MO-292081_48272_CA_IAR_20220202_Initial Abatement Action Report

hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS
Via Email
February 2, 2022
NC DEQ Division of Waste Management
UST Section
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Attention: Ms. Beverly Trudy
RE: IAA Report
726 W. Sugar Creek Road
Charlotte, NC
H&H Job No. CHP-046
Dear Beverly,
On behalf of Dream.Key Partners, Hart & Hickman is submitting the attached Initial Abetment
Action (IAA) Report for the above referenced property located in Charlotte, Mecklenburg County,
North Carolina.
If you have any questions or comments, please do not hesitate to contact me.
Sincerely,
Hart & Hickman, PC
Stephen R. Libbey, P.G.
Project Manager
Enclosures
cc: Alex Walker, DKP (via email)
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

Initial Abatement Action Report
726 W. Sugar Creek Road
Charlotte, North Carolina
DEQ Incident No. TBD
H&H Job No. CHP-046
February 2, 2022
hart � hickman
SMARTER ENVIRONMENTAL SOLUTIONS
C-1269 Engineering
#C-245 Geology
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

Initial Abatement Action Report
A. Site Information
1. Site Identification
Date of Report: February 2.2022
Facility ID: NA UST Incident Number: TBD
Site Name: 726 W. Sugar Creek Road
Site Street Address: 726 W. Sugar Creek Road
City, Town: Charlotte Zip Code: 28269 County: Mecklenburg
Description of Geographical Data Point: Former UST location
Location Method: Google Earth
Latitude: 35.2690°N Longitude:-80.7941°W
2. Information about Contacts Associated with the Leaking UST System
UST Owner: Unknown
Address: Tel.:
UST Operator: Unknown
Address: Tel.:
Property Owner: DreamKey Partners
Address: 4601 Charlotte Park Drive Ste 350 Charlotte, NC 28217
Tel.: [phone]
Property Occupant: Undeveloped _
Address: Tel.:
Consultant/Contractor: Hart & Hickman PC
Address: 2923 South Tryon Street, Suite 100, Charlotte, NC 28203
Tel.: [phone] (Attn: Steve Libbey,_PG)
Analytical Laboratory: Waypaint Analytical _State Cert. No. 402
Address: 449 pringbrook Road, Charlotte, NC 28224 Tel.: [phone]
3. Information About Release
Date Discovered: January 13.2022
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release: Heating Oil UST
Sizes and contents of UST system: One 550-gallon heating oil UST
4. Certification
I, Stephen Libbey, PG a Licensed Geologist at Hart & Hickman, PC, do certify that the
lir��uj"
information contained in this report is correct and accurate to the best of my knoI l
�I qR�a.,
SEAL
Hart & Hickman, PC is licensed to practice geology/engineering in North CR
certification numbers of the company are C-245/C-1269. �►,►+rl�I11►►►►►�
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B. Site History and Characterization
1. UST Owner and Operator Information:
UST ID Number
UST-1
Facility ID Number
N/A
Name of Owner
Dates of Ownership
Unknown
Street Address
City
State
Zip
Telephone Number
Name of Operator
Dates of Operation
Unknown
Street Address
City
State
Zip
Telephone Number
2 hart 'ti hickman
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2. UST/AST Information:
Was
release
Approximate
Description of
Date
UST ID
Current/Last
Previous
Capacity
Construction
Status of
associated
Tank
Associated Piping and
Tank
Number
Contents
Contents
(gallons)
Details
UST
with the
Dimensions
Pumps
Installed
UST
LUS:T-1
S stem?
I Heating Oil
I N/A
1 550
1 Steel
1 6' x 3.33'
1 N/A
Unknown
I Removed
I Yes
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3. Non -UST spills at the site:
No non -UST spills are known to have occurred at the site.
4. Description of release:
On January 13, 2022, Buckeye Elm Contracting, LLC (Buckeye) of Columbus,
OH removed the inactive 550-gallon heating oil UST at the subject property.
Based on field evidence of impacted soils at the time of closure, soil over -
excavation activities were initiated following UST removal in accordance with
DEQ guidance. UST removal and soil excavation activities are presented in
Section D.
5. Site characteristics:
The site is approximately 1.39 acres in area and formerly contained a 1,757 ft2
single-family residence (726 W. Sugar Creek) and a 725 ft2 single-family
residence (724 W. Sugar Creek). A site location map is presented as Figure 1,
and a site map is presented as Figure 2.
The subject property is located in the Piedmont Physiographic Province of North
Carolina. According to the Geologic Map of North Carolina dated 1985, the
subject property lies within the Charlotte Belt. In the site area, underlying
bedrock is composed of granitic rock. The land surface of the area is generally
characterized as gently sloping, which may become moderately steep where
intersected by streams.
In the Piedmont, the bedrock is overlain by a mantle of weathered rock termed
saprolite or residuum. The saprolite consists of unconsolidated clay, silt, and sand
with lesser amounts of rock fragments. Due to the range of parent rock types and
their variable susceptibility to weathering, the saprolite ranges widely in color,
texture, and thickness. Generally, the saprolite is thickest near interstream divides
and thins toward streambeds. In profile, the saprolite normally grades from
clayey soils near the land surface to highly weathered rock above competent
bedrock.
The occurrence and movement of groundwater in the Piedmont is typically within
two separate but interconnected water -bearing zones. A shallow water -bearing
zone occurs within the saprolite, and a deeper water -bearing zone occurs within
the underlying bedrock.
The site is located at an approximate elevation of 770 ft above mean sea level.
Topography in the source area generally slopes to the northeast (Figure 1). Based
on topography, H&H anticipates that the groundwater flow direction at the site is
to the northeast toward an unnamed tributary of Little Sugar Creek located
approximately 900 ft from the former UST.
Visual observations during excavation activities and soil sample collection
indicated that the soil surrounding UST system consisted of orange to brown silty
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clays (saprolite). Groundwater and bedrock were not encountered in the
excavation.
Municipal water is available to the site and the areas surrounding the site. A
formal water supply well survey was not performed. No obvious water supply
wells were observed during area reconnaissance.
6. Initial abatement actions, assessment activities, and corrective actions
performed to date:
Prior to the January 2022 UST removal activities, no other known initial
abatement actions, assessments, or corrective action activities were conducted at
the site.
C. Site Check Report
Not applicable.
D. UST Closure Report following UST-12 format and Site Investigation Report
for Permanent Closure or Change -in -Service of UST (UST-2 Form)
1. Preparations for closure including the steps taken to notify authorities,
permits obtained and the steps taken to clean and purge the tanks:
Prior to the UST closure activities, a permit authorizing the UST removal was
obtained from the City of Charlotte Fire Department. A copy of the UST removal
permit application is provided in Appendix A.
Prior to removal, residual fluids were removed from the tank. Then, the tank was
triple -rinsed with a pressure washer and vacuum truck by EVO Environmental
and Industrial Resources (EVO) of Winston-Salem, NC in accordance with
Mecklenburg County requirements. Approximately 267 gallons of residual fluids
and rinse water were removed from the UST. Following removal of the residual
fluids and rinse water, the UST was purged of combustible vapors with dry -ice
and subsequently tested with a combustible gas indicator to ensure that potentially
combustible vapors had dissipated.
2. Closure procedures:
Initially, soil was removed from the top and sides of the UST with a back hoe so
that the tank could be removed from the ground. Soils encountered during the
excavation were evaluated in the field for the presence of odors and staining, and
for the presence of organic vapor readings with a photoionization detector (PID).
The PID was calibrated prior to its use against an isobutylene standard.
Following removal, the UST was inspected for holes or other signs of structural
damage. The UST was single -walled and constructed of steel. The bottom
surface of the tank was moderately pitted and contained several small holes.
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3. Note the amount of residual material pumped from the tank and describes
the storage, sampling and disposal of the residual material and the disposal
of the tank, pumps and piping:
As stated above, EVO removed approximately 267 gallons of residual and rinse
liquids from the UST. The fluid was disposed by EVO at their facility in
Winston-Salem, North Carolina. The disposal certificate for the residual fluid is
included in Appendix B.
The UST was transported off -site for disposal at CMC Commercial Metals
recycling in Charlotte, North Carolina. The tank disposal certificate is included in
Appendix C.
4. Initial response actions and initial abatement actions:
Initial response and abatement actions are discussed in the following section.
5. Soil excavation and Site Investigation activities:
After removal of the UST, one closure soil sample (UST-1 Stockpile) was
collected in accordance with DEQ guidelines. The closure sample was analyzed
for gasoline range total petroleum hydrocarbons (TPH-GRO) by EPA Method
5030/8015C and diesel range total petroleum hydrocarbons (TPH-DRO) by EPA
Method 3550/8015C. The analytical results for the closure soil sample indicated
the presence of TPH-DRO and TPH-GRO at concentrations of 441 mg/kg and
4,150 mg/kg, respectively. The detected concentrations exceed the DEQ action
levels of 50 mg/kg and 100 mg/kg for TPH-GRO and TPH-DRO, respectively.
Approximately 19.2 tons of impacted soils were excavated from the UST basin on
January 13, 2022. The excavated soil was transported to Environmental Soils,
Inc. in Lattimore, North Carolina for proper disposal. A copy of the certificate of
disposal, non -hazardous waste manifests, and certified weight tickets for the
excavated soil are provided in Appendix D.
The dimensions of the UST basin excavation were approximately 9 ft long by 5 ft
wide by 9 ft deep. The approximate extent of the excavation is depicted on Figure
2.
Following soil over -excavation activities, four confirmation sidewall soil samples
(UST-1 North, UST-1 South, UST-1 East, and UST-1 West) and one confirmation
base soil sample (UST-1 Base) were collected from the excavation. In
accordance with DEQ guidance, the collected post -excavation soil samples were
analyzed for volatile organic compounds (VOCs) by EPA Method 826013/5035A,
semi-VOCs (SVOCs) by EPA Method 8270, and extractable petroleum
hydrocarbons (EPH) and volatile petroleum hydrocarbons (VPH) using the
Massachusetts Department of Environmental Protection (MADEP) Methods.
The results of analyses of the post -excavation samples from the UST basin
excavation indicated that post -excavation samples contained trace concentrations
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of acetone. However, the detected concentrations did not exceed DEQ Soil -to -
Groundwater or Residential Maximum Soil Contaminant Concentrations
(MSCCs). No other target compounds were detected above the laboratory
detection limits in the samples.
All soil samples were analyzed by a North Carolina certified laboratory. A chain -
of -custody record was completed for samples collected and included sample
description, date collected, time collected, matrix, sample container information,
and analyses required. The chain -of -custody was signed by H&H prior to
placement in an iced cooler for shipment to the laboratory. Prior to shipment, the
cooler was closed with a seal indicating the H&H representative's signature and
date such that a potential disturbance of the cooler contents could be detected by
the laboratory.
Soil sample results are presented in Table 1 and the sample locations are depicted
on Figure 2. Laboratory analytical sheets are included in Appendix E.
Following soil removal, the excavation was backfilled with clean imported
backfill material. The imported backfill material consisted primarily of brown
silty clays.
E. Free Product Investigation and Recovery Report
Not applicable.
F. Groundwater and Surface Water Investigation
Not applicable.
G. Initial Response and Abatement Activities
See Section B.
H. Excavation of Contaminated Soil
See Section D.
I. Conclusions and Recommendations:
In January 2022, one inactive 550-gallon heating oil UST was removed from the
site. Approximately 19.2 tons of impacted soils were excavated for off -site
disposal. Analytical results of post -excavation confirmation soil samples indicate
that concentrations do not exceed DEQ MSCCs.
Based on the results of the initial abatement activities, impacted soil has been
adequately removed to concentrations below MSCCs. As a result, H&H
recommends that DEQ issue a no further action (NFA) letter for the UST incident.
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Table 1
Summary of Heating Oil UST Soil Sample Results
724 W. Sugar Creek Road
Charlotte, North Carolina
H&H Job. No. CHP-046
5030/
3550/
Analytical Method
8015C
8015C
MADEP
MADEP
MADEP
MADEP
MADEP
MADEP
MADEP
MADEP
8260B
8270D
U
In
U
U
U
U
In
U
Contaminant of Concern
a
Q
z
Q
o
E
0
Q
a°
N
o0
_00
co
U
O
N
U
N
U
U
O
O
U
U
U
U
U
O
U(Z
U
U
U
Date
Sample
Incident
=
_
_
_
_
= Q
=
= o
m
Sample ID
p
Collected
Source Area
Depth ft
p ( )
Phase
>
>
w
°
=
wQ
>
wQ
6
"
Q
m
cn
UST-1 Stockpile
01/13/22
UST
5
CL
441
4,150
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
UST-1 North
01/13/22
UST
6
IA
NA
NA
<1.54
<5.76
<11.5
BRL
<15.3
<0.787
<17.8
BRL
0.008 J
ALL BRL
UST-1 South
01/13/22
UST
6
IA
NA
NA
<1.56
<5.82
<11.7
BRL
<15.6
<0.795
<18.1
BRL
0.009 J
ALL BRL
UST-1 East
01/13/22
UST
6
IA
NA
NA
<1.54
<5.77
<11.7
BRL
<15.4
<0.789
<18.0
BRL
0.006 J
ALL BRL
UST-1 West
01/13/22
UST
6
IA
NA
NA
<1.47
<5.51
<11.1
BRL
<14.7
<0.753
<17.1
BRL
0.006 J
ALL BRL
UST-1 Base
01/13/22
UST
9
IA
NA
NA
<1.52
<5.66
<11.4
BRL
<15.2
<0.775
<17.5
BRL
0.004 J
ALL BRL
Action Level (mg/kg)
50
100
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Soil to Ground Water MSCC (mg/kg)
NS
NS
68
NS
NS
540
NS
NS
NS
31
24
Varies
Residential MSCC (mg/kg)
NS
NS
625
NS
NS
1,500
31,200
NS
NS
469
14,000
Varies
Industrial/Commercial MSCC (mg/kg)
NS
NS
9,340
NS
NS
40,000
467,000
NS
NS
7,000
210,000
Varies
Notes:
Apart from VPH and EPH, only those compounds detected are shown.
Concentrations are reported in milligrams per kilogram (mg/kg).
UST = Underground Storage Tank Basin; CL = Closure Sample; IA = Initial Abatement Sample; TPH = Total Petroleum Hydrocarbons; GRO = Gasoline Range Organics; DRO = Diesel Range Organics; MADEP =
Massachusetts Department of Environmental Protection; VPH = Volatile Petroleum Hydrocarbons; EPH = Extractable Petroleum Hydrocarbons; NA = Not Analyzed; NS = Not Specified; MSCC = Maximum Soil
Contaminant Concentration; BRL = Below Reporting Limits; J = Estimated value between method detection limit and laboratory reporting limit.
Table 1 (Page 1 of 1)
https:/Iharthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Charlotte Mecklenburg Housing Partnership - CHP/CHP-046 Yuma St UST Geophysical/01 13 2022 UST Removal/Soil Data.xls
2/1/2022 Hart & Hickman, PC

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Lake Plaza
USGS The National' Map: NatioAal Boundaries Dataset, 3DEP Elevation
Program, Geographic -.Names Information System, National Hydrography
Dataset, National Land Cover Database, Nafional Structures Dataset,
-
------ "and National Transportation Dataset; USGS Global Ecosystems; U.S.
o Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data;
U.S. Depaqment of State Humanitarian Information Unit; and NOAA
National'Centers fof Environmental Information, U.S. Coastal Relief
Model. Data refreshed August, 2021.
0 2,000 4,000
(9 SCALE IN FEET
U.S.G.S. QUADRANGLE MAP
DERITA, NORTH CAROLINA 2013
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)

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PARCEL LINE
17_11 APPROXIMATE LOCATION OF UST
SOIL SAMPLE LOCATION
NOTES
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY, 2021.
2. BASE DATA OBTAINED FROM MECKLENBURG COUNTY
GIS,2022.
N
APPROXIMATE
0 30 60
mommommommmimmi
SCALE IN FEET
SITE AND SAMPLE LOCATIONS MAP
—IFCF
726 W. SUGAR CREEK ROAD
CHARLOTTE, NORTH CAROLINA
• 2923 South Tryon Street -Suite 100
hart h i c k m a n Charlotte, North Carolina 28203
704-586-0007(p)704-586-0373(f
SMARTER ENVIRONMENTAL SOLUTIONS License # C-1269 / #C-245 Geology
DATE: 1-27-22 REVISION NO. 0
JOB NO. CHP-046 FIGURE NO. 2

Appendix A
UST Removal Permit Application
14
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CHARLOTTE FIRE DEPARTMENT
FIRE MARSHAL'S OFFICE
Tank Removal and Safeguarding Permit Application
Applicant
This is the company name and mailing address of the tank removal company.
Name BUCKEYE ELM CONTRACTING
Address: Po Box 1o26
Phone Number:
City/State: MOCKSVILLE N.C.
Cell Number: [phone]
Location and Type of Project
Zip Code: 27028
This is the facility name and address of the tank removal project. If vacant property, indicate "Vacant" for facility name.
Facility Name: VACANT Address: 724 &726 SUGAR CREEK ROAD CHARLOTTE NC
Type of Project: r,7 Tank Removal El Tank Abandonment Tank Type: ❑A/G ©B/G
Tank Information
If more than 4 tanks, complete a separate sheet.
Tank 1) Product: FUEL OIL Size: 1000 GAL Tank 2) Product: FUEL OIL size: 550 GAL
Tank 3) Product: Size: Tank 4) Product: Size:
Tanks Transported To: RECYCLING YARD
Responsible Applicant
Nance: MARK MABE
Title: SOUTHEASTERN DIVISION MGR
Signature: Date:
I certify that the information provided nd contained herein is true and accurate to the best of my knowledge. The issuance of a
permit shall not be deemed as approva to violate any provisions of the North Carolina State Fire Code. The code official has the
right to inspect the site to ensure compliance with provisions of thefire ire code, and to issue a Stop Work Order for unsafe practices.
NOTE! A site plan of the iob site shall be submitted with this application
Return the completed and signed application, site plan, and check to:
Charlotte Fire Department — Fire Prevention Bureau
500 Dalton Avenue
Charlotte, North Carolina 28206
Phone: [phone] Email: [e-mail]
Enclosed Checks Must be Payable to "The City of Charlotte"
If you wish to pay by credit card, contact the Fire Prevention Bureau Office to provide necessary information.
Permit Code: _� 6 Fee: $ 235
CFD Office Use Only
Check No.
Issue Date: /
Issued by Inspector:
Information Collected By:
Entry Date: / / -
Permit No.
Entered By:
Emp. #:

Appendix B
Certificate of Disposal and Non -Hazardous Waste Manifest — Residual Liquids
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-Aw
AE!XIC3
CORPORATION
1703 Vargrave Street
Winston-Salem, NC 27107
ph 336-725-5844
fax [phone]
• !: ,;1,111
,!
Evo Corporation does hereby certify that 267 gallons of non -hazardous product
received on 1/13/2022 from:
Generator: Mayfield Apartments. LLC
Originating at: 724 & 726 W. Sugar Creek Road
Charlotte, NC
EC Waste 1D #: 012220
has been disposed of by Eva Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
Signature
Thomas W. Hammett
CEO
Evo Corporation
www.evocorp.net

EVO CORPORATION
1703 Vargrave Streets Winston-Salem, NC 27107
--------------- ------------- --- __---------------------------------- _._.__._.._.._.W_..-_._-_....---._-_._--_ -
MATERIAL DESCRIPTION 'QUANTITY `VVEI H
Gross Weight (lb ),
Empty Weight ht (Ib )_:
Net Wei ght (Iles);
Quantity � ,
- 7
Nel ate Hai,
ont rnln me
Tons Drums Pails Sacs Yards Other: ' A
INFORMATIONe.___________._____________________..___________
L---- _____ ____________________.______-_-m--_
Transporter: j Phone -
Truck ; q Contact:
As- the transporter, I certify that the materials described above being shipped render this nor -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate_
Driver Icr�tor� _. _ .. ' ---f""�.__.-_-.....__.._-___ Date;
__.__.-_--___-____.-------------- r,-------- __--_.___-.--__-___--_.__...............__._._-.._-__-..---.__-._-.-.____.___.
FACILITY INFORMA I N
Evo Project - 0122201703 ---
.v Phone: - --
5844
Muston-Salem NC 27107 Tony Usher
Cor rtct.
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and or disposal in a manner that has beer, authorized by the State of forth Carolina.
0 rPwiQdLLC
FacilitySignature: ate
White/Facility Canary/invoice

Appendix C
Tank Disposal Certificate
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SMARTER ENVIRONMENTAL SOLUTIONS

/AO`M�Nh6
BUCKEYE ELM
CONTRACTING
CERTIFICATE OF DISMANTLING & DESTRUCTION
This certificate confirms the dismantling and destruction of (one) 550-gallon steel underground storage
tank removed from 724 W. Sugar Creek Road, Charlotte, NC on January 13, 2022.
The tank was transported to CMC Commercial Metals at 419 Atando Avenue, Charlotte, NC 28206 for
recycling.
Mark Mabe January 13, 2022 20-22-0006
Project Manager Date Buckeye Elm Job Number

Appendix D
Certificate of Disposal, Non -Hazardous Waste Manifests, and Weight Tickets -
Impacted Soil
14
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ENVIRONMENTAL SOILS, INC.
APPROVAL#
LOCATION OF SOIL:
TRANSPORTER:
TIME:
DATE:
DRIVER SIGNATURE
TIME:
DATE:
DRIVER SIGNATURE
TIME:
DATE:
DRIVER SIGNATURE
TI M E:
DATE:
DRIVER SIGNATURE
P.O. BOX 295
LATTIMORE, N.C. 28089
704-434-0075
NON -HAZARDOUS PETROLEUM CONTAMINATED SOIL
TRUCK #
LICENSE #
TRUCK#_
LICENSE #
TRUCK #_
LICENSE #
TRUCK #-
LICENSE #
MANIFEST #
INSPECTED & ACCEPTED BY ENVIRONMENTAL SOILS, INC.
SUPERVISOR'S SIGNATURE
GROSS WT.
LBS.
TARE WT.
LBS.
1 1 T WT<,
L '.
GROSS WT.
LBS.
TARE WT.
LBS.
NNE 1t T
L
GROSS WT.
LBS.
TARE: WT.
LBS.
LBS;
GROSS WT.
LBS.
TARE WT.
LBS.
TOTAL NET WT.
TOTAL EQUIV-TONS

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] - Fax [phone]
Non -Hazardous Waste Manifest #
Date f � 0q9, Load Number _
(numbered sequentially as trucks are dispatched)
EA17RONAIIENTAL CONSULE4NT i��
Contact: 4JQA&-) des. Phonetot �15 �� Fax:
.A I
GENER
Add?eD�ssl
Contact:
147ASTE ORIGJ7VATIONP0INT Complete Address:
Class &.Type of Contaminate in soil "n-
SOURCE OFCONE434LIV iTION- (ex. UST or other source)
GENEP,4TORS CERTIFICWTIONOFWASTE CONSTITUENTS: In lieu ofsubmitting analytical data (methods
8240 and 8270) verifying that the waste in question does not contain o2ganic constitztents other tl?an those which would
norn2ally appear in analysis of virgin petrolewn p -oduct residue, lam submitting this Certificate of Waste
Constituents. I certify that I ant familiarwith the source of contamination of the soil and further certify the source, to
the best of sny knowledge, contains no contaminants other than that listed above.
?, �00 UAICO" Nw y
TRANSPORTER: M uWro G p � tLT GM 01 A)(..e- - U l/ Gv k ; l�) &
Contact: N a6N-- 70 - 9 QQ - 41 �_5 Phone: .70 4 -q 60 ` � 165
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivers, to the t
facility designate. -Z i -1
Carrier Signature: Date: { I
TRUCK #: 111 Q qa - TAG #: VOLUME. 0
TRUCK DRIVER SIGNATURE:-� DATE:
DESTINATION Environmental Soils Inc. 910 Croyvdy Rd, Shelby, NC 29150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facility Signature:
Signature:
Company Name
Date. I - 11, s�-�2 2
Date: 5
Title:
White/Facility Canary/Invoice Goldenrod/Generator Pink/Carrier

ENVIRONMENTAL SOILS, INC.
P.O. BOX 295
LATTIMORE N.C. 28089-0489
704/434-0075
[phone] FAX
Job Name:
Truck# P'yl L)- Ll ! >
Gross Wgt.
Tare Wgt:
Net Wgt..
Tons:
PUBLIC WEIGHMAS T ER
LICENSE EXPIRES JUNE 30, 202:•
Weighed by: ^ fin' RICE
II�E sfY4LI c3� �d€t7�GLi
_NVIfONMENTAL SOILS, INC.
P.O. BOX 295
LATTIMORE, N.C. 28089-0489
704/434-0075
[phone] FAX
Job Name:
Tr_+uck#
25
Gross Wgt.:
Tare Wgt:
Net Wgt_:
Tons:
PUBLIC WEIGHMASTER
Weighed by: LICENSE EXPIRES JUNE 30, 2042
MATI: RICE
INVALID UNLESS SIGNED

Appendix E
Laboratory Analytical Report
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

Waypointo
ANALYTICAL
1 /21 /2022
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-013-0026
Client Project Description: CHP-046
Dear Andrew Besu:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/13/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
a'-1
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 92

Waypoint.0
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2022
North Carolina
State Program
402
12/31/2022
South Carolina
State Program
99012
07/31/2022
South Carolina
State Program
99012
12/31/2021
Page 1 of 1 00016/22-013-0026
Page 2 of 92

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Sample Summary Table
Report Number: 22-013-0026
Client Project Description: CHP-046
Lab No Client Sample ID Matrix Date Collected Date Received
92274
UST-1
Base
Solids
01/13/2022
12:35
01/13/2022
15:45
92275
UST-1
North
Solids
01/13/2022
12:45
01/13/2022
15:45
92276
UST-1
South
Solids
01/13/2022
13:05
01/13/2022
15:45
92277
UST-1
East
Solids
01/13/2022
13:00
01/13/2022
15:45
92278
UST-1
West
Solids
01/13/2022
12:55
01/13/2022
15:45
92279
UST-1
Stockpile
Solids
01/13/2022
12:25
01/13/2022
15:45
Page 3 of 92

