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HomeMy WebLinkAbout3412_Forsyth_OldSalisburyRoad_CDLF_Nov2021GW_FID1681547_20220607DENR USE ONLY ❑Paper Report [:]Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): HDR Engineering, Inc. of the Carolinas Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Mark P. Filardi E-mail: Mark.Filardi@hdrinc.com Phone: 704-338-6787 NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) Old Salisbury Road Landfill 3336 Old Salisbury Road 34-12 0.0500 November 8-12, 2021 Winston-Salem, NC 27127 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring �X Detection Monitoring Assessment Monitoring ❑ Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells �X Groundwater monitoring data from private water supply wells ❑ Leachate monitoring data ❑ Surface water monitoring data Methane gas monitoring data Corrective action data (specify) Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Mark P. Filardi Senior Geologist 704-338-6787 (Print) Title (Area Code) Telephone Number 1/18/22 Affix NC Licensed/ Professional Geologist Seal Signature Date 440 South Church Street Suite 1200, Charlotte, NC 28202 Facility Representative Address F-0116 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 This page intentionally left blank. FN Winston-Salem / Forsyth County UtI9i 140ties Water • Wastewater • Solid Waste HDR Project No. 10311293 i Assessment Monitoring Report Groundwater and Surface Water Sampling Event — November 2021 Old Salisbury Road Landfill NCDEQ Permit NO. 34-12 Forsyth County, North Carolina January 2022 This page intentionally left blank. Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report Contents Contents 1 General...............................................................................................................................1 1.1 Facility Background...................................................................................................... 1 1.2 Regulatory Authority.................................................................................................... 1 1.3 Assessment Monitoring................................................................................................ 1 1.4 Geologic Characteristics.............................................................................................. 3 1.4.1 Regional Geologic and Hydrogeologic Setting ...................................................... 3 1.4.2 Site Specific Topography and Drainage................................................................ 3 1.4.3 Site Specific Hydrogeology................................................................................... 3 2 Monitoring Network.............................................................................................................4 3 Data Collection................................................................................................................... 6 3.1 Water Level Measurements......................................................................................... 6 3.2 Groundwater Flow........................................................................................................ 7 3.3 Sample Collection and Analysis................................................................................... 8 4 Analytical Results...............................................................................................................10 4.1 Groundwater...............................................................................................................10 4.2 Surface Water.............................................................................................................11 4.3 Landfill Gas.................................................................................................................12 5 Summary...........................................................................................................................12 6 Recommendations.............................................................................................................13 Tables Table 1 Existing groundwater monitoring well details................................................................. 4 Table 2 Sampling Parameters and Schedule............................................................................. 5 Table 3 Groundwater Measurements and Elevations — November 8, 2021................................ 6 Table 4 Historic Groundwater Elevations................................................................................... 6 Table5 Interwell Flow................................................................................................................ 7 Table6 Lab detections............................................................................................................... 9 Table7 Gas readings................................................................................................................12 January 2022 i Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Contents Figures Figure 1 Groundwater contours and sample locations................................................................ 2 Figure 2 Historical groundwater elevations................................................................................. 7 Figure 3 MW-2R groundwater detections..................................................................................11 Appendices Appendix A — Summary of Monitoring Results Appendix B — Laboratory Reports Appendix C — Field Data Appendix D — Electronic Files (Paper Copies Only) Acronyms 2B 15A NCAC Subchapter 02B — Surface Water and Wetlands Standards 2L 15A NCAC Subchapter 02L — Groundwater Classification and Standards pg/L micrograms per liter EPA United States Environmental Protection Agency FID NCDEQ File Identification MCL Maximum contaminant level MDL method detection limit MSL Mean sea level NA Not applicable NCAC North Carolina Administrative Code NCDEQ North Carolina Department of Environmental Quality' ND not detected in sample NE standard not established NS not sampled NTU Nephelometric turbidity units OSR Old Salisbury Road PCB polychlorinated biphenyl PCE tetrachloroethene PRL practical reporting limit PVC polyvinyl chloride PWR Partially weathered rock SVOC semi -volatile organic compound VOC volatile organic compound USGS U.S. Geological Survey January 2022 ii Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� General 1 General HDR Engineering, Inc. of the Carolinas (HDR), on behalf of Winston-Salem/Forsyth County Utilities (the City), is submitting this assessment monitoring report for the Old Salisbury Road C&D Landfill (OSR) located in Forsyth County, North Carolina (Figure 1). 1.1 Facility Background OSR covers approximately 56 acres within a 140-acre tract north of Friedberg Church Road and west of Old Salisbury Road in Forsyth County, North Carolina. The facility was issued a permit to operate on July 3, 1996 and opened in August of the same year. 1.2 Regulatory Authority OSR is currently operating under North Carolina Department of Environmental Quality (NCDEQ) facility permit number 34-12, dated February 28, 2020 (FID 1389508). Groundwater monitoring and reporting requirements are outlined in items 14 to 21 of the permit. North Carolina Solid Waste Management (SWM) Rules 15A NCAC 13B .0544(b) and .0544(c) define the requirements of groundwater and surface water monitoring plans, respectively, as applicable to OSR. The groundwater monitoring plan (FID 1388728) dated January 2020, was approved by NCDEQ on February 28, 2020. 1.3 Assessment Monitoring OSR is in assessment monitoring due to exceedances of groundwater quality standards, as specified in 15 NCAC 02L .0202 (2L Standards), for benzene and tetrachloroethene (PCE) detected in well MW-2R in 2011. On December 9, 2011, an assessment monitoring plan for MW-2R was submitted in accordance with 15A NCAC 1313. The assessment monitoring plan can be summarized as: • Groundwater monitoring wells MW-1 R, MW-2R, MW-4R and MW-15 will be sampled semi-annually for Appendix I constituents and the previously detected Appendix I I constituents, as specified in 40 CFR §258; • All 14 groundwater monitoring wells (including MW-1 R, MW-2R, MW-4R and MW-15) will be sampled during every other fall event (odd years) for the entire Appendix 11 constituent list. • Additional Appendix 11 constituents detected during these events will be added to the sampling program for subsequent semi-annual events. January 2022 SURVEY BOUNDARY MM-8 746.19 MM-7 �o I I I I ; 10 �J A-755 75980 MW-3R�0F MM-6 772,12 MW-7 7h2.41 # I � 01 850 u LEGEND EXISTING CONTOURS PROPERTY BOUNDARY PERMIT/PHASE BOUNDARY 735 GROUNDWATER CONTOURS SURVEY BOUNDARY EXISTING ABANDONED MONITORING WELLS (MW&OW) e • METHANE PROBES(MM) SWA SURFACE WATER APPROXIMATE GROUNDWATER FLOW - NOTES �MM-9 1. THE SITE TOPOGRAPHIC INFORMATION PROVIDED BY CARTOGRAPHIC AERIAL MAPPING INC. FOR 72690 BRADY SURVEYING COMPANY DATED JAN. 5 2019. MW MM-10 ? SW-2 2. PROPERTY BOUNDARY TAKEN FROM DATA SUPPLIED BY BRADY SURVEYING, INC. DATED �1 ll MARCH 14, 1994. o 0 3. GROUNDWATER ELEVATIONS ARE IN MEAN SEA o o LEVEL, MEASURED ON NOVEMBER 8, 2021 (SHOWN n \ NEXT TO WELL LABEL). 780 84 G , 7,9� MM-4S M rvI-4D ` MM-3 �i 774.23 -MW-5R _ PROJECT TITLE OLD SALISBURY ROAD C & D LANDFILL SHEET TITLE GROUNDWATER CONTOURS AND SAMPLE LOCATIONS 4. MW-15 IS NOT USED TO DEVELOP THE GROUNDWATER SURFACE SHOWN DUE TO IT BEING 728.56 INSTALLED IN BEDROCK. MW-11 130 . 'o o`ro �MM-11 0 SCALE IN FEET dip 733,C7 1 200 100 0 200 4W 0 v LANDFILL PERMIT BOUNDARY ^ \ MM-12 \ `r 742.92 MVJ-13 PROPERTY LINE 7 — W-4 80 790 764.03 ��AA'N-15 SW-1 800 I B-1 00 ±-\ 82 �g0 • ap0 �qg5 000• 804.59 MW-1 R s. MM-2S MM-2D PROJECT NUMBER 10125427 PROJECT MANAGER M. PLUMMER, P.E. DATE NOV. 2021 REFERENCE SHEET LAYOUT 2 REFERENCE DOCUMENT OOD-03 EXHIBIT NUMBER FIGURE A Figure 1 Groundwater contours and sample locations Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� General 1.4 Geologic Characteristics Regional and site -specific geology and hydrogeology were originally presented in the July 2003 Ground Water Monitoring Plan and the 2003 Design Hydrogeologic Investigation Report. The summaries that follow are taken from those reports. 1.4.1 Regional Geologic and Hydrogeologic Setting As shown on the 1985 Geologic Map of North Carolina, OSR is in the Raleigh Belt of the Piedmont Physiographic Province. This province is characterized by metamorphic and igneous rocks, which have been extensively weathered and eroded, forming an undulating topography. Subsurface conditions generally consist of topsoil underlain by residual soils, saprolite, partially weathered rock (PWR), and bedrock. There is generally a gradual transition between material types with varying thickness. Bedrock in the Raleigh Belt is characterized by numerous plutons with granitic to gabbroic composition that have intruded gneiss, schist, metavolcanic rocks, and metamorphosed mafic complexes (basalt, gabbro, and ultramafic rocks). Typically, bedrock is overlain by PWR and saprolite. Saprolite retains some of the original (relict) structural features of the parent rock and varies in thickness from a few feet to over 100 feet. The near surface residual soils are formed by physical and chemical weathering of the saprolite and usually do not retain the relict structural features. Groundwater is present within fractures and joints in the bedrock and within the pore spaces of the overlying saprolite and residual soils. Groundwater is primarily recharged by precipitation and commonly located within the saprolite layer. Groundwater moves laterally toward streams and surface water bodies and generally follows the surface topography. 1.4.2 Site Specific Topography and Drainage Surface drainage at OSR generally follows topography and flows toward the South Fork Muddy Creek and its tributaries. A small area on the southeast portion of the site drains south into Miller Creek. Both the South Fork Muddy Creek and Miller Creek flow west where they converge with Muddy Creek and eventually discharge to the Yadkin River. 1.4.3 Site Specific Hydrogeology As documented in the Design Hydrogeological Investigation Report submitted by HDR on December 2, 2003, the uppermost aquifer underlying the facility is comprised of three stratigraphic units. The downward progression of the three units is saprolite transitioning into PWR, then bedrock. Groundwater flows through pore spaces within the saprolite and PWR, while groundwater flow through the bedrock is primarily through fractures. OSR was constructed within the unconsolidated micaceous silty sands and sandy silts produced by the in -situ weathering of the granodioritic parent rock. There is no evidence of discrete flow patterns resulting from relict quartz veins, dikes, healed fractures, or strong preferential alignment of minerals (i.e., foliation). In general, groundwater flows from areas of higher elevation to areas of lower elevation and mimics surface topography. January 2022 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Monitoring Network 2 Monitoring Network The monitoring network consists of 14 groundwater wells and 4 surface water sampling locations. Well construction details are presented in Table 1. Sampling of monitoring wells and surface water locations is conducted on a semi-annual basis, as summarized in Table 2. Groundwater monitoring well MW-1 R is located hydraulically upgradient of the landfill and is considered as the background well for the site. Upstream surface water (SW-1) and downstream surface water (SW-2) samples are obtained from the adjacent stream to the east. Two surface water samples (SW-3 and SW-4) are obtained from the drainage channel in the vicinity of MW- 2R. Surface water sampling location SW-3 is located south of the entrance road near MW-2R; while SW-4 is located on the north side of the entrance road, downstream of SW-3. Table 1 Existing groundwater monitoring well details Depth to Top Of NC State NC State Well Well Top of Screened Casing Ground OSR LF Plane Plane Diameter Depth Screen (ft Interval Screened Elevation Elevation WELL Installed Northing Easting (inches) (ft bgs) bgs) (ft) Interval Geology (ft MSL) (ft MSL) MW-1R 12/27/1995 820,411 1,622,983 2 60 45 15 Granitic saprolite 836.42 833.40 MW-2R 12/29/1995 820,974 1,622,722 2 23 8 15 Granitic saprolite 785.22 781.81 MW-3R 7/7/1999 821,237 1,621,463 2 27 12 15 Granitic saprolite 776.60 772.90 MW-4R 12/28/1995 820,435 1,621,428 2 20 5 15 Granitic saprolite 767.96 765.70 MW-5R 12/29/1995 820,137 1,622,130 2 32 17 15 Granitic saprolite 784.36 782.30 MW-7 12/28/1995 820,886 1,621,424 2 48 33 15 Granitic saprolite 803.66 802.10 MW-8 7/7/1999 821,930 1,621,485 2 27 12 15 Granitic saprolite 762.50 759.80 MW-9 8/11/2004 822,311 1,621,986 2 60 45 15 Sand 790.28 788.04 MW-10 8/10/2004 822,626 1,622,699 2 21 6 15 Sand 738.21 735.70 MW-11 8/10/2004 822,307 1,622,838 2 20 5 15 Sand 732.59 730.35 MW-12 8/9/2004 821,844 1,622,955 2 16 6 10 Silt 739.07 736.41 MW-13 8/9/2004 821,500 1,622,915 2 20 5 15 Sand 751.23 749.19 MW-14 8/11/2004 822,420 1,622,260 2 60 45 15 Sand 783.88 781.44 MW-15 4/6/2012 821,083 1,622,884 2 48.2 33.2 15 Bedrock 802.85 800.58 January 2022 4 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Monitoring Network Table 2 Sampling Parameters and Schedule Method Parameters}' Frequency Monitoring wells Surface water EPA 300.0 Sulfafie9111&.- liiiiiiiiiiiiA 2WAMMLAll All EPA 6010 Trar_e metals WMar All All EPA 7470 Mercury 2xlyear Pesticides: all Fall of odd AI Bone ,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,, years(201} Pesticides recently detected: EPA 8081 4.4`-DDDr 4, -DOT, aid rin, alpha-SHC. delta- MW-1 R. MW-2R, BHC, endosulfan I, endosulfan II. endnn. endrin 2xlyear MW-4. MVO!-7, MVV- None aldehyde, heplachlor, heplachlor epoxide & 10 a MVV-15 methoxychlor EPA 8082 PCBs all None Herblcides: all Fall of odd AN None years (2021) EPA8151 H"Cides previously detected= ..........................,,,,,,.,,,,............................... MW-1 R. MW-2Rr 2,4,5-TP (Silvex), 2.4-D ............. year MVV-4R & MW-15 None App I VOCs, tetrahydrofuFan 2xlyear 1 r4-dioxane EPA 8200 Appendix II 1/CCs- All pp FaI of c-dd None ,,,1,„ years D2 """ ., Appendix II UCCs recently detected: None,,,, Bich lorodillucrorrnethane SVOCs: All Fall of odd Ail None years(2021,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,,, _ EPA 8270 SVOCs recently detected: benzo(a)anlhracene, ly W-11R, MW-2R. bi5(2-6thylhexyl)phthalate. chrysene, 2xfyear MW-3R, MVV-4R & W-2 dibenZ(arh)anlhracener & indeno(1,2,3-Cd)pyrene MVV-15 SM 232013 ...... A1..k...a...Mn.l.....ty ................ ,,,,.....2xf....ye.......ar ............. ......... ..........,,,,� AA SM 2540C Total dissolved solids 2xlyear Al All SM 4500 Chloride, cyanide. sulfide T 2xfyear All Field Temperature, specific conductancer dissolved 2xfyear Al All oxygen, redox, turbidity. pH Field Total well depth, static water level 2xfyear WEN NA NA - Not applicable January 2022 5 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Data Collection 3 Data Collection 3.1 Water Level Measurements On November 8, 2021, static groundwater level measurements were obtained from the 14 existing groundwater monitoring wells, MW-1 R through MW-15 (MW-6R was abandoned). Groundwater depths were measured to the nearest 0.01 foot from the top of the PVC casing prior to purging each well. Depth to water data was used to calculate static groundwater elevations for the current sampling event (Table 3). Historic groundwater elevations are presented in Table 4 and depicted on Figure 2. Table 3 Groundwater Measurements and Elevations - November 8, 2021 Well ID Top of Casing Elevation (ft) Ground Surface Elevation (ft) Depth to Water (ft) Groundwater Elevation (ft) Mw-1 R 836.42 833.40 31.83 804.59 M W -2 R 785.22 781.81 7.82 777.40 Mw-3R T76.60 772.90 16.8 759.80 MW-4R 767.06 765.70 5.55 762.41 MW-SR 784.36 782.30 10.13 774.23 MW-7 803.66 802.10 31.54 772.12 Mw-8 762.50 759.80 16.31 746.19 MW-9 790.28 788.04 48.6 741.68 Mw-10 73821 735.70 11.31 726.90 MW-11 732.59 730.35 4.03 728.56 MW-12 739.07 736.41 5A 733.67 MW-13 751.23 749.19 8.31 742.92 MW-14 783.88 781.44 49.68 734.20 MW 15 832 r.� 800.58 38.82 764.03 Table 4 Historic Groundwater Elevations Well ID 17-Nov 18-May is -Nov 19-May 1"nv 20-May 20-Nov 21-May MW-1Ra 801.59 800.85 801.34 802.55 803.08 803.E 804.27 803.93 M-2R 777 777.39 777.75 778.47 777.35 778.53 778.25 779.14 MW-3111' 7562 757.57 760.08 762.49 759.64 763.59 762.36 764.09 MW-4R 759.064 759.6 759.94 762.32 761.04 763.11 763.05 764.94 MW-5111 73-35 773.56 774.95 773.89 775.06 774.85 775.78 MW-7 767.01 766.57 767.21 789.41 769.81 771_15 771.86 773.16 IAW-8 6 747.73 752.07 746.75 7M-13 750.54 752.58 (41VV-9 737.45 736.82 736.9 738.65 739.68 740 740.78 741.14 MW-10 r�M-57 726.7 727.98 726.64 727.78 727.33 728.32 M -11 728.22 728.81 729.27 728.96 729-99 729.22 729.37 730.05 MW-12 733.nM34.46 734.E 734.13 734.26 734.52 734.45 735.24 M-13 742.19 742.75 743.34 743.15 742.87 743.36 743.47 744.16 MW-14 73� 731.60 731.94 733-39 733-3 733.78 734.03 734.65 A MW-15 763_48 763.71 764.08 765.11 763.87 765.04 764.62 765.58 January 2022 6 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Data Collection 810 800 E m a° 790 m m 780 c 0 770 m W m 760 cc t 750 0 730 720 1s3 Aa 0 0 0 A$ A° ti� ti1 titi ti3 tiN 15 ti6 -Sl Ns ^r9 Z� fti tti 113 Vag` Val` �a1` yap` 0a1 0a1 0a1 Nat- 0a1 Nat Nab` Nab` �Sll a� Nay` �a'` dal` Na"` 0,11 Ocl Ocl Sample Date Figure 2 Historical groundwater elevations tM W-1R f M W-2R --t-- M W-5R tM W-6R --4--M W-7 M W-15 —X—M W-4R —4rM W-3R —8--M W-8 M W-13 M W-9 M W-12 M W-14 fMW-11 tMW-10 Hydraulic gradients were calculated between representative well pairs positioned apparently perpendicular to groundwater flow. The flow velocities have been calculated based on the historic average hydraulic conductivity of 0.466 ft/day for the PWR material and an effective porosity of 25 percent, as presented in Table 2-9 of the December 2003 OSR Design Hydrogeologic Investigation Report. Historically (based on data from May 2003), estimated groundwater flow velocities ranged from approximately 10 feet per year (ft/yr) from well MW-13 to MW-10 to approximately 49 ft/yr from well MW-2R to MW-15. Estimated groundwater flow velocities for this sampling event ranged from 9 ft/yr to 47 ft/yr between the same well pairs. Historic and recent groundwater flow velocities are presented in Table 5. Table 5 Interwell Flow Min. Velocity fty r Based on Historic Record JA"• Range of Travel Time velocity r {Years) Nov 2D18 May 2019 Flow Velocity ftyrj Nov 2019 May 2020 Nov 2020 May 2021 Nov 2021 M MW-4R �R 17 18 s2.8 1e 18 1 a 18 18 17 1 a A4W-1R to MW2R 22 30 20.8 28.2 26 2U 28 28 29 27 30 Mw-2Rto M W-13 41 44 42 43 42 43 42 42 42 h4W-13 to MW 10 9 10 1161 127.3 10 10 7 1D 7 10 Mw-2R to M W-15 ¢� 419 47 47 47 48 47 47 January 2022 7 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Data Collection 3.3 Sample Collection and Analysis HDR collected samples from the 14 wells and 4 surface water locations between November 8 and 12, 2021. Groundwater was purged and sampled from each well using low -flow sampling techniques until stabilization of field parameters (pH, conductivity, redox, temperature, turbidity, and dissolved oxygen) was achieved. Samples were collected using dedicated QED TM MicroPurge® pumps that were installed in August 2004, except MW-15, which is sampled with a variable speed submersible pump. Field parameters were recorded and are presented in Appendix C. Surface water samples were collected from locations outside of the landfill boundary to evaluate potential groundwater to surface water interaction. Surface water locations SW-1 through SW-4 were sampled during the November 2021 event. Prior to sample collection, field parameters (pH, conductivity, redox, temperature, turbidity, and dissolved oxygen) were measured with a water quality meter and recorded on field data sheets (Appendix C). Samples were labeled with the project name, sample ID, date, and time the sample was collected. This same information was recorded on a chain -of -custody form. The samples were placed in a cooler with ice, then transported under chain -of -custody protocol to Pace Analytical Services, LLC (Pace) in Huntersville, North Carolina (NC Wastewater Cert. #12) for analysis. January 2022 Table 6 - Lab Detections Parameters 213 Standards • • Well ID MW-1R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4 FBA Sulfate 250,000 250,000 503 42,200 977 174,000 8,380 36,800 8,300 2,140 165,000 11,900 87,600 22,300 <1,000 25,500 7,440 13,900 21,800 66,700 <1,000 Antimony Arsenic 5,300 150 1 10 <5.0 <10.0 <5.0 <10.0 <5.0 <10.0 <5.0 <10.0 <5.0 <10.0 <5.0 <10.0 <5.0 <10.0 <5.0 5.1 <10.0 <5.0 <10.0 <5.0 <10.0 <5.0 <10.0 <5.0 <10.0 <5.0 <10.0 <5.0 8.5 <5.0 8.3 <5.0 <10.0 <5.0 <10.0 <5.0 <10.0 Barium 21,000 700 274 397 259 203 56.3 192 57.6 181 109 95.6 145 514 272 16.1 535 92.5 278 202 <5.0 Beryllium 6.5 4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.4 <1.0 <1.0 2.0 <1.0 <1.0 <1.0 <1.0 Cadmium NE 2 0.58 0.44 0.46 0.66 <1.0 0.82 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.48 <1.0 <1.0 <1.0 <1.0 Chromium 11 10 <5.0 5.8 <5.0 3.7 7.1 <5.0 4.9 <5.0 6.1 5.2 <5.0 <5.0 4.1 <5.0 24.8 <5.0 <5.0 <5.0 <5.0 Cobalt Copper NE NE 1 1,000 <5.0 <5.0 6.0 <5.0 •. <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 4_4 <5.0 <5.0 <5.0 <5.0 <5.0 4_3 <5.0 <5.0 <5.0 <5.0 13.0 13.8 <5.0 <5.0 4.5 <5.0 <5.0 <5.0 <5.0 <5.0 Iron Lead 1,000 NE 300 15 <50.0 <5.0 iiiiiiiiiii <5.0 <5.0 <5.0 196 <5.0 87.9 <5.0 60.9 <5.0 167 <5.0 5.3 <5.0 <5.0 238 <5.0 <5.0 166 <5.0 69,000 18.3 1,500 <5.0 26,700 <5.0 3,110 <5.0 <50.0 <5.0 Manganese NE 50 28.7 qIIIME <5.0 3_9 L 1 11 1,250 549 5,640 6,400 <5.0 Nickel 25 100 <5.0 17.7 <5.0 13.9 <5.0 <5.0 <5.0 <5.0 12.5 3.6 10.2 11.3 9.6 <5.0 12.2 3.5 7.4 8.8 <5.0 Silver NE 20 <5.0 7.3 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 9.6 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Sodium NE NE 15,000 59,400 2,010 92,000 13,300 18,400 11,200 18,900 92,900 12,300 23,300 18,300 18,800 15,700 17,900 15,300 26,100 42,400 <5,000 Vanadium Zinc NE NE 0.3 1,000 <5.0 <10.0 <10.0 <10.0 <10.0 <10.0 <5.0 9_8 <5.0 <10.0 <5.0 <10.0 <10.0 10.0 <10.0 <5.0 11.1 11.3 <5.0 11.2 65.8 70.2 4.5 <10.0 35.3 <10.0 38.4 <10.0 <5.0 <10.0 Mercury 0.012 1 <0.20 <0.20 <0.20 <0.20 <0.20 0.35 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 4,4'-DDE NE NE <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 0.177 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 INS INS INS INS <0.0500 Hexachlorobenzene NE 0.02 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 <0.0500 INS INS INS INS 0.0305 2,4-Dichlorophenoxyacetic acid (2,4-D) 70 70 <2.00 <2.00 <2.00 <2.00 <2.00 <2.00 <2.00 <2.00 <2.00 <2.00 2.86 <2.00 <2.00 <2.00 INS INS INS INS <2.00 1,1-Dichloroethane NE 6 <1.0 <1.0 <1.0 <1.0 <1.0 0.92 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1,4-Dichlorobenzene NE 6 <1.0 0.67 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Benzene 1.19 1 <1.0 <1.0 <1.0 <1.0 0.69 <1.0 <1.0 0.47 <1.0 0.41 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Chloroethane NE 3,000 <1.0 4.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 cis-1,2-Dichloroethene NE 70 0_8 1.3 <1.0 <1.0 <1.0 0.83 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Dichlorodifluoromethane NE 1,000 <1.0 0.74 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Ethylbenzene 97 600 0.37 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 lodomethane NE NE <20.0 9.9 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 <20.0 m&p-Xylene 670 500 <2.0 <2.0 <2.0 <2.0 <2.0 0.74 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 Methylene Chloride 11,000 3 <5.0 2_2 <5.0 <5.0 <5.0 3_0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 o-Xylene NE 500 <1.0 <1.0 <1.0 <1.0 <1.0 0.48 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Tetrachloroethene 0.7 0.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.55 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Tetrahydrofuran 3,100 2,000 <10.0 19.5 <10.0 14.7 <10.0 68.8 <10.0 <10.0 65.1 <10.0 <10.0 12.7 <10.0 4_8 <10.0 <10.0 <10.0 9_6 <10.0 Trichloroethene 2.5 3 <1.0 1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Trichlorofluoromethane NE 2,000 <1.0 0.61 <1.0 <1.0 <1.0 4.4 <1.0 0.38 <1.0 <1.0 <1.0 <1.0 1.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Vinyl Chloride NE 0.03 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1,4-Dioxane (p-Dioxane) NE 3 <2.0 <2.0 <2.0 2.4 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 3.3 <2.0 7.4 <2.0 Alkalinity, Total as CaCO3 20,000 NE 88,700 782,000 63,100 585,000 32,000 85,000 30,000 33,800 734,000 81,300 296,000 93,800 63,000 104,000 71,400 111,000 379,000 453,000 <5,000 Dissolved Solids Chloride NE 1 230,000 500,000 250,000 152,000 9,750 46,800 129,000 2,360 ill pipTotal • . � 61,500 165,000 14,100 207,000 10,000 84,000 3,800 145,000 3,640 �� 43,900 176,000 8,460 489,000 22,400 276,000 49,800 160,000 3,650 247,000 37,700 199,000 24,400 202,000 21,900 477,000 25,100 644,000 50,000 <25,000 <1,000 Cyanide 1 5 70 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <80.0 <8.0 7_8 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 Notes: Methods used for analysis include: EPA 300.0, EPA 6010D, EPA 7470A, EPA 808113, EPA 8151, EPA 8260D, EPA 8260D Mod., SM 232013, SM 2540C, SM 4500-CL-E, and SM 4500-CN-E All Concentrations reported in pg/L • Concentration Exceeds 2L Standards Yellow Highlight: Concentration Exceeds 213 Standards Italics: Estimated Concentration below the Method Reporting Limit (MRL) but above the Method Detection Limit (MDL) (J-flag). INS: Not Sampled This page intentionally left blank. Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Analytical Results 4 Analytical Results 4.1 Groundwater During this sampling event, 41 detections met or exceeded the 2L Standards. These exceedances consisted of 10 parameters (VOCs, metals, pesticides, herbicides, and TDS) at 12 well locations. Appendix II semi-volatiles were last detected in groundwater samples during the November 2017 sampling event. Concentrations of constituents detected during this sampling event are presented in Table 6. Historical detections are presented in Appendix A. A copy of the laboratory report is provided in Appendix B. Static water levels and field parameters recorded prior to sample collection are presented in Appendix C. An electronic file containing the analytical data in NCDEQ electronic data deliverable format will be submitted to NCDEQ electronically. In 2011, concentrations of benzene and tetrachloroethene (PCE) above 2L Standards in well MW-2R triggered assessment monitoring. During this event, MW-2R exceeded the 2L Standard for 1,4-dioxane, benzene, and vinyl chloride. The trends of constituents in MW-2R detected above the current standard and select constituents of concern are shown on Figure 3. January 2022 10 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Analytical Results Select MW-2R Groundwater Detections OSR Construction & Demolition Landfill Permit 34-12 1000000 100000 10000 c m U c 100 U 10 1 0.1 i I I— I I I I I I I I I I I 11 N-Slaa10 �01' NS 1 D�A 1 �5 1 a6 1 �11 �0 10 "0 �� L" �2a a2O Date Collected Figure 3 MW-2R groundwater detections —*--Total Dissolved Solids —Alkalinity, Total as CaCO3 Sulfate Sodium --X---Chloride Manganese —� I ron Barium --@--Tetrahydrofuran —Cobalt 04 Selenium ♦ Antimony o Thallium - Chromium x Arsenic —Methylene Chloride —e-1,4-Dioxane(p-Dioxane) —1FBenzene x Lead $Vanadium - 6 Tetrachloroethene Vinyl chloride f bis(2-Ethylhexyl)phthalate ■ Cadmium - 4,4'-DDT Heptachlor Chlorom ethan e O delta-BHC * Aldrin alpha-BHC 4.2 Surface Water Surface water analytical results were compared to 15A NCAC 02B (213 Standards). Note that there are no 2B Standards for alkalinity, iron, tetra hydrofuran, or 1,4-dioxane. Therefore, EPA Nationally Recommended Water Quality Criteria for Class C freshwater (Class C Standards) were applied, where applicable. • Concentrations of chromium, iron, and alkalinity reported in sample SW-1 exceeded applicable criteria. • Concentrations of iron and alkalinity in samples SW-2, SW-3, and SW-4 exceeded applicable criteria. • 1,4-dioxane was detected in SW-2 and SW-4. However, there is no 213 Standard or EPA Class C Standards for this constituent. Laboratory data for surface water samples collected during the current monitoring event are included in Appendix B. January 2022 11 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Summary 4.3 Landfill Gas Landfill gas was measured at MW-2R and wells in the vicinity of MM-1 during the current sampling event. Measured carbon dioxide (CO2) and oxygen (02) levels exceeded ambient levels in MM-1 during the current monitoring event. These levels are consistent with historic levels, as shown in Table 7. Gas field readings are included in Appendix C. Note that the City is responsible for quarterly sampling of all methane monitoring wells and related reporting, which is not included in this document. Table 7 Gas readings Date ID # H2S ppm CH4 N CO2 N 02 N 12-Nov-19 MM-1 0.0% 12-Nov-19 MW-13 0.0% 0.0% 21.1 % 12-Nov-19 MW-15 0.0% 0.2% 20.7% 12-Nov-19 MW-1 R I 0.0% 0.0% 21.1 % 12-Nov-19 MW-2R 0.0%-4 0.0% 21.0% 4-May-20 MM-1 1 0.0% 4•% 15.6% 4-May-20 MW-13 0 0.1% 0.1% 20.9% 4-May-20 MW-15 I 0 0.0% 0.2% -1 21.2% 4-May-20 MW-1 R 0.0% 0.1% 20.9% M 4-May-20 W-2R I 0 0.0% 0.1% L 20.7% 3-Nov-20 MM-1 0.0% 1.5% 19.2% 3-Nov-20 MW-1 R 0.0% 0.1 % 20.7% 3-Nov-20 MW-2R T 0.0% 0.1% 20.4% 3-Nov-20 MW-13 0.0% 0.2% 21.0% 3-Nov-20 MW-15 0.0% 0.5% 20.3% 11-May-21 MM-1 0.0% 1.3% ' 11-May-21 MW-1 R 0.0% 0.2% 21.1 % 11-May-21 MW-2R 0.0% 0.1% 20.8% 11-May-21 MW-13 0.0% 0.1% 21.0% 11-May-21 MW-15 I 0.0% 0.2% 21.1% 8-Nov-21 MM-1 0.0% 4.3% 18.2% 8-Nov-21 MW-1 R I 0.0% 0.2% 21.2% 8-Nov-21 MW-2R 0.0% 0.5% 20.8% 8-Nov-21 MW-13 0.0% 1.3% 20.8% 8-Nov-21 MW-15 0.0% 0.4% 20.8% Notes: Normal atmospheric range for CO2 is 0.0% to 1.3%. Normal atmospheric range for 02 is greater than 19.5% Highlighted cells are outside of normal atmospheric ranges 5 Summary • During this sampling event, 41 detections (10 parameters at 12 well locations) exceeded the 2L Standards in groundwater samples. In general, the quantity of detections and magnitude of concerntrations are consistent with results from previous events. • Chromium excceded the 2B Standard in SW-1. • Alkalinity and iron exceeded the Class C Standards in SW-1 through SW-4. • Tetrahydrofuran was detected below Class WS and Class C Standards. January 2022 12 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Recommendations • 1,4-dioxane was detected in SW-2 and SW-4. However, there is no 2B Standard or EPA Class C Standards for this constituent. • Results of limitied landfill gas monitoring conducted during this event indicate that the concentrations of carbon dioxide and oxygen in MM-1 were outside of ambient levels. These measurements are consistent with previous readings at this monitoring location. Methane concentrations in the wells and monitoring points did not exceed the lower explosive limit (LEL) of 5.0 percent during this event. 6 Recommendations Based on the results of groundwater, surface water, and landfill gas monitoring conducted during this semi-annual event, recently detected Appendix II VOCs will be updated to include the constituents listed below: • 1,1-Dichloroethane • 1,4-Dichlorobenzene • Benzene • Chloroethane • cis-1,2-Dichloroethene • Dichlorodifluoromethane • Ethylbenzene • lodomethane • m&p-Xylene • Methylene Chloride • o-Xylene • Tetrachloroethene • Tetrahydrofuran • Trichloroethene • Trichlorofluoromethane • Vinyl chloride SVOCs were not detected during this event and therefore will not be sampled until fall of 2023. January 2022 13 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report Appendix A — Summary of Monitoring Results 1-tv---,*IF Appendix Summary � pp Y of i. Monitoring Results Detections of Concern Groundwater Detections by Well Location Surface Water Detections Historical Detections by Date Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results This page intentionally left blank. Al 50 pg/L 50 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L NE pg/L NE pg/L 40 pg/L 40 pg/L 40 pg/L 0.008 pg/L 0.008 pg/L 0.004 pg/L 0.004 pg/L NE pg/L NE pg/L NE pg/L NE pg/L 200 pg/L 200 pg/L 1000 pg/L 1000 pg/L 0.005 pg/L 0.005 pg/L 0.005 pg/L 100 pg/L 100 pg/L 100 pg/L 0.05 pg/L 0.05 pg/L 0.05 pg/L 6 pg/L 6 pg/L 6 pg/L 0.4 pg/L 0.4 pg/L 6 pg/L 6 pg/L Facility Permit34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Value Column N Labels N N N W r r n n c0 Row Labels Herbicides O z 2 O z 2 O z @ � O z 2 a)O o z 2i O z c N 2 O z cu 2 MCPP Pesticides Heptachlor Heptachlor epoxide MW-10 �---------- ■..0.09 ■ - . i. I . -■■■■■■■■■■■■■■®■ Butylbenzylphthalate q -■■■■■■■■®■■■■■■■ SW-2 NEEMENNEENNEENNE11 2 • NEENNEENEENEENEEN . .. W-S GW Revised.xlsb 1 of 4 Al 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 40 pg/L 40 pg/L 40 pg/L 40 pg/L NE pg/L NE pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 700 pg/L 700 pg/L 3000 pg/L 3000 pg/L 3000 pg/L 70 pg/L 70 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L Facility Permit34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Value Column Labels '• 1,4-Dioxane p-Dioxane MW-2R 2.3 2.1 MW-4R 2.4 MW-7 2.4 1.5 1.5 2.2 1.8 2 MW-10 MW-12 1.9 2.6 MW-13 SW-2 2.5 2.2 2.7 1.3 SW-3 1.3 SW-4 2-Hexanone MW-10 0.72 0.69 1 SW-2 1.8 SW-4 3.1 4-Meth I-2-pentanone MIBK MW-10 0.65 1.7 1.1 2.8 2.5 2.6 5.6 Acetone MW-2R 10.3 MW-3R 21.4 MW-4R 11 MW-5R 18.4 M W-7 15.7 M W-8 15.8 MW-10 16.4 13.7 12.1 22.5 14.1 11.8 MW-11 21.1 MW-12 12.1 MW-13 17.3 MW-14 14.7 MW-15 13.2 SW-1 11.2 SW-2 12.9 SW-3 16.2 SW-4 16 Benzene MW-2R MW-4R 0.38 MW-5R 0.28 MW-7 0.69 0.6 0.64 0.48 0.6 0.68 0.37 0.41 0.39 0.38 0.43 0.42 0.26 0.3 MW-10 0.47 0.48 0.56 0.78 0.33 0.55 0.55 0.57 0.52 0.83 0.5 MW-12 0.41 0.37 0.29 0.25 0.33 SW-3 0.73 0.42 SW-4 0.99 0.25 Carbon Disulfide MW-10 2.1 2 5.2 Chloroethane MW-2R 4.3 MW-7 0.85 Chloroform MW-15 0.45 0.44 0.44 0.4 0.44 0.7 0.44 0.3 Chloromethane MW-2R 0.25 MW-7 0.1 MW-11 0.23 SW-2 0.12 cis- 1,2-Dichloroethene MW-1 R 0.8 1.3 1.2 1.2 1.1 0.9 0.85 0.71 0.76 0.62 0.38 0.2 MW-2R 1.3 1.2 0.58 0.84 0.95 0.67 0.38 0.55 0.66 0.6 0.51 0.47 0.26 MW-7 0.83 0.74 1.7 0.91 1.4 1.5 0.86 0.85 1.1 1.1 1.1 1.1 0.77 0.8 0.7 MW-10 0.23 0.27 0.23 0.2 0.33 MW-12 0.4 0.23 SW-2 0.33 SW-3 0.26 W-S GW Revised.xlsb 2 of 4 Al 70 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 600 pg/L 600 pg/L 600 pg/L NE pg/L NE pg/L 500 pg/L 500 pg/L 500 pg/L 500 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 500 pg/L 500 pg/L 500 pg/L 500 pg/L 500 pg/L 0.7 pg/L 0.7 pg/L 0.7 pg/L 0.7 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 600 pg/L 600 pg/L 600 pg/L 600 pg/L 600 pg/L 600 pg/L 600 pg/L 600 pg/L Facility Permit34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Value Column Labels '• SW-4 1.1 0.32 Dichlorodifluoromethane MW-2R 0.74 0.26 MW-7 0.52 0.62 1 MW-9 1.1 0.57 1.1 0.9 1.4 0.99 1.2 1.7 1.2 1.5 0.88 0.76 MW-12 0.23 MW-14 3.7 4.1 2.4 2.4 4.5 3 2.4 3 3.6 3.9 3.6 2.3 3.6 2.1 Eth (benzene MW-1 R 0.37 0.34 0.38 MW-10 0.41 0.53 0.55 0.4 1 lodomethane MW-2R 9.9 m&p-X lene MW-5R 0.73 MW-7 0.74 0.95 0.72 0.93 1 1.1 1.7 1.6 1.4 1.2 2.2 1.8 0.84 1.5 MW-10 0.68 1.3 1.1 1.2 2.1 0.68 1.2 Methylene Chloride MW-1 R 2.3 MW-2R 2.2 1.1 1.3 2.3 MW-3R 2.3 MW-4R 2.9 MW-5R MW-7 1.7 2.1 MW-8 1.1 MW-10 2.8 1.2 MW-11 1.4 MW-12 2 2 MW-14 1.6 MW-15 2.4 SW-1 2 SW-2 SW-3 1 SW-4 1.2 o-Xylene MW-5R 0.45 MW-7 0.48 0.46 0.66 0.46 0.54 0.68 0.59 0.65 0.62 0.68 0.46 0.63 0.47 0.27 0.4 MW-10 0.34 0.84 0.28 0.53 0.78 1.1 0.97 1 2.1 0.43 0.9 MW-11 0.27 Tetrachloroethene OM MW-2R MW-7 0.48 MW-14 0.55 0.68 0.65 0.53 0.48 0.52 0.61 Tetrahydrofuran MW-2R 19.5 25.2 12.9 38.6 83 51.3 45.4 46 59.1 28 36.3 39.1 49.6 35.8 35 MW-4R 14.7 16.8 13.4 11.4 8.6 11.4 9.3 13.6 3.5 7 5.8 MW-7 68.8 77.5 90.9 70.5 77.9 80.4 50.5 24.9 20.1 32 21.7 13.5 17.7 14 MW-10 65.1 89.1 69.6 130 141 113 169 192 135 131 182 237 6.1 120 145 MW-11 4.5 MW-12 5.9 11.4 26.8 12.4 MW-13 12.7 11.4 MW-15 4.8 6.5 8.9 8.2 9.2 14.8 12 16.8 27.3 19.8 17 SW-2 61.3 SW-3 6.1 3.4 6.3 3.3 SW-4 9.6 5.5 3.5 9.1 6.7 13.7 5.7 3.5 3.6 4.1 Toluene MW-2R 0.27 MW-5R 1.7 MW-10 0.26 0.35 0.27 0.6 MW-11 1 MW-12 0.74 MW-13 0.58 SW-2 0.52 W-S GW Revised.xlsb 3 of 4 Al 3 pg/L 3 pg/L 3 pg/L 3 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 88 pg/L 88 pg/L 0.03 pg/L 0.03 pg/L 500 pg/L 500 pg/L Facility Permit34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Value Column Labels '• Trichloroethene MW-1 R 0.65 MW-2R 1 1.4 1 1.1 1.1 0.97 0.9 0.93 1.3 0.93 1 1.2 0.71 0.66 0.8 MW-7 0.58 Trichlorofl uoromethane MW-2R 0.61 0.61 1.5 0.71 1 1.5 MW-7 4.4 10.2 5.4 5.6 4 2 1.2 1.2 1.6 1.6 0.91 1.5 0.92 1.4 0.8 MW-9 0.38 1.2 0.66 1.3 0.86 1.7 1.3 1.3 1.4 1.2 1.4 1 1.3 1.1 1 MW-12 0.81 1 0.89 1.4 0.52 1 2.8 1.4 0.82 0.2 MW-14 1.7 2.5 1.6 1 1.5 0.92 0.86 0.79 0.8 0.87 0.75 0.58 1.1 0.54 0.6 MW-15 0.21 0.42 0.22 0.71 2.1 4.4 5.1 4.8 4.4 SW-4 0.32 Vinyl acetate MW-2R 2 Vinyl chloride MW-2R X lenes Total MW-10 1.1 W-S GW Revised.xlsb 4 of 4 A2 NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 5 pg/L 70 pg/L 70 pg/L 600 pg/L 300.0 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 3 pg/L 1000 pg/L 6 pg/L 350 pg/L 0.4 pg/L 6 pg/L 3 pg/L 50 pg/L 70 pg/L NE pg/L NE pg/L 4000 pg/L 40 pg/L 0.1 pg/L 6000 pg/L 0.002 pg/L NE pg/L 0.006 pg/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 3 pg/L 2 pg/L 250000 pg/L 3000 pg/L 70 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 1000 pg/L 2 pg/L 2 pg/L 0.008 pg/L NE pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L NS pg/L 40 pg/L 3 pg/L 6 pg/L 100 pg/L NS pg/L 500 pg/L 20 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Labels Historical detections by well location ,M W-1 R Alkalinity, Total as CaCO3 88700 91100 90800 86600 84000 83800 84100 76100 71400 Arsenic 5.8 Barium 274 271 291 290 290 285 284 263 260 Benzo(a)anthracene Beryllium 0.5 bis(2-Ethylhexyl )phthalate Cadmium 0.58 Carbon Disulfide Chloride 9750 9990 9610 9050 9150 9770 8920 9040 9290 Chromium 4 Chrysene cis-1,2-Dichloroethene 0.8 1.3 1.2 1.2 1.1 0.9 0.85 0.71 0.76 0.62 Cyanide Ethylbenzene 0.37 0.34 Iron 81.8 111 43.1 Lead Manganese 28.71 31.41 32.3 31.41 24.7 19.51 16.7 17.6 11.8 Mercury 0.57 0.34 0.23 Methylene Chloride Nickel 1.5 Selenium Silver Sodium 15000 15000 15900 16800 16300 15800 16500 15500 15200 Sulfate 503 1130 Toluene Total Dissolved Solids 152000 160000 153000 172000 180000 202000 164000 166000 153000 Trichloroethene 0.65 Zinc 4.3 5.2 5.1 5 MW-2R 1,1-Dichloroethane 0.39 0.46 0.6 0.43 0.39 0.54 0.48 0.48 1,1-Dichloroethene 1,2-Dichloroethane 0.24 1,4-Dichlorobenzene 0.67 0.52 0.51 0.56 0.45 0.41 0.37 0.46 1,4-Dioxane (p-Dioxane) 2.3 2.1 2,4,5-TP (Silvex) 0.072 2,4-D 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Butanone (MEK) 2-Hexanone 4,4'-DDT Acetone 10.3 Aldrin Alkalinity, Total as CaCO3 782000 692000 765000 688000 736000 577000 573000 663000 670000 587000 alpha-BHC Antimony Arsenic 4.8 Barium 397 299 317 309 359 260 258 289 323 323 Benzene bis(2-Ethylhexyl )phthalate Cadmium 0.44 0.45 0.66 Chloride 46800 50400 49300 64300 52500 42300 34500 42200 47600 50400 Chloroethane 4.3 Chloroform Chloromethane Chromium 5.8 3.3 2.7 cis-1,2-Dichloroethene 1.31 1.21 0.58 0.841 0.951 .671 0.381 0.551 0.66 0.6 0.51 Cobalt • 0 . 6 6.5 18.6 9.6 2.6 Copper Cyanide 4.1 5 delta-BHC Dichlorod'Ifluoromethane 0.74 Endrin Endrin aldehyde Heptachlor lodomethane 9.9 Iron 7700 5270 3360 3650 • •0 690 090 60 8 1 3.2 Lead m&p-Xylene Manganese 20100 13500 13200 11300 12700 8240 8920 10300 1.11 • �� Mercury Methane Methoxychlor Methylene Chloride 2.2 1.1 Naphthalene Nickel 17.7 14 19.4 21.1 21.1 13.4 16.1 16.8 20.3 17 Nitrogen, Ammonia o-Xylene Selenium 6.1 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 5 pg/L 70 pg/L 70 pg/L 600 pg/L 300.0 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 3 pg/L 1000 pg/L 6 pg/L 350 pg/L 0.4 pg/L 6 pg/L 3 pg/L 50 pg/L 70 pg/L NE pg/L NE pg/L 4000 pg/L 40 pg/L 0.1 pg/L 6000 pg/L 0.002 pg/L NE pg/L 0.006 pg/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 3 pg/L 2 pg/L 250000 pg/L 3000 pg/L 70 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 1000 pg/L 2 pg/L 2 pg/L 0.008 pg/L NE pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L NS pg/L 40 pg/L 3 pg/L 6 pg/L 100 pg/L NS pg/L 500 pg/L 20 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location •MW-1R Alkalinity, Total as CaCO3 68600 64300 54900 48100 39600 37600 30000 28100 29800 26300 27100 27500 Arsenic Barium 272 241 228 207 164 142 124 106 109 91.7 93.8 82.6 Benzo(a)anthracene Beryllium bis(2-Ethy1hexyl)phthalate 2.4 Cadmium Carbon Disulfide Chloride 8860 9630 9000 8510 7640 7090 5600 5880 5910 5320 5350 Chromium Chrysene 1.5 cis-1,2-Dichloroethene 0.38 0.2 Cyanide 4.4 Ethylbenzene 0.38 Iron 54.8 96.2 78.8 82.8 85.8 52.9 Lead Manganese 12.5 7.3 7.2 2.8 2.9 Mercury Methylene Chloride 2.3 Nickel Selenium Silver Sodium 15800 14600 13300 13200 11600 10600 10800 9940 9080 9180 9440 7670 Sulfate 1380 1080 1070 1700 1720 Toluene Total Dissolved Solids 165000 154000 138000 78000 133000 120000 91000 103000 84000 95000 93000 95000 Trichloroethene Zinc 5.5 5.7 5.6 MW-2R 1,1-Dichloroethane 0.53 0.49 1.1 0.83 1.3 1.2 1.2 1.1 1,1-Dichloroethene 36.6 1,2-Dichloroethane 1,4-Dichlorobenzene 0.39 0.38 0.4 1,4-Dioxane (p-Dioxane) 2,4,5-TP (Silvex) 0.14 0.23 2,4-D 0.43 1.1 2,4-Dinitrotoluene 5.9 2,6-Dinitrotoluene 8.1 2-Butanone (MEK) 2-Hexanone 0.48 4,4'-DDT Acetone 20.3 Aldrin Alkalinity, Total as CaCO3 571000 482000 440000 358000 453000 344000 349000 363000 277000 196000 alpha-BHC Antimony Arsenic Barium 272 324 279 287 339 324 311 324 335 366 Benzene 1.1 bis(2-Ethy1hexyl)phthalate Cadmium Chloride 47600 47700 48700 44200 49800 50500 56700 50000 64000 61500 Chloroethane 2.1 Chloroform 0.16 Chloromethane 0.25 Chromium 2.8 2.6 3.4 cis-1,2-Dichloroethene 0.47 1 0.261 0.51 0.381 0.41 0.261 0.251 0.33 Cobalt 6.3 9.6 Copper Cyanide 5.1 7.5 4.2 delta-BHC Dichlorodifluoromethane 0.26 Endrin 0.27 Endrin aldehyde 0.23 0.28 Heptachlor I ' lodomethane Iron :� .� �:� .� :� •� 3.3 Lead m&p-Xylene Manganese �•�� •� •r1 ::r • 1 ::1 is :1 Mercury Methane Methoxychlor 0.83 Methylene Chloride 1.3 2.37 0.86 1.3 1.6 1.9 Nickel 18.5 17.9 18 17 25.9 20.6 27.1 20.7 21.8 22.3 Nitrogen, Ammonia o-Xylene 0.33 0.31 0.54 0.54 0.63 1 Selenium 16.5 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 5 pg/L 70 pg/L 70 pg/L 600 pg/L 300.0 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 3 pg/L 1000 pg/L 6 pg/L 350 pg/L 0.4 pg/L 6 pg/L 3 pg/L 50 pg/L 70 pg/L NE pg/L NE pg/L 4000 pg/L 40 pg/L 0.1 pg/L 6000 pg/L 0.002 pg/L NE pg/L 0.006 pg/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 3 pg/L 2 pg/L 250000 pg/L 3000 pg/L 70 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 1000 pg/L 2 pg/L 2 pg/L 0.008 pg/L NE pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L NS pg/L 40 pg/L 3 pg/L 6 pg/L 100 pg/L NS pg/L 500 pg/L 20 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location •M W-1 R Alkalinity, Total as CaCO3 Arsenic Barium 84.7 85.4 85.3 92.8 74.3 85 90.3 105 81 94 82 78 48 95 96.3 460 Benzo(a)anthracene Beryllium bis(2-Ethylhexyl)phthalate Cadmium Carbon Disulfide Chloride Chromium 1.4 0.96 1.4 2 0.88 0.64 0.49 2 3.5 Chrysene cis-1, 2-Dichloroethene Cyanide Ethylbenzene I ron Lead Manganese Mercury Methylene Chloride Nickel Selenium 5.5 Silver 0.51 0.29 0.48 0.62 0.43 Sodium Sulfate Toluene Total Dissolved Solids Trichloroethene Zinc MW-2R 1,1-Dichloroethane 1.2 1.1 1,1-Dichloroethene 38.7 1,2-Dichloroethane 1,4-Dichlorobenzene 1,4-Dioxane (p-Dioxane) 2,4,5-TP (Silvex) 2,4-D 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Butanone (MEK) 2-Hexanone 4,4'-DDT Acetone 3.7 Aldrin Alkalinity, Total as CaCO3 219000 165000 alpha-BHC Antimony Arsenic Barium 351 273 223 103 80.7 88.5 98.8 102 107 79 90 52 62 43 52 55 60 Benzene bis(2-Ethylhexyl)phthalate Cadmium Chloride 62400 39900 Chloroethane Chloroform 0.26 0.36 3.4 Chloromethane Chromium 5.4 0.49 1.2 1.6 0.5 0.79 2.2 cis-1,2-Dichloroethene 0.46 0.26 Cobalt Copper Cyanide delta-BHC Dichlorod'Ifluoromethane Endrin Endrin aldehyde Heptachlor Iodomethane I ron MI Lead m&p-Xylene 0.66 0.74 Manganese r Mercury 0.34 Methane 1280 Methoxychlor Methylene Chloride Naphthalene Nickel 20.9 Nitrogen, Ammonia 0.12 o-Xylene 1.2 0.84 17 Selenium Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 5 pg/L 70 pg/L 70 pg/L 600 pg/L 300.0 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 3 pg/L 1000 pg/L 6 pg/L 350 pg/L 0.4 pg/L 6 pg/L 3 pg/L 50 pg/L 70 pg/L NE pg/L NE pg/L 4000 pg/L 40 pg/L 0.1 pg/L 6000 pg/L 0.002 pg/L NE pg/L 0.006 pg/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 3 pg/L 2 pg/L 250000 pg/L 3000 pg/L 70 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 1000 pg/L 2 pg/L 2 pg/L 0.008 pg/L NE pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L NS pg/L 40 pg/L 3 pg/L 6 pg/L 100 pg/L NS pg/L 500 pg/L 20 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location •MW-1 R Alkalinity, Total as CaCO3 Arsenic 5.8 Barium 120 100 130 280 87 150 110 130 150 160 100 290 100 180 224 Benzo(a)anthracene Beryllium bis(2-Ethy1hexyl)phthalate Cadmium Carbon Disulfide 28 23 Chloride Chromium 4.3 2.3 5 6.6 6.6 5.2 7.8 3 6 Chrysene cis-1,2-Dich loroethene Cyanide Ethylbenzene Iron Lead 10 12 6 Manganese Mercury 0.2 Methylene Chloride Nickel Selenium Silver Sodium Sulfate Toluene 21 Total Dissolved Solids Trichloroethene Zinc MW-2R 1,1-Dichloroethane 1,1-Dichloroethene 1,2-Dichloroethane 1,4-Dichlorobenzene 1,4-Dioxane (p-Dioxane) 2,4,5-TP (Silvex) 2,4-D 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Butanone (MEK) 86 2-Hexanone 4,4'-DDT Acetone Aldrin Alkalinity, Total as CaCO3 alpha-BHC Antimony Arsenic Barium 56 140 100 160 280 61 180 120 150 190 340 200 160 350 Benzene bis(2-Ethy1hexyl)phthalate Cadmium 1.9 Chloride Chloroethane Chloroform Chloromethane Chromium 2.1 3.9 3 7.8 4 9 cis-1,2-Dich loroethene Cobalt Copper Cyanide delta-BHC Dich lorodifluoromethane Endrin Endrin aldehyde Heptachlor lodomethane Iron Lead 7 8.9 6.5 6.9 14 8 m&p-Xylene Manganese Mercury 0.4 Methane Methoxychlor Methylene Chloride Naphthalene Nickel Nitrogen, Ammonia o-Xylene Selenium Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 20 Ng/L NE pg/L 250000 pg/L NE pg/L 0.7 pg/L 2000 pg/L 0.2 pg/L 600 pg/L 500000 pg/L 3 pg/L 2000 pg/L 0.3 pg/L 88 pg/L 0.03 pg/L 500 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 200 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 2000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 1000 pg/L 2 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 42 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 2000 pg/L 0.2 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Labels Historical detections by well location •w Labels Silver o 7.3 o Sodium 59400 52400 59400 65600 71900 57300 64400 73200 77600 72400 Sulfate 42200 53800 70300 76400 111000 85100 95900 105000 122000 110000 Sulfide 82.2 80.1 Tetrachloroethene ' 38.6 83 51.3 45.4 46 59.1 28 Tetrahydrofuran 19.5 25.2 12.9 36.3 Thallium Toluene Total Dissolved Solids • 0000 808000 850000 840000 938000 1150000 726000 888000 :��� • ��� Trichloroethene 1 1.4 1 0.97 0.9 0.93 1.3 0.93 1 Trichlorofluoromethane 0.61 0.61 1.5 Vanadium :424.E Vinyl acetate 2 Vinyl chloride Xylenes (Total) Zinc 18 MW-3R Acetone Alkalinity, Total as CaCO3 63100 78900 81100 70900 69800 488000 192000 115000 78900 Arsenic 6.2 8.5 6.4 5.7 9 Barium 259 246 273 257 286 320 275 234 278 Benzo(g, h, i)perylene Beryllium 0.35 bis(2-Ethylhexyl )phthalate Cadmium 0.46 Carbon Disulfide Chloride 2360 2120 1920 3320 2000 44600 2660 2180 2650 Chromium Cobalt 6.1 Copper Cyanide 6.3 6.4 5 Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene Iron 11 72900 71800 76500 74900 78700 91800 90800 84300 Lead 1 5.11 1 1 3.4 4.9 3.4 Manganese 4140 4440 5020 5640 6180 6850 7940 8100 1 0.65 Mercury Methylene Chloride Nickel 1.2 Selenium 7.8 6.3 Silver Sodium 2010 1850 2120 2150 2520 2540 2770 2680 2380 Sulfate 977 1910 589 801 771 1210 1300 691 Tin 4.8 Total Dissolved Solids 129000 122000 146000 146000 213000 177000 164000 Vanadium Zinc MW-4R 1,4-Dioxane (p-Dioxane) 2.4 4,4'-DDT Acetone 11 Alkalinity, Total as CaCO3 585000 627000 577000 517000 384000 129000 291000 101000 461000 315000 Arsenic Barium 203 168 201 176 166 216 222 270 198 343 Benzene Butylbenzylphthalate 1.7 Cadmium 0.66 0.48 Chloride 61500 53600 52700 42100 34000 2220 25200 12500 49200 35800 Chloromethane Chromium 3.7 6.4 3.2 Cobalt 0 Copper Cyanide delta-BHC Endosulfan II Iron 2100 1930 1430 1080 1020 476 475 3980 Lead Manganese 1220 10600 1080 90 r 584 357 Mercury Methylene Chloride Nickel 13.9 8.8 9.7 8 7.4 8.4 5 4.1 7.5 5.8 Selenium Silver Sodium 92000 79400 84800 73800 62300 71200 42600 17800 65500 42100 Sulfate 174000 180000 189000 162000 122000 163000 104000 50300 179000 125000 Sulfide 105 Tetrahydrofuran 14.7 16.8 13.4 11.4 8.6 11.4 9.3 Thallium 0.029 Total Dissolved Solids 167000 496000 250000 Vanadium ��5'1' Zinc 5.9 5.2 19.9 Highlighted cells are at or above the Current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 20 pg/L NE pg/L 250000 pg/L NE pg/L 0.7 pg/L 2000 pg/L 0.2 pg/L 600 pg/L 500000 pg/L 3 pg/L 2000 pg/L 0.3 pg/L 88 pg/L 0.03 pg/L 500 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 200 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 2000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 1000 pg/L 2 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 42 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 2000 pg/L 0.2 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location P • Silver 5.2 Sodium 70200 61500 61400 51400 58300 59700 46200 45700 43400 38400 Sulfate 121000 115000 115000 98400 117000 136000 128000 115000 79500 95000 Sulfide Tetrachloroethene 49.6 35.8 34.6 79.2 72.6 99.6 111 93.2 152 Tetrahydrofuran 39.1 Thallium Toluene 0.27 Total Dissolved Solids oil 769000 :06000 632000 .•000 549000 654000 589000 564000 531000 Trichloroethene 1.2 0.71 0.66 0.79 0.85 0.71 0.89 0.68 0.77 0.82 Trichlorofluoromethane 0.71 1 1.5 2.4 3.7 12 12.1 16.9 20.9 Vanadium Vinyl acetate Vinyl chloride I r F12.2 Xylenes (Total) 0.98 1.6 Zinc 5.8 8.7 16.8 21.1 24.5 35.2 MW-3R Acetone 21.4 Alkalinity, Total as CaCO3 114000 133000 87800 102000 107000 177000 155000 155000 175000 142000 150000 Arsenic 5.5 3.9 3.3 8.9 Barium 309 297 278 271 214 221 205 201 216 173 228 Benzo(g,h,i)perylene 1 Beryllium bis(2-Ethylhexyl)phthalate Cadmium Carbon Disulfide Chloride 2520 2050 2470 2990 2990 2940 3260 3620 3860 3920 Chromium Cobalt r Copper 6.2 Cyanide 4.4 4.7 10.4 7.1 8.1 9.1 6.5 Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene Iron • 11 of of �� .��r �r 61 Lead 3.4 3.5 3.8 2.7 2.7 Manganese 6800 7100 7980, 93801 9260 9990 9630 11600 9310 Mercury Methylene Chloride 2.3 Nickel Selenium 5 5.5 Silver Sodium 2240 2450 2310 2590 2770 Sulfate 1530 1800 2200 3000 3740 4230 3400 5070 5420 6860 Tin 5.8 Total Dissolved Solids 133000 168000 188000 137000 182000 191000 187000 193000 175000 172000 168000 Vanadium Zinc 8.7 10.5 MW-4R 1,4-Dioxane (p-Dioxane) 4,4'-DDT Acetone Alkalinity, Total as CaCO3 454000 99000 144000 117000 286000 222000 224000 203000 174000 64300 143000 Arsenic Barium 255 210 184 306 305 264 296 375 400 407 328 Benzene 0.38 0.42 0.28 0.27 B utylbenzylphthalate Cadmium Chloride 58400 13800 16900 22200 50500 29700 36500 33700 34500 33200 29200 Chloromethane Chromium 3.2 Cobalt 4 2.8 Copper Cyanide 4.2 4.3 5.9 delta-BHC 0�.• Endosulfan II 0.12 Iron 214 292 126 89.5 158 145 Lead Manganese 8 515 407 315 1040 Mercury Methylene Chloride 2.9 Nickel 8 3.2 3.7 2.8 7.2 5.3 Selenium 11.5 Silver Sodium 71000 14500 23800 23000 55400 39700 42600 42600 43600 40400 35300 Sulfate 193000 48700 70300 72700 143000 85200 113000 97600 73600 98700 61800 Sulfide Tetrahydrofuran 13.6 3.5 7 5.8 15.9 11.8 11.7 8.5 13.5 8.8 Thallium Total Dissolved Solids M 241000 161000 304000 m s 445000 496000 413000 435000 374000 345000 Vanadium Zinc 8.4 17.8 5.9 7.5 7.2 13.6 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 20 Ng/L NE Ng/L 250000 Ng/L NE Ng/L 0.7 Ng/L 2000 Ng/L 0.2 Ng/L 600 Ng/L 500000 Ng/L 3 Ng/L 2000 Ng/L 0.3 Ng/L 88 Ng/L 0.03 Ng/L 500 Ng/L 1000 Ng/L 6000 Ng/L NE Ng/L 10 Ng/L 700 Ng/L 200 Ng/L 4 Ng/L 3 Ng/L 2 Ng/L 700 Ng/L 250000 Ng/L 10 Ng/L 1 Ng/L 1000 Ng/L 70 Ng/L 0.005 Ng/L 0.05 Ng/L 300 Ng/L 15 Ng/L 50 Ng/L 1 Ng/L 3 Ng/L 100 Ng/L 20 Ng/L 20 Ng/L NE Ng/L 250000 Ng/L 2000 Ng/L 500000 Ng/L 0.3 Ng/L 1000 Ng/L 3 Ng/L 0.1 Ng/L 6000 Ng/L NE Ng/L 10 Ng/L 700 Ng/L 1 Ng/L 1000 Ng/L 2 Ng/L 250000 Ng/L 3 Ng/L 10 Ng/L 1 Ng/L 1000 Ng/L 70 Ng/L 0.019 Ng/L 42 Ng/L 300 Ng/L 15 Ng/L 50 Ng/L 1 Ng/L 3 Ng/L 100 Ng/L 20 Ng/L 20 Ng/L NE Ng/L 250000 Ng/L NE Ng/L 2000 Ng/L 0.2 Ng/L 500000 Ng/L 0.3 Ng/L 1000 Ng/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical RP detections by well location • Silver 5 2.5 0.85 0.67 0.68 0.58 1.2 0.93 Sodium 31800 27200 Sulfate 96300 Sulfide Tetrachloroethene Tetrahydrofuran 197 274 226 Thallium Toluene Total Dissolved Solids 498000 Trichloroethene 0.88 0.65 Trichlorofluoromethane 20.1 31.6 36.1 21.9 22.2 Vanadium Vinyl acetate Vinyl chloride Xylenes (Total) Zinc 33.3 MW-3R Acetone Alkalinity, Total as CaCO3 155000 Arsenic 4 Barium 237 301 302 314 289 252 231 293 273 310 230 290 300 300 340 270 200 Benzo(g, h, i)perylene Beryllium bis(2-Ethylhexyl)phthalate Cadmium 0.82 Carbon Disulfide 26.1 3.3 Chloride Chromium 0.63 2.3 3.7 2.3 Cobalt Copper Cyanide Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene Iron r of Lead 14 Manganese Mercury Methylene Chloride Nickel Selenium 11.8 4.9 18.1 Silver 0.6 0.45 1 0.29 1.5 0.87 Sodium Sulfate Tin Total Dissolved Solids 180000 Vanadium Zinc MW-4R 1,4-Dioxane (p-Dioxane) 4,4'-DDT Acetone Alkalinity, Total as CaCO3 Arsenic 9.2 Barium 126 335 55.9 334 58.3 263 172 287 200 220 220 180 150 140 380 97 Benzene Butylbenzylphthalate Cadmium Chloride Chloromethane 0.15 Chromium 1.3 0.68 1.3 5.4 1.2 0.58 0.4 2.6 Cobalt Copper Cyanide delta-BHC Endosulfan II I ron Lead 4.8 Manganese Mercury Methylene Chloride Nickel Selenium Silver 0.88 1.3 2.4 2.6 0.94 Sodium Sulfate Sulfide Tetrahydrofuran Thallium Total Dissolved Solids Vanadium Zinc Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide 0.7 pg/L Tetrachloroethene 2000 pg/L Tetrahydrofuran 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 88 pg/L Vinyl acetate 0.03 pg/L Vinyl chloride 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-3R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 3 pg/L bis(2-Ethy1hexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon Disulfide 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-4R 3 pg/L 1,4-Dioxane (p-Dioxane) 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 1000 pg/L Butylbenzylphthalate 2 pg/L Cadmium 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.019 pg/L delta-BHC 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide 2000 pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc Old Salisbury Road Landfill (C&D) M � •TM. ffer-M—Ne 1• ma I 611FAM 111618011031 N 0 p. Q O Z 5 N 0 j O Z j O Z . 2 U O R 2 U O R No,. • • -,rr 950 1500 r• 1400 860 8 800 790 1230 15 19 50 100 24 77 25 16 28 20 21 35 53 80 40 39 32 26 r 27 15 15 r 12 900 • r • r :• 720 7 860 950 2000 850 95 38 28 60 110 300 130 55 47 ■ 21 36 40 50 76 43 29 16 17 r .