3901_Granville_Oxford_MSWLF_Unit2_Feb22GW_FID1684611_20220617

GARRETT� /
& MOORE
Engineering for the Power and Waste Industries
June 15, 2022
Ms. Jaclynne Drummond
Department. of Environmental Quality
Solid Waste Section
Asheville Regional Office
2090 US Highway 70
Swannanoa, North Carolina 28778
0aclynne.drummond(a)-ncdenr.gov
RE: Water Quality Monitoring Report — February 2022 Event
Granville County Oxford Unit 2 Landfill
Oxford, North Carolina
Permit # 3901—MSWLF-2012
Dear Jackie:
On behalf of Granville County, please find attached the Water Quality Monitoring Report for the
Oxford Unit 2 Landfill for the 1st semi-annual sampling event of 2022. If you have any questions
or require further assistance regarding this matter, please do not hesitate to call me at 919-792-
1903.
Sincerely,
Garrett & Moore, Inc.
S efan Bra , P.E.
Cc: Jason Falls, Granville County
1029 West South Street • Raleigh, North Carolina 27 • O: 919-792-1900 • F: 866-311-7206

hart '� hickman
SMARTER ENVIRONMENTAL SOLUTIONS
Via E-Mail
sbray@garrett-moore. com
June 14, 2022
Garrett & Moore, Inc.
1029 West South Street
Raleigh, NC 27603
Attn: Mr. Stefan Bray, PE
Re: Water Quality Monitoring Report — February 2022
Granville County Oxford Unit 2 Landfill
Oxford, Granville County, NC
Facility Permit No. 3901-MSWLF-2012
H&H Job No. GMI-005
Dear Stefan:
Hart & Hickman, PC (H&H) is submitting the attached Water Quality Monitoring Report —
February 2022 documenting sample results for the Oxford Unit 2 Landfill for the first semiannual
sampling event of 2022. H&H appreciates the opportunity to work with you on this project. If
you have any questions or require additional information, please do not hesitate to contact us at
704-586-0007.
Very truly yours,
Hart & Hickman, PC
Jason Soban, PG
Project Manager
Jeffrey 011ison
Project Environmental Scientist
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007 main
3921 Sunset Ridge Rd, Suite 301
Raleigh, NC 27607 www.harthickman.com
919.847.4241 main

_ /l.___ 6�I I i�/Z'-
Signature Date
2923 S Tryon Street, Suite 100, Charlotte, NC 28203
Facility Representative Address
C-1269 (Engineering) 245 (Geology)
NC PE Firm License Number (if applicable effective May 1, 2009)
ENR USE ONLY-± ❑Paper Report ❑Eleclronic Data - Email CD data loaded: Yes / No) Doc/Event #:
NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant; facility owner):
Garrett & Moore, Inc.
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Stefan Bray Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Granville County 6854 Landfill Road 3901- .1600 February 15-17, 2022
Oxford Landfill Unit 2 Oxford, NC 27565 MSWLF-2012
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑ Detection Monitoring 0 Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells HGroundwater monitoring data from private water supply wells
Leachate monitoring data ❑
Surface water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
e No. No groundwater or surface water standards were exceeded.
Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values. NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Jason Soban, PG Consultant for Facility [phone]
Facility Representative Name (Print) Title (Area Code) Telephone Nu
Affix NC Licensed/ Professional Geologist Seal
ril►t�11te9010"0
.•�''� .......... C A R !,, '+,,
SEAL =
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Revised 6/2009

Water Quality Monitoring Report
February 2022
Granville County Oxford Unit 2 Landfill
Oxford, North Carolina
Permit No. 3901-MSWLF-2012
H&H Job No. GMI-005
June 14, 2022
oJ�j�V OF�99�' THE COUNTY OF
'�yoy 774% `ye NORTH CAROLINA
ZOIm .h AR��.
GMUZEn
&MOOREtA2
Engineering for the Power and Waste Industries
hart � hickman
SMARTER ENVIRONMENTAL SOLUTIONS
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

Water Quality Monitoring Report — February 2022
Granville County Oxford Unit 2 Landfill
Oxford, North Carolina
Permit No. 3901-MSWLF-2012
H&H Job No. GMI-005
Table of Contents
Section Pate
1.0 Introduction.................................................................................................................1
1.1
Site Information........................................................................................................1
1.2
Regulatory Status......................................................................................................2
1.3
Groundwater Monitoring Program...........................................................................2
1.4
Surface Water Monitoring Program.........................................................................2
2.0 Water Quality Monitoring Activities........................................................................3
2.1
Water Level Measurements......................................................................................3
2.2
Groundwater Sampling Methods..............................................................................3
2.3
Surface Water Sampling Methods............................................................................4
2.4
Sample Equipment Management..............................................................................4
2.5
Sample Handling and Laboratory Analyses
.............................................................4
3.0 Water Quality Monitoring Results............................................................................6
3.1
Groundwater Flow and Hydraulic Gradient
.............................................................6
3.2
Groundwater Analytical Results...............................................................................7
3.3
Surface Water Analytical Results.............................................................................8
3.4
Quality Assurance/Quality Control Results
..............................................................8
4.0 Conclusions
................................................................................................................10
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List of Tables
Table 1
Summary of Well Construction Details
Table 2
Summary of Groundwater Elevations
Table 3
Summary of Field Parameters
Table 4
Summary of Groundwater Flow Velocity
Table 5
Summary of Constituent Detections (February 2022)
List of Figures
Figure 1 Site Location Map
Figure 2 Site Plan
Figure 3 Groundwater Potentiometric Map (February 15, 2022)
List of Appendices
Appendix A
Groundwater and Surface Water Sampling Records
Appendix B
Laboratory Analytical Reports
Appendix C
Summary of Historical Groundwater Elevations
Appendix D
Summary of Historical Constituents in Groundwater
Appendix E
Summary of Historical Constituents in Surface Water
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Water Quality Monitoring Report — February 2022
Granville County Oxford Unit 2 Landfill
Oxford, North Carolina
Permit No. 3901-MSWLF-2012
H&H Job No. GMI-005
1.0 Introduction
This Water Quality Monitoring Report (Report) has been prepared by Hart & Hickman, PC (H&H)
to document the methods and results of semiannual groundwater and surface water monitoring
activities conducted at the Granville County Oxford Unit 2 Landfill located at 6584 Landfill Road,
Oxford, Granville County, North Carolina. A site location map is included as Figure 1. Water
quality monitoring at the site was performed in general accordance with the Water Quality
Monitoring Plan (March 2019) which was approved by the North Carolina Department of
Environmental Quality (DEQ) Solid Waste Section (SWS).
1.1 Site Information
The Granville County Oxford Landfill consists of two separate waste disposal units (Unit 1 and
Unit 2). The facility is owned and operated by Granville County under Permit Numbers 3901-
CDLF-1997 (Unit 1) and 3901-MSWLF-2012 (Unit 2) issued by DEQ SWS. The permitted
facility consists of approximately 283 acres, of which approximately 29 acres constitutes the Unit
1 waste unit and 37.3 acres constitutes the Unit 2 waste unit. A site layout map that depicts the
facility features is included as Figure 2.
The Oxford Unit 1 Landfill is a former unlined municipal solid waste (MSW) landfill originally
permitted for disposal of domestic, institutional, industrial, agricultural, and demolition wastes.
The Oxford Unit 1 Landfill was closed in 1997. Between 1997 and 2017, the facility disposed of
construction and demolition (C&D) waste on top of the closed MSW landfill in accordance with
the Transition Plan dated 1994. The subject Oxford Unit 2 Landfill is a Subtitle-D MSW landfill
which was permitted to operate in February 2013 and began receiving waste in May 2013. This
Report covers water quality monitoring conducted at the Oxford Unit 2 Landfill. A separate Water
Quality Monitoring Report will be submitted for the Oxford Unit 1 Landfill.
1
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1.2 Regulatory Status
The Granville County Oxford Unit 2 Landfill is currently in a Detection Monitoring Program.
Water quality monitoring is completed following the North Carolina Administrative Code Title
15A-Environmental Quality Chapter 13 Sub -Chapter B Solid Waste Management Rule
(NCSWMR) § 1633. Statistical analyses of the laboratory data when required is prepared
following the required compliance demonstration of the NCSWMR Rule .1632(g), (h), and (i).
1.3 Groundwater Monitoring Program
The groundwater monitoring program at the Oxford Unit 2 Landfill consists of the following six
monitoring wells: MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S. Monitoring well MW-
7 is located south and upgradient of the landfill and serves as a background location. Compliance
monitoring well MW-8 serves to monitor groundwater conditions downgradient of the leachate
tank area which is located south to southwest and upgradient of the landfill. Compliance
monitoring wells MW-9, MW-10, MW-11, and NES-2S are located along the northern
downgradient side of the landfill. Groundwater samples are collected semiannually for analysis
of North Carolina Solid Waste Management Rules Appendix I list of constituents (hereafter
referred to as Appendix I constituents). The monitoring well locations and other site features are
identified on Figure 2. A summary of well construction details is provided in Table 1.
1.4 Surface Water Monitoring Program
The surface water monitoring program at the Oxford Unit 2 Landfill consists of collecting samples
from two locations which are located upstream (SW-3) and downstream (SW-4) of the waste unit.
The sampling points are situated along an unnamed tributary to Little Grassy Creek which runs
along the eastern side of the landfill. Little Grassy Creek is classified as a Class C (Aquatic Life
and Secondary Recreation) stream. The locations of the surface water monitoring points are
identified on Figure 2. Surface water samples are collected semiannually and analyzed for NC
Appendix I constituents plus 1,4-dioxane.
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2.0 Water Quality Monitoring Activities
2.1 Water Level Measurements
On February 15, 2022, Environmental Field Management, Inc. (EFM) measured depth -to -water
and total depths in monitoring wells MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S.
Depth -to -water measurements were collected from the top -of -casing utilizing a decontaminated
electronic water level indicator. Depth -to -water measurements were made after the wells were
opened for a sufficient period of time to allow water levels to equilibrate with atmospheric
pressure. Water level measurements and calculated groundwater elevations are presented in Table
2.
2.2 Groundwater Sampling Methods
On February 15 and 17, 2022, EFM collected groundwater samples from site monitoring wells
MW-7, MW-8, MW-9, MW-10, MW-11, and NES-2S. Monitoring well MW-7 serves as the
upgradient background well for the facility, and monitoring wells MW-8, MW-9, MW-10, MW-
11, and NES-2S serve as compliance monitoring wells. The groundwater samples were collected
and handled in accordance with the sampling protocols included in the site WQMP as well as the
DEQ SWS Guidelines for Groundwater, Soil, and Surface Water Sampling document.
Monitoring wells were purged utilizing a peristaltic pump under low flow (<200 milliliters/minute)
conditions. Water levels were recorded during the purging process to ensure the pump rate did not
cause significant drawdown of the water column, and samples were collected following
stabilization of field parameters over three consecutive readings. Field measurements of pH,
temperature, specific conductance, oxygen reduction potential (ORP), and dissolved oxygen (DO)
were measured using a YSI Pro Plus water quality meter. Turbidity was measured using a Hach
2100Q turbidity meter. A summary of the final field parameters recorded prior to sample
collection are presented in Table 3. Copies of groundwater sampling forms containing pertinent
information recorded in the field during purging and sampling at each monitoring well are
provided in Appendix A.
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The results of the field -measured water quality parameters indicate that the values measured in
groundwater collected from site monitoring wells were within applicable stabilization criteria.
Groundwater at the site is acidic based on the pH values measured in the field (5.49 to 7.39
Standard Units). Specific conductance values in site groundwater ranged from 173.6 (MW-11) to
395.6 (MW-7) microsiemens per centimeter (µS/cm). Turbidity values ranged from 1.21 (MW-8)
to 11.2 (MW-11) nephelometric turbidity units (NTUs).
2.3 Surface Water Sampling Methods
On February 15, 2022, EFM collected surface water samples from sample locations SW-3 and
SW-4 (Figure 2). Surface water samples were collected in general accordance with the WQMP
as well as the DEQ SWS Guidelines for Groundwater, Soil, and Surface Water Sampling
document. Field parameters were measured during sample collection and copies of surface water
sampling forms are provided in Appendix A. A summary of field parameters recorded prior to
sample collection is provided in Table 3.
2.4 Sample Equipment Management
All reusable sampling equipment (e.g., water level indicator) was properly decontaminated
between sampling locations with a non -phosphate soap and water wash, followed by multiple
rinses with distilled water. New disposable nitrile or latex gloves were worn during all sampling
activities. Disposable sampling equipment/material was discarded after each use.
2.5 Sample Handling and Laboratory Analyses
Upon sample collection, samples for laboratory analysis were placed directly into dedicated
laboratory -supplied sample bottles, labeled, and placed into ice -filled coolers. A chain -of -custody
record was completed and included sample description, analyses required, matrix, sample
container information, and date and time of sample collection. The samples were transported on
ice, under standard protocol, to Pace Analytical Services, Inc. (Pace) in Huntersville, North
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Carolina. Pace is a North Carolina -certified laboratory. The laboratory analytical reports and
chain -of -custody records for the February 2022 sampling event are included in Appendix B. A
summary of samples collected during the subject reporting period is provided below.
The groundwater samples from monitoring wells MW-7, MW-8, MW-9, MW-10, MW-11, and
NES-2S were analyzed for NC Appendix I constituents plus 1,4-dioxane. The surface water
samples from SW-1 and SW- 2 were analyzed for NC Appendix I constituents plus 1,4-dioxane.
s
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3.0 Water Quality Monitoring Results
Groundwater and surface water monitoring activities were conducted at the site on February 15
and 17, 2022. Groundwater and surface water samples were collected and analyzed in accordance
with the DEQ approved WQMP (March 2019). The monitoring results are discussed in the
following sections.
3.1 Groundwater Flow and Hydraulic Gradient
A summary of monitoring well gauging and water level elevation data is provided in Table 2.
Historical groundwater elevation data is provided in Appendix C. Groundwater flow direction,
average hydraulic gradient, and average interstitial flow velocity were derived from water -level
measurements recorded during the February 2022 sampling event. A potentiometric map
generated from the February 15, 2022 gauging event is provided as Figure 3. The February 2022
water levels are within the range of historical seasonal fluctuations observed at the site. Consistent
with historical trends, the overall direction of shallow groundwater flow at the site is generally to
the north to northwest towards an unnamed tributary to Little Grassy Creek.
The hydraulic gradient in the vicinity of each well was derived by dividing the elevation difference
between water table elevations measured at the monitoring wells and proximal potentiometric
contour lines, by the perpendicular horizontal distance between the wells and potentiometric
contours (Figure 3 and Table 4). The potentiometric contours indicate an average hydraulic
gradient of approximately 0.030 ft/ft. Results of in -situ slug testing reported by others (LaBella
Associates, 2021) indicate an average hydraulic conductivity value in the bedrock aquifer of
approximately 4.43 feet/day. Using the horizontal hydraulic gradient measurements, the
individual estimate of hydraulic conductivity, and an assumed effective porosity of 0.15 (LaBella
Associates, 2021), the range of average interstitial groundwater flow velocities for the shallow
bedrock aquifer was calculated using the following equation: VX = (K/ne) x dh/dl.
0
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Where:
VX = average interstitial groundwater flow velocity;
K = hydraulic conductivity;
ne = effective porosity; and,
dh/dl = horizontal hydraulic gradient
Average linear flow velocities are estimated to range between approximately 85 to 325 feet/year
(approximately 0.234 to 0.891 feet/day) with a geometric mean of approximately 143 feet/year
(0.391 feet/day). These values are consistent with prior monitoring events. Table 4 summarizes
the data used to calculate the average interstitial groundwater flow velocity in the vicinity of each
monitoring well.
3.2 Groundwater Analytical Results
Semiannual groundwater sampling consisted of collecting samples from six site monitoring wells.
A summary of groundwater constituent detections from the February 2022 sampling event is
provided in Table 5. Historical analytical results are presented in Appendix D. A summary of
groundwater results is provided below.
Organic Anal
The analytical results indicate no organic constituents were detected at concentrations above
laboratory method detection limits (MDLs).
Inorganic Analyses
The analytical results indicate metals arsenic (MW-7, MW-8, and MW-9), barium (MW-7, MW-
8, MW-9, MW-10, and MW-11), and copper (MW-8) were detected at concentrations above
MDLs in one or more wells during the February 2022 sampling event. The metal detections were
all below their respective North Carolina 2L Groundwater Standards (2L Standards), and
concentrations are consistent with historical detections at each location.
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3.3 Surface Water Analytical Results
Semiannual surface water sampling consisted of collecting samples from two locations, one
upstream (SW-3) and one downstream (SW-4) location. A summary of surface water constituent
detections from the February 2022 sampling event is provided in Table 5. Historical analytical
results are presented in Appendix E. A discussion of the results for the February 2022 sampling
event is provided below.
The analytical results indicate barium was detected above the laboratory MDL in the samples
collected from SW-3 and SW-4. The detected concentrations of barium are below its North
Carolina In -Stream Target Value for Surface Water (ISTV). No other constituents were detected
above MDLs during the February 2022 sampling event.
3.4 Quality Assurance/Quality Control Results
Quality assurance procedures and protocols for sampling activities were conducted in general
accordance with the DEQ approved WQMP. Quality assurance samples included the collection
of a trip blank and field blank sample. Samples were received by the lab in good condition and
met holding times and preservation requirements. Based upon a review of the data packages, no
significant quality assurance/quality control (QA/QC) issues were identified for the laboratory
analyses. In summary, the QA/QC results indicate that the data collected during the semiannual
monitoring event is suitable for its intended purpose.
Trip Blanks
Laboratory -filled trip blanks accompanied the sampling team during sampling and the transport of
VOC samples to the laboratory. The trip blank samples serve as a QC check on potential external
contamination and/or cross -contamination between VOC water samples during shipping and
storage. The trip blank sample was analyzed for Appendix I VOCs and 1,4-dioxane. The results
indicate no constituents were detected above laboratory MDLs.
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A field blank sample was collected in the field by exposing laboratory -supplied deionized water
to the sampling environment. The field blank is used to evaluate the potential for contamination
of a sample by site contaminants from a source not associated with the samples collected. The
field blank sample was analyzed for Appendix II constituents and 1,4-dioxane. The field blank
sample was non -detect with the exception of a low concentration of methylene chloride. However,
site samples collected during the sampling event did not indicate detectable concentrations of
methylene chloride. Methylene chloride is a common laboratory contaminant and the low
detection in the field blank sample may be a result of laboratory cleaning processes.
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4.0 Conclusions
The analytical results for groundwater and surface water samples collected during the February
2022 event indicate no constituents were detected at concentrations above standards. Based on the
water quality monitoring results, the Granville County Oxford Unit 2 Landfill will remain in the
Detection Monitoring Program. The next semiannual sampling event will be conducted in August
2022.
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Table 1
Summary of Well Construction Details
Granville County Oxford Unit 2 Landfill
Oxford, North Carolina
H&H Job No. GMI-005
Ground
TOC
Top of
Top
Bottom
Bottom
Auger
Total Depth
Total Depth
Screened
Well ID
Date Installed
Northing
Easting
Elevation
Elevation
(ft BGS)
(ft BTOC)
Screen
Screen
Screen
Screen
Refusal
Lithology
Comments
(ft AMSL)
(ft AMSL)
(ft BGS)
(Ft BTOC)
(Ft BGS)
(Ft BTOC)
(ft BGS)
MW-7
7/28/2008
953292.1160
2112043.44800
531.24
534.24
34.50
37.50
19.50
22.50
34.50
37.50
34.50
Saprolite
Background Well Units
1 & 2
MW-8
7/18/2012
953360.2000
2111527.6910
500.57
503.31
25.00
20.00
10.00
12.74
20.00
22.74
1.00
Bedrock
Unit 2 Compliance
MW-9
10/6/2008
954799.7410
2112842.3890
485.05
487.51
40.00
43.00
20.00
22.46
40.00
42.46
1.50
Bedrock
Unit 2 Compliance
MW-10
10/2/2008
955136.0000
2112571.1750
481.81
484.92
30.00
32.90
15.00
18.11
30.00
33.11
6.00
Bedrock
Unit 2 Compliance
MW-11
10/5/2008
954795.8510
2111957.0410
476.43
478.72
20.00
22.90
5.00
7.30
20.00
22.30
6.00
Bedrock
Unit 2 Compliance
MW-12
8/1/2008
954077.4350
2112567.4920
519.29
521.30
50.00
52.30
40.00
42.00
50.00
52.00
31.00
Bedrock
Not Sampled
NES-2S
5/1/2004
955091.2902
2111945.3411
474.53
477.20
21.50
24.17
11.00
13.67
21.00
23.67
9.00
Saprolite
Unit 2 Compliance &
1
Unit 1 Performance
Notes:
Well information obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event.
ft = feet; AMSL = above mean sea level; AGS = above ground surface
TOC = top of casing; BTOC = below top of casing; * = estimated value
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Table 1 (Page 1 of 1)
Hart & Hickman, PC

Table 2
Summary of Groundwater Elevations
Granville County Oxford Unit 2 Landfill
Oxford, North Carolina
H&H Job No. GMI-005
Well ID
Total Depth
(ft BTOC)
TOC Elevation
(ft AMSL)
February 15, 2022
Depth To Groundwater
(ft BTOC)
Groundwater Elevation
(ft AMSL)
MW-7
37.50
534.24
26.75
507.49
MW-8
22.74
503.31
3.21
500.10
MW-9
42.46
487.51
8.11
479.40
MW-10
33.11
484.92
8.74
476.18
MW-11
22.30
478.72
5.50
473.22
NES-2S
23.67
477.20
5.94
471.26
Notes:
Well information obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event.
TOC = top of casing; ft BTOC = feet below top of casing
ft AMSL= feet above mean sea level
Table 2 (Page 1 of 1)
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 First Half GWM/Tables/Oxford Unit 2 Tables.xlsx Hart & Hickman, Pl,/

Table 3
Summary of Field Parameters
Granville County Oxford Unit 2 Landfill
Oxford, North Carolina
H&H Job No. GMI-005
Sample ID
Sample Date
Field Parameter
Results
Units
Groundwater
MW-7
2/17/2022
Conductivity
395.6
PS/CM
Dissolved Oxygen
1.21
mg/I
Oxidation Reduction Potential
209.9
mV
pH
5.92
S.U.
Temperature
15.0
°C
Turbidity
2.09
NTU
MW-8
2/15/2022
Conductivity
264.7
PS/CM
Dissolved Oxygen
0.25
mg/I
Oxidation Reduction Potential
39.9
mV
pH
7.39
S.U.
Temperature
12.5
oC
Turbidity
1.21
NTU
MW-9
2/15/2022
Conductivity
374.1
PS/CM
Dissolved Oxygen
3.42
mg/I
Oxidation Reduction Potential
172.5
mV
pH
6.84
S.U.
Temperature
11.7
oC
Turbidity
1.84
NTU
MW-10
2/15/2022
Conductivity
352
PS/CM
Dissolved Oxygen
1.69
mg/I
Oxidation Reduction Potential
121.1
mV
pH
6.44
S.U.
Temperature
13.6
oC
Turbidity
7.4
NTU
MW-11
2/15/2022
Conductivity
173.6
PS/CM
Dissolved Oxygen
1.14
mg/I
Oxidation Reduction Potential
158.0
mV
pH
5.49
S.U.
Temperature
11.9
oC
Turbidity
11.2
NTU
NES-2S
2/17/2022
Conductivity
233.0
PS/CM
Dissolved Oxygen
0.08
mg/I
Oxidation Reduction Potential
131.1
mV
pH
5.90
S.U.
Temperature
14.5
oC
Turbidity
1.5
NTU
Table 3 (Page 1 of 2)
Hart & Hickman, PC
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 First Half GWM/Tables/Oxford Unit 2
Tables.xlsx

Table 3
Summary of Field Parameters
Granville County Oxford Unit 2 Landfill
Oxford, North Carolina
H&H Job No. GMI-005
Sample ID
Sample Date
Field Parameter
Results
Units
Surface Water
SW-3
2/15/2022
Conductivity
66.9
PS/cm
Dissolved Oxygen
9.46
mg/I
Oxidation Reduction Potential
144.2
mV
pH
6.88
S.U.
Temperature
6.0
oC
Turbidity
12.5
NTU
SW-4
2/15/2022
Conductivity
111
PS/cm
Dissolved Oxygen
9.38
mg/I
Oxidation Reduction Potential
147.4
mV
pH
7.00
S.U.
Temperature
7.1
oC
Turbidity
69.2
NTU
Notes:
S.U. = standard units; °C = degrees Celsius; pS/cm = microsiemens per centimeter
NTU = nephelometric turbidity unit; mg/L = milligrams per liter; mV = millivolts
ORP = oxidation reduction potential
Table 3 (Page 2 of 2)
Hart & Hickman, PC
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 First Half GWM/Tables/Oxford Unit 2
Tables.xlsx

Table 4
Summary of Groundwater Flow Velocity
Granville County Oxford Unit 2 Landfill
Oxford, North Carolina
H&H Job No. GMI-005
Well ID
Hydraulic
Conductivity(l)Elevation
(ft/day)
Groundwater
ft AMSL
( )
Reference
Elevation
(ft AMSL)
Delta
Elevation
(ft)
Map Length
(ft)
Hydraulic
Gradient (ft/ft)
Effective
(l)
Porosity
Groundwater
Flow Velocity
(ft/day)
Groundwater
Flow Velocity
(ft/year)
MW-7
4.43
507.49
500.00
7.49
248.30
0.030
0.15
0.891
325.17
MW-8
4.43
500.10
495.00
5.10
327.80
0.016
0.15
0.459
167.71
MW-9
4.43
479.40
475.00
4.40
521.55
0.008
0.15
0.249
90.94
MW-10
4.43
476.18
480.00
3.82
481.80
0.008
0.15
0.234
85.47
MW-11
4.43
473.22
470.00
3.22
188.32
0.017
0.15
0.505
184.32
NES-2S
4.43
471.26
475.00
3.74
370.62
0.010
0.15
0.298
108.78
Minimum
--
--
--
--
0.008
--
0.234
85.47
Maximum
--
--
--
--
0.030
--
0.891
325.17
Geometric Mean
--
--
--
--
0.013
--
0.391
142.85
Notes:
1) Hydraulic conductivity and porosity values from Labella Associates Water Quality Monitoring Report - February 2021 Event.
Hydraulic conductivity is based on the geometric mean of bedrock wells at the facility in 2019 and the effective porosity
value for fractured bedrock was estimated at 15%.
ft = feet; ft/day = feet per day; ft/year = feet per year
AMSL = feet above mean sea level; -- = not applicable
Vx = (K/ne) x dh/dl
Vx = groundwater flow velocity
K = hydraulic conductivity
ne = effective porosity
dh/dl = hydraulic gradient
Table 4 (Page 1 of 1)
Hart & Hickman, PC

Table 5
Summary of Constituent Detections (February 2022)
Granville County Oxford Unit 2 Landfill
Butner, North Carolina
H&H Job No. GMI-005
Well ID
Sample Date
Parameter
Result
(Ng/L)
Qualifier
Analytical Method
MDL
W/L)
MRL
W/L)
Standard
(Ng/L)
Source (+&2)
Groundwater
MW-7
02/17/22
Arsenic
5.9
J
EPA 6010D
4.7
10.0
10
NC 2L
Barium
3.8
J
EPA 6010D
3.5
5.0
700
NC 2L
MW-8
02/15/22
Arsenic
4.9
J
EPA 6010D
4.7
10.0
10
NC 2L
Barium
37.5
--
EPA 6010D
3.5
5.0
700
NC 2L
Copper
4.5
J
EPA 6010D
4.3
5.0
1000
NC 2L
MW-9
02/15/22
Arsenic
5.4
J
EPA 6010D
4.7
10.0
10
NC 2L
Barium
76.5
--
EPA 6010D
3.5
5.0
700
NC 2L
MW-10
02/15/22
Barium
37.5
--
EPA 6010D
1 3.5
5.0
1 700
1 NC 2L
MW-11
02/15/22
Barium
29.0
--
EPA 6010D
3.5
1 5.0
700
NC 2L
Surface Water
SW-3
02/15/22
Barium
16.6
--
EPA 6010D
3.5
5
21,000
ISTV
SW-4
02/15/22
Barium
29.7
--
EPA 6010D
3.5
5
21,000
ISTV
Notes:
1. NC 2L Standards are the Title 15A NCAC 02L .0202 Groundwater Standards dated April 1, 2022.
2. 15A NCAC 2B Water Quality Standards (213 Standards) for Surface Water (Class C Waters) not established; therefore, the
value shown is the North Carolina In -Stream Target Values for Surface Waters (ISTV; July 26, 2021)
pg/L = micrograms per liter; MDL = method detection limit; MRL = method reporting limit; -- = not applicable;
J = Estimated concentration above the MDL and below the MRL.
Table 5 (Page 1 of 1)
Hart & Hickman, PC

APPROXIMATE
LIMITS OF WASTE
UNIT 1
\'
J 4
S i ER i , 4. , .
""^^ERTY BOUNDARY
OXIMATE
LIIVII 13 OF WASTE
UNIT 2
nI
USGS The National Map: National Boundaries Dataset, 3DEP Elevation
\ Program, Geographic Names Information System, National Hydrography
Dataset, National Land Cover Database, National Structures Dataset, and
National Transportation Dataset; USGS Global Ecosystems; U.S. Census
Bureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S.
\ Department of State Humanitarian Information Unit; and NOAA National
Centers for Environmental Information, U.S. Coastal Relief Model. Data
refreshed August, 2021.
0 2,000 4,000
Niiii
SCALE IN FEET
U.S.G.S. QUADRANGLE MAP
BEREA, NORTH CAROLINA 2019
OXFORD, NORTH CAROLINA 2019
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)

4661,
el
IGO
_ woe ) \ �� . \ / �b ( �• I f \� , t \ {� J ' �° / 5ss o f /
508 ��` b
\ � `r� ,�\ Ir � � >r-- l�i-1, �JJ� \ \\ �3 11 �^ter'-�-�\ \ \ o EJ �� /� C\.i �• � i // r�� 1 `�`\\ \I
.°`
l '' b-O 417,Q ) (I \ \ \ .-• . \ . t� 1 ! 1 ! ) I I -i5BO
/ lAlmolmCi
mw-1
o�.
1
\\lea Z1 ��Jr /•~ :�,�ji' —� �1� I � /,`�/ .//�i/' �) � \� \� ��j 1 � I 1 I 1 `�,�,_%' � '�/,;
F
• 4°L �,J-e $.} •J . I �., o cv',J�. \ jar �` C +Y Vl \ \ I j I
ot
it le
M l \ Jam✓ �/� >`' \-� /�__�✓ S, /�, �\ \� +` I
2gIL
—
p,

MW-6R
(497.75)�
500
SOS
MW-2
(506.51)�
UNIT 1
P
515`
MI W-1Ae !�
510
NES-2S (471.26) MW-10
NES-2D (474.68) /(476.18)
J-2 ,
NIT 2
LEGEND
SITE PROPERTY BOUNDARY
— — — — —
APPROXIMATE LIMITS OF WASTE
SURFACE WATER FEATURE
GROUNDWATER MONITORING WELL
SURFACE WATER SAMPLE POINT
(498.23)
GROUNDWATER ELEVATION (FT MSL)
500
GROUNDWATER ELEVATION CONTOUR
(FT MSL)
APPROXIMATE GROUNDWATER FLOW
DIRECTION
UNNAMED TRIBUTARY
LITTLE GRASSY CREEV
NOTES:
1. APPROXIMATE LIMITS OF WASTE AND LOCATIONS OF
MW-9 ENVIRONMENTAL MONITORING POINTS OBTAINED FROM
(479.40) LABELLA GROUNDWATER MONITORING REPORTS.
i
2. AERIAL IMAGERY OBTAINED FROM NC ONEMAP, 2021.
9
APPROXIMATE
0 500 1,000
SCALE IN FEET
GROUNDWATER POTENTIOMETRIC MAP
(FEBRUARY 15, 2022)
low OXFORD LANDFILL
GRANVILLE COUNTY
OXFORD, NORTH CAROLINA
hart� hickman 3921Sunset Ridge Road, Suite 301
1, i� Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(0
�� ' �, _ • SMARTER ENVIRONMENTAL SOLUTIONS License # C-1269 / #C-245 Geology
3 DATE: 6-6-22 REVISION NO. 0
�, JOB NO. GMI-004 FIGURE NO. 3

Appendix A
Groundwater and Surface Water Sampling Records
14
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

WELL NO.: l —
GROUNDWATER SAMPLE
PERMIT NO.:
COLLECTION RECORD
?roject No.: Unit �
Client: Garrett and Moore
'roject Name: Oxford Landfill Permit#
39-01 Project Location: Granville County
►Veather Conditions:
cQ 61 Sampling Date:2/ 1-1 /2022
1. WATER LEVEL DATA (measured
a. Depth to LNAPL:
from to of inner well casing)
NA (ft) b. Depth to Water: 17 S (ft)
C. Depth to DNAPL:
e. LNAPL Thickness: (a-6)
NA (ft) d. Total Well Depth: -3 7, S -7 (ft)
NA (ft) f. DNAPL Thickness:' (c-d) NA (ft)
g. Length of Water Column:
16 0'$ (ft) (a-d)
h. Well Volume:
1 � 7 (gal) Conversion Factors
:. WELL PURGE DATA
a. Purge Method: P rist
(a x cf = h)
is/Subm um /Bailer(3 volume) Well I.D. Conv. Fact. (cf)
b. Field Testing Equipment:
YSI'PRO+; Hach 2100 1 0.041
C. Required Total Purge Volume
(1f x 2c) (gals.): �/,/ ® 0.163
d. Total Volume and Number
of Well Volumes Removed: 4 0.653
e. Begin Purge Time: t)c� (5
End Purge Time: ng 6 1.470
Lapse
Purge Temp
pH
Spec. Cond.
Eh/ORP
Diss O
TURB
Water
Lead
No.
Time
(min.)
Rate (deg. C)
(ml/min) (#10%0)
(0.1s..)
(t0.i)
(OAUS/cm)
(t10%)
(1.0mV)
(±10mv)
(0.1mg1L)
(t10%)
(LONTU)
(<IONTU)
Color
Odor
Level
(ft)
goo
lq,b
S..1
1
A
c
Al v
1�
a01D
tLO
7Qq'(
7L
`f
20
va
kslo
j(
3CC.)
_o
r�
i
. SAMPLE COLLECTION DATA Sampling Personnel:
Sampling Method(s) & Equip: (o mil'
Sample I.D. (Name, Date, Time):! ' M (7 �1
Sample Analytical Parameters/Method: AP I OCs
HACH s/n: 1 a ; YSI s/n: %4t 06 / '7
Fe+2= Aj k mg/1 CO2= f `1 mg/1
'ample Start Time: End SampleTime: 1 0
'OMMENTS:

WELL NO.: Mw-
GROUNDWATER SAMPLE
COLLECTION RECORD PERMIT NO.:
Project No.: Unit 21
Client: Garrett and Moore
Project Name: Oxford Landfill Pertnif#
39-01 Project Location: Granville County
Weather Conditions: .
u �' Sampling Date: 2/ S- %2022
1. WATER LEVEL DATA (measured
a. Depth to LNAPL:
friomtop of inner well casing)
NA (ft) b. Depth, to Water: 3, 1 (ft)
C. Depth to DNAPL:
NA (ft) d. Total Well Depth: a3:-1(ft)
e. LNAPL Thickness: (a-b�
NA (ft) f. DNAPL Thickness: (c-d) NA (ft)
g. Length of Water Column:
)z, j (ft) (a-d)
h. Well Volume: 3 ,'3
(gal) Conversion Factors
2. WELL PURGE DATA
(a x cf = h)
a. Purge Method: eris
ltic/Subm pump/Bailer(3 volume) well I.D. Conv. Fact. (ct)
b. Field Testing Equipmen :
( YSI PRO+; Hach 2100 1 0.041
C. Required Total Purge Volume
(1f x 2c) (gals.): '40 0.163
d. Total Volume and Number
of Well Volumes Removed: p(„4 4 0.653
e. Begin Purge Time: Q
End Purge Time: 6 1.470
Lapse
Purge
Temp
pHl
Spec. Cond.
Eh/ORP;Dis;s02
TURB
Water
Read
No.
Time
(min.)
Rate
(ml/min)
(deg. C)
(#10%)
(0.1s.u.)
(t0.)I)
(O.1uS/cm)
(#10%0)
(1.0mV)
(±10mv)
)
(1.ONTU)
(<IONTU)
Color
Odor
Level
(ft)
7h
X?a.a
S51
9,51
k3.�
MM
cq-
No
14
3a ._
5
a-k)
P-q
o
0
)-, [�
�t c�
�FB, n
o,a�
f 3
c.
n� b
)00
0.
.31
O I `1
I I)-)-
N©
3,,�37
�Lb0
4
3
��
`���(6,aS
1.5
kh)
1 j.�
i
l
3. SAMPLE COLLECTION DATA Sampling Personnel:o �-
Sampling Method(s) & Equip: ou1i dJ'O 1 —M k/
Sample I.D. (Name, Date, Time): l -h�-
Sample Analytical Parameters/Method: Cocs
HACH s/n: YSIs/n:
Fe+2= mg/1 CO2= mg/1
Sample Start Time: (Oy O End SampleTime: lop
COMMENTS:

i
WELL NO.:
GROUNDWATER SAMPLE
COLLECTION RECORD PERMIT No.:
Project No.: Unit 2 Client: Garrett and Moore "
Project Name: Oxford Landfill Permit# 39-01 Project Location: Granville County
Weather Conditions: 1 .i` � s Sampling Date: 2/ 5 /2022
1. WATER LEVEL DATA (measuxed om top of inner well casing)
a. Depth to LNAPL: NA (ft) b. Depth to Water: 19.11 00
C. Depth to DNAPL: j NA (ft) d. Total Well Depth: az ,9 (ft)
e. LNAPL Thickness: (a-d) NA (ft) f. DNAPL Thickness: (c-d) NA (ft)
g. Length of Water Column: (ft) (a-d)
h. Well Volume: (gal) Conversion Factors
2. WELL PURGE DATA (a x cf = h)
a. Purge Method: P ista tic/Subm pumpBailer(3 volume) Well I.D. Conv. Fact. (ct)
b. Field Testing EquipmeultYSI PRO+; Hach 2100 1 0.041
C. Required Total Purge Volume (1f x 2c) (gals.): / � 0.163
d. Total Volume and Number) of Well Volumes Removed: J� 4 0.653
e. Be in Purge Time: ` End Purge Time: 6 1.470
Lapse
Purge
Temp
pHl
Spec. Cond.
Eh/ORP
Diss 02
TURB
Water
Read
Time
Rate
(deg. C)
(0.1s.h.)
(0.1uS/cm)
(1.OmV)
(0.1mg/L)
(LONTU)
Color
Odor
Level
No.
(min.)
(ml/min)
(±10%)
(±0.1)
(±10%)
(±10mV)
(±10%)
(<10NTU)
-
00
h ..
36�, 5
F� ,2-
3
cQ�
,o
2--�
o
(0
6 IS1
� o
IS"
L
,
C-r
oo
3-IL I
IN,2-
LF1
1, G01
9�0
?-7q.o
3,47
1, 6 I
c'r
No
6.141
-7y.c
129,c
k-7
v
wo
1i
g'
-7 Lf,
l'�a.
a 2.-
L q
I,I
i
it
3. SAMPLE COLLECTION DAT Sampling Personnel:
Sampling Method(s) & Equip: yow ouj
Sample I.D. (Name, Date, Time):!;
Sample Analytical Parameters/Method: AP COCs'
HACH s/n: �' �� ; YSI s/n: r
Fe+2= m /l CO2= A/A mg/1
Sample Start Time: 3 c(o End SampleTime:
COMMENTS:

WELL NO.: /Y1 W "
GROUNDWATER SAMPLE
COLLECTION RECORD PERMIT NO.:
Project No.: Unit 21 Client: Garrett and Moore
Project Name: Oxford Landfill Permit# 39-01 Project Location: Granville County
Weather Conditions: SVy 1 a S Sampling Date: 2/ 1572022
1. WATER LEVEL DATA (measured from top of inner well casing)
a. Depth to LNAPL: NA (ft) b.. Depth to Water:
r-7 (ft)
C. Depth to DNAPL: NA (ft) d. Total Well Depth:
o- (ft)
e. LNAPL Thickness: (a-b',) NA (ft) f, DNAPL Thickness:
(c-d) NA (ft)
g. Length of Water Column: . l (ft) (a-d)
h. Well Volume: 3-6 (gal)
Conversion Factors
2. WELL PURGE DATA
Purge Method: Peristaltic Subm
(a x cf = h)
Well I.D. Conv. Fact.
a. pump/Bailer(3 volume)
(cf)
b. Field Testing Equipment: I YSI PRO+; Hach 21001"
1 0.041
✓
C. Required Total Purge Volume (1f x 2c) (gals.): ,rwz
� 0.163
d. Total Volume and Numberl,of Well Volumes Removed:
4 0.653
e. Be in Purge Time: /,A V`71 End Purge Time: I_? a-1
6 1.470
Lapse
Purge
Temp
pHJ
Spec. Cond.
Eh/ORP
Diss 02
TURB
Water
Read
Time
Rate
(deg. C)
(0.1s.u.)
(0.1uS/cm
(1.OmV)
(0.1mg/L)
(LONTU)
Color Odor
Level
No.
(min.)
(ml/min)
(t10%)
(t0.1)
(±10%)
(t1OmV)
(#10%)
(<10NTU)
(ft)
©0
la.
,k
8.
3
0
9 J
yy.j
JC4F4& a d
R '7
��.�..
p� C:✓
3��.�p
'.
rJ`,'
oet
!®
dD10
� r�
�.�.rj
I S-
'-:2 co
13_
116,9
ITE
L0
(�)-® o
..Jal'7
lVe 1
rJ
-7
.3 5
2 1D 0`
. 16
3 L
12-o -7
1 •
�
3�
i
i
3. SAMPLE COLLECTION DATA Sampling Personnel:
�j�' /,F�{
Sampling Method(s) & Equip: Lt7C41
Sample I.D. (Name, Date, Time): 1, .39 01---M 1.(./(.C).
Sample Analytical Parameters/Method: APP I WCs 1L4 !., Y—/�*0
HACH s/n: 09 1 �)-(DC- ; YSI s/n: iMq 0 -Z-Q �f
Fe+2= r✓ mg/l CO2= mg/1
Sample Start. Time: 1937 0 1 End SampleTime: f - 41,C>
COMMENTS:

i
WELL NO.: I
I
GROUNDWATER SAMPLE
COLLECTION RECORD PERMIT No.:
Project No.: Unit 2
Client; Garrett and Moore
Project Name: Oxford Landfill PermiI
# 39-01 Project Location: Granville Count
Weather Conditions: , f1
q'i 1y' `r Sampling Date: 2/ '" /2022
1. WATER LEVEL DATA (measured
fi om top of inner well casing)
a. Depth to LNAPL:
NA (ft) b. Depth to Water:"® (ft)
C. Depth to DNAPL:
NA (ft) d. Total Well Depth: `1(, & (ft)
e. LNAPL Thickness: (a-b)
NA (ft) f. DNAPL Thickness: (c-d) NA (ft)
g. Length of Water Column:
' ( I (ft) (a-d)
h. Well Volume:,
1 (gal) Conversion Factors
2. WELL PURGE DATA
(a x cf = h)
a. Purge Method: P ris
a is/Subm pump/Bailer(3 volume) Well I.D. Conv. Fact. (co
b. Field Testing Equipmen :
YSI PRO+; Hach 2100 1 0.041
C. Required Total Purge Volume
(1f x 2c) (gals.): 0 0.163
d. Total Volume and Number)
of Well Volumes Removed: 4 0.653
e. Begin Purge Time:
End Purge Time: 6 1.470
Lapse
Purge
Temp
p
Spec. Cond. Eh/ORP
Diss 02
TURB
Water
Read
Time
Rate
(deg. C)
(0.11)
(0.1uS/cm) (1.OmV)
(0.1mg/L)
(LONTU)
Color
Odor
Level
No.
(min.)
(ml/min)
(±10%)
(±O.i)
(±10%) (±10mV)
(±10%)
(<lONTU)
(ft)
I
s
(Q
02
f ). 2-
,
DO
7 (J-
o
5'G
w S
goo
Qa o
I qL
1,30
97G
a�vr-
og
I<
a
din
P. ()
, , 5
1 5-"-f
I
I f `
c-
AJ 0
S-4
6
P-0
ss
7s-��
� s=�
a-G
A/0
s
3V
OQ
i,
Sys
15-7,
. ��
;v
2ov
-11
(Sl0
f<I
i�
3. SAMPLE COLLECTION DATA Sampling Personnel:
Sampling Method(s) & Equip: '(Ow
Sample I.D. (Name, Date, Time):! �' I -- M W i a/ a 2
11
Sample Analytical Parameters/Method: PP 1 Cocs
HACH s/n; gVto 7-7 ; Ysl s/n:
Fe+2= mg/1 CO2= 4/6 mg/1
Sample Start Time: h� fs- End SampleTime:1� S �"
COMMENTS:

WELL NO.:N w.S -a
GROUNDWATER SAMPLE
PERMIT NO.: 3 cIl
COLLECTION RECORD
Project No.: Unit 21 Client: Garrett and Moore
Project Name: Oxford Landfill Permit# 39-01 Project Location: Granville Count
Weather Conditions: _-'V co-01 Sampling Date: 2/ 0 /2022-
1. WATER LEVEL DATA (me sued from top of inner well casing)
a. Depth to LNAPL: NA (ft) b. Depth to Water: (ft)
C. Depth to DNAPL: NA (ft) d. Total Well Depth: 2Y41 (ft)
e. LNAPL Thickness: (a-b) NA (ft) f. DNAPL Thickness: (c-d) NA (ft)
—It
g. Length of Water Column: (ft) (a-d)
h. Well Volume: (gal) Conversion Factors
2. WELL PURGE DATA (a x cf = h)
a. Purge Method: (Peristaltic altic ubm pump/Bailer(3 volume) we11LD. Conv. Fact. (cf)
b. Field Testing Equipment: 1 YSI PRO+; Hach 2100 1 0.041
C. Required Total Purge VoIn a (If x 2c) (gals.): AIA 2 0.163
d. Total Volume and Number of Well Volumes Removed: 4 0.653
e. Be in Purge Time: End Purge Time: p 6 1.470
Lapse
Purge
Temp
pH
Spec. Cond.
Eh/ORP
Diss 02
TURB
Water
Read
No.
Time
(min.)
Rate
(ml/min)
(deg. C)
(#10%)
(0.1sa�.)
(f0.)
(OJUS/cm)
(#10%)
(1.0mv)
(t10mv)
(Oamg/L)
(#10%)
(LONTU)
(<10NTU)
Color
Odor
Level
00
13.3
6.9,
2A?-3
t" 11
01
un
G,,00
a3s-
�'l�ao
r
4. �
i�C16AEa
1
---
r"
ki
5RI
2
to
I�,l
S'
��a
�sdFg
�'
0(
3
Is'
xoo-
f0
5:
;a4a
NO
011
A
f
Jam'
,
(A
5,b
I d3 1
G,1
Q. 13
rjo
W
S
)-5
"
r s
S 0
I dfflO
133,
0 0)
5,
✓
ra;
6 w
®
x o
0
(XI
b 05
1< !�
(
rid
61 06
!I
L I
3. SAMPLE COLLECTION DATA ampling Personnel: A 4V
Sampling Method(s) & Equip: 44W )U"!:
Sample I.D. (Name, Date, Time): 31 Q-1,rls) 5 (1 a s 1 K-0-911
Analytical Parameters/Method: APP C
Sample AnalyticOCs
/n:cy
HACH s . �� 6 ; YSI s/n: jr f oo�2�f %
Fe+2= mg/1 CO2= mg/I
Sample Start Time: (d End SampleTime: 1
COMMENTS:

i
WELL NO.: J
GROUNDWATER SAMPLE PERMIT NO.: /
COLLECTION RECORD
Project No.: LW 77
Project Name: Oxford Landfill Permit#
Weather Conditions:
1. WATER LEVEL DATA (measuAed
a. Depth to LNAPL:
C. Depth to DNAPL:
e. LNAPL Thickness: (a-b)
g. Length of Water Column:
h. Well Volume:
2. WELL PURGE DATA
a. Purge Method: Surface
b. Field Testing Equipment:
C. Required Total Purge Vol
d. Total Volume and Numbed
1 Client: Garrett and Moore
39-01 Project Location: Granville County
o " Sampling Date: 2/ 1 —/2022
from top of inner well casing)
NA (ft) b. Depth to Water: NA (ft)
1 NA (ft) d. Total Well Depth: NA (ft)
NA (ft) f. DNAPL Thickness: (c-d) NA (ft)
NA (ft) (a-d)
I A (gal) Conversion Factors
(a x cf = h)
Water well I.D. Conv. Fact: (cf)
YSI PRO+; Hach 2100Q 1 0.041
me (lf x 2c) (gals.): NA 2 0.163
of Well Volumes Removed: NA 4 0.653
Sw
Sample
Point
`
Temp
(deg. C)
(±10%)
pH
(0.1s
(±O.1)
u.)
Spec. Cond.
(0.1uS/cm)
(±10%)
Eh/ORP
(1.0mV)
(±10mV)
Diss 02
(0.1mg/L)
(±10%)
TURB
(LONTU)
(<10NTU)
Color
Odor
Sample ,
Time
nitl
qt9
sw-
?'J®f
to 41;
25 Z
(3(.
1.5. 3
�, �i
."�
C
Ol�rc'9
%
sw-
2-
310
C'9
-,g
11R, r
r0S ,
Ajer--
13 -7
Unit2
B01
sw-
31ol
I.
To
v
M
tql, q
C' 3 7
cR. Z
cipil
Afe
1 q
sw-
3
3101
1
ft,
11-s
.
Al v
r 3
I
i
3. SAMPLE COLLECTION DATA Sampling Personnel:
Sampling Method(s) & Equip: Grab
Sample Analytical Parameters'Method: APP I + 1,4-Dioxane
HACH s/n: ; YSI! s/n: 16000641
j
Sample Start Time: End SampleTime:
COMMENTS:

Appendix B
Laboratory Analytical Reports
14
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 16, 2022
Stefan Bray, PE
Garrett & Moore
1029 West South Street
Raleigh, NC 27603
RE: Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Dear Stefan Bray, PE:
Enclosed are the analytical results for sample(s) received by the laboratory on February 16, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 69

lacmnalyfica('
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
OXFORD COMPLIANCE UNITS 1 & 2
92588929
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92588929001
3901-TRIP BLANK 01
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92588929002
3901-SW1
EPA 601OD
RDT
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92588929003
3901-SW2
EPA 601OD
RDT
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92588929004
3901-SW4
EPA 601OD
RDT
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92588929005
3901-SW3
EPA 601OD
RDT
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92588929006
3901-MW8
EPA 601OD
RDT
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92588929007
3901-MW11
EPA 601OD
RDT
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92588929008
3901-MW10
EPA 601OD
RDT
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92588929009
3901-MW9
EPA 601OD
RDT
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92588929010
3901-MW2
EPA 601OD
RDT
16
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 7470A
DBB
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 120.1-1982
YEG
1
PASI-A
SM 2540C-2015
ZMC
1
PASI-A
EPA 9040C
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
SM 4500-CI-E-2011
MMB
1
PASI-A
92588929011
3901-MW3R
EPA 601OD
RDT
16
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 7470A
DBB
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 120.1-1982
YEG
1
PASI-A
SM 2540C-2015
ZMC
1
PASI-A
EPA 9040C
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
SM 4500-CI-E-2011
MMB
1
PASI-A
92588929012
3901-MW6R
EPA 601OD
RDT
16
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 7470A
DBB
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 120.1-1982
YEG
1
PASI-A
SM 2540C-2015
ZMC
1
PASI-A
EPA 9040C
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
SM 4500-CI-E-2011
MMB
1
PASI-A
92588929013
3901-FB01
EPA 601OD
RDT
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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leAnalyiical
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9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-TRIP BLANK 01
Lab ID: 92588929001 Collected:
02/15/22
00:00
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/18/22 09:18
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/18/22 09:18
107-13-1
Benzene
ND
ug/L
1.0
1
02/18/22 09:18
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/18/22 09:18
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/18/22 09:18
75-27-4
Bromoform
ND
ug/L
1.0
1
02/18/22 09:18
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/18/22 09:18
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
02/18/22 09:18
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/18/22 09:18
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/18/22 09:18
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/18/22 09:18
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/18/22 09:18
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/18/22 09:18
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/18/22 09:18
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/18/22 09:18
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/18/22 09:18
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/18/22 09:18
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/18/22 09:18
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 09:18
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 09:18
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/18/22 09:18
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/18/22 09:18
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/18/22 09:18
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:18
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:18
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:18
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:18
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:18
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:18
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/18/22 09:18
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/18/22 09:18
591-78-6
lodomethane
ND
ug/L
20.0
1
02/18/22 09:18
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/18/22 09:18
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/18/22 09:18
108-10-1
Styrene
ND
ug/L
1.0
1
02/18/22 09:18
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 09:18
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 09:18
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/18/22 09:18
127-18-4
Toluene
ND
ug/L
1.0
1
02/18/22 09:18
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/18/22 09:18
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/18/22 09:18
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/18/22 09:18
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/18/22 09:18
75-69-4 v2
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/18/22 09:18
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/18/22 09:18
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/18/22 09:18
75-01-4
REPORT OF LABORATORY ANALYSIS
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Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 69

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[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-TRIP BLANK 01
Parameters
Lab ID: 92588929001 Collected: 02/15/22 00:00
Results Units Report Limit DF
Received: 02/16/22 16:50 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
02/18/22 09:18
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100 %
70-130
1
02/18/22 09:18
460-00-4
1,2-Dichloroethane-d4 (S)
97 %
70-130
1
02/18/22 09:18
17060-07-0
Toluene-d8 (S)
102 %
70-130
1
02/18/22 09:18
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L
2.0
1
02/18/22 12:29
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91 %
70-130
1
02/18/22 12:29
17060-07-0
Toluene-d8 (S)
97 %
66-133
1
02/18/22 12:29
2037-26-5
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-SW1
Lab ID: 92588929002 Collected:
02/15/22
13:30
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
Antimony
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:28
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:28
7440-38-2
Barium
16.7
ug/L
5.0
1
03/01/2210:25
03/13/2219:28
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:28
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:28
7440-43-9
Chromium
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:28
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:28
7440-48-4
Copper
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:28
7440-50-8
Lead
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:28
7439-92-1
Nickel
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:28
7440-02-0
Selenium
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:28
7782-49-2
Silver
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:28
7440-22-4
Vanadium
6.1
ug/L
5.0
1
03/01/2210:25
03/13/2219:28
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:28
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method:
EPA 3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 04:10
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/18/22 09:36
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/18/22 09:36
107-13-1
Benzene
ND
ug/L
1.0
1
02/18/22 09:36
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/18/22 09:36
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/18/22 09:36
75-27-4
Bromoform
ND
ug/L
1.0
1
02/18/22 09:36
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/18/22 09:36
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
02/18/22 09:36
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/18/22 09:36
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/18/22 09:36
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/18/22 09:36
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/18/22 09:36
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/18/22 09:36
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/18/22 09:36
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/18/22 09:36
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/18/22 09:36
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/18/22 09:36
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/18/22 09:36
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 09:36
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 09:36
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/18/22 09:36
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/18/22 09:36
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/18/22 09:36
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:36
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-SW1 Lab ID: 92588929002 Collected: 02/15/22 13:30 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:36
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:36
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:36
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:36
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:36
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/18/22 09:36
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/18/22 09:36
591-78-6
lodomethane
ND
ug/L
20.0
1
02/18/22 09:36
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/18/22 09:36
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/18/22 09:36
108-10-1
Styrene
ND
ug/L
1.0
1
02/18/22 09:36
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 09:36
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 09:36
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/18/22 09:36
127-18-4
Toluene
ND
ug/L
1.0
1
02/18/22 09:36
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/18/22 09:36
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/18/22 09:36
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/18/22 09:36
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/18/22 09:36
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/18/22 09:36
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/18/22 09:36
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
02/18/22 09:36
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
02/18/22 09:36
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
02/18/22 09:36
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
02/18/22 09:36
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
02/18/22 09:36
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
02/18/22 13:08
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
93
%
70-130
1
02/18/22 13:08
17060-07-0
Toluene-d8 (S)
97
%
66-133
1
02/18/22 13:08
2037-26-5
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
IH
Page 8 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-SW2
Lab ID: 92588929003 Collected:
02/15/22
13:57
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
Antimony
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:42
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:42
7440-38-2
Barium
23.2
ug/L
5.0
1
03/01/2210:25
03/13/2219:42
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:42
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:42
7440-43-9
Chromium
3.7J
ug/L
5.0
1
03/01/2210:25
03/13/2219:42
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:42
7440-48-4
Copper
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:42
7440-50-8
Lead
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:42
7439-92-1
Nickel
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:42
7440-02-0
Selenium
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:42
7782-49-2
Silver
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:42
7440-22-4
Vanadium
9.9
ug/L
5.0
1
03/01/2210:25
03/13/2219:42
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:42
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method:
EPA 3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 04:30
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/18/22 09:54
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/18/22 09:54
107-13-1
Benzene
ND
ug/L
1.0
1
02/18/22 09:54
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/18/22 09:54
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/18/22 09:54
75-27-4
Bromoform
ND
ug/L
1.0
1
02/18/22 09:54
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/18/22 09:54
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
02/18/22 09:54
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/18/22 09:54
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/18/22 09:54
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/18/22 09:54
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/18/22 09:54
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/18/22 09:54
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/18/22 09:54
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/18/22 09:54
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/18/22 09:54
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/18/22 09:54
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/18/22 09:54
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 09:54
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 09:54
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/18/22 09:54
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/18/22 09:54
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/18/22 09:54
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:54
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-SW2 Lab ID: 92588929003 Collected: 02/15/22 13:57 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:54
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:54
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:54
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:54
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:54
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/18/22 09:54
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/18/22 09:54
591-78-6
lodomethane
ND
ug/L
20.0
1
02/18/22 09:54
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/18/22 09:54
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/18/22 09:54
108-10-1
Styrene
ND
ug/L
1.0
1
02/18/22 09:54
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 09:54
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 09:54
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/18/22 09:54
127-18-4
Toluene
ND
ug/L
1.0
1
02/18/22 09:54
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/18/22 09:54
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/18/22 09:54
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/18/22 09:54
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/18/22 09:54
75-69-4 v2
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/18/22 09:54
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/18/22 09:54
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/18/22 09:54
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
02/18/22 09:54
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
02/18/22 09:54
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
02/18/22 09:54
17060-07-0
Toluene-d8(S)
102
%
70-130
1
02/18/22 09:54
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
5.2
ug/L
2.0
1
02/18/22 13:27
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92
%
70-130
1
02/18/22 13:27
17060-07-0
Toluene-d8 (S)
98
%
66-133
1
02/18/22 13:27
2037-26-5
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-SW4
Lab ID: 92588929004 Collected:
02/15/22
14:14
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
Antimony
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:45
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:45
7440-38-2
Barium
29.7
ug/L
5.0
1
03/01/2210:25
03/13/2219:45
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:45
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:45
7440-43-9
Chromium
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:45
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:45
7440-48-4
Copper
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:45
7440-50-8
Lead
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:45
7439-92-1
Nickel
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:45
7440-02-0
Selenium
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:45
7782-49-2
Silver
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:45
7440-22-4
Vanadium
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:45
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:45
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method:
EPA 3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 04:34
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/18/22 10:12
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/18/22 10:12
107-13-1
Benzene
ND
ug/L
1.0
1
02/18/22 10:12
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/18/22 10:12
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/18/22 10:12
75-27-4
Bromoform
ND
ug/L
1.0
1
02/18/22 10:12
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/18/22 10:12
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
02/18/22 10:12
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/18/22 10:12
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/18/22 10:12
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/18/22 10:12
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/18/22 10:12
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/18/22 10:12
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/18/22 10:12
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/18/22 10:12
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/18/22 10:12
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/18/22 10:12
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/18/22 10:12
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 10:12
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 10:12
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/18/22 10:12
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/18/22 10:12
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/18/22 10:12
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/18/22 10:12
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-SW4 Lab ID: 92588929004 Collected: 02/15/22 14:14 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 10:12
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 10:12
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/18/22 10:12
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 10:12
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 10:12
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/18/22 10:12
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/18/22 10:12
591-78-6
lodomethane
ND
ug/L
20.0
1
02/18/22 10:12
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/18/22 10:12
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/18/22 10:12
108-10-1
Styrene
ND
ug/L
1.0
1
02/18/22 10:12
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 10:12
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 10:12
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/18/22 10:12
127-18-4
Toluene
ND
ug/L
1.0
1
02/18/22 10:12
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/18/22 10:12
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/18/22 10:12
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/18/22 10:12
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/18/22 10:12
75-69-4 v2
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/18/22 10:12
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/18/22 10:12
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/18/22 10:12
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
02/18/22 10:12
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
02/18/22 10:12
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
02/18/22 10:12
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
02/18/22 10:12
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
02/18/22 13:46
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
89
%
70-130
1
02/18/22 13:46
17060-07-0
Toluene-d8 (S)
97
%
66-133
1
02/18/22 13:46
2037-26-5
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-SW3
Lab ID: 92588929005 Collected:
02/15/22
14:34
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
Antimony
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:49
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:49
7440-38-2
Barium
16.6
ug/L
5.0
1
03/01/2210:25
03/13/2219:49
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:49
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:49
7440-43-9
Chromium
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:49
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:49
7440-48-4
Copper
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:49
7440-50-8
Lead
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:49
7439-92-1
Nickel
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:49
7440-02-0
Selenium
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:49
7782-49-2
Silver
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:49
7440-22-4
Vanadium
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:49
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:49
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method:
EPA 3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 04:38
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/18/22 10:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/18/22 10:30
107-13-1
Benzene
ND
ug/L
1.0
1
02/18/22 10:30
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/18/22 10:30
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/18/22 10:30
75-27-4
Bromoform
ND
ug/L
1.0
1
02/18/22 10:30
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/18/22 10:30
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
02/18/22 10:30
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/18/22 10:30
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/18/22 10:30
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/18/22 10:30
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/18/22 10:30
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/18/22 10:30
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/18/22 10:30
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/18/22 10:30
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/18/22 10:30
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/18/22 10:30
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/18/22 10:30
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 10:30
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 10:30
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/18/22 10:30
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/18/22 10:30
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/18/22 10:30
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/18/22 10:30
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-SW3 Lab ID: 92588929005 Collected: 02/15/22 14:34 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 10:30
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 10:30
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/18/22 10:30
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 10:30
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 10:30
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/18/22 10:30
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/18/22 10:30
591-78-6
lodomethane
ND
ug/L
20.0
1
02/18/22 10:30
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/18/22 10:30
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/18/22 10:30
108-10-1
Styrene
ND
ug/L
1.0
1
02/18/22 10:30
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 10:30
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 10:30
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/18/22 10:30
127-18-4
Toluene
ND
ug/L
1.0
1
02/18/22 10:30
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/18/22 10:30
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/18/22 10:30
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/18/22 10:30
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/18/22 10:30
75-69-4 v2
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/18/22 10:30
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/18/22 10:30
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/18/22 10:30
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
02/18/22 10:30
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
02/18/22 10:30
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
02/18/22 10:30
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
02/18/22 10:30
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
02/18/22 14:05
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91
%
70-130
1
02/18/22 14:05
17060-07-0
Toluene-d8 (S)
97
%
66-133
1
02/18/22 14:05
2037-26-5
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW8
Lab ID: 92588929006 Collected:
02/15/22
10:40
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
Antimony
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:52
7440-36-0
Arsenic
4.9J
ug/L
10.0
1
03/01/2210:25
03/13/2219:52
7440-38-2
Barium
37.5
ug/L
5.0
1
03/01/2210:25
03/13/2219:52
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:52
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:52
7440-43-9
Chromium
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:52
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:52
7440-48-4
Copper
4.5J
ug/L
5.0
1
03/01/2210:25
03/13/2219:52
7440-50-8
Lead
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:52
7439-92-1
Nickel
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:52
7440-02-0
Selenium
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:52
7782-49-2
Silver
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:52
7440-22-4
Vanadium
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:52
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:52
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method:
EPA 3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 04:42
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/18/22 10:48
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/18/22 10:48
107-13-1
Benzene
ND
ug/L
1.0
1
02/18/22 10:48
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/18/22 10:48
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/18/22 10:48
75-27-4
Bromoform
ND
ug/L
1.0
1
02/18/22 10:48
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/18/22 10:48
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
02/18/22 10:48
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/18/22 10:48
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/18/22 10:48
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/18/22 10:48
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/18/22 10:48
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/18/22 10:48
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/18/22 10:48
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/18/22 10:48
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/18/22 10:48
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/18/22 10:48
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/18/22 10:48
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 10:48
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 10:48
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/18/22 10:48
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/18/22 10:48
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/18/22 10:48
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/18/22 10:48
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW8 Lab ID: 92588929006 Collected: 02/15/22 10:40 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 10:48
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 10:48
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/18/22 10:48
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 10:48
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 10:48
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/18/22 10:48
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/18/22 10:48
591-78-6
lodomethane
ND
ug/L
20.0
1
02/18/22 10:48
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/18/22 10:48
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/18/22 10:48
108-10-1
Styrene
ND
ug/L
1.0
1
02/18/22 10:48
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 10:48
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 10:48
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/18/22 10:48
127-18-4
Toluene
ND
ug/L
1.0
1
02/18/22 10:48
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/18/22 10:48
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/18/22 10:48
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/18/22 10:48
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/18/22 10:48
75-69-4 v2
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/18/22 10:48
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/18/22 10:48
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/18/22 10:48
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
02/18/22 10:48
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
02/18/22 10:48
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
02/18/22 10:48
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
02/18/22 10:48
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
02/18/22 14:25
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
89
%
70-130
1
02/18/22 14:25
17060-07-0
Toluene-d8 (S)
97
%
66-133
1
02/18/22 14:25
2037-26-5
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW11
Lab ID: 92588929007 Collected:
02/15/22
11:45
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
Antimony
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:56
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:56
7440-38-2
Barium
29.0
ug/L
5.0
1
03/01/2210:25
03/13/2219:56
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:56
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/01/2210:25
03/13/2219:56
7440-43-9
Chromium
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:56
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:56
7440-48-4
Copper
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:56
7440-50-8
Lead
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:56
7439-92-1
Nickel
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:56
7440-02-0
Selenium
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:56
7782-49-2
Silver
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:56
7440-22-4
Vanadium
ND
ug/L
5.0
1
03/01/2210:25
03/13/2219:56
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/2210:25
03/13/2219:56
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method:
EPA 3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 04:46
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/18/22 11:06
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/18/22 11:06
107-13-1
Benzene
ND
ug/L
1.0
1
02/18/22 11:06
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/18/22 11:06
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/18/22 11:06
75-27-4
Bromoform
ND
ug/L
1.0
1
02/18/22 11:06
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/18/22 11:06
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
02/18/22 11:06
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/18/22 11:06
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/18/22 11:06
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/18/22 11:06
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/18/22 11:06
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/18/22 11:06
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/18/22 11:06
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/18/22 11:06
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/18/22 11:06
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/18/22 11:06
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/18/22 11:06
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 11:06
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 11:06
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/18/22 11:06
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/18/22 11:06
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/18/22 11:06
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/18/22 11:06
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW11 Lab ID: 92588929007 Collected: 02/15/22 11:45 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 11:06
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 11:06
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/18/22 11:06
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 11:06
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 11:06
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/18/22 11:06
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/18/22 11:06
591-78-6
lodomethane
ND
ug/L
20.0
1
02/18/22 11:06
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/18/22 11:06
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/18/22 11:06
108-10-1
Styrene
ND
ug/L
1.0
1
02/18/22 11:06
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 11:06
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 11:06
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/18/22 11:06
127-18-4
Toluene
ND
ug/L
1.0
1
02/18/22 11:06
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/18/22 11:06
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/18/22 11:06
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/18/22 11:06
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/18/22 11:06
75-69-4 v2
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/18/22 11:06
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/18/22 11:06
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/18/22 11:06
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
02/18/22 11:06
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
02/18/22 11:06
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
02/18/22 11:06
17060-07-0
Toluene-d8(S)
102
%
70-130
1
02/18/22 11:06
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
02/18/22 14:44
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91
%
70-130
1
02/18/22 14:44
17060-07-0
Toluene-d8 (S)
98
%
66-133
1
02/18/22 14:44
2037-26-5
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW10
Lab ID: 92588929008 Collected:
02/15/22
13:30
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
Antimony
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:50
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 20:50
7440-38-2
Barium
37.5
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:50
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/01/22 10:25
03/13/22 20:50
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/01/22 10:25
03/13/22 20:50
7440-43-9
Chromium
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:50
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:50
7440-48-4
Copper
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:50
7440-50-8
Lead
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:50
7439-92-1
Nickel
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:50
7440-02-0
Selenium
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 20:50
7782-49-2
Silver
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:50
7440-22-4
Vanadium
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:50
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 20:50
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method:
EPA 3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 04:58
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/18/22 11:25
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/18/22 11:25
107-13-1
Benzene
ND
ug/L
1.0
1
02/18/22 11:25
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/18/22 11:25
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/18/22 11:25
75-27-4
Bromoform
ND
ug/L
1.0
1
02/18/22 11:25
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/18/22 11:25
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
02/18/22 11:25
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/18/22 11:25
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/18/22 11:25
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/18/22 11:25
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/18/22 11:25
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/18/22 11:25
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/18/22 11:25
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/18/22 11:25
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/18/22 11:25
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/18/22 11:25
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/18/22 11:25
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 11:25
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 11:25
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/18/22 11:25
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/18/22 11:25
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/18/22 11:25
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/18/22 11:25
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW10 Lab ID: 92588929008 Collected: 02/15/22 13:30 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 11:25
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 11:25
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/18/22 11:25
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 11:25
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 11:25
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/18/22 11:25
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/18/22 11:25
591-78-6
lodomethane
ND
ug/L
20.0
1
02/18/22 11:25
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/18/22 11:25
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/18/22 11:25
108-10-1
Styrene
ND
ug/L
1.0
1
02/18/22 11:25
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 11:25
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 11:25
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/18/22 11:25
127-18-4
Toluene
ND
ug/L
1.0
1
02/18/22 11:25
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/18/22 11:25
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/18/22 11:25
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/18/22 11:25
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/18/22 11:25
75-69-4 v2
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/18/22 11:25
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/18/22 11:25
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/18/22 11:25
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
02/18/22 11:25
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
02/18/22 11:25
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
02/18/22 11:25
17060-07-0
Toluene-d8(S)
102
%
70-130
1
02/18/22 11:25
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
02/18/22 11:53
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
95
%
70-130
1
02/18/22 11:53
17060-07-0
Toluene-d8(S)
100
%
66-133
1
02/18/22 11:53
2037-26-5
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW9
Lab ID: 92588929009 Collected:
02/15/22
13:40
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
Antimony
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:54
7440-36-0
Arsenic
5AJ
ug/L
10.0
1
03/01/22 10:25
03/13/22 20:54
7440-38-2
Barium
76.5
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:54
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/01/22 10:25
03/13/22 20:54
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/01/22 10:25
03/13/22 20:54
7440-43-9
Chromium
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:54
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:54
7440-48-4
Copper
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:54
7440-50-8
Lead
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:54
7439-92-1
Nickel
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:54
7440-02-0
Selenium
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 20:54
7782-49-2
Silver
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:54
7440-22-4
Vanadium
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 20:54
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 20:54
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method:
EPA 3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 05:02
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/18/22 11:43
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/18/22 11:43
107-13-1
Benzene
ND
ug/L
1.0
1
02/18/22 11:43
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/18/22 11:43
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/18/22 11:43
75-27-4
Bromoform
ND
ug/L
1.0
1
02/18/22 11:43
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/18/22 11:43
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
02/18/22 11:43
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/18/22 11:43
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/18/22 11:43
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/18/22 11:43
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/18/22 11:43
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/18/22 11:43
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/18/22 11:43
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/18/22 11:43
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/18/22 11:43
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/18/22 11:43
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/18/22 11:43
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 11:43
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 11:43
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/18/22 11:43
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/18/22 11:43
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/18/22 11:43
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/18/22 11:43
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW9 Lab ID: 92588929009 Collected: 02/15/22 13:40 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 11:43
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 11:43
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/18/22 11:43
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 11:43
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 11:43
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/18/22 11:43
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/18/22 11:43
591-78-6
lodomethane
ND
ug/L
20.0
1
02/18/22 11:43
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/18/22 11:43
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/18/22 11:43
108-10-1
Styrene
ND
ug/L
1.0
1
02/18/22 11:43
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 11:43
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 11:43
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/18/22 11:43
127-18-4
Toluene
ND
ug/L
1.0
1
02/18/22 11:43
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/18/22 11:43
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/18/22 11:43
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/18/22 11:43
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/18/22 11:43
75-69-4 v2
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/18/22 11:43
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/18/22 11:43
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/18/22 11:43
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
02/18/22 11:43
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
02/18/22 11:43
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
02/18/22 11:43
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
02/18/22 11:43
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
02/18/22 12:12
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
02/18/22 12:12
17060-07-0
Toluene-d8 (S)
102
%
66-133
1
02/18/22 12:12
2037-26-5
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW2
Lab ID: 92588929010 Collected:
02/15/22
15:46
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 20:57
7440-36-0
Arsenic
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 20:57
7440-38-2
Barium
12.5 ug/L
5.0
1
03/01/22 10:25
03/13/22 20:57
7440-39-3
Beryllium
ND ug/L
1.0
1
03/01/22 10:25
03/13/22 20:57
7440-41-7
Cadmium
ND ug/L
1.0
1
03/01/22 10:25
03/13/22 20:57
7440-43-9
Chromium
4.OJ ug/L
5.0
1
03/01/22 10:25
03/13/22 20:57
7440-47-3
Cobalt
5.8 ug/L
5.0
1
03/01/22 10:25
03/13/22 20:57
7440-48-4
Copper
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 20:57
7440-50-8
Iron
5110 ug/L
50.0
1
03/01/22 10:25
03/13/22 20:57
7439-89-6
Lead
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 20:57
7439-92-1
Manganese
192 ug/L
5.0
1
03/01/22 10:25
03/13/22 20:57
7439-96-5
Nickel
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 20:57
7440-02-0
Selenium
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 20:57
7782-49-2
Silver
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 20:57
7440-22-4
Vanadium
12.5 ug/L
5.0
1
03/01/22 10:25
03/13/22 20:57
7440-62-2
Zinc
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 20:57
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND ug/L
0.47
1
02/25/22 12:06
02/28/22 05:06
7440-28-0
7470 Mercury
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical Services -Asheville
Mercury
ND ug/L
0.20
1
03/02/2211:15
03/03/2214:44
7439-97-6
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
02/18/22 12:01
67-64-1
Acrylonitrile
ND ug/L
10.0
1
02/18/22 12:01
107-13-1
Benzene
ND ug/L
1.0
1
02/18/22 12:01
71-43-2
Bromochloromethane
ND ug/L
1.0
1
02/18/22 12:01
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
02/18/22 12:01
75-27-4
Bromoform
ND ug/L
1.0
1
02/18/22 12:01
75-25-2
Bromomethane
ND ug/L
2.0
1
02/18/22 12:01
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
02/18/22 12:01
78-93-3
Carbon disulfide
ND ug/L
2.0
1
02/18/22 12:01
75-15-0
Carbon tetrachloride
ND ug/L
1.0
1
02/18/22 12:01
56-23-5
Chlorobenzene
ND ug/L
1.0
1
02/18/22 12:01
108-90-7
Chloroethane
ND ug/L
1.0
1
02/18/22 12:01
75-00-3 IK,v2
Chloroform
ND ug/L
1.0
1
02/18/22 12:01
67-66-3
Chloromethane
ND ug/L
1.0
1
02/18/22 12:01
74-87-3
1,2-Dibromo-3-chloropropane
ND ug/L
2.0
1
02/18/22 12:01
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
02/18/22 12:01
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
02/18/22 12:01
106-93-4
Dibromomethane
ND ug/L
1.0
1
02/18/22 12:01
74-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW2 Lab ID: 92588929010 Collected: 02/15/22 15:46 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
1,2-Dichlorobenzene
ND ug/L
1.0
1
02/18/22 12:01
95-50-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
02/18/22 12:01
106-46-7
trans-1,4-Dichloro-2-butene
ND ug/L
1.0
1
02/18/22 12:01
110-57-6
1,1-Dichloroethane
ND ug/L
1.0
1
02/18/22 12:01
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
02/18/22 12:01
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
02/18/22 12:01
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
02/18/22 12:01
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
02/18/22 12:01
156-60-5
1,2-Dichloropropene
ND ug/L
1.0
1
02/18/22 12:01
78-87-5
cis-1,3-Dichloropropene
ND ug/L
1.0
1
02/18/22 12:01
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
02/18/22 12:01
10061-02-6
Ethylbenzene
ND ug/L
1.0
1
02/18/22 12:01
100-41-4
2-Hexanone
ND ug/L
5.0
1
02/18/22 12:01
591-78-6
lodomethane
ND ug/L
20.0
1
02/18/22 12:01
74-88-4
Methylene Chloride
ND ug/L
5.0
1
02/18/22 12:01
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
02/18/22 12:01
108-10-1
Styrene
ND ug/L
1.0
1
02/18/22 12:01
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
02/18/22 12:01
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
02/18/22 12:01
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
02/18/22 12:01
127-18-4
Tetrahydrofuran
ND ug/L
10.0
1
02/18/22 12:01
109-99-9
Toluene
ND ug/L
1.0
1
02/18/22 12:01
108-88-3
1,1,1-Trichloroethane
ND ug/L
1.0
1
02/18/22 12:01
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
02/18/22 12:01
79-00-5
Trichloroethene
ND ug/L
1.0
1
02/18/22 12:01
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
02/18/22 12:01
75-69-4 v2
1,2,3-Trichloropropane
ND ug/L
1.0
1
02/18/22 12:01
96-18-4
Vinyl acetate
ND ug/L
2.0
1
02/18/22 12:01
108-05-4 IH
Vinyl chloride
ND ug/L
1.0
1
02/18/22 12:01
75-01-4
Xylene (Total)
ND ug/L
1.0
1
02/18/22 12:01
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100 %
70-130
1
02/18/22 12:01
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
02/18/22 12:01
17060-07-0
Toluene-d8 (S)
102 %
70-130
1
02/18/22 12:01
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L
2.0
1
02/18/22 15:03
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
93 %
70-130
1
02/18/22 15:03
17060-07-0
Toluene-d8 (S)
97 %
66-133
1
02/18/22 15:03
2037-26-5
120.1 Specific Conductance
Analytical Method: EPA 120.1-1982
Pace Analytical Services -Asheville
Specific Conductance
65.3 umhos/cm
10.0
1
02/23/22 11:33
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM
without the written consent of Pace Analytical Services, LLC.
Page 24 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW2
Lab ID: 92588929010 Collected: 02/15/22 15:46
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
117000 ug/L 25000
1
02/21/22 19:03
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.0 Std. Units 0.10
1
02/21/22 18:32 H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
8380 ug/L 1000
1
02/23/22 20:35 14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
3980 ug/L 1000
1
02/25/22 21:02 16887-00-6
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW3R
Lab ID: 92588929011 Collected:
02/15/22
14:27
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:01
7440-36-0
Arsenic
5AJ ug/L
10.0
1
03/01/22 10:25
03/13/22 21:01
7440-38-2
Barium
23.0 ug/L
5.0
1
03/01/22 10:25
03/13/22 21:01
7440-39-3
Beryllium
ND ug/L
1.0
1
03/01/22 10:25
03/13/22 21:01
7440-41-7
Cadmium
ND ug/L
1.0
1
03/01/22 10:25
03/13/22 21:01
7440-43-9
Chromium
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:01
7440-47-3
Cobalt
4.8J ug/L
5.0
1
03/01/22 10:25
03/13/22 21:01
7440-48-4
Copper
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:01
7440-50-8
Iron
351 ug/L
50.0
1
03/01/22 10:25
03/13/22 21:01
7439-89-6
Lead
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:01
7439-92-1
Manganese
1140 ug/L
5.0
1
03/01/22 10:25
03/13/22 21:01
7439-96-5
Nickel
7.3 ug/L
5.0
1
03/01/22 10:25
03/13/22 21:01
7440-02-0
Selenium
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 21:01
7782-49-2
Silver
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:01
7440-22-4
Vanadium
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:01
7440-62-2
Zinc
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 21:01
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND ug/L
0.47
1
02/25/22 12:06
02/28/22 05:10
7440-28-0
7470 Mercury
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical Services -Asheville
Mercury
ND ug/L
0.20
1
03/02/2211:15
03/03/2214:46
7439-97-6
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
02/18/22 12:19
67-64-1
Acrylonitrile
ND ug/L
10.0
1
02/18/22 12:19
107-13-1
Benzene
ND ug/L
1.0
1
02/18/22 12:19
71-43-2
Bromochloromethane
ND ug/L
1.0
1
02/18/22 12:19
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
02/18/22 12:19
75-27-4
Bromoform
ND ug/L
1.0
1
02/18/22 12:19
75-25-2
Bromomethane
ND ug/L
2.0
1
02/18/22 12:19
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
02/18/22 12:19
78-93-3
Carbon disulfide
ND ug/L
2.0
1
02/18/22 12:19
75-15-0
Carbon tetrachloride
ND ug/L
1.0
1
02/18/22 12:19
56-23-5
Chlorobenzene
ND ug/L
1.0
1
02/18/22 12:19
108-90-7
Chloroethane
ND ug/L
1.0
1
02/18/22 12:19
75-00-3 IK,v2
Chloroform
ND ug/L
1.0
1
02/18/22 12:19
67-66-3
Chloromethane
ND ug/L
1.0
1
02/18/22 12:19
74-87-3
1,2-Dibromo-3-chloropropane
ND ug/L
2.0
1
02/18/22 12:19
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
02/18/22 12:19
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
02/18/22 12:19
106-93-4
Dibromomethane
ND ug/L
1.0
1
02/18/22 12:19
74-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW3R Lab ID: 92588929011 Collected: 02/15/22 14:27 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
1,2-Dichlorobenzene
ND ug/L
1.0
1
02/18/22 12:19
95-50-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
02/18/22 12:19
106-46-7
trans-1,4-Dichloro-2-butene
ND ug/L
1.0
1
02/18/22 12:19
110-57-6
1,1-Dichloroethane
ND ug/L
1.0
1
02/18/22 12:19
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
02/18/22 12:19
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
02/18/22 12:19
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
02/18/22 12:19
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
02/18/22 12:19
156-60-5
1,2-Dichloropropene
ND ug/L
1.0
1
02/18/22 12:19
78-87-5
cis-1,3-Dichloropropene
ND ug/L
1.0
1
02/18/22 12:19
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
02/18/22 12:19
10061-02-6
Ethylbenzene
ND ug/L
1.0
1
02/18/22 12:19
100-41-4
2-Hexanone
ND ug/L
5.0
1
02/18/22 12:19
591-78-6
lodomethane
ND ug/L
20.0
1
02/18/22 12:19
74-88-4
Methylene Chloride
ND ug/L
5.0
1
02/18/22 12:19
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
02/18/22 12:19
108-10-1
Styrene
ND ug/L
1.0
1
02/18/22 12:19
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
02/18/22 12:19
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
02/18/22 12:19
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
02/18/22 12:19
127-18-4
Tetrahydrofuran
ND ug/L
10.0
1
02/18/22 12:19
109-99-9
Toluene
ND ug/L
1.0
1
02/18/22 12:19
108-88-3
1,1,1-Trichloroethane
ND ug/L
1.0
1
02/18/22 12:19
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
02/18/22 12:19
79-00-5
Trichloroethene
ND ug/L
1.0
1
02/18/22 12:19
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
02/18/22 12:19
75-69-4 v2
1,2,3-Trichloropropane
ND ug/L
1.0
1
02/18/22 12:19
96-18-4
Vinyl acetate
ND ug/L
2.0
1
02/18/22 12:19
108-05-4 IH
Vinyl chloride
ND ug/L
1.0
1
02/18/22 12:19
75-01-4
Xylene (Total)
ND ug/L
1.0
1
02/18/22 12:19
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100 %
70-130
1
02/18/22 12:19
460-00-4
1,2-Dichloroethane-d4 (S)
97 %
70-130
1
02/18/22 12:19
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
02/18/22 12:19
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
14.2 ug/L
2.0
1
02/18/22 15:22
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
95 %
70-130
1
02/18/22 15:22
17060-07-0
Toluene-d8 (S)
98 %
66-133
1
02/18/22 15:22
2037-26-5
120.1 Specific Conductance
Analytical Method: EPA 120.1-1982
Pace Analytical Services -Asheville
Specific Conductance
274 umhos/cm
10.0
1
02/23/22 11:35
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM
without the written consent of Pace Analytical Services, LLC.
Page 27 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW3R
Lab ID: 92588929011 Collected: 02/15/22 14:27
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
175000 ug/L 25000
1
02/21/22 19:03
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.7 Std. Units 0.10
1
02/21/22 18:27 H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
6760 ug/L 1000
1
02/23/22 20:50 14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
14600 ug/L 1000
1
02/25/22 21:03 16887-00-6
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 28 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW6R
Lab ID: 92588929012 Collected:
02/15/22
16:04
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:04
7440-36-0
Arsenic
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 21:04
7440-38-2
Barium
147 ug/L
5.0
1
03/01/22 10:25
03/13/22 21:04
7440-39-3
Beryllium
ND ug/L
1.0
1
03/01/22 10:25
03/13/22 21:04
7440-41-7
Cadmium
0.47J ug/L
1.0
1
03/01/22 10:25
03/13/22 21:04
7440-43-9
Chromium
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:04
7440-47-3
Cobalt
5.8 ug/L
5.0
1
03/01/22 10:25
03/13/22 21:04
7440-48-4
Copper
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:04
7440-50-8
Iron
6030 ug/L
50.0
1
03/01/22 10:25
03/13/22 21:04
7439-89-6
Lead
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:04
7439-92-1
Manganese
2390 ug/L
5.0
1
03/01/22 10:25
03/13/22 21:04
7439-96-5
Nickel
3.6J ug/L
5.0
1
03/01/22 10:25
03/13/22 21:04
7440-02-0
Selenium
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 21:04
7782-49-2
Silver
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:04
7440-22-4
Vanadium
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 21:04
7440-62-2
Zinc
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 21:04
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND ug/L
0.47
1
02/25/22 12:06
02/28/22 05:14
7440-28-0
7470 Mercury
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical Services -Asheville
Mercury
ND ug/L
0.20
1
03/02/2211:15
03/03/2214:53
7439-97-6
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
02/18/22 12:37
67-64-1
Acrylonitrile
ND ug/L
10.0
1
02/18/22 12:37
107-13-1
Benzene
ND ug/L
1.0
1
02/18/22 12:37
71-43-2
Bromochloromethane
ND ug/L
1.0
1
02/18/22 12:37
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
02/18/22 12:37
75-27-4
Bromoform
ND ug/L
1.0
1
02/18/22 12:37
75-25-2
Bromomethane
ND ug/L
2.0
1
02/18/22 12:37
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
02/18/22 12:37
78-93-3
Carbon disulfide
ND ug/L
2.0
1
02/18/22 12:37
75-15-0
Carbon tetrachloride
ND ug/L
1.0
1
02/18/22 12:37
56-23-5
Chlorobenzene
ND ug/L
1.0
1
02/18/22 12:37
108-90-7
Chloroethane
ND ug/L
1.0
1
02/18/22 12:37
75-00-3 IK,v2
Chloroform
ND ug/L
1.0
1
02/18/22 12:37
67-66-3
Chloromethane
ND ug/L
1.0
1
02/18/22 12:37
74-87-3
1,2-Dibromo-3-chloropropane
ND ug/L
2.0
1
02/18/22 12:37
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
02/18/22 12:37
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
02/18/22 12:37
106-93-4
Dibromomethane
ND ug/L
1.0
1
02/18/22 12:37
74-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW6R Lab ID: 92588929012 Collected: 02/15/22 16:04 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
1,2-Dichlorobenzene
ND ug/L
1.0
1
02/18/22 12:37
95-50-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
02/18/22 12:37
106-46-7
trans-1,4-Dichloro-2-butene
ND ug/L
1.0
1
02/18/22 12:37
110-57-6
1,1-Dichloroethane
1.4 ug/L
1.0
1
02/18/22 12:37
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
02/18/22 12:37
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
02/18/22 12:37
75-35-4
cis-1,2-Dichloroethene
0.82J ug/L
1.0
1
02/18/22 12:37
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
02/18/22 12:37
156-60-5
1,2-Dichloropropene
ND ug/L
1.0
1
02/18/22 12:37
78-87-5
cis-1,3-Dichloropropene
ND ug/L
1.0
1
02/18/22 12:37
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
02/18/22 12:37
10061-02-6
Ethylbenzene
ND ug/L
1.0
1
02/18/22 12:37
100-41-4
2-Hexanone
ND ug/L
5.0
1
02/18/22 12:37
591-78-6
lodomethane
ND ug/L
20.0
1
02/18/22 12:37
74-88-4
Methylene Chloride
ND ug/L
5.0
1
02/18/22 12:37
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
02/18/22 12:37
108-10-1
Styrene
ND ug/L
1.0
1
02/18/22 12:37
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
02/18/22 12:37
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
02/18/22 12:37
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
02/18/22 12:37
127-18-4
Tetrahydrofuran
ND ug/L
10.0
1
02/18/22 12:37
109-99-9
Toluene
ND ug/L
1.0
1
02/18/22 12:37
108-88-3
1,1,1-Trichloroethane
ND ug/L
1.0
1
02/18/22 12:37
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
02/18/22 12:37
79-00-5
Trichloroethene
ND ug/L
1.0
1
02/18/22 12:37
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
02/18/22 12:37
75-69-4 v2
1,2,3-Trichloropropane
ND ug/L
1.0
1
02/18/22 12:37
96-18-4
Vinyl acetate
ND ug/L
2.0
1
02/18/22 12:37
108-05-4 IH
Vinyl chloride
ND ug/L
1.0
1
02/18/22 12:37
75-01-4
Xylene (Total)
ND ug/L
1.0
1
02/18/22 12:37
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
1
02/18/22 12:37
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
02/18/22 12:37
17060-07-0
Toluene-d8 (S)
102 %
70-130
1
02/18/22 12:37
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
9.1 ug/L
2.0
1
02/18/22 11:34
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
106 %
70-130
1
02/18/22 11:34
17060-07-0
Toluene-d8(S)
102 %
66-133
1
02/18/22 11:34
2037-26-5
120.1 Specific Conductance
Analytical Method: EPA 120.1-1982
Pace Analytical Services -Asheville
Specific Conductance
1030 umhos/cm
10.0
1
02/23/22 11:37
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM
without the written consent of Pace Analytical Services, LLC.
Page 30 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-MW6R
Parameters
Lab ID: 92588929012 Collected: 02/15/22 16:04
Results Units Report Limit DF
Received: 02/16/22 16:50 Matrix: Water
Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
732000 ug/L 50000
1
02/21/22 19:03 1g
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
7.3 Std. Units 0.10
1
02/21/22 18:36 H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
6150 ug/L 1000
1
02/23/22 21:06 14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
147000 ug/L 5000
5
02/25/22 21:04 16887-00-6
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 69