Waypoint. (2)
449 Springbrook Rd, Charlotte, NC
28217
Main 704.529.6364
ANALYTICAL
www.waypointana
lyti ca I som
Summary of Detected Analytes
Project:
C H P-046
Report Number: 22-013-0026
Client Sample ID Lab Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
UST-1 Base
V 92274
8260D
Acetone
0.004
mg/Kg
- dry
0.002
01/14/2022 12:15
J
SW-DRYWT
Moisture
19.5
%
01/19/202212:09
UST-1 North
V 92275
8260D
Acetone
0.008
mg/Kg
- dry
0.003
01/14/2022 12:43
J
SW-DRYWT
Moisture
20.8
%
01/19/202212:09
UST-1 South
V 92276
8260D
Acetone
0.009
mq/Kg
- dry
0.003
01/14/2022 13:10
J
SW-DRYWT
Moisture
21.6
%
01/19/202212:09
UST-1 East
V 92277
8260D
Acetone
0.006
mq/Kg
- dry
0.003
01/14/2022 13:38
J
SW-DRYWT
Moisture
21.0
%
01/19/202212:09
UST-1 West
V 92278
8260D
Acetone
0.006
mq/Kg
- dry
0.002
01/14/2022 14:06
J
SW-DRYWT
Moisture
17.2
%
01/19/202212:09
UST-1 Stockpile
V 92279
8015C DRO
Diesel Range Organics (C10-C28)
4150
mg/Kg
- dry
295
01/20/2022 13:25
8015C GRO
Gasoline Range Organics (C6-C10)
441
mg/Kg
- dry
0.562
01/14/2022 08:53
SW-DRYWT
Moisture
20.9
%
01/19/202212:09
Page 4 of 92

Waypointo
ANALYTICAL
Client: Hart & Hickman (Charlotte)
Project: CHP-046
Lab Report Number: 22-013-0026
Date: 1 /21 /2022
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
CASE NARRATIVE
Massachusetts EPH Method MADEP-EPH
Analyte: Aliphatic C9-C18
QC Batch No: V14062/V13950
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
37300 ug/kg which calculates to a recovery of 46.5% which is within the acceptable recovery range.
Sample 92278 (UST-1 West)
Analyte: Aliphatic C9-C18
QC Batch No: V14062/V13950
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual MS result was
36600ug/kg which calculates to a recovery of 45.76% which is inside the acceptable recovery range.
Analyte: Aliphatic C9-C18
QC Batch No: V14062/V13950
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual MS result
was 35500ug/kg which calculates to a recovery of 44.16% which is inside the acceptable recovery range.
Total Petroleum Hydrocarbons - Extractable Method 8015C DRO
Sample 92080
Analyte: Diesel Range Organics (C10-C28)
QC Batch No: V14020/V13929
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Analyte: Diesel Range Organics (C10-C28)
QC Batch No: V14020/V13929
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Sample 92279 (UST-1 Stockpile)
Analyte: o-Terphenyl
QC Batch No: V14020/V13929
Surrogate(s) flagged for recovery outside QC limits in this project sample due to a required dilution. The dilution
factor resulted in surrogate concentration(s) below the minimum detectable level. Batch QC samples (method
blank and laboratory control samples) all showed surrogates within QC limits.
Semivolatile Organic Compounds - GUMS Method 8270E
Analyte: 2,4-Dinitrophenol
QC Batch No: V13927/V13898
Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual
result was 939 ug/kg which calculates to a recovery of 56.3% which is within the acceptable recovery range.
Sample 92274 (UST-1 Base)
Analyte: 2,4-Dinitrophenol
QC Batch No: V13927/V13898
Page 5 of 92

Waypointo
ANALYTICAL
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was
1230 ug/kg which calculates to a recovery of 73.7% which is within the acceptable recovery range.
Analyte: 2,4-Dinitrophenol
QC Batch No: V13927/V13898
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1120 ug/kg which calculates to a recovery of 67% which is within the acceptable recovery range.
Analyte: 2,4-Dinitrophenol
QC Batch No: V14113/V13898
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
1050 ug/kg which calculates to a recovery of 62.7% which is within the acceptable recovery range.
Analyte: 3,3'-Dichlorobenzidine
QC Batch No: V13927/V13898
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
550 ug/kg which calculates to a recovery of 32.9% which is within the acceptable recovery range.
Sample 92274 (UST-1 Base)
Analyte: 3,3'-Dichlorobenzidine
QC Batch No: V13927/V13898
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was
689 ug/kg which calculates to a recovery of 41.4% which is within the acceptable recovery range.
Analyte: 3,3'-Dichlorobenzidine
QC Batch No: V13927/V13898
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 634
ug/kg which calculates to a recovery of 37.8% which is within the acceptable recovery range.
Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V13927/V13898
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
964 ug/kg which calculates to a recovery of 57.8% which is within the acceptable recovery range.
Sample 92274 (UST-1 Base)
Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V13927/V13898
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1070 ug/kg which calculates to a recovery of 64.3% which is within the acceptable recovery range.
Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V13927/V13898
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was
1170 ug/kg which calculates to a recovery of 70.3% which is within the acceptable recovery range.
Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V14113/V13898
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
1100 ug/kg which calculates to a recovery of 66.2% which is within the acceptable recovery range.
Analyte: Benzoic Acid
QC Batch No: V13927/V13898
Page 6 of 92

Waypointo
ANALYTICAL
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
432 ug/kg which calculates to a recovery of 25.9% which is within the acceptable recovery range.
Sample 92274 (UST-1 Base)
Analyte: Benzoic Acid
QC Batch No: V13927/V13898
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was
1010 ug/kg which calculates to a recovery of 60.4% which is within the acceptable recovery range.
Analyte: Benzoic Acid
QC Batch No: V1 3927/V1 3898
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 876
ug/kg which calculates to a recovery of 52.4% which is within the acceptable recovery range.
Analyte: Benzoic Acid
QC Batch No: V14113/V13898
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
513 ug/kg which calculates to a recovery of 30.8% which is within the acceptable recovery range.
Sample 92274 (UST-1 Base)
Analyte: Indeno(1,2,3-cd)pyrene
QC Batch No: V13927/V13898
Relative Percent Difference (RPD) for the MS duplicate analysis was outside of the allowable QC limits.
Sample 92278 (UST-1 West)
Analyte: 2,4-Dinitrophenol
QC Batch No: V14113/V13928
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was
1260 ug/kg which calculates to a recovery of 75.4% which is within the acceptable recovery range.
Analyte: 2,4-Dinitrophenol
QC Batch No: V14113/V13928
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1230 ug/kg which calculates to a recovery of 73.7% which is within the acceptable recovery range.
Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V14113/V13928
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was
1230 ug/kg which calculates to a recovery of 73.7% which is within the acceptable recovery range.
Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V14113/V13928
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1200 ug/kg which calculates to a recovery of 71.8% which is within the acceptable recovery range.
Analyte: Benzoic Acid
QC Batch No: V14113/V13928
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was
1070 ug/kg which calculates to a recovery of 64.3% which is within the acceptable recovery range.
Analyte: Benzoic Acid
QC Batch No: V14113/V13928
Page 7 of 92

Waypointo
ANALYTICAL
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1050 ug/kg which calculates to a recovery of 63% which is within the acceptable recovery range.
Page 8 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92274 Matrix: Solids
Sample ID: UST-1 Base Sampled: 1/13/2022 12:35
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Moisture
19.5 %
1 01/19/2212:09 SJL SW-DRYWT
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions J Estimated value L Limit Exceeded
MQL Method Quantitation Limit
Page 9 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92274
Matrix: Solids
Sample ID: UST-1 Base
Sampled:
1/13/2022 12:35
Analytical Method: 8260D
Prep Batch(es):
V13890
01/14/22 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
0.0043
mg/Kg - dry
0.002
0.024
1
01/14/22 12:15
TBL
V13891
Acrolein
<0.001
mg/Kg - dry
0.001
0.024
1
01/14/22 12:15
TBL
V13891
Acrylonitrile
<0.0009
mg/Kg - dry
0.0009
0.024
1
01/14/22 12:15
TBL
V13891
Benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:15
TBL
V13891
Bromobenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:15
TBL
V13891
Bromochloromethane
<0.0010
mg/Kg - dry
0.0010
0.006
1
01/14/22 12:15
TBL
V13891
Bromodichloromethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
Bromoform
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
Bromomethane
<0.002
mg/Kg - dry
0.002
0.012
1
01/14/22 12:15
TBL
V13891
n-Butylbenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:15
TBL
V13891
sec -Butyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:15
TBL
V13891
tert-Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:15
TBL
V13891
Carbon Disulfide
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 12:15
TBL
V13891
Carbon Tetrachloride
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
Chlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 12:15
TBL
V13891
Chlorodibromomethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
Chloroethane
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 12:15
TBL
V13891
Chloroform
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
Chloromethane
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 12:15
TBL
V13891
2-Chlorotoluene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:15
TBL
V13891
4-Chlorotoluene
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 12:15
TBL
V13891
Di -Isopropyl Ether (DIPE)
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 12:15
TBL
V13891
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 10 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92274
Matrix: Solids
Sample ID: UST-1 Base
Sampled:
1/13/2022 12:35
Analytical Method: 8260D
Prep Batch(es):
V13890
01/14/22 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.0005
mg/Kg - dry
0.0005
0.012
1
01/14/22 12:15
TBL
V13891
1,2-Dibromoethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:15
TBL
V13891
Dibromomethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:15
TBL
V13891
1,2-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.006
1
01/14/22 12:15
TBL
V13891
1,3-Dichlorobenzene
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 12:15
TBL
V13891
1,4-Dichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:15
TBL
V13891
Dichlorodifluoromethane
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 12:15
TBL
V13891
1,1-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
1,2-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
1,1-Dichloroethene
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 12:15
TBL
V13891
cis- 1,2-Dich loroethene
<0.0010
mg/Kg - dry
0.0010
0.006
1
01/14/22 12:15
TBL
V13891
trans-1,2-Dichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
1,2-Dichloropropane
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 12:15
TBL
V13891
1,3-Dichloropropane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:15
TBL
V13891
2,2-Dichloropropane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
1,1-Dichloropropene
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 12:15
TBL
V13891
cis- 1,3-Dich loropropene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:15
TBL
V13891
trans-1,3-Dichloropropene
<0.0010
mg/Kg - dry
0.0010
0.006
1
01/14/22 12:15
TBL
V13891
Ethanol
<0.017
mg/Kg - dry
0.017
0.310
1
01/14/22 12:15
TBL
V13891
Ethylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:15
TBL
V13891
Ethyl Tertiary Butyl Ether (ETBE)
<0.001
mg/Kg - dry
0.001
0.062
1
01/14/22 12:15
TBL
V13891
Hexachlorobutadiene
<0.0010
mg/Kg - dry
0.0010
0.012
1
01/14/22 12:15
TBL
V13891
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 11 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92274
Matrix: Solids
Sample ID: UST-1 Base
Sampled:
1/13/2022 12:35
Analytical Method: 8260D
Prep Batch(es):
V13890
01/14/22 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
n-Hexane
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 12:15
TBL
V13891
2-Hexanone
<0.0008
mg/Kg - dry
0.0008
0.024
1
01/14/22 12:15
TBL
V13891
Isopropyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:15
TBL
V13891
4-Isopropyl toluene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
Methyl Ethyl Ketone (MEK)
<0.0008
mg/Kg - dry
0.0008
0.024
1
01/14/22 12:15
TBL
V13891
Methyl tert-butyl ether (MTBE)
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 12:15
TBL
V13891
4-Methyl-2-Pentanone
<0.018
mg/Kg - dry
0.018
0.024
1
01/14/22 12:15
TBL
V13891
Methylene Chloride
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 12:15
TBL
V13891
Naphthalene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 12:15
TBL
V13891
n-Propylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:15
TBL
V13891
Styrene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
1,1,1,2-Tetrachloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
1,1,2,2-Tetrachloroethane
<0.0004
mg/Kg - dry
0.0004
0.006
1
01/14/22 12:15
TBL
V13891
Tetrachloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
Toluene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 12:15
TBL
V13891
1,2,3-Trichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.012
1
01/14/22 12:15
TBL
V13891
1,2,4-Trichlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 12:15
TBL
V13891
1,1,1-Trichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
1,1,2-Trichloroethane
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:15
TBL
V13891
Trichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:15
TBL
V13891
Trichlorofluoromethane
<0.002
mg/Kg - dry
0.002
0.012
1
01/14/22 12:15
TBL
V13891
1,2,3-Trichloropropane
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 12:15
TBL
V13891
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 12 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Report Date : 01/21/2022
Received : 01/13/2022
Lab No : 92274 Matrix: Solids
Sample ID: UST-1 Base Sampled: 1/13/2022 12:35
Analytical Method: 8260D Prep Batch(es): V13890 01/14/22 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:15
TBL
V13891
1,3,5-Trimethyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:15
TBL
V13891
Vinyl Acetate
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 12:15
TBL
V13891
Vinyl Chloride
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 12:15
TBL
V13891
o-Xylene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:15
TBL
V13891
m,p-Xylene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 12:15
TBL
V13891
Xylene (Total)
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:15
V13891
Surrogate:4-Bromofluorobenzene
98.8
Limits:70-130%
1 01/14/22 12:15 TBL
V13891
Surrogate: Dibromofluoromethane
97.7
Limits:
84-123%
1 01/14/22 12:15 TBL
V13891
Surrogate: Toluene-d8
85.8
Limits:
76-129%
1 01/14/22 12:15 TBL
V13891
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.144
mg/Kg - dry
0.144
0.821
1
01/18/22 18:29
JMV
V13927
Acenaphthylene
<0.130
mg/Kg - dry
0.130
0.821
1
01/18/22 18:29
JMV
V13927
Aniline
<0.188
mg/Kg - dry
0.188
0.821
1
01/18/22 18:29
JMV
V13927
Anthracene
<0.177
mg/Kg - dry
0.177
0.821
1
01/18/22 18:29
JMV
V13927
Benzo(a)anthracene
<0.172
mg/Kg - dry
0.172
0.821
1
01/18/22 18:29
JMV
V13927
Benzo(a)pyrene
<0.182
mg/Kg - dry
0.182
0.821
1
01/18/22 18:29
JMV
V13927
Benzo(b)fluoranthene
<0.181
mg/Kg - dry
0.181
0.821
1
01/18/22 18:29
JMV
V13927
Benzo(g,h,i)perylene
<0.168
mg/Kg - dry
0.168
0.821
1
01/18/22 18:29
JMV
V13927
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 13 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92274
Matrix: Solids
Sample ID: UST-1 Base
Sampled:
1/13/2022 12:35
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.170
mg/Kg - dry
0.170
0.821
1
01/18/22 18:29
JMV
V13927
Benzoic Acid
<0.720
mg/Kg - dry
0.720
2.48
1
01/18/22 18:29
JMV
V13927
Benzyl alcohol
<0.130
mg/Kg - dry
0.130
0.821
1
01/18/22 18:29
JMV
V13927
Bis(2-Chloroethoxy)methane
<0.146
mg/Kg - dry
0.146
0.821
1
01/18/22 18:29
JMV
V13927
Bis(2-Chloroethyl)ether
<0.132
mg/Kg - dry
0.132
0.821
1
01/18/22 18:29
JMV
V13927
Bis(2-Chloroisopropyl)ether
<0.168
mg/Kg - dry
0.168
0.409
1
01/18/22 18:29
JMV
V13927
Bis(2-ethylhexyl)phthalate
<0.149
mg/Kg - dry
0.149
0.821
1
01/18/22 18:29
JMV
V13927
4-13romophenyl phenyl ether
<0.135
mg/Kg - dry
0.135
0.821
1
01/18/22 18:29
JMV
V13927
Butyl benzyl phthalate
<0.140
mg/Kg - dry
0.140
0.409
1
01/18/22 18:29
JMV
V13927
4-Chloro-3-methylphenol
<0.114
mg/Kg - dry
0.114
0.821
1
01/18/22 18:29
JMV
V13927
4-Chloroaniline
<0.139
mg/Kg - dry
0.139
0.409
1
01/18/22 18:29
JMV
V13927
2-Chloronaphthalene
<0.144
mg/Kg - dry
0.144
0.821
1
01/18/22 18:29
JMV
V13927
2-Chlorophenol
<0.122
mg/Kg - dry
0.122
0.821
1
01/18/22 18:29
JMV
V13927
4-Chlorophenyl phenyl ether
<0.156
mg/Kg - dry
0.156
1.24
1
01/18/22 18:29
JMV
V13927
Chrysene
<0.176
mg/Kg - dry
0.176
0.821
1
01/18/22 18:29
JMV
V13927
Dibenz(a,h)anthracene
<0.285
mg/Kg - dry
0.285
0.821
1
01/18/22 18:29
JMV
V13927
Dibenzofuran
<0.147
mg/Kg - dry
0.147
0.821
1
01/18/22 18:29
JMV
V13927
1,2-Dichlorobenzene
<0.117
mg/Kg - dry
0.117
0.821
1
01/18/22 18:29
JMV
V13927
1,3-Dichlorobenzene
<0.120
mg/Kg - dry
0.120
0.821
1
01/18/22 18:29
JMV
V13927
1,4-Dichlorobenzene
<0.121
mg/Kg - dry
0.121
0.409
1
01/18/22 18:29
JMV
V13927
3,3'-Dichlorobenzidine
<0.182
mg/Kg - dry
0.182
0.821
1
01/18/22 18:29
JMV
V13927
2,4-Dichlorophenol
<0.119
mg/Kg - dry
0.119
0.821
1
01/18/22 18:29
JMV
V13927
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 14 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92274
Matrix: Solids
Sample ID: UST-1 Base
Sampled:
1/13/2022 12:35
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.223
mg/Kg - dry
0.223
0.821
1
01/18/22 18:29
JMV
V13927
Dimethyl phthalate
<0.216
mg/Kg - dry
0.216
0.821
1
01/18/22 18:29
JMV
V13927
2,4-Dimethyl phenol
<0.134
mg/Kg - dry
0.134
0.409
1
01/18/22 18:29
JMV
V13927
Di-n-butyl phthalate
<0.132
mg/Kg - dry
0.132
0.821
1
01/18/22 18:29
JMV
V13927
4,6-Dinitro-2-methylphenol
<0.298
mg/Kg - dry
0.298
1.86
1
01/18/22 18:29
JMV
V13927
2,4-Dinitrophenol
<0.645
mg/Kg - dry
0.645
1.86
1
01/18/22 18:29
JMV
V13927
2,4-Dinitrotoluene
<0.120
mg/Kg - dry
0.120
0.821
1
01/18/22 18:29
JMV
V13927
2,6-Dinitrotoluene
<0.134
mg/Kg - dry
0.134
0.821
1
01/18/22 18:29
JMV
V13927
Di-n-Octyl Phthalate
<0.177
mg/Kg - dry
0.177
0.409
1
01/18/22 18:29
JMV
V13927
Fluoranthene
<0.152
mg/Kg - dry
0.152
0.821
1
01/18/22 18:29
JMV
V13927
Fluorene
<0.159
mg/Kg - dry
0.159
0.821
1
01/18/22 18:29
JMV
V13927
Hexachlorobenzene
<0.131
mg/Kg - dry
0.131
0.821
1
01/18/22 18:29
JMV
V13927
Hexachlorobutadiene
<0.121
mg/Kg - dry
0.121
0.821
1
01/18/22 18:29
JMV
V13927
Hexachlorocyclopentadiene
<0.195
mg/Kg - dry
0.195
0.821
1
01/18/22 18:29
JMV
V13927
Hexachloroethane
<0.098
mg/Kg - dry
0.098
0.821
1
01/18/22 18:29
JMV
V13927
Indeno(1,2,3-cd)pyrene
<0.222
mg/Kg - dry
0.222
0.821
1
01/18/22 18:29
JMV
V13927
Isophorone
<0.237
mg/Kg - dry
0.237
0.821
1
01/18/22 18:29
JMV
V13927
1-Methylnaphthalene
<0.131
mg/Kg - dry
0.131
0.821
1
01/18/22 18:29
JMV
V13927
2-Methylnaphthalene
<0.124
mg/Kg - dry
0.124
0.821
1
01/18/22 18:29
JMV
V13927
2-Methylphenol
<0.120
mg/Kg - dry
0.120
0.821
1
01/18/22 18:29
JMV
V13927
3&4 Methylphenol
<0.105
mg/Kg - dry
0.105
0.821
1
01/18/22 18:29
JMV
V13927
Naphthalene
<0.178
mg/Kg - dry
0.178
0.821
1
01/18/22 18:29
JMV
V13927
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 15 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Report Number : 22-013-0026
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
REPORT OF ANAL YSIS
Report Date : 01/21/2022
Received : 01/13/2022
Lab No : 92274
Sample ID: UST-1 Base
Matrix: Solids
Sampled: 1/13/2022 12:35
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.120
mg/Kg - dry
0.120
0.821
1
01/18/22 18:29
JMV
V13927
3-Nitroaniline
<0.149
mg/Kg - dry
0.149
0.821
1
01/18/22 18:29
JMV
V13927
4-Nitroaniline
<0.115
mg/Kg - dry
0.115
0.409
1
01/18/22 18:29
JMV
V13927
Nitrobenzene
<0.144
mg/Kg - dry
0.144
0.409
1
01/18/22 18:29
JMV
V13927
2-Nitrophenol
<0.110
mg/Kg - dry
0.110
0.821
1
01/18/22 18:29
JMV
V13927
4-Nitrophenol
<0.145
mg/Kg - dry
0.145
0.821
1
01/18/22 18:29
JMV
V13927
N-N itrosodimethyla mine
<0.326
mg/Kg - dry
0.326
0.821
1
01/18/22 18:29
JMV
V13927
N-Nitrosodiphenylamine
<0.224
mg/Kg - dry
0.224
0.821
1
01/18/22 18:29
JMV
V13927
N-Nitroso-di-n-propylamine
<0.146
mg/Kg - dry
0.146
0.821
1
01/18/22 18:29
JMV
V13927
Pentachlorophenol
<0.431
mg/Kg - dry
0.431
1.24
1
01/18/22 18:29
JMV
V13927
Phenanthrene
<0.258
mg/Kg - dry
0.258
0.821
1
01/18/22 18:29
JMV
V13927
Phenol
<0.139
mg/Kg - dry
0.139
0.821
1
01/18/22 18:29
JMV
V13927
Pyrene
<0.166
mg/Kg - dry
0.166
0.821
1
01/18/22 18:29
JMV
V13927
Pyridine
<0.098
mg/Kg - dry
0.098
0.409
1
01/18/22 18:29
JMV
V13927
1,2,4-Trichlorobenzene
<0.132
mg/Kg - dry
0.132
0.821
1
01/18/22 18:29
JMV
V13927
2,4,5-Trichlorophenol
<0.119
mg/Kg - dry
0.119
0.821
1
01/18/22 18:29
JMV
V13927
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 16 of 92