■ 10 r r17 Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb A2 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 70 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 10 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 200 pg/L 6 pg/L 3 pg/L 0.1 pg/L NE pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 0.019 pg/L 2 pg/L 700 pg/L 250000 pg/L 3000 pg/L 3 pg/L 10 pg/L 70 pg/L 70 pg/L 1000 pg/L 0.002 pg/L 40 pg/L 0.004 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L NE pg/L 250000 pg/L 0.7 pg/L 2000 pg/L 500000 pg/L 3 pg/L 2000 pg/L 500 pg/L 1000 pg/L 6000 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Labels Historical detections by well location MW-5R Acetone Alkalinity, Total as CaCO3 32000 597000 35000 35700 34300 29200 35600 33600 33500 Arsenic Barium 56.3 57.7 57.3 56.5 58.3 55.8 59.8 52.5 53.2 Benzene 0.28 Beryllium 0.2 bis(2-Ethylhexyl )phthalate Cadmium Carbon Disulfide Chloride 14100 53100 15400 14500 14800 15600 15100 15200 16200 Chloromethane Chromium 7.1 6 5.8 6.8 5.6 5.4 5.5 5.3 Cobalt Cyanide 7.2 Iron 196 211 218 63.5 88.2 37.9 Lead m&p-Xylene 0.73 Manganese 4.6 3 4.2 Mercury 0.69 Methylene Chloride Nickel 1.6 o-Xylene 0.45 Silver Sodium 13300 13200 13700 17100 14100 13000 14600 12800 13500 Sulfate 8380 12000 8100 7770 8380 8620 8090 8220 7830 Toluene 1.7 Total Dissolved Solids 165000 153000 154000 163000 169000 175000 156000 164000 144000 Vanadium Zinc MW-6R Arsenic Barium Chromium Lead Mercury MW-7 1,1,1-Trchloroethane 1,1-Dichloroethane 0.92 0.96 1.8 0.9 1.3 1.3 1.3 1.1 1.6 1.4 1,4-Dioxane (p-Dioxane) 2.4 1.5 1.5 2.2 1.8 2 4,4'-DDD 4,4'-DDE 0.177 Acetone Alkalinity, Total as CaCO3 85000 69100 78900 71600 82700 54200 78500 75900 80400 Arsenic Barium 192 121 139 136 163 168 161 158 152 Benzene 0.69 0.6 0.64 0.48 0.6 0.68 0.37 0.41 0.39 0.38 Beryllium 0.78 0.61 0.62 2.1 beta-BHC Cadmium 0.82 Carbon Disulfide Chloride 10000 7910 6510 5910 7500 6470 6580 6490 7390 Chloroethane 0.85 Chloromethane Chromium cis-1,2-Dichloroethene 0.83 0.74 1.7 0.91 1.4 1.5 0.86 0.85 1.1 1.1 Cyanide Dichlorodifluoromethane 0.52 Dieldrin Endosulfan I Heptachlor epoxide Iron 87.9 21.5 35 25 Lead 5.4 m&p-Xylene 0.74 0.95 0.72 0.93 1 1.1 1.7 1.6 1.4 Manganese 47.6 44 43.8 43 Mercury Methylene Chloride 1.7 Nickel 1.3 o-Xylene 0.48 0.46 0.66 0.46 0.54 0.68 0.59 0.65 0.62 0.68 Silver Sodium 18400 14900 16500 16200 18400 17500 17700 16600 15300 Sulfate 36800 9840 8080 10400 13000 12800 12700 14200 13400 Tetrachloroethene Tetrahydrofuran 68.8 77.5 90.9 70.5 77.9 80.4 50.5 24.9 20.1 Total Dissolved Solids 207000 145000 139000 165000 168000 192000 171000 181000 175000 Trichloroethene 0.58 Trichlorofluoromethane 4.4 10.2 5.4 5.6 4 2 1.2 1.2 1.6 1.6 Xylenes (Total) Zinc 9.8 5 6 9 5 MW-8 Acetone Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 70 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 10 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 200 pg/L 6 pg/L 3 pg/L 0.1 pg/L NE pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 0.019 pg/L 2 pg/L 700 pg/L 250000 pg/L 3000 pg/L 3 pg/L 10 pg/L 70 pg/L 70 pg/L 1000 pg/L 0.002 pg/L 40 pg/L 0.004 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L NE pg/L 250000 pg/L 0.7 pg/L 2000 pg/L 500000 pg/L 3 pg/L 2000 pg/L 500 pg/L 1000 pg/L 6000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location Row Labels MW-5R o o Acetone 18.4 Alkalinity, Total as CaCO3 32300 32700 30800 32300 28600 24000 31900 31700 34800 31200 134000 32800 Arsenic Barium 57.1 55.9 55.9 92.7 54 58.2 54.4 53.9 57.7 53.4 57.5 85.2 Benzene Beryllium bis(2-Ethylhexyl)phthalate 1 Cadmium Carbon Disulfide Chloride 15100 16400 15300 16200 15700 15500 13900 15200 16200 16100 16100 16400 Chloromethane Chromium 4.6 5.8 5.1 4.8 4.8 5.6 5.2 Cobalt Cyanide 4.4 5.1 Iron 68.4 87.8 113 221 123 126 102 209 � Lead m&p-Xylene Manganese : • 2.6 6.1 43.5 Mercury Methylene Chloride Nickel o-Xylene Silver Sodium 13900 14200 13100 11300 13100 13700 13600 13800 13000 14500 14200 13300 Sulfate 7740 8450 7620 7430 8000 8180 8060 8310 11200 8400 7910 7020 Toluene Total Dissolved Solids 156000 145000 154000 104000 166000 163000 167000 154000 131000 157000 149000 139000 Vanadium Zinc 7.3 11.4 15.3 MW-6R Arsenic Barium Chromium Lead Mercury MW-7 1,1,1-Trich loroethane 1,1-Dichloroethane 1.3 1.5 1.2 0.91 1.1 1.3 0.81 0.9 0.84 1.2 1.2 1,4-Dioxane (p-Dioxane) 4,4'-DDD 4,4'-DDE Acetone 15.7 Alkalinity, Total as CaCO3 85000 80100 71700 67300 64100 62400 51900 51600 63500 51900 50200 Arsenic Barium 163 140 129 140 122 111 90.8 98.8 115 95.1 100 Benzene 0.43 0.42 0.26 0.29 Beryllium 0.58 beta-BHC Cadmium Carbon Disulfide Chloride 5290 4820 4430 6050 4340 4300 3600 5160 5340 3810 Chloroethane 1.3 Chloromethane 0.13 Chromium cis-1,2-Dichloroethene 1.1 1.1 0.77 0.8 0.73 0.73 0.37 0.54 0.72 0.62 0.5 Cyanide 5 Dichlorodifluoromethane 0.62 1 Dieldrin OffI , Endosulfan 1 0.15 Heptachlor epoxide �.. Iron 25.2 76.5 Lead m&p-Xylene 1.2 2.2 1.8 0.84 1.5 1.1 0.96 Manganese 35.6 28.8 33.6 27.1 22.9 15.5 19.4 24.9 17.4 10.2 Mercury Methylene Chloride 2.1 2.9 Nickel o-Xylene 0.46 0.63 0.47 0.27 0.4 0.36 0.27 Silver Sodium 17800 16200 16400 15700 16300 16600 14200 13000 14300 13900 13700 Sulfate 6720 3800 2930 10100 1850 1360 2090 Tetrachloroethene 0.48 Tetrahydrofuran 32 21.7 13.5 17.7 14.1 8.8 5.2 13.7 24.2 26 18.9 Total Dissolved Solids 175000 153000 137000 78000 145000 138000 126000 116000 108000 111000 109000 Trichloroethene Trichlorofluoromethane 0.91 1.5 0.92 1.4 0.79 1.2 0.62 0.47 0.25 0.29 Xylenes (Total) 1.2 0.79 Zinc 8.9 5.7 5.2 6.8 MW-8 Acetone 15.8 Highlighted cells are at or above the Current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 6000 Ng/L NE Ng/L 10 Ng/L 700 Ng/L 1 Ng/L 4 Ng/L 3 Ng/L 2 Ng/L 700 Ng/L 250000 Ng/L 3 Ng/L 10 Ng/L 1 Ng/L 70 Ng/L 300 Ng/L 15 Ng/L 500 Ng/L 50 Ng/L 1 Ng/L 3 Ng/L 100 Ng/L 500 Ng/L 20 Ng/L NE Ng/L 250000 Ng/L 600 Ng/L 500000 Ng/L 0.3 Ng/L 1000 Ng/L 10 Ng/L 700 Ng/L 10 Ng/L 15 Ng/L 1 Ng/L 200 Ng/L 6 Ng/L 3 Ng/L 0.1 Ng/L NE Ng/L 6000 Ng/L NE Ng/L 10 Ng/L 700 Ng/L 1 Ng/L 4 Ng/L 0.019 Ng/L 2 Ng/L 700 Ng/L 250000 Ng/L 3000 Ng/L 3 Ng/L 10 Ng/L 70 Ng/L 70 Ng/L 1000 Ng/L 0.002 Ng/L 40 Ng/L 0.004 Ng/L 300 Ng/L 15 Ng/L 500 Ng/L 50 Ng/L 1 Ng/L 3 Ng/L 100 Ng/L 500 Ng/L 20 Ng/L NE Ng/L 250000 Ng/L 0.7 Ng/L 2000 Ng/L 500000 Ng/L 3 Ng/L 2000 Ng/L 500 Ng/L 1000 Ng/L 6000 Ng/L Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location MW-5R Acetone Alkalinity, Total as CaCO3 Arsenic 4.2 5.1 5 Barium 63.7 53 54.3 66.8 52.6 56.1 57.5 70.6 58 58 57 54 53 80 76 65 Benzene Beryllium bis(2-Ethylhexyl)phthalate Cadmium Carbon Disulfide Chloride Chloromethane Chromium 7.6 5.8 5 8.6 5.2 5.3 5.6 8.4 6.4 6.2 6.2 3.5 5.6 7.3 8.7 Cobalt Cyanide I ron Lead 5.1 m&p-Xylene Manganese Mercury 0.4 Methylene Chloride Nickel o-Xylene Silver 0.57 0.16 0.46 0.6 0.28 0.78 0.56 Sodium Sulfate Toluene Total Dissolved Solids Vanadium Zinc MW-6R Arsenic Barium 28 25 Chromium 2.2 2.4 Lead Mercury MW-7 1,1,1-Tdchloroethane 0.82 1,1-Dichloroethane 1.9 3.8 1,4-Dioxane (p-Dioxane) 4,4'-DDD 4,4'-DDE Acetone Alkalinity, Total as CaCO3 47700 Arsenic 3.4 8.6 Barium 97.1 104 100 99.3 104 86.9 99 95.7 101 89 76 74 60 53 63 180 Benzene Beryllium beta-BHC Cadmium Carbon Disulfide 12.5 Chloride Chloroethane Chloromethane Chromium 0.55 0.65 0.91 7.3 4.4 Mali cis-1,2-Dichloroethene 0.67 0.71 Cyanide Dichlorod'Ifluoromethane Dieldrin Endosulfan I Heptachlor epoxide I ron Lead m&p-Xylene 1.4 Manganese 12.7 Mercury 0.24 Methylene Chloride Nickel o-Xylene 0.39 Silver 0.84 0.23 0.56 0.88 0.42 0.96 0.66 Sodium 12000 Sulfate Tetrachloroethene Tetrahydrofuran Total Dissolved Solids 124000 Trichloroethene Trichlorofluoromethane 0.34 0.48 Xylenes (Total) Zinc MW-8 Acetone 3.8 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 70 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 10 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 200 pg/L 6 pg/L 3 pg/L 0.1 pg/L NE pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 0.019 pg/L 2 pg/L 700 pg/L 250000 pg/L 3000 pg/L 3 pg/L 10 pg/L 70 pg/L 70 pg/L 1000 pg/L 0.002 pg/L 40 pg/L 0.004 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L NE pg/L 250000 pg/L 0.7 pg/L 2000 pg/L 500000 pg/L 3 pg/L 2000 pg/L 500 pg/L 1000 pg/L 6000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location 70" MW-5R 777-77 Acetone 150 Alkalinity, Total as CaCO3 Arsenic 7 5 5 Barium 72 65 150 610 270 400 200 200 240 480 610 330 620 Benzene Beryllium bis(2-Ethylhexyl)phthalate Cadmium Carbon Disulfide 25 Chloride Chloromethane Chromium 9.5 7.4 8.1 Cobalt Cyanide Iron Lead 13 7.6 7.6 8.2 14 m&p-Xylene Manganese Mercury 0.8 Methylene Chloride Nickel o-Xylene Silver Sodium Sulfate Toluene Total Dissolved Solids Vanadium Zinc MW-6R Arsenic 530 Barium 24 41 180 62 41 82 59 160 36C 260 300 590 Chromium 3.2 4.1 2.6 2.8 Lead 7.6 5.8 Wo 14 14 11 Mercury MW-7 1,1,1-Trich loroethane 1,1-Dichloroethane 1,4-Dioxane (p-Dioxane) 4,4'-DDD 4,4'-DDE Acetone Alkalinity, Total as CaCO3 Arsenic 9.8 Barium 130 210 84 360 390m&i-.iojmtciiiijor4iiijoi-iiiiI rr M .rI i WIN SUNNI Benzene Beryllium beta-BHC Cadmium Carbon Disulfide 9 Chloride Chloroethane Chloromethane Chromium 6.8==M 2.5 cis-1,2-Dich loroethene Cyanide Dich lorodifluoromethane Dieldrin Endosulfan I Heptachlor epoxide Iron Lead 5.3 6 8.7 12 1 6 m&p-Xylene Manganese Mercury 0.2 0.4 Methylene Chloride Nickel o-Xylene Silver 2.6 Sodium Sulfate Tetrachloroethene Tetrahydrofuran Total Dissolved Solids Trichloroethene Trichlorofluoromethane Xylenes (Total) Zinc MW-8 Acetone Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 100 pg/L Di-n-octylphthalate 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 1000 pg/L DichlorodiFluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 20 pg/L Silver NE pg/L Sodium 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 1000 295001 252001 250001 25300 26600 24200 2701 5.8 57.6 54 55.8 52.9 50.9 47.8 36 41 0.41 3800 4370 4410 4090 3860 4290 3110 361 60.9 125 27 42.4 39.3 37 3.5 4.2 3.3 4 4.4 3 0.35 112001 109001 111001 129001 10800 9620 8300 8810 98E 8300 8580 8940 9360 7860 6560 1060 2980 474 84000 93000 76000 93000 78000 170000 68000 75000 820f 5. 33800 31000 38900 33900 39000 29700 33500 31800 279f 5.1 181 238 193 238 203 217 215 193 1£ 0.28 36401 80401 47701 63701 41901 68301 534301 48301 1 442 167�I-7 0.57 481 43.5I 910.41 1481 0.992501 35.31 171 1E 5.2 19.5 5.1 5.3 7.1 10.7 4.2 10. 18900 15100 20600 16200 23400 14100 15700 14300 149f Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit Old Salisbury Road Landfill (C&D) MCL Value Historical detections by well location NE pg/L • Alkalinity, Total as CaCO3 20800 25800 24800 23200 20000 22800 21300 19700 22800 19500 20100 10 pg/L Arsenic 2.6 700 pg/L Barium 42.9 44 38.3 34.4 30 38 30.7 25.4 28.5 26.9 27.5 4 pg/L Beryllium 250000 pg/L Chloride 3060 2670 1960 2040 1960 1350 1800 1510 2070 1860 10 pg/L Chromium 4.1 70 pg/L Cyanide 9.9 4.3 5.1 100 pg/L Di-n-octylphthalate 5.6 300 pg/L Iron 48.6 54 136 61.5 60.8 57.8 15 pg/L Lead 50 pg/L Manganese 3 2.7 2.9 3.3 3.4 19.9 6.8 1 pg/L Mercury 3 pg/L Methylene Chloride 1.1 20 pg/L Silver NE pg/L Sodium 9240 9700 8280 7940 6940 7810 6160 5580 6120 6980 6250 250000 pg/L Sulfate 2700 4090 1630 1350 1860 2100 500000 pg/L Total Dissolved Solids 67000 67000 87000 79000 61000 64000 50000 61000 51000 58000 52000 1000 pg/L Zinc 7.1 15.2 MW-9 NE pg/L Alkalinity, Total as CaCO3 25400 23300 21200 23400 18900 18300 18300 18400 21700 17200 20100 10 pg/L Arsenic 3.5 700 pg/L Barium 207 195 197 186 182 193 168 170 174 142 142 4 pg/L Beryllium 3 pg/L bis(2-Ethy1hexyl)phthalate 250000 pg/L Chloride 4610 4360 6850 4710 4290 3610 3610 3950 4300 3560 10 pg/L Chromium 70 pg/L Cyanide 4.7 1000 pg/L Dichlorodifluoromethane 1.5 0.88 0.76 0.28 0.28 300 pg/L Iron 149 128 55.9 136 15 pg/L Lead 50 pg/L Manganese 4.6 8.5 6.3 4 3.5 7.6 6.9 16.6 20 pg/L Silver NE pg/L Sodium 15400 15700 14200 14500 14500 14600 12400 13500 12900 13100 12600 Highlighted cells are at or above the Current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 100 pg/L Di-n-octylphthalate 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 1000 pg/L DichlorodiFluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 20 pg/L Silver NE pg/L Sodium 19600 24.4 151 81000 45.4 Old Salisbury Road Landfill (C&D) Historical detections by well location 27.3 26.8 28.8 27.2 25 32.8 24 0.96 0.62 1.4 0.78 0.97 0.42 0.1 0.1 0.16 0.15 0.13 0. 17400 141 153 157 134 128 17 7 m 29 1241 1241 1171 1401 1401 1001 1001 851 951 240 0.181 0.361 0.22 14 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 100 pg/L Di-n-octylphthalate 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 3 pg/L bis(2-Ethy1hexyl)phthalate 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 20 pg/L Silver NE pg/L Sodium 48 Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 250000 pg/L 500000 pg/L 2000 pg/L 1000 pg/L 3 pg/L 40 pg/L NE pg/L 6000 pg/L NE pg/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 40 pg/L 600 pg/L 0.008 pg/L 0.004 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 2000 pg/L 0.2 pg/L 2000 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 500 pg/L 1000 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Labels Historical detections by well location • Sulfate 2140 2480 3610 Total Dissolved Solids 145000 155000 134000 130000 157000 190000 139000 133000 136000 Trichlorofluoromethane 0.38 1.2 0.66 1.3 0.86 1.7 1.3 1.3 1.4 1.2 Zinc MW-10 1,4-Dioxane (p-Dioxane) 2-Hexanone 0.72 4-Methyl-2-pentanone (MIBK) 0.65 1.7 1.1 2.8 Acetone 16.4 13.7 12.1 22.5 Alkalinity, Total as CaCO3 734000 682000 535000 635000 726000 506000 652000 506000 520000 446000 Antimony Arsenic Barium 109 106 60.2 66 111 65.6 83.1 94.7 106 221 Benzene 0.47 0.48 0.56 0.78 0.33 0.55 0.55 0.57 0.52 Beryllium Cadmium 0.62 Carbon Disulfide 2.1 2 Chloride 43900 45400 30800 63100 71800 65100 88500 158000 163000 :��� Chromium 6.1 4 5.6 4.1 4.6 4.2 cis-1,2-Dichloroethene 0.23 0.27 0.23 0.2 Cobalt 4.4 3.1 Copper Cyanide 4.3 4.8 Endosulfan I Ethylbenzene 0.41 0.53 Heptachlor Heptachlor epoxide Iron 3950 2780 1870 2740 4490 2320 5030 3300 8 is 5.3 5.8 3.7 2.6 3.9 Lead 4.1 m&p-Xylene 0.68 1.3 1.1 1.2 Manganese Ms •8 26400 28600 14600 25700 31400 20500 24700 17500 Mercury Methylene Chloride Nickel 12.5 9.3 8.4 7.9 11 7.2 11.1 8.5 7.6 6.9 o-Xylene 0.34 0.84 0.28 0.53 0.78 1.1 0.97 1 Selenium 12 Silver 9.6 Sodium 92900 108000 77400 148000 138000 136000 151000 157000 138000 123000 Sulfate 165000 202000 156000 235000 64100 N@e lIUI ��� Ill Sulfide 242 192 347 240 127 Tetrahydrofuran 65.1 89.1 69.6 130 141 113 169 192 135 131 182 Thallium 0.043 Tin 7.1 Toluene 0.2 00.35 0.27 Total Dissolved Solids 1070000 1080000 804000 1180000 1380000 1110000 1370000 1360000 1 11� ut I11 Trich lorofluoromethane Vanadium Xylenes (Total) 1.1 Zinc 5.4 MW-11 4,4'-DDT Acetone 21.1 Alkalinity, Total as CaCO3 81300 91700 94700 127000 102000 154000 161000 130000 130000 135000 Barium 95.6 78.1 87 98.1 91.6 100 95.8 82.8 89.8 102 Benzo(g, h, i)perylene Beryllium 0.23 Chloride 8460 10100 11100 11000 11400 12300 11800 12500 13000 13500 Chloromethane 0.23 Chromium 5.2 Cobalt Copper Cyanide 4 4.4 Iron 24600 19000 21800 23700 24100 27500 28200 27300 • �� . �� Lead Manganese •� rr r :� •� Mercury Methylene Chloride Nickel 3.6 o-Xylene 0.27 Selenium 5.5 Silver Sodium 12300 11700 12700 12400 13500 12800 13600 12000 12300 11700 Sulfate 11900 16800 23200 22800 23900 22300 20700 15300 16200 14100 Sulfide 56.8 53.8 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 250000 pg/L 500000 pg/L 2000 pg/L 1000 pg/L 3 pg/L 40 pg/L NE pg/L 6000 pg/L NE pg/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 40 pg/L 600 pg/L 0.008 pg/L 0.004 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 2000 pg/L 0.2 pg/L 2000 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 500 pg/L 1000 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location ir • Sulfate 960 3440 1110 2030 2100 3200 Total Dissolved Solids 141000 135000 103000 142000 134000 141000 107000 124000 100000 118000 123000 Trichlorofluoromethane 1.4 1 1.3 1.1 0.98 0.96 0.47 0.69 0.36 0.49 Zinc 5.1 5.3 MW-10 1,4-Dioxane (p-Dioxane) 2-Hexanone 0.69 0.96 4-Methyl-2-pentanone (MIBK) 2.5 2.6 5.6 2.2 Acetone 14.1 11.8 Alkalinity, Total as CaCO3 626000 29000 48200 47300 42200 31400 26700 32100 25500 413000 Antimony Arsenic 2.6 5.2 Barium 148 292 241 660 262 132 112 115 101 96.5 Benzene 0.83 0.46 0.44 Beryllium 3.2 1.9 2.8 1.4 Cadmium Carbon Disulfide 5.2 Chloride 202000 9640 47400 51800 2220 1820 1790 2040 1800 Chromium 6.4 9.1 3.5 6.7 cis-1,2-Dichloroethene 0.33 0.35 Cobalt Copper 16.4 6.3 3.8 Cyanide 5.4 4.1 9.8 Endosulfan 1 0.17 Ethylbenzene 0.55 0.4 1 0.73 Heptachlor Heptachlor epoxide Iron I .•1 84.3 92.8 218 55.1 Lead 2.6 8.5 11.6 4.1 m&p-Xylene 2.1 0.68 1.2 1.1 Manganese 10.9 7.9 5.1 NEREA of Mercury 0.12 0.12 0.29 0.33 0.51 Methylene Chloride 2.8 1.2 Nickel 10.7 4.7 3.9 5.9 o-Xylene 2.1 0.43 0.85 0.65 Selenium Silver Sodium 184000 10300 19800 14100 6860 5280 Sulfate 15800 63600 8770 Sulfide 260 Tetrahydrofuran 237 6.1 120 145 106 18.6 5 Thallium Tin 3.1 8.5 Toluene 0.63 Total Dissolved Solids s 1 8 1 8 311000 403000 279000 86000 63000 66000 46000 63000 49000 Trichlorofluoromethane 0.2 0.33 0.38 0.49 Vanadium 1 Xylenes (Total) Zinc 5.1 34 27.2 21.2 6.2 MW-11 4,4'-DDT 0.05 Acetone Alkalinity, Total as CaCO3 107000 104000 127000 132000 143000 175000 161000 189000 153000 120000 Barium 93.1 103 97.2 93.7 96.8 94.3 87.8 87 76.8 70.3 Benzo(g,h,i)perylene 1.3 Beryllium Chloride 14500 14500 14900 14400 15000 12400 14000 14200 12900 10800 Chloromethane Chromium Cobalt Copper 2.8 Cyanide 4.1 4.2 Iron 35700 33400 32100 30700 29000 26300 is 29400 34600 314001 Lead 2.91 3.6 Manganese .8 1820 2020 1990 2030• 0 1890 1740 1580 Mercury Methylene Chloride 1.4 Nickel o-Xylene Selenium 5.6 Silver Sodium 12000 11200 12000 9460 10000 8490 9070 8290 8770 7460 Sulfate 17100 15200 19100 15300 12800 10700 10400 11000 10400 9700 Sulfide 130 Highlighted cells are at or above the Current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 250000 pg/L 500000 pg/L 2000 pg/L 1000 pg/L 3 pg/L 40 pg/L NE pg/L 6000 pg/L NE pg/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 40 pg/L 600 pg/L 0.008 pg/L 0.004 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 2000 pg/L 0.2 pg/L 2000 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 500 pg/L 1000 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location • Sulfate Total Dissolved Solids 128000 Trichlorofluoromethane 0.42 0.26 Zinc MW-10 1,4-Dioxane (p-Dioxane) 2-Hexanone 4-Methyl-2-pentanone (MIBK) Acetone Alkalinity, Total as CaCO3 21700 Antimony Arsenic Barium 91.3 80.7 38.9 46.6 39.1 38.9 41.9 42 40.8 52 71 48 46 82 55 98 Benzene Beryllium Cadmium Carbon Disulfide 13 Chloride Chromium 0.63 0.65 cis-1, 2-Dichloroethene Cobalt Copper Cyanide Endosulfan I Ethylbenzene Heptachlor Heptachlor epoxide I ron Lead 6.8 m&p-Xylene Manganese 6.8 Mercury 0.2 Methylene Chloride Nickel o-Xylene Selenium 6.2 Silver 0.12 0.19 Sodium Sulfate Sulfide Tetrahydrofuran Thallium Tin Toluene Total Dissolved Solids 89000 Trichlorofluoromethane 0.68 0.52 Vanadium Xylenes (Total) Zinc MW-11 4,4'-DDT Acetone Alkalinity, Total as CaCO3 122000 Barium 57.5 56.2 48.1 37.6 31.8 28.4 28.6 29.2 23.1 25 24 26 27 24 28 47 Benzo(g, h, i)perylene Beryllium Chloride 8480 Chloromethane Chromium 3.9 3.3 Cobalt Copper Cyanide Iron oil Lead Manganese Mercury Methylene Chloride Nickel o-Xylene Selenium 8.7 Silver 1.2 0.48 0.5 0.79 0.41 0.39 Sodium 6480 Sulfate 7590 Sulfide Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 1000 pg/L Zinc MW-10 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 2-Hexanone NE pg/L 4-Methyl-2-pentanone (MIBK) 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 1 pg/L Antimony 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 4 pg/L Beryllium 2 pg/L Cadmium 700 pg/L Carbon Disulfide 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 40 pg/L Endosulfan 1 600 pg/L Ethylbenzene 0.008 pg/L Heptachlor 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 500 pg/L o-Xylene 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide 2000 pg/L Tetrahydrofuran 0.2 pg/L Thallium 2000 pg/L Tin 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-11 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 500 pg/L o-Xylene 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 2000 pg/L 0.2 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 70 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 70 pg/L 1000 pg/L 100 pg/L 0.05 pg/L 300 pg/L 50 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L 2000 pg/L 0.2 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 3 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 0.005 pg/L 0.05 pg/L 200 pg/L 4 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Labels Historical detections by well location • Tetrahydrofuran 4.5 Thallium Toluene 1 Total Dissolved Solids 176000 183000 194000 230000 240000 236000 237000 232000 218000 226000 Vanadium Zinc 10 4.2 MW-12 1,4-Dioxane (p-Dioxane) 1.9 I 2.6 2,4-D 2.86 Acetone Alkalinity, Total as CaCO3 296000 299000 174000 333000 150000 176000 117000 65800 73800 Arsenic Barium 145 141 95.9 224 146 200 132 82.8 84.2 Benzene 0.41 0.37 0.29 0.25 0.33 Benzo(g, h, i)perylene Beryllium 0.88 Chloride 22400 28000 14100 29500 17600 34000 14400 11100 10400 Chloromethane Chromium cis-1,2-Dichloroethene 0.4 0.23 Cobalt Cyanide 4.8 Dichlorod ifluoromethane Di-n-octylphthalate Indeno(1,2,3-cd)pyrene Iron 1020 877 947 2560 937 1990 175 125 3440 3840 2380 6410 1500 2260 Manganese Methylene Chloride Nickel 10.2 9 5.1 10.6 4.3 6.2 3.3 Silver Sodium 23300 25000 18300 28600 17400 20700 17600 13400 13200 Sulfate 87600 92500 90400 227000 99500 149000 91700 64300 62400 Tetrahydrofuran 5.9 Thallium Toluene 0.74 Total Dissolved Solids 489000 337000 369000 ME 1118 301000 218000 219000 Trichlorofluoromethane 0.81 1 0.89 1.4 0.52 Vanadium Zinc MW-13 1,1-Dichloroethene 1,4-Dioxane (p-Dioxane) Acetone Alkalinity, Total as CaCO3 93800 90900 83400 66400 58500 52800 52800 47200 44600 Arsenic 5 Barium 514 397 292 196 156 138 124 114 116 Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g, h, i)perylene Beryllium 1.4 1.4 0.78 0.72 0.78 0.6 0.69 0.63 0.52 Chloride 49800 39000 20700 8400 6310 6290 5120 4790 4770 Chromium 3.8 Cobalt Copper 4.3 Cyanide Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene Iron 238 1 80.8 87.9 42.3 71.8 108 193 Lead Manganese 1 27.4 6.9 5.2 9.8 7.4 17.9 Mercury 0.3 0.52 Nickel 11.3 1.5 Silver Sodium 18300 15900 15000 12600 11500 9940 10900 9540 9740 Sulfate 22300 14100 7030 6520 5450 5910 5650 4510 4960 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 2000 pg/L 0.2 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 70 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 70 pg/L 1000 pg/L 100 pg/L 0.05 pg/L 300 pg/L 50 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L 2000 pg/L 0.2 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 3 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 0.005 pg/L 0.05 pg/L 200 pg/L 4 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location • Tetrahydrofuran 4.4 Thallium Toluene Total Dissolved Solids 189000 236000 281000 239000 228000 207000 236000 228000 220000 161000 Vanadium Zinc 92 MW-12 1,4-Dioxane (p-Dioxane) 2,4-D Acetone 12.1 Alkalinity, Total as CaCO3 64500 72900 55900 41000 19200 40500 45500 39300 29600 40200 37200 Arsenic Barium 113 144 190 95.7 60.9 59.2 61.1 47.6 50.1 50.5 46.9 Benzene Benzo(g,h,i)perylene 1.2 Beryllium Chloride 19700 23300 26000 9000 8070 8240 6180 6230 5820 4900 8200 Chloromethane Chromium cis-1,2-Dich loroethene Cobalt Cyanide 5.3 Dichlorodifluoromethane 0.23 Di-n-octylphthalate 5.6 Indeno(1,2,3-cd)pyrene Iron 274 253 Manganese 49.6 9.7 14.6 13.2 33.6 15.7 Methylene Chloride 2 2 Nickel 4.4 6.2 5.5 3.2 4.1 Silver Sodium 16200 19200 19200 13700 11200 12800 11000 10500 11100 11000 11600 Sulfate 86100 129000 169000 70800 73600 32800 48000 27400 51800 24200 20500 Tetrahydrofuran 11.4 26.8 12.4 Thallium 0.021 Toluene Total Dissolved Solids 288000 286000 382000 234000 163000 135000 149000 126000 138000 127000 130000 Trichlorofluoromethane 1 2.8 1.4 0.82 0.22 0.32 Vanadium Zinc 30.8 MW-13 1,1-Dichloroethene 1,4-Dioxane (p-Dioxane) Acetone 17.3 Alkalinity, Total as CaCO3 42400 42300 41000 37100 36900 36200 46400 43200 58700 43900 52200 Arsenic 2.6 Barium 120 91.6 210 71.5 89.3 130 77.1 106 176 279 144 Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene 1.5 Beryllium 2.2 0.68 0.66 1.2 2.4 3.5 1.4 Chloride 4310 4100 4590 3270 3760 5870 3880 5700 3820 6150 5380 Chromium 2.9 3 7.1 Cobalt Copper 8.5 3.8 7.6 6.9 Cyanide 5 Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene Iron 58 232 1 • so .1 Lead 8 2.9 5.4 6.5=7.5 Manganese 9.7 26.7 41.2 34.1 48.8 Mercury Nickel 6.4 Silver Sodium 10000 9380 9420 12200 10700 10700 11200 11700 19100 14600 16700 Sulfate 5670 5390 7280 10100 9330 8660 8680 9360 7820 9770 9420 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 2000 pg/L 0.2 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 70 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 70 pg/L 1000 pg/L 100 pg/L 0.05 pg/L 300 pg/L 50 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L 2000 pg/L 0.2 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 3 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 0.005 pg/L 0.05 pg/L 200 pg/L 4 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location • Tetrahydrofuran 12.1 Thallium Toluene Total Dissolved Solids 165000 Vanadium Zinc MW-12 1,4-Dioxane (p-Dioxane) 2,4-D Acetone Alkalinity, Total as CaCO3 40200 Arsenic 2.7 Barium 60.1 39.1 44.9 40.6 38 34.5 57.9 60.5 47.3 31 66 55 77 50 77 74 Benzene Benzo(g, h, i)perylene Beryllium Chloride 8030 Chloromethane 0.21 Chromium 2.6 1.1 2.4 2 1.8 4 2.1 cis-1, 2-Dichloroethene Cobalt Cyanide Dichlorod'Ifluoromethane Di-n-octylphthalate Indeno(1,2,3-cd)pyrene Iron I Manganese Methylene Chloride Nickel 71530( Silver 0.7 0.2 0.39 0.37 0.15 0.26 Sodium Sulfate Tetrahydrofuran Thallium Toluene Total Dissolved Solids 124000 Trich lorofluoromethane Vanadium Zinc MW-13 1,1-Dichloroethene 19.8 1,4-Dioxane (p-Dioxane) Acetone Alkalinity, Total as CaCO3 44500 Arsenic Barium 139 164 176 126 117 79.2 88.7 64.6 85.6 79 62 65 59 46 57 160 Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g, h, i)perylene Beryllium 2.3 Chloride Chromium 5.5 3.9 4 1.7 0.8 1.6 2.2 1.1 2 4.8 9.2 Cobalt Copper 6.1 Cyanide Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene I ron , Lead 6.4 4.3 11 Manganese Mercury Nickel Silver 0.72 0.4 0.41 0.44 0.21 Sodium 20200 Sulfate 9460 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit 2000 pg/L Tetrahydrofuran 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-12 3 pg/L 1,4-Dioxane (p-Dioxane) 70 pg/L 2,4-D 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 100 pg/L Di-n-octylphthalate 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 2000 pg/L Tetrahydrofuran 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc MW-13 350 pg/L 1,1-Dichloroethene 3 pg/L 1,4-Dioxane (p-Dioxane) 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 2000 pg/L 2000 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 3 pg/L 250000 pg/L 3 pg/L 10 pg/L 1000 pg/L 70 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L 0.7 pg/L 0.2 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 70 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 250000 pg/L 70 pg/L 10 pg/L 1000 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 3 pg/L 100 pg/L NE pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Labels Historical detections by well location • Sulfide Tetrahydrofuran 12.7 11.4 Tin Toluene 0.58 Total Dissolved Solids 276000 230000 158000 126000 115000 115000 111000 107000 90000 Trich lorofluoromethane Vanadium Zinc 11.1 MW-14 Acetone Alkalinity, Total as CaCO3 63000 69100 66900 65500 66600 64900 67100 61800 63500 Arsenic 5.1 Barium 272 241 256 241 238 234 246 212 214 Beryllium 0.81 0.61 0.83 0.59 0.54 bis(2-Ethylhexyl )phthalate Chloride 3650 3830 3860 3730 3710 3870 3840 3930 3620 Chloromethane Chromium 4.1 Copper Cyanide 7.8 Dichlorodifluoromethane 3.7 4.1 2.4 2.4 4.5 3 2.4 3 3.6 3.9 Iron 49.7 40.3 36.2 124 93.9 Lead Manganese 38.3 17.4 18.4 Mercury Methylene Chloride Nickel 9.6 3.7 4.5 3.9 6 4.4 6.3 2.6 Silver Sodium 18800 18200 19600 17900 18600 17400 18600 16900 17100 Sulfate Tetrachloroethene 0.55 0.68 0.65 0.53 0.48 0.52 Thallium Total Dissolved Solids 160000 158000 146000 150000 152000 163000 154000 152000 142000 Trichlorofluoromethane 1.7 2.5 1.6 1 1.5 0.92 0.86 0.79 0.8 0.87 Vanadium Zinc 11.3 5.3 MW-15 1,1-Dichloroethene 2,4-D 0.27 4,4'-DDD Acetone Alkalinity, Total as CaCO3 104000 95200 83500 96500 91300 74200 89900 112000 110000 Arsenic Barium 16.1 6.4 41.1 23.8 13.5 29.8 24.4 11.4 17.1 Beryllium 0.22 Chloride 37700 43500 61400 55500 72100 115000 128000 89700 89800 Chloroform 0.45 0.44 0.44 Chromium Copper 2.5 3 Cyanide 4.2 Iron 166 107 Lead Manganese Methylene Chloride Nickel 1.6 Sodium 15700 14900 18900 99700 19900 23000 26100 20500 19800 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 2000 pg/L 2000 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 3 pg/L 250000 pg/L 3 pg/L 10 pg/L 1000 pg/L 70 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L 0.7 pg/L 0.2 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 70 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 250000 pg/L 70 pg/L 10 pg/L 1000 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 3 pg/L 100 pg/L NE pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location • Sulfide 151 106 178 Tetrahydrofuran Tin 2.5 Toluene Total Dissolved Solids 89000 79000 145000 110000 107000 119000 113000 114000 87000 144000 110000 Trichlorofluoromethane Vanadium Zinc 5.7 12.8 40.5 8.6 7.9 13.7 17.2 37.3 51 20 MW-14 Acetone 14.7 Alkalinity, Total as CaCO3 55300 59700 50400 51500 45200 42300 37400 32800 35600 28900 30100 Arsenic Barium 221 188 188 183 179 193 163 140 254 160 122 Beryllium 0.6 0.57 0.83 0.63 0.54 0.6 bis(2-Ethy1hexyl)phthalate Chloride 3260 3410 3470 3930 3510 3720 3630 4100 4290 4790 Chloromethane Chromium 4.5 6.6 6 Copper 4.8 9.5 5.8 Cyanide 4.3 5.3 6 Dichlorodifluoromethane 3.6 2.3 3.6 2.1 Iron 134 123 142 r� Lead Manganese 18.1 13.7 21.6 25.7 1 40.2 on Mercury Methylene Chloride 1.6 Nickel 2.7 2.8 2.8 5.3 8.6 13.7 12.5 Silver Sodium 16900 16200 15400 15800 14500 14400 12800 12300 13500 15000 14300 Sulfate 663 1400 1080 1790 Tetrachloroethene 0.61 Thallium 0.048 Total Dissolved Solids 130000 118000 85000 135000 131000 119000 124000 123000 102000 127000 145000 Trichlorofluoromethane 0.75 0.58 1.1 0.54 0.59 0.57 0.34 Vanadium Zinc 6.3 13.3 11.7 27.4 23 MW-15 1,1-Dichloroethene 3.1 2,4-D 4,4'-DDD 0.062 Acetone 13.2 Alkalinity, Total as CaCO3 98100 101000 104000 103000 91500 54700 96600 64300 78900 77600 75300 Arsenic 4.5 7.1 5.7 Barium 22.7 14 11 74 105 41.5 8.6 23.8 59.6 143 115 Beryllium Chloride 104000 98000 94000 113000 98200 146000 83400 124000 124000 143000 60600 Chloroform 0.4 0.44 0.7 0.44 0.26 0.49 0.77 0.63 0.49 1.4 Chromium 5.4 7.6 6.7 7.2 Copper 2.6 7.1 8.8 10.5 Cyanide 5.2 Iron 8 227 233 292 239 8 :� �.II1 Lead 6 6.8 9.5 7.6 Manganese 33 34.7 14 .� Methylene Chloride 2.4 Nickel 2.7 3.9 4.3 Sodium 21600 20200 20100 21800 20300 24000 24200 25300 26700 21200 16300 Highlighted cells are at or above the Current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 2000 pg/L 2000 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 3 pg/L 250000 pg/L 3 pg/L 10 pg/L 1000 pg/L 70 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L 0.7 pg/L 0.2 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 70 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 250000 pg/L 70 pg/L 10 pg/L 1000 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 3 pg/L 100 pg/L NE pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location • Sulfide Tetrahydrofuran 18.6 Tin Toluene Total Dissolved Solids 159000 Trichlorofluoromethane 18.6 Vanadium ' Zinc 31.6 MW-14 Acetone Alkalinity, Total as CaCO3 30400 Arsenic 7.3 8.3 Barium 143 125 129 130 242 97.9 583 186 130 210 460 250 120 69 66 170 Beryllium bis(2-Ethylhexyl)phthalate Chloride Chloromethane 0.24 Chromium 1.8 2.3 3 = 0.4 8 4.1 1.7 6.6 3.9 3.2 Copper Cyanide Dichlorod ifluoromethane Iron r Lead 7.2 5.2 13 5.9 8 Manganese Mercury 0.1 0.44 Methylene Chloride Nickel Silver 0.74 0.39 0.54 0.46 0.56 0.48 Sodium 12700 Sulfate Tetrachloroethene Thallium Total Dissolved Solids 138000 Trich lorofluoromethane Vanadium Zinc 12 MW-15 1,1-Dichloroethene 2,4-D 4,4'-DDD Acetone Alkalinity, Total as CaCO3 Arsenic Barium Beryllium Chloride Chloroform Chromium Copper Cyanide I ron Lead Manganese Methylene Chloride Nickel Sodium Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit NE pg/L Sulfide 2000 pg/L Tetrahydrofuran 2000 pg/L Tin 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc MW-14 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 3 pg/L bis(2-Ethy1hexyl)phthalate 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1000 pg/L Copper 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc MW-15 350 pg/L 1,1-Dichloroethene 70 pg/L 2,4-D 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 250000 pg/L Chloride 70 pg/L Chloroform 10 pg/L Chromium 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 250000 Ng/L NE Ng/L 2000 Ng/L 0.2 Ng/L 500000 Ng/L 2000 Ng/L 0.3 Ng/L 1000 Ng/L 6000 Ng/L NE Ng/L 10 Ng/L 700 Ng/L 4 Ng/L 2 Ng/L 250000 Ng/L 10 Ng/L 1 Ng/L 1000 Ng/L 70 Ng/L 2 Ng/L 300 Ng/L 15 Ng/L 50 Ng/L 1 Ng/L 3 Ng/L 100 Ng/L 20 Ng/L 20 Ng/L NE Ng/L 250000 Ng/L NE Ng/L 500000 Ng/L 0.3 Ng/L 1000 Ng/L 3 Ng/L 40 Ng/L NE Ng/L NE Ng/L 6000 Ng/L NE Ng/L 10 Ng/L 700 Ng/L 0.05 Ng/L 0.005 Ng/L 0.05 Ng/L 200 Ng/L 0.5 Ng/L 4 Ng/L 3 Ng/L 250000 Ng/L 3 Ng/L 10 Ng/L 5 Ng/L 70 Ng/L 1 Ng/L 1000 Ng/L 70 Ng/L 0.005 Ng/L 0.05 Ng/L 300 Ng/L 15 Ng/L 50 Ng/L 1 Ng/L 3 Ng/L 100 Ng/L 20 Ng/L 20 Ng/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Labels Historical detections by well location moor • Sulfate 25500 27400 36600 38300 40600 45900 49900 54600 59600 Sulfide Tetrahydrofuran 4.8 6.5 8.9 8.2 9.2 14.8 Thallium Total Dissolved Solids 247000 237000 262000 269000 311000 448000 395000 369000 370000 Trichlorofluoromethane 0.21 0.42 0.22 0.71 Vanadium Zinc 11.2 5.1 5.1 5.8 6.6 7.1 SW-1 Acetone Alkalinity, Total as CaCO3 71400 36800 39400 40100 15900 22300 27400 49200 43600 Arsenic 8.5 8.5 Barium 535 70.7 30.5 25.6 120 109 47 68.2 47.5 Beryllium 2 0.54 Cadmium 0.48 Chloride 24400 29600 14500 12100 35100 55400 18300 29700 35700 Chromium 3.8 Cobalt Copper 13.8 5.5 Cyanide Endrin Iron MII .91 r •:r :� .� •�� 3.4 Lead Manganese 48.5 Mercury Methylene Chloride Nickel 12.2 2.5 Selenium Silver Sodium 17900 15000 9360 10400 17000 19400 11800 15600 17000 Sulfate 7440 7570 979 533 7890 7970 4140 2060 2730 Sulfide 52.1 Total Dissolved Solids 199000 144000 85000 76000 143000 174000 106000 131000 123000 Vanadium Zinc �M70.2 16.1 5.2 SW-2 1,4-Dioxane (p-Dioxane) 2.5 2.2 2.7 1.3 2-Hexanone 3, 3'-Dich lorobenzid ine 3-Methylcholanthrene Acetone 12.9 Alkalinity, Total as CaCO3 111000 309000 87000 78800 74900 54900 62600 56000 57600 Arsenic 8.3 Barium 92.5 96.9 99.3 100 110 85.6 78.8 74.2 65.4 Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g, h, i)perylene Benzo(k)fluoranthene Beryllium bis(2-Ethylhexyl )phthalate Chloride 21900 9880 19700 19300 20200 19400 12800 13500 15200 Chloromethane 0.12 Chromium 2.8 3.8 Chrysene cis-1,2-Dichloroethene 0.33 Cobalt Copper 2.2 4.1 Cyanide 4.2 Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene Iron �� ,r r :•r �� � Lead Manganese 549 3180 755 1040 825 680 Mercury Methylene Chloride Nickel 3.5 1.6 Selenium 4.7 Silver Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 250000 pg/L NE pg/L 2000 pg/L 0.2 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 2 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 40 pg/L NE pg/L NE pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 0.005 pg/L 0.05 pg/L 200 pg/L 0.5 pg/L 4 pg/L 3 pg/L 250000 pg/L 3 pg/L 10 pg/L 5 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location •w Labels Sulfate 58300 58700 63700 70000 65400 43800 59500 o 53200 41200 o 35600 25800 Sulfide 100 Tetrahydrofuran 12 16.8 27.3 19.8 16.9 15.5 21.4 14.7 7.4 6.3 Thallium 0.049 Total Dissolved Solids 410000 371000 418000 362000 360000 464000 373000 410000 442000 298000 260000 Trichlorofluoromethane 2.1 4.4 5.1 4.8 4.4 3.9 5.3 7.6 4.3 8.1 7.3 Vanadium Zinc 16.2 6.3 5.9 35.4 49 5.3 17.1 22.7 45.6 51.1 SW-1 Acetone 11.2 Alkalinity, Total as CaCO3 33200 57400 27700 35100 44500 63700 45200 72700 58000 79700 47200 Arsenic 3.6 5.9 Barium 86.8 65.9 69.5 65 72.2 276 65.8 71.1 58.9 63.3 70.4 Beryllium 1.1 Cadmium 0.7 Chloride 49200 26800 26000 21600 31500 19500 23700 18100 20600 19700 25300 Chromium Cobalt Copper 8.6 3.9 16.4 Cyanide 4.4 4.7 Endrin 0.08 Iron I 1 .18 :111 .•�� �r �� Lead Manganese Mercury Methylene Chloride 2 Nickel 8.7 Selenium 7 Silver Sodium 23000 14200 13000 12800 16000 12500 14500 13000 12400 15500 14300 Sulfate 2530 3410 4320 4460 3690 3130 2820 2190 2700 2090 Sulfide Total Dissolved Solids 143000 116000 118000 113000 140000 122000 126000 125000 104000 131000 98000 Vanadium Zinc 10.1 7.2 7.5 69.8 SW-2 1,4-Dioxane (p-Dioxane) 2-Hexanone 1.8 3,3'-Dichlorobenzidine 3.6 3-Methylcholanthrene 2.9 Acetone Alkalinity, Total as CaCO3 46200 58800 32300 43200 33200 2390 41300 48900 48600 44700 44200 Arsenic 3.7 6.2 Barium 77.5 108 73.1 70 11 171 59.7 50.1 51.7 46.5 53.4 Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene 1.8 Benzo(k)fluoranthene Beryllium 3.7 0.64 bis(2-Ethy1hexyl)phthalate 1.1 Chloride 13800 6190 9720 12500 4050 28200 10700 11600 10800 10300 11300 Chloromethane Chromium r 3.2 Chrysene 1.1 cis-1,2-Dich loroethene Cobalt Copper 81.6 3.2 Cyanide Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene Iron U M r .1 '9111 Lead 2.7 7.4 Manganese r I I I 1. 0.2 Mercury Methylene Chloride Nickel 16A 3.1 Selenium Silver Highlighted cells are at or above the Current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 250000 pg/L NE pg/L 2000 pg/L 0.2 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 2 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 40 pg/L NE pg/L NE pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 0.005 pg/L 0.05 pg/L 200 pg/L 0.5 pg/L 4 pg/L 3 pg/L 250000 pg/L 3 pg/L 10 pg/L 5 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location • Sulfate Sulfide Tetrahydrofuran Thallium Total Dissolved Solids Trich lorofluoromethane Vanadium Zinc SW-1 Acetone 2.2 22.7 Alkalinity, Total as CaCO3 19600 Arsenic 3.7 Barium 42.5 69.9 61.9 92.5 77.7 45.6 78.2 79.7 70.3 88 54 120 73 8 53 500 Beryllium Cadmium Chloride 19100 Chromium 0.61 0.67 1.2 0.61 4.2 3.2 Cobalt Copper Cyanide Endrin I ron Lead Manganese Mercury Methylene Chloride Nickel Selenium Silver 0.4 0.28 0.62 0.39 0.37 0.51 Sodium 9390 Sulfate Sulfide Total Dissolved Solids 140000 Vanadium Zinc SW-2 1,4-Dioxane (p-Dioxane) 2-Hexanone 3, 3'-Dich lorobenzid ine 3-Methylcholanthrene Acetone 4 Alkalinity, Total as CaCO3 26100 Arsenic 5.5 Barium 81 49.2 57.6 59.4 52.1 46.3 50.6 50.6 49.4 300 44 150 51 47 65 63 Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g, h, i)perylene Benzo(k)fluoranthene Beryllium bis(2-Ethylhexyl)phthalate Chloride 10900 Chloromethane Chromium 0.42 4.7 Chrysene cis-1, 2-Dichloroethene Cobalt Copper Cyanide Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene I ron Lead 11 7.6 Manganese :1 Mercury 0.08 Methylene Chloride Nickel Selenium Silver 0.2 0.2 0.36 0.5 0.26 0.26 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit 250000 pg/L Sulfate NE pg/L Sulfide 2000 pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc SW-1 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 2 pg/L Cadmium 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 2 pg/L Endrin 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-2 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 2-Hexanone NE pg/L 3,3'-Dichlorobenzidine NE pg/L 3-Methylcholanthrene 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 0.05 pg/L Benzo(a)anthracene 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 0.5 pg/L Benzo(k)fluoranthene 4 pg/L Beryllium 3 pg/L bis(2-Ethy1hexyl)phthalate 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the Current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 250000 pg/L NE pg/L 2000 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 40 pg/L 0.1 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 1 pg/L 250000 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 42 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L NE pg/L 250000 pg/L NE pg/L 2000 pg/L 2000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 3 pg/L 40 pg/L 0.1 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 1 pg/L 250000 pg/L 70 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 42 pg/L 2 pg/L 300 pg/L 15 pg/L 50 pg/L 3 pg/L 100 pg/L NE pg/L 250000 pg/L 2000 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Labels Historical detections by well location 12 •w Labels Sodium o 15300 9850 14400 14200 o 14500 12300 11900 11300 11600 Sulfate 13900 79400 21200 19300 16600 13500 20000 11100 9920 Sulfide Tetrahydrofuran 61.3 Toluene Total Dissolved Solids 202000 420000 174000 171000 166000 182000 144000 135000 125000 Vanadium Zinc 250 5 SW-3 1,4-Dioxane (p-Dioxane) 1.3 3&4-Methylphenol(m&p Cresol) 4,4'-DDD 4,4'-DDT Acetone Alkalinity, Total as CaCO3 379000 361000 324000 330000 360000 473000 181000 356000 477000 Barium 278 246 191 169 189 273 122 223 217 Benzene 0.73 Chloride 25100 22400 21600 19600 26100 28000 12000 22300 33800 Chromium cis-1, 2-Dichloroethene Cobalt Copper Cyanide Endosulfan II Iron L ••�� �� err �� �� 5 7.3 Lead Manganese 5640 3870 3400 3280 5130 7890 2130 6310 0.18 Mercury Methylene Chloride Nickel 7.4 4 6.9 3.9 5.5 Sodium 26100 21000 23800 22500 27200 34000 16900 27000 35500 Sulfate 21800 14000 18800 28600 29600 43600 16000 18500 33800 Sulfide 54 Tetrahydrofuran 6.1 3.4 Tin Total Dissolved Solids 477000 402000 406000 421000 415000 .: 241000 413000 Vanadium Zinc 7.1 SW-4 1,1-Dichloroethene 1,4-Dioxane (p-Dioxane) 2-Hexanone 4,4'-DDD 4,4'-DDT Acetone Alkalinity, Total as CaCO3 453000 411000 299000 281000 207000 265000 145000 211000 192000 Barium 202 310 153 170 215 382 124 138 110 Benzene 0.99 0.25 Chloride 50000 57000 33600 42200 44300 18700 24800 29800 36800 Chloroform Chromium 4.7 cis-1,2-Dichloroethene 1.1 0.32 Cobalt Copper 5.8 Cyanide 4.1 Endosulfan II Endrin aldehyde Iron 3110 26000 5080 5580 17400 38700 3890 3020 •� 3.6 Lead Manganese 6400 3600 4840 4510 2960 7710 1470 3580, Methylene Chloride Nickel 8.8 4.9 4.8 4.4 2.6 Sodium 42400 37800 31400 31400 29100 22000 20000 23400 25600 Sulfate 66700 75000 53700 68200 52500 17400 27500 24400 26700 Tetrahydrofuran 9.6 5.5 3.5 9.1 6.7 13.7 5.7 Total Dissolved Solids 452000 471000 392000 444000 236000 327000 317000 . • • § I r . r . I 1 1 Trichlorofluoromethane 0.32 Vanadium Zinc rMM107 14.4 90.1 6.9 8.3 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 250000 pg/L NE pg/L 2000 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 40 pg/L 0.1 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 1 pg/L 250000 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 42 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L NE pg/L 250000 pg/L NE pg/L 2000 pg/L 2000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 3 pg/L 40 pg/L 0.1 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 1 pg/L 250000 pg/L 70 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 42 pg/L 2 pg/L 300 pg/L 15 pg/L 50 pg/L 3 pg/L 100 pg/L NE pg/L 250000 pg/L 2000 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location • Sodium 11600 10200 8420 11300 8390 17600 9840 10300 9160 9990 9896 Sulfate 10900 6270 17100 11600 7280 5620 12700 5490 5090 4240 6180 Sulfide 142 Tetrahydrofuran 18.4 Toluene 0.52 Total Dissolved Solids 129000 106000 113000 105000 125000 117000 120000 114000 91000 101000 101000 Vanadium Zinc 249 28 SW-3 1,4-Dioxane (p-Dioxane) 3&4-Methylphenol(m&p Cresol) 3.6 4,4'-DDD 0.079 4,4'-DDT 0.09 Acetone 16.2 Alkalinity, Total as CaCO3 251000 520000 161000 210000 118000 389000 259000 516000 293000 317000 221000 160000 Barium 173 270 114 152 105 206 181 348 185 315 179 123 Benzene 0.42 0.54 0.32 0.88 0.34 0.25 Chloride 18400 34000 10500 16300 27000 27000 16900 34800 20000 24300 22800 20900 Chromium 3.4 cis-1,2-Dichloroethene 0.26 Cobalt Copper 4.4 Cyanide 4.6 6 7� =171 Endosulfan II Iron it 3390 4160 5270 8890 11700 9560 16500 9370 3230 2.7 Lead Manganese 2310 3860 1420 5080 4320 8930 3990 5200 3760 1890 Mercury Methylene Chloride 1 Nickel 3.6 6.8 2.8 2.8 4.8 12 Sodium 24600 38400 14700 20900 18200 29900 29900 41100 25000 33800 21300 18500 Sulfate 15200 18500 11400 27000 17000 16800 26300 62500 20100 36400 26400 19800 Sulfide Tetrahydrofuran 6.3 3.3 10.2 9.7 18.9 5.1 4.8 4.5 Tin 2.8 Total Dissolved Solids 321000r 231000 300000 233000 473000 319000 , 327000 432000 329000 237000 Vanadium Zinc 9.6 13.6 10.8 SW-4 1,1-Dichloroethene 0.58 1,4-Dioxane (p-Dioxane) 2-Hexanone 3.1 4,4'-DDD 0.062 4,4'-DDT 0.054 Acetone 16 Alkalinity, Total as CaCO3 187000 240000 148000 187000 242000 140000 158000 152000 147000 220000 158000 131000 Barium 121 128 113 115 187 82.8 126 101 106 151 136 105 Benzene Chloride 27400 27900 20300 19800 19000 24300 30800 31000 26900 28800 30900 23600 Chloroform 0.97 Chromium cis-1,2-Dichloroethene Cobalt Copper Cyanide 5.6 Endosulfan II 0.066 Endrin aldehyde 0.061 Iron :1 8 1520 2240 9220 638, 2520 1790 4180 1640 2140 1060 Lead Manganese •11 Methylene Chloride 1.2 Nickel 2.5 3.6 Sodium 23400 26000 16900 20200 23800 17800 24400 20100 18200 29000 20000 17900 Sulfate 18200 28600 16600 24900 23500 17600 23500 23000 13200 32300 23600 19500 Tetrahydrofuran 3.5 3.6 4.1 4.4 Total Dissolved Solids 289000 325000 229000 267000 371000 222000 257000 2700001 255000 349000 272000 234000 Trichlorofluoromethane 0.27 0.25 1.4 Vanadium Zinc 7.3 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 250000 pg/L NE pg/L 2000 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 40 pg/L 0.1 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 1 pg/L 250000 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 42 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L NE pg/L 250000 pg/L NE pg/L 2000 pg/L 2000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 3 pg/L 40 pg/L 0.1 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 1 pg/L 250000 pg/L 70 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 42 pg/L 2 pg/L 300 pg/L 15 pg/L 50 pg/L 3 pg/L 100 pg/L NE pg/L 250000 pg/L 2000 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location • Sodium 8650 Sulfate 38300 Sulfide Tetrahydrofuran Toluene Total Dissolved Solids 189000 Vanadium Zinc 13.5 SW-3 1,4-Dioxane (p-Dioxane) 3&4-Methylphenol(m&p Cresol) 4,4'-DDD 4,4'-DDT Acetone Alkalinity, Total as CaCO3 Barium Benzene Chloride Chromium cis-1, 2-Dichloroethene Cobalt Copper Cyanide Endosulfan II I ron Lead Manganese Mercury Methylene Chloride Nickel Sodium Sulfate Sulfide Tetrahydrofuran Tin Total Dissolved Solids Vanadium Zinc SW-4 1,1-Dichloroethene 1,4-Dioxane (p-Dioxane) 2-Hexanone 4,4'-DDD 4,4'-DDT Acetone Alkalinity, Total as CaCO3 Barium Benzene Chloride Chloroform Chromium cis-1, 2-Dichloroethene Cobalt Copper Cyanide Endosulfan 11 Endrin aldehyde I ron Lead Manganese Methylene Chloride Nickel Sodium Sulfate Tetrahydrofuran Total Dissolved Solids Trich lorofluoromethane Vanadium Zinc Highlighted cells are at or above the Current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 250000 pg/L NE pg/L 2000 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 40 pg/L 0.1 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 1 pg/L 250000 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 42 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L NE pg/L 250000 pg/L NE pg/L 2000 pg/L 2000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 3 pg/L 40 pg/L 0.1 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 1 pg/L 250000 pg/L 70 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 42 pg/L 2 pg/L 300 pg/L 15 pg/L 50 pg/L 3 pg/L 100 pg/L NE pg/L 250000 pg/L 2000 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location • Sodium Sulfate Sulfide Tetrahydrofuran Toluene Total Dissolved Solids Vanadium Zinc SW-3 1,4-Dioxane (p-Dioxane) 3&4-Methylphenol(m&p Cresol) 4,4'-DDD 4,4'-DDT Acetone Alkalinity, Total as CaCO3 Barium Benzene Chloride Chromium cis-1,2-Dich loroethene Cobalt Copper Cyanide Endosulfan II Iron Lead Manganese Mercury Methylene Chloride Nickel Sodium Sulfate Sulfide Tetrahydrofuran Tin Total Dissolved Solids Vanadium Zinc SW-4 1,1-Dichloroethene 1,4-Dioxane (p-Dioxane) 2-Hexanone 4,4'-DDD 4,4'-DDT Acetone Alkalinity, Total as CaCO3 Barium Benzene Chloride Chloroform Chromium cis-1,2-Dich loroethene Cobalt Copper Cyanide Endosulfan II Endrin aldehyde Iron Lead Manganese Methylene Chloride Nickel Sodium Sulfate Tetrahydrofuran Total Dissolved Solids Trichlorofluoromethane Vanadium Zinc Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb Old Salisbury Road Landfill Surface Water Detections within the last 6 years A3 ZB�units MaxofResult ColumnLabels Row 2000 pg/L Acetone 11.2 20000 pg/L Alkalinity, Total as CaC( 71400 36800 39400 40100 15900 22300 27400 49200 43600 33200 57400 27700 150 pg/L Arsenic 8.5 8.5 3.6 21000 pg/L Barium 535 70.7 30.5 25.6 120 109 47 68.2 47.5 86.8 65.9 69.5 6.5 pg/L Beryllium 2 0.54 NE pg/L Cadmium 0.48 230000 pg/L Chloride 24400 29600 14500 12100 35100 55400 18300 29700 35700 49200 26800 26000 11 pg/L Chromium 24.8 3.8 NE pg/L Cobalt 13 NE pg/L Copper 13.8 5.5 8.6 5 pg/L Cyanide 4.4 4.7 1000 pg/L Iron 69000 794 12600 1550 6980 889 1840 6560 4900 5040 5660 5520 NE pg/L Lead 18.3 3.4 NE pg/L Manganese 1250 63.9 488 255 149 48.5 135 926 461 804 1050 465 11000 pg/L Methylene Chloride 2 25 pg/L Nickel 12.2 2.5 NE pg/L Sodium 17900 15000 9360 10400 17000 19400 11800 15600 17000 23000 14200 13000 250000 pg/L Sulfate 7440 7570 979 533 7890 7970 4140 2060 2730 2530 3410 4320 NE pg/L Sulfide 52.1 NE pg/L Total Dissolved Solids 199000 144000 85000 76000 143000 174000 106000 131000 123000 143000 116000 118000 NE pg/L Vanadium 65.8 9.2 NE pg/L Zinc 70.2 16.1 5.2 10.1 7.2 r � � NE pg/L 2000 pg/L 20000 pg/L 150 pg/L 21000 pg/L 230000 pg/L NE pg/L 11 pg/L NE pg/L NE pg/L 5 pg/L 5 pg/L NE pg/L 1000 pg/L NE pg/L NE pg/L 11000 pg/L 25 pg/L NE pg/L NE pg/L 250000 pg/L 3100 pg/L 11 pg/L NE pg/L NE pg/L NE pg/L 1,4-Dioxane (p-Dioxane: 3.3 2.5 2.2 2.7 1.3 Acetone Alkalinity, Total as CaC( 111000 309000 87000 78800 74900 54900 62600 56000 Arsenic 8.3 Barium 92.5 96.9 99.3 100 110 85.6 78.8 74.2 Chloride 21900 9880 19700 19300 20200 19400 12800 13500 Chloromethane Chromium 2.8 cis-1,2-Dichloroethene Copper 2.2 4.1 Cyanide 4.2 Dibenz(a,h)anthracene 2 Indeno(1,2,3-cd)pyrene 2.2 Iron 1500 464 2870 4030 8890 4370 4140 2540 Lead Manganese 549 3180 755 1040 825 680 615 397 Methylene Chloride Nickel 3.5 1.6 Selenium 4.7 Sodium 15300 9850 14400 14200 14500 12300 11900 11300 Sulfate 13900 79400 21200 19300 16600 13500 20000 11100 Tetrahydrofuran Toluene Total Dissolved Solids 202000 420000 174000 171000 166000 182000 144000 135000 Vanadium 4.5 2.4 3.2 Zinc 250 5 12.9 57600 46200 58800 32300 3.7 65.4 77.5 108 73.1 15200 13800 6190 9720 0.12 3.8 0.33 61.3 1740 1790 29900 1510 2.7 196 304 1160 317 3.1 11600 11600 10200 8420 9920 10900 6270 17100 0.52 125000 129000 106000 113000 12/21/2021 1 of 2 Old Salisbury Road Landfill Surface Water Detections within the last 6 years A3 -ZIB�units MaxofResult ColumnLabels Row NE pg/L 1.3 1,4-Dioxane (p-Dioxane) 2000 pg/L Acetone 16.2 20000 pg/L Alkalinity, Total as CaC( 379000 361000 324000 330000 360000 473000 181000 356000 477000 251000 520000 161000 21000 pg/L Barium 278 246 191 169 189 273 122 223 217 173 270 114 1.19 pg/L Benzene 6.73 0.42 230000 pg/L Chloride 25100 22400 21600 19600 26100 28000 12000 22300 33800 18400 34000 10500 NE pg/L cis-1,2-Dichloroethene 0.26 NE pg/L Cobalt 4.5 4.2 12.6 5.3 7.2 3 6.8 5 pg/L Cyanide 4.6 6 1000 pg/L Iron 26700 29900 8300 7910 5650 13000 2500 13100 1720 8240 10500 3390 NE pg/L Lead 5 7.3 NE pg/L Manganese 5640 3870 3400 3280 5130 7890 2130 6310 7340 4750 8350 2310 0.012 pg/L Mercury 0.18 11000 pg/L Methylene Chloride 1 25 pg/L Nickel 7.4 4 6.9 3.9 5.5 3.6 6.8 NE pg/L Sodium 26100 21000 23800 22500 27200 34000 16900 27000 35500 24600 38400 14700 250000 pg/L Sulfate 21800 14000 18800 28600 29600 43600 16000 18500 33800 15200 18500 11400 NE pg/L Sulfide 54 3100 pg/L Tetrahydrofuran 6.1 3.4 6.3 NE pg/L Tin 2.8 NE pg/L Total Dissolved Solids 477000 402000 406000 421000 415000 668000 241000 413000 600000 321000 623000 231000 NE pg/L Vanadium 35.3 7.9 2 2.5 NE pg/L Zinc 7.1 9.6 NE pg/L 7.4 16.5 3.2 6.6 6.5 1,4-Dioxane (p-Dioxane', 2000 pg/L Acetone 16 20000 pg/L Alkalinity, Total as CaC( 453000 411000 299000 281000 207000 265000 145000 211000 192000 187000 240000 148000 21000 pg/L Barium 202 310 153 170 215 382 124 138 110 121 128 113 1.19 pg/L Benzene 0.99 0.25 230000 pg/L Chloride 50000 57000 33600 42200 44300 18700 24800 29800 36800 27400 27900 20300 11 pg/L Chromium 4.7 NE pg/L cis-1,2-Dichloroethene 1.1 0.32 NE pg/L Cobalt 5.3 6.4 2.6 11.6 NE pg/L Copper 5.8 5 pg/L Cyanide 4.1 5.6 1000 pg/L Iron 3110 26000 5080 5580 17400 38700 3890 3020 802 1480 1520 1520 NE pg/L Lead 3.6 NE pg/L Manganese 6400 3600 4840 4510 2960 7710 1470 3580 1020 2900 2930 1930 11000 pg/L Methylene Chloride 1.2 25 pg/L Nickel 8.8 4.9 4.8 4.4 2.6 2.5 NE pg/L Sodium 42400 37800 31400 31400 29100 22000 20000 23400 25600 23400 26000 16900 250000 pg/L Sulfate 66700 75000 53700 68200 52500 17400 27500 24400 26700 18200 28600 16600 3100 pg/L Tetrahydrofuran 9.6 5.5 3.5 9.1 6.7 13.7 5.7 3.5 3.6 NE pg/L Total Dissolved Solids 644000 606000 452000 471000 392000 444000 236000 327000 317000 289000 325000 229000 NE pg/L Trichlorofluoromethane 0.32 NE pg/L Vanadium 38.4 4.6 7.6 4.5 NE pg/L Zinc 14.4 90.1 6.9 8.3 7.3 12/21/2021 2 of 2 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itel Historical detections by date 250000 pg/L 1 pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 0.3 pg/L 1000 pg/L 1 pg/L NE pg/L 0.02 pg/L 70 pg/L 6 pg/L 6 pg/L 1 pg/L 3000 pg/L 70 pg/L 1000 pg/L 600 pg/L NE pg/L 500 pg/L 3 pg/L 500 pg/L November-21 pg/L EPA 300.0 Sulfate EPA 6010D Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Silver Sodium Vanadium Zinc EPA 7470A Mercury EPA 8081E 4,4'-DDE Hexachlorobenzene EPA 8151 2,4-D EPA 8260D 1,1-Dichloroethane 1,4-Dichlorobenzene Benzene Chloroethane cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene lodomethane m&p-Xylene Methylene Chloride o-Xylene 503 42200 977 174000 8380 36800 8300 2140 165000 11900 87600 22300 25500 5.1 274 397 259 203 56.3 192 57.6 181 109 95.6 145 514 272 16.1 1 1.4 0.58 0.44 0.46 0.66 0.82 5.8 3.7 7.1 4.9 6.1 5.2 4.1 • 6 i 4.4 4.3 I 196 87.9 60.9 167 5.3 238 166 20100 17.7 4140 1220 13.9 207126400 12.5 1190 3.6 3440 10.2 11.3 9.6 7.3 9.6 15000 59400 2010 92000 13300 18400 11200 18900 92900 12300 23300 18300 18800 15700 9.8 10 11.1 11.3 11.2 0.35 0.177 2.86 0.92 0.67 1 4.3 0.69 0.47 0.41 0.8 1.3 0.83 0.74 3.7 0.37 9.9 0.74 2.2 1 0.48 12/21/2021 1 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 0.03 pg/L 3 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 300 Ng/L 15 pg/L 50 pg/L 100 Ng/L NE pg/L 0.3 pg/L 1 pg/L 6 pg/L 6 pg/L 1 pg/L 70 pg/L 1000 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 0.55 1:101:111111FIB-1 Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide ft Field Static Water Level May-21 pg/L EPA 300.0 Sulfate EPA 601 OD Arsenic Barium Beryllium Chromium Cobalt Iron Lead Manganese Nickel Sodium Vanadium EPA 7470A Mercury EPA 8260D 1,1-Dichloroethane 1,4-Dichlorobenzene Benzene cis-1,2-Dichloroethene Dichlorodifluoromethane o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane 19.5 14.7 68.8 65.1 12.7 4.8 1 0.61 4A 0.38 1.7 2.4 88700 782000 63100 585000 32000 85000 30000 33800 734000 81300 296000 93800 63000 104000 152000 ���� 129000 ••.��� 165000 207000 84000 145000 ���� 176000 489000 276000 160000 247000 9750 46800 2360 61500 14100 10000 3800 3640 43900 8460 22400 49800 3650 37700 7.8 31.83 7.82 16.8 5.55 10.13 31.54 16.31 48.6 11.31 4.03 5.4 8.31 49.68 38.82 1130 53800 1910 180000 12000 9840 8580 202000 16800 92500 14100 27400 6.2 271 299 246 168 57.7 121 54 238 106 78.1 141 397 241 6.4 1.4 6 •• •.1 81.8 � r r � 5.1 .1 5.8 •111 1 49.7 107 31.4 14 1 1.1 8.8 4.6 47.6 19.5 of 9.3 8 8 9 3.7 15000 52400 1850 79400 13200 14900 10900 15100 108000 11700 25000 15900 18200 14900 0.3 0.39 0.96 0.52 1.3 1.2 0.6 0.74 0.48 0.37 1.1 4.1 0.46 0.68 25.2 16.8 77.5 89.1 11.4 6.5 1.4 10.2 1.2 2.5 12/21 /2021 2 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 3 pg/L NE Ng/L 500000 pg/L 250000 pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 0.3 pg/L 1 pg/L 6 pg/L 6 pg/L 1 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 3 pg/L NE pg/L 6U�LUMMMIIIIIFBA EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride ft Field Static Water Level November-20 pg/L EPA 300.0 Sulfate EPA 601 OD Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Sodium Vanadium EPA 7470A Mercury EPA 8260D 1,1-Dichloroethane 1,4-Dichlorobenzene Benzene cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2540C 1.5 91100 692000 78900 627000 597000 69100 29500 31000 682000 91700 299000 90900 69100 95200 160000 .11111 122000 � 111 153000 145000 93000 155000 @ M o l 183000 M 230000 158000 237000 9990 50400 2120 53600 53100 7910 4370 8040 45400 10100 28000 39000 3830 43500 32.49 6.08 12.51 3.02 8.58 30.5 9.92 49.14 9.89 2.54 3.83 7.07 49.23 37.27 70300 589 189000 8100 8080 8940 2480 156000 23200 90400 7030 36600 4.8 8.5 5.8 5 291 317 273 201 57.3 139 55.8 193 60.2 87 95.9 292 256 41.1 0.78 0.45 0.48 5.8 4.2 6.5 6.1 148;'. 32.3 .1 11 19.4 88 1 1 .1 9.7 5.4 A7t i 1530 23803.5 5.1 4.5 7.8 5.5 15900 59400 2120 8480C 13700 16500 11100 20600 77400 12700 18300 15000 19600 18900 1.8 0.51 0.64 1.2 0.58 1.7 0.57 2.4 0.34 0.95 0.66 0.65 12.9 13.4 90.9 69.6 1 0.61 5.4 0.66 1.6 1.5 1.9 90800 765000 81100 5770001 350001 78900 25200 38900 535000 94700 174000 83400 66900 83500 12/21 /2021 3 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 500000 Ng/L 250000 pg/L 70 pg/L NE pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 10 pg/L 1 pg/L 300 pg/L 50 pg/L 100 pg/L NE pg/L 2000 pg/L 0.3 pg/L 1 pg/L 6 pg/L 6 pg/L 1 pg/L 3000 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 0.03 pg/L 3 pg/L NE pg/L n c FB-1 146000 ���� 154000 139000 76000 134000 .