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-FB01
Lab ID: 92588929013 Collected:
02/15/22
11:30
Received: 02/16/22 16:50 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
Antimony
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 21:08
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 21:08
7440-38-2
Barium
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 21:08
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/01/22 10:25
03/13/22 21:08
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/01/22 10:25
03/13/22 21:08
7440-43-9
Chromium
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 21:08
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 21:08
7440-48-4
Copper
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 21:08
7440-50-8
Lead
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 21:08
7439-92-1
Nickel
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 21:08
7440-02-0
Selenium
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 21:08
7782-49-2
Silver
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 21:08
7440-22-4
Vanadium
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 21:08
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 21:08
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method:
EPA 3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 05:18
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/18/22 09:00
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/18/22 09:00
107-13-1
Benzene
ND
ug/L
1.0
1
02/18/22 09:00
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/18/22 09:00
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/18/22 09:00
75-27-4
Bromoform
ND
ug/L
1.0
1
02/18/22 09:00
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/18/22 09:00
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
02/18/22 09:00
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/18/22 09:00
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/18/22 09:00
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/18/22 09:00
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/18/22 09:00
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/18/22 09:00
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/18/22 09:00
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/18/22 09:00
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/18/22 09:00
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/18/22 09:00
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/18/22 09:00
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 09:00
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/18/22 09:00
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/18/22 09:00
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/18/22 09:00
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/18/22 09:00
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:00
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 69

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Sample: 3901-FB01 Lab ID: 92588929013 Collected: 02/15/22 11:30 Received: 02/16/22 16:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:00
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/18/22 09:00
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:00
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:00
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/18/22 09:00
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/18/22 09:00
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/18/22 09:00
591-78-6
lodomethane
ND
ug/L
20.0
1
02/18/22 09:00
74-88-4
Methylene Chloride
4.1J
ug/L
5.0
1
02/18/22 09:00
75-09-2 C7
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/18/22 09:00
108-10-1
Styrene
ND
ug/L
1.0
1
02/18/22 09:00
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 09:00
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/18/22 09:00
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/18/22 09:00
127-18-4
Toluene
ND
ug/L
1.0
1
02/18/22 09:00
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/18/22 09:00
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/18/22 09:00
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/18/22 09:00
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/18/22 09:00
75-69-4 v2
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/18/22 09:00
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/18/22 09:00
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/18/22 09:00
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
02/18/22 09:00
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
02/18/22 09:00
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
02/18/22 09:00
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
02/18/22 09:00
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
02/18/22 12:49
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91
%
70-130
1
02/18/22 12:49
17060-07-0
Toluene-d8 (S)
97
%
66-133
1
02/18/22 12:49
2037-26-5
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 33 of 69

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
QC Batch: 681648 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92588929010, 92588929011, 92588929012
METHOD BLANK: 3565706
Matrix:
Water
Associated Lab Samples: 92588929010, 92588929011,
92588929012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
ug/L
ND
0.20
03/03/2214:07
LABORATORY CONTROL SAMPLE:
3565707
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
ug/L
2.5
2.5
101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3565708 3565709
MS MSD
92588471014 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.5 2.6 98 104 75-125 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC.
Page 34 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
QC Batch: 681460 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92588929002, 92588929003, 92588929004, 92588929005, 92588929006, 92588929007, 92588929008,
92588929009,92588929010,92588929011,92588929012,92588929013
METHOD BLANK: 3565071 Matrix: Water
Associated Lab Samples: 92588929002, 92588929003, 92588929004, 92588929005, 92588929006, 92588929007, 92588929008,
92588929009,92588929010,92588929011,92588929012,92588929013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony
ug/L
ND
5.0
03/13/2219:13
Arsenic
ug/L
ND
10.0
03/13/2219:13
Barium
ug/L
ND
5.0
03/13/2219:13
Beryllium
ug/L
ND
1.0
03/13/2219:13
Cadmium
ug/L
ND
1.0
03/13/2219:13
Chromium
ug/L
ND
5.0
03/13/2219:13
Cobalt
ug/L
ND
5.0
03/13/2219:13
Copper
ug/L
ND
5.0
03/13/2219:13
Iron
ug/L
ND
50.0
03/13/2219:13
Lead
ug/L
ND
5.0
03/13/2219:13
Manganese
ug/L
ND
5.0
03/13/2219:13
Nickel
ug/L
ND
5.0
03/13/2219:13
Selenium
ug/L
ND
10.0
03/13/2219:13
Silver
ug/L
ND
5.0
03/13/2219:13
Vanadium
ug/L
ND
5.0
03/13/2219:13
Zinc
ug/L
ND
10.0
03/13/2219:13
LABORATORY CONTROL SAMPLE:
Parameter
3565072
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
495
99
80-120
Arsenic
ug/L
500
492
98
80-120
Barium
ug/L
500
490
98
80-120
Beryllium
ug/L
500
507
101
80-120
Cadmium
ug/L
500
490
98
80-120
Chromium
ug/L
500
501
100
80-120
Cobalt
ug/L
500
485
97
80-120
Copper
ug/L
500
512
102
80-120
Iron
ug/L
5000
5090
102
80-120
Lead
ug/L
500
492
98
80-120
Manganese
ug/L
500
501
100
80-120
Nickel
ug/L
500
489
98
80-120
Selenium
ug/L
500
487
97
80-120
Silver
ug/L
250
246
99
80-120
Vanadium
ug/L
500
490
98
80-120
Zinc
ug/L
500
484
97
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 69

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
OXFORD COMPLIANCE UNITS 1 & 2
92588929
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3565073
3565074
MS
MSD
92588929002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
522
474
104
95
75-125
10
Arsenic
ug/L
ND
500
500
519
476
104
95
75-125
9
Barium
ug/L
16.7
500
500
523
478
101
92
75-125
9
Beryllium
ug/L
ND
500
500
531
488
106
98
75-125
8
Cadmium
ug/L
ND
500
500
513
466
102
93
75-125
10
Chromium
ug/L
ND
500
500
525
480
105
95
75-125
9
Cobalt
ug/L
ND
500
500
506
461
101
92
75-125
9
Copper
ug/L
ND
500
500
536
484
107
96
75-125
10
Iron
ug/L
3080
5000
5000
8880
8510
116
109
75-125
4
Lead
ug/L
ND
500
500
513
467
103
93
75-125
9
Manganese
ug/L
66.2
500
500
583
538
103
94
75-125
8
Nickel
ug/L
ND
500
500
511
464
102
92
75-125
10
Selenium
ug/L
ND
500
500
532
489
106
98
75-125
8
Silver
ug/L
ND
250
250
258
233
103
93
75-125
10
Vanadium
ug/L
6.1
500
500
518
470
102
93
75-125
10
Zinc
ug/L
ND
500
500
513
468
101
92
75-125
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 36 of 69

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
QC Batch: 680098 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92588929002, 92588929003, 92588929004, 92588929005, 92588929006, 92588929007, 92588929008,
92588929009,92588929010,92588929011,92588929012,92588929013
METHOD BLANK: 3558310 Matrix: Water
Associated Lab Samples: 92588929002, 92588929003, 92588929004, 92588929005, 92588929006, 92588929007, 92588929008,
92588929009,92588929010,92588929011,92588929012,92588929013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Thallium ug/L ND 0.47 02/28/22 03:54
LABORATORY CONTROL SAMPLE: 3558311
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 25 24.6 98 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3558312 3558313
MS MSD
92588929002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 25.0 25.1 100 100 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC.
Page 37 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
QC Batch: 679200 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92588929001, 92588929002, 92588929003, 92588929004, 92588929005, 92588929006, 92588929007,
92588929008,92588929009,92588929010,92588929011,92588929012,92588929013
METHOD BLANK: 3554181 Matrix: Water
Associated Lab Samples: 92588929001, 92588929002, 92588929003, 92588929004, 92588929005, 92588929006, 92588929007,
92588929008,92588929009,92588929010,92588929011,92588929012,92588929013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
02/18/22 08:41
1,1,1-Trichloroethane
ug/L
ND
1.0
02/18/22 08:41
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
02/18/22 08:41
1,1,2-Trichloroethane
ug/L
ND
1.0
02/18/22 08:41
1,1-Dichloroethane
ug/L
ND
1.0
02/18/22 08:41
1,1-Dichloroethene
ug/L
ND
1.0
02/18/22 08:41
1,2,3-Trichloropropane
ug/L
ND
1.0
02/18/22 08:41
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
02/18/22 08:41
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
02/18/22 08:41
1,2-Dichlorobenzene
ug/L
ND
1.0
02/18/22 08:41
1,2-Dichloroethane
ug/L
ND
1.0
02/18/22 08:41
1,2-Dichloropropane
ug/L
ND
1.0
02/18/22 08:41
1,4-Dichlorobenzene
ug/L
ND
1.0
02/18/22 08:41
2-Butanone (MEK)
ug/L
ND
5.0
02/18/22 08:41
2-Hexanone
ug/L
ND
5.0
02/18/22 08:41
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
02/18/22 08:41
Acetone
ug/L
ND
25.0
02/18/22 08:41
Acrylonitrile
ug/L
ND
10.0
02/18/22 08:41
Benzene
ug/L
ND
1.0
02/18/22 08:41
Bromochloromethane
ug/L
ND
1.0
02/18/22 08:41
Bromodichloromethane
ug/L
ND
1.0
02/18/22 08:41
Bromoform
ug/L
ND
1.0
02/18/22 08:41
Bromomethane
ug/L
ND
2.0
02/18/22 08:41
Carbon disulfide
ug/L
ND
2.0
02/18/22 08:41
Carbon tetrachloride
ug/L
ND
1.0
02/18/22 08:41
Chlorobenzene
ug/L
ND
1.0
02/18/22 08:41
Chloroethane
ug/L
ND
1.0
02/18/22 08:41 IK,v2
Chloroform
ug/L
ND
1.0
02/18/22 08:41
Chloromethane
ug/L
ND
1.0
02/18/22 08:41
cis-1,2-Dichloroethene
ug/L
ND
1.0
02/18/22 08:41
cis-1,3-Dichloropropene
ug/L
ND
1.0
02/18/22 08:41
Dibromochloromethane
ug/L
ND
1.0
02/18/22 08:41
Dibromomethane
ug/L
ND
1.0
02/18/22 08:41
Ethylbenzene
ug/L
ND
1.0
02/18/22 08:41
lodomethane
ug/L
ND
20.0
02/18/22 08:41
Methylene Chloride
ug/L
ND
5.0
02/18/22 08:41
Styrene
ug/L
ND
1.0
02/18/22 08:41
Tetrachloroethene
ug/L
ND
1.0
02/18/22 08:41
Tetrahydrofuran
ug/L
ND
10.0
02/18/22 08:41
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
METHOD BLANK: 3554181 Matrix: Water
Associated Lab Samples: 92588929001, 92588929002, 92588929003, 92588929004, 92588929005, 92588929006, 92588929007,
92588929008,92588929009,92588929010,92588929011,92588929012,92588929013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Toluene
ug/L
ND
1.0
02/18/22 08:41
trans-1,2-Dichloroethene
ug/L
ND
1.0
02/18/22 08:41
trans- 1,3-Dichloropropene
ug/L
ND
1.0
02/18/22 08:41
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
02/18/22 08:41
Trichloroethene
ug/L
ND
1.0
02/18/22 08:41
Trichlorofluoromethane
ug/L
ND
1.0
02/18/22 08:41 v2
Vinyl acetate
ug/L
ND
2.0
02/18/22 08:41 IK
Vinyl chloride
ug/L
ND
1.0
02/18/22 08:41
Xylene (Total)
ug/L
ND
1.0
02/18/22 08:41
1,2-Dichloroethane-d4 (S)
%
96
70-130
02/18/22 08:41
4-Bromofluorobenzene (S)
%
101
70-130
02/18/22 08:41
Toluene-d8 (S)
%
102
70-130
02/18/22 08:41
LABORATORY CONTROL SAMPLE: 3554182
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
47.6
95
70-130
1,1,1-Trichloroethane
ug/L
50
46.2
92
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.8
100
70-130
1,1,2-Trichloroethane
ug/L
50
48.4
97
70-130
1,1-Dichloroethane
ug/L
50
49.1
98
70-130
1,1-Dichloroethene
ug/L
50
52.1
104
70-132
1,2,3-Trichloropropane
ug/L
50
49.4
99
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
49.9
100
70-132
1,2-Dibromoethane (EDB)
ug/L
50
49.4
99
70-130
1,2-Dichlorobenzene
ug/L
50
47.5
95
70-130
1,2-Dichloroethane
ug/L
50
44.9
90
70-130
1,2-Dichloropropane
ug/L
50
48.2
96
70-130
1,4-Dichlorobenzene
ug/L
50
47.3
95
70-130
2-Butanone (MEK)
ug/L
100
97.7
98
70-133
2-Hexanone
ug/L
100
102
102
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
100
100
70-130
Acetone
ug/L
100
95.1
95
70-144
Acrylonitrile
ug/L
250
257
103
70-130
Benzene
ug/L
50
48.8
98
70-130
Bromochloromethane
ug/L
50
46.9
94
70-130
Bromodichloromethane
ug/L
50
44.8
90
70-130
Bromoform
ug/L
50
46.0
92
70-131
Bromomethane
ug/L
50
42.3
85
30-177
Carbon disulfide
ug/L
50
50.1
100
70-133
Carbon tetrachloride
ug/L
50
45.6
91
70-130
Chlorobenzene
ug/L
50
46.9
94
70-130
Chloroethane
ug/L
50
24.7
49
46-131 IK,v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 39 of 69

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
LABORATORY CONTROL SAMPLE:
Parameter
3554182
Units
Spike LCS
Conc. Result
Chloroform
ug/L
50
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
Methylene Chloride
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Tetrahydrofuran
ug/L
500
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits Qualifiers
46.1
92
70-130
45.6
91
49-130
48.6
97
70-130
49.9
100
70-130
48.0
96
70-130
44.4
89
70-130
48.0
96
70-130
93.1
93
47-140
48.6
97
68-130
51.5
103
70-130
45.7
91
70-130
523
105
70-130
47.3
95
70-130
50.1
100
70-130
48.8
98
70-130
49.1
98
25-200
46.2
92
70-130
38.2
76
61-130 v2
122
122
70-1401H
45.7
91
59-142
149
99
70-130
89
70-130
104
70-130
99
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3554183
MS
92588929009 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3554184
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
19.9
19.9
100
99
70-135
0
1,1,1-Trichloroethane
ug/L
ND
20
20
19.9
19.3
99
97
70-148
3
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.1
19.6
96
98
70-131
2
1,1,2-Trichloroethane
ug/L
ND
20
20
19.5
19.3
97
96
70-136
1
1,1-Dichloroethane
ug/L
ND
20
20
20.1
19.9
100
99
70-147
1
1,1-Dichloroethene
ug/L
ND
20
20
21.6
20.7
108
104
70-158
4
1,2,3-Trichloropropane
ug/L
ND
20
20
17.0
19.1
85
96
67-137
12
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
20.9
20.3
104
101
69-136
3
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
20.0
19.9
100
99
70-137
1
1,2-Dichlorobenzene
ug/L
ND
20
20
20.3
20.2
101
101
70-133
0
1,2-Dichloroethane
ug/L
ND
20
20
18.3
17.7
91
89
67-138
3
1,2-Dichloropropane
ug/L
ND
20
20
19.9
19.8
99
99
70-138
0
1,4-Dichlorobenzene
ug/L
ND
20
20
20.4
20.4
102
102
70-133
0
2-Butanone (MEK)
ug/L
ND
40
40
36.3
37.2
91
93
61-147
3
2-Hexanone
ug/L
ND
40
40
39.6
40.2
99
101
67-139
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
37.3
37.4
93
94
67-136
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC.
Page 40 of 69

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3554183
MS
92588929009 Spike
Parameter Units Result Conc.
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Ethylbenzene
lodomethane
Methylene Chloride
Styrene
Tetrachloroethene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethene
trans- 1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
40
100
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
20
200
20
20
20
20
20
20
40
20
60
MSD
Spike
Conc.
40
100
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
20
200
20
20
20
20
20
20
40
20
60
3554184
MS
Result
34.6
97.5
20.4
18.9
19.0
18.8
19.1
20.1
20.0
20.3
15.4
18.8
16.1
20.3
19.9
20.0
18.4
21.3
34.2
19.3
21.4
19.8
193
20.1
20.6
19.5
11.6
19.6
16.2
43.4
16.9
65.2
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
35.0
87
87
55-159
98.4
98
98
68-140
20.2
102
101
67-150
18.7
95
94
70-146
18.5
95
93
70-138
18.6
94
93
57-138
18.0
96
90
10-200
19.6
100
98
70-152
19.5
100
97
70-147
20.2
101
101
70-137
14.7
77
73
51-166
19.1
94
95
70-144
15.6
81
78
24-161
19.7
101
99
67-148
19.5
100
97
70-142
19.4
100
97
68-138
18.0
92
90
70-134
20.8
106
104
68-143
32.7
85
82
20-161
18.9
97
95
64-148
21.5
107
107
70-136
19.3
99
96
70-139
195
96
97
65-145
19.8
100
99
47-157
20.7
103
103
70-149
19.4
98
97
70-138
13.8
58
69
31-145
19.1
98
95
70-149
15.8
81
79
61-154
43.8
108
109
48-156
16.5
85
82
55-172
64.0
109
107
66-145
98
97
70-130
102
103
70-130
98
98
70-130
RPD Qual
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC.
1
1
1
1
2
1
6 v2
3
3
0
5 IK
1
3
3
2
3
2
2
4
2
0
3
1
1
0
1
17 v2
3
3
1 IH
3
2
Page 41 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
QC Batch: 679312 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92588929001, 92588929002, 92588929003, 92588929004, 92588929005, 92588929006, 92588929007,
92588929010,92588929011,92588929013
METHOD BLANK: 3554438 Matrix:
Water
Associated Lab Samples:
92588929001, 92588929002, 92588929003, 92588929004, 92588929005,
92588929006, 92588929007,
92588929010,92588929011,92588929013
Blank
Reporting
Parameter
Units Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L ND
2.0
02/18/22 11:12
1,2-Dichloroethane-d4 (S)
% 88
70-130
02/18/22 11:12
Toluene-d8 (S)
% 95
66-133
02/18/22 11:12
LABORATORY CONTROL SAMPLE: 3554439
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 19.1 95 70-130
1,2-Dichloroethane-d4 (S) % 88 70-130
Toluene-d8(S) % 94 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3554440
3554441
MS
MSD
92588929002 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 19.2
18.4 96
92
64-141 4
1,2-Dichloroethane-d4 (S)
%
92
91
70-130
Toluene-d8(S)
%
97
97
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 42 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
QC Batch: 679313 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92588929008, 92588929009, 92588929012
METHOD BLANK: 3554442
Matrix:
Water
Associated Lab Samples:
92588929008, 92588929009, 92588929012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
02/18/22 11:15
1,2-Dichloroethane-d4 (S)
%
99
70-130
02/18/22 11:15
Toluene-d8 (S)
%
101
66-133
02/18/22 11:15
LABORATORY CONTROL SAMPLE: 3554443
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 18.9 95 70-130
1,2-Dichloroethane-d4 (S) % 98 70-130
Toluene-d8 (S) % 100 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3554444
3554445
MS
MSD
92588929012 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 9.1 20
20 27.5
27.6 92
93
64-141 0
1,2-Dichloroethane-d4 (S)
%
111
105
70-130
Toluene-d8(S)
%
108
106
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 43 of 69

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
QC Batch: 680112 Analysis Method: EPA 120.1-1982
QC Batch Method: EPA 120.1-1982 Analysis Description: 120.1 Specific Conductance
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92588929010, 92588929011, 92588929012
METHOD BLANK: 3558377 Matrix: Water
Associated Lab Samples: 92588929010, 92588929011, 92588929012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Specific Conductance umhos/cm ND 10.0 02/23/22 11:16
LABORATORY CONTROL SAMPLE: 3558378
Spike LCS
Parameter Units Conc. Result
Specific Conductance umhos/cm 1410 1410
SAMPLE DUPLICATE: 3558379
92588085001 Dup
Parameter Units Result Result
Specific Conductance umhos/cm ND ND
SAMPLE DUPLICATE: 3558380
92589173003 Dup
Parameter Units Result Result
Specific Conductance umhos/cm 503 503
LCS % Rec
% Rec Limits Qualifiers
100 90-110
RPD Qualifiers
RPD Qualifiers
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 69

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
QC Batch: 679275 Analysis Method: SM 2540C-2015
QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92588929010, 92588929011, 92588929012
METHOD BLANK: 3557224
Matrix:
Water
Associated Lab Samples: 92588929010, 92588929011,
92588929012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Dissolved Solids
ug/L
ND
25000
02/21/22 19:02
LABORATORY CONTROL SAMPLE:
3554364
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Dissolved Solids
ug/L
251000
256000
102 90-110
SAMPLE DUPLICATE: 3554365
92588929010 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids ug/L 117000 113000 3
SAMPLE DUPLICATE: 3554366
92588691005 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids ug/L 260 mg/L 279000 7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 69

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
QC Batch: 679776 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92588929010, 92588929011, 92588929012
SAMPLE DUPLICATE: 3556711
92588244001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.9 6.8 0 H3
SAMPLE DUPLICATE: 3556712
92589141005 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.6 6.7 1 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC.
Page 46 of 69

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
QC Batch: 680314 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92588929010, 92588929011, 92588929012
METHOD BLANK: 3559188
Matrix:
Water
Associated Lab Samples: 92588929010, 92588929011,
92588929012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Sulfate
ug/L
ND
1000
02/23/2219:17
LABORATORY CONTROL SAMPLE:
3559189
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Sulfate
ug/L
50000
47100
94 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3559190 3559191
MS MSD
92589265001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate ug/L 3.9 50000 50000 54000 54700 100 102 90-110 1
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3559192 3559193
MS MSD
92588691003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate ug/L 78.5 50000 50000 122000 123000 87 90 90-110 1 M1
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC.
Page 47 of 69

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
QC Batch: 681054 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92588929010, 92588929011, 92588929012
METHOD BLANK: 3563226
Matrix:
Water
Associated Lab Samples: 92588929010, 92588929011,
92588929012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chloride
ug/L
ND
1000
02/25/22 20:50
LABORATORY CONTROL SAMPLE:
3563227
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Chloride
ug/L
20000
19900
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3563228 3563229
MS MSD
92588521001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride ug/L 132 10000 10000 140000 141000 76 92 90-110 1 M1
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3563230 3563231
MS MSD
92588589002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride ug/L 3280 10000 10000 3140000 3530000 -1420 2490 90-110 12 M1,R1
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC.
Page 48 of 69

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
1g Constant weight could not be achieved for this sample after 3 drying cycles. The final weight change was 0.0012g.
C7 Analyte is a possible laboratory contaminant (not present in method blank).
H3 Sample was received or analysis requested beyond the recognized method holding time.
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 49 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92588929002
3901-SW1
EPA 3010A
681460
EPA 6010D
681667
92588929003
3901-SW2
EPA 3010A
681460
EPA 6010D
681667
92588929004
3901-SW4
EPA 3010A
681460
EPA 6010D
681667
92588929005
3901-SW3
EPA 3010A
681460
EPA 6010D
681667
92588929006
3901-MW8
EPA 3010A
681460
EPA 6010D
681667
92588929007
3901-MW11
EPA 3010A
681460
EPA 6010D
681667
92588929008
3901-MW10
EPA 3010A
681460
EPA 6010D
681667
92588929009
3901-MW9
EPA 3010A
681460
EPA 6010D
681667
92588929010
3901-MW2
EPA 3010A
681460
EPA 6010D
681667
92588929011
3901-MW3R
EPA 3010A
681460
EPA 6010D
681667
92588929012
3901-MW6R
EPA 3010A
681460
EPA 6010D
681667
92588929013
3901-FB01
EPA 3010A
681460
EPA 6010D
681667
92588929002
3901-SW1
EPA 3010A
680098
EPA 6020B
681086
92588929003
3901-SW2
EPA 3010A
680098
EPA 6020B
681086
92588929004
3901-SW4
EPA 3010A
680098
EPA 6020B
681086
92588929005
3901-SW3
EPA 3010A
680098
EPA 6020B
681086
92588929006
3901-MW8
EPA 3010A
680098
EPA 6020B
681086
92588929007
3901-MW11
EPA 3010A
680098
EPA 6020B
681086
92588929008
3901-MW10
EPA 3010A
680098
EPA 6020B
681086
92588929009
3901-MW9
EPA 3010A
680098
EPA 6020B
681086
92588929010
3901-MW2
EPA 3010A
680098
EPA 6020B
681086
92588929011
3901-MW3R
EPA 3010A
680098
EPA 6020B
681086
92588929012
3901-MW6R
EPA 3010A
680098
EPA 6020B
681086
92588929013
3901-FB01
EPA 3010A
680098
EPA 6020B
681086
92588929010
3901-MW2
EPA 7470A
681648
EPA 7470A
682130
92588929011
3901-MW3R
EPA 7470A
681648
EPA 7470A
682130
92588929012
3901-MW6R
EPA 7470A
681648
EPA 7470A
682130
92588929001
3901-TRIP BLANK 01
EPA 8260D
679200
92588929002
3901-SW1
EPA 8260D
679200
92588929003
3901-SW2
EPA 8260D
679200
92588929004
3901-SW4
EPA 8260D
679200
92588929005
3901-SW3
EPA 8260D
679200
92588929006
3901-MW8
EPA 8260D
679200
92588929007
3901-MW11
EPA 8260D
679200
92588929008
3901-MW10
EPA 8260D
679200
92588929009
3901-MW9
EPA 8260D
679200
92588929010
3901-MW2
EPA 8260D
679200
92588929011
3901-MW3R
EPA 8260D
679200
92588929012
3901-MW6R
EPA 8260D
679200
92588929013
3901-FB01
EPA 8260D
679200
92588929001
3901-TRIP BLANK 01
EPA 8260D Mod.
679312
92588929002
3901-SW1
EPA 8260D Mod.
679312
92588929003
3901-SW2
EPA 8260D Mod.
679312
92588929004
3901-SW4
EPA 8260D Mod.
679312
92588929005
3901-SW3
EPA 8260D Mod.
679312
92588929006
3901-MW8
EPA 8260D Mod.
679312
92588929007
3901-MW11
EPA 8260D Mod.
679312
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/16/2022 11:09 AM without the written consent of Pace Analytical Services, LLC. Page 50 of 69

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: OXFORD COMPLIANCE UNITS 1 & 2
Pace Project No.: 92588929
Lab ID
Sample ID
QC Batch Method
QC Batch
92588929008
3901-MW10
EPA8260D Mod.
679313
92588929009
3901-MW9
EPA8260D Mod.
679313
92588929010
3901-MW2
EPA8260D Mod.
679312
92588929011
3901-MW3R
EPA8260D Mod.
679312
92588929012
3901-MW6R
EPA8260D Mod.
679313
92588929013
3901-FB01
EPA 8260D Mod.
679312
92588929010
3901-MW2
EPA 120.1-1982
680112
92588929011
3901-MW3R
EPA 120.1-1982
680112
92588929012
3901-MW6R
EPA 120.1-1982
680112
92588929010
3901-MW2
SM 2540C-2015
679275
92588929011
3901-MW3R
SM 2540C-2015
679275
92588929012
3901-MW6R
SM 2540C-2015
679275
92588929010
3901-MW2
EPA 9040C
679776
92588929011
3901-MW3R
EPA 9040C
679776
92588929012
3901-MW6R
EPA 9040C
679776
92588929010
3901-MW2
EPA 300.0 Rev 2.1 1993
680314
92588929011
3901-MW3R
EPA 300.0 Rev 2.1 1993
680314
92588929012
3901-MW6R
EPA 300.0 Rev 2.1 1993
680314
92588929010
3901-MW2
SM 4500-CI-E-2011
681054
92588929011
3901-MW3R
SM 4500-CI-E-2011
681054
92588929012
3901-MW6R
SM 4500-CI-E-2011
681054
Date: 03/16/2022 11:09 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 51 of 69

