL
mg/kg dry
0.0084
0.0016
1
*8260D
3/5/20 13:41
TLB
P000102
Chlorobenzene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 13:41
TLB
P000102
Chloroethane
BRL
mg/kg dry
0.017
0.0016
1
*8260D
3/5/20 13:41
TLB
P000102
Chloroform
BRL
mg/kg dry
0.0084
0.0010
1
*8260D
3/5/20 13:41
TLB
P000102
Chloromethane
BRL
mg/kg dry
0.017
0.0025
1
*8260D
3/5/20 13:41
TLB
P000102
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 13:41
TLB
P000102
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0084
0.00082
1
*8260D
3/5/20 13:41
TLB
P000102
Dibromochloromethane
BRL
mg/kg dry
0.0084
0.00056
1
*8260D
3/5/20 13:41
TLB
P000102
Dichlorodifluoromethane
BRL
mg/kg dry
0.017
0.0024
1
*8260D
3/5/20 13:41
TLB
P000102
Ethylbenzene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 13:41
TLB
P000102
Isopropyl Ether
BRL
mg/kg dry
0.0084
0.0012
1
*8260D
3/5/20 13:41
TLB
P000102
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0084
0.00097
1
*8260D
3/5/20 13:41
TLB
P000102
m,p-Xylenes
BRL
mg/kg dry
0.017
0.0021
1
*8260D
3/5/20 13:41
TLB
P000102
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Basin
Attn: Matt Ingalls Sample ID: 0030027-06
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:10
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.033
0.00058
1
*8260D
3/5/20 13:41
TLB
P000102
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.033
0.0020
1
*8260D
3/5/20 13:41
TLB
P000102
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.033
0.00068
1
*8260D
3/5/20 13:41
TLB
P000102
Methylene Chloride
BRL
mg/kg dry
0.0084
0.0014
1
*8260D
3/5/20 13:41
TLB
P000102
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0084
0.0012
1
*8260D
3/5/20 13:41
TLB
P000102
Naphthalene
BRL
mg/kg dry
0.017
0.00084
1
*8260D
3/5/20 13:41
TLB
P000102
n-Butylbenzene
BRL
mg/kg dry
0.0084
0.00078
1
*8260D
3/5/20 13:41
TLB
P000102
n-Propylbenzene
BRL
mg/kg dry
0.0084
0.0012
1
*8260D
3/5/20 13:41
TLB
P000102
o-Xylene
BRL
mg/kg dry
0.0084
0.00089
1
*8260D
3/5/20 13:41
TLB
P000102
sec-Butylbenzene
BRL
mg/kg dry
0.0084
0.00090
1
*8260D
3/5/20 13:41
TLB
P000102
Styrene
BRL
mg/kg dry
0.0084
0.00081
1
*8260D
3/5/20 13:41
TLB
P000102
tert-Butylbenzene
BRL
mg/kg dry
0.0084
0.00099
1
*8260D
3/5/20 13:41
TLB
P000102
Tetrachloroethylene
BRL
mg/kg dry
0.0084
0.0015
1
*8260D
3/5/20 13:41
TLB
P000102
Toluene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 13:41
TLB
P000102
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0084
0.0016
1
*8260D
3/5/20 13:41
TLB
P000102
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0084
0.00072
1
*8260D
3/5/20 13:41
TLB
P000102
Trichloroethylene
BRL
mg/kg dry
0.0084
0.0016
1
*8260D
3/5/20 13:41
TLB
P000102
Trichlorofluoromethane
BRL
mg/kg dry
0.017
0.0023
1
*8260D
3/5/20 13:41
TLB
P000102
Vinyl acetate
BRL
mg/kg dry
0.017
0.00091
1
*8260D
3/5/20 13:41
TLB
P000102
Vinyl chloride
BRL
mg/kg dry
0.017
0.0017
1
*8260D
3/5/20 13:41
TLB
P000102
Xylenes, total
BRL
mg/kg dry
0.025
0.0030
1
*8260D
3/5/20 13:41
TLB
P000102
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
92 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
21
4.2
100
*MADEP VPH
3/5/20 18:24
TBL
P000106
C9-C12 Aliphatics
BRL
mg/kg dry
21
1.9
100
*MADEP VPH
3/5/20 18:24
TBL
P000106
C9-Cl0 Aromatics
BRL
mg/kg dry
21
2.0
100
*MADEP VPH
3/5/20 18:24
TBL
P000106
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
109 %
70-130
2,5-Dibromotoluene (FID)
115 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waynt.�
03/10/2020
PA
ANALYTICAL
Hart & Hickman (Charlotte)
Project: WIT-019
Client Sample ID: UST-2 Sidewall-N
Attn: Matt Ingalls
Sample ID: 0030027-07
2923 South Tryon St. Ste 100
Work Order: 0030027
Charlotte, NC 28203
Sample Matrix: Solid
Time Collected: 03/02/20 14:15
Time Submitted: 03/03/20 11:55
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
160 mg/kg dry
32 1.6
1 *MADEP EPH 3/7/20 5:09 ZRC P000104
C19-C36 Aliphatics
49 mg/kg dry
32 5.5
1 *MADEP EPH 317/20 5:09 ZRC P000104
C11-C22 Aromatics
64 mg/kg dry
32 8.8
1 'MADEP EPH 3/7120 5:09 ZRC P000104
Surrogate
Recovery Control Limits
1-Chlorooctadecane
75 % 40-140
o-Terphenyl
67 % 40-140
2-Fluorobiphenyl
71 % 40-140
2-Bromonaphthalene
69 % 40-140
General Chemistry Parameters
% Solids
76.4
% by
0.100
0.100
1
*SM2540 G
3/6120 9:04
EDV
P000110
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.86
0.15
1
*8270E
3/5/20 21:38
JMV
P000087
1,2-Dichlorobenzene
BRL
mg/kg dry
0.86
0.14
1
*8270E
3/5/20 21:38
JMV
P000087
1,3-Dichlorobenzene
BRL
mg/kg dry
0.86
0.13
1
*8270E
3/5/20 21:38
JMV
P000087
1,4-Dichlorobenzene
BRL
mg/kg dry
0.43
0.14
1
*8270E
3/5/20 21:38
JMV
P000087
1-Methyl naphthalene
BRL
mg/kg dry
0.86
0.013
1
*8270E
3/5/20 21:38
JMV
P000087
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.86
0.18
1
*8270E
3/5/20 21:38
JMV
P000087
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.86
0.21
1
*8270E
3/5/20 21:38
JMV
P000087
2,4-Dichlorophenol
BRL
mg/kg dry
0.86
0.17
1
*8270E
3/5/20 21:38
JMV
P000087
2,4-Dimethyl phenol
BRL
mg/kg dry
0.43
0.18
1
*8270E
3/5/20 21:38
JMV
P000087
2,4-Dinitrophenol
BRL
mg/kg dry
2.0
0.51
1
*8270E
3/5/20 21:38
JMV
P000087
2,4-Dinitrotoluene
BRL
mg/kg dry
0.86
0.23
1
*8270E
3/5/20 21:38
JMV
P000087
2,6-Dinitrotoluene
BRL
mg/kg dry
0.86
0.22
1
*8270E
3/5/20 21:38
JMV
P000087
2-Chloronaphthalene
BRL
mg/kg dry
0.86
0.21
1
*8270E
3/5/20 21:38
JMV
P000087
2-Chlorophenol
BRL
mg/kg dry
0.86
0.16
1
*8270E
3/5/20 21:38
JMV
P000087
2-Methyl naphthalene
BRL
mg/kg dry
0.86
0.017
1
*8270E
3/5/20 21:38
JMV
P000087
2-Methylphenol
BRL
mg/kg dry
0.86
0.16
1
*8270E
3/5/20 21:38
JMV
P000087
2-Nitrophenol
BRL
mg/kg dry
0.86
0.14
1
*8270E
3/5/20 21:38
JMV
P000087
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.86
0.17
1
*8270E
3/5/20 21:38
JMV
P000087
3/4-Methyl phenol
BRL
mg/kg dry
0.86
0.19
1
*8270E
3/5/20 21:38
JMV
P000087
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
2.0
0.48
1
*8270E
3/5/20 21:38
JMV
P000087
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.86
0.20
1
*8270E
3/5/20 21:38
JMV
P000087
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.86
0.16
1
*8270E
3/5/20 21:38
JMV
P000087
4-Chloroaniline
BRL
mg/kg dry
0.43
0.10
1
*8270E
3/5/20 21:38
JMV
P000087
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
*8270E
3/5/20 21:38
JMV
P000087
4-Nitrophenol
BRL
mg/kg dry
0.86
0.21
1
*8270E
3/5/20 21:38
JMV
P000087
Acenaphthene
BRL
mg/kg dry
0.86
0.020
1
*8270E
3/5/20 21:38
JMV
P000087
Acenaphthylene
BRL
mg/kg dry
0.86
0.017
1
*8270E
3/5/20 21:38
JMV
P000087
Anthracene
BRL
mg/kg dry
0.86
0.0095
1
*8270E
3/5/20 21:38
JMV
P000087
Azobenzene
BRL
mg/kg dry
0.86
0.18
1
*8270E
3/5/20 21:38
JMV
P000087
Benzo(a)anthracene
BRL
mg/kg dry
0.86
0.010
1
*8270E
3/5/20 21:38
JMV
P000087
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-N
Attn: Matt Ingalls Sample ID: 0030027-07
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:15
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.86
0.0077
1
*8270E
3/5/20 21:38
JMV
P000087
Benzo(b)fluoranthene
BRL
mg/kg dry
0.86
0.0080
1
*8270E
3/5/20 21:38
JMV
P000087
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.86
0.0085
1
*8270E
3/5/20 21:38
JMV
P000087
Benzo(k)fluoranthene
BRL
mg/kg dry
0.86
0.0092
1
*8270E
3/5/20 21:38
JMV
P000087
Benzoic Acid
BRL
mg/kg dry
2.6
0.72
1
*8270E
3/5/20 21:38
JMV
P000087
Benzyl alcohol
BRL
mg/kg dry
0.86
0.16
1
*8270E
3/5/20 21:38
JMV
P000087
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.86
0.16
1
*8270E
3/5/20 21:38
JMV
P000087
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.86
0.14
1
*8270E
3/5/20 21:38
JMV
P000087
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 21:38
JMV
P000087
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.86
0.19
1
*8270E
3/5/20 21:38
JMV
P000087
Butyl benzyl phthalate
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 21:38
JMV
P000087
Chrysene
BRL
mg/kg dry
0.86
0.010
1
*8270E
3/5/20 21:38
JMV
P000087
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.86
0.025
1
*8270E
3/5/20 21:38
JMV
P000087
Dibenzofuran
BRL
mg/kg dry
0.86
0.23
1
*8270E
3/5/20 21:38
JMV
P000087
Diethyl phthalate
BRL
mg/kg dry
0.86
0.22
1
*8270E
3/5/20 21:38
JMV
P000087
Dimethyl phthalate
BRL
mg/kg dry
0.86
0.21
1
*8270E
3/5/20 21:38
JMV
P000087
Di-n-butyl phthalate
BRL
mg/kg dry
0.86
0.21
1
*8270E
3/5/20 21:38
JMV
P000087
Di-n-octyl phthalate
BRL
mg/kg dry
0.43
0.22
1
*8270E
3/5/20 21:38
JMV
P000087
Fluoranthene
BRL
mg/kg dry
0.86
0.0098
1
*8270E
3/5/20 21:38
JMV
P000087
Fluorene
BRL
mg/kg dry
0.86
0.015
1
*8270E
3/5/20 21:38
JMV
P000087
Hexachlorobenzene
BRL
mg/kg dry
0.86
0.19
1
*8270E
3/5/20 21:38
JMV
P000087
Hexachlorobutadiene
BRL
mg/kg dry
0.86
0.19
1
*8270E
3/5/20 21:38
JMV
P000087
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.86
0.30
1
*8270E
3/5/20 21:38
JMV
P000087
Hexachloroethane
BRL
mg/kg dry
0.86
0.14
1
*8270E
3/5/20 21:38
JMV
P000087
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.86
0.024
1
*8270E
3/5/20 21:38
JMV
P000087
Isophorone
BRL
mg/kg dry
0.86
0.19
1
*8270E
3/5/20 21:38
JMV
P000087
Naphthalene
BRL
mg/kg dry
0.86
0.018
1
*8270E
3/5/20 21:38
JMV
P000087
Nitrobenzene
BRL
mg/kg dry
0.43
0.18
1
*8270E
3/5/20 21:38
JMV
P000087
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.86
0.20
1
*8270E
3/5/20 21:38
JMV
P000087
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.86
0.24
1
*8270E
3/5/20 21:38
JMV
P000087
Pentachlorophenol
BRL
mg/kg dry
1.3
0.55
1
*8270E
3/5/20 21:38
JMV
P000087
Phenanthrene
BRL
mg/kg dry
0.86
0.0094
1
*8270E
3/5/20 21:38
JMV
P000087
Phenol
BRL
mg/kg dry
0.86
0.14
1
*8270E
3/5/20 21:38
JMV
P000087
Pyrene
BRL
mg/kg dry
0.86
0.013
1
*8270E
3/5/20 21:38
JMV
P000087
Pyridine
BRL
mg/kg dry
0.43
0.082
1
*8270E
3/5/20 21:38
JMV
P000087
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
75 %
39-132
2-Fluorobiphenyl
67 %
44-115
2-Fluorophenol
71 %
35-115
Nitrobenzene-d5
64 %
37-122
Phenol-d5
68 %
34-121
Terphenyl-d14
77 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-N
Attn: Matt Ingalls Sample ID: 0030027-07
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:15
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0064
0.00079
1
*8260D
3/5/20 14:11
TLB
P000102
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0064
0.00095
1
*8260D
3/5/20 14:11
TLB
P000102
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0064
0.00047
1
*8260D
3/5/20 14:11
TLB
P000102
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0064
0.00070
1
*8260D
3/5/20 14:11
TLB
P000102
1,1-Dichloroethane
BRL
mg/kg dry
0.0064
0.0012
1
*8260D
3/5/20 14:11
TLB
P000102
1,1-Dichloroethylene
BRL
mg/kg dry
0.0064
0.0012
1
*8260D
3/5/20 14:11
TLB
P000102
1,1-Dichloropropylene
BRL
mg/kg dry
0.0064
0.00099
1
*8260D
3/5/20 14:11
TLB
P000102
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00092
1
*8260D
3/5/20 14:11
TLB
P000102
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0064
0.00073
1
*8260D
3/5/20 14:11
TLB
P000102
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00062
1
*8260D
3/5/20 14:11
TLB
P000102
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0064
0.00068
1
*8260D
3/5/20 14:11
TLB
P000102
1,2-Dibromoethane
BRL
mg/kg dry
0.0064
0.00058
1
*8260D
3/5/20 14:11
TLB
P000102
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0064
0.00072
1
*8260D
3/5/20 14:11
TLB
P000102
1,2-Dichloroethane
BRL
mg/kg dry
0.0064
0.00077
1
*8260D
3/5/20 14:11
TLB
P000102
1,2-Dichloropropane
BRL
mg/kg dry
0.0064
0.00097
1
*8260D
3/5/20 14:11
TLB
P000102
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0064
0.00081
1
*8260D
3/5/20 14:11
TLB
P000102
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0064
0.00080
1
*8260D
3/5/20 14:11
TLB
P000102
1,3-Dichloropropane
BRL
mg/kg dry
0.0064
0.00054
1
*8260D
3/5/20 14:11
TLB
P000102
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0064
0.00082
1
*8260D
3/5/20 14:11
TLB
P000102
2,2-Dichloropropane
BRL
mg/kg dry
0.0064
0.00080
1
*8260D
3/5/20 14:11
TLB
P000102
2-Chlorotoluene
BRL
mg/kg dry
0.0064
0.00086
1
*8260D
3/5/20 14:11
TLB
P000102
4-Chlorotoluene
BRL
mg/kg dry
0.0064
0.00073
1
*8260D
3/5/20 14:11
TLB
P000102
4-Isopropyltoluene
BRL
mg/kg dry
0.0064
0.0016
1
*8260D
3/5/20 14:11
TLB
P000102
Acetone
BRL CCVH
mg/kg dry
0.026
0.0016
1
*8260D
3/5/20 14:11
TLB
P000102
Benzene
BRL
mg/kg dry
0.0064
0.0010
1
*8260D
3/5/20 14:11
TLB
P000102
Bromobenzene
BRL
mg/kg dry
0.0064
0.00090
1
*8260D
3/5/20 14:11
TLB
P000102
Bromochloromethane
BRL
mg/kg dry
0.0064
0.0011
1
*8260D
3/5/20 14:11
TLB
P000102
Bromodichloromethane
BRL
mg/kg dry
0.0064
0.00061
1
*8260D
3/5/20 14:11
TLB
P000102
Bromoform
BRL
mg/kg dry
0.0064
0.00050
1
*8260D
3/5/20 14:11
TLB
P000102
Bromomethane
BRL
mg/kg dry
0.013
0.0032
1
*8260D
3/5/20 14:11
TLB
P000102
Carbon Tetrachloride
BRL
mg/kg dry
0.0064
0.0013
1
*8260D
3/5/20 14:11
TLB
P000102
Chlorobenzene
BRL
mg/kg dry
0.0064
0.0010
1
*8260D
3/5/20 14:11
TLB
P000102
Chloroethane
BRL
mg/kg dry
0.013
0.0012
1
*8260D
3/5/20 14:11
TLB
P000102
Chloroform
BRL
mg/kg dry
0.0064
0.00079
1
*8260D
3/5/20 14:11
TLB
P000102
Chloromethane
BRL
mg/kg dry
0.013
0.0020
1
*8260D
3/5/20 14:11
TLB
P000102
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0064
0.0010
1
*8260D
3/5/20 14:11
TLB
P000102
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0064
0.00064
1
*8260D
3/5/20 14:11
TLB
P000102
Dibromochloromethane
BRL
mg/kg dry
0.0064
0.00043
1
*8260D
3/5/20 14:11
TLB
P000102
Dichlorodifluoromethane
BRL
mg/kg dry
0.013
0.0018
1
*8260D
3/5/20 14:11
TLB
P000102
Ethylbenzene
BRL
mg/kg dry
0.0064
0.00097
1
*8260D
3/5/20 14:11
TLB
P000102
Isopropyl Ether
BRL
mg/kg dry
0.0064
0.00095
1
*8260D
3/5/20 14:11
TLB
P000102
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0064
0.00075
1
*8260D
3/5/20 14:11
TLB
P000102
m,p-Xylenes
BRL
mg/kg dry
0.013
0.0017
1
*8260D
3/5/20 14:11
TLB
P000102
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-N
Attn: Matt Ingalls Sample ID: 0030027-07
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:15
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.026
0.00045
1
*8260D
3/5/20 14:11
TLB
P000102
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.026
0.0015
1
*8260D
3/5/20 14:11
TLB
P000102
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.026
0.00053
1
*8260D
3/5/20 14:11
TLB
P000102
Methylene Chloride
BRL
mg/kg dry
0.0064
0.0010
1
*8260D
3/5/20 14:11
TLB
P000102
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0064
0.00090
1
*8260D
3/5/20 14:11
TLB
P000102
Naphthalene
BRL
mg/kg dry
0.013
0.00065
1
*8260D
3/5/20 14:11
TLB
P000102
n-Butylbenzene
BRL
mg/kg dry
0.0064
0.00060
1
*8260D
3/5/20 14:11
TLB
P000102
n-Propylbenzene
BRL
mg/kg dry
0.0064
0.00094
1
*8260D
3/5/20 14:11
TLB
P000102
o-Xylene
BRL
mg/kg dry
0.0064
0.00069
1
*8260D
3/5/20 14:11
TLB
P000102
sec-Butylbenzene
BRL
mg/kg dry
0.0064
0.00070
1
*8260D
3/5/20 14:11
TLB
P000102
Styrene
BRL
mg/kg dry
0.0064
0.00063
1
*8260D
3/5/20 14:11
TLB
P000102
tert-Butylbenzene
BRL
mg/kg dry
0.0064
0.00077
1
*8260D
3/5/20 14:11
TLB
P000102
Tetrachloroethylene
BRL
mg/kg dry
0.0064
0.0012
1
*8260D
3/5/20 14:11
TLB
P000102
Toluene
BRL
mg/kg dry
0.0064
0.0010
1
*8260D
3/5/20 14:11
TLB
P000102
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0064
0.0012
1
*8260D
3/5/20 14:11
TLB
P000102
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0064
0.00055
1
*8260D
3/5/20 14:11
TLB
P000102
Trichloroethylene
BRL
mg/kg dry
0.0064
0.0013
1
*8260D
3/5/20 14:11
TLB
P000102
Trichlorofluoromethane
BRL
mg/kg dry
0.013
0.0017
1
*8260D
3/5/20 14:11
TLB
P000102
Vinyl acetate
BRL
mg/kg dry
0.013
0.00070
1
*8260D
3/5/20 14:11
TLB
P000102
Vinyl chloride
BRL
mg/kg dry
0.013
0.0013
1
*8260D
3/5/20 14:11
TLB
P000102
Xylenes, total
BRL
mg/kg dry
0.019
0.0023
1
*8260D
3/5/20 14:11
TLB
P000102
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