� ��� 194000 337000 158000 146000 262000 Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D Sulfide ft Field Static Water Level May-20 feet Field Static Water Level Ng/L EPA 300.0 Sulfate EPA 601 OD Arsenic Barium Beryllium Cadmium Chromium Cobalt Iron Manganese Nickel Sodium Tin Vanadium EPA 7470A Mercury EPA 8260D 1,1-Dichloroethane 1,4-Dichlorobenzene Benzene Chloroethane cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 153000 ���� 9610 49300 1920 52700 15400 6510 4410 47170 30800 11100 14100 20700 3860 61400 6.3 82.2 32.15 6.97 14.24 4.91 9.51 31.8 11.96 49.5 10.88 3.22 4.61 7.76 49.85 38.23 32.82 6.69 13.01 4.85 9.3 32.51 9.37 50.28 10.43 3.37 4.55 7.87 50.1 37.81 76400 801 162000 7770 10400 9360 nffklo 22800 227000 6520 38300 5.8 290 309 257 176 56.5 136 52.9 238 66 98.1 224 196 241 23.8 0.72 0.62 6.8 5.6 4 31.4 21.1 • r 1 1 1.8 107.111 8 211 125 43.5 5.1 1 so 7.9 1 . @ 10.6 80.8 27.4 3.9 16800 65600 2150 73800 17100 16200 12900 16200 148000 1240C 28600 12600 17900 19700 4.8 7.1 0.65 0.69 9 0.52 0.66 0.46 0.9 0.56 0.48 0.56 0.29 0.85 1.2 0.84 0.91 0.52 1.1 2.4 0.72 0.46 0.34 0.53 38.6 11.4 70.5 130 8.9 1.1 5.6 1.3 1 2.2 86600 6880001 709001 5170001 35700 71600 25000 33900 6350001 1270001 3330001 66400 65500 96500 12/21 /2021 4 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 11111 • 1000 • pg/L 1111 . 11 . 11 • 1 . 11 . 1 ./L pg/L 1 1000 :EPA • • • 11 . Concentration MW-1R --llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■lllllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■lllllllllll■lllllllllll■- MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL SM 1 Dissolved Solids - SM 411 ■NE Sulfide feet Field Static Water Level Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Fiel ..mv Field REDOX EPA 300.0 EPA 601 OD Manganese SeleniumNE Sodium. 1• 8260D - - Chloride 840000 '.111 854000 111 - 111 • 111 1111 1180000 1111 812000 .111 1111 .•111 __- • 1 1 . • 11 llllllllllli 11 1 1 llllllllllllllllllll,lllllllllll� ' 1 • 1 lllllllllll.�•... 1 1 111 • 1 1 : • 11 lllllllllll..n�.. 11 111111111111111,11111111111111111- ---------------__- �����-�����®llllllllllllli'®llllllllllllll'®®__- ---------------__- 111 ® 111 ®: :1 - 111 ®:.1 ®. 1 266000 •11 •• 11 �- •1.11 __- -®1 "" -------------__- - 27.1 11.5 72.6 ----- 11.4 1.9 ----__- 6180 78700 1020 4490 24100 937 ®®®�®' 12700 6180 901 ©- -®--IIIIIIIIIIIIIIIIIIIITiI-�®�' 95.4 31400 1570 1500 58.8 143 ®' _�- _�- 11 •1111111111111� . 11 11- :•11 1:11 •11 :111 •• •11 11 :.11 ••11__- 3 1.6 1.8 5.1 ---- 4 1.3 1.6 -- 1.5 ====C============= 1.5EPA --------------__- 3.9 4 ---- 4.8 --------__- 12/21 /2021 5 of 46 A4 Facility Permit Qualifier 34-12 Old Salisbury Road Landfill (C&D) (Multiple Itel Historical detections by date 500 pg/L 0.7 pg/L 2000 pg/L 600 pg/L 3 pg/L 2000 pg/L 0.03 pg/L 3 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 0.45 o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D Sulfide pmhos/cm Field Field Specific Conductance deg C Field Field Temperature May-19 feet Field Static Water Level Total Well Depth mg/I Field 83 8.6 1.7 1.1 84000 736000 69800 384000 34300 180000 .111 179000 169000 9150 52500 2000 34000 14800 6.4 221.9 1450 375.6 967 175.7 13 13.7 14.5 16.1 15.7 100.3 20.5 43.18 16.43 28.22 120 42 54 40 60 13.1 154.41 141 1 0.48 8.2 0.58 1.5 58500 666001 91300 115000 152000 311000 6310 3710 72100 144.9 192.41 507.6 14.2 14.2 16.3 24.421 151.2 113.25 401 1201 96 12/21 /2021 6 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 250000 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 1 pg/L 3 pg/L 6 pg/L 6000 pg/L 1 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 2.31 1.78 3.85 1.58 11.68 0.94 12.52 11. 44 4.17 6.8 4.97 8.11 3.07 3.65 � = FB-1 Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX Ng/L EPA 300.0 Sulfate EPA 6010D Barium Beryllium Chromium Cobalt Copper Iron Manganese Nickel Sodium Vanadium Zinc EPA 7470A Mercury EPA 8260E Mod. _ 1,4-Dioxane (p-Dioxane) EPA 8260D 1,1-Dichloroethane Acetone Benzene cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D 3.37 11.71 59.87 19.46 7.55 0.94 3.05 9.06 23.79 12.98 2.42 4.17 3 24.7 10.46 12.09 12.43 121 11.42 10.47 10.24 10.26 12.49 11.57 11.53 10.45 10.25 12.15 193 333.4 293.4 297.8 81.6 165.9 65.1 47.7 603.7 608.2 -469.8 -402.2 219.3 111.2 85100 1210 163000 8620 12800 6560 235000 22300 149000 5910 45900 285 260 320 216 55.8 168 47.8 217 65.6 100 200 138 234 29.8 0.61 0.6 0.61 5.4 3.5 9.6 19.5 4690 8240 1 13.4 91800 6850 1130 8.4 63.5 3.3 14 7.1 232011 20500 7.2 275001 1740 1990 2260-5.2 6.2 42.3 36.2 38.3 4.4 1 15800 57300 2540 71200 13000 17500 9620 14100 136000 12800 20700 9940 17400 23000 5.2 18 5.9 5.1 2.3 2 0.43 1.3 10.2 0.68 0.33 0.33 0.9 0.67 1.5 0.4 1.4 3 1 0.68 0.28 0.52 51.3 11.4 80.4 113 9.2 0.97 2 1.7 0.81 0.92 83800 577000 488000 129000 29200 54200 26600 29700 506000 154000 176000 52800 64900 74200 202000 l IIW Wes " 11$1 167000 175000 192000 170000 190000M 1111 115000 163000 448000 30000 9770 42300 44600 2220 15600 6470 4290 6830 65100 12300 34000 6290 3870 115000 7.2 12/21 /2021 7 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R I MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Sulfide Field Field Specific Conductance deg C Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX Field Field Specific Conductance deg C Field Field Temperature feet Field Static Water Level Total - Depth Field Oxygen, Dissolved NTU FieldTurbidity Std. Units -�� ,----r------___ now =$, �®' ' ®®�-IIIIIIIIIIIIIIIIiE3®�®®' ' llllllllllllllll�®®®__- 12/21 /2021 8 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 250000 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 1 pg/L NE t1g/L 6 pg/L NE pg/L 1 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 600 pg/L 3 pg/L 2000 pg/L 88 pg/L 3 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010D Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Sodium Vanadium Zinc EPA 7470A Mercury EPA 8151 MCPP EPA 8260E 1,1-Dichloroethane 4-Methyl-2-pentanone (MIBK) Benzene cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl acetate EPA 8260B Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D 5.4 6.3 6.3 6.3 6.2 5.6 5.7 5.7 6.5 5.9 5.9 5.5 5.7 6.1 -135.3 -43.2 -69.5 48 198.2 30.8 145 158.8 -175.7 -55.8 -39.6 -27.7 163.8 -59.7 95900 1300 104000 8090 12700 1060 so@ 20700 91700 5650 49900 284 258 275 222 59.8 161 36 215 83.1 95.8 132 124 246 24.4 0.62 0.88 0.69 0.83 1 3.3 5.5 4.2 5.6 6 2.6 1.1 42.4 250 2.6 71.8 25.8 16.7 : • 1 16.1 •5 44 4 10.7 i s 11.1 3.3 9.8 6.3 2.8 16500 64400 2770 42600 14600 17700 8300 15700 151000 13600 17600 10900 18600 26100 5.1 5.2 6 5.3 5.8 0.57 1.3 0.65 0.37 0.55 0.85 0.38 0.86 0.99 2.4 1.1 0.59 0.53 1 :: 45.4 50.5 169 0.26 0.9 1.2 1.3 1 0.86 0.21 2 2.1 2.4 84100 573000 192000 291000 35600 78500 24200 33500 652000 161000 117000 52800 67100 89900 164000 .1IIO 213000 496000 156000 171000 68000 13900011 0111 237000 301000 111000 154000 395000 8920 34500 2660 25200 15100 6580 3110 5330 88500 11800 14400 5120 3840 128000 678 4.1 5 12/21 /2021 9 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units NE pg/L 1111 . 1 . ' : 1000 . 11 . 1Manganese, • 11 ./L NE •/L r 1 . 4 1 . NE pg/L 6000 .. Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Sulfide Field Field Specific Conductance deg C Field Field Temperature feet Field Static Water Level Total Well Depth Oxygen, Dissolved NTU FieldField Field Turbidity Std. Units Field.mv Field REDOX ` 300.0 ` 6010 ..: . Nickel-®--------�-__- Sodium11 6020B EPA r ` 8260 enzene - . • • , ®®��-lllllllllllllllll:l3®�®�����__- ---------------__- 1 111 ®.' 1 11 ®: 1 - 11 ®':1 - 307000__- ---------------__- --®------------__- 20Yllllllllll®���� 10.4 18�������� --©----------©__- ® 4260 84300 3980�-®�® 3300 27300 ®�� 453 __- 10300 8100 357 17500 1580 95.5 507 __- 11111111111113 : 11 : 11 - .. I I IIIIIIIIIIfID 11 111 111 .1111111111111� . • 11 1 11 __- --- 10.3 4.3EPA ----------__- -----------__- ---------------__- ---------------__- --------------__- --------------__- 12/21 /2021 10 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 6 pg/L 6 pg/L 6000 pg/L 1 pg/L 700 pg/L 0.41 0.55 = FIB-1 Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D Sulfide Nmhos/cm Field Field Specific Conductance `C Field Field Temperature December-17 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene Acetone Benzene Carbon Disulfide 0.45 0.71 0.55 0.85 0.23 1.2 3 1.7 0.68 1.7 2.4 0.65 0.78 46 24.9 192 5.9 14.8 0.93 1.2 1.3 0.89 0.79 0.42 76100 663000 115000 101000 33600 75900 27000 31800 506000 130000 65800 47200 61800 112000 166000 -11 177000 250000 164000 181000 75000 133000 II II � � 232000 218000 107000 152000 369000 9040 42200 2180 12500 15200 6490 3660 4830 158000 12500 11100 4790 3930 89700 5 4.8 4.4 4.8 4.2 105 240 221.7 1391 423.5 343.9 176.7 234.9 70.7 155.8 1840 349.9 304.2 121.8 183.9 641 22 17.2 18.7 18.2 17.3 17.8 16.5 18.9 17.4 17.9 17 16.2 19.1 16.9 35.1 8.3 21.15 9.44 11.5 37 18.55 52.94 12.18 4.14 5.46 9.09 5209. 39.58 60 21 27 20 50 48 27 60 21 20 15.7 20 60 48 3.3 0.4 0.5 0.6 5.1 1 4.5 6.2 0.1 0.1 0.3 1.3 2.9 2.3 2.8 2.4 9.4 9.6 4.2 3.5 9.7 9.6 7.8 9.8 9.7 9.7 7.4 2.7 5.6 6.4 6.4 6.1 6.1 5.6 5.7 5.7 6.4 6.1 6 5.8 5.6 6.1 112.4 -38.8 -37.4 100.2 106.5 78.2 169.8 132.7 -50.6 -43.9 163.2 216.5 150.5 105.1 0.54 1.6 0.37 13.7 0.39 0.57 1 2.1 12/21/2021 11 of 46 A4 Facility Permit Qualifier 70 pg/L Chloroform 70 pg/L cis-1,2-Dichloroethene 1000 pg/L Dichlorodifluoromethane 600 pg/L Ethylbenzene 500 pg/L m&p-Xylene 3 pg/L Methylene Chloride 500 pg/L o-Xylene 0.7 pg/L Tetrachloroethene 2000 pg/L Tetrahydrofuran 600 pg/L Toluene 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 0.03 pg/L Vinyl chloride 500 pg/L Xylenes (Total) pmhos/cm Field Field Specific Conductance >C Field Field Temperature November-17 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH 34-12 Old Salisbury Road Landfill (C&D) (Multiple Itel Historical detections by date 0.44 0.76 0.66 1.1 0.271 0.23 1.7 3.6 0.41 1.6 1.3 1.1 0.62 1.1 59.1 135 0.35 0.651 1.31 0.58 0.81 0.22 IN 214.6 1320 383.61 1140 175.11 1 236.6 75.21 148.6 18731 329.2 308.61 111.4 169.21 832 11.7 5.7 7.7 11.8 11.4 9.9 6.7 11 11.7 12.5 11.2 11.2 9.9 8.2 69.55 16.44 40.74 8.92 11.42 73.26 35.28 105.72 24.24 8.7 10.61 18 103.92 39.37 60 21 27 20 30 48 27 60 21 20 15.7 20 60 50.85 0.6 2.09 0.3 0.23 5.95 0.5 4.2 6.3 0.1 0.1 0.34 4.3 3.3 4.36 1.1 11.87 7.6 8.94 j 0.92j 0.1 0.4 7.9 9.3 8.9 1.61 2.8 2.4 98.53 5.6 6.3 6.4 6.21 6.11 5.6 5.6 5.5 6.3 6.1 6.1 5.6 12/21 /2021 12 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 300 pg/L 15 pg/L 50 Ng/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 1 pg/L 50 pg/L 70 pg/L 0.3 pg/L 6 pg/L 6 pg/L NE pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 0.03 pg/L 1000 pg/L NE pg/L 500000 pg/L 250000 pg/L my Field REDOX Ng/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium Beryllium Chromium Cobalt Iron Lead Manganese Nickel Sodium Vanadium Zinc EPA 7470 Mercury EPA 8151 2,4,5-TP (Silvex) 2,4-D Pentachlorophenol EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8270 Butylbenzylphthalate SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-S2D 158.6 -10.1 -109.6 48.5 70.4 135.5 166.3 2068. 44.7 -43 60.9 182.2 215.5 65.2 122000 179000 7830 13400 4740 64100 16200 62400 4960 59600 9 260 323 278 198 53.2 152 46.5 196 106 89.8 84.2 116 214 17.1 0.52 0.54 4 2.7 3.2 1 4.9 7.2 4.6 3.8 3.2 43.1 1 1 3.4 37.9 25 37.6 166 1 • 11 125 193 93.9 1 1 11.8 1.11 20.3 1 1 1 7.5 4.2 43 3.6 10.6 .11 7.6 •1 17.9 18.4 15200 77600 2380 65500 13500 15300 9860 14900 138000 12300 13200 9740 17100 19800 539 5.8 5 5.3 7.1 0.23 0.072 0.27 0.018 0.48 1.4 0.46 1.1 12.1 0.38 0.52 0.44 0.62 0.6 1.1 0.23 1.2 3.9 1.4 1.1 0.68 0.97 28 20.1 131 0.93 1.5 1.6 1.2 0.52 0.87 0.71 1.7 71400 670000 78900 461000 33500 80400 28200 27900 520000 130000 73800 44600 63500 110000 153000 :111 164000 111 144000 175000 82000 136000 1111 218000 219000 90000 142000 370000 9290 47600 2650 49200 16200 7390 3860 4430 163000 13000 10400 4770 3620 89800 12121 /2021 13 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units NE pg/L 1111 . 11 • 1 • 11 • 1 • NE pg/L 1 • 1 . 1 . .111 . • pg/L 1 • •11 .Ethylbenzene 11 • Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Sulfide Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA 300.0 - ` 6010 Cobalt Manganese Sodium' ` 8260 . - - Acetone Carbon Disulfide • - - - - - ---------------__- 1111 - 111 ----- 333000 11 ----__- ---------------__- -®-®-----®�----__- ---------®-----__- 20.6 3870 - - 59.9 302 ----- ----- 21.8 2400 -----__- 26700 ----__- 9200 - 801 ----- 8390 1720 ----__- 1 1 llllllllllllllllllll, 1 1 llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll, 1 1 1 1 1 11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --------- ' ' -----__- --------- 2.7 -----__- ---------------__- -------------__- -----®®----__- 2.1700 -------------__- ------------__- --------------__- ---------®-----__- 12/21 /2021 14 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itel Historical detections by date 2000 pg/L 600 pg/L 3 pg/L NE pg/L 500000 pg/L 250000 pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L Tetrahydrofuran Toluene Trichloroethene SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride pmhos/cm Field Field Specific Conductance .0 Field Field Temperature May-17 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium Beryllium Chromium 1 36.3 1 9.3 11 1821 4.5 0.27 1 587000 315000 446000 135000 • .1 l s oil r' $ $' 226000 50400 35800 :1$ $ 13500 1246 756 1714 354.9 24.3 14.8 23 16.6 70.19 7.83 36.9 8.21 21.4 73.38 30.33 105.64 11.55 3.94 9.22 8.7 51.86 77.72 60 27 50 48 27 60 15.71 20 60 50.85 1.3 0.5 5.4 0.4 5.4 6.51 0.3 4.03 3.28 3.06 3.5 5.3 3.1 4.2 1.16 0.4 9.26 1.75 5.42 23.24 5.5 6.3 5.9 5.5 5.6 5.5 5.9 5.6 5.5 6.3 179.6 60 182.6 210.2 195 178.8 107.5 138.8 147 121 7740 6720 2700 960 86100 5670 663 58300 5.5 272 309 57.1 163 42.9 207 113 120 221 22.7 0.6 4.6 12/21 /2021 15 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units •/L 300 • 1 ... 11 . NE •/L 1 • 111 • 1 .111 • 1 . 3 pg/L 11 . 1 ./L 111 . NE pg/L 11111 ./L 1111 . 1 . Concentration MW-1R MW-2R MW-3R 11.5 MW-4R ------------__- MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Cobalt Iron Copper • Manganese Sodium:11-�- ` 8260 Acetone Methylene Chloride------ o-Xylene--------------__- Tetrachloroethene - - Alkalinity, Total as • SM 1 Total Dissolved Solids - SM 1 1 Field Field Specific Conductance oc Field -Field Temperature feet Field Static Water Level Oxygen,Total Well Depth FielDissolvedNTU Field Turbidity Std. Units Field �- --®------------_ 89300 714 1740 18.2 - ®- -----------®--®__- 6460 --- 51.9 ©�-- 134 �� 359 __- '11- :111111111111� 11-- . 11 1111 .•11 --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll, 1 1 llllllllllllllllllll, 1 1 1 1• 111111111111111,11111111111111111- ---------------_�- ---- 4.4 --------- 5 __- ---------------__- --------------�__- 3.1 --------__- -------------�-__- -------®--IIIIIIIIIIIIIIIIIIIIO-�®__- .:.11 -111 - 11 - 111 1:1111 -- 11 �11 11 •: 11 __- ---------------__- 111 111 -- ::111 :•111 1111 1111 __- ®"' 1 -lllllllllll��...11llllllllllllllllll, 11 llllllllllllllllllll,lllllllllll� 1 . 1 llllllllllilllllllllllllllllllll,llllllllllllllllllll, ' 11 lllllllllli�lllllllllll....... 1 111 111111111111111,11111111111111111- ---------------__- --®-®--®-----®-__- ��llllllllllll�llllllllllll�llllllllllll�llllllllllll�llllllllllll���lllllllllllll�llllllllllll�llllllllllll�llllllllllll�llllllllllll�llllllllllll�lllllll�llllllll�� '®' ®' ' llllllllM11lllllllll�llllllll®' IIIIIIIIIIIIIIIIIIII,IIIIIIIIIiLSi1111111111+��r.11llllY:Y�Jlllllllllllll�llllllllllll�lllllllll�lllllllll� 1 1 111111111111�111111111111111,11111111111111111- ®��lllllllllllll®®�lllllllllllll®®���������� 12/21 /2021 16 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 0.3 pg/L 1000 pg/L 0.008 pg/L 0.004 pg/L 6 pg/L 6 pg/L NE pg/L 6000 pg/L 1 pg/L 700 pg/L 70 pg/L 3 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 5.6 6.2 6.3 6.1 5.9 5.6 5.7 5.5 6.2 6 5.9 5.7 5.6 6.4 1:1411:111111 FBA Field pH my Field REDOX Ng/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium Beryllium Chromium Cobalt Iron Lead Manganese Nickel Selenium Sodium Vanadium Zinc EPA 8081 Heptachlor Heptachlor epoxide EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Carbon Disulfide Chloroform Chloromethane cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E 137.2 24.1 61.4 176.7 242.9 152 217.5 272 62.3 16.7 175.1 241.4 270.5 177.E 1380 121000 1530 193000 8450 3800 4090 3440 1II 17100 129000 5390 1400 58700 3.9 2.6 241 272 297 255 55.9 140 44 195 148 93.1 144 91.6 188 14 0.58 0.57 2.8 5.8 4.1 6.4 96.2 •:0 86400 3.5 214 149 2.6 of 274 123 7.3 18.5 8 35.6 2.7 8.5 10.7 6.2 26.7 13.7 5 14600 70200 2450 71000 14200 16200 9700 15700 184000 12000 19200 9380 16200 20200 5.7 8.4 7.3 5.7 5.1 12.8 6.3 0.53 1.5 0.39 2.5 14.1 25.4 0.38 0.42 0.83 5.2 0.44 0.4 0.2 0.47 1.1 0.33 0.62 0.88 2.3 0.38 0.55 2.2 2.1 0.63 2.1 0.48 39.1 13.6 21.7 237 26.8 16.8 1.2 1.5 1 2.8 0.58 4.4 64300 571000 133000 454000 32700 80100 25800 23300 626000 107000 72900 42300 59700 101000 154000 : 11 � 168000 153000 67000 135000 Us 0 0 0 -189000 286000 79000 118000 371000 9630 47600 2050 58400 16400 4820 2670 4360 202000 14500 23300 4100 34101 98000 12121 /2021 17 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 1 . 1111 • 1 . 11 • 1 . 111 . 11 . 1 .Manganese• Concentration MW-1R --IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■®IIIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIIII■IIIIIIIIIIIII■IIIIIIIIIIIIII■- MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL .-Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA .1 Chloride Field Field Specific Conductance Field Temperature Field Static Water Level .. 300.0 - .. . 1 1 ... . • • - mom --IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIIIIIIIII■IIIIIIIIIIIII■IIIIIIIIIIIII■- 3.7Field --------__- -�l�IIIIIIIIIIIIIIIIIIIIIF� �� Tfeet 1�111111111111����111111111111111111111111111111111111111111- --1111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111- --11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- ---------------__- 1:1 111 :11w: 11 ®111111111111111111111111111®®IIIIIIIIIIIIIIIIIIIIIIIII, :11 11 .•111 ®IIIIIIIIIIIIIIIIIIIIIIIII, • 1111111111111111111111111111111111111111111- ---------------__- 4.7 -------------__- --®------®-----__- ��IIIIIIIIIIIIIiJlllllllllllll�lllllllllllllllllllllllllllllllll�Illllllllllllllll�lllllllllllllll�lllllllllllllllll�llllllllllllllllll�lllllllllllllllll�lllllllllllllllll�lllllllllllllllll�llllllllllllllllllllllllllllllllllllllmlllllllllllll■IIIIIIIIIIIII■- ®----®-- 13.6 --__- 18 10.2----- 705 3.1 -----__- E4360 77200111111111111---� ----- 11800 19.1 29400 --IIIIIIIIIIIIIIIIIIID-;�-__- 312 11000 312 ® 10900 6800 515 �� 530 1820 90.8 284 116 __- 12/21 /2021 18 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 11 • 1 ./L NE •/L 2000 . 1 •/L 111 . 40 • • • 1 . 3 pg/L 11 . 1 ./L 0.03 . NE pg/L 11111 . 1111 . 1 . Concentration MW-1R -®llllllllllllllll■®llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll�llllllllllllllll■®llllllllllllllll�®llllllllllllllll■lllllllllll■lllllllllll■- MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Selenium Sodium11 Vanadium EPA 1 .. 8081 • EPA 8260 ■ • - - Methylene Chloride® o-Xylene--------------__- Tetrachloroethene • •- SM 1. Alkalinity, Total as • SM 1 Dissolved Solids - SM 1 1 feet -Field WaterStatic - _ Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX Field --®------------__- • 1111111111111� 11 11- .�11 ®' '1 11 1 11 11 11� 'II 1 ---------®--®--_®- 4.2 4.2 ---- 20 -- 22.6 --__- - ---------------__- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- ---------------__- ------®--------__- ---------------__- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- 1.7 ------------__- --------------�__- 4.4 3.4 3.2 - 9.5 6 - 1.3 -------------__- ---------------__- 0.72 -------------__- I•11 , 111 111K 1=111 __- ---------------__- 1 769000 ::111 111 111 - 111 . 111 1 111 111 .111 111 111 111 :111 __- • 111 11 lllllllllll :11 11 llllllllllllllllllll,lllllllllli�iiJalllllllllll'.•+•'lllllllllll.,.n...11llllllllll....a.. 11 . 111 lllllllllli:rr.•.11lllllllll..a... '' 111 111111111111111,11111111111111111- ---------------__- -®��---®-®®----__- --11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --®11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --IIIIIIIIIIIIIIIIIIII011111111111111111111�11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --1111111111111111111�11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- 12/21 /2021 19 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itel Historical detections by date 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L Field Specific Conductance >C Field Field Temperature November-15 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium Beryllium Chromium Cobalt Copper 365.E 13.6 72.25 16.3 43.76 20.31 23.2 60 21 27 20 30 2.2 2 0.2 3.3 5.9 1 5.6 3 9.6 1 5.4 6.1 6.3 5.8 5.8 34.8 -35.2 -91.6 48.8 52.6 1070 115000 2200 70300 7430 207 279 271 184 92.7 1 1 6.2 9 36.731 107.71 24.151 7.17 9.511 17.47 104.891 78.88 8 27 60 21 20 15.58 20 60 50.85 7 4.4 6.3 0.2 0.1 3.4 1.2 4.8 2.8 1 1.6 2.6 295 9.3 8.9 51.6 5.9 154.9 5 5.4 5.3 5.4 5.9 5.8 5.5 5.4 6.2 9 4 54.3 77.7 38.7 23.3 5.2 49.61 34.8 0 1350 1110 63600 19100 70800 10100 1080 70000 2.6 4.5 0 34.4 186 241 97.2 95.7 71.5 183 74 1.9 0.68 0.63 3.5 5.4 6.3 2.8 7.1 12/21 /2021 20 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 300 Ng/L 15 Ng/L 50 Ng/L 100 pg/L 20 pg/L NE Ng/L pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 1 pg/L 40 pg/L 0.008 pg/L 0.004 pg/L 6 pg/L 6 pg/L 40 pg/L NE pg/L 6000 pg/L 1 pg/L 70 pg/L 3 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 600 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L NE pg/L 200 pg/L 0.005 pg/L 100 pg/L 0.05 pg/L NE pg/L 500000 pg/L 250000 pg/L �� 3.8 •�� = FIB-1 48.6 ••� 8.5 33.2 •�� 49.6 •� •2.8 6 3.9 Iron Lead Manganese Nickel Selenium Sodium Thallium Tin Vanadium Zinc EPA 7470 Mercury EPA 8081 Endosulfan 1 Heptachlor Heptachlor epoxide EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene 2-Hexanone 4-Methyl-2-pentanone (MIBK) Acetone Benzene Chloroform Chloromethane cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8270 2,4-Dinitrotoluene 2,6-Dinitrotoluene Benzo(g,h,i)perylene Dibenz(a,h)anthracene Di-n-octylphthalate Indeno(1,2,3-cd)pyrene SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E 82.8 2.8 tell � � 3.7 : • � 33.6 3.3 4 ]1400 13200 6 2590 23800 11300 15700 7940 14500 1980 g1206wO 13700 12200 15800 218000.2 8 5.6 5.8 8.7 5.9 7.1 27.2 8.6 6.3 35.4 0.12 0.17 0 0.91 0.38 0.69 2.6 11.8 0.44 0.25 0.26 0.8 0.26 1 0.761 0.231 2.1 0.4 1 0.84 0.68 1.3 2.3 0.27 1.2 0.43 2 1.1 1 35.8 7 17.7 120 19.8 0.27 0.66 1 1.4 1.1 0.82 0.54 4.8 1 5.9 8.1 1 5.6 5.6 48100 440000 102000 144000 32300 67300 23200 23400 48200 127000 41000 37100 51500 103000 78000 :LI11l 1370001 161000 104000 78000 79000 142000 403000 281000 234000 110000 135000 362000 8510 487001 2990 16900 16200 6050 2040 4710 47400 14900 9000 3270 3930 113000 12121 /2021 21 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 1 . 1111 • 1 •/L 11 . 1 • NE pg/L 1 . 1 1 • 1 • NE pg/L Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Cyanide Field Field-----------__- - - Field Field Temperature feet Field Total Well Depth FieldStatic Water Level Field Oxygen, Dissolved NTU TurbidityStd. Units FieldField.mv Field REDOX ' 300.0 ' 6010 Chromium----®----®--®-®__- Manganese Sodium. EPA 1EPA 8151 ' 8260 • - - - - - --- ®' �llllllll�lllllllll+rn�.11lllllll�llllllllllllllllllll,lllllllll®•' ram}-,�, ' lllllllllllll®llllllllll�' ' 11 : llllllll�lllllllll®111111111111111111111111,11111111111111111- ®®��-lllllllllllllllll:l3®�®�����__- ®®®-lllllllllllllllli'm®���®®��__- ---------------__- 11 •:�11 111 11 :111 -�®" 1 1 1� 11 .11 �� ' 'II __- ---------------__- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®llllllllllllllllllll,llllllllllllllllllll,®®11111111111111111111,111111111111111,11111111111111111- - 20.3 10.1 15.2 ----- 4.8 2.5 ----__- 9560 56000 3650 31400 524 1400 695 10600 11900 7980 315 736 1990 271 1 1 1 1 llllllllllllllllllll, 1 1 1 1 1 llllllllllllllllllll, 1 1 � 1 1�� 1 1off1 1 1 off1 1 1 1 1 111111111111111,11111111111111111- 5.1 -------------__- 11.4 8.8 - 4.3 ---- 4.9 3.2 - 3.4 - 24.7 ---------------__- -------------__- -®-------------__- ---------------__- -®llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- 1.7 -----------__- 12/21 /2021 22 of 46 A4 Facility Permit 34-12 Qualifier (Multiple Ite Old Salisbury Road Landfill (C&D) Historical detections by date 70 pg/L 3 pg/L 70 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 600 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L i 0.26 Chloroform Chloromethane cis-1,2-Dichloroethene Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride Nmhos/cm Field Field Specific Conductance 'C Field Field Temperature November-14 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mV 0.13 0.73 1 1.5 1.2 2.3 2.1 0.4 0.85 34.6 5.8 14.1 1451 16.9 0.63 0.79 1.5 0.79 0.98 0.22 0.59 4.4 39600 358000 107000 117000 28600 64100 20000 18900 47300 132000 19200 36900 45200 91500 133000 MI 182000 304000 166000 145000 61000 134000 279000 239000 163000 107000 131000 360000 7640 44200 2990 22200 15700 4340 1960 4290 51800 14400 8070 3760 3510 98200 153.1 985 363.4 422 175.1 194.8 50.9 148.3 297.2 407.8 234.3 115 150.1 611 18 13.7 15 13.3 14.7 16.7 16.1 17.5 17.1 13.4 14.9 18.7 17.1 17.3 Mw 69.7 17.18 21.87 18.4 22.36 36.9 37.58 104.74 24.68 5.4 10.76 18.48 103.8 79 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 1 0.5 6.3 0.5 5 0.5 2.3 8.3 0.5 0.5 0.5 3.8 1.25 1.7 3.53 5.2 10 3.6 1.2 9.1 2 98 9.9 5.2 152 7.8 20.1 5.6 6.1 6 5.9 61 5.5 5.1 5.9 5.91 5.6 5.6 6.2 12/21 /2021 23 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 1 pg/L 6 pg/L 6 pg/L NE pg/L 1 pg/L 3000 pg/L 70 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L = FB-1 Field REDOX Ng/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Sodium Vanadium Zinc EPA 7470 Mercury EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene 4-Methyl-2-pentanone (MIBK) Benzene Chloroethane cis-1,2-Dichloroethene Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S21) 194 38 13 158 198 184 224 252 198 -61 101 232 242 182 1720 117000 3740 143000 8180 13 00 2100 12800 32800 8660 43800 2.6 3.5 142 339 221 305 58.2 111 38 193 262 96.8 59.2 130 193 41.5 1.4 1.2 0.6 3.4 4.8 3 4.5 9.6 3.8 4.8 85.8 :1 11 2.7 126 221 76.5 55.9 4.1 3.6 1 1 5.4 . 1 233 2.9 • :: 1 :1 1 1 2.6 22.9 19.9 7.6 1 1 1 1 33 25.91 7.2 4.1 5.3 10600 58300 2770 55400 13700 16600 7810 14600 6860 10000 12800 10700 14400 24000 mil 16.8 7.2 5.3 6.2 13.7 13.3 5.3 0.33 1.1 1.3 0.4 2.2 0.42 0.44 2.1 0.5 0.73 0.35 0.73 1.1 1.1 0.33 2.9 0.36 0.65 79.2 15.9 8.8 106 15.5 0.85 2.4 1.2 0.96 0.57 3.9 37600 453000 177000 286000 24000 62400 22800 18300 42200 143000 40500 36200 42300 54700 120000 ••111 191000 EVEJUS11 163000 138000 64000 141000 86000 228000 135000 119000 119000 464000 7090 49800 2940 50500 15500 4300 1350 3610 2220 15000 8240 5870 3720 146000 4.4 4.2 00.4 4.3 5.1 12/21 /2021 24 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units NE pg/L 1111 • 1 ./L 1 pg/L ./L 11 • 1 . 11 . NE pg/L 111 . 1 ./L 1 . 11 ■ 1 ./L Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Sulfide Field Field Specific Conductance Field Field Temperature Field Static Water Level Total Well ■Field Oxygen, Dissolved NTU Turbidity FieldField Std. Units Field.mv Field REDOX ' 300.0 ' 6010 Arsenic--------------__- Chromium Cobalt • Manganese - - Sodium1: EPA 1 EPA .1 Chloroform--------------�__- ■ . - - - Chloride - - Tetrachloroethene infeet 1 =rr or __IIIIIIIIIIIIIIIIIIID_®_®_-_®_©_®_©_�_�_�_®_�_____-_ ---------------__- __- ---------------__- 5.4 -------------__- ----------__- =- 50I 320 46.6 -®=®==® 30 -� 797950 9260 641 ------------__- 1 1960 196 ®®®®=== 1 1 1ME ' 1 1 llllllllllllllllllll, ' 1 1 . 1 1 llllllllllllllllllll, 1 1 llllllllll�' 1 1 1 lllllllllllllllllllll,llllllllll'� 1 1 1111111111111111,11111111111111111- ----®-------llllllllllllll®llllllllllllll'®-__- ---------------__- ---------------__- 1.8 ------------__- 3.7 -------------®_- -------------__- 1.8 -------------__- 12121 /2021 25 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L 250000 pg/L 700 pg/L 1 pg/L 300 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 50 pg/L 70 pg/L 6 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 3.7 0.62 0.47 0.2 0.32 0.34 5.3 = FB-1 Trichlorofluoromethane SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride Nmhos/cm Field Field Specific Conductance 'C Field Field Temperature November-13 feet Field Static Water Level Total Well Depth mg/1 Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Barium Cobalt Iron Manganese Nickel Sodium Vanadium Zinc EPA 8151 2,4,5-TP (Silvex) 2,4-D EPA 8260 1,1-Dichloroethane Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane 30000 344000 155000 222000 31900 51900 21300 18300 31400 175000 45500 46400 37400 96600 91000 f•111 00 1870 445000 167000 126000 50000 107000 63000 207000 149000 113000 124000 373000 5600 50500 3260 29700 13900 3600 18001 3610 1820 12400 6180 3880 3630 83400 137 1040 367 715 194 171 64 155 86 430 243 149 156 623 18.4 19.6 18.7 14.8 14.7 17.2 16 17.7 15 14.4 15 16.6 17.7 17.8 71.87 16.65 45.08 18.63 22.73 76.44 36.08 106.03 24.77 9.1 10.56 18.83 104.66 79.28 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 8.7 0.9 0.7 7.5 5.61 0.5 10.2 9.2 2.2 0.5 6.51 1.3 6.5 2.8 1 3 1 12 3 2 5 11 4 8 9 123 250 21 5.6 5.6 5.9 5.8 5.9 5.5 5.4 5.2 5.2 5.9 5.8 5.4 5.41 6.2 228 68 -8 207 239 200 357 363 327 -66 189 280 355 241 128000 3400 113000 8310 10400 27400 9360 53200 106 311 201 296 53.9 98.8 25.4 170 112 87.8 47.6 106 140 23.8 • 89.5 136 136 84.3 253 1 239 1 27.1 9990 6.3 19.4 6.8 6.9 7.9 1 48.8 1 14 9940 46200 42600 13800 13000 5580 13500 9070 10500 11700 12300 25300 12.2 17.1 0.23 1.1 1.3 0.9 0.27 0.77 0.41 0.54 0.28 12/21 /2021 26 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 500 . 1 ./L 2000 . 0.03 NE pg/L 11111 . r 111 . 300 . r ... Concentration MW-1R MW-2R 3 MW-3R -------------__- MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Chloride . Tetrachloroethene .. .. Alkalinity, Total as 03 Dissolved Solids Field Field Specific Conductance oc Field Field Temperature May-1 3 feet Field Static Water Level TotalDepth Field Oxygen, DissolvedNTU Field Turbidity Std. Units Field Field pH mv Field REDOX .. 300.0 .. 6010 Cobalt18.2 •, , - • , -------------__- 2.2 -------------__- 0.95 -------------__- 1I III .� 1 I111111111111111,11111111111111111- 1 111 654000 111 �16I 111 1111111111111111,11111111111111111- --lllllllllllllllial®---------�®__- ---------------__- ---------------__- 64.1 35.3 ---------��1-__- ------ 65.1 - 6.6 --__- 877 34100 ��--� 867llllllllllllll 30700 324 8610 5820 4 440 7880 9630 496 1890 ® 158 240 160 __- 12/21 /2021 27 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 100 pg/L NE pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6 pg/L 40 pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 500 pg/L 3 pg/L 6 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 500 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 20.7 8.6 Nickel Sodium Tin Vanadium Zinc EPA 8260 1,1-Dichloroethane 2-Hexanone Acetone Benzene Chloroform cis-1,2-Dichloroethene m&p-Xylene Methylene Chloride Naphthalene o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Xylenes (Total) SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide Nmhos/cm Field Field Specific Conductance 'C Field Field Temperature November-12 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field 9080 45700 42600 13000 14300 6120 12900 8290 11100 19100 13500 26700 5.8 21.1 10.5 13.6 37.3 27.4 22.7 1.2 0.84 0.48 20.3 0.63 0.26 0.72 0.96 1.3 0.54 0.27 111 8.5 24.2 7.4 0.68 12.1 0.25 0.36 0.38 4.3 1.2 29800 363000 175000 203000 34800 63500 22800 21700 32100 189000 29600 58700 35600 78900 84000 ,-11� 175000 413000 131000 108000 51000 100000 46000 228000 138000 87000 102000 442000 5910 50000 3860 33700 16200 5340 2070 4300 2040 14200 5820 3820 4290 124000 8.1 5 68 802 217 382 116 106 31 88 43 400 197 136 81 403 20.9 19.7 15.7 15.6 15.2 16.3 17.5 18.1 16.3 14.7 14.7 16.5 18.2 17.9 72.24 17.78 45.36 1926. 22.81 77.49 37.56 105.53 25.13 8.94 10.71 18.71 104.68 79.91 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 5.5 1.5 1.2 2.3 6.4 1.8 9.8 7.3 4.4 0.9 3 2.3 6.4 2.3 1 1 25 14 14 7 1 1 1 25 1 605 329 456 5.7 5.8 5.6 5.7 5.8 5.4 5.7 5.5 5 6.1 5.9 5.5 5.5 6.5 12/21 /2021 28 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 0.1 pg/L 0.002 pg/L 42 pg/L 2 pg/L 2 pg/L 0.004 pg/L 6 pg/L 1 pg/L 3000 pg/L 70 pg/L 70 pg/L 1000 pg/L 3 pg/L 6 pg/L 500 pg/L 0.7 pg/L 2000 pg/L 3 pg/L 2000 pg/L 500 pg/L 0.05 pg/L 3 pg/L 5 pg/L NE pg/L 500000 pg/L 250000 pg/L 236 77 16 181 245 197 260 352 366 -61 150 246 365 160 REDOX Ng/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Sodium Vanadium Zinc EPA 8081 4,4'-DDD Dieldrin Endosulfan II Endrin Endrin aldehyde Heptachlor epoxide EPA 8260 1,1-Dichloroethane Benzene Chloroethane Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane Methylene Chloride Naphthalene o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Xylenes (Total) EPA 8270 Benzo(a)anthracene bis(2-Ethylhexyl)phthalate Chrysene SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E 79500 5420 73600 8400 2090 10400 24200 9770 35600 7.1 91.7 335 173 40C 53.4 95.1 26.9 142 101 76.8 50.5 279 160 143 3.5 6 6.7 6.9 5.8 10.5 1 i i 102 60.8 218 1 11 7.5 1 9.5 21.8 17.4 5.1 33.6 13.7 9180 43400 43600 14500 13900 6980 13100 5280 8770 11000 14600 15000 21200 24.5 15.2 92 30.8 51 23 45.6 0.062 1 0.12 0.27 0.23 1.2 1.2 1.3 :25 0.49 0.62 0.28 1.6 0.63 93.2 13.5 26 6.3 0.77 16.9 0.29 0.49 0.49 8.1 0.98 0.79 2.4 1.5 1.1 1 26300 277000 142000 174000 31200 51900 19500 17200 25500 153000 40200 43900 28900 77600 95000 me 172000 435000 157000 111000 58000 118000 63000 220000 127000 144000 127000 298000 5320 640001 3920 34500 16100 38101 1860 3560 1800 12900 4900 6150 47901 143000 12121 /2021 29 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itel Historical detections by date 70 pg/L NE pg/L 250000 pg/L 10 pg/L Cyanide SM 4500-S2D Sulfide pmhos/cm Field Field Specific Conductance °C Field Field Temperature April-12 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Arsenic 9.1 106 100 100 842 283 655 175 147 49 134 63 354 158 136 137 434 16 14 15.2 13.3 15.9 14.5 15.6 16 16.3 16 16.1 15.8 15.8 15.5 36.43 7.99 21.01 8.24 10.55 38.23 15.03 52.4 11.92 4.13 5.04 8.92 5203. 39.39 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 5 2.9 0.8 0.7 8.7 0.8 6.7 7.2 4.8 0.5 5.4 1.6 6.9 2.5 1 4 3 7 2 1 7 2 2 14 8 150 32 112 5.2 5.8 5.8 5.5 5.4 5.51 5.5 5.2 5.2 5.5 6.1 5.9 5.8 6.4 166 43 -24 156 189 185 176 180 196 -78 166 189 177 121 95000 6860 98700 7910 9700 20500 9420 25800 1 5.7 12/21 /2021 30 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 11 • 11 . 1Manganese, . 11 ./L 1 • NE pg/L 1 •• 111 • 1 1 . 1 1 1 0.006 . 0.019 . 1 1 . 0.002 0.008 ./L 1 1 1 ./L 1 . 1 ./L 1 • 11 . 1 ./L 111 . 0.005 • 11 • 1 1 1 • Concentration MW-1R �®" MW-2R MW-3R lllllllllllll®' MW-4R lllllllllllll�®llllllllllllllll■ MW-5R MW-6R MW-7 11 MW-8 ®IIIIIIIIIIIIIIIYiilllllllllllll�llllllllllll�llllllllllll�llllllllllllll�®®lllllllllll■lllllllllll■- MW-9!�7MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Cobalt . Nickel-®-----------®-__- Sodium Vanadium------------ .. 8081 - - ■ ■ ■ - - ■ ■ .. .: - . - Dieldrin Heptachlor Heptachlor epoxide • EPA .1 Chloroform--------------®__- ■ • - - - Chloride Naphthalene o-Xylene-------------__- Tetrachloroethene . . . . - EPA 1 • - - - - - - _ ■ • - - - 14.8 16.4 21.5 -----------__- 3190I 41500 26300 539 3760 1140 10000 __- 8280 9310 370 --®i --- 1580 ® 91.5 170 327 __- -®-------------__- ® 1 1 llllllllllllllllllll, 1 1 1 1 1 llllllllllllllllllll, 111111111111® . 1 1 llllllllllllllllllll . MOO 1 1 1 1 1 1 111111111111111,11111111111111111- 7.2 - 23.4 __- ---------------__- ------ 0.13 --------__- 0.54 - 0.14 ------ 1 1 11111111111111111111,---__- 0.12 0.12 ---- 0.1 --------__- 0.18 - 0.069 0.081 --------__- 0.48 -------------__- ------ 0.066 --------__- -------------__- ---------------__- 1.5 -------------__- 3.2 -------------__- 1.7 -------------__- ------------®__- ---------------__- ------------ 1.1 --__- -- 5.5 ------------__- ------------ 1.2 --__- 12/21/2021 31 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 0.05 •/L NE • 11111 . 1111 .Chloride 1 . NE pg/L 1111 . 1 . 300 • 1 ./L NE pg/L 111 ■ NE pg/L 11111 •/L Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 1.2 MW-13 1.5 MW-14 --__- MW-15 Trip Blank EQBL lndeno(1,2,3-cd)pyrene----------- SIM 1 : Alkalinity, Total• SIM 1 . Dissolved . . SIM ' 11 SIM ' 11 Cyanide SIM 11 ) Sulfide Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Fiel -• ■ •-llllllllllllllllllll,® EPA 300.0 EPA 6010 Cobalt--- • Manganese Sodium SM 1 Alkalinity, 0 SM 1 Total Dissolved • • SM 1 1 ---------------__- 11 ••111 1111 •� 11111 - 1 11 1 11 1 11 111 1111 11 11 1 11 11 __- ------------__- 111 531000 •:111 �111•111 - 1.111 111 111•111 . 111 1111 1111 111 •1111 __- ------------__- 11 ---------------__- --------------__- ---------------__- ------------llllllllllllll�--__- 11 11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- ---------------__- ----------__- ---------------__- ---- 14.7 15 -- 368 3540 ----------__- ----------__- 11 11 ----------__- ----®----------__- ---------------__- 11 -- 111 : 11 11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,---__- ---------------__- • 111 -- 111 • 111 11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,---__- ---------------__- 12121 /2021 32 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 1111 ./L 250000 • 1 •/L 11 . 1 . . 11 pg/L 1 ./L 1 111 . 1 ./L Concentration MW-1R --llllllllllllllll■ MW-2R MW-3R MW-4R 11 MW-5R . 11 MW-6R llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■lllllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■lllllllllll■lllllllllll■- MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL ChlorideField Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Fiel-®®---lllllllllllllllll:f3®�®����-__- Oxygen, Dissolved NTU •TurbidityStd. Units FieldField.mv Field REDOX EPA 300.0 ' ' 6010 Chromium------------®--__- • .. Manganese Silver Sodium:11 EPA .1 M-Dichloroethene -��---©��llllllllllllllllllll©®�®�-__- lllllllllll�--__- ---------------__- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®11111111111111111111,11111111111111111111,111111111111111,11111111111111111- 11.8 -------------__- 2980 40300 ----®- 424 23000 3030 6140 2050 -__- -_ 7920 7310 -_-_-_®_�_-_�_ 1250 58.3 140 71 -©�llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,111111111111111,11111111111111111- ---- I l l lllllllllli"- 1 11 11 -__- ------------ 10.8 --__- -®-----®----®' lllllllllllllllll®-__- ---------------__- -------------__- 12/21 /2021 33 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 6000 . 1 ./L 1 • 3 pg/L 11 . 1 ./L 111 . NE pg/L 11111 ./L NS pg/L NE pg/L Concentration MW-1R -®llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■lllllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllll®' MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank ' EQBL ®- Acetone Chloroform-------------__- • - - - Methylene Chloride o-Xylene-®-------------__- Tetrachloroethene . . SIM 1 : Alkalinity, Total as CaCO3•111 SIM 1 Total Dissolved Solids••:111 SIM 11 Fiel--llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,---__- Field Field Specific Conductance •Field Temperaturefeet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA 350.1 Nitrogen, Ammonia EPA 6010 Sodium11 ' 8260 2 -------------__- ------------__- 3.5 -------------_ 3.2 - 1.8 -------------__- -®-------------__- ---------------__- 111 --- 11 •.1111 11 111 '1 11 �� 11 111 -__- ---------------__- :1111 --- '111 111 :111 :•111 . 111 '111 •111 :111 -__- -------------__- ---------------__- 12/21 /2021 34 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units • 1 ./L NE pg/L 250000 •/L 700pg/L 200 . 6000 ./L r .Chloroform-------------__- 500 Concentration MW-1R MW-2R 1.6 MW-3R -------------__- MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Tetrachloroethene Alkalinity, Total as CaCO3 Field Field Specific Conductance ChlorideStatic Water Level Field Field Temperature May-1 1 feet Field Total Well Depth Field Oxygen, Dissolved NTU Turbidity FieldField Std. Units Field.mv Fiel__llllllllllllllll_®_�_-_�_®_�_®_�_�_�_®_-_____-_ -• ■ • EPA 6010 Barium EPA 8260 .. Acetone--------------__- 1.6 -------------__- -------------__- ®®��-lllllllllllllllll:l3®�®����-__- --------------__- 1.3 -------------__- ----------llllllllllll�-�-__- ----®--------__- 12/21 /2021 35 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units • 11 . 1 •/L 111 ./L 111 . 11pg/L 1 • Concentration MW-1R MW-2R 4.1 MW-3R -------------__- MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Chloride - - Tetrachloroethene Tetrahydrofuran Field Field Specific Conductance oc Field - • TemperatureField Waterfeet Static - - Total Well-•FielField Oxygen, Dissolved NTU •TurbidityStd. Units Field Field pH mv Field REDOX .. 6010 Barium EPA .1 Chloride Field Specific Conductance oc FieldField - - - ------------__- 1.4 -------------__- -----��-----__- �' �lllllllll�lllllllllllllllllllllllll�...11llllllllllllllllll,llllllllliilllllllll� 1 1 IIIIIIIIII�IIIIIIIIIIIIiJlllllllllll�llllllllllll�®11111111111111111111,111111111111111,11111111111111111- ����lllllllllllll®-®' ���®�lllllllllllll®lllllllllllll®-__- ---------------__- ®�lllllllllllll®®- 11 lllllllllllll®���®' llllllllllllll�-__- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®11111111111111111111,11111111111111111111,111111111111111,11111111111111111- -®�-®--------__- 4.2Field -------------__- ®'' ����-®®����llllllllllllll®llllllllllllll®-__- 12/21 /2021 36 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA 8260 Field Field Specific Conductance oc Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA 6010 EPA 8260 -�111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111- 12/21 /2021 37 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 111 .Trichlorofluoromethane Concentration MW-1R -®-------------__- MW-2R MW-3R MW-4R MW-5R MW-6R IF MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Field Field Specific Conductance Field Field TemperatureStatic Water Level feet Field Total Well Depth FielField Oxygen, Dissolved NTU •TurbidityStd. Units Field Field pH mv Fiel �• . • FieldFieldSpecific. .oc Field Field • feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field rbidity TuStd. Units Field Field pH �����-IIIIIIIIIIIIIIT•�3= ------------lllllllllllll�--__- 12/21 /2021 38 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 11 1 .Chromium pg/L 3 pg/L 11 • 1 • 1 • pg/L Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL mv Field REDOX .. . 1 1 Carbon Disulfide Methylene Chloride Field EPA 8260Field Field Specific Conductance oc Water700 Field Field Temperature feet Static - - Total Well -•Field Oxygen, Dissolved Std. Units Field Field pH mv Field REDOX ' ' 6010 EPA .1700 Carbon Disulfide Field--11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- Field Specific Conductance®llllllllllllll...11llllllllllllllm®llllllllllllllllllll,®lllllllllllllllll�®®®llllllllllllll{�llllllllllllllllmllllllllllllll��a..11llllllllllllllllll,lllllllllllllll,llllllllllllllll1- • Temperature--11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- Field ---------------__- 10.7 -__- ---------------__- 1-���lllllllllllllll®®��®-__- ---------------__- -11111111111137®®�����-__- llllllllllllllll�-__- -��-------__- ---------------__- lllllllllllllllll®-__- 12/21 /2021 39 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units r .Chromium r . r 700 . r . Concentration ' feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH mv Field REDOX EPA 6010 Barium EPA 8260 Field Field Specific Conductance March --®-------------__- oc Field Field Temperature i :feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH mv Field REDOX EPA 6010 EPA r MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R I MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL 40.2 -__- ------------- -------------__- 26.2 -__- ---------------__- J-� lllllllllllll� -___ ®�lllllllllll®-®� ' --®------------__- ---------------__- 12/21 /2021 40 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 4000 • .111 . „pg/L Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL ` 8260 . Acetone Field Field Specific Conductance Field Field • - • feet TotalField = :-Level Field Oxygen,Std. Units FieldField. mv Field .. Barium Field Field Specific Conductance FieldField�®wwwww®www®lllllllll®llllllllllll■lllllll■■� A - feet Field :. = Level Field Std. Units Oxygen, DissolvedField Field • mv Fiel��wwwwwww�ww®ww■■� - .. ---------------�■- ---------------®■- ��llllllllll�llllllllll�lllllllll�llllllllllllllll■��������llllllllllllllll■lllllllllll■■- ��wwww■�■ww�wwwww■■� ���������������llllllll■■� ���������������lllllll■■� ��®wwwwww�wwwww■■� ®®wwwwllllllllllllllmllllllllllllllm®wwwww■■� ��w®www®®wwww®w■■� ��wwwwww®wwwww■■� ��wwwwlllllllllllll®llllllllllllllmllllllllllllllm®wllllllllllllllm®ww■■� ��®wwwww®®wwww■■� ��wwwwwww�www®w■■� ��wwwwwww�wwwwwllllllll■■� ��wwwwwww�wwwww■■� ��®wwwwllllllllllllllm®�®wwww■■� ■ �■ ���������������lllllll■■� �■ �llllllll■■■ ���������������llllllll■■� �wwwwwww�wwwww■■� www®www®®wwwlllllllllllll®llllllllllll■lllllll■■� ���������������llllllll■■� ��®wwwwww�wwwww■■� 12/21/2021 41 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 4 111 • 11 . 1 . 1 ./L 11 • 11pg/L 11 • Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL - ' Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH mv Field RED• Arsenic-------------�-__- Field Field Specific Conductance Field Temperature April-06 Barium .. 6010 ---------------_�- --llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,llllllllllllllllllll,®11111111111111111111,111111111111111,11111111111111111- -- 24Field ------------__- ®�lllllllllllll®®-llllllllllllll�®®�®���-__- ®®��-lllllllllllllllll:l3®�®����-__- ®����-IIIIIIIIIIIIIIIIiFi®�®�®lllllllllllll®®-__- llllllllllllll�-__- -- 211111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,11111111111111111- ------------- 23Field -__- ---------------__- llllllllllllllllll®���-__- 12/21 /2021 42 of 46 A4 Facility Permit Qualifier 15 Ng/L Lead EPA 7470 1 Ng/L Mercury EPA 8260 3 Ng/L Chloromethane June-05 Ng/L (blank) 700 Ng/L Barium 10 Ng/L Chromium 20 Ng/L Selenium November-04 Ng/L (blank) 10 Ng/L Arsenic 700 Ng/L Barium 10 Ng/L Chromium August-04 Ng/L (blank) 700 Ng/L Barium 10 Ng/L Chromium 15 Ng/L Lead 20 Ng/L Selenium May-04 Ng/L (blank) 10 Ng/L Arsenic 700 Ng/L Barium 10 Ng/L Chromium 15 Ng/L Lead November-03 Ng/L (blank) 10 Ng/L Arsenic 700 Ng/L Barium 10 Ng/L Chromium 15 Ng/L Lead 34-12 Old Salisbury Road Landfill (C&D) (Multiple Itel Historical detections by date 5.9 0.341 1 1 0.41 1 0.241 0.261 1 0.21 1 1 1 0.44 I 481 431 3001 1501 531 I 531 251 851 821 241 501 461 691 I I I I 5.6 5.1 95 52 340 140 80 63 30 95 55 28 77 57 66 2 2.3 4.4 2.4 3.9 2.1 4.8 14 ®® 26 18 ®-- 820 150 981 471 741 160 170 3.3 9.2 3.2 6.8� 11� 8 12/21 /2021 43 of 46 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Itei Historical detections by date 2L Units 1 . 1 ./L 11 . 1 . 1 . 1 .Arsenic 11 . 1 . .11 . 1 . 11 . 1 . 1 . • 1 . Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank EQBL Barium Cadmium---- 1 i------___ Arsenic--®------------__- November-011 • Toluene - . 2.7 ----------__- 17-------__- ®--®®- ����-------__- ©- 15 - 23 26llllllllllllllll l 23 -------__- -- 21 -----------__- 17 36 12IIIIIIIIIIIIIIIIIIID 16 ------__- ®:1 22 �� ®----- 16 - 11 19 35 900 95 36 � 140 ® 95 38 1300 2700 270 94 36 150 ------__- ------__- ------__- ------__- Mllllt ------___ -- 18llllllllllllllll� 16 46 ------__- ------__- �®:1 -� 16 950 50 53 ®i 38 I 49lllllllllllllllii� lllllllllllllllli� 1300 210 26 2600 92 210Z ------__- �1 ------___ 45811 2600420------__- ©- -11�;� -- �� 31 1500 1 �� -- 100 28 80 82IIIIIIIIIIIlllll l 580 240 65 400 -------__- -------__- 12/21 /2021 44 of 46 2L Units Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Blank EQBL IIJ T 860 §§IMIUI �MME IJ 14 24 60 29 � 62 I] 40 40-® 950960 ]�- 110 38 - 190 �- 50 j 30 13 13 10 a. 10 _ -_,__ J9 1100 1400 20001300 12 210 77 300 96 12 350 m 68I 39 76 29 36 &i� 860 850 820 � 1200 49 34 25 130 170 33 430 m 19 32 43 69 201 38 rj]��.1]Y]�j9MEMI-Ii] 1800 11 43 16 55 16 14 410 ® 31 26 29 31� 53 g 800 750 3 ----- 28 - 70 21 180 27 23 A4 Facility Permit 34-12 Qualifier (Multiple Old Salisbury Road Landfill (C&D) Historical detections by date 700 10 15 1 4000 700 2 700 10 15 1 October-96 Ng/L (blank) Barium Chromium Lead Mercury January-96 pg/L (blank) 2-Butanone (MEK) Barium Cadmium Carbon Disulfide Chromium Lead Mercury 180 6 0.2 16 815 790 20 720 970 47 43 10 21 16 20llllllllllllllllllllllffll6 0.3 0.4 2 86 224 350 595 1111111111111IME 23 12 6 1.80.4 0.71.7 0.8 12/21/2021 46 of 46 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix B — Laboratory Reports Appendix Laboratory Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix B — Laboratory Reports This page intentionally left blank. lLIL, yilcal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 December 02, 2021 Mark Filardi HDR 440 S. Church St Suite 900 Charlotte, NC 28202 RE: Project: OSR LANDFILL Pace Project No.: 92572199 Dear Mark Filardi: Enclosed are the analytical results for sample(s) received by the laboratory on November 12, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, ��K— 4--- Tyler Forney tyler.forney@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Charles Gruenberg REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 185 lacmnalyfical(e' www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92572199 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Mold Certification #: LAB0152 Texas Certification #: T 104704245-17-14 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: VT2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A21-A 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: OSR LANDFILL Pace Project No.: 92572199 Lab ID Sample ID Matrix Date Collected Date Received 92572199001 MW-1R Water 11/10/2113:30 11/12/2114:00 92572199002 MW-2R Water 11/08/2114:00 11/12/2114:00 92572199003 MW-3R Water 11/11/2116:00 11/12/2114:00 92572199004 MW-4R Water 11/12/2111:30 11/12/2114:00 92572199005 MW-5R Water 11/11/2118:05 11/12/2114:00 92572199006 MW-7 Water 11/12/2110:00 11/12/2114:00 92572199007 MW-8 Water 11/12/2108:30 11/12/2114:00 92572199008 MW-9 Water 11/11/2114:50 11/12/2114:00 92572199009 MW-10 Water 11/09/2112:20 11/12/2114:00 92572199010 MW-11 Water 11/09/2110:20 11/12/2114:00 92572199011 MW-12 Water 11/08/2117:40 11/12/2114:00 92572199012 MW-13 Water 11/08/2116:30 11/12/2114:00 92572199013 MW-14 Water 11/11/2112:50 11/12/2114:00 92572199014 MW-15 Water 11/08/2111:50 11/12/2114:00 92572199015 SW-1 Water 11/11/2111:40 11/12/2114:00 92572199016 SW-3 Water 11/08/2114:30 11/12/2114:00 92572199017 SW-4 Water 11/08/2115:20 11/12/2114:00 92572199018 SW-2 Water 11/09/2112:40 11/12/2114:00 92572199019 E13-1 Water 11/08/2112:20 11/12/2114:00 92572199020 1713-1 Water 11/08/2112:45 11/12/2114:00 92572199021 T13-1 Water 11/12/2100:00 11/12/2114:00 92572199022 T13-2 Water 11/12/2100:00 11/12/2114:00 92572199023 T13-3 Water 11/12/2100:00 11/12/2114:00 92572199024 T13-4 Water 11/12/2100:00 11/12/2114:00 92572199025 T13-5 Water 11/12/2100:00 11/12/2114:00 92572199026 T13-6 Water 11/12/2100:00 11/12/2114:00 92572199027 T13-7 Water 11/12/2100:00 11/12/2114:00 92572199028 T13-8 Water 11/12/2100:00 11/12/2114:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR LANDFILL 92572199 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92572199001 MW-1 R EPA 8081 B AMM 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199002 MW-2R EPA 8081 B MTJ 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD CBV, RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D NSCQ 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 MMB 1 PASI-A 92572199003 MW-3R EPA 8081 B AO 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL Pace Project No.: 92572199 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199004 MW-4R EPA 8081B AMM 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 EWS 1 PASI-A SM 2540C-2015 ZMC 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199005 MW-5R EPA 8081 B AO 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 YEG 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199006 MW-7 EPA 8081 B AO 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL Pace Project No.: 92572199 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 EWS 1 PASI-A SM 2540C-2015 ZMC 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199007 MW-8 EPA 8081 B AO 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 EWS 1 PASI-A SM 2540C-2015 ZMC 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199008 MW-9 EPA 8081 B HLJ 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 EWS 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL Pace Project No.: 92572199 Analytes Lab ID Sample ID Method Analysts Reported Laboratory SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199009 MW-10 EPA 8081 B AMM 23 PAN EPA 8151 AO, KLM 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD CBV, RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 ZMC 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199010 MW-11 EPA 8081 B AO 23 PAN EPA 8151 AO, KLM 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 ZMC 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199011 MW-12 EPA 8081 B MTJ 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D NSCQ 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL Pace Project No.: 92572199 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 MMB 1 PASI-A 92572199012 MW-13 EPA 8081 B MTJ 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D NSCQ 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 MMB 1 PASI-A 92572199013 MW-14 EPA 8081B HLJ 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A D13131 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 EWS 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199014 MW-115 EPA 8081 B MTJ 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL Pace Project No.: 92572199 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D NSCQ 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 MMB 1 PASI-A 92572199015 SW-1 EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 EWS 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199016 SW-3 EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8260D NSCQ 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 MMB 1 PASI-A 92572199017 SW-4 EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL Pace Project No.: 92572199 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 MMB 1 PASI-A 92572199018 SW-2 EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 ZMC 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 KDF1 1 PASI-A 92572199019 EB-1 EPA 8081 B MTJ 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 MMB 1 PASI-A 92572199020 F13-1 EPA 8081 B MTJ 23 PAN EPA 8151 AO 11 PAN EPA 8082A SEM 8 PASI-C EPA 601 OD RDT 18 PASI-A EPA7470A DBB1 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL Pace Project No.: 92572199 Analytes Lab ID Sample ID Method Analysts Reported Laboratory SM 2320B-2011 SMK 1 PASI-A SM 2540C-2015 MJP 1 PASI-A SM 4500-S2D-2011 JP1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 KDF1 1 PASI-A SM 4500-CN-E-2016 MMB 1 PASI-A 92572199021 T13-1 EPA 8260D CL 53 PASI-C 92572199022 T13-2 EPA 8260D CL 53 PASI-C 92572199023 T13-3 EPA 8260D CL 53 PASI-C 92572199024 T13-4 EPA 8260D CL 53 PASI-C 92572199025 T13-5 EPA 8260D CL 53 PASI-C 92572199026 T13-6 EPA 8260D CL 53 PASI-C 92572199027 T13-7 EPA 8260D CL 53 PASI-C 92572199028 T13-8 EPA 8260D CL 53 PASI-C PAN = Pace National - Mt. Juliet PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92572199 Lab Sample ID Method 92572199001 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 7470A EPA 8260D EPA 8260D SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199002 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 SUMMARY OF DETECTION Client Sample ID Parameters Result Units Report Limit Analyzed MWA R Barium 274 ug/L 5.0 11/29/2117:37 Cadmium 0.58J ug/L 1.0 11/29/2117:37 Manganese 28.7 ug/L 5.0 11/29/2117:37 Sodium 15000 ug/L 5000 11/29/2117:37 Mercury 3.1 ug/L 0.20 11/25/2108:58 cis-1,2-Dichloroethene 0.801 ug/L 1.0 11/16/2106:42 Ethylbenzene 0.37J ug/L 1.0 11/16/2106:42 Alkalinity, Total as CaCO3 88700 ug/L 5000 11/18/21 14:57 Total Dissolved Solids 152000 ug/L 25000 11/16/21 10:21 Sulfate 503J ug/L 1000 11/13/2120:55 Chloride 9750 ug/L 1000 11/19/2108:03 MW-2R Barium 397 ug/L 5.0 11/29/2117:41 Cadmium 0.44J ug/L 1.0 11/29/2117:41 Chromium 5.8 ug/L 5.0 11/29/2117:41 Cobalt 26.2 ug/L 5.0 11/29/2117:41 Copper 6.0 ug/L 5.0 11/29/2117:41 Iron 7700 ug/L 50.0 11/29/2117:41 Manganese 20100 ug/L 50.0 11/30/2113:47 Nickel 17.7 ug/L 5.0 11/29/2117:41 Silver 7.3 ug/L 5.0 11/29/2117:41 Sodium 59400 ug/L 5000 11/29/2117:41 Vanadium 96.9 ug/L 5.0 11/29/2117:41 Benzene 3.7 ug/L 1.0 11/13/21 19:03 Chloroethane 4.3 ug/L 1.0 11/13/21 19:03 1,4-Dichlorobenzene 0.67J ug/L 1.0 11/13/21 19:03 Dichlorodifluoromethane 0.74J ug/L 1.0 11/13/21 19:03 cis-1,2-Dichloroethene 1.3 ug/L 1.0 11/13/21 19:03 lodomethane 9.91 ug/L 20.0 11/13/21 19:03 Methylene Chloride 2.2J ug/L 5.0 11/13/21 19:03 Tetrahydrofuran 19.5 ug/L 10.0 11/13/21 19:03 Trichloroethene 1.0 ug/L 1.0 11/13/21 19:03 Trichlorofluoromethane 0.61J ug/L 1.0 11/13/21 19:03 Vinyl chloride 1.0 ug/L 1.0 11/13/21 19:03 1,4-Dioxane (p-Dioxane) 4.1 ug/L 2.0 11/16/21 00:19 Alkalinity, Total as CaCO3 782000 ug/L 5000 11/16/21 15:06 Total Dissolved Solids 920000 ug/L 50000 11/14/21 17:02 Sulfate 42200 ug/L 1000 11/13/2121:11 Chloride 46800 ug/L 2000 11/19/2108:04 92572199003 MW-3R EPA 601OD Barium 259 ug/L 5.0 11/29/2117:44 EPA 601OD Cadmium 0.46J ug/L 1.0 11/29/2117:44 EPA 601OD Cobalt 