Document Name; Document Revised: November 15, 2021
i Sample Condition Upon Receipt (SOUR) Page 1 of 2
i�(1a><ICdt+ Document No,; Issuing Authority:
F•CAR-CS-033-Rev.08 Pace Carolinas Oualitv Offira
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville [D.' Ralelgh❑ Mechanicsville❑ Atlanta[] Kernersville❑
Sample Upon Receipt ConditionClient Name: Project #i: WQ# ■ 92588929
Courier: ❑Fed Ex ❑UPS
❑ ❑LISPS Client
❑lI�II� 11 11111111111111
Commercial ❑Face Other:
925$$929
Custody Seal Present? Dyes �fo Seals Intact? ❑Yes
Date/Initlals Persan Examining Contents: Z r r 7` Cf2��q n
Packing Material: ❑Bubble Wrap �bble Bags ❑None [I Other Biological Tissue row? f�T1{f '
Thermometer -
Gun ID:
OrNet
[]Blue❑None
❑Yes ❑Na N/A
-U-TO-0
Type of
Ice:
Correction Factor:
Cooler Temp: Add/Subtract (°C)
Temp should be above freezing to 6°C
-Cooler-Temp-Corrected-('Cl-
❑5amples out of temp Criteria. Samples on ice, cooling process
USDA Regulated Soil (O�N/A, water sample)
as
Did samples originate in a quarantine zone within the United
[]Yes No
States: CA, NY, or
SC (check
maps)?
Did samples originate from a foreign source {internationally,
includingHawali and Puerto Rica)? ❑yes ❑No
Comments/Discrepancy,
Chain of Custody Present?
Dyes
QN0
N/A
1.
Samples Arrived within Hold Time?
❑ es
[]No
❑N/A
2.
Short Hold Time Analysis (c72 hr.)?
❑Yes
ao
N/A
3.
Rush Turn Around Time Requested)
❑yes
[X.-
N/A
a,
Sufficient Volume?
2fts
MNo
ONJA
S.
Correct Containers Used?
CrYes
❑No
❑N/A
6.
-Pace Containers Used?
es
❑No
❑NIA
Containers Intact?
[des
ONO
N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑Na
jTNN/A
8.
Sample Labels Match COC?
Ids
❑No
©N/A
9.
iteadspace in VOA Vials (>S•6mm)? Dyes [?No ❑N/A 10,
Trip Blank Present? ❑No ❑N/AI-
Qfes11,
Trip Blank Custody Seals Present? res ❑No ❑N/A
COMMENTS/SAMPLE DISCREPANCY - Field Data Required? ❑Yes []No
CLIENT NOTIFICATION/RESOLUTION Lot ID of split containers:
Project Manager SCURF Review:
Project Manager SRF Review:
Date:
Date:
Page 52 of 69

Document Name:
d Sample Condition Upon Recell
Analytical Document No.:
F-CAR•CS•033•Rev.08
*Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
Document Revised, November 15, 2021
Page 2 of 2
Issuing Authority:
Pace Carolinas Oualitv Office+
Project It WO# : 92!588929
samples. i
Exceptions: VOA, Coiiform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg [�-Y
`*Bottom half of box is to list number of bottles N
PM: AIIB Due Date: 03/02/22
CLIEN'r : 92-Garrett
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Hate preservation adjusted
Time preservation
Amount of Preservative
Lot A
adjusted
added
Note; Whenever there is a discrepancy alletTn
Cut of hold, incorrect preservative, out of temp, incorrect containers.
Page 53 of 69

Document Name:
Document Issued: November 15, 2021
m
Analytical
Bottle Identification Form (BIF)
Page 1 of 1
Document No.:
Issuing Authority:
F-CAR-CS-043-Rev.01
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
EKeeptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Project 1# WO# + 92588929
—7 PM: AMB Due Dale: 03/02/22
POj !r CLIIEN'r: 92-Garrett
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Page 54 of 69

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(YIN)
Page 55 of 69

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
March 3, 2022
Angela Baioni
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: Oxford Compliance Units 1 &2
Client Job Number:
Project Number: 92588929
Laboratory Work Order Number: 22C0019
Enclosed are results of analyses for samples as received by the laboratory on March 1, 2022. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Raymond J. McCarthy
Project Manager
�rr�.� =sr t•

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
22CO019-01
22CO019-02
22CO019-03
Sample Preparation Information
QC Data
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
B302218
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
5
5
6
7
8
9
9
9
10
11
12

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100 REPORT DATE: 3/3/2022
Huntersville, NC 28078 PURCHASE ORDER NUMBER:
ATTN: Angela Baioni
PROJECT NUMBER: 92588929
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 22C0019
The results of analyses performed on the following samples submitted to CON -TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION: Oxford Compliance Units 1 &2
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
3901-MW2 22C0019-01 Water SM21-23 2320B
3901-MW3R 22C0019-02 Water SM21-23 2320B
3901-MW6R 22C0019-03 Water SM21-23 2320B
Page 3 of 14

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
Qualifications:
H-09
SM21-23 2320B
Sample received by laboratory with insufficient time remaining to perform analysis within the recommended holding time.
Analyte & Samples(s) Qualified:
Alkalinity
22C0019-02[3901-MW3R], 22C0019-03[3901-MW6R]
PR-18
Headspace present in sample container.
Analyte & Samples(s) Qualified:
Alkalinity
22C0019-01[3901-MW2], 22C0019-02[3901-MW3R], 22C0019-03[3901-MW6R], B302218-MS1
The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
d�
Lisa A. Worthington
Technical Representative
7
STT3c{SLS�:L•
• 1 •

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Oxford Compliance Units 1 &2 Sample Description: Work Order: 22C0019
Date Received: 3/l/2022
Field Sample #: 3901-MW2 Sampled: 2/15/2022 15:46
Sample ID: 22C0019-01
Sample Matrix: Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Alkalinity 9.0 1.0 0.65 mg/L 1 PR-18 SM21-23 2320B 3/l/22 3/l/22 15:27 IS
Page 5 of 14

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Oxford Compliance Units 1 &2 Sample Description: Work Order: 22C0019
Date Received: 3/l/2022
Field Sample #: 3901-MW3R Sampled: 2/15/2022 14:27
Sample ID: 22C0019-02
Sample Matrix: Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Alkalinity 100 1.0 0.65 mg/L 1 H-09, PR-18 SM21-23 2320B 3/l/22 3/l/22 15:53 IS
Page 6 of 14

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Oxford Compliance Units 1 &2 Sample Description: Work Order: 22C0019
Date Received: 3/l/2022
Field Sample #: 3901-MW6R Sampled: 2/15/2022 16:04
Sample ID: 22C0019-03
Sample Matrix: Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Alkalinity 260 1.0 0.65 mg/L 1 H-09, PR-18 SM21-23 2320B 3/l/22 3/l/22 16:11 IS
Page 7 of 14

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Sample Extraction Data
SM21-23 2320B
Lab Number [Field ID] Batch Initial [mL] Final [mL] Date
22CO019-01 [3901-MW2]
B302218
100
100
03/01/22
22CO019-02 [3901-MW3R]
B302218
100
100
03/01/22
22CO019-03 [3901-MW6R]
B302218
100
100
03/01/22
Page 8 of 14

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B302218 - SM21-23 2320B
Blank (B302218-BLK1)
Prepared & Analyzed: 03/01/22
Alkalinity
LCS (B302218-BS1)
ND 1.0
mg/L
Prepared & Analyzed: 03/01/22
Alkalinity
LCS Dup (B302218-BSD1)
30 1.0
mg/L
32.5 92.3 90-110
Prepared & Analyzed: 03/01/22
Alkalinity
Matrix Spike (B302218-MSI)
30 1.0
Source: 22CO019-01
mg/L
32.5 92.3 90-110 0.00 5.47
Prepared & Analyzed: 03/01/22
Alkalinity
60 1.0
mg/L
50.0 9.0 102 77.8-122 PR-18
Page 9 of 14

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
FLAG/QUALIFIER SUMMARY
* QC result is outside of established limits.
j Wide recovery limits established for difficult compound.
$ Wide RPD limits established for difficult compound.
# Data exceeded client recommended or regulatory level
ND Not Detected
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
H-09 Sample received by laboratory with insufficient time remaining to perform analysis within the recommended
holding time.
PR-18 Headspace present in sample container.
ST.T3:L'�S� i!
� . • •

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SM21-23 2320B in Water
Alkalinity CT,MA,NH,NY,RI,NC,ME,VA
Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditation:
Code Description Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2017
100033
03/l/2024
MA
Massachusetts DEP
M-MA100
06/30/2022
CT
Connecticut Department of Publilc Health
PH-0165
12/31/2022
NY
New York State Department of Health
10899 NELAP
04/l/2022
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2023
RI
Rhode Island Department of Health
LA000373
12/30/2022
NC
North Carolina Div. of Water Quality
652
12/31/2022
NJ
New Jersey DEP
MA007 NELAP
06/30/2022
FL
Florida Department of Health
E871027 NELAP
06/30/2022
VT
Vermont Department of Health Lead Laboratory
LL720741
07/30/2022
ME
State of Maine
MA00100
06/9/2023
VA
Commonwealth of Virginia
460217
12/14/2022
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2022
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2022
NC-DW
North Carolina Department of Health
25703
07/31/2022
PA
Commonwealth of Pennsylvania DEP
68-05812
06/30/2022
MI
Dept. of Env, Great Lakes, and Energy
9100
09/6/2022
ST.T3NCT.S� i!

Table of Contents
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Table of Contents
FedEO Tracking
546528651319
ADD NICKNAME
Delivered
Tuesday, March 1, 2022 at 10:20 am
FROM
ASHEVILLE, NC US
Fravel History
TIME ZONE
Local Scan Time
Tuesday, March 1,
2022
10:20 AM
9:01 AM
8:17 AM
7:28 AM
4:16 AM
Monday, February 28, 2022
11:19 PM
11:06 PM
7;50 PM
DELIVERED
Signed for by: F.FOUST
GET STATUS UPDATES
OBTAIN PROOF OF DELIVERY
TO
EAST LONGMEADOW, MA US
MANAGE DELIVERY _ v
EAST LONGMEADOW, MA Delivered
WINDSOR LOCKS, CT On FedEx vehicle for delivery
WINDSOR LOCKS, CT At local FedEx facility
EAST GRANBY, CT At destination sort facility
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MEMPHIS, TN
ASHEVILLE, NC
Shipment arriving On -Time
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Left FedEx origin facility
Page 13 of 14

Table of Contents
I Have Not Confirmed Sample Container
Numbers With Lab Staff Before Relinquishing
ATiALYTICAL LABOF3A'Y-ORY
Over Samples .� !
.: Doc#;2 .:Rey 5.. ... ...
Login Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client 1 L f ='�0,0 rk/ILA L 0-ff
Received By 7L d Date Time
How were the samples In Cooler No Cooler On Ice No Ice
received? Direct from Sampling Ambient Melted Ice
Were samples within By Gun # j Actual Temp
Temperature? 2-8°C By Blank # Actual Temp -
Was Custody Seal intact? Were Samples Tampered with?�
Was COC Relinquished ? Does Chain Agree With Samples?
Are there broken/leaking/loose caps on any samples? y--
Is COC in ink/ Legible? Were samples received within holding time?
Did COC include all Client � Analysis % Sampler Name
pertinent Information? Project ID's Collection Dates/Times
Are Sample labels filled out and legible? _
Are there Lab to Filters? (�
Are there Rushes?
Are there Short Holds? P
Is there enough Volume? [
is there Heoo�pace where applicable?
Proper MedWtortainers Used?
Were trip blan'.Iss received? 7 -
Do all samples have the proper pH? �E Acid
tnp- 1 Liter Amb.
HCL- 500 mL Amb.
Meoh- 250 mL Amb.
Bisulfate- Flashpoint
DI- Other Glass
Thinsulfate-I I SOC Kit
500 mL Plastic 8oz Amb/Clear
250 mL Plastic 4oz Amb/Clear
Col./Bacteria 2oz Amb/Clear
Other Plastic Encore
Plastic Bap Frozen:
Unp
HCL-
1 ;Liter Amb.
500 mL Amb.
1 Liter Plastic
500 mL Plastic
16 oz Amb.
8oz Amb/Clear
Meoh-
250 mL Amb.
250 mL Plastic
4oz Amb/Clear
Bisulfate-
Col./Bacteria
Flash pint
2oz Amb/Clear
DI_
I Other Plastic
Other Glass
Encore
lll-rhinv iffnt.-i
I SOC Kit
I
Plastic Bag
Frozen:

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 24, 2022
Stefan Bray, PE
Garrett & Moore
1029 West South Street
Raleigh, NC 27603
RE: Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Dear Stefan Bray, PE:
Enclosed are the analytical results for sample(s) received by the laboratory on February 17, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
WC+1,�a,i0Jt
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 99

lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification M 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
OXFORD COMPLIANCE UNITS 1/2
92589141
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92589141001
3901-MW-4R
EPA 601OD
RDT
16
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 7470A
DBB
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 120.1-1982
YEG
1
PASI-A
SM 2540C-2015
MA62
1
PASI-A
EPA 9040C
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
SM 4500-CI-E-2011
MMB
1
PASI-A
92589141002
3901-NES2S UNIT 1
HACH 10206
AMI
1
PASI-E
RSK 175 Modified
MAD
3
PASI-C
EPA 8260D
NSCQ
4
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
2
PASI-A
SM 531OB-2014
MDW
1
PASI-A
92589141003
3901-NES21)
HACH 10206
AMI
1
PASI-E
RSK 175 Modified
MAD
3
PASI-C
EPA 8260D
NSCQ
4
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
2
PASI-A
SM 531OB-2014
MDW
1
PASI-A
92589141004
3901-NES2S UNIT 2
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92589141005
3901-MW7 UNIT 1
HACH 10206
AMI
1
PASI-E
EPA 8081 B
SEM
4
PASI-C
EPA 8082A
SEM
8
PASI-C
RSK 175 Modified
MAD
3
PASI-C
EPA 601 OD
RDT
17
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 7470A
DBB
1
PASI-A
EPA 8270E
PKS
112
PASI-C
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 120.1-1982
YEG
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
SM 2540C-2015
MA62
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 9040C
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
2
PASI-A
SM 4500-CI-E-2011
MMB
1
PASI-A
SM 531OB-2014
MDW
1
PASI-A
92589141006
3901-MW5R
HACH 10206
AMI
1
PASI-E
EPA 8081 B
SEM
4
PASI-C
EPA 8082A
SEM
8
PASI-C
RSK 175 Modified
MAD
3
PASI-C
EPA 601 OD
RDT
17
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 7470A
DBB
1
PASI-A
EPA 8270E
PKS
112
PASI-C
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 120.1-1982
YEG
1
PASI-A
SM 2540C-2015
MA62
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 9040C
YEG
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
2
PASI-A
SM 531OB-2014
MDW
1
PASI-A
92589141007
3901-MW7 UNIT 2
EPA 601OD
RDT
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92589141008
3901-TRIP BLANK 03
EPA 8260D
NSCQ
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 99

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW-4R Lab ID: 92589141001 Collected: 02/16/22 12:00 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:43
7440-36-0
Arsenic
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 22:43
7440-38-2
Barium
62.6 ug/L
5.0
1
03/01/22 10:25
03/13/22 22:43
7440-39-3
Beryllium
ND ug/L
1.0
1
03/01/22 10:25
03/13/22 22:43
7440-41-7
Cadmium
ND ug/L
1.0
1
03/01/22 10:25
03/13/22 22:43
7440-43-9
Chromium
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:43
7440-47-3
Cobalt
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:43
7440-48-4
Copper
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:43
7440-50-8
Iron
662 ug/L
50.0
1
03/01/22 10:25
03/13/22 22:43
7439-89-6
Lead
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:43
7439-92-1
Manganese
35.9 ug/L
5.0
1
03/01/22 10:25
03/13/22 22:43
7439-96-5
Nickel
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:43
7440-02-0
Selenium
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 22:43
7782-49-2
Silver
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:43
7440-22-4
Vanadium
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:43
7440-62-2
Zinc
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 22:43
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND ug/L
0.47
1
02/25/22 12:06
02/28/22 05:22
7440-28-0
7470 Mercury
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical Services -Asheville
Mercury
ND ug/L
0.20
1
03/02/2211:15
03/03/2214:56
7439-97-6
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
02/21/22 14:59
67-64-1
Acrylonitrile
ND ug/L
10.0
1
02/21/22 14:59
107-13-1
Benzene
ND ug/L
1.0
1
02/21/22 14:59
71-43-2
Bromochloromethane
ND ug/L
1.0
1
02/21/22 14:59
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
02/21/22 14:59
75-27-4
Bromoform
ND ug/L
1.0
1
02/21/22 14:59
75-25-2
Bromomethane
ND ug/L
2.0
1
02/21/22 14:59
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
02/21/22 14:59
78-93-3
Carbon disulfide
ND ug/L
2.0
1
02/21/22 14:59
75-15-0
Carbon tetrachloride
ND ug/L
1.0
1
02/21/22 14:59
56-23-5
Chlorobenzene
ND ug/L
1.0
1
02/21/22 14:59
108-90-7
Chloroethane
ND ug/L
1.0
1
02/21/22 14:59
75-00-3
Chloroform
ND ug/L
1.0
1
02/21/22 14:59
67-66-3
Chloromethane
ND ug/L
1.0
1
02/21/22 14:59
74-87-3
1,2-Dibromo-3-chloropropane
ND ug/L
2.0
1
02/21/22 14:59
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
02/21/22 14:59
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
02/21/22 14:59
106-93-4
Dibromomethane
ND ug/L
1.0
1
02/21/22 14:59
74-95-3
REPORT OF LABORATORY ANALYSIS
v2
IK,v2
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW-4R Lab ID: 92589141001 Collected: 02/16/22 12:00 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
1,2-Dichlorobenzene
ND ug/L
1.0
1
02/21/22 14:59
95-50-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
02/21/22 14:59
106-46-7
trans-1,4-Dichloro-2-butene
ND ug/L
1.0
1
02/21/22 14:59
110-57-6
1,1-Dichloroethane
ND ug/L
1.0
1
02/21/22 14:59
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
02/21/22 14:59
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
02/21/22 14:59
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
02/21/22 14:59
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
02/21/22 14:59
156-60-5
1,2-Dichloropropene
ND ug/L
1.0
1
02/21/22 14:59
78-87-5
cis-1,3-Dichloropropene
ND ug/L
1.0
1
02/21/22 14:59
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
02/21/22 14:59
10061-02-6
Ethylbenzene
ND ug/L
1.0
1
02/21/22 14:59
100-41-4
2-Hexanone
ND ug/L
5.0
1
02/21/22 14:59
591-78-6
lodomethane
ND ug/L
20.0
1
02/21/22 14:59
74-88-4
Methylene Chloride
ND ug/L
5.0
1
02/21/22 14:59
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
02/21/22 14:59
108-10-1
Styrene
ND ug/L
1.0
1
02/21/22 14:59
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
1
02/21/22 14:59
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
02/21/22 14:59
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
02/21/22 14:59
127-18-4
Tetrahydrofuran
ND ug/L
10.0
1
02/21/22 14:59
109-99-9
Toluene
ND ug/L
1.0
1
02/21/22 14:59
108-88-3
1,1,1-Trichloroethane
ND ug/L
1.0
1
02/21/22 14:59
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
02/21/22 14:59
79-00-5
Trichloroethene
ND ug/L
1.0
1
02/21/22 14:59
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
02/21/22 14:59
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
1
02/21/22 14:59
96-18-4
Vinyl acetate
ND ug/L
2.0
1
02/21/22 14:59
108-05-4 IH
Vinyl chloride
ND ug/L
1.0
1
02/21/22 14:59
75-01-4
Xylene (Total)
ND ug/L
1.0
1
02/21/22 14:59
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97 %
70-130
1
02/21/22 14:59
460-00-4
1,2-Dichloroethane-d4 (S)
86 %
70-130
1
02/21/22 14:59
17060-07-0
Toluene-d8(S)
102 %
70-130
1
02/21/22 14:59
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
23.7 ug/L
2.0
1
02/21/22 21:34
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
95 %
70-130
1
02/21/22 21:34
17060-07-0
Toluene-d8(S)
98 %
66-133
1
02/21/22 21:34
2037-26-5
120.1 Specific Conductance
Analytical Method: EPA 120.1-1982
Pace Analytical Services -Asheville
Specific Conductance
824 umhos/cm
10.0
1
02/23/22 11:40
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM
without the written consent of Pace Analytical Services, LLC.
Page 6 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW-4R
Lab ID: 92589141001 Collected: 02/16/22
12:00
Received: 02/17/22 14:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
526000 ug/L 50000
1
02/20/22 13:11
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
7.4 Std. Units 0.10
1
02/21/22 18:44 H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
8370 ug/L 1000
1
02/24/22 07:46 14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
69200 ug/L 6000
6
03/10/22 21:30 16887-00-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-NES2S UNIT 1 Lab ID: 92589141002 Collected: 02/17/22 10:05 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HACH 10206 Nitrogen, Nitrate
Nitrogen, Nitrate
RSK 175 Headspace
Ethane
Ethene
Methane
8260D MSV Low Level Landfill
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Chloride
Sulfate
531013 TOC
Total Organic Carbon
Date: 03/24/2022 06:11 PM
Analytical Method: HACH 10206
Pace Analytical Services - Eden
ND mg/L
0.30
Analytical Method: RSK 175 Modified
Pace Analytical Services - Charlotte
ND ug/L
10.0
ND ug/L
10.0
28.2 ug/L
10.0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND ug/L
1.0
98 %
70-130
99 %
70-130
101 %
70-130
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
2.0
94 %
70-130
98 %
66-133
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L
100
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services -Asheville
9.7 mg/L
1.0
23.3 mg/L
1.0
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
0.79J mg/L
1.0
1 02/18/22 14:46 14797-55-8
1 02/18/22 20:44 74-84-0
1 02/18/22 20:44 74-85-1
1 02/18/22 20:44 74-82-8
1 02/21 /22 16:12
75-01-4
1 02/21 /22 16:12
460-00-4
1 02/21 /22 16:12
17060-07-0
1 02/21 /22 16:12
2037-26-5
1 02/21 /22 20:36 123-91-1
1 02/21 /22 20:36 17060-07-0
1 02/21 /22 20:36 2037-26-5
1 02/19/22 04:16 18496-25-8
1 02/24/22 09:10 16887-00-6
1 02/24/22 09:10 14808-79-8
1 02/25/2210:18 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-NES2D Lab ID: 92589141003 Collected: 02/17/22 11:42 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HACH 10206 Nitrogen, Nitrate
Nitrogen, Nitrate
RSK 175 Headspace
Ethane
Ethene
Methane
8260D MSV Low Level Landfill
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Chloride
Sulfate
531013 TOC
Total Organic Carbon
Date: 03/24/2022 06:11 PM
Analytical Method: HACH 10206
Pace Analytical Services - Eden
0.22J mg/L
0.30
Analytical Method: RSK 175 Modified
Pace Analytical Services - Charlotte
ND ug/L
10.0
ND ug/L
10.0
ND ug/L
10.0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND ug/L
1.0
98 %
70-130
88 %
70-130
101 %
70-130
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
2.0
90 %
70-130
98 %
66-133
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L
100
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services -Asheville
5.0 mg/L
1.0
50.1 mg/L
1.0
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
ND mg/L
1.0
1 02/18/22 14:46 14797-55-8
1 02/18/22 20:59 74-84-0
1 02/18/22 20:59 74-85-1
1 02/18/22 20:59 74-82-8
1 02/21 /22 18:00
75-01-4
1 02/21 /22 18:00
460-00-4
1 02/21 /22 18:00
17060-07-0
1 02/21 /22 18:00
2037-26-5
1 02/21 /22 22:12 123-91-1
1 02/21 /22 22:12 17060-07-0
1 02/21 /22 22:12 2037-26-5
1 02/19/22 04:16 18496-25-8
1 02/24/22 09:24 16887-00-6
1 02/24/22 09:24 14808-79-8
1 02/25/2210:37 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-NES2S UNIT 2
Lab ID: 92589141004 Collected:
02/17/22
10:05
Received: 02/17/22 14:00 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/21/22 18:18
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/21/22 18:18
107-13-1
Benzene
ND
ug/L
1.0
1
02/21/22 18:18
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/21/22 18:18
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/21/22 18:18
75-27-4
Bromoform
ND
ug/L
1.0
1
02/21/22 18:18
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/21/22 18:18
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
02/21/22 18:18
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/21/22 18:18
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/21/22 18:18
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/21/22 18:18
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/21/22 18:18
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/21/22 18:18
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/21/22 18:18
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/21/22 18:18
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/21/22 18:18
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/21/22 18:18
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/21/22 18:18
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/21/22 18:18
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/21/22 18:18
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/21/22 18:18
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/21/22 18:18
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/21/22 18:18
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/21/22 18:18
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/21/22 18:18
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/21/22 18:18
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/21/22 18:18
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/21/22 18:18
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/21/22 18:18
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/21/22 18:18
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/21/22 18:18
591-78-6
lodomethane
ND
ug/L
20.0
1
02/21/22 18:18
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/21/22 18:18
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/21/22 18:18
108-10-1
Styrene
ND
ug/L
1.0
1
02/21/22 18:18
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/21/22 18:18
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/21/22 18:18
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/21/22 18:18
127-18-4
Toluene
ND
ug/L
1.0
1
02/21/22 18:18
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/21/22 18:18
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/21/22 18:18
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/21/22 18:18
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/21/22 18:18
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/21/22 18:18
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/21/22 18:18
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/21/22 18:18
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-NES2S UNIT 2
Parameters
Lab ID: 92589141004 Collected: 02/17/22 10:05
Results Units Report Limit DF
Received: 02/17/22 14:00 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
02/21/22 18:18
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
1
02/21/22 18:18
460-00-4
1,2-Dichloroethane-d4 (S)
96 %
70-130
1
02/21/22 18:18
17060-07-0
Toluene-d8(S)
108 %
70-130
1
02/21/22 18:18
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L
2.0
1
02/21/22 22:32
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
95 %
70-130
1
02/21/22 22:32
17060-07-0
Toluene-d8(S)
99 %
66-133
1
02/21/22 22:32
2037-26-5
Date: 03/24/2022 06:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW7 UNIT 1 Lab ID: 92589141005 Collected: 02/17/22 09:35 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206
Pace Analytical Services - Eden
Nitrogen, Nitrate 0.29J mg/L 0.30 1 02/18/22 14:46 14797-55-8
8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
beta-BHC
Endosulfan I
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB RVE
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
ND ug/L 0.045 1 02/23/2217:48 02/28/2211:08 319-85-7
ND ug/L 0.045 1 02/23/2217:48 02/28/2211:08 959-98-8
65 % 10-184 1 02/23/2217:48 02/28/2211:08 877-09-8
87 % 10-154 1 02/23/2217:48 02/28/2211:08 2051-24-3
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
0.42 1
02/24/22 16:01
02/28/22 22:32
12674-11-2
ND
ug/L
0.42 1
02/24/22 16:01
02/28/22 22:32
11104-28-2
ND
ug/L
0.42 1
02/24/22 16:01
02/28/22 22:32
11141-16-5
ND
ug/L
0.42 1
02/24/22 16:01
02/28/22 22:32
53469-21-9
ND
ug/L
0.42 1
02/24/22 16:01
02/28/22 22:32
12672-29-6
ND
ug/L
0.42 1
02/24/22 16:01
02/28/22 22:32
11097-69-1
ND
ug/L
0.42 1
02/24/22 16:01
02/28/22 22:32
11096-82-5
53
%
10-181 1
02/24/22 16:01
02/28/22 22:32
2051-24-3
RSK 175 Headspace
Analytical Method: RSK 175 Modified
Pace Analytical Services - Charlotte
Ethane
ND ug/L
10.0
1
02/18/22 21:14
74-84-0
Ethene
ND ug/L
10.0
1
02/18/22 21:14
74-85-1
Methane
ND ug/L
10.0
1
02/18/22 21:14
74-82-8
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:47
7440-36-0
Arsenic
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 22:47
7440-38-2
Barium
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:47
7440-39-3
Beryllium
ND ug/L
1.0
1
03/01/22 10:25
03/13/22 22:47
7440-41-7
Cadmium
ND ug/L
1.0
1
03/01/22 10:25
03/13/22 22:47
7440-43-9
Chromium
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:47
7440-47-3
Cobalt
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:47
7440-48-4
Copper
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:47
7440-50-8
Iron
ND ug/L
50.0
1
03/01/22 10:25
03/13/22 22:47
7439-89-6
Lead
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:47
7439-92-1
Manganese
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:47
7439-96-5
Nickel
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:47
7440-02-0
Selenium
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 22:47
7782-49-2
Silver
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 22:47
7440-22-4
Thallium
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 22:47
7440-28-0
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced,
except
in full,
Date: 03/24/2022 06:11 PM
without the written consent of Pace Analytical Services,
LLC.
Page 12 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW7 UNIT 1
Lab ID: 92589141005 Collected:
02/17/22
09:35
Received: 02/17/22 14:00 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
Vanadium
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 22:47
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 22:47
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 05:26
7440-28-0
7470 Mercury
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical Services
-Asheville
Mercury
ND
ug/L
0.20
1
03/02/2211:15
03/03/2214:58
7439-97-6
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services
- Charlotte
Acenaphthene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
83-32-9
Acenaphthylene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
208-96-8
Acetophenone
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
98-86-2
2-Acetylaminofluorene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
53-96-3
4-Aminobiphenyl
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
92-67-1
Anthracene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
120-12-7
Benzo(a)anthracene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
56-55-3
Benzo(a)pyrene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
50-32-8
Benzo(b)fluoranthene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
191-24-2
Benzo(k)fluoranthene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
207-08-9
Benzyl alcohol
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:07
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
101-55-3
Butylbenzylphthalate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
59-50-7
4-Chloroaniline
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:07
106-47-8
Chlorobenzilate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
510-15-6
bis(2-Chloroethoxy)methane
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
111-44-4
2-Chloronaphthalene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
91-58-7
2-Chlorophenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
7005-72-3
Chrysene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
218-01-9
Diallate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
53-70-3
Dibenzofuran
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:07
91-94-1
2,4-Dichlorophenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
120-83-2
2,6-Dichlorophenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
87-65-0
Diethylphthalate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
84-66-2
Dimethoate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
4.5
1
02/23/22 09:21
02/26/22 16:07
60-11-7 IL,v1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW7 UNIT 1 Lab ID: 92589141005 Collected: 02/17/22 09:35 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
7,12-Dimethylbenz(a)anthracene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
45.5
1
02/23/22 09:21
02/26/22 16:07
119-93-7
2,4-Dimethylphenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
105-67-9
Dimethylphthalate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
131-11-3
Di-n-butylphthalate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:07
534-52-1
1,3-Dinitrobenzene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
99-65-0
2,4-Dinitrophenol
ND
ug/L
45.5
1
02/23/22 09:21
02/26/22 16:07
51-28-5
2,4-Dinitrotoluene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
121-14-2
2,6-Dinitrotoluene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
606-20-2
Di-n-octylphthalate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
117-84-0
Diphenylamine
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
122-39-4
Disulfoton
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.5
1
02/23/22 09:21
02/26/22 16:07
117-81-7
Ethyl methanesulfonate
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:07
62-50-0
Famphur
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
52-85-7
Fluoranthene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
206-44-0
Fluorene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
87-68-3
Hexachlorobenzene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
77-47-4
Hexachloroethane
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
67-72-1
Hexachloropropene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
193-39-5
Isodrin
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
465-73-6
Isophorone
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
78-59-1
Isosafrole
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
120-58-1
Kepone
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:07
143-50-0
Methapyrilene
ND
ug/L
45.5
1
02/23/22 09:21
02/26/22 16:07
91-80-5
3-Methylcholanthrene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
56-49-5
Methyl methanesulfonate
ND
ug/L
4.5
1
02/23/22 09:21
02/26/22 16:07
66-27-3
2-Methylnaphthalene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
91-57-6
Methyl parathion
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
15831-10-4
1-Naphthalenamine
ND
ug/L
4.5
1
02/23/22 09:21
02/26/22 16:07
134-32-7
2-Naphthalenamine
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
91-59-8
1,4-Naphthoquinone
ND
ug/L
4.5
1
02/23/22 09:21
02/26/22 16:07
130-15-4
2-Nitroaniline
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:07
88-74-4
3-Nitroaniline
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:07
99-09-2
4-Nitroaniline
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:07
100-01-6
Nitrobenzene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
98-95-3
2-Nitrophenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
88-75-5
4-Nitrophenol
ND
ug/L
45.5
1
02/23/22 09:21
02/26/22 16:07
100-02-7
5-Nitro-o-toluidine
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
99-55-8
N-Nitrosodiethylamine
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
55-18-5
REPORT OF LABORATORY ANALYSIS
Qual
IH,v1
IH
IH.v1
IL
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Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 99

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW7 UNIT 1
Parameters
8270E APP9 RV
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
ANALYTICAL RESULTS
Lab ID: 92589141005 Collected: 02/17/22 09:35 Received: 02/17/22 14:00 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No
Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
62-75-9
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
924-16-3
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
621-64-7
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
86-30-6
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
10595-95-6
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
100-75-4
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
930-55-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
126-68-1
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
108-60-1
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
56-38-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
608-93-5
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
82-68-8
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:07
87-86-5
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
62-44-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
85-01-8
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
108-95-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
106-50-3
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
298-02-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
23950-58-5
v1
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
129-00-0
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
94-59-7
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
95-94-3
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
58-90-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
297-97-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
95-53-4
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
95-95-4
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
88-06-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:07
99-35-4
37
%
10-144
1
02/23/22 09:21
02/26/22 16:07
4165-60-0
1g
37
%
10-130
1
02/23/22 09:21
02/26/22 16:07
321-60-8
71
%
34-163
1
02/23/22 09:21
02/26/22 16:07
1718-51-0
13
%
10-130
1
02/23/22 09:21
02/26/22 16:07
13127-88-3
6
%
10-130
1
02/23/22 09:21
02/26/22 16:07
367-12-4
SO
9
%
10-144
1
02/23/22 09:21
02/26/22 16:07
118-79-6
SO
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
02/21/2215:17
67-64-1
ND
ug/L
10.0
1
02/21/2215:17
107-13-1
ND
ug/L
1.0
1
02/21/2215:17
71-43-2
ND
ug/L
1.0
1
02/21/2215:17
74-97-5
ND
ug/L
1.0
1
02/21/2215:17
75-27-4
ND
ug/L
1.0
1
02/21/2215:17
75-25-2
ND
ug/L
2.0
1
02/21/2215:17
74-83-9
v2
ND
ug/L
5.0
1
02/21/2215:17
78-93-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 99

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW7 UNIT 1 Lab ID: 92589141005 Collected: 02/17/22 09:35 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 03/24/2022 06:11 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
99 %
85 %
102 %
2.0
1
02/21/22 15:17
75-15-0
1.0
1
02/21/22 15:17
56-23-5
1.0
1
02/21/22 15:17
108-90-7
1.0
1
02/21/22 15:17
75-00-3 IK,v2
1.0
1
02/21/22 15:17
67-66-3
1.0
1
02/21/22 15:17
74-87-3
2.0
1
02/21/22 15:17
96-12-8
1.0
1
02/21/22 15:17
124-48-1
1.0
1
02/21/22 15:17
106-93-4
1.0
1
02/21/22 15:17
74-95-3
1.0
1
02/21/22 15:17
95-50-1
1.0
1
02/21/22 15:17
106-46-7
1.0
1
02/21/22 15:17
110-57-6
1.0
1
02/21/22 15:17
75-34-3
1.0
1
02/21/22 15:17
107-06-2
1.0
1
02/21/22 15:17
75-35-4
1.0
1
02/21/22 15:17
156-59-2
1.0
1
02/21/22 15:17
156-60-5
1.0
1
02/21/22 15:17
78-87-5
1.0
1
02/21/22 15:17
10061-01-5
1.0
1
02/21/22 15:17
10061-02-6
1.0
1
02/21/22 15:17
100-41-4
5.0
1
02/21/22 15:17
591-78-6
20.0
1
02/21/22 15:17
74-88-4
5.0
1
02/21/22 15:17
75-09-2
5.0
1
02/21/22 15:17
108-10-1
1.0
1
02/21/22 15:17
100-42-5
1.0
1
02/21/22 15:17
630-20-6
1.0
1
02/21/22 15:17
79-34-5
1.0
1
02/21/22 15:17
127-18-4
10.0
1
02/21/22 15:17
109-99-9
1.0
1
02/21/22 15:17
108-88-3
1.0
1
02/21/22 15:17
71-55-6
1.0
1
02/21/22 15:17
79-00-5
1.0
1
02/21/22 15:17
79-01-6
1.0
1
02/21/22 15:17
75-69-4
1.0
1
02/21/22 15:17
96-18-4
2.0
1
02/21/22 15:17
108-05-4 I H
1.0
1
02/21/22 15:17
75-01-4
1.0
1
02/21/22 15:17
1330-20-7
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02/21/22 15:17 460-00-4
02/21/22 15:17 17060-07-0
02/21/22 15:17 2037-26-5
Page 16 of 99

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW7 UNIT 1
Lab ID: 92589141005 Collected:
02/17/22 09:35
Received: 02/17/22 14:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L
2.0
1
02/21/22 20:56
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
93 %
70-130
1
02/21/22 20:56
17060-07-0
Toluene-d8(S)
98 %
66-133
1
02/21/22 20:56
2037-26-5
120.1 Specific Conductance
Analytical Method: EPA 120.1-1982
Pace Analytical Services -Asheville
Specific Conductance
427 umhos/cm
10.0
1
02/23/22 11:47
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
268000 ug/L
25000
1
02/20/22 13:19
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
Sulfide
ND ug/L
100
1
02/19/22 04:16
18496-25-8
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.6 Std. Units
0.10
1
02/21/22 19:10
H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services -Asheville
Chloride
8.6 mg/L
1.0
1
02/24/22 09:38
16887-00-6
Sulfate
57.5 mg/L
1.0
1
02/24/22 09:38
14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
9330 ug/L
1000
1
03/10/22 21:20
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L
1.0
1
02/25/22 10:57
7440-44-0
Date: 03/24/2022 06:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW5R Lab ID: 92589141006 Collected: 02/17/22 11:48 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206
Pace Analytical Services - Eden
Nitrogen, Nitrate ND mg/L 0.30 1 02/18/22 14:46 14797-55-8
8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
beta-BHC
Endosulfan I
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
8082 GCS PCB RVE
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
ND ug/L 0.045 1 02/23/2217:48 02/28/2211:20 319-85-7
ND ug/L 0.045 1 02/23/2217:48 02/28/2211:20 959-98-8
45 % 10-184 1 02/23/2217:48 02/28/2211:20 877-09-8
85 % 10-154 1 02/23/2217:48 02/28/2211:20 2051-24-3
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND
ug/L
0.50
1
02/24/22 16:01
02/28/22 22:45
12674-11-2
ND
ug/L
0.50
1
02/24/22 16:01
02/28/22 22:45
11104-28-2
ND
ug/L
0.50
1
02/24/22 16:01
02/28/22 22:45
11141-16-5
ND
ug/L
0.50
1
02/24/22 16:01
02/28/22 22:45
53469-21-9
ND
ug/L
0.50
1
02/24/22 16:01
02/28/22 22:45
12672-29-6
ND
ug/L
0.50
1
02/24/22 16:01
02/28/22 22:45
11097-69-1
ND
ug/L
0.50
1
02/24/22 16:01
02/28/22 22:45
11096-82-5
82
%
10-181
1
02/24/22 16:01
02/28/22 22:45
2051-24-3
RSK 175 Headspace
Analytical Method: RSK 175 Modified
Pace Analytical Services - Charlotte
Ethane
ND ug/L
10.0
1
02/18/22 21:29
74-84-0
Ethene
ND ug/L
10.0
1
02/18/22 21:29
74-85-1
Methane
81.6 ug/L
10.0
1
02/18/22 21:29
74-82-8
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 23:15
7440-36-0
Arsenic
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 23:15
7440-38-2
Barium
40.8 ug/L
5.0
1
03/01/22 10:25
03/13/22 23:15
7440-39-3
Beryllium
ND ug/L
1.0
1
03/01/22 10:25
03/13/22 23:15
7440-41-7
Cadmium
ND ug/L
1.0
1
03/01/22 10:25
03/13/22 23:15
7440-43-9
Chromium
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 23:15
7440-47-3
Cobalt
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 23:15
7440-48-4
Copper
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 23:15
7440-50-8
Iron
ND ug/L
50.0
1
03/01/22 10:25
03/13/22 23:15
7439-89-6
Lead
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 23:15
7439-92-1
Manganese
103 ug/L
5.0
1
03/01/22 10:25
03/13/22 23:15
7439-96-5
Nickel
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 23:15
7440-02-0
Selenium
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 23:15
7782-49-2
Silver
ND ug/L
5.0
1
03/01/22 10:25
03/13/22 23:15
7440-22-4
Thallium
ND ug/L
10.0
1
03/01/22 10:25
03/13/22 23:15
7440-28-0
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced,
except
in full,
Date: 03/24/2022 06:11 PM
without the written consent of Pace Analytical Services,
LLC.
Page 18 of 99