Waypowint
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
hwd
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92274 Matrix: Solids
Sample ID: UST-1 Base Sampled: 1/13/2022 12:35
Analytical Method: 8270E Prep Batch(es): V13898 01/18/22 08:30
Prep Method: 3546
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
2,4,6-Trichlorophenol
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d 14
Surrogate: 2,4,6-Tribromophenol
<0.120 mg/Kg - dry
0.120 0.821
72.5
Limits: 34-121%
62.9
Limits: 44-115%
77.8
Limits: 35-115%
68.9
Limits: 37-122%
69.5
Limits: 54-127%
55.4
Limits: 39-132%
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
1 01/18/22 18:29 JMV V13927
1 01/18/22 18:29 JMV V13927
1 01/18/22 18:29 JMV V13927
1 01/18/22 18:29 JMV V13927
1 01/18/22 18:29 JMV V13927
1 01/18/22 18:29 JMV V13927
1 01/18/22 18:29 JMV V13927
DF Dilution Factor
MQL Method Quantitation Limit
Page 17 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026
Lab No : 92274
Sample ID: UST-1 Base
REPOR T OF A NA L YSIS
Matrix: Solids
Sampled: 1/13/2022 12:35
Analytical Method: MADEP-EPH
Prep Batch(es):
V13950 01/19/22 09:35
Prep Method: MAEPH (Prep)
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Aliphatic C9-C18
<11.4
mg/Kg - dry
11.4 61.9 1
01/20/22 14:32 JC1
V14062
Aliphatic C19-C36
<15.2
mg/Kg - dry
15.2 61.9 1
01/20/22 14:32 JC1
V14062
Aromatic C11-C22
<17.5
mg/Kg - dry
17.5 61.9 1
01/20/22 14:32 JC1
V14062
Surrogate:2-Bromonaphthalene
82.7
Limits:40-140%
1 01/20/22 14:32 JC1
V14062
Surrogate: Chlorooctadecane
93.5
Limits: 40-140%
1 01/20/22 14:32 JC1
V14062
Surrogate: OTP Surrogate
65.3
Limits: 40-140%
1 01/20/22 14:32 JC1
V14062
Surrogate:2-Fluorobiphenyl
71.4
Limits:40-140%
1 01/20/22 14:32 JC1
V14062
Analytical Method: MADEP-VPH
Prep Batch(es):
V13839 01/14/22 08:00
Prep Method: MAVPH (Prep)
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Aliphatic C5-C8 <1.52
mg/Kg - dry
1.52 9.94
100 01/14/22 14:17 TBL
V13840
Aliphatic C9-C12 <5.66
mg/Kg - dry
5.66 9.94
100 01/14/22 14:17 TBL
V13840
Aromatic C9-C10 <0.775
mg/Kg - dry
0.775 9.94
100 01/14/22 14:17 TBL
V13840
Surrogate: 2,5-Dibromotoluene (FID)
88.6
Limits: 70-130%
100 01/14/22 14:17 TBL
V13840
Surrogate: 2,5-Dibromotoluene (PID)
82.3
Limits: 70-130%
100 01/14/22 14:17 TBL
V13840
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 18 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92275 Matrix: Solids
Sample ID : UST-1 North Sampled: 1/13/2022 12:45
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Moisture
20.8 %
1 01/19/2212:09 SJL SW-DRYWT
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions J Estimated value L Limit Exceeded
MQL Method Quantitation Limit
Page 19 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92275
Matrix: Solids
Sample ID : UST-1 North
Sampled:
1/13/2022 12:45
Analytical Method: 8260D
Prep Batch(es):
V13890
01/14/22 08:00
Prep Method: 5035
LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
0.0083
mg/Kg - dry
0.003
0.025
1
01/14/22 12:43
TBL
V13891
Acrolein
<0.001
mg/Kg - dry
0.001
0.025
1
01/14/22 12:43
TBL
V13891
Acrylonitrile
<0.0009
mg/Kg - dry
0.0009
0.025
1
01/14/22 12:43
TBL
V13891
Benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:43
TBL
V13891
Bromobenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:43
TBL
V13891
Bromochloromethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
Bromodichloromethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
Bromoform
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
Bromomethane
<0.002
mg/Kg - dry
0.002
0.012
1
01/14/22 12:43
TBL
V13891
n-Butylbenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:43
TBL
V13891
sec -Butyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:43
TBL
V13891
tert-Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:43
TBL
V13891
Carbon Disulfide
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 12:43
TBL
V13891
Carbon Tetrachloride
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
Chlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 12:43
TBL
V13891
Chlorodibromomethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
Chloroethane
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 12:43
TBL
V13891
Chloroform
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
Chloromethane
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 12:43
TBL
V13891
2-Chlorotoluene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:43
TBL
V13891
4-Chlorotoluene
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 12:43
TBL
V13891
Di -Isopropyl Ether (DIPE)
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 12:43
TBL
V13891
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 20 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026
REPORT OF ANAL YSIS
Lab No : 92275 Matrix: Solids
Sample ID : UST-1 North Sampled: 1/13/2022 12:45
Analytical Method: 8260D Prep Batch(es): V13890 01/14/22 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 12:43
TBL
V13891
1,2-Dibromoethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:43
TBL
V13891
Dibromomethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:43
TBL
V13891
1,2-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.006
1
01/14/22 12:43
TBL
V13891
1,3-Dichlorobenzene
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 12:43
TBL
V13891
1,4-Dichlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 12:43
TBL
V13891
Dichlorodifluoromethane
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 12:43
TBL
V13891
1,1-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
1,2-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
1,1-Dichloroethene
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 12:43
TBL
V13891
cis- 1,2-Dich loroethene
<0.0010
mg/Kg - dry
0.0010
0.006
1
01/14/22 12:43
TBL
V13891
trans-1,2-Dichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
1,2-Dichloropropane
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:43
TBL
V13891
1,3-Dichloropropane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:43
TBL
V13891
2,2-Dichloropropane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
1,1-Dichloropropene
<0.0010
mg/Kg - dry
0.0010
0.006
1
01/14/22 12:43
TBL
V13891
cis- 1,3-Dich loropropene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:43
TBL
V13891
trans-1,3-Dichloropropene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
Ethanol
<0.017
mg/Kg - dry
0.017
0.315
1
01/14/22 12:43
TBL
V13891
Ethylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:43
TBL
V13891
Ethyl Tertiary Butyl Ether (ETBE) <0.001
mg/Kg - dry
0.001
0.063
1
01/14/22 12:43
TBL
V13891
Hexachlorobutadiene
<0.0010
mg/Kg - dry
0.0010
0.012
1
01/14/22 12:43
TBL
V13891
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 21 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92275
Matrix: Solids
Sample ID : UST-1 North
Sampled:
1/13/2022 12:45
Analytical Method: 8260D
Prep Batch(es):
V13890
01/14/22 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
n-Hexane
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 12:43
TBL
V13891
2-Hexanone
<0.0008
mg/Kg - dry
0.0008
0.025
1
01/14/22 12:43
TBL
V13891
Isopropyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:43
TBL
V13891
4-Isopropyl toluene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
Methyl Ethyl Ketone (MEK)
<0.0008
mg/Kg - dry
0.0008
0.025
1
01/14/22 12:43
TBL
V13891
Methyl tert-butyl ether (MTBE)
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 12:43
TBL
V13891
4-Methyl-2-Pentanone
<0.018
mg/Kg - dry
0.018
0.025
1
01/14/22 12:43
TBL
V13891
Methylene Chloride
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 12:43
TBL
V13891
Naphthalene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 12:43
TBL
V13891
n-Propylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:43
TBL
V13891
Styrene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
1,1,1,2-Tetrachloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
1,1,2,2-Tetrachloroethane
<0.0004
mg/Kg - dry
0.0004
0.006
1
01/14/22 12:43
TBL
V13891
Tetrachloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
Toluene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 12:43
TBL
V13891
1,2,3-Trichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.012
1
01/14/22 12:43
TBL
V13891
1,2,4-Trichlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 12:43
TBL
V13891
1,1,1-Trichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
1,1,2-Trichloroethane
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:43
TBL
V13891
Trichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 12:43
TBL
V13891
Trichlorofluoromethane
<0.002
mg/Kg - dry
0.002
0.012
1
01/14/22 12:43
TBL
V13891
1,2,3-Trichloropropane
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 12:43
TBL
V13891
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 22 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Report Date : 01/21/2022
Received : 01/13/2022
Lab No : 92275 Matrix: Solids
Sample ID : UST-1 North Sampled: 1/13/2022 12:45
Analytical Method: 8260D Prep Batch(es): V13890 01/14/22 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:43
TBL
V13891
1,3,5-Trimethyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 12:43
TBL
V13891
Vinyl Acetate
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 12:43
TBL
V13891
Vinyl Chloride
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 12:43
TBL
V13891
o-Xylene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:43
TBL
V13891
m,p-Xylene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 12:43
TBL
V13891
Xylene (Total)
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 12:43
V13891
Surrogate:4-Bromofluorobenzene
98.8
Limits:70-130%
1 01/14/22 12:43 TBL
V13891
Surrogate: Dibromofluoromethane
99.0
Limits:
84-123%
1 01/14/22 12:43 TBL
V13891
Surrogate: Toluene-d8
86.7
Limits:
76-129%
1 01/14/22 12:43 TBL
V13891
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.146
mg/Kg - dry
0.146
0.833
1
01/18/22 18:52
JMV
V13927
Acenaphthylene
<0.132
mg/Kg - dry
0.132
0.833
1
01/18/22 18:52
JMV
V13927
Aniline
<0.191
mg/Kg - dry
0.191
0.833
1
01/18/22 18:52
JMV
V13927
Anthracene
<0.180
mg/Kg - dry
0.180
0.833
1
01/18/22 18:52
JMV
V13927
Benzo(a)anthracene
<0.175
mg/Kg - dry
0.175
0.833
1
01/18/22 18:52
JMV
V13927
Benzo(a)pyrene
<0.185
mg/Kg - dry
0.185
0.833
1
01/18/22 18:52
JMV
V13927
Benzo(b)fluoranthene
<0.184
mg/Kg - dry
0.184
0.833
1
01/18/22 18:52
JMV
V13927
Benzo(g,h,i)perylene
<0.171
mg/Kg - dry
0.171
0.833
1
01/18/22 18:52
JMV
V13927
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 23 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92275
Matrix: Solids
Sample ID : UST-1 North
Sampled:
1/13/2022 12:45
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.172
mg/Kg - dry
0.172
0.833
1
01/18/22 18:52
JMV
V13927
Benzoic Acid
<0.732
mg/Kg - dry
0.732
2.53
1
01/18/22 18:52
JMV
V13927
Benzyl alcohol
<0.132
mg/Kg - dry
0.132
0.833
1
01/18/22 18:52
JMV
V13927
Bis(2-Chloroethoxy)methane
<0.148
mg/Kg - dry
0.148
0.833
1
01/18/22 18:52
JMV
V13927
Bis(2-Chloroethyl)ether
<0.135
mg/Kg - dry
0.135
0.833
1
01/18/22 18:52
JMV
V13927
Bis(2-Chloroisopropyl)ether
<0.171
mg/Kg - dry
0.171
0.416
1
01/18/22 18:52
JMV
V13927
Bis(2-ethylhexyl)phthalate
<0.151
mg/Kg - dry
0.151
0.833
1
01/18/22 18:52
JMV
V13927
4-13romophenyl phenyl ether
<0.137
mg/Kg - dry
0.137
0.833
1
01/18/22 18:52
JMV
V13927
Butyl benzyl phthalate
<0.142
mg/Kg - dry
0.142
0.416
1
01/18/22 18:52
JMV
V13927
4-Chloro-3-methylphenol
<0.116
mg/Kg - dry
0.116
0.833
1
01/18/22 18:52
JMV
V13927
4-Chloroaniline
<0.141
mg/Kg - dry
0.141
0.416
1
01/18/22 18:52
JMV
V13927
2-Chloronaphthalene
<0.146
mg/Kg - dry
0.146
0.833
1
01/18/22 18:52
JMV
V13927
2-Chlorophenol
<0.123
mg/Kg - dry
0.123
0.833
1
01/18/22 18:52
JMV
V13927
4-Chlorophenyl phenyl ether
<0.159
mg/Kg - dry
0.159
1.26
1
01/18/22 18:52
JMV
V13927
Chrysene
<0.179
mg/Kg - dry
0.179
0.833
1
01/18/22 18:52
JMV
V13927
Dibenz(a,h)anthracene
<0.290
mg/Kg - dry
0.290
0.833
1
01/18/22 18:52
JMV
V13927
Dibenzofuran
<0.150
mg/Kg - dry
0.150
0.833
1
01/18/22 18:52
JMV
V13927
1,2-Dichlorobenzene
<0.119
mg/Kg - dry
0.119
0.833
1
01/18/22 18:52
JMV
V13927
1,3-Dichlorobenzene
<0.122
mg/Kg - dry
0.122
0.833
1
01/18/22 18:52
JMV
V13927
1,4-Dichlorobenzene
<0.123
mg/Kg - dry
0.123
0.416
1
01/18/22 18:52
JMV
V13927
3,3'-Dichlorobenzidine
<0.185
mg/Kg - dry
0.185
0.833
1
01/18/22 18:52
JMV
V13927
2,4-Dichlorophenol
<0.120
mg/Kg - dry
0.120
0.833
1
01/18/22 18:52
JMV
V13927
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 24 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92275
Matrix: Solids
Sample ID : UST-1 North
Sampled:
1/13/2022 12:45
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.227
mg/Kg - dry
0.227
0.833
1
01/18/22 18:52
JMV
V13927
Dimethyl phthalate
<0.219
mg/Kg - dry
0.219
0.833
1
01/18/22 18:52
JMV
V13927
2,4-Dimethyl phenol
<0.136
mg/Kg - dry
0.136
0.416
1
01/18/22 18:52
JMV
V13927
Di-n-butyl phthalate
<0.135
mg/Kg - dry
0.135
0.833
1
01/18/22 18:52
JMV
V13927
4,6-Dinitro-2-methylphenol
<0.303
mg/Kg - dry
0.303
1.89
1
01/18/22 18:52
JMV
V13927
2,4-Dinitrophenol
<0.656
mg/Kg - dry
0.656
1.89
1
01/18/22 18:52
JMV
V13927
2,4-Dinitrotoluene
<0.121
mg/Kg - dry
0.121
0.833
1
01/18/22 18:52
JMV
V13927
2,6-Dinitrotoluene
<0.136
mg/Kg - dry
0.136
0.833
1
01/18/22 18:52
JMV
V13927
Di-n-Octyl Phthalate
<0.180
mg/Kg - dry
0.180
0.416
1
01/18/22 18:52
JMV
V13927
Fluoranthene
<0.155
mg/Kg - dry
0.155
0.833
1
01/18/22 18:52
JMV
V13927
Fluorene
<0.161
mg/Kg - dry
0.161
0.833
1
01/18/22 18:52
JMV
V13927
Hexachlorobenzene
<0.133
mg/Kg - dry
0.133
0.833
1
01/18/22 18:52
JMV
V13927
Hexachlorobutadiene
<0.123
mg/Kg - dry
0.123
0.833
1
01/18/22 18:52
JMV
V13927
Hexachlorocyclopentadiene
<0.198
mg/Kg - dry
0.198
0.833
1
01/18/22 18:52
JMV
V13927
Hexachloroethane
<0.100
mg/Kg - dry
0.100
0.833
1
01/18/22 18:52
JMV
V13927
Indeno(1,2,3-cd)pyrene
<0.226
mg/Kg - dry
0.226
0.833
1
01/18/22 18:52
JMV
V13927
Isophorone
<0.241
mg/Kg - dry
0.241
0.833
1
01/18/22 18:52
JMV
V13927
1-Methylnaphthalene
<0.133
mg/Kg - dry
0.133
0.833
1
01/18/22 18:52
JMV
V13927
2-Methylnaphthalene
<0.126
mg/Kg - dry
0.126
0.833
1
01/18/22 18:52
JMV
V13927
2-Methylphenol
<0.122
mg/Kg - dry
0.122
0.833
1
01/18/22 18:52
JMV
V13927
3&4 Methylphenol
<0.107
mg/Kg - dry
0.107
0.833
1
01/18/22 18:52
JMV
V13927
Naphthalene
<0.181
mg/Kg - dry
0.181
0.833
1
01/18/22 18:52
JMV
V13927
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 25 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Report Number : 22-013-0026
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
REPORT OF ANAL YSIS
Report Date : 01/21/2022
Received : 01/13/2022
Lab No : 92275
Sample ID : UST-1 North
Matrix: Solids
Sampled: 1/13/2022 12:45
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.122
mg/Kg - dry
0.122
0.833
1
01/18/22 18:52
JMV
V13927
3-Nitroaniline
<0.151
mg/Kg - dry
0.151
0.833
1
01/18/22 18:52
JMV
V13927
4-Nitroaniline
<0.117
mg/Kg - dry
0.117
0.416
1
01/18/22 18:52
JMV
V13927
Nitrobenzene
<0.146
mg/Kg - dry
0.146
0.416
1
01/18/22 18:52
JMV
V13927
2-Nitrophenol
<0.112
mg/Kg - dry
0.112
0.833
1
01/18/22 18:52
JMV
V13927
4-Nitrophenol
<0.147
mg/Kg - dry
0.147
0.833
1
01/18/22 18:52
JMV
V13927
N-N itrosodimethyla mine
<0.332
mg/Kg - dry
0.332
0.833
1
01/18/22 18:52
JMV
V13927
N-Nitrosodiphenylamine
<0.228
mg/Kg - dry
0.228
0.833
1
01/18/22 18:52
JMV
V13927
N-Nitroso-di-n-propylamine
<0.148
mg/Kg - dry
0.148
0.833
1
01/18/22 18:52
JMV
V13927
Pentachlorophenol
<0.438
mg/Kg - dry
0.438
1.26
1
01/18/22 18:52
JMV
V13927
Phenanthrene
<0.262
mg/Kg - dry
0.262
0.833
1
01/18/22 18:52
JMV
V13927
Phenol
<0.141
mg/Kg - dry
0.141
0.833
1
01/18/22 18:52
JMV
V13927
Pyrene
<0.169
mg/Kg - dry
0.169
0.833
1
01/18/22 18:52
JMV
V13927
Pyridine
<0.100
mg/Kg - dry
0.100
0.416
1
01/18/22 18:52
JMV
V13927
1,2,4-Trichlorobenzene
<0.135
mg/Kg - dry
0.135
0.833
1
01/18/22 18:52
JMV
V13927
2,4,5-Trichlorophenol
<0.121
mg/Kg - dry
0.121
0.833
1
01/18/22 18:52
JMV
V13927
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 26 of 92

Waypowint
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
hwd
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92275 Matrix: Solids
Sample ID : UST-1 North Sampled: 1/13/2022 12:45
Analytical Method: 8270E Prep Batch(es): V13898 01/18/22 08:30
Prep Method: 3546
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
2,4,6-Trichlorophenol
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d 14
Surrogate: 2,4,6-Tribromophenol
<0.121 mg/Kg - dry
0.121 0.833
82.9
Limits: 34-121%
70.7
Limits: 44-115%
88.0
Limits: 35-115%
71.9
Limits: 37-122%
73.1
Limits: 54-127%
57.7
Limits: 39-132%
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
1 01/18/22 18:52 JMV V13927
1 01/18/22 18:52 JMV V13927
1 01/18/22 18:52 JMV V13927
1 01/18/22 18:52 JMV V13927
1 01/18/22 18:52 JMV V13927
1 01/18/22 18:52 JMV V13927
1 01/18/22 18:52 JMV V13927
DF Dilution Factor
MQL Method Quantitation Limit
Page 27 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026
Lab No : 92275
Sample ID : UST-1 North
REPOR T OF A NA L YSIS
Matrix: Solids
Sampled: 1/13/2022 12:45
Analytical Method: MADEP-EPH
Prep Batch(es):
V13950 01/19/22 09:35
Prep Method: MAEPH (Prep)
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Aliphatic C9-C18
<11.5
mg/Kg - dry
11.5 62.6 1
01/20/22 15:09 JC1
V14062
Aliphatic C19-C36
<15.3
mg/Kg - dry
15.3 62.6 1
01/20/22 15:09 JC1
V14062
Aromatic C11-C22
<17.8
mg/Kg - dry
17.8 62.6 1
01/20/22 15:09 JC1
V14062
Surrogate:2-Bromonaphthalene
84.4
Limits:40-140%
1 01/20/22 15:09 JC1
V14062
Surrogate: Chlorooctadecane
98.5
Limits: 40-140%
1 01/20/22 15:09 JC1
V14062
Surrogate: OTP Surrogate
64.1
Limits: 40-140%
1 01/20/22 15:09 JC1
V14062
Surrogate:2-Fluorobiphenyl
68.3
Limits:40-140%
1 01/20/22 15:09 JC1
V14062
Analytical Method: MADEP-VPH
Prep Batch(es):
V13839 01/14/22 08:00
Prep Method: MAVPH (Prep)
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Aliphatic C5-C8 <1.54
mg/Kg - dry
1.54 10.1
100 01/14/22 14:41 TBL
V13840
Aliphatic C9-C12 <5.76
mg/Kg - dry
5.76 10.1
100 01/14/22 14:41 TBL
V13840
Aromatic C9-C10 <0.787
mg/Kg - dry
0.787 10.1
100 01/14/22 14:41 TBL
V13840
Surrogate: 2,5-Dibromotoluene (FID)
83.1
Limits: 70-130%
100 01/14/22 14:41 TBL
V13840
Surrogate: 2,5-Dibromotoluene (PID)
77.6
Limits: 70-130%
100 01/14/22 14:41 TBL
V13840
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 28 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92276 Matrix: Solids
Sample ID : UST-1 South Sampled: 1/13/2022 13:05
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Moisture
21.6 %
1 01/19/2212:09 SJL SW-DRYWT
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions J Estimated value L Limit Exceeded
MQL Method Quantitation Limit
Page 29 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92276
Matrix: Solids
Sample ID : UST-1 South
Sampled:
1/13/2022 13:05
Analytical Method: 8260D
Prep Batch(es):
V13890
01/14/22 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
0.0093
mg/Kg - dry
0.003
0.025
1
01/14/22 13:10
TBL
V13891
Acrolein
<0.001
mg/Kg - dry
0.001
0.025
1
01/14/22 13:10
TBL
V13891
Acrylonitrile
<0.0010
mg/Kg - dry
0.0010
0.025
1
01/14/22 13:10
TBL
V13891
Benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:10
TBL
V13891
Bromobenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:10
TBL
V13891
Bromochloromethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
Bromodichloromethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
Bromoform
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
Bromomethane
<0.002
mg/Kg - dry
0.002
0.012
1
01/14/22 13:10
TBL
V13891
n-Butylbenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:10
TBL
V13891
sec -Butyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:10
TBL
V13891
tert-Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:10
TBL
V13891
Carbon Disulfide
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 13:10
TBL
V13891
Carbon Tetrachloride
<0.002
mg/Kg - dry
0.002
0.006
1
01/14/22 13:10
TBL
V13891
Chlorobenzene
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 13:10
TBL
V13891
Chlorodibromomethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
Chloroethane
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:10
TBL
V13891
Chloroform
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
Chloromethane
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 13:10
TBL
V13891
2-Chlorotoluene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:10
TBL
V13891
4-Chlorotoluene
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 13:10
TBL
V13891
Di -Isopropyl Ether (DIPE)
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 13:10
TBL
V13891
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 30 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026
REPORT OF ANAL YSIS
Lab No : 92276 Matrix: Solids
Sample ID : UST-1 South Sampled: 1/13/2022 13:05
Analytical Method: 8260D Prep Batch(es): V13890 01/14/22 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 13:10
TBL
V13891
1,2-Dibromoethane
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 13:10
TBL
V13891
Dibromomethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:10
TBL
V13891
1,2-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.006
1
01/14/22 13:10
TBL
V13891
1,3-Dichlorobenzene
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 13:10
TBL
V13891
1,4-Dichlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 13:10
TBL
V13891
Dichlorodifluoromethane
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:10
TBL
V13891
1,1-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
1,2-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
1,1-Dichloroethene
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 13:10
TBL
V13891
cis- 1,2-Dich loroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
trans- 1.2-Dichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
1,2-Dichloropropane
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:10
TBL
V13891
1,3-Dichloropropane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:10
TBL
V13891
2,2-Dichloropropane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
1,1-Dichloropropene
<0.0010
mg/Kg - dry
0.0010
0.006
1
01/14/22 13:10
TBL
V13891
cis- 1,3-Dich loropropene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:10
TBL
V13891
trans-1,3-Dichloropropene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
Ethanol
<0.017
mg/Kg - dry
0.017
0.318
1
01/14/22 13:10
TBL
V13891
Ethylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:10
TBL
V13891
Ethyl Tertiary Butyl Ether (ETBE) <0.001
mg/Kg - dry
0.001
0.063
1
01/14/22 13:10
TBL
V13891
Hexachlorobutadiene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:10
TBL
V13891
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 31 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92276
Matrix: Solids
Sample ID : UST-1 South
Sampled:
1/13/2022 13:05
Analytical Method: 8260D
Prep Batch(es):
V13890
01/14/22 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
n-Hexane
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 13:10
TBL
V13891
2-Hexanone
<0.0008
mg/Kg - dry
0.0008
0.025
1
01/14/22 13:10
TBL
V13891
Isopropyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:10
TBL
V13891
4-Isopropyl toluene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
Methyl Ethyl Ketone (MEK)
<0.0008
mg/Kg - dry
0.0008
0.025
1
01/14/22 13:10
TBL
V13891
Methyl tert-butyl ether (MTBE)
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 13:10
TBL
V13891
4-Methyl-2-Pentanone
<0.019
mg/Kg - dry
0.019
0.025
1
01/14/22 13:10
TBL
V13891
Methylene Chloride
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:10
TBL
V13891
Naphthalene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:10
TBL
V13891
n-Propylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:10
TBL
V13891
Styrene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
1,1,1,2-Tetrachloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
1,1,2,2-Tetrachloroethane
<0.0004
mg/Kg - dry
0.0004
0.006
1
01/14/22 13:10
TBL
V13891
Tetrachloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
Toluene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 13:10
TBL
V13891
1,2,3-Trichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.012
1
01/14/22 13:10
TBL
V13891
1,2,4-Trichlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 13:10
TBL
V13891
1,1,1-Trichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
1,1,2-Trichloroethane
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:10
TBL
V13891
Trichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:10
TBL
V13891
Trichlorofluoromethane
<0.002
mg/Kg - dry
0.002
0.012
1
01/14/22 13:10
TBL
V13891
1,2,3-Trichloropropane
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 13:10
TBL
V13891
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 32 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Report Date : 01/21/2022
Received : 01/13/2022
Lab No : 92276 Matrix: Solids
Sample ID : UST-1 South Sampled: 1/13/2022 13:05
Analytical Method: 8260D Prep Batch(es): V13890 01/14/22 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:10
TBL
V13891
1,3,5-Trimethyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:10
TBL
V13891
Vinyl Acetate
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 13:10
TBL
V13891
Vinyl Chloride
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 13:10
TBL
V13891
o-Xylene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:10
TBL
V13891
m,p-Xylene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:10
TBL
V13891
Xylene (Total)
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:10
V13891
Surrogate:4-Bromofluorobenzene
97.1
Limits:70-130%
1 01/14/22 13:10 TBL
V13891
Surrogate: Dibromofluoromethane
100
Limits:
84-123%
1 01/14/22 13:10 TBL
V13891
Surrogate: Toluene-d8
86.4
Limits:
76-129%
1 01/14/22 13:10 TBL
V13891
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.147
mg/Kg - dry
0.147
0.841
1
01/18/22 19:15
JMV
V13927
Acenaphthylene
<0.133
mg/Kg - dry
0.133
0.841
1
01/18/22 19:15
JMV
V13927
Aniline
<0.193
mg/Kg - dry
0.193
0.841
1
01/18/22 19:15
JMV
V13927
Anthracene
<0.182
mg/Kg - dry
0.182
0.841
1
01/18/22 19:15
JMV
V13927
Benzo(a)anthracene
<0.177
mg/Kg - dry
0.177
0.841
1
01/18/22 19:15
JMV
V13927
Benzo(a)pyrene
<0.187
mg/Kg - dry
0.187
0.841
1
01/18/22 19:15
JMV
V13927
Benzo(b)fluoranthene
<0.186
mg/Kg - dry
0.186
0.841
1
01/18/22 19:15
JMV
V13927
Benzo(g,h,i)perylene
<0.173
mg/Kg - dry
0.173
0.841
1
01/18/22 19:15
JMV
V13927
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 33 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92276
Matrix: Solids
Sample ID : UST-1 South
Sampled:
1/13/2022 13:05
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.174
mg/Kg - dry
0.174
0.841
1
01/18/22 19:15
JMV
V13927
Benzoic Acid
<0.739
mg/Kg - dry
0.739
2.55
1
01/18/22 19:15
JMV
V13927
Benzyl alcohol
<0.133
mg/Kg - dry
0.133
0.841
1
01/18/22 19:15
JMV
V13927
Bis(2-Chloroethoxy)methane
<0.150
mg/Kg - dry
0.150
0.841
1
01/18/22 19:15
JMV
V13927
Bis(2-Chloroethyl)ether
<0.136
mg/Kg - dry
0.136
0.841
1
01/18/22 19:15
JMV
V13927
Bis(2-Chloroisopropyl)ether
<0.173
mg/Kg - dry
0.173
0.420
1
01/18/22 19:15
JMV
V13927
Bis(2-ethylhexyl)phthalate
<0.153
mg/Kg - dry
0.153
0.841
1
01/18/22 19:15
JMV
V13927
4-13romophenyl phenyl ether
<0.139
mg/Kg - dry
0.139
0.841
1
01/18/22 19:15
JMV
V13927
Butyl benzyl phthalate
<0.144
mg/Kg - dry
0.144
0.420
1
01/18/22 19:15
JMV
V13927
4-Chloro-3-methylphenol
<0.117
mg/Kg - dry
0.117
0.841
1
01/18/22 19:15
JMV
V13927
4-Chloroaniline
<0.142
mg/Kg - dry
0.142
0.420
1
01/18/22 19:15
JMV
V13927
2-Chloronaphthalene
<0.147
mg/Kg - dry
0.147
0.841
1
01/18/22 19:15
JMV
V13927
2-Chlorophenol
<0.125
mg/Kg - dry
0.125
0.841
1
01/18/22 19:15
JMV
V13927
4-Chlorophenyl phenyl ether
<0.160
mg/Kg - dry
0.160
1.28
1
01/18/22 19:15
JMV
V13927
Chrysene
<0.181
mg/Kg - dry
0.181
0.841
1
01/18/22 19:15
JMV
V13927
Dibenz(a,h)anthracene
<0.293
mg/Kg - dry
0.293
0.841
1
01/18/22 19:15
JMV
V13927
Dibenzofuran
<0.151
mg/Kg - dry
0.151
0.841
1
01/18/22 19:15
JMV
V13927
1,2-Dichlorobenzene
<0.120
mg/Kg - dry
0.120
0.841
1
01/18/22 19:15
JMV
V13927
1,3-Dichlorobenzene
<0.124
mg/Kg - dry
0.124
0.841
1
01/18/22 19:15
JMV
V13927
1,4-Dichlorobenzene
<0.124
mg/Kg - dry
0.124
0.420
1
01/18/22 19:15
JMV
V13927
3,3'-Dichlorobenzidine
<0.187
mg/Kg - dry
0.187
0.841
1
01/18/22 19:15
JMV
V13927
2,4-Dichlorophenol
<0.122
mg/Kg - dry
0.122
0.841
1
01/18/22 19:15
JMV
V13927
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 34 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92276
Matrix: Solids
Sample ID : UST-1 South
Sampled:
1/13/2022 13:05
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.229
mg/Kg - dry
0.229
0.841
1
01/18/22 19:15
JMV
V13927
Dimethyl phthalate
<0.221
mg/Kg - dry
0.221
0.841
1
01/18/22 19:15
JMV
V13927
2,4-Dimethyl phenol
<0.137
mg/Kg - dry
0.137
0.420
1
01/18/22 19:15
JMV
V13927
Di-n-butyl phthalate
<0.136
mg/Kg - dry
0.136
0.841
1
01/18/22 19:15
JMV
V13927
4,6-Dinitro-2-methylphenol
<0.306
mg/Kg - dry
0.306
1.91
1
01/18/22 19:15
JMV
V13927
2,4-Dinitrophenol
<0.663
mg/Kg - dry
0.663
1.91
1
01/18/22 19:15
JMV
V13927
2,4-Dinitrotoluene
<0.123
mg/Kg - dry
0.123
0.841
1
01/18/22 19:15
JMV
V13927
2,6-Dinitrotoluene
<0.137
mg/Kg - dry
0.137
0.841
1
01/18/22 19:15
JMV
V13927
Di-n-Octyl Phthalate
<0.182
mg/Kg - dry
0.182
0.420
1
01/18/22 19:15
JMV
V13927
Fluoranthene
<0.156
mg/Kg - dry
0.156
0.841
1
01/18/22 19:15
JMV
V13927
Fluorene
<0.163
mg/Kg - dry
0.163
0.841
1
01/18/22 19:15
JMV
V13927
Hexachlorobenzene
<0.135
mg/Kg - dry
0.135
0.841
1
01/18/22 19:15
JMV
V13927
Hexachlorobutadiene
<0.124
mg/Kg - dry
0.124
0.841
1
01/18/22 19:15
JMV
V13927
Hexachlorocyclopentadiene
<0.200
mg/Kg - dry
0.200
0.841
1
01/18/22 19:15
JMV
V13927
Hexachloroethane
<0.101
mg/Kg - dry
0.101
0.841
1
01/18/22 19:15
JMV
V13927
Indeno(1,2,3-cd)pyrene
<0.228
mg/Kg - dry
0.228
0.841
1
01/18/22 19:15
JMV
V13927
Isophorone
<0.243
mg/Kg - dry
0.243
0.841
1
01/18/22 19:15
JMV
V13927
1-Methylnaphthalene
<0.135
mg/Kg - dry
0.135
0.841
1
01/18/22 19:15
JMV
V13927
2-Methylnaphthalene
<0.127
mg/Kg - dry
0.127
0.841
1
01/18/22 19:15
JMV
V13927
2-Methylphenol
<0.123
mg/Kg - dry
0.123
0.841
1
01/18/22 19:15
JMV
V13927
3&4 Methylphenol
<0.108
mg/Kg - dry
0.108
0.841
1
01/18/22 19:15
JMV
V13927
Naphthalene
<0.183
mg/Kg - dry
0.183
0.841
1
01/18/22 19:15
JMV
V13927
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 35 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Report Number : 22-013-0026
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
REPORT OF ANAL YSIS
Report Date : 01/21/2022
Received : 01/13/2022
Lab No : 92276
Sample ID : UST-1 South
Matrix: Solids
Sampled: 1/13/2022 13:05
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.123
mg/Kg - dry
0.123
0.841
1
01/18/22 19:15
JMV
V13927
3-Nitroaniline
<0.153
mg/Kg - dry
0.153
0.841
1
01/18/22 19:15
JMV
V13927
4-Nitroaniline
<0.119
mg/Kg - dry
0.119
0.420
1
01/18/22 19:15
JMV
V13927
Nitrobenzene
<0.147
mg/Kg - dry
0.147
0.420
1
01/18/22 19:15
JMV
V13927
2-Nitrophenol
<0.113
mg/Kg - dry
0.113
0.841
1
01/18/22 19:15
JMV
V13927
4-Nitrophenol
<0.149
mg/Kg - dry
0.149
0.841
1
01/18/22 19:15
JMV
V13927
N-N itrosodimethyla mine
<0.335
mg/Kg - dry
0.335
0.841
1
01/18/22 19:15
JMV
V13927
N-Nitrosodiphenylamine
<0.230
mg/Kg - dry
0.230
0.841
1
01/18/22 19:15
JMV
V13927
N-Nitroso-di-n-propylamine
<0.150
mg/Kg - dry
0.150
0.841
1
01/18/22 19:15
JMV
V13927
Pentachlorophenol
<0.442
mg/Kg - dry
0.442
1.28
1
01/18/22 19:15
JMV
V13927
Phenanthrene
<0.265
mg/Kg - dry
0.265
0.841
1
01/18/22 19:15
JMV
V13927
Phenol
<0.142
mg/Kg - dry
0.142
0.841
1
01/18/22 19:15
JMV
V13927
Pyrene
<0.170
mg/Kg - dry
0.170
0.841
1
01/18/22 19:15
JMV
V13927
Pyridine
<0.101
mg/Kg - dry
0.101
0.420
1
01/18/22 19:15
JMV
V13927
1,2,4-Trichlorobenzene
<0.136
mg/Kg - dry
0.136
0.841
1
01/18/22 19:15
JMV
V13927
2,4,5-Trichlorophenol
<0.122
mg/Kg - dry
0.122
0.841
1
01/18/22 19:15
JMV
V13927
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 36 of 92