10.1 ug/L 5.0 11/29/2117:44 EPA 601OD Iron 72900 ug/L 50.0 11/29/2117:44 EPA 601OD Manganese 4140 ug/L 5.0 11/29/2117:44 EPA 601OD Sodium 2010J ug/L 5000 11/29/2117:44 REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92572199 Lab Sample ID Client Sample ID Method Parameters 92572199003 EPA 6010D SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199004 EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199005 EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199006 EPA 8081 B EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 6010D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D EPA 8260D MW-3R Vanadium Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-4R Barium Cadmium Chromium Cobalt Iron Manganese Nickel Sodium Vanadium Tetrahydrofuran 1,4-Dioxane (p-Dioxane) Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-5R Barium Chromium Iron Sodium Vanadium Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-7 4,4'-DDE Barium Cadmium Iron Manganese Sodium Zinc Benzene 1,1-Dichloroethane cis-1,2-Dichloroethene Methylene Chloride Tetrahydrofuran Trichlorofluoromethane m&p-Xylene SUMMARY OF DETECTION Result Units Report Limit Analyzed Qualifiers 25.8 ug/L 5.0 11/29/2117:44 63100 ug/L 5000 11/18/2115:06 129000 ug/L 25000 11/16/2110:26 977J ug/L 1000 11/13/21 21:26 2360 ug/L 1000 11/19/2108:05 203 ug/L 5.0 11/29/2117:47 0.66J ug/L 1.0 11/29/2117:47 3.7J ug/L 5.0 11/29/2117:47 96.3 ug/L 5.0 11/29/2117:47 2100 ug/L 50.0 11/29/2117:47 1220 ug/L 5.0 11/29/2117:47 13.9 ug/L 5.0 11/29/2117:47 92000 ug/L 5000 11/29/2117:47 9.3 ug/L 5.0 11/29/2117:47 14.7 ug/L 10.0 11/16/2107:19 6.7 ug/L 2.0 11/16/2100:58 585000 ug/L 5000 11/24/21 13:17 996000 ug/L 50000 11/17/2116:49 174000 ug/L 4000 11/16/2112:03 61500 ug/L 3000 11/19/21 08:21 56.3 ug/L 5.0 11/29/2117:50 7.1 ug/L 5.0 11/29/2117:50 196 ug/L 50.0 11/29/2117:50 13300 ug/L 5000 11/29/2117:50 5.5 ug/L 5.0 11/29/2117:50 32000 ug/L 5000 11 /23/21 13:27 M 1 165000 ug/L 25000 11/16/2110:26 8380 ug/L 1000 11/13/21 22:43 14100 ug/L 1000 11/19/2108:06 0.177 ug/L 0.0500 11/20/2100:45 192 ug/L 5.0 11/29/2117:55 0.82J ug/L 1.0 11/29/2117:55 87.9 ug/L 50.0 11/29/2117:55 207 ug/L 5.0 11/29/2117:55 18400 ug/L 5000 11/29/2117:55 9.8J ug/L 10.0 11/29/2117:55 0.69J ug/L 1.0 11/16/2107:55 0.92J ug/L 1.0 11/16/2107:55 0.83J ug/L 1.0 11/16/2107:55 3.OJ ug/L 5.0 11/16/2107:55 C9 68.8 ug/L 10.0 11/16/2107:55 4.4 ug/L 1.0 11/16/2107:55 0.74J ug/L 2.0 11/16/2107:55 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92572199 Lab Sample ID Method 92572199006 EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199007 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 7470A SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199008 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 8260D SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 SUMMARY OF DETECTION Client Sample ID Parameters Result Units Report Limit Analyzed MW-7 o-Xylene 0.48J ug/L 1.0 11/16/2107:55 1,4-Dioxane (p-Dioxane) 2.4 ug/L 2.0 11/16/21 01:36 Alkalinity, Total as CaCO3 85000 ug/L 5000 11/24/21 13:30 Total Dissolved Solids 207000 ug/L 25000 11/17/21 16:50 Sulfate 36800 ug/L 1000 11/13/2122:59 Chloride 10000 ug/L 1000 11/19/2108:07 MW-8 Barium 57.6 ug/L 5.0 11/29/2117:58 Chromium 4.9J ug/L 5.0 11/29/2117:58 Iron 60.9 ug/L 50.0 11/29/2117:58 Manganese 3.9J ug/L 5.0 11/29/2117:58 Sodium 11200 ug/L 5000 11/29/2117:58 Mercury 0.35 ug/L 0.20 11/25/2109:24 Alkalinity, Total as CaCO3 30000 ug/L 5000 11/24/21 13:35 Total Dissolved Solids 84000 ug/L 25000 11/17/21 16:50 Sulfate 8300 ug/L 1000 11/13/2123:14 Chloride 3800 ug/L 1000 11/19/2108:08 MW-9 Arsenic 5.1J ug/L 10.0 11/29/2118:08 Barium 181 ug/L 5.0 11/29/2118:08 Iron 167 ug/L 50.0 11/29/2118:08 Manganese 5.2 ug/L 5.0 11/29/2118:08 Sodium 18900 ug/L 5000 11/29/2118:08 Trichlorofluoromethane 0.38J ug/L 1.0 11/16/2108:31 Alkalinity, Total as CaCO3 33800 ug/L 5000 11/24/21 09:39 Total Dissolved Solids 145000 ug/L 25000 11/16/21 10:26 Sulfate 2140 ug/L 1000 11/13/2123:29 Chloride 3640 ug/L 1000 11/19/2108:10 92572199009 MW-10 EPA 601OD Antimony 6.2 ug/L 5.0 11/29/2118:12 EPA 601OD Barium 109 ug/L 5.0 11/29/2118:12 EPA 601OD Chromium 6.1 ug/L 5.0 11/29/2118:12 EPA 601OD Cobalt 4.6J ug/L 5.0 11/29/2118:12 EPA 601OD Copper 4AJ ug/L 5.0 11/29/2118:12 EPA 601OD Iron 3950 ug/L 50.0 11/29/2118:12 EPA 601OD Lead 5.3 ug/L 5.0 11/29/2118:12 EPA 601OD Manganese 26400 ug/L 50.0 11/30/2113:51 EPA 601OD Nickel 12.5 ug/L 5.0 11/29/2118:12 EPA 601OD Silver 9.6 ug/L 5.0 11/29/2118:12 EPA 601OD Sodium 92900 ug/L 5000 11/29/2118:12 EPA 601OD Vanadium 125 ug/L 5.0 11/29/2118:12 EPA 8260D Benzene 0.47J ug/L 1.0 11/16/2109:08 EPA 8260D Tetrahydrofuran 65.1 ug/L 10.0 11/16/2109:08 EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) 4.3 ug/L 2.0 11/16/21 02:33 SM 2320B-2011 Alkalinity, Total as CaCO3 734000 ug/L 5000 11/17/21 14:50 SM 2540C-2015 Total Dissolved Solids 1070000 ug/L 50000 11/15/21 17:12 REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92572199 Lab Sample ID Client Sample ID Method Parameters 92572199009 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199010 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199011 EPA 8151 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199012 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 MW-10 Sulfate Chloride MW-11 Barium Chromium Iron Manganese Nickel Sodium Vanadium Zinc Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride MW-12 2,4-D Barium Iron Manganese Nickel Sodium Vanadium Benzene 1,4-Dioxane (p-Dioxane) Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride M W-13 Barium Beryllium Copper Iron Manganese Nickel Sodium Zinc Tetrahydrofuran 1,4-Dioxane (p-Dioxane) Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride SUMMARY OF DETECTION Result Units Report Limit Analyzed Qualifiers 165000 ug/L 3000 11/16/2112:18 43900 ug/L 2000 11/19/2108:22 95.6 ug/L 5.0 11/29/2118:15 5.2 ug/L 5.0 11/29/2118:15 24600 ug/L 50.0 11/29/2118:15 1190 ug/L 5.0 11/29/2118:15 3.6J ug/L 5.0 11/29/2118:15 12300 ug/L 5000 11/29/2118:15 13.2 ug/L 5.0 11/29/2118:15 10.0 ug/L 10.0 11/29/2118:15 81300 ug/L 5000 11/17/21 14:59 176000 ug/L 25000 11/15/2117:12 11900 ug/L 1000 11/14/21 01:48 8460 ug/L 1000 11/19/2108:12 2.86 ug/L 2.00 11/16/2120:57 145 ug/L 5.0 11/29/2118:18 1020 ug/L 50.0 11/29/2118:18 3440 ug/L 5.0 11/29/2118:18 10.2 ug/L 5.0 11/29/2118:18 23300 ug/L 5000 11/29/2118:18 22.4 ug/L 5.0 11/29/2118:18 0.41J ug/L 1.0 11/13/2119:20 5.7 ug/L 2.0 11/16/2103:11 296000 ug/L 5000 11/17/2109:33 489000 ug/L 25000 11/14/2117:02 87600 ug/L 1000 11/14/21 02:04 22400 ug/L 1000 11/19/2108:13 514 ug/L 5.0 11/29/2118:21 1.4 ug/L 1.0 11/29/2118:21 4.3J ug/L 5.0 11/29/2118:21 238 ug/L 50.0 11/29/2118:21 155 ug/L 5.0 11/29/2118:21 11.3 ug/L 5.0 11/29/21 18:21 18300 ug/L 5000 11/29/2118:21 11.1 ug/L 10.0 11/29/2118:21 12.7 ug/L 10.0 11/13/2119:38 5.6 ug/L 2.0 11/16/2103:31 93800 ug/L 5000 11/16/2115:45 276000 ug/L 25000 11/14/2117:02 22300 ug/L 1000 11/14/2102:19 49800 ug/L 2000 11/24/21 11:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92572199 Lab Sample ID Method 92572199013 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 8260D EPA 8260D EPA 8260D SM 2320B-2011 SM 2540C-2015 SM 4500-CI-E-2011 SM 4500-CN-E-2016 92572199014 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 8260D SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199015 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 SUMMARY OF DETECTION Client Sample ID Parameters Result Units Report Limit Analyzed MW-14 Barium 272 ug/L 5.0 11/29/2118:25 Chromium 4.1J ug/L 5.0 11/29/2118:25 Iron 1780 ug/L 50.0 11/29/2118:25 Manganese 134 ug/L 5.0 11/29/2118:25 Nickel 9.6 ug/L 5.0 11/29/2118:25 Sodium 18800 ug/L 5000 11/29/2118:25 Vanadium 5.2 ug/L 5.0 11/29/2118:25 Zinc 11.3 ug/L 10.0 11/29/2118:25 Dichlorodifluoromethane 3.7 ug/L 1.0 11/16/2108:50 Tetrachloroethene 0.55J ug/L 1.0 11/16/2108:50 Trichlorofluoromethane 1.7 ug/L 1.0 11/16/2108:50 Alkalinity, Total as CaCO3 63000 ug/L 5000 11/24/21 10:18 Total Dissolved Solids 160000 ug/L 25000 11/16/21 10:26 Chloride 3650 ug/L 1000 11/24/2111:21 Cyanide 7.8J ug/L 8.0 11/16/2115:28 MW-15 Barium 16.1 ug/L 5.0 11/30/2100:13 Iron 166 ug/L 50.0 11/30/2100:13 Manganese 314 ug/L 5.0 11/30/2100:13 Sodium 15700 ug/L 5000 11/30/2100:13 Zinc 11.2 ug/L 10.0 11/30/2100:13 Tetrahydrofuran 4.8J ug/L 10.0 11/13/2119:56 Alkalinity, Total as CaCO3 104000 ug/L 5000 11/16/21 16:05 Total Dissolved Solids 247000 ug/L 25000 11/14/21 17:02 Sulfate 25500 ug/L 1000 11/14/2102:50 Chloride 37700 ug/L 5000 11/24/2111:22 SW-1 Arsenic 8.5J ug/L 10.0 11/30/2100:32 Barium 535 ug/L 5.0 11/30/2100:32 Beryllium 2.0 ug/L 1.0 11/30/2100:32 Cadmium 0.48J ug/L 1.0 11/30/2100:32 Chromium 24.8 ug/L 5.0 11/30/2100:32 Cobalt 13.0 ug/L 5.0 11/30/2100:32 Copper 13.8 ug/L 5.0 11/30/2100:32 Iron 69000 ug/L 50.0 11/30/2100:32 Lead 18.3 ug/L 5.0 11/30/2100:32 Manganese 1250 ug/L 5.0 11/30/2100:32 Nickel 12.2 ug/L 5.0 11/30/2100:32 Sodium 17900 ug/L 5000 11/30/2100:32 Vanadium 65.8 ug/L 5.0 11/30/2100:32 Zinc 70.2 ug/L 10.0 11/30/2100:32 Alkalinity, Total as CaCO3 71400 ug/L 5000 11/24/21 10:31 Total Dissolved Solids 199000 ug/L 25000 11/16/21 10:26 Sulfate 7440 ug/L 1000 11/14/2103:05 Chloride 24400 ug/L 1000 11/24/2111:23 REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL Pace Project No.: 92572199 Lab Sample ID Client Sample ID Method Parameters 92572199016 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199017 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 8260D EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199018 EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 601 OD EPA 8260D Mod. SM 2320B-2011 SM 2540C-2015 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 92572199020 EPA 8081 B SW-3 Barium Cobalt Iron Manganese Nickel Sodium Vanadium Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride SW-4 Barium Iron Manganese Nickel Sodium Vanadium Tetrahydrofuran 1,4-Dioxane (p-Dioxane) Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride SW-2 Arsenic Barium Iron Manganese Nickel Sodium Vanadium 1,4-Dioxane (p-Dioxane) Alkalinity, Total as CaCO3 Total Dissolved Solids Sulfate Chloride FB-1 Hexachlorobenzene SUMMARY OF DETECTION Result Units Report Limit Analyzed Qualifiers 278 ug/L 5.0 11/30/2100:36 4.5J ug/L 5.0 11/30/2100:36 26700 ug/L 50.0 11/30/2100:36 5640 ug/L 5.0 11/30/2100:36 7.4 ug/L 5.0 11/30/2100:36 26100 ug/L 5000 11/30/2100:36 35.3 ug/L 5.0 11/30/2100:36 379000 ug/L 5000 11/16/2116:13 477000 ug/L 25000 11/14/2117:02 21800 ug/L 1000 11/14/21 03:21 25100 ug/L 1000 11/24/2111:23 202 ug/L 5.0 11/30/2100:39 3110 ug/L 50.0 11/30/2100:39 6400 ug/L 5.0 11/30/2100:39 8.8 ug/L 5.0 11/30/2100:39 42400 ug/L 5000 11/30/2100:39 38.4 ug/L 5.0 11/30/2100:39 9.6J ug/L 10.0 11/16/2106:06 7.4 ug/L 2.0 11/15/2122:20 453000 ug/L 5000 11/17/2109:42 644000 ug/L 25000 11/14/2117:02 66700 ug/L 1000 11/14/2103:36 50000 ug/L 3000 11/24/21 11:39 8.3J ug/L 10.0 11/30/2100:42 92.5 ug/L 5.0 11/30/2100:42 1500 ug/L 50.0 11/30/2100:42 549 ug/L 5.0 11/30/2100:42 3.5J ug/L 5.0 11/30/2100:42 15300 ug/L 5000 11/30/2100:42 4.5J ug/L 5.0 11/30/2100:42 3.3 ug/L 2.0 11/15/2122:39 111000 ug/L 5000 11/17/2115:08 202000 ug/L 25000 11/15/2117:12 13900 ug/L 1000 11/14/2103:52 21900 ug/L 1000 11/24/2111:25 0.0305J ug/L 0.0500 11/16/2117:59 J REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MWAR Lab ID: 92572199001 Collected: 11/10/21 13:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/16/2116:56 11/17/2115:02 309-00-2 ND ug/L 0.0500 0.0172 1 11/16/2116:56 11/17/2115:02 319-84-6 LO ND ug/L 0.0500 0.0208 1 11/16/2116:56 11/17/2115:02 319-85-7 ND ug/L 0.0500 0.0150 1 11/16/2116:56 11/17/2115:02 319-86-8 LO ND ug/L 0.0500 0.0209 1 11/16/2116:56 11/17/2115:02 58-89-9 LO ND ug/L 5.00 0.0198 1 11/16/2116:56 11/17/2115:02 57-74-9 ND ug/L 0.0500 0.0177 1 11/16/2116:56 11/17/2115:02 72-54-8 LO ND ug/L 0.0500 0.0154 1 11/16/2116:56 11/17/2115:02 72-55-9 LO ND ug/L 0.0500 0.0198 1 11/16/2116:56 11/17/2115:02 50-29-3 LO ND ug/L 0.0500 0.0162 1 11/16/2116:56 11/17/2115:02 60-57-1 LO ND ug/L 0.0500 0.0160 1 11/16/2116:56 11/17/2115:02 959-98-8 LO ND ug/L 0.0500 0.0164 1 11/16/2116:56 11/17/2115:02 33213-65-9 LO ND ug/L 0.0500 0.0217 1 11/16/2116:56 11/17/2115:02 1031-07-8 LO ND ug/L 0.0500 0.0161 1 11/16/2116:56 11/17/2115:02 72-20-8 LO ND ug/L 0.0500 0.0237 1 11/16/2116:56 11/17/2115:02 7421-93-4 ND ug/L 0.0500 0.0219 1 11/16/2116:56 11/17/2115:02 53494-70-5 ND ug/L 0.0500 0.0176 1 11/16/2116:56 11/17/2115:02 118-74-1 ND ug/L 0.0500 0.0148 1 11/16/2116:56 11/17/2115:02 76-44-8 ND ug/L 0.0500 0.0183 1 11/16/2116:56 11/17/2115:02 1024-57-3 LO ND ug/L 0.0500 0.0193 1 11/16/2116:56 11/17/2115:02 72-43-5 LO ND ug/L 0.500 0.168 1 11/16/2116:56 11/17/2115:02 8001-35-2 159 % 10.0-128 1 11/16/2116:56 11/17/2115:02 2051-24-3 ST 75.6 % 10.0-127 1 11/16/2116:56 11/17/2115:02 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/16/2112:43 11/17/2118:44 94-75-7 R1 ND ug/L 2.00 0.344 1 11/16/2112:43 11/17/2118:44 127-20-8 L0,R1 ND ug/L 2.00 0.302 1 11/16/2112:43 11/17/2118:44 94-82-6 R1 ND ug/L 2.00 0.245 1 11/16/2112:43 11/17/2118:44 1918-00-9 R1 ND ug/L 2.00 1.04 1 11/16/2112:43 11/17/2118:44 15165-67-0 R1 ND ug/L 2.00 0.250 1 11/16/2112:43 11/17/2118:44 88-85-7 R1 ND ug/L 100 13.1 1 11/16/2112:43 11/17/2118:44 94-74-6 R1 ND ug/L 100 66.0 1 11/16/2112:43 11/17/2118:44 7085-19-0 R1 ND ug/L 2.00 0.258 1 11/16/2112:43 11/17/2118:44 93-76-5 ND ug/L 2.00 0.335 1 11/16/2112:43 11/17/2118:44 93-72-1 100 % 14.0-158 1 11/16/2112:43 11/17/2118:44 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.45 0.43 1 11/15/2107:08 11/16/2112:54 12674-11-2 ND ug/L 0.45 0.41 1 11/15/2107:08 11/16/2112:54 11104-28-2 ND ug/L 0.45 0.33 1 11/15/2107:08 11/16/2112:54 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MWAR Lab ID: 92572199001 Collected: 11/10/21 13:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.45 0.24 1 11/15/21 07:08 11/16/21 12:54 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.45 0.37 1 11/15/21 07:08 11/16/21 12:54 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.45 0.23 1 11/15/21 07:08 11/16/21 12:54 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.45 0.38 1 11/15/21 07:08 11/16/21 12:54 11096-82-5 Surrogates Decachlorobiphenyl (S) 165 % 10-181 1 11/15/21 07:08 11/16/21 12:54 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2117:37 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:37 7440-38-2 Barium 274 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:37 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/29/2117:37 7440-41-7 Cadmium 0.58J ug/L 1.0 0.40 1 11/16/2114:13 11/29/2117:37 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/29/2117:37 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/29/2117:37 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/29/2117:37 7440-50-8 Iron ND ug/L 50.0 41.5 1 11/16/2114:13 11/29/2117:37 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2117:37 7439-92-1 Manganese 28.7 ug/L 5.0 3.4 1 11/16/2114:13 11/29/2117:37 7439-96-5 Nickel ND ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:37 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:37 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/29/2117:37 7440-22-4 Sodium 15000 ug/L 5000 611 1 11/16/2114:13 11/29/2117:37 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/29/2117:37 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 11/16/2114:13 11/29/2117:37 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/29/2117:37 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury 3.1 ug/L 0.20 0.12 1 11/18/2116:15 11/25/2108:58 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 8.3 2.2 1 11/15/21 06:49 11/16/21 11:09 56-55-3 Chrysene ND ug/L 8.3 2.3 1 11/15/21 06:49 11/16/21 11:09 218-01-9 Dibenz(a,h)anthracene ND ug/L 8.3 2.5 1 11/15/21 06:49 11/16/21 11:09 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 3.1 1 11/15/21 06:49 11/16/21 11:09 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 8.3 2.4 1 11/15/21 06:49 11/16/21 11:09 193-39-5 Surrogates Nitrobenzene-d5 (S) 64 % 10-144 1 11/15/21 06:49 11/16/21 11:09 4165-60-0 2-Fluorobiphenyl (S) 51 % 10-130 1 11/15/21 06:49 11/16/21 11:09 321-60-8 Terphenyl-d14 (S) 62 % 34-163 1 11/15/21 06:49 11/16/21 11:09 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 19 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MWAR Lab ID: 92572199001 Collected: 11/10/21 13:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2106:42 67-64-1 ND ug/L 10.0 1.8 1 11/16/2106:42 107-13-1 ND ug/L 1.0 0.34 1 11/16/2106:42 71-43-2 ND ug/L 1.0 0.47 1 11/16/2106:42 74-97-5 ND ug/L 1.0 0.31 1 11/16/2106:42 75-27-4 ND ug/L 1.0 0.34 1 11/16/2106:42 75-25-2 ND ug/L 2.0 1.7 1 11/16/2106:42 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2106:42 78-93-3 ND ug/L 2.0 0.73 1 11/16/2106:42 75-15-0 ND ug/L 1.0 0.33 1 11/16/2106:42 56-23-5 ND ug/L 1.0 0.28 1 11/16/2106:42 108-90-7 ND ug/L 1.0 0.65 1 11/16/2106:42 75-00-3 ND ug/L 1.0 0.43 1 11/16/2106:42 67-66-3 ND ug/L 1.0 0.54 1 11/16/2106:42 74-87-3 ND ug/L 2.0 0.34 1 11/16/2106:42 96-12-8 ND ug/L 1.0 0.36 1 11/16/2106:42 124-48-1 ND ug/L 1.0 0.27 1 11/16/2106:42 106-93-4 ND ug/L 1.0 0.39 1 11/16/2106:42 74-95-3 ND ug/L 1.0 0.34 1 11/16/2106:42 95-50-1 ND ug/L 1.0 0.33 1 11/16/2106:42 106-46-7 ND ug/L 1.0 0.56 1 11/16/2106:42 110-57-6 ND ug/L 1.0 0.35 1 11/16/2106:42 75-71-8 ND ug/L 1.0 0.37 1 11/16/2106:42 75-34-3 ND ug/L 1.0 0.32 1 11/16/2106:42 107-06-2 ND ug/L 1.0 0.35 1 11/16/2106:42 75-35-4 0.801 ug/L 1.0 0.38 1 11/16/2106:42 156-59-2 ND ug/L 1.0 0.40 1 11/16/2106:42 156-60-5 ND ug/L 1.0 0.36 1 11/16/2106:42 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 06:42 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2106:42 10061-02-6 0.37J ug/L 1.0 0.30 1 11/16/2106:42 100-41-4 ND ug/L 5.0 0.48 1 11/16/2106:42 591-78-6 ND ug/L 20.0 9.7 1 11/16/2106:42 74-88-4 ND ug/L 5.0 2.0 1 11/16/2106:42 75-09-2 ND ug/L 5.0 2.7 1 11/16/2106:42 108-10-1 ND ug/L 1.0 0.29 1 11/16/2106:42 100-42-5 ND ug/L 1.0 0.31 1 11/16/2106:42 630-20-6 ND ug/L 1.0 0.22 1 11/16/2106:42 79-34-5 ND ug/L 1.0 0.29 1 11/16/2106:42 127-18-4 ND ug/L 10.0 3.5 1 11/16/2106:42 109-99-9 ND ug/L 1.0 0.48 1 11/16/2106:42 108-88-3 ND ug/L 1.0 0.33 1 11/16/2106:42 71-55-6 ND ug/L 1.0 0.32 1 11/16/2106:42 79-00-5 ND ug/L 1.0 0.38 1 11/16/2106:42 79-01-6 ND ug/L 1.0 0.30 1 11/16/2106:42 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 20 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MWAR Lab ID: 92572199001 Collected: 11/10/21 13:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 06:42 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 06:42 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 06:42 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 06:42 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 06:42 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 06:42 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 06:42 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 06:42 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 11/16/21 00:00 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 11/16/21 00:00 17060-07-0 Toluene-d8 (S) 92 % 66-133 1 11/16/21 00:00 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 88700 ug/L 5000 5000 1 11/18/21 14:57 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 152000 ug/L 25000 25000 1 11/16/21 10:21 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:29 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 503J ug/L 1000 500 1 11/13/2120:55 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 9750 ug/L 1000 500 1 11/19/2108:03 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:24 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 21 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-2R Lab ID: 92572199002 Collected: 11/08/21 14:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2100:25 309-00-2 ND ug/L 0.0500 0.0172 1 11/15/2106:10 11/16/2100:25 319-84-6 ND ug/L 0.0500 0.0208 1 11/15/2106:10 11/16/2100:25 319-85-7 ND ug/L 0.0500 0.0150 1 11/15/2106:10 11/16/2100:25 319-86-8 ND ug/L 0.0500 0.0209 1 11/15/2106:10 11/16/2100:25 58-89-9 ND ug/L 5.00 0.0198 1 11/15/2106:10 11/16/2100:25 57-74-9 ND ug/L 0.0500 0.0177 1 11/15/2106:10 11/16/2100:25 72-54-8 ND ug/L 0.0500 0.0154 1 11/15/2106:10 11/16/2100:25 72-55-9 ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2100:25 50-29-3 ND ug/L 0.0500 0.0162 1 11/15/2106:10 11/16/2100:25 60-57-1 ND ug/L 0.0500 0.0160 1 11/15/2106:10 11/16/2100:25 959-98-8 ND ug/L 0.0500 0.0164 1 11/15/2106:10 11/16/2100:25 33213-65-9 ND ug/L 0.0500 0.0217 1 11/15/2106:10 11/16/2100:25 1031-07-8 ND ug/L 0.0500 0.0161 1 11/15/2106:10 11/16/2100:25 72-20-8 ND ug/L 0.0500 0.0237 1 11/15/2106:10 11/16/2100:25 7421-93-4 ND ug/L 0.0500 0.0219 1 11/15/2106:10 11/16/2100:25 53494-70-5 ND ug/L 0.0500 0.0176 1 11/15/2106:10 11/16/2100:25 118-74-1 ND ug/L 0.0500 0.0148 1 11/15/2106:10 11/16/2100:25 76-44-8 ND ug/L 0.0500 0.0183 1 11/15/2106:10 11/16/2100:25 1024-57-3 ND ug/L 0.0500 0.0193 1 11/15/2106:10 11/16/2100:25 72-43-5 ND ug/L 0.500 0.168 1 11/15/2106:10 11/16/2100:25 8001-35-2 25.9 % 10.0-128 1 11/15/2106:10 11/16/2100:25 2051-24-3 50.5 % 10.0-127 1 11/15/2106:10 11/16/2100:25 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/15/2108:09 11/16/2120:44 94-75-7 ND ug/L 2.00 0.344 1 11/15/2108:09 11/16/2120:44 127-20-8 ND ug/L 2.00 0.302 1 11/15/2108:09 11/16/2120:44 94-82-6 ND ug/L 2.00 0.245 1 11/15/2108:09 11/16/2120:44 1918-00-9 ND ug/L 2.00 1.04 1 11/15/2108:09 11/16/2120:44 15165-67-0 ND ug/L 2.00 0.250 1 11/15/2108:09 11/16/2120:44 88-85-7 ND ug/L 100 13.1 1 11/15/2108:09 11/16/2120:44 94-74-6 ND ug/L 100 66.0 1 11/15/2108:09 11/16/2120:44 7085-19-0 ND ug/L 2.00 0.258 1 11/15/2108:09 11/16/2120:44 93-76-5 ND ug/L 2.00 0.335 1 11/15/2108:09 11/16/2120:44 93-72-1 128 % 14.0-158 1 11/15/2108:09 11/16/2120:44 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.42 0.39 1 11/15/2107:08 11/16/2113:06 12674-11-2 ND ug/L 0.42 0.38 1 11/15/2107:08 11/16/2113:06 11104-28-2 ND ug/L 0.42 0.30 1 11/15/2107:08 11/16/2113:06 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. LO Page 22 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-2R Lab ID: 92572199002 Collected: 11/08/21 14:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.42 0.22 1 11/15/21 07:08 11/16/21 13:06 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.42 0.34 1 11/15/21 07:08 11/16/21 13:06 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.42 0.21 1 11/15/21 07:08 11/16/21 13:06 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.42 0.35 1 11/15/21 07:08 11/16/21 13:06 11096-82-5 Surrogates Decachlorobiphenyl (S) 77 % 10-181 1 11/15/21 07:08 11/16/21 13:06 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2117:41 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:41 7440-38-2 Barium 397 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:41 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/29/2117:41 7440-41-7 Cadmium 0.44J ug/L 1.0 0.40 1 11/16/2114:13 11/29/2117:41 7440-43-9 Chromium 5.8 ug/L 5.0 3.7 1 11/16/2114:13 11/29/2117:41 7440-47-3 Cobalt 26.2 ug/L 5.0 3.6 1 11/16/2114:13 11/29/2117:41 7440-48-4 Copper 6.0 ug/L 5.0 4.3 1 11/16/2114:13 11/29/2117:41 7440-50-8 Iron 7700 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2117:41 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2117:41 7439-92-1 Manganese 20100 ug/L 50.0 34.3 10 11/16/2114:13 11/30/2113:47 7439-96-5 Nickel 17.7 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:41 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:41 7782-49-2 Silver 7.3 ug/L 5.0 2.5 1 11/16/2114:13 11/29/2117:41 7440-22-4 Sodium 59400 ug/L 5000 611 1 11/16/2114:13 11/29/2117:41 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/29/2117:41 7440-31-5 Vanadium 96.9 ug/L 5.0 3.9 1 11/16/2114:13 11/29/2117:41 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/29/2117:41 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:07 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 8.3 2.2 1 11/15/21 06:49 11/15/21 15:15 56-55-3 Chrysene ND ug/L 8.3 2.3 1 11/15/21 06:49 11/15/21 15:15 218-01-9 Dibenz(a,h)anthracene ND ug/L 8.3 2.5 1 11/15/21 06:49 11/15/21 15:15 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 3.1 1 11/15/21 06:49 11/15/21 15:15 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 8.3 2.4 1 11/15/21 06:49 11/15/21 15:15 193-39-5 Surrogates Nitrobenzene-d5 (S) 69 % 10-144 1 11/15/21 06:49 11/15/21 15:15 4165-60-0 2-Fluorobiphenyl (S) 52 % 10-130 1 11/15/21 06:49 11/15/21 15:15 321-60-8 Terphenyl-d14 (S) 69 % 34-163 1 11/15/21 06:49 11/15/21 15:15 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-2R Lab ID: 92572199002 Collected: 11/08/21 14:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/13/2119:03 67-64-1 ND ug/L 10.0 1.8 1 11/13/2119:03 107-13-1 3.7 ug/L 1.0 0.34 1 11/13/2119:03 71-43-2 ND ug/L 1.0 0.47 1 11/13/2119:03 74-97-5 ND ug/L 1.0 0.31 1 11/13/2119:03 75-27-4 ND ug/L 1.0 0.34 1 11/13/2119:03 75-25-2 ND ug/L 2.0 1.7 1 11/13/2119:03 74-83-9 ND ug/L 5.0 4.0 1 11/13/2119:03 78-93-3 ND ug/L 2.0 0.73 1 11/13/2119:03 75-15-0 ND ug/L 1.0 0.33 1 11/13/2119:03 56-23-5 ND ug/L 1.0 0.28 1 11/13/2119:03 108-90-7 4.3 ug/L 1.0 0.65 1 11/13/2119:03 75-00-3 ND ug/L 1.0 0.43 1 11/13/2119:03 67-66-3 ND ug/L 1.0 0.54 1 11/13/2119:03 74-87-3 ND ug/L 2.0 0.34 1 11/13/2119:03 96-12-8 ND ug/L 1.0 0.36 1 11/13/2119:03 124-48-1 ND ug/L 1.0 0.27 1 11/13/2119:03 106-93-4 ND ug/L 1.0 0.39 1 11/13/2119:03 74-95-3 ND ug/L 1.0 0.34 1 11/13/2119:03 95-50-1 0.67J ug/L 1.0 0.33 1 11/13/2119:03 106-46-7 ND ug/L 1.0 0.56 1 11/13/2119:03 110-57-6 0.74J ug/L 1.0 0.35 1 11/13/2119:03 75-71-8 ND ug/L 1.0 0.37 1 11/13/2119:03 75-34-3 ND ug/L 1.0 0.32 1 11/13/2119:03 107-06-2 ND ug/L 1.0 0.35 1 11/13/2119:03 75-35-4 1.3 ug/L 1.0 0.38 1 11/13/2119:03 156-59-2 ND ug/L 1.0 0.40 1 11/13/2119:03 156-60-5 ND ug/L 1.0 0.36 1 11/13/2119:03 78-87-5 ND ug/L 1.0 0.36 1 11 /13/21 19:03 10061-01-5 ND ug/L 1.0 0.36 1 11/13/2119:03 10061-02-6 ND ug/L 1.0 0.30 1 11/13/2119:03 100-41-4 ND ug/L 5.0 0.48 1 11/13/2119:03 591-78-6 9.91 ug/L 20.0 9.7 1 11/13/2119:03 74-88-4 2.2J ug/L 5.0 2.0 1 11/13/2119:03 75-09-2 ND ug/L 5.0 2.7 1 11/13/2119:03 108-10-1 ND ug/L 1.0 0.29 1 11/13/2119:03 100-42-5 ND ug/L 1.0 0.31 1 11/13/2119:03 630-20-6 ND ug/L 1.0 0.22 1 11/13/2119:03 79-34-5 ND ug/L 1.0 0.29 1 11/13/2119:03 127-18-4 19.5 ug/L 10.0 3.5 1 11/13/2119:03 109-99-9 ND ug/L 1.0 0.48 1 11/13/2119:03 108-88-3 ND ug/L 1.0 0.33 1 11/13/2119:03 71-55-6 ND ug/L 1.0 0.32 1 11/13/2119:03 79-00-5 1.0 ug/L 1.0 0.38 1 11/13/21 19:03 79-01-6 0.61J ug/L 1.0 0.30 1 11/13/2119:03 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 Page 24 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-2R Lab ID: 92572199002 Collected: 11/08/21 14:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/13/21 19:03 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/13/21 19:03 108-05-4 v1 Vinyl chloride 1.0 ug/L 1.0 0.39 1 11/13/21 19:03 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/13/21 19:03 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/13/21 19:03 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 11/13/21 19:03 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 11/13/21 19:03 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 11/13/21 19:03 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 4.1 ug/L 2.0 0.86 1 11/16/21 00:19 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 88 % 70-130 1 11/16/21 00:19 17060-07-0 Toluene-d8 (S) 85 % 66-133 1 11/16/21 00:19 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 782000 ug/L 5000 5000 1 11/16/21 15:06 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 920000 ug/L 50000 50000 1 11/14/21 17:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2102:58 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 42200 ug/L 1000 500 1 11/13/2121:11 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 46800 ug/L 2000 1000 2 11/19/2108:04 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/17/2113:31 11/18/2110:30 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 25 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-3R Lab ID: 92572199003 Collected: 11/11/21 16:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/17/2113:25 11/18/2115:00 309-00-2 ND ug/L 0.0500 0.0172 1 11/17/2113:25 11/18/2115:00 319-84-6 ND ug/L 0.0500 0.0208 1 11/17/2113:25 11/18/2115:00 319-85-7 ND ug/L 0.0500 0.0150 1 11/17/2113:25 11/18/2115:00 319-86-8 ND ug/L 0.0500 0.0209 1 11/17/2113:25 11/18/2115:00 58-89-9 ND ug/L 5.00 0.0198 1 11/17/2113:25 11/18/2115:00 57-74-9 ND ug/L 0.0500 0.0177 1 11/17/2113:25 11/18/2115:00 72-54-8 ND ug/L 0.0500 0.0154 1 11/17/2113:25 11/18/2115:00 72-55-9 ND ug/L 0.0500 0.0198 1 11/17/2113:25 11/18/2115:00 50-29-3 ND ug/L 0.0500 0.0162 1 11/17/2113:25 11/18/2115:00 60-57-1 ND ug/L 0.0500 0.0160 1 11/17/2113:25 11/18/2115:00 959-98-8 ND ug/L 0.0500 0.0164 1 11/17/2113:25 11/18/2115:00 33213-65-9 ND ug/L 0.0500 0.0217 1 11/17/2113:25 11/18/2115:00 1031-07-8 ND ug/L 0.0500 0.0161 1 11/17/2113:25 11/18/2115:00 72-20-8 ND ug/L 0.0500 0.0237 1 11/17/2113:25 11/18/2115:00 7421-93-4 ND ug/L 0.0500 0.0219 1 11/17/2113:25 11/18/2115:00 53494-70-5 ND ug/L 0.0500 0.0176 1 11/17/2113:25 11/18/2115:00 118-74-1 ND ug/L 0.0500 0.0148 1 11/17/2113:25 11/18/2115:00 76-44-8 ND ug/L 0.0500 0.0183 1 11/17/2113:25 11/18/2115:00 1024-57-3 ND ug/L 0.0500 0.0193 1 11/17/2113:25 11/18/2115:00 72-43-5 ND ug/L 0.500 0.168 1 11/17/2113:25 11/18/2115:00 8001-35-2 57.1 % 10.0-128 1 11/17/2113:25 11/18/2115:00 2051-24-3 85.7 % 10.0-127 1 11/17/2113:25 11/18/2115:00 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/17/2111:48 11/18/2123:05 94-75-7 ND ug/L 2.00 0.344 1 11/17/2111:48 11/18/2123:05 127-20-8 ND ug/L 2.00 0.302 1 11/17/2111:48 11/18/2123:05 94-82-6 ND ug/L 2.00 0.245 1 11/17/2111:48 11/18/2123:05 1918-00-9 ND ug/L 2.00 1.04 1 11/17/2111:48 11/18/2123:05 15165-67-0 ND ug/L 2.00 0.250 1 11/17/2111:48 11/18/2123:05 88-85-7 ND ug/L 100 13.1 1 11/17/2111:48 11/18/2123:05 94-74-6 ND ug/L 100 66.0 1 11/17/2111:48 11/18/2123:05 7085-19-0 ND ug/L 2.00 0.258 1 11/17/2111:48 11/18/2123:05 93-76-5 ND ug/L 2.00 0.335 1 11/17/2111:48 11/18/2123:05 93-72-1 87.3 % 14.0-158 1 11/17/2111:48 11/18/2123:05 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.45 0.43 1 11/15/2107:08 11/16/2113:17 12674-11-2 ND ug/L 0.45 0.41 1 11/15/2107:08 11/16/2113:17 11104-28-2 ND ug/L 0.45 0.33 1 11/15/2107:08 11/16/2113:17 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 26 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-3R Lab ID: 92572199003 Collected: 11/11/21 16:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.45 0.24 1 11/15/21 07:08 11/16/21 13:17 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.45 0.37 1 11/15/21 07:08 11/16/21 13:17 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.45 0.23 1 11/15/21 07:08 11/16/21 13:17 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.45 0.38 1 11/15/21 07:08 11/16/21 13:17 11096-82-5 Surrogates Decachlorobiphenyl (S) 131 % 10-181 1 11/15/21 07:08 11/16/21 13:17 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2117:44 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:44 7440-38-2 Barium 259 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:44 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/29/2117:44 7440-41-7 Cadmium 0.46J ug/L 1.0 0.40 1 11/16/2114:13 11/29/2117:44 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/29/2117:44 7440-47-3 Cobalt 10.1 ug/L 5.0 3.6 1 11/16/2114:13 11/29/2117:44 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/29/2117:44 7440-50-8 Iron 72900 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2117:44 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2117:44 7439-92-1 Manganese 4140 ug/L 5.0 3.4 1 11/16/2114:13 11/29/2117:44 7439-96-5 Nickel ND ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:44 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:44 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/29/2117:44 7440-22-4 Sodium 2010J ug/L 5000 611 1 11/16/2114:13 11/29/2117:44 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/29/2117:44 7440-31-5 Vanadium 25.8 ug/L 5.0 3.9 1 11/16/2114:13 11/29/2117:44 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/29/2117:44 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:10 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 8.3 2.2 1 11/15/21 06:49 11/16/21 12:50 56-55-3 Chrysene ND ug/L 8.3 2.3 1 11/15/21 06:49 11/16/21 12:50 218-01-9 Dibenz(a,h)anthracene ND ug/L 8.3 2.5 1 11/15/21 06:49 11/16/21 12:50 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 3.1 1 11/15/21 06:49 11/16/21 12:50 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 8.3 2.4 1 11/15/21 06:49 11/16/21 12:50 193-39-5 Surrogates Nitrobenzene-d5 (S) 74 % 10-144 1 11/15/21 06:49 11/16/21 12:50 4165-60-0 2-Fluorobiphenyl (S) 62 % 10-130 1 11/15/21 06:49 11/16/21 12:50 321-60-8 Terphenyl-d14 (S) 68 % 34-163 1 11/15/21 06:49 11/16/21 12:50 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 27 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-3R Lab ID: 92572199003 Collected: 11/11/21 16:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2107:01 67-64-1 ND ug/L 10.0 1.8 1 11/16/2107:01 107-13-1 ND ug/L 1.0 0.34 1 11/16/2107:01 71-43-2 ND ug/L 1.0 0.47 1 11/16/2107:01 74-97-5 ND ug/L 1.0 0.31 1 11/16/2107:01 75-27-4 ND ug/L 1.0 0.34 1 11/16/2107:01 75-25-2 ND ug/L 2.0 1.7 1 11/16/2107:01 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2107:01 78-93-3 ND ug/L 2.0 0.73 1 11/16/2107:01 75-15-0 ND ug/L 1.0 0.33 1 11/16/2107:01 56-23-5 ND ug/L 1.0 0.28 1 11/16/2107:01 108-90-7 ND ug/L 1.0 0.65 1 11/16/2107:01 75-00-3 ND ug/L 1.0 0.43 1 11/16/2107:01 67-66-3 ND ug/L 1.0 0.54 1 11/16/2107:01 74-87-3 ND ug/L 2.0 0.34 1 11/16/2107:01 96-12-8 ND ug/L 1.0 0.36 1 11/16/2107:01 124-48-1 ND ug/L 1.0 0.27 1 11/16/2107:01 106-93-4 ND ug/L 1.0 0.39 1 11/16/2107:01 74-95-3 ND ug/L 1.0 0.34 1 11/16/2107:01 95-50-1 ND ug/L 1.0 0.33 1 11/16/2107:01 106-46-7 ND ug/L 1.0 0.56 1 11/16/2107:01 110-57-6 ND ug/L 1.0 0.35 1 11/16/2107:01 75-71-8 ND ug/L 1.0 0.37 1 11/16/2107:01 75-34-3 ND ug/L 1.0 0.32 1 11/16/2107:01 107-06-2 ND ug/L 1.0 0.35 1 11/16/2107:01 75-35-4 ND ug/L 1.0 0.38 1 11/16/2107:01 156-59-2 ND ug/L 1.0 0.40 1 11/16/2107:01 156-60-5 ND ug/L 1.0 0.36 1 11/16/2107:01 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 07:01 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2107:01 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2107:01 100-41-4 ND ug/L 5.0 0.48 1 11/16/2107:01 591-78-6 ND ug/L 20.0 9.7 1 11/16/2107:01 74-88-4 ND ug/L 5.0 2.0 1 11/16/2107:01 75-09-2 ND ug/L 5.0 2.7 1 11/16/2107:01 108-10-1 ND ug/L 1.0 0.29 1 11/16/2107:01 100-42-5 ND ug/L 1.0 0.31 1 11/16/2107:01 630-20-6 ND ug/L 1.0 0.22 1 11/16/2107:01 79-34-5 ND ug/L 1.0 0.29 1 11/16/2107:01 127-18-4 ND ug/L 10.0 3.5 1 11/16/2107:01 109-99-9 ND ug/L 1.0 0.48 1 11/16/2107:01 108-88-3 ND ug/L 1.0 0.33 1 11/16/2107:01 71-55-6 ND ug/L 1.0 0.32 1 11/16/2107:01 79-00-5 ND ug/L 1.0 0.38 1 11/16/2107:01 79-01-6 ND ug/L 1.0 0.30 1 11/16/2107:01 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 28 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-3R Lab ID: 92572199003 Collected: 11/11/21 16:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 07:01 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 07:01 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 07:01 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 07:01 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 07:01 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 07:01 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 11/16/21 07:01 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 07:01 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 11/16/21 00:39 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 11/16/21 00:39 17060-07-0 Toluene-d8 (S) 89 % 66-133 1 11/16/21 00:39 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 63100 ug/L 5000 5000 1 11/18/21 15:06 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 129000 ug/L 25000 25000 1 11/16/21 10:26 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:38 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 977J ug/L 1000 500 1 11/13/2121:26 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 2360 ug/L 1000 500 1 11/19/2108:05 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:25 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 29 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-4R Lab ID: 92572199004 Collected: 11/12/21 11:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/19/2108:13 11/20/2100:36 309-00-2 ND ug/L 0.0500 0.0172 1 11/19/2108:13 11/20/2100:36 319-84-6 ND ug/L 0.0500 0.0208 1 11/19/2108:13 11/20/2100:36 319-85-7 ND ug/L 0.0500 0.0150 1 11/19/2108:13 11/20/2100:36 319-86-8 ND ug/L 0.0500 0.0209 1 11/19/2108:13 11/20/2100:36 58-89-9 ND ug/L 5.00 0.0198 1 11/19/2108:13 11/20/2100:36 57-74-9 ND ug/L 0.0500 0.0177 1 11/19/2108:13 11/20/2100:36 72-54-8 ND ug/L 0.0500 0.0154 1 11/19/2108:13 11/20/2100:36 72-55-9 ND ug/L 0.0500 0.0198 1 11/19/2108:13 11/20/2100:36 50-29-3 ND ug/L 0.0500 0.0162 1 11/19/2108:13 11/20/2100:36 60-57-1 ND ug/L 0.0500 0.0160 1 11/19/2108:13 11/20/2100:36 959-98-8 ND ug/L 0.0500 0.0164 1 11/19/2108:13 11/20/2100:36 33213-65-9 ND ug/L 0.0500 0.0217 1 11 /19/21 08:13 11 /20/21 00:36 1031-07-8 ND ug/L 0.0500 0.0161 1 11/19/2108:13 11/20/2100:36 72-20-8 ND ug/L 0.0500 0.0237 1 11/19/2108:13 11/20/2100:36 7421-93-4 ND ug/L 0.0500 0.0219 1 11/19/2108:13 11/20/2100:36 53494-70-5 ND ug/L 0.0500 0.0176 1 11/19/2108:13 11/20/2100:36 118-74-1 ND ug/L 0.0500 0.0148 1 11/19/2108:13 11/20/2100:36 76-44-8 ND ug/L 0.0500 0.0183 1 11/19/2108:13 11/20/2100:36 1024-57-3 ND ug/L 0.0500 0.0193 1 11/19/2108:13 11/20/2100:36 72-43-5 ND ug/L 0.500 0.168 1 11 /19/21 08:13 11 /20/21 00:36 8001-35-2 75.9 % 10.0-128 1 11 /19/21 08:13 11 /20/21 00:36 2051-24-3 69.6 % 10.0-127 1 11/19/2108:13 11/20/2100:36 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/17/2119:44 11/19/2102:26 94-75-7 LO ND ug/L 2.00 0.344 1 11/17/2119:44 11/19/2102:26 127-20-8 LO ND ug/L 2.00 0.302 1 11/17/2119:44 11/19/2102:26 94-82-6 ND ug/L 2.00 0.245 1 11/17/2119:44 11/19/2102:26 1918-00-9 ND ug/L 2.00 1.04 1 11/17/2119:44 11/19/2102:26 15165-67-0 ND ug/L 2.00 0.250 1 11/17/2119:44 11/19/2102:26 88-85-7 ND ug/L 100 13.1 1 11/17/2119:44 11/19/2102:26 94-74-6 ND ug/L 100 66.0 1 11/17/2119:44 11/19/2102:26 7085-19-0 ND ug/L 2.00 0.258 1 11/17/2119:44 11/19/2102:26 93-76-5 ND ug/L 2.00 0.335 1 11/17/2119:44 11/19/2102:26 93-72-1 163 % 14.0-158 1 11/17/2119:44 11/19/2102:26 19719-28-9 ST Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.45 0.43 1 11/15/2107:08 11/16/2113:52 12674-11-2 ND ug/L 0.45 0.41 1 11/15/2107:08 11/16/2113:52 11104-28-2 ND ug/L 0.45 0.33 1 11/15/2107:08 11/16/2113:52 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 30 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-4R Lab ID: 92572199004 Collected: 11/12/21 11:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.45 0.24 1 11/15/21 07:08 11/16/21 13:52 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.45 0.37 1 11/15/21 07:08 11/16/21 13:52 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.45 0.23 1 11/15/21 07:08 11/16/21 13:52 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.45 0.38 1 11/15/21 07:08 11/16/21 13:52 11096-82-5 Surrogates Decachlorobiphenyl (S) 88 % 10-181 1 11/15/21 07:08 11/16/21 13:52 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2117:47 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:47 7440-38-2 Barium 203 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:47 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/29/2117:47 7440-41-7 Cadmium 0.66J ug/L 1.0 0.40 1 11/16/2114:13 11/29/2117:47 7440-43-9 Chromium 3.7J ug/L 5.0 3.7 1 11/16/2114:13 11/29/2117:47 7440-47-3 Cobalt 96.3 ug/L 5.0 3.6 1 11/16/2114:13 11/29/2117:47 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/29/2117:47 7440-50-8 Iron 2100 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2117:47 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2117:47 7439-92-1 Manganese 1220 ug/L 5.0 3.4 1 11/16/2114:13 11/29/2117:47 7439-96-5 Nickel 13.9 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:47 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:47 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/29/2117:47 7440-22-4 Sodium 92000 ug/L 5000 611 1 11/16/2114:13 11/29/2117:47 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/29/2117:47 7440-31-5 Vanadium 9.3 ug/L 5.0 3.9 1 11/16/2114:13 11/29/2117:47 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/29/2117:47 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:12 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 10.0 2.7 1 11/15/21 06:49 11/16/21 18:51 56-55-3 Chrysene ND ug/L 10.0 2.8 1 11/15/21 06:49 11/16/21 18:51 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 3.0 1 11/15/21 06:49 11/16/21 18:51 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 3.7 1 11/15/21 06:49 11/16/21 18:51 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.9 1 11/15/21 06:49 11/16/21 18:51 193-39-5 Surrogates Nitrobenzene-d5 (S) 61 % 10-144 1 11/15/21 06:49 11/16/21 18:51 4165-60-0 2-Fluorobiphenyl (S) 56 % 10-130 1 11/15/21 06:49 11/16/21 18:51 321-60-8 Terphenyl-d14 (S) 64 % 34-163 1 11/15/21 06:49 11/16/21 18:51 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 31 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-4R Lab ID: 92572199004 Collected: 11/12/21 11:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2107:19 67-64-1 ND ug/L 10.0 1.8 1 11/16/2107:19 107-13-1 ND ug/L 1.0 0.34 1 11/16/2107:19 71-43-2 ND ug/L 1.0 0.47 1 11/16/2107:19 74-97-5 ND ug/L 1.0 0.31 1 11/16/2107:19 75-27-4 ND ug/L 1.0 0.34 1 11/16/2107:19 75-25-2 ND ug/L 2.0 1.7 1 11/16/2107:19 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2107:19 78-93-3 ND ug/L 2.0 0.73 1 11/16/2107:19 75-15-0 ND ug/L 1.0 0.33 1 11/16/2107:19 56-23-5 ND ug/L 1.0 0.28 1 11/16/2107:19 108-90-7 ND ug/L 1.0 0.65 1 11/16/2107:19 75-00-3 ND ug/L 1.0 0.43 1 11/16/2107:19 67-66-3 ND ug/L 1.0 0.54 1 11/16/2107:19 74-87-3 ND ug/L 2.0 0.34 1 11/16/2107:19 96-12-8 ND ug/L 1.0 0.36 1 11/16/2107:19 124-48-1 ND ug/L 1.0 0.27 1 11/16/2107:19 106-93-4 ND ug/L 1.0 0.39 1 11/16/2107:19 74-95-3 ND ug/L 1.0 0.34 1 11/16/2107:19 95-50-1 ND ug/L 1.0 0.33 1 11/16/2107:19 106-46-7 ND ug/L 1.0 0.56 1 11/16/2107:19 110-57-6 ND ug/L 1.0 0.35 1 11/16/2107:19 75-71-8 ND ug/L 1.0 0.37 1 11/16/2107:19 75-34-3 ND ug/L 1.0 0.32 1 11/16/2107:19 107-06-2 ND ug/L 1.0 0.35 1 11/16/2107:19 75-35-4 ND ug/L 1.0 0.38 1 11/16/2107:19 156-59-2 ND ug/L 1.0 0.40 1 11/16/2107:19 156-60-5 ND ug/L 1.0 0.36 1 11/16/2107:19 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 07:19 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2107:19 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2107:19 100-41-4 ND ug/L 5.0 0.48 1 11/16/2107:19 591-78-6 ND ug/L 20.0 9.7 1 11/16/2107:19 74-88-4 ND ug/L 5.0 2.0 1 11/16/2107:19 75-09-2 ND ug/L 5.0 2.7 1 11/16/2107:19 108-10-1 ND ug/L 1.0 0.29 1 11/16/2107:19 100-42-5 ND ug/L 1.0 0.31 1 11/16/2107:19 630-20-6 ND ug/L 1.0 0.22 1 11/16/2107:19 79-34-5 ND ug/L 1.0 0.29 1 11/16/2107:19 127-18-4 14.7 ug/L 10.0 3.5 1 11/16/2107:19 109-99-9 ND ug/L 1.0 0.48 1 11/16/2107:19 108-88-3 ND ug/L 1.0 0.33 1 11/16/2107:19 71-55-6 ND ug/L 1.0 0.32 1 11/16/2107:19 79-00-5 ND ug/L 1.0 0.38 1 11/16/2107:19 79-01-6 ND ug/L 1.0 0.30 1 11/16/2107:19 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 32 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-4R Lab ID: 92572199004 Collected: 11/12/21 11:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 07:19 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 07:19 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 07:19 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 07:19 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 07:19 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 07:19 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 07:19 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 07:19 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 6.7 ug/L 2.0 0.86 1 11/16/21 00:58 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 11/16/21 00:58 17060-07-0 Toluene-d8 (S) 89 % 66-133 1 11/16/21 00:58 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 585000 ug/L 5000 5000 1 11/24/21 13:17 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 996000 ug/L 50000 50000 1 11/17/21 16:49 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/18/2105:16 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 174000 ug/L 4000 2000 4 11/16/2112:03 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 61500 ug/L 3000 1500 3 11/19/2108:21 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:36 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 33 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-5R Lab ID: 92572199005 Collected: 11/11/21 18:05 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/17/2113:25 11/18/2115:09 309-00-2 ND ug/L 0.0500 0.0172 1 11/17/2113:25 11/18/2115:09 319-84-6 ND ug/L 0.0500 0.0208 1 11/17/2113:25 11/18/2115:09 319-85-7 ND ug/L 0.0500 0.0150 1 11/17/2113:25 11/18/2115:09 319-86-8 ND ug/L 0.0500 0.0209 1 11/17/2113:25 11/18/2115:09 58-89-9 ND ug/L 5.00 0.0198 1 11/17/2113:25 11/18/2115:09 57-74-9 ND ug/L 0.0500 0.0177 1 11/17/2113:25 11/18/2115:09 72-54-8 ND ug/L 0.0500 0.0154 1 11/17/2113:25 11/18/2115:09 72-55-9 ND ug/L 0.0500 0.0198 1 11/17/2113:25 11/18/2115:09 50-29-3 ND ug/L 0.0500 0.0162 1 11/17/2113:25 11/18/2115:09 60-57-1 ND ug/L 0.0500 0.0160 1 11/17/2113:25 11/18/2115:09 959-98-8 ND ug/L 0.0500 0.0164 1 11/17/2113:25 11/18/2115:09 33213-65-9 ND ug/L 0.0500 0.0217 1 11/17/2113:25 11/18/2115:09 1031-07-8 ND ug/L 0.0500 0.0161 1 11/17/2113:25 11/18/2115:09 72-20-8 ND ug/L 0.0500 0.0237 1 11/17/2113:25 11/18/2115:09 7421-93-4 ND ug/L 0.0500 0.0219 1 11/17/2113:25 11/18/2115:09 53494-70-5 ND ug/L 0.0500 0.0176 1 11/17/2113:25 11/18/2115:09 118-74-1 ND ug/L 0.0500 0.0148 1 11/17/2113:25 11/18/2115:09 76-44-8 ND ug/L 0.0500 0.0183 1 11/17/2113:25 11/18/2115:09 1024-57-3 ND ug/L 0.0500 0.0193 1 11/17/2113:25 11/18/2115:09 72-43-5 ND ug/L 0.500 0.168 1 11/17/2113:25 11/18/2115:09 8001-35-2 60.1 % 10.0-128 1 11/17/2113:25 11/18/2115:09 2051-24-3 85.5 % 10.0-127 1 11/17/2113:25 11/18/2115:09 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/17/2111:48 11/18/2123:20 94-75-7 ND ug/L 2.00 0.344 1 11/17/2111:48 11/18/2123:20 127-20-8 ND ug/L 2.00 0.302 1 11/17/2111:48 11/18/2123:20 94-82-6 ND ug/L 2.00 0.245 1 11/17/2111:48 11/18/2123:20 1918-00-9 ND ug/L 2.00 1.04 1 11/17/2111:48 11/18/2123:20 15165-67-0 ND ug/L 2.00 0.250 1 11/17/2111:48 11/18/2123:20 88-85-7 ND ug/L 100 13.1 1 11/17/2111:48 11/18/2123:20 94-74-6 ND ug/L 100 66.0 1 11/17/2111:48 11/18/2123:20 7085-19-0 ND ug/L 2.00 0.258 1 11/17/2111:48 11/18/2123:20 93-76-5 ND ug/L 2.00 0.335 1 11/17/2111:48 11/18/2123:20 93-72-1 99.2 % 14.0-158 1 11/17/2111:48 11/18/2123:20 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.42 0.39 1 11/15/2107:08 11/16/2114:04 12674-11-2 ND ug/L 0.42 0.38 1 11/15/2107:08 11/16/2114:04 11104-28-2 ND ug/L 0.42 0.30 1 11/15/2107:08 11/16/2114:04 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 34 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-5R Lab ID: 92572199005 Collected: 11/11/21 18:05 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.42 0.22 1 11/15/21 07:08 11/16/21 14:04 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.42 0.34 1 11/15/21 07:08 11/16/21 14:04 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.42 0.21 1 11/15/21 07:08 11/16/21 14:04 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.42 0.35 1 11/15/21 07:08 11/16/21 14:04 11096-82-5 Surrogates Decachlorobiphenyl (S) 153 % 10-181 1 11/15/21 07:08 11/16/21 14:04 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2117:50 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:50 7440-38-2 Barium 56.3 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:50 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/29/2117:50 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/29/2117:50 7440-43-9 Chromium 7.1 ug/L 5.0 3.7 1 11/16/2114:13 11/29/2117:50 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/29/2117:50 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/29/2117:50 7440-50-8 Iron 196 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2117:50 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2117:50 7439-92-1 Manganese ND ug/L 5.0 3.4 1 11/16/2114:13 11/29/2117:50 7439-96-5 Nickel ND ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:50 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:50 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/29/2117:50 7440-22-4 Sodium 13300 ug/L 5000 611 1 11/16/2114:13 11/29/2117:50 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/29/2117:50 7440-31-5 Vanadium 5.5 ug/L 5.0 3.9 1 11/16/2114:13 11/29/2117:50 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/29/2117:50 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:15 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 9.1 2.4 1 11/15/21 06:49 11/16/21 13:15 56-55-3 Chrysene ND ug/L 9.1 2.5 1 11/15/21 06:49 11/16/21 13:15 218-01-9 Dibenz(a,h)anthracene ND ug/L 9.1 2.7 1 11/15/21 06:49 11/16/21 13:15 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.5 3.4 1 11/15/21 06:49 11/16/21 13:15 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 9.1 2.6 1 11/15/21 06:49 11/16/21 13:15 193-39-5 Surrogates Nitrobenzene-d5 (S) 63 % 10-144 1 11/15/21 06:49 11/16/21 13:15 4165-60-0 2-Fluorobiphenyl (S) 54 % 10-130 1 11/15/21 06:49 11/16/21 13:15 321-60-8 Terphenyl-d14 (S) 64 % 34-163 1 11/15/21 06:49 11/16/21 13:15 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 35 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-5R Lab ID: 92572199005 Collected: 11/11/21 18:05 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2107:37 67-64-1 ND ug/L 10.0 1.8 1 11/16/2107:37 107-13-1 ND ug/L 1.0 0.34 1 11/16/2107:37 71-43-2 ND ug/L 1.0 0.47 1 11/16/2107:37 74-97-5 ND ug/L 1.0 0.31 1 11/16/2107:37 75-27-4 ND ug/L 1.0 0.34 1 11/16/2107:37 75-25-2 ND ug/L 2.0 1.7 1 11/16/2107:37 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2107:37 78-93-3 ND ug/L 2.0 0.73 1 11/16/2107:37 75-15-0 ND ug/L 1.0 0.33 1 11/16/2107:37 56-23-5 ND ug/L 1.0 0.28 1 11/16/2107:37 108-90-7 ND ug/L 1.0 0.65 1 11/16/2107:37 75-00-3 ND ug/L 1.0 0.43 1 11/16/2107:37 67-66-3 ND ug/L 1.0 0.54 1 11/16/2107:37 74-87-3 ND ug/L 2.0 0.34 1 11/16/2107:37 96-12-8 ND ug/L 1.0 0.36 1 11/16/2107:37 124-48-1 ND ug/L 1.0 0.27 1 11/16/2107:37 106-93-4 ND ug/L 1.0 0.39 1 11/16/2107:37 74-95-3 ND ug/L 1.0 0.34 1 11/16/2107:37 95-50-1 ND ug/L 1.0 0.33 1 11/16/2107:37 106-46-7 ND ug/L 1.0 0.56 1 11/16/2107:37 110-57-6 ND ug/L 1.0 0.35 1 11/16/2107:37 75-71-8 ND ug/L 1.0 0.37 1 11/16/2107:37 75-34-3 ND ug/L 1.0 0.32 1 11/16/2107:37 107-06-2 ND ug/L 1.0 0.35 1 11/16/2107:37 75-35-4 ND ug/L 1.0 0.38 1 11/16/2107:37 156-59-2 ND ug/L 1.0 0.40 1 11/16/2107:37 156-60-5 ND ug/L 1.0 0.36 1 11/16/2107:37 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 07:37 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2107:37 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2107:37 100-41-4 ND ug/L 5.0 0.48 1 11/16/2107:37 591-78-6 ND ug/L 20.0 9.7 1 11/16/2107:37 74-88-4 ND ug/L 5.0 2.0 1 11/16/2107:37 75-09-2 ND ug/L 5.0 2.7 1 11/16/2107:37 108-10-1 ND ug/L 1.0 0.29 1 11/16/2107:37 100-42-5 ND ug/L 1.0 0.31 1 11/16/2107:37 630-20-6 ND ug/L 1.0 0.22 1 11/16/2107:37 79-34-5 ND ug/L 1.0 0.29 1 11/16/2107:37 127-18-4 ND ug/L 10.0 3.5 1 11/16/2107:37 109-99-9 ND ug/L 1.0 0.48 1 11/16/2107:37 108-88-3 ND ug/L 1.0 0.33 1 11/16/2107:37 71-55-6 ND ug/L 1.0 0.32 1 11/16/2107:37 79-00-5 ND ug/L 1.0 0.38 1 11/16/2107:37 79-01-6 ND ug/L 1.0 0.30 1 11/16/2107:37 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 36 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-5R Lab ID: 92572199005 Collected: 11/11/21 18:05 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 07:37 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 07:37 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 07:37 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 07:37 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 07:37 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 07:37 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 07:37 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 07:37 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 11/16/21 01:17 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 11/16/21 01:17 17060-07-0 Toluene-d8 (S) 91 % 66-133 1 11/16/21 01:17 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 32000 ug/L 5000 5000 1 11/23/21 13:27 M1 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 165000 ug/L 25000 25000 1 11/16/21 10:26 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:38 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 8380 ug/L 1000 500 1 11/13/2122:43 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 14100 ug/L 1000 500 1 11/19/2108:06 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:26 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 37 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-7 Lab ID: 92572199006 Collected: 11/12/21 10:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/19/2108:13 11/20/2100:45 309-00-2 ND ug/L 0.0500 0.0172 1 11/19/2108:13 11/20/2100:45 319-84-6 ND ug/L 0.0500 0.0208 1 11/19/2108:13 11/20/2100:45 319-85-7 ND ug/L 0.0500 0.0150 1 11/19/2108:13 11/20/2100:45 319-86-8 ND ug/L 0.0500 0.0209 1 11/19/2108:13 11/20/2100:45 58-89-9 ND ug/L 5.00 0.0198 1 11/19/2108:13 11/20/2100:45 57-74-9 ND ug/L 0.0500 0.0177 1 11/19/2108:13 11/20/2100:45 72-54-8 0.177 ug/L 0.0500 0.0154 1 11/19/2108:13 11/20/2100:45 72-55-9 ND ug/L 0.0500 0.0198 1 11/19/2108:13 11/20/2100:45 50-29-3 ND ug/L 0.0500 0.0162 1 11/19/2108:13 11/20/2100:45 60-57-1 ND ug/L 0.0500 0.0160 1 11/19/2108:13 11/20/2100:45 959-98-8 ND ug/L 0.0500 0.0164 1 11/19/2108:13 11/20/2100:45 33213-65-9 ND ug/L 0.0500 0.0217 1 11 /19/21 08:13 11 /20/21 00:45 1031-07-8 ND ug/L 0.0500 0.0161 1 11/19/2108:13 11/20/2100:45 72-20-8 ND ug/L 0.0500 0.0237 1 11/19/2108:13 11/20/2100:45 7421-93-4 ND ug/L 0.0500 0.0219 1 11/19/2108:13 11/20/2100:45 53494-70-5 ND ug/L 0.0500 0.0176 1 11/19/2108:13 11/20/2100:45 118-74-1 ND ug/L 0.0500 0.0148 1 11/19/2108:13 11/20/2100:45 76-44-8 ND ug/L 0.0500 0.0183 1 11/19/2108:13 11/20/2100:45 1024-57-3 ND ug/L 0.0500 0.0193 1 11/19/2108:13 11/20/2100:45 72-43-5 ND ug/L 0.500 0.168 1 11 /19/21 08:13 11 /20/21 00:45 8001-35-2 122 % 10.0-128 1 11 /19/21 08:13 11 /20/21 00:45 2051-24-3 107 % 10.0-127 1 11/19/2108:13 11/20/2100:45 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/17/2119:44 11/19/2102:42 94-75-7 LO ND ug/L 2.00 0.344 1 11/17/2119:44 11/19/2102:42 127-20-8 LO ND ug/L 2.00 0.302 1 11/17/2119:44 11/19/2102:42 94-82-6 ND ug/L 2.00 0.245 1 11/17/2119:44 11/19/2102:42 1918-00-9 ND ug/L 2.00 1.04 1 11/17/2119:44 11/19/2102:42 15165-67-0 ND ug/L 2.00 0.250 1 11/17/2119:44 11/19/2102:42 88-85-7 ND ug/L 100 13.1 1 11/17/2119:44 11/19/2102:42 94-74-6 ND ug/L 100 66.0 1 11/17/2119:44 11/19/2102:42 7085-19-0 ND ug/L 2.00 0.258 1 11/17/2119:44 11/19/2102:42 93-76-5 ND ug/L 2.00 0.335 1 11/17/2119:44 11/19/2102:42 93-72-1 182 % 14.0-158 1 11/17/2119:44 11/19/2102:42 19719-28-9 ST Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.42 0.39 1 11/15/2107:08 11/16/2114:16 12674-11-2 ND ug/L 0.42 0.38 1 11/15/2107:08 11/16/2114:16 11104-28-2 ND ug/L 0.42 0.30 1 11/15/2107:08 11/16/2114:16 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 38 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-7 Lab ID: 92572199006 Collected: 11/12/21 10:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.42 0.22 1 11/15/21 07:08 11/16/21 14:16 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.42 0.34 1 11/15/21 07:08 11/16/21 14:16 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.42 0.21 1 11/15/21 07:08 11/16/21 14:16 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.42 0.35 1 11/15/21 07:08 11/16/21 14:16 11096-82-5 Surrogates Decachlorobiphenyl (S) 64 % 10-181 1 11/15/21 07:08 11/16/21 14:16 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2117:55 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:55 7440-38-2 Barium 192 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:55 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/29/2117:55 7440-41-7 Cadmium 0.82J ug/L 1.0 0.40 1 11/16/2114:13 11/29/2117:55 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/29/2117:55 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/29/2117:55 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/29/2117:55 7440-50-8 Iron 87.9 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2117:55 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2117:55 7439-92-1 Manganese 207 ug/L 5.0 3.4 1 11/16/2114:13 11/29/2117:55 7439-96-5 Nickel ND ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:55 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:55 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/29/2117:55 7440-22-4 Sodium 18400 ug/L 5000 611 1 11/16/2114:13 11/29/2117:55 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/29/2117:55 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 11/16/2114:13 11/29/2117:55 7440-62-2 Zinc 9.8J ug/L 10.0 9.5 1 11/16/2114:13 11/29/2117:55 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:17 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 9.1 2.4 1 11/15/21 06:49 11/16/21 19:17 56-55-3 Chrysene ND ug/L 9.1 2.5 1 11/15/21 06:49 11/16/21 19:17 218-01-9 Dibenz(a,h)anthracene ND ug/L 9.1 2.7 1 11/15/21 06:49 11/16/21 19:17 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.5 3.4 1 11/15/21 06:49 11/16/21 19:17 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 9.1 2.6 1 11/15/21 06:49 11/16/21 19:17 193-39-5 Surrogates Nitrobenzene-d5 (S) 70 % 10-144 1 11/15/21 06:49 11/16/21 19:17 