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW5R
Lab ID: 92589141006 Collected:
02/17/22
11:48
Received: 02/17/22 14:00 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services
-Asheville
Vanadium
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 23:15
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 23:15
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 05:30
7440-28-0
7470 Mercury
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Pace Analytical Services
-Asheville
Mercury
ND
ug/L
0.20
1
03/02/2211:15
03/03/2215:01
7439-97-6
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services
- Charlotte
Acenaphthene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
83-32-9
Acenaphthylene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
208-96-8
Acetophenone
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
98-86-2
2-Acetylaminofluorene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
53-96-3
4-Aminobiphenyl
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
92-67-1
Anthracene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
120-12-7
Benzo(a)anthracene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
56-55-3
Benzo(a)pyrene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
50-32-8
Benzo(b)fluoranthene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
191-24-2
Benzo(k)fluoranthene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
207-08-9
Benzyl alcohol
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:32
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
101-55-3
Butylbenzylphthalate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
59-50-7
4-Chloroaniline
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:32
106-47-8
Chlorobenzilate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
510-15-6
bis(2-Chloroethoxy)methane
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
111-44-4
2-Chloronaphthalene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
91-58-7
2-Chlorophenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
7005-72-3
Chrysene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
218-01-9
Diallate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
2303-16-4
Dibenz(a,h)anthracene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
53-70-3
Dibenzofuran
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
132-64-9
3,3'-Dichlorobenzidine
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:32
91-94-1
2,4-Dichlorophenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
120-83-2
2,6-Dichlorophenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
87-65-0
Diethylphthalate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
84-66-2
Dimethoate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
60-51-5
P-Dimethylaminoazobenzene
ND
ug/L
4.5
1
02/23/22 09:21
02/26/22 16:32
60-11-7 IL,v1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW5R Lab ID: 92589141006 Collected: 02/17/22 11:48 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E APP9 RV
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
7,12-Dimethylbenz(a)anthracene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
57-97-6
3,3'-Dimethylbenzidine
ND
ug/L
45.5
1
02/23/22 09:21
02/26/22 16:32
119-93-7
2,4-Dimethylphenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
105-67-9
Dimethylphthalate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
131-11-3
Di-n-butylphthalate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:32
534-52-1
1,3-Dinitrobenzene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
99-65-0
2,4-Dinitrophenol
ND
ug/L
45.5
1
02/23/22 09:21
02/26/22 16:32
51-28-5
2,4-Dinitrotoluene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
121-14-2
2,6-Dinitrotoluene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
606-20-2
Di-n-octylphthalate
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
117-84-0
Diphenylamine
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
122-39-4
Disulfoton
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
298-04-4
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.5
1
02/23/22 09:21
02/26/22 16:32
117-81-7
Ethyl methanesulfonate
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:32
62-50-0
Famphur
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
52-85-7
Fluoranthene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
206-44-0
Fluorene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
87-68-3
Hexachlorobenzene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
77-47-4
Hexachloroethane
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
67-72-1
Hexachloropropene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
1888-71-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
193-39-5
Isodrin
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
465-73-6
Isophorone
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
78-59-1
Isosafrole
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
120-58-1
Kepone
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:32
143-50-0
Methapyrilene
ND
ug/L
45.5
1
02/23/22 09:21
02/26/22 16:32
91-80-5
3-Methylcholanthrene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
56-49-5
Methyl methanesulfonate
ND
ug/L
4.5
1
02/23/22 09:21
02/26/22 16:32
66-27-3
2-Methylnaphthalene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
91-57-6
Methyl parathion
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
298-00-0
2-Methylphenol(o-Cresol)
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
15831-10-4
1-Naphthalenamine
ND
ug/L
4.5
1
02/23/22 09:21
02/26/22 16:32
134-32-7
2-Naphthalenamine
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
91-59-8
1,4-Naphthoquinone
ND
ug/L
4.5
1
02/23/22 09:21
02/26/22 16:32
130-15-4
2-Nitroaniline
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:32
88-74-4
3-Nitroaniline
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:32
99-09-2
4-Nitroaniline
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:32
100-01-6
Nitrobenzene
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
98-95-3
2-Nitrophenol
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
88-75-5
4-Nitrophenol
ND
ug/L
45.5
1
02/23/22 09:21
02/26/22 16:32
100-02-7
5-Nitro-o-toluidine
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
99-55-8
N-Nitrosodiethylamine
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
55-18-5
REPORT OF LABORATORY ANALYSIS
Qual
IH,v1
IH
IH.v1
IL
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW5R
Parameters
8270E APP9 RV
N-Nitrosodimethylamine
N-Nitroso-di-n-butylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
N-Nitrosomethylethylamine
N-Nitrosopiperidine
N-Nitrosopyrrolidine
O, O,O-Triethyl phosphorothioate
2,2'-Oxybis(1-chloropropane)
Parathion (Ethyl parathion)
Pentachlorobenzene
Pentachloronitrobenzene
Pentachlorophenol
Phenacetin
Phenanthrene
Phenol
p-Phenylenediamine
Phorate
Pronamide
Pyrene
Safrole
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
Thionazin
O-Toluidine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
1,3,5-Trinitrobenzene
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
ANALYTICAL RESULTS
Lab ID: 92589141006 Collected: 02/17/22 11:48 Received: 02/17/22 14:00 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No
Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
62-75-9
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
924-16-3
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
621-64-7
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
86-30-6
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
10595-95-6
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
100-75-4
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
930-55-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
126-68-1
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
108-60-1
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
56-38-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
608-93-5
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
82-68-8
ND
ug/L
18.2
1
02/23/22 09:21
02/26/22 16:32
87-86-5
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
62-44-2
v1
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
85-01-8
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
108-95-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
106-50-3
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
298-02-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
23950-58-5
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
129-00-0
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
94-59-7
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
95-94-3
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
58-90-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
297-97-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
95-53-4
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
95-95-4
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
88-06-2
ND
ug/L
9.1
1
02/23/22 09:21
02/26/22 16:32
99-35-4
33
%
10-144
1
02/23/22 09:21
02/26/22 16:32
4165-60-0
1g
38
%
10-130
1
02/23/22 09:21
02/26/22 16:32
321-60-8
62
%
34-163
1
02/23/22 09:21
02/26/22 16:32
1718-51-0
3
%
10-130
1
02/23/22 09:21
02/26/22 16:32
13127-88-3
SO
0
%
10-130
1
02/23/22 09:21
02/26/22 16:32
367-12-4
SO
1
%
10-144
1
02/23/22 09:21
02/26/22 16:32
118-79-6
SO
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
02/21/2216:30
67-64-1
ND
ug/L
10.0
1
02/21/2216:30
107-13-1
ND
ug/L
1.0
1
02/21/2216:30
71-43-2
ND
ug/L
1.0
1
02/21/2216:30
74-97-5
ND
ug/L
1.0
1
02/21/2216:30
75-27-4
ND
ug/L
1.0
1
02/21/2216:30
75-25-2
ND
ug/L
2.0
1
02/21/2216:30
74-83-9
v2
ND
ug/L
5.0
1
02/21/2216:30
78-93-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW5R Lab ID: 92589141006 Collected: 02/17/22 11:48 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 03/24/2022 06:11 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
1.2
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
0.991
ug/L
0.71J
ug/L
ND
ug/L
1.4
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
0.881
ug/L
ND
ug/L
100 %
94 %
103 %
2.0
1
02/21/22 16:30
75-15-0
1.0
1
02/21/22 16:30
56-23-5
1.0
1
02/21/22 16:30
108-90-7
1.0
1
02/21/22 16:30
75-00-3 IK,v2
1.0
1
02/21/22 16:30
67-66-3
1.0
1
02/21/22 16:30
74-87-3
2.0
1
02/21/22 16:30
96-12-8
1.0
1
02/21/22 16:30
124-48-1
1.0
1
02/21/22 16:30
106-93-4
1.0
1
02/21/22 16:30
74-95-3
1.0
1
02/21/22 16:30
95-50-1
1.0
1
02/21/22 16:30
106-46-7
1.0
1
02/21/22 16:30
110-57-6
1.0
1
02/21/22 16:30
75-34-3
1.0
1
02/21/22 16:30
107-06-2
1.0
1
02/21/22 16:30
75-35-4
1.0
1
02/21/22 16:30
156-59-2
1.0
1
02/21/22 16:30
156-60-5
1.0
1
02/21/22 16:30
78-87-5
1.0
1
02/21/22 16:30
10061-01-5
1.0
1
02/21/22 16:30
10061-02-6
1.0
1
02/21/22 16:30
100-41-4
5.0
1
02/21/22 16:30
591-78-6
20.0
1
02/21/22 16:30
74-88-4
5.0
1
02/21/22 16:30
75-09-2
5.0
1
02/21/22 16:30
108-10-1
1.0
1
02/21/22 16:30
100-42-5
1.0
1
02/21/22 16:30
630-20-6
1.0
1
02/21/22 16:30
79-34-5
1.0
1
02/21/22 16:30
127-18-4
10.0
1
02/21/22 16:30
109-99-9
1.0
1
02/21/22 16:30
108-88-3
1.0
1
02/21/22 16:30
71-55-6
1.0
1
02/21/22 16:30
79-00-5
1.0
1
02/21/22 16:30
79-01-6
1.0
1
02/21/22 16:30
75-69-4
1.0
1
02/21/22 16:30
96-18-4
2.0
1
02/21/22 16:30
108-05-4 I H
1.0
1
02/21/22 16:30
75-01-4
1.0
1
02/21/22 16:30
1330-20-7
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02/21/22 16:30 460-00-4
02/21/22 16:30 17060-07-0
02/21/22 16:30 2037-26-5
Page 22 of 99

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW5R
Lab ID: 92589141006 Collected:
02/17/22 11:48
Received: 02/17/22 14:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
47.4 ug/L
2.0
1
02/21/22 21:53
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91 %
70-130
1
02/21/22 21:53
17060-07-0
Toluene-d8(S)
102 %
66-133
1
02/21/22 21:53
2037-26-5
120.1 Specific Conductance
Analytical Method: EPA 120.1-1982
Pace Analytical Services -Asheville
Specific Conductance
512 umhos/cm
10.0
1
02/23/22 11:49
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
Total Dissolved Solids
328000 ug/L
25000
1
02/20/22 13:19
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
Sulfide
ND ug/L
100
1
02/19/22 04:17
18496-25-8
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.8 Std. Units
0.10
1
02/21/22 19:18
H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services -Asheville
Chloride
43.6 mg/L
1.0
1
02/24/22 09:52
16887-00-6
Sulfate
8.5 mg/L
1.0
1
02/24/22 09:52
14808-79-8
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
1.5 mg/L
1.0
1
02/25/22 11:47
7440-44-0
Date: 03/24/2022 06:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW7 UNIT 2 Lab ID: 92589141007 Collected: 02/17/22 09:35 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 23:18
7440-36-0
Arsenic
5.9J
ug/L
10.0
1
03/01/22 10:25
03/13/22 23:18
7440-38-2
Barium
3.8J
ug/L
5.0
1
03/01/22 10:25
03/13/22 23:18
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/01/22 10:25
03/13/22 23:18
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/01/22 10:25
03/13/22 23:18
7440-43-9
Chromium
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 23:18
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 23:18
7440-48-4
Copper
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 23:18
7440-50-8
Lead
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 23:18
7439-92-1
Nickel
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 23:18
7440-02-0
Selenium
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 23:18
7782-49-2
Silver
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 23:18
7440-22-4
Vanadium
ND
ug/L
5.0
1
03/01/22 10:25
03/13/22 23:18
7440-62-2
Zinc
ND
ug/L
10.0
1
03/01/22 10:25
03/13/22 23:18
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
02/25/22 12:06
02/28/22 05:34
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
02/21/22 16:48
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/21/22 16:48
107-13-1
Benzene
ND
ug/L
1.0
1
02/21/22 16:48
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/21/22 16:48
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/21/22 16:48
75-27-4
Bromoform
ND
ug/L
1.0
1
02/21/22 16:48
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/21/22 16:48
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
02/21/22 16:48
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/21/22 16:48
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/21/22 16:48
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/21/22 16:48
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/21/22 16:48
75-00-3
Chloroform
ND
ug/L
1.0
1
02/21/22 16:48
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/21/22 16:48
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/21/22 16:48
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/21/22 16:48
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/21/22 16:48
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/21/22 16:48
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/21/22 16:48
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/21/22 16:48
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/21/22 16:48
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/21/22 16:48
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/21/22 16:48
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/21/22 16:48
75-35-4
REPORT OF LABORATORY ANALYSIS
v2
IK,v2
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 99

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-MW7 UNIT 2 Lab ID: 92589141007 Collected: 02/17/22 09:35 Received: 02/17/22 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/21/22 16:48
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/21/22 16:48
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/21/22 16:48
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/21/22 16:48
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/21/22 16:48
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/21/22 16:48
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/21/22 16:48
591-78-6
lodomethane
ND
ug/L
20.0
1
02/21/22 16:48
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/21/22 16:48
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/21/22 16:48
108-10-1
Styrene
ND
ug/L
1.0
1
02/21/22 16:48
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/21/22 16:48
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/21/22 16:48
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/21/22 16:48
127-18-4
Toluene
ND
ug/L
1.0
1
02/21/22 16:48
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/21/22 16:48
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/21/22 16:48
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/21/22 16:48
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/21/22 16:48
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/21/22 16:48
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/21/22 16:48
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/21/22 16:48
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
02/21/22 16:48
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
02/21/22 16:48
460-00-4
1,2-Dichloroethane-d4 (S)
91
%
70-130
1
02/21/22 16:48
17060-07-0
Toluene-d8(S)
102
%
70-130
1
02/21/22 16:48
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
02/21/22 22:51
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91
%
70-130
1
02/21/22 22:51
17060-07-0
Toluene-d8(S)
98
%
66-133
1
02/21/22 22:51
2037-26-5
Date: 03/24/2022 06:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-TRIP BLANK 03
Lab ID: 92589141008 Collected:
02/17/22
00:00
Received: 02/17/22 14:00 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services
- Charlotte
Acetone
ND
ug/L
25.0
1
02/21/22 14:05
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
02/21/22 14:05
107-13-1
Benzene
ND
ug/L
1.0
1
02/21/22 14:05
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
02/21/22 14:05
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
02/21/22 14:05
75-27-4
Bromoform
ND
ug/L
1.0
1
02/21/22 14:05
75-25-2
Bromomethane
ND
ug/L
2.0
1
02/21/22 14:05
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
02/21/22 14:05
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
02/21/22 14:05
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
02/21/22 14:05
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
02/21/22 14:05
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/21/22 14:05
75-00-3 IK,v2
Chloroform
ND
ug/L
1.0
1
02/21/22 14:05
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/21/22 14:05
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
02/21/22 14:05
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
02/21/22 14:05
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
02/21/22 14:05
106-93-4
Dibromomethane
ND
ug/L
1.0
1
02/21/22 14:05
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
02/21/22 14:05
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
02/21/22 14:05
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
02/21/22 14:05
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
02/21/22 14:05
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
02/21/22 14:05
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
02/21/22 14:05
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
02/21/22 14:05
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
02/21/22 14:05
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
02/21/22 14:05
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
02/21/22 14:05
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
02/21/22 14:05
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
02/21/22 14:05
100-41-4
2-Hexanone
ND
ug/L
5.0
1
02/21/22 14:05
591-78-6
lodomethane
ND
ug/L
20.0
1
02/21/22 14:05
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
02/21/22 14:05
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
02/21/22 14:05
108-10-1
Styrene
ND
ug/L
1.0
1
02/21/22 14:05
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
02/21/22 14:05
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
02/21/22 14:05
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
02/21/22 14:05
127-18-4
Toluene
ND
ug/L
1.0
1
02/21/22 14:05
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
02/21/22 14:05
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
02/21/22 14:05
79-00-5
Trichloroethene
ND
ug/L
1.0
1
02/21/22 14:05
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/21/22 14:05
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
02/21/22 14:05
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
02/21/22 14:05
108-05-4 IH
Vinyl chloride
ND
ug/L
1.0
1
02/21/22 14:05
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Sample: 3901-TRIP BLANK 03
Parameters
Lab ID: 92589141008 Collected: 02/17/22 00:00
Results Units Report Limit DF
Received: 02/17/22 14:00 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
02/21/22 14:05
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
101 %
70-130
1
02/21/22 14:05
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
02/21/22 14:05
17060-07-0
Toluene-d8(S)
112 %
70-130
1
02/21/22 14:05
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L
2.0
1
02/21/22 20:17
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92 %
70-130
1
02/21/22 20:17
17060-07-0
Toluene-d8(S)
98 %
66-133
1
02/21/22 20:17
2037-26-5
Date: 03/24/2022 06:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 99

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 679301 Analysis Method: HACH 10206
QC Batch Method: HACH 10206 Analysis Description: 10206 Nitrogen, Nitrate
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92589141002, 92589141003, 92589141005, 92589141006
METHOD BLANK: 3554422
Matrix:
Water
Associated Lab Samples: 92589141002, 92589141003, 92589141005, 92589141006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/L
ND
0.30
02/18/22 10:48
LABORATORY CONTROL SAMPLE:
3554423
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/L
5
5.0
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3554424 3554425
MS MSD
92588849001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L ND 5 5 5.0 5.1 100 101 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 679501 Analysis Method: RSK 175 Modified
QC Batch Method: RSK 175 Modified Analysis Description: RSK 175 HEADSPACE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92589141002, 92589141003, 92589141005, 92589141006
METHOD BLANK: 3555557
Matrix:
Water
Associated Lab Samples:
92589141002, 92589141003, 92589141005, 92589141006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Ethane
ug/L
ND
10.0
02/18/2218:42
Ethene
ug/L
ND
10.0
02/18/2218:42
Methane
ug/L
ND
10.0
02/18/2218:42
LABORATORY CONTROL SAMPLE:
3555558
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Ethane
ug/L
658 656
100
70-130
Ethene
ug/L
1120 1220
108
70-130
Methane
ug/L
396 391
99
70-130
MATRIX SPIKE SAMPLE:
3555639
92588124005 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Ethane
ug/L
41.9 658
718
103
70-130
Ethene
ug/L
ND 1120
1280
113
70-130
Methane
ug/L
10300 396
10300
4
70-130 M1
SAMPLE DUPLICATE: 3555638
92588124003 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Ethane
ug/L
ND 7.2J
Ethene
ug/L
ND 2.7J
Methane
ug/L
1680 1610
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 681648 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92589141001, 92589141005, 92589141006
METHOD BLANK: 3565706
Matrix:
Water
Associated Lab Samples: 92589141001, 92589141005, 92589141006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
ug/L
ND
0.20
03/03/2214:07
LABORATORY CONTROL SAMPLE:
3565707
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
ug/L
2.5
2.5
101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3565708 3565709
MS MSD
92588471014 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.5 2.6 98 104 75-125 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 30 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 681459 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92589141001, 92589141005, 92589141006, 92589141007
METHOD BLANK: 3565066 Matrix: Water
Associated Lab Samples: 92589141001, 92589141005, 92589141006, 92589141007
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Iron
ug/L
ND
Lead
ug/L
ND
Manganese
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0 03/13/22 21:47
10.0 03/13/22 21:47
5.0 03/13/22 21:47
1.0 03/13/22 21:47
1.0 03/13/22 21:47
5.0 03/13/22 21:47
5.0 03/13/22 21:47
5.0 03/13/22 21:47
50.0 03/13/22 21:47
5.0 03/13/22 21:47
5.0 03/13/22 21:47
5.0 03/13/22 21:47
10.0 03/13/22 21:47
5.0 03/13/22 21:47
10.0 03/13/22 21:47
5.0 03/13/22 21:47
10.0 03/13/22 21:47
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3565067
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
491
98
80-120
Arsenic
ug/L
500
485
97
80-120
Barium
ug/L
500
486
97
80-120
Beryllium
ug/L
500
496
99
80-120
Cadmium
ug/L
500
482
96
80-120
Chromium
ug/L
500
491
98
80-120
Cobalt
ug/L
500
479
96
80-120
Copper
ug/L
500
507
101
80-120
Iron
ug/L
5000
4960
99
80-120
Lead
ug/L
500
491
98
80-120
Manganese
ug/L
500
487
97
80-120
Nickel
ug/L
500
478
96
80-120
Selenium
ug/L
500
477
95
80-120
Silver
ug/L
250
245
98
80-120
Thallium
ug/L
500
480
96
80-120
Vanadium
ug/L
500
479
96
80-120
Zinc
ug/L
500
477
95
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
OXFORD COMPLIANCE UNITS 1/2
92589141
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3565068
3565069
MS
MSD
92588907002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
530
530
106
106
75-125
0
Arsenic
ug/L
ND
500
500
525
522
104
104
75-125
0
Barium
ug/L
27.9
500
500
538
539
102
102
75-125
0
Beryllium
ug/L
ND
500
500
534
534
107
107
75-125
0
Cadmium
ug/L
ND
500
500
512
513
102
103
75-125
0
Chromium
ug/L
ND
500
500
524
524
104
104
75-125
0
Cobalt
ug/L
ND
500
500
502
502
100
100
75-125
0
Copper
ug/L
ND
500
500
536
537
107
107
75-125
0
Iron
ug/L
848
5000
5000
6360
6300
110
109
75-125
1
Lead
ug/L
ND
500
500
513
514
102
103
75-125
0
Manganese
ug/L
18.6
500
500
532
528
103
102
75-125
1
Nickel
ug/L
ND
500
500
504
506
100
101
75-125
0
Selenium
ug/L
ND
500
500
546
546
109
109
75-125
0
Silver
ug/L
ND
250
250
260
261
104
104
75-125
0
Thallium
ug/L
ND
500
500
504
503
101
100
75-125
0
Vanadium
ug/L
4AJ
500
500
513
514
102
102
75-125
0
Zinc
ug/L
ND
500
500
511
512
102
102
75-125
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 680098 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92589141001, 92589141005, 92589141006, 92589141007
METHOD BLANK: 3558310
Matrix:
Water
Associated Lab Samples: 92589141001, 92589141005, 92589141006, 92589141007
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.47
02/28/22 03:54
LABORATORY CONTROL SAMPLE:
3558311
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
24.6
98 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3558312 3558313
MS MSD
92588929002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 25.0 25.1 100 100 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 33 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 679682 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92589141001, 92589141002, 92589141003, 92589141004, 92589141005, 92589141006, 92589141007,
92589141008
METHOD BLANK: 3556222
Matrix: Water
Associated Lab Samples: 92589141001, 92589141002, 92589141003, 92589141004, 92589141005, 92589141006, 92589141007,
92589141008
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
02/21/22 12:34
1,1,1-Trichloroethane
ug/L
ND
1.0
02/21/22 12:34
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
02/21/22 12:34
1,1,2-Trichloroethane
ug/L
ND
1.0
02/21/22 12:34
1,1-Dichloroethane
ug/L
ND
1.0
02/21/22 12:34
1,1-Dichloroethene
ug/L
ND
1.0
02/21/22 12:34
1,2,3-Trichloropropane
ug/L
ND
1.0
02/21/22 12:34
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
02/21/22 12:34
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
02/21/22 12:34
1,2-Dichlorobenzene
ug/L
ND
1.0
02/21/22 12:34
1,2-Dichloroethane
ug/L
ND
1.0
02/21/22 12:34
1,2-Dichloropropane
ug/L
ND
1.0
02/21/22 12:34
1,4-Dichlorobenzene
ug/L
ND
1.0
02/21/22 12:34
2-Butanone (MEK)
ug/L
ND
5.0
02/21/22 12:34
2-Hexanone
ug/L
ND
5.0
02/21/22 12:34
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
02/21/22 12:34
Acetone
ug/L
ND
25.0
02/21/22 12:34
Acrylonitrile
ug/L
ND
10.0
02/21/22 12:34
Benzene
ug/L
ND
1.0
02/21/22 12:34
Bromochloromethane
ug/L
ND
1.0
02/21/22 12:34
Bromodichloromethane
ug/L
ND
1.0
02/21/22 12:34
Bromoform
ug/L
ND
1.0
02/21/22 12:34
Bromomethane
ug/L
ND
2.0
02/21/22 12:34
Carbon disulfide
ug/L
ND
2.0
02/21/22 12:34
Carbon tetrachloride
ug/L
ND
1.0
02/21/22 12:34
Chlorobenzene
ug/L
ND
1.0
02/21/22 12:34
Chloroethane
ug/L
ND
1.0
02/21/22 12:34
Chloroform
ug/L
ND
1.0
02/21/22 12:34
Chloromethane
ug/L
ND
1.0
02/21/22 12:34
cis-1,2-Dichloroethene
ug/L
ND
1.0
02/21/22 12:34
cis-1,3-Dichloropropene
ug/L
ND
1.0
02/21/22 12:34
Dibromochloromethane
ug/L
ND
1.0
02/21/22 12:34
Dibromomethane
ug/L
ND
1.0
02/21/22 12:34
Ethylbenzene
ug/L
ND
1.0
02/21/22 12:34
lodomethane
ug/L
ND
20.0
02/21/22 12:34
Methylene Chloride
ug/L
ND
5.0
02/21/22 12:34
Styrene
ug/L
ND
1.0
02/21/22 12:34
Tetrachloroethene
ug/L
ND
1.0
02/21/22 12:34
Tetrahydrofuran
ug/L
ND
10.0
02/21/22 12:34
Qualifiers
v2
IK,v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
METHOD BLANK: 3556222 Matrix: Water
Associated Lab Samples: 92589141001, 92589141002, 92589141003, 92589141004, 92589141005, 92589141006, 92589141007,
92589141008
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
02/21/22 12:34
trans-1,2-Dichloroethene
ug/L
ND
1.0
02/21/22 12:34
trans- 1,3-Dichloropropene
ug/L
ND
1.0
02/21/22 12:34
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
02/21/22 12:34
Trichloroethene
ug/L
ND
1.0
02/21/22 12:34
Trichlorofluoromethane
ug/L
ND
1.0
02/21/22 12:34
Vinyl acetate
ug/L
ND
2.0
02/21/22 12:34 IH
Vinyl chloride
ug/L
ND
1.0
02/21/22 12:34
Xylene (Total)
ug/L
ND
1.0
02/21/22 12:34
1,2-Dichloroethane-d4 (S)
%
97
70-130
02/21/22 12:34
4-Bromofluorobenzene (S)
%
101
70-130
02/21/22 12:34
Toluene-d8 (S)
%
103
70-130
02/21/22 12:34
LABORATORY CONTROL SAMPLE: 3556223
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
50.4
101
70-130
1,1,1-Trichloroethane
ug/L
50
48.8
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.9
102
70-130
1,1,2-Trichloroethane
ug/L
50
52.7
105
70-130
1,1-Dichloroethane
ug/L
50
50.5
101
70-130
1,1-Dichloroethene
ug/L
50
54.1
108
70-132
1,2,3-Trichloropropane
ug/L
50
49.3
99
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
54.2
108
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.6
103
70-130
1,2-Dichlorobenzene
ug/L
50
51.2
102
70-130
1,2-Dichloroethane
ug/L
50
42.8
86
70-130
1,2-Dichloropropane
ug/L
50
44.6
89
70-130
1,4-Dichlorobenzene
ug/L
50
50.7
101
70-130
2-Butanone (MEK)
ug/L
100
102
102
70-133
2-Hexanone
ug/L
100
108
108
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
111
111
70-130
Acetone
ug/L
100
97.9
98
70-144
Acrylonitrile
ug/L
250
263
105
70-130
Benzene
ug/L
50
53.6
107
70-130
Bromochloromethane
ug/L
50
48.4
97
70-130
Bromodichloromethane
ug/L
50
44.7
89
70-130
Bromoform
ug/L
50
49.4
99
70-131
Bromomethane
ug/L
50
39.1
78
30-177 v2
Carbon disulfide
ug/L
50
52.5
105
70-133
Carbon tetrachloride
ug/L
50
51.5
103
70-130
Chlorobenzene
ug/L
50
49.3
99
70-130
Chloroethane
ug/L
50
24.7
49
46-131 IK,v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
LABORATORY CONTROL SAMPLE:
Parameter
3556223
Units
Spike LCS
Conc. Result
Chloroform
ug/L
50
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
Methylene Chloride
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Tetrahydrofuran
ug/L
500
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits Qualifiers
46.6
93
70-130
45.4
91
49-130
49.6
99
70-130
55.9
112
70-130
50.8
102
70-130
42.7
85
70-130
50.8
102
70-130
98.0
98
47-140
48.1
96
68-130
53.6
107
70-130
48.7
97
70-130
539
108
70-130
52.0
104
70-130
51.9
104
70-130
54.7
109
70-130
53.1
106
25-200
48.0
96
70-130
40.2
80
61-130
125
125
70-1401H
46.8
94
59-142
157
105
70-130
87
70-130
104
70-130
107
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3556224
MS
92589141001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3556225
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.0
21.4
105
107
70-135
2
1,1,1-Trichloroethane
ug/L
ND
20
20
19.8
20.4
99
102
70-148
3
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.4
20.4
97
102
70-131
5
1,1,2-Trichloroethane
ug/L
ND
20
20
19.8
20.7
99
103
70-136
4
1,1-Dichloroethane
ug/L
ND
20
20
19.9
20.4
100
102
70-147
2
1,1-Dichloroethene
ug/L
ND
20
20
22.0
22.1
110
111
70-158
0
1,2,3-Trichloropropane
ug/L
ND
20
20
18.5
19.7
92
99
67-137
7
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
20.3
22.1
102
111
69-136
8
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
20.3
21.3
101
106
70-137
5
1,2-Dichlorobenzene
ug/L
ND
20
20
21.0
21.9
105
110
70-133
4
1,2-Dichloroethane
ug/L
ND
20
20
17.2
17.8
86
89
67-138
3
1,2-Dichloropropane
ug/L
ND
20
20
19.8
20.6
99
103
70-138
4
1,4-Dichlorobenzene
ug/L
ND
20
20
21.0
21.5
105
107
70-133
2
2-Butanone (MEK)
ug/L
ND
40
40
33.8
37.5
84
94
61-147
11
2-Hexanone
ug/L
ND
40
40
33.6
37.7
84
94
67-139
11
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
32.5
36.5
81
91
67-136
11
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 36 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3556224
MS
92589141001 Spike
Parameter Units Result Conc.
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Ethylbenzene
lodomethane
Methylene Chloride
Styrene
Tetrachloroethene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethene
trans- 1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
40
100
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
20
200
20
20
20
20
20
20
40
20
60
MSD
Spike
Conc.
40
100
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
20
200
20
20
20
20
20
20
40
20
60
3556225
MS
Result
32.7
91.9
21.6
20.1
18.8
20.1
13.9
21.6
21.6
21.6
14.9
19.7
16.8
20.0
19.2
21.0
20.1
21.9
34.4
18.4
19.1
21.7
164
21.3
20.2
18.6
11.4
21.4
17.1
32.1
18.1
67.7
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
34.3
82
86
55-159
97.5
92
98
68-140
22.0
108
110
67-150
20.8
101
104
70-146
19.4
94
97
70-138
20.9
101
104
57-138
15.8
69
79
10-200
22.1
108
111
70-152
21.3
108
107
70-147
21.6
108
108
70-137
14.2
74
71
51-166
19.0
99
95
70-144
17.1
84
86
24-161
20.0
100
100
67-148
20.0
96
100
70-142
21.3
105
107
68-138
20.7
101
104
70-134
22.0
110
110
68-143
41.8
86
105
20-161
18.9
92
95
64-148
19.0
96
95
70-136
21.8
108
109
70-139
179
82
89
65-145
21.7
106
108
47-157
21.1
101
106
70-149
19.3
93
97
70-138
12.6
57
63
31-145
21.9
107
109
70-149
16.9
85
84
61-154
34.3
80
86
48-156
18.0
90
90
55-172
68.9
113
115
66-145
83
85
70-130
101
101
70-130
96
97
70-130
RPD Qual
5
6
2
3
3
4
13
2
1
0
4 IK
4
2
0
4
2
3
0
19
3
0
0
9
2
4
4
10
2
1
7 IH
1
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 37 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 679789 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92589141001, 92589141002, 92589141003, 92589141004, 92589141005, 92589141006, 92589141007,
92589141008
METHOD BLANK: 3556763
Matrix:
Water
Associated Lab Samples:
92589141001, 92589141002, 92589141003, 92589141004, 92589141005,
92589141006, 92589141007,
92589141008
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
02/21/22 16:46
1,2-Dichloroethane-d4 (S)
%
91
70-130
02/21/22 16:46
Toluene-d8 (S)
%
95
66-133
02/21/22 16:46
LABORATORY CONTROL SAMPLE: 3556764
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 19.8 99 70-130
1,2-Dichloroethane-d4 (S) % 89 70-130
Toluene-d8 (S) % 95 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3556765
3556766
MS
MSD
92589141002 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 20.8
21.4 104
107
64-141 3
1,2-Dichloroethane-d4 (S)
%
93
93
70-130
Toluene-d8(S)
%
98
99
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 680340
Analysis Method: EPA 8081 B
QC Batch Method: EPA 3510C
Analysis Description: 8081 OC Pesticides Red Vol
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92589141005, 92589141006
METHOD BLANK: 3559373
Matrix: Water
Associated Lab Samples: 92589141005, 92589141006
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
beta-BHC
ug/L
ND 0.050
02/28/22 09:01
Endosulfan I
ug/L
ND 0.050
02/28/22 09:01
Decachlorobiphenyl (S)
%
82 10-154
02/28/22 09:01
Tetrachloro-m-xylene (S)
%
71 10-184
02/28/22 09:01
LABORATORY CONTROL SAMPLE:
3559374
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
beta-BHC
ug/L
0.25 0.22
86 39-176
Endosulfan I
ug/L
0.25 0.21
86 44-145
Decachlorobiphenyl (S)
%
95 10-154
Tetrachloro-m-xylene (S)
%
82 10-184
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3559375 3559376
MS MSD
92587167004
Spike Spike MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
beta-BHC
ug/L ND
0.25 0.25 0.23
0.22 92 87
30-188 6
Endosulfan I
ug/L ND
0.25 0.25 0.23
0.11 93 44
19-168 72 R1
Decachlorobiphenyl (S)
%
102 68
10-154
Tetrachloro-m-xylene (S)
%
78 25
10-184
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 39 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 680708 Analysis Method: EPA 8082A
QC Batch Method: EPA 3510C Analysis Description: 8082 GCS PCB
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92589141005, 92589141006
METHOD BLANK: 3561079
Matrix:
Water
Associated Lab Samples:
92589141005, 92589141006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
ND
0.50
03/01/22 02:45
PCB-1221 (Aroclor 1221)
ug/L
ND
0.50
03/01/22 02:45
PCB-1232 (Aroclor 1232)
ug/L
ND
0.50
03/01/22 02:45
PCB-1242 (Aroclor 1242)
ug/L
ND
0.50
03/01/22 02:45
PCB-1248 (Aroclor 1248)
ug/L
ND
0.50
03/01/22 02:45
PCB-1254 (Aroclor 1254)
ug/L
ND
0.50
03/01/22 02:45
PCB-1260 (Aroclor 1260)
ug/L
ND
0.50
03/01/22 02:45
Decachlorobiphenyl (S)
%
81
10-181
03/01/22 02:45
LABORATORY CONTROL SAMPLE: 3561075
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
PCB-1016 (Aroclor 1016) ug/L 5 4.0 80 41-137
PCB-1260 (Aroclor 1260) ug/L 5 3.7 73 42-156
Decachlorobiphenyl (S) % 85 10-181
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3561076
3561077
MS
MSD
92589151004 Spike
Spike MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc. Result
Result
% Rec
% Rec
Limits RPD Qual
PCB-1016 (Aroclor 1016)
ug/L
ND 10
10 13.8
10.9
138
109
22-145 23
PCB-1260 (Aroclor 1260)
ug/L
ND 10
10 8.9
6.6
89
66
10-167 30
Decachlorobiphenyl (S)
%
99
75
10-181
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 680247 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water APP9 RV MSSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92589141005, 92589141006
METHOD BLANK: 3558848
Associated Lab Samples: 92589141005, 92589141006
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4,5-Tetrachlorobenzene
ug/L
ND
10.0
02/25/22 23:25
1,3,5-Trinitrobenzene
ug/L
ND
10.0
02/25/22 23:25
1,3-Dinitrobenzene
ug/L
ND
10.0
02/25/22 23:25
1,4-Naphthoquinone
ug/L
ND
5.0
02/25/22 23:25
1-Naphthalenamine
ug/L
ND
5.0
02/25/22 23:25
2,2'-Oxybis(1-chloropropane)
ug/L
ND
10.0
02/25/22 23:25
2,3,4,6-Tetrachlorophenol
ug/L
ND
10.0
02/25/22 23:25
2,4,5-Trichlorophenol
ug/L
ND
10.0
02/25/22 23:25
2,4,6-Trichlorophenol
ug/L
ND
10.0
02/25/22 23:25
2,4-Dichlorophenol
ug/L
ND
10.0
02/25/22 23:25
2,4-Dimethylphenol
ug/L
ND
10.0
02/25/22 23:25
2,4-Dinitrophenol
ug/L
ND
50.0
02/25/22 23:25
2,4-Dinitrotoluene
ug/L
ND
10.0
02/25/22 23:25
2,6-Dichlorophenol
ug/L
ND
10.0
02/25/22 23:25
2,6-Dinitrotoluene
ug/L
ND
10.0
02/25/22 23:25
2-Acetylaminofluorene
ug/L
ND
10.0
02/25/22 23:25
2-Chloronaphthalene
ug/L
ND
10.0
02/25/22 23:25
2-Chlorophenol
ug/L
ND
10.0
02/25/22 23:25
2-Methylnaphthalene
ug/L
ND
10.0
02/25/22 23:25
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
02/25/22 23:25
2-Naphthalenamine
ug/L
ND
10.0
02/25/22 23:25
2-Nitroaniline
ug/L
ND
20.0
02/25/22 23:25
2-Nitrophenol
ug/L
ND
10.0
02/25/22 23:25
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
10.0
02/25/22 23:25
3,3'-Dichlorobenzidine
ug/L
ND
20.0
02/25/22 23:25
3,3'-Dimethylbenzidine
ug/L
ND
50.0
02/25/22 23:25
3-Methylcholanthrene
ug/L
ND
10.0
02/25/22 23:25
3-Nitroaniline
ug/L
ND
20.0
02/25/22 23:25
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
02/25/22 23:25
4-Aminobiphenyl
ug/L
ND
10.0
02/25/22 23:25
4-Bromophenylphenyl ether
ug/L
ND
10.0
02/25/22 23:25
4-ChIoro-3-methyl phenol
ug/L
ND
10.0
02/25/22 23:25
4-Chloroaniline
ug/L
ND
20.0
02/25/22 23:25
4-Chlorophenylphenyl ether
ug/L
ND
10.0
02/25/22 23:25
4-Nitroaniline
ug/L
ND
20.0
02/25/22 23:25
4-Nitrophenol
ug/L
ND
50.0
02/25/22 23:25
5-Nitro-o-toluidine
ug/L
ND
10.0
02/25/22 23:25
7,12-Dimethylbenz(a)anthracene
ug/L
ND
10.0
02/25/22 23:25
Acenaphthene
ug/L
ND
10.0
02/25/22 23:25
Acenaphthylene
ug/L
ND
10.0
02/25/22 23:25
IH
IL
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
METHOD BLANK: 3558848
Associated Lab Samples: 92589141005, 92589141006
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Acetophenone
ug/L
ND
10.0
02/25/22 23:25
Anthracene
ug/L
ND
10.0
02/25/22 23:25
Benzo(a)anthracene
ug/L
ND
10.0
02/25/22 23:25
Benzo(a)pyrene
ug/L
ND
10.0
02/25/22 23:25
Benzo(b)fluoranthene
ug/L
ND
10.0
02/25/22 23:25
Benzo(g,h,i)perylene
ug/L
ND
10.0
02/25/22 23:25
Benzo(k)fluoranthene
ug/L
ND
10.0
02/25/22 23:25
Benzyl alcohol
ug/L
ND
20.0
02/25/22 23:25
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
02/25/22 23:25
bis(2-Chloroethyl) ether
ug/L
ND
10.0
02/25/22 23:25
bis(2-Ethylhexyl)phthalate
ug/L
ND
6.0
02/25/22 23:25
Butylbenzylphthalate
ug/L
ND
10.0
02/25/22 23:25
Chlorobenzilate
ug/L
ND
10.0
02/25/22 23:25
Chrysene
ug/L
ND
10.0
02/25/22 23:25
Di-n-butylphthalate
ug/L
ND
10.0
02/25/22 23:25
Di-n-octylphthalate
ug/L
ND
10.0
02/25/22 23:25
Diallate
ug/L
ND
10.0
02/25/22 23:25
Dibenz(a,h)anthracene
ug/L
ND
10.0
02/25/22 23:25
Dibenzofuran
ug/L
ND
10.0
02/25/22 23:25
Diethylphthalate
ug/L
ND
10.0
02/25/22 23:25
Dimethoate
ug/L
ND
10.0
02/25/22 23:25
Dimethylphthalate
ug/L
ND
10.0
02/25/22 23:25
Diphenylamine
ug/L
ND
10.0
02/25/22 23:25
Disulfoton
ug/L
ND
10.0
02/25/22 23:25
Ethyl methanesulfonate
ug/L
ND
20.0
02/25/22 23:25
Famphur
ug/L
ND
10.0
02/25/22 23:25
Fluoranthene
ug/L
ND
10.0
02/25/22 23:25
Fluorene
ug/L
ND
10.0
02/25/22 23:25
Hexachloro-1,3-butadiene
ug/L
ND
10.0
02/25/22 23:25
Hexachlorobenzene
ug/L
ND
10.0
02/25/22 23:25
Hexachlorocyclopentadiene
ug/L
ND
10.0
02/25/22 23:25
Hexachloroethane
ug/L
ND
10.0
02/25/22 23:25
Hexachloropropene
ug/L
ND
10.0
02/25/22 23:25
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
02/25/22 23:25
Isodrin
ug/L
ND
10.0
02/25/22 23:25
Isophorone
ug/L
ND
10.0
02/25/22 23:25
Isosafrole
ug/L
ND
10.0
02/25/22 23:25
Kepone
ug/L
ND
20.0
02/25/22 23:25
Methapyrilene
ug/L
ND
50.0
02/25/22 23:25
Methyl methanesulfonate
ug/L
ND
5.0
02/25/22 23:25
Methyl parathion
ug/L
ND
10.0
02/25/22 23:25
N-Nitroso-di-n-butylamine
ug/L
ND
10.0
02/25/22 23:25
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
02/25/22 23:25
N-Nitrosodiethylamine
ug/L
ND
10.0
02/25/22 23:25
N-Nitrosodimethylamine
ug/L
ND
10.0
02/25/22 23:25
IH
IH
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
METHOD BLANK: 3558848
Associated Lab Samples: 92589141005, 92589141006
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
N-Nitrosodiphenylamine
ug/L
ND
10.0
02/25/22 23:25
N-Nitrosomethylethylamine
ug/L
ND
10.0
02/25/22 23:25
N-Nitrosopiperidine
ug/L
ND
10.0
02/25/22 23:25
N-Nitrosopyrrolidine
ug/L
ND
10.0
02/25/22 23:25
Nitrobenzene
ug/L
ND
10.0
02/25/22 23:25
O,O,O-Triethylphosphorothioate
ug/L
ND
10.0
02/25/22 23:25
O-Toluidine
ug/L
ND
10.0
02/25/22 23:25
P-Dimethylaminoazobenzene
ug/L
ND
5.0
02/25/22 23:25 IL
p-Phenylenediamine
ug/L
ND
10.0
02/25/22 23:25
Parathion (Ethyl parathion)
ug/L
ND
10.0
02/25/22 23:25
Pentachlorobenzene
ug/L
ND
10.0
02/25/22 23:25
Pentachloronitrobenzene
ug/L
ND
10.0
02/25/22 23:25
Pentachlorophenol
ug/L
ND
20.0
02/25/22 23:25
Phenacetin
ug/L
ND
10.0
02/25/22 23:25
Phenanthrene
ug/L
ND
10.0
02/25/22 23:25
Phenol
ug/L
ND
10.0
02/25/22 23:25
Phorate
ug/L
ND
10.0
02/25/22 23:25
Pronamide
ug/L
ND
10.0
02/25/22 23:25
Pyrene
ug/L
ND
10.0
02/25/22 23:25
Safrole
ug/L
ND
10.0
02/25/22 23:25
Thionazin
ug/L
ND
10.0
02/25/22 23:25
2,4,6-Tribromophenol (S)
%
66
10-144
02/25/22 23:25
2-Fluorobiphenyl (S)
%
53
10-130
02/25/22 23:25
2-Fluorophenol (S)
%
28
10-130
02/25/22 23:25
Nitrobenzene-d5 (S)
%
54
10-144
02/25/22 23:25
Phenol-d6 (S)
%
31
10-130
02/25/22 23:25
Terphenyl-d14 (S)
%
86
34-163
02/25/22 23:25
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3558849
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4,5-Tetrachlorobenzene
ug/L
50
33.4
67
17-130
1,3,5-Trinitrobenzene
ug/L
50
54.6
109
44-200
1,3-Dinitrobenzene
ug/L
50
52.8
106
39-159
1,4-Naphthoquinone
ug/L
50
55.0
110
10-159
1-Naphthalenamine
ug/L
50
30.0
60
10-130
2,2'-Oxybis(1-chloropropane)
ug/L
50
39.8
80
28-130
2,3,4,6-Tetrachlorophenol
ug/L
50
47.8
96
10-200
2,4,5-Trichlorophenol
ug/L
50
48.4
97
35-130
2,4,6-Trichlorophenol
ug/L
50
45.6
91
31-130
2,4-Dichlorophenol
ug/L
50
45.5
91
35-130
2,4-Dimethylphenol
ug/L
50
42.0
84
34-130
2,4-Dinitrophenol
ug/L
250
228
91
10-153
2,4-Dinitrotoluene
ug/L
50
50.1
100
37-136
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
LABORATORY CONTROL SAMPLE:
Parameter
3558849
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,6-Dichlorophenol
ug/L
50
48.5
97
31-139
2,6-Dinitrotoluene
ug/L
50
50.9
102
33-136
2-Acetylaminofluorene
ug/L
50
48.5
97
19-181
2-Chloronaphthalene
ug/L
50
38.6
77
26-130
2-Chlorophenol
ug/L
50
39.6
79
37-130
2-Methylnaphthalene
ug/L
50
39.3
79
29-130
2-Methylphenol(o-Cresol)
ug/L
50
39.3
79
35-130
2-Naphthalenamine
ug/L
50
27.2
54
10-136
2-Nitroaniline
ug/L
100
96.4
96
37-130
2-Nitrophenol
ug/L
50
46.9
94
32-130
3&4-Methyl phenol (m&p Cresol)
ug/L
50
37.9
76
34-130
3,3'-Dichlorobenzidine
ug/L
100
86.4
86
34-136
3,3'-Dimethylbenzidine
ug/L
100
94.6
95
10-2001H
3-Methylcholanthrene
ug/L
50
40.1
80
39-190
3-Nitroaniline
ug/L
100
100
100
37-138IL
4,6-Dinitro-2-methyl phenol
ug/L
100
85.2
85
21-157
4-Aminobiphenyl
ug/L
50
29.6
59
17-137
4-Bromophenylphenyl ether
ug/L
50
44.3
89
38-130
4-ChIoro-3-methyl phenol
ug/L
100
90.6
91
37-130
4-Chloroaniline
ug/L
100
87.4
87
38-130
4-Chlorophenylphenyl ether
ug/L
50
45.3
91
33-130
4-Nitroaniline
ug/L
100
102
102
42-137
4-Nitrophenol
ug/L
250
156
62
10-130
5-Nitro-o-toluidine
ug/L
50
50.9
102
39-170
7,12-Dimethylbenz(a)anthracene
ug/L
50
37.8
76
33-139
Acenaphthene
ug/L
50
43.1
86
33-130
Acenaphthylene
ug/L
50
44.0
88
35-130
Acetophenone
ug/L
50
43.7
87
36-130
Anthracene
ug/L
50
43.1
86
48-130
Benzo(a)anthracene
ug/L
50
45.9
92
48-137
Benzo(a)pyrene
ug/L
50
31.0
62
49-138
Benzo(b)fluoranthene
ug/L
50
31.6
63
52-138
Benzo(g,h,i)perylene
ug/L
50
31.1
62
48-140
Benzo(k)fluoranthene
ug/L
50
30.5
61
48-139
Benzyl alcohol
ug/L
100
85.6
86
35-130
bis(2-Chloroethoxy)methane
ug/L
50
45.2
90
34-130
bis(2-Chloroethyl) ether
ug/L
50
42.8
86
36-130
bis(2-Ethylhexyl)phthalate
ug/L
50
47.3
95
32-165
Butylbenzylphthalate
ug/L
50
48.9
98
34-161
Chlorobenzilate
ug/L
50
44.2
88
43-176
Chrysene
ug/L
50
45.0
90
47-131
Di-n-butylphthalate
ug/L
50
47.8
96
39-144
Di-n-octylphthalate
ug/L
50
44.7
89
30-170
Diallate
ug/L
50
44.8
90
33-143
Dibenz(a,h)anthracene
ug/L
50
33.0
66
49-138
Dibenzofuran
ug/L
50
44.0
88
33-130
Diethylphthalate
ug/L
50
47.4
95
38-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 99