92 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
25
5.0
100
*MADEP VPH
3/5/20 18:53
TBL
P000106
C9-C12 Aliphatics
BRL
mg/kg dry
25
2.2
100
*MADEP VPH
3/5/20 18:53
TBL
P000106
C9-Cl0 Aromatics
BRL
mg/kg dry
25
2.4
100
*MADEP VPH
3/5/20 18:53
TBL
P000106
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
115 %
70-130
2,5-Dibromotoluene (FID)
123 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waynt.�
03/10/2020
PA
ANALYTICAL
Hart & Hickman (Charlotte)
Project: WIT-019
Client Sample ID: UST-2 Sidewall-E
Attn: Matt Ingalls
Sample ID: 0030027-08
2923 South Tryon St. Ste 100
Work
Order: 0030027
Charlotte, NC 28203
Sample Matrix: Solid
Time
Collected: 03/02/20 14:20
Time
Submitted: 03/03/20 11:55
Parameter
Result Units
Report
MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
BRL
mg/kg dry
32
1.6
1
*MADEP EPH 3/7/20 5:46
ZRC
P000104
C19-C36 Aliphatics
BRL
mg/kg dry
32
5.3
1
*MADEP EPH 3/7/20 5:46
ZRC
P000104
C11-C22Aromatics
BRL
mg/kg dry
32
8.6
1
*MADEP EPH 3/7/20 5:46
ZRC
P000104
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
61 %
40-140
o-Terphenyl
62 %
40-140
2-Fluorobiphenyl
72 %
40-140
2-Bromonaphthalene
69 %
40-140
General Chemistry Parameters
% Solids
77.4
% by
0.100
0.100
1
*SM2540 G 316120 9:04
EDV
P000110
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.85
0.15
1
*8270E 3/5/20 22:01
JMV
P000087
1,2-Dichlorobenzene
BRL
mg/kg dry
0.85
0.14
1
*8270E 3/5/20 22:01
JMV
P000087
1,3-Dichlorobenzene
BRL
mg/kg dry
0.85
0.13
1
*8270E 3/5/20 22:01
JMV
P000087
1,4-Dichlorobenzene
BRL
mg/kg dry
0.43
0.13
1
*8270E 3/5/20 22:01
JMV
P000087
1-Methyl naphthalene
BRL
mg/kg dry
0.85
0.013
1
*8270E 3/5/20 22:01
JMV
P000087
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.85
0.18
1
*8270E 3/5/20 22:01
JMV
P000087
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.85
0.21
1
*8270E 3/5/20 22:01
JMV
P000087
2,4-Dichlorophenol
BRL
mg/kg dry
0.85
0.17
1
*8270E 3/5/20 22:01
JMV
P000087
2,4-Dimethylphenol
BRL
mg/kg dry
0.43
0.18
1
*8270E 3/5/20 22:01
JMV
P000087
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.50
1
*8270E 3/5/20 22:01
JMV
P000087
2,4-Dinitrotoluene
BRL
mg/kg dry
0.85
0.23
1
*8270E 3/5/20 22:01
JMV
P000087
2,6-Dinitrotoluene
BRL
mg/kg dry
0.85
0.22
1
*8270E 3/5/20 22:01
JMV
P000087
2-Chloronaphthalene
BRL
mg/kg dry
0.85
0.21
1
*8270E 3/5/20 22:01
JMV
P000087
2-Chlorophenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/5/20 22:01
JMV
P000087
2-Methyl naphthalene
BRL
mg/kg dry
0.85
0.017
1
*8270E 3/5/20 22:01
JMV
P000087
2-Methylphenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/5/20 22:01
JMV
P000087
2-Nitrophenol
BRL
mg/kg dry
0.85
0.14
1
*8270E 3/5/20 22:01
JMV
P000087
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.85
0.17
1
*8270E 3/5/20 22:01
JMV
P000087
3/4-Methyl phenol
BRL
mg/kg dry
0.85
0.18
1
*8270E 3/5/20 22:01
JMV
P000087
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.47
1
*8270E 3/5/20 22:01
JMV
P000087
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.85
0.20
1
*8270E 3/5/20 22:01
JMV
P000087
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/5/20 22:01
JMV
P000087
4-Chloroaniline
BRL
mg/kg dry
0.43
0.10
1
*8270E 3/5/20 22:01
JMV
P000087
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
*8270E 3/5/20 22:01
JMV
P000087
4-Nitrophenol
BRL
mg/kg dry
0.85
0.21
1
*8270E 3/5/20 22:01
JMV
P000087
Acenaphthene
BRL
mg/kg dry
0.85
0.019
1
*8270E 3/5/20 22:01
JMV
P000087
Acenaphthylene
BRL
mg/kg dry
0.85
0.017
1
*8270E 3/5/20 22:01
JMV
P000087
Anthracene
BRL
mg/kg dry
0.85
0.0094
1
*8270E 3/5/20 22:01
JMV
P000087
Azobenzene
BRL
mg/kg dry
0.85
0.18
1
*8270E 3/5/20 22:01
JMV
P000087
Benzo(a)anthracene
BRL
mg/kg dry
0.85
0.010
1
*8270E 3/5/20 22:01
JMV
P000087
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-E
Attn: Matt Ingalls Sample ID: 0030027-08
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:20
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.85
0.0076
1
*8270E
3/5/20 22:01
JMV
P000087
Benzo(b)fluoranthene
BRL
mg/kg dry
0.85
0.0079
1
*8270E
3/5/20 22:01
JMV
P000087
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.85
0.0084
1
*8270E
3/5/20 22:01
JMV
P000087
Benzo(k)fluoranthene
BRL
mg/kg dry
0.85
0.0090
1
*8270E
3/5/20 22:01
JMV
P000087
Benzoic Acid
BRL
mg/kg dry
2.6
0.71
1
*8270E
3/5/20 22:01
JMV
P000087
Benzyl alcohol
BRL
mg/kg dry
0.85
0.16
1
*8270E
3/5/20 22:01
JMV
P000087
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.85
0.16
1
*8270E
3/5/20 22:01
JMV
P000087
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.85
0.14
1
*8270E
3/5/20 22:01
JMV
P000087
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 22:01
JMV
P000087
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/5/20 22:01
JMV
P000087
Butyl benzyl phthalate
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 22:01
JMV
P000087
Chrysene
BRL
mg/kg dry
0.85
0.010
1
*8270E
3/5/20 22:01
JMV
P000087
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.85
0.025
1
*8270E
3/5/20 22:01
JMV
P000087
Dibenzofuran
BRL
mg/kg dry
0.85
0.23
1
*8270E
3/5/20 22:01
JMV
P000087
Diethyl phthalate
BRL
mg/kg dry
0.85
0.22
1
*8270E
3/5/20 22:01
JMV
P000087
Dimethyl phthalate
BRL
mg/kg dry
0.85
0.20
1
*8270E
3/5/20 22:01
JMV
P000087
Di-n-butyl phthalate
BRL
mg/kg dry
0.85
0.21
1
*8270E
3/5/20 22:01
JMV
P000087
Di-n-octyl phthalate
BRL
mg/kg dry
0.43
0.22
1
*8270E
3/5/20 22:01
JMV
P000087
Fluoranthene
BRL
mg/kg dry
0.85
0.0097
1
*8270E
3/5/20 22:01
JMV
P000087
Fluorene
BRL
mg/kg dry
0.85
0.015
1
*8270E
3/5/20 22:01
JMV
P000087
Hexachlorobenzene
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/5/20 22:01
JMV
P000087
Hexachlorobutadiene
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/5/20 22:01
JMV
P000087
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.85
0.29
1
*8270E
3/5/20 22:01
JMV
P000087
Hexachloroethane
BRL
mg/kg dry
0.85
0.13
1
*8270E
3/5/20 22:01
JMV
P000087
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.85
0.024
1
*8270E
3/5/20 22:01
JMV
P000087
Isophorone
BRL
mg/kg dry
0.85
0.18
1
*8270E
3/5/20 22:01
JMV
P000087
Naphthalene
BRL
mg/kg dry
0.85
0.018
1
*8270E
3/5/20 22:01
JMV
P000087
Nitrobenzene
BRL
mg/kg dry
0.43
0.18
1
*8270E
3/5/20 22:01
JMV
P000087
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.85
0.20
1
*8270E
3/5/20 22:01
JMV
P000087
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.85
0.23
1
*8270E
3/5/20 22:01
JMV
P000087
Pentachlorophenol
BRL
mg/kg dry
1.3
0.54
1
*8270E
3/5/20 22:01
JMV
P000087
Phenanthrene
BRL
mg/kg dry
0.85
0.0093
1
*8270E
3/5/20 22:01
JMV
P000087
Phenol
BRL
mg/kg dry
0.85
0.14
1
*8270E
3/5/20 22:01
JMV
P000087
Pyrene
BRL
mg/kg dry
0.85
0.012
1
*8270E
3/5/20 22:01
JMV
P000087
Pyridine
BRL
mg/kg dry
0.43
0.081
1
*8270E
3/5/20 22:01
JMV
P000087
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
90 %
39-132
2-Fluorobiphenyl
73 %
44-115
2-Fluorophenol
79 %
35-115
Nitrobenzene-d5
68 %
37-122
Phenol-d5
77 %
34-121
Terphenyl-d14
83 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-E
Attn: Matt Ingalls Sample ID: 0030027-08
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:20
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0067
0.00082
1
*8260D
3/5/20 14:41
TLB
P000102
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0067
0.00099
1
*8260D
3/5/20 14:41
TLB
P000102
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0067
0.00049
1
*8260D
3/5/20 14:41
TLB
P000102
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0067
0.00072
1
*8260D
3/5/20 14:41
TLB
P000102
1,1-Dichloroethane
BRL
mg/kg dry
0.0067
0.0012
1
*8260D
3/5/20 14:41
TLB
P000102
1,1-Dichloroethylene
BRL
mg/kg dry
0.0067
0.0012
1
*8260D
3/5/20 14:41
TLB
P000102
1,1-Dichloropropylene
BRL
mg/kg dry
0.0067
0.0010
1
*8260D
3/5/20 14:41
TLB
P000102
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00096
1
*8260D
3/5/20 14:41
TLB
P000102
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0067
0.00076
1
*8260D
3/5/20 14:41
TLB
P000102
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.013
0.00064
1
*8260D
3/5/20 14:41
TLB
P000102
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0067
0.00071
1
*8260D
3/5/20 14:41
TLB
P000102
1,2-Dibromoethane
BRL
mg/kg dry
0.0067
0.00060
1
*8260D
3/5/20 14:41
TLB
P000102
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0067
0.00075
1
*8260D
3/5/20 14:41
TLB
P000102
1,2-Dichloroethane
BRL
mg/kg dry
0.0067
0.00080
1
*8260D
3/5/20 14:41
TLB
P000102
1,2-Dichloropropane
BRL
mg/kg dry
0.0067
0.0010
1
*8260D
3/5/20 14:41
TLB
P000102
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0067
0.00084
1
*8260D
3/5/20 14:41
TLB
P000102
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0067
0.00083
1
*8260D
3/5/20 14:41
TLB
P000102
1,3-Dichloropropane
BRL
mg/kg dry
0.0067
0.00056
1
*8260D
3/5/20 14:41
TLB
P000102
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0067
0.00085
1
*8260D
3/5/20 14:41
TLB
P000102
2,2-Dichloropropane
BRL
mg/kg dry
0.0067
0.00084
1
*8260D
3/5/20 14:41
TLB
P000102
2-Chlorotoluene
BRL
mg/kg dry
0.0067
0.00090
1
*8260D
3/5/20 14:41
TLB
P000102
4-Chlorotoluene
BRL
mg/kg dry
0.0067
0.00076
1
*8260D
3/5/20 14:41
TLB
P000102
4-Isopropyltoluene
BRL
mg/kg dry
0.0067
0.0017
1
*8260D
3/5/20 14:41
TLB
P000102
Acetone
BRL CCVH
mg/kg dry
0.027
0.0017
1
*8260D
3/5/20 14:41
TLB
P000102
Benzene
BRL
mg/kg dry
0.0067
0.0010
1
*8260D
3/5/20 14:41
TLB
P000102
Bromobenzene
BRL
mg/kg dry
0.0067
0.00093
1
*8260D
3/5/20 14:41
TLB
P000102
Bromochloromethane
BRL
mg/kg dry
0.0067
0.0011
1
*8260D
3/5/20 14:41
TLB
P000102
Bromodichloromethane
BRL
mg/kg dry
0.0067
0.00064
1
*8260D
3/5/20 14:41
TLB
P000102
Bromoform
BRL
mg/kg dry
0.0067
0.00052
1
*8260D
3/5/20 14:41
TLB
P000102
Bromomethane
BRL
mg/kg dry
0.013
0.0033
1
*8260D
3/5/20 14:41
TLB
P000102
Carbon Tetrachloride
BRL
mg/kg dry
0.0067
0.0013
1
*8260D
3/5/20 14:41
TLB
P000102
Chlorobenzene
BRL
mg/kg dry
0.0067
0.0010
1
*8260D
3/5/20 14:41
TLB
P000102
Chloroethane
BRL
mg/kg dry
0.013
0.0013
1
*8260D
3/5/20 14:41
TLB
P000102
Chloroform
BRL
mg/kg dry
0.0067
0.00082
1
*8260D
3/5/20 14:41
TLB
P000102
Chloromethane
BRL
mg/kg dry
0.013
0.0020
1
*8260D
3/5/20 14:41
TLB
P000102
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0067
0.0011
1
*8260D
3/5/20 14:41
TLB
P000102
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0067
0.00066
1
*8260D
3/5/20 14:41
TLB
P000102
Dibromochloromethane
BRL
mg/kg dry
0.0067
0.00045
1
*8260D
3/5/20 14:41
TLB
P000102
Dichlorodifluoromethane
BRL
mg/kg dry
0.013
0.0019
1
*8260D
3/5/20 14:41
TLB
P000102
Ethylbenzene
BRL
mg/kg dry
0.0067
0.0010
1
*8260D
3/5/20 14:41
TLB
P000102
Isopropyl Ether
BRL
mg/kg dry
0.0067
0.00099
1
*8260D
3/5/20 14:41
TLB
P000102
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0067
0.00078
1
*8260D
3/5/20 14:41
TLB
P000102
m,p-Xylenes
BRL
mg/kg dry
0.013
0.0017
1
*8260D
3/5/20 14:41
TLB
P000102
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-E
Attn: Matt Ingalls Sample ID: 0030027-08
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:20
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.027
0.00046
1
*8260D
3/5/20 14:41
TLB
P000102
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.027
0.0016
1
*8260D
3/5/20 14:41
TLB
P000102
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.027
0.00055
1
*8260D
3/5/20 14:41
TLB
P000102
Methylene Chloride
BRL
mg/kg dry
0.0067
0.0011
1
*8260D
3/5/20 14:41
TLB
P000102
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0067
0.00094
1
*8260D
3/5/20 14:41
TLB
P000102
Naphthalene
BRL
mg/kg dry
0.013
0.00068
1
*8260D
3/5/20 14:41
TLB
P000102
n-Butylbenzene
BRL
mg/kg dry
0.0067
0.00063
1
*8260D
3/5/20 14:41
TLB
P000102
n-Propylbenzene
BRL
mg/kg dry
0.0067
0.00097
1
*8260D
3/5/20 14:41
TLB
P000102
o-Xylene
BRL
mg/kg dry
0.0067
0.00071
1
*8260D
3/5/20 14:41
TLB
P000102
sec-Butylbenzene
BRL
mg/kg dry
0.0067
0.00072
1
*8260D
3/5/20 14:41
TLB
P000102
Styrene
BRL
mg/kg dry
0.0067
0.00065
1
*8260D
3/5/20 14:41
TLB
P000102
tert-Butylbenzene
BRL
mg/kg dry
0.0067
0.00080
1
*8260D
3/5/20 14:41
TLB
P000102
Tetrachloroethylene
BRL
mg/kg dry
0.0067
0.0012
1
*8260D
3/5/20 14:41
TLB
P000102
Toluene
BRL
mg/kg dry
0.0067
0.0011
1
*8260D
3/5/20 14:41
TLB
P000102
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0067
0.0013
1
*8260D
3/5/20 14:41
TLB
P000102
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0067
0.00057
1
*8260D
3/5/20 14:41
TLB
P000102
Trichloroethylene
BRL
mg/kg dry
0.0067
0.0013
1
*8260D
3/5/20 14:41
TLB
P000102
Trichlorofluoromethane
BRL
mg/kg dry
0.013
0.0018
1
*8260D
3/5/20 14:41
TLB
P000102
Vinyl acetate
BRL
mg/kg dry
0.013
0.00073
1
*8260D
3/5/20 14:41
TLB
P000102
Vinyl chloride
BRL
mg/kg dry
0.013
0.0013
1
*8260D
3/5/20 14:41
TLB
P000102
Xylenes, total
BRL
mg/kg dry
0.020
0.0024
1
*8260D
3/5/20 14:41
TLB
P000102
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
92 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
23
4.5
100
*MADEP VPH
3/5/20 19:23
TBL
P000106
C9-C12 Aliphatics
BRL
mg/kg dry
23
2.0
100
*MADEP VPH
3/5/20 19:23
TBL
P000106
C9-Cl0 Aromatics
BRL
mg/kg dry
23
2.1
100
*MADEP VPH
3/5/20 19:23
TBL
P000106
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
115 %
70-130
2,5-Dibromotoluene (FID)
122 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waynt.�
03/10/2020
PA
ANALYTICAL
Hart & Hickman (Charlotte)
Project: WIT-019
Client Sample ID: UST-2 Sidewall-S
Attn: Matt Ingalls
Sample ID: 0030027-09
2923 South Tryon St. Ste 100
Work
Order: 0030027
Charlotte, NC 28203
Sample Matrix: Solid
Time
Collected: 03/02/20 14:30
Time
Submitted: 03/03/20 11:55
Parameter
Result Units
Report
MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
BRL
mg/kg dry
31
1.6
1
*MADEP EPH 3/7/20 6:58
ZRC
P000104
C19-C36 Aliphatics
BRL
mg/kg dry
31
5.3
1
*MADEP EPH 3/7/20 6:58
ZRC
P000104
C11-C22Aromatics
BRL
mg/kg dry
31
8.6
1
*MADEP EPH 3/7/20 6:58
ZRC
P000104
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
71 %
40-140
o-Terphenyl
67 %
40-140
2-Fluorobiphenyl
71 %
40-140
2-Bromonaphthalene
53 %
40-140
General Chemistry Parameters
% Solids
77.2
% by
0.100
0.100
1
*SM2540 G 316120 9:04
EDV
P000110
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.85
0.15
1
*8270E 3/5/20 22:24
JMV
P000087
1,2-Dichlorobenzene
BRL
mg/kg dry
0.85
0.14
1
*8270E 3/5/20 22:24
JMV
P000087
1,3-Dichlorobenzene
BRL
mg/kg dry
0.85
0.13
1
*8270E 3/5/20 22:24
JMV
P000087
1,4-Dichlorobenzene
BRL
mg/kg dry
0.43
0.13
1
*8270E 3/5/20 22:24
JMV
P000087
1-Methyl naphthalene
BRL
mg/kg dry
0.85
0.013
1
*8270E 3/5/20 22:24
JMV
P000087
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.85
0.18
1
*8270E 3/5/20 22:24
JMV
P000087
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.85
0.21
1
*8270E 3/5/20 22:24
JMV
P000087
2,4-Dichlorophenol
BRL
mg/kg dry
0.85
0.17
1
*8270E 3/5/20 22:24
JMV
P000087
2,4-Dimethylphenol
BRL
mg/kg dry
0.43
0.18
1
*8270E 3/5/20 22:24
JMV
P000087
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.50
1
*8270E 3/5/20 22:24
JMV
P000087
2,4-Dinitrotoluene
BRL
mg/kg dry
0.85
0.23
1
*8270E 3/5/20 22:24
JMV
P000087
2,6-Dinitrotoluene
BRL
mg/kg dry
0.85
0.22
1
*8270E 3/5/20 22:24
JMV
P000087
2-Chloronaphthalene
BRL
mg/kg dry
0.85
0.21
1
*8270E 3/5/20 22:24
JMV
P000087
2-Chlorophenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/5/20 22:24
JMV
P000087
2-Methyl naphthalene
BRL
mg/kg dry
0.85
0.017
1
*8270E 3/5/20 22:24
JMV
P000087
2-Methylphenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/5/20 22:24
JMV
P000087
2-Nitrophenol
BRL
mg/kg dry
0.85
0.14
1
*8270E 3/5/20 22:24
JMV
P000087
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.85
0.17
1
*8270E 3/5/20 22:24
JMV
P000087
3/4-Methyl phenol
BRL
mg/kg dry
0.85
0.19
1
*8270E 3/5/20 22:24
JMV
P000087
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.47
1
*8270E 3/5/20 22:24
JMV
P000087