4165-60-0 2-Fluorobiphenyl (S) 67 % 10-130 1 11/15/21 06:49 11/16/21 19:17 321-60-8 Terphenyl-d14 (S) 71 % 34-163 1 11/15/21 06:49 11/16/21 19:17 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 39 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-7 Lab ID: 92572199006 Collected: 11/12/21 10:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2107:55 67-64-1 ND ug/L 10.0 1.8 1 11/16/2107:55 107-13-1 0.69J ug/L 1.0 0.34 1 11/16/2107:55 71-43-2 ND ug/L 1.0 0.47 1 11/16/2107:55 74-97-5 ND ug/L 1.0 0.31 1 11/16/2107:55 75-27-4 ND ug/L 1.0 0.34 1 11/16/2107:55 75-25-2 ND ug/L 2.0 1.7 1 11/16/2107:55 74-83-9 ND ug/L 5.0 4.0 1 11/16/2107:55 78-93-3 ND ug/L 2.0 0.73 1 11/16/2107:55 75-15-0 ND ug/L 1.0 0.33 1 11/16/2107:55 56-23-5 ND ug/L 1.0 0.28 1 11/16/2107:55 108-90-7 ND ug/L 1.0 0.65 1 11/16/2107:55 75-00-3 ND ug/L 1.0 0.43 1 11/16/2107:55 67-66-3 ND ug/L 1.0 0.54 1 11/16/2107:55 74-87-3 ND ug/L 2.0 0.34 1 11/16/2107:55 96-12-8 ND ug/L 1.0 0.36 1 11/16/2107:55 124-48-1 ND ug/L 1.0 0.27 1 11/16/2107:55 106-93-4 ND ug/L 1.0 0.39 1 11/16/2107:55 74-95-3 ND ug/L 1.0 0.34 1 11/16/2107:55 95-50-1 ND ug/L 1.0 0.33 1 11/16/2107:55 106-46-7 ND ug/L 1.0 0.56 1 11/16/2107:55 110-57-6 ND ug/L 1.0 0.35 1 11/16/2107:55 75-71-8 0.92J ug/L 1.0 0.37 1 11/16/2107:55 75-34-3 ND ug/L 1.0 0.32 1 11/16/2107:55 107-06-2 ND ug/L 1.0 0.35 1 11/16/2107:55 75-35-4 0.83J ug/L 1.0 0.38 1 11/16/2107:55 156-59-2 ND ug/L 1.0 0.40 1 11/16/2107:55 156-60-5 ND ug/L 1.0 0.36 1 11/16/2107:55 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 07:55 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2107:55 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2107:55 100-41-4 ND ug/L 5.0 0.48 1 11/16/2107:55 591-78-6 ND ug/L 20.0 9.7 1 11/16/2107:55 74-88-4 3.0.1 ug/L 5.0 2.0 1 11/16/2107:55 75-09-2 ND ug/L 5.0 2.7 1 11/16/2107:55 108-10-1 ND ug/L 1.0 0.29 1 11/16/2107:55 100-42-5 ND ug/L 1.0 0.31 1 11/16/2107:55 630-20-6 ND ug/L 1.0 0.22 1 11/16/2107:55 79-34-5 ND ug/L 1.0 0.29 1 11/16/2107:55 127-18-4 68.8 ug/L 10.0 3.5 1 11/16/2107:55 109-99-9 ND ug/L 1.0 0.48 1 11/16/2107:55 108-88-3 ND ug/L 1.0 0.33 1 11/16/2107:55 71-55-6 ND ug/L 1.0 0.32 1 11/16/2107:55 79-00-5 ND ug/L 1.0 0.38 1 11/16/2107:55 79-01-6 4.4 ug/L 1.0 0.30 1 11/16/2107:55 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 C9 Page 40 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-7 Lab ID: 92572199006 Collected: 11/12/21 10:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 07:55 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 07:55 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 07:55 75-01-4 m&p-Xylene 0.74J ug/L 2.0 0.71 1 11/16/21 07:55 179601-23-1 o-Xylene 0.48.1 ug/L 1.0 0.34 1 11/16/21 07:55 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 11/16/21 07:55 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 07:55 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 07:55 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 2.4 ug/L 2.0 0.86 1 11/16/21 01:36 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 01:36 17060-07-0 Toluene-d8 (S) 88 % 66-133 1 11/16/21 01:36 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 85000 ug/L 5000 5000 1 11/24/21 13:30 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 207000 ug/L 25000 25000 1 11/17/21 16:50 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/18/2105:17 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 36800 ug/L 1000 500 1 11/13/2122:59 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 10000 ug/L 1000 500 1 11/19/2108:07 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:37 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 41 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-8 Lab ID: 92572199007 Collected: 11/12/21 08:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/19/2108:13 11/20/2100:55 309-00-2 ND ug/L 0.0500 0.0172 1 11/19/2108:13 11/20/2100:55 319-84-6 ND ug/L 0.0500 0.0208 1 11/19/2108:13 11/20/2100:55 319-85-7 ND ug/L 0.0500 0.0150 1 11/19/2108:13 11/20/2100:55 319-86-8 ND ug/L 0.0500 0.0209 1 11/19/2108:13 11/20/2100:55 58-89-9 ND ug/L 5.00 0.0198 1 11/19/2108:13 11/20/2100:55 57-74-9 ND ug/L 0.0500 0.0177 1 11/19/2108:13 11/20/2100:55 72-54-8 ND ug/L 0.0500 0.0154 1 11/19/2108:13 11/20/2100:55 72-55-9 ND ug/L 0.0500 0.0198 1 11/19/2108:13 11/20/2100:55 50-29-3 ND ug/L 0.0500 0.0162 1 11/19/2108:13 11/20/2100:55 60-57-1 ND ug/L 0.0500 0.0160 1 11/19/2108:13 11/20/2100:55 959-98-8 ND ug/L 0.0500 0.0164 1 11/19/2108:13 11/20/2100:55 33213-65-9 ND ug/L 0.0500 0.0217 1 11 /19/21 08:13 11 /20/21 00:55 1031-07-8 ND ug/L 0.0500 0.0161 1 11/19/2108:13 11/20/2100:55 72-20-8 ND ug/L 0.0500 0.0237 1 11/19/2108:13 11/20/2100:55 7421-93-4 ND ug/L 0.0500 0.0219 1 11/19/2108:13 11/20/2100:55 53494-70-5 ND ug/L 0.0500 0.0176 1 11/19/2108:13 11/20/2100:55 118-74-1 ND ug/L 0.0500 0.0148 1 11/19/2108:13 11/20/2100:55 76-44-8 ND ug/L 0.0500 0.0183 1 11/19/2108:13 11/20/2100:55 1024-57-3 ND ug/L 0.0500 0.0193 1 11/19/2108:13 11/20/2100:55 72-43-5 ND ug/L 0.500 0.168 1 11 /19/21 08:13 11 /20/21 00:55 8001-35-2 37.9 % 10.0-128 1 11 /19/21 08:13 11 /20/21 00:55 2051-24-3 75.4 % 10.0-127 1 11/19/2108:13 11/20/2100:55 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/17/2119:44 11/19/2103:13 94-75-7 ND ug/L 2.00 0.344 1 11/17/2119:44 11/19/2103:13 127-20-8 ND ug/L 2.00 0.302 1 11/17/2119:44 11/19/2103:13 94-82-6 ND ug/L 2.00 0.245 1 11/17/2119:44 11/19/2103:13 1918-00-9 ND ug/L 2.00 1.04 1 11/17/2119:44 11/19/2103:13 15165-67-0 ND ug/L 2.00 0.250 1 11/17/2119:44 11/19/2103:13 88-85-7 ND ug/L 100 13.1 1 11/17/2119:44 11/19/2103:13 94-74-6 ND ug/L 100 66.0 1 11/17/2119:44 11/19/2103:13 7085-19-0 ND ug/L 2.00 0.258 1 11/17/2119:44 11/19/2103:13 93-76-5 ND ug/L 2.00 0.335 1 11/17/2119:44 11/19/2103:13 93-72-1 99.0 % 14.0-158 1 11/17/2119:44 11/19/2103:13 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.50 0.47 1 11/15/2107:08 11/16/2114:27 12674-11-2 ND ug/L 0.50 0.45 1 11/15/2107:08 11/16/2114:27 11104-28-2 ND ug/L 0.50 0.36 1 11/15/2107:08 11/16/2114:27 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. LO LO Page 42 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-8 Lab ID: 92572199007 Collected: 11/12/21 08:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.50 0.26 1 11/15/21 07:08 11/16/21 14:27 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 0.40 1 11/15/21 07:08 11/16/21 14:27 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.50 0.25 1 11/15/21 07:08 11/16/21 14:27 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 0.42 1 11/15/21 07:08 11/16/21 14:27 11096-82-5 Surrogates Decachlorobiphenyl (S) 153 % 10-181 1 11/15/21 07:08 11/16/21 14:27 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2117:58 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:58 7440-38-2 Barium 57.6 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:58 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/29/2117:58 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/29/2117:58 7440-43-9 Chromium 4.9J ug/L 5.0 3.7 1 11/16/2114:13 11/29/2117:58 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/29/2117:58 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/29/2117:58 7440-50-8 Iron 60.9 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2117:58 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2117:58 7439-92-1 Manganese 3.9J ug/L 5.0 3.4 1 11/16/2114:13 11/29/2117:58 7439-96-5 Nickel ND ug/L 5.0 3.5 1 11/16/2114:13 11/29/2117:58 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2117:58 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/29/2117:58 7440-22-4 Sodium 11200 ug/L 5000 611 1 11/16/2114:13 11/29/2117:58 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/29/2117:58 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 11/16/2114:13 11/29/2117:58 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/29/2117:58 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury 0.35 ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:24 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 10.0 2.7 1 11/15/21 06:49 11/16/21 19:42 56-55-3 Chrysene ND ug/L 10.0 2.8 1 11/15/21 06:49 11/16/21 19:42 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 3.0 1 11/15/21 06:49 11/16/21 19:42 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 3.7 1 11/15/21 06:49 11/16/21 19:42 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 2.9 1 11/15/21 06:49 11/16/21 19:42 193-39-5 Surrogates Nitrobenzene-d5 (S) 71 % 10-144 1 11/15/21 06:49 11/16/21 19:42 4165-60-0 2-Fluorobiphenyl (S) 66 % 10-130 1 11/15/21 06:49 11/16/21 19:42 321-60-8 Terphenyl-d14 (S) 77 % 34-163 1 11/15/21 06:49 11/16/21 19:42 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 43 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-8 Lab ID: 92572199007 Collected: 11/12/21 08:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2108:13 67-64-1 ND ug/L 10.0 1.8 1 11/16/2108:13 107-13-1 ND ug/L 1.0 0.34 1 11/16/2108:13 71-43-2 ND ug/L 1.0 0.47 1 11/16/2108:13 74-97-5 ND ug/L 1.0 0.31 1 11/16/2108:13 75-27-4 ND ug/L 1.0 0.34 1 11/16/2108:13 75-25-2 ND ug/L 2.0 1.7 1 11/16/2108:13 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2108:13 78-93-3 ND ug/L 2.0 0.73 1 11/16/2108:13 75-15-0 ND ug/L 1.0 0.33 1 11/16/2108:13 56-23-5 ND ug/L 1.0 0.28 1 11/16/2108:13 108-90-7 ND ug/L 1.0 0.65 1 11/16/2108:13 75-00-3 ND ug/L 1.0 0.43 1 11/16/2108:13 67-66-3 ND ug/L 1.0 0.54 1 11/16/2108:13 74-87-3 ND ug/L 2.0 0.34 1 11/16/2108:13 96-12-8 ND ug/L 1.0 0.36 1 11/16/2108:13 124-48-1 ND ug/L 1.0 0.27 1 11/16/2108:13 106-93-4 ND ug/L 1.0 0.39 1 11/16/2108:13 74-95-3 ND ug/L 1.0 0.34 1 11/16/2108:13 95-50-1 ND ug/L 1.0 0.33 1 11/16/2108:13 106-46-7 ND ug/L 1.0 0.56 1 11/16/2108:13 110-57-6 ND ug/L 1.0 0.35 1 11/16/2108:13 75-71-8 ND ug/L 1.0 0.37 1 11/16/2108:13 75-34-3 ND ug/L 1.0 0.32 1 11/16/2108:13 107-06-2 ND ug/L 1.0 0.35 1 11/16/2108:13 75-35-4 ND ug/L 1.0 0.38 1 11/16/2108:13 156-59-2 ND ug/L 1.0 0.40 1 11/16/2108:13 156-60-5 ND ug/L 1.0 0.36 1 11/16/2108:13 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 08:13 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2108:13 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2108:13 100-41-4 ND ug/L 5.0 0.48 1 11/16/2108:13 591-78-6 ND ug/L 20.0 9.7 1 11/16/2108:13 74-88-4 ND ug/L 5.0 2.0 1 11/16/2108:13 75-09-2 ND ug/L 5.0 2.7 1 11/16/2108:13 108-10-1 ND ug/L 1.0 0.29 1 11/16/2108:13 100-42-5 ND ug/L 1.0 0.31 1 11/16/2108:13 630-20-6 ND ug/L 1.0 0.22 1 11/16/2108:13 79-34-5 ND ug/L 1.0 0.29 1 11/16/2108:13 127-18-4 ND ug/L 10.0 3.5 1 11/16/2108:13 109-99-9 ND ug/L 1.0 0.48 1 11/16/2108:13 108-88-3 ND ug/L 1.0 0.33 1 11/16/2108:13 71-55-6 ND ug/L 1.0 0.32 1 11/16/2108:13 79-00-5 ND ug/L 1.0 0.38 1 11/16/2108:13 79-01-6 ND ug/L 1.0 0.30 1 11/16/2108:13 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 44 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-8 Lab ID: 92572199007 Collected: 11/12/21 08:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 08:13 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 08:13 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 08:13 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 08:13 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 08:13 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 11/16/21 08:13 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 11/16/21 08:13 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 11/16/21 08:13 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 11/16/21 01:55 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 11/16/21 01:55 17060-07-0 Toluene-d8 (S) 91 % 66-133 1 11/16/21 01:55 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 30000 ug/L 5000 5000 1 11/24/21 13:35 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 84000 ug/L 25000 25000 1 11/17/21 16:50 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/18/2105:17 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 8300 ug/L 1000 500 1 11/13/2123:14 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 3800 ug/L 1000 500 1 11/19/2108:08 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:38 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 45 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-9 Lab ID: 92572199008 Collected: 11/11/21 14:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/18/2114:40 11/19/2108:05 309-00-2 ND ug/L 0.0500 0.0172 1 11/18/2114:40 11/19/2108:05 319-84-6 ND ug/L 0.0500 0.0208 1 11/18/2114:40 11/19/2108:05 319-85-7 ND ug/L 0.0500 0.0150 1 11/18/2114:40 11/19/2108:05 319-86-8 ND ug/L 0.0500 0.0209 1 11/18/2114:40 11/19/2108:05 58-89-9 ND ug/L 5.00 0.0198 1 11/18/2114:40 11/19/2108:05 57-74-9 ND ug/L 0.0500 0.0177 1 11/18/2114:40 11/19/2108:05 72-54-8 ND ug/L 0.0500 0.0154 1 11/18/2114:40 11/19/2108:05 72-55-9 ND ug/L 0.0500 0.0198 1 11/18/2114:40 11/19/2108:05 50-29-3 ND ug/L 0.0500 0.0162 1 11/18/2114:40 11/19/2108:05 60-57-1 ND ug/L 0.0500 0.0160 1 11/18/2114:40 11/19/2108:05 959-98-8 ND ug/L 0.0500 0.0164 1 11/18/2114:40 11/19/2108:05 33213-65-9 ND ug/L 0.0500 0.0217 1 11/18/2114:40 11/19/2108:05 1031-07-8 ND ug/L 0.0500 0.0161 1 11/18/2114:40 11/19/2108:05 72-20-8 ND ug/L 0.0500 0.0237 1 11/18/2114:40 11/19/2108:05 7421-93-4 ND ug/L 0.0500 0.0219 1 11/18/2114:40 11/19/2108:05 53494-70-5 ND ug/L 0.0500 0.0176 1 11/18/2114:40 11/19/2108:05 118-74-1 ND ug/L 0.0500 0.0148 1 11/18/2114:40 11/19/2108:05 76-44-8 ND ug/L 0.0500 0.0183 1 11/18/2114:40 11/19/2108:05 1024-57-3 ND ug/L 0.0500 0.0193 1 11/18/2114:40 11/19/2108:05 72-43-5 ND ug/L 0.500 0.168 1 11/18/2114:40 11/19/2108:05 8001-35-2 92.1 % 10.0-128 1 11/18/2114:40 11/19/2108:05 2051-24-3 92.9 % 10.0-127 1 11/18/2114:40 11/19/2108:05 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/17/2111:48 11/18/2123:36 94-75-7 ND ug/L 2.00 0.344 1 11/17/2111:48 11/18/2123:36 127-20-8 ND ug/L 2.00 0.302 1 11/17/2111:48 11/18/2123:36 94-82-6 ND ug/L 2.00 0.245 1 11/17/2111:48 11/18/2123:36 1918-00-9 ND ug/L 2.00 1.04 1 11/17/2111:48 11/18/2123:36 15165-67-0 ND ug/L 2.00 0.250 1 11/17/2111:48 11/18/2123:36 88-85-7 ND ug/L 100 13.1 1 11/17/2111:48 11/18/2123:36 94-74-6 ND ug/L 100 66.0 1 11/17/2111:48 11/18/2123:36 7085-19-0 ND ug/L 2.00 0.258 1 11/17/2111:48 11/18/2123:36 93-76-5 ND ug/L 2.00 0.335 1 11/17/2111:48 11/18/2123:36 93-72-1 92.2 % 14.0-158 1 11/17/2111:48 11/18/2123:36 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.42 0.39 1 11/15/2107:08 11/16/2114:39 12674-11-2 ND ug/L 0.42 0.38 1 11/15/2107:08 11/16/2114:39 11104-28-2 ND ug/L 0.42 0.30 1 11/15/2107:08 11/16/2114:39 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 46 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-9 Lab ID: 92572199008 Collected: 11/11/21 14:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.42 0.22 1 11/15/21 07:08 11/16/21 14:39 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.42 0.34 1 11/15/21 07:08 11/16/21 14:39 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.42 0.21 1 11/15/21 07:08 11/16/21 14:39 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.42 0.35 1 11/15/21 07:08 11/16/21 14:39 11096-82-5 Surrogates Decachlorobiphenyl (S) 85 % 10-181 1 11/15/21 07:08 11/16/21 14:39 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2118:08 7440-36-0 Arsenic 5.11 ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:08 7440-38-2 Barium 181 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:08 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/29/2118:08 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/29/2118:08 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/29/2118:08 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/29/2118:08 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/29/2118:08 7440-50-8 Iron 167 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2118:08 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2118:08 7439-92-1 Manganese 5.2 ug/L 5.0 3.4 1 11/16/2114:13 11/29/2118:08 7439-96-5 Nickel ND ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:08 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:08 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/29/2118:08 7440-22-4 Sodium 18900 ug/L 5000 611 1 11/16/2114:13 11/29/2118:08 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/29/2118:08 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 11/16/2114:13 11/29/2118:08 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/29/2118:08 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:26 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 8.3 2.2 1 11/15/21 06:49 11/16/21 15:28 56-55-3 Chrysene ND ug/L 8.3 2.3 1 11/15/21 06:49 11/16/21 15:28 218-01-9 Dibenz(a,h)anthracene ND ug/L 8.3 2.5 1 11/15/21 06:49 11/16/21 15:28 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 3.1 1 11/15/21 06:49 11/16/21 15:28 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 8.3 2.4 1 11/15/21 06:49 11/16/21 15:28 193-39-5 Surrogates Nitrobenzene-d5 (S) 60 % 10-144 1 11/15/21 06:49 11/16/21 15:28 4165-60-0 2-Fluorobiphenyl (S) 54 % 10-130 1 11/15/21 06:49 11/16/21 15:28 321-60-8 Terphenyl-d14 (S) 63 % 34-163 1 11/15/21 06:49 11/16/21 15:28 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 47 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-9 Lab ID: 92572199008 Collected: 11/11/21 14:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2108:31 67-64-1 ND ug/L 10.0 1.8 1 11/16/2108:31 107-13-1 ND ug/L 1.0 0.34 1 11/16/2108:31 71-43-2 ND ug/L 1.0 0.47 1 11/16/2108:31 74-97-5 ND ug/L 1.0 0.31 1 11/16/2108:31 75-27-4 ND ug/L 1.0 0.34 1 11/16/2108:31 75-25-2 ND ug/L 2.0 1.7 1 11/16/2108:31 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2108:31 78-93-3 ND ug/L 2.0 0.73 1 11/16/2108:31 75-15-0 ND ug/L 1.0 0.33 1 11/16/2108:31 56-23-5 ND ug/L 1.0 0.28 1 11/16/2108:31 108-90-7 ND ug/L 1.0 0.65 1 11/16/2108:31 75-00-3 ND ug/L 1.0 0.43 1 11/16/2108:31 67-66-3 ND ug/L 1.0 0.54 1 11/16/2108:31 74-87-3 ND ug/L 2.0 0.34 1 11/16/2108:31 96-12-8 ND ug/L 1.0 0.36 1 11/16/2108:31 124-48-1 ND ug/L 1.0 0.27 1 11/16/2108:31 106-93-4 ND ug/L 1.0 0.39 1 11/16/2108:31 74-95-3 ND ug/L 1.0 0.34 1 11/16/2108:31 95-50-1 ND ug/L 1.0 0.33 1 11/16/2108:31 106-46-7 ND ug/L 1.0 0.56 1 11/16/2108:31 110-57-6 ND ug/L 1.0 0.35 1 11/16/2108:31 75-71-8 ND ug/L 1.0 0.37 1 11/16/2108:31 75-34-3 ND ug/L 1.0 0.32 1 11/16/2108:31 107-06-2 ND ug/L 1.0 0.35 1 11/16/2108:31 75-35-4 ND ug/L 1.0 0.38 1 11/16/2108:31 156-59-2 ND ug/L 1.0 0.40 1 11/16/2108:31 156-60-5 ND ug/L 1.0 0.36 1 11/16/2108:31 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 08:31 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2108:31 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2108:31 100-41-4 ND ug/L 5.0 0.48 1 11/16/2108:31 591-78-6 ND ug/L 20.0 9.7 1 11/16/2108:31 74-88-4 ND ug/L 5.0 2.0 1 11/16/2108:31 75-09-2 ND ug/L 5.0 2.7 1 11/16/2108:31 108-10-1 ND ug/L 1.0 0.29 1 11/16/2108:31 100-42-5 ND ug/L 1.0 0.31 1 11/16/2108:31 630-20-6 ND ug/L 1.0 0.22 1 11/16/2108:31 79-34-5 ND ug/L 1.0 0.29 1 11/16/2108:31 127-18-4 ND ug/L 10.0 3.5 1 11/16/2108:31 109-99-9 ND ug/L 1.0 0.48 1 11/16/2108:31 108-88-3 ND ug/L 1.0 0.33 1 11/16/2108:31 71-55-6 ND ug/L 1.0 0.32 1 11/16/2108:31 79-00-5 ND ug/L 1.0 0.38 1 11/16/2108:31 79-01-6 0.38J ug/L 1.0 0.30 1 11/16/2108:31 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 48 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-9 Lab ID: 92572199008 Collected: 11/11/21 14:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 08:31 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 08:31 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 08:31 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 08:31 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 08:31 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 08:31 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 11/16/21 08:31 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 11/16/21 08:31 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 11/16/21 02:14 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 02:14 17060-07-0 Toluene-d8 (S) 89 % 66-133 1 11/16/21 02:14 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 33800 ug/L 5000 5000 1 11/24/21 09:39 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 145000 ug/L 25000 25000 1 11/16/21 10:26 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:39 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 2140 ug/L 1000 500 1 11/13/2123:29 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 3640 ug/L 1000 500 1 11/19/2108:10 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:27 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 49 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-10 Lab ID: 92572199009 Collected: 11/09/21 12:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/16/2111:40 11/18/2113:52 309-00-2 ND ug/L 0.0500 0.0172 1 11/16/2111:40 11/18/2113:52 319-84-6 ND ug/L 0.0500 0.0208 1 11/16/2111:40 11/18/2113:52 319-85-7 ND ug/L 0.0500 0.0150 1 11/16/2111:40 11/18/2113:52 319-86-8 ND ug/L 0.0500 0.0209 1 11/16/2111:40 11/18/2113:52 58-89-9 ND ug/L 5.00 0.0198 1 11/16/2111:40 11/18/2113:52 57-74-9 ND ug/L 0.0500 0.0177 1 11/16/2111:40 11/18/2113:52 72-54-8 ND ug/L 0.0500 0.0154 1 11/16/2111:40 11/18/2113:52 72-55-9 ND ug/L 0.0500 0.0198 1 11/16/2111:40 11/18/2113:52 50-29-3 ND ug/L 0.0500 0.0162 1 11/16/2111:40 11/18/2113:52 60-57-1 ND ug/L 0.0500 0.0160 1 11/16/2111:40 11/18/2113:52 959-98-8 ND ug/L 0.0500 0.0164 1 11/16/2111:40 11/18/2113:52 33213-65-9 ND ug/L 0.0500 0.0217 1 11/16/2111:40 11/18/2113:52 1031-07-8 ND ug/L 0.0500 0.0161 1 11/16/2111:40 11/18/2113:52 72-20-8 ND ug/L 0.0500 0.0237 1 11/16/2111:40 11/18/2113:52 7421-93-4 ND ug/L 0.0500 0.0219 1 11/16/2111:40 11/18/2113:52 53494-70-5 ND ug/L 0.0500 0.0176 1 11/16/2111:40 11/18/2113:52 118-74-1 ND ug/L 0.0500 0.0148 1 11/16/2111:40 11/18/2113:52 76-44-8 ND ug/L 0.0500 0.0183 1 11/16/2111:40 11/18/2113:52 1024-57-3 ND ug/L 0.0500 0.0193 1 11/16/2111:40 11/18/2113:52 72-43-5 ND ug/L 0.500 0.168 1 11/16/2111:40 11/18/2113:52 8001-35-2 67.1 % 10.0-128 1 11/16/2111:40 11/18/2113:52 2051-24-3 87.9 % 10.0-127 1 11/16/2111:40 11/18/2113:52 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/15/2117:01 11/17/2100:30 94-75-7 LO ND ug/L 2.00 0.344 1 11/15/2117:01 11/17/2100:30 127-20-8 LO ND ug/L 2.00 0.302 1 11/15/2117:01 11/17/2100:30 94-82-6 LO ND ug/L 2.00 0.245 1 11/15/2117:01 11/17/2100:30 1918-00-9 LO ND ug/L 2.00 1.04 1 11/15/2117:01 11/17/2100:30 15165-67-0 LO ND ug/L 2.00 0.250 1 11/15/2117:01 11/19/2102:50 88-85-7 ND ug/L 100 13.1 1 11/15/2117:01 11/17/2100:30 94-74-6 ND ug/L 100 66.0 1 11/15/2117:01 11/17/2100:30 7085-19-0 ND ug/L 2.00 0.258 1 11/15/2117:01 11/17/2100:30 93-76-5 LO ND ug/L 2.00 0.335 1 11/15/2117:01 11/17/2100:30 93-72-1 LO 114 % 14.0-158 1 11/15/2117:01 11/17/2100:30 19719-28-9 238 % 14.0-158 1 11/15/2117:01 11/19/2102:50 19719-28-9 ST Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.42 0.39 1 11/15/2107:08 11/16/2114:50 12674-11-2 ND ug/L 0.42 0.38 1 11/15/2107:08 11/16/2114:50 11104-28-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 50 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-10 Lab ID: 92572199009 Collected: 11/09/21 12:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Sodium Tin Vanadium Zinc 7470 Mercury Mercury 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate I ndeno(1,2,3-cd )pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.42 0.30 1 11/15/2107:08 11/16/2114:50 11141-16-5 ND ug/L 0.42 0.22 1 11/15/2107:08 11/16/2114:50 53469-21-9 ND ug/L 0.42 0.34 1 11/15/2107:08 11/16/2114:50 12672-29-6 ND ug/L 0.42 0.21 1 11/15/2107:08 11/16/2114:50 11097-69-1 ND ug/L 0.42 0.35 1 11/15/2107:08 11/16/2114:50 11096-82-5 92 % 10-181 1 11/15/2107:08 11/16/2114:50 2051-24-3 Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville 6.2 ug/L 5.0 3.0 1 11/16/2114:13 11/29/2118:12 7440-36-0 ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:12 7440-38-2 109 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:12 7440-39-3 N D ug/L 1.0 0.70 1 11 /16/21 14:13 11 /29/21 18:12 7440-41-7 ND ug/L 1.0 0.40 1 11/16/2114:13 11/29/2118:12 7440-43-9 6.1 ug/L 5.0 3.7 1 11/16/2114:13 11/29/2118:12 7440-47-3 4.6J ug/L 5.0 3.6 1 11/16/2114:13 11/29/2118:12 7440-48-4 4.4J ug/L 5.0 4.3 1 11/16/2114:13 11/29/2118:12 7440-50-8 3950 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2118:12 7439-89-6 5.3 ug/L 5.0 4.5 1 11/16/2114:13 11/29/2118:12 7439-92-1 26400 ug/L 50.0 34.3 10 11/16/2114:13 11/30/2113:51 7439-96-5 12.5 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:12 7440-02-0 ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:12 7782-49-2 9.6 ug/L 5.0 2.5 1 11/16/2114:13 11/29/2118:12 7440-22-4 92900 ug/L 5000 611 1 11/16/2114:13 11/29/2118:12 7440-23-5 N D ug/L 5.0 4.7 1 11 /16/21 14:13 11 /29/21 18:12 7440-31-5 125 ug/L 5.0 3.9 1 11/16/2114:13 11/29/2118:12 7440-62-2 ND ug/L 10.0 9.5 1 11/16/2114:13 11/29/2118:12 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:29 7439-97-6 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 9.1 2.4 1 11/15/2106:49 11/16/2110:19 56-55-3 ND ug/L 9.1 2.5 1 11/15/2106:49 11/16/2110:19 218-01-9 ND ug/L 9.1 2.7 1 11/15/2106:49 11/16/2110:19 53-70-3 ND ug/L 5.5 3.4 1 11/15/2106:49 11/16/2110:19 117-81-7 ND ug/L 9.1 2.6 1 11/15/2106:49 11/16/2110:19 193-39-5 64 % 10-144 1 11/15/2106:49 11/16/2110:19 4165-60-0 48 % 10-130 1 11/15/2106:49 11/16/2110:19 321-60-8 63 % 34-163 1 11/15/2106:49 11/16/2110:19 1718-51-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 51 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-10 Lab ID: 92572199009 Collected: 11/09/21 12:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2109:08 67-64-1 ND ug/L 10.0 1.8 1 11/16/2109:08 107-13-1 0.47J ug/L 1.0 0.34 1 11/16/2109:08 71-43-2 ND ug/L 1.0 0.47 1 11/16/2109:08 74-97-5 ND ug/L 1.0 0.31 1 11/16/2109:08 75-27-4 ND ug/L 1.0 0.34 1 11/16/2109:08 75-25-2 ND ug/L 2.0 1.7 1 11/16/2109:08 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2109:08 78-93-3 ND ug/L 2.0 0.73 1 11/16/2109:08 75-15-0 ND ug/L 1.0 0.33 1 11/16/2109:08 56-23-5 ND ug/L 1.0 0.28 1 11/16/2109:08 108-90-7 ND ug/L 1.0 0.65 1 11/16/2109:08 75-00-3 ND ug/L 1.0 0.43 1 11/16/2109:08 67-66-3 ND ug/L 1.0 0.54 1 11/16/2109:08 74-87-3 ND ug/L 2.0 0.34 1 11/16/2109:08 96-12-8 ND ug/L 1.0 0.36 1 11/16/2109:08 124-48-1 ND ug/L 1.0 0.27 1 11/16/2109:08 106-93-4 ND ug/L 1.0 0.39 1 11/16/2109:08 74-95-3 ND ug/L 1.0 0.34 1 11/16/2109:08 95-50-1 ND ug/L 1.0 0.33 1 11/16/2109:08 106-46-7 ND ug/L 1.0 0.56 1 11/16/2109:08 110-57-6 ND ug/L 1.0 0.35 1 11/16/2109:08 75-71-8 ND ug/L 1.0 0.37 1 11/16/2109:08 75-34-3 ND ug/L 1.0 0.32 1 11/16/2109:08 107-06-2 ND ug/L 1.0 0.35 1 11/16/2109:08 75-35-4 ND ug/L 1.0 0.38 1 11/16/2109:08 156-59-2 ND ug/L 1.0 0.40 1 11/16/2109:08 156-60-5 ND ug/L 1.0 0.36 1 11/16/2109:08 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 09:08 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2109:08 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2109:08 100-41-4 ND ug/L 5.0 0.48 1 11/16/2109:08 591-78-6 ND ug/L 20.0 9.7 1 11/16/2109:08 74-88-4 ND ug/L 5.0 2.0 1 11/16/2109:08 75-09-2 ND ug/L 5.0 2.7 1 11/16/2109:08 108-10-1 ND ug/L 1.0 0.29 1 11/16/2109:08 100-42-5 ND ug/L 1.0 0.31 1 11/16/2109:08 630-20-6 ND ug/L 1.0 0.22 1 11/16/2109:08 79-34-5 ND ug/L 1.0 0.29 1 11/16/2109:08 127-18-4 65.1 ug/L 10.0 3.5 1 11/16/2109:08 109-99-9 ND ug/L 1.0 0.48 1 11/16/2109:08 108-88-3 ND ug/L 1.0 0.33 1 11/16/2109:08 71-55-6 ND ug/L 1.0 0.32 1 11/16/2109:08 79-00-5 ND ug/L 1.0 0.38 1 11/16/2109:08 79-01-6 ND ug/L 1.0 0.30 1 11/16/2109:08 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 52 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-10 Lab ID: 92572199009 Collected: 11/09/21 12:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 09:08 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 09:08 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 09:08 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 09:08 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 09:08 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 09:08 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 09:08 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 11/16/21 09:08 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 4.3 ug/L 2.0 0.86 1 11/16/21 02:33 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 11/16/21 02:33 17060-07-0 Toluene-d8 (S) 87 % 66-133 1 11/16/21 02:33 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 734000 ug/L 5000 5000 1 11/17/21 14:50 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 1070000 ug/L 50000 50000 1 11/15/21 17:12 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:24 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 165000 ug/L 3000 1500 3 11/16/2112:18 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 43900 ug/L 2000 1000 2 11/19/2108:22 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:21 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 53 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-11 Lab ID: 92572199010 Collected: 11/09/21 10:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/16/2111:40 11/17/2119:27 309-00-2 ND ug/L 0.0500 0.0172 1 11/16/2111:40 11/17/2119:27 319-84-6 ND ug/L 0.0500 0.0208 1 11/16/2111:40 11/17/2119:27 319-85-7 ND ug/L 0.0500 0.0150 1 11/16/2111:40 11/17/2119:27 319-86-8 ND ug/L 0.0500 0.0209 1 11/16/2111:40 11/17/2119:27 58-89-9 ND ug/L 5.00 0.0198 1 11/16/2111:40 11/17/2119:27 57-74-9 ND ug/L 0.0500 0.0177 1 11/16/2111:40 11/17/2119:27 72-54-8 ND ug/L 0.0500 0.0154 1 11/16/2111:40 11/17/2119:27 72-55-9 ND ug/L 0.0500 0.0198 1 11/16/2111:40 11/17/2119:27 50-29-3 ND ug/L 0.0500 0.0162 1 11/16/2111:40 11/17/2119:27 60-57-1 ND ug/L 0.0500 0.0160 1 11/16/2111:40 11/17/2119:27 959-98-8 ND ug/L 0.0500 0.0164 1 11/16/2111:40 11/17/2119:27 33213-65-9 ND ug/L 0.0500 0.0217 1 11/16/2111:40 11/17/2119:27 1031-07-8 ND ug/L 0.0500 0.0161 1 11/16/2111:40 11/17/2119:27 72-20-8 ND ug/L 0.0500 0.0237 1 11/16/2111:40 11/17/2119:27 7421-93-4 ND ug/L 0.0500 0.0219 1 11/16/2111:40 11/17/2119:27 53494-70-5 ND ug/L 0.0500 0.0176 1 11/16/2111:40 11/17/2119:27 118-74-1 ND ug/L 0.0500 0.0148 1 11/16/2111:40 11/17/2119:27 76-44-8 ND ug/L 0.0500 0.0183 1 11/16/2111:40 11/17/2119:27 1024-57-3 ND ug/L 0.0500 0.0193 1 11/16/2111:40 11/17/2119:27 72-43-5 ND ug/L 0.500 0.168 1 11/16/2111:40 11/17/2119:27 8001-35-2 77.8 % 10.0-128 1 11/16/2111:40 11/17/2119:27 2051-24-3 87.4 % 10.0-127 1 11/16/2111:40 11/17/2119:27 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/15/2117:01 11/17/2100:44 94-75-7 LO ND ug/L 2.00 0.344 1 11/15/2117:01 11/17/2100:44 127-20-8 LO ND ug/L 2.00 0.302 1 11/15/2117:01 11/17/2100:44 94-82-6 LO ND ug/L 2.00 0.245 1 11/15/2117:01 11/17/2100:44 1918-00-9 LO ND ug/L 2.00 1.04 1 11/15/2117:01 11/17/2100:44 15165-67-0 LO ND ug/L 2.00 0.250 1 11/15/2117:01 11/19/2103:05 88-85-7 ND ug/L 100 13.1 1 11/15/2117:01 11/17/2100:44 94-74-6 ND ug/L 100 66.0 1 11/15/2117:01 11/17/2100:44 7085-19-0 ND ug/L 2.00 0.258 1 11/15/2117:01 11/17/2100:44 93-76-5 LO ND ug/L 2.00 0.335 1 11/15/2117:01 11/17/2100:44 93-72-1 LO 91.0 % 14.0-158 1 11/15/2117:01 11/17/2100:44 19719-28-9 94.4 % 14.0-158 1 11/15/2117:01 11/19/2103:05 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.45 0.43 1 11/15/2107:08 11/16/2115:02 12674-11-2 ND ug/L 0.45 0.41 1 11/15/2107:08 11/16/2115:02 11104-28-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 54 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-11 Lab ID: 92572199010 Collected: 11/09/21 10:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Sodium Tin Vanadium Zinc 7470 Mercury Mercury 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate I ndeno(1,2,3-cd )pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.45 0.33 1 11/15/2107:08 11/16/2115:02 11141-16-5 ND ug/L 0.45 0.24 1 11/15/2107:08 11/16/2115:02 53469-21-9 ND ug/L 0.45 0.37 1 11/15/2107:08 11/16/2115:02 12672-29-6 ND ug/L 0.45 0.23 1 11/15/2107:08 11/16/2115:02 11097-69-1 ND ug/L 0.45 0.38 1 11/15/2107:08 11/16/2115:02 11096-82-5 107 % 10-181 1 11/15/2107:08 11/16/2115:02 2051-24-3 Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2118:15 7440-36-0 ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:15 7440-38-2 95.6 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:15 7440-39-3 N D ug/L 1.0 0.70 1 11 /16/21 14:13 11 /29/21 18:15 7440-41-7 ND ug/L 1.0 0.40 1 11/16/2114:13 11/29/2118:15 7440-43-9 5.2 ug/L 5.0 3.7 1 11/16/2114:13 11/29/2118:15 7440-47-3 ND ug/L 5.0 3.6 1 11/16/2114:13 11/29/2118:15 7440-48-4 ND ug/L 5.0 4.3 1 11/16/2114:13 11/29/2118:15 7440-50-8 24600 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2118:15 7439-89-6 ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2118:15 7439-92-1 1190 ug/L 5.0 3.4 1 11/16/2114:13 11/29/2118:15 7439-96-5 3.6J ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:15 7440-02-0 ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:15 7782-49-2 ND ug/L 5.0 2.5 1 11/16/2114:13 11/29/2118:15 7440-22-4 12300 ug/L 5000 611 1 11/16/2114:13 11/29/2118:15 7440-23-5 N D ug/L 5.0 4.7 1 11 /16/21 14:13 11 /29/21 18:15 7440-31-5 13.2 ug/L 5.0 3.9 1 11/16/2114:13 11/29/2118:15 7440-62-2 10.0 ug/L 10.0 9.5 1 11/16/2114:13 11/29/2118:15 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:31 7439-97-6 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 8.3 2.2 1 11/15/2106:49 11/16/2110:44 56-55-3 ND ug/L 8.3 2.3 1 11/15/2106:49 11/16/2110:44 218-01-9 ND ug/L 8.3 2.5 1 11/15/2106:49 11/16/2110:44 53-70-3 ND ug/L 5.0 3.1 1 11/15/2106:49 11/16/2110:44 117-81-7 ND ug/L 8.3 2.4 1 11/15/2106:49 11/16/2110:44 193-39-5 57 % 10-144 1 11/15/2106:49 11/16/2110:44 4165-60-0 44 % 10-130 1 11/15/2106:49 11/16/2110:44 321-60-8 60 % 34-163 1 11/15/2106:49 11/16/2110:44 1718-51-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 55 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-11 Lab ID: 92572199010 Collected: 11/09/21 10:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2109:26 67-64-1 ND ug/L 10.0 1.8 1 11/16/2109:26 107-13-1 ND ug/L 1.0 0.34 1 11/16/2109:26 71-43-2 ND ug/L 1.0 0.47 1 11/16/2109:26 74-97-5 ND ug/L 1.0 0.31 1 11/16/2109:26 75-27-4 ND ug/L 1.0 0.34 1 11/16/2109:26 75-25-2 ND ug/L 2.0 1.7 1 11/16/2109:26 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2109:26 78-93-3 ND ug/L 2.0 0.73 1 11/16/2109:26 75-15-0 ND ug/L 1.0 0.33 1 11/16/2109:26 56-23-5 ND ug/L 1.0 0.28 1 11/16/2109:26 108-90-7 ND ug/L 1.0 0.65 1 11/16/2109:26 75-00-3 ND ug/L 1.0 0.43 1 11/16/2109:26 67-66-3 ND ug/L 1.0 0.54 1 11/16/2109:26 74-87-3 ND ug/L 2.0 0.34 1 11/16/2109:26 96-12-8 ND ug/L 1.0 0.36 1 11/16/2109:26 124-48-1 ND ug/L 1.0 0.27 1 11/16/2109:26 106-93-4 ND ug/L 1.0 0.39 1 11/16/2109:26 74-95-3 ND ug/L 1.0 0.34 1 11/16/2109:26 95-50-1 ND ug/L 1.0 0.33 1 11/16/2109:26 106-46-7 ND ug/L 1.0 0.56 1 11/16/2109:26 110-57-6 ND ug/L 1.0 0.35 1 11/16/2109:26 75-71-8 ND ug/L 1.0 0.37 1 11/16/2109:26 75-34-3 ND ug/L 1.0 0.32 1 11/16/2109:26 107-06-2 ND ug/L 1.0 0.35 1 11/16/2109:26 75-35-4 ND ug/L 1.0 0.38 1 11/16/2109:26 156-59-2 ND ug/L 1.0 0.40 1 11/16/2109:26 156-60-5 ND ug/L 1.0 0.36 1 11/16/2109:26 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 09:26 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2109:26 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2109:26 100-41-4 ND ug/L 5.0 0.48 1 11/16/2109:26 591-78-6 ND ug/L 20.0 9.7 1 11/16/2109:26 74-88-4 ND ug/L 5.0 2.0 1 11/16/2109:26 75-09-2 ND ug/L 5.0 2.7 1 11/16/2109:26 108-10-1 ND ug/L 1.0 0.29 1 11/16/2109:26 100-42-5 ND ug/L 1.0 0.31 1 11/16/2109:26 630-20-6 ND ug/L 1.0 0.22 1 11/16/2109:26 79-34-5 ND ug/L 1.0 0.29 1 11/16/2109:26 127-18-4 ND ug/L 10.0 3.5 1 11/16/2109:26 109-99-9 ND ug/L 1.0 0.48 1 11/16/2109:26 108-88-3 ND ug/L 1.0 0.33 1 11/16/2109:26 71-55-6 ND ug/L 1.0 0.32 1 11/16/2109:26 79-00-5 ND ug/L 1.0 0.38 1 11/16/2109:26 79-01-6 ND ug/L 1.0 0.30 1 11/16/2109:26 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 56 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-11 Lab ID: 92572199010 Collected: 11/09/21 10:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 09:26 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 09:26 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 09:26 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 09:26 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 09:26 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 09:26 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 09:26 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 09:26 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 11/16/21 02:52 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 86 % 70-130 1 11/16/21 02:52 17060-07-0 Toluene-d8 (S) 87 % 66-133 1 11/16/21 02:52 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 81300 ug/L 5000 5000 1 11/17/21 14:59 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 176000 ug/L 25000 25000 1 11/15/21 17:12 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:25 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 11900 ug/L 1000 500 1 11/14/2101:48 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 8460 ug/L 1000 500 1 11/19/2108:12 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:22 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 57 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-12 Lab ID: 92572199011 Collected: 11/08/21 17:40 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2100:35 309-00-2 ND ug/L 0.0500 0.0172 1 11/15/2106:10 11/16/2100:35 319-84-6 ND ug/L 0.0500 0.0208 1 11/15/2106:10 11/16/2100:35 319-85-7 ND ug/L 0.0500 0.0150 1 11/15/2106:10 11/16/2100:35 319-86-8 ND ug/L 0.0500 0.0209 1 11/15/2106:10 11/16/2100:35 58-89-9 ND ug/L 5.00 0.0198 1 11/15/2106:10 11/16/2100:35 57-74-9 ND ug/L 0.0500 0.0177 1 11/15/2106:10 11/16/2100:35 72-54-8 ND ug/L 0.0500 0.0154 1 11/15/2106:10 11/16/2100:35 72-55-9 ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2100:35 50-29-3 ND ug/L 0.0500 0.0162 1 11/15/2106:10 11/16/2100:35 60-57-1 ND ug/L 0.0500 0.0160 1 11/15/2106:10 11/16/2100:35 959-98-8 ND ug/L 0.0500 0.0164 1 11/15/2106:10 11/16/2100:35 33213-65-9 ND ug/L 0.0500 0.0217 1 11/15/2106:10 11/16/2100:35 1031-07-8 ND ug/L 0.0500 0.0161 1 11/15/2106:10 11/16/2100:35 72-20-8 ND ug/L 0.0500 0.0237 1 11/15/2106:10 11/16/2100:35 7421-93-4 ND ug/L 0.0500 0.0219 1 11/15/2106:10 11/16/2100:35 53494-70-5 ND ug/L 0.0500 0.0176 1 11/15/2106:10 11/16/2100:35 118-74-1 ND ug/L 0.0500 0.0148 1 11/15/2106:10 11/16/2100:35 76-44-8 ND ug/L 0.0500 0.0183 1 11/15/2106:10 11/16/2100:35 1024-57-3 ND ug/L 0.0500 0.0193 1 11/15/2106:10 11/16/2100:35 72-43-5 ND ug/L 0.500 0.168 1 11/15/2106:10 11/16/2100:35 8001-35-2 27.6 % 10.0-128 1 11/15/2106:10 11/16/2100:35 2051-24-3 69.3 % 10.0-127 1 11/15/2106:10 11/16/2100:35 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2.86 ug/L 2.00 0.547 1 11/15/2108:09 11/16/2120:57 94-75-7 ND ug/L 2.00 0.344 1 11/15/2108:09 11/16/2120:57 127-20-8 ND ug/L 2.00 0.302 1 11/15/2108:09 11/16/2120:57 94-82-6 ND ug/L 2.00 0.245 1 11/15/2108:09 11/16/2120:57 1918-00-9 ND ug/L 2.00 1.04 1 11/15/2108:09 11/16/2120:57 15165-67-0 ND ug/L 2.00 0.250 1 11/15/2108:09 11/16/2120:57 88-85-7 ND ug/L 100 13.1 1 11/15/2108:09 11/16/2120:57 94-74-6 ND ug/L 100 66.0 1 11/15/2108:09 11/16/2120:57 7085-19-0 ND ug/L 2.00 0.258 1 11/15/2108:09 11/16/2120:57 93-76-5 ND ug/L 2.00 0.335 1 11/15/2108:09 11/16/2120:57 93-72-1 115 % 14.0-158 1 11/15/2108:09 11/16/2120:57 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.45 0.43 1 11/15/2107:08 11/16/2115:13 12674-11-2 ND ug/L 0.45 0.41 1 11/15/2107:08 11/16/2115:13 11104-28-2 ND ug/L 0.45 0.33 1 11/15/2107:08 11/16/2115:13 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. LO Page 58 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-12 Lab ID: 92572199011 Collected: 11/08/21 17:40 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.45 0.24 1 11/15/21 07:08 11/16/21 15:13 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.45 0.37 1 11/15/21 07:08 11/16/21 15:13 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.45 0.23 1 11/15/21 07:08 11/16/21 15:13 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.45 0.38 1 11/15/21 07:08 11/16/21 15:13 11096-82-5 Surrogates Decachlorobiphenyl (S) 80 % 10-181 1 11/15/21 07:08 11/16/21 15:13 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2118:18 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:18 7440-38-2 Barium 145 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:18 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/29/2118:18 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/29/2118:18 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/29/2118:18 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/29/2118:18 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/29/2118:18 7440-50-8 Iron 1020 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2118:18 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2118:18 7439-92-1 Manganese 3440 ug/L 5.0 3.4 1 11/16/2114:13 11/29/2118:18 7439-96-5 Nickel 10.2 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:18 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:18 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/29/2118:18 7440-22-4 Sodium 23300 ug/L 5000 611 1 11/16/2114:13 11/29/2118:18 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/29/2118:18 7440-31-5 Vanadium 22.4 ug/L 5.0 3.9 1 11/16/2114:13 11/29/2118:18 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/29/2118:18 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:34 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 8.3 2.2 1 11/15/21 06:49 11/15/21 15:40 56-55-3 Chrysene ND ug/L 8.3 2.3 1 11/15/21 06:49 11/15/21 15:40 218-01-9 Dibenz(a,h)anthracene ND ug/L 8.3 2.5 1 11/15/21 06:49 11/15/21 15:40 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 3.1 1 11/15/21 06:49 11/15/21 15:40 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 8.3 2.4 1 11/15/21 06:49 11/15/21 15:40 193-39-5 Surrogates Nitrobenzene-d5 (S) 65 % 10-144 1 11/15/21 06:49 11/15/21 15:40 4165-60-0 2-Fluorobiphenyl (S) 52 % 10-130 1 11/15/21 06:49 11/15/21 15:40 321-60-8 Terphenyl-d14 (S) 68 % 34-163 1 11/15/21 06:49 11/15/21 15:40 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 59 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-12 Lab ID: 92572199011 Collected: 11/08/21 17:40 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/13/2119:20 67-64-1 ND ug/L 10.0 1.8 1 11/13/2119:20 107-13-1 0.41J ug/L 1.0 0.34 1 11/13/2119:20 71-43-2 ND ug/L 1.0 0.47 1 11/13/2119:20 74-97-5 ND ug/L 1.0 0.31 1 11/13/2119:20 75-27-4 ND ug/L 1.0 0.34 1 11/13/2119:20 75-25-2 ND ug/L 2.0 1.7 1 11/13/2119:20 74-83-9 ND ug/L 5.0 4.0 1 11/13/2119:20 78-93-3 ND ug/L 2.0 0.73 1 11/13/2119:20 75-15-0 ND ug/L 1.0 0.33 1 11/13/2119:20 56-23-5 ND ug/L 1.0 0.28 1 11/13/2119:20 108-90-7 ND ug/L 1.0 0.65 1 11/13/2119:20 75-00-3 ND ug/L 1.0 0.43 1 11/13/2119:20 67-66-3 ND ug/L 1.0 0.54 1 11/13/2119:20 74-87-3 ND ug/L 2.0 0.34 1 11/13/2119:20 96-12-8 ND ug/L 1.0 0.36 1 11/13/2119:20 124-48-1 ND ug/L 1.0 0.27 1 11/13/2119:20 106-93-4 ND ug/L 1.0 0.39 1 11/13/2119:20 74-95-3 ND ug/L 1.0 0.34 1 11/13/2119:20 95-50-1 ND ug/L 1.0 0.33 1 11/13/2119:20 106-46-7 ND ug/L 1.0 0.56 1 11/13/2119:20 110-57-6 ND ug/L 1.0 0.35 1 11/13/2119:20 75-71-8 ND ug/L 1.0 0.37 1 11/13/2119:20 75-34-3 ND ug/L 1.0 0.32 1 11/13/2119:20 107-06-2 ND ug/L 1.0 0.35 1 11/13/2119:20 75-35-4 ND ug/L 1.0 0.38 1 11/13/2119:20 156-59-2 ND ug/L 1.0 0.40 1 11/13/2119:20 156-60-5 ND ug/L 1.0 0.36 1 11/13/2119:20 78-87-5 ND ug/L 1.0 0.36 1 11 /13/21 19:20 10061-01-5 ND ug/L 1.0 0.36 1 11/13/2119:20 10061-02-6 ND ug/L 1.0 0.30 1 11/13/2119:20 100-41-4 ND ug/L 5.0 0.48 1 11/13/2119:20 591-78-6 ND ug/L 20.0 9.7 1 11/13/2119:20 74-88-4 ND ug/L 5.0 2.0 1 11/13/2119:20 75-09-2 ND ug/L 5.0 2.7 1 11/13/2119:20 108-10-1 ND ug/L 1.0 0.29 1 11/13/2119:20 100-42-5 ND ug/L 1.0 0.31 1 11/13/2119:20 630-20-6 ND ug/L 1.0 0.22 1 11/13/2119:20 79-34-5 ND ug/L 1.0 0.29 1 11/13/2119:20 127-18-4 ND ug/L 10.0 3.5 1 11/13/2119:20 109-99-9 ND ug/L 1.0 0.48 1 11/13/2119:20 108-88-3 ND ug/L 1.0 0.33 1 11/13/2119:20 71-55-6 ND ug/L 1.0 0.32 1 11/13/2119:20 79-00-5 ND ug/L 1.0 0.38 1 11/13/2119:20 79-01-6 ND ug/L 1.0 0.30 1 11/13/2119:20 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 Page 60 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-12 Lab ID: 92572199011 Collected: 11/08/21 17:40 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/13/21 19:20 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/13/21 19:20 108-05-4 v1 Vinyl chloride ND ug/L 1.0 0.39 1 11/13/21 19:20 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/13/21 19:20 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/13/21 19:20 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 11/13/21 19:20 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 11/13/21 19:20 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 11/13/21 19:20 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 5.7 ug/L 2.0 0.86 1 11/16/21 03:11 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 11/16/21 03:11 17060-07-0 Toluene-d8 (S) 89 % 66-133 1 11/16/21 03:11 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 296000 ug/L 5000 5000 1 11/17/21 09:33 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 489000 ug/L 25000 25000 1 11/14/21 17:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2102:59 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 87600 ug/L 1000 500 1 11/14/2102:04 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 22400 ug/L 1000 500 1 11/19/2108:13 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 80.0 60.0 10 11/17/2113:31 11/18/2112:11 57-12-5 D3 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 61 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-13 Lab ID: 92572199012 Collected: 11/08/21 16:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2100:46 309-00-2 ND ug/L 0.0500 0.0172 1 11/15/2106:10 11/16/2100:46 319-84-6 ND ug/L 0.0500 0.0208 1 11/15/2106:10 11/16/2100:46 319-85-7 ND ug/L 0.0500 0.0150 1 11/15/2106:10 11/16/2100:46 319-86-8 ND ug/L 0.0500 0.0209 1 11/15/2106:10 11/16/2100:46 58-89-9 ND ug/L 5.00 0.0198 1 11/15/2106:10 11/16/2100:46 57-74-9 ND ug/L 0.0500 0.0177 1 11/15/2106:10 11/16/2100:46 72-54-8 ND ug/L 0.0500 0.0154 1 11/15/2106:10 11/16/2100:46 72-55-9 ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2100:46 50-29-3 ND ug/L 0.0500 0.0162 1 11/15/2106:10 11/16/2100:46 60-57-1 ND ug/L 0.0500 0.0160 1 11/15/2106:10 11/16/2100:46 959-98-8 ND ug/L 0.0500 0.0164 1 11/15/2106:10 11/16/2100:46 33213-65-9 ND ug/L 0.0500 0.0217 1 11/15/2106:10 11/16/2100:46 1031-07-8 ND ug/L 0.0500 0.0161 1 11/15/2106:10 11/16/2100:46 72-20-8 ND ug/L 0.0500 0.0237 1 11/15/2106:10 11/16/2100:46 7421-93-4 ND ug/L 0.0500 0.0219 1 11/15/2106:10 11/16/2100:46 53494-70-5 ND ug/L 0.0500 0.0176 1 11/15/2106:10 11/16/2100:46 118-74-1 ND ug/L 0.0500 0.0148 1 11/15/2106:10 11/16/2100:46 76-44-8 ND ug/L 0.0500 0.0183 1 11/15/2106:10 11/16/2100:46 1024-57-3 ND ug/L 0.0500 0.0193 1 11/15/2106:10 11/16/2100:46 72-43-5 ND ug/L 0.500 0.168 1 11/15/2106:10 11/16/2100:46 8001-35-2 12.6 % 10.0-128 1 11/15/2106:10 11/16/2100:46 2051-24-3 51.5 % 10.0-127 1 11/15/2106:10 11/16/2100:46 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/15/2108:09 11/16/2121:11 94-75-7 ND ug/L 2.00 0.344 1 11/15/2108:09 11/16/2121:11 127-20-8 LO ND ug/L 2.00 0.302 1 11/15/2108:09 11/16/2121:11 94-82-6 ND ug/L 2.00 0.245 1 11/15/2108:09 11/16/2121:11 1918-00-9 ND ug/L 2.00 1.04 1 11/15/2108:09 11/16/2121:11 15165-67-0 ND ug/L 2.00 0.250 1 11/15/2108:09 11/16/2121:11 88-85-7 ND ug/L 100 13.1 1 11/15/2108:09 11/16/2121:11 94-74-6 ND ug/L 100 66.0 1 11/15/2108:09 11/16/2121:11 7085-19-0 ND ug/L 2.00 0.258 1 11/15/2108:09 11/16/2121:11 93-76-5 ND ug/L 2.00 0.335 1 11/15/2108:09 11/16/2121:11 93-72-1 185 % 14.0-158 1 11/15/2108:09 11/16/2121:11 19719-28-9 ST Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.50 0.47 1 11/15/2107:08 11/16/2115:25 12674-11-2 ND ug/L 0.50 0.45 1 11/15/2107:08 11/16/2115:25 11104-28-2 ND ug/L 0.50 0.36 1 11/15/2107:08 11/16/2115:25 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 62 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-13 Lab ID: 92572199012 Collected: 11/08/21 16:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.50 0.26 1 11/15/21 07:08 11/16/21 15:25 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 0.40 1 11/15/21 07:08 11/16/21 15:25 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.50 0.25 1 11/15/21 07:08 11/16/21 15:25 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 0.42 1 11/15/21 07:08 11/16/21 15:25 11096-82-5 Surrogates Decachlorobiphenyl (S) 117 % 10-181 1 11/15/21 07:08 11/16/21 15:25 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2118:21 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:21 7440-38-2 Barium 514 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:21 7440-39-3 Beryllium 1.4 ug/L 1.0 0.70 1 11/16/2114:13 11/29/2118:21 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/29/2118:21 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/29/2118:21 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/29/2118:21 7440-48-4 Copper 4.3J ug/L 5.0 4.3 1 11/16/2114:13 11/29/2118:21 7440-50-8 Iron 238 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2118:21 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2118:21 7439-92-1 Manganese 155 ug/L 5.0 3.4 1 11/16/2114:13 11/29/2118:21 7439-96-5 Nickel 11.3 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:21 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:21 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/29/2118:21 7440-22-4 Sodium 18300 ug/L 5000 611 1 11/16/2114:13 11/29/2118:21 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/29/2118:21 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 11/16/2114:13 11/29/2118:21 7440-62-2 Zinc 11.1 ug/L 10.0 9.5 1 11/16/2114:13 11/29/2118:21 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:36 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 8.3 2.2 1 11/15/21 06:49 11/15/21 16:05 56-55-3 Chrysene ND ug/L 8.3 2.3 1 11/15/21 06:49 11/15/21 16:05 218-01-9 Dibenz(a,h)anthracene ND ug/L 8.3 2.5 1 11/15/21 06:49 11/15/21 16:05 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 3.1 1 11/15/21 06:49 11/15/21 16:05 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 8.3 2.4 1 11/15/21 06:49 11/15/21 16:05 193-39-5 Surrogates Nitrobenzene-d5 (S) 70 % 10-144 1 11/15/21 06:49 11/15/21 16:05 4165-60-0 2-Fluorobiphenyl (S) 54 % 10-130 1 11/15/21 06:49 11/15/21 16:05 321-60-8 Terphenyl-d14 (S) 72 % 34-163 1 11/15/21 06:49 11/15/21 16:05 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 63 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-13 Lab ID: 92572199012 Collected: 11/08/21 16:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/13/2119:38 67-64-1 ND ug/L 10.0 1.8 1 11/13/2119:38 107-13-1 ND ug/L 1.0 0.34 1 11/13/2119:38 71-43-2 ND ug/L 1.0 0.47 1 11/13/2119:38 74-97-5 ND ug/L 1.0 0.31 1 11/13/2119:38 75-27-4 ND ug/L 1.0 0.34 1 11/13/2119:38 75-25-2 ND ug/L 2.0 1.7 1 11/13/2119:38 74-83-9 ND ug/L 5.0 4.0 1 11/13/2119:38 78-93-3 ND ug/L 2.0 0.73 1 11/13/2119:38 75-15-0 ND ug/L 1.0 0.33 1 11/13/2119:38 56-23-5 ND ug/L 1.0 0.28 1 11/13/2119:38 108-90-7 ND ug/L 1.0 0.65 1 11/13/2119:38 75-00-3 ND ug/L 1.0 0.43 1 11/13/2119:38 67-66-3 ND ug/L 1.0 0.54 1 11/13/2119:38 74-87-3 ND ug/L 2.0 0.34 1 11/13/2119:38 96-12-8 ND ug/L 1.0 0.36 1 11/13/2119:38 124-48-1 ND ug/L 1.0 0.27 1 11/13/2119:38 106-93-4 ND ug/L 1.0 0.39 1 11/13/2119:38 74-95-3 ND ug/L 1.0 0.34 1 11/13/2119:38 95-50-1 ND ug/L 1.0 0.33 1 11/13/2119:38 106-46-7 ND ug/L 1.0 0.56 1 11/13/2119:38 110-57-6 ND ug/L 1.0 0.35 1 11/13/2119:38 75-71-8 ND ug/L 1.0 0.37 1 11/13/2119:38 75-34-3 ND ug/L 1.0 0.32 1 11/13/2119:38 107-06-2 ND ug/L 1.0 0.35 1 11/13/2119:38 75-35-4 ND ug/L 1.0 0.38 1 11/13/2119:38 156-59-2 ND ug/L 1.0 0.40 1 11/13/2119:38 156-60-5 ND ug/L 1.0 0.36 1 11/13/2119:38 78-87-5 ND ug/L 1.0 0.36 1 11 /13/21 19:38 10061-01-5 ND ug/L 1.0 0.36 1 11/13/2119:38 10061-02-6 ND ug/L 1.0 0.30 1 11/13/2119:38 100-41-4 ND ug/L 5.0 0.48 1 11/13/2119:38 591-78-6 ND ug/L 20.0 9.7 1 11/13/2119:38 74-88-4 ND ug/L 5.0 2.0 1 11/13/2119:38 75-09-2 ND ug/L 5.0 2.7 1 11/13/2119:38 108-10-1 ND ug/L 1.0 0.29 1 11/13/2119:38 100-42-5 ND ug/L 1.0 0.31 1 11/13/2119:38 630-20-6 ND ug/L 1.0 0.22 1 11/13/2119:38 79-34-5 ND ug/L 1.0 0.29 1 11/13/2119:38 127-18-4 12.7 ug/L 10.0 3.5 1 11/13/2119:38 109-99-9 ND ug/L 1.0 0.48 1 11/13/2119:38 108-88-3 ND ug/L 1.0 0.33 1 11/13/2119:38 71-55-6 ND ug/L 1.0 0.32 1 11/13/2119:38 79-00-5 ND ug/L 1.0 0.38 1 11/13/2119:38 79-01-6 ND ug/L 1.0 0.30 1 11/13/2119:38 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 Page 64 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-13 Lab ID: 92572199012 Collected: 11/08/21 16:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/13/21 19:38 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/13/21 19:38 108-05-4 v1 Vinyl chloride ND ug/L 1.0 0.39 1 11/13/21 19:38 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/13/21 19:38 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/13/21 19:38 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 11/13/21 19:38 460-00-4 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 11/13/21 19:38 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 11/13/21 19:38 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 5.6 ug/L 2.0 0.86 1 11/16/21 03:31 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 11/16/21 03:31 17060-07-0 Toluene-d8 (S) 87 % 66-133 1 11/16/21 03:31 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 93800 ug/L 5000 5000 1 11/16/21 15:45 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 276000 ug/L 25000 25000 1 11/14/21 17:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2102:59 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 22300 ug/L 1000 500 1 11/14/2102:19 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 49800 ug/L 2000 1000 2 11/24/2111:20 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/17/2113:31 11/18/2110:32 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 65 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-14 Lab ID: 92572199013 Collected: 11/11/21 12:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/18/2114:40 11/19/2108:14 309-00-2 ND ug/L 0.0500 0.0172 1 11/18/2114:40 11/19/2108:14 319-84-6 ND ug/L 0.0500 0.0208 1 11/18/2114:40 11/19/2108:14 319-85-7 ND ug/L 0.0500 0.0150 1 11/18/2114:40 11/19/2108:14 319-86-8 ND ug/L 0.0500 0.0209 1 11/18/2114:40 11/19/2108:14 58-89-9 ND ug/L 5.00 0.0198 1 11/18/2114:40 11/19/2108:14 57-74-9 ND ug/L 0.0500 0.0177 1 11/18/2114:40 11/19/2108:14 72-54-8 ND ug/L 0.0500 0.0154 1 11/18/2114:40 11/19/2108:14 72-55-9 ND ug/L 0.0500 0.0198 1 11/18/2114:40 11/19/2108:14 50-29-3 ND ug/L 0.0500 0.0162 1 11/18/2114:40 11/19/2108:14 60-57-1 ND ug/L 0.0500 0.0160 1 11/18/2114:40 11/19/2108:14 959-98-8 ND ug/L 0.0500 0.0164 1 11/18/2114:40 11/19/2108:14 33213-65-9 ND ug/L 0.0500 0.0217 1 11/18/2114:40 11/19/2108:14 1031-07-8 ND ug/L 0.0500 0.0161 1 11/18/2114:40 11/19/2108:14 72-20-8 ND ug/L 0.0500 0.0237 1 11/18/2114:40 11/19/2108:14 7421-93-4 ND ug/L 0.0500 0.0219 1 11/18/2114:40 11/19/2108:14 53494-70-5 ND ug/L 0.0500 0.0176 1 11/18/2114:40 11/19/2108:14 118-74-1 ND ug/L 0.0500 0.0148 1 11/18/2114:40 11/19/2108:14 76-44-8 ND ug/L 0.0500 0.0183 1 11/18/2114:40 11/19/2108:14 1024-57-3 ND ug/L 0.0500 0.0193 1 11/18/2114:40 11/19/2108:14 72-43-5 ND ug/L 0.500 0.168 1 11/18/2114:40 11/19/2108:14 8001-35-2 86.2 % 10.0-128 1 11/18/2114:40 11/19/2108:14 2051-24-3 111 % 10.0-127 1 11/18/2114:40 11/19/2108:14 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/17/2111:48 11/18/2123:51 94-75-7 ND ug/L 2.00 0.344 1 11/17/2111:48 11/18/2123:51 127-20-8 ND ug/L 2.00 0.302 1 11/17/2111:48 11/18/2123:51 94-82-6 ND ug/L 2.00 0.245 1 11/17/2111:48 11/18/2123:51 1918-00-9 ND ug/L 2.00 1.04 1 11/17/2111:48 11/18/2123:51 15165-67-0 ND ug/L 2.00 0.250 1 11/17/2111:48 11/18/2123:51 88-85-7 ND ug/L 100 13.1 1 11/17/2111:48 11/18/2123:51 94-74-6 ND ug/L 100 66.0 1 11/17/2111:48 11/18/2123:51 7085-19-0 ND ug/L 2.00 0.258 1 11/17/2111:48 11/18/2123:51 93-76-5 ND ug/L 2.00 0.335 1 11/17/2111:48 11/18/2123:51 93-72-1 107 % 14.0-158 1 11/17/2111:48 11/18/2123:51 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.50 0.47 1 11/15/2107:08 11/16/2115:37 12674-11-2 ND ug/L 0.50 0.45 1 11/15/2107:08 11/16/2115:37 11104-28-2 ND ug/L 0.50 0.36 1 11/15/2107:08 11/16/2115:37 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 66 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-14 Lab ID: 92572199013 Collected: 11/11/21 12:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.50 0.26 1 11/15/21 07:08 11/16/21 15:37 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 0.40 1 11/15/21 07:08 11/16/21 15:37 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.50 0.25 1 11/15/21 07:08 11/16/21 15:37 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 0.42 1 11/15/21 07:08 11/16/21 15:37 11096-82-5 Surrogates Decachlorobiphenyl (S) 119 % 10-181 1 11/15/21 07:08 11/16/21 15:37 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/29/2118:25 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:25 7440-38-2 Barium 272 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:25 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/29/2118:25 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/29/2118:25 7440-43-9 Chromium 4.1J ug/L 5.0 3.7 1 11/16/2114:13 11/29/2118:25 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/29/2118:25 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/29/2118:25 7440-50-8 Iron 1780 ug/L 50.0 41.5 1 11/16/2114:13 11/29/2118:25 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/29/2118:25 7439-92-1 Manganese 134 ug/L 5.0 3.4 1 11/16/2114:13 11/29/2118:25 7439-96-5 Nickel 9.6 ug/L 5.0 3.5 1 11/16/2114:13 11/29/2118:25 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/29/2118:25 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/29/2118:25 7440-22-4 Sodium 18800 ug/L 5000 611 1 11/16/2114:13 11/29/2118:25 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/29/2118:25 7440-31-5 Vanadium 5.2 ug/L 5.0 3.9 