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
LABORATORY CONTROL SAMPLE:
Parameter
3558849
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Dimethoate
ug/L
50
50.4
101
46-173
Dimethylphthalate
ug/L
50
46.6
93
37-130
Diphenylamine
ug/L
50
40.6
81
35-135
Disulfoton
ug/L
50
39.1
78
34-139
Ethyl methanesulfonate
ug/L
50
44.0
88
33-133
Famphur
ug/L
100
69.0
69
10-1301H
Fluoranthene
ug/L
50
47.7
95
46-137
Fluorene
ug/L
50
46.1
92
37-130
Hexachloro-1,3-butadiene
ug/L
50
26.2
52
11-130
Hexachlorobenzene
ug/L
50
42.6
85
38-130
Hexachlorocyclopentadiene
ug/L
50
31.0
62
10-130
Hexachloroethane
ug/L
50
24.8
50
14-130
Hexachloropropene
ug/L
50
18.5
37
10-130
Indeno(1,2,3-cd)pyrene
ug/L
50
31.3
63
41-130
Isodrin
ug/L
50
43.1
86
36-139
Isophorone
ug/L
50
45.1
90
33-130
Isosafrole
ug/L
50
39.0
78
22-130
Kepone
ug/L
100
67.5
68
10-130
Methapyrilene
ug/L
50
ND
20
10-1731H
Methyl methanesulfonate
ug/L
50
38.6
77
33-130
Methyl parathion
ug/L
50
58.1
116
39-200
N-Nitroso-di-n-butylamine
ug/L
50
40.7
81
22-130
N-Nitroso-di-n-propylamine
ug/L
50
45.9
92
36-130
N-Nitrosodiethylamine
ug/L
50
43.6
87
23-136
N-Nitrosodimethylamine
ug/L
50
33.6
67
34-130
N-Nitrosodiphenylamine
ug/L
50
40.6
81
37-130
N-Nitrosomethylethylamine
ug/L
50
41.0
82
18-137
N-Nitrosopiperidine
ug/L
50
47.3
95
25-142
N-Nitrosopyrrolidine
ug/L
50
42.7
85
24-146
Nitrobenzene
ug/L
50
42.9
86
36-130
O,O,O-Triethylphosphorothioate
ug/L
50
43.9
88
29-130
O-Toluidine
ug/L
50
39.7
79
27-132
P-Dimethylaminoazobenzene
ug/L
50
20.5
41
17-130IL
p-Phenylenediamine
ug/L
ND
Parathion (Ethyl parathion)
ug/L
50
51.3
103
32-200
Pentachlorobenzene
ug/L
50
41.2
82
27-130
Pentachloronitrobenzene
ug/L
50
53.4
107
47-164
Pentachlorophenol
ug/L
100
86.0
86
23-149
Phenacetin
ug/L
50
52.5
105
44-181
Phenanthrene
ug/L
50
44.1
88
44-130
Phenol
ug/L
50
26.1
52
18-130
Phorate
ug/L
50
44.0
88
18-183
Pronamide
ug/L
50
52.0
104
45-163
Pyrene
ug/L
50
42.8
86
47-134
Safrole
ug/L
50
43.0
86
27-130
Thionazin
ug/L
50
49.7
99
36-162
2,4,6-Tribromophenol (S)
%
93
10-144
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
LABORATORY CONTROL SAMPLE:
3558849
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
2-Fluorobiphenyl (S)
%
78
10-130
2-Fluorophenol(S)
%
61
10-130
Nitrobenzene-d5 (S)
%
86
10-144
Phenol-d6 (S)
%
51
10-130
Terphenyl-d14 (S)
%
82
34-163
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3558850
MS
35697686001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3558851
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,2,4,5-Tetrachlorobenzene
ug/L
4.51-1
50
50
16.3
23.7
33
47
10-130
37 R1
1,3,5-Trinitrobenzene
ug/L
5.51-1
50
50
21.6
30.1
43
60
50-200
33 M1,R1
1,3-Dinitrobenzene
ug/L
3.81-1
50
50
29.9
43.0
60
86
43-161
36 R1
1,4-Naphthoquinone
ug/L
4.41-1
50
50
11.2
17.4
22
35
10-184
43 R1
1-Naphthalenamine
ug/L
4.1U
50
50
16.1
28.7
32
57
10-130
56 R1
2,2'-Oxybis(1-chloropropane)
ug/L
1.21-1
50
50
19.3
28.8
39
58
12-142
39 R1
2,3,4,6-Tetrachlorophenol
ug/L
1.51-1
50
50
24.6
34.0
49
68
10-198
32 R1
2,4,5-Trichlorophenol
ug/L
1.41-1
50
50
27.6
30.0
55
60
10-143
8
2,4,6-Trichlorophenol
ug/L
1.61-1
50
50
23.7
33.2
47
66
10-147
33 R1
2,4-Dichlorophenol
ug/L
1.41-1
50
50
22.9
34.8
46
70
10-138
41 R1
2,4-Dimethylphenol
ug/L
1.71-1
50
50
22.5
34.1
45
68
25-130
41 R1
2,4-Dinitrophenol
ug/L
26.01-1
250
250
ND
ND
10
10
10-165
2,4-Dinitrotoluene
ug/L
1.61-1
50
50
29.7
41.2
59
82
29-148
33 R1
2,6-Dichlorophenol
ug/L
4.21-1
50
50
21.6
31.2
43
62
33-139
36 R1
2,6-Dinitrotoluene
ug/L
1.71-1
50
50
46.9
63.8
94
128
26-146
31 R1
2-Acetylaminofluorene
ug/L
4.1 U
50
50
35.6
48.3
71
97
27-172
30
2-Chloronaphthalene
ug/L
1.71-1
50
50
19.6
29.4
39
59
11-130
40 R1
2-Chlorophenol
ug/L
1.21-1
50
50
19.8
29.6
40
59
10-133
40 R1
2-Methylnaphthalene
ug/L
1.91-1
50
50
19.1
28.7
38
57
13-130
40 R1
2-Methylphenol(o-Cresol)
ug/L
1.91-1
50
50
21.6
32.1
43
64
20-130
39 R1
2-Naphthalenamine
ug/L
5.41-1
50
50
19.8
30.5
40
61
10-135
42 R1
2-Nitroaniline
ug/L
3.01-1
100
100
55.0
73.7
55
74
24-136
29
2-Nitrophenol
ug/L
1.41-1
50
50
22.3
33.4
45
67
10-153
40 R1
3&4-Methyl phenol (m&p
ug/L
1.21-1
50
50
20.2
36.2
40
72
16-130
57 R1
Cresol)
3,3'-Dichlorobenzidine
ug/L
8.1U
100
100
8.9J
12.1J
9
12
10-153
M1
3,3'-Dimethylbenzidine
ug/L
31.1U
100
100
ND
ND
0
0
10-200
IH,M1
3-Methylcholanthrene
ug/L
5.81-1
50
50
27.8
39.6
56
79
53-181
35 R1
3-Nitroaniline
ug/L
3.81-1
100
100
61.0
82.6
61
83
22-151
30IL
4,6-Dinitro-2-methyl phenol
ug/L
3.41-1
100
100
23.3
27.0
23
27
10-180
14
4-Aminobiphenyl
ug/L
4.71-1
50
50
11.5
18.0
23
36
10-139
44 R1
4-Bromophenylphenyl ether
ug/L
1.81-1
50
50
25.5
36.1
51
72
25-130
34 R1
4-Chloro-3-methyl phenol
ug/L
3.31-1
100
100
61.6
90.0
62
90
25-133
37 R1
4-Chloroaniline
ug/L
3.61-1
100
100
47.9
67.9
48
68
14-132
34 R1
4-Chlorophenylphenyl ether
ug/L
2.01-1
50
50
23.2
34.3
46
69
19-130
38 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 46 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3558850
MS
35697686001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3558851
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
4-Nitroaniline
ug/L
5.1 U
100
100
62.1
84.3
62
84
29-150
30
4-Nitrophenol
ug/L
6.61-1
250
250
38.1J
54.4
15
22
10-130
5-Nitro-o-toluidine
ug/L
3.81-1
50
50
26.2
39.0
52
78
48-163
39 R1
7,12-
ug/L
3.01-1
50
50
23.0
32.8
46
66
40-140
35 R1
Di methyl benz(a)anth racene
Acenaphthene
ug/L
2.01-1
50
50
21.7
32.8
43
66
16-130
41 R1
Acenaphthylene
ug/L
2.01-1
50
50
22.4
33.7
45
67
15-137
40 R1
Acetophenone
ug/L
1.51-1
50
50
22.2
33.4
44
67
28-130
40 R1
Anthracene
ug/L
2.31-1
50
50
26.5
38.2
53
76
37-136
36 R1
Benzo(a)anthracene
ug/L
2.71-1
50
50
27.4
40.6
55
81
40-145
39 R1
Benzo(a)pyrene
ug/L
2.81-1
50
50
18.2
27.3
36
55
41-146
40 M1,R1
Benzo(b)fluoranthene
ug/L
2.61-1
50
50
18.1
26.9
36
54
39-151
39 M1,R1
Benzo(g,h,i)perylene
ug/L
2.81-1
50
50
19.1
28.8
38
58
40-147
40 M1,R1
Benzo(k)fluoranthene
ug/L
2.71-1
50
50
17.0
25.8
34
52
40-146
41 M1,R1
Benzyl alcohol
ug/L
2.91-1
100
100
43.1
65.9
43
66
25-130
42 R1
bis(2-Chloroethoxy)methane
ug/L
1.81-1
50
50
26.2
38.7
52
77
23-130
39 R1
bis(2-Chloroethyl) ether
ug/L
1.91-1
50
50
20.8
31.2
42
62
25-130
40 R1
bis(2-Ethylhexyl)phthalate
ug/L
3.71-1
50
50
31.2
45.1
59
87
28-166
36 R1
Butylbenzylphthalate
ug/L
3.1 U
50
50
29.7
44.4
59
89
33-165
40 R1
Chlorobenzilate
ug/L
3.81-1
50
50
29.6
49.2
59
98
55-170
50 R1
Chrysene
ug/L
2.81-1
50
50
27.1
39.7
54
79
38-141
38 R1
Di-n-butylphthalate
ug/L
2.21-1
50
50
30.1
43.1
60
86
32-153
36 R1
Di-n-octylphthalate
ug/L
3.91-1
50
50
27.1
40.7
54
81
30-175
40 R1
Diallate
ug/L
3.41-1
50
50
25.5
36.7
51
73
39-141
36 R1
Dibenz(a,h)anthracene
ug/L
3.01-1
50
50
19.6
30.2
39
60
39-148
42 R1
Dibenzofuran
ug/L
2.1 U
50
50
22.4
33.6
45
67
20-130
40 R1
Diethylphthalate
ug/L
2.01-1
50
50
28.0
39.9
56
80
28-142
35 R1
Dimethoate
ug/L
3.71-1
50
50
30.6
40.1
61
80
57-167
27
Dimethylphthalate
ug/L
2.1 U
50
50
26.2
37.6
52
75
26-136
36 R1
Diphenylamine
ug/L
3.01-1
50
50
27.4
38.2
55
76
38-132
33 R1
Disulfoton
ug/L
4.61-1
50
50
25.0
34.4
50
69
40-140
32 R1
Ethyl methanesulfonate
ug/L
3.01-1
50
50
21.3
31.8
43
64
38-134
40 R1
Famphur
ug/L
6.1 U
100
100
29.6
25.8
30
26
10-130
14 IH
Fluoranthene
ug/L
2.21-1
50
50
28.0
41.1
56
82
39-143
38 R1
Fluorene
ug/L
2.1U
50
50
24.0
36.0
48
72
24-132
40 R1
Hexachloro-1,3-butadiene
ug/L
1.81-1
50
50
13.8
20.6
28
41
10-130
39 R1
Hexachlorobenzene
ug/L
2.21-1
50
50
22.9
33.5
46
67
29-130
37 R1
Hexachlorocyclopentadiene
ug/L
1.61-1
50
50
11.1
12.2
22
24
10-130
9
Hexachloroethane
ug/L
1.41-1
50
50
13.8
19.8
28
40
10-130
36 R1
Hexachloropropene
ug/L
7.01-1
50
50
8.3J
11.7
17
23
10-130
Indeno(1,2,3-cd)pyrene
ug/L
2.91-1
50
50
19.0
28.5
38
57
39-148
40 M1,R1
Isodrin
ug/L
2.81-1
50
50
27.6
38.6
55
77
45-138
33 R1
Isophorone
ug/L
1.71-1
50
50
23.1
34.2
46
68
23-130
39 R1
Isosafrole
ug/L
2.51-1
50
50
20.3
29.7
41
59
25-130
38 R1
Kepone
ug/L
14.1 U
100
100
37.9
30.1
38
30
10-130
23
Methapyrilene
ug/L
17.01-1
50
50
49.3J
71.5
99
143
10-181
IH
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 47 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3558850
MS
35697686001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3558851
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Methyl methanesulfonate
ug/L
3.1U
50
50
18.8
27.1
38
54
31-130
37 R1
Methyl parathion
ug/L
3.71-1
50
50
34.7
45.2
69
90
53-197
26
N-Nitroso-di-n-butylamine
ug/L
8.71-1
50
50
26.4
40.3
53
81
28-130
42 R1
N-Nitroso-di-n-propylamine
ug/L
1.31-1
50
50
23.1
34.0
46
68
25-130
38 R1
N-Nitrosodiethylamine
ug/L
2.31-1
50
50
22.2
32.2
44
64
29-132
37 R1
N-Nitrosodimethylamine
ug/L
1.91-1
50
50
17.5
25.4
35
51
22-130
37 R1
N-Nitrosodiphenylamine
ug/L
3.01-1
50
50
27.4
38.2
55
76
26-134
33 R1
N-Nitrosomethylethylamine
ug/L
7.51-1
50
50
21.3
30.1
43
60
24-133
34 R1
N-Nitrosopiperidine
ug/L
2.51-1
50
50
22.6
32.3
45
65
29-141
35 R1
N-Nitrosopyrrolidine
ug/L
3.1 U
50
50
21.3
31.9
43
64
29-140
40 R1
Nitrobenzene
ug/L
1.91-1
50
50
21.1
31.3
42
63
25-130
39 R1
0,0,0-
ug/L
2.61-1
50
50
19.8
29.4
40
59
30-130
39 R1
Triethyl phosphorothioate
O-Toluidine
ug/L
3.1J
50
50
32.8
47.1
59
88
27-130
36 R1
P-Dimethylaminoazobenzene
ug/L
2.41-1
50
50
13.6
19.3
27
39
20-130
341L,R1
p-Phenylenediamine
ug/L
10.01-1
ND
ND
Parathion (Ethyl parathion)
ug/L
3.91-1
50
50
33.3
45.8
67
92
48-200
32 R1
Pentachlorobenzene
ug/L
3.41-1
50
50
20.3
30.0
41
60
23-130
39 R1
Pentachloronitrobenzene
ug/L
3.31-1
50
50
31.1
43.4
62
87
57-159
33 R1
Pentachlorophenol
ug/L
3.81-1
100
100
43.0
55.7
43
56
10-175
26
Phenacetin
ug/L
3.61-1
50
50
38.8
47.8
78
96
57-179
21
Phenanthrene
ug/L
2.01-1
50
50
26.6
37.8
53
76
36-133
35 R1
Phenol
ug/L
1.41-1
50
50
14.5
24.2
29
48
10-130
50 R1
Phorate
ug/L
3.61-1
50
50
25.7
35.8
51
72
21-192
33 R1
Pronamide
ug/L
3.1U
50
50
34.0
47.3
68
95
55-162
33 R1
Pyrene
ug/L
2.21-1
50
50
27.2
39.4
54
79
40-143
37 R1
Safrole
ug/L
2.31-1
50
50
19.5
29.9
39
60
25-130
42 R1
Thionazin
ug/L
2.91-1
50
50
32.4
48.1
65
96
50-157
39 R1
2,4,6-Tribromophenol (S)
%
58
84
10-144
2-Fluorobiphenyl (S)
%
37
56
10-130
2-Fluorophenol(S)
%
29
44
10-130
Nitrobenzene-d5 (S)
%
43
64
10-144
Phenol-d6 (S)
%
28
42
10-130
Terphenyl-d14(S)
%
49
73
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 48 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 680112 Analysis Method: EPA 120.1-1982
QC Batch Method: EPA 120.1-1982 Analysis Description: 120.1 Specific Conductance
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92589141001, 92589141005, 92589141006
METHOD BLANK: 3558377 Matrix: Water
Associated Lab Samples: 92589141001, 92589141005, 92589141006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Specific Conductance umhos/cm ND 10.0 02/23/22 11:16
LABORATORY CONTROL SAMPLE: 3558378
Spike LCS
Parameter Units Conc. Result
Specific Conductance umhos/cm 1410 1410
SAMPLE DUPLICATE: 3558379
92588085001 Dup
Parameter Units Result Result
Specific Conductance umhos/cm ND ND
SAMPLE DUPLICATE: 3558380
92589173003 Dup
Parameter Units Result Result
Specific Conductance umhos/cm 503 503
LCS % Rec
% Rec Limits Qualifiers
100 90-110
RPD Qualifiers
RPD Qualifiers
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 679567 Analysis Method: SM 2540C-2015
QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92589141001
METHOD BLANK: 3555767
Associated Lab Samples: 92589141001
Parameter
Units
Total Dissolved Solids
ug/L
LABORATORY CONTROL SAMPLE:
3555768
Parameter
Units
Total Dissolved Solids
ug/L
SAMPLE DUPLICATE: 3555769
Parameter
Units
Total Dissolved Solids
ug/L
SAMPLE DUPLICATE: 3555770
Parameter
Total Dissolved Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25000 02/20/2213:10
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250000 260000 104 90-110
92588387009 Dup
Result Result RPD Qualifiers
131 mg/L 129000 2
92588973001 Dup
Units Result Result
ug/L 98.0 mg/L 101000
RPD Qualifiers
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 99

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 679568 Analysis Method: SM 2540C-2015
QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92589141005, 92589141006
METHOD BLANK: 3555771 Matrix: Water
Associated Lab Samples: 92589141005, 92589141006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids ug/L ND 25000 02/20/22 13:17
LABORATORY CONTROL SAMPLE: 3555772
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids ug/L 250000 252000 101 90-110
SAMPLE DUPLICATE: 3555773
92588973011 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids ug/L 84.0 mg/L 90000 7
SAMPLE DUPLICATE: 3555774
92589115001 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids ug/L 163 mg/L 155000 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 679516 Analysis Method: SM 4500-S2D-2011
QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92589141002, 92589141003, 92589141005, 92589141006
METHOD BLANK: 3555616
Matrix:
Water
Associated Lab Samples: 92589141002, 92589141003, 92589141005, 92589141006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Sulfide
ug/L
ND
100
02/19/22 04:05
LABORATORY CONTROL SAMPLE:
3555617
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Sulfide
ug/L
500
512
102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3555618 3555619
MS MSD
92588963002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfide ug/L ND 500 500 498 530 99 105 80-120 6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3555620 3555621
MS MSD
92588963001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfide ug/L ND 500 500 484 486 97 97 80-120 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 52 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 679776 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92589141001, 92589141005, 92589141006
SAMPLE DUPLICATE: 3556711
92588244001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.9 6.8 0 H3
SAMPLE DUPLICATE: 3556712
92589141005 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.6 6.7 1 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 680471
Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993
Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92589141001, 92589141002,
92589141003, 92589141005, 92589141006
METHOD BLANK: 3560303
Matrix: Water
Associated Lab Samples: 92589141001, 92589141002,
92589141003, 92589141005, 92589141006
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chloride ug/L
ND 1000
02/24/22 07:19
Sulfate ug/L
ND 1000
02/24/22 07:19
LABORATORY CONTROL SAMPLE: 3560304
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Chloride ug/L
50000 50700
101 90-110
Sulfate ug/L
50000 49700
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3560305 3560306
MS MSD
92589141001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Chloride ug/L 68800
50000 50000 108000
106000 78 74
90-110 2 M1
Sulfate ug/L 8370
50000 50000 62500
62300 108 108
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3560307 3560308
MS MSD
92589586001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Chloride ug/L 45.7
50000 50000 98100
97000 105 103
90-110 1
mg/L
Sulfate ug/L 8.9
50000 50000 62600
61300 107 105
90-110 2
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 54 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 683933 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92589141001, 92589141005
METHOD BLANK: 3577260
Matrix:
Water
Associated Lab Samples: 92589141001, 92589141005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chloride
ug/L
ND
1000
03/10/22 21:06
LABORATORY CONTROL SAMPLE:
3577261
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Chloride
ug/L
20000
21000
105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3577262 3577263
MS MSD
92590742004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride ug/L 7.3 10000 10000 18000 18100 107 108 90-110 0
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3577264 3577265
MS MSD
92590742005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride ug/L 6.2 10000 10000 17300 16800 110 105 90-110 3
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 55 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
QC Batch: 680719 Analysis Method: SM 531 OB-2014
QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92589141002, 92589141003, 92589141005, 92589141006
METHOD BLANK: 3561131
Matrix:
Water
Associated Lab Samples: 92589141002, 92589141003, 92589141005, 92589141006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Organic Carbon
mg/L
ND
1.0
02/25/22 09:41
LABORATORY CONTROL SAMPLE:
3561132
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Organic Carbon
mg/L
25
24.1
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3561133 3561134
MS MSD
92589141005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L ND 25 25 25.0 25.2 99 99 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3561135 3561136
MS MSD
92589141006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 1.5 25 25 26.2 26.1 99 98 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 56 of 99

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
1g Re -extraction conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time
H3 Sample was received or analysis requested beyond the recognized method holding time.
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/24/2022 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
OXFORD COMPLIANCE
92589141
UNITS 1/2
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92589141002
3901-NES2S UNIT 1
HACH 10206
679301
92589141003
3901-NES21)
HACH 10206
679301
92589141005
3901-MW7 UNIT 1
HACH 10206
679301
92589141006
3901-MW5R
HACH 10206
679301
92589141005
3901-MW7 UNIT 1
EPA 3510C
680340
EPA 8081 B
681224
92589141006
3901-MW5R
EPA 3510C
680340
EPA 8081B
681224
92589141005
3901-MW7 UNIT 1
EPA 3510C
680708
EPA 8082A
681222
92589141006
3901-MW5R
EPA 3510C
680708
EPA 8082A
681222
92589141002
3901-NES2S UNIT 1
RSK 175 Modified
679501
92589141003
3901-NES213
RSK 175 Modified
679501
92589141005
3901-MW7 UNIT 1
RSK 175 Modified
679501
92589141006
3901-MW5R
RSK 175 Modified
679501
92589141001
3901-MW-4R
EPA 3010A
681459
EPA6010D
681665
92589141005
3901-MW7 UNIT 1
EPA 3010A
681459
EPA6010D
681665
92589141006
3901-MW5R
EPA 3010A
681459
EPA6010D
681665
92589141007
3901-MW7 UNIT 2
EPA 3010A
681459
EPA6010D
681665
92589141001
3901-MW-4R
EPA 3010A
680098
EPA 6020B
681086
92589141005
3901-MW7 UNIT 1
EPA 3010A
680098
EPA 6020B
681086
92589141006
3901-MW5R
EPA 3010A
680098
EPA 6020B
681086
92589141007
3901-MW7 UNIT 2
EPA 3010A
680098
EPA 6020B
681086
92589141001
3901-MW-4R
EPA 7470A
681648
EPA 7470A
682130
92589141005
3901-MW7 UNIT 1
EPA 7470A
681648
EPA 7470A
682130
92589141006
3901-MW5R
EPA 7470A
681648
EPA 7470A
682130
92589141005
3901-MW7 UNIT 1
EPA 3510C
680247
EPA 8270E
680584
92589141006
3901-MW5R
EPA 3510C
680247
EPA 8270E
680584
92589141001
3901-MW-4R
EPA 8260D
679682
92589141002
3901-NES2S UNIT 1
EPA 8260D
679682
92589141003
3901-NES21)
EPA 8260D
679682
92589141004
3901-NES2S UNIT 2
EPA 8260D
679682
92589141005
3901-MW7 UNIT 1
EPA 8260D
679682
92589141006
3901-MW5R
EPA 8260D
679682
92589141007
3901-MW7 UNIT 2
EPA 8260D
679682
92589141008
3901-TRIP BLANK 03
EPA 8260D
679682
92589141001
3901-MW-4R
EPA 8260D Mod.
679789
92589141002
3901-NES2S UNIT 1
EPA 8260D Mod.
679789
92589141003
3901-NES213
EPA 8260D Mod.
679789
92589141004
3901-NES2S UNIT 2
EPA 8260D Mod.
679789
92589141005
3901-MW7 UNIT 1
EPA 8260D Mod.
679789
92589141006
3901-MW5R
EPA 8260D Mod.
679789
92589141007
3901-MW7 UNIT 2
EPA 8260D Mod.
679789
92589141008
3901-TRIP BLANK 03
EPA 8260D Mod.
679789
92589141001
3901-MW-4R
EPA 120.1-1982
680112
92589141005
3901-MW7 UNIT 1
EPA 120.1-1982
680112
92589141006
3901-MW5R
EPA 120.1-1982
680112
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 03/24/2022 06:11 PM
without the written consent of Pace Analytical Services, LLC.
Page 58 of 99

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: OXFORD COMPLIANCE UNITS 1/2
Pace Project No.: 92589141
Lab ID
Sample ID
QC Batch Method
QC Batch
92589141001
3901-MW-4R
SM 254OC-2015
679567
92589141005
3901-MW7 UNIT 1
SM 2540C-2015
679568
92589141006
3901-MW5R
SM 2540C-2015
679568
92589141002
3901-NES2S UNIT 1
SM 4500-S2D-2011
679516
92589141003
3901-NES213
SM 4500-S2D-2011
679516
92589141005
3901-MW7 UNIT 1
SM 4500-S2D-2011
679516
92589141006
3901-MW5R
SM 4500-S2D-2011
679516
92589141001
3901-MW-4R
EPA 9040C
679776
92589141005
3901-MW7 UNIT 1
EPA9040C
679776
92589141006
3901-MW5R
EPA9040C
679776
92589141001
3901-MW-4R
EPA 300.0 Rev 2.1 1993
680471
92589141002
3901-NES2S UNIT 1
EPA 300.0 Rev 2.1 1993
680471
92589141003
3901-NES213
EPA 300.0 Rev 2.1 1993
680471
92589141005
3901-MW7 UNIT 1
EPA 300.0 Rev 2.1 1993
680471
92589141006
3901-MW5R
EPA 300.0 Rev 2.1 1993
680471
92589141001
3901-MW-4R
SM 4500-CI-E-2011
683933
92589141005
3901-MW7 UNIT 1
SM 4500-CI-E-2011
683933
92589141002
3901-NES2S UNIT 1
SM 5310E-2014
680719
92589141003
3901-NES213
SM 531OB-2014
680719
92589141005
3901-MW7 UNIT 1
SM 5310E-2014
680719
92589141006
3901-MW5R
SM 531OB-2014
680719
Date: 03/24/2022 06:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 59 of 99

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N

�'
�CeARB�ytICa1 ,
Document Name:
Sample Condition Upon Receipt (SOUR)
Document Revised: November 15, 2021
Page 2 of 2
Document No.:
F-CAR-CS-033-Rev.08
Issuing Authority:
Pace Carolinas Quality office
*Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
Project a WO#: 928'589141
PM: AI18 Due Date: 03/03/22
CLIENT: 92—Garrett
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Note: Whenever there is a clMrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification office (Le,
out of hold, incorrect preservative, out of temp, incorrect containers,
Page 61 of 99