Waypowint
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
hwd
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92276 Matrix: Solids
Sample ID : UST-1 South Sampled: 1/13/2022 13:05
Analytical Method: 8270E
Prep Method: 3546
Test Results
2,4,6-Trichlorophenol <0.123
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d 14
Surrogate: 2,4,6-Tribromophenol
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
Prep Batch(es): V13898 01/18/22 08:30
Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
mg/Kg - dry 0.123 0.841
81.1
Limits: 34-121%
67.7
Limits: 44-115%
82.9
Limits: 35-115%
70.7
Limits: 37-122%
73.1
Limits: 54-127%
58.4
Limits: 39-132%
1 01/18/22 19:15 JMV V13927
1 01/18/22 19:15 JMV V13927
1 01/18/22 19:15 JMV V13927
1 01/18/22 19:15 JMV V13927
1 01/18/22 19:15 JMV V13927
1 01/18/22 19:15 JMV V13927
1 01/18/22 19:15 JMV V13927
DF Dilution Factor
MQL Method Quantitation Limit
Page 37 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026
Lab No : 92276
Sample ID : UST-1 South
REPOR T OF A NA L YSIS
Matrix: Solids
Sampled: 1/13/2022 13:05
Analytical Method: MADEP-EPH
Prep Batch(es):
V13950 01/19/22 09:35
Prep Method: MAEPH (Prep)
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Aliphatic C9-C18
<11.7
mg/Kg - dry
11.7 63.6 1
01/20/22 15:45 JC1
V14062
Aliphatic C19-C36
<15.6
mg/Kg - dry
15.6 63.6 1
01/20/22 15:45 JC1
V14062
Aromatic C11-C22
<18.1
mg/Kg - dry
18.1 63.6 1
01/20/22 15:45 JC1
V14062
Surrogate:2-Bromonaphthalene
98.7
Limits:40-140%
1 01/20/22 15:45 JC1
V14062
Surrogate: Chlorooctadecane
93.5
Limits: 40-140%
1 01/20/22 15:45 JC1
V14062
Surrogate: OTP Surrogate
79.9
Limits: 40-140%
1 01/20/22 15:45 JC1
V14062
Surrogate:2-Fluorobiphenyl
80.5
Limits:40-140%
1 01/20/22 15:45 JC1
V14062
Analytical Method: MADEP-VPH
Prep Batch(es):
V13839 01/14/22 08:00
Prep Method: MAVPH (Prep)
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Aliphatic C5-C8 <1.56
mg/Kg - dry
1.56 10.2
100 01/14/22 15:05 TBL
V13840
Aliphatic C9-C12 <5.82
mg/Kg - dry
5.82 10.2
100 01/14/22 15:05 TBL
V13840
Aromatic C9-C10 <0.795
mg/Kg - dry
0.795 10.2
100 01/14/22 15:05 TBL
V13840
Surrogate: 2,5-Dibromotoluene (FID)
77.1
Limits: 70-130%
100 01/14/22 15:05 TBL
V13840
Surrogate: 2,5-Dibromotoluene (PID)
79.1
Limits: 70-130%
100 01/14/22 15:05 TBL
V13840
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 38 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92277 Matrix: Solids
Sample ID : UST-1 East Sampled: 1/13/2022 13:00
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Moisture
21.0 %
1 01/19/2212:09 SJL SW-DRYWT
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions J Estimated value L Limit Exceeded
MQL Method Quantitation Limit
Page 39 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92277
Matrix: Solids
Sample ID : UST-1 East
Sampled:
1/13/2022 13:00
Analytical Method: 8260D
Prep Batch(es):
V13890
01/14/22 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
0.0063
mg/Kg - dry
0.003
0.025
1
01/14/22 13:38
TBL
V13891
Acrolein
<0.001
mg/Kg - dry
0.001
0.025
1
01/14/22 13:38
TBL
V13891
Acrylonitrile
<0.0009
mg/Kg - dry
0.0009
0.025
1
01/14/22 13:38
TBL
V13891
Benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:38
TBL
V13891
Bromobenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:38
TBL
V13891
Bromochloromethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
Bromodichloromethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
Bromoform
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
Bromomethane
<0.002
mg/Kg - dry
0.002
0.012
1
01/14/22 13:38
TBL
V13891
n-Butylbenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:38
TBL
V13891
sec -Butyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:38
TBL
V13891
tert-Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:38
TBL
V13891
Carbon Disulfide
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 13:38
TBL
V13891
Carbon Tetrachloride
<0.002
mg/Kg - dry
0.002
0.006
1
01/14/22 13:38
TBL
V13891
Chlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 13:38
TBL
V13891
Chlorodibromomethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
Chloroethane
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:38
TBL
V13891
Chloroform
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
Chloromethane
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 13:38
TBL
V13891
2-Chlorotoluene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:38
TBL
V13891
4-Chlorotoluene
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 13:38
TBL
V13891
Di -Isopropyl Ether (DIPE)
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 13:38
TBL
V13891
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 40 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026
REPORT OF ANAL YSIS
Lab No : 92277 Matrix: Solids
Sample ID : UST-1 East Sampled: 1/13/2022 13:00
Analytical Method: 8260D Prep Batch(es): V13890 01/14/22 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 13:38
TBL
V13891
1,2-Dibromoethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:38
TBL
V13891
Dibromomethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:38
TBL
V13891
1,2-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.006
1
01/14/22 13:38
TBL
V13891
1,3-Dichlorobenzene
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 13:38
TBL
V13891
1,4-Dichlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 13:38
TBL
V13891
Dichlorodifluoromethane
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:38
TBL
V13891
1,1-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
1,2-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
1,1-Dichloroethene
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 13:38
TBL
V13891
cis- 1,2-Dich loroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
trans- 1.2-Dichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
1,2-Dichloropropane
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:38
TBL
V13891
1,3-Dichloropropane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:38
TBL
V13891
2,2-Dichloropropane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
1,1-Dichloropropene
<0.0010
mg/Kg - dry
0.0010
0.006
1
01/14/22 13:38
TBL
V13891
cis- 1,3-Dich loropropene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:38
TBL
V13891
trans-1,3-Dichloropropene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
Ethanol
<0.017
mg/Kg - dry
0.017
0.316
1
01/14/22 13:38
TBL
V13891
Ethylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:38
TBL
V13891
Ethyl Tertiary Butyl Ether (ETBE) <0.001
mg/Kg - dry
0.001
0.063
1
01/14/22 13:38
TBL
V13891
Hexachlorobutadiene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:38
TBL
V13891
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 41 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92277
Matrix: Solids
Sample ID : UST-1 East
Sampled:
1/13/2022 13:00
Analytical Method: 8260D
Prep Batch(es):
V13890
01/14/22 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
n-Hexane
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 13:38
TBL
V13891
2-Hexanone
<0.0008
mg/Kg - dry
0.0008
0.025
1
01/14/22 13:38
TBL
V13891
Isopropyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:38
TBL
V13891
4-Isopropyl toluene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
Methyl Ethyl Ketone (MEK)
<0.0008
mg/Kg - dry
0.0008
0.025
1
01/14/22 13:38
TBL
V13891
Methyl tert-butyl ether (MTBE)
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 13:38
TBL
V13891
4-Methyl-2-Pentanone
<0.018
mg/Kg - dry
0.018
0.025
1
01/14/22 13:38
TBL
V13891
Methylene Chloride
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:38
TBL
V13891
Naphthalene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:38
TBL
V13891
n-Propylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:38
TBL
V13891
Styrene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
1,1,1,2-Tetrachloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
1,1,2,2-Tetrachloroethane
<0.0004
mg/Kg - dry
0.0004
0.006
1
01/14/22 13:38
TBL
V13891
Tetrachloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
Toluene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 13:38
TBL
V13891
1,2,3-Trichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.012
1
01/14/22 13:38
TBL
V13891
1,2,4-Trichlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 13:38
TBL
V13891
1,1,1-Trichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
1,1,2-Trichloroethane
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:38
TBL
V13891
Trichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 13:38
TBL
V13891
Trichlorofluoromethane
<0.002
mg/Kg - dry
0.002
0.012
1
01/14/22 13:38
TBL
V13891
1,2,3-Trichloropropane
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 13:38
TBL
V13891
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 42 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Report Date : 01/21/2022
Received : 01/13/2022
Lab No : 92277 Matrix: Solids
Sample ID : UST-1 East Sampled: 1/13/2022 13:00
Analytical Method: 8260D Prep Batch(es): V13890 01/14/22 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:38
TBL
V13891
1,3,5-Trimethyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 13:38
TBL
V13891
Vinyl Acetate
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 13:38
TBL
V13891
Vinyl Chloride
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 13:38
TBL
V13891
o-Xylene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:38
TBL
V13891
m,p-Xylene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 13:38
TBL
V13891
Xylene (Total)
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 13:38
V13891
Surrogate:4-Bromofluorobenzene
98.2
Limits:70-130%
1 01/14/22 13:38 TBL
V13891
Surrogate: Dibromofluoromethane
101
Limits:
84-123%
1 01/14/22 13:38 TBL
V13891
Surrogate: Toluene-d8
86.7
Limits:
76-129%
1 01/14/22 13:38 TBL
V13891
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.146
mg/Kg - dry
0.146
0.836
1
01/18/22 19:38
JMV
V13927
Acenaphthylene
<0.132
mg/Kg - dry
0.132
0.836
1
01/18/22 19:38
JMV
V13927
Aniline
<0.192
mg/Kg - dry
0.192
0.836
1
01/18/22 19:38
JMV
V13927
Anthracene
<0.181
mg/Kg - dry
0.181
0.836
1
01/18/22 19:38
JMV
V13927
Benzo(a)anthracene
<0.175
mg/Kg - dry
0.175
0.836
1
01/18/22 19:38
JMV
V13927
Benzo(a)pyrene
<0.186
mg/Kg - dry
0.186
0.836
1
01/18/22 19:38
JMV
V13927
Benzo(b)fluoranthene
<0.184
mg/Kg - dry
0.184
0.836
1
01/18/22 19:38
JMV
V13927
Benzo(g,h,i)perylene
<0.172
mg/Kg - dry
0.172
0.836
1
01/18/22 19:38
JMV
V13927
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 43 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92277
Matrix: Solids
Sample ID : UST-1 East
Sampled:
1/13/2022 13:00
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.173
mg/Kg - dry
0.173
0.836
1
01/18/22 19:38
JMV
V13927
Benzoic Acid
<0.734
mg/Kg - dry
0.734
2.53
1
01/18/22 19:38
JMV
V13927
Benzyl alcohol
<0.132
mg/Kg - dry
0.132
0.836
1
01/18/22 19:38
JMV
V13927
Bis(2-Chloroethoxy)methane
<0.149
mg/Kg - dry
0.149
0.836
1
01/18/22 19:38
JMV
V13927
Bis(2-Chloroethyl)ether
<0.135
mg/Kg - dry
0.135
0.836
1
01/18/22 19:38
JMV
V13927
Bis(2-Chloroisopropyl)ether
<0.172
mg/Kg - dry
0.172
0.417
1
01/18/22 19:38
JMV
V13927
Bis(2-ethylhexyl)phthalate
<0.151
mg/Kg - dry
0.151
0.836
1
01/18/22 19:38
JMV
V13927
4-13romophenyl phenyl ether
<0.137
mg/Kg - dry
0.137
0.836
1
01/18/22 19:38
JMV
V13927
Butyl benzyl phthalate
<0.143
mg/Kg - dry
0.143
0.417
1
01/18/22 19:38
JMV
V13927
4-Chloro-3-methylphenol
<0.117
mg/Kg - dry
0.117
0.836
1
01/18/22 19:38
JMV
V13927
4-Chloroaniline
<0.141
mg/Kg - dry
0.141
0.417
1
01/18/22 19:38
JMV
V13927
2-Chloronaphthalene
<0.146
mg/Kg - dry
0.146
0.836
1
01/18/22 19:38
JMV
V13927
2-Chlorophenol
<0.124
mg/Kg - dry
0.124
0.836
1
01/18/22 19:38
JMV
V13927
4-Chlorophenyl phenyl ether
<0.159
mg/Kg - dry
0.159
1.27
1
01/18/22 19:38
JMV
V13927
Chrysene
<0.179
mg/Kg - dry
0.179
0.836
1
01/18/22 19:38
JMV
V13927
Dibenz(a,h)anthracene
<0.291
mg/Kg - dry
0.291
0.836
1
01/18/22 19:38
JMV
V13927
Dibenzofuran
<0.150
mg/Kg - dry
0.150
0.836
1
01/18/22 19:38
JMV
V13927
1,2-Dichlorobenzene
<0.119
mg/Kg - dry
0.119
0.836
1
01/18/22 19:38
JMV
V13927
1,3-Dichlorobenzene
<0.123
mg/Kg - dry
0.123
0.836
1
01/18/22 19:38
JMV
V13927
1,4-Dichlorobenzene
<0.123
mg/Kg - dry
0.123
0.417
1
01/18/22 19:38
JMV
V13927
3,3'-Dichlorobenzidine
<0.186
mg/Kg - dry
0.186
0.836
1
01/18/22 19:38
JMV
V13927
2,4-Dichlorophenol
<0.121
mg/Kg - dry
0.121
0.836
1
01/18/22 19:38
JMV
V13927
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 44 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92277
Matrix: Solids
Sample ID : UST-1 East
Sampled:
1/13/2022 13:00
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.227
mg/Kg - dry
0.227
0.836
1
01/18/22 19:38
JMV
V13927
Dimethyl phthalate
<0.220
mg/Kg - dry
0.220
0.836
1
01/18/22 19:38
JMV
V13927
2,4-Dimethyl phenol
<0.136
mg/Kg - dry
0.136
0.417
1
01/18/22 19:38
JMV
V13927
Di-n-butyl phthalate
<0.135
mg/Kg - dry
0.135
0.836
1
01/18/22 19:38
JMV
V13927
4,6-Dinitro-2-methylphenol
<0.303
mg/Kg - dry
0.303
1.90
1
01/18/22 19:38
JMV
V13927
2,4-Dinitrophenol
<0.658
mg/Kg - dry
0.658
1.90
1
01/18/22 19:38
JMV
V13927
2,4-Dinitrotoluene
<0.122
mg/Kg - dry
0.122
0.836
1
01/18/22 19:38
JMV
V13927
2,6-Dinitrotoluene
<0.136
mg/Kg - dry
0.136
0.836
1
01/18/22 19:38
JMV
V13927
Di-n-Octyl Phthalate
<0.181
mg/Kg - dry
0.181
0.417
1
01/18/22 19:38
JMV
V13927
Fluoranthene
<0.155
mg/Kg - dry
0.155
0.836
1
01/18/22 19:38
JMV
V13927
Fluorene
<0.162
mg/Kg - dry
0.162
0.836
1
01/18/22 19:38
JMV
V13927
Hexachlorobenzene
<0.134
mg/Kg - dry
0.134
0.836
1
01/18/22 19:38
JMV
V13927
Hexachlorobutadiene
<0.123
mg/Kg - dry
0.123
0.836
1
01/18/22 19:38
JMV
V13927
Hexachlorocyclopentadiene
<0.198
mg/Kg - dry
0.198
0.836
1
01/18/22 19:38
JMV
V13927
Hexachloroethane
<0.100
mg/Kg - dry
0.100
0.836
1
01/18/22 19:38
JMV
V13927
Indeno(1,2,3-cd)pyrene
<0.226
mg/Kg - dry
0.226
0.836
1
01/18/22 19:38
JMV
V13927
Isophorone
<0.241
mg/Kg - dry
0.241
0.836
1
01/18/22 19:38
JMV
V13927
1-Methylnaphthalene
<0.134
mg/Kg - dry
0.134
0.836
1
01/18/22 19:38
JMV
V13927
2-Methylnaphthalene
<0.126
mg/Kg - dry
0.126
0.836
1
01/18/22 19:38
JMV
V13927
2-Methylphenol
<0.122
mg/Kg - dry
0.122
0.836
1
01/18/22 19:38
JMV
V13927
3&4 Methylphenol
<0.107
mg/Kg - dry
0.107
0.836
1
01/18/22 19:38
JMV
V13927
Naphthalene
<0.182
mg/Kg - dry
0.182
0.836
1
01/18/22 19:38
JMV
V13927
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 45 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Report Number : 22-013-0026
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
REPORT OF ANAL YSIS
Report Date : 01/21/2022
Received : 01/13/2022
Lab No : 92277
Sample ID : UST-1 East
Matrix: Solids
Sampled: 1/13/2022 13:00
Analytical Method: 8270E
Prep Batch(es):
V13898
01/18/22 08:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.122
mg/Kg - dry
0.122
0.836
1
01/18/22 19:38
JMV
V13927
3-Nitroaniline
<0.151
mg/Kg - dry
0.151
0.836
1
01/18/22 19:38
JMV
V13927
4-Nitroaniline
<0.118
mg/Kg - dry
0.118
0.417
1
01/18/22 19:38
JMV
V13927
Nitrobenzene
<0.146
mg/Kg - dry
0.146
0.417
1
01/18/22 19:38
JMV
V13927
2-Nitrophenol
<0.112
mg/Kg - dry
0.112
0.836
1
01/18/22 19:38
JMV
V13927
4-Nitrophenol
<0.148
mg/Kg - dry
0.148
0.836
1
01/18/22 19:38
JMV
V13927
N-N itrosodimethyla mine
<0.332
mg/Kg - dry
0.332
0.836
1
01/18/22 19:38
JMV
V13927
N-Nitrosodiphenylamine
<0.229
mg/Kg - dry
0.229
0.836
1
01/18/22 19:38
JMV
V13927
N-Nitroso-di-n-propylamine
<0.149
mg/Kg - dry
0.149
0.836
1
01/18/22 19:38
JMV
V13927
Pentachlorophenol
<0.439
mg/Kg - dry
0.439
1.27
1
01/18/22 19:38
JMV
V13927
Phenanthrene
<0.263
mg/Kg - dry
0.263
0.836
1
01/18/22 19:38
JMV
V13927
Phenol
<0.141
mg/Kg - dry
0.141
0.836
1
01/18/22 19:38
JMV
V13927
Pyrene
<0.169
mg/Kg - dry
0.169
0.836
1
01/18/22 19:38
JMV
V13927
Pyridine
<0.100
mg/Kg - dry
0.100
0.417
1
01/18/22 19:38
JMV
V13927
1,2,4-Trichlorobenzene
<0.135
mg/Kg - dry
0.135
0.836
1
01/18/22 19:38
JMV
V13927
2,4,5-Trichlorophenol
<0.121
mg/Kg - dry
0.121
0.836
1
01/18/22 19:38
JMV
V13927
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 46 of 92