1 11/16/2114:13 11/29/2118:25 7440-62-2 Zinc 11.3 ug/L 10.0 9.5 1 11/16/2114:13 11/29/2118:25 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:38 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 8.3 2.2 1 11/15/21 06:49 11/16/21 18:26 56-55-3 Chrysene ND ug/L 8.3 2.3 1 11/15/21 06:49 11/16/21 18:26 218-01-9 Dibenz(a,h)anthracene ND ug/L 8.3 2.5 1 11/15/21 06:49 11/16/21 18:26 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 3.1 1 11/15/21 06:49 11/16/21 18:26 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 8.3 2.4 1 11/15/21 06:49 11/16/21 18:26 193-39-5 Surrogates Nitrobenzene-d5 (S) 67 % 10-144 1 11/15/21 06:49 11/16/21 18:26 4165-60-0 2-Fluorobiphenyl (S) 61 % 10-130 1 11/15/21 06:49 11/16/21 18:26 321-60-8 Terphenyl-d14 (S) 80 % 34-163 1 11/15/21 06:49 11/16/21 18:26 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 67 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-14 Lab ID: 92572199013 Collected: 11/11/21 12:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2108:50 67-64-1 ND ug/L 10.0 1.8 1 11/16/2108:50 107-13-1 ND ug/L 1.0 0.34 1 11/16/2108:50 71-43-2 ND ug/L 1.0 0.47 1 11/16/2108:50 74-97-5 ND ug/L 1.0 0.31 1 11/16/2108:50 75-27-4 ND ug/L 1.0 0.34 1 11/16/2108:50 75-25-2 ND ug/L 2.0 1.7 1 11/16/2108:50 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2108:50 78-93-3 ND ug/L 2.0 0.73 1 11/16/2108:50 75-15-0 ND ug/L 1.0 0.33 1 11/16/2108:50 56-23-5 ND ug/L 1.0 0.28 1 11/16/2108:50 108-90-7 ND ug/L 1.0 0.65 1 11/16/2108:50 75-00-3 ND ug/L 1.0 0.43 1 11/16/2108:50 67-66-3 ND ug/L 1.0 0.54 1 11/16/2108:50 74-87-3 ND ug/L 2.0 0.34 1 11/16/2108:50 96-12-8 ND ug/L 1.0 0.36 1 11/16/2108:50 124-48-1 ND ug/L 1.0 0.27 1 11/16/2108:50 106-93-4 ND ug/L 1.0 0.39 1 11/16/2108:50 74-95-3 ND ug/L 1.0 0.34 1 11/16/2108:50 95-50-1 ND ug/L 1.0 0.33 1 11/16/2108:50 106-46-7 ND ug/L 1.0 0.56 1 11/16/2108:50 110-57-6 3.7 ug/L 1.0 0.35 1 11/16/2108:50 75-71-8 ND ug/L 1.0 0.37 1 11/16/2108:50 75-34-3 ND ug/L 1.0 0.32 1 11/16/2108:50 107-06-2 ND ug/L 1.0 0.35 1 11/16/2108:50 75-35-4 ND ug/L 1.0 0.38 1 11/16/2108:50 156-59-2 ND ug/L 1.0 0.40 1 11/16/2108:50 156-60-5 ND ug/L 1.0 0.36 1 11/16/2108:50 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 08:50 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2108:50 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2108:50 100-41-4 ND ug/L 5.0 0.48 1 11/16/2108:50 591-78-6 ND ug/L 20.0 9.7 1 11/16/2108:50 74-88-4 ND ug/L 5.0 2.0 1 11/16/2108:50 75-09-2 ND ug/L 5.0 2.7 1 11/16/2108:50 108-10-1 ND ug/L 1.0 0.29 1 11/16/2108:50 100-42-5 ND ug/L 1.0 0.31 1 11/16/2108:50 630-20-6 ND ug/L 1.0 0.22 1 11/16/2108:50 79-34-5 0.55.11 ug/L 1.0 0.29 1 11/16/2108:50 127-18-4 ND ug/L 10.0 3.5 1 11/16/2108:50 109-99-9 ND ug/L 1.0 0.48 1 11/16/2108:50 108-88-3 ND ug/L 1.0 0.33 1 11/16/2108:50 71-55-6 ND ug/L 1.0 0.32 1 11/16/2108:50 79-00-5 ND ug/L 1.0 0.38 1 11/16/2108:50 79-01-6 1.7 ug/L 1.0 0.30 1 11/16/2108:50 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 68 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-14 Lab ID: 92572199013 Collected: 11/11/21 12:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 08:50 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 08:50 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 08:50 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 08:50 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 08:50 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 08:50 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 08:50 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 11/16/21 08:50 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 11/15/21 21:03 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 111 % 70-130 1 11/15/21 21:03 17060-07-0 Toluene-d8 (S) 111 % 66-133 1 11/15/21 21:03 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 63000 ug/L 5000 5000 1 11/24/21 10:18 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 160000 ug/L 25000 25000 1 11/16/21 10:26 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:39 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 11/14/2102:34 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 3650 ug/L 1000 500 1 11/24/2111:21 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide 7.8J ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:28 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 69 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-15 Lab ID: 92572199014 Collected: 11/08/21 11:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2100:56 309-00-2 ND ug/L 0.0500 0.0172 1 11/15/2106:10 11/16/2100:56 319-84-6 ND ug/L 0.0500 0.0208 1 11/15/2106:10 11/16/2100:56 319-85-7 ND ug/L 0.0500 0.0150 1 11/15/2106:10 11/16/2100:56 319-86-8 ND ug/L 0.0500 0.0209 1 11/15/2106:10 11/16/2100:56 58-89-9 ND ug/L 5.00 0.0198 1 11/15/2106:10 11/16/2100:56 57-74-9 ND ug/L 0.0500 0.0177 1 11/15/2106:10 11/16/2100:56 72-54-8 ND ug/L 0.0500 0.0154 1 11/15/2106:10 11/16/2100:56 72-55-9 ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2100:56 50-29-3 ND ug/L 0.0500 0.0162 1 11/15/2106:10 11/16/2100:56 60-57-1 ND ug/L 0.0500 0.0160 1 11/15/2106:10 11/16/2100:56 959-98-8 ND ug/L 0.0500 0.0164 1 11/15/2106:10 11/16/2100:56 33213-65-9 ND ug/L 0.0500 0.0217 1 11/15/2106:10 11/16/2100:56 1031-07-8 ND ug/L 0.0500 0.0161 1 11/15/2106:10 11/16/2100:56 72-20-8 ND ug/L 0.0500 0.0237 1 11/15/2106:10 11/16/2100:56 7421-93-4 ND ug/L 0.0500 0.0219 1 11/15/2106:10 11/16/2100:56 53494-70-5 ND ug/L 0.0500 0.0176 1 11/15/2106:10 11/16/2100:56 118-74-1 ND ug/L 0.0500 0.0148 1 11/15/2106:10 11/16/2100:56 76-44-8 ND ug/L 0.0500 0.0183 1 11/15/2106:10 11/16/2100:56 1024-57-3 ND ug/L 0.0500 0.0193 1 11/15/2106:10 11/16/2100:56 72-43-5 ND ug/L 0.500 0.168 1 11/15/2106:10 11/16/2100:56 8001-35-2 36.0 % 10.0-128 1 11/15/2106:10 11/16/2100:56 2051-24-3 70.1 % 10.0-127 1 11/15/2106:10 11/16/2100:56 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/15/2108:09 11/16/2121:24 94-75-7 ND ug/L 2.00 0.344 1 11/15/2108:09 11/16/2121:24 127-20-8 ND ug/L 2.00 0.302 1 11/15/2108:09 11/16/2121:24 94-82-6 ND ug/L 2.00 0.245 1 11/15/2108:09 11/16/2121:24 1918-00-9 ND ug/L 2.00 1.04 1 11/15/2108:09 11/16/2121:24 15165-67-0 ND ug/L 2.00 0.250 1 11/15/2108:09 11/16/2121:24 88-85-7 ND ug/L 100 13.1 1 11/15/2108:09 11/16/2121:24 94-74-6 ND ug/L 100 66.0 1 11/15/2108:09 11/16/2121:24 7085-19-0 ND ug/L 2.00 0.258 1 11/15/2108:09 11/16/2121:24 93-76-5 ND ug/L 2.00 0.335 1 11/15/2108:09 11/16/2121:24 93-72-1 102 % 14.0-158 1 11/15/2108:09 11/16/2121:24 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.42 0.39 1 11/15/2107:08 11/16/2115:48 12674-11-2 ND ug/L 0.42 0.38 1 11/15/2107:08 11/16/2115:48 11104-28-2 ND ug/L 0.42 0.30 1 11/15/2107:08 11/16/2115:48 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. LO Page 70 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-15 Lab ID: 92572199014 Collected: 11/08/21 11:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.42 0.22 1 11/15/21 07:08 11/16/21 15:48 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.42 0.34 1 11/15/21 07:08 11/16/21 15:48 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.42 0.21 1 11/15/21 07:08 11/16/21 15:48 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.42 0.35 1 11/15/21 07:08 11/16/21 15:48 11096-82-5 Surrogates Decachlorobiphenyl (S) 145 % 10-181 1 11/15/21 07:08 11/16/21 15:48 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/30/2100:13 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:13 7440-38-2 Barium 16.1 ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:13 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/30/2100:13 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/30/2100:13 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/30/2100:13 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/30/2100:13 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/30/2100:13 7440-50-8 Iron 166 ug/L 50.0 41.5 1 11/16/2114:13 11/30/2100:13 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/30/2100:13 7439-92-1 Manganese 314 ug/L 5.0 3.4 1 11/16/2114:13 11/30/2100:13 7439-96-5 Nickel ND ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:13 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:13 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/30/2100:13 7440-22-4 Sodium 15700 ug/L 5000 611 1 11/16/2114:13 11/30/2100:13 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/30/2100:13 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 11/16/2114:13 11/30/2100:13 7440-62-2 Zinc 11.2 ug/L 10.0 9.5 1 11/16/2114:13 11/30/2100:13 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:41 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 9.1 2.4 1 11/15/21 06:49 11/15/21 16:30 56-55-3 Chrysene ND ug/L 9.1 2.5 1 11/15/21 06:49 11/15/21 16:30 218-01-9 Dibenz(a,h)anthracene ND ug/L 9.1 2.7 1 11/15/21 06:49 11/15/21 16:30 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.5 3.4 1 11/15/21 06:49 11/15/21 16:30 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 9.1 2.6 1 11/15/21 06:49 11/15/21 16:30 193-39-5 Surrogates Nitrobenzene-d5 (S) 76 % 10-144 1 11/15/21 06:49 11/15/21 16:30 4165-60-0 2-Fluorobiphenyl (S) 61 % 10-130 1 11/15/21 06:49 11/15/21 16:30 321-60-8 Terphenyl-d14 (S) 79 % 34-163 1 11/15/21 06:49 11/15/21 16:30 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 71 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-15 Lab ID: 92572199014 Collected: 11/08/21 11:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/13/2119:56 67-64-1 ND ug/L 10.0 1.8 1 11/13/2119:56 107-13-1 ND ug/L 1.0 0.34 1 11/13/2119:56 71-43-2 ND ug/L 1.0 0.47 1 11/13/2119:56 74-97-5 ND ug/L 1.0 0.31 1 11/13/2119:56 75-27-4 ND ug/L 1.0 0.34 1 11/13/2119:56 75-25-2 ND ug/L 2.0 1.7 1 11/13/2119:56 74-83-9 ND ug/L 5.0 4.0 1 11/13/2119:56 78-93-3 ND ug/L 2.0 0.73 1 11/13/2119:56 75-15-0 ND ug/L 1.0 0.33 1 11/13/2119:56 56-23-5 ND ug/L 1.0 0.28 1 11/13/2119:56 108-90-7 ND ug/L 1.0 0.65 1 11/13/2119:56 75-00-3 ND ug/L 1.0 0.43 1 11/13/2119:56 67-66-3 ND ug/L 1.0 0.54 1 11/13/2119:56 74-87-3 ND ug/L 2.0 0.34 1 11/13/2119:56 96-12-8 ND ug/L 1.0 0.36 1 11/13/2119:56 124-48-1 ND ug/L 1.0 0.27 1 11/13/2119:56 106-93-4 ND ug/L 1.0 0.39 1 11/13/2119:56 74-95-3 ND ug/L 1.0 0.34 1 11/13/2119:56 95-50-1 ND ug/L 1.0 0.33 1 11/13/2119:56 106-46-7 ND ug/L 1.0 0.56 1 11/13/2119:56 110-57-6 ND ug/L 1.0 0.35 1 11/13/2119:56 75-71-8 ND ug/L 1.0 0.37 1 11/13/2119:56 75-34-3 ND ug/L 1.0 0.32 1 11/13/2119:56 107-06-2 ND ug/L 1.0 0.35 1 11/13/2119:56 75-35-4 ND ug/L 1.0 0.38 1 11/13/2119:56 156-59-2 ND ug/L 1.0 0.40 1 11/13/2119:56 156-60-5 ND ug/L 1.0 0.36 1 11/13/2119:56 78-87-5 ND ug/L 1.0 0.36 1 11 /13/21 19:56 10061-01-5 ND ug/L 1.0 0.36 1 11/13/2119:56 10061-02-6 ND ug/L 1.0 0.30 1 11/13/2119:56 100-41-4 ND ug/L 5.0 0.48 1 11/13/2119:56 591-78-6 ND ug/L 20.0 9.7 1 11/13/2119:56 74-88-4 ND ug/L 5.0 2.0 1 11/13/2119:56 75-09-2 ND ug/L 5.0 2.7 1 11/13/2119:56 108-10-1 ND ug/L 1.0 0.29 1 11/13/2119:56 100-42-5 ND ug/L 1.0 0.31 1 11/13/2119:56 630-20-6 ND ug/L 1.0 0.22 1 11/13/2119:56 79-34-5 ND ug/L 1.0 0.29 1 11/13/2119:56 127-18-4 4.8.1 ug/L 10.0 3.5 1 11/13/2119:56 109-99-9 ND ug/L 1.0 0.48 1 11/13/2119:56 108-88-3 ND ug/L 1.0 0.33 1 11/13/2119:56 71-55-6 ND ug/L 1.0 0.32 1 11/13/2119:56 79-00-5 ND ug/L 1.0 0.38 1 11/13/2119:56 79-01-6 ND ug/L 1.0 0.30 1 11/13/2119:56 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 Page 72 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: MW-15 Lab ID: 92572199014 Collected: 11/08/21 11:50 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/13/21 19:56 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/13/21 19:56 108-05-4 v1 Vinyl chloride ND ug/L 1.0 0.39 1 11/13/21 19:56 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/13/21 19:56 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/13/21 19:56 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 11/13/21 19:56 460-00-4 1,2-Dichloroethane-d4 (S) 96 % 70-130 1 11/13/21 19:56 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 11/13/21 19:56 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 11/15/21 21:22 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 110 % 70-130 1 11/15/21 21:22 17060-07-0 Toluene-d8 (S) 111 % 66-133 1 11/15/21 21:22 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 104000 ug/L 5000 5000 1 11/16/21 16:05 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 247000 ug/L 25000 25000 1 11/14/21 17:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2102:59 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 25500 ug/L 1000 500 1 11/14/2102:50 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 37700 ug/L 5000 2500 5 11/24/2111:22 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/17/2113:31 11/18/2110:33 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 73 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-1 Lab ID: 92572199015 Collected: 11/11/21 11:40 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/30/2100:32 7440-36-0 Arsenic 8.5J ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:32 7440-38-2 Barium 535 ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:32 7440-39-3 Beryllium 2.0 ug/L 1.0 0.70 1 11/16/2114:13 11/30/2100:32 7440-41-7 Cadmium 0.48J ug/L 1.0 0.40 1 11/16/2114:13 11/30/2100:32 7440-43-9 Chromium 24.8 ug/L 5.0 3.7 1 11/16/2114:13 11/30/2100:32 7440-47-3 Cobalt 13.0 ug/L 5.0 3.6 1 11/16/2114:13 11/30/2100:32 7440-48-4 Copper 13.8 ug/L 5.0 4.3 1 11/16/2114:13 11/30/2100:32 7440-50-8 Iron 69000 ug/L 50.0 41.5 1 11/16/2114:13 11/30/2100:32 7439-89-6 Lead 18.3 ug/L 5.0 4.5 1 11/16/2114:13 11/30/2100:32 7439-92-1 Manganese 1250 ug/L 5.0 3.4 1 11/16/2114:13 11/30/2100:32 7439-96-5 Nickel 12.2 ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:32 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:32 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/30/2100:32 7440-22-4 Sodium 17900 ug/L 5000 611 1 11/16/2114:13 11/30/2100:32 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/30/2100:32 7440-31-5 Vanadium 65.8 ug/L 5.0 3.9 1 11/16/2114:13 11/30/2100:32 7440-62-2 Zinc 70.2 ug/L 10.0 9.5 1 11/16/2114:13 11/30/2100:32 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 12/02/2021 09:16 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:43 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/16/21 06:24 67-64-1 1.8 1 11/16/21 06:24 107-13-1 0.34 1 11/16/21 06:24 71-43-2 0.47 1 11/16/21 06:24 74-97-5 0.31 1 11/16/21 06:24 75-27-4 0.34 1 11/16/21 06:24 75-25-2 1.7 1 11/16/21 06:24 74-83-9 4.0 1 11/16/21 06:24 78-93-3 0.73 1 11/16/21 06:24 75-15-0 0.33 1 11/16/21 06:24 56-23-5 0.28 1 11/16/21 06:24 108-90-7 0.65 1 11/16/21 06:24 75-00-3 0.43 1 11/16/21 06:24 67-66-3 0.54 1 11/16/21 06:24 74-87-3 0.34 1 11/16/21 06:24 96-12-8 0.36 1 11/16/21 06:24 124-48-1 0.27 1 11/16/21 06:24 106-93-4 0.39 1 11/16/21 06:24 74-95-3 0.34 1 11/16/21 06:24 95-50-1 0.33 1 11/16/21 06:24 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 74 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-1 Lab ID: 92572199015 Collected: 11/11/21 11:40 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.56 1 11/16/2106:24 110-57-6 ND ug/L 1.0 0.35 1 11/16/2106:24 75-71-8 ND ug/L 1.0 0.37 1 11/16/2106:24 75-34-3 ND ug/L 1.0 0.32 1 11/16/2106:24 107-06-2 ND ug/L 1.0 0.35 1 11/16/2106:24 75-35-4 ND ug/L 1.0 0.38 1 11/16/2106:24 156-59-2 ND ug/L 1.0 0.40 1 11/16/2106:24 156-60-5 ND ug/L 1.0 0.36 1 11/16/2106:24 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 06:24 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2106:24 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2106:24 100-41-4 ND ug/L 5.0 0.48 1 11/16/2106:24 591-78-6 ND ug/L 20.0 9.7 1 11/16/2106:24 74-88-4 ND ug/L 5.0 2.0 1 11/16/2106:24 75-09-2 ND ug/L 5.0 2.7 1 11/16/2106:24 108-10-1 ND ug/L 1.0 0.29 1 11/16/2106:24 100-42-5 ND ug/L 1.0 0.31 1 11/16/2106:24 630-20-6 ND ug/L 1.0 0.22 1 11/16/2106:24 79-34-5 ND ug/L 1.0 0.29 1 11/16/2106:24 127-18-4 ND ug/L 10.0 3.5 1 11/16/2106:24 109-99-9 ND ug/L 1.0 0.48 1 11/16/2106:24 108-88-3 ND ug/L 1.0 0.33 1 11/16/2106:24 71-55-6 ND ug/L 1.0 0.32 1 11/16/2106:24 79-00-5 ND ug/L 1.0 0.38 1 11/16/2106:24 79-01-6 ND ug/L 1.0 0.30 1 11/16/2106:24 75-69-4 ND ug/L 1.0 0.26 1 11/16/2106:24 96-18-4 ND ug/L 2.0 1.3 1 11/16/2106:24 108-05-4 ND ug/L 1.0 0.39 1 11/16/2106:24 75-01-4 ND ug/L 2.0 0.71 1 11/16/2106:24 179601-23-1 ND ug/L 1.0 0.34 1 11/16/2106:24 95-47-6 97 % 70-130 1 11/16/2106:24 460-00-4 91 % 70-130 1 11/16/2106:24 17060-07-0 100 % 70-130 1 11/16/2106:24 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/15/2121:41 123-91-1 109 % 70-130 1 11/15/2121:41 17060-07-0 110 % 66-133 1 11/15/2121:41 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 71400 ug/L 5000 5000 1 11/24/21 10:31 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 75 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-1 Parameters Lab ID: 92572199015 Collected: Report Results Units Limit 11/11/21 11:40 MDL DF Received: 11/12/21 14:00 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 199000 ug/L 25000 25000 1 11/16/21 10:26 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:40 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 7440 ug/L 1000 500 1 11/14/2103:05 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 24400 ug/L 1000 500 1 11/24/2111:23 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:29 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 76 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-3 Lab ID: 92572199016 Collected: 11/08/21 14:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/30/2100:36 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:36 7440-38-2 Barium 278 ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:36 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/30/2100:36 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/30/2100:36 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/30/2100:36 7440-47-3 Cobalt 4.5J ug/L 5.0 3.6 1 11/16/2114:13 11/30/2100:36 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/30/2100:36 7440-50-8 Iron 26700 ug/L 50.0 41.5 1 11/16/2114:13 11/30/2100:36 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/30/2100:36 7439-92-1 Manganese 5640 ug/L 5.0 3.4 1 11/16/2114:13 11/30/2100:36 7439-96-5 Nickel 7.4 ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:36 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:36 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/30/2100:36 7440-22-4 Sodium 26100 ug/L 5000 611 1 11/16/2114:13 11/30/2100:36 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/30/2100:36 7440-31-5 Vanadium 35.3 ug/L 5.0 3.9 1 11/16/2114:13 11/30/2100:36 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/30/2100:36 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 12/02/2021 09:16 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:45 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/13/2118:45 67-64-1 1.8 1 11 /13/21 18:45 107-13-1 0.34 1 11 /13/21 18:45 71-43-2 0.47 1 11/13/2118:45 74-97-5 0.31 1 11/13/2118:45 75-27-4 0.34 1 11/13/2118:45 75-25-2 1.7 1 11/13/2118:45 74-83-9 4.0 1 11/13/2118:45 78-93-3 0.73 1 11/13/2118:45 75-15-0 0.33 1 11/13/2118:45 56-23-5 0.28 1 11 /13/21 18:45 108-90-7 0.65 1 11/13/2118:45 75-00-3 0.43 1 11/13/2118:45 67-66-3 0.54 1 11/13/2118:45 74-87-3 0.34 1 11/13/2118:45 96-12-8 0.36 1 11 /13/21 18:45 124-48-1 0.27 1 11 /13/21 18:45 106-93-4 0.39 1 11/13/2118:45 74-95-3 0.34 1 11/13/2118:45 95-50-1 0.33 1 11 /13/21 18:45 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 77 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-3 Lab ID: 92572199016 Collected: 11/08/21 14:30 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.56 1 11/13/2118:45 110-57-6 v1 ND ug/L 1.0 0.35 1 11/13/2118:45 75-71-8 ND ug/L 1.0 0.37 1 11/13/2118:45 75-34-3 ND ug/L 1.0 0.32 1 11/13/2118:45 107-06-2 ND ug/L 1.0 0.35 1 11/13/2118:45 75-35-4 ND ug/L 1.0 0.38 1 11/13/2118:45 156-59-2 ND ug/L 1.0 0.40 1 11/13/2118:45 156-60-5 ND ug/L 1.0 0.36 1 11/13/2118:45 78-87-5 ND ug/L 1.0 0.36 1 11 /13/21 18:45 10061-01-5 ND ug/L 1.0 0.36 1 11/13/2118:45 10061-02-6 ND ug/L 1.0 0.30 1 11/13/2118:45 100-41-4 ND ug/L 5.0 0.48 1 11/13/2118:45 591-78-6 ND ug/L 20.0 9.7 1 11/13/2118:45 74-88-4 ND ug/L 5.0 2.0 1 11/13/2118:45 75-09-2 ND ug/L 5.0 2.7 1 11/13/2118:45 108-10-1 ND ug/L 1.0 0.29 1 11/13/2118:45 100-42-5 ND ug/L 1.0 0.31 1 11/13/2118:45 630-20-6 ND ug/L 1.0 0.22 1 11/13/2118:45 79-34-5 ND ug/L 1.0 0.29 1 11/13/2118:45 127-18-4 ND ug/L 10.0 3.5 1 11/13/2118:45 109-99-9 ND ug/L 1.0 0.48 1 11/13/2118:45 108-88-3 ND ug/L 1.0 0.33 1 11/13/2118:45 71-55-6 ND ug/L 1.0 0.32 1 11/13/2118:45 79-00-5 ND ug/L 1.0 0.38 1 11/13/2118:45 79-01-6 ND ug/L 1.0 0.30 1 11/13/2118:45 75-69-4 ND ug/L 1.0 0.26 1 11/13/2118:45 96-18-4 ND ug/L 2.0 1.3 1 11/13/2118:45 108-05-4 v1 ND ug/L 1.0 0.39 1 11/13/2118:45 75-01-4 ND ug/L 2.0 0.71 1 11/13/2118:45 179601-23-1 ND ug/L 1.0 0.34 1 11/13/2118:45 95-47-6 97 % 70-130 1 11/13/2118:45 460-00-4 97 % 70-130 1 11/13/2118:45 17060-07-0 102 % 70-130 1 11/13/2118:45 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 0.86 1 11/15/2122:01 123-91-1 112 % 70-130 1 11/15/2122:01 17060-07-0 109 % 66-133 1 11/15/2122:01 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 379000 ug/L 5000 5000 1 11/16/2116:13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 78 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-3 Parameters Lab ID: 92572199016 Collected: Report Results Units Limit 11/08/21 14:30 MDL DF Received: 11/12/21 14:00 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 477000 ug/L 25000 25000 1 11/14/21 17:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:00 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 21800 ug/L 1000 500 1 11/14/2103:21 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 25100 ug/L 1000 500 1 11/24/2111:23 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/17/2113:31 11/18/2110:35 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 79 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-4 Lab ID: 92572199017 Collected: 11/08/21 15:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/30/2100:39 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:39 7440-38-2 Barium 202 ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:39 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/30/2100:39 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/30/2100:39 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/30/2100:39 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/30/2100:39 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/30/2100:39 7440-50-8 Iron 3110 ug/L 50.0 41.5 1 11/16/21 14:13 11/30/21 00:39 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/30/2100:39 7439-92-1 Manganese 6400 ug/L 5.0 3.4 1 11/16/2114:13 11/30/2100:39 7439-96-5 Nickel 8.8 ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:39 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:39 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/30/2100:39 7440-22-4 Sodium 42400 ug/L 5000 611 1 11/16/2114:13 11/30/2100:39 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/30/2100:39 7440-31-5 Vanadium 38.4 ug/L 5.0 3.9 1 11/16/2114:13 11/30/2100:39 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/30/2100:39 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 12/02/2021 09:16 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:53 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 5.1 1 11/16/21 06:06 67-64-1 1.8 1 11/16/21 06:06 107-13-1 0.34 1 11/16/21 06:06 71-43-2 0.47 1 11/16/21 06:06 74-97-5 0.31 1 11/16/21 06:06 75-27-4 0.34 1 11/16/21 06:06 75-25-2 1.7 1 11/16/21 06:06 74-83-9 4.0 1 11/16/21 06:06 78-93-3 0.73 1 11/16/21 06:06 75-15-0 0.33 1 11/16/21 06:06 56-23-5 0.28 1 11/16/21 06:06 108-90-7 0.65 1 11/16/21 06:06 75-00-3 0.43 1 11/16/21 06:06 67-66-3 0.54 1 11/16/21 06:06 74-87-3 0.34 1 11/16/21 06:06 96-12-8 0.36 1 11/16/21 06:06 124-48-1 0.27 1 11/16/21 06:06 106-93-4 0.39 1 11/16/21 06:06 74-95-3 0.34 1 11/16/21 06:06 95-50-1 0.33 1 11/16/21 06:06 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 80 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-4 Lab ID: 92572199017 Collected: 11/08/21 15:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.56 1 11/16/2106:06 110-57-6 ND ug/L 1.0 0.35 1 11/16/2106:06 75-71-8 ND ug/L 1.0 0.37 1 11/16/2106:06 75-34-3 ND ug/L 1.0 0.32 1 11/16/2106:06 107-06-2 ND ug/L 1.0 0.35 1 11/16/2106:06 75-35-4 ND ug/L 1.0 0.38 1 11/16/2106:06 156-59-2 ND ug/L 1.0 0.40 1 11/16/2106:06 156-60-5 ND ug/L 1.0 0.36 1 11/16/2106:06 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 06:06 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2106:06 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2106:06 100-41-4 ND ug/L 5.0 0.48 1 11/16/2106:06 591-78-6 ND ug/L 20.0 9.7 1 11/16/2106:06 74-88-4 ND ug/L 5.0 2.0 1 11/16/2106:06 75-09-2 ND ug/L 5.0 2.7 1 11/16/2106:06 108-10-1 ND ug/L 1.0 0.29 1 11/16/2106:06 100-42-5 ND ug/L 1.0 0.31 1 11/16/2106:06 630-20-6 ND ug/L 1.0 0.22 1 11/16/2106:06 79-34-5 ND ug/L 1.0 0.29 1 11/16/2106:06 127-18-4 9.6J ug/L 10.0 3.5 1 11/16/2106:06 109-99-9 ND ug/L 1.0 0.48 1 11/16/2106:06 108-88-3 ND ug/L 1.0 0.33 1 11/16/2106:06 71-55-6 ND ug/L 1.0 0.32 1 11/16/2106:06 79-00-5 ND ug/L 1.0 0.38 1 11/16/2106:06 79-01-6 ND ug/L 1.0 0.30 1 11/16/2106:06 75-69-4 ND ug/L 1.0 0.26 1 11/16/2106:06 96-18-4 ND ug/L 2.0 1.3 1 11/16/2106:06 108-05-4 ND ug/L 1.0 0.39 1 11/16/2106:06 75-01-4 ND ug/L 2.0 0.71 1 11/16/2106:06 179601-23-1 ND ug/L 1.0 0.34 1 11/16/2106:06 95-47-6 97 % 70-130 1 11/16/2106:06 460-00-4 89 % 70-130 1 11/16/2106:06 17060-07-0 100 % 70-130 1 11/16/2106:06 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 7.4 ug/L 2.0 0.86 1 11/15/2122:20 123-91-1 108 % 70-130 1 11/15/2122:20 17060-07-0 108 % 66-133 1 11/15/2122:20 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 453000 ug/L 5000 5000 1 11/17/2109:42 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 81 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-4 Parameters Lab ID: 92572199017 Collected: Report Results Units Limit 11/08/21 15:20 MDL DF Received: 11/12/21 14:00 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 644000 ug/L 25000 25000 1 11/14/21 17:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:00 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 66700 ug/L 1000 500 1 11/14/2103:36 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 50000 ug/L 3000 1500 3 11/24/2111:39 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/17/2113:31 11/18/2110:37 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 82 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-2 Lab ID: 92572199018 Collected: 11/09/21 12:40 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/30/2100:42 7440-36-0 Arsenic 8.3J ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:42 7440-38-2 Barium 92.5 ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:42 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/30/2100:42 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/30/2100:42 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/30/2100:42 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/30/2100:42 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/30/2100:42 7440-50-8 Iron 1500 ug/L 50.0 41.5 1 11/16/2114:13 11/30/2100:42 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/30/2100:42 7439-92-1 Manganese 549 ug/L 5.0 3.4 1 11/16/2114:13 11/30/2100:42 7439-96-5 Nickel 3.5J ug/L 5.0 3.5 1 11/16/21 14:13 11/30/21 00:42 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:42 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/30/2100:42 7440-22-4 Sodium 15300 ug/L 5000 611 1 11/16/2114:13 11/30/2100:42 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/30/2100:42 7440-31-5 Vanadium 4.5J ug/L 5.0 3.9 1 11/16/2114:13 11/30/2100:42 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/30/2100:42 7440-66-6 7470 Mercury Mercury 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Date: 12/02/2021 09:16 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:55 7439-97-6 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 9.1 2.4 1 11/15/2104:46 11/16/2120:00 56-55-3 ND ug/L 9.1 2.5 1 11/15/2104:46 11/16/2120:00 218-01-9 ND ug/L 9.1 2.7 1 11/15/2104:46 11/16/2120:00 53-70-3 ND ug/L 5.5 3.4 1 11/15/2104:46 11/16/2120:00 117-81-7 ND ug/L 9.1 2.6 1 11/15/2104:46 11/16/2120:00 193-39-5 61 % 10-144 47 % 10-130 56 % 34-163 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 1 11/15/2104:46 11/16/2120:00 4165-60-0 1 11/15/2104:46 11/16/2120:00 321-60-8 1 11 /15/21 04:46 11/16/21 20:00 1718-51-0 5.1 1 11/16/21 05:48 67-64-1 1.8 1 11/16/21 05:48 107-13-1 0.34 1 11/16/21 05:48 71-43-2 0.47 1 11/16/21 05:48 74-97-5 0.31 1 11/16/21 05:48 75-27-4 0.34 1 11/16/21 05:48 75-25-2 1.7 1 11/16/21 05:48 74-83-9 4.0 1 11/16/21 05:48 78-93-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 Page 83 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-2 Lab ID: 92572199018 Collected: 11/09/21 12:40 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 2.0 0.73 1 11/16/2105:48 75-15-0 ND ug/L 1.0 0.33 1 11/16/2105:48 56-23-5 ND ug/L 1.0 0.28 1 11/16/2105:48 108-90-7 ND ug/L 1.0 0.65 1 11/16/2105:48 75-00-3 ND ug/L 1.0 0.43 1 11/16/2105:48 67-66-3 ND ug/L 1.0 0.54 1 11/16/2105:48 74-87-3 ND ug/L 2.0 0.34 1 11/16/2105:48 96-12-8 ND ug/L 1.0 0.36 1 11/16/2105:48 124-48-1 ND ug/L 1.0 0.27 1 11/16/2105:48 106-93-4 ND ug/L 1.0 0.39 1 11/16/2105:48 74-95-3 ND ug/L 1.0 0.34 1 11/16/2105:48 95-50-1 ND ug/L 1.0 0.33 1 11/16/2105:48 106-46-7 ND ug/L 1.0 0.56 1 11/16/2105:48 110-57-6 ND ug/L 1.0 0.35 1 11/16/2105:48 75-71-8 ND ug/L 1.0 0.37 1 11/16/2105:48 75-34-3 ND ug/L 1.0 0.32 1 11/16/2105:48 107-06-2 ND ug/L 1.0 0.35 1 11/16/2105:48 75-35-4 ND ug/L 1.0 0.38 1 11/16/2105:48 156-59-2 ND ug/L 1.0 0.40 1 11/16/2105:48 156-60-5 ND ug/L 1.0 0.36 1 11/16/2105:48 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 05:48 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2105:48 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2105:48 100-41-4 ND ug/L 5.0 0.48 1 11/16/2105:48 591-78-6 ND ug/L 20.0 9.7 1 11/16/2105:48 74-88-4 ND ug/L 5.0 2.0 1 11/16/2105:48 75-09-2 ND ug/L 5.0 2.7 1 11/16/2105:48 108-10-1 ND ug/L 1.0 0.29 1 11/16/2105:48 100-42-5 ND ug/L 1.0 0.31 1 11/16/2105:48 630-20-6 ND ug/L 1.0 0.22 1 11/16/2105:48 79-34-5 ND ug/L 1.0 0.29 1 11/16/2105:48 127-18-4 ND ug/L 10.0 3.5 1 11/16/2105:48 109-99-9 ND ug/L 1.0 0.48 1 11/16/2105:48 108-88-3 ND ug/L 1.0 0.33 1 11/16/2105:48 71-55-6 ND ug/L 1.0 0.32 1 11/16/2105:48 79-00-5 ND ug/L 1.0 0.38 1 11/16/2105:48 79-01-6 ND ug/L 1.0 0.30 1 11/16/2105:48 75-69-4 ND ug/L 1.0 0.26 1 11/16/2105:48 96-18-4 ND ug/L 2.0 1.3 1 11/16/2105:48 108-05-4 ND ug/L 1.0 0.39 1 11/16/2105:48 75-01-4 ND ug/L 2.0 0.71 1 11/16/2105:48 179601-23-1 ND ug/L 1.0 0.34 1 11/16/2105:48 95-47-6 98 % 70-130 1 11/16/2105:48 460-00-4 91 % 70-130 1 11/16/2105:48 17060-07-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 84 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: SW-2 Lab ID: 92572199018 Collected: 11/09/21 12:40 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Surrogates Toluene-d8 (S) 100 % 70-130 1 11/16/21 05:48 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 3.3 ug/L 2.0 0.86 1 11/15/21 22:39 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 11/15/21 22:39 17060-07-0 Toluene-d8 (S) 106 % 66-133 1 11/15/21 22:39 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 111000 ug/L 5000 5000 1 11/17/21 15:08 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 202000 ug/L 25000 25000 1 11/15/21 17:12 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:25 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 13900 ug/L 1000 500 1 11/14/2103:52 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 21900 ug/L 1000 500 1 11/24/2111:25 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/16/2109:20 11/16/2115:23 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 85 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: E13-1 Lab ID: 92572199019 Collected: 11/08/21 12:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2117:50 309-00-2 ND ug/L 0.0500 0.0172 1 11/15/2106:10 11/16/2117:50 319-84-6 ND ug/L 0.0500 0.0208 1 11/15/2106:10 11/16/2117:50 319-85-7 ND ug/L 0.0500 0.0150 1 11/15/2106:10 11/16/2117:50 319-86-8 ND ug/L 0.0500 0.0209 1 11/15/2106:10 11/16/2117:50 58-89-9 ND ug/L 5.00 0.0198 1 11/15/2106:10 11/16/2117:50 57-74-9 ND ug/L 0.0500 0.0177 1 11/15/2106:10 11/16/2117:50 72-54-8 ND ug/L 0.0500 0.0154 1 11/15/2106:10 11/16/2117:50 72-55-9 ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2117:50 50-29-3 ND ug/L 0.0500 0.0162 1 11/15/2106:10 11/16/2117:50 60-57-1 ND ug/L 0.0500 0.0160 1 11/15/2106:10 11/16/2117:50 959-98-8 ND ug/L 0.0500 0.0164 1 11/15/2106:10 11/16/2117:50 33213-65-9 ND ug/L 0.0500 0.0217 1 11/15/2106:10 11/16/2117:50 1031-07-8 ND ug/L 0.0500 0.0161 1 11/15/2106:10 11/16/2117:50 72-20-8 ND ug/L 0.0500 0.0237 1 11/15/2106:10 11/16/2117:50 7421-93-4 ND ug/L 0.0500 0.0219 1 11/15/2106:10 11/16/2117:50 53494-70-5 ND ug/L 0.0500 0.0176 1 11/15/2106:10 11/16/2117:50 118-74-1 ND ug/L 0.0500 0.0148 1 11/15/2106:10 11/16/2117:50 76-44-8 ND ug/L 0.0500 0.0183 1 11/15/2106:10 11/16/2117:50 1024-57-3 ND ug/L 0.0500 0.0193 1 11/15/2106:10 11/16/2117:50 72-43-5 ND ug/L 0.500 0.168 1 11/15/2106:10 11/16/2117:50 8001-35-2 4.99 % 10.0-128 1 11/15/2106:10 11/16/2117:50 2051-24-3 SR 55.6 % 10.0-127 1 11/15/2106:10 11/16/2117:50 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/15/2108:09 11/16/2121:37 94-75-7 ND ug/L 2.00 0.344 1 11/15/2108:09 11/16/2121:37 127-20-8 LO ND ug/L 2.00 0.302 1 11/15/2108:09 11/16/2121:37 94-82-6 ND ug/L 2.00 0.245 1 11/15/2108:09 11/16/2121:37 1918-00-9 ND ug/L 2.00 1.04 1 11/15/2108:09 11/16/2121:37 15165-67-0 ND ug/L 2.00 0.250 1 11/15/2108:09 11/16/2121:37 88-85-7 ND ug/L 100 13.1 1 11/15/2108:09 11/16/2121:37 94-74-6 ND ug/L 100 66.0 1 11/15/2108:09 11/16/2121:37 7085-19-0 ND ug/L 2.00 0.258 1 11/15/2108:09 11/16/2121:37 93-76-5 ND ug/L 2.00 0.335 1 11/15/2108:09 11/16/2121:37 93-72-1 97.7 % 14.0-158 1 11/15/2108:09 11/16/2121:37 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.42 0.39 1 11/15/2107:08 11/16/2116:00 12674-11-2 ND ug/L 0.42 0.38 1 11/15/2107:08 11/16/2116:00 11104-28-2 ND ug/L 0.42 0.30 1 11/15/2107:08 11/16/2116:00 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 86 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: EB-1 Lab ID: 92572199019 Collected: 11/08/21 12:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.42 0.22 1 11/15/21 07:08 11/16/21 16:00 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.42 0.34 1 11/15/21 07:08 11/16/21 16:00 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.42 0.21 1 11/15/21 07:08 11/16/21 16:00 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.42 0.35 1 11/15/21 07:08 11/16/21 16:00 11096-82-5 Surrogates Decachlorobiphenyl (S) 88 % 10-181 1 11/15/21 07:08 11/16/21 16:00 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/30/2100:45 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:45 7440-38-2 Barium ND ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:45 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/30/2100:45 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/30/2100:45 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/30/2100:45 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/30/2100:45 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/30/2100:45 7440-50-8 Iron ND ug/L 50.0 41.5 1 11/16/2114:13 11/30/2100:45 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/30/2100:45 7439-92-1 Manganese ND ug/L 5.0 3.4 1 11/16/2114:13 11/30/2100:45 7439-96-5 Nickel ND ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:45 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:45 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/30/2100:45 7440-22-4 Sodium ND ug/L 5000 611 1 11/16/2114:13 11/30/2100:45 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/30/2100:45 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 11/16/2114:13 11/30/2100:45 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/30/2100:45 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2109:57 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 8.3 2.2 1 11/15/21 04:46 11/16/21 19:02 56-55-3 Chrysene ND ug/L 8.3 2.3 1 11/15/21 04:46 11/16/21 19:02 218-01-9 Dibenz(a,h)anthracene ND ug/L 8.3 2.5 1 11/15/21 04:46 11/16/21 19:02 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.0 3.1 1 11/15/21 04:46 11/16/21 19:02 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 8.3 2.4 1 11/15/21 04:46 11/16/21 19:02 193-39-5 Surrogates Nitrobenzene-d5 (S) 51 % 10-144 1 11/15/21 04:46 11/16/21 19:02 4165-60-0 2-Fluorobiphenyl (S) 36 % 10-130 1 11/15/21 04:46 11/16/21 19:02 321-60-8 Terphenyl-d14 (S) 55 % 34-163 1 11/15/21 04:46 11/16/21 19:02 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 87 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: EB-1 Lab ID: 92572199019 Collected: 11/08/21 12:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2104:17 67-64-1 ND ug/L 10.0 1.8 1 11/16/2104:17 107-13-1 ND ug/L 1.0 0.34 1 11/16/2104:17 71-43-2 ND ug/L 1.0 0.47 1 11/16/2104:17 74-97-5 ND ug/L 1.0 0.31 1 11/16/2104:17 75-27-4 ND ug/L 1.0 0.34 1 11/16/2104:17 75-25-2 ND ug/L 2.0 1.7 1 11/16/2104:17 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2104:17 78-93-3 ND ug/L 2.0 0.73 1 11/16/2104:17 75-15-0 ND ug/L 1.0 0.33 1 11/16/2104:17 56-23-5 ND ug/L 1.0 0.28 1 11/16/2104:17 108-90-7 ND ug/L 1.0 0.65 1 11/16/2104:17 75-00-3 ND ug/L 1.0 0.43 1 11/16/2104:17 67-66-3 ND ug/L 1.0 0.54 1 11/16/2104:17 74-87-3 ND ug/L 2.0 0.34 1 11/16/2104:17 96-12-8 ND ug/L 1.0 0.36 1 11/16/2104:17 124-48-1 ND ug/L 1.0 0.27 1 11/16/2104:17 106-93-4 ND ug/L 1.0 0.39 1 11/16/2104:17 74-95-3 ND ug/L 1.0 0.34 1 11/16/2104:17 95-50-1 ND ug/L 1.0 0.33 1 11/16/2104:17 106-46-7 ND ug/L 1.0 0.56 1 11/16/2104:17 110-57-6 ND ug/L 1.0 0.35 1 11/16/2104:17 75-71-8 ND ug/L 1.0 0.37 1 11/16/2104:17 75-34-3 ND ug/L 1.0 0.32 1 11/16/2104:17 107-06-2 ND ug/L 1.0 0.35 1 11/16/2104:17 75-35-4 ND ug/L 1.0 0.38 1 11/16/2104:17 156-59-2 ND ug/L 1.0 0.40 1 11/16/2104:17 156-60-5 ND ug/L 1.0 0.36 1 11/16/2104:17 78-87-5 ND ug/L 1.0 0.36 1 11/16/2104:17 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2104:17 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2104:17 100-41-4 ND ug/L 5.0 0.48 1 11/16/2104:17 591-78-6 ND ug/L 20.0 9.7 1 11/16/2104:17 74-88-4 ND ug/L 5.0 2.0 1 11/16/2104:17 75-09-2 ND ug/L 5.0 2.7 1 11/16/2104:17 108-10-1 ND ug/L 1.0 0.29 1 11/16/2104:17 100-42-5 ND ug/L 1.0 0.31 1 11/16/2104:17 630-20-6 ND ug/L 1.0 0.22 1 11/16/2104:17 79-34-5 ND ug/L 1.0 0.29 1 11/16/2104:17 127-18-4 ND ug/L 10.0 3.5 1 11/16/2104:17 109-99-9 ND ug/L 1.0 0.48 1 11/16/2104:17 108-88-3 ND ug/L 1.0 0.33 1 11/16/2104:17 71-55-6 ND ug/L 1.0 0.32 1 11/16/2104:17 79-00-5 ND ug/L 1.0 0.38 1 11/16/2104:17 79-01-6 ND ug/L 1.0 0.30 1 11/16/2104:17 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 88 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: E13-1 Lab ID: 92572199019 Collected: 11/08/21 12:20 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 04:17 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 04:17 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 04:17 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 04:17 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 04:17 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 11/16/21 04:17 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 04:17 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 04:17 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 11/15/21 18:35 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 88 % 70-130 1 11/15/21 18:35 17060-07-0 Toluene-d8 (S) 92 % 66-133 1 11/15/21 18:35 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 ND ug/L 5000 5000 1 11/16/21 16:29 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids ND ug/L 25000 25000 1 11/14/21 17:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:01 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 11/14/2105:40 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride ND ug/L 1000 500 1 11/24/2111:27 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/17/2113:32 11/18/2110:59 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 89 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: F13-1 Lab ID: 92572199020 Collected: 11/08/21 12:45 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Pesticides (GC) 8081 B Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Hexachlorobenzene Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) Date: 12/02/2021 09:16 AM Analytical Method: EPA 8081 B Preparation Method: 3510C Pace National - Mt. Juliet ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2117:59 309-00-2 ND ug/L 0.0500 0.0172 1 11/15/2106:10 11/16/2117:59 319-84-6 ND ug/L 0.0500 0.0208 1 11/15/2106:10 11/16/2117:59 319-85-7 ND ug/L 0.0500 0.0150 1 11/15/2106:10 11/16/2117:59 319-86-8 ND ug/L 0.0500 0.0209 1 11/15/2106:10 11/16/2117:59 58-89-9 ND ug/L 5.00 0.0198 1 11/15/2106:10 11/16/2117:59 57-74-9 ND ug/L 0.0500 0.0177 1 11/15/2106:10 11/16/2117:59 72-54-8 ND ug/L 0.0500 0.0154 1 11/15/2106:10 11/16/2117:59 72-55-9 ND ug/L 0.0500 0.0198 1 11/15/2106:10 11/16/2117:59 50-29-3 ND ug/L 0.0500 0.0162 1 11/15/2106:10 11/16/2117:59 60-57-1 ND ug/L 0.0500 0.0160 1 11/15/2106:10 11/16/2117:59 959-98-8 ND ug/L 0.0500 0.0164 1 11/15/2106:10 11/16/2117:59 33213-65-9 ND ug/L 0.0500 0.0217 1 11/15/2106:10 11/16/2117:59 1031-07-8 ND ug/L 0.0500 0.0161 1 11/15/2106:10 11/16/2117:59 72-20-8 ND ug/L 0.0500 0.0237 1 11/15/2106:10 11/16/2117:59 7421-93-4 ND ug/L 0.0500 0.0219 1 11/15/2106:10 11/16/2117:59 53494-70-5 0.0305J ug/L 0.0500 0.0176 1 11/15/2106:10 11/16/2117:59 118-74-1 J ND ug/L 0.0500 0.0148 1 11/15/2106:10 11/16/2117:59 76-44-8 ND ug/L 0.0500 0.0183 1 11/15/2106:10 11/16/2117:59 1024-57-3 ND ug/L 0.0500 0.0193 1 11/15/2106:10 11/16/2117:59 72-43-5 ND ug/L 0.500 0.168 1 11/15/2106:10 11/16/2117:59 8001-35-2 4.59 % 10.0-128 1 11/15/2106:10 11/16/2117:59 2051-24-3 SR 47.7 % 10.0-127 1 11/15/2106:10 11/16/2117:59 877-09-8 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 11/15/2108:09 11/16/2121:51 94-75-7 ND ug/L 2.00 0.344 1 11/15/2108:09 11/16/2121:51 127-20-8 LO ND ug/L 2.00 0.302 1 11/15/2108:09 11/16/2121:51 94-82-6 ND ug/L 2.00 0.245 1 11/15/2108:09 11/16/2121:51 1918-00-9 ND ug/L 2.00 1.04 1 11/15/2108:09 11/16/2121:51 15165-67-0 ND ug/L 2.00 0.250 1 11/15/2108:09 11/16/2121:51 88-85-7 ND ug/L 100 13.1 1 11/15/2108:09 11/16/2121:51 94-74-6 ND ug/L 100 66.0 1 11/15/2108:09 11/16/2121:51 7085-19-0 ND ug/L 2.00 0.258 1 11/15/2108:09 11/16/2121:51 93-76-5 ND ug/L 2.00 0.335 1 11/15/2108:09 11/16/2121:51 93-72-1 99.4 % 14.0-158 1 11/15/2108:09 11/16/2121:51 19719-28-9 Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.45 0.43 1 11/15/2107:08 11/16/2116:12 12674-11-2 ND ug/L 0.45 0.41 1 11/15/2107:08 11/16/2116:12 11104-28-2 ND ug/L 0.45 0.33 1 11/15/2107:08 11/16/2116:12 11141-16-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 90 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: FB-1 Lab ID: 92572199020 Collected: 11/08/21 12:45 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1242 (Aroclor 1242) ND ug/L 0.45 0.24 1 11/15/21 07:08 11/16/21 16:12 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.45 0.37 1 11/15/21 07:08 11/16/21 16:12 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.45 0.23 1 11/15/21 07:08 11/16/21 16:12 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.45 0.38 1 11/15/21 07:08 11/16/21 16:12 11096-82-5 Surrogates Decachlorobiphenyl (S) 97 % 10-181 1 11/15/21 07:08 11/16/21 16:12 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 11/16/2114:13 11/30/2100:49 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:49 7440-38-2 Barium ND ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:49 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 11/16/2114:13 11/30/2100:49 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 11/16/2114:13 11/30/2100:49 7440-43-9 Chromium ND ug/L 5.0 3.7 1 11/16/2114:13 11/30/2100:49 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 11/16/2114:13 11/30/2100:49 7440-48-4 Copper ND ug/L 5.0 4.3 1 11/16/2114:13 11/30/2100:49 7440-50-8 Iron ND ug/L 50.0 41.5 1 11/16/2114:13 11/30/2100:49 7439-89-6 Lead ND ug/L 5.0 4.5 1 11/16/2114:13 11/30/2100:49 7439-92-1 Manganese ND ug/L 5.0 3.4 1 11/16/2114:13 11/30/2100:49 7439-96-5 Nickel ND ug/L 5.0 3.5 1 11/16/2114:13 11/30/2100:49 7440-02-0 Selenium ND ug/L 10.0 4.7 1 11/16/2114:13 11/30/2100:49 7782-49-2 Silver ND ug/L 5.0 2.5 1 11/16/2114:13 11/30/2100:49 7440-22-4 Sodium ND ug/L 5000 611 1 11/16/2114:13 11/30/2100:49 7440-23-5 Tin ND ug/L 5.0 4.7 1 11/16/2114:13 11/30/2100:49 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 11/16/2114:13 11/30/2100:49 7440-62-2 Zinc ND ug/L 10.0 9.5 1 11/16/2114:13 11/30/2100:49 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 11/18/2116:15 11/25/2110:00 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 9.1 2.4 1 11/15/21 04:46 11/16/21 19:31 56-55-3 Chrysene ND ug/L 9.1 2.5 1 11/15/21 04:46 11/16/21 19:31 218-01-9 Dibenz(a,h)anthracene ND ug/L 9.1 2.7 1 11/15/21 04:46 11/16/21 19:31 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 5.5 3.4 1 11/15/21 04:46 11/16/21 19:31 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 9.1 2.6 1 11/15/21 04:46 11/16/21 19:31 193-39-5 Surrogates Nitrobenzene-d5 (S) 59 % 10-144 1 11/15/21 04:46 11/16/21 19:31 4165-60-0 2-Fluorobiphenyl (S) 43 % 10-130 1 11/15/21 04:46 11/16/21 19:31 321-60-8 Terphenyl-d14 (S) 59 % 34-163 1 11/15/21 04:46 11/16/21 19:31 1718-51-0 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 91 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: FB-1 Lab ID: 92572199020 Collected: 11/08/21 12:45 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2104:35 67-64-1 ND ug/L 10.0 1.8 1 11/16/2104:35 107-13-1 ND ug/L 1.0 0.34 1 11/16/2104:35 71-43-2 ND ug/L 1.0 0.47 1 11/16/2104:35 74-97-5 ND ug/L 1.0 0.31 1 11/16/2104:35 75-27-4 ND ug/L 1.0 0.34 1 11/16/2104:35 75-25-2 ND ug/L 2.0 1.7 1 11/16/2104:35 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2104:35 78-93-3 ND ug/L 2.0 0.73 1 11/16/2104:35 75-15-0 ND ug/L 1.0 0.33 1 11/16/2104:35 56-23-5 ND ug/L 1.0 0.28 1 11/16/2104:35 108-90-7 ND ug/L 1.0 0.65 1 11/16/2104:35 75-00-3 ND ug/L 1.0 0.43 1 11/16/2104:35 67-66-3 ND ug/L 1.0 0.54 1 11/16/2104:35 74-87-3 ND ug/L 2.0 0.34 1 11/16/2104:35 96-12-8 ND ug/L 1.0 0.36 1 11/16/2104:35 124-48-1 ND ug/L 1.0 0.27 1 11/16/2104:35 106-93-4 ND ug/L 1.0 0.39 1 11/16/2104:35 74-95-3 ND ug/L 1.0 0.34 1 11/16/2104:35 95-50-1 ND ug/L 1.0 0.33 1 11/16/2104:35 106-46-7 ND ug/L 1.0 0.56 1 11/16/2104:35 110-57-6 ND ug/L 1.0 0.35 1 11/16/2104:35 75-71-8 ND ug/L 1.0 0.37 1 11/16/2104:35 75-34-3 ND ug/L 1.0 0.32 1 11/16/2104:35 107-06-2 ND ug/L 1.0 0.35 1 11/16/2104:35 75-35-4 ND ug/L 1.0 0.38 1 11/16/2104:35 156-59-2 ND ug/L 1.0 0.40 1 11/16/2104:35 156-60-5 ND ug/L 1.0 0.36 1 11/16/2104:35 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 04:35 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2104:35 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2104:35 100-41-4 ND ug/L 5.0 0.48 1 11/16/2104:35 591-78-6 ND ug/L 20.0 9.7 1 11/16/2104:35 74-88-4 ND ug/L 5.0 2.0 1 11/16/2104:35 75-09-2 ND ug/L 5.0 2.7 1 11/16/2104:35 108-10-1 ND ug/L 1.0 0.29 1 11/16/2104:35 100-42-5 ND ug/L 1.0 0.31 1 11/16/2104:35 630-20-6 ND ug/L 1.0 0.22 1 11/16/2104:35 79-34-5 ND ug/L 1.0 0.29 1 11/16/2104:35 127-18-4 ND ug/L 10.0 3.5 1 11/16/2104:35 109-99-9 ND ug/L 1.0 0.48 1 11/16/2104:35 108-88-3 ND ug/L 1.0 0.33 1 11/16/2104:35 71-55-6 ND ug/L 1.0 0.32 1 11/16/2104:35 79-00-5 ND ug/L 1.0 0.38 1 11/16/2104:35 79-01-6 ND ug/L 1.0 0.30 1 11/16/2104:35 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 92 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: F13-1 Lab ID: 92572199020 Collected: 11/08/21 12:45 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 04:35 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 04:35 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 04:35 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 04:35 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 04:35 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 04:35 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 04:35 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 11/16/21 04:35 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 0.86 1 11/15/21 18:54 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 11/15/21 18:54 17060-07-0 Toluene-d8 (S) 98 % 66-133 1 11/15/21 18:54 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 ND ug/L 5000 5000 1 11/16/21 16:34 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids ND ug/L 25000 25000 1 11/14/21 17:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 11/13/2103:01 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 11/14/2105:55 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride ND ug/L 1000 500 1 11/24/2111:28 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2016 Preparation Method: SM 4500-CN-E-2016 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 11/17/2113:32 11/18/2111:01 57-12-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 93 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: TB-1 Lab ID: 92572199021 Collected: 11/12/21 00:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2101:52 67-64-1 ND ug/L 10.0 1.8 1 11/16/2101:52 107-13-1 ND ug/L 1.0 0.34 1 11/16/2101:52 71-43-2 ND ug/L 1.0 0.47 1 11/16/2101:52 74-97-5 ND ug/L 1.0 0.31 1 11/16/2101:52 75-27-4 ND ug/L 1.0 0.34 1 11/16/2101:52 75-25-2 ND ug/L 2.0 1.7 1 11/16/2101:52 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2101:52 78-93-3 ND ug/L 2.0 0.73 1 11/16/2101:52 75-15-0 ND ug/L 1.0 0.33 1 11/16/2101:52 56-23-5 ND ug/L 1.0 0.28 1 11/16/2101:52 108-90-7 ND ug/L 1.0 0.65 1 11/16/2101:52 75-00-3 ND ug/L 1.0 0.43 1 11/16/2101:52 67-66-3 ND ug/L 1.0 0.54 1 11/16/2101:52 74-87-3 ND ug/L 2.0 0.34 1 11/16/2101:52 96-12-8 ND ug/L 1.0 0.36 1 11/16/2101:52 124-48-1 ND ug/L 1.0 0.27 1 11/16/2101:52 106-93-4 ND ug/L 1.0 0.39 1 11/16/2101:52 74-95-3 ND ug/L 1.0 0.34 1 11/16/2101:52 95-50-1 ND ug/L 1.0 0.33 1 11/16/2101:52 106-46-7 ND ug/L 1.0 0.56 1 11/16/2101:52 110-57-6 ND ug/L 1.0 0.35 1 11/16/2101:52 75-71-8 ND ug/L 1.0 0.37 1 11/16/2101:52 75-34-3 ND ug/L 1.0 0.32 1 11/16/2101:52 107-06-2 ND ug/L 1.0 0.35 1 11/16/2101:52 75-35-4 ND ug/L 1.0 0.38 1 11/16/2101:52 156-59-2 ND ug/L 1.0 0.40 1 11/16/2101:52 156-60-5 ND ug/L 1.0 0.36 1 11/16/2101:52 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 01:52 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2101:52 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2101:52 100-41-4 ND ug/L 5.0 0.48 1 11/16/2101:52 591-78-6 ND ug/L 20.0 9.7 1 11/16/2101:52 74-88-4 ND ug/L 5.0 2.0 1 11/16/2101:52 75-09-2 ND ug/L 5.0 2.7 1 11/16/2101:52 108-10-1 ND ug/L 1.0 0.29 1 11/16/2101:52 100-42-5 ND ug/L 1.0 0.31 1 11/16/2101:52 630-20-6 ND ug/L 1.0 0.22 1 11/16/2101:52 79-34-5 ND ug/L 1.0 0.29 1 11/16/2101:52 127-18-4 ND ug/L 10.0 3.5 1 11/16/2101:52 109-99-9 ND ug/L 1.0 0.48 1 11/16/2101:52 108-88-3 ND ug/L 1.0 0.33 1 11/16/2101:52 71-55-6 ND ug/L 1.0 0.32 1 11/16/2101:52 79-00-5 ND ug/L 1.0 0.38 1 11/16/2101:52 79-01-6 ND ug/L 1.0 0.30 1 11/16/2101:52 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 94 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: T13-1 Parameters Lab ID: Results 92572199021 Units Collected: Report Limit 11/12/21 00:00 MDL DF Received: 11/12/21 14:00 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 01:52 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 01:52 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 01:52 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 01:52 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 01:52 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 11/16/21 01:52 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 11/16/21 01:52 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 01:52 2037-26-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 95 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: TB-2 Lab ID: 92572199022 Collected: 11/12/21 00:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2102:10 67-64-1 ND ug/L 10.0 1.8 1 11/16/2102:10 107-13-1 ND ug/L 1.0 0.34 1 11/16/2102:10 71-43-2 ND ug/L 1.0 0.47 1 11/16/2102:10 74-97-5 ND ug/L 1.0 0.31 1 11/16/2102:10 75-27-4 ND ug/L 1.0 0.34 1 11/16/2102:10 75-25-2 ND ug/L 2.0 1.7 1 11/16/2102:10 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2102:10 78-93-3 ND ug/L 2.0 0.73 1 11/16/2102:10 75-15-0 ND ug/L 1.0 0.33 1 11/16/2102:10 56-23-5 ND ug/L 1.0 0.28 1 11/16/2102:10 108-90-7 ND ug/L 1.0 0.65 1 11/16/2102:10 75-00-3 ND ug/L 1.0 0.43 1 11/16/2102:10 67-66-3 ND ug/L 1.0 0.54 1 11/16/2102:10 74-87-3 ND ug/L 2.0 0.34 1 11/16/2102:10 96-12-8 ND ug/L 1.0 0.36 1 11/16/2102:10 124-48-1 ND ug/L 1.0 0.27 1 11/16/2102:10 106-93-4 ND ug/L 1.0 0.39 1 11/16/2102:10 74-95-3 ND ug/L 1.0 0.34 1 11/16/2102:10 95-50-1 ND ug/L 1.0 0.33 1 11/16/2102:10 106-46-7 ND ug/L 1.0 0.56 1 11/16/2102:10 110-57-6 ND ug/L 1.0 0.35 1 11/16/2102:10 75-71-8 ND ug/L 1.0 0.37 1 11/16/2102:10 75-34-3 ND ug/L 1.0 0.32 1 11/16/2102:10 107-06-2 ND ug/L 1.0 0.35 1 11/16/2102:10 75-35-4 ND ug/L 1.0 0.38 1 11/16/2102:10 156-59-2 ND ug/L 1.0 0.40 1 11/16/2102:10 156-60-5 ND ug/L 1.0 0.36 1 11/16/2102:10 78-87-5 ND ug/L 1.0 0.36 1 11/16/2102:10 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2102:10 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2102:10 100-41-4 ND ug/L 5.0 0.48 1 11/16/2102:10 591-78-6 ND ug/L 20.0 9.7 1 11/16/2102:10 74-88-4 ND ug/L 5.0 2.0 1 11/16/2102:10 75-09-2 ND ug/L 5.0 2.7 1 11/16/2102:10 108-10-1 ND ug/L 1.0 0.29 1 11/16/2102:10 100-42-5 ND ug/L 1.0 0.31 1 11/16/2102:10 630-20-6 ND ug/L 1.0 0.22 1 11/16/2102:10 79-34-5 ND ug/L 1.0 0.29 1 11/16/2102:10 127-18-4 ND ug/L 10.0 3.5 1 11/16/2102:10 109-99-9 ND ug/L 1.0 0.48 1 11/16/2102:10 108-88-3 ND ug/L 1.0 0.33 1 11/16/2102:10 71-55-6 ND ug/L 1.0 0.32 1 11/16/2102:10 79-00-5 ND ug/L 1.0 0.38 1 11/16/2102:10 79-01-6 ND ug/L 1.0 0.30 1 11/16/2102:10 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 96 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: T13-2 Parameters Lab ID: Results 92572199022 Units Collected: Report Limit 11/12/21 00:00 MDL DF Received: 11/12/21 14:00 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 02:10 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 02:10 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 02:10 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 02:10 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 02:10 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 02:10 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 11/16/21 02:10 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 02:10 2037-26-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 97 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: TB-3 Lab ID: 92572199023 Collected: 11/12/21 00:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2102:28 67-64-1 ND ug/L 10.0 1.8 1 11/16/2102:28 107-13-1 ND ug/L 1.0 0.34 1 11/16/2102:28 71-43-2 ND ug/L 1.0 0.47 1 11/16/2102:28 74-97-5 ND ug/L 1.0 0.31 1 11/16/2102:28 75-27-4 ND ug/L 1.0 0.34 1 11/16/2102:28 75-25-2 ND ug/L 2.0 1.7 1 11/16/2102:28 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2102:28 78-93-3 ND ug/L 2.0 0.73 1 11/16/2102:28 75-15-0 ND ug/L 1.0 0.33 1 11/16/2102:28 56-23-5 ND ug/L 1.0 0.28 1 11/16/2102:28 108-90-7 ND ug/L 1.0 0.65 1 11/16/2102:28 75-00-3 ND ug/L 1.0 0.43 1 11/16/2102:28 67-66-3 ND ug/L 1.0 0.54 1 11/16/2102:28 74-87-3 ND ug/L 2.0 0.34 1 11/16/2102:28 96-12-8 ND ug/L 1.0 0.36 1 11/16/2102:28 124-48-1 ND ug/L 1.0 0.27 1 11/16/2102:28 106-93-4 ND ug/L 1.0 0.39 1 11/16/2102:28 74-95-3 ND ug/L 1.0 0.34 1 11/16/2102:28 95-50-1 ND ug/L 1.0 0.33 1 11/16/2102:28 106-46-7 ND ug/L 1.0 0.56 1 11/16/2102:28 110-57-6 ND ug/L 1.0 0.35 1 11/16/2102:28 75-71-8 ND ug/L 1.0 0.37 1 11/16/2102:28 75-34-3 ND ug/L 1.0 0.32 1 11/16/2102:28 107-06-2 ND ug/L 1.0 0.35 1 11/16/2102:28 75-35-4 ND ug/L 1.0 0.38 1 11/16/2102:28 156-59-2 ND ug/L 1.0 0.40 1 11/16/2102:28 156-60-5 ND ug/L 1.0 0.36 1 11/16/2102:28 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 02:28 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2102:28 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2102:28 100-41-4 ND ug/L 5.0 0.48 1 11/16/2102:28 591-78-6 ND ug/L 20.0 9.7 1 11/16/2102:28 74-88-4 ND ug/L 5.0 2.0 1 11/16/2102:28 75-09-2 ND ug/L 5.0 2.7 1 11/16/2102:28 108-10-1 ND ug/L 1.0 0.29 1 11/16/2102:28 100-42-5 ND ug/L 1.0 0.31 1 11/16/2102:28 630-20-6 ND ug/L 1.0 0.22 1 11/16/2102:28 79-34-5 ND ug/L 1.0 0.29 1 11/16/2102:28 127-18-4 ND ug/L 10.0 3.5 1 11/16/2102:28 109-99-9 ND ug/L 1.0 0.48 1 11/16/2102:28 108-88-3 ND ug/L 1.0 0.33 1 11/16/2102:28 71-55-6 ND ug/L 1.0 0.32 1 11/16/2102:28 79-00-5 ND ug/L 1.0 0.38 1 11/16/2102:28 79-01-6 ND ug/L 1.0 0.30 1 11/16/2102:28 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 98 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: T13-3 Parameters Lab ID: Results 92572199023 Units Collected: Report Limit 11/12/21 00:00 MDL DF Received: 11/12/21 14:00 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 02:28 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 02:28 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 02:28 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 02:28 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 02:28 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 02:28 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 02:28 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 02:28 2037-26-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 99 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: TB-4 Lab ID: 92572199024 Collected: 11/12/21 00:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2102:46 67-64-1 ND ug/L 10.0 1.8 1 11/16/2102:46 107-13-1 ND ug/L 1.0 0.34 1 11/16/2102:46 71-43-2 ND ug/L 1.0 0.47 1 11/16/2102:46 74-97-5 ND ug/L 1.0 0.31 1 11/16/2102:46 75-27-4 ND ug/L 1.0 0.34 1 