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.85
0.20
1
*8270E 3/5/20 22:24
JMV
P000087
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/5/20 22:24
JMV
P000087
4-Chloroaniline
BRL
mg/kg dry
0.43
0.10
1
*8270E 3/5/20 22:24
JMV
P000087
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
*8270E 3/5/20 22:24
JMV
P000087
4-Nitrophenol
BRL
mg/kg dry
0.85
0.21
1
*8270E 3/5/20 22:24
JMV
P000087
Acenaphthene
BRL
mg/kg dry
0.85
0.020
1
*8270E 3/5/20 22:24
JMV
P000087
Acenaphthylene
BRL
mg/kg dry
0.85
0.017
1
*8270E 3/5/20 22:24
JMV
P000087
Anthracene
BRL
mg/kg dry
0.85
0.0095
1
*8270E 3/5/20 22:24
JMV
P000087
Azobenzene
BRL
mg/kg dry
0.85
0.18
1
*8270E 3/5/20 22:24
JMV
P000087
Benzo(a)anthracene
BRL
mg/kg dry
0.85
0.010
1
*8270E 3/5/20 22:24
JMV
P000087
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-S
Attn: Matt Ingalls Sample ID: 0030027-09
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:30
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.85
0.0076
1
*8270E
3/5/20 22:24
JMV
P000087
Benzo(b)fluoranthene
BRL
mg/kg dry
0.85
0.0079
1
*8270E
3/5/20 22:24
JMV
P000087
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.85
0.0084
1
*8270E
3/5/20 22:24
JMV
P000087
Benzo(k)fluoranthene
BRL
mg/kg dry
0.85
0.0091
1
*8270E
3/5/20 22:24
JMV
P000087
Benzoic Acid
BRL
mg/kg dry
2.6
0.71
1
*8270E
3/5/20 22:24
JMV
P000087
Benzyl alcohol
BRL
mg/kg dry
0.85
0.16
1
*8270E
3/5/20 22:24
JMV
P000087
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.85
0.16
1
*8270E
3/5/20 22:24
JMV
P000087
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.85
0.14
1
*8270E
3/5/20 22:24
JMV
P000087
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 22:24
JMV
P000087
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/5/20 22:24
JMV
P000087
Butyl benzyl phthalate
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 22:24
JMV
P000087
Chrysene
BRL
mg/kg dry
0.85
0.010
1
*8270E
3/5/20 22:24
JMV
P000087
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.85
0.025
1
*8270E
3/5/20 22:24
JMV
P000087
Dibenzofuran
BRL
mg/kg dry
0.85
0.23
1
*8270E
3/5/20 22:24
JMV
P000087
Diethyl phthalate
BRL
mg/kg dry
0.85
0.22
1
*8270E
3/5/20 22:24
JMV
P000087
Dimethyl phthalate
BRL
mg/kg dry
0.85
0.20
1
*8270E
3/5/20 22:24
JMV
P000087
Di-n-butyl phthalate
BRL
mg/kg dry
0.85
0.21
1
*8270E
3/5/20 22:24
JMV
P000087
Di-n-octyl phthalate
BRL
mg/kg dry
0.43
0.22
1
*8270E
3/5/20 22:24
JMV
P000087
Fluoranthene
BRL
mg/kg dry
0.85
0.0097
1
*8270E
3/5/20 22:24
JMV
P000087
Fluorene
BRL
mg/kg dry
0.85
0.015
1
*8270E
3/5/20 22:24
JMV
P000087
Hexachlorobenzene
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/5/20 22:24
JMV
P000087
Hexachlorobutadiene
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/5/20 22:24
JMV
P000087
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.85
0.29
1
*8270E
3/5/20 22:24
JMV
P000087
Hexachloroethane
BRL
mg/kg dry
0.85
0.13
1
*8270E
3/5/20 22:24
JMV
P000087
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.85
0.024
1
*8270E
3/5/20 22:24
JMV
P000087
Isophorone
BRL
mg/kg dry
0.85
0.18
1
*8270E
3/5/20 22:24
JMV
P000087
Naphthalene
BRL
mg/kg dry
0.85
0.018
1
*8270E
3/5/20 22:24
JMV
P000087
Nitrobenzene
BRL
mg/kg dry
0.43
0.18
1
*8270E
3/5/20 22:24
JMV
P000087
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.85
0.20
1
*8270E
3/5/20 22:24
JMV
P000087
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.85
0.23
1
*8270E
3/5/20 22:24
JMV
P000087
Pentachlorophenol
BRL
mg/kg dry
1.3
0.55
1
*8270E
3/5/20 22:24
JMV
P000087
Phenanthrene
BRL
mg/kg dry
0.85
0.0093
1
*8270E
3/5/20 22:24
JMV
P000087
Phenol
BRL
mg/kg dry
0.85
0.14
1
*8270E
3/5/20 22:24
JMV
P000087
Pyrene
BRL
mg/kg dry
0.85
0.012
1
*8270E
3/5/20 22:24
JMV
P000087
Pyridine
BRL
mg/kg dry
0.43
0.082
1
*8270E
3/5/20 22:24
JMV
P000087
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
89 %
39-132
2-Fluorobiphenyl
77 %
44-115
2-Fluorophenol
82 %
35-115
Nitrobenzene-d5
72 %
37-122
Phenol-d5
77 %
34-121
Terphenyl-d14
79 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-S
Attn: Matt Ingalls Sample ID: 0030027-09
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:30
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0084
0.0010
1
*8260D
3/5/20 15:11
TLB
P000102
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0084
0.0012
1
*8260D
3/5/20 15:11
TLB
P000102
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0084
0.00061
1
*8260D
3/5/20 15:11
TLB
P000102
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0084
0.00090
1
*8260D
3/5/20 15:11
TLB
P000102
1,1-Dichloroethane
BRL
mg/kg dry
0.0084
0.0015
1
*8260D
3/5/20 15:11
TLB
P000102
1,1-Dichloroethylene
BRL
mg/kg dry
0.0084
0.0015
1
*8260D
3/5/20 15:11
TLB
P000102
1,1-Dichloropropylene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 15:11
TLB
P000102
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.017
0.0012
1
*8260D
3/5/20 15:11
TLB
P000102
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0084
0.00095
1
*8260D
3/5/20 15:11
TLB
P000102
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.017
0.00080
1
*8260D
3/5/20 15:11
TLB
P000102
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0084
0.00089
1
*8260D
3/5/20 15:11
TLB
P000102
1,2-Dibromoethane
BRL
mg/kg dry
0.0084
0.00075
1
*8260D
3/5/20 15:11
TLB
P000102
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0084
0.00093
1
*8260D
3/5/20 15:11
TLB
P000102
1,2-Dichloroethane
BRL
mg/kg dry
0.0084
0.0010
1
*8260D
3/5/20 15:11
TLB
P000102
1,2-Dichloropropane
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 15:11
TLB
P000102
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0084
0.0011
1
*8260D
3/5/20 15:11
TLB
P000102
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0084
0.0010
1
*8260D
3/5/20 15:11
TLB
P000102
1,3-Dichloropropane
BRL
mg/kg dry
0.0084
0.00070
1
*8260D
3/5/20 15:11
TLB
P000102
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0084
0.0011
1
*8260D
3/5/20 15:11
TLB
P000102
2,2-Dichloropropane
BRL
mg/kg dry
0.0084
0.0010
1
*8260D
3/5/20 15:11
TLB
P000102
2-Chlorotoluene
BRL
mg/kg dry
0.0084
0.0011
1
*8260D
3/5/20 15:11
TLB
P000102
4-Chlorotoluene
BRL
mg/kg dry
0.0084
0.00095
1
*8260D
3/5/20 15:11
TLB
P000102
4-Isopropyltoluene
BRL
mg/kg dry
0.0084
0.0021
1
*8260D
3/5/20 15:11
TLB
P000102
Acetone
BRL CCVH
mg/kg dry
0.033
0.0021
1
*8260D
3/5/20 15:11
TLB
P000102
Benzene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 15:11
TLB
P000102
Bromobenzene
BRL
mg/kg dry
0.0084
0.0012
1
*8260D
3/5/20 15:11
TLB
P000102
Bromochloromethane
BRL
mg/kg dry
0.0084
0.0014
1
*8260D
3/5/20 15:11
TLB
P000102
Bromodichloromethane
BRL
mg/kg dry
0.0084
0.00080
1
*8260D
3/5/20 15:11
TLB
P000102
Bromoform
BRL
mg/kg dry
0.0084
0.00065
1
*8260D
3/5/20 15:11
TLB
P000102
Bromomethane
BRL
mg/kg dry
0.017
0.0041
1
*8260D
3/5/20 15:11
TLB
P000102
Carbon Tetrachloride
BRL
mg/kg dry
0.0084
0.0016
1
*8260D
3/5/20 15:11
TLB
P000102
Chlorobenzene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 15:11
TLB
P000102
Chloroethane
BRL
mg/kg dry
0.017
0.0016
1
*8260D
3/5/20 15:11
TLB
P000102
Chloroform
BRL
mg/kg dry
0.0084
0.0010
1
*8260D
3/5/20 15:11
TLB
P000102
Chloromethane
BRL
mg/kg dry
0.017
0.0025
1
*8260D
3/5/20 15:11
TLB
P000102
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 15:11
TLB
P000102
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0084
0.00083
1
*8260D
3/5/20 15:11
TLB
P000102
Dibromochloromethane
BRL
mg/kg dry
0.0084
0.00056
1
*8260D
3/5/20 15:11
TLB
P000102
Dichlorodifluoromethane
BRL
mg/kg dry
0.017
0.0024
1
*8260D
3/5/20 15:11
TLB
P000102
Ethylbenzene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 15:11
TLB
P000102
Isopropyl Ether
BRL
mg/kg dry
0.0084
0.0012
1
*8260D
3/5/20 15:11
TLB
P000102
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0084
0.00097
1
*8260D
3/5/20 15:11
TLB
P000102
m,p-Xylenes
BRL
mg/kg dry
0.017
0.0021
1
*8260D
3/5/20 15:11
TLB
P000102
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-S
Attn: Matt Ingalls Sample ID: 0030027-09
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:30
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.033
0.00058
1
*8260D
3/5/20 15:11
TLB
P000102
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.033
0.0020
1
*8260D
3/5/20 15:11
TLB
P000102
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.033
0.00068
1
*8260D
3/5/20 15:11
TLB
P000102
Methylene Chloride
BRL
mg/kg dry
0.0084
0.0014
1
*8260D
3/5/20 15:11
TLB
P000102
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0084
0.0012
1
*8260D
3/5/20 15:11
TLB
P000102
Naphthalene
BRL
mg/kg dry
0.017
0.00085
1
*8260D
3/5/20 15:11
TLB
P000102
n-Butylbenzene
BRL
mg/kg dry
0.0084
0.00078
1
*8260D
3/5/20 15:11
TLB
P000102
n-Propylbenzene
BRL
mg/kg dry
0.0084
0.0012
1
*8260D
3/5/20 15:11
TLB
P000102
o-Xylene
BRL
mg/kg dry
0.0084
0.00089
1
*8260D
3/5/20 15:11
TLB
P000102
sec-Butylbenzene
BRL
mg/kg dry
0.0084
0.00090
1
*8260D
3/5/20 15:11
TLB
P000102
Styrene
BRL
mg/kg dry
0.0084
0.00081
1
*8260D
3/5/20 15:11
TLB
P000102
tert-Butylbenzene
BRL
mg/kg dry
0.0084
0.00099
1
*8260D
3/5/20 15:11
TLB
P000102
Tetrachloroethylene
BRL
mg/kg dry
0.0084
0.0015
1
*8260D
3/5/20 15:11
TLB
P000102
Toluene
BRL
mg/kg dry
0.0084
0.0013
1
*8260D
3/5/20 15:11
TLB
P000102
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0084
0.0016
1
*8260D
3/5/20 15:11
TLB
P000102
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0084
0.00072
1
*8260D
3/5/20 15:11
TLB
P000102
Trichloroethylene
BRL
mg/kg dry
0.0084
0.0016
1
*8260D
3/5/20 15:11
TLB
P000102
Trichlorofluoromethane
BRL
mg/kg dry
0.017
0.0023
1
*8260D
3/5/20 15:11
TLB
P000102
Vinyl acetate
BRL
mg/kg dry
0.017
0.00091
1
*8260D
3/5/20 15:11
TLB
P000102
Vinyl chloride
BRL
mg/kg dry
0.017
0.0017
1
*8260D
3/5/20 15:11
TLB
P000102
Xylenes, total
BRL
mg/kg dry
0.025
0.0030
1
*8260D
3/5/20 15:11
TLB
P000102
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
92 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
25
5.0
100
*MADEP VPH
3/5/20 19:52
TBL
P000106
C9-C12 Aliphatics
BRL
mg/kg dry
25
2.2
100
*MADEP VPH
3/5/20 19:52
TBL
P000106
C9-Cl0 Aromatics
BRL
mg/kg dry
25
2.4
100
*MADEP VPH
3/5/20 19:52
TBL
P000106
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
111 %
70-130
2,5-Dibromotoluene (FID)
118 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waynt.�
03/10/2020
PA
ANALYTICAL
Hart & Hickman (Charlotte)
Project: WIT-019
Client Sample ID: UST-2 Sidewall-W
Attn: Matt Ingalls
Sample ID: 0030027-10
2923 South Tryon St. Ste 100
Work
Order: 0030027
Charlotte, NC 28203
Sample Matrix: Solid
Time
Collected: 03/02/20 14:30
Time
Submitted: 03/03/20 11:55
Parameter
Result Units
Report
MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
BRL
mg/kg dry
32
1.6
1
*MADEP EPH 3/7/20 7:35
ZRC
P000104
C19-C36 Aliphatics
BRL
mg/kg dry
32
5.4
1
*MADEP EPH 3/7/20 7:35
ZRC
P000104
C11-C22Aromatics
BRL
mg/kg dry
32
8.8
1
*MADEP EPH 3/7/20 7:35
ZRC
P000104
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
88 %
40-140
o-Terphenyl
89 %
40-140
2-Fluorobiphenyl
77 %
40-140
2-Bromonaphthalene
56 %
40-140
General Chemistry Parameters
% Solids
77.1
% by
0.100
0.100
1
*SM2540 G 316120 9:04
EDV
P000110
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.86
0.15
1
*8270E 3/5/20 22:47
JMV
P000087
1,2-Dichlorobenzene
BRL
mg/kg dry
0.86
0.14
1
*8270E 3/5/20 22:47
JMV
P000087
1,3-Dichlorobenzene
BRL
mg/kg dry
0.86
0.13
1
*8270E 3/5/20 22:47
JMV
P000087
1,4-Dichlorobenzene
BRL
mg/kg dry
0.43
0.13
1
*8270E 3/5/20 22:47
JMV
P000087
1-Methyl naphthalene
BRL
mg/kg dry
0.86
0.013
1
*8270E 3/5/20 22:47
JMV
P000087
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.86
0.18
1
*8270E 3/5/20 22:47
JMV
P000087
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.86
0.21
1
*8270E 3/5/20 22:47
JMV
P000087
2,4-Dichlorophenol
BRL
mg/kg dry
0.86
0.17
1
*8270E 3/5/20 22:47
JMV
P000087
2,4-Dimethylphenol
BRL
mg/kg dry
0.43
0.18
1
*8270E 3/5/20 22:47
JMV
P000087
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.50
1
*8270E 3/5/20 22:47
JMV
P000087
2,4-Dinitrotoluene
BRL
mg/kg dry
0.86
0.23
1
*8270E 3/5/20 22:47
JMV
P000087
2,6-Dinitrotoluene
BRL
mg/kg dry
0.86
0.22
1
*8270E 3/5/20 22:47
JMV
P000087
2-Chloronaphthalene
BRL
mg/kg dry
0.86
0.21
1
*8270E 3/5/20 22:47
JMV
P000087
2-Chlorophenol
BRL
mg/kg dry
0.86
0.16
1
*8270E 3/5/20 22:47
JMV
P000087
2-Methyl naphthalene
BRL
mg/kg dry
0.86
0.017
1
*8270E 3/5/20 22:47
JMV
P000087
2-Methylphenol
BRL
mg/kg dry
0.86
0.16
1
*8270E 3/5/20 22:47
JMV
P000087
2-Nitrophenol
BRL
mg/kg dry
0.86
0.14
1
*8270E 3/5/20 22:47
JMV
P000087
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.86
0.17
1
*8270E 3/5/20 22:47
JMV
P000087
3/4-Methyl phenol
BRL
mg/kg dry
0.86
0.19
1
*8270E 3/5/20 22:47
JMV
P000087
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.47
1
*8270E 3/5/20 22:47
JMV
P000087
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.86
0.20
1
*8270E 3/5/20 22:47
JMV
P000087
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.86
0.16
1
*8270E 3/5/20 22:47
JMV
P000087
4-Chloroaniline
BRL
mg/kg dry
0.43
0.10
1
*8270E 3/5/20 22:47
JMV
P000087
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
*8270E 3/5/20 22:47
JMV
P000087
4-Nitrophenol
BRL
mg/kg dry
0.86
0.21
1
*8270E 3/5/20 22:47
JMV
P000087
Acenaphthene
BRL
mg/kg dry
0.86
0.020
1
*8270E 3/5/20 22:47
JMV
P000087
Acenaphthylene
BRL
mg/kg dry
0.86
0.017
1
*8270E 3/5/20 22:47
JMV
P000087
Anthracene
BRL
mg/kg dry
0.86
0.0095
1
*8270E 3/5/20 22:47
JMV
P000087
Azobenzene
BRL
mg/kg dry
0.86
0.18
1
*8270E 3/5/20 22:47
JMV
P000087
Benzo(a)anthracene
BRL
mg/kg dry
0.86
0.010
1
*8270E 3/5/20 22:47
JMV
P000087
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-W
Attn: Matt Ingalls Sample ID: 0030027-10
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:30
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.86
0.0077
1
*8270E
3/5/20 22:47
JMV
P000087
Benzo(b)fluoranthene
BRL
mg/kg dry
0.86
0.0079
1
*8270E
3/5/20 22:47
JMV
P000087
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.86
0.0084
1
*8270E
3/5/20 22:47
JMV
P000087
Benzo(k)fluoranthene
BRL
mg/kg dry
0.86
0.0091
1
*8270E
3/5/20 22:47
JMV
P000087
Benzoic Acid
BRL
mg/kg dry
2.6
0.71
1
*8270E
3/5/20 22:47
JMV
P000087
Benzyl alcohol
BRL
mg/kg dry
0.86
0.16
1
*8270E
3/5/20 22:47
JMV
P000087
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.86
0.16
1
*8270E
3/5/20 22:47
JMV
P000087
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.86
0.14
1
*8270E
3/5/20 22:47
JMV
P000087
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 22:47
JMV
P000087
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.86
0.19
1
*8270E
3/5/20 22:47
JMV
P000087
Butyl benzyl phthalate
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/5/20 22:47
JMV
P000087
Chrysene
BRL
mg/kg dry
0.86
0.010
1
*8270E
3/5/20 22:47
JMV
P000087
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.86
0.025
1
*8270E
3/5/20 22:47
JMV
P000087
Dibenzofuran
BRL
mg/kg dry
0.86
0.23
1
*8270E
3/5/20 22:47
JMV
P000087
Diethyl phthalate
BRL
mg/kg dry
0.86
0.22
1
*8270E
3/5/20 22:47
JMV
P000087
Dimethyl phthalate
BRL
mg/kg dry
0.86
0.20
1
*8270E
3/5/20 22:47
JMV
P000087
Di-n-butyl phthalate
BRL
mg/kg dry
0.86
0.21
1
*8270E
3/5/20 22:47
JMV
P000087
Di-n-octyl phthalate
BRL
mg/kg dry
0.43
0.22
1
*8270E
3/5/20 22:47
JMV
P000087
Fluoranthene
BRL
mg/kg dry
0.86
0.0097
1
*8270E
3/5/20 22:47
JMV
P000087
Fluorene
BRL
mg/kg dry
0.86
0.015
1
*8270E
3/5/20 22:47
JMV
P000087
Hexachlorobenzene
BRL
mg/kg dry
0.86
0.19
1
*8270E
3/5/20 22:47
JMV
P000087
Hexachlorobutadiene
BRL
mg/kg dry
0.86
0.19
1
*8270E
3/5/20 22:47
JMV
P000087
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.86
0.29
1
*8270E
3/5/20 22:47
JMV
P000087
Hexachloroethane
BRL
mg/kg dry
0.86
0.13
1
*8270E
3/5/20 22:47
JMV
P000087
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.86