Waypowint
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
hwd
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92277 Matrix: Solids
Sample ID : UST-1 East Sampled: 1/13/2022 13:00
Analytical Method: 8270E Prep Batch(es): V13898 01/18/22 08:30
Prep Method: 3546
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
2,4,6-Trichlorophenol
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d 14
Surrogate: 2,4,6-Tribromophenol
<0.122 mg/Kg - dry
0.122 0.836
75.7
Limits: 34-121%
65.3
Limits: 44-115%
82.0
Limits: 35-115%
68.9
Limits: 37-122%
70.1
Limits: 54-127%
54.2
Limits: 39-132%
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
1 01/18/22 19:38 JMV V13927
1 01/18/22 19:38 JMV V13927
1 01/18/22 19:38 JMV V13927
1 01/18/22 19:38 JMV V13927
1 01/18/22 19:38 JMV V13927
1 01/18/22 19:38 JMV V13927
1 01/18/22 19:38 JMV V13927
DF Dilution Factor
MQL Method Quantitation Limit
Page 47 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026
Lab No : 92277
Sample ID : UST-1 East
REPOR T OF A NA L YSIS
Matrix: Solids
Sampled: 1/13/2022 13:00
Analytical Method: MADEP-EPH
Prep Batch(es):
V13950 01/19/22 09:35
Prep Method: MAEPH (Prep)
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Aliphatic C9-C18
<11.7
mg/Kg - dry
11.7 63.4 1
01/20/22 16:21 JC1
V14062
Aliphatic C19-C36
<15.4
mg/Kg - dry
15.4 63.4 1
01/20/22 16:21 JC1
V14062
Aromatic C11-C22
<18.0
mg/Kg - dry
18.0 63.4 1
01/20/22 16:21 JC1
V14062
Surrogate:2-Bromonaphthalene
91.3
Limits:40-140%
1 01/20/22 16:21 JC1
V14062
Surrogate: Chlorooctadecane
84.5
Limits: 40-140%
1 01/20/22 16:21 JC1
V14062
Surrogate: OTP Surrogate
68.0
Limits: 40-140%
1 01/20/22 16:21 JC1
V14062
Surrogate:2-Fluorobiphenyl
74.8
Limits:40-140%
1 01/20/22 16:21 JC1
V14062
Analytical Method: MADEP-VPH
Prep Batch(es):
V13839 01/14/22 08:00
Prep Method: MAVPH (Prep)
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Aliphatic C5-C8 <1.54
mg/Kg - dry
1.54 10.1
100 01/14/22 15:28 TBL
V13840
Aliphatic C9-C12 <5.77
mg/Kg - dry
5.77 10.1
100 01/14/22 15:28 TBL
V13840
Aromatic C9-C10 <0.789
mg/Kg - dry
0.789 10.1
100 01/14/22 15:28 TBL
V13840
Surrogate: 2,5-Dibromotoluene (FID)
94.4
Limits: 70-130%
100 01/14/22 15:28 TBL
V13840
Surrogate: 2,5-Dibromotoluene (PID)
84.5
Limits: 70-130%
100 01/14/22 15:28 TBL
V13840
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 48 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92278 Matrix: Solids
Sample ID: UST-1 West Sampled: 1/13/2022 12:55
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Moisture
17.2 %
1 01/19/2212:09 SJL SW-DRYWT
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions J Estimated value L Limit Exceeded
MQL Method Quantitation Limit
Page 49 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92278
Matrix: Solids
Sample ID: UST-1 West
Sampled:
1/13/2022 12:55
Analytical Method: 8260D
Prep Batch(es):
V13890
01/14/22 08:00
Prep Method: 5035
LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
0.0063
mg/Kg - dry
0.002
0.024
1
01/14/22 14:06
TBL
V13891
Acrolein
<0.001
mg/Kg - dry
0.001
0.024
1
01/14/22 14:06
TBL
V13891
Acrylonitrile
<0.0009
mg/Kg - dry
0.0009
0.024
1
01/14/22 14:06
TBL
V13891
Benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 14:06
TBL
V13891
Bromobenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 14:06
TBL
V13891
Bromochloromethane
<0.0010
mg/Kg - dry
0.0010
0.006
1
01/14/22 14:06
TBL
V13891
Bromodichloromethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
Bromoform
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
Bromomethane
<0.002
mg/Kg - dry
0.002
0.012
1
01/14/22 14:06
TBL
V13891
n-Butylbenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 14:06
TBL
V13891
sec -Butyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 14:06
TBL
V13891
tert-Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 14:06
TBL
V13891
Carbon Disulfide
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 14:06
TBL
V13891
Carbon Tetrachloride
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
Chlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 14:06
TBL
V13891
Chlorodibromomethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
Chloroethane
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 14:06
TBL
V13891
Chloroform
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
Chloromethane
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 14:06
TBL
V13891
2-Chlorotoluene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 14:06
TBL
V13891
4-Chlorotoluene
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 14:06
TBL
V13891
Di -Isopropyl Ether (DIPE)
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 14:06
TBL
V13891
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 50 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026
REPORT OF ANAL YSIS
Lab No : 92278 Matrix: Solids
Sample ID: UST-1 West Sampled: 1/13/2022 12:55
Analytical Method: 8260D Prep Batch(es): V13890 01/14/22 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dibromo-3-Chloropropane
<0.0005
mg/Kg - dry
0.0005
0.012
1
01/14/22 14:06
TBL
V13891
1,2-Dibromoethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 14:06
TBL
V13891
Dibromomethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 14:06
TBL
V13891
1,2-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.006
1
01/14/22 14:06
TBL
V13891
1,3-Dichlorobenzene
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 14:06
TBL
V13891
1,4-Dichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 14:06
TBL
V13891
Dichlorodifluoromethane
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 14:06
TBL
V13891
1,1-Dichloroethane
<0.0010
mg/Kg - dry
0.0010
0.006
1
01/14/22 14:06
TBL
V13891
1,2-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
1,1-Dichloroethene
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 14:06
TBL
V13891
cis- 1,2-Dich loroethene
<0.0010
mg/Kg - dry
0.0010
0.006
1
01/14/22 14:06
TBL
V13891
trans-1,2-Dichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
1,2-Dichloropropane
<0.0005
mg/Kg - dry
0.0005
0.006
1
01/14/22 14:06
TBL
V13891
1,3-Dichloropropane
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 14:06
TBL
V13891
2,2-Dichloropropane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
1,1-Dichloropropene
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 14:06
TBL
V13891
cis- 1,3-Dich loropropene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 14:06
TBL
V13891
trans-1,3-Dichloropropene
<0.0010
mg/Kg - dry
0.0010
0.006
1
01/14/22 14:06
TBL
V13891
Ethanol
<0.016
mg/Kg - dry
0.016
0.301
1
01/14/22 14:06
TBL
V13891
Ethylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 14:06
TBL
V13891
Ethyl Tertiary Butyl Ether (ETBE) <0.001
mg/Kg - dry
0.001
0.060
1
01/14/22 14:06
TBL
V13891
Hexachlorobutadiene
<0.0010
mg/Kg - dry
0.0010
0.012
1
01/14/22 14:06
TBL
V13891
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 51 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92278
Matrix: Solids
Sample ID: UST-1 West
Sampled:
1/13/2022 12:55
Analytical Method: 8260D
Prep Batch(es):
V13890
01/14/22 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
n-Hexane
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 14:06
TBL
V13891
2-Hexanone
<0.0007
mg/Kg - dry
0.0007
0.024
1
01/14/22 14:06
TBL
V13891
Isopropyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 14:06
TBL
V13891
4-Isopropyl toluene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
Methyl Ethyl Ketone (MEK)
<0.0008
mg/Kg - dry
0.0008
0.024
1
01/14/22 14:06
TBL
V13891
Methyl tert-butyl ether (MTBE)
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 14:06
TBL
V13891
4-Methyl-2-Pentanone
<0.018
mg/Kg - dry
0.018
0.024
1
01/14/22 14:06
TBL
V13891
Methylene Chloride
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 14:06
TBL
V13891
Naphthalene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 14:06
TBL
V13891
n-Propylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 14:06
TBL
V13891
Styrene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
1,1,1,2-Tetrachloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
1,1,2,2-Tetrachloroethane
<0.0004
mg/Kg - dry
0.0004
0.006
1
01/14/22 14:06
TBL
V13891
Tetrachloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
Toluene
<0.0008
mg/Kg - dry
0.0008
0.006
1
01/14/22 14:06
TBL
V13891
1,2,3-Trichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.012
1
01/14/22 14:06
TBL
V13891
1,2,4-Trichlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.012
1
01/14/22 14:06
TBL
V13891
1,1,1-Trichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
1,1,2-Trichloroethane
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 14:06
TBL
V13891
Trichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
01/14/22 14:06
TBL
V13891
Trichlorofluoromethane
<0.002
mg/Kg - dry
0.002
0.012
1
01/14/22 14:06
TBL
V13891
1,2,3-Trichloropropane
<0.0009
mg/Kg - dry
0.0009
0.006
1
01/14/22 14:06
TBL
V13891
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 52 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Report Date : 01/21/2022
Received : 01/13/2022
Lab No : 92278 Matrix: Solids
Sample ID: UST-1 West Sampled: 1/13/2022 12:55
Analytical Method: 8260D Prep Batch(es): V13890 01/14/22 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2,4-Trimethyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 14:06
TBL
V13891
1,3,5-Trimethyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
01/14/22 14:06
TBL
V13891
Vinyl Acetate
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 14:06
TBL
V13891
Vinyl Chloride
<0.0006
mg/Kg - dry
0.0006
0.012
1
01/14/22 14:06
TBL
V13891
o-Xylene
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 14:06
TBL
V13891
m,p-Xylene
<0.001
mg/Kg - dry
0.001
0.012
1
01/14/22 14:06
TBL
V13891
Xylene (Total)
<0.0006
mg/Kg - dry
0.0006
0.006
1
01/14/22 14:06
V13891
Surrogate:4-Bromofluorobenzene
97.4
Limits:70-130%
1 01/14/22 14:06 TBL
V13891
Surrogate: Dibromofluoromethane
99.7
Limits:
84-123%
1 01/14/22 14:06 TBL
V13891
Surrogate: Toluene-d8
86.9
Limits:
76-129%
1 01/14/22 14:06 TBL
V13891
Analytical Method: 8270E
Prep Batch(es):
V13928
01/18/22 13:43
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.140
mg/Kg - dry
0.140
0.798
1
01/21/22 14:27
JMV
V14113
Acenaphthylene
<0.126
mg/Kg - dry
0.126
0.798
1
01/21/22 14:27
JMV
V14113
Aniline
<0.183
mg/Kg - dry
0.183
0.798
1
01/21/22 14:27
JMV
V14113
Anthracene
<0.172
mg/Kg - dry
0.172
0.798
1
01/21/22 14:27
JMV
V14113
Benzo(a)anthracene
<0.167
mg/Kg - dry
0.167
0.798
1
01/21/22 14:27
JMV
V14113
Benzo(a)pyrene
<0.177
mg/Kg - dry
0.177
0.798
1
01/21/22 14:27
JMV
V14113
Benzo(b)fluoranthene
<0.176
mg/Kg - dry
0.176
0.798
1
01/21/22 14:27
JMV
V14113
Benzo(g,h,i)perylene
<0.164
mg/Kg - dry
0.164
0.798
1
01/21/22 14:27
JMV
V14113
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 53 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92278
Matrix: Solids
Sample ID: UST-1 West
Sampled:
1/13/2022 12:55
Analytical Method: 8270E
Prep Batch(es):
V13928
01/18/22 13:43
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzo(k)fluoranthene
<0.165
mg/Kg - dry
0.165
0.798
1
01/21/22 14:27
JMV
V14113
Benzoic Acid
<0.700
mg/Kg - dry
0.700
2.42
1
01/21/22 14:27
JMV
V14113
Benzyl alcohol
<0.126
mg/Kg - dry
0.126
0.798
1
01/21/22 14:27
JMV
V14113
Bis(2-Chloroethoxy)methane
<0.142
mg/Kg - dry
0.142
0.798
1
01/21/22 14:27
JMV
V14113
Bis(2-Chloroethyl)ether
<0.129
mg/Kg - dry
0.129
0.798
1
01/21/22 14:27
JMV
V14113
Bis(2-Chloroisopropyl)ether
<0.164
mg/Kg - dry
0.164
0.398
1
01/21/22 14:27
JMV
V14113
Bis(2-ethylhexyl)phthalate
<0.144
mg/Kg - dry
0.144
0.798
1
01/21/22 14:27
JMV
V14113
4-13romophenyl phenyl ether
<0.131
mg/Kg - dry
0.131
0.798
1
01/21/22 14:27
JMV
V14113
Butyl benzyl phthalate
<0.136
mg/Kg - dry
0.136
0.398
1
01/21/22 14:27
JMV
V14113
4-Chloro-3-methyl phenol
<0.111
mg/Kg - dry
0.111
0.798
1
01/21/22 14:27
JMV
V14113
4-Chloroaniline
<0.135
mg/Kg - dry
0.135
0.398
1
01/21/22 14:27
JMV
V14113
2-Chloronaphthalene
<0.140
mg/Kg - dry
0.140
0.798
1
01/21/22 14:27
JMV
V14113
2-Chlorophenol
<0.118
mg/Kg - dry
0.118
0.798
1
01/21/22 14:27
JMV
V14113
4-Chlorophenyl phenyl ether
<0.152
mg/Kg - dry
0.152
1.21
1
01/21/22 14:27
JMV
V14113
Chrysene
<0.171
mg/Kg - dry
0.171
0.798
1
01/21/22 14:27
JMV
V14113
Dibenz(a,h)anthracene
<0.277
mg/Kg - dry
0.277
0.798
1
01/21/22 14:27
JMV
V14113
Dibenzofuran
<0.143
mg/Kg - dry
0.143
0.798
1
01/21/22 14:27
JMV
V14113
1,2-Dichlorobenzene
<0.114
mg/Kg - dry
0.114
0.798
1
01/21/22 14:27
JMV
V14113
1,3-Dichlorobenzene
<0.117
mg/Kg - dry
0.117
0.798
1
01/21/22 14:27
JMV
V14113
1,4-Dichlorobenzene
<0.117
mg/Kg - dry
0.117
0.398
1
01/21/22 14:27
JMV
V14113
3,3'-Dichlorobenzidine
<0.177
mg/Kg - dry
0.177
0.798
1
01/21/22 14:27
JMV
V14113
2,4-Dichlorophenol
<0.115
mg/Kg - dry
0.115
0.798
1
01/21/22 14:27
JMV
V14113
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 54 of 92

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01102
Hart & Hickman (Charlotte) Project CHP-046
Andrew Besu Report Date : 01/21/2022
2923 South Tryon St. Ste 100 Information : Received : 01/13/2022
Charlotte , NC 28203
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92278
Matrix: Solids
Sample ID: UST-1 West
Sampled:
1/13/2022 12:55
Analytical Method: 8270E
Prep Batch(es):
V13928
01/18/22 13:43
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.217
mg/Kg - dry
0.217
0.798
1
01/21/22 14:27
JMV
V14113
Dimethyl phthalate
<0.210
mg/Kg - dry
0.210
0.798
1
01/21/22 14:27
JMV
V14113
2,4-Dimethyl phenol
<0.130
mg/Kg - dry
0.130
0.398
1
01/21/22 14:27
JMV
V14113
Di-n-butyl phthalate
<0.129
mg/Kg - dry
0.129
0.798
1
01/21/22 14:27
JMV
V14113
4,6-Dinitro-2-methylphenol
<0.289
mg/Kg - dry
0.289
1.81
1
01/21/22 14:27
JMV
V14113
2,4-Dinitrophenol
<0.628
mg/Kg - dry
0.628
1.81
1
01/21/22 14:27
JMV
V14113
2,4-Dinitrotoluene
<0.116
mg/Kg - dry
0.116
0.798
1
01/21/22 14:27
JMV
V14113
2,6-Dinitrotoluene
<0.130
mg/Kg - dry
0.130
0.798
1
01/21/22 14:27
JMV
V14113
Di-n-Octyl Phthalate
<0.172
mg/Kg - dry
0.172
0.398
1
01/21/22 14:27
JMV
V14113
Fluoranthene
<0.148
mg/Kg - dry
0.148
0.798
1
01/21/22 14:27
JMV
V14113
Fluorene
<0.154
mg/Kg - dry
0.154
0.798
1
01/21/22 14:27
JMV
V14113
Hexachlorobenzene
<0.128
mg/Kg - dry
0.128
0.798
1
01/21/22 14:27
JMV
V14113
Hexachlorobutadiene
<0.117
mg/Kg - dry
0.117
0.798
1
01/21/22 14:27
JMV
V14113
Hexachlorocyclopentadiene
<0.189
mg/Kg - dry
0.189
0.798
1
01/21/22 14:27
JMV
V14113
Hexachloroethane
<0.095
mg/Kg - dry
0.095
0.798
1
01/21/22 14:27
JMV
V14113
Indeno(1,2,3-cd)pyrene
<0.216
mg/Kg - dry
0.216
0.798
1
01/21/22 14:27
JMV
V14113
Isophorone
<0.230
mg/Kg - dry
0.230
0.798
1
01/21/22 14:27
JMV
V14113
1-Methylnaphthalene
<0.128
mg/Kg - dry
0.128
0.798
1
01/21/22 14:27
JMV
V14113
2-Methylnaphthalene
<0.120
mg/Kg - dry
0.120
0.798
1
01/21/22 14:27
JMV
V14113
2-Methylphenol
<0.117
mg/Kg - dry
0.117
0.798
1
01/21/22 14:27
JMV
V14113
3&4 Methylphenol
<0.102
mg/Kg - dry
0.102
0.798
1
01/21/22 14:27
JMV
V14113
Naphthalene
<0.173
mg/Kg - dry
0.173
0.798
1
01/21/22 14:27
JMV
V14113
Qualifiers/ *
Outside QC Limit
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 55 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Report Number : 22-013-0026
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
REPORT OF ANAL YSIS
Report Date : 01/21/2022
Received : 01/13/2022
Lab No : 92278
Sample ID: UST-1 West
Matrix: Solids
Sampled: 1/13/2022 12:55
Analytical Method: 8270E
Prep Batch(es):
V13928
01/18/22 13:43
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Nitroaniline
<0.116
mg/Kg - dry
0.116
0.798
1
01/21/22 14:27
JMV
V14113
3-Nitroaniline
<0.144
mg/Kg - dry
0.144
0.798
1
01/21/22 14:27
JMV
V14113
4-Nitroaniline
<0.112
mg/Kg - dry
0.112
0.398
1
01/21/22 14:27
JMV
V14113
Nitrobenzene
<0.140
mg/Kg - dry
0.140
0.398
1
01/21/22 14:27
JMV
V14113
2-Nitrophenol
<0.107
mg/Kg - dry
0.107
0.798
1
01/21/22 14:27
JMV
V14113
4-Nitrophenol
<0.141
mg/Kg - dry
0.141
0.798
1
01/21/22 14:27
JMV
V14113
N-N itrosodimethyla mine
<0.317
mg/Kg - dry
0.317
0.798
1
01/21/22 14:27
JMV
V14113
N-Nitrosodiphenylamine
<0.218
mg/Kg - dry
0.218
0.798
1
01/21/22 14:27
JMV
V14113
N-Nitroso-di-n-propylamine
<0.142
mg/Kg - dry
0.142
0.798
1
01/21/22 14:27
JMV
V14113
Pentachlorophenol
<0.419
mg/Kg - dry
0.419
1.21
1
01/21/22 14:27
JMV
V14113
Phenanthrene
<0.251
mg/Kg - dry
0.251
0.798
1
01/21/22 14:27
JMV
V14113
Phenol
<0.135
mg/Kg - dry
0.135
0.798
1
01/21/22 14:27
JMV
V14113
Pyrene
<0.161
mg/Kg - dry
0.161
0.798
1
01/21/22 14:27
JMV
V14113
Pyridine
<0.095
mg/Kg - dry
0.095
0.398
1
01/21/22 14:27
JMV
V14113
1,2,4-Trichlorobenzene
<0.129
mg/Kg - dry
0.129
0.798
1
01/21/22 14:27
JMV
V14113
2,4,5-Trichlorophenol
<0.116
mg/Kg - dry
0.116
0.798
1
01/21/22 14:27
JMV
V14113
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 56 of 92

Waypowint
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
hwd
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92278 Matrix: Solids
Sample ID: UST-1 West Sampled: 1/13/2022 12:55
Analytical Method: 8270E Prep Batch(es): V13928 01/18/22 13:43
Prep Method: 3546
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
2,4,6-Trichlorophenol
Surrogate: Phenol-d5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Nitrobenzene-d5
Surrogate: 4-Terphenyl-d 14
Surrogate: 2,4,6-Tribromophenol
<0.116 mg/Kg - dry
0.116 0.798
84.4
Limits: 34-121%
79.0
Limits: 44-115%
89.2
Limits: 35-115%
73.7
Limits: 37-122%
85.6
Limits: 54-127%
72.5
Limits: 39-132%
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
1 01/21/22 14:27 JMV V14113
1 01/21/2214:27 JMV V14113
1 01/21/2214:27 JMV V14113
1 01/21/2214:27 JMV V14113
1 01/21/2214:27 JMV V14113
1 01/21/2214:27 JMV V14113
1 01/21/2214:27 JMV V14113
DF Dilution Factor
MQL Method Quantitation Limit
Page 57 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026
Lab No : 92278
Sample ID: UST-1 West
REPOR T OF A NA L YSIS
Matrix: Solids
Sampled: 1/13/2022 12:55
Analytical Method: MADEP-EPH
Prep Batch(es):
V13950 01/19/22 09:35
Prep Method: MAEPH (Prep)
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Aliphatic C9-C18
<11.1
mg/Kg - dry
11.1 60.4 1
01/20/22 16:57 JC1
V14062
Aliphatic C19-C36
<14.7
mg/Kg - dry
14.7 60.4 1
01/20/22 16:57 JC1
V14062
Aromatic C11-C22
<17.1
mg/Kg - dry
17.1 60.4 1
01/20/22 16:57 JC1
V14062
Surrogate:2-Bromonaphthalene
89.0
Limits:40-140%
1 01/20/22 16:57 JC1
V14062
Surrogate: Chlorooctadecane
83.5
Limits: 40-140%
1 01/20/22 16:57 JC1
V14062
Surrogate: OTP Surrogate
72.0
Limits: 40-140%
1 01/20/22 16:57 JC1
V14062
Surrogate:2-Fluorobiphenyl
72.3
Limits:40-140%
1 01/20/22 16:57 JC1
V14062
Analytical Method: MADEP-VPH
Prep Batch(es):
V13839 01/14/22 08:00
Prep Method: MAVPH (Prep)
Test
Results
Units
MDL MQL DF
Date / Time By
Analytical
Analyzed
Batch
Aliphatic C5-C8 <1.47
mg/Kg - dry
1.47 9.66
100 01/14/22 15:52 TBL
V13840
Aliphatic C9-C12 <5.51
mg/Kg - dry
5.51 9.66
100 01/14/22 15:52 TBL
V13840
Aromatic C9-C10 <0.753
mg/Kg - dry
0.753 9.66
100 01/14/22 15:52 TBL
V13840
Surrogate: 2,5-Dibromotoluene (FID)
87.0
Limits: 70-130%
100 01/14/22 15:52 TBL
V13840
Surrogate: 2,5-Dibromotoluene (PID)
80.8
Limits: 70-130%
100 01/14/22 15:52 TBL
V13840
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 58 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026 REPOR T OF A NA L YSIS
Lab No : 92279 Matrix: Solids
Sample ID : UST-1 Stockpile Sampled: 1/13/2022 12:25
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Moisture
20.9 %
1 01/19/2212:09 SJL SW-DRYWT
Qualifiers/ * Outside QC Limit DF Dilution Factor
Definitions J Estimated value L Limit Exceeded
MQL Method Quantitation Limit
Page 59 of 92

WavDdibnto
ANALYTICAL
01102
Hart & Hickman (Charlotte)
Andrew Besu
2923 South Tryon St. Ste 100
Charlotte , NC 28203
Project CHP-046
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Date : 01/21/2022
Received : 01/13/2022
Report Number : 22-013-0026
REPOR T OF A NA L YSIS
Lab No : 92279
Matrix: Solids
Sample ID: UST-1 Stockpile
Sampled: 1/13/2022
12:25
Analytical Method: 8015C DRO
Prep Batch(es):
V13929
01/18/22 13:43
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Diesel Range Organics (C10-C28)
4150
mg/Kg - dry
295
632
50 01/20/22 13:25 JMV
V14020
Surrogate: OTP Surrogate
0 *
Limits:
31-123%
50 01/20/22 13:25 JMV
V14020
Analytical Method: 8015C GRO
Prep Batch(es):
V13822
01/14/22 08:00
Prep Method: 5035 MED
Test
Results
Units
MDL
MQL
DF Date / Time By
Analytical
Analyzed
Batch
Gasoline Range Organics (C6-C10)
441
mg/Kg - dry
0.562
68.0
500 01/14/22 08:53 TBL
V13823
Surrogate: a,a,a-Trifluorotoluene
112
Limits:
50-137%
500 01/14/22 08:53 TBL
V13823
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 60 of 92

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13929 QC Analytical Batch(es): V14020
QC Prep Batch Method: 3546 Analysis Method: 8015C DRO
Analysis Description: Total Petroleum Hydrocarbons - Extractable
Lab Reagent Blank LRB-V13929 Matrix: SOL
Associated Lab Samples: 92279
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Diesel Range Organics (C10-C28) mg/Kg <4.65 4.65 10.0 01/19/22 15:34
OTP Surrogate (S) 01/19/22 15:34 63.7 31-123
Laboratory Control Sample LCS-V13929
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Diesel Range Organics (00-C28) mg/Kg
66.7 58.9
88.3
46-126
OTP Surrogate (S)
65.4
31-123
Matrix Spike & Matrix Spike Duplicate
V 92080-MS-V13929 V 92080-MSD-V13929
MS Spike MSD MS Result
MSD
MS MSD %Rec Max
Parameter Units
Result Conc. Spike
Result
%Rec %Rec Limits RPD RPD
Conc.
Diesel Range Organics (C10-C28) mg/Kg 11500 66.6 66.6 7230
OTP Surrogate (S)
6910 -6400* -6700* 50-117 4.5 24
I* 1.7* 31-123
* QC Fail Date: 01/21/2022 04:07 PM Page 1 of 30
Page 61 of 92