11/16/2102:46 75-25-2 ND ug/L 2.0 1.7 1 11/16/2102:46 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2102:46 78-93-3 ND ug/L 2.0 0.73 1 11/16/2102:46 75-15-0 ND ug/L 1.0 0.33 1 11/16/2102:46 56-23-5 ND ug/L 1.0 0.28 1 11/16/2102:46 108-90-7 ND ug/L 1.0 0.65 1 11/16/2102:46 75-00-3 ND ug/L 1.0 0.43 1 11/16/2102:46 67-66-3 ND ug/L 1.0 0.54 1 11/16/2102:46 74-87-3 ND ug/L 2.0 0.34 1 11/16/2102:46 96-12-8 ND ug/L 1.0 0.36 1 11/16/2102:46 124-48-1 ND ug/L 1.0 0.27 1 11/16/2102:46 106-93-4 ND ug/L 1.0 0.39 1 11/16/2102:46 74-95-3 ND ug/L 1.0 0.34 1 11/16/2102:46 95-50-1 ND ug/L 1.0 0.33 1 11/16/2102:46 106-46-7 ND ug/L 1.0 0.56 1 11/16/2102:46 110-57-6 ND ug/L 1.0 0.35 1 11/16/2102:46 75-71-8 ND ug/L 1.0 0.37 1 11/16/2102:46 75-34-3 ND ug/L 1.0 0.32 1 11/16/2102:46 107-06-2 ND ug/L 1.0 0.35 1 11/16/2102:46 75-35-4 ND ug/L 1.0 0.38 1 11/16/2102:46 156-59-2 ND ug/L 1.0 0.40 1 11/16/2102:46 156-60-5 ND ug/L 1.0 0.36 1 11/16/2102:46 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 02:46 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2102:46 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2102:46 100-41-4 ND ug/L 5.0 0.48 1 11/16/2102:46 591-78-6 ND ug/L 20.0 9.7 1 11/16/2102:46 74-88-4 ND ug/L 5.0 2.0 1 11/16/2102:46 75-09-2 ND ug/L 5.0 2.7 1 11/16/2102:46 108-10-1 ND ug/L 1.0 0.29 1 11/16/2102:46 100-42-5 ND ug/L 1.0 0.31 1 11/16/2102:46 630-20-6 ND ug/L 1.0 0.22 1 11/16/2102:46 79-34-5 ND ug/L 1.0 0.29 1 11/16/2102:46 127-18-4 ND ug/L 10.0 3.5 1 11/16/2102:46 109-99-9 ND ug/L 1.0 0.48 1 11/16/2102:46 108-88-3 ND ug/L 1.0 0.33 1 11/16/2102:46 71-55-6 ND ug/L 1.0 0.32 1 11/16/2102:46 79-00-5 ND ug/L 1.0 0.38 1 11/16/2102:46 79-01-6 ND ug/L 1.0 0.30 1 11/16/2102:46 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 100 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: T13-4 Parameters Lab ID: Results 92572199024 Units Collected: Report Limit 11/12/21 00:00 MDL DF Received: 11/12/21 14:00 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 02:46 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 02:46 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 02:46 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 02:46 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 02:46 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 02:46 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 11/16/21 02:46 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 02:46 2037-26-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 101 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: TB-5 Lab ID: 92572199025 Collected: 11/12/21 00:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2103:04 67-64-1 ND ug/L 10.0 1.8 1 11/16/2103:04 107-13-1 ND ug/L 1.0 0.34 1 11/16/2103:04 71-43-2 ND ug/L 1.0 0.47 1 11/16/2103:04 74-97-5 ND ug/L 1.0 0.31 1 11/16/2103:04 75-27-4 ND ug/L 1.0 0.34 1 11/16/2103:04 75-25-2 ND ug/L 2.0 1.7 1 11/16/2103:04 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2103:04 78-93-3 ND ug/L 2.0 0.73 1 11/16/2103:04 75-15-0 ND ug/L 1.0 0.33 1 11/16/2103:04 56-23-5 ND ug/L 1.0 0.28 1 11/16/2103:04 108-90-7 ND ug/L 1.0 0.65 1 11/16/2103:04 75-00-3 ND ug/L 1.0 0.43 1 11/16/2103:04 67-66-3 ND ug/L 1.0 0.54 1 11/16/2103:04 74-87-3 ND ug/L 2.0 0.34 1 11/16/2103:04 96-12-8 ND ug/L 1.0 0.36 1 11/16/2103:04 124-48-1 ND ug/L 1.0 0.27 1 11/16/2103:04 106-93-4 ND ug/L 1.0 0.39 1 11/16/2103:04 74-95-3 ND ug/L 1.0 0.34 1 11/16/2103:04 95-50-1 ND ug/L 1.0 0.33 1 11/16/2103:04 106-46-7 ND ug/L 1.0 0.56 1 11/16/2103:04 110-57-6 ND ug/L 1.0 0.35 1 11/16/2103:04 75-71-8 ND ug/L 1.0 0.37 1 11/16/2103:04 75-34-3 ND ug/L 1.0 0.32 1 11/16/2103:04 107-06-2 ND ug/L 1.0 0.35 1 11/16/2103:04 75-35-4 ND ug/L 1.0 0.38 1 11/16/2103:04 156-59-2 ND ug/L 1.0 0.40 1 11/16/2103:04 156-60-5 ND ug/L 1.0 0.36 1 11/16/2103:04 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 03:04 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2103:04 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2103:04 100-41-4 ND ug/L 5.0 0.48 1 11/16/2103:04 591-78-6 ND ug/L 20.0 9.7 1 11/16/2103:04 74-88-4 ND ug/L 5.0 2.0 1 11/16/2103:04 75-09-2 ND ug/L 5.0 2.7 1 11/16/2103:04 108-10-1 ND ug/L 1.0 0.29 1 11/16/2103:04 100-42-5 ND ug/L 1.0 0.31 1 11/16/2103:04 630-20-6 ND ug/L 1.0 0.22 1 11/16/2103:04 79-34-5 ND ug/L 1.0 0.29 1 11/16/2103:04 127-18-4 ND ug/L 10.0 3.5 1 11/16/2103:04 109-99-9 ND ug/L 1.0 0.48 1 11/16/2103:04 108-88-3 ND ug/L 1.0 0.33 1 11/16/2103:04 71-55-6 ND ug/L 1.0 0.32 1 11/16/2103:04 79-00-5 ND ug/L 1.0 0.38 1 11/16/2103:04 79-01-6 ND ug/L 1.0 0.30 1 11/16/2103:04 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 102 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: T13-5 Parameters Lab ID: Results 92572199025 Units Collected: Report Limit 11/12/21 00:00 MDL DF Received: 11/12/21 14:00 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 03:04 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 03:04 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 03:04 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 03:04 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 03:04 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 03:04 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 11/16/21 03:04 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 11/16/21 03:04 2037-26-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 103 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: TB-6 Lab ID: 92572199026 Collected: 11/12/21 00:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2103:23 67-64-1 ND ug/L 10.0 1.8 1 11/16/2103:23 107-13-1 ND ug/L 1.0 0.34 1 11/16/2103:23 71-43-2 ND ug/L 1.0 0.47 1 11/16/2103:23 74-97-5 ND ug/L 1.0 0.31 1 11/16/2103:23 75-27-4 ND ug/L 1.0 0.34 1 11/16/2103:23 75-25-2 ND ug/L 2.0 1.7 1 11/16/2103:23 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2103:23 78-93-3 ND ug/L 2.0 0.73 1 11/16/2103:23 75-15-0 ND ug/L 1.0 0.33 1 11/16/2103:23 56-23-5 ND ug/L 1.0 0.28 1 11/16/2103:23 108-90-7 ND ug/L 1.0 0.65 1 11/16/2103:23 75-00-3 ND ug/L 1.0 0.43 1 11/16/2103:23 67-66-3 ND ug/L 1.0 0.54 1 11/16/2103:23 74-87-3 ND ug/L 2.0 0.34 1 11/16/2103:23 96-12-8 ND ug/L 1.0 0.36 1 11/16/2103:23 124-48-1 ND ug/L 1.0 0.27 1 11/16/2103:23 106-93-4 ND ug/L 1.0 0.39 1 11/16/2103:23 74-95-3 ND ug/L 1.0 0.34 1 11/16/2103:23 95-50-1 ND ug/L 1.0 0.33 1 11/16/2103:23 106-46-7 ND ug/L 1.0 0.56 1 11/16/2103:23 110-57-6 ND ug/L 1.0 0.35 1 11/16/2103:23 75-71-8 ND ug/L 1.0 0.37 1 11/16/2103:23 75-34-3 ND ug/L 1.0 0.32 1 11/16/2103:23 107-06-2 ND ug/L 1.0 0.35 1 11/16/2103:23 75-35-4 ND ug/L 1.0 0.38 1 11/16/2103:23 156-59-2 ND ug/L 1.0 0.40 1 11/16/2103:23 156-60-5 ND ug/L 1.0 0.36 1 11/16/2103:23 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 03:23 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2103:23 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2103:23 100-41-4 ND ug/L 5.0 0.48 1 11/16/2103:23 591-78-6 ND ug/L 20.0 9.7 1 11/16/2103:23 74-88-4 ND ug/L 5.0 2.0 1 11/16/2103:23 75-09-2 ND ug/L 5.0 2.7 1 11/16/2103:23 108-10-1 ND ug/L 1.0 0.29 1 11/16/2103:23 100-42-5 ND ug/L 1.0 0.31 1 11/16/2103:23 630-20-6 ND ug/L 1.0 0.22 1 11/16/2103:23 79-34-5 ND ug/L 1.0 0.29 1 11/16/2103:23 127-18-4 ND ug/L 10.0 3.5 1 11/16/2103:23 109-99-9 ND ug/L 1.0 0.48 1 11/16/2103:23 108-88-3 ND ug/L 1.0 0.33 1 11/16/2103:23 71-55-6 ND ug/L 1.0 0.32 1 11/16/2103:23 79-00-5 ND ug/L 1.0 0.38 1 11/16/2103:23 79-01-6 ND ug/L 1.0 0.30 1 11/16/2103:23 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 104 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: T13-6 Parameters Lab ID: Results 92572199026 Units Collected: Report Limit 11/12/21 00:00 MDL DF Received: 11/12/21 14:00 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 03:23 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 03:23 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 03:23 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 03:23 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 03:23 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 11/16/21 03:23 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 03:23 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 03:23 2037-26-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 105 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: TB-7 Lab ID: 92572199027 Collected: 11/12/21 00:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2103:41 67-64-1 ND ug/L 10.0 1.8 1 11/16/2103:41 107-13-1 ND ug/L 1.0 0.34 1 11/16/2103:41 71-43-2 ND ug/L 1.0 0.47 1 11/16/2103:41 74-97-5 ND ug/L 1.0 0.31 1 11/16/2103:41 75-27-4 ND ug/L 1.0 0.34 1 11/16/2103:41 75-25-2 ND ug/L 2.0 1.7 1 11/16/2103:41 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2103:41 78-93-3 ND ug/L 2.0 0.73 1 11/16/2103:41 75-15-0 ND ug/L 1.0 0.33 1 11/16/2103:41 56-23-5 ND ug/L 1.0 0.28 1 11/16/2103:41 108-90-7 ND ug/L 1.0 0.65 1 11/16/2103:41 75-00-3 ND ug/L 1.0 0.43 1 11/16/2103:41 67-66-3 ND ug/L 1.0 0.54 1 11/16/2103:41 74-87-3 ND ug/L 2.0 0.34 1 11/16/2103:41 96-12-8 ND ug/L 1.0 0.36 1 11/16/2103:41 124-48-1 ND ug/L 1.0 0.27 1 11/16/2103:41 106-93-4 ND ug/L 1.0 0.39 1 11/16/2103:41 74-95-3 ND ug/L 1.0 0.34 1 11/16/2103:41 95-50-1 ND ug/L 1.0 0.33 1 11/16/2103:41 106-46-7 ND ug/L 1.0 0.56 1 11/16/2103:41 110-57-6 ND ug/L 1.0 0.35 1 11/16/2103:41 75-71-8 ND ug/L 1.0 0.37 1 11/16/2103:41 75-34-3 ND ug/L 1.0 0.32 1 11/16/2103:41 107-06-2 ND ug/L 1.0 0.35 1 11/16/2103:41 75-35-4 ND ug/L 1.0 0.38 1 11/16/2103:41 156-59-2 ND ug/L 1.0 0.40 1 11/16/2103:41 156-60-5 ND ug/L 1.0 0.36 1 11/16/2103:41 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 03:41 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2103:41 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2103:41 100-41-4 ND ug/L 5.0 0.48 1 11/16/2103:41 591-78-6 ND ug/L 20.0 9.7 1 11/16/2103:41 74-88-4 ND ug/L 5.0 2.0 1 11/16/2103:41 75-09-2 ND ug/L 5.0 2.7 1 11/16/2103:41 108-10-1 ND ug/L 1.0 0.29 1 11/16/2103:41 100-42-5 ND ug/L 1.0 0.31 1 11/16/2103:41 630-20-6 ND ug/L 1.0 0.22 1 11/16/2103:41 79-34-5 ND ug/L 1.0 0.29 1 11/16/2103:41 127-18-4 ND ug/L 10.0 3.5 1 11/16/2103:41 109-99-9 ND ug/L 1.0 0.48 1 11/16/2103:41 108-88-3 ND ug/L 1.0 0.33 1 11/16/2103:41 71-55-6 ND ug/L 1.0 0.32 1 11/16/2103:41 79-00-5 ND ug/L 1.0 0.38 1 11/16/2103:41 79-01-6 ND ug/L 1.0 0.30 1 11/16/2103:41 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 106 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: T13-7 Parameters Lab ID: Results 92572199027 Units Collected: Report Limit 11/12/21 00:00 MDL DF Received: 11/12/21 14:00 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 03:41 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 03:41 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 03:41 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 03:41 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 03:41 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/16/21 03:41 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 11/16/21 03:41 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/16/21 03:41 2037-26-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 107 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: TB-8 Lab ID: 92572199028 Collected: 11/12/21 00:00 Received: 11/12/21 14:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 12/02/2021 09:16 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 5.1 1 11/16/2103:59 67-64-1 ND ug/L 10.0 1.8 1 11/16/2103:59 107-13-1 ND ug/L 1.0 0.34 1 11/16/2103:59 71-43-2 ND ug/L 1.0 0.47 1 11/16/2103:59 74-97-5 ND ug/L 1.0 0.31 1 11/16/2103:59 75-27-4 ND ug/L 1.0 0.34 1 11/16/2103:59 75-25-2 ND ug/L 2.0 1.7 1 11/16/2103:59 74-83-9 v2 ND ug/L 5.0 4.0 1 11/16/2103:59 78-93-3 ND ug/L 2.0 0.73 1 11/16/2103:59 75-15-0 ND ug/L 1.0 0.33 1 11/16/2103:59 56-23-5 ND ug/L 1.0 0.28 1 11/16/2103:59 108-90-7 ND ug/L 1.0 0.65 1 11/16/2103:59 75-00-3 ND ug/L 1.0 0.43 1 11/16/2103:59 67-66-3 ND ug/L 1.0 0.54 1 11/16/2103:59 74-87-3 ND ug/L 2.0 0.34 1 11/16/2103:59 96-12-8 ND ug/L 1.0 0.36 1 11/16/2103:59 124-48-1 ND ug/L 1.0 0.27 1 11/16/2103:59 106-93-4 ND ug/L 1.0 0.39 1 11/16/2103:59 74-95-3 ND ug/L 1.0 0.34 1 11/16/2103:59 95-50-1 ND ug/L 1.0 0.33 1 11/16/2103:59 106-46-7 ND ug/L 1.0 0.56 1 11/16/2103:59 110-57-6 ND ug/L 1.0 0.35 1 11/16/2103:59 75-71-8 ND ug/L 1.0 0.37 1 11/16/2103:59 75-34-3 ND ug/L 1.0 0.32 1 11/16/2103:59 107-06-2 ND ug/L 1.0 0.35 1 11/16/2103:59 75-35-4 ND ug/L 1.0 0.38 1 11/16/2103:59 156-59-2 ND ug/L 1.0 0.40 1 11/16/2103:59 156-60-5 ND ug/L 1.0 0.36 1 11/16/2103:59 78-87-5 ND ug/L 1.0 0.36 1 11 /16/21 03:59 10061-01-5 ND ug/L 1.0 0.36 1 11/16/2103:59 10061-02-6 ND ug/L 1.0 0.30 1 11/16/2103:59 100-41-4 ND ug/L 5.0 0.48 1 11/16/2103:59 591-78-6 ND ug/L 20.0 9.7 1 11/16/2103:59 74-88-4 ND ug/L 5.0 2.0 1 11/16/2103:59 75-09-2 ND ug/L 5.0 2.7 1 11/16/2103:59 108-10-1 ND ug/L 1.0 0.29 1 11/16/2103:59 100-42-5 ND ug/L 1.0 0.31 1 11/16/2103:59 630-20-6 ND ug/L 1.0 0.22 1 11/16/2103:59 79-34-5 ND ug/L 1.0 0.29 1 11/16/2103:59 127-18-4 ND ug/L 10.0 3.5 1 11/16/2103:59 109-99-9 ND ug/L 1.0 0.48 1 11/16/2103:59 108-88-3 ND ug/L 1.0 0.33 1 11/16/2103:59 71-55-6 ND ug/L 1.0 0.32 1 11/16/2103:59 79-00-5 ND ug/L 1.0 0.38 1 11/16/2103:59 79-01-6 ND ug/L 1.0 0.30 1 11/16/2103:59 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 108 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL Pace Project No.: 92572199 Sample: T13-8 Parameters Lab ID: Results 92572199028 Units Collected: Report Limit 11/12/21 00:00 MDL DF Received: 11/12/21 14:00 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.26 1 11/16/21 03:59 96-18-4 Vinyl acetate ND ug/L 2.0 1.3 1 11/16/21 03:59 108-05-4 Vinyl chloride ND ug/L 1.0 0.39 1 11/16/21 03:59 75-01-4 m&p-Xylene ND ug/L 2.0 0.71 1 11/16/21 03:59 179601-23-1 o-Xylene ND ug/L 1.0 0.34 1 11/16/21 03:59 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 11/16/21 03:59 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 11/16/21 03:59 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 11/16/21 03:59 2037-26-5 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 109 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 1772920 Analysis Method: EPA 8081 B QC Batch Method: 3510C Analysis Description: Pesticides (GC) 8081 B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199019, 92572199020 METHOD BLANK: R3730057-1 Matrix: Water Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199019, 92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Aldrin ug/L ND 0.0500 0.0198 11/15/21 21:17 alpha-BHC ug/L ND 0.0500 0.0172 11/15/21 21:17 beta-BHC ug/L ND 0.0500 0.0208 11/15/21 21:17 delta-BHC ug/L ND 0.0500 0.0150 11/15/21 21:17 gamma-BHC (Lindane) ug/L ND 0.0500 0.0209 11/15/21 21:17 4,4'-DDD ug/L ND 0.0500 0.0177 11/15/21 21:17 4,4'-DDE ug/L ND 0.0500 0.0154 11/15/21 21:17 4,4'-DDT ug/L ND 0.0500 0.0198 11/15/21 21:17 Dieldrin ug/L ND 0.0500 0.0162 11/15/21 21:17 Endosulfan I ug/L ND 0.0500 0.0160 11/15/21 21:17 Endosulfan 11 ug/L ND 0.0500 0.0164 11/15/21 21:17 Endosulfan sulfate ug/L ND 0.0500 0.0217 11/15/21 21:17 Endrin ug/L ND 0.0500 0.0161 11/15/21 21:17 Endrin aldehyde ug/L ND 0.0500 0.0237 11/15/21 21:17 Endrin ketone ug/L ND 0.0500 0.0219 11/15/21 21:17 Heptachlor ug/L ND 0.0500 0.0148 11/15/21 21:17 Heptachlor epoxide ug/L ND 0.0500 0.0183 11/15/21 21:17 Hexachlorobenzene ug/L ND 0.0500 0.0176 11/15/21 21:17 Methoxychlor ug/L ND 0.0500 0.0193 11/15/21 21:17 Chlordane (Technical) ug/L ND 5.00 0.0198 11/15/21 21:17 Toxaphene ug/L ND 0.500 0.168 11/15/21 21:17 Decachlorobiphenyl (S) % 62 10.0-128 11/15/21 21:17 Tetrachloro-m-xylene (S) % 80.7 10.0-127 11/15/21 21:17 LABORATORY CONTROL SAMPLE: Parameter R3730057-2 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Aldrin ug/L 1.00 0.794 79.4 22.0-124 alpha-BHC ug/L 1.00 0.876 87.6 54.0-130 beta-BHC ug/L 1.00 0.879 87.9 53.0-136 delta-BHC ug/L 1.00 0.852 85.2 54.0-133 gamma-BHC (Lindane) ug/L 1.00 0.848 84.8 55.0-129 4,4'-DDD ug/L 1.00 0.792 79.2 56.0-140 4,4'-DDE ug/L 1.00 0.795 79.5 52.0-128 4,4'-DDT ug/L 1.00 0.751 75.1 50.0-141 Dieldrin ug/L 1.00 0.826 82.6 59.0-133 Endosulfan I ug/L 1.00 0.844 84.4 57.0-131 Endosulfan II ug/L 1.00 0.832 83.2 58.0-133 Endosulfan sulfate ug/L 1.00 0.800 80.0 58.0-133 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 110 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 LABORATORY CONTROL SAMPLE: R3730057-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Endrin ug/L 1.00 0.804 80.4 57.0-134 Endrin aldehyde ug/L 1.00 0.731 73.1 53.0-129 Endrin ketone ug/L 1.00 0.838 83.8 60.0-145 Heptachlor ug/L 1.00 0.815 81.5 27.0-132 Heptachlor epoxide ug/L 1.00 0.810 81.0 57.0-130 Hexachlorobenzene ug/L 1.00 0.838 83.8 30.0-114 Methoxychlor ug/L 1.00 0.757 75.7 54.0-155 Decachlorobiphenyl (S) % 56.4 10.0-128 Tetrachloro-m-xylene (S) % 80.1 10.0-127 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3730057-3 R3730057-4 MS MSD L1429893-02 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Aldrin ug/L ND 1.00 1.00 0.413 0.560 41.3 56.0 10.0-141 30.2 40 alpha-BHC ug/L ND 1.00 1.00 2.78 4.91 278 491 10.0-145 55.4 40 MH,R1 beta-BHC ug/L ND 1.00 1.00 0.506 1.50 50.6 150 14.0-146 99.1 35 MH,R1 delta-BHC ug/L ND 1.00 1.00 0.464 0.813 46.4 81.3 17.0-143 54.7 38 R1 gamma-BHC (Lindane) ug/L ND 1.00 1.00 0.473 1.13 47.3 113 14.0-141 82.0 40 R1 4,4'-DDD ug/L ND 1.00 1.00 0.383 0.529 38.3 52.9 10.0-160 32.0 38 4,4'-DDE ug/L ND 1.00 1.00 0.348 0.484 34.8 48.4 10.0-159 32.7 35 4,4'-DDT ug/L ND 1.00 1.00 0.349 0.472 34.9 47.2 10.0-160 30.0 38 Dieldrin ug/L ND 1.00 1.00 0.418 0.584 41.8 58.4 10.0-158 33.1 38 Endosulfan I ug/L ND 1.00 1.00 0.441 0.603 44.1 60.3 10.0-153 31.0 36 Endosulfan II ug/L ND 1.00 1.00 0.454 0.617 45.4 61.7 10.0-159 30.4 39 Endosulfan sulfate ug/L ND 1.00 1.00 0.442 0.603 44.2 60.3 23.0-147 30.8 35 Endrin ug/L ND 1.00 1.00 0.414 0.568 41.4 56.8 10.0-160 31.4 39 Endrin aldehyde ug/L ND 1.00 1.00 0.432 0.584 43.2 58.4 10.0-148 29.9 38 Endrin ketone ug/L ND 1.00 1.00 0.445 0.608 44.5 60.8 10.0-160 31.0 40 Heptachlor ug/L ND 1.00 1.00 0.386 0.787 38.6 78.7 16.0-136 68.4 40 R1 Heptachlor epoxide ug/L ND 1.00 1.00 0.413 0.562 41.3 56.2 10.0-160 30.6 36 Hexachlorobenzene ug/L ND 1.00 1.00 0.656 0.852 65.6 85.2 10.0-130 26.0 40 Methoxychlor ug/L ND 1.00 1.00 0.406 0.553 40.6 55.3 10.0-160 30.7 34 Decachlorobiphenyl (S) % 36.7 49.9 10.0-128 Tetrachloro-m-xylene (S) % 45.5 60.6 10.0-127 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 111 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 1774130 Analysis Method: EPA 8081 B QC Batch Method: 3510C Analysis Description: Pesticides (GC) 8081 B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92572199009, 92572199010 METHOD BLANK: R3730728-1 Associated Lab Samples: 92572199009, 92572199010 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Aldrin ug/L ND 0.0500 0.0198 11/17/21 12:06 alpha-BHC ug/L ND 0.0500 0.0172 11/17/21 12:06 beta-BHC ug/L ND 0.0500 0.0208 11/17/21 12:06 delta-BHC ug/L ND 0.0500 0.0150 11/17/21 12:06 gamma-BHC (Lindane) ug/L ND 0.0500 0.0209 11/17/21 12:06 4,4'-DDD ug/L ND 0.0500 0.0177 11/17/21 12:06 4,4'-DDE ug/L ND 0.0500 0.0154 11/17/21 12:06 4,4'-DDT ug/L ND 0.0500 0.0198 11/17/21 12:06 Dieldrin ug/L ND 0.0500 0.0162 11/17/21 12:06 Endosulfan I ug/L ND 0.0500 0.0160 11/17/21 12:06 Endosulfan 11 ug/L ND 0.0500 0.0164 11/17/21 12:06 Endosulfan sulfate ug/L ND 0.0500 0.0217 11/17/21 12:06 Endrin ug/L ND 0.0500 0.0161 11/17/21 12:06 Endrin aldehyde ug/L ND 0.0500 0.0237 11/17/21 12:06 Endrin ketone ug/L ND 0.0500 0.0219 11/17/21 12:06 Heptachlor ug/L ND 0.0500 0.0148 11/17/21 12:06 Heptachlor epoxide ug/L ND 0.0500 0.0183 11/17/21 12:06 Hexachlorobenzene ug/L ND 0.0500 0.0176 11/17/21 12:06 Methoxychlor ug/L ND 0.0500 0.0193 11/17/21 12:06 Chlordane (Technical) ug/L ND 5.00 0.0198 11/17/21 12:06 Toxaphene ug/L ND 0.500 0.168 11/17/21 12:06 Decachlorobiphenyl (S) % 81.8 10.0-128 11/17/21 12:06 Tetrachloro-m-xylene (S) % 73.8 10.0-127 11/17/21 12:06 LABORATORY CONTROL SAMPLE: R3730728-2 Qualifiers Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Aldrin ug/L 1.00 0.986 98.6 22.0-124 alpha-BHC ug/L 1.00 1.03 103 54.0-130 beta-BHC ug/L 1.00 1.04 104 53.0-136 delta-BHC ug/L 1.00 1.00 100 54.0-133 gamma-BHC (Lindane) ug/L 1.00 0.997 99.7 55.0-129 4,4'-DDD ug/L 1.00 0.985 98.5 56.0-140 4,4'-DDE ug/L 1.00 1.01 101 52.0-128 4,4'-DDT ug/L 1.00 0.997 99.7 50.0-141 Dieldrin ug/L 1.00 1.01 101 59.0-133 Endosulfan I ug/L 1.00 1.03 103 57.0-131 Endosulfan II ug/L 1.00 1.02 102 58.0-133 Endosulfan sulfate ug/L 1.00 0.986 98.6 58.0-133 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 112 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 LABORATORY CONTROL SAMPLE: R3730728-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Endrin ug/L 1.00 0.992 99.2 57.0-134 Endrin aldehyde ug/L 1.00 0.914 91.4 53.0-129 Endrin ketone ug/L 1.00 1.05 105 60.0-145 Heptachlor ug/L 1.00 1.00 100 27.0-132 Heptachlor epoxide ug/L 1.00 0.976 97.6 57.0-130 Hexachlorobenzene ug/L 1.00 0.974 97.4 30.0-114 Methoxychlor ug/L 1.00 1.01 101 54.0-155 Decachlorobiphenyl (S) % 105 10.0-128 Tetrachloro-m-xylene (S) % 93.1 10.0-127 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3731713-1 R3731713-2 MS MSD L1430877-01 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Aldrin ug/L ND 1.00 1.00 0.694 0.803 69.4 80.3 10.0-141 14.6 40 alpha-BHC ug/L ND 1.00 1.00 0.748 0.846 74.8 84.6 10.0-145 12.3 40 beta-BHC ug/L ND 1.00 1.00 0.797 0.874 79.7 87.4 14.0-146 9.22 35 delta-BHC ug/L ND 1.00 1.00 0.752 0.846 75.2 84.6 17.0-143 11.8 38 gamma-BHC (Lindane) ug/L ND 1.00 1.00 0.730 0.814 73.0 81.4 14.0-141 10.9 40 4,4'-DDD ug/L ND 1.00 1.00 0.733 0.864 73.3 86.4 10.0-160 16.4 38 4,4'-DDE ug/L ND 1.00 1.00 0.727 0.821 72.7 82.1 10.0-159 12.1 35 4,4'-DDT ug/L ND 1.00 1.00 0.747 0.912 74.7 91.2 10.0-160 19.9 38 Dieldrin ug/L ND 1.00 1.00 0.736 0.824 73.6 82.4 10.0-158 11.3 38 Endosulfan I ug/L ND 1.00 1.00 0.732 0.838 73.2 83.8 10.0-153 13.5 36 Endosulfan II ug/L ND 1.00 1.00 0.747 0.818 74.7 81.8 10.0-159 9.07 39 Endosulfan sulfate ug/L ND 1.00 1.00 0.884 0.826 88.4 82.6 23.0-147 6.78 35 Endrin ug/L ND 1.00 1.00 0.718 0.818 71.8 81.8 10.0-160 13.0 39 Endrin aldehyde ug/L ND 1.00 1.00 0.630 0.733 63.0 73.3 10.0-148 15.1 38 Endrin ketone ug/L ND 1.00 1.00 0.970 0.929 97.0 92.9 10.0-160 4.32 40 Heptachlor ug/L ND 1.00 1.00 0.725 0.814 72.5 81.4 16.0-136 11.6 40 Heptachlor epoxide ug/L ND 1.00 1.00 0.755 0.875 75.5 87.5 10.0-160 14.7 36 Hexachlorobenzene ug/L ND 1.00 1.00 0.744 0.822 74.4 82.2 10.0-130 9.96 40 Methoxychlor ug/L ND 1.00 1.00 0.800 0.892 80.0 89.2 10.0-160 10.9 34 P9 Decachlorobiphenyl (S) % 134 72.7 10.0-128 ST Tetrachloro-m-xylene (S) % 69.1 75.3 10.0-127 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 113 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 1774835 Analysis Method: EPA 8081 B QC Batch Method: 3510C Analysis Description: Pesticides (GC) 8081 B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92572199001 METHOD BLANK: R3730820-1 Associated Lab Samples: 92572199001 Parameter Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan 11 Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Chlordane (Technical) Toxaphene Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Matrix: Water Units Blank Result Reporting Limit MDL Analyzed ug/L ND 0.0500 0.0198 11/17/2111:49 ug/L ND 0.0500 0.0172 11/17/2111:49 ug/L ND 0.0500 0.0208 11/17/2111:49 ug/L ND 0.0500 0.0150 11/17/2111:49 ug/L ND 0.0500 0.0209 11/17/2111:49 ug/L ND 0.0500 0.0177 11/17/2111:49 ug/L ND 0.0500 0.0154 11/17/2111:49 ug/L ND 0.0500 0.0198 11/17/2111:49 ug/L ND 0.0500 0.0162 11/17/2111:49 ug/L ND 0.0500 0.0160 11/17/2111:49 ug/L ND 0.0500 0.0164 11/17/2111:49 ug/L ND 0.0500 0.0217 11/17/2111:49 ug/L ND 0.0500 0.0161 11/17/2111:49 ug/L ND 0.0500 0.0237 11/17/2111:49 ug/L ND 0.0500 0.0219 11/17/2111:49 ug/L ND 0.0500 0.0148 11/17/2111:49 ug/L ND 0.0500 0.0183 11/17/2111:49 ug/L ND 0.0500 0.0176 11/17/2111:49 ug/L ND 0.0500 0.0193 11/17/2111:49 ug/L ND 5.00 0.0198 11/17/2111:49 ug/L ND 0.500 0.168 11/17/2111:49 % 126 10.0-128 11 /17/21 11:49 % 94.5 10.0-127 11 /17/21 11:49 LABORATORY CONTROL SAMPLE: R3730820-5 Qualifiers Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Aldrin ug/L 1.00 0.819 81.9 22.0-124 alpha-BHC ug/L 1.00 1.39 139 54.0-130 LO beta-BHC ug/L 1.00 1.33 133 53.0-136 delta-BHC ug/L 1.00 1.41 141 54.0-133 LO gamma-BHC (Lindane) ug/L 1.00 1.39 139 55.0-129 LO 4,4'-DDD ug/L 1.00 1.51 151 56.0-140 LO 4,4'-DDE ug/L 1.00 1.41 141 52.0-128 LO 4,4'-DDT ug/L 1.00 1.70 170 50.0-141 LO Dieldrin ug/L 1.00 1.41 141 59.0-133 LO Endosulfan I ug/L 1.00 1.43 143 57.0-131 LO Endosulfan II ug/L 1.00 1.42 142 58.0-133 LO Endosulfan sulfate ug/L 1.00 1.41 141 58.0-133 LO Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 114 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 LABORATORY CONTROL SAMPLE: R3730820-5 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Endrin ug/L 1.00 1.50 150 57.0-134 LO Endrin aldehyde ug/L 1.00 1.25 125 53.0-129 Endrin ketone ug/L 1.00 1.43 143 60.0-145 Heptachlor ug/L 1.00 1.12 112 27.0-132 Heptachlor epoxide ug/L 1.00 1.38 138 57.0-130 LO Hexachlorobenzene ug/L 1.00 1.04 104 30.0-114 Methoxychlor ug/L 1.00 1.58 158 54.0-155 LO Decachlorobiphenyl (S) % 135 10.0-128 ST Tetrachloro-m-xylene (S) % 102 10.0-127 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3730820-6 R3730820-7 MS MSD L1430638-04 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Aldrin ug/L ND 1.00 1.00 0.954 0.899 95.4 89.9 10.0-141 5.94 40 alpha-BHC ug/L ND 1.00 1.00 1.16 1.10 116 110 10.0-145 5.31 40 beta-BHC ug/L ND 1.00 1.00 1.05 0.993 105 99.3 14.0-146 5.58 35 delta-BHC ug/L ND 1.00 1.00 1.21 1.14 121 114 17.0-143 5.96 38 gamma-BHC (Lindane) ug/L ND 1.00 1.00 1.20 1.09 120 109 14.0-141 9.61 40 4,4'-DDD ug/L ND 1.00 1.00 1.18 1.14 118 114 10.0-160 3.45 38 4,4'-DDE ug/L ND 1.00 1.00 1.11 1.09 111 109 10.0-159 1.82 35 4,4'-DDT ug/L ND 1.00 1.00 1.47 1.38 147 138 10.0-160 6.32 38 Dieldrin ug/L ND 1.00 1.00 1.13 1.09 113 109 10.0-158 3.60 38 Endosulfan I ug/L ND 1.00 1.00 1.03 1.02 103 102 10.0-153 0.976 36 Endosulfan II ug/L ND 1.00 1.00 1.08 1.07 108 107 10.0-159 0.930 39 Endosulfan sulfate ug/L ND 1.00 1.00 1.17 1.12 117 112 23.0-147 4.37 35 Endrin ug/L ND 1.00 1.00 1.20 1.15 120 115 10.0-160 4.26 39 Endrin aldehyde ug/L ND 1.00 1.00 1.01 0.986 101 98.6 10.0-148 2.40 38 Endrin ketone ug/L ND 1.00 1.00 1.44 1.19 144 119 10.0-160 19.0 40 Heptachlor ug/L ND 1.00 1.00 1.75 1.37 175 137 16.0-136 24.4 40 MH,P9 Heptachlor epoxide ug/L ND 1.00 1.00 1.12 1.07 112 107 10.0-160 4.57 36 Hexachlorobenzene ug/L ND 1.00 1.00 1.00 0.943 100 94.3 10.0-130 5.87 40 Methoxychlor ug/L ND 1.00 1.00 1.37 1.32 137 132 10.0-160 3.72 34 Decachlorobiphenyl (S) % 115 106 10.0-128 Tetrachloro-m-xylene (S) % 93.8 87.7 10.0-127 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 115 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 1775183 Analysis Method: EPA 8081 B QC Batch Method: 3510C Analysis Description: Pesticides (GC) 8081 B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92572199003, 92572199005 METHOD BLANK: R3731337-1 Associated Lab Samples: 92572199003, 92572199005 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers Aldrin ug/L ND 0.0500 0.0198 11/18/21 11:29 alpha-BHC ug/L ND 0.0500 0.0172 11/18/21 11:29 beta-BHC ug/L ND 0.0500 0.0208 11/18/21 11:29 delta-BHC ug/L ND 0.0500 0.0150 11/18/21 11:29 gamma-BHC (Lindane) ug/L ND 0.0500 0.0209 11/18/21 11:29 4,4'-DDD ug/L ND 0.0500 0.0177 11/18/21 11:29 4,4'-DDE ug/L ND 0.0500 0.0154 11/18/21 11:29 4,4'-DDT ug/L ND 0.0500 0.0198 11/18/21 11:29 Dieldrin ug/L ND 0.0500 0.0162 11/18/21 11:29 Endosulfan I ug/L ND 0.0500 0.0160 11/18/21 11:29 Endosulfan 11 ug/L ND 0.0500 0.0164 11/18/21 11:29 Endosulfan sulfate ug/L ND 0.0500 0.0217 11/18/21 11:29 Endrin ug/L ND 0.0500 0.0161 11/18/21 11:29 Endrin aldehyde ug/L ND 0.0500 0.0237 11/18/21 11:29 Endrin ketone ug/L ND 0.0500 0.0219 11/18/21 11:29 Heptachlor ug/L ND 0.0500 0.0148 11/18/21 11:29 Heptachlor epoxide ug/L ND 0.0500 0.0183 11/18/21 11:29 Hexachlorobenzene ug/L ND 0.0500 0.0176 11/18/21 11:29 Methoxychlor ug/L ND 0.0500 0.0193 11/18/21 11:29 Chlordane (Technical) ug/L ND 5.00 0.0198 11/18/21 11:29 Toxaphene ug/L ND 0.500 0.168 11/18/21 11:29 Decachlorobiphenyl (S) % 30.6 10.0-128 11/18/21 11:29 Tetrachloro-m-xylene (S) % 91.8 10.0-127 11/18/21 11:29 LABORATORY CONTROL SAMPLE & LCSD: Parameter R3731337-2 Spike Units Conc. R3731337-3 LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Limits RPD Max RPD Qualifiers Aldrin ug/L 1.00 0.881 0.844 88.1 84.4 22.0-124 4.29 34 alpha-BHC ug/L 1.00 1.03 1.03 103 103 54.0-130 0.00 23 beta-BHC ug/L 1.00 0.998 0.995 99.8 99.5 53.0-136 0.301 20 delta-BHC ug/L 1.00 1.02 1.03 102 103 54.0-133 0.976 20 gamma-BHC (Lindane) ug/L 1.00 1.02 1.01 102 101 55.0-129 0.985 20 4,4'-DDD ug/L 1.00 0.961 0.922 96.1 92.2 56.0-140 4.14 22 4,4'-DDE ug/L 1.00 0.904 0.886 90.4 88.6 52.0-128 2.01 22 4,4'-DDT ug/L 1.00 0.933 0.918 93.3 91.8 50.0-141 1.62 23 Dieldrin ug/L 1.00 0.990 0.951 99.0 95.1 59.0-133 4.02 20 Endosulfan I ug/L 1.00 0.983 0.948 98.3 94.8 57.0-131 3.63 20 Endosulfan II ug/L 1.00 0.966 0.937 96.6 93.7 58.0-133 3.05 20 Endosulfan sulfate ug/L 1.00 0.913 0.896 91.3 89.6 58.0-133 1.88 21 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 116 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 LABORATORY CONTROL SAMPLE & LCSD: R3731337-2 R3731337-3 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Endrin ug/L 1.00 1.00 0.967 100 96.7 57.0-134 3.36 21 Endrin aldehyde ug/L 1.00 0.848 0.859 84.8 85.9 53.0-129 1.29 20 Endrin ketone ug/L 1.00 0.976 0.952 97.6 95.2 60.0-145 2.49 20 Heptachlor ug/L 1.00 0.966 0.936 96.6 93.6 27.0-132 3.15 31 Heptachlor epoxide ug/L 1.00 0.941 0.905 94.1 90.5 57.0-130 3.90 20 Hexachlorobenzene ug/L 1.00 0.950 0.945 95.0 94.5 30.0-114 0.528 30 Methoxychlor ug/L 1.00 0.919 0.878 91.9 87.8 54.0-155 4.56 24 Decachlorobiphenyl (S) % 54.4 53.9 10.0-128 Tetrachloro-m-xylene (S) % 89.4 87.6 10.0-127 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 117 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 1775935 Analysis Method: EPA 8081 B QC Batch Method: 3510C Analysis Description: Pesticides (GC) 8081 B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92572199008, 92572199013 METHOD BLANK: R3731646-1 Associated Lab Samples: 92572199008, 92572199013 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Aldrin ug/L ND 0.0500 0.0198 11/19/21 07:04 alpha-BHC ug/L ND 0.0500 0.0172 11/19/21 07:04 beta-BHC ug/L ND 0.0500 0.0208 11/19/21 07:04 delta-BHC ug/L ND 0.0500 0.0150 11/19/21 07:04 gamma-BHC (Lindane) ug/L ND 0.0500 0.0209 11/19/21 07:04 4,4'-DDD ug/L ND 0.0500 0.0177 11/19/21 07:04 4,4'-DDE ug/L ND 0.0500 0.0154 11/19/21 07:04 4,4'-DDT ug/L ND 0.0500 0.0198 11/19/21 07:04 Dieldrin ug/L ND 0.0500 0.0162 11/19/21 07:04 Endosulfan I ug/L ND 0.0500 0.0160 11/19/21 07:04 Endosulfan 11 ug/L ND 0.0500 0.0164 11/19/21 07:04 Endosulfan sulfate ug/L ND 0.0500 0.0217 11/19/21 07:04 Endrin ug/L ND 0.0500 0.0161 11/19/21 07:04 Endrin aldehyde ug/L ND 0.0500 0.0237 11/19/21 07:04 Endrin ketone ug/L ND 0.0500 0.0219 11/19/21 07:04 Heptachlor ug/L ND 0.0500 0.0148 11/19/21 07:04 Heptachlor epoxide ug/L ND 0.0500 0.0183 11/19/21 07:04 Hexachlorobenzene ug/L ND 0.0500 0.0176 11/19/21 07:04 Methoxychlor ug/L ND 0.0500 0.0193 11/19/21 07:04 Chlordane (Technical) ug/L ND 5.00 0.0198 11/19/21 07:04 Toxaphene ug/L ND 0.500 0.168 11/19/21 07:04 Decachlorobiphenyl (S) % 57 10.0-128 11/19/21 07:04 Tetrachloro-m-xylene (S) % 98.9 10.0-127 11/19/21 07:04 LABORATORY CONTROL SAMPLE: R3731646-2 Qualifiers Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Aldrin ug/L 1.00 0.955 95.5 22.0-124 alpha-BHC ug/L 1.00 1.12 112 54.0-130 beta-BHC ug/L 1.00 1.10 110 53.0-136 delta-BHC ug/L 1.00 1.09 109 54.0-133 gamma-BHC (Lindane) ug/L 1.00 1.12 112 55.0-129 4,4'-DDD ug/L 1.00 0.989 98.9 56.0-140 4,4'-DDE ug/L 1.00 0.969 96.9 52.0-128 4,4'-DDT ug/L 1.00 0.828 82.8 50.0-141 Dieldrin ug/L 1.00 1.06 106 59.0-133 Endosulfan I ug/L 1.00 1.06 106 57.0-131 Endosulfan II ug/L 1.00 1.07 107 58.0-133 Endosulfan sulfate ug/L 1.00 1.06 106 58.0-133 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 118 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 LABORATORY CONTROL SAMPLE: R3731646-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Endrin ug/L 1.00 1.05 105 57.0-134 Endrin aldehyde ug/L 1.00 0.885 88.5 53.0-129 Endrin ketone ug/L 1.00 1.16 116 60.0-145 Heptachlor ug/L 1.00 1.02 102 27.0-132 Heptachlor epoxide ug/L 1.00 1.06 106 57.0-130 Hexachlorobenzene ug/L 1.00 1.12 112 30.0-114 Methoxychlor ug/L 1.00 0.975 97.5 54.0-155 Decachlorobiphenyl (S) % 90.9 10.0-128 Tetrachloro-m-xylene (S) % 99.2 10.0-127 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3731646-3 R3731646-4 MS MSD L1430638-05 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Aldrin ug/L ND 1.00 1.00 0.696 0.520 69.6 52.0 10.0-141 28.9 40 P9 alpha-BHC ug/L ND 1.00 1.00 0.766 0.704 76.6 70.4 10.0-145 8.44 40 beta-BHC ug/L ND 1.00 1.00 0.821 0.777 82.1 77.7 14.0-146 5.51 35 delta-BHC ug/L ND 1.00 1.00 0.805 0.754 80.5 75.4 17.0-143 6.54 38 gamma-BHC (Lindane) ug/L ND 1.00 1.00 0.761 0.660 76.1 66.0 14.0-141 14.2 40 4,4'-DDD ug/L ND 1.00 1.00 0.466 0.292 46.6 29.2 10.0-160 45.9 38 R1 4,4'-DDE ug/L ND 1.00 1.00 0.372 0.196 37.2 19.6 10.0-159 62.0 35 R1 4,4'-DDT ug/L ND 1.00 1.00 0.420 0.206 42.0 20.6 10.0-160 68.4 38 R1 Dieldrin ug/L ND 1.00 1.00 0.575 0.440 57.5 44.0 10.0-158 26.6 38 Endosulfan I ug/L ND 1.00 1.00 0.572 0.446 57.2 44.6 10.0-153 24.8 36 Endosulfan II ug/L ND 1.00 1.00 0.639 0.530 63.9 53.0 10.0-159 18.6 39 Endosulfan sulfate ug/L ND 1.00 1.00 0.719 0.575 71.9 57.5 23.0-147 22.3 35 Endrin ug/L ND 1.00 1.00 0.609 0.445 60.9 44.5 10.0-160 31.1 39 Endrin aldehyde ug/L ND 1.00 1.00 0.623 0.565 62.3 56.5 10.0-148 9.76 38 Endrin ketone ug/L ND 1.00 1.00 0.759 0.639 75.9 63.9 10.0-160 17.2 40 Heptachlor ug/L ND 1.00 1.00 0.605 0.334 60.5 33.4 16.0-136 57.7 40 R1 Heptachlor epoxide ug/L ND 1.00 1.00 0.534 0.423 53.4 42.3 10.0-160 23.2 36 Hexachlorobenzene ug/L ND 1.00 1.00 1.04 0.749 104 74.9 10.0-130 32.5 40 P9 Methoxychlor ug/L ND 1.00 1.00 0.546 0.360 54.6 36.0 10.0-160 41.1 34 R1 Decachlorobiphenyl (S) % 44.9 24.8 10.0-128 Tetrachloro-m-xylene (S) % 56.4 37.4 10.0-127 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 119 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 1776686 Analysis Method: EPA 8081 B QC Batch Method: 3510C Analysis Description: Pesticides (GC) 8081 B Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92572199004, 92572199006, 92572199007 METHOD BLANK: R3732913-1 Matrix: Associated Lab Samples: 92572199004, 92572199006, 92572199007 Blank Parameter Units Result Water Reporting Limit MDL Analyzed Qualifiers Aldrin ug/L ND 0.0500 0.0198 11/19/21 22:49 alpha-BHC ug/L ND 0.0500 0.0172 11/19/21 22:49 beta-BHC ug/L ND 0.0500 0.0208 11/19/21 22:49 delta-BHC ug/L ND 0.0500 0.0150 11/19/21 22:49 gamma-BHC (Lindane) ug/L ND 0.0500 0.0209 11/19/21 22:49 4,4'-DDD ug/L ND 0.0500 0.0177 11/19/21 22:49 4,4'-DDE ug/L ND 0.0500 0.0154 11/19/21 22:49 4,4'-DDT ug/L ND 0.0500 0.0198 11/19/21 22:49 Dieldrin ug/L ND 0.0500 0.0162 11/19/21 22:49 Endosulfan I ug/L ND 0.0500 0.0160 11/19/21 22:49 Endosulfan 11 ug/L ND 0.0500 0.0164 11/19/21 22:49 Endosulfan sulfate ug/L ND 0.0500 0.0217 11/19/21 22:49 Endrin ug/L ND 0.0500 0.0161 11/19/21 22:49 Endrin aldehyde ug/L ND 0.0500 0.0237 11/19/21 22:49 Endrin ketone ug/L ND 0.0500 0.0219 11/19/21 22:49 Heptachlor ug/L ND 0.0500 0.0148 11/19/21 22:49 Heptachlor epoxide ug/L ND 0.0500 0.0183 11/19/21 22:49 Hexachlorobenzene ug/L ND 0.0500 0.0176 11/19/21 22:49 Methoxychlor ug/L ND 0.0500 0.0193 11/19/21 22:49 Chlordane (Technical) ug/L ND 5.00 0.0198 11/19/21 22:49 Toxaphene ug/L ND 0.500 0.168 11/19/21 22:49 Decachlorobiphenyl (S) % 92.7 10.0-128 11/19/21 22:49 Tetrachloro-m-xylene (S) % 77.9 10.0-127 11/19/21 22:49 LABORATORY CONTROL SAMPLE: Parameter R3732913-2 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Aldrin ug/L 1.00 0.879 87.9 22.0-124 alpha-BHC ug/L 1.00 1.07 107 54.0-130 beta-BHC ug/L 1.00 1.03 103 53.0-136 delta-BHC ug/L 1.00 1.09 109 54.0-133 gamma-BHC (Lindane) ug/L 1.00 1.06 106 55.0-129 4,4'-DDD ug/L 1.00 1.03 103 56.0-140 4,4'-DDE ug/L 1.00 1.02 102 52.0-128 4,4'-DDT ug/L 1.00 1.09 109 50.0-141 Dieldrin ug/L 1.00 1.05 105 59.0-133 Endosulfan I ug/L 1.00 1.07 107 57.0-131 Endosulfan II ug/L 1.00 0.967 96.7 58.0-133 Endosulfan sulfate ug/L 1.00 0.965 96.5 58.0-133 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 120 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 LABORATORY CONTROL SAMPLE: R3732913-2 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Endrin ug/L 1.00 1.04 104 57.0-134 Endrin aldehyde ug/L 1.00 0.806 80.6 53.0-129 Endrin ketone ug/L 1.00 1.02 102 60.0-145 Heptachlor ug/L 1.00 1.21 121 27.0-132 Heptachlor epoxide ug/L 1.00 1.07 107 57.0-130 Hexachlorobenzene ug/L 1.00 0.983 98.3 30.0-114 Methoxychlor ug/L 1.00 1.15 115 54.0-155 Decachlorobiphenyl (S) % 59.0 10.0-128 Tetrachloro-m-xylene (S) % 84.8 10.0-127 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3732913-3 R3732913-4 MS MSD L1432341-19 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Aldrin ug/L ND 0.970 0.952 0.753 0.780 77.6 81.9 10.0-141 3.52 40 P9 alpha-BHC ug/L ND 0.970 0.952 0.914 0.951 94.2 99.9 10.0-145 3.97 40 P9 beta-BHC ug/L ND 0.970 0.952 0.934 0.933 96.3 98.0 14.0-146 0.107 35 P9 delta-BHC ug/L ND 0.970 0.952 1.04 1.04 107 109 17.0-143 0.00 38 P9 gamma-BHC (Lindane) ug/L ND 0.970 0.952 0.944 0.962 97.3 101 14.0-141 1.89 40 P9 4,4'-DDD ug/L ND 0.970 0.952 1.01 1.04 104 109 10.0-160 2.93 38 P9 4,4'-DDE ug/L ND 0.970 0.952 0.951 0.988 98.0 104 10.0-159 3.82 35 P9 4,4'-DDT ug/L ND 0.970 0.952 1.09 1.13 112 119 10.0-160 3.60 38 P9 Dieldrin ug/L ND 0.970 0.952 1.00 1.03 103 108 10.0-158 2.96 38 P9 Endosulfan I ug/L ND 0.970 0.952 1.00 0.961 103 101 10.0-153 3.98 36 P9 Endosulfan II ug/L ND 0.970 0.952 0.945 0.974 97.4 102 10.0-159 3.02 39 P9 Endosulfan sulfate ug/L ND 0.970 0.952 0.938 0.954 96.7 100 23.0-147 1.69 35 P9 Endrin ug/L ND 0.970 0.952 0.972 1.00 100 105 10.0-160 2.84 39 P9 Endrin aldehyde ug/L ND 0.970 0.952 0.795 0.819 82.0 86.0 10.0-148 2.97 38 P9 Endrin ketone ug/L ND 0.970 0.952 0.998 1.01 103 106 10.0-160 1.20 40 P9 Heptachlor ug/L ND 0.970 0.952 1.04 1.07 107 112 16.0-136 2.84 40 P9 Heptachlor epoxide ug/L ND 0.970 0.952 0.972 0.994 100 104 10.0-160 2.24 36 P9 Hexachlorobenzene ug/L ND 0.970 0.952 0.681 0.771 70.2 81.0 10.0-130 12.4 40 P9 Methoxychlor ug/L ND 0.970 0.952 1.11 1.13 114 119 10.0-160 1.79 34 P9 Decachlorobiphenyl (S) % 75.2 77.2 10.0-128 Tetrachloro-m-xylene (S) % 60.8 70.5 10.0-127 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 121 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 1774237 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199019, 92572199020 METHOD BLANK: R3731171-1 Matrix: Water Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199019, 92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed 2,4-D ug/L ND 2.00 0.547 11/16/21 18:31 Dalapon ug/L ND 2.00 0.344 11/16/21 18:31 2,4-DB ug/L ND 2.00 0.302 11/16/21 18:31 Dicamba ug/L ND 2.00 0.245 11/16/21 18:31 Dichloroprop ug/L ND 2.00 1.04 11/16/21 18:31 Dinoseb ug/L ND 2.00 0.250 11/16/21 18:31 MCPA ug/L ND 100 13.1 11/16/21 18:31 MCPP ug/L ND 100 66.0 11/16/21 18:31 2,4,5-T ug/L ND 2.00 0.258 11/16/21 18:31 2,4,5-TP (Silvex) ug/L ND 2.00 0.335 11/16/21 18:31 2,4-DCAA (S) % 101 14.0-158 11/16/21 18:31 Qualifiers LABORATORY CONTROL SAMPLE: Parameter R3731171-2 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,4-D ug/L 5.00 5.72 114 50.0-120 Dalapon ug/L 5.00 11.9 238 32.0-120 E,LO 2,4-DB ug/L 5.00 5.42 108 53.0-140 Dicamba ug/L 5.00 5.29 106 51.0-120 Dichloroprop ug/L 5.00 5.21 104 55.0-127 Dinoseb ug/L 5.00 4.43 88.6 36.0-134 MCPA ug/L 500 512 102 10.0-160 E,P9 MCPP ug/L 500 341 68.2 10.0-160 E 2,4,5-T ug/L 5.00 5.27 105 54.0-120 2,4,5-TP (Silvex) ug/L 5.00 5.23 105 50.0-125 2,4-DCAA (S) % 114 14.0-158 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 122 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 1774587 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92572199009, 92572199010 METHOD BLANK: R3731172-1 Associated Lab Samples: 92572199009, 92572199010 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 2,4-D ug/L ND 2.00 0.547 11/16/21 18:58 Dalapon ug/L ND 2.00 0.344 11/16/21 18:58 2,4-DB ug/L ND 2.00 0.302 11/16/21 18:58 Dicamba ug/L ND 2.00 0.245 11/16/21 18:58 Dichloroprop ug/L ND 2.00 1.04 11/16/21 18:58 Dinoseb ug/L ND 2.00 0.250 11/16/21 18:58 MCPA ug/L ND 100 13.1 11/16/21 18:58 MCPP ug/L ND 100 66.0 11/16/21 18:58 2,4,5-T ug/L ND 2.00 0.258 11/16/21 18:58 2,4,5-TP (Silvex) ug/L ND 2.00 0.335 11/16/21 18:58 2,4-DCAA (S) % 97 14.0-158 11/16/21 18:58 LABORATORY CONTROL SAMPLE: R3731172-2 Parameter Units 2,4-D ug/L Dalapon ug/L 2,4-DB ug/L Dicamba ug/L Dichloroprop ug/L Dinoseb ug/L MCPA ug/L MCPP ug/L 2,4,5-T ug/L 2,4,5-TP (Silvex) ug/L 2,4-DCAA (S) % Qualifiers Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 5.00 7.15 143 50.0-120 LO 5.00 13.3 266 32.0-120 E, LO 5.00 7.03 141 53.0-140 LO 5.00 6.49 130 51.0-120 LO 5.00 6.44 129 55.0-127 LO 5.00 5.73 115 36.0-134 500 438 87.6 10.0-160 E 500 404 80.8 10.0-160 E 5.00 6.60 132 54.0-120 LO 5.00 6.54 131 50.0-125 LO 121 14.0-158 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 123 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 1774793 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92572199001 METHOD BLANK: R3731007-1 Associated Lab Samples: 92572199001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 2,4-D ug/L ND 2.00 0.547 11/17/21 16:06 Dalapon ug/L ND 2.00 0.344 11/17/21 16:06 2,4-DB ug/L ND 2.00 0.302 11/17/21 16:06 Dicamba ug/L ND 2.00 0.245 11/17/21 16:06 Dichloroprop ug/L ND 2.00 1.04 11/17/21 16:06 Dinoseb ug/L ND 2.00 0.250 11/17/21 16:06 MCPA ug/L ND 100 13.1 11/17/21 16:06 MCPP ug/L ND 100 66.0 11/17/21 16:06 2,4,5-T ug/L ND 2.00 0.258 11/17/21 16:06 2,4,5-TP (Silvex) ug/L ND 2.00 0.335 11/17/21 16:06 2,4-DCAA (S) % 67.8 14.0-158 11/17/21 16:06 Qualifiers LABORATORY CONTROL SAMPLE & LCSD: R3731007-2 R3731007-3 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 2,4-D ug/L 5.00 5.43 3.54 109 70.8 50.0-120 42.1 20 R1 Dalapon ug/L 5.00 6.82 3.42 136 68.4 32.0-120 66.4 20 L0,P9,R1 2,4-DB ug/L 5.00 5.92 3.52 118 70.4 53.0-140 50.8 20 R1 Dicamba ug/L 5.00 5.08 3.81 102 76.2 51.0-120 28.6 20 R1 Dichloroprop ug/L 5.00 4.63 3.06 92.6 61.2 55.0-127 40.8 20 R1 Dinoseb ug/L 5.00 4.50 2.97 90.0 59.4 36.0-134 41.0 20 P9,R1 MCPA ug/L 500 547 324 109 64.8 10.0-160 51.2 40 E,P9,R1 MCPP ug/L 500 389 293 77.8 58.6 10.0-160 28.2 23 E,P9,R1 2,4,5-T ug/L 5.00 4.58 3.85 91.6 77.0 54.0-120 17.3 20 P9 2,4,5-TP (Silvex) ug/L 5.00 3.96 3.45 79.2 69.0 50.0-125 13.8 20 2,4-DCAA (S) % 99.8 62.0 14.0-158 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 124 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 1775491 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92572199003, 92572199005, 92572199008, 92572199013 METHOD BLANK: R3731590-1 Matrix: Water Associated Lab Samples: 92572199003, 92572199005, 92572199008, 92572199013 Blank Reporting Parameter Units Result Limit MDL Analyzed 2,4-D ug/L ND 2.00 0.547 11/18/21 13:46 Dalapon ug/L ND 2.00 0.344 11/18/21 13:46 2,4-DB ug/L ND 2.00 0.302 11/18/21 13:46 Dicamba ug/L ND 2.00 0.245 11/18/21 13:46 Dichloroprop ug/L ND 2.00 1.04 11/18/21 13:46 Dinoseb ug/L ND 2.00 0.250 11/18/21 13:46 MCPA ug/L ND 100 13.1 11/18/21 13:46 MCPP ug/L ND 100 66.0 11/18/21 13:46 2,4,5-T ug/L ND 2.00 0.258 11/18/21 13:46 2,4,5-TP (Silvex) ug/L ND 2.00 0.335 11/18/21 13:46 2,4-DCAA (S) % 72.8 14.0-158 11/18/21 13:46 Qualifiers LABORATORY CONTROL SAMPLE: Parameter R3731590-2 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,4-D ug/L 5.00 4.25 85.0 50.0-120 P9 Dalapon ug/L 5.00 5.00 100 32.0-120 2,4-DB ug/L 5.00 4.28 85.6 53.0-140 Dicamba ug/L 5.00 4.55 91.0 51.0-120 Dichloroprop ug/L 5.00 3.72 74.4 55.0-127 Dinoseb ug/L 5.00 3.67 73.4 36.0-134 P9 MCPA ug/L 500 377 75.4 10.0-160 E,P9 MCPP ug/L 500 314 62.8 10.0-160 E,P9 2,4,5-T ug/L 5.00 4.20 84.0 54.0-120 P9 2,4,5-TP (Silvex) ug/L 5.00 3.70 74.0 50.0-125 2,4-DCAA (S) % 69.4 14.0-158 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 125 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 1776016 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92572199004, 92572199006, 92572199007 METHOD BLANK: R3731591-1 Matrix: Water Associated Lab Samples: 92572199004, 92572199006, 92572199007 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4-D ug/L ND 2.00 0.547 11/18/21 14:48 Dalapon ug/L ND 2.00 0.344 11/18/21 14:48 2,4-DB ug/L ND 2.00 0.302 11/18/21 14:48 Dicamba ug/L ND 2.00 0.245 11/18/21 14:48 Dichloroprop ug/L ND 2.00 1.04 11/18/21 14:48 Dinoseb ug/L ND 2.00 0.250 11/18/21 14:48 MCPA ug/L ND 100 13.1 11/18/21 14:48 MCPP ug/L ND 100 66.0 11/18/21 14:48 2,4,5-T ug/L ND 2.00 0.258 11/18/21 14:48 2,4,5-TP (Silvex) ug/L ND 2.00 0.335 11/18/21 14:48 2,4-DCAA (S) % 96.6 14.0-158 11/18/21 14:48 LABORATORY CONTROL SAMPLE & LCSD: R3731591-2 R3731591-3 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 2,4-D ug/L 5.00 6.41 6.50 128 130 50.0-120 1.39 20 LO,P9 Dalapon ug/L 5.00 6.89 7.22 138 144 32.0-120 4.68 20 LO 2,4-DB ug/L 5.00 6.72 6.90 134 138 53.0-140 2.64 20 P9 Dicamba ug/L 5.00 5.62 5.65 112 113 51.0-120 0.532 20 Dichloroprop ug/L 5.00 5.56 5.63 111 113 55.0-127 1.25 20 Dinoseb ug/L 5.00 4.95 5.15 99.0 103 36.0-134 3.96 20 P9 MCPA ug/L 500 523 524 105 105 10.0-160 0.191 40 E,P9 MCPP ug/L 500 463 474 92.6 94.8 10.0-160 2.35 23 E,P9 2,4,5-T ug/L 5.00 4.59 4.57 91.8 91.4 54.0-120 0.437 20 2,4,5-TP (Silvex) ug/L 5.00 4.16 4.16 83.2 83.2 50.0-125 0.00 20 2,4-DCAA (S) % 103 108 14.0-158 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 126 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660190 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008,92572199009,92572199010,92572199011,92572199012,92572199013,92572199014, 92572199015,92572199016,92572199017,92572199018,92572199019,92572199020 METHOD BLANK: 3459272 Matrix: Water Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008,92572199009,92572199010,92572199011,92572199012,92572199013,92572199014, 92572199015,92572199016,92572199017,92572199018,92572199019,92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.12 11/25/2108:53 LABORATORY CONTROL SAMPLE: 3459273 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.6 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3459274 3459275 MS MSD 92572199001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L 3.1 2.5 2.5 5.5 5.0 94 75 75-125 9 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 127 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660178 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008,92572199009,92572199010,92572199011,92572199012,92572199013 METHOD BLANK: 3459210 Matrix: Water Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008,92572199009,92572199010,92572199011,92572199012,92572199013 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Antimony ug/L ND 5.0 3.0 11/29/2116:55 Arsenic ug/L ND 10.0 4.7 11/29/2116:55 Barium ug/L ND 5.0 3.5 11/29/2116:55 Beryllium ug/L ND 1.0 0.70 11/29/2116:55 Cadmium ug/L ND 1.0 0.40 11/29/2116:55 Chromium ug/L ND 5.0 3.7 11/29/2116:55 Cobalt ug/L ND 5.0 3.6 11/29/2116:55 Copper ug/L ND 5.0 4.3 11/29/2116:55 Iron ug/L ND 50.0 41.5 11/29/2116:55 Lead ug/L ND 5.0 4.5 11/29/2116:55 Manganese ug/L ND 5.0 3.4 11/29/2116:55 Nickel ug/L ND 5.0 3.5 11/29/2116:55 Selenium ug/L ND 10.0 4.7 11/29/2116:55 Silver ug/L ND 5.0 2.5 11/29/2116:55 Sodium ug/L ND 5000 611 11/29/2116:55 Tin ug/L ND 5.0 4.7 11/29/2116:55 Vanadium ug/L ND 5.0 3.9 11/29/2116:55 Zinc ug/L ND 10.0 9.5 11/29/2116:55 LABORATORY CONTROL SAMPLE: 3459211 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 500 464 93 80-120 Arsenic ug/L 500 468 94 80-120 Barium ug/L 500 485 97 80-120 Beryllium ug/L 500 490 98 80-120 Cadmium ug/L 500 472 94 80-120 Chromium ug/L 500 464 93 80-120 Cobalt ug/L 500 454 91 80-120 Copper ug/L 500 486 97 80-120 Iron ug/L 5000 4770 95 80-120 Lead ug/L 500 473 95 80-120 Manganese ug/L 500 461 92 80-120 Nickel ug/L 500 468 94 80-120 Selenium ug/L 500 458 92 80-120 Silver ug/L 250 234 94 80-120 Sodium ug/L 5000 4810J 96 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 128 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 LABORATORY CONTROL SAMPLE: 3459211 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Tin ug/L 500 463 93 80-120 Vanadium ug/L 500 466 93 80-120 Zinc ug/L 500 461 92 80-120 MATRIX SPIKE & MATRIX Parameter SPIKE DUPLICATE: 3459797 MS 92572115001 Spike Units Result Conc. MSD Spike Conc. 3459798 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual Antimony ug/L ND 500 500 486 492 97 98 75-125 1 20 Arsenic ug/L ND 500 500 482 481 96 96 75-125 0 20 Barium ug/L 7.4 500 500 490 496 96 98 75-125 1 20 Beryllium ug/L ND 500 500 486 492 97 98 75-125 1 20 Cadmium ug/L ND 500 500 490 495 98 99 75-125 1 20 Chromium ug/L ND 500 500 478 488 95 97 75-125 2 20 Cobalt ug/L ND 500 500 465 469 93 94 75-125 1 20 Copper ug/L ND 500 500 496 500 99 100 75-125 1 20 Iron ug/L 185 5000 5000 5040 5060 97 98 75-125 0 20 Lead ug/L ND 500 500 486 490 97 98 75-125 1 20 Manganese ug/L ND 500 500 481 484 96 96 75-125 1 20 Nickel ug/L ND 500 500 482 486 96 97 75-125 1 20 Selenium ug/L ND 500 500 509 515 102 103 75-125 1 20 Silver ug/L ND 250 250 243 245 97 98 75-125 1 20 Sodium ug/L 3460J 5000 5000 8250 8300 96 97 75-125 1 20 Tin ug/L ND 500 500 483 488 97 98 75-125 1 20 Vanadium ug/L ND 500 500 482 490 96 98 75-125 1 20 Zinc ug/L ND 500 500 483 488 96 97 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 129 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660179 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199014, 92572199015, 92572199016, 92572199017, 92572199018, 92572199019, 92572199020 METHOD BLANK: 3459215 Matrix: Water Associated Lab Samples: 92572199014, 92572199015, 92572199016, 92572199017, 92572199018, 92572199019, 92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Antimony ug/L ND 5.0 3.0 11/30/2100:06 Arsenic ug/L ND 10.0 4.7 11/30/2100:06 Barium ug/L ND 5.0 3.5 11/30/2100:06 Beryllium ug/L ND 1.0 0.70 11/30/2100:06 Cadmium ug/L ND 1.0 0.40 11/30/2100:06 Chromium ug/L ND 5.0 3.7 11/30/2100:06 Cobalt ug/L ND 5.0 3.6 11/30/2100:06 Copper ug/L ND 5.0 4.3 11/30/2100:06 Iron ug/L ND 50.0 41.5 11/30/2100:06 Lead ug/L ND 5.0 4.5 11/30/2100:06 Manganese ug/L ND 5.0 3.4 11/30/2100:06 Nickel ug/L ND 5.0 3.5 11/30/2100:06 Selenium ug/L ND 10.0 4.7 11/30/2100:06 Silver ug/L ND 5.0 2.5 11/30/2100:06 Sodium ug/L ND 5000 611 11/30/2100:06 Tin ug/L ND 5.0 4.7 11/30/2100:06 Vanadium ug/L ND 5.0 3.9 11/30/2100:06 Zinc ug/L ND 10.0 9.5 11/30/2100:06 LABORATORY CONTROL SAMPLE: Parameter 3459216 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 500 506 101 80-120 Arsenic ug/L 500 503 101 80-120 Barium ug/L 500 502 100 80-120 Beryllium ug/L 500 501 100 80-120 Cadmium ug/L 500 498 100 80-120 Chromium ug/L 500 492 98 80-120 Cobalt ug/L 500 490 98 80-120 Copper ug/L 500 499 100 80-120 Iron ug/L 5000 4780 96 80-120 Lead ug/L 500 508 102 80-120 Manganese ug/L 500 465 93 80-120 Nickel ug/L 500 496 99 80-120 Selenium ug/L 500 501 100 80-120 Silver ug/L 250 242 97 80-120 Sodium ug/L 5000 4930J 99 80-120 Tin ug/L 500 501 100 80-120 Vanadium ug/L 500 499 100 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 130 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 LABORATORY CONTROL SAMPLE: 3459216 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Zinc ug/L 500 502 100 80-120 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3459217 3459218 MS MSD 92572199014 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 525 520 104 103 75-125 1 20 Arsenic ug/L ND 500 500 510 498 101 99 75-125 2 20 Barium ug/L 16.1 500 500 509 511 99 99 75-125 0 20 Beryllium ug/L ND 500 500 495 498 99 100 75-125 1 20 Cadmium ug/L ND 500 500 507 508 101 101 75-125 0 20 Chromium ug/L ND 500 500 493 496 98 99 75-125 1 20 Cobalt ug/L ND 500 500 481 482 96 96 75-125 0 20 Copper ug/L ND 500 500 496 501 98 100 75-125 1 20 Iron ug/L 166 5000 5000 4870 4910 94 95 75-125 1 20 Lead ug/L ND 500 500 500 503 100 101 75-125 1 20 Manganese ug/L 314 500 500 764 766 90 90 75-125 0 20 Nickel ug/L ND 500 500 490 491 97 98 75-125 0 20 Selenium ug/L ND 500 500 532 536 106 107 75-125 1 20 Silver ug/L ND 250 250 250 249 100 99 75-125 1 20 Sodium ug/L 15700 5000 5000 20000 20000 86 85 75-125 0 20 Tin ug/L ND 500 500 512 515 102 103 75-125 1 20 Vanadium ug/L ND 500 500 509 512 101 102 75-125 1 20 Zinc ug/L 11.2 500 500 512 511 100 100 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 131 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659690 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199016 METHOD BLANK: 3457145 Matrix: Water Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199016 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 11/13/21 11:42 1,1,1-Trichloroethane ug/L ND 1.0 0.33 11/13/21 11:42 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 11/13/21 11:42 1,1,2-Trichloroethane ug/L ND 1.0 0.32 11/13/21 11:42 1,1-Dichloroethane ug/L ND 1.0 0.37 11/13/21 11:42 1,1-Dichloroethene ug/L ND 1.0 0.35 11/13/21 11:42 1,2,3-Trichloropropane ug/L ND 1.0 0.26 11/13/21 11:42 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 11/13/21 11:42 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 11/13/21 11:42 1,2-Dichlorobenzene ug/L ND 1.0 0.34 11/13/21 11:42 1,2-Dichloroethane ug/L ND 1.0 0.32 11/13/21 11:42 1,2-Dichloropropane ug/L ND 1.0 0.36 11/13/21 11:42 1,4-Dichlorobenzene ug/L ND 1.0 0.33 11/13/21 11:42 2-Butanone (MEK) ug/L ND 5.0 4.0 11/13/21 11:42 2-Hexanone ug/L ND 5.0 0.48 11/13/21 11:42 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 11/13/21 11:42 Acetone ug/L ND 25.0 5.1 11/13/21 11:42 Acrylonitrile ug/L ND 10.0 1.8 11/13/21 11:42 Benzene ug/L ND 1.0 0.34 11/13/21 11:42 Bromochloromethane ug/L ND 1.0 0.47 11/13/21 11:42 Bromodichloromethane ug/L ND 1.0 0.31 11/13/21 11:42 Bromoform ug/L ND 1.0 0.34 11/13/21 11:42 Bromomethane ug/L ND 2.0 1.7 11/13/21 11:42 Carbon disulfide ug/L ND 2.0 0.73 11/13/21 11:42 Carbon tetrachloride ug/L ND 1.0 0.33 11/13/21 11:42 Chlorobenzene ug/L ND 1.0 0.28 11/13/21 11:42 Chloroethane ug/L ND 1.0 0.65 11/13/21 11:42 Chloroform ug/L ND 1.0 0.43 11/13/21 11:42 Chloromethane ug/L ND 1.0 0.54 11/13/21 11:42 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 11/13/21 11:42 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 11/13/21 11:42 Dibromochloromethane ug/L ND 1.0 0.36 11/13/21 11:42 Dibromomethane ug/L ND 1.0 0.39 11/13/21 11:42 Dichlorodifluoromethane ug/L ND 1.0 0.35 11/13/21 11:42 Ethylbenzene ug/L ND 1.0 0.30 11/13/21 11:42 lodomethane ug/L ND 20.0 9.7 11/13/21 11:42 m&p-Xylene ug/L ND 2.0 0.71 11/13/21 11:42 Methylene Chloride ug/L ND 5.0 2.0 11/13/21 11:42 o-Xylene ug/L ND 1.0 0.34 11/13/21 11:42 Styrene ug/L ND 1.0 0.29 11/13/21 11:42 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 132 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 METHOD BLANK: 3457145 Matrix: Water Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199016 Blank Reporting Parameter Units Result Limit MDL Analyzed Tetrachloroethene ug/L ND 1.0 0.29 11/13/21 11:42 Tetrahydrofuran ug/L ND 10.0 3.5 11/13/21 11:42 Toluene ug/L ND 1.0 0.48 11/13/21 11:42 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 11/13/21 11:42 trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 11/13/21 11:42 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 11/13/21 11:42 Trichloroethene ug/L ND 1.0 0.38 11/13/21 11:42 Trichlorofluoromethane ug/L ND 1.0 0.30 11/13/21 11:42 Vinyl acetate ug/L ND 2.0 1.3 11/13/21 11:42 Vinyl chloride ug/L ND 1.0 0.39 11/13/21 11:42 1,2-Dichloroethane-d4 (S) % 104 70-130 11/13/21 11:42 4-Bromofluorobenzene (S) % 96 70-130 11/13/21 11:42 Toluene-d8 (S) % 104 70-130 11/13/21 11:42 LABORATORY CONTROL SAMPLE: Parameter 3457146 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 50.5 101 70-130 1,1,1-Trichloroethane ug/L 50 50.3 101 70-130 1,1,2,2-Tetrachloroethane ug/L 50 49.7 99 70-130 1,1,2-Trichloroethane ug/L 50 49.1 98 70-130 1,1-Dichloroethane ug/L 50 50.1 100 70-130 1,1-Dichloroethene ug/L 50 52.8 106 70-132 1,2,3-Trichloropropane ug/L 50 49.8 100 70-130 1,2-Dibromo-3-chloropropane ug/L 50 53.8 108 70-132 1,2-Dibromoethane (EDB) ug/L 50 50.3 101 70-130 1,2-Dichlorobenzene ug/L 50 49.7 99 70-130 1,2-Dichloroethane ug/L 50 49.7 99 70-130 1,2-Dichloropropane ug/L 50 49.5 99 70-130 1,4-Dichlorobenzene ug/L 50 51.5 103 70-130 2-Butanone (MEK) ug/L 100 120 120 70-133 2-Hexanone ug/L 100 115 115 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 110 110 70-130 Acetone ug/L 100 116 116 70-144 Acrylonitrile ug/L 250 271 108 70-130 Benzene ug/L 50 48.3 97 70-130 Bromochloromethane ug/L 50 49.6 99 70-130 Bromodichloromethane ug/L 50 47.7 95 70-130 Bromoform ug/L 50 48.6 97 70-131 Bromomethane ug/L 50 46.4 93 30-177 Carbon disulfide ug/L 50 49.4 99 70-133 Carbon tetrachloride ug/L 50 50.7 101 70-130 Chlorobenzene ug/L 50 49.1 98 70-130 Chloroethane ug/L 50 47.7 95 46-131 Qualifiers v1 v1 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 133 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 LABORATORY CONTROL SAMPLE: Parameter 3457146 Units Spike LCS Conc. Result Chloroform ug/L 50 Chloromethane ug/L 50 cis-1,2-Dichloroethene ug/L 50 cis-1,3-Dichloropropene ug/L 50 Dibromochloromethane ug/L 50 Dibromomethane ug/L 50 Dichlorodifluoromethane ug/L 50 Ethylbenzene ug/L 50 lodomethane ug/L 100 m&p-Xylene ug/L 100 Methylene Chloride ug/L 50 o-Xylene ug/L 50 Styrene ug/L 50 Tetrachloroethene ug/L 50 Tetrahydrofuran ug/L 500 Toluene ug/L 50 trans-1,2-Dichloroethene ug/L 50 trans- 1,3-Dichloropropene ug/L 50 trans-1,4-Dichloro-2-butene ug/L 50 Trichloroethene ug/L 50 Trichlorofluoromethane ug/L 50 Vinyl acetate ug/L 100 Vinyl chloride ug/L 50 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % LCS % Rec % Rec Limits Qualifiers 48.5 97 70-130 53.3 107 49-130 50.0 100 70-130 49.8 100 70-130 51.2 102 70-130 45.8 92 70-130 53.9 108 52-134 48.9 98 70-130 85.7 86 47-140 97.4 97 70-130 53.9 108 