0.024
1
*8270E
3/5/20 22:47
JMV
P000087
Isophorone
BRL
mg/kg dry
0.86
0.18
1
*8270E
3/5/20 22:47
JMV
P000087
Naphthalene
BRL
mg/kg dry
0.86
0.018
1
*8270E
3/5/20 22:47
JMV
P000087
Nitrobenzene
BRL
mg/kg dry
0.43
0.18
1
*8270E
3/5/20 22:47
JMV
P000087
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.86
0.20
1
*8270E
3/5/20 22:47
JMV
P000087
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.86
0.23
1
*8270E
3/5/20 22:47
JMV
P000087
Pentachlorophenol
BRL
mg/kg dry
1.3
0.55
1
*8270E
3/5/20 22:47
JMV
P000087
Phenanthrene
BRL
mg/kg dry
0.86
0.0093
1
*8270E
3/5/20 22:47
JMV
P000087
Phenol
BRL
mg/kg dry
0.86
0.14
1
*8270E
3/5/20 22:47
JMV
P000087
Pyrene
BRL
mg/kg dry
0.86
0.012
1
*8270E
3/5/20 22:47
JMV
P000087
Pyridine
BRL
mg/kg dry
0.43
0.082
1
*8270E
3/5/20 22:47
JMV
P000087
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
90 %
39-132
2-Fluorobiphenyl
80 %
44-115
2-Fluorophenol
79 %
35-115
Nitrobenzene-d5
72 %
37-122
Phenol-d5
75 %
34-121
Terphenyl-d14
77 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-W
Attn: Matt Ingalls Sample ID: 0030027-10
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:30
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0061
0.00074
1
*8260D
3/5/20 15:41
TLB
P000102
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0061
0.00089
1
*8260D
3/5/20 15:41
TLB
P000102
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0061
0.00044
1
*8260D
3/5/20 15:41
TLB
P000102
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0061
0.00066
1
*8260D
3/5/20 15:41
TLB
P000102
1,1-Dichloroethane
BRL
mg/kg dry
0.0061
0.0011
1
*8260D
3/5/20 15:41
TLB
P000102
1,1-Dichloroethylene
BRL
mg/kg dry
0.0061
0.0011
1
*8260D
3/5/20 15:41
TLB
P000102
1,1-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00094
1
*8260D
3/5/20 15:41
TLB
P000102
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00087
1
*8260D
3/5/20 15:41
TLB
P000102
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0061
0.00069
1
*8260D
3/5/20 15:41
TLB
P000102
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.012
0.00058
1
*8260D
3/5/20 15:41
TLB
P000102
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0061
0.00064
1
*8260D
3/5/20 15:41
TLB
P000102
1,2-Dibromoethane
BRL
mg/kg dry
0.0061
0.00054
1
*8260D
3/5/20 15:41
TLB
P000102
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00068
1
*8260D
3/5/20 15:41
TLB
P000102
1,2-Dichloroethane
BRL
mg/kg dry
0.0061
0.00072
1
*8260D
3/5/20 15:41
TLB
P000102
1,2-Dichloropropane
BRL
mg/kg dry
0.0061
0.00091
1
*8260D
3/5/20 15:41
TLB
P000102
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0061
0.00076
1
*8260D
3/5/20 15:41
TLB
P000102
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00076
1
*8260D
3/5/20 15:41
TLB
P000102
1,3-Dichloropropane
BRL
mg/kg dry
0.0061
0.00051
1
*8260D
3/5/20 15:41
TLB
P000102
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0061
0.00077
1
*8260D
3/5/20 15:41
TLB
P000102
2,2-Dichloropropane
BRL
mg/kg dry
0.0061
0.00076
1
*8260D
3/5/20 15:41
TLB
P000102
2-Chlorotoluene
BRL
mg/kg dry
0.0061
0.00081
1
*8260D
3/5/20 15:41
TLB
P000102
4-Chlorotoluene
BRL
mg/kg dry
0.0061
0.00069
1
*8260D
3/5/20 15:41
TLB
P000102
4-Isopropyltoluene
BRL
mg/kg dry
0.0061
0.0015
1
*8260D
3/5/20 15:41
TLB
P000102
Acetone
BRL CCVH
mg/kg dry
0.024
0.0015
1
*8260D
3/5/20 15:41
TLB
P000102
Benzene
BRL
mg/kg dry
0.0061
0.00095
1
*8260D
3/5/20 15:41
TLB
P000102
Bromobenzene
BRL
mg/kg dry
0.0061
0.00084
1
*8260D
3/5/20 15:41
TLB
P000102
Bromochloromethane
BRL
mg/kg dry
0.0061
0.0010
1
*8260D
3/5/20 15:41
TLB
P000102
Bromodichloromethane
BRL
mg/kg dry
0.0061
0.00058
1
*8260D
3/5/20 15:41
TLB
P000102
Bromoform
BRL
mg/kg dry
0.0061
0.00047
1
*8260D
3/5/20 15:41
TLB
P000102
Bromomethane
BRL
mg/kg dry
0.012
0.0030
1
*8260D
3/5/20 15:41
TLB
P000102
Carbon Tetrachloride
BRL
mg/kg dry
0.0061
0.0012
1
*8260D
3/5/20 15:41
TLB
P000102
Chlorobenzene
BRL
mg/kg dry
0.0061
0.00095
1
*8260D
3/5/20 15:41
TLB
P000102
Chloroethane
BRL
mg/kg dry
0.012
0.0012
1
*8260D
3/5/20 15:41
TLB
P000102
Chloroform
BRL
mg/kg dry
0.0061
0.00074
1
*8260D
3/5/20 15:41
TLB
P000102
Chloromethane
BRL
mg/kg dry
0.012
0.0018
1
*8260D
3/5/20 15:41
TLB
P000102
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0061
0.00095
1
*8260D
3/5/20 15:41
TLB
P000102
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00060
1
*8260D
3/5/20 15:41
TLB
P000102
Dibromochloromethane
BRL
mg/kg dry
0.0061
0.00041
1
*8260D
3/5/20 15:41
TLB
P000102
Dichlorodifluoromethane
BRL
mg/kg dry
0.012
0.0017
1
*8260D
3/5/20 15:41
TLB
P000102
Ethylbenzene
BRL
mg/kg dry
0.0061
0.00091
1
*8260D
3/5/20 15:41
TLB
P000102
Isopropyl Ether
BRL
mg/kg dry
0.0061
0.00089
1
*8260D
3/5/20 15:41
TLB
P000102
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0061
0.00071
1
*8260D
3/5/20 15:41
TLB
P000102
m,p-Xylenes
BRL
mg/kg dry
0.012
0.0016
1
*8260D
3/5/20 15:41
TLB
P000102
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
S A i • .0 03/10/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall-W
Attn: Matt Ingalls Sample ID: 0030027-10
2923 South Tryon St. Ste 100 Work Order: 0030027
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/02/20 14:30
Time Submitted: 03/03/20 11:55
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.024
0.00042
1
*8260D
3/5/20 15:41
TLB
P000102
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.024
0.0014
1
*8260D
3/5/20 15:41
TLB
P000102
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.024
0.00050
1
*8260D
3/5/20 15:41
TLB
P000102
Methylene Chloride
BRL
mg/kg dry
0.0061
0.00098
1
*8260D
3/5/20 15:41
TLB
P000102
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0061
0.00085
1
*8260D
3/5/20 15:41
TLB
P000102
Naphthalene
BRL
mg/kg dry
0.012
0.00061
1
*8260D
3/5/20 15:41
TLB
P000102
n-Butylbenzene
BRL
mg/kg dry
0.0061
0.00057
1
*8260D
3/5/20 15:41
TLB
P000102
n-Propylbenzene
BRL
mg/kg dry
0.0061
0.00088
1
*8260D
3/5/20 15:41
TLB
P000102
o-Xylene
BRL
mg/kg dry
0.0061
0.00065
1
*8260D
3/5/20 15:41
TLB
P000102
sec-Butylbenzene
BRL
mg/kg dry
0.0061
0.00066
1
*8260D
3/5/20 15:41
TLB
P000102
Styrene
BRL
mg/kg dry
0.0061
0.00059
1
*8260D
3/5/20 15:41
TLB
P000102
tert-Butylbenzene
BRL
mg/kg dry
0.0061
0.00072
1
*8260D
3/5/20 15:41
TLB
P000102
Tetrachloroethylene
BRL
mg/kg dry
0.0061
0.0011
1
*8260D
3/5/20 15:41
TLB
P000102
Toluene
BRL
mg/kg dry
0.0061
0.00097
1
*8260D
3/5/20 15:41
TLB
P000102
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0061
0.0012
1
*8260D
3/5/20 15:41
TLB
P000102
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0061
0.00052
1
*8260D
3/5/20 15:41
TLB
P000102
Trichloroethylene
BRL
mg/kg dry
0.0061
0.0012
1
*8260D
3/5/20 15:41
TLB
P000102
Trichlorofluoromethane
BRL
mg/kg dry
0.012
0.0016
1
*8260D
3/5/20 15:41
TLB
P000102
Vinyl acetate
BRL
mg/kg dry
0.012
0.00066
1
*8260D
3/5/20 15:41
TLB
P000102
Vinyl chloride
BRL
mg/kg dry
0.012
0.0012
1
*8260D
3/5/20 15:41
TLB
P000102
Xylenes, total
BRL
mg/kg dry
0.018
0.0022
1
*8260D
3/5/20 15:41
TLB
P000102
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
102 %
70-130
Dibromofluoromethane
104 %
84-123
Toluene-d8
92 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
23
4.5
100
*MADEP VPH
3/5/20 20:21
TBL
P000106
C9-C12 Aliphatics
BRL
mg/kg dry
23
2.0
100
*MADEP VPH
3/5/20 20:21
TBL
P000106
C9-Cl0 Aromatics
BRL
mg/kg dry
23
2.2
100
*MADEP VPH
3/5/20 20:21
TBL
P000106
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
102 %
70-130
2,5-Dibromotoluene (FID)
108 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Way poi nt.
ANALYTICAL
Hart & Hickman (Charlotte)
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Parameter
Laboratory Report
03/10/2020
Project: WIT-019 Client Sample ID: Stockpile-1
Sample ID: 0030027-11
Work Order: 0030027
Sample Matrix: Solid Time Collected: 03/02/20 15:00
Time Submitted: 03/03/20 11:55
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL
mg/kg dry
9.0 3.0
1 *8015C 3/5/20 19:55
NMB P000089
Surrogate
Recovery
Control Limits
o-Terphenyl
91 %
31-123
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL
mg/kg dry
9.1 2.5
50 *8015C 3/5/20 18:14
TBL P000105
Surrogate
Recovery
Control Limits
a,a,a-Trifluorotoluene
117 %
50-137
General Chemistry Parameters
% Solids 78.0
% by
0.100 0.100
1 *SM2540 G 3/6/20 9:04
EDV P000110
Weight
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Way poi nt.
ANALYTICAL
Hart & Hickman (Charlotte)
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Parameter
Diesel Range Organics by GC/FID
Laboratory Report
03/10/2020
Project: WIT-019 Client Sample ID: Stockpile-2
Sample ID: 0030027-12
Work Order: 0030027
Sample Matrix: Solid Time Collected: 03/02/20 14:45
Time Submitted: 03/03/20 11:55
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics 860 mg/kg dry 91 30 10 *8015C 3/6/20 7:47 NMB P000089
Surrogate
Recovery Control Limits
Gasoline Range Organics by GC/FID
Gasoline Range Organics 410 mg/kg dry 78 21 500 *8015C 3/5/20 18:43 TBL P000105
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 77.3 % by 0.100 0.100 1 *SM2540 G 3/6/20 9:04 EDV P000110
Weight
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypo�nt.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000102 - 5035
Reporting
Result Limit Units
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P000102-BLK1)
Prepared & Analyzed: 03/05/20
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000102 - 5035
Reporting
Result Limit Units
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P000102-BLK1)
Prepared & Analyzed: 03/05/20
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
50.2
ug/L
50.00 100 70-130
Surrogate: Dibromofluoromethane
51.1
ug/L
50.00 102 84-123
Surrogate: Toluene-d8
46.1
ug/L
50.00 92 76-129
LCS (P000102-BSI)
Prepared &Analyzed: 03/05/20
1,1,1,2-Tetrachloroethane
0.0484
0.0050
mg/kg wet
0.05000
97
72-115
1, 1,1 -Trichloroethane
0.0488
0.0050
mg/kg wet
0.05000
98
67-131
1,1,2,2-Tetrachloroethane
0.0514
0.0050
mg/kg wet
0.05000
103
56-126
1,1,2-Trichloroethane
0.0484
0.0050
mg/kg wet
0.05000
97
70-133
1,1-Dichloroethane
0.0494
0.0050
mg/kg wet
0.05000
99
74-127
1,1-Dichloroethylene
0.0479
0.0050
mg/kg wet
0.05000
96
67-149
1, 1 -Dichloropropylene
0.0490
0.0050
mg/kg wet
0.05000
98
71-130
1,2,3-Trichlorobenzene
0.0480
0.010
mg/kg wet
0.05000
96
68-130
1,2,3-Trichloropropane
0.0490
0.0050
mg/kg wet
0.05000
98
60-137
1,2,4-Trichlorobenzene
0.0483
0.010
mg/kg wet
0.05000
97
66-125
1,2,4-Trimethylbenzene
0.0475
0.0050
mg/kg wet
0.05000
95
69-129
1,2-Dibromoethane
0.0502
0.0050
mg/kg wet
0.05000
100
70-132
1,2-Dichlorobenzene
0.0471
0.0050
mg/kg wet
0.05000
94
72-123
1,2-Dichloroethane
0.0491
0.0050
mg/kg wet
0.05000
98
68-128
1,2-Dichloropropane
0.0516
0.0050
mg/kg wet
0.05000
103
73-130
1,3,5-Trimethylbenzene
0.0471
0.0050
mg/kg wet
0.05000
94
69-128
1,3-Dichlorobenzene
0.0464
0.0050
mg/kg wet
0.05000
93
71-120
1,3-Dichloropropane
0.0483
0.0050
mg/kg wet
0.05000
97
75-124
1,4-Dichlorobenzene
0.0460
0.0050
mg/kg wet
0.05000
92
71-123
2,2-Dichloropropane
0.0495
0.0050
mg/kg wet
0.05000
99
50-142
2-Chlorotoluene
0.0468
0.0050
mg/kg wet
0.05000
94
67-124
4-Chlorotoluene
0.0468
0.0050
mg/kg wet
0.05000
94
71-126
4-Isopropyltoluene
0.0479
0.0050
mg/kg wet
0.05000
96
68-129
Acetone
0.116
0.020
mg/kg wet
0.1000
116
29-198
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000102 - 5035
Reporting
Result Limit Units
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P000102-BS1)
Prepared &Analyzed: 03/05/20
Benzene
0.0496
0.0050
mg/kg wet
0.05000
99
74-127
Bromobenzene
0.0463
0.0050
mg/kg wet
0.05000
93
73-125
Bromochloromethane
0.0517
0.0050
mg/kg wet
0.05000
103
72-134
Bromodichloromethane
0.0520
0.0050
mg/kg wet
0.05000
104
75-122
Bromoform
0.0469
0.0050
mg/kg wet
0.05000
94
66-135
Bromomethane
0.0528
0.010
mg/kg wet
0.05000
106
20-180
Carbon Tetrachloride
0.0485
0.0050
mg/kg wet
0.05000
97
64-143
Chlorobenzene
0.0466
0.0050
mg/kg wet
0.05000
93
74-118
Chloroethane
0.0398
0.010
mg/kg wet
0.05000
80
33-149
Chloroform
0.0500
0.0050
mg/kg wet
0.05000
100
73-127
Chloromethane
0.0465
0.010
mg/kg wet
0.05000
93
45-143
cis-1,2-Dichloroethylene
0.0502
0.0050
mg/kg wet
0.05000
100
76-134
cis-1,3-Dichloropropylene
0.0533
0.0050
mg/kg wet
0.05000
107
71-125
Dibromochloromethane
0.0506
0.0050
mg/kg wet
0.05000
101
73-122
Dichlorodifluoromethane
0.0469
0.010
mg/kg wet
0.05000
94
26-146
Ethylbenzene
0.0460
0.0050
mg/kg wet
0.05000
92
74-128
Isopropyl Ether
0.0525
0.0050
mg/kg wet
0.05000
105
59-159
Isopropylbenzene (Cumene)
0.0471
0.0050
mg/kg wet
0.05000
94
68-126
m,p-Xylenes
0.0941
0.010
mg/kg wet
0.1000
94
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0573
0.020
mg/kg wet
0.05000
115
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0569
0.020
mg/kg wet
0.05000
114
63-149
Methyl Isobutyl Ketone
0.0573
0.020
mg/kg wet
0.05000
115
57-162
Methylene Chloride
0.0474
0.0050
mg/kg wet
0.05000
95
74-129
Methyl-tert-Butyl Ether
0.0540
0.0050
mg/kg wet
0.05000
108
70-130
Naphthalene
0.0503
0.010
mg/kg wet
0.05000
101
57-157
n-Butylbenzene
0.0476
0.0050
mg/kg wet
0.05000
95
65-135
n-Propylbenzene
0.0466
0.0050
mg/kg wet
0.05000
93
67-130
o-Xylene
0.0478
0.0050
mg/kg wet
0.05000
96
74-126
sec-Butylbenzene
0.0468
0.0050
mg/kg wet
0.05000
94
66-131
Styrene
0.0508
0.0050
mg/kg wet
0.05000
102
77-121
tert-Butyl benzene
0.0472
0.0050
mg/kg wet
0.05000
94
67-132
Tetrachloroethylene
0.0496
0.0050
mg/kg wet
0.05000
99
68-130
Toluene
0.0498
0.0050
mg/kg wet
0.05000
100
71-129
trans- 1,2-Dichloroethylene
0.0491
0.0050
mg/kg wet
0.05000
98
73-132
trans- 1,3-Dichloropropylene
0.0533
0.0050
mg/kg wet
0.05000
107
68-123
Trichloroethylene
0.0484
0.0050
mg/kg wet
0.05000
97
75-133
Trichlorofluoromethane
0.0464
0.010
mg/kg wet
0.05000
93
44-146
Vinyl acetate
0.0786
0.010
mg/kg wet
0.05000
157
85-161
Vinyl chloride
0.0496
0.010
mg/kg wet
0.05000
99
48-147
Xylenes, total
0.142
0.015
mg/kg wet
0.1500
95
74-126
Surrogate:4-Bromofluorobenzene
50.4
ug/L
50.00
101
70-130
Surrogate: Dibromofluoromethane
50.8
ug/L
50.00
102
84-123
Surrogate: Toluene-d8
46.9
ug/L
50.00
94
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000102 - 5035
Reporting
Result Limit Units
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (P000102-MS1)
Source: 0030027-02
Prepared &Analyzed: 03/05/20
1,1,1,2-Tetrachloroethane
0.0508
0.0065
mg/kg dry
0.06499
BRL
78
60-120
1,1,1-Trichloroethane
0.0533
0.0065
mg/kg dry
0.06499
BRL
82
52-139
1,1,2,2-Tetrachloroethane
0.0500
0.0065
mg/kg dry
0.06499
BRL
77
39-135
1,1,2-Trichloroethane
0.0499
0.0065
mg/kg dry
0.06499
BRL
77
44-140
1,1-Dichloroethane
0.0545
0.0065
mg/kg dry
0.06499
BRL
84
59-137
1,1-Dichloroethylene
0.0514
0.0065
mg/kg dry
0.06499
BRL
79
54-162
1, 1 -Dichloropropylene
0.0530
0.0065
mg/kg dry
0.06499
BRL
82
55-137
1,2,3-Trichlorobenzene
0.0435
0.013
mg/kg dry
0.06499
BRL
67
34-120
1,2,3-Trichloropropane
0.0482
0.0065
mg/kg dry
0.06499
BRL
74
45-139
1,2,4-Trichlorobenzene
0.0419
0.013
mg/kg dry
0.06499
BRL
64
35-116
1,2,4-Trimethylbenzene
0.0457
0.0065
mg/kg dry
0.06499
BRL
70
38-142
1,2-Dibromoethane
0.0507
0.0065
mg/kg dry
0.06499
BRL
78
49-132
1,2-Dichlorobenzene
0.0455
0.0065
mg/kg dry
0.06499
BRL
70
42-130
1,2-Dichloroethane
0.0496
0.0065
mg/kg dry
0.06499
BRL
76
51-131
1,2-Dichloropropane
0.0542
0.0065
mg/kg dry
0.06499
BRL
83
55-138
1,3,5-Trimethylbenzene
0.0472
0.0065
mg/kg dry
0.06499
BRL
73
44-140
1,3-Dichlorobenzene
0.0438
0.0065
mg/kg dry
0.06499
BRL
67
41-129
1,3-Dichloropropane
0.0490
0.0065
mg/kg dry
0.06499
BRL
75
53-129
1,4-Dichlorobenzene
0.0434
0.0065
mg/kg dry
0.06499
BRL
67
44-134
2,2-Dichloropropane
0.0518
0.0065
mg/kg dry
0.06499
BRL
80
30-147
2-Chlorotoluene
0.0452
0.0065
mg/kg dry
0.06499
BRL
70
46-132
4-Chlorotoluene
0.0452
0.0065
mg/kg dry
0.06499
BRL
70
44-135
4-Isopropyltoluene