ANALYTICAL ENVIRONMENTAL SERVICES, INC.
AES
February 28, 2022
Angela Baioni
Pace Analytical
9800 Kincey Ave Suite 100
Huntersville NC 28078-8400
RE: 92589141
Dear Angela Baioni: Order No: 2202P36
Analytical Environmental Services, Inc. received 2 samples on 2/22/2022 7:50:00 AM
for the analyses presented in following report.
"No problems were encountered during the analyses except as noted in the Case Narrative or by qualifiers in
the report or QC Summary. Additionally, all results for the associated Quality Control samples were within
EPA and/or AES established limits.
AES' certifications are as follows:
-NELAP/Florida State Laboratory ID E87582 for analysis of Non -Potable Water, Solid & Chemical Materials,
Air & Emissions for Organics, and Drinking Water Microbiology & Metals, effective 07/01/21-06/30/22.
-North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent, effective until
12/31/22.
-South Carolina Environmental Laboratory Certification number 98016003 effective until 6/30/22.
These results relate only to the items tested as received. This report may only be reproduced in full and with
written permission from the laboratory.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
Vag IACLOntA,
Paris Masoudi
Project Manager
3080 Presi4ential Drive • Atlanta, Georgia 30340 -Tel: 770.457,8177 • Fax: 770.457_S188 • Toll P.,e:800.972.4889
www.aesatlanta.com
Page 62 of 99
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Analytical Environmental Services, Inc
Date: 28-Feb-22
Client:
Pace Analytical
Client Sample ID:
3901-MW7 UNIT 1
Project Name:
92589141
Collection Date:
2/17/2022 9:35:00 AM
Lab ID:
2202P36-001
Matrix:
Aqueous
Analyses
Result
Reporting
Qual
Limit
Units
BatcbID
Dilution
Factor
Date Analyzed Analyst
CHLORINATED HERBICIDES, APPENDIX II LIST SW8151A
(SW35100
2,4,5-T
BRL
2.0
ug/L
331471
1
02/25/2022 20:01
UH
2,4,5-TP (Silvex)
BRL
2.0
ug/L
331471
1
02/25/2022 20:01
UH
2,4-D
BRL
2.0
ug/L
331471
1
02/25/2022 20:01
UH
Dinoseb
BRL
5.0
ug/L
331471
1
02/25/2022 20:01
UH
Pentachlorophenol
BRL
1.0
ug/L
331471
1
02/25/2022 20:01
UH
Surr: DCAA
87.8
47-120
%REC
331471
1
02/25/2022 20:01
UH
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitation range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
Page 64 of 99
Page 3 of 9

Analytical Environmental Services, Inc
Date: 28-Feb-22
Client:
Pace Analytical
Client Sample ID:
3901-MW5R
Project Name:
92589141
Collection Date:
2/17/2022 11:48:00 AM
Lab ID:
2202P36-002
Matrix:
Aqueous
Analyses
Result
Reporting
Qual
Limit
Units
BatcbID
Dilution
Factor
Date Analyzed Analyst
CHLORINATED HERBICIDES, APPENDIX II LIST SW8151A
(SW3510C)
2,4,5-T
BRL
2.0
ug/L
331471
1
02/25/2022 20:21
UH
2,4,5-TP (Silvex)
BRL
2.0
ug/L
331471
1
02/25/2022 20:21
UH
2,4-D
BRL
2.0
ug/L
331471
1
02/25/2022 20:21
UH
Dinoseb
BRL
5.0
ug/L
331471
1
02/25/2022 20:21
UH
Pentachlorophenol
BRL
1.0
ug/L
331471
1
02/25/2022 20:21
UH
Surr: DCAA
58.3
47-120
%REC
331471
1
02/25/2022 20:21
UH
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiitation range)
S Spike Recovery outside limits due to matrix
Nan See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
Page 65 of 99
Page 4 of 9

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Analytical Environmental Services, Inc
Date: 28-Feb-22
Client: Pace Analytical
Project Name: 92589141 Dates Report
Lab Order: 2202P36
Lab Sample ID
Client Sample ID
Collection Date
Matrix
Test Name TCLP Date
Prep Date
Analysis Date
2202P36-001A
3901-MW7 UNIT 1
2/17/2022 9:35:OOAM
Aqueous
CHLORINATED HERBICIDES, APPENDI;
2/24/2022 9:23:11AM
02/25/2022
2202P36-002A
3901-MW5R
2/17/2022 11:48:OOAM
Aqueous
CHLORINATED HERBICIDES, APPENDI:
2/24/2022 9:23:11AM
02/25/2022
Page 67 of 99
Page 6 of 9

Analytical Environmental Services, Inc
Client:
Pace Analytical
Project Name:
92589141
Workorder:
2202P36
Date: 28-Feb-22
ANALYTICAL QC SUMMARY REPORT
BatchID: 331471
Sample ID: MB-331471
Client ID:
Units: ug/L
Prep Date: 02/24/2022
Run No: 478687
SampleType: MBLK
TestCode:
CHLORINATED HERBICIDES, APPENDIX II LIST SW8151A BatchID: 331471
Analysis Date: 02/25/2022
Seq No: 11063113
Analyte
Result
RPT Limit SPK value SPK Ref Val %REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-T
BRL
2.0
2,4,5-TP (Silvex)
BRL
2.0
2,4-D
BRL
2.0
Dinoseb
BRL
5.0
Pentachlorophenol
BRL
1.0
Surr: DCAA
2.373
0 5.000 47.5 47 120
Sample ID: LCS-331471
Client ID:
Units: ug/L
Prep Date: 02/24/2022
Run No: 478687
SampleType: LCS
TestCode:
CHLORINATED HERBICIDES, APPENDIX II LIST SW8151A BatchID: 331471
Analysis Date: 02/25/2022
Seq No: 11063114
Analyte
Result
RPT Limit SPK value SPK Ref Val %REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-T
3.755
2.0
5.000
75.1
50.1
120
2,4,5-TP (Silvex)
3.861
2.0
5.000
77.2
50.2
120
2,4-D
3.664
2.0
5.000
73.3
50.1
120
Surr: DCAA
4.650
0
5.000
93.0
47
120
Sample ID: 2202P03-005EMS
Client ID:
Units: ug/L
Prep Date: 02/24/2022
Run No: 478687
SampleType: MS
TestCode:
CHLORINATED HERBICIDES, APPENDIX II LIST SW8151A BatchlD: 331471
Analysis Date: 02/25/2022
Seq No: 11063115
Analyte
Result
RPT Limit SPK value SPK Ref Val %REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-T
3.745
2.0
5.000
74.9
44.9
120
2,4,5-TP (Silvex)
3.846
2.0
5.000
76.9
45.2
120
2,4-D
3.675
2.0
5.000
73.5
40
120
Surr: DCAA
4.387
0
5.000
87.7
47
120
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 68 of 99
Page 7 of 9

Analytical Environmental Services, Inc
Client:
Pace Analytical
Project Name:
92589141
Workorder:
2202P36
Date: 28-Feb-22
ANALYTICAL QC SUMMARY REPORT
BatchID: 331471
Sample ID: 2202P03-005EMSD
Client ID:
Units: ug/L
Prep Date: 02/24/2022
Run No: 478687
SampleType: MSD
TestCode:
CHLORINATED HERBICIDES, APPENDIX II LIST SW8151A BatchID: 331471
Analysis Date: 02/25/2022
Seq No: 11063116
Analyte
Result
RPT Limit SPK value SPK Ref Val %REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-T
4.139
2.0
5.000
82.8
44.9
120
3.745
9.99
24
2,4,5-TP (Silvex)
4.247
2.0
5.000
84.9
45.2
120
3.846
9.92
18.9
2,4-D
4.368
2.0
5.000
87.4
40
120
3.675
17.2
20.7
Surr: DCAA
4.658
0
5.000
93.2
47
120
4.387
0
0
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 69 of 99
Page 8 of 9

End of Report
Page 70 of 99
Page 9 of 9

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
March 14, 2022
Angela Baioni
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: Oxford Compliance Units 1/2
Client Job Number:
Project Number: 92589141
Laboratory Work Order Number: 22C0325
Enclosed are results of analyses for samples as received by the laboratory on March 4, 2022. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Raymond J. McCarthy
Project Manager
STT3Li6SLL

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
22CO325-01
22CO325-02
22CO325-03
22CO325-04
22CO325-05
Sample Preparation Information
QC Data
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
B302607
B303120
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
5
5
6
7
8
9
10
11
11
11
11
12
13
14
STT WA*Awa L
• . • • •

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100 REPORT DATE: 3/14/2022
Huntersville, NC 28078 PURCHASE ORDER NUMBER:
ATTN: Angela Baioni
PROJECT NUMBER: 92589141
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 22C0325
The results of analyses performed on the following samples submitted to CON -TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION: Oxford Compliance Units 1/2
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
3901-MW-4R
22C0325-01
Water
SM21-23 2320B
3901-NES2S UNIT 1
22C0325-02
Water
SM21-23 2320B
3901-NES21)
22C0325-03
Water
SM21-23 2320B
3901-MW7 UNIT 1
22C0325-04
Water
SM21-23 2320B
3901-MW5R
22C0325-05
Water
SM21-23 2320B
Page 3 of 16

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
Qualifications:
H-03
Sample received after recommended holding time was exceeded.
SM21-23 2320B
Analyte & Samples(s) Qualified:
Alkalinity
22C0325-01[3901-MW-4R], 22C0325-02[3901-NES2S UNIT 11, 22C0325-03[3901-NES2D], 22C0325-04[3901-MW7 UNIT 11, 22C0325-05[3901-MW5R]
PR-18
Headspace present in sample container.
Analyte & Samples(s) Qualified:
Alkalinity
22C0325-01 [3901-MW-4R], 22C0325-02[3901-NES2S UNIT 1], 22C0325-03[3901-NES2D], 22C0325-04[3901-MW7 UNIT 1]
The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
d�
Lisa A. Worthington
Technical Representative
�ST.TS 331161
a

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Oxford Compliance Units 1/2 Sample Description: Work Order: 22C0325
Date Received: 3/4/2022
Field Sample #: 3901-MW-4R Sampled: 2/16/2022 12:00
Sample ID: 22C0325-01
Sample Matrix: Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Alkalinity 310 1.0 0.65 mg/L 1 H-03, PR-18 SM21-23 2320B 3/7/22 3/7/22 14:53 IS
Page 5 of 16

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Oxford Compliance Units 1/2 Sample Description: Work Order: 22C0325
Date Received: 3/4/2022
Field Sample #: 3901-NES2S UNIT 1 Sampled: 2/17/2022 10:05
Sample ID: 22C0325-02
Sample Matrix: Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Alkalinity 69 1.0 0.65 mg/L 1 H-03, PR-18 SM21-23 2320B 3/7/22 3/7/22 15:02 IS
Page 6 of 16

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Oxford Compliance Units 1/2 Sample Description: Work Order: 22C0325
Date Received: 3/4/2022
Field Sample #: 3901-NES2D Sampled: 2/17/2022 11:42
Sample ID: 22C0325-03
Sample Matrix: Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Alkalinity 170 1.0 0.65 mg/L 1 H-03, PR-18 SM21-23 2320B 3/7/22 3/7/22 15:17 IS
Page 7 of 16

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Oxford Compliance Units 1/2 Sample Description: Work Order: 22C0325
Date Received: 3/4/2022
Field Sample #: 3901-MW7 UNIT 1 Sampled: 2/17/2022 09:35
Sample ID: 22C0325-04
Sample Matrix: Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Alkalinity 150 1.0 0.65 mg/L 1 H-03, PR-18 SM21-23 2320B 3/7/22 3/7/22 15:26 IS
Page 8 of 16

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: Oxford Compliance Units 1/2 Sample Description: Work Order: 22C0325
Date Received: 3/4/2022
Field Sample #: 3901-MW5R Sampled: 2/17/2022 11:48
Sample ID: 22C0325-05
Sample Matrix: Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Alkalinity 190 1.0 0.65 mg/L 1 H-03 SM21-23 2320B 3/14/22 3/14/22 9:34 IS
Page 9 of 16

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Sample Extraction Data
SM21-23 2320B
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
22CO325-01[3901-MW-4R]
B302607
100
100
03/07/22
22CO325-02 [3901-NES2S UNIT 1]
B302607
100
100
03/07/22
22CO325-03[3901-NES2D]
B302607
100
100
03/07/22
22CO325-04 [3901-MW7 UNIT 1]
B302607
100
100
03/07/22
SM21-23 2320B
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
22CO325-05[3901-MW5R]
B303120
100
100
03/14/22
Page 10 of 16

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B302607 - SM21-23 2320B
Blank (B302607-BLK1)
Prepared & Analyzed: 03/07/22
Alkalinity
LCS (B302607-BSI)
ND
1.0
mg/L
Prepared & Analyzed: 03/07/22
Alkalinity
LCS Dup (B302607-BSD1)
30
1.0
mg/L
32.5 92.3 90-110
Prepared & Analyzed: 03/07/22
Alkalinity
Batch B303120 - SM21-23 2320B
30
1.0
mg/L
32.5 92.3 90-110 0.00 5.47
Blank (B303120-BLK1)
Prepared & Analyzed: 03/14/22
Alkalinity
LCS (B303120-BS1)
ND
1.0
mg/L
Prepared & Analyzed: 03/14/22
Alkalinity
LCS Dup (B303120-BSD1)
30
1.0
mg/L
32.5 92.3 90-110
Prepared & Analyzed: 03/14/22
Alkalinity
30
1.0
mg/L
32.5 92.3 90-110 0.00 5.47
Page 11 of 16

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
FLAG/QUALIFIER SUMMARY
* QC result is outside of established limits.
j Wide recovery limits established for difficult compound.
$ Wide RPD limits established for difficult compound.
# Data exceeded client recommended or regulatory level
ND Not Detected
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
H-03 Sample received after recommended holding time was exceeded.
PR-18 Headspace present in sample container.
ST.T3A►l.SLL

con -test®
A Pace Analytical Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SM21-23 2320B in Water
Alkalinity CT,MA,NH,NY,RI,NC,ME,VA
Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditation:
Code Description Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2017
100033
03/l/2024
MA
Massachusetts DEP
M-MA100
06/30/2022
CT
Connecticut Department of Publilc Health
PH-0165
12/31/2022
NY
New York State Department of Health
10899 NELAP
04/l/2022
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2023
RI
Rhode Island Department of Health
LA000373
12/30/2022
NC
North Carolina Div. of Water Quality
652
12/31/2022
NJ
New Jersey DEP
MA007 NELAP
06/30/2022
FL
Florida Department of Health
E871027 NELAP
06/30/2022
VT
Vermont Department of Health Lead Laboratory
LL720741
07/30/2022
ME
State of Maine
MA00100
06/9/2023
VA
Commonwealth of Virginia
460217
12/14/2022
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2022
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2022
NC-DW
North Carolina Department of Health
25703
07/31/2022
PA
Commonwealth of Pennsylvania DEP
68-05812
06/30/2022
MI
Dept. of Env, Great Lakes, and Energy
9100
09/6/2022
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Table of Contents
FedEx� Tracking
546528651536
ADD NICKNAME
Delivered
Friday, March 4, 2022 at 9:01 am
DELIVERED
Signed for by: R.REBECCA
GET STATUS UPDATES
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ST.T3_L'�SLL

Table of Contents
I Have Not Confirmed Sample Container
Numbers With Lab Staff Before Relinquishing
Over Samples
s
CC), n do= tq-. -go Ir
AI�dAI.'VitCAL LABC3i=tA"1"ORY
Doc#;277 :Rev 5 2Q.1.7
Login Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client CLz {
Received By f y= Date Time < 1
How were the samples In Cooler No Cooler On ice j No Ice
received? Direct from Sampling Ambient Melted Ice
Were samples within
By Gun # _ Actual Temp -- S
Temperature? 2-6°C -
By Blank #
Actual Temp -
Was Custody Seal Intact?
IF
Were Samples Tampered with? ('
Was COC Relinquished ?
-
Does Chain Agree With Samples?
Are there broken/leaking/loose caps on any samples?
Is COC in ink/ Legible? -
Were samples received within holding time?
Did COC include all Client
�.
Analysis f Sampler Name
pertinent Information? Project
ID`s -, Collection Dates/Times
Are Sample labels filled out and legible?
Are there Lab to Filters?
Who was notified?
Are there Rushes?
Who was notified?
Are there Short Holds?
Who was notified?
Is there enough Volume?
�---
Is there Headspace where applicable?
,!
MS/MSD?
Proper Media/Containers used?
Is splitting samples required?
Were trip blanks received?
�
On COC? _
Do all samples have the proper pH?
NI J
Acid Base
Lin -
1 Liter Amb.
1 Liter Plastic
16 oz Amb.
HCL-
500 mL Amb.
500 mL Plastic
8oz Amb/Clear
Meoh-
250 mL Amb.
250 mL Plastic
4oz Amb/Clear
Bisulfate-
Flashpoint
Col./Bacteria
2oz Amb/Clear
DI-
Other Glass
Other Plastic
Encore
Thiosulfate-
SOC Kit
Plastic Bag
Frozen:
Suifuric-
I
I Perchlorate
ZlDlock
Unp-
1 Liter Amb.
1 Liter Plastic
16 oz Amb.
HCL-
500 mL Amb.
500 mL Plastic
8oz Amb/Clear
Meoh-
250 mL Amb.
260 mL Plastic
4oz Amb/Clear
Bisulfate-
Col./Bacteria
Flash pint
2oz AmblClear
DI-
Other Plastic
Other Glass
Encore
lThiosulfate-I
I SOC Kit
I
Plastic Bag
I
JFrozen:
Page 16 of 16 1

aceAna lytical
LELAP CERTIFICATE NUMBER: 01955
DOD-ELAP ACCREDITATION NUMBER: 74960
ANALYTICAL RESULTS
•:I
Pace Analytical Gulf Coast
7979 Innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 03/04/2022
Report Y 222022255
�1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i III
Project 92589141 Oxford Compliance
Samples Collected 2/17/22
Deliver To Additional Recipients
Angela Baioni Vivian Sipe, Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
9800 Kincey Ave
Suite 100
Huntersville, NC 28078
[phone]
PJLA
1" ing
DOD ELAF
Pages 87 of qA
Pace Gulf Coast Report#: 222022255 Page 1 of 13

Report#: 222022255
aceAnarytical
Project ID: 92589141 Oxford Compliance Report Date: 03/04/2022
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
" Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis — when appended to Client Sample ID
Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
Pace Gulf Coast Report 222022255
Papa 89 of qA
Pace Gulf Coast Report#: 222022255 Page 2 of 13

aceAnarytical Report#: 222022255
Project ID: 92589141 Oxford Compliance Report Date: 03/04/2022
Certifications
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
PaQa Rq of qA
Pace Gulf Coast Report#: 222022255 Page 3 of 13

Report#: 222022255
aceAnarytical
Project ID: 92589141 Oxford Compliance Report Date: 03/04/2022
Case Narrative
Client: Pace Analytical Services Report: 222022255
Pace Analytical Gulf Coast received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
PaQa qQ of qq
Pace Gulf Coast Report#: 222022255 Page 4 of 13

1 2.AruOical
Report#: 222022255
Project ID: 92589141 Oxford Compliance Report Date: 03/04/2022
Sample Summary
Lab ID Client ID Matrix Collect Date Receive Date
22202225501
3901-NES2S UNIT 1
22202225502
3901-NES21D
22202225503
3901-MW7 UNIT 1
22202225504
2901-MW5R
22202225505
3901-NES2S UNIT 1
22202225506
3901-NES2S
22202225507
3901-MW7 UNIT 1
22202225508
3901-MW5R
Water
2/17/2210:05
2/22/22 10:00
Water
2/17/2211:42
2/22/22 10:00
Water
2/17/22 09:35
2/22/22 10:00
Water
2/17/2211:48
2/22/22 10:00
Bubble Strip
2/17/22 10:05
2/22/22 10:00
Bubble Strip
2/17/22 11:42
2/22/22 10:00
Bubble Strip
2/17/22 09:35
2/22/22 10:00
Bubble Strip
2/17/22 11:48
2/22/22 10:00
PaQa q1 of qq
Pace Gulf Coast Report#: 222022255 Page 5 of 13

Report#:
222022255
aceAnarytical
Project ID:
92589141 Oxford Compliance
Report
Date: 03/04/2022
Detect Summary
Results and Detection Limits are adjusted for dilution and
moisture when applicable
AM23G
Lab ID
Client ID
Parameter
Units
Result
Dil.
%Moist
22202225501
3901-NES2S UNIT 1
Acetic Acid
mg/L
0.16J
1
NA
22202225501
3901-NES2S UNIT 1
Formic Acid
mg/L
4.5
1
NA
22202225501
3901-NES2S UNIT 1
Hexanoic Acid
mg/L
0.12J
1
NA
22202225501
3901-NES2S UNIT 1
Lactic Acid
mg/L
0.48J
1
NA
22202225502
3901-NES2D
Formic Acid
mg/L
0.42J
1
NA
22202225502
3901-NES2D
Lactic Acid
mg/L
0.16J
1
NA
22202225503
3901-MW7 UNIT 1
Acetic Acid
mg/L
0.28J
1
NA
22202225503
3901-MW7 UNIT 1
Formic Acid
mg/L
4.8
1
NA
22202225503
3901-MW7 UNIT 1
Hexanoic Acid
mg/L
0.078J
1
NA
22202225503
3901-MW7 UNIT 1
Lactic Acid
mg/L
1.7
1
NA
22202225504
2901-MW5R
Formic Acid
mg/L
1.3
1
NA
22202225504
2901-MW5R
Lactic Acid
mg/L
0.16J
1
NA
AM20GAX
Lab ID
Client ID
Parameter
Units
Result
Dil.
%Moist
22202225505
3901-NES2S UNIT 1
Hydrogen
nM
0.72J
1
NA
22202225506
3901-NES2S
Hydrogen
nM
1.3J
1
NA
22202225507
3901-MW7 UNIT 1
Hydrogen
nM
1.6J
1
NA
22202225508
3901-MW5R
Hydrogen
nM
1.2J
1
NA
PaQa q? of qq
Pace Gulf Coast Report#: 222022255 Page 6 of 13

Report#: 222022255
aceAr�alytrca!
Project ID: 92589141 Oxford Compliance Report Date: 03/04/2022
Sample Results
3901-N ES2S U NIT 1 Collect Date 02/17/2022 10:05 Lab ID 22202225501
Receive Date 02/22/2022 10:00 Matrix Water
23G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 02/28/2217:14 734787 SLL2 NA
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.16J
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
4.5
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.12J
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.48J
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
3901-NES213 Collect Date 02/17/2022 11:42 Lab ID 22202225502
Receive Date 02/22/2022 10:00 Matrix Water
23G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 03/02/2218:35 735017 SLL2 NA
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.12U
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
0.42J
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.16J
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
3901-MW7 UNIT 1 Collect Date 02/17/2022 09:35 Lab ID 22202225503
Receive Date 02/22/2022 10:00 Matrix Water
23G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 03/03/22 09:55 735017 SLL2 NA
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.28J
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
4.8
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.078J
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
PaQa q'i of qq
Pace Gulf Coast Report#: 222022255 Page 7 of 13

aceAnalytica! Report#: 222022255
Project ID: 92589141 Oxford Compliance Report Date: 03/04/2022
Sample Results
3901-MW7 UNIT 1 Collect Date 02/17/2022 09:35 Lab ID 22202225503
Receive Date 02/22/2022 10:00 Matrix Water
3G (Continued)
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 03/03/22 09:55 735017 SLL2 NA
CAS#
Parameter
Result
DL
LOQ
Units
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
1.7
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
2901-MW5R Collect Date 02/17/2022 11:48 Lab ID 22202225504
Receive Date 02/22/2022 10:00 Matrix Water
3G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 03/03/2210:16 735017 SLL2 NA
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.12U
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
1.3
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.16J
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
3901-N ES2S U NIT 1 Collect Date 02/17/2022 10:05 Lab ID 22202225505
Receive Date 02/22/2022 10:00 Matrix Bubble Strip
OGAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 03/03/2215:12 735189 CWB NA
CAS# Parameter
1333-74-0 Hydrogen
Result DL LOQ
0.72J 0.49 1.9
Units
nM
Pages q4 of qq
Pace Gulf Coast Report#: 222022255 Page 8 of 13

Report#: 222022255
aceAr�alytrca!
Project ID: 92589141 Oxford Compliance Report Date: 03/04/2022
Sample Results
3901-NES2S Collect Date 02/17/2022 11:42 Lab ID 22202225506
Receive Date 02/22/2022 10:00 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 03/03/2215:25 735189 CWB NA
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
1.3J
0.49
1.9
nM
3901-MW7 UNIT 1 Collect Date 02/17/2022 09:35 Lab ID 22202225507
Receive Date 02/22/2022 10:00 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 03/03/2215:38 735189 CWB NA
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
1.6J
0.49
1.9
nM
3901-MW5R Collect Date 02/17/2022 11:48 Lab ID 22202225508
Receive Date 02/22/2022 10:00 Matrix Bubble Strip
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 03/03/2215:50 735189 CWB NA
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
1.2J
0.49
1.9
nM
PaQa q5 of qq
Pace Gulf Coast Report#: 222022255 Page 9 of 13

aceAnalytica! Report#: 222022255
Project ID: 92589141 Oxford Compliance Report Date: 03/04/2022
General Chemistry QC Summary
Analytical Batch Client ID
MB734787
LCS734787
LCSD734787
734787 Lab ID
2312586
2312587
2312588
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
02/28/22 10:04
02/28/22 09:42
03/01/22 13:12
Matrix
Water
Water
Water
AM23G
Units
mg/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Acetic Acid
64-19-7
0.12U
0.12
2.0
1.8
88
70 - 130
2.0
1.9
94
7
20
Butyric Acid
107-92-6
0.058U
0.058
2.0
1.8
89
70 - 130
2.0
1.8
90
2
20
Formic Acid
64-18-6
0.055U
0.055
2.0
1.7
84
70 - 130
2.0
1.7
83
1
20
Hexanoic Acid
142-62-1
0.058U
0.058
2.0
1.8
88
70 - 130
2.0
1.9
97
10
20
i-Hexanoic Acid
646-07-1
0.056U
0.056
2.0
2.4
122
70 - 130
2.0
2.5
124
2
20
i-Pentanoic Acid
503-74-2
0.061 U
0.061
2.0
1.9
96
70 - 130
2.0
2.0
98
2
20
Lactic Acid
50-21-5
0.053U
0.053
2.0
2.6
128
70 - 130
2.0
2.4
123
4
20
Pentanoic Acid
109-52-4
0.056U
0.056
2.0
1.9
95
70 - 130
2.0
2.0
100
5
20
Propionic Acid
79-09-4
0.053U
0.053
2.0
1.8
90
70 - 130
2.0
1.8
92
3
20
Pyruvic Acid
127-17-3
0.060U
0.060
2.0
1.7
85
70 - 130
2.0
1.8
89
4
20
Analytical Batch Client ID
MB735017
LCS735017
LCSD735017
735017 Lab ID
2313816
2313817
2313818
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
03/02/22 17:30
03/02/22 17:09
03/03/22 14:55
Matrix
Water
Water
Water
AM23G
Units
mg/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Acetic Acid
64-19-7
0.12U
0.12
2.0
1.9
95
70 - 130
2.0
1.8
90
5
20
Butyric Acid
107-92-6
0.058U
0.058
2.0
1.8
92
70 - 130
2.0
1.7
86
7
20
Formic Acid
64-18-6
0.055U
0.055
2.0
1.6
81
70 - 130
2.0
1.6
80
1
20
Hexanoic Acid
142-62-1
0.058U
0.058
2.0
1.8
93
70 - 130
2.0
1.8
91
2
20
i-Hexanoic Acid
646-07-1
0.056U
0.056
2.0
2.5
126
70 - 130
2.0
2.4
119
6
20
i-Pentanoic Acid
503-74-2
0.061 U
0.061
2.0
1.9
97
70 - 130
2.0
1.9
97
0
20
Lactic Acid
50-21-5
0.053U
0.053
2.0
2.5
127
70 - 130
2.0
2.4
122
4
20
Pentanoic Acid
109-52-4
0.056U
0.056
2.0
2.0
99
70 - 130
2.0
2.0
100
0
20
Propionic Acid
79-09-4
0.053U
0.053
2.0
1.8
91
70 - 130
2.0
1.8
92
1
20
Pyruvic Acid
127-17-3
0.060U
0.060
2.0
1.8
88
70 - 130
2.0
1.8
92
4
20
PaQa qR of qq
Pace Gulf Coast Report#: 222022255 Page 10 of 13

aceAnalytica! Report#: 222022255
Project ID: 92589141 Oxford Compliance Report Date: 03/04/2022
General Chromatography QC Summary
Analytical Batch Client ID
MB735189
LCS735189
LCSD735189
735189 Lab ID
2314705
2314706
2314707
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
03/03/22 14:48
03/03/22 14:22
03/03/22 14:36
Matrix
Bubble Strip
Bubble Strip
Bubble Strip
AM20GAX
Units
nM
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Hydrogen 1333-74-0
0.49U
1 0.491
121
101
87
1 70 - 130
1 121
10189
1 1
1 20
Pages W of qA
Pace Gulf Coast Report#: 222022255 Page 11 of 13

Internal Transfer Chain of Custody
II iii I II I I II I I I I I II I IIII
❑ Samples Pre -Logged into eCOC
1A/,...i ,J,... Al.. m... nvrnDn rInnn DI IAAIr`F I InIITC 1/9
State Of Origin: NC
Cert. Needed: ❑ Yes
nwnar QACaivPd natP-
aceAnalytical `.'
www.pacelabs.com
❑ No
2/17/2n22 Results Requested Bv: 3/3/2022
Report To Subcontract To
Requested
Analysis
Angela Baioni Pace Gulf Coast
Pace Analytical Charlotte 7979 Innovation Park Dr
9800 KinceyAve. Suite 100 Baton Rouge, LA 70820
Huntersville, NC 28078 Phone [phone]
Phone[phone]
a
0
a
L
v
LL
�
Preserved Containers
N
0
i
2
Sample
Collect
d
o
Item
Sample ID
Type
Daterrime
Lab ID
Matrix
LAB USE ONLY
1
3901-NES2S UNIT 1
PS
2/17/2022 10:05
92589141002
Water
1
1
X
X
i
2
3901-NES2D
PS
2/171202211:42
92589141003
Water
1
1
X
X
2
3
3901-MW7 UNIT 1
PS
2/17/2022 09:35
92589141005
Water
1
1
X
X
3
4
3901-MW5R
PS
2/17/202211:48
92589141006
Water
1
1
44—
T
X
5
Comments
Transfers
Rele ed By
Date/Time
Received By
Date/Time
23 3e3�
1
.. w
s
ed�c
_� a
Irj
z Zz 0
y
3
Cooler Temperature on Receipt °C Custody Seal Y or N Received on Ice Y or N
samples Intact Y or N
***In order to maintain client confidentiality, location/name of the sampling site, samplers name and signature may not be provided on this COC document.
This chain of custody is considered complete as is since this information is available in the owner laboratory.
q 875 y-S'tl 2� b
Monday. February 21, 2022 11:14:32 AM
no i Ce
Client ID: 4367 - Pace Analytical Services
SDG: 222022255
PM: RWe III III
PaQa qR of qA
Pace Gulf Coast Report#: 222022255 Page 12 of 13

(��-aceAnalyfical'SAMPLE RECEIVING CHECKLIST IIIIIIIIIIIII III
SAMPLE DELIVERY GROUP
222022255
CHECKLIST
YES
NO
Client PM RWe
Transport Method
Samples received with proper thermal preservation?
*❑
❑
4367 - Pace Analytical Services
F®DC
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
*❑
*❑
❑
❑
Profile Number
Received By
282148
Fbberts, George S.
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
0
0
❑
❑
Line Item(s)
Receive Date(s)
10 - IVY, 002, VFA
02/22/22
11 - Hydrogen
Preservative added to any containers?
❑
�I❑
If received, was headspace for VOC water containers < 6mm?
*❑
❑
Samples collected in containers provided by Pace Gulf Coast?
0
❑
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Thermometer ID: E38
Temp °C
None
None
987548492680
23.3
987548492691
1.3
NOTES
Revision 1.6
Pace Gulf Coast Report#: 222022255
Page 1 of 1
Pages QA of QQ
Page 13 of 13

Appendix C
Summary of Historical Groundwater Elevations
14
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

Appendix C
Summary of Historical Groundwater Elevations
Granville County Oxford Unit 2 Landfill
Oxford North Carolina
H&H Job No. GMI-005
Date
Groundwater Elevations (ft AMSL)
Background
Downgradient
MW-7
MW-8
I MW-9
MW-10
MW-11
NES-2S
06/13/12
513.48
503.31
479.70
477.42
473.20
468.81
08/22/12
509.73
500.82
477.97
475.31
471.50
469.36
09/25/12
508.45
499.85
478.10
475.06
471.86
469.30
10/17/12
507.95
499.90
478.00
474.23
471.04
467.98
08/06/13
514.33
499.92
478.81
475.32
472.80
469.29
02/25/14
511.75
499.91
480.34
476.26
473.47
470.28
08/12/14
511.98
500.16
479.91
476.54
473.42
470.29
03/12/15
516.39
499.99
479.73
476.47
473.66
470.63
08/18/15
512.39
499.86
478.41
474.92
472.17
469.25
02/16/16
515.79
499.90
481.44
476.37
474.12
471.15
08/10/16
514.29
499.82
478.86
475.51
472.91
470.40
02/14/17
510.89
496.36
479.36
475.97
472.77
468.85
08/23/17
508.84
499.61
477.86
474.74
472.02
469.80
02/07/18
505.74
499.86
479.88
476.25
473.54
471.40
08/14/18
510.22
499.95
478.22
475.31
473.57*
470.81
02/05/19
515.74
500.01
480.72
476.63
474.03
472.18
08/07/19
512.11
500.15
478.86
475.75
473.09
472.31
09/04/19
NM
NM
NM
475.09
NM
NM
02/12/20
511.37
499.99
481.41
477.10
475.06
472.76
03/19/20
512.89
NM
NM
476.33
473.90
471.82
04/23/20
NM
NM
NM
NM
NM
472.06
08/26/20
512.24
499.98
479.78
476.64
473.97
453.00
09/29/20
NM
NM
NM
476.76
NM
NM
02/10/21
517.28
499.88
481.52
476.92
474.32
472.06
08/18/21
511.96
500.19
478.96
475.95
473.13
471.20
02/15/22
507.49
500.10
479.40
476.18
473.22
471.26
Notes:
Groundwater elevations from June 2012 through February 2021 obtained from
LaBella Associates Water Quality Monitoring Report - February 2021 Event.
Groundwater elevations from August 2021 obtained from Garrett & Moore, Inc.
Water Quality Monitoring Report - August 2021 Event.
ft AMSL = ft above mean sea level
-- = not applicable; NM = not measured
Appendix C (Page 1 of 1)
Hart & Hickman, PC
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 First Half GWM/Tables/Oxford
Unit 2 historical data ENW.xlsx

Appendix D
Summary of Historical Constituents in Groundwater
14
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

Appendix D
Summary of Historical Constituents in Groundwater
Granville County Oxford Unit 2 Landfill
Granville County, North Carolina
H&H Job No. GMI-005
Analyte
Sample Date
MDL
MRL
MW-7
MW-8
MW-9
MW-10
MW-11
NES-2S
Blanks
Inorganics
Antimony
02/15/22
3
5
---
ND
ND
ND
ND
---
NICK = 1 pg/L
Arsenic
03/12/15
2.5
10
4.2 J
ND
ND
ND
ND
ND
ND
08/18/15
---
10
ND
ND
ND
ND
ND
ND
ND
NC2L = 10 pg/L
02/18/16
2.5
10
ND
ND
2.7
ND
3.9 J
ND
ND
08/11/16
2.5
10
ND
ND
ND
3.1 J
3.2 J
ND
ND
02/14/17
5
10
ND
ND
ND
ND
ND
ND
ND
08/23/17
5
10
ND
ND
ND
ND
ND
ND
ND
02/06/18
---
10
ND
ND
ND
ND
ND
ND
ND
08/16/18
5
10
ND
ND
ND
ND
NM
ND
ND
02/05/19
5
10
ND
ND
ND
ND
ND
ND
ND
08/08/19
5
10
ND
ND
ND
ND
ND
ND
ND
02/14/20
4.7
10
ND
ND
ND
ND
ND
---
ND
03/19/20111
4.7
10
ND
NS
NS
NS
NS
ND
ND
08/26/20
4.7
10
ND
ND
ND
ND
ND J
5.2 J
---
02/10/21
4.7
10
4.7 J
5.5 J
ND
ND
---
ND
ND
08/17/21
---
10.0
---
ND
ND
ND
ND
---
NA
02/15/22
4.7
10
5.9 J
4.9 J
5.4 J
ND
ND
NA
Barium
06/13/12
---
100
9.2 J
36.8 J
59.2 J
48.2 J
30.6 J
31.4 J
ND
08/22/12
---
100
ND
37.3 J
60.9 J
58.9 J
85 J
28.2 J
ND
NC2L = 700 pg/L
09/25/12
---
100
10.3 J
40.8 J
64.2 J
72.7 J
43.8 J
30.5 J
ND
10/17/12
---
100
24.2 J
57.3 J
65.1 J
48.7 J
110
28 J
ND
08/06/13
---
100
ND
37.1 J
66.5 J
36.8 J
28.5 J
24.8 J
ND
02/25/14
---
100
ND
43.6 J
65 J
41.1 J
20.3 J
58.6 J
ND
08/13/14
5
100
6.2 J
52.7 J
72.7 J
40.7 J
19.7 J
21.7 J
ND
03/12/15
2.5
100
9.8 J
47.9 J
76.3 J
49.1 J
19.1 J
35.5 J
ND
08/18/15
---
100
11 J
45.6 J
72.1 J
43.5 J
20.5 J
31.3 J
ND
02/18/16
2.5
100
14.8 J
59.5 J
76.1 J
54.2 J
31.8 J
28.6 J
ND
08/11/16
2.5
100
6.2 J
42.9 J
81 J
61.2 J
49.9 J
31.1 J
ND
02/14/17
2.5
100
11.8 J
41.9 J
89 J
46.2 J
40.8 J
27.6 J
ND
08/23/17
2.5
100
25.2 J
42.6 J
126
40.8 J
51.4 J
33.8 J
ND
02/06/18
---
100
19.3 J
62.6 J
90.7 J
47.1 J
33.9 J
25.4 J
ND
08/16/18
2.5
100
3.8 J
40.3 J
68.9 J
47.5 J
NM
25.8 J
ND
02/05/19
2.5
5
4 J
39.8
78
59.4
27.7
19.6
ND
08/08/19
2.5
5
4.5 J
40.2
71.4
60.5
30.1
ND
ND
02/14/20
1
5
11
39.3
85
47.2
45
---
ND
03/19/20(1�
1
5
NS
NS
NS
NS
NS
31.8
ND
08/26/20
3.5
5
8.8
37.9
73.7
49.3
35.6
32.4
---
02/10/21
3.5
5
ND
40.1
76.3
60.6
31.2
ND
4 J
08/17/21
---
5.0
---
37.0
76.2
50.2
27.0
---
NA
02/15/22
3.5
5
3.8 J
37.5
76.5
37.5
29.0
NA
---
Cadmium
08/23/17
0.5
1
ND
ND
ND
0.56 J
ND
ND
ND
02/06/18
---
1
ND
ND
ND
ND
0.59 J
ND
ND
NICK = 2 pg/L
08/16/18
0.5
1
ND
ND
ND
ND
NM
ND
ND
02/05/19
0.5
1
ND
ND
ND
ND
ND
ND
ND
08/08/19
0.5
1
ND
ND
ND
ND
ND
ND
ND
02/14/20
0.4
1
ND
ND
ND
ND
0.45 J
---
ND
03/19/20111
0.4
1
NS
NS
NS
NS
NS
ND
ND
08/26/20
0.4
1
ND
ND
ND
ND
ND
ND
---
02/10/21
0.4
1
ND
ND
ND
ND
ND
ND
ND
08/17/21
---
1.0
---
ND
ND
ND
ND
---
NA
02/15/22
0.4
1
ND
ND
ND
ND
ND
NA
Chromium
06/13/12
---
10
ND
ND
ND
10.9
ND
ND
ND
08/22/12
---
10
ND
ND
ND
10.4
18.3
ND
ND
NC2L = 10 pg/L
09/25/12
---
10
ND
ND
ND
10.3
ND
ND
ND
10/17/12
---
10
ND
ND
ND
15.8
20.9
ND
ND
08/06/13
---
10
ND
ND
ND
ND
ND
ND
ND
02/25/14
---
10
ND
ND
ND
ND
ND
ND
ND
08/13/14
---
10
ND
ND
ND
5.1 J
ND
ND
ND
03/12/15
2.5
10
ND
3 J
ND
ND
ND
ND
ND
08/18/15
---
10
ND
ND
ND
ND
ND
ND
ND
02/18/16
2.5
10
ND
ND
ND
ND
ND
3 J
ND
08/11/16
2.5
10
2.8 J
ND
ND
4.3 J
6.3 J
ND
ND
02/14/17
2.5
10
ND
ND
ND
ND
4.4 J
ND
ND
08/23/17
2.5
10
ND
ND
ND
ND
4.5 J
ND
ND
02/06/18
---
10
4.4 J
ND
ND
ND
ND
ND
ND
08/16/18
2.5
10
ND
ND
ND
ND
NM
ND
ND
02/05/19
2.5
5
ND
ND
ND
ND
ND
ND
ND
08/08/19
2.5
5
ND
ND
ND
1 J
ND
ND
ND
02/14/20
1
5
3 J
ND
1.6 J
2.6 J
8.8
---
ND
03/19/20(1�
1
5
NS
NS
NS
NS
NS
ND
ND
08/26/20
3.7
5
ND
ND
ND
ND
ND
ND
---
02/10/21
3.7
5
ND
ND
ND
ND
ND
ND
ND
08/17/21
---
5.0
---
ND
ND
ND
ND
---
NA
02/15/22
3.7
5
ND
ND
ND
ND
ND
NA
Cobalt
06/13/12
---
10
ND
ND
ND
ND
ND
ND
ND
08/22/12
---
10
ND
ND
ND
ND
ND
ND
ND
NICK = 1 pg/L
09/25/12
---
10
ND
ND
ND
ND
ND
ND
ND
10/17/12
---
10
10.3
ND
ND
ND
12.4
ND
ND
08/06/13
---
10
ND
ND
ND
ND
ND
ND
ND
02/25/14
---
10
ND
ND
ND
ND
ND
ND
ND
08/13/14
5
10
ND
ND
ND
ND
ND
ND
ND
03/12/15
2.5
10
ND
ND
ND
ND
ND
3.6 J
ND
08/18/15
---
10
ND
ND
ND
ND
ND
ND
ND
02/18/16
2.5
10
ND
ND
ND
ND
ND
ND
ND
08/11/16
2.5
10
ND
ND
ND
ND
ND
ND
ND
02/14/17
2.5
10
ND
ND
ND
ND
ND
3.2 J
ND
08/23/17
2.5
10
ND
ND
ND
ND
ND
ND
ND
02/06/18
---
10
3.4 J
ND
ND
ND
ND
ND
ND
08/16/18
2.5
10
ND
ND
ND
ND
NM
ND
ND
02/05/19
2.5
5
ND
ND
ND
ND
ND
ND
ND
08/08/19
2.5
5
ND
ND
ND
ND
1.2 J
ND
ND
02/14/20
1.1
5
2.7 J
ND
ND
ND
3.9 J
---
ND
03/19/20111
1.1
5
NS
NS
NS
NS
NS
4.1 J
ND
08/26/20
3.6
5
ND
ND
ND
ND
ND
ND
---
02/10/21
3.6
5
ND
ND
ND
ND
ND
ND
ND
08/17/21
---
5.0
---
ND
ND
ND
ND
---
NA
02/15/22
3.6
5
ND
ND
ND
ND
ND
NA
Appendix D (Page 1 of �4+)
https.//harthick.sharepoinLcom/sites/MasterFiles-1/Shared Docum--AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 First Half GW M/Tables/Oxford UM 2 historical data_ENW Hart & Hickman, Pl.