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13822 QC Analytical Batch(es): V13823
QC Prep Batch Method: 5035 MED Analysis Method: 8015C GRO
Analysis Description: Total Petroleum Hydrocarbons - Volatile
Lab Reagent Blank LRB-V13822 Matrix: SOL
Associated Lab Samples: 92279
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Gasoline Range Organics (C6-C10) mg/Kg 1.02 0.041 5.00 01/14/22 07:25
a,a,a-Trifluorotoluene (S) 01/14/22 07:25 101 50-137
Laboratory Control Sample LCS-V13822
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Gasoline Range Organics (C6-00) mg/Kg
50.0 52.3
105
41-138
a,a,a-Trifluorotoluene (S)
108
50-137
Matrix Spike & Matrix Spike Duplicate
V 92279-MS-V13822 V 92279-MSD-V13822
MS Spike MSD MS Result
MSD
MS MSD %Rec Max
Parameter Units
Result Conc. Spike
Result
%Rec %Rec Limits RPD RPD
Conc.
Gasoline Range Organics (C6-C10) mg/Kg 349 50.0 50.0 348
a,a,a-Trifluorotoluene (S)
340 -2.0* -18* 41-138 2.3 34
141* 130 50-137
* QC Fail Date: 01/21/2022 04:07 PM Page 2 of 30
Page 62 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13890
QC Prep Batch Method: 5035 LOW
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V13890
Associated Lab Samples: 92274, 92275, 92276, 92277, 92278
QC Analytical Batch(es): V13891
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Matrix: SOL
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
mg/Kg
<0.002
0.002
0.020
01/14/22 10:44
Acrolein
mg/Kg
<0.001
0.001
0.020
01/14/22 10:44
Acrylonitrile
mg/Kg
<0.0008
0.0008
0.020
01/14/22 10:44
Benzene
mg/Kg
<0.0006
0.0006
0.005
01/14/22 10:44
Bromobenzene
mg/Kg
<0.0005
0.0005
0.005
01/14/22 10:44
Bromochloromethane
mg/Kg
<0.0008
0.0008
0.005
01/14/22 10:44
Bromodichloromethane
mg/Kg
<0.001
0.001
0.005
01/14/22 10:44
Bromoform
mg/Kg
<0.001
0.001
0.005
01/14/22 10:44
Bromomethane
mg/Kg
<0.001
0.001
0.010
01/14/22 10:44
n-Butylbenzene
mg/Kg
<0.0005
0.0005
0.005
01/14/22 10:44
sec -Butyl benzene
mg/Kg
<0.0006
0.0006
0.005
01/14/22 10:44
tert-Butyl benzene
mg/Kg
<0.0005
0.0005
0.005
01/14/22 10:44
Carbon Disulfide
mg/Kg
<0.0006
0.0006
0.005
01/14/22 10:44
Carbon Tetrachloride
mg/Kg
<0.001
0.001
0.005
01/14/22 10:44
Chlorobenzene
mg/Kg
<0.0007
0.0007
0.005
01/14/22 10:44
Chlorodibromomethane
mg/Kg
<0.0009
0.0009
0.005
01/14/22 10:44
Chloroethane
mg/Kg
<0.0009
0.0009
0.010
01/14/22 10:44
Chloroform
mg/Kg
<0.001
0.001
0.005
01/14/22 10:44
Chloromethane
mg/Kg
<0.0006
0.0006
0.010
01/14/22 10:44
2-Chlorotoluene
mg/Kg
<0.0005
0.0005
0.005
01/14/22 10:44
4-Chlorotoluene
mg/Kg
<0.0004
0.0004
0.005
01/14/22 10:44
Di -Isopropyl Ether (DIPE)
mg/Kg
<0.0007
0.0007
0.005
01/14/22 10:44
1,2-Dibromo-3-Chloropropane
mg/Kg
<0.0004
0.0004
0.010
01/14/22 10:44
1,2-Dibromoethane
mg/Kg
<0.0006
0.0006
0.005
01/14/22 10:44
Dibromomethane
mg/Kg
<0.0006
0.0006
0.005
01/14/22 10:44
1,2-Dichlorobenzene
mg/Kg
<0.0003
0.0003
0.005
01/14/22 10:44
1,3-Dichlorobenzene
mg/Kg
<0.0004
0.0004
0.005
01/14/22 10:44
Date:
01/21/2022 04:07 PM
Page 3 of 30
Page 63 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13890
QC Prep Batch Method: 5035 LOW
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V13890
Associated Lab Samples: 92274, 92275, 92276, 92277, 92278
QC Analytical Batch(es): V13891
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Matrix: SOL
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.0006
0.0006
0.005
01/14/22 10:44
Dichlorodifluoromethane
mg/Kg
<0.001
0.001
0.010
01/14/22 10:44
1,1-Dichloroethane
mg/Kg
<0.0008
0.0008
0.005
01/14/22 10:44
1,2-Dichloroethane
mg/Kg
<0.001
0.001
0.005
01/14/22 10:44
1,1-Dichloroethene
mg/Kg
<0.0007
0.0007
0.005
01/14/22 10:44
cis-1,2-Dichloroethene
mg/Kg
<0.0008
0.0008
0.005
01/14/22 10:44
trans-1,2-Dichloroethene
mg/Kg
<0.001
0.001
0.005
01/14/22 10:44
1,2-Dichloropropane
mg/Kg
<0.0004
0.0004
0.005
01/14/22 10:44
1,3-Dichloropropane
mg/Kg
<0.0006
0.0006
0.005
01/14/22 10:44
2,2-Dichloropropane
mg/Kg
<0.001
0.001
0.005
01/14/22 10:44
1,1-Dichloropropene
mg/Kg
<0.0008
0.0008
0.005
01/14/22 10:44
cis-1,3-Dichloropropene
mg/Kg
<0.0005
0.0005
0.005
01/14/22 10:44
trans-1,3-Dichloropropene
mg/Kg
<0.0008
0.0008
0.005
01/14/22 10:44
Ethanol
mg/Kg
<0.014
0.014
0.250
01/14/22 10:44
Ethylbenzene
mg/Kg
<0.0006
0.0006
0.005
01/14/22 10:44
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
<0.0008
0.0008
0.050
01/14/22 10:44
Hexachlorobutadiene
mg/Kg
<0.0008
0.0008
0.010
01/14/22 10:44
n-Hexane
mg/Kg
<0.0007
0.0007
0.010
01/14/22 10:44
2-Hexanone
mg/Kg
<0.0006
0.0006
0.020
01/14/22 10:44
Isopropyl benzene
mg/Kg
<0.0005
0.0005
0.005
01/14/22 10:44
4-Isopropyl toluene
mg/Kg
<0.001
0.001
0.005
01/14/22 10:44
Methyl Ethyl Ketone (MEK)
mg/Kg
<0.0007
0.0007
0.020
01/14/22 10:44
Methyl tert-butyl ether (MTBE)
mg/Kg
<0.0006
0.0006
0.005
01/14/22 10:44
4-Methyl-2-Pentanone
mg/Kg
<0.015
0.015
0.020
01/14/22 10:44
Methylene Chloride
mg/Kg
<0.001
0.001
0.010
01/14/22 10:44
Naphthalene
mg/Kg
<0.0010
0.0010
0.010
01/14/22 10:44
n-Propylbenzene
mg/Kg
<0.0005
0.0005
0.005
01/14/22 10:44
Date:
01/21/2022 04:07 PM
Page 4 of 30
Page 64 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13890
QC Prep Batch Method: 5035 LOW
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank
Associated Lab Samples:
Parameter
LRB-V13890
92274, 92275, 92276, 92277, 92278
Blank MDL
Units Result
Styrene
mg/Kg
<0.001
0.001
1,1,1,2-Tetrachloroethane
mg/Kg
<0.001
0.001
1,1,2,2-Tetrachloroethane
mg/Kg
<0.0003
0.0003
Tetrachloroethene
mg/Kg
<0.0009
0.0009
Toluene
mg/Kg
<0.0007
0.0007
1,2,3-Trichlorobenzene
mg/Kg
<0.0005
0.0005
1,2,4-Trichlorobenzene
mg/Kg
<0.0006
0.0006
1,1,1-Trichloroethane
mg/Kg
<0.001
0.001
1,1,2-Trichloroethane
mg/Kg
<0.0005
0.0005
Trichloroethene
mg/Kg
<0.0009
0.0009
Trichlorofluoromethane
mg/Kg
<0.002
0.002
1,2,3-Trichloropropane
mg/Kg
< 0.0007
0.0007
1,2,4-Trimethyl benzene
mg/Kg
<0.0005
0.0005
1,3,5-Trimethyl benzene
mg/Kg
<0.0005
0.0005
Vinyl Acetate
mg/Kg
<0.0005
0.0005
Vinyl Chloride
mg/Kg
<0.0005
0.0005
o-Xylene
mg/Kg
<0.0005
0.0005
m,p-Xylene
mg/Kg
<0.001
0.001
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
QC Analytical Batch(es): V13891
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Matrix: SOL
MQL Analyzed % % Rec
Recovery Limits
0.005
01/14/22 10:44
0.005
01/14/22 10:44
0.005
01/14/22 10:44
0.005
01/14/22 10:44
0.005
01/14/22 10:44
0.010
01/14/22 10:44
0.010
01/14/22 10:44
0.005
01/14/22 10:44
0.005
01/14/22 10:44
0.005
01/14/22 10:44
0.010
01/14/22 10:44
0.005
01/14/22 10:44
0.005
01/14/22 10:44
0.005
01/14/22 10:44
0.010
01/14/22 10:44
0.010
01/14/22 10:44
0.005
01/14/22 10:44
0.010
01/14/22 10:44
O1/14/22 10:44 97.4 70-130
O1/14/22 10:44 97.8 84-123
O1/14/22 10:44 86.6 76-129
Laboratory Control Sample & LCSD LCS-V13890 LCSD-V13890
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter Units
Conc.
Result
Result
%Rec
a/o Rec
Limits
Acetone mg/Kg
0.100
0.074
0.071
74.0
71.9
29-198
RPD Max
RPD
2.8 20
Date: 01/21/2022 04:07 PM
Page 65 of 92
Page 5 of 30

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13890 QC Analytical Batch(es): V13891
QC Prep Batch Method: 5035 LOW Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V13890 LCSD-V13890
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Acrolein
mg/Kg
0.100
0.104
0.100
104
100
70-130
3.9
20
Acrylonitrile
mg/Kg
0.100
0.109
0.107
109
107
65-134
1.8
20
Benzene
mg/Kg
0.050
0.047
0.043
94.8
86.6
74-127
9.0
20
Bromobenzene
mg/Kg
0.050
0.054
0.051
109
103
73-125
5.8
20
Bromochloromethane
mg/Kg
0.050
0.047
0.045
94.6
90.8
72-134
4.0
20
Bromodichloromethane
mg/Kg
0.050
0.047
0.044
94.6
88.4
75-122
6.7
20
Bromoform
mg/Kg
0.050
0.044
0.042
88.4
85.8
66-135
2.9
20
Bromomethane
mg/Kg
0.050
0.044
0.040
88.6
81.6
20-180
8.2
20
n-Butylbenzene
mg/Kg
0.050
0.040
0.045
80.4
91.6
65-135
13.0
20
sec -Butyl benzene
mg/Kg
0.050
0.040
0.045
81.4
91.8
66-131
12.0
20
tert-Butyl benzene
mg/Kg
0.050
0.045
0.040
90.6
81.4
67-132
10.6
20
Carbon Disulfide
mg/Kg
0.050
0.047
0.042
95.6
85.4
61-129
11.2
20
Carbon Tetrachloride
mg/Kg
0.050
0.047
0.043
94.6
87.8
64-143
7.4
20
Chlorobenzene
mg/Kg
0.050
0.041
0.039
83.6
78.8
74-118
5.9
20
Chlorodibromomethane
mg/Kg
0.050
0.042
0.040
85.8
81.4
73-122
5.2
20
Chloroethane
mg/Kg
0.050
0.051
0.047
102
94.2
33-149
7.9
20
Chloroform
mg/Kg
0.050
0.046
0.043
92.2
86.6
73-127
6.2
20
Chloromethane
mg/Kg
0.050
0.047
0.042
94.2
84.8
45-143
10.5
20
2-Chlorotoluene
mg/Kg
0.050
0.041
0.043
83.4
86.4
67-124
3.5
20
4-Chlorotoluene
mg/Kg
0.050
0.043
0.052
87.0
104
71-126
18.1
20
Di -Isopropyl Ether(DIPE)
mg/Kg
0.050
0.047
0.044
94.6
88.8
59-159
6.3
20
1,2-Dibromo-3-Chloropropane
mg/Kg
0.050
0.040
0.042
80.8
85.6
55-157
5.7
20
1,2-Dibromoethane
mg/Kg
0.050
0.042
0.040
85.4
80.4
70-132
6.0
20
Dibromomethane
mg/Kg
0.050
0.047
0.045
95.8
91.8
74-133
4.2
20
1,2-Dichlorobenzene
mg/Kg
0.050
0.046
0.040
93.4
80.0
72-123
15.4
20
1,3-Dichlorobenzene
mg/Kg
0.050
0.040
0.041
81.2
82.8
71-120
1.9
20
Date: 01/21/2022 04:07 PM Page 6 of 30
Page 66 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13890 QC Analytical Batch(es): V13891
QC Prep Batch Method: 5035 LOW Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V13890 LCSD-V13890
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
1,4-Dichlorobenzene
mg/Kg
0.050
0.041
0.041
83.6
83.2
71-123
0.4
20
Dichlorodifluoromethane
mg/Kg
0.050
0.055
0.049
111
99.4
26-146
11.2
20
1,1-Dichloroethane
mg/Kg
0.050
0.047
0.043
94.2
86.6
74-127
8.4
20
1,2-Dichloroethane
mg/Kg
0.050
0.045
0.043
91.2
86.2
68-128
5.6
20
1,1-Dichloroethene
mg/Kg
0.050
0.046
0.042
92.8
84.2
67-149
9.7
20
cis-1,2-Dichloroethene
mg/Kg
0.050
0.047
0.043
95.0
87.6
76-134
8.1
20
trans-1,2-Dichloroethene
mg/Kg
0.050
0.047
0.042
94.4
84.8
73-132
10.7
20
1,2-Dichloropropane
mg/Kg
0.050
0.047
0.044
94.4
88.2
73-130
6.7
20
1,3-Dichloropropane
mg/Kg
0.050
0.041
0.039
83.2
78.2
75-124
6.1
20
2,2-Dichloropropane
mg/Kg
0.050
0.046
0.041
92.4
83.4
50-142
10.2
20
1,1-Dichloropropene
mg/Kg
0.050
0.048
0.044
97.4
88.0
71-130
10.1
20
cis-1,3-Dichloropropene
mg/Kg
0.050
0.047
0.045
95.6
90.8
71-125
5.1
20
trans-1,3-Dichloropropene
mg/Kg
0.050
0.048
0.045
96.4
91.8
68-123
4.8
20
Ethanol
mg/Kg
1.25
1.22
1.16
97.6
92.8
70-130
5.0
20
Ethylbenzene
mg/Kg
0.050
0.042
0.039
85.8
79.2
74-128
8.0
20
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
0.100
0.093
0.089
93.8
89.9
70-130
4.2
20
Hexachlorobutadiene
mg/Kg
0.050
0.039
0.035
78.4
70.4
64-125
10.7
20
n-Hexane
mg/Kg
0.050
0.050
0.044
101
89.4
70-130
12.5
20
2-Hexanone
mg/Kg
0.050
0.041
0.041
82.2
82.0
61-157
0.2
20
Isopropyl benzene
mg/Kg
0.050
0.047
0.044
95.8
88.0
68-126
8.4
20
4-Isopropyl toluene
mg/Kg
0.050
0.040
0.041
81.0
83.8
68-129
3.3
20
Methyl Ethyl Ketone (MEK)
mg/Kg
0.050
0.037
0.036
75.0
72.4
63-149
3.5
20
Methyl tert-butyl ether (MTBE)
mg/Kg
0.050
0.045
0.044
91.0
89.0
70-130
2.2
20
4-Methyl-2-Pentanone
mg/Kg
0.050
0.047
0.046
95.2
93.8
57-162
1.4
20
Methylene Chloride
mg/Kg
0.050
0.044
0.041
89.2
83.4
74-129
6.7
20
Naphthalene
mg/Kg
0.050
0.040
0.046
81.0
92.4
57-157
13.1
20
Date: 01/21/2022 04:07 PM Page 7 of 30
Page 67 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13890 QC Analytical Batch(es): V13891
QC Prep Batch Method: 5035 LOW Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V13890 LCSD-V13890
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
n-Propylbenzene
mg/Kg
0.050
0.041
0.043
82.0
86.0
67-130
4.7
20
Styrene
mg/Kg
0.050
0.043
0.040
86.6
80.6
77-121
7.1
20
1,1,1,2-Tetrachloroethane
mg/Kg
0.050
0.042
0.039
84.8
78.2
72-115
8.0
20
1,1,2,2-Tetrachloroethane
mg/Kg
0.050
0.042
0.041
84.6
82.6
56-126
2.3
20
Tetrachloroethene
mg/Kg
0.050
0.047
0.043
95.0
87.4
68-130
8.3
20
Toluene
mg/Kg
0.050
0.047
0.043
94.8
87.4
71-129
8.1
20
1,2,3-Trichlorobenzene
mg/Kg
0.050
0.059
0.042
119
85.0
68-130
33.1*
20
1,2,4-Trichlorobenzene
mg/Kg
0.050
0.044
0.054
89.6
109
66-125
19.8
20
1,1,1-Trichloroethane
mg/Kg
0.050
0.048
0.043
96.0
86.8
67-131
10.0
20
1,1,2-Trichloroethane
mg/Kg
0.050
0.041
0.040
83.2
80.6
70-133
3.1
20
Trichloroethene
mg/Kg
0.050
0.047
0.044
95.4
88.6
75-133
7.3
20
Trichlorofluoromethane
mg/Kg
0.050
0.054
0.047
109
95.6
44-146
13.2
20
1,2,3-Trichloropropane
mg/Kg
0.050
0.050
0.048
101
96.4
60-137
4.2
20
1,2,4-Trimethyl benzene
mg/Kg
0.050
0.046
0.046
92.2
92.0
69-129
0.2
20
1,3,5-Trimethylbenzene
mg/Kg
0.050
0.040
0.044
81.8
88.4
69-128
7.7
20
Vinyl Acetate
mg/Kg
0.050
0.053
0.050
107
102
60-140
5.1
20
Vinyl Chloride
mg/Kg
0.050
0.052
0.046
104
92.4
48-147
12.1
20
o-Xylene
mg/Kg
0.050
0.042
0.039
85.6
79.0
74-126
8.0
20
m,p-Xylene
mg/Kg
0.100
0.087
0.080
87.5
80.8
75-124
7.9
20
4-Bromofluorobenzene (S)
96.0
96.6
70-130
Dibromofluoromethane (S)
93.4
94.0
84-123
Toluene-d8 (S)
88.8
86.6
76-129
* QC Fail Date: 01/21/2022 04:07 PM Page 8 of 30
Page 68 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13898
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V13898
Associated Lab Samples: 92274, 92275, 92276, 92277
QC Analytical Batch(es): V13927
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix: SOL
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acenaphthene
mg/Kg
<0.116
0.116
0.660
01/18/22 12:57
Acenaphthylene
mg/Kg
<0.105
0.105
0.660
01/18/22 12:57
Aniline
mg/Kg
<0.152
0.152
0.660
01/18/22 12:57
Anthracene
mg/Kg
<0.143
0.143
0.660
01/18/22 12:57
Benzo(a)anthracene
mg/Kg
<0.139
0.139
0.660
01/18/22 12:57
Benzo(a)pyrene
mg/Kg
<0.147
0.147
0.660
01/18/22 12:57
Benzo(b)fluoranthene
mg/Kg
<0.146
0.146
0.660
01/18/22 12:57
Benzo(g,h,i)perylene
mg/Kg
<0.136
0.136
0.660
01/18/22 12:57
Benzo(k)fluoranthene
mg/Kg
<0.137
0.137
0.660
01/18/22 12:57
Benzoic Acid
mg/Kg
<0.580
0.580
2.00
01/18/22 12:57
Benzyl alcohol
mg/Kg
<0.105
0.105
0.660
01/18/22 12:57
Bis(2-Chloroethoxy)methane
mg/Kg
<0.118
0.118
0.660
01/18/22 12:57
Bis(2-Chloroethyl)ether
mg/Kg
<0.107
0.107
0.660
01/18/22 12:57
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.136
0.136
0.330
01/18/22 12:57
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.120
0.120
0.660
01/18/22 12:57
4-Bromophenyl phenyl ether
mg/Kg
<0.109
0.109
0.660
01/18/22 12:57
Butyl benzyl phthalate
mg/Kg
<0.113
0.113
0.330
01/18/22 12:57
4-Chloro-3-methylphenol
mg/Kg
<0.092
0.092
0.660
01/18/22 12:57
4-Chloroaniline
mg/Kg
<0.112
0.112
0.330
01/18/22 12:57
2-Chloronaphthalene
mg/Kg
<0.116
0.116
0.660
01/18/22 12:57
2-Chlorophenol
mg/Kg
<0.098
0.098
0.660
01/18/22 12:57
4-Chlorophenyl phenyl ether
mg/Kg
<0.126
0.126
1.00
01/18/22 12:57
Chrysene
mg/Kg
<0.142
0.142
0.660
01/18/22 12:57
Dibenz(a,h)anth racene
mg/Kg
<0.230
0.230
0.660
01/18/22 12:57
Dibenzofuran
mg/Kg
<0.119
0.119
0.660
01/18/22 12:57
1,2-Dichlorobenzene
mg/Kg
<0.094
0.094
0.660
01/18/22 12:57
1,3-Dichlorobenzene
mg/Kg
<0.097
0.097
0.660
01/18/22 12:57
Date:
01/21/2022 04:07 PM
Page 9 of 30
Page 69 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13898
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V13898
Associated Lab Samples: 92274, 92275, 92276, 92277
QC Analytical Batch(es): V13927
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix: SOL
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.097
0.097
0.330
01/18/22 12:57
3,3'-Dichlorobenzidine
mg/Kg
<0.147
0.147
0.660
01/18/22 12:57
2,4-Dichlorophenol
mg/Kg
<0.095
0.095
0.660
01/18/22 12:57
Diethyl phthalate
mg/Kg
<0.180
0.180
0.660
01/18/22 12:57
Dimethyl phthalate
mg/Kg
<0.174
0.174
0.660
01/18/22 12:57
2,4-Dimethylphenol
mg/Kg
<0.108
0.108
0.330
01/18/22 12:57
Di-n-butyl phthalate
mg/Kg
<0.107
0.107
0.660
01/18/22 12:57
4,6- Din itro-2-methylphenol
mg/Kg
<0.240
0.240
1.50
01/18/22 12:57
2,4-Dinitrophenol
mg/Kg
<0.520
0.520
1.50
01/18/22 12:57
2,4-Dinitrotoluene
mg/Kg
<0.096
0.096
0.660
01/18/22 12:57
2,6-Dinitrotoluene
mg/Kg
<0.108
0.108
0.660
01/18/22 12:57
Di-n-Octyl Phthalate
mg/Kg
<0.143
0.143
0.330
01/18/22 12:57
Fluoranthene
mg/Kg
<0.123
0.123
0.660
01/18/22 12:57
Fluorene
mg/Kg
<0.128
0.128
0.660
01/18/22 12:57
Hexachlorobenzene
mg/Kg
<0.106
0.106
0.660
01/18/22 12:57
Hexachlorobutadiene
mg/Kg
<0.097
0.097
0.660
01/18/22 12:57
Hexachlorocyclopentadiene
mg/Kg
<0.157
0.157
0.660
01/18/22 12:57
Hexachloroethane
mg/Kg
<0.079
0.079
0.660
01/18/22 12:57
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.179
0.179
0.660
01/18/22 12:57
Isophorone
mg/Kg
<0.191
0.191
0.660
01/18/22 12:57
1-Methylnaphthalene
mg/Kg
<0.106
0.106
0.660
01/18/22 12:57
2-Methylnaphthalene
mg/Kg
<0.100
0.100
0.660
01/18/22 12:57
2-Methylphenol
mg/Kg
<0.097
0.097
0.660
01/18/22 12:57
3&4 Methylphenol
mg/Kg
<0.084
0.084
0.660
01/18/22 12:57
Naphthalene
mg/Kg
<0.144
0.144
0.660
01/18/22 12:57
2-Nitroaniline
mg/Kg
<0.096
0.096
0.660
01/18/22 12:57
3-Nitroaniline
mg/Kg
<0.120
0.120
0.660
01/18/22 12:57
Date:
01/21/2022 04:07 PM
Page 10 of 30
Page 70 of 92