0.0452
0.0065
mg/kg dry
0.06499
BRL
70
32-144
Acetone
0.0648
0.026
mg/kg dry
0.1300
0.00630
45
34-143
Benzene
0.0528
0.0065
mg/kg dry
0.06499
BRL
81
60-135
Bromobenzene
0.0453
0.0065
mg/kg dry
0.06499
BRL
70
45-135
Bromochloromethane
0.0537
0.0065
mg/kg dry
0.06499
BRL
83
55-136
Bromodichloromethane
0.0533
0.0065
mg/kg dry
0.06499
BRL
82
55-127
Bromoform
0.0464
0.0065
mg/kg dry
0.06499
BRL
71
40-136
Bromomethane
0.0476
0.013
mg/kg dry
0.06499
BRL
73
30-137
Carbon Tetrachloride
0.0511
0.0065
mg/kg dry
0.06499
BRL
79
48-153
Chlorobenzene
0.0474
0.0065
mg/kg dry
0.06499
BRL
73
57-125
Chloroethane
0.0430
0.013
mg/kg dry
0.06499
BRL
66
16-177
Chloroform
0.0543
0.0065
mg/kg dry
0.06499
BRL
84
56-137
Chloromethane
0.0478
0.013
mg/kg dry
0.06499
BRL
74
40-145
cis-1,2-Dichloroethylene
0.0524
0.0065
mg/kg dry
0.06499
BRL
81
58-140
cis-1,3-Dichloropropylene
0.0531
0.0065
mg/kg dry
0.06499
BRL
82
42-135
Dibromochloromethane
0.0506
0.0065
mg/kg dry
0.06499
BRL
78
49-127
Dichlorodifluoromethane
0.0324
0.013
mg/kg dry
0.06499
BRL
50
25-151
Ethylbenzene
0.0478
0.0065
mg/kg dry
0.06499
BRL
74
44-144
Isopropyl Ether
0.0534
0.0065
mg/kg dry
0.06499
BRL
82
51-155
Isopropylbenzene (Cumene)
0.0472
0.0065
mg/kg dry
0.06499
BRL
73
41-140
m,p-Xylenes
0.0970
0.013
mg/kg dry
0.1300
BRL
75
36-148
Methyl Butyl Ketone (2-Hexanone)
0.0462
0.026
mg/kg dry
0.06499
BRL
71
30-147
Methyl Ethyl Ketone (2-Butanone)
0.0418
0.026
mg/kg dry
0.06499
BRL
64
24-160
Methyl Isobutyl Ketone
0.0564
0.026
mg/kg dry
0.06499
BRL
87
25-163
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000102 - 5035
Reporting
Result Limit Units
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (P000102-MS1)
Source: 0030027-02
Prepared &Analyzed: 03/05/20
Methylene Chloride
0.0600
0.0065
mg/kg dry
0.06499
0.00334
87
53-144
Methyl-tert-Butyl Ether
0.0529
0.0065
mg/kg dry
0.06499
BRL
81
49-135
Naphthalene
0.0487
0.013
mg/kg dry
0.06499
0.00185
72
32-127
n-Butylbenzene
0.0426
0.0065
mg/kg dry
0.06499
BRL
66
23-148
n-Propylbenzene
0.0447
0.0065
mg/kg dry
0.06499
BRL
69
35-144
o-Xylene
0.0483
0.0065
mg/kg dry
0.06499
BRL
74
43-143
sec-Butylbenzene
0.0445
0.0065
mg/kg dry
0.06499
BRL
69
34-144
Styrene
0.0508
0.0065
mg/kg dry
0.06499
BRL
78
42-132
tert-Butyl benzene
0.0461
0.0065
mg/kg dry
0.06499
BRL
71
36-150
Tetrachloroethylene
0.0519
0.0065
mg/kg dry
0.06499
BRL
80
47-142
Toluene
0.0532
0.0065
mg/kg dry
0.06499
0.00231
78
57-135
trans- 1,2-Dichloroethylene
0.0518
0.0065
mg/kg dry
0.06499
BRL
80
58-141
trans- 1,3-Dichloropropylene
0.0535
0.0065
mg/kg dry
0.06499
BRL
82
41-124
Trichloroethylene
0.0498
0.0065
mg/kg dry
0.06499
BRL
77
38-164
Trichlorofluoromethane
0.0474
0.013
mg/kg dry
0.06499
BRL
73
30-157
Vinyl acetate
0.0292
0.013
mg/kg dry
0.06499
BRL
45
61-154
Vinyl chloride
0.0497
0.013
mg/kg dry
0.06499
BRL
77
40-156
Xylenes, total
0.145
0.019
mg/kg dry
0.1950
BRL
75
36-148
Surrogate:4-Bromofluorobenzene
50.2
ug/L
50.00
100
70-130
Surrogate: Dibromofluoromethane
51.3
ug/L
50.00
103
84-123
Surrogate: Toluene-d8
46.1
ug/L
50.00
92
76-129
Matrix Spike Dup (P000102-MSD1)
Source: 0030027-02
Prepared & Analyzed: 03/05/20
1,1,1,2-Tetrachloroethane
0.0497
0.0065
mg/kg dry
0.06499
BRL
76
60-120
2
15
1,1,1-Trichloroethane
0.0510
0.0065
mg/kg dry
0.06499
BRL
78
52-139
4
21
1,1,2,2-Tetrachloroethane
0.0486
0.0065
mg/kg dry
0.06499
BRL
75
39-135
3
22
1,1,2-Trichloroethane
0.0486
0.0065
mg/kg dry
0.06499
BRL
75
44-140
3
21
1,1-Dichloroethane
0.0531
0.0065
mg/kg dry
0.06499
BRL
82
59-137
3
21
1,1-Dichloroethylene
0.0505
0.0065
mg/kg dry
0.06499
BRL
78
54-162
2
22
1, 1 -Dichloropropylene
0.0519
0.0065
mg/kg dry
0.06499
BRL
80
55-137
2
19
1,2,3-Trichlorobenzene
0.0445
0.013
mg/kg dry
0.06499
BRL
68
34-120
2
41
1,2,3-Trichloropropane
0.0468
0.0065
mg/kg dry
0.06499
BRL
72
45-139
3
25
1,2,4-Trichlorobenzene
0.0424
0.013
mg/kg dry
0.06499
BRL
65
35-116
1
62
1,2,4-Trimethylbenzene
0.0453
0.0065
mg/kg dry
0.06499
BRL
70
38-142
0.9
24
1,2-Dibromoethane
0.0496
0.0065
mg/kg dry
0.06499
BRL
76
49-132
2
15
1,2-Dichlorobenzene
0.0451
0.0065
mg/kg dry
0.06499
BRL
69
42-130
0.9
21
1,2-Dichloroethane
0.0484
0.0065
mg/kg dry
0.06499
BRL
74
51-131
3
13
1,2-Dichloropropane
0.0528
0.0065
mg/kg dry
0.06499
BRL
81
55-138
3
16
1,3,5-Trimethylbenzene
0.0470
0.0065
mg/kg dry
0.06499
BRL
72
44-140
0.4
29
1,3-Dichlorobenzene
0.0436
0.0065
mg/kg dry
0.06499
BRL
67
41-129
0.6
24
1,3-Dichloropropane
0.0479
0.0065
mg/kg dry
0.06499
BRL
74
53-129
2
15
1,4-Dichlorobenzene
0.0433
0.0065
mg/kg dry
0.06499
BRL
67
44-134
0.03
21
2,2-Dichloropropane
0.0507
0.0065
mg/kg dry
0.06499
BRL
78
30-147
2
20
2-Chlorotoluene
0.0446
0.0065
mg/kg dry
0.06499
BRL
69
46-132
1
29
4-Chlorotoluene
0.0446
0.0065
mg/kg dry
0.06499
BRL
69
44-135
1
23
4-Isopropyltoluene
0.0452
0.0065
mg/kg dry
0.06499
BRL
70
32-144
0.06
22
Acetone
0.0608
0.026
mg/kg dry
0.1300
0.00630
42
34-143
6
49
IN
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000102 - 5035
Reporting
Result Limit Units
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P000102-MSD1)
Source: 0030027-02
Prepared &Analyzed: 03/05/20
Benzene
0.0515
0.0065
mg/kg dry
0.06499
BRL
79
60-135
2
20
Bromobenzene
0.0458
0.0065
mg/kg dry
0.06499
BRL
70
45-135
1
25
Bromochloromethane
0.0535
0.0065
mg/kg dry
0.06499
BRL
82
55-136
0.4
18
Bromodichloromethane
0.0519
0.0065
mg/kg dry
0.06499
BRL
80
55-127
3
17
Bromoform
0.0457
0.0065
mg/kg dry
0.06499
BRL
70
40-136
1
35
Bromomethane
0.0465
0.013
mg/kg dry
0.06499
BRL
72
30-137
2
30
Carbon Tetrachloride
0.0501
0.0065
mg/kg dry
0.06499
BRL
77
48-153
2
23
Chlorobenzene
0.0466
0.0065
mg/kg dry
0.06499
BRL
72
57-125
2
14
Chloroethane
0.0434
0.013
mg/kg dry
0.06499
BRL
67
16-177
0.9
47
Chloroform
0.0529
0.0065
mg/kg dry
0.06499
BRL
81
56-137
3
18
Chloromethane
0.0469
0.013
mg/kg dry
0.06499
BRL
72
40-145
2
26
cis-1,2-Dichloroethylene
0.0510
0.0065
mg/kg dry
0.06499
BRL
79
58-140
3
28
cis-1,3-Dichloropropylene
0.0518
0.0065
mg/kg dry
0.06499
BRL
80
42-135
2
32
Dibromochloromethane
0.0489
0.0065
mg/kg dry
0.06499
BRL
75
49-127
3
24
Dichlorodifluoromethane
0.0313
0.013
mg/kg dry
0.06499
BRL
48
25-151
3
37
Ethylbenzene
0.0466
0.0065
mg/kg dry
0.06499
BRL
72
44-144
3
19
Isopropyl Ether
0.0519
0.0065
mg/kg dry
0.06499
BRL
80
51-155
3
13
Isopropylbenzene (Cumene)
0.0470
0.0065
mg/kg dry
0.06499
BRL
72
41-140
0.4
27
m,p-Xylenes
0.0947
0.013
mg/kg dry
0.1300
BRL
73
36-148
2
20
Methyl Butyl Ketone (2-Hexanone)
0.0435
0.026
mg/kg dry
0.06499
BRL
67
30-147
6
42
Methyl Ethyl Ketone (2-Butanone)
0.0387
0.026
mg/kg dry
0.06499
BRL
60
24-160
8
42
Methyl Isobutyl Ketone
0.0532
0.026
mg/kg dry
0.06499
BRL
82
25-163
6
44
Methylene Chloride
0.0558
0.0065
mg/kg dry
0.06499
0.00334
81
53-144
7
14
Methyl-tert-Butyl Ether
0.0513
0.0065
mg/kg dry
0.06499
BRL
79
49-135
3
22
Naphthalene
0.0479
0.013
mg/kg dry
0.06499
0.00185
71
32-127
2
44
n-Butylbenzene
0.0431
0.0065
mg/kg dry
0.06499
BRL
66
23-148
1
39
n-Propylbenzene
0.0448
0.0065
mg/kg dry
0.06499
BRL
69
35-144
0.2
27
o-Xylene
0.0474
0.0065
mg/kg dry
0.06499
BRL
73
43-143
2
17
sec-Butylbenzene
0.0445
0.0065
mg/kg dry
0.06499
BRL
69
34-144
0.06
28
Styrene
0.0496
0.0065
mg/kg dry
0.06499
BRL
76
42-132
2
28
tert-Butyl benzene
0.0459
0.0065
mg/kg dry
0.06499
BRL
71
36-150
0.5
29
Tetrachloroethylene
0.0506
0.0065
mg/kg dry
0.06499
BRL
78
47-142
3
26
Toluene
0.0520
0.0065
mg/kg dry
0.06499
0.00231
76
57-135
2
22
trans- 1,2-Dichloroethylene
0.0510
0.0065
mg/kg dry
0.06499
BRL
78
58-141
2
18
trans- 1,3-Dichloropropylene
0.0526
0.0065
mg/kg dry
0.06499
BRL
81
41-124
2
20
Trichloroethylene
0.0490
0.0065
mg/kg dry
0.06499
BRL
75
38-164
2
18
Trichlorofluoromethane
0.0460
0.013
mg/kg dry
0.06499
BRL
71
30-157
3
27
Vinyl acetate
0.0358
0.013
mg/kg dry
0.06499
BRL
55
61-154
20
35
Vinyl chloride
0.0484
0.013
mg/kg dry
0.06499
BRL
75
40-156
3
35
Xylenes, total
0.142
0.019
mg/kg dry
0.1950
BRL
73
36-148
2
20
Surrogate:4-Bromofluorobenzene
50.5
ug/L
50.00
101
70-130
Surrogate: Dibromofluoromethane
51.3
ug/L
50.00
103
84-123
Surrogate: Toluene-d8
46.2
ug/L
50.00
92
76-129
M
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P000087 - 3546
Blank (P000087-BLK1)
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methyl naphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methyl naphthalene
2-Methylphenol
2-Nitrophenol
3,3'-Dichlorobenzidine
3/4-Methyl phenol
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-C h loro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
B is(2-Ch loroethyl )ether
Bis(2-chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
1.5 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
1.5 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
1.0 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
2.0 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
Prepared: 03/04/20 Analyzed: 03/05/20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000087 - 3546
Reporting
Result Limit Units
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P000087-BLK1)
Prepared: 03/04/20 Analyzed: 03/05/20
Di-n-butyl phthalate
BRL
0.66
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
Fluoranthene
BRL
0.66
mg/kg wet
Fluorene
BRL
0.66
mg/kg wet
Hexachlorobenzene
BRL
0.66
mg/kg wet
Hexachlorobutadiene
BRL
0.66
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.66
mg/kg wet
Hexachloroethane
BRL
0.66
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.66
mg/kg wet
Isophorone
BRL
0.66
mg/kg wet
Naphthalene
BRL
0.66
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.66
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.66
mg/kg wet
Pentachlorophenol
BRL
1.0
mg/kg wet
Phenanthrene
BRL
0.66
mg/kg wet
Phenol
BRL
0.66
mg/kg wet
Pyrene
BRL
0.66
mg/kg wet
Pyridine
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
2.74
mg/kg wet
3.333
82
39-132
Surrogate: 2-Fluorobiphenyl
1.26
mg/kg wet
1.667
76
44-115
Surrogate: 2-Fluorophenol
2.74
mg/kg wet
3.333
82
35-115
Surrogate: Nitrobenzene-d5
1.12
mg/kg wet
1.667
67
37-122
Surrogate: Phenol-d5
2.66
mg/kg wet
3.333
80
34-121
Surrogate: Terphenyl-04
1.24
mg/kg wet
1.667
74
54-127
LCS (P000087-BS1)
Prepared: 03/04/20 Analyzed: 03/05/20
1,2,4-Trichlorobenzene
1.07
0.66
mg/kg wet
1.667
64
34-118
1,2-Dichlorobenzene
1.16
0.66
mg/kg wet
1.667
69
33-117
1,3-Dichlorobenzene
1.14
0.66
mg/kg wet
1.667
69
30-115
1,4-Dichlorobenzene
1.12
0.33
mg/kg wet
1.667
67
31-115
1-Methyl naphthalene
1.23
0.66
mg/kg wet
1.667
74
40-119
2,4,5-Trichlorophenol
1.26
0.66
mg/kg wet
1.667
76
62-124
2,4,6-Trichlorophenol
1.34
0.66
mg/kg wet
1.667
80
39-126
2,4-Dichlorophenol
1.17
0.66
mg/kg wet
1.667
70
40-122
2,4-Dimethylphenol
1.33
0.33
mg/kg wet
1.667
80
30-127
2,4-Dinitrophenol
0.847
1.5
mg/kg wet
1.667
51
27-129
2,4-Dinitrotoluene
1.37
0.66
mg/kg wet
1.667
82
48-126
2,6-Dinitrotoluene
1.31
0.66
mg/kg wet
1.667
78
46-124
2-Chloronaphthalene
1.20
0.66
mg/kg wet
1.667
72
41-114
2-Chlorophenol
1.24
0.66
mg/kg wet
1.667
74
34-121
2-Methyl naphthalene
1.17
0.66
mg/kg wet
1.667
70
38-122
2-Methylphenol
1.31
0.66
mg/kg wet
1.667
78
32-122
2-Nitrophenol
1.12
0.66
mg/kg wet
1.667
67
36-123
3,3'-Dichlorobenzidine
1.31
0.66
mg/kg wet
1.667
78
22-121
3/4-Methyl phenol
1.20
0.66
mg/kg wet
1.667
72
34-119
4,6-Dinitro-2-methylphenol
1.10
1.5
mg/kg wet
1.667
66
29-132
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P000087 - 3546
LCS (P000087-BSI)
4-Bromophenyl phenyl ether
4-C h loro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
B i s(2-Ch loroethyl )ether
Bis(2-chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Chrysene
Dibenzo(a, h )anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-N itroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Surrogate: 2, 4, 6-Tribromophenol
Prepared: 03/04/20 Analyzed: 03/05/20
1.26
0.66
mg/kg wet
1.667
76
46-124
1.18
0.66
mg/kg wet
1.667
71
45-122
0.974
0.33
mg/kg wet
1.667
58
17-106
1.24
1.0
mg/kg wet
1.667
74
45-121
1.44
0.66
mg/kg wet
1.667
86
30-132
1.30
0.66
mg/kg wet
1.667
78
40-123
1.39
0.66
mg/kg wet
1.667
84
32-132
1.34
0.66
mg/kg wet
1.667
80
47-123
1.33
0.66
mg/kg wet
1.667
80
39-125
1.28
0.66
mg/kg wet
1.667
77
49-126
1.36
0.66
mg/kg wet
1.667
81
45-129
1.32
0.66
mg/kg wet
1.667
79
45-132
1.35
0.66
mg/kg wet
1.667
81
43-134
1.31
0.66
mg/kg wet
1.667
79
47-132
0.755
2.0
mg/kg wet
1.667
45
10-83
1.24
0.66
mg/kg wet
1.667
74
29-122
1.06
0.66
mg/kg wet
1.667
63
36-121
0.969
0.66
mg/kg wet
1.667
58
31-120
1.05
0.33
mg/kg wet
1.667
63
33-131
1.33
0.66
mg/kg wet
1.667
80
51-133
1.30
0.33
mg/kg wet
1.667
78
48-132
1.28
0.66
mg/kg wet
1.667
77
50-124
0.848
0.66
mg/kg wet
1.667
51
45-134
1.31
0.66
mg/kg wet
1.667
78
44-120
1.22
0.66
mg/kg wet
1.667
73
50-124
1.14
0.66
mg/kg wet
1.667
68
48-124
1.33
0.66
mg/kg wet
1.667
80
51-128
1.46
0.33
mg/kg wet
1.667
87
45-140
1.32
0.66
mg/kg wet
1.667
79
50-127
1.27
0.66
mg/kg wet
1.667
76
43-125
1.25
0.66
mg/kg wet
1.667
75
45-122
1.10
0.66
mg/kg wet
1.667
66
32-123
0.922
0.66
mg/kg wet
1.667
55
32-117
1.07
0.66
mg/kg wet
1.667
64
28-117
1.49
0.66
mg/kg wet
1.667
90
45-133
0.897
0.66
mg/kg wet
1.667
54
30-122
1.11
0.66
mg/kg wet
1.667
67
35-123
0.956
0.33
mg/kg wet
1.667
57
34-122
1.20
0.66
mg/kg wet
1.667
72
36-120
1.60
0.66
mg/kg wet
1.667
96
38-127
1.35
1.0
mg/kg wet
1.667
81
25-133
1.32
0.66
mg/kg wet
1.667
79
50-121
1.24
0.66
mg/kg wet
1.667
74
34-121
1.39
0.66
mg/kg wet
1.667
83
47-127
0.853
0.33
mg/kg wet
1.667
51
10-60
2.62
mg/kg wet
3.333
79
39-132
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting
Analyte Result Limit Units
Batch P000087 - 3546
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P000087-BSI)
Prepared: 03/04/20 Analyzed: 03/05/20
Surrogate: 2-Fluorobiphenyl
1.19
mg/kg wet
1.667
71
44-115
Surrogate: 2-Fluorophenol
2.54
mg/kg wet
3.333
76
35-115
Surrogate: Nitrobenzene-d5
1.01
mg/kg wet
1.667
61
37-122
Surrogate: Phenol-d5
2.44
mg/kg wet
3.333
73
34-121
Surrogate: Terphenyl-d14
1.32
mg/kg wet
1.667
79
54-127
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P000106 - MADEP VPH (S)
Blank (P000106-BLK1)
Prepared & Analyzed: 03/05/20
C5-C8 Aliphatics
BRL
5.0
mg/kg wet
C9-C12 Aliphatics
BRL
5.0
mg/kg wet
C9-Cl0 Aromatics
BRL
5.0
mg/kg wet
Surrogate: 2,5-Dibromotoluene (PID)
9810
ug/L
10000 98
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10400
ug/L
10000 104
70-130
LCS (P000106-BS1)
Prepared &Analyzed: 03/05/20
C5-C8 Aliphatics
29.8
5.0
mg/kg wet
32.00 93
70-130
C9-Cl0 Aromatics
9.72
5.0
mg/kg wet
10.67 91
70-130
C9-C12 Aliphatic
31.6
5.0
mg/kg wet
32.00 99
70-130
Surrogate: 2,5-Dibromotoluene (PID)
10000
ug/L
10000 100
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10800
ug/L
10000 108
70-130
1-CS Dup (P000106-13SD1)
Prepared & Analyzed: 03/05/20
C5-C8 Aliphatics
30.7
5.0
mg/kg wet
32.00 96
70-130 3 50
C9-Cl0 Aromatics
9.73
5.0
mg/kg wet
10.67 91
70-130 0.04 50
C9-C12 Aliphatic
31.2
5.0
mg/kg wet
32.00 98
70-130 1 50
Surrogate: 2,5-Dibromotoluene (PID)
9810
ug/L
10000 98
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10600
ug/L
10000 106
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Gasoline Range Organics by GC/FID - Quality Control
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P000105 - 5030B
Blank (P000105-BLK1) Prepared & Analyzed: 03/05/20
Gasoline Range Organics BRL 5.0 mg/kg wet
Surrogate: a,a,a-Trifluorotoluene 4.25 mg/kg wet 5.000 85 50-137
LCS (P000105-BS1) Prepared &Analyzed: 03/05/20
Gasoline Range Organics 60.7 5.0 mg/kg wet 50.00 121 41-138
Surrogate: a,a,a-Trifluorotoluene 4.60 mg/kg wet 5.000 92 50-137
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P000104 - 3546
Blank (P000104-BLK1)
Prepared: 03/05/20 Analyzed: 03/06/20
C9-C18 Aliphatics
BRL
25
mg/kg wet
C19-C36 Aliphatics
BRL
25
mg/kg wet
C1 1-C22 Aromatics
BRL
25
mg/kg wet
Surrogate: 1-Chlorooctadecane
1.23