Appendix D
Summary of Historical Constituents in Groundwater
Granville County Oxford Unit 2 Landfill
Granville County, North Carolina
H&H Job No. GMI-005
Analyte
Sample Date
MDL
MRL
MW-7
MW-8
MW-9
MW-10
MW-11
NES-2S
Blanks
Copper
06/13/12
---
10
ND
ND
ND
46
ND
ND
ND
08/22/12
---
10
ND
ND
ND
56.2
19.8
ND
ND
NC21- = 1,000 pg/L
09/25/12
---
10
7.4 J
ND
ND
63.6
5.7 J
ND
ND
10/17/12
---
10
19.9
7.6 J
ND
35.5
23.1
ND
ND
08/06/13
---
10
ND
ND
ND
ND
ND
ND
ND
02/25/14
---
10
ND
ND
ND
7.9 J
ND
ND
ND
08/13/14
5
10
ND
11.6
ND
13.4
ND
ND
ND
03/12/15
2.5
10
ND
47
ND
6 J
ND
3.3 J
ND
08/18/15
---
10
2.8 J
26.6
ND
12.3
ND
4.3 J
ND
02/18/16
2.5
10
ND
7.8 J
ND
ND
ND
ND
ND
08/11/16
2.5
10
ND
30.7
ND
14.6
4.5 J
2.7 J
ND
02/14/17
2.5
10
ND
16.6
3.2 J
9.9 J
4.9 J
3.9 J
ND
08/23/17
2.5
10
8.8 J
6.4 J
ND
6.4 J
4.5 J
ND
ND
02/06/18
---
10
18.6
133
3.7 J
5.4 J
ND
ND
ND
08/16/18
2.5
10
ND
24.7
ND
3.6 J
NM
ND
ND
02/05/19
2.5
5
ND
11
ND
3 J
ND
ND
ND
08/08/19
2.5
5
2.5 J
8.3
ND
6.9
ND
ND
ND
02/14/20
2.1
5
5.5
11.8
ND
4.6 J
17.6
---
ND
03/19/20(1)
2.1
5
NS
NS
NS
NS
NS
ND
ND
08/26/20
4.3
5
ND
10.9
ND
5.6
ND
ND
---
02/10/21
4.3
5
ND
7.8
ND
4.5 J
ND
ND
ND J
08/17/21
---
5.0
---
4.6 J
ND
8.7
ND
---
NA
02/15/22
4.3
5
ND
4.5 J
ND
ND
ND
NA
Iron
02/06/18
---
300
9990
1500
1190
1670
1630
353
ND
08/16/18
25
300
340
---
---
---
NM
---
27.8 J
NC21- = 300 pg/L
02/05/19
25
50
183
---
---
---
---
---
ND
08/08/19
25
50
176
---
---
---
---
---
---
02/14/20
19.5
50
3750
---
---
---
---
---
ND
Resample
03/19/20(1)
0.9
5
1310
NS
NS
NS
ND
NS
ND
08/26/20
41.5
50
1570
---
---
---
---
1030
---
02/10/21
41.5
50
---
---
---
---
---
---
ND
08/17/21
---
---
---
NA
NA
NA
NA
---
NA
02/15/22
---
---
NA
NA
NA
NA
NA
NA
Lead
02/14/17
2.5
10
ND
ND
ND
ND
2.9 J
ND
ND
08/23/17
2.5
10
ND
ND
ND
ND
ND
ND
ND
NC21- = 15 pg/L
02/06/18
2.5
10
ND
ND
ND
ND
ND
ND
ND
08/16/18
2.5
10
ND
ND
ND
ND
NM
ND
ND
02/14/20
1.6
5
ND
1.8 J
1.9 J
ND
4.2 J
---
ND
03/19/20(1)
1.6
5
NS
NS
NS
NS
NS
ND
ND
02/10/21
1.6
5
ND
ND
ND
ND
ND
---
ND
08/17/21
---
5.0
---
ND
ND
ND
ND
---
NA
02/15/22
4.5
5
ND
ND
ND
ND
ND
---
---
Manganese
02/06/18
---
50
241
394
53
25.8 J
410
411
ND
08/16/18
2.5
50
6.7 J
---
---
---
NM
---
ND
NC21- = 50 pg/L
02/05/19
2.5
5
5.5
---
---
---
---
---
ND
08/08/19
2.5
5
6
---
---
---
---
---
---
02/14/20
0.9
5
85.8
---
---
---
---
---
ND
Resample
03/19/20(1)
0.9
5
26.4
NS
NS
NS
ND
NS
ND
08/26/20
3.4
5
35.2
---
431
---
02/10/21
3.4
5
---
---
---
---
---
---
ND
08/17/21
---
---
---
NA
NA
NA
NA
---
NA
02/15/22
---
---
NA
NA
NA
NA
NA
NA
Nickel
06/13/12
---
50
ND
ND
ND
ND
ND
ND
ND
08/22/12
---
50
ND
ND
ND
ND
6.1 J
ND
ND
NC21- = 100 pg/L
09/25/12
---
50
ND
ND
ND
ND
ND
ND
ND
10/17/12
---
50
ND
ND
ND
6.9 J
8.9 J
ND
ND
08/06/13
---
50
ND
ND
ND
ND
ND
ND
ND
02/25/14
---
50
ND
ND
ND
ND
ND
ND
ND
08/13/14
5
50
ND
ND
ND
ND
ND
ND
ND
03/12/15
2.5
50
ND
ND
ND
ND
ND
ND
ND
08/18/15
---
50
ND
ND
ND
ND
2.7 J
ND
ND
02/18/16
2.5
50
ND
ND
ND
ND
2.9 J
ND
ND
08/11/16
2.5
50
ND
ND
ND
ND
6.2 J
ND
ND
02/14/17
2.5
50
ND
ND
ND
ND
5.2 J
ND
ND
08/23/17
2.5
50
5.2 J
ND
ND
2.8 J
5.8 J
ND
ND
02/06/18
---
50
5.9 J
ND
ND
ND
3.4 J
ND
ND
08/16/18
2.5
50
ND
ND
ND
ND
NM
ND
ND
02/05/19
2.5
5
ND
ND
ND
ND
2.7 J
ND
ND
08/08/19
2.5
5
0.93 J
ND
ND
1.6 J
3.2 J
ND
ND
02/14/20
0.9
5
2.5 J
ND
ND
1.3 J
16
---
ND
03/19/20(1)
0.9
5
NS
NS
NS
NS
NS
1.5 J
ND
08/26/20
3.5
5
ND
ND
ND
ND
4 J
ND
---
02/10/21
3.5
5
ND
ND
ND
ND
ND
ND
ND
08/17/21
---
5.0
---
ND
ND
ND
ND
---
NA
02/15/22
3.5
5
---
ND
ND
ND
ND
NA
Thallium
06/13/12
---
5.5
ND
ND
ND
ND
ND
ND
ND
08/22/12
---
5.5
ND
6.8
6.8
ND
ND
ND
ND
NC21- = 2 pg/L
09/25/12
---
5.5
ND
ND
ND
ND
ND
ND
ND
10/17/12
---
5.5
ND
ND
ND
ND
ND
ND
ND
08/06/13
---
5.5
ND
ND
ND
ND
ND
ND
ND
02/25/14
---
5.5
ND
ND
ND
ND
ND
ND
ND
08/13/14
5.4
5.5
ND
ND
ND
ND
ND
ND
ND
03/12/15
5
5.5
ND
ND
ND
ND
ND
ND
ND
08/18/15
---
5.5
ND
ND
ND
ND
ND
ND
ND
02/18/16
5
5.5
ND
ND
ND
ND
ND
ND
ND
08/11/16
5
5.5
ND
ND
ND
ND
ND
ND
ND
02/14/17
0.02
5.5
0.039 J
0.059 J
ND
ND
ND
ND
ND
08/23/17
0.02
5.5
0.04 J
0.044 J
ND
ND
0.021 J
ND
ND
02/06/18
---
0.1
ND
0.034 J
ND
ND
ND
ND
ND
08/16/18
0.02
5.5
ND
ND
ND
ND
NM
ND
ND
02/05/19
0.06
0.1
ND
ND
ND
ND
ND
ND
ND
08/08/19
0.06
0.1
ND
ND
ND
ND
ND
ND
ND
02/14/20
0.06
0.1
ND
ND
ND
ND
ND
---
ND
03/19/20(1)
0.06
0.1
NS
NS
NS
NS
NS
ND
ND
08/26/20
0.05
0.1
ND
ND
ND
ND
ND
ND
---
02/10/21
0.05
0.1
ND
ND
ND
ND
ND
ND
ND
08/17/21
---
0.47
---
ND
ND
ND
ND
---
NA
02/15/22
0.05
0.47
1 ND
ND
ND
ND
ND
NA
Appendix D (Page 2 of .�
-4+)
https.//harthick.sharepo t.-/sit-Wt.,R 1/Shared DocumenWAAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 First Half GW M/Tables/Oxford UM 2 historical data_ENW Hart & Hickman, Pl.

Appendix D
Summary of Historical Constituents in Groundwater
Granville County Oxford Unit 2 Landfill
Granville County, North Carolina
H&H Job No. GMI-005
Analyte
Sample Date
MDL
MRL
MW-7
MW-8
MW-9
MW-10
MW-11
NES-2S
Blanks
Total Dissolved Solids, Dissolved
08/26/20
25000
25000
262000
---
---
---
---
---
ND
08/17/21
---
---
---
NA
NA
NA
NA
---
---
NC 2L = 500,000 pg/L
02/10/21
25000
25000
274000
---
---
---
---
---
ND
08/17/21
---
---
---
NA
NA
NA
NA
---
NA
02/15/22
---
---
NA
NA
NA
NA
NA
NA
---
Vanadium
06/13/12
---
25
5.2 J
ND
ND
27.8
17.3 J
11 J
ND
08/22/12
---
25
ND
ND
ND
30.2
69.5
9 J
ND
NC21- = 7 pg/L
09/25/12
---
25
8.3 J
ND
ND
33.4
16.5 J
8.2 J
ND
10/17/12
---
25
29.7
ND
ND
19.5 J
63.8 J
6.2 J
ND
08/06/13
---
25
ND
ND
ND
ND
9.2 J
ND
ND
02/25/14
---
25
ND
ND
ND
10.2 J
ND
ND
ND
08/13/14
5
25
ND
ND
ND
11.8 J
ND
ND
ND
03/12/15
2.5
25
ND
4.4 J
7.3 J
5 J
ND
6.7 J
ND
08/18/15
---
25
6.1 J
ND
ND
6.5 J
3.6 J
9.1 J
ND
02/18/16
2.5
25
ND
2.9 J
ND
ND
ND
ND
ND
08/11/16
2.5
25
ND
ND
5.8 J
10 J
14.3 J
6.6 J
ND
02/14/17
2.5
25
ND
ND
5.2 J
4 J
9.1 J
5.4 J
ND
08/23/17
2.5
25
18.6 J
ND
2.6 J
4.6 J
11.9 J
6.4 J
ND
02/06/18
---
25
23.5 J
3.4 J
4.4 J
4.7 J
3.3 J
ND
ND
08/16/18
2.5
25
ND
ND
ND
2.9 J
NM
2.5 J
ND
02/05/19
2.5
5
ND
ND
ND
2.9 J
ND
ND
ND
08/08/19
2.5
5
2.2 J
ND
ND
5.3
1.8
ND
ND
Resample
09/04/19
1.3
5
NS
NS
NS
ND
NS
NS
NS
02/14/20
1.3
5
9.2
ND
3.4 J
5.5
13.3
---
ND
03/19/20111
1.3
5
7.9 J
NS
NS
3.2 J
ND
5.6
ND
Resample
04/23/20
1.3
5
NS
NS
NS
NS
NS
3 J
ND
08/26/20
3.9
5
4.4 J
ND
ND
5.5
ND
ND
---
09/29/20
3.9
5
---
---
---
ND
---
---
---
02/10/21
3.9
5
ND
ND
ND
4.4 J
ND
ND
ND
08/17/21
---
5.0
---
ND
ND
ND
ND
---
NA
02/15/22
3.9
5
ND
ND
ND
ND
ND
NA
Zinc
06/13/12
---
10
ND
ND
ND
10.5
ND
ND
ND
08/22/12
---
10
ND
ND
32
31
21.9
10.6
ND
NC21-= 1,000 pg/L
09/25/12
---
10
11.7
ND
ND
14.8
ND
ND
ND
10/17/12
---
10
32.5
ND
ND
10.5
29
ND
ND
08/06/13
---
10
ND
ND
ND
ND
ND
ND
ND
02/25/14
---
10
ND
ND
ND
ND
ND
ND
ND
08/13/14
10
10
ND
ND
ND
ND
ND
ND
ND
03/12/15
5
10
9.8 B
10.9 B
10.7 B
8.7 B
7.8 B
9.9 B
6.1 J
08/18/15
---
10
8.9 B
ND
ND
ND
ND
5.2 B
11.5 J
02/18/16
5
10
ND
13.1
ND
ND
ND
8.6 J
ND
08/11/16
5
10
7.2 J
5.4 J
ND
19.5
11.7
8.7 J
ND
02/14/17
5
10
7 J
6 J
5.4 J
5.3 J
8.3 J
6 J
ND
08/23/17
5
10
18
ND
6.3 J
5.1 J
15.5
6.9 J
ND
02/06/18
---
10
ND
ND
ND
ND
ND
ND
ND
08/16/18
5
10
ND
ND
ND
ND
NM
ND
ND
02/05/19
5
10
ND
ND
ND
ND
ND
ND
ND
08/08/19
5
10
ND
ND
ND
ND
ND
ND
ND
02/14/20
3.9
10
9.6 J
ND
ND
ND
20.2
---
ND
03/19/20(lt
3.9
10
NS
NS
NS
NS
NS
ND
ND
08/26/20
9.5
10
ND
ND
ND
ND
ND
ND
---
02/10/21
9.5
10
ND
ND
ND
ND
ND
ND
ND
08/17/21
---
10.0
---
ND
ND
ND
ND
---
NA
02/15/22
9.5
10
ND
ND
ND
ND
ND
NA
Organics
1,4-Dioxane
08/16/18
1.9
2
ND
ND
ND
ND
NM
ND
ND
02/05/19
1.9
2
ND
ND
ND
ND
ND
ND
ND
NC21- = 3 pg/L
08/08/19
1.9
2
ND
ND
ND
ND
ND
ND
ND
02/14/20
1.2
2
ND
ND
ND
ND
ND
ND
ND
08/26/20
1.2
2
ND
ND
ND
ND
ND
ND
ND
02/10/21
1.2
2
ND
ND
ND
ND
ND
ND
ND
08/17/21
---
2.0
---
ND
ND
ND
ND
---
ND
02/15/22
0.86
2
ND
ND
ND
ND
ND
---
cis-1,2-Dichloroethane
08/18/15
5
5
0.71 J
0.36 J
ND
ND
ND
ND
ND
02/18/16
5
5
ND
ND
ND
ND
ND
ND
ND
NC21- = 70 pg/L
08/11/16
5
5
ND
ND
ND
ND
ND
ND
ND
02/14/17
0.19
5
ND
ND
ND
ND
ND
ND
ND
08/23/17
0.19
5
ND
ND
ND
ND
ND
ND
ND
02/06/18
0.19
5
ND
ND
ND
ND
ND
ND
ND
08/16/18
0.19
5
ND
ND
ND
ND
NM
ND
ND
02/05/19
0.29
1
ND
ND
ND
ND
ND
ND
ND
08/08/19
0.29
1
ND
ND
ND
ND
ND
ND
ND
02/14/20
0.29
1
ND
ND
ND
ND
ND
ND
ND
08/26/20
0.29
1
ND
ND
ND
ND
ND
ND
ND
02/10/21
0.29
1
---
ND
ND
ND
ND
ND
ND
08/17/21
---
---
ND
ND
ND
ND
---
ND
02/15/22
0.38
1
ND
ND
ND
ND
ND
---
Methylene Chloride
02/14/17
0.97
1
ND
ND
ND
ND
ND
ND
1
08/23/17
0.97
1
ND
ND
ND
ND
ND
ND
2.7
NC21-= 5 pg/L
02/06/18
---
1
0
ND
ND
ND
ND
ND
ND
08/16/18
0.97
1
ND
0
ND
ND
ND
ND
ND
02/05/19
3.7
5
ND
ND
0
ND
ND
ND
ND
08/08/19
3.7
5
ND
ND
ND
ND
ND
ND
ND
02/14/20
3.7
5
ND
ND
ND
ND
ND
ND
ND
08/26/20
3.7
5
ND
ND
ND
ND
ND
ND
ND
02/10/21
3.7
5
ND
ND
ND
ND
ND
ND
ND
08/17/21
---
5.0
---
ND
ND
ND
ND
---
ND
02/15/22
2
5
ND
ND
ND
ND
ND
Appendix D (Page 3 of �4+)
https.//harthick.sharepoint.-/s,t-/MasterFiI--1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 -Granville Co. Oxford LF Unit 2/2022 First Half GW M/Tables/Oxford Unit 2 histarical data_ENW Hart & Hickman, Pl.

Appendix D
Summary of Historical Constituents in Groundwater
Granville County Oxford Unit 2 Landfill
Granville County, North Carolina
H&H Job No. GMI-005
Analyte
Sample Date
MDL
MRL
MW-7
MW-8
MW-9
MW-10
MW-11
NES-2S
Blanks
Sulfate
08/26/20
500
1000
53300
---
---
---
---
ND
02/10/21
500
1000
65000
---
---
---
---
24900
ND
NICK = 250,000 pg/L
08/17/21
---
---
NA
NA
NA
NA
NA
---
NA
02/15/22
---
---
NA
NA
NA
NA
NA
NA
ND
Trichlorofluoromethane
06/13/12
---
1
ND
ND
ND
ND
0.78 B
0.85 B
0.74 J
08/22/12
---
1
ND
ND
ND
ND
ND
ND
ND
NC2L = 2,000 pg/L
09/25/12
---
1
ND
ND
ND
ND
ND
ND
ND
10/17/12
---
1
ND
ND
ND
ND
ND
ND
ND
08/06/13
---
1
ND
ND
ND
ND
ND
ND
ND
02/25/14
---
1
ND
ND
ND
ND
ND
ND
ND
08/13/14
---
2
ND
ND
ND
ND
ND
ND
ND
03/12/15
0.2
1
ND
ND
ND
ND
ND
ND
ND
08/18/15
---
1
ND
ND
ND
ND
ND
ND
ND
02/18/16
0.2
1
ND
ND
ND
ND
ND
ND
ND
08/11/16
0.2
1
ND
ND
ND
ND
ND
ND
ND
02/14/17
0.2
1
ND
ND
ND
ND
ND
ND
ND
08/23/17
0.2
1
ND
ND
ND
ND
ND
ND
ND
02/06/18
---
1
ND
ND
ND
ND
ND
ND
ND
08/16/18
0.2
1
ND
ND
ND
ND
NM
ND
ND
02/05/19
0.31
1
ND
ND
ND
ND
ND
ND
ND
08/08/19
0.31
1
ND
ND
ND
ND
ND
ND
ND
02/14/20
0.31
1
ND
ND
ND
ND
ND
ND
ND
08/26/20
0.31
1
ND
ND
ND
ND
ND
ND
ND
02/10/21
0.31
1
ND
ND
ND
ND
ND
ND
ND
08/17/21
---
1.0
---
ND
ND
ND
ND
---
ND
02/15/22
0.3
1
ND
ND
ND
ND
ND
---
I ---
Notes:
Analytical results from September June 2012 through February 2021 obtained from LaBella Associates Water Quality Monitoring Report - February 2021 Event.
Analytical results from August 2021 obtained from Garrett & Moore, Inc. Water Quality Monitoring Report - August 2021 Event.
The March 19, 2020 sampling event was a resampling event for MW-7, MW-10, and MW-11; however, it was the initial 2020 semiannual sampling event for NES-2S.
NC 2L Standards are the Title 15A NCAC 02L.0202 Groundwater Standards dated April 1, 2022.
Bold concentrations exceed the NC2L Standard for groundwater.
Detections of cis- 1,2-dichloroethylene in MW-7 and MW-8 in August 2015 are suspect. Results for the Unit 1 MW-7 sample, collected in concurrence with the Unit 2 sample,
was reported as non -detect for cis-1,2-dichloroethylene.
NES-2S 8/17/21 sample data shown in table collected on 8/18/21.
All concentrations are in micrograms per liter (pg/L).
ND = not detected; RL = reporting limit; NM = not measured; NS = not samples; NE = not established; --- = data not available/not reported;
B = blank -qualified data, result is expected to be biased high based on concentrations in the blank; NA = not analyzed/not available;
J = Estimated value between the MDL and the MRL; MDL = laboratory method detection limit; MRL = laboratory method reporting limit.
Appendix D (Page 4 of �4+)
https.//harthick.sharepoinLcom/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 First Half GW M/Tables/Oxford Unit 2 histarical data_ENW Hart & Hickman, Pl.

Appendix E
Summary of Historical Constituents in Surface Water
14
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

Appendix E
Summary of Historical Constituents in Surface Water
Granville County Oxford Unit 2 Landfill
Granville County, North Carolina
H&H Job No. GMI-005
Analyte
Sample Date
MDL
MRL
SW-3
SW-4
Blanks
Inorganics
Arsenic
03/12/15
2.5
10
ND
ND
ND
08/19/15
2.5
10
ND
ND
ND
NC2B (1> = 150 pq/L
02/18/16
2.5
10
ND
ND
ND
08/11/16
2.5
10
ND
ND
ND
02/14/17
5
10
ND
ND
ND
08/23/17
5
10
ND
ND
ND
02/06/18
5
10
ND
ND
ND
08/16/18
5
10
ND
ND
ND
02/05/19
5
10
ND
6.1 J
ND
08/08/19
4.7
10
ND
ND
ND
02/14/20
4.7
10
ND
ND
ND
08/26/20
4.7
10
ND
7.2 J
---
02/10/21
4.7
10
4.7 J
Dry
ND
08/17/21
---
10.0
ND
ND
---
02/15/22
4.7
10
ND
ND
---
Barium
08/13/14
5
100
22.1 J
33.9 J
ND
03/12/15
2.5
100
22.5 J
24.6 J
ND
ISTV (3)= 21,000 pg/L
08/19/15
2.5
100
23.9 J
32.7 J
ND
02/18/16
2.5
100
22 J
26.3 J
ND
08/11/16
2.5
100
23.4 J
26.5 J
ND
02/14/17
2.5
100
18.6 J
21.4 J
ND
08/23/17
2.5
100
32.3 J
33.3 J
ND
02/06/18
2.5
100
23.7 J
32.3 J
ND
08/16/18
2.5
100
24.2 J
38.2 J
ND
02/05/19
2.5
5
22.9
23.1
ND
08/08/19
1
5
23.3
44.5
ND
02/14/20
1
5
26.5
29.3
ND
08/26/20
3.5
5
21.2
47.5
---
02/10/21
3.5
5
18.8
DRY
ND
08/17/21
---
5.0
19.9
28.5
---
02/15/22
3.5
5
16.6
29.7
---
Beryllium
08/11/16
0.5
1
ND
ND
ND
02/14/17
0.5
1
ND
ND
ND
NC2B 6.5 pq/L
08/23/17
0.5
1
ND
ND
ND
02/06/18
0.5
1
ND
ND
ND
08/16/18
0.5
1
ND
ND
ND
02/05/19
0.5
1
ND
ND
ND
08/08/19
0.2
1
ND
ND
ND
02/14/20
0.2
1
ND
ND
ND
08/26/20
0.7
1
ND
ND
---
02/10/21
0.7
1
ND
DRY
ND
08/17/21
---
1.0
ND
ND
---
02/15/22
0.7
1
ND
ND
---
Chromium
08/13/14
5
10
ND
ND
ND
03/12/15
2.5
10
ND
2.6 J
ND
NC2B SW-3 (4) = 16.94 pg/L
08/19/15
2.5
10
ND
ND
ND
NC2B SW-4 (4) = 26.82 pg/L
02/18/16
2.5
10
ND
ND
ND
08/11/16
2.5
10
5.2 J
ND
ND
9/13/16(5)
2.5
10
NS
NS
ND
02/14/17
2.5
10
3 J
ND
ND
08/23/17
2.5
10
ND
ND
ND
02/06/18
2.5
10
ND
2.7 J
ND
08/16/18
2.5
10
ND
ND
ND
02/05/19
2.5
5
ND
ND
ND
08/08/19
1
5
ND
2.2 J
ND
02/14/20
1
5
2.6 J
3.1 J
ND
08/26/20
3.7
5
ND
9.8
---
02/10/21
3.7
5
ND
DRY
ND
08/17/21
---
5.0
ND
ND
---
02/15/22
3.7
5
ND
ND
---
Cobalt
08/11/16
2.5
10
ND
ND
ND
02/14/17
2.5
10
ND
ND
ND
ISTV (3) = 1.6 pq/L
08/23/17
2.5
10
ND
ND
ND
02/06/18
2.5
10
ND
ND
ND
08/16/18
2.5
10
ND
ND
ND
02/05/19
2.5
5
ND
ND
ND
08/08/19
1.1
5
ND
2.9 J
--
02/14/20
1.1
5
ND
ND
ND
08/26/20
3.6
5
ND
ND
---
02/10/21
3.6
5
ND
DRY
ND
08/17/21
---
5.0
ND
ND
---
1
1
1 3.6
1 5
1 ND
I ND
---
Appendix E (Page 1 of
3)
https://harthick.sharepoint.com/sitesIMasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 First Half GWM/Tables/Oxford Unit 2 historical data_ENW.xlsx Hart & Hickman, PC

Appendix E
Summary of Historical Constituents in Surface Water
Granville County Oxford Unit 2 Landfill
Granville County, North Carolina
H&H Job No. GMI-005
Analyte
Sample Date
MDL
MRL
SW-3
SW-4
Blanks
Copper
08/13/14
5
10
ND
ND
ND
03/12/15
2.5
10
ND
ND
ND
NC26 SW-3 1.92 pg/L
08/19/15
2.5
10
ND
ND
ND
NC2B SW-4 (4) = 3.10 pg/L
02/18/16
2.5
10
ND
ND
ND
08/11/16
2.5
10
ND
ND
ND
9/13/16(5)
2.5
10
NS
NS
3.5 B
02/14/17
2.5
10
ND
ND
ND
08/23/17
2.5
10
ND
ND
ND
02/06/18
2.5
10
2.7 J
3.6 J
ND
08/16/18
2.5
10
ND
ND
ND
02/05/19
2.5
5
ND
ND
ND
08/08/19
2.1
5
2.7 J
2.7 J
ND
02/14/20
2.1
5
2.8 J
2.9 J
ND
08/26/20
4.3
5
ND
8.1
---
02/10/21
4.3
5
ND
DRY
ND
08/17/21
---
5.0
ND
ND
---
02/15/22
4.3
5
ND
ND
---
Hardness, Total (SM 23408)
02/05/19
662
662
13800
17400
---
08/08/19
131
662
17400
28200
---
02/14/20
131
662
10800
12300
---
08/26/20
131
662
14900
34900
---
02/10/21
131
662
---
DRY
---
08/17/21
---
662
16,500
28,900
---
02/15/22
---
---
NA
NA
---
Iron
02/06/18
25
300
1520
2920
ND
08/16/18
25
300
---
---
27.8 J
NRWQC (2) = 1,000 pg/L
02/05/19
25
50
---
---
ND
02/14/20
19.5
50
---
---
ND
02/10/21
41.5
50
---
DRY
---
08/17/21
---
---
NA
NA
---
02/15/22
---
---
NA
NA
---
Lead
02/18/16
2.5
10
ND
ND
2.7 J
08/11/16
2.5
10
ND
ND
ND
9/13/16(5)
2.5
10
NS
NS
ND
02/14/17
2.5
10
ND
ND
ND
NC2B SW-3 (4) = 0.34 pg/L
08/23/17
2.5
10
ND
ND
ND
NC26 SW-4 (41 = 0.64 pg/L
02/06/18
2.5
10
ND
ND
ND
08/16/18
2.5
10
ND
ND
ND
02/05/19
2.5
5
ND
ND
ND
08/08/19
1.6
5
ND
1.6 J
---
02/14/20
1.6
5
ND
ND
ND
08/26/20
4.5
5
ND
ND
---
02/10/21
4.5
5
ND
DRY
ND
08/17/21
---
5.0
ND
ND
---
02/15/22
4.5
5
ND
ND
---
Manganese
02/06/18
2.5
50
11.6 J
25.8 J
ND
08/16/18
2.5
50
---
---
ND
NRWQC (2) = 100 pg/L
02/05/19
2.5
5
---
---
ND
02/14/20
0.9
5
---
---
ND
02/10/21
3.4
5
---
DRY
---
08/17/21
---
---
NA
NA
---
02/15/22
---
---
NA
NA
---
Nickel
08/13/14
5
50
ND
ND
ND
03/12/15
2.5
50
ND
ND
ND
NC26 SW-3 (41 = 11.33 pg/L
08/19/15
2.5
50
ND
ND
ND
NC2B SW-4 (4) = 18.20 pg/L
02/18/16
2.5
50
ND
ND
ND
08/11/16
2.5
50
2.8 J
ND
ND
02/14/17
2.5
50
ND
ND
ND
08/23/17
2.5
50
ND
ND
ND
02/06/18
2.5
50
ND
ND
ND
08/16/18
2.5
50
ND
ND
ND
02/05/19
2.5
5
ND
ND
ND
08/08/19
0.9
5
ND
1.9 J
ND
02/14/20
0.9
5
1.2 J
1.3 J
ND
08/26/20
3.5
5
ND
4.3 J
---
02/10/21
3.5
5
ND
DRY
ND
08/17/21
---
5.0
ND
ND
---
02/15/22
3.5
5
ND
ND
---
Selenium
08/11/16
5
10
ND
ND
ND
02/14/17
5
10
ND
ND
ND
NC2B 5 pg/L
08/23/17
5
10
ND
ND
ND
02/06/18
5
10
ND
ND
ND
08/16/18
5
10
ND
ND
ND
02/05/19
5
10
ND
ND
ND
08/08/19
4.7
10
ND
ND
ND
02/14/20
4.7
10
ND
ND
ND
08/26/20
4.7
10
ND
ND
---
02/10/21
4.7
10
ND
DRY
ND
08/17/21
---
10.0
ND
ND
---
02/15/22
4.7
10
ND
ND
---
Appendix E (Page 2 of
3)
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 First Half GWM/Tables/Oxford Unit 2 historical data_ENW Hart & Hickman, PC

Appendix E
Summary of Historical Constituents in Surface Water
Granville County Oxford Unit 2 Landfill
Granville County, North Carolina
H&H Job No. GMI-005
Analyte
Sample Date
MDL
MRL
SW-3
SW-4
Blanks
Vanadium
08/13/14
5
25
ND
9.3 J
ND
03/12/15
2.5
25
3.1 J
6.3 J
ND
NC213 NE
08/19/15
2.5
25
2.7 J
4.3 J
ND
02/18/16
2.5
25
ND
ND
ND
08/11/16
2.5
25
ND
2.7 J
ND
02/14/17
2.5
25
ND
ND
ND
08/23/17
2.5
25
4.6 J
ND
ND
02/06/18
2.5
25
4.3 J
8.2 J
ND
08/16/18
2.5
25
3.7 J
ND
ND
02/05/19
2.5
5
ND
ND
ND
08/08/19
1.3
5
3.3 J
7.9
ND
02/14/20
1.3
5
3.8 J
6.1
ND
08/26/20
3.9
5
ND
24.3
---
02/10/21
3.9
5
ND
DRY
ND
08/17/21
---
5.0
ND
ND
---
02/15/22
3.9
5
ND
ND
---
Zinc
08/13/14
5
10
ND
ND
ND
03/12/15
5
10
8.5 B
10.8 B
6.1 J
NC26 SW-3141 = 25.46 lag/L
08/19/15
5
10
ND
ND
11.5 J
NC2B SW-4 (4) = 40.93 tag/L
02/18/16
5
10
ND
ND
ND
08/11/16
5
10
13
5.6 J
ND
9/13/16(5)
5
10
---
---
ND
02/14/17
5
10
7 J
ND
ND
08/23/17
5
10
ND
ND
ND
02/06/18
5
10
ND
ND
ND
08/16/18
5
10
ND
ND
ND
02/05/19
5
10
ND
ND
ND
08/08/19
3.9
10
ND
7.2 J
ND
02/14/20
3.9
10
4 J
4.7 J
ND
08/26/20
9.5
10
ND
11.3
---
02/10/21
9.5
10
ND
DRY
ND
08/17/21
---
10.0
ND
ND
---
02/15/22
9.5
10
ND
ND
---
Organics
1,4-Dioxane (p-Dioxane)
08/16/18
1.9
2
ND
ND
ND
02/05/19
1.9
2
ND
ND
ND
ISTV 13)= 80 µg/L
08/08/19
1.2
2
ND
ND
ND
02/14/20
1.2
2
ND
ND
ND
08/26/20
1.2
2
ND
ND
ND
02/10/21
1.2
2
ND
DRY
ND
08/17/21
---
2.0
ND
ND
---
02/15/22
0.86
2
ND
ND
---
2-Hexanone
08/11/16
0.46
50
ND
ND
ND
02/14/17
0.46
50
ND
ND
ND
NC2B NE
08/23/17
0.46
50
ND
ND
ND
02/06/18
0.46
50
ND
ND
ND
08/16/18
0.46
50
ND
ND
ND
02/05/19
0.57
5
ND
ND
ND
08/08/19
0.57
5
ND
ND
ND
02/14/20
0.57
5
ND
ND
ND
08/26/20
0.57
5
ND
ND
ND
02/10/21
0.57
5
ND
DRY
ND
08/17/21
---
5.0
---
---
---
02/15/22
0.48
5
ND
ND
---
Methylene Chloride
08/26/20
3.7
5
---
8.2
---
02/10/21
3.7
5
ND
DRY
ND
ISTV (2) = 11,000 lag/L
08/17/21
---
5.0
ND
ND
---
02/15/22
2
5
ND
ND
---
Toluene
08/26/20
0.24
1
ND
0.33 J
ND
02/10/21
0.24
1
ND
DRY
ND
NC2B 11 tag/L
08/17/21
---
1.0
ND
ND
---
02/15/22
0.48
1
ND
ND
---
Notes:
1. 15A NCAC 26 Water Quality Standards (213 Standards) for Surface Water (Class C) dated July 26, 2021.
2. No 213 Standard established, value shown is EPA Nationally Recommended Water Quality Criteria (NRWQC) for Aquatic
Life & Human Health.
3. No 213 Standard or NWQC established, value shown is North Carolina In -Stream Target Values for Surface Waters (ISTV).
4. NC 213 Standards for hardness -dependent metals calculated using total hardness values obtained from Garrett & Moore, Inc.
Water Quality Monitoring Report - August 2021 Event (SW-3 = 16,500 ug/L; SW-4 = 28,900 ug/L).
5. The 9/13/16 sampling event was a resampling event.
Analytical results from November 1996 through February 2021 obtained from LaBella Associates Water Quality Monitoring
Report - February 2021 Event.
Analytical results from August 2021 obtained from Garrett & Moore, Inc. Water Quality Monitoring Report - August 2021 Event.
Bold concentrations exceed the NC 213 Standard or ISTV.
All concentrations are in micrograms per liter (tag/L).
J = Estimated concentration above the laboratory method detection limit and below the laboratory method reporting limit;
B = blank -qualified data; result is expected to be biased high based on concentrations in the blanks.
MRL = method reporting limit; MDL = laboratory detection limit; ND = Not detected above laboratory method reporting limit
NR = Not Reported; NE= Not established; --- = Not Sampled/ Data not available.
DRY = Surface water point considered to be dry
Data shown in parentheses indicate dissolved concentrations.
Hardness - SW-1 = 24,700 ug/L; SW-2 = 46,600 ug/L;
Appendix E (Page 3 of 3)
Hart & Hickman, PC
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Garrett & Moore/GMI-005 - Granville Co. Oxford LF Unit 2/2022 First Half GWM/Tables/Oxford Unit 2 historical data_ENW