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Hart & Hickman (Charlotte)
Project Description:
CHP-046
Report No:
22-013-0026
QC Prep:
V13898
QC Analytical Batch(es): V13927
QC Prep Batch Method:
3546
Analysis Method:
8270E
Analysis Description:
Semivolatile Organic
Compounds -
GC/MS
Lab Reagent Blank
LRB-V13898
Matrix: SOL
Associated Lab Samples:
92274, 92275, 92276, 92277
Blank
MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
4-Nitroaniline
mg/Kg
<0.093
0.093
0.330
01/18/22 12:57
Nitrobenzene
mg/Kg
<0.116
0.116
0.330
01/18/22 12:57
2-Nitrophenol
mg/Kg
<0.088
0.088
0.660
01/18/22 12:57
4-Nitrophenol
mg/Kg
<0.117
0.117
0.660
01/18/22 12:57
N-Nitrosodimethylamine
mg/Kg
<0.263
0.263
0.660
01/18/22 12:57
N-Nitrosodiphenylamine
mg/Kg
<0.181
0.181
0.660
01/18/22 12:57
N-Nitroso-di-n-propylamine
mg/Kg
<0.118
0.118
0.660
01/18/22 12:57
Pentachlorophenol
mg/Kg
<0.347
0.347
1.00
01/18/22 12:57
Phenanthrene
mg/Kg
<0.208
0.208
0.660
01/18/22 12:57
Phenol
mg/Kg
<0.112
0.112
0.660
01/18/22 12:57
Pyrene
mg/Kg
<0.134
0.134
0.660
01/18/22 12:57
Pyridine
mg/Kg
<0.079
0.079
0.330
01/18/22 12:57
1,2,4-Trichlorobenzene
mg/Kg
<0.107
0.107
0.660
01/18/22 12:57
2,4,5-Trichlorophenol
mg/Kg
<0.096
0.096
0.660
01/18/22 12:57
2,4,6-Trichlorophenol
mg/Kg
<0.096
0.096
0.660
01/18/22 12:57
2-Fluorobiphenyl(S)
01/18/22 12:57
70.0
44-115
2-Fluorophenol(S)
01/18/22 12:57
82.8
35-115
Nitrobenzene-d5 (S)
01/18/22 12:57
68.8
37-122
4-Terphenyl-d14 (S)
01/18/22 12:57
74.2
54-127
2,4,6-Tribromophenol (S)
01/18/22 12:57
60.6
39-132
Phenol-d5 (S)
01/18/22 12:57
78.0
34-121
Laboratory Control Sample
LCS-V13898
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Acenaphthene
mg/Kg
1.67
1.19
71.2
40-123
Acenaphthylene
mg/Kg
1.67
1.26
75.4
32-132
Date: 01/21/2022 04:07 PM Page 11 of 30
Page 71 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13898 QC Analytical Batch(es): V13927
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V13898
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Aniline
mg/Kg
1.67
1.13
67.6
12-197
Anthracene
mg/Kg
1.67
1.29
77.2
47-123
Benzo(a)anthracene
mg/Kg
1.67
1.26
75.4
49-126
Benzo(a)pyrene
mg/Kg
1.67
1.57
94.0
45-129
Benzo(b)fluoranthene
mg/Kg
1.67
1.52
91.0
45-132
Benzo(g,h,i)perylene
mg/Kg
1.67
1.35
80.8
43-134
Benzo(k)fluoranthene
mg/Kg
1.67
1.35
80.8
47-132
Benzoic Acid
mg/Kg
1.67
<0.580
0.0*
10-83
Benzyl alcohol
mg/Kg
1.67
1.32
79.0
29-122
Bis(2-Chloroethoxy)methane
mg/Kg
1.67
1.46
87.4
36-121
Bis(2-Chloroethyl)ether
mg/Kg
1.67
1.26
75.4
31-120
Bis(2-Chloroisopropyl)ether
mg/Kg
1.67
1.27
76.0
33-131
Bis(2-ethylhexyl)phthalate
mg/Kg
1.67
0.921
55.1
51-133
4-Bromophenyl phenyl ether
mg/Kg
1.67
1.06
63.4
46-124
Butyl benzyl phthalate
mg/Kg
1.67
0.970
58.0
48-132
4-Chloro-3-methyl phenol
mg/Kg
1.67
1.24
74.2
45-122
4-Chloroaniline
mg/Kg
1.67
0.861
51.5
17-106
2-Chloronaphthalene
mg/Kg
1.67
1.17
70.0
41-114
2-Chlorophenol
mg/Kg
1.67
1.26
75.4
34-121
4-Chlorophenyl phenyl ether
mg/Kg
1.67
1.15
68.8
45-121
Chrysene
mg/Kg
1.67
1.32
79.0
50-124
Dibenz(a,h)anthracene
mg/Kg
1.67
0.828
49.5
45-134
Dibenzofuran
mg/Kg
1.67
1.20
71.8
44-120
1,2-Dichlorobenzene
mg/Kg
1.67
1.08
64.6
33-117
1,3-Dichlorobenzene
mg/Kg
1.67
1.10
65.8
30-115
1,4-Dichlorobenzene
mg/Kg
1.67
1.08
64.6
31-115
3,3'-Dichlorobenzidine
mg/Kg
1.67
0.550
0.0*
22-121
* QC Fail Date: 01/21/2022 04:07 PM Page 12 of 30
Page 72 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13898 QC Analytical Batch(es): V13927
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V13898
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
2,4-Dichlorophenol
mg/Kg
1.67
1.17
70.0
40-122
Diethyl phthalate
mg/Kg
1.67
1.26
75.4
50-124
Dimethyl phthalate
mg/Kg
1.67
1.24
74.2
48-124
2,4-Dimethylphenol
mg/Kg
1.67
1.34
80.2
30-127
Di-n-butyl phthalate
mg/Kg
1.67
1.34
80.2
51-128
4,6- Din itro-2-methylphenol
mg/Kg
1.67
0.964
0.0*
29-132
2,4-Dinitrophenol
mg/Kg
1.67
0.939
0.0*
27-129
2,4-Dinitrotoluene
mg/Kg
1.67
1.26
75.4
48-126
2,6-Dinitrotoluene
mg/Kg
1.67
1.25
74.8
46-124
Di-n-Octyl Phthalate
mg/Kg
1.67
1.00
59.8
45-140
Fluoranthene
mg/Kg
1.67
1.29
77.2
50-127
Fluorene
mg/Kg
1.67
1.24
74.2
43-125
Hexachlorobenzene
mg/Kg
1.67
1.02
61.0
45-122
Hexachlorobutadiene
mg/Kg
1.67
0.984
58.9
32-123
Hexachlorocyclopentadiene
mg/Kg
1.67
0.790
47.3
32-117
Hexachloroethane
mg/Kg
1.67
1.08
64.6
28-117
Indeno(1,2,3-cd)pyrene
mg/Kg
1.67
1.28
76.6
45-133
Isophorone
mg/Kg
1.67
1.15
68.8
30-122
1-Methylnaphthalene
mg/Kg
1.67
1.08
64.6
40-119
2-Methylnaphthalene
mg/Kg
1.67
1.09
65.2
38-122
2-Methylphenol
mg/Kg
1.67
1.28
76.6
32-122
3&4 Methylphenol
mg/Kg
1.67
1.08
64.6
34-119
Naphthalene
mg/Kg
1.67
1.16
69.4
35-123
2-Nitroaniline
mg/Kg
1.67
1.20
71.8
44-127
3-Nitroaniline
mg/Kg
1.67
1.06
63.4
33-119
4-Nitroaniline
mg/Kg
1.67
1.12
67.0
63-147
Nitrobenzene
mg/Kg
1.67
1.18
70.6
34-122
* QC Fail Date: 01/21/2022 04:07 PM Page 13 of 30
Page 73 of 92

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13898
QC Prep Batch Method: 3546
Laboratory Control Sample
Parameter
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-N itroso-d i-n-propyl a m i ne
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
4-Terphenyl-d14 (S)
2,4,6-Tribromophenol (S)
Phenol-d5 (S)
LCS-V13898
Spike
Units Conc.
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
QC Analytical Batch(es): V13927
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
LCS
Result
1.08
1.14
1.02
1.40
1.09
1.28
1.31
1.33
1.32
0.830
0.988
1.20
1.11
LCS %Rec
64.6
68.2
61.0
83.8
65.2
76.6
78.4
79.6
79.0
49.7
59.1
71.8
66.4
57.6
66.3
58.2
58.3
49.2
65.4
Rec
Limits
36-123
30-132
10-146
38-127
36-120
25-133
50-121
34-121
47-127
10-80
34-118
41-124
39-126
44-115
35-115
37-122
54-127
39-132
34-121
Matrix Spike & Matrix Spike Duplicate
V 92274-MS-V13898
V 92274-MSD-V13898
MS Spike
MSD
MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Acenaphthene
mg/Kg
<0.116
1.67
1.66
1.25
1.33
74.8
80.1
40-123
6.2
20
Acenaphthylene
mg/Kg
<0.105
1.67
1.66
1.31
1.41
78.4
84.9
32-132
7.3
20
Aniline
mg/Kg
<0.152
1.67
1.66
0.891
0.832
53.3
50.1
12-197
6.8
20
Date: 01/21/2022 04:07 PM Page 14 of 30
Page 74 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13898 QC Analytical Batch(es): V13927
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 92274-MS-V13898 V 92274-MSD-V13898
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Anthracene
mg/Kg
<0.143
1.67
1.66
1.28
1.37
76.6
82.5
47-123
6.7
20
Benzo(a)anthracene
mg/Kg
<0.139
1.67
1.66
1.23
1.36
73.6
81.9
49-126
10.0
20
Benzo(a)pyrene
mg/Kg
<0.147
1.67
1.66
1.52
1.65
91.0
99.3
45-129
8.2
20
Benzo(b)fluoranthene
mg/Kg
<0.146
1.67
1.66
1.31
1.44
78.4
86.7
45-132
9.4
20
Benzo(g,h,i)perylene
mg/Kg
<0.136
1.67
1.66
1.26
1.37
75.4
82.5
43-134
8.3
20
Benzo(k)fluoranthene
mg/Kg
<0.137
1.67
1.66
1.30
1.44
77.8
86.7
47-132
10.2
20
Benzoic Acid
mg/Kg
<0.580
1.67
1.66
0.876
1.01
0.0*
0.0*
10-83
0.0
20
Benzyl alcohol
mg/Kg
<0.105
1.67
1.66
1.41
1.50
84.4
90.3
29-122
6.1
20
Bis(2-Chloroethoxy)methane
mg/Kg
<0.118
1.67
1.66
1.33
1.58
79.6
95.1
36-121
17.1
20
Bis(2-Chloroethyl)ether
mg/Kg
<0.107
1.67
1.66
1.34
1.42
80.2
85.5
31-120
5.7
20
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.136
1.67
1.66
1.28
1.41
76.6
84.9
33-131
9.6
20
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.120
1.67
1.66
0.890
1.06
53.2
63.8
51-133
17.4
20
4-Bromophenyl phenyl ether
mg/Kg
<0.109
1.67
1.66
1.08
1.17
64.6
70.4
46-124
8.0
20
Butyl benzyl phthalate
mg/Kg
<0.113
1.67
1.66
0.921
1.02
55.1
61.4
48-132
10.2
20
4-Chloro-3-methyl phenol
mg/Kg
<0.092
1.67
1.66
1.14
1.38
68.2
83.1
45-122
19.0
20
4-Chloroaniline
mg/Kg
<0.112
1.67
1.66
0.836
1.00
50.0
60.2
17-106
17.8
20
2-Chloronaphthalene
mg/Kg
<0.116
1.67
1.66
1.21
1.35
72.4
81.3
41-114
10.9
20
2-Chlorophenol
mg/Kg
<0.098
1.67
1.66
1.30
1.45
77.8
87.3
34-121
10.9
20
4-Chlorophenyl phenyl ether
mg/Kg
<0.126
1.67
1.66
1.16
1.30
69.4
78.3
45-121
11.3
20
Chrysene
mg/Kg
<0.142
1.67
1.66
1.25
1.37
74.8
82.5
50-124
9.1
20
Dibenz(a,h)anth racene
mg/Kg
<0.230
1.67
1.66
0.788
0.876
47.1
52.7
45-134
10.5
20
Dibenzofuran
mg/Kg
<0.119
1.67
1.66
1.24
1.34
74.2
80.7
44-120
7.7
20
1,2-Dichlorobenzene
mg/Kg
<0.094
1.67
1.66
1.09
1.18
65.2
71.0
33-117
7.9
20
1,3-Dichlorobenzene
mg/Kg
<0.097
1.67
1.66
1.10
1.19
65.8
71.6
30-115
7.8
20
1,4-Dichlorobenzene
mg/Kg
<0.097
1.67
1.66
1.07
1.15
64.0
69.2
31-115
7.2
20
3,3'-Dichlorobenzidine
mg/Kg
<0.147
1.67
1.66
0.634
0.689
0.0*
41.5
22-121
4.2
20
* QC Fail Date: 01/21/2022 04:07 PM Page 15 of 30
Page 75 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13898 QC Analytical Batch(es): V13927
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 92274-MS-V13898 V 92274-MSD-V13898
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
2,4-Dichlorophenol
mg/Kg
<0.095
1.67
1.66
1.09
1.32
65.2
79.5
40-122
19.0
20
Diethyl phthalate
mg/Kg
<0.180
1.67
1.66
1.27
1.40
76.0
84.3
50-124
9.7
20
Dimethyl phthalate
mg/Kg
<0.174
1.67
1.66
1.25
1.36
74.8
81.9
48-124
8.4
30
2,4-Dimethylphenol
mg/Kg
<0.108
1.67
1.66
1.31
1.46
78.4
87.9
30-127
10.8
20
Di-n-butyl phthalate
mg/Kg
<0.107
1.67
1.66
1.34
1.42
80.2
85.5
51-128
5.7
20
4,6- Din itro-2-methylphenol
mg/Kg
<0.240
1.67
1.66
1.07
1.17
0.0*
0.0*
29-132
0.0
20
2,4-Dinitrophenol
mg/Kg
<0.520
1.67
1.66
1.12
1.23
0.0*
0.0*
27-129
0.0
20
2,4-Dinitrotoluene
mg/Kg
<0.096
1.67
1.66
1.26
1.41
75.4
84.9
48-126
11.2
20
2,6-Dinitrotoluene
mg/Kg
<0.108
1.67
1.66
1.32
1.36
79.0
81.9
46-124
2.9
20
Di-n-Octyl Phthalate
mg/Kg
<0.143
1.67
1.66
0.929
1.06
55.6
63.8
45-140
13.1
20
Fluoranthene
mg/Kg
<0.123
1.67
1.66
1.28
1.34
76.6
80.7
50-127
4.5
20
Fluorene
mg/Kg
<0.128
1.67
1.66
1.28
1.41
76.6
84.9
43-125
9.6
20
Hexachlorobenzene
mg/Kg
<0.106
1.67
1.66
1.01
1.12
60.4
67.4
45-122
10.3
20
Hexachlorobutadiene
mg/Kg
<0.097
1.67
1.66
0.896
1.06
53.6
63.8
32-123
16.7
20
Hexachlorocyclopentadiene
mg/Kg
<0.157
1.67
1.66
0.882
1.02
52.8
61.4
32-117
14.5
20
Hexachloroethane
mg/Kg
<0.079
1.67
1.66
1.04
1.13
62.2
68.0
28-117
8.2
20
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.179
1.67
1.66
1.25
1.58
74.8
95.1
45-133
23.3*
20
Isophorone
mg/Kg
<0.191
1.67
1.66
1.06
1.24
63.4
74.6
30-122
15.6
20
1-Methylnaphthalene
mg/Kg
<0.106
1.67
1.66
1.01
1.19
60.4
71.6
40-119
16.3
20
2-Methylnaphthalene
mg/Kg
<0.100
1.67
1.66
1.01
1.17
60.4
70.4
38-122
14.6
20
2-Methylphenol
mg/Kg
<0.097
1.67
1.66
1.25
1.38
74.8
83.1
32-122
9.8
20
3&4 Methylphenol
mg/Kg
<0.085
1.67
1.66
1.09
1.23
65.2
74.0
34-119
12.0
20
Naphthalene
mg/Kg
<0.144
1.67
1.66
1.09
1.26
65.2
75.9
35-123
14.4
20
2-Nitroaniline
mg/Kg
<0.096
1.67
1.66
1.27
1.41
76.0
84.9
44-127
10.4
20
3-Nitroaniline
mg/Kg
<0.120
1.67
1.66
1.19
1.35
71.2
81.3
33-119
12.5
20
4-Nitroaniline
mg/Kg
<0.093
1.67
1.66
1.16
1.20
69.4
72.2
63-147
3.3
20
* QC Fail Date: 01/21/2022 04:07 PM Page 16 of 30
Page 76 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13898 QC Analytical Batch(es): V13927
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 92274-MS-V13898 V 92274-MSD-V13898
MS Spike MSD MS Result MSD MS MSD %Rec Max
Parameter Units Result Conc. Spike Result a/oRec %Rec Limits RPD RPD
Conc.
Nitrobenzene
mg/Kg
<0.116
1.67
1.66
1.13
1.29
67.6
77.7
34-122
2-Nitrophenol
mg/Kg
<0.088
1.67
1.66
0.981
1.19
58.7
71.6
32-123
4-Nitrophenol
mg/Kg
<0.117
1.67
1.66
1.23
1.39
73.6
83.7
30-132
N-Nitrosodimethylamine
mg/Kg
<0.263
1.67
1.66
1.01
1.15
60.4
69.2
10-146
N-Nitrosodiphenylamine
mg/Kg
<0.181
1.67
1.66
1.43
1.50
85.6
90.3
38-127
N-Nitroso-di-n-propylamine
mg/Kg
<0.118
1.67
1.66
1.12
1.23
67.0
74.0
36-120
Pentachlorophenol
mg/Kg
<0.347
1.67
1.66
1.31
1.36
78.4
81.9
25-133
Phenanthrene
mg/Kg
<0.208
1.67
1.66
1.27
1.37
76.0
82.5
50-121
Phenol
mg/Kg
<0.112
1.67
1.66
1.34
1.46
80.2
87.9
34-121
Pyrene
mg/Kg
<0.134
1.67
1.66
1.26
1.41
75.4
84.9
47-127
Pyridine
mg/Kg
<0.079
1.67
1.66
0.474
0.506
28.3
30.4
10-80
1,2,4-Trichlorobenzene
mg/Kg
<0.107
1.67
1.66
0.945
1.08
56.5
65.0
34-118
2,4,5-Trichlorophenol
mg/Kg
<0.096
1.67
1.66
1.20
1.29
71.8
77.7
41-124
2,4,6-Trichlorophenol
mg/Kg
<0.096
1.67
1.66
1.23
1.29
73.6
77.7
39-126
2-Fluorobiphenyl (S)
62.8
67.4
44-115
2-Fluorophenol (S)
73.3
80.4
35-115
Nitrobenzene-d5 (S)
57.0
66.2
37-122
4-Terphenyl-d14 (S)
61.0
66.8
54-127
2,4,6-Tribromophenol (S)
55.3
59.1
39-132
Phenol-d5(S)
70.0
75.6
34-121
13.2
19.2
12.2
12.9
4.7
9.3
3.7
7.5
8.5
11.2
6.5
13.3
7.2
4.7
20
20
20
30
20
20
20
20
20
20
20
20
20
20
Date: 01/21/2022 04:07 PM Page 17 of 30
Page 77 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13928
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V14113
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V13928 Matrix: SOL
Associated Lab Samples: 92278
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acenaphthene
mg/Kg
<0.116
0.116
0.660
01/21/22 12:55
Acenaphthylene
mg/Kg
<0.105
0.105
0.660
01/21/22 12:55
Aniline
mg/Kg
<0.152
0.152
0.660
01/21/22 12:55
Anthracene
mg/Kg
<0.143
0.143
0.660
01/21/22 12:55
Benzo(a)anthracene
mg/Kg
<0.139
0.139
0.660
01/21/22 12:55
Benzo(a)pyrene
mg/Kg
<0.147
0.147
0.660
01/21/22 12:55
Benzo(b)fluoranthene
mg/Kg
<0.146
0.146
0.660
01/21/22 12:55
Benzo(g,h,i)perylene
mg/Kg
<0.136
0.136
0.660
01/21/22 12:55
Benzo(k)fluoranthene
mg/Kg
<0.137
0.137
0.660
01/21/22 12:55
Benzoic Acid
mg/Kg
<0.580
0.580
2.00
01/21/22 12:55
Benzyl alcohol
mg/Kg
<0.105
0.105
0.660
01/21/22 12:55
Bis(2-Chloroethoxy)methane
mg/Kg
<0.118
0.118
0.660
01/21/22 12:55
Bis(2-Chloroethyl)ether
mg/Kg
<0.107
0.107
0.660
01/21/22 12:55
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.136
0.136
0.330
01/21/22 12:55
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.120
0.120
0.660
01/21/22 12:55
4-Bromophenyl phenyl ether
mg/Kg
<0.109
0.109
0.660
01/21/22 12:55
Butyl benzyl phthalate
mg/Kg
<0.113
0.113
0.330
01/21/22 12:55
4-Chloro-3-methyl phenol
mg/Kg
<0.092
0.092
0.660
01/21/22 12:55
4-Chloroaniline
mg/Kg
<0.112
0.112
0.330
01/21/22 12:55
2-Chloronaphthalene
mg/Kg
<0.116
0.116
0.660
01/21/22 12:55
2-Chlorophenol
mg/Kg
<0.098
0.098
0.660
01/21/22 12:55
4-Chlorophenyl phenyl ether
mg/Kg
<0.126
0.126
1.00
01/21/22 12:55
Chrysene
mg/Kg
<0.142
0.142
0.660
01/21/22 12:55
Dibenz(a,h)anth racene
mg/Kg
<0.230
0.230
0.660
01/21/22 12:55
Dibenzofuran
mg/Kg
<0.119
0.119
0.660
01/21/22 12:55
1,2-Dichlorobenzene
mg/Kg
<0.094
0.094
0.660
01/21/22 12:55
1,3-Dichlorobenzene
mg/Kg
<0.097
0.097
0.660
01/21/22 12:55
Date:
01/21/2022 04:07 PM
Page 18 of 30
Page 78 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13928
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V14113
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V13928 Matrix: SOL
Associated Lab Samples: 92278
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.097
0.097
0.330
01/21/22 12:55
3,3'-Dichlorobenzidine
mg/Kg
<0.147
0.147
0.660
01/21/22 12:55
2,4-Dichlorophenol
mg/Kg
<0.095
0.095
0.660
01/21/22 12:55
Diethyl phthalate
mg/Kg
<0.180
0.180
0.660
01/21/22 12:55
Dimethyl phthalate
mg/Kg
<0.174
0.174
0.660
01/21/22 12:55
2,4-Dimethylphenol
mg/Kg
<0.108
0.108
0.330
01/21/22 12:55
Di-n-butyl phthalate
mg/Kg
<0.107
0.107
0.660
01/21/22 12:55
4,6- Din itro-2-methylphenol
mg/Kg
<0.240
0.240
1.50
01/21/22 12:55
2,4-Dinitrophenol
mg/Kg
<0.520
0.520
1.50
01/21/22 12:55
2,4-Dinitrotoluene
mg/Kg
<0.096
0.096
0.660
01/21/22 12:55
2,6-Dinitrotoluene
mg/Kg
<0.108
0.108
0.660
01/21/22 12:55
Di-n-Octyl Phthalate
mg/Kg
<0.143
0.143
0.330
01/21/22 12:55
Fluoranthene
mg/Kg
<0.123
0.123
0.660
01/21/22 12:55
Fluorene
mg/Kg
<0.128
0.128
0.660
01/21/22 12:55
Hexachlorobenzene
mg/Kg
<0.106
0.106
0.660
01/21/22 12:55
Hexachlorobutadiene
mg/Kg
<0.097
0.097
0.660
01/21/22 12:55
Hexachlorocyclopentadiene
mg/Kg
<0.157
0.157
0.660
01/21/22 12:55
Hexachloroethane
mg/Kg
<0.079
0.079
0.660
01/21/22 12:55
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.179
0.179
0.660
01/21/22 12:55
Isophorone
mg/Kg
<0.191
0.191
0.660
01/21/22 12:55
1-Methylnaphthalene
mg/Kg
<0.106
0.106
0.660
01/21/22 12:55
2-Methylnaphthalene
mg/Kg
<0.100
0.100
0.660
01/21/22 12:55
2-Methylphenol
mg/Kg
<0.097
0.097
0.660
01/21/22 12:55
3&4 Methylphenol
mg/Kg
<0.084
0.084
0.660
01/21/22 12:55
Naphthalene
mg/Kg
<0.144
0.144
0.660
01/21/22 12:55
2-Nitroaniline
mg/Kg
<0.096
0.096
0.660
01/21/22 12:55
3-Nitroaniline
mg/Kg
<0.120
0.120
0.660
01/21/22 12:55
Date:
01/21/2022 04:07 PM
Page 19 of 30
Page 79 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13928 QC Analytical Batch(es): V14113
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V13928 Matrix: SOL
Associated Lab Samples: 92278
Blank
MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
4-Nitroaniline
mg/Kg
<0.093
0.093
0.330
01/21/22 12:55
Nitrobenzene
mg/Kg
<0.116
0.116
0.330
01/21/22 12:55
2-Nitrophenol
mg/Kg
<0.088
0.088
0.660
01/21/22 12:55
4-Nitrophenol
mg/Kg
<0.117
0.117
0.660
01/21/22 12:55
N-Nitrosodimethylamine
mg/Kg
<0.263
0.263
0.660
01/21/22 12:55
N-Nitrosodiphenylamine
mg/Kg
<0.181
0.181
0.660
01/21/22 12:55
N-Nitroso-di-n-propylamine
mg/Kg
<0.118
0.118
0.660
01/21/22 12:55
Pentachlorophenol
mg/Kg
<0.347
0.347
1.00
01/21/22 12:55
Phenanthrene
mg/Kg
<0.208
0.208
0.660
01/21/22 12:55
Phenol
mg/Kg
<0.112
0.112
0.660
01/21/22 12:55
Pyrene
mg/Kg
<0.134
0.134
0.660
01/21/22 12:55
Pyridine
mg/Kg
<0.079
0.079
0.330
01/21/22 12:55
1,2,4-Trichlorobenzene
mg/Kg
<0.107
0.107
0.660
01/21/22 12:55
2,4,5-Trichlorophenol
mg/Kg
<0.096
0.096
0.660
01/21/22 12:55
2,4,6-Trichlorophenol
mg/Kg
<0.096
0.096
0.660
01/21/22 12:55
2-Fluorobiphenyl (S)
01/21/22 12:55
82.0
44-115
2-Fluorophenol (S)
01/21/22 12:55
91.2
35-115
Nitrobenzene-d5 (S)
01/21/22 12:55
73.0
37-122
4-Terphenyl-d14 (S)
01/21/22 12:55
83.8
54-127
2,4,6-Tribromophenol (S)
01/21/22 12:55
72.6
39-132
Phenol-d5 (S)
01/21/22 12:55
87.0
34-121
Laboratory Control Sample
LCS-V13928
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Acenaphthene
mg/Kg
1.67
1.44
86.2
40-123
Acenaphthylene
mg/Kg
1.67
1.47
88.0
32-132
Date:
01/21/2022 04:07 PM
Page 20 of 30
Page 80 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13928 QC Analytical Batch(es): V14113
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V13928
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Aniline
mg/Kg
1.67
1.34
80.2
12-197
Anthracene
mg/Kg
1.67
1.39
83.2
47-123
Benzo(a)anthracene
mg/Kg
1.67
1.38
82.6
49-126
Benzo(a)pyrene
mg/Kg
1.67
1.79
107
45-129
Benzo(b)fluoranthene
mg/Kg
1.67
1.64
98.2
45-132
Benzo(g,h,i)perylene
mg/Kg
1.67
1.48
88.6
43-134
Benzo(k)fluoranthene
mg/Kg
1.67
1.40
83.8
47-132
Benzoic Acid
mg/Kg
1.67
<0.580
0.0*
10-83
Benzyl alcohol
mg/Kg
1.67
1.56
93.4
29-122
Bis(2-Chloroethoxy)methane
mg/Kg
1.67
1.55
92.8
36-121
Bis(2-Chloroethyl)ether
mg/Kg
1.67
1.31
78.4
31-120
Bis(2-Chloroisopropyl)ether
mg/Kg
1.67
1.15
68.8
33-131
Bis(2-ethylhexyl)phthalate
mg/Kg
1.67
1.21
72.4
51-133
4-Bromophenyl phenyl ether
mg/Kg
1.67
1.31
78.4
46-124
Butyl benzyl phthalate
mg/Kg
1.67
1.27
76.0
48-132
4-Chloro-3-methyl phenol
mg/Kg
1.67
1.47
88.0
45-122
4-Chloroaniline
mg/Kg
1.67
1.08
64.6
17-106
2-Chloronaphthalene
mg/Kg
1.67
1.43
85.6
41-114
2-Chlorophenol
mg/Kg
1.67
1.47
88.0
34-121
4-Chlorophenyl phenyl ether
mg/Kg
1.67
1.40
83.8
45-121
Chrysene
mg/Kg
1.67
1.34
80.2
50-124
Dibenz(a,h)anthracene
mg/Kg
1.67
1.00
59.8
45-134
Dibenzofuran
mg/Kg
1.67
1.45
86.8
44-120
1,2-Dichlorobenzene
mg/Kg
1.67
1.19
71.2
33-117
1,3-Dichlorobenzene
mg/Kg
1.67
1.24
74.2
30-115
1,4-Dichlorobenzene
mg/Kg
1.67
1.20
71.8
31-115
3,3'-Dichlorobenzidine
mg/Kg
1.67
0.946
56.6
22-121
* QC Fail Date: 01/21/2022 04:07 PM Page 21 of 30
Page 81 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13928 QC Analytical Batch(es): V14113
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V13928
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
2,4-Dichlorophenol
mg/Kg
1.67
1.37
82.0
40-122
Diethyl phthalate
mg/Kg
1.67
1.50
89.8
50-124
Dimethyl phthalate
mg/Kg
1.67
1.45
86.8
48-124
2,4-Dimethylphenol
mg/Kg
1.67
1.50
89.8
30-127
Di-n-butyl phthalate
mg/Kg
1.67
1.52
91.0
51-128
4,6- Din itro-2-methylphenol
mg/Kg
1.67
1.10
0.0*
29-132
2,4-Dinitrophenol
mg/Kg
1.67
1.05
0.0*
27-129
2,4-Dinitrotoluene
mg/Kg
1.67
1.46
87.4
48-126
2,6-Dinitrotoluene
mg/Kg
1.67
1.46
87.4
46-124
Di-n-Octyl Phthalate
mg/Kg
1.67
1.27
76.0
45-140
Fluoranthene
mg/Kg
1.67
1.42
85.0
50-127
Fluorene
mg/Kg
1.67
1.50
89.8
43-125
Hexachlorobenzene
mg/Kg
1.67
1.24
74.2
45-122
Hexachlorobutadiene
mg/Kg
1.67
1.16
69.4
32-123
Hexachlorocyclopentadiene
mg/Kg
1.67
1.01
60.4
32-117
Hexachloroethane
mg/Kg
1.67
1.15
68.8
28-117
Indeno(1,2,3-cd)pyrene
mg/Kg
1.67
1.53
91.6
45-133
Isophorone
mg/Kg
1.67
1.18
70.6
30-122
1-Methylnaphthalene
mg/Kg
1.67
1.26
75.4
40-119
2-Methylnaphthalene
mg/Kg
1.67
1.21
72.4
38-122
2-Methylphenol
mg/Kg
1.67
1.36
81.4
32-122
3&4 Methylphenol
mg/Kg
1.67
1.20
71.8
34-119
Naphthalene
mg/Kg
1.67
1.30
77.8
35-123
2-Nitroaniline
mg/Kg
1.67
1.52
91.0
44-127
3-Nitroaniline
mg/Kg
1.67
1.41
84.4
33-119
4-Nitroaniline
mg/Kg
1.67
1.42
85.0
63-147
Nitrobenzene
mg/Kg
1.67
1.25
74.8
34-122
* QC Fail Date: 01/21/2022 04:07 PM Page 22 of 30
Page 82 of 92