mg/kg wet
2.000
61
40-140
Surrogate: o-Terphenyl
1.27
mg/kg wet
2.000
63
40-140
Surrogate: 2-Fluorobiphenyl
2.81
mg/kg wet
4.000
70
40-140
Surrogate: 2-Bromonaphthalene
2.80
mg/kg wet
4.000
70
40-140
LCS (P000104-BSI)
Prepared: 03/05/20
Analyzed: 03/06/20
C9-C18 Aliphatics
39.7
25
mg/kg wet
60.00
66
40-140
C19-C36 Aliphatics
69.8
25
mg/kg wet
80.00
87
40-140
C11-C22 Aromatics
145
25
mg/kg wet
170.0
85
40-140
Surrogate: 1-Chlorooctadecane
1.56
mg/kg wet
2.000
78
40-140
Surrogate: o-Terphenyl
1.60
mg/kg wet
2.000
80
40-140
Surrogate: 2-Fluorobiphenyl
2.92
mg/kg wet
4.000
73
40-140
Surrogate: 2-Bromonaphthalene
2.04
mg/kg wet
4.000
51
40-140
Matrix Spike (P000104-MS1)
Source: 0030027-01
Prepared: 03/05/20
Analyzed: 03/06/20
C9-Cl8 Aliphatics
54.6
31
mg/kg dry
75.44 3.67
68
40-140
C19-C36 Aliphatics
90.0
31
mg/kg dry
100.6 BRL
90
40-140
C11-C22 Aromatics
175
31
mg/kg dry
213.7 BRL
82
40-140
Surrogate: 1-Chlorooctadecane
1.74
mg/kg dry
2.515
69
40-140
Surrogate: o-Terphenyl
1.78
mg/kg dry
2.515
71
40-140
Surrogate: 2-Fluorobiphenyl
4.09
mg/kg dry
5.029
81
40-140
Surrogate: 2-Bromonaphthalene
2.89
mg/kg dry
5.029
57
40-140
Matrix Spike Dup (P000104-MSD1)
Source: 0030027-01
Prepared: 03/05/20
Analyzed: 03/06/20
C9-C18 Aliphatics
64.6
31
mg/kg dry
74.70 3.67
82
40-140 17 50
C19-C36 Aliphatics
105
31
mg/kg dry
99.60 BRL
105
40-140 15 50
C11-C22 Aromatics
205
31
mg/kg dry
211.7 BRL
97
40-140 16 50
Surrogate: 1-Chlorooctadecane
1.99
mg/kg dry
2.490
80
40-140
Surrogate: o-Terphenyl
2.11
mg/kg dry
2.490
85
40-140
Surrogate: 2-Fluorobiphenyl
4.06
mg/kg dry
4.980
81
40-140
Surrogate: 2-Bromonaphthalene
3.50
mg/kg dry
4.980
70
40-140
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Diesel Range Organics by GC/FID - Quality Control
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P000089 - 3546
Blank (P000089-BLK1)
Prepared: 03/04/20 Analyzed: 03/05/20
Diesel Range Organics
BRL 7.0 mg/kg wet
Surrogate: o-Terphenyl
1.12 mg/kg wet
1.333 84 31-123
LCS (P000089-BS1)
Prepared: 03/04/20 Analyzed: 03/05/20
Diesel Range Organics
57.1 7.0 mg/kg wet
66.67 86 46-126
Surrogate: o-Terphenyl
1.11 mg/kg wet
1.333 83 31-123
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
General Chemistry Parameters - Quality Control
Level II QC Report
3/10/20
Work Order: 0030027
Time Submitted: 3/3/2020 11:55:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P000098 - Solids, Dry Weight
Duplicate (P000098-DUP2) Source: 0030027-02 Prepared: 03/05/20 Analyzed: 03/06/20
% Solids 76.9 0.100 % by Weight 76.9 0.07 20
Batch P000110 - Solids, Dry Weight
Duplicate (P000110-DUP1) Source: 0030027-08 Prepared: 03/05/20 Analyzed: 03/06/20
% Solids 77.9 0.100 % by Weight 77.4 0.6 20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Extraction Data
Prep Method: 3546
Lab Number Batch Initial Final Date/Time
0030027-11 P000089 29.97 g 1 mL 03/04/20 15:45
0030027-12 P000089 29.99 g 1 mL 03/04/20 15:45
Prep Method: 3546
Lab Number Batch Initial Final Date/Time
0030027-01
P000104
10.07
g
2 mL
03/05/20 10:45
0030027-02
P000104
10.17
g
2 mL
03/05/20 10:45
0030027-03
P000104
10.03
g
2 mL
03/05/20 10:45
0030027-04
P000104
10.05
g
2 mL
03/05/20 10:45
0030027-05
P000104
10.02
g
2 mL
03/05/20 10:45
0030027-06
P000104
10.14
g
2 mL
03/05/20 10:45
0030027-07
P000104
10.1
g
2 mL
03/05/20 10:45
0030027-08
P000104
10.19
g
2 mL
03/05/20 10:45
0030027-09
P000104
10.31
g
2 mL
03/05/20 10:45
0030027-10
P000104
10.09
g
2 mL
03/05/20 10:45
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
0030027-11
P000105
3.52
mL
5 mL
03/05/20 11:24
0030027-12
P000105
4.17
mL
5 mL
03/05/20 11:24
Prep Method: Solids, Dry
Weight
Lab Number
Batch
Initial
Final
Date/Time
0030027-01
P000098
30
g 30 g
03/05/20
8:44
0030027-02
P000098
30
g 30 g
03/05/20
8:44
0030027-03
P000098
30
g 30 g
03/05/20
8:44
0030027-04
P000098
30
g 30 g
03/05/20
8:44
0030027-05
P000098
30
g 30 g
03/05/20
8:44
0030027-06
P000098
30
g 30 g
03/05/20
8:44
0030027-07
P000110
30
g 30 g
03/05/20
14:15
0030027-08
P000110
30
g 30 g
03/05/20
14:15
0030027-09
P000110
30
g 30 g
03/05/20
14:15
0030027-10
P000110
30
g 30 g
03/05/20
14:15
0030027-11
P000110
30
g 30 g
03/05/20
14:15
0030027-12
P000110
30
g 30 g
03/05/20
14:15
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
0030027-01
P000087
30.01
g 1 mL
03/04/20 15:45
0030027-02
P000087
30
g 1 mL
03/04/20 15:45
0030027-03
P000087
29.98
g 1 mL
03/04/20 15:45
0030027-04
P000087
30.04
g 1 mL
03/04/20 15:45
0030027-05
P000087
29.99
g 1 mL
03/04/20 15:45
0030027-06
P000087
29.99
g 1 mL
03/04/20 15:45
0030027-07
P000087
30
g 1 mL
03/04/20 15:45
0030027-08
P000087
30.02
g 1 mL
03/04/20 15:45
0030027-09
P000087
30.02
g 1 mL
03/04/20 15:45
0030027-10
P000087
29.99
g 1 mL
03/04/20 15:45
Prep Method: 5035
Lab Number
Batch
Initial
Final
Date/Time
0030027-01 P000102 5.61 g 5 mL 03/05/20 11:17
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Extraction Data
Prep Method: 5035
Lab Number Batch Initial Final Date/Time
0030027-02
P000102
3.54
g 5 mL
03/05/20 11:17
0030027-03
P000102
5.11
g 5 mL
03/05/20 11:17
0030027-04
P000102
4.9
g 5 mL
03/05/20 11:17
0030027-05
P000102
4.07
g 5 mL
03/05/20 11:17
0030027-06
P000102
4.19
g 5 mL
03/05/20 11:17
0030027-07
P000102
5.07
g 5 mL
03/05/20 11:17
0030027-08
P000102
4.81
g 5 mL
03/05/20 11:17
0030027-09
P000102
3.87
g 5 mL
03/05/20 11:17
0030027-10
P000102
5.34
g 5 mL
03/05/20 11:17
Prep Method: MADEP VPH (S)
Lab Number
Batch
Initial
Final
Date/Time
0030027-01
P000106
3.77
g 16
mL
03/05/20
11:24
0030027-02
P000106
3.93
g 16
mL
03/05/20
11:24
0030027-03
P000106
4.49
g 16
mL
03/05/20
11:24
0030027-04
P000106
5.54
g 16
mL
03/05/20
11:24
0030027-05
P000106
4.57
g 16
mL
03/05/20
11:24
0030027-06
P000106
4.95
g 16
mL
03/05/20
11:24
0030027-07
P000106
3.91
g 16
mL
03/05/20
11:24
0030027-08
P000106
4.27
g 16
mL
03/05/20
11:24
0030027-09
P000106
3.82
g 16
mL
03/05/20
11:24
0030027-10
P000106
4.24
g 16
mL
03/05/20
11:24
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

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Case Narrative
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte)
Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: WIT-019
Lab Submittal Date: 03/19/2020
Work Order: 0030269
3/26/20 12:17
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
a,j
Angela D. Overcash
Senior Project Manager
Data Qualifiers Key Reference:
CCVH CCV result is above control limits but within method parameters. Result is considered estimated.
D RPD value outside of the control limits.
L Parameter reported with possible low bias. LCS recovery below the QC limit.
M Matrix spike outside of the control limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

0
Waypoint.
ANALYTICAL
Sample Receipt Summary
03/26/2020
Work Order: 0030269
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
UST-2 Sidewall N2 0030269-01 Solid 03/18/20 16:10 03/19/20 9:18
Samples were received in good condition at 3.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Summary of Detections
WayPAoi nt . 03/26/209
NALYTICAL Work Order: 003026
Waypoint ID Client ID Parameter Method Result Units
There were no detections reported.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
• �.
Waynt.�
03/26/2020
PA
ANALYTICAL
Hart & Hickman (Charlotte)
Project: WIT-019
Client Sample ID: UST-2 Sidewall N2
Attn: Matt Ingalls
Sample ID: 0030269-01
2923 South Tryon St. Ste 100
Work
Order: 0030269
Charlotte, NC 28203
Sample Matrix: Solid
Time
Collected: 03/18/20 16:10
Time
Submitted: 03/19/20 09:18
Parameter
Result Units
Report
MDL
Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
BRL
mg/kg dry
32
1.6
1
*MADEP EPH 3/24/20 21:08
ZRC
P000422
C19-C36 Aliphatics
BRL
mg/kg dry
32
5.4
1
*MADEP EPH 3/24/20 21:08
ZRC
P000422
C11-C22Aromatics
BRL
mg/kg dry
32
8.8
1
*MADEP EPH 3/24/20 21:08
ZRC
P000422
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
66 %
40-140
o-Terphenyl
60 %
40-140
2-Fluorobiphenyl
72 %
40-140
2-Bromonaphthalene
75 %
40-140
General Chemistry Parameters
% Solids
77.3
% by
0.100
0.100
1
*SM2540 G 3125/20 10:45
EDV
P000479
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.85
0.15
1
*8270E 3/24/20 20:41
JMV
P000476
1,2-Dichlorobenzene
BRL
mg/kg dry
0.85
0.14
1
*8270E 3/24/20 20:41
JMV
P000476
1,3-Dichlorobenzene
BRL
mg/kg dry
0.85
0.13
1
*8270E 3/24/20 20:41
JMV
P000476
1,4-Dichlorobenzene
BRL
mg/kg dry
0.43
0.13
1
*8270E 3/24/20 20:41
JMV
P000476
1-Methyl naphthalene
BRL
mg/kg dry
0.85
0.013
1
*8270E 3/24/20 20:41
JMV
P000476
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.85
0.18
1
*8270E 3/24/20 20:41
JMV
P000476
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.85
0.21
1
*8270E 3/24/20 20:41
JMV
P000476
2,4-Dichlorophenol
BRL
mg/kg dry
0.85
0.17
1
*8270E 3/24/20 20:41
JMV
P000476
2,4-Dimethylphenol
BRL
mg/kg dry
0.43
0.18
1
*8270E 3/24/20 20:41
JMV
P000476
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.50
1
*8270E 3/24/20 20:41
JMV
P000476
2,4-Dinitrotoluene
BRL
mg/kg dry
0.85
0.23
1
*8270E 3/24/20 20:41
JMV
P000476
2,6-Dinitrotoluene
BRL
mg/kg dry
0.85
0.22
1
*8270E 3/24/20 20:41
JMV
P000476
2-Chloronaphthalene
BRL
mg/kg dry
0.85
0.21
1
*8270E 3/24/20 20:41
JMV
P000476
2-Chlorophenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/24/20 20:41
JMV
P000476
2-Methyl naphthalene
BRL
mg/kg dry
0.85
0.017
1
*8270E 3/24/20 20:41
JMV
P000476
2-Methylphenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/24/20 20:41
JMV
P000476
2-Nitrophenol
BRL
mg/kg dry
0.85
0.14
1
*8270E 3/24/20 20:41
JMV
P000476
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.85
0.17
1
*8270E 3/24/20 20:41
JMV
P000476
3/4-Methyl phenol
BRL
mg/kg dry
0.85
0.18
1
*8270E 3/24/20 20:41
JMV
P000476
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.47
1
*8270E 3/24/20 20:41
JMV
P000476
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.85
0.20
1
*8270E 3/24/20 20:41
JMV
P000476
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.85
0.16
1
*8270E 3/24/20 20:41
JMV
P000476
4-Chloroaniline
BRL
mg/kg dry
0.43
0.10
1
*8270E 3/24/20 20:41
JMV
P000476
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.3
0.26
1
*8270E 3/24/20 20:41
JMV
P000476
4-Nitrophenol
BRL
mg/kg dry
0.85
0.21
1
*8270E 3/24/20 20:41
JMV
P000476
Acenaphthene
BRL
mg/kg dry
0.85
0.020
1
*8270E 3/24/20 20:41
JMV
P000476
Acenaphthylene
BRL
mg/kg dry
0.85
0.017
1
*8270E 3/24/20 20:41
JMV
P000476
Anthracene
BRL
mg/kg dry
0.85
0.0094
1
*8270E 3/24/20 20:41
JMV
P000476
Azobenzene
BRL
mg/kg dry
0.85
0.18
1
*8270E 3/24/20 20:41
JMV
P000476
Benzo(a)anthracene
BRL
mg/kg dry
0.85
0.010
1
*8270E 3/24/20 20:41
JMV
P000476
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
IR A i • .0 03/26/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall N2
Attn: Matt Ingalls Sample ID: 0030269-01
2923 South Tryon St. Ste 100 Work Order: 0030269
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/18/20 16:10
Time Submitted: 03/19/20 09:18
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.85
0.0076
1
*8270E
3/24/20 20:41
JMV
P000476
Benzo(b)fluoranthene
BRL
mg/kg dry
0.85
0.0079
1
*8270E
3/24/20 20:41
JMV
P000476
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.85
0.0084
1
*8270E
3/24/20 20:41
JMV
P000476
Benzo(k)fluoranthene
BRL
mg/kg dry
0.85
0.0091
1
*8270E
3/24/20 20:41
JMV
P000476
Benzoic Acid
BRL
mg/kg dry
2.6
0.71
1
*8270E
3/24/20 20:41
JMV
P000476
Benzyl alcohol
BRL
mg/kg dry
0.85
0.16
1
*8270E
3/24/20 20:41
JMV
P000476
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.85
0.16
1
*8270E
3/24/20 20:41
JMV
P000476
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.85
0.14
1
*8270E
3/24/20 20:41
JMV
P000476
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/24/20 20:41
JMV
P000476
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/24/20 20:41
JMV
P000476
Butyl benzyl phthalate
BRL
mg/kg dry
0.43
0.15
1
*8270E
3/24/20 20:41
JMV
P000476
Chrysene
BRL
mg/kg dry
0.85
0.010
1
*8270E
3/24/20 20:41
JMV
P000476
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.85
0.025
1
*8270E
3/24/20 20:41
JMV
P000476
Dibenzofuran
BRL
mg/kg dry
0.85
0.23
1
*8270E
3/24/20 20:41
JMV
P000476
Diethyl phthalate
BRL
mg/kg dry
0.85
0.22
1
*8270E
3/24/20 20:41
JMV
P000476
Dimethyl phthalate
BRL
mg/kg dry
0.85
0.20
1
*8270E
3/24/20 20:41
JMV
P000476
Di-n-butyl phthalate
BRL
mg/kg dry
0.85
0.21
1
*8270E
3/24/20 20:41
JMV
P000476
Di-n-octyl phthalate
BRL
mg/kg dry
0.43
0.22
1
*8270E
3/24/20 20:41
JMV
P000476
Fluoranthene
BRL
mg/kg dry
0.85
0.0097
1
*8270E
3/24/20 20:41
JMV
P000476
Fluorene
BRL
mg/kg dry
0.85
0.015
1
*8270E
3/24/20 20:41
JMV
P000476
Hexachlorobenzene
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/24/20 20:41
JMV
P000476
Hexachlorobutadiene
BRL
mg/kg dry
0.85
0.19
1
*8270E
3/24/20 20:41
JMV
P000476
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.85
0.29
1
*8270E
3/24/20 20:41
JMV
P000476
Hexachloroethane
BRL
mg/kg dry
0.85
0.13
1
*8270E
3/24/20 20:41
JMV
P000476
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.85
0.024
1
*8270E
3/24/20 20:41
JMV
P000476
Isophorone
BRL
mg/kg dry
0.85
0.18
1
*8270E
3/24/20 20:41
JMV
P000476
Naphthalene
BRL
mg/kg dry
0.85
0.018
1
*8270E
3/24/20 20:41
JMV
P000476
Nitrobenzene
BRL
mg/kg dry
0.43
0.18
1
*8270E
3/24/20 20:41
JMV
P000476
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.85
0.20
1
*8270E
3/24/20 20:41
JMV
P000476
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.85
0.23
1
*8270E
3/24/20 20:41
JMV
P000476
Pentachlorophenol
BRL
mg/kg dry
1.3
0.54
1
*8270E
3/24/20 20:41
JMV
P000476
Phenanthrene
BRL
mg/kg dry
0.85
0.0093
1
*8270E
3/24/20 20:41
JMV
P000476
Phenol
BRL
mg/kg dry
0.85
0.14
1
*8270E
3/24/20 20:41
JMV
P000476
Pyrene
BRL
mg/kg dry
0.85
0.012
1
*8270E
3/24/20 20:41
JMV
P000476
Pyridine
BRL
mg/kg dry
0.43
0.081
1
*8270E
3/24/20 20:41
JMV
P000476
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
77 %
39-132
2-Fluorobiphenyl
70 %
44-115
2-Fluorophenol
74 %
35-115
Nitrobenzene-d5
67 %
37-122
Phenol-d5
71 %
34-121
Terphenyl-d14
73 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
IR A i • .0 03/26/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall N2
Attn: Matt Ingalls Sample ID: 0030269-01
2923 South Tryon St. Ste 100 Work Order: 0030269
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/18/20 16:10
Time Submitted: 03/19/20 09:18
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0077
0.00095
1
*8260D
3/23/20 17:20
TLB
P000454
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0077
0.0011
1
*8260D
3/23/20 17:20
TLB
P000454
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0077
0.00056
1
*8260D
3/23/20 17:20
TLB
P000454
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0077
0.00084
1
*8260D
3/23/20 17:20
TLB
P000454
1,1-Dichloroethane
BRL
mg/kg dry
0.0077
0.0014
1
*8260D
3/23/20 17:20
TLB
P000454
1,1-Dichloroethylene
BRL
mg/kg dry
0.0077
0.0014
1
*8260D
3/23/20 17:20
TLB
P000454
1,1-Dichloropropylene
BRL
mg/kg dry
0.0077
0.0012
1
*8260D
3/23/20 17:20
TLB
P000454
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.015
0.0011
1
*8260D
3/23/20 17:20
TLB
P000454
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0077
0.00088
1
*8260D
3/23/20 17:20
TLB
P000454
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.015
0.00074
1
*8260D
3/23/20 17:20
TLB
P000454
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0077
0.00082
1
*8260D
3/23/20 17:20
TLB
P000454
1,2-Dibromoethane
BRL
mg/kg dry
0.0077
0.00069
1
*8260D
3/23/20 17:20
TLB
P000454
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0077
0.00086
1
*8260D
3/23/20 17:20
TLB
P000454
1,2-Dichloroethane
BRL
mg/kg dry
0.0077
0.00092
1
*8260D
3/23/20 17:20
TLB
P000454
1,2-Dichloropropane
BRL
mg/kg dry
0.0077
0.0012
1
*8260D
3/23/20 17:20
TLB
P000454
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0077
0.00097
1
*8260D
3/23/20 17:20
TLB
P000454
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0077
0.00096
1
*8260D
3/23/20 17:20
TLB
P000454
1,3-Dichloropropane
BRL
mg/kg dry
0.0077
0.00065
1
*8260D
3/23/20 17:20
TLB
P000454
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0077
0.00098
1
*8260D
3/23/20 17:20
TLB
P000454
2,2-Dichloropropane
BRL
mg/kg dry
0.0077
0.00096
1
*8260D
3/23/20 17:20
TLB
P000454
2-Chlorotoluene
BRL
mg/kg dry
0.0077
0.0010
1
*8260D
3/23/20 17:20
TLB
P000454
4-Chlorotoluene
BRL
mg/kg dry
0.0077
0.00088
1
*8260D
3/23/20 17:20
TLB
P000454
4-Isopropyltoluene
BRL
mg/kg dry
0.0077
0.0019
1
*8260D
3/23/20 17:20
TLB
P000454
Acetone
BRL CCVH
mg/kg dry
0.031
0.0020
1
*8260D
3/23/20 17:20
TLB
P000454
Benzene
BRL
mg/kg dry
0.0077
0.0012
1
*8260D
3/23/20 17:20
TLB
P000454
Bromobenzene
BRL
mg/kg dry
0.0077
0.0011
1
*8260D
3/23/20 17:20
TLB
P000454
Bromochloromethane
BRL
mg/kg dry
0.0077
0.0013
1
*8260D
3/23/20 17:20
TLB
P000454
Bromodichloromethane
BRL
mg/kg dry
0.0077
0.00074
1
*8260D
3/23/20 17:20
TLB
P000454
Bromoform
BRL
mg/kg dry
0.0077
0.00060
1
*8260D
3/23/20 17:20
TLB
P000454
Bromomethane
BRL
mg/kg dry
0.015
0.0038
1
*8260D
3/23/20 17:20
TLB
P000454
Carbon Tetrachloride
BRL
mg/kg dry
0.0077
0.0015
1
*8260D
3/23/20 17:20
TLB
P000454
Chlorobenzene
BRL
mg/kg dry
0.0077
0.0012
1
*8260D
3/23/20 17:20
TLB
P000454
Chloroethane
BRL
mg/kg dry
0.015
0.0015
1
*8260D
3/23/20 17:20
TLB
P000454
Chloroform
BRL
mg/kg dry
0.0077
0.00095
1
*8260D
3/23/20 17:20
TLB
P000454
Chloromethane
BRL
mg/kg dry
0.015
0.0024
1
*8260D
3/23/20 17:20
TLB
P000454
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0077
0.0012
1
*8260D
3/23/20 17:20
TLB
P000454
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0077
0.00076
1
*8260D
3/23/20 17:20
TLB
P000454
Dibromochloromethane
BRL
mg/kg dry
0.0077
0.00052
1
*8260D
3/23/20 17:20
TLB
P000454
Dichlorodifluoromethane
BRL
mg/kg dry
0.015
0.0022
1
*8260D
3/23/20 17:20
TLB
P000454
Ethylbenzene
BRL
mg/kg dry
0.0077
0.0012
1
*8260D
3/23/20 17:20
TLB
P000454
Isopropyl Ether
BRL
mg/kg dry
0.0077
0.0011
1
*8260D
3/23/20 17:20
TLB
P000454
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0077
0.00090
1
*8260D
3/23/20 17:20
TLB
P000454
m,p-Xylenes
BRL
mg/kg dry
0.015
0.0020
1
*8260D
3/23/20 17:20
TLB
P000454
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Laboratory Report
IR A i • .0 03/26/2020
- -ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Client Sample ID: UST-2 Sidewall N2
Attn: Matt Ingalls Sample ID: 0030269-01
2923 South Tryon St. Ste 100 Work Order: 0030269
Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 03/18/20 16:10
Time Submitted: 03/19/20 09:18
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.031
0.00054
1
*8260D
3/23/20 17:20
TLB
P000454
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.031
0.0018
1
*8260D
3/23/20 17:20
TLB
P000454
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.031
0.00063
1
*8260D
3/23/20 17:20
TLB
P000454
Methylene Chloride
BRL
mg/kg dry
0.0077
0.0013
1
*8260D
3/23/20 17:20
TLB
P000454
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0077
0.0011
1
*8260D
3/23/20 17:20
TLB
P000454
Naphthalene
BRL
mg/kg dry
0.015
0.00078
1
*8260D
3/23/20 17:20
TLB
P000454
n-Butylbenzene
BRL
mg/kg dry
0.0077
0.00072
1
*8260D
3/23/20 17:20
TLB
P000454
n-Propylbenzene
BRL
mg/kg dry
0.0077
0.0011
1
*8260D
3/23/20 17:20
TLB
P000454
o-Xylene
BRL
mg/kg dry
0.0077
0.00082
1
*8260D
3/23/20 17:20
TLB
P000454
sec-Butylbenzene
BRL
mg/kg dry
0.0077
0.00084
1
*8260D
3/23/20 17:20
TLB
P000454
Styrene
BRL
mg/kg dry
0.0077
0.00075
1
*8260D
3/23/20 17:20
TLB
P000454
tert-Butylbenzene
BRL
mg/kg dry
0.0077
0.00092
1
*8260D
3/23/20 17:20
TLB
P000454
Tetrachloroethylene
BRL
mg/kg dry
0.0077
0.0014
1
*8260D
3/23/20 17:20
TLB
P000454
Toluene
BRL
mg/kg dry
0.0077
0.0012
1
*8260D
3/23/20 17:20
TLB
P000454
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0077
0.0015
1
*8260D
3/23/20 17:20
TLB
P000454
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0077
0.00066
1
*8260D
3/23/20 17:20
TLB
P000454
Trichloroethylene
BRL
mg/kg dry
0.0077
0.0015
1
*8260D
3/23/20 17:20
TLB
P000454
Trichlorofluoromethane
BRL
mg/kg dry
0.015
0.0021
1
*8260D
3/23/20 17:20
TLB
P000454
Vinyl acetate
BRL
mg/kg dry
0.015
0.00084
1
*8260D
3/23/20 17:20
TLB
P000454
Vinyl chloride
BRL
mg/kg dry
0.015
0.0015
1
*8260D
3/23/20 17:20
TLB
P000454
Xylenes, total
BRL
mg/kg dry
0.023
0.0028
1
*8260D
3/23/20 17:20
TLB
P000454
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
102 %
84-123
Toluene-d8
98 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
22
4.4
100
*MADEP VPH
3/23/20 19:01
TBL
P000424
C9-C12 Aliphatics
BRL
mg/kg dry
22
1.9
100
*MADEP VPH
3/23/20 19:01
TBL
P000424
C9-Cl0 Aromatics
BRL
mg/kg dry
22
2.1
100
*MADEP VPH
3/23/20 19:01
TBL
P000424
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
101 %
70-130
2,5-Dibromotoluene (FID)
107 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

(2)
Waypo�nt.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000454 - 5035
Reporting
Result Limit Units
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P000454-BLK1)
Prepared & Analyzed: 03/23/20
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000454 - 5035
Reporting
Result Limit Units
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P000454-BLK1)
Prepared & Analyzed: 03/23/20
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
50.1
ug/L
50.00 100 70-130
Surrogate: Dibromofluoromethane
50.0
ug/L
50.00 100 84-123
Surrogate: Toluene-d8
49.5
ug/L
50.00 99 76-129
LCS (P000454-BSI)
Prepared &Analyzed:
03/23/20
1,1,1,2-Tetrachloroethane
0.0499
0.0050
mg/kg wet
0.05000
100
72-115
1, 1,1 -Trichloroethane
0.0483
0.0050
mg/kg wet
0.05000
97
67-131
1,1,2,2-Tetrachloroethane
0.0519
0.0050
mg/kg wet
0.05000
104
56-126
1,1,2-Trichloroethane
0.0516
0.0050
mg/kg wet
0.05000
103
70-133
1,1-Dichloroethane
0.0498
0.0050
mg/kg wet
0.05000
100
74-127
1,1-Dichloroethylene
0.0481
0.0050
mg/kg wet
0.05000
96
67-149
1, 1 -Dichloropropylene
0.0490
0.0050
mg/kg wet
0.05000
98
71-130
1,2,3-Trichlorobenzene
0.0503
0.010
mg/kg wet
0.05000
101
68-130
1,2,3-Trichloropropane
0.0528
0.0050
mg/kg wet
0.05000
106
60-137
1,2,4-Trichlorobenzene
0.0516
0.010
mg/kg wet
0.05000
103
66-125
1,2,4-Trimethylbenzene
0.0509
0.0050
mg/kg wet
0.05000
102
69-129
1,2-Dibromoethane
0.0527
0.0050
mg/kg wet
0.05000
105
70-132
1,2-Dichlorobenzene
0.0494
0.0050
mg/kg wet
0.05000
99
72-123
1,2-Dichloroethane
0.0497
0.0050
mg/kg wet
0.05000
99
68-128
1,2-Dichloropropane
0.0514
0.0050
mg/kg wet
0.05000
103
73-130
1,3,5-Trimethylbenzene
0.0496
0.0050
mg/kg wet
0.05000
99
69-128
1,3-Dichlorobenzene
0.0490
0.0050
mg/kg wet
0.05000
98
71-120
1,3-Dichloropropane
0.0512
0.0050
mg/kg wet
0.05000
102
75-124
1,4-Dichlorobenzene
0.0489
0.0050
mg/kg wet
0.05000
98
71-123
2,2-Dichloropropane
0.0493
0.0050
mg/kg wet
0.05000
99
50-142
2-Chlorotoluene
0.0496
0.0050
mg/kg wet
0.05000
99
67-124
4-Chlorotoluene
0.0496
0.0050
mg/kg wet
0.05000
99
71-126
4-Isopropyltoluene
0.0510
0.0050
mg/kg wet
0.05000
102
68-129
Acetone
0.149
0.020
mg/kg wet
0.1000
149
29-198
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000454 - 5035
Reporting
Result Limit Units
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P000454-BS1)
Prepared &Analyzed: 03/23/20
Benzene
0.0489
0.0050
mg/kg wet
0.05000
98
74-127
Bromobenzene
0.0498
0.0050
mg/kg wet
0.05000
100
73-125
Bromochloromethane
0.0488
0.0050
mg/kg wet
0.05000
98
72-134
Bromodichloromethane
0.0509
0.0050
mg/kg wet
0.05000
102
75-122
Bromoform
0.0477
0.0050
mg/kg wet
0.05000
95
66-135
Bromomethane
0.0509
0.010
mg/kg wet
0.05000
102
20-180
Carbon Tetrachloride
0.0478
0.0050
mg/kg wet
0.05000
96
64-143
Chlorobenzene
0.0489
0.0050
mg/kg wet
0.05000
98
74-118
Chloroethane
0.0456
0.010
mg/kg wet
0.05000
91
33-149
Chloroform
0.0495
0.0050
mg/kg wet
0.05000
99
73-127
Chloromethane
0.0496
0.010
mg/kg wet
0.05000
99
45-143
cis-1,2-Dichloroethylene
0.0502
0.0050
mg/kg wet
0.05000
100
76-134
cis-1,3-Dichloropropylene
0.0528
0.0050
mg/kg wet
0.05000
106
71-125
Dibromochloromethane
0.0527
0.0050
mg/kg wet
0.05000
105
73-122
Dichlorodifluoromethane
0.0484
0.010
mg/kg wet
0.05000
97
26-146
Ethylbenzene
0.0481
0.0050
mg/kg wet
0.05000
96
74-128
Isopropyl Ether
0.0513
0.0050
mg/kg wet
0.05000
103
59-159
Isopropylbenzene (Cumene)
0.0496
0.0050
mg/kg wet
0.05000
99
68-126
m,p-Xylenes
0.0988
0.010
mg/kg wet
0.1000
99
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0680
0.020
mg/kg wet
0.05000
136
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0630
0.020
mg/kg wet
0.05000
126
63-149
Methyl Isobutyl Ketone
0.0590
0.020
mg/kg wet
0.05000
118
57-162
Methylene Chloride
0.0479
0.0050
mg/kg wet
0.05000
96
74-129
Methyl-tert-Butyl Ether
0.0522
0.0050
mg/kg wet
0.05000
104
70-130
Naphthalene
0.0540
0.010
mg/kg wet
0.05000
108
57-157
n-Butylbenzene
0.0512
0.0050
mg/kg wet
0.05000
102
65-135
n-Propylbenzene
0.0497
0.0050
mg/kg wet
0.05000
99
67-130
o-Xylene
0.0499
0.0050
mg/kg wet
0.05000
100
74-126
sec-Butylbenzene
0.0503
0.0050
mg/kg wet
0.05000
101
66-131
Styrene
0.0533
0.0050
mg/kg wet
0.05000
107
77-121
tert-Butyl benzene
0.0497
0.0050
mg/kg wet
0.05000
99
67-132
Tetrachloroethylene
0.0476
0.0050
mg/kg wet
0.05000
95
68-130
Toluene
0.0492
0.0050
mg/kg wet
0.05000
98
71-129
trans- 1,2-Dichloroethylene
0.0494
0.0050
mg/kg wet
0.05000
99
73-132
trans- 1,3-Dichloropropylene
0.0540
0.0050
mg/kg wet
0.05000
108
68-123
Trichloroethylene
0.0496
0.0050
mg/kg wet
0.05000
99
75-133
Trichlorofluoromethane
0.0450
0.010
mg/kg wet
0.05000
90
44-146
Vinyl acetate
0.0549
0.010
mg/kg wet
0.05000
110
85-161
Vinyl chloride
0.0510
0.010
mg/kg wet
0.05000
102
48-147
Xylenes, total
0.149
0.015
mg/kg wet
0.1500
99
74-126
Surrogate:4-Bromofluorobenzene
49.7
ug/L
50.00
99
70-130
Surrogate: Dibromofluoromethane
50.2
ug/L
50.00
100
84-123
Surrogate: Toluene-d8
49.9
ug/L
50.00
100
76-129
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P000476 - 3546
Blank (P000476-BLK1)
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methyl naphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methyl naphthalene
2-Methylphenol
2-Nitrophenol
3,3'-Dichlorobenzidine
3/4-Methyl phenol
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-C h loro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
B is(2-Ch loroethyl )ether
Bis(2-chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
1.5 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
1.5 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
1.0 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
2.0 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.33 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
0.66 mg/kg wet
Prepared & Analyzed: 03/24/20
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000476 - 3546
Reporting
Result Limit Units
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P000476-BLK1)
Prepared & Analyzed: 03/24/20
Di-n-butyl phthalate
BRL
0.66
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
Fluoranthene
BRL
0.66
mg/kg wet
Fluorene
BRL
0.66
mg/kg wet
Hexachlorobenzene
BRL
0.66
mg/kg wet
Hexachlorobutadiene
BRL
0.66
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.66
mg/kg wet
Hexachloroethane
BRL
0.66
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.66
mg/kg wet
Isophorone
BRL
0.66
mg/kg wet
Naphthalene
BRL
0.66
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.66
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.66
mg/kg wet
Pentachlorophenol
BRL
1.0
mg/kg wet
Phenanthrene
BRL
0.66
mg/kg wet
Phenol
BRL
0.66
mg/kg wet
Pyrene
BRL
0.66
mg/kg wet
Pyridine
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
2.28
mg/kg wet
3.333
68
39-132
Surrogate: 2-Fluorobiphenyl
1.10
mg/kg wet
1.667
66
44-115
Surrogate: 2-Fluorophenol
2.37
mg/kg wet
3.333
71
35-115
Surrogate: Nitrobenzene-d5
1.04
mg/kg wet
1.667
63
37-122
Surrogate: Phenol-d5
2.22
mg/kg wet
3.333
67
34-121
Surrogate: Terphenyl-04
1.14
mg/kg wet
1.667
68
54-127
LCS (P000476-BS1)
Prepared &Analyzed: 03/24/20
1,2,4-Trichlorobenzene
1.29
0.66
mg/kg wet
1.667
78
34-118
1,2-Dichlorobenzene
1.19
0.66
mg/kg wet
1.667
72
33-117
1,3-Dichlorobenzene
1.18
0.66
mg/kg wet
1.667
71
30-115
1,4-Dichlorobenzene
1.16
0.33
mg/kg wet
1.667
70
31-115
1-Methyl naphthalene
1.37
0.66
mg/kg wet
1.667
82
40-119
2,4,5-Trichlorophenol
1.32
0.66
mg/kg wet
1.667
79
62-124
2,4,6-Trichlorophenol
1.41
0.66
mg/kg wet
1.667
84
39-126
2,4-Dichlorophenol
1.34
0.66
mg/kg wet
1.667
80
40-122
2,4-Dimethylphenol
1.68
0.33
mg/kg wet
1.667
101
30-127
2,4-Dinitrophenol
0.853
1.5
mg/kg wet
1.667
51
27-129
2,4-Dinitrotoluene
1.44
0.66
mg/kg wet
1.667
86
48-126
2,6-Dinitrotoluene
1.44
0.66
mg/kg wet
1.667
87
46-124
2-Chloronaphthalene
1.31
0.66
mg/kg wet
1.667
78
41-114
2-Chlorophenol
1.33
0.66
mg/kg wet
1.667
80
34-121
2-Methyl naphthalene
1.29
0.66
mg/kg wet
1.667
78
38-122
2-Methylphenol
1.37
0.66
mg/kg wet
1.667
82
32-122
2-Nitrophenol
1.29
0.66
mg/kg wet
1.667
77
36-123
3,3'-Dichlorobenzidine
1.40
0.66
mg/kg wet
1.667
84
22-121
3/4-Methyl phenol
1.27
0.66
mg/kg wet
1.667
76
34-119
4,6-Dinitro-2-methylphenol
1.39
1.5
mg/kg wet
1.667
84
29-132
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000476 - 3546
LCS (P000476-BSI)
4-Bromophenyl phenyl ether
4-C h loro-3-methyl phenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
B i s(2-Ch loroethyl )ether
Bis(2-chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
Butyl benzyl phthalate
Chrysene
Dibenzo(a, h )anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-N itroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
Surrogate: 2, 4, 6-Tribromophenol
Reporting
Result Limit Units
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Prepared & Analyzed: 03/24/20
1.43
0.66
mg/kg wet
1.667
86
46-124
1.38
0.66
mg/kg wet
1.667
83
45-122
1.25
0.33
mg/kg wet
1.667
75
17-106
1.31
1.0
mg/kg wet
1.667
79
45-121
1.46
0.66
mg/kg wet
1.667
87
30-132
1.39
0.66
mg/kg wet
1.667
83
40-123
1.46
0.66
mg/kg wet
1.667
87
32-132
1.50
0.66
mg/kg wet
1.667
90
47-123
1.55
0.66
mg/kg wet
1.667
93
39-125
1.40
0.66
mg/kg wet
1.667
84
49-126
1.54
0.66
mg/kg wet
1.667
93
45-129
1.46
0.66
mg/kg wet
1.667
88
45-132
1.48
0.66
mg/kg wet
1.667
89
43-134
1.49
0.66
mg/kg wet
1.667
90
47-132
BRL
2.0
mg/kg wet
1.667
10-83
1.37
0.66
mg/kg wet
1.667
82
29-122
1.22
0.66
mg/kg wet
1.667
73
36-121
1.05
0.66
mg/kg wet
1.667
63
31-120
1.17
0.33
mg/kg wet
1.667
70
33-131
1.51
0.66
mg/kg wet
1.667
90
51-133
1.47
0.33
mg/kg wet
1.667
88
48-132
1.42
0.66
mg/kg wet
1.667
85
50-124
0.627
0.66
mg/kg wet
1.667
38
45-134
1.33
0.66
mg/kg wet
1.667
80
44-120
1.36
0.66
mg/kg wet
1.667
82
50-124
1.35
0.66
mg/kg wet
1.667
81
48-124
1.56
0.66
mg/kg wet
1.667
93
51-128
1.54
0.33
mg/kg wet
1.667
92
45-140
1.49
0.66
mg/kg wet
1.667
89
50-127
1.37
0.66
mg/kg wet
1.667
82
43-125
1.42
0.66
mg/kg wet
1.667
85
45-122
1.33
0.66
mg/kg wet
1.667
80
32-123
1.22
0.66
mg/kg wet
1.667
73
32-117
1.13
0.66
mg/kg wet
1.667
68
28-117
1.54
0.66
mg/kg wet
1.667
92
45-133
1.09
0.66
mg/kg wet
1.667
65
30-122
1.24
0.66
mg/kg wet
1.667
74
35-123
1.17
0.33
mg/kg wet
1.667
70
34-122
1.29
0.66
mg/kg wet
1.667
78
36-120
1.81
0.66
mg/kg wet
1.667
109
38-127
1.50
1.0
mg/kg wet
1.667
90
25-133
1.45
0.66
mg/kg wet
1.667
87
50-121
1.36
0.66
mg/kg wet
1.667
81
34-121
1.54
0.66
mg/kg wet
1.667
92
47-127
0.788
0.33
mg/kg wet
1.667
47
10-60
2.97
mg/kg wet
3.333
89
39-132
L
L
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000476 - 3546
Reporting
Result Limit Units
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P000476-BS1)
Prepared & Analyzed: 03/24/20
Surrogate: 2-Fluorobiphenyl
1.27
mg/kg wet
1.667 76
44-115
Surrogate: 2-Fluorophenol
2.72
mg/kg wet
3.333 82
35-115