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13928
QC Prep Batch Method: 3546
Laboratory Control Sample
Parameter
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-N itroso-d i-n-propyl a m i ne
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
4-Terphenyl-d14 (S)
2,4,6-Tribromophenol (S)
Phenol-d5 (S)
LCS-V13928
Spike
Units Conc.
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
QC Analytical Batch(es): V14113
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
LCS
Result
1.27
1.41
1.11
1.61
1.20
1.52
1.42
1.48
1.43
0.899
1.19
1.43
1.47
LCS %Rec
76.0
84.4
66.4
96.4
71.8
91.0
85.0
88.6
85.6
53.8
71.2
85.6
88.0
83.2
91.5
71.8
80.8
77.1
86.7
Rec
Limits
36-123
30-132
10-146
38-127
36-120
25-133
50-121
34-121
47-127
10-80
34-118
41-124
39-126
44-115
35-115
37-122
54-127
39-132
34-121
Matrix Spike & Matrix Spike Duplicate
V 92278-MS-V13928
V 92278-MSD-V13928
MS Spike
MSD
MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Acenaphthene
mg/Kg
<0.116
1.67
1.67
1.27
1.33
76.0
79.6
40-123
4.6
20
Acenaphthylene
mg/Kg
<0.105
1.67
1.67
1.33
1.41
79.6
84.4
32-132
5.8
20
Aniline
mg/Kg
<0.152
1.67
1.67
0.912
0.924
54.6
55.3
12-197
1.3
20
Date: 01/21/2022 04:07 PM Page 23 of 30
Page 83 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13928 QC Analytical Batch(es): V14113
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 92278-MS-V13928 V 92278-MSD-V13928
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Anthracene
mg/Kg
<0.143
1.67
1.67
1.39
1.36
83.2
81.4
47-123
2.1
20
Benzo(a)anthracene
mg/Kg
<0.139
1.67
1.67
1.33
1.39
79.6
83.2
49-126
4.4
20
Benzo(a)pyrene
mg/Kg
<0.147
1.67
1.67
1.73
1.72
104
103
45-129
0.5
20
Benzo(b)fluoranthene
mg/Kg
<0.146
1.67
1.67
1.51
1.50
90.4
89.8
45-132
0.6
20
Benzo(g,h,i)perylene
mg/Kg
<0.136
1.67
1.67
1.42
1.46
85.0
87.4
43-134
2.7
20
Benzo(k)fluoranthene
mg/Kg
<0.137
1.67
1.67
1.42
1.45
85.0
86.8
47-132
2.0
20
Benzoic Acid
mg/Kg
<0.580
1.67
1.67
1.05
1.07
0.0*
0.0*
10-83
0.0
20
Benzyl alcohol
mg/Kg
<0.105
1.67
1.67
1.51
1.56
90.4
93.4
29-122
3.2
20
Bis(2-Chloroethoxy)methane
mg/Kg
<0.118
1.67
1.67
1.42
1.50
85.0
89.8
36-121
5.4
20
Bis(2-Chloroethyl)ether
mg/Kg
<0.107
1.67
1.67
1.37
1.37
82.0
82.0
31-120
0.0
20
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.136
1.67
1.67
1.10
1.16
65.8
69.4
33-131
5.3
20
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.120
1.67
1.67
1.15
1.14
68.8
68.2
51-133
0.8
20
4-Bromophenyl phenyl ether
mg/Kg
<0.109
1.67
1.67
1.23
1.27
73.6
76.0
46-124
3.2
20
Butyl benzyl phthalate
mg/Kg
<0.113
1.67
1.67
1.22
1.23
73.0
73.6
48-132
0.8
20
4-Chloro-3-methyl phenol
mg/Kg
<0.092
1.67
1.67
1.35
1.43
80.8
85.6
45-122
5.7
20
4-Chloroaniline
mg/Kg
<0.112
1.67
1.67
1.00
1.01
59.8
60.4
17-106
0.9
20
2-Chloronaphthalene
mg/Kg
<0.116
1.67
1.67
1.26
1.31
75.4
78.4
41-114
3.8
20
2-Chlorophenol
mg/Kg
<0.098
1.67
1.67
1.35
1.40
80.8
83.8
34-121
3.6
20
4-Chlorophenyl phenyl ether
mg/Kg
<0.126
1.67
1.67
1.27
1.30
76.0
77.8
45-121
2.3
20
Chrysene
mg/Kg
<0.142
1.67
1.67
1.34
1.35
80.2
80.8
50-124
0.7
20
Dibenz(a,h)anth racene
mg/Kg
<0.230
1.67
1.67
0.938
0.953
56.1
57.0
45-134
1.5
20
Dibenzofuran
mg/Kg
<0.119
1.67
1.67
1.28
1.31
76.6
78.4
44-120
2.3
20
1,2-Dichlorobenzene
mg/Kg
<0.094
1.67
1.67
1.18
1.17
70.6
70.0
33-117
0.8
20
1,3-Dichlorobenzene
mg/Kg
<0.097
1.67
1.67
1.16
1.20
69.4
71.8
30-115
3.3
20
1,4-Dichlorobenzene
mg/Kg
<0.097
1.67
1.67
1.17
1.18
70.0
70.6
31-115
0.8
20
3,3'-Dichlorobenzidine
mg/Kg
<0.147
1.67
1.67
0.867
0.902
51.9
54.0
22-121
3.9
20
* QC Fail Date: 01/21/2022 04:07 PM Page 24 of 30
Page 84 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13928 QC Analytical Batch(es): V14113
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 92278-MS-V13928 V 92278-MSD-V13928
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
2,4-Dichlorophenol
mg/Kg
<0.095
1.67
1.67
1.32
1.35
79.0
80.8
40-122
2.2
20
Diethyl phthalate
mg/Kg
<0.180
1.67
1.67
1.40
1.41
83.8
84.4
50-124
0.7
20
Dimethyl phthalate
mg/Kg
<0.174
1.67
1.67
1.35
1.38
80.8
82.6
48-124
2.1
30
2,4-Dimethylphenol
mg/Kg
<0.108
1.67
1.67
1.48
1.49
88.6
89.2
30-127
0.6
20
Di-n-butyl phthalate
mg/Kg
<0.107
1.67
1.67
1.51
1.51
90.4
90.4
51-128
0.0
20
4,6- Din itro-2-methylphenol
mg/Kg
<0.240
1.67
1.67
1.20
1.23
0.0*
0.0*
29-132
0.0
20
2,4-Dinitrophenol
mg/Kg
<0.520
1.67
1.67
1.23
1.26
0.0*
0.0*
27-129
0.0
20
2,4-Dinitrotoluene
mg/Kg
<0.096
1.67
1.67
1.36
1.40
81.4
83.8
48-126
2.8
20
2,6-Dinitrotoluene
mg/Kg
<0.108
1.67
1.67
1.35
1.42
80.8
85.0
46-124
5.0
20
Di-n-Octyl Phthalate
mg/Kg
<0.143
1.67
1.67
1.20
1.21
71.8
72.4
45-140
0.8
20
Fluoranthene
mg/Kg
<0.123
1.67
1.67
1.41
1.38
84.4
82.6
50-127
2.1
20
Fluorene
mg/Kg
<0.128
1.67
1.67
1.35
1.38
80.8
82.6
43-125
2.1
20
Hexachlorobenzene
mg/Kg
<0.106
1.67
1.67
1.19
1.17
71.2
70.0
45-122
1.6
20
Hexachlorobutadiene
mg/Kg
<0.097
1.67
1.67
1.06
1.10
63.4
65.8
32-123
3.7
20
Hexachlorocyclopentadiene
mg/Kg
<0.157
1.67
1.67
0.951
0.990
56.9
59.2
32-117
4.0
20
Hexachloroethane
mg/Kg
<0.079
1.67
1.67
1.09
1.14
65.2
68.2
28-117
4.4
20
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.179
1.67
1.67
1.44
1.44
86.2
86.2
45-133
0.0
20
Isophorone
mg/Kg
<0.191
1.67
1.67
1.16
1.18
69.4
70.6
30-122
1.7
20
1-Methylnaphthalene
mg/Kg
<0.106
1.67
1.67
1.16
1.20
69.4
71.8
40-119
3.3
20
2-Methylnaphthalene
mg/Kg
<0.100
1.67
1.67
1.16
1.19
69.4
71.2
38-122
2.5
20
2-Methylphenol
mg/Kg
<0.097
1.67
1.67
1.30
1.34
77.8
80.2
32-122
3.0
20
3&4 Methylphenol
mg/Kg
<0.084
1.67
1.67
1.14
1.15
68.2
68.8
34-119
0.8
20
Naphthalene
mg/Kg
<0.144
1.67
1.67
1.22
1.26
73.0
75.4
35-123
3.2
20
2-Nitroaniline
mg/Kg
<0.096
1.67
1.67
1.37
1.37
82.0
82.0
44-127
0.0
20
3-Nitroaniline
mg/Kg
<0.120
1.67
1.67
1.21
1.28
72.4
76.6
33-119
5.6
20
4-Nitroaniline
mg/Kg
<0.093
1.67
1.67
1.33
1.35
79.6
80.8
63-147
1.4
20
* QC Fail Date: 01/21/2022 04:07 PM Page 25 of 30
Page 85 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13928 QC Analytical Batch(es): V14113
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 92278-MS-V13928 V 92278-MSD-V13928
MS Spike MSD MS Result MSD MS MSD %Rec Max
Parameter Units Result Conc. Spike Result a/oRec %Rec Limits RPD RPD
Conc.
Nitrobenzene
mg/Kg
<0.116
1.67
1.67
1.17
1.22
70.0
73.0
34-122
2-Nitrophenol
mg/Kg
<0.088
1.67
1.67
1.17
1.25
70.0
74.8
32-123
4-Nitrophenol
mg/Kg
<0.117
1.67
1.67
1.26
1.27
75.4
76.0
30-132
N-Nitrosodimethylamine
mg/Kg
<0.263
1.67
1.67
1.07
1.13
64.0
67.6
10-146
N-Nitrosodiphenylamine
mg/Kg
<0.181
1.67
1.67
1.56
1.58
93.4
94.6
38-127
N-Nitroso-di-n-propylamine
mg/Kg
<0.118
1.67
1.67
1.11
1.16
66.4
69.4
36-120
Pentachlorophenol
mg/Kg
<0.347
1.67
1.67
1.51
1.52
90.4
91.0
25-133
Phenanthrene
mg/Kg
<0.208
1.67
1.67
1.40
1.42
83.8
85.0
50-121
Phenol
mg/Kg
<0.112
1.67
1.67
1.36
1.39
81.4
83.2
34-121
Pyrene
mg/Kg
<0.134
1.67
1.67
1.43
1.47
85.6
88.0
47-127
Pyridine
mg/Kg
<0.079
1.67
1.67
0.540
0.628
32.3
37.6
10-80
1,2,4-Trichlorobenzene
mg/Kg
<0.107
1.67
1.67
1.09
1.14
65.2
68.2
34-118
2,4,5-Trichlorophenol
mg/Kg
<0.096
1.67
1.67
1.30
1.34
77.8
80.2
41-124
2,4,6-Trichlorophenol
mg/Kg
<0.096
1.67
1.67
1.32
1.39
79.0
83.2
39-126
2-Fluorobiphenyl (S)
73.0
76.0
44-115
2-Fluorophenol (S)
86.7
88.3
35-115
Nitrobenzene-d5 (S)
70.0
70.6
37-122
4-Terphenyl-d14 (S)
80.2
82.0
54-127
2,4,6-Tribromophenol (S)
71.7
76.0
39-132
Phenol-d5 (S)
82.2
83.2
34-121
4.1
6.6
0.7
5.4
1.2
4.4
0.6
1.4
2.1
2.7
15.0
4.4
3.0
5.1
20
20
20
30
20
20
20
20
20
20
20
20
20
20
Date: 01/21/2022 04:07 PM Page 26 of 30
Page 86 of 92

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Hart & Hickman (Charlotte)
Project Description:
CHP-046
Report No:
22-013-0026
QC Prep:
V13950
QC Analytical Batch(es): V14062
QC Prep Batch Method:
MAEPH (Prep)
Analysis Method:
MADEP-EPH
Analysis Description:
Massachusetts EPH
Lab Reagent Blank
LRB-V13950
Matrix: SOL
Associated Lab Samples:
92274, 92275, 92276, 92277, 92278
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
Aliphatic C9-C18
mg/Kg
<9.20 9.20
50.0
01/20/22 12:03
Aliphatic C19-06
mg/Kg
<12.2 12.2
50.0
01/20/22 12:03
Aromatic C11-C22
mg/Kg
<14.2 14.2
50.0
01/20/22 12:03
2-Fluorobiphenyl(S)
01/20/22 12:03
71.7
40-140
2-Bromonaphthalene (S)
01/20/22 12:03
87.7
40-140
Chlorooctadecane (S)
01/20/22 12:03
96.5
40-140
OTP Surrogate (S)
01/20/22 12:03
72.0
40-140
Laboratory Control Sample
LCS-V13950
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Aliphatic C9-C18
mg/Kg
80.0
37.3
0.0*
40-140
Aliphatic C19-06
mg/Kg
60.0
72.8
121
40-140
Aromatic C11-C22
mg/Kg
170
126
74.1
40-140
2-Fluorobiphenyl (S)
79.5
40-140
2-Bromonaphthalene (S)
100
40-140
Chlorooctadecane (S)
97.0
40-140
OTP Surrogate (S)
77.0
40-140
Matrix Spike & Matrix Spike Duplicate
V 92278-MS-V13950
V 92278-MSD-V13950
MS Spike
MSD MS Result
MSD MS
MSD
%Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec
Limits RPD RPD
Conc.
Aliphatic C9-C18
Aliphatic C19-06
Aromatic C11-C22
2-Fluorobiphenyl (S)
mg/Kg <9.20 80.0 80.3 36.6
35.5 0.0*
0.0*
40-140 0.0 50
mg/Kg <12.2 60.0 60.2 73.7
73.1 123
121
40-140 0.8 50
mg/Kg <14.2 170 171 121
126 71.1
73.6
40-140 4.0 50
78.2
82.3
40-140
* QC Fail Date: 01/21/2022 04:07 PM Page 27 of 30
Page 87 of 92

Waypointo
ANALYTICAL
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V13950 QC Analytical Batch(es): V14062
QC Prep Batch Method: MAEPH (Prep) Analysis Method: MADEP-EPH
Analysis Description: Massachusetts EPH
Matrix Spike & Matrix Spike Duplicate V 92278-MS-V13950 V 92278-MSD-V13950
MS Spike MSD MS Result MSD MS MSD %Rec Max
Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD
Conc.
2-Bromonaphthalene (S)
97.7
102
40-140
Chlorooctadecane (S)
90.5
93.0
40-140
OTP Surrogate (S)
73.5
75.1
40-140
Date: 01/21/2022 04:07 PM Page 28 of 30
Page 88 of 92

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Prep: V13839
QC Analytical Batch(es): V13840
QC Prep Batch Method: MAVPH (Prep)
Analysis Method:
MADEP-VPH
Analysis Description:
Massachusetts VPH
Lab Reagent Blank
LRB-V13839
Matrix: SOL
Associated Lab Samples: 92274, 92275, 92276, 92277, 92278
Blank MDL
MQL
Analyzed
%
% Rec
Parameter Units
Result
Recovery
Limits
Aliphatic C5-C8 mg/Kg
<1.22 1.22
8.00
01/14/22 13:53
Aliphatic C9-C12 mg/Kg
<4.56 4.56
8.00
01/14/22 13:53
Aromatic C9-C10 mg/Kg
<0.624 0.624
8.00
01/14/22 13:53
2,5-Dibromotoluene (FID)(S)
01/14/22 13:53
83.5
70-130
2,5-Dibromotoluene (PID)(S)
01/14/22 13:53
78.1
70-130
Laboratory Control Sample & LCSD
LCS-V13839 LCSD-V13839
Spike
LCS LCSD
LCS LCSD
% Rec
Parameter Units
Conc.
Result Result
%Rec a/o Rec
Limits
RPD
Max
RPD
Aliphatic C5-C8 mg/Kg
32.0
34.0 33.6
106 105
70-130
1.1
50
Aliphatic C9-C12 mg/Kg
32.0
30.9 30.7
96.5 95.9
70-130
0.6
50
Aromatic C9-C10 mg/Kg
10.7
10.3 10.1
96.2 94.3
70-130
1.9
50
2,5-Dibromotoluene (FID) (S)
85.3 92.3
70-130
2,5-Dibromotoluene (PID) (S)
79.9 85.4
70-130
Date: 01/21/2022 04:07 PM Page 29 of 30
Page 89 of 92

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Hart & Hickman (Charlotte)
Project Description: CHP-046
Report No: 22-013-0026
QC Analytical Batch: V13967
Analysis Method: SW-DRYWT
Analysis Description: Dry Weight Determination
Duplicate V 92208-DUP
Result DUP
Parameter Units Result
Moisture % 12.1 12.0
RPD Max RPD Analyzed
0.8 20.0 01/19/2212:09
Date: 01/21/2022 04:07 PM Page 30 of 30
Page 90 of 92

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01102
Customer Name: Hart & Hickman (Charlotte)
Report Number: 22-013-0026
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IRT-15 3.2C
Shipping container/cooler uncompromised?
CO,) Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample Iabel(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
U Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
U Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
C*J No
0 N/A
Soil VOA method 5035 — compliance criteria met
F_ High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No 0 N/A
F Low concentration EnCore samplers (48 hr)
I✓ Low conc pre -weighed vials (Sod Bis -14 d)
0Yes ONo
Signature: Sarah J. Locklear
Date & Time: 01/13/2022 16:43:14
Page 91 of 92

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Page 92 of 92

Beverly, Trudy
From: Steve Libbey <[e-mail]>
Sent: Thursday, February 10, 2022 11:10 AM
To: Beverly, Trudy
Subject: RE: [External] Home Heating Oil UST Release; 724 West Sugar Creek, Charlotte, NC
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Thanks! You can send the response to me.
Steve
From: Beverly, Trudy <[e-mail]>
Sent: Thursday, February 10, 2022 10:59 AM
To: Steve Libbey <[e-mail]>
Subject: RE: [External] Home Heating Oil UST Release; 724 West Sugar Creek, Charlotte, NC
Hey Steve,
I don't have time to review the report today. I'll try to get to it tomorrow morning and get back with you. Do you have
an email address for the rp/property owner for sending a response to the review?
Thanks,
Trudy
D�. E
fH
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlygncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-pro2Tam
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
bit.ps://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
htti)s:Hfiles.ne.izov/nedep/Waste%2OMana2ement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policy.odf
https:Hfiles.nc. gov/ncdegfWaste%20Management/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Steve Libbey [mailto:[e-mail]]
Sent: Thursday, February 10, 2022 10:26 AM
To: Beverly, Trudy <[e-mail]>
Subject: RE: [External] Home Heating Oil UST Release; 724 West Sugar Creek, Charlotte, NC

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Hi Trudy, I understand you haven't had this report long, but the client emailed me about it this morning. Apparently, the
bank has requested an NFA letter for the closing documents. Have you had a chance to look at this report? I'd like to
give them a realistic timeframe for when they can expect an NFA letter?
Thanks,
Steve
From: Beverly, Trudy <[e-mail]>
Sent: Thursday, February 3, 2022 6:42 AM
To: Steve Libbey <[e-mail]>
Subject: RE: [External] Home Heating Oil UST Release; 724 West Sugar Creek, Charlotte, NC
Received.
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
it r- ��- North Carolina Department of Environmental Quality
5� UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.Beverlykncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-manaaement/ust
Branch's Above Ground Storage Tanks Website Address: https:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-proeram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. eov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaeement-eis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hi�2s://deg.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httos://files.nc.eov/ncdep/Waste%2OManaeement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policv.adf
hops://files.nc.,gov/ncdegiWaste%2OManagement/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Steve Libbey[mailto:[e-mail]]
Sent: Wednesday, February 2, 2022 4:39 PM
To: Beverly, Trudy <[e-mail]>
Subject: RE: [External] Home Heating Oil UST Release; 724 West Sugar Creek, Charlotte, NC
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Hi Trudy, the IAA is attached.
Please call me if you have any questions.
Thanks,

Steve
9wd m Llbbelr. PG.ProMamer
Hwt & Hlckmm, PC
2823 S Trpn frod. SuitQ IGO • Cbmtome. NG 28M
www T� a7 Mobile #�a
From: Beverly, Trudy <[e-mail]>
Sent: Wednesday, January 19, 2022 11:56 AM
To: Steve Libbey <[e-mail]>
Subject: RE: [External] Home Heating Oil UST Release; 724 West Sugar Creek, Charlotte, NC
Hey Steve,
I handle unregulated usts for Mecklenburg county. The UST-61 got to the correct project manager. Document
received. Please email future documentation related to the release to me.
Have a wonderful day,
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
� mentLLY� UST Section, Mooresville Regional Office
rtnnrt o1 Kirmvn
704.235.2182 (Office)
Trudy. B everlygriedenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: ht_pt s://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://dea.ne. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-mans
File Review Procedures:
htips://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
httDs: //dea.nc. gov/about/divisions/waste-mana2ement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https:Hfiles.nc.gov/ncdecliW aste°/"2OManagement[DWM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policy.ndf
https:Hfiles.nc.gov/ncdeq/Waste%2OManagement/D WMfU ST/Corrective%2OAction/UST°/a20file%20names%20for°/`2OLaserfiche.docx
From: Steve Libbey [mailto:[e-mail]]
Sent: Wednesday, January 19, 2022 11:12 AM
To: Beverly, Trudy <[e-mail]>
Subject: [External] Home Heating Oil UST Release; 724 West Sugar Creek, Charlotte, NC
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Hi Trudy, please find attached a 24-Hour Release Notice for a heating oil UST removed at the above -referenced
address. Please let me know if it needs to be sent to someone else.
Please call me if you have any questions or would like to discuss the UST closure activities.

Thanks,
Steve
Swm l.lbbey, PG. Project der
Ilea l!i I Ikkmeq. PC
2923 81 Sleet. S+uke 100 • Charlotte. NC 2 i
Direct OAN • Wbilm IM-302
VIM'-arthaaom I UE3 a