Surrogate: Nitrobenzene-d5
1.23
mg/kg wet
1.667 74
37-122
Surrogate: Phenol-d5
2.56
mg/kg wet
3.333 77
34-121
Surrogate: Terphenyl-04
1.42
mg/kg wet
1.667 85
54-127
Matrix Spike (P000476-MS1)
Source: 0030269-01
Prepared &Analyzed: 03/24/20
1,2,4-Trichlorobenzene
1.66
0.85
mg/kg dry
2.150
BRL
77
34-118
1,2-Dichlorobenzene
1.60
0.85
mg/kg dry
2.150
BRL
74
33-117
1,3-Dichlorobenzene
1.53
0.85
mg/kg dry
2.150
BRL
71
30-115
1,4-Dichlorobenzene
1.53
0.43
mg/kg dry
2.150
BRL
71
31-115
1-Methyl naphthalene
1.78
0.85
mg/kg dry
2.150
BRL
83
40-119
2,4,5-Trichlorophenol
1.75
0.85
mg/kg dry
2.150
BRL
81
45-121
2,4,6-Trichlorophenol
1.84
0.85
mg/kg dry
2.150
BRL
86
39-126
2,4-Dichlorophenol
1.72
0.85
mg/kg dry
2.150
BRL
80
40-122
2,4-Dimethylphenol
2.14
0.43
mg/kg dry
2.150
BRL
100
30-127
2,4-Dinitrophenol
1.25
1.9
mg/kg dry
2.150
BRL
58
27-129
2,4-Dinitrotoluene
1.82
0.85
mg/kg dry
2.150
BRL
84
48-126
2,6-Dinitrotoluene
1.88
0.85
mg/kg dry
2.150
BRL
87
46-124
2-Chloronaphthalene
1.75
0.85
mg/kg dry
2.150
BRL
82
41-114
2-Chlorophenol
1.78
0.85
mg/kg dry
2.150
BRL
83
34-121
2-Methyl naphthalene
1.69
0.85
mg/kg dry
2.150
BRL
79
38-122
2-Methylphenol
1.85
0.85
mg/kg dry
2.150
BRL
86
32-122
2-Nitrophenol
1.66
0.85
mg/kg dry
2.150
BRL
77
36-123
3,3'-Dichlorobenzidine
1.83
0.85
mg/kg dry
2.150
BRL
85
22-121
3/4-Methyl phenol
1.68
0.85
mg/kg dry
2.150
BRL
78
34-119
4,6-Dinitro-2-methylphenol
1.75
1.9
mg/kg dry
2.150
BRL
81
29-132
4-Bromophenyl phenyl ether
1.84
0.85
mg/kg dry
2.150
BRL
85
46-124
4-Chloro-3-methylphenol
1.78
0.85
mg/kg dry
2.150
BRL
83
45-122
4-Chloroaniline
1.66
0.43
mg/kg dry
2.150
BRL
77
17-106
4-Chlorophenyl phenyl ether
1.73
1.3
mg/kg dry
2.150
BRL
80
45-121
4-Nitrophenol
1.79
0.85
mg/kg dry
2.150
BRL
83
30-132
Acenaphthene
1.82
0.85
mg/kg dry
2.150
BRL
85
40-123
Acenaphthylene
1.94
0.85
mg/kg dry
2.150
BRL
90
32-132
Anthracene
1.89
0.85
mg/kg dry
2.150
BRL
88
47-123
Azobenzene
1.93
0.85
mg/kg dry
2.150
BRL
90
39-125
Benzo(a)anthracene
1.80
0.85
mg/kg dry
2.150
BRL
84
49-126
Benzo(a)pyrene
1.98
0.85
mg/kg dry
2.150
BRL
92
45-129
Benzo(b)fluoranthene
1.87
0.85
mg/kg dry
2.150
BRL
87
45-132
Benzo(g,h,i)perylene
1.91
0.85
mg/kg dry
2.150
BRL
89
43-134
Benzo(k)fluoranthene
1.91
0.85
mg/kg dry
2.150
BRL
89
47-132
Benzoic Acid
BRL
2.6
mg/kg dry
2.150
BRL
10-83 M
Benzyl alcohol
1.85
0.85
mg/kg dry
2.150
BRL
86
29-122
bis(2-Chloroethoxy)methane
1.60
0.85
mg/kg dry
2.150
BRL
74
36-121
Bis(2-Chloroethyl)ether
1.35
0.85
mg/kg dry
2.150
BRL
63
31-120
Bis(2-chloroisopropyl)ether
1.54
0.43
mg/kg dry
2.150
BRL
72
33-131
Bis(2-Ethylhexyl)phthalate
1.97
0.85
mg/kg dry
2.150
BRL
91
51-133
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000476 - 3546
Reporting
Result Limit Units
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (P000476-MS1)
Source: 0030269-01
Prepared &Analyzed: 03/24/20
Butyl benzyl phthalate
1.84
0.43
mg/kg dry
2.150
BRL
86
48-132
Chrysene
1.80
0.85
mg/kg dry
2.150
BRL
84
50-124
Dibenzo(a,h)anthracene
0.835
0.85
mg/kg dry
2.150
BRL
39
45-134
Dibenzofuran
1.73
0.85
mg/kg dry
2.150
BRL
81
44-120
Diethyl phthalate
1.76
0.85
mg/kg dry
2.150
BRL
82
50-124
Dimethyl phthalate
1.73
0.85
mg/kg dry
2.150
BRL
81
48-124
Di-n-butyl phthalate
1.98
0.85
mg/kg dry
2.150
BRL
92
51-128
Di-n-octyl phthalate
1.98
0.43
mg/kg dry
2.150
BRL
92
45-140
Fluoranthene
1.91
0.85
mg/kg dry
2.150
BRL
89
50-127
Fluorene
1.81
0.85
mg/kg dry
2.150
BRL
84
43-125
Hexachlorobenzene
1.82
0.85
mg/kg dry
2.150
BRL
84
45-122
Hexachlorobutadiene
1.73
0.85
mg/kg dry
2.150
BRL
80
32-123
Hexachlorocyclopentadiene
1.67
0.85
mg/kg dry
2.150
BRL
78
32-117
Hexachloroethane
1.44
0.85
mg/kg dry
2.150
BRL
67
28-117
Indeno(1,2,3-cd)pyrene
1.99
0.85
mg/kg dry
2.150
BRL
92
45-133
Isophorone
1.39
0.85
mg/kg dry
2.150
BRL
65
30-122
Naphthalene
1.63
0.85
mg/kg dry
2.150
BRL
76
35-123
Nitrobenzene
1.47
0.43
mg/kg dry
2.150
BRL
68
34-122
N-Nitroso-di-n-propylamine
1.73
0.85
mg/kg dry
2.150
BRL
80
36-120
N-Nitrosodiphenylamine
2.26
0.85
mg/kg dry
2.150
BRL
105
38-127
Pentachlorophenol
1.87
1.3
mg/kg dry
2.150
BRL
87
25-133
Phenanthrene
1.85
0.85
mg/kg dry
2.150
BRL
86
50-121
Phenol
1.79
0.85
mg/kg dry
2.150
BRL
83
34-121
Pyrene
1.96
0.85
mg/kg dry
2.150
BRL
91
47-127
Pyridine
1.04
0.43
mg/kg dry
2.150
BRL
48
20-150
Surrogate: 2,4,6-Trlbromophenol
3.78
mg/kg dry
4.301
88
39-132
Surrogate: 2-Fluorobiphenyl
1.69
mg/kg dry
2.150
79
44-115
Surrogate: 2-Fluorophenol
3.63
mg/kg dry
4.301
84
35-115
Surrogate: Nitrobenzene-d5
1.53
mg/kg dry
2.150
71
37-122
Surrogate: Phenol-d5
3.37
mg/kg dry
4.301
78
34-121
Surrogate: TerphenyW14
1.80
mg/kg dry
2.150
84
54-127
T
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Waypoint
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P000476 - 3546
Reporting
Result Limit Units
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P000476-MSD1)
Source: 0030269-01
Prepared &Analyzed: 03/24/20
1,2,4-Trichlorobenzene
1.22
0.85
mg/kg dry
2.153
BRL
57
34-118
31
20
1,2-Dichlorobenzene
1.11
0.85
mg/kg dry
2.153
BRL
52
33-117
36
20
1,3-Dichlorobenzene
1.08
0.85
mg/kg dry
2.153
BRL
50
30-115
34
20
1,4-Dichlorobenzene
1.07
0.43
mg/kg dry
2.153
BRL
50
31-115
35
20
1-Methyl naphthalene
1.32
0.85
mg/kg dry
2.153
BRL
61
40-119
30
20
2,4,5-Trichlorophenol
1.25
0.85
mg/kg dry
2.153
BRL
58
45-121
34
35
2,4,6-Trichlorophenol
1.30
0.85
mg/kg dry
2.153
BRL
60
39-126
35
20
2,4-Dichlorophenol
1.25
0.85
mg/kg dry
2.153
BRL
58
40-122
32
20
2,4-Dimethylphenol
1.58
0.43
mg/kg dry
2.153
BRL
73
30-127
30
20
2,4-Dinitrophenol
0.901
1.9
mg/kg dry
2.153
BRL
42
27-129
32
20
2,4-Dinitrotoluene
1.31
0.85
mg/kg dry
2.153
BRL
61
48-126
32
20
2,6-Dinitrotoluene
1.33
0.85
mg/kg dry
2.153
BRL
62
46-124
34
20
2-Chloronaphthalene
1.27
0.85
mg/kg dry
2.153
BRL
59
41-114
32
20
2-Chlorophenol
1.27
0.85
mg/kg dry
2.153
BRL
59
34-121
33
20
2-Methyl naphthalene
1.25
0.85
mg/kg dry
2.153
BRL
58
38-122
30
20
2-Methylphenol
1.34
0.85
mg/kg dry
2.153
BRL
62
32-122
32
20
2-Nitrophenol
1.25
0.85
mg/kg dry
2.153
BRL
58
36-123
28
20
3,3'-Dichlorobenzidine
1.36
0.85
mg/kg dry
2.153
BRL
63
22-121
30
20
3/4-Methyl phenol
1.17
0.85
mg/kg dry
2.153
BRL
54
34-119
36
20
4,6-Dinitro-2-methylphenol
1.25
1.9
mg/kg dry
2.153
BRL
58
29-132
33
20
4-Bromophenyl phenyl ether
1.33
0.85
mg/kg dry
2.153
BRL
62
46-124
32
20
4-Chloro-3-methylphenol
1.29
0.85
mg/kg dry
2.153
BRL
60
45-122
32
20
4-Chloroaniline
1.22
0.43
mg/kg dry
2.153
BRL
57
17-106
30
20
4-Chlorophenyl phenyl ether
1.25
1.3
mg/kg dry
2.153
BRL
58
45-121
32
20
4-Nitrophenol
1.31
0.85
mg/kg dry
2.153
BRL
61
30-132
31
20
Acenaphthene
1.36
0.85
mg/kg dry
2.153
BRL
63
40-123
29
20
Acenaphthylene
1.41
0.85
mg/kg dry
2.153
BRL
66
32-132
31
20
Anthracene
1.39
0.85
mg/kg dry
2.153
BRL
65
47-123
31
20
Azobenzene
1.43
0.85
mg/kg dry
2.153
BRL
66
39-125
30
20
Benzo(a)anthracene
1.30
0.85
mg/kg dry
2.153
BRL
60
49-126
33
20
Benzo(a)pyrene
1.42
0.85
mg/kg dry
2.153
BRL
66
45-129
33
20
Benzo(b)fluoranthene
1.38
0.85
mg/kg dry
2.153
BRL
64
45-132
30
20
Benzo(g,h,i)perylene
1.33
0.85
mg/kg dry
2.153
BRL
62
43-134
35
20
Benzo(k)fluoranthene
1.35
0.85
mg/kg dry
2.153
BRL
63
47-132
34
20
Benzoic Acid
BRL
2.6
mg/kg dry
2.153
BRL
10-83
20
Benzyl alcohol
1.28
0.85
mg/kg dry
2.153
BRL
60
29-122
36
20
bis(2-Chloroethoxy)methane
1.19
0.85
mg/kg dry
2.153
BRL
55
36-121
30
20
Bis(2-Chloroethyl)ether
0.980
0.85
mg/kg dry
2.153
BRL
46
31-120
32
20
Bis(2-chloroisopropyl)ether
1.08
0.43
mg/kg dry
2.153
BRL
50
33-131
35
20
Bis(2-Ethylhexyl)phthalate
1.38
0.85
mg/kg dry
2.153
BRL
64
51-133
35
20
Butyl benzyl phthalate
1.37
0.43
mg/kg dry
2.153
BRL
63
48-132
30
20
Chrysene
1.29
0.85
mg/kg dry
2.153
BRL
60
50-124
33
20
Dibenzo(a,h)anthracene
0.534
0.85
mg/kg dry
2.153
BRL
25
45-134
44
20
Dibenzofuran
1.27
0.85
mg/kg dry
2.153
BRL
59
44-120
31
20
Diethyl phthalate
1.25
0.85
mg/kg dry
2.153
BRL
58
50-124
34
20
Dimethyl phthalate
1.25
0.85
mg/kg dry
2.153
BRL
58
48-124
32
20
Ill
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Semivolatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P000476 - 3546
Matrix Spike Dup (P000476-MSD1)
Source: 0030269-01
Prepared & Analyzed: 03/24/20
Di-n-butyl phthalate
1.47
0.85
mg/kg dry
2.153
BRL
68
51-128
Di-n-octyl phthalate
1.42
0.43
mg/kg dry
2.153
BRL
66
45-140
Fluoranthene
1.42
0.85
mg/kg dry
2.153
BRL
66
50-127
Fluorene
1.30
0.85
mg/kg dry
2.153
BRL
60
43-125
Hexachlorobenzene
1.31
0.85
mg/kg dry
2.153
BRL
61
45-122
Hexachlorobutadiene
1.23
0.85
mg/kg dry
2.153
BRL
57
32-123
Hexachlorocyclopentadiene
1.17
0.85
mg/kg dry
2.153
BRL
54
32-117
Hexachloroethane
1.04
0.85
mg/kg dry
2.153
BRL
48
28-117
Indeno(1,2,3-cd)pyrene
1.42
0.85
mg/kg dry
2.153
BRL
66
45-133
Isophorone
1.03
0.85
mg/kg dry
2.153
BRL
48
30-122
Naphthalene
1.21
0.85
mg/kg dry
2.153
BRL
56
35-123
Nitrobenzene
1.09
0.43
mg/kg dry
2.153
BRL
51
34-122
N-Nitroso-di-n-propylamine
1.22
0.85
mg/kg dry
2.153
BRL
57
36-120
N-Nitrosodiphenylamine
1.69
0.85
mg/kg dry
2.153
BRL
78
38-127
Pentachlorophenol
1.34
1.3
mg/kg dry
2.153
BRL
62
25-133
Phenanthrene
1.35
0.85
mg/kg dry
2.153
BRL
63
50-121
Phenol
1.34
0.85
mg/kg dry
2.153
BRL
62
34-121
Pyrene
1.42
0.85
mg/kg dry
2.153
BRL
66
47-127
Pyridine
0.705
0.43
mg/kg dry
2.153
BRL
33
20-150
Surrogate: 2,4,6-Tribromophenol
2.70
mg/kg dry
4.305
63
39-132
Surrogate: 2-Fluorobiphenyl
1.21
mg/kg dry
2.153
56
44-115
Surrogate: 2-Fluorophenol
2.52
mg/kg dry
4.305
59
35-115
Surrogate: Nitrobenzene-d5
1.11
mg/kg dry
2.153
52
37-122
Surrogate: Phenol-d5
2.40
mg/kg dry
4.305
56
34-121
Surrogate: Terphenyl-04
1.30
mg/kg dry
2.153
60
54-127
30 20 D
33 20 D
30 20 D
33 20 D
32 20 D
34 20 D
35 20 D
32 20 D
33 20 D
30 20 D
30 20 D
30 20 D
35 20 D
29 20 D
33 20 D
31 20 D
29 20 D
32 20 D
38 60
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P000424 - MADEP VPH (S)
Blank (P000424-BLK1)
Prepared & Analyzed: 03/23/20
C5-C8 Aliphatics
BRL
5.0
mg/kg wet
C9-C12 Aliphatics
BRL
5.0
mg/kg wet
C9-Cl0 Aromatics
BRL
5.0
mg/kg wet
Surrogate: 2,5-Dibromotoluene (PID)
10100
ug/L
10000 101
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10600
ug/L
10000 106
70-130
LCS (P000424-BS1)
Prepared &Analyzed: 03/23/20
C5-C8 Aliphatics
36.8
5.0
mg/kg wet
32.00 115
70-130
C9-Cl0 Aromatics
9.33
5.0
mg/kg wet
10.67 87
70-130
C9-C12 Aliphatic
31.2
5.0
mg/kg wet
32.00 97
70-130
Surrogate: 2,5-Dibromotoluene (PID)
9860
ug/L
10000 99
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10700
ug/L
10000 107
70-130
1-CS Dup (P000424-13SD1)
Prepared & Analyzed: 03/23/20
C5-C8 Aliphatics
37.8
5.0
mg/kg wet
32.00 118
70-130 3 50
C9-Cl0 Aromatics
9.33
5.0
mg/kg wet
10.67 87
70-130 0.02 50
C9-C12 Aliphatic
32.0
5.0
mg/kg wet
32.00 100
70-130 3 50
Surrogate: 2,5-Dibromotoluene (PID)
9700
ug/L
10000 97
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10600
ug/L
10000 106
70-130
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Q)
Waypoint.
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019
Attn: Matt Ingalls
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Analyte
Batch P000422 - 3546
Reporting
Result Limit Units
Level II QC Report
3/26/20
Work Order: 0030269
Time Submitted: 3/19/2020 9:18:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P000422-BLK1)
Prepared: 03/20/20 Analyzed: 03/24/20
C9-C18 Aliphatics
BRL
25
mg/kg wet
C19-C36 Aliphatics
BRL
25
mg/kg wet
C1 1-C22 Aromatics
BRL
25
mg/kg wet
Surrogate: 1-Chlorooctadecane
1.32
mg/kg wet
1.998
66
40-140
Surrogate: o-Terphenyl
1.41
mg/kg wet
1.998
71
40-140
Surrogate: 2-Fluorobiphenyl
3.11
mg/kg wet
3.996
78
40-140
Surrogate: 2-Bromonaphthalene
3.33
mg/kg wet
3.996
83
40-140
LCS (P000422-BSI)
Prepared: 03/20/20
Analyzed: 03/24/20
C9-C18 Aliphatics
32.8
25
mg/kg wet
59.76
55
40-140
C19-C36 Aliphatics
61.3
25
mg/kg wet
79.68
77
40-140
C11-C22 Aromatics
127
25
mg/kg wet
169.3
75
40-140
Surrogate: 1-Chlorooctadecane
1.39
mg/kg wet
1.992
70
40-140
Surrogate: o-Terphenyl
1.47
mg/kg wet
1.992
74
40-140
Surrogate: 2-Fluorobiphenyl
3.36
mg/kg wet
3.984
84
40-140
Surrogate: 2-Bromonaphthalene
3.36
mg/kg wet
3.984
84
40-140
Matrix Spike (P000422-MS1)
Source: 0030269-01
Prepared: 03/20/20
Analyzed: 03/24/20
C9-Cl8 Aliphatics
41.4
31
mg/kg dry
75.51 BRL
55
40-140
C19-C36 Aliphatics
76.8
31
mg/kg dry
100.7 BRL
76
40-140
C11-C22 Aromatics
159
31
mg/kg dry
213.9 BRL
74
40-140
Surrogate: 1-Chlorooctadecane
1.66
mg/kg dry
2.517
66
40-140
Surrogate: o-Terphenyl
1.74
mg/kg dry
2.517
69
40-140
Surrogate: 2-Fluorobiphenyl
4.20
mg/kg dry
5.034
83
40-140
Surrogate: 2-Bromonaphthalene
4.15
mg/kg dry
5.034
82
40-140
Matrix Spike Dup (P000422-MSD1)
Source: 0030269-01
Prepared: 03/20/20 Analyzed: 03/24/20
C9-C18 Aliphatics
40.6
32
mg/kg dry
75.73 BRL
54
40-140 2 50
C19-C36 Aliphatics
75.8
32
mg/kg dry
101.0 BRL
75
40-140 1 50
C11-C22 Aromatics
160
32
mg/kg dry
214.6 BRL
75
40-140 1 50
Surrogate: 1-Chlorooctadecane
1.79
mg/kg dry
2.524
71
40-140
Surrogate: o-Terphenyl
1.79
mg/kg dry
2.524
71
40-140
Surrogate: 2-Fluorobiphenyl
4.19
mg/kg dry
5.048
83
40-140
Surrogate: 2-Bromonaphthalene
4.35
mg/kg dry
5.048
86
40-140
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

® Level II QC Report
Waynt.
� 3/26/20
poi
ANALYTICAL
Hart & Hickman (Charlotte) Project: WIT-019 Work Order: 0030269
Attn: Matt Ingalls Time Submitted: 3/19/2020 9:18:OOAM
2923 South Tryon St. Ste 100
Charlotte, NC 28203
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P000479 - Solids, Dry Weight
Duplicate (P000479-DUP1) Source: 0030269-01 Prepared: 03/24/20 Analyzed: 03/25/20
% Solids 77.4 0.100 % by Weight 77.3 0.2 20
Sample Extraction Data
Prep Method: 3546
Lab Number Batch
Initial
Final
Date/Time
0030269-01 P000422
10.02 g
2 mL
03/20/20 12:29
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final
Date/Time
0030269-01 P000479
30 g
30 g
03/24/20 13:40
Prep Method: 3546
Lab Number Batch
Initial
Final
Date/Time
0030269-01 P000476
30.01 g
1 mL
03/24/20 13:50
Prep Method: 5035
Lab Number Batch
Initial
Final
Date/Time
0030269-01 P000454
4.18 g
5 mL
03/23/20 8:37
Prep Method: MADEP VPH (S)
Lab Number Batch
Initial
Final
Date/Time
0030269-01 P0O0424
4.39 g
16 mL
03/23/20 8:39
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

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Beverly, Trudy
From: Beverly, Trudy
Sent: Thursday, March 3, 2022 7:36 PM
To: Steve Libbey
Subject: RE: [External] Puckett/Nash Assemblage, Charlotte, NC
Do you have a UST-61 form for this one?
Thanks,
Trudy
UruarmrM ment�l4w��
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: hops://deq.nc.gov/about/divisions/waste-manaaement/ust
Branch's Above Ground Storage Tanks Website Address: ht!ps:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-proeram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hops: //deg.nc. gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.eov/nedeci/Waste%2OMana2ement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policy.odf
htips:Hfiles.nc. gov/ncdeq/\Vaste%2OManagement/D WMiUST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Steve Libbey [mailto:[e-mail]]
Sent: Thursday, March 3, 2022 4:23 PM
To: Beverly, Trudy <[e-mail]>
Subject: [External] Puckett/Nash Assemblage, Charlotte, NC
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Hi Trudy, please find attached an IAA report for this site. You discussed this site with Ayla in our office early last
year. Recall, we weren't able to remove the impacted soil stockpiles due to site access issues (-485 cut off the original
site access roads). Access was gained and the stockpiles were removed in October 2021.
Please call me if you have any questions.
Thanks,
Steve
Stephen Libbey, PG, Project Manager
Hart & Hickman, PC

Id 2923 S Tryon Street, Suite 100 • Charlotte, NC 28203
Direct:704-887-4606 Mobile:[phone]
www.harthickman.com