68-130 48.7 97 70-130 49.5 99 70-130 48.2 96 70-130 582 116 70-130 46.2 92 70-130 51.6 103 70-130 49.3 99 70-130 68.1 136 25-200 v1 48.5 97 70-130 46.5 93 61-130 125 125 70-140 v1 52.2 104 59-142 105 70-130 98 70-130 98 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457159 MS 92571653001 Spike Parameter Units Result Conc. MSD Spike Conc. 3457160 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L 2000 2000 2200 1890 110 94 70-135 15 30 1,1,1-Trichloroethane ug/L 2000 2000 2360 2170 118 109 70-148 8 30 1,1,2,2-Tetrachloroethane ug/L 2000 2000 2200 2020 110 101 70-131 8 30 1,1,2-Trichloroethane ug/L 2000 2000 2220 2050 111 102 70-136 8 30 1,1-Dichloroethane ug/L 2000 2000 2300 2160 115 108 70-147 6 30 1,1-Dichloroethene ug/L 2000 2000 2410 2300 120 115 70-158 5 30 1,2,3-Trichloropropane ug/L 2000 2000 2110 1890 106 94 67-137 11 30 1,2-Dibromo-3- ug/L 2000 2000 2260 1990 113 99 69-136 13 30 chloropropane 1,2-Dibromoethane (EDB) ug/L 2000 2000 2220 2010 111 101 70-137 10 30 1,2-Dichlorobenzene ug/L 2000 2000 2170 2020 108 101 70-133 7 30 1,2-Dichloroethane ug/L 2000 2000 2150 1990 107 99 67-138 8 30 1,2-Dichloropropane ug/L 2000 2000 2330 2120 117 106 70-138 10 30 1,4-Dichlorobenzene ug/L 2000 2000 2230 2030 112 101 70-133 10 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 134 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457159 3457160 MS MSD 92571653001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2-Butanone (MEK) ug/L 4000 4000 4600 4220 115 106 61-147 9 30 2-Hexanone ug/L 4000 4000 4380 3900 109 98 67-139 11 30 4-Methyl-2-pentanone ug/L 4000 4000 4300 3880 107 97 67-136 10 30 (MIBK) Acetone ug/L 4000 4000 4560 4390 114 110 55-159 4 30 Acrylonitrile ug/L 10000 10000 11400 10600 114 106 68-140 7 30 Benzene ug/L 9310 2000 2000 11400 11100 107 90 67-150 3 30 Bromochloromethane ug/L 2000 2000 2390 2130 119 107 70-146 11 30 Bromodichloromethane ug/L 2000 2000 2180 2010 109 101 70-138 8 30 Bromoform ug/L 2000 2000 2050 1860 102 93 57-138 10 30 Bromomethane ug/L 2000 2000 2160 2190 108 109 10-200 1 30 v2 Carbon disulfide ug/L 2000 2000 2410 2160 120 108 70-152 11 30 Carbon tetrachloride ug/L 2000 2000 2390 2150 120 107 70-147 11 30 Chlorobenzene ug/L 2000 2000 2240 2000 112 100 70-137 11 30 Chloroethane ug/L 2000 2000 2550 2360 128 118 51-166 8 30 Chloroform ug/L 2000 2000 2310 2080 116 104 70-144 11 30 Chloromethane ug/L 2000 2000 2210 2030 108 99 24-161 8 30 cis-1,2-Dichloroethene ug/L 2000 2000 2290 2140 115 107 67-148 7 30 cis-1,3-Dichloropropene ug/L 2000 2000 2020 1880 101 94 70-142 7 30 Dibromochloromethane ug/L 2000 2000 2160 1980 108 99 68-138 9 30 Dibromomethane ug/L 2000 2000 2070 1940 104 97 70-134 7 30 Dichlorodifluoromethane ug/L 2000 2000 2410 2190 121 109 43-155 10 30 Ethylbenzene ug/L 1120 2000 2000 3340 3130 111 100 68-143 7 30 lodomethane ug/L 4000 4000 4210 4110 105 103 20-161 2 30 v2 m&p-Xylene ug/L 4000 4000 5650 5140 112 99 53-157 9 30 Methylene Chloride ug/L 2000 2000 2440 2290 116 109 64-148 6 30 o-Xylene ug/L 2000 2000 2200 2050 107 100 68-143 7 30 Styrene ug/L 2000 2000 2200 1990 110 100 70-136 10 30 Tetrachloroethene ug/L 2000 2000 2140 1930 107 97 70-139 10 30 Tetrahydrofuran ug/L 20000 20000 22900 21300 114 106 65-145 7 30 Toluene ug/L 1710 2000 2000 3840 3620 107 96 47-157 6 30 trans-1,2-Dichloroethene ug/L 2000 2000 2410 2210 121 110 70-149 9 30 trans-1,3-Dichloropropene ug/L 2000 2000 1950 1750 98 88 70-138 11 30 trans-1,4-Dichloro-2-butene ug/L 2000 2000 1960 1670 98 83 31-145 16 30 Trichloroethene ug/L 2000 2000 2330 2070 117 103 70-149 12 30 Trichlorofluoromethane ug/L 2000 2000 2260 2030 113 102 61-154 11 30 Vinyl acetate ug/L 4000 4000 4980 4500 125 113 48-156 10 30 Vinyl chloride ug/L 2000 2000 2470 2260 123 113 55-172 9 30 1,2-Dichloroethane-d4 (S) % 96 100 70-130 4-Bromofluorobenzene (S) % 98 97 70-130 Toluene-d8 (S) % 99 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 135 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659894 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92572199001, 92572199003, 92572199004, 92572199005, 92572199015, 92572199017, 92572199018, 92572199019,92572199020,92572199021,92572199022,92572199023,92572199024,92572199025, 92572199026,92572199027,92572199028 METHOD BLANK: 3457924 Matrix: Water Associated Lab Samples: 92572199001, 92572199003, 92572199004, 92572199005, 92572199015, 92572199017, 92572199018, 92572199019,92572199020,92572199021,92572199022,92572199023,92572199024,92572199025, 92572199026,92572199027,92572199028 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 11/16/21 01:34 1,1,1-Trichloroethane ug/L ND 1.0 0.33 11/16/21 01:34 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 11/16/21 01:34 1,1,2-Trichloroethane ug/L ND 1.0 0.32 11/16/21 01:34 1,1-Dichloroethane ug/L ND 1.0 0.37 11/16/21 01:34 1,1-Dichloroethene ug/L ND 1.0 0.35 11/16/21 01:34 1,2,3-Trichloropropane ug/L ND 1.0 0.26 11/16/21 01:34 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 11/16/21 01:34 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 11/16/21 01:34 1,2-Dichlorobenzene ug/L ND 1.0 0.34 11/16/21 01:34 1,2-Dichloroethane ug/L ND 1.0 0.32 11/16/21 01:34 1,2-Dichloropropane ug/L ND 1.0 0.36 11/16/21 01:34 1,4-Dichlorobenzene ug/L ND 1.0 0.33 11/16/21 01:34 2-Butanone (MEK) ug/L ND 5.0 4.0 11/16/21 01:34 2-Hexanone ug/L ND 5.0 0.48 11/16/21 01:34 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 11/16/21 01:34 Acetone ug/L ND 25.0 5.1 11/16/21 01:34 Acrylonitrile ug/L ND 10.0 1.8 11/16/21 01:34 Benzene ug/L ND 1.0 0.34 11/16/21 01:34 Bromochloromethane ug/L ND 1.0 0.47 11/16/21 01:34 Bromodichloromethane ug/L ND 1.0 0.31 11/16/21 01:34 Bromoform ug/L ND 1.0 0.34 11/16/21 01:34 Bromomethane ug/L ND 2.0 1.7 11/16/21 01:34 Carbon disulfide ug/L ND 2.0 0.73 11/16/21 01:34 Carbon tetrachloride ug/L ND 1.0 0.33 11/16/21 01:34 Chlorobenzene ug/L ND 1.0 0.28 11/16/21 01:34 Chloroethane ug/L ND 1.0 0.65 11/16/21 01:34 Chloroform ug/L ND 1.0 0.43 11/16/21 01:34 Chloromethane ug/L ND 1.0 0.54 11/16/21 01:34 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 11/16/21 01:34 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 11/16/21 01:34 Dibromochloromethane ug/L ND 1.0 0.36 11/16/21 01:34 Dibromomethane ug/L ND 1.0 0.39 11/16/21 01:34 Dichlorodifluoromethane ug/L ND 1.0 0.35 11/16/21 01:34 Ethylbenzene ug/L ND 1.0 0.30 11/16/21 01:34 lodomethane ug/L ND 20.0 9.7 11/16/21 01:34 m&p-Xylene ug/L ND 2.0 0.71 11/16/21 01:34 v2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 136 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 METHOD BLANK: 3457924 Matrix: Water Associated Lab Samples: 92572199001, 92572199003, 92572199004, 92572199005, 92572199015, 92572199017, 92572199018, 92572199019,92572199020,92572199021,92572199022,92572199023,92572199024,92572199025, 92572199026,92572199027,92572199028 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Methylene Chloride ug/L ND 5.0 2.0 11/16/21 01:34 o-Xylene ug/L ND 1.0 0.34 11/16/21 01:34 Styrene ug/L ND 1.0 0.29 11/16/21 01:34 Tetrachloroethene ug/L ND 1.0 0.29 11/16/21 01:34 Tetrahydrofuran ug/L ND 10.0 3.5 11/16/21 01:34 Toluene ug/L ND 1.0 0.48 11/16/21 01:34 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 11/16/21 01:34 trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 11/16/21 01:34 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 11/16/21 01:34 Trichloroethene ug/L ND 1.0 0.38 11/16/21 01:34 Trichlorofluoromethane ug/L ND 1.0 0.30 11/16/21 01:34 Vinyl acetate ug/L ND 2.0 1.3 11/16/21 01:34 Vinyl chloride ug/L ND 1.0 0.39 11/16/21 01:34 1,2-Dichloroethane-d4 (S) % 91 70-130 11/16/21 01:34 4-Bromofluorobenzene (S) % 97 70-130 11/16/21 01:34 Toluene-d8 (S) % 100 70-130 11/16/21 01:34 LABORATORY CONTROL SAMPLE: Parameter 3457925 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 50.9 102 70-130 1,1,1-Trichloroethane ug/L 50 52.9 106 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.2 106 70-130 1,1,2-Trichloroethane ug/L 50 53.5 107 70-130 1,1-Dichloroethane ug/L 50 55.2 110 70-130 1,1-Dichloroethene ug/L 50 53.5 107 70-132 1,2,3-Trichloropropane ug/L 50 49.9 100 70-130 1,2-Dibromo-3-chloropropane ug/L 50 54.7 109 70-132 1,2-Dibromoethane (EDB) ug/L 50 52.6 105 70-130 1,2-Dichlorobenzene ug/L 50 52.3 105 70-130 1,2-Dichloroethane ug/L 50 49.0 98 70-130 1,2-Dichloropropane ug/L 50 54.7 109 70-130 1,4-Dichlorobenzene ug/L 50 52.1 104 70-130 2-Butanone (MEK) ug/L 100 103 103 70-133 2-Hexanone ug/L 100 92.9 93 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 96.6 97 70-130 Acetone ug/L 100 102 102 70-144 Acrylonitrile ug/L 250 276 110 70-130 Benzene ug/L 50 53.0 106 70-130 Bromochloromethane ug/L 50 57.1 114 70-130 Bromodichloromethane ug/L 50 50.4 101 70-130 Bromoform ug/L 50 50.3 101 70-131 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 137 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 LABORATORY CONTROL SAMPLE: 3457925 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Bromomethane ug/L 50 40.2 80 30-177 v3 Carbon disulfide ug/L 50 59.5 119 70-133 Carbon tetrachloride ug/L 50 47.2 94 70-130 Chlorobenzene ug/L 50 52.3 105 70-130 Chloroethane ug/L 50 36.9 74 46-131 Chloroform ug/L 50 55.4 111 70-130 Chloromethane ug/L 50 57.9 116 49-130 cis-1,2-Dichloroethene ug/L 50 54.1 108 70-130 cis-1,3-Dichloropropene ug/L 50 52.9 106 70-130 Dibromochloromethane ug/L 50 51.5 103 70-130 Dibromomethane ug/L 50 53.4 107 70-130 Dichlorodifluoromethane ug/L 50 62.2 124 52-134 Ethylbenzene ug/L 50 51.6 103 70-130 lodomethane ug/L 100 105 105 47-140 m&p-Xylene ug/L 100 103 103 70-130 Methylene Chloride ug/L 50 51.5 103 68-130 o-Xylene ug/L 50 52.3 105 70-130 Styrene ug/L 50 54.2 108 70-130 Tetrachloroethene ug/L 50 50.3 101 70-130 Tetrahydrofuran ug/L 500 517 103 70-130 Toluene ug/L 50 52.6 105 70-130 trans-1,2-Dichloroethene ug/L 50 54.5 109 70-130 trans- 1,3-Dichloropropene ug/L 50 51.0 102 70-130 trans-1,4-Dichloro-2-butene ug/L 50 44.5 89 25-200 Trichloroethene ug/L 50 52.0 104 70-130 Trichlorofluoromethane ug/L 50 43.3 87 61-130 Vinyl acetate ug/L 100 107 107 70-140 Vinyl chloride ug/L 50 60.9 122 59-142 1,2-Dichloroethane-d4 (S) % 88 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457926 3457927 MS MSD 92572199005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 22.6 19.8 113 99 70-135 13 30 1,1,1-Trichloroethane ug/L ND 20 20 24.3 20.7 122 104 70-148 16 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 23.8 20.6 119 103 70-131 14 30 1,1,2-Trichloroethane ug/L ND 20 20 24.4 21.3 122 106 70-136 14 30 1,1-Dichloroethane ug/L ND 20 20 24.7 21.6 124 108 70-147 14 30 1,1-Dichloroethene ug/L ND 20 20 24.3 20.4 121 102 70-158 17 30 1,2,3-Trichloropropane ug/L ND 20 20 21.9 19.2 109 96 67-137 13 30 1,2-Dibromo-3- ug/L ND 20 20 22.8 20.0 114 100 69-136 13 30 chloropropane Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 138 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457926 MS 92572199005 Spike Parameter Units Result Conc. MSD Spike Conc. 3457927 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,2-Dibromoethane (EDB) ug/L ND 20 20 23.4 20.3 117 101 70-137 15 30 1,2-Dichlorobenzene ug/L ND 20 20 23.8 21.0 119 105 70-133 12 30 1,2-Dichloroethane ug/L ND 20 20 21.5 18.7 108 93 67-138 14 30 1,2-Dichloropropane ug/L ND 20 20 25.1 21.6 126 108 70-138 15 30 1,4-Dichlorobenzene ug/L ND 20 20 24.3 20.9 121 104 70-133 15 30 2-Butanone (MEK) ug/L ND 40 40 45.8 39.1 114 98 61-147 16 30 2-Hexanone ug/L ND 40 40 41.5 36.5 104 91 67-139 13 30 4-Methyl-2-pentanone ug/L ND 40 40 43.3 37.4 108 93 67-136 15 30 (MIBK) Acetone ug/L ND 40 40 44.2 38.0 110 95 55-159 15 30 Acrylonitrile ug/L ND 100 100 126 108 126 108 68-140 15 30 Benzene ug/L ND 20 20 24.9 21.7 125 108 67-150 14 30 Bromochloromethane ug/L ND 20 20 25.4 21.9 127 109 70-146 15 30 Bromodichloromethane ug/L ND 20 20 22.6 19.5 113 97 70-138 15 30 Bromoform ug/L ND 20 20 20.8 17.5 104 88 57-138 17 30 Bromomethane ug/L ND 20 20 19.9 16.7 100 84 10-200 17 30 v3 Carbon disulfide ug/L ND 20 20 27.9 23.6 140 118 70-152 17 30 Carbon tetrachloride ug/L ND 20 20 23.0 19.7 115 98 70-147 16 30 Chlorobenzene ug/L ND 20 20 24.1 21.1 121 105 70-137 14 30 Chloroethane ug/L ND 20 20 22.8 20.6 114 103 51-166 10 30 Chloroform ug/L ND 20 20 25.0 22.7 125 114 70-144 10 30 Chloromethane ug/L ND 20 20 25.3 22.3 127 112 24-161 13 30 cis-1,2-Dichloroethene ug/L ND 20 20 25.0 21.5 125 108 67-148 15 30 cis-1,3-Dichloropropene ug/L ND 20 20 23.9 20.6 120 103 70-142 15 30 Dibromochloromethane ug/L ND 20 20 22.3 19.1 112 96 68-138 15 30 Dibromomethane ug/L ND 20 20 23.8 20.9 119 105 70-134 13 30 Dichlorodifluoromethane ug/L ND 20 20 29.5 25.7 148 129 43-155 14 30 v1 Ethylbenzene ug/L ND 20 20 24.1 21.0 120 105 68-143 14 30 lodomethane ug/L ND 40 40 40.8 35.2 102 88 20-161 15 30 m&p-Xylene ug/L ND 40 40 48.3 42.4 121 106 53-157 13 30 Methylene Chloride ug/L ND 20 20 22.9 20.4 115 102 64-148 12 30 o-Xylene ug/L ND 20 20 23.7 20.7 119 104 68-143 13 30 Styrene ug/L ND 20 20 24.1 21.1 121 106 70-136 13 30 Tetrachloroethene ug/L ND 20 20 23.8 20.9 119 104 70-139 13 30 Tetrahydrofuran ug/L ND 200 200 229 197 115 98 65-145 15 30 Toluene ug/L ND 20 20 24.7 21.7 124 108 47-157 13 30 trans-1,2-Dichloroethene ug/L ND 20 20 25.4 22.1 127 111 70-149 14 30 trans-1,3-Dichloropropene ug/L ND 20 20 22.8 19.8 114 99 70-138 14 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 21.2 17.9 106 90 31-145 17 30 Trichloroethene ug/L ND 20 20 24.9 21.7 124 108 70-149 14 30 Trichlorofluoromethane ug/L ND 20 20 22.1 19.0 110 95 61-154 15 30 Vinyl acetate ug/L ND 40 40 47.3 40.6 118 102 48-156 15 30 Vinyl chloride ug/L ND 20 20 28.6 24.9 143 124 55-172 14 30 1,2-Dichloroethane-d4 (S) % 89 85 70-130 4-Bromofluorobenzene (S) % 100 101 70-130 Toluene-d8 (S) % 101 101 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 139 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659895 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92572199006, 92572199007, 92572199008, 92572199009, 92572199010, 92572199013 METHOD BLANK: 3457933 Matrix: Water Associated Lab Samples: 92572199006, 92572199007, 92572199008, 92572199009, 92572199010, 92572199013 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.31 11/16/21 01:16 1,1,1-Trichloroethane ug/L ND 1.0 0.33 11/16/21 01:16 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 11/16/21 01:16 1,1,2-Trichloroethane ug/L ND 1.0 0.32 11/16/21 01:16 1,1-Dichloroethane ug/L ND 1.0 0.37 11/16/21 01:16 1,1-Dichloroethene ug/L ND 1.0 0.35 11/16/21 01:16 1,2,3-Trichloropropane ug/L ND 1.0 0.26 11/16/21 01:16 1,2-Dibromo-3-chloropropane ug/L ND 2.0 0.34 11/16/21 01:16 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.27 11/16/21 01:16 1,2-Dichlorobenzene ug/L ND 1.0 0.34 11/16/21 01:16 1,2-Dichloroethane ug/L ND 1.0 0.32 11/16/21 01:16 1,2-Dichloropropane ug/L ND 1.0 0.36 11/16/21 01:16 1,4-Dichlorobenzene ug/L ND 1.0 0.33 11/16/21 01:16 2-Butanone (MEK) ug/L ND 5.0 4.0 11/16/21 01:16 2-Hexanone ug/L ND 5.0 0.48 11/16/21 01:16 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 2.7 11/16/21 01:16 Acetone ug/L ND 25.0 5.1 11/16/21 01:16 Acrylonitrile ug/L ND 10.0 1.8 11/16/21 01:16 Benzene ug/L ND 1.0 0.34 11/16/21 01:16 Bromochloromethane ug/L ND 1.0 0.47 11/16/21 01:16 Bromodichloromethane ug/L ND 1.0 0.31 11/16/21 01:16 Bromoform ug/L ND 1.0 0.34 11/16/21 01:16 Bromomethane ug/L ND 2.0 1.7 11/16/21 01:16 Carbon disulfide ug/L ND 2.0 0.73 11/16/21 01:16 Carbon tetrachloride ug/L ND 1.0 0.33 11/16/21 01:16 Chlorobenzene ug/L ND 1.0 0.28 11/16/21 01:16 Chloroethane ug/L ND 1.0 0.65 11/16/21 01:16 Chloroform ug/L ND 1.0 0.43 11/16/21 01:16 Chloromethane ug/L ND 1.0 0.54 11/16/21 01:16 cis-1,2-Dichloroethene ug/L ND 1.0 0.38 11/16/21 01:16 cis-1,3-Dichloropropene ug/L ND 1.0 0.36 11/16/21 01:16 Dibromochloromethane ug/L ND 1.0 0.36 11/16/21 01:16 Dibromomethane ug/L ND 1.0 0.39 11/16/21 01:16 Dichlorodifluoromethane ug/L ND 1.0 0.35 11/16/21 01:16 Ethylbenzene ug/L ND 1.0 0.30 11/16/21 01:16 lodomethane ug/L ND 20.0 9.7 11/16/21 01:16 m&p-Xylene ug/L ND 2.0 0.71 11/16/21 01:16 Methylene Chloride ug/L ND 5.0 2.0 11/16/21 01:16 o-Xylene ug/L ND 1.0 0.34 11/16/21 01:16 Styrene ug/L ND 1.0 0.29 11/16/21 01:16 v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 140 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 METHOD BLANK: 3457933 Matrix: Water Associated Lab Samples: 92572199006, 92572199007, 92572199008, 92572199009, 92572199010, 92572199013 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Tetrachloroethene ug/L ND 1.0 0.29 11/16/21 01:16 Tetrahydrofuran ug/L ND 10.0 3.5 11/16/21 01:16 Toluene ug/L ND 1.0 0.48 11/16/21 01:16 trans-1,2-Dichloroethene ug/L ND 1.0 0.40 11/16/21 01:16 trans- 1,3-Dichloropropene ug/L ND 1.0 0.36 11/16/21 01:16 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.56 11/16/21 01:16 Trichloroethene ug/L ND 1.0 0.38 11/16/21 01:16 Trichlorofluoromethane ug/L ND 1.0 0.30 11/16/21 01:16 Vinyl acetate ug/L ND 2.0 1.3 11/16/21 01:16 Vinyl chloride ug/L ND 1.0 0.39 11/16/21 01:16 1,2-Dichloroethane-d4 (S) % 92 70-130 11/16/21 01:16 4-Bromofluorobenzene (S) % 98 70-130 11/16/21 01:16 Toluene-d8 (S) % 100 70-130 11/16/21 01:16 LABORATORY CONTROL SAMPLE: Parameter 3457934 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 48.9 98 70-130 1,1,1-Trichloroethane ug/L 50 51.0 102 70-130 1,1,2,2-Tetrachloroethane ug/L 50 51.8 104 70-130 1,1,2-Trichloroethane ug/L 50 53.8 108 70-130 1,1-Dichloroethane ug/L 50 52.9 106 70-130 1,1-Dichloroethene ug/L 50 50.0 100 70-132 1,2,3-Trichloropropane ug/L 50 49.1 98 70-130 1,2-Dibromo-3-chloropropane ug/L 50 54.1 108 70-132 1,2-Dibromoethane (EDB) ug/L 50 51.2 102 70-130 1,2-Dichlorobenzene ug/L 50 51.6 103 70-130 1,2-Dichloroethane ug/L 50 47.5 95 70-130 1,2-Dichloropropane ug/L 50 54.1 108 70-130 1,4-Dichlorobenzene ug/L 50 51.6 103 70-130 2-Butanone (MEK) ug/L 100 102 102 70-133 2-Hexanone ug/L 100 92.5 93 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 98.5 99 70-130 Acetone ug/L 100 101 101 70-144 Acrylonitrile ug/L 250 275 110 70-130 Benzene ug/L 50 52.2 104 70-130 Bromochloromethane ug/L 50 55.7 111 70-130 Bromodichloromethane ug/L 50 49.9 100 70-130 Bromoform ug/L 50 49.5 99 70-131 Bromomethane ug/L 50 41.8 84 30-177 v3 Carbon disulfide ug/L 50 57.1 114 70-133 Carbon tetrachloride ug/L 50 47.2 94 70-130 Chlorobenzene ug/L 50 50.9 102 70-130 Chloroethane ug/L 50 35.2 70 46-131 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 141 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 LABORATORY CONTROL SAMPLE: Parameter 3457934 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Chloroform ug/L 50 54.5 109 70-130 Chloromethane ug/L 50 57.9 116 49-130 cis-1,2-Dichloroethene ug/L 50 52.2 104 70-130 cis-1,3-Dichloropropene ug/L 50 52.4 105 70-130 Dibromochloromethane ug/L 50 50.7 101 70-130 Dibromomethane ug/L 50 53.1 106 70-130 Dichlorodifluoromethane ug/L 50 62.0 124 52-134 Ethylbenzene ug/L 50 49.7 99 70-130 lodomethane ug/L 100 103 103 47-140 m&p-Xylene ug/L 100 101 101 70-130 Methylene Chloride ug/L 50 49.3 99 68-130 o-Xylene ug/L 50 50.4 101 70-130 Styrene ug/L 50 52.4 105 70-130 Tetrachloroethene ug/L 50 48.7 97 70-130 Tetrahydrofuran ug/L 500 517 103 70-130 Toluene ug/L 50 51.8 104 70-130 trans-1,2-Dichloroethene ug/L 50 52.5 105 70-130 trans- 1,3-Dichloropropene ug/L 50 50.8 102 70-130 trans-1,4-Dichloro-2-butene ug/L 50 49.2 98 25-200 Trichloroethene ug/L 50 51.7 103 70-130 Trichlorofluoromethane ug/L 50 42.0 84 61-130 Vinyl acetate ug/L 100 105 105 70-140 Vinyl chloride ug/L 50 60.2 120 59-142 1,2-Dichloroethane-d4 (S) % 86 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8(S) % 101 70-130 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457935 MS 92572324004 Spike Parameter Units Result Conc. MSD Spike Conc. 3457936 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 21.3 19.9 107 100 70-135 7 30 1,1,1-Trichloroethane ug/L ND 20 20 22.2 20.8 111 104 70-148 6 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 21.8 20.6 109 103 70-131 6 30 1,1,2-Trichloroethane ug/L ND 20 20 22.5 21.1 113 106 70-136 6 30 1,1-Dichloroethane ug/L ND 20 20 23.2 22.0 116 110 70-147 6 30 1,1-Dichloroethene ug/L ND 20 20 21.9 21.3 109 106 70-158 3 30 1,2,3-Trichloropropane ug/L ND 20 20 20.4 19.2 102 96 67-137 6 30 1,2-Dibromo-3- ug/L ND 20 20 20.9 19.9 104 99 69-136 5 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 21.9 20.4 110 102 70-137 7 30 1,2-Dichlorobenzene ug/L ND 20 20 21.8 20.7 109 104 70-133 5 30 1,2-Dichloroethane ug/L ND 20 20 20.0 18.6 100 93 67-138 7 30 1,2-Dichloropropane ug/L ND 20 20 23.3 21.6 116 108 70-138 8 30 1,4-Dichlorobenzene ug/L ND 20 20 22.1 20.9 111 105 70-133 6 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 142 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457935 3457936 MS MSD 92572324004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2-Butanone (MEK) ug/L ND 40 40 41.0 39.7 102 99 61-147 3 30 2-Hexanone ug/L ND 40 40 38.4 36.4 96 91 67-139 5 30 4-Methyl-2-pentanone ug/L ND 40 40 39.5 37.0 99 92 67-136 6 30 (MIBK) Acetone ug/L ND 40 40 40.7 38.2 102 95 55-159 6 30 Acrylonitrile ug/L ND 100 100 115 107 115 107 68-140 8 30 Benzene ug/L ND 20 20 22.9 21.5 114 107 67-150 6 30 Bromochloromethane ug/L ND 20 20 23.5 21.9 117 110 70-146 7 30 Bromodichloromethane ug/L ND 20 20 20.8 19.2 104 96 70-138 8 30 Bromoform ug/L ND 20 20 18.4 17.4 92 87 57-138 6 30 Bromomethane ug/L ND 20 20 18.6 16.3 93 82 10-200 13 30 v3 Carbon disulfide ug/L ND 20 20 24.5 23.4 122 117 70-152 5 30 Carbon tetrachloride ug/L ND 20 20 21.0 19.8 105 99 70-147 6 30 Chlorobenzene ug/L ND 20 20 22.4 21.2 112 106 70-137 5 30 Chloroethane ug/L ND 20 20 21.6 19.8 108 99 51-166 9 30 Chloroform ug/L ND 20 20 23.3 22.5 117 113 70-144 4 30 Chloromethane ug/L ND 20 20 22.6 22.0 113 110 24-161 3 30 cis-1,2-Dichloroethene ug/L ND 20 20 22.7 21.5 113 107 67-148 5 30 cis-1,3-Dichloropropene ug/L ND 20 20 21.6 20.2 108 101 70-142 7 30 Dibromochloromethane ug/L ND 20 20 20.2 19.1 101 95 68-138 6 30 Dibromomethane ug/L ND 20 20 22.2 20.7 111 103 70-134 7 30 Dichlorodifluoromethane ug/L ND 20 20 26.9 25.5 135 127 43-155 6 30 v1 Ethylbenzene ug/L ND 20 20 22.2 21.0 111 105 68-143 6 30 lodomethane ug/L ND 40 40 41.3 37.9 103 95 20-161 9 30 m&p-Xylene ug/L ND 40 40 44.9 42.5 112 106 53-157 5 30 Methylene Chloride ug/L ND 20 20 21.2 20.3 106 101 64-148 5 30 o-Xylene ug/L ND 20 20 22.2 21.0 111 105 68-143 5 30 Styrene ug/L ND 20 20 22.6 21.5 113 107 70-136 5 30 Tetrachloroethene ug/L ND 20 20 21.8 21.1 109 105 70-139 4 30 Tetrahydrofuran ug/L ND 200 200 209 198 105 99 65-145 6 30 Toluene ug/L ND 20 20 22.9 21.3 114 106 47-157 7 30 trans-1,2-Dichloroethene ug/L ND 20 20 23.5 22.2 117 111 70-149 6 30 trans-1,3-Dichloropropene ug/L ND 20 20 20.9 19.4 105 97 70-138 7 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 19.2 17.8 96 89 31-145 8 30 Trichloroethene ug/L ND 20 20 22.7 21.1 114 106 70-149 7 30 Trichlorofluoromethane ug/L ND 20 20 20.2 18.7 101 94 61-154 7 30 Vinyl acetate ug/L ND 40 40 43.1 40.0 108 100 48-156 8 30 Vinyl chloride ug/L ND 20 20 26.1 24.7 130 124 55-172 5 30 1,2-Dichloroethane-d4 (S) % 86 86 70-130 4-Bromofluorobenzene (S) % 100 102 70-130 Toluene-d8 (S) % 100 100 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 143 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659986 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199019, 92572199020 METHOD BLANK: 3458546 Matrix: Water Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199019, 92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 11/15/21 17:57 1,2-Dichloroethane-d4 (S) % 98 70-130 11/15/21 17:57 Toluene-d8 (S) % 97 66-133 11/15/21 17:57 LABORATORY CONTROL SAMPLE: 3458547 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 20.0 100 70-130 1,2-Dichloroethane-d4 (S) % 98 70-130 Toluene-d8 (S) % 98 66-133 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3458548 3458549 MS MSD 92572283002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane(p-Dioxane) ug/L 7.5 20 20 28.9 28.4 107 104 64-141 2 30 1,2-Dichloroethane-d4 (S) % 65 65 70-130 30 S2 Toluene-d8 (S) % 87 88 66-133 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 144 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659988 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92572199004, 92572199005, 92572199006, 92572199007, 92572199008, 92572199009, 92572199010, 92572199011,92572199012 METHOD BLANK: 3458552 Matrix: Water Associated Lab Samples: 92572199004, 92572199005, 92572199006, 92572199007, 92572199008, 92572199009, 92572199010, 92572199011,92572199012 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 11/15/21 18:16 1,2-Dichloroethane-d4 (S) % 97 70-130 11/15/21 18:16 Toluene-d8 (S) % 100 66-133 11/15/21 18:16 LABORATORY CONTROL SAMPLE: 3458553 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane(p-Dioxane) ug/L 20 19.5 97 70-130 1,2-Dichloroethane-d4 (S) % 96 70-130 Toluene-d8 (S) % 97 66-133 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3458554 3458555 MS MSD 92572199012 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L 5.6 20 20 25.7 27.5 100 109 64-141 7 30 1,2-Dichloroethane-d4 (S) % 95 92 70-130 30 Toluene-d8 (S) % 87 89 66-133 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 145 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659996 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92572199013, 92572199014, 92572199015, 92572199016, 92572199017, 92572199018 METHOD BLANK: 3458579 Matrix: Water Associated Lab Samples: 92572199013, 92572199014, 92572199015, 92572199016, 92572199017, 92572199018 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 0.86 11/15/21 13:59 1,2-Dichloroethane-d4 (S) % 104 70-130 11/15/21 13:59 Toluene-d8 (S) % 103 66-133 11/15/21 13:59 LABORATORY CONTROL SAMPLE: 3458580 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 19.2 96 70-130 1,2-Dichloroethane-d4 (S) % 104 70-130 Toluene-d8 (S) % 102 66-133 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3458581 3458582 MS MSD 92572199013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 21.3 20.0 106 100 64-141 6 30 1,2-Dichloroethane-d4 (S) % 108 107 70-130 30 Toluene-d8 (S) % 106 105 66-133 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 146 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659766 Analysis Method: EPA 8082A QC Batch Method: EPA 3510C Analysis Description: 8082 GCS PCB Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008,92572199009,92572199010,92572199011,92572199012,92572199013,92572199014, 92572199019,92572199020 METHOD BLANK: 3457331 Matrix: Water Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008,92572199009,92572199010,92572199011,92572199012,92572199013,92572199014, 92572199019,92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/L ND 0.50 0.47 11/16/21 16:47 PCB-1221 (Aroclor 1221) ug/L ND 0.50 0.45 11/16/21 16:47 PCB-1232 (Aroclor 1232) ug/L ND 0.50 0.36 11/16/21 16:47 PCB-1242 (Aroclor 1242) ug/L ND 0.50 0.26 11/16/21 16:47 PCB-1248 (Aroclor 1248) ug/L ND 0.50 0.40 11/16/21 16:47 PCB-1254 (Aroclor 1254) ug/L ND 0.50 0.25 11/16/21 16:47 PCB-1260 (Aroclor 1260) ug/L ND 0.50 0.42 11/16/21 16:47 Decachlorobiphenyl (S) % 110 10-181 11/16/21 16:47 LABORATORY CONTROL SAMPLE: 3457332 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L 5 6.2 124 41-137 PCB-1260 (Aroclor 1260) ug/L 5 6.2 123 42-156 Decachlorobiphenyl (S) % 144 10-181 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457333 3457334 MS MSD 92572199003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual PCB-1016 (Aroclor 1016) ug/L ND 4.5 4.2 5.7 4.8 126 116 22-145 17 30 PCB-1260 (Aroclor 1260) ug/L ND 4.5 4.2 5.2 4.8 115 116 10-167 8 30 Decachlorobiphenyl (S) % 97 94 10-181 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 147 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659764 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008,92572199009,92572199010,92572199011,92572199012,92572199013,92572199014 METHOD BLANK: 3457323 Matrix: Water Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008,92572199009,92572199010,92572199011,92572199012,92572199013,92572199014 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Benzo(a)anthracene ug/L ND 10.0 2.7 11/15/21 12:23 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 3.7 11/15/21 12:23 Chrysene ug/L ND 10.0 2.8 11/15/21 12:23 Dibenz(a,h)anthracene ug/L ND 10.0 3.0 11/15/21 12:23 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 2.9 11/15/21 12:23 2,4,6-Tribromophenol (S) % 54 10-144 11/15/21 12:23 2-Fluorobiphenyl (S) % 48 10-130 11/15/21 12:23 2-Fluorophenol (S) % 36 10-130 11/15/21 12:23 Nitrobenzene-d5 (S) % 52 10-144 11/15/21 12:23 Phenol-d6 (S) % 26 10-130 11/15/21 12:23 Terphenyl-d14 (S) % 67 34-163 11/15/21 12:23 LABORATORY CONTROL SAMPLE: Parameter 3457324 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Benzo(a)anthracene ug/L 50 35.9 72 48-137 bis(2-Ethylhexyl)phthalate ug/L 50 33.8 68 32-165 Chrysene ug/L 50 35.6 71 47-131 Dibenz(a,h)anthracene ug/L 50 40.0 80 49-138 Indeno(1,2,3-cd)pyrene ug/L 50 38.9 78 41-130 2,4,6-Tribromophenol (S) % 74 10-144 2-Fluorobiphenyl (S) % 53 10-130 2-Fluorophenol(S) % 34 10-130 Nitrobenzene-d5 (S) % 56 10-144 Phenol-d6 (S) % 27 10-130 Terphenyl-d14 (S) % 66 34-163 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 148 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659765 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92572199018, 92572199019, 92572199020 METHOD BLANK: 3457327 Matrix: Water Associated Lab Samples: 92572199018, 92572199019, 92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Benzo(a)anthracene ug/L ND 10.0 2.7 11/15/21 13:13 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 3.7 11/15/21 13:13 Chrysene ug/L ND 10.0 2.8 11/15/21 13:13 Dibenz(a,h)anthracene ug/L ND 10.0 3.0 11/15/21 13:13 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 2.9 11/15/21 13:13 2-Fluorobiphenyl (S) % 40 10-130 11/15/21 13:13 Nitrobenzene-d5 (S) % 48 10-144 11/15/21 13:13 Terphenyl-d14 (S) % 57 34-163 11/15/21 13:13 LABORATORY CONTROL SAMPLE: Parameter 3457328 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Benzo(a)anthracene ug/L 50 34.3 69 48-137 bis(2-Ethylhexyl)phthalate ug/L 50 36.5 73 32-165 Chrysene ug/L 50 34.8 70 47-131 Dibenz(a,h)anthracene ug/L 50 37.4 75 49-138 Indeno(1,2,3-cd)pyrene ug/L 50 36.9 74 41-130 2-Fluorobiphenyl (S) % 51 10-130 Nitrobenzene-d5 (S) % 59 10-144 Terphenyl-d14 (S) % 63 34-163 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457329 3457330 MS MSD 92572324002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Benzo(a)anthracene ug/L ND 83.3 83.3 55.6 57.3 67 69 40-145 3 30 bis(2-Ethylhexyl)phthalate ug/L ND 83.3 83.3 61.8 65.7 74 79 28-166 6 30 Chrysene ug/L ND 83.3 83.3 55.6 57.6 67 69 38-141 4 30 Dibenz(a,h)anthracene ug/L ND 83.3 83.3 59.3 61.2 71 73 39-148 3 30 Indeno(1,2,3-cd)pyrene ug/L ND 83.3 83.3 56.3 58.2 68 70 39-148 3 30 2-Fluorobiphenyl (S) % 37 34 10-130 Nitrobenzene-d5(S) % 48 42 10-144 Terphenyl-d14(S) % 58 59 34-163 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 149 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660077 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199016, 92572199017, 92572199019, 92572199020 METHOD BLANK: 3458773 Matrix: Water Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199016, 92572199017, 92572199019, 92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 5000 11/16/21 13:01 LABORATORY CONTROL SAMPLE: 3458774 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 52900 106 80-120 LABORATORY CONTROL SAMPLE: 3458775 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 49800 100 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3458776 3458777 MS MSD 92571974001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 23.6 mg/L 50000 50000 73200 85800 99 124 80-120 16 25 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3458778 3458779 MS MSD 92571974002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 77.0 mg/L 50000 50000 813000 770000 1470 1390 80-120 5 25 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 150 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660430 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199009, 92572199010, 92572199018 METHOD BLANK: 3460306 Matrix: Water Associated Lab Samples: 92572199009, 92572199010, 92572199018 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 5000 11/17/21 12:32 LABORATORY CONTROL SAMPLE: 3460307 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 51400 103 80-120 LABORATORY CONTROL SAMPLE: 3460308 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 52900 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3460309 3460310 MS MSD 92572607003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 180 mg/L 50000 50000 219000 229000 77 97 80-120 4 25 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3460311 3460312 MS MSD 92572607007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 314 mg/L 50000 50000 154000 158000 -320 -313 80-120 3 25 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 151 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660747 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199001, 92572199003 METHOD BLANK: 3462135 Matrix: Water Associated Lab Samples: 92572199001, 92572199003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 5000 11/18/21 11:20 LABORATORY CONTROL SAMPLE: 3462136 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 50800 102 80-120 LABORATORY CONTROL SAMPLE: 3462137 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 51400 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3462138 3462139 MS MSD 92571927010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 43.0 mg/L 50000 50000 89600 91900 93 98 80-120 3 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3462140 3462141 MS MSD 92571927011 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 193 mg/L 50000 50000 189000 187000 -7 -11 80-120 1 25 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 152 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 661211 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199005 METHOD BLANK: 3464449 Associated Lab Samples: 92572199005 Parameter Units Alkalinity, Total as CaCO3 ug/L LABORATORY CONTROL SAMPLE: 3464450 Parameter Units Alkalinity, Total as CaCO3 ug/L Matrix: Water Blank Reporting Result Limit ND 5000 Spike LCS Conc. Result 50000 58000 MDL Analyzed Qualifiers 5000 11 /23/21 12:24 LCS % Rec % Rec Limits Qualifiers 116 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3464452 3464453 MS MSD 92572199005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 32000 50000 50000 98000 98000 132 132 80-120 0 25 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 153 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 662075 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199004, 92572199006, 92572199007, 92572199008, 92572199013, 92572199015 METHOD BLANK: 3468884 Matrix: Water Associated Lab Samples: 92572199004, 92572199006, 92572199007, 92572199008, 92572199013, 92572199015 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 5000 11/24/21 09:20 LABORATORY CONTROL SAMPLE: 3468885 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 53000 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3468887 3468888 MS MSD 92572199008 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 33800 50000 50000 82000 84000 96 100 80-120 2 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3468889 3468890 MS MSD 92572199007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 30000 50000 50000 84000 80000 108 100 80-120 5 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 154 of 185 acc mnalytical www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, INC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659745 Analysis Method: SM 2540C-2015 QC Batch Method: SM 254OC-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92572199002,92572199011,92572199012,92572199014,92572199016,92572199017,92572199019, 92572199020 METHOD BLANK: 3457284 Matrix: Water Associated Lab Samples: 92572199002,92572199011,92572199012,92572199014,92572199016,92572199017,92572199019, 92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 25000 11/14/21 17:02 LABORATORY CONTROL SAMPLE: 3457285 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids ug/L 250000 258000 103 90-110 SAMPLE DUPLICATE: 3457286 92572199002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 920000 908000 1 25 SAMPLE DUPLICATE: 3457287 92571612015 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 141 mg/L 141000 0 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 155 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659939 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199009, 92572199010, 92572199018 METHOD BLANK: 3458100 Matrix: Water Associated Lab Samples: 92572199009, 92572199010, 92572199018 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 25000 11/15/21 17:11 LABORATORY CONTROL SAMPLE: 3458101 Spike LCS Parameter Units Conc. Result Total Dissolved Solids ug/L 250000 246000 SAMPLE DUPLICATE: 3458102 92571917008 Dup Parameter Units Result Result Total Dissolved Solids ug/L 782 mg/L 820000 LCS % Rec % Rec Limits Qualifiers 98 90-110 Max RPD RPD Qualifiers 5 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 156 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660091 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199001, 92572199003, 92572199005, 92572199008, 92572199013, 92572199015 METHOD BLANK: 3458811 Matrix: Water Associated Lab Samples: 92572199001, 92572199003, 92572199005, 92572199008, 92572199013, 92572199015 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 25000 11/16/21 10:21 LABORATORY CONTROL SAMPLE: 3458812 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids ug/L 250000 258000 103 90-110 SAMPLE DUPLICATE: 3458813 92572115005 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 240 mg/L 243000 1 25 SAMPLE DUPLICATE: 3458814 92572199005 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 165000 161000 2 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 157 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660562 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199004, 92572199006, 92572199007 METHOD BLANK: 3461103 Matrix: Water Associated Lab Samples: 92572199004, 92572199006, 92572199007 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 25000 11/17/21 16:49 LABORATORY CONTROL SAMPLE: 3461104 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids ug/L 250000 250000 100 90-110 SAMPLE DUPLICATE: 3461105 92572374003 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 87.0 mg/L 90000 3 25 SAMPLE DUPLICATE: 3461106 92572382006 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 2620 mg/L 2770000 6 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 158 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659632 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199016, 92572199017, 92572199019, 92572199020 METHOD BLANK: 3456933 Matrix: Water Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199016, 92572199017, 92572199019, 92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 50.0 11/13/2102:56 LABORATORY CONTROL SAMPLE: 3456934 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 496 99 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3456935 3456936 MS MSD 92571859002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 400 399 79 79 80-120 0 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3456937 3456938 MS MSD 92571859012 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L 0.36 mg/L 500 500 850 943 98 117 80-120 10 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 159 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659633 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199009, 92572199010, 92572199018 METHOD BLANK: 3456939 Matrix: Water Associated Lab Samples: 92572199009, 92572199010, 92572199018 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 50.0 11/13/2103:11 LABORATORY CONTROL SAMPLE: 3456940 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 503 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3456941 3456942 MS MSD 92571859013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 116 128 23 25 80-120 10 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3456943 3456944 MS MSD 92571859023 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 403 423 80 84 80-120 5 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 160 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659634 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199001, 92572199003, 92572199005, 92572199008, 92572199013, 92572199015 METHOD BLANK: 3456945 Matrix: Water Associated Lab Samples: 92572199001, 92572199003, 92572199005, 92572199008, 92572199013, 92572199015 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 50.0 11/13/2103:27 LABORATORY CONTROL SAMPLE: 3456946 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 497 99 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3456947 3456948 MS MSD 92572216003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 503 528 99 104 80-120 5 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3456951 3456952 MS MSD 92572062013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 519 522 99 99 80-120 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 161 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660668 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199004, 92572199006, 92572199007 METHOD BLANK: 3461934 Matrix: Water Associated Lab Samples: 92572199004, 92572199006, 92572199007 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 50.0 11/18/2105:10 LABORATORY CONTROL SAMPLE: 3461935 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 531 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3461936 3461937 MS MSD 92572216002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 532 560 104 110 80-120 5 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3461938 3461939 MS MSD 92572216001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 512 543 99 105 80-120 6 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 162 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659676 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008 METHOD BLANK: 3457087 Matrix: Water Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfate ug/L ND 1000 500 11/13/2114:45 LABORATORY CONTROL SAMPLE: 3457088 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 50500 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457089 3457090 MS MSD 92571324001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 311 mg/L 50000 50000 361000 356000 99 88 90-110 1 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457091 3457092 MS MSD 92571997001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 51.7 mg/L 50000 50000 91700 93000 80 83 90-110 1 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 163 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659677 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199009,92572199010,92572199011,92572199012,92572199013,92572199014,92572199015, 92572199016,92572199017,92572199018,92572199019,92572199020 METHOD BLANK: 3457101 Matrix: Water Associated Lab Samples: 92572199009,92572199010,92572199011,92572199012,92572199013,92572199014,92572199015, 92572199016,92572199017,92572199018,92572199019,92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfate ug/L ND 1000 500 11/13/2123:45 LABORATORY CONTROL SAMPLE: 3457102 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 48600 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457103 3457104 MS MSD 92572199009 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 165000 50000 50000 210000 213000 91 96 90-110 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457105 3457106 MS MSD 92572259001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L ND 50000 50000 48800 49600 97 99 90-110 2 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 164 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660538 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008,92572199009,92572199010,92572199011 METHOD BLANK: 3460909 Matrix: Water Associated Lab Samples: 92572199001, 92572199002, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008,92572199009,92572199010,92572199011 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride ug/L ND 1000 500 11/19/2107:47 LABORATORY CONTROL SAMPLE: 3460910 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20800 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3460911 3460912 MS MSD 92571749001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 33.3 mg/L 10000 10000 43200 43300 99 99 90-110 0 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3460913 3460914 MS MSD 92571749002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 10 mg/L 10000 10000 20100 20400 101 105 90-110 2 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 165 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 661720 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199012, 92572199013, 92572199014, 92572199015, 92572199016, 92572199017, 92572199018, 92572199019,92572199020 METHOD BLANK: 3467059 Matrix: Water Associated Lab Samples: 92572199012, 92572199013, 92572199014, 92572199015, 92572199016, 92572199017, 92572199018, 92572199019,92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride ug/L ND 1000 500 11/24/2111:08 LABORATORY CONTROL SAMPLE: 3467060 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20100 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3467061 3467062 MS MSD 92572996001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 995 mg/L 10000 10000 984000 980000 -117 -153 90-110 0 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3467063 3467064 MS MSD 92573126001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 1.2 mg/L 10000 10000 11100 11000 99 97 90-110 1 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 166 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 659812 Analysis Method: SM 4500-CN-E-2016 QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199001, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008, 92572199009,92572199010,92572199013,92572199015,92572199018 METHOD BLANK: 3457478 Matrix: Water Associated Lab Samples: 92572199001, 92572199003, 92572199004, 92572199005, 92572199006, 92572199007, 92572199008, 92572199009,92572199010,92572199013,92572199015,92572199018 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 11/16/2115:06 LABORATORY CONTROL SAMPLE: 3457479 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 99.9 100 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457480 3457481 MS MSD 92571738003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L 0.20 mg/L 100 100 251 232 51 32 80-120 8 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3457482 3457483 MS MSD 92571822001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 66.6 82.5 63 79 80-120 21 10 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 167 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660374 Analysis Method: SM 4500-CN-E-2016 QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199016, 92572199017 METHOD BLANK: 3460134 Matrix: Water Associated Lab Samples: 92572199002, 92572199011, 92572199012, 92572199014, 92572199016, 92572199017 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 11/18/2110:13 LABORATORY CONTROL SAMPLE: 3460135 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 101 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3460136 3460137 MS MSD 92570682001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 91.2 89.1 88 86 80-120 2 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3460138 3460139 MS MSD 92570815002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 76.1 73.3 76 73 80-120 4 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 168 of 185 lacieAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL Pace Project No.: 92572199 QC Batch: 660377 Analysis Method: SM 4500-CN-E-2016 QC Batch Method: SM 4500-CN-E-2016 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92572199019, 92572199020 METHOD BLANK: 3460141 Matrix: Water Associated Lab Samples: 92572199019, 92572199020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 11/18/2110:38 LABORATORY CONTROL SAMPLE: 3460142 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 101 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3460143 3460144 MS MSD 92571467002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L 0.016 100 100 77.5 72.6 62 57 80-120 7 10 M1 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3460145 3460146 MS MSD 92571875002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 31.4 58.2 31 58 80-120 60 10 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 169 of 185 Pace Analytical Services, LLC ceAnalj&al ® 9800 Kiney Ave. Suite 100 Huntersville, NC 28078078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: OSR LANDFILL Pace Project No.: 92572199 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS C9 Common Laboratory Contaminant. D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. E Analyte concentration exceeded the calibration range. The reported result is estimated. J Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs. LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. MH Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased high. P9 RPD between the primary and confirmatory analysis exceeded 40%. R1 RPD value was outside control limits. S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re -analysis). SR Surrogate recovery was below laboratory control limits. Results may be biased low. ST Surrogate recovery was above laboratory control limits. Results may be biased high. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 170 of 185 Pace Analytical Services, LLC ceAnalj&al ® 9800 Kiney Ave. Suite 100 Huntersville, NC 28078078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: OSR LANDFILL Pace Project No.: 92572199 ANALYTE QUALIFIERS v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 171 of 185 laneAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LANDFILL 92572199 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92572199001 MWA R 3510C 1774835 EPA 8081 B 1774835 92572199002 MW-2R 3510C 1772920 EPA 8081 B 1772920 92572199003 MW-3R 3510C 1775183 EPA 8081 B 1775183 92572199004 MW-4R 3510C 1776686 EPA 8081 B 1776686 92572199005 MW-5R 3510C 1775183 EPA 8081 B 1775183 92572199006 MW-7 3510C 1776686 EPA 8081 B 1776686 92572199007 MW-8 3510C 1776686 EPA 8081 B 1776686 92572199008 MW-9 3510C 1775935 EPA 8081 B 1775935 92572199009 MW-10 3510C 1774130 EPA 8081 B 1774130 92572199010 MW-11 3510C 1774130 EPA 8081 B 1774130 92572199011 MW-12 3510C 1772920 EPA 8081 B 1772920 92572199012 MW-13 3510C 1772920 EPA 8081 B 1772920 92572199013 MW-14 3510C 1775935 EPA 8081 B 1775935 92572199014 MW-15 3510C 1772920 EPA 8081 B 1772920 92572199019 EB-1 3510C 1772920 EPA 8081 B 1772920 92572199020 FB-1 3510C 1772920 EPA 8081 B 1772920 92572199001 MWA R 8151A 1774793 EPA 8151 1774793 92572199002 MW-2R 8151A 1774237 EPA 8151 1774237 92572199003 MW-3R 8151A 1775491 EPA 8151 1775491 92572199004 MW-4R 8151A 1776016 EPA 8151 1776016 92572199005 MW-5R 8151A 1775491 EPA 8151 1775491 92572199006 MW-7 8151A 1776016 EPA 8151 1776016 92572199007 MW-8 8151A 1776016 EPA 8151 1776016 92572199008 MW-9 8151A 1775491 EPA 8151 1775491 92572199009 MW-10 8151A 1774587 EPA 8151 1774587 92572199010 MW-11 8151A 1774587 EPA 8151 1774587 92572199011 MW-12 8151A 1774237 EPA 8151 1774237 92572199012 MW-13 8151A 1774237 EPA 8151 1774237 92572199013 MW-14 8151A 1775491 EPA 8151 1775491 92572199014 MW-15 8151A 1774237 EPA 8151 1774237 92572199019 EB-1 8151A 1774237 EPA 8151 1774237 92572199020 FBA 8151A 1774237 EPA 8151 1774237 92572199001 MWA R EPA 3510C 659766 EPA 8082A 660039 92572199002 MW-2R EPA 3510C 659766 EPA 8082A 660039 92572199003 MW-3R EPA 3510C 659766 EPA 8082A 660039 92572199004 MW-4R EPA 3510C 659766 EPA 8082A 660039 92572199005 MW-5R EPA 3510C 659766 EPA 8082A 660039 92572199006 MW-7 EPA 3510C 659766 EPA 8082A 660039 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 172 of 185 laneAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR LANDFILL Pace Project No.: 92572199 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92572199007 MW-8 EPA 3510C 659766 EPA 8082A 660039 92572199008 MW-9 EPA 3510C 659766 EPA 8082A 660039 92572199009 MW-10 EPA 3510C 659766 EPA 8082A 660039 92572199010 MW-11 EPA 3510C 659766 EPA 8082A 660039 92572199011 MW-12 EPA 3510C 659766 EPA 8082A 660039 92572199012 MW-13 EPA 3510C 659766 EPA 8082A 660039 92572199013 MW-14 EPA 3510C 659766 EPA 8082A 660039 92572199014 MW-15 EPA 3510C 659766 EPA 8082A 660039 92572199019 EB-1 EPA 3510C 659766 EPA 8082A 660039 92572199020 FB-1 EPA 3510C 659766 EPA 8082A 660039 92572199001 MWA R EPA 3010A 660178 EPA 6010D 660307 92572199002 MW-2R EPA 3010A 660178 EPA 6010D 660307 92572199003 MW-3R EPA 3010A 660178 EPA 6010D 660307 92572199004 MW-4R EPA 3010A 660178 EPA 6010D 660307 92572199005 MW-5R EPA 3010A 660178 EPA 6010D 660307 92572199006 MW-7 EPA 3010A 660178 EPA 6010D 660307 92572199007 MW-8 EPA 3010A 660178 EPA 6010D 660307 92572199008 MW-9 EPA 3010A 660178 EPA 6010D 660307 92572199009 MW-10 EPA 3010A 660178 EPA 6010D 660307 92572199010 MW-11 EPA 3010A 660178 EPA 6010D 660307 92572199011 MW-12 EPA 3010A 660178 EPA 6010D 660307 92572199012 MW-13 EPA 3010A 660178 EPA 6010D 660307 92572199013 MW-14 EPA 3010A 660178 EPA 6010D 660307 92572199014 MW-15 EPA 3010A 660179 EPA 6010D 660303 92572199015 SW-1 EPA 3010A 660179 EPA 6010D 660303 92572199016 SW-3 EPA 3010A 660179 EPA 6010D 660303 92572199017 SW-4 EPA 3010A 660179 EPA 6010D 660303 92572199018 SW-2 EPA 3010A 660179 EPA 6010D 660303 92572199019 EB-1 EPA 3010A 660179 EPA 6010D 660303 92572199020 FB-1 EPA 3010A 660179 EPA 6010D 660303 92572199001 MWA R EPA 7470A 660190 EPA 7470A 661107 92572199002 MW-2R EPA 7470A 660190 EPA 7470A 661107 92572199003 MW-3R EPA 7470A 660190 EPA 7470A 661107 92572199004 MW-4R EPA 7470A 660190 EPA 7470A 661107 92572199005 MW-5R EPA 7470A 660190 EPA 7470A 661107 92572199006 MW-7 EPA 7470A 660190 EPA 7470A 661107 92572199007 MW-8 EPA 7470A 660190 EPA 7470A 661107 92572199008 MW-9 EPA 7470A 660190 EPA 7470A 661107 92572199009 MW-10 EPA 7470A 660190 EPA 7470A 661107 92572199010 MW-11 EPA 7470A 660190 EPA 7470A 661107 92572199011 MW-12 EPA 7470A 660190 EPA 7470A 661107 92572199012 MW-13 EPA 7470A 660190 EPA 7470A 661107 92572199013 MW-14 EPA 7470A 660190 EPA 7470A 661107 92572199014 MW-15 EPA 7470A 660190 EPA 7470A 661107 92572199015 SW-1 EPA 7470A 660190 EPA 7470A 661107 92572199016 SW-3 EPA 7470A 660190 EPA 7470A 661107 92572199017 SW-4 EPA 7470A 660190 EPA 7470A 661107 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 173 of 185 laneAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LANDFILL 92572199 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92572199018 SW-2 EPA 7470A 660190 EPA 7470A 661107 92572199019 EB-1 EPA 7470A 660190 EPA 7470A 661107 92572199020 FB-1 EPA 7470A 660190 EPA 7470A 661107 92572199001 MWA R EPA 3510C 659764 EPA 8270E 659839 92572199002 MW-2R EPA 3510C 659764 EPA 8270E 659839 92572199003 MW-3R EPA 3510C 659764 EPA 8270E 659839 92572199004 MW-4R EPA 3510C 659764 EPA 8270E 659839 92572199005 MW-5R EPA 3510C 659764 EPA 8270E 659839 92572199006 MW-7 EPA 3510C 659764 EPA 8270E 659839 92572199007 MW-8 EPA 3510C 659764 EPA 8270E 659839 92572199008 MW-9 EPA 3510C 659764 EPA 8270E 659839 92572199009 MW-10 EPA 3510C 659764 EPA 8270E 659839 92572199010 MW-11 EPA 3510C 659764 EPA 8270E 659839 92572199011 MW-12 EPA 3510C 659764 EPA 8270E 659839 92572199012 MW-13 EPA 3510C 659764 EPA 8270E 659839 92572199013 MW-14 EPA 3510C 659764 EPA 8270E 659839 92572199014 MW-15 EPA 3510C 659764 EPA 8270E 659839 92572199018 SW-2 EPA 3510C 659765 EPA 8270E 659848 92572199019 EB-1 EPA 3510C 659765 EPA 8270E 659848 92572199020 FB-1 EPA 3510C 659765 EPA 8270E 659848 92572199001 MWA R EPA 8260D 659894 92572199002 MW-2R EPA 8260D 659690 92572199003 MW-3R EPA 8260D 659894 92572199004 MW-4R EPA 8260D 659894 92572199005 MW-5R EPA 8260D 659894 92572199006 MW-7 EPA 8260D 659895 92572199007 MW-8 EPA 8260D 659895 92572199008 MW-9 EPA 8260D 659895 92572199009 MW-10 EPA 8260D 659895 92572199010 MW-11 EPA 8260D 659895 92572199011 MW-12 EPA 8260D 659690 92572199012 MW-13 EPA 8260D 659690 92572199013 MW-14 EPA 8260D 659895 92572199014 MW-15 EPA 8260D 659690 92572199015 SW-1 EPA 8260D 659894 92572199016 SW-3 EPA 8260D 659690 92572199017 SW-4 EPA 8260D 659894 92572199018 SW-2 EPA 8260D 659894 92572199019 EB-1 EPA 8260D 659894 92572199020 FB-1 EPA 8260D 659894 92572199021 TB-1 EPA 8260D 659894 92572199022 TB-2 EPA 8260D 659894 92572199023 TB-3 EPA 8260D 659894 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 174 of 185 laneAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR LANDFILL Pace Project No.: 92572199 Lab ID Sample ID QC Batch Method QC Batch 92572199024 TB-4 EPA 8260D 659894 92572199025 TB-5 EPA 8260D 659894 92572199026 TB-6 EPA 8260D 659894 92572199027 TB-7 EPA 8260D 659894 92572199028 TB-8 EPA 8260D 659894 92572199001 MWA R EPA 8260D Mod. 659986 92572199002 MW-2R EPA 8260D Mod. 659986 92572199003 MW-3R EPA 8260D Mod. 659986 92572199004 MW-4R EPA 8260D Mod. 659988 92572199005 MW-5R EPA 8260D Mod. 659988 92572199006 MW-7 EPA 8260D Mod. 659988 92572199007 MW-8 EPA 8260D Mod. 659988 92572199008 MW-9 EPA 8260D Mod. 659988 92572199009 MW-10 EPA 8260D Mod. 659988 92572199010 MW-11 EPA 8260D Mod. 659988 92572199011 MW-12 EPA 8260D Mod. 659988 92572199012 MW-13 EPA 8260D Mod. 659988 92572199013 MW-14 EPA 8260D Mod. 659996 92572199014 MW-15 EPA 8260D Mod. 659996 92572199015 SW-1 EPA 8260D Mod. 659996 92572199016 SW-3 EPA 8260D Mod. 659996 92572199017 SW-4 EPA 8260D Mod. 659996 92572199018 SW-2 EPA 8260D Mod. 659996 92572199019 EB-1 EPA 8260D Mod. 659986 92572199020 FB-1 EPA 8260D Mod. 659986 92572199001 MWA R SM 2320E-2011 660747 92572199002 MW-2R SM 2320B-2011 660077 92572199003 MW-3R SM 2320B-2011 660747 92572199004 MW-4R SM 2320B-2011 662075 92572199005 MW-5R SM 2320B-2011 661211 92572199006 MW-7 SM 2320B-2011 662075 92572199007 MW-8 SM 2320B-2011 662075 92572199008 MW-9 SM 2320B-2011 662075 92572199009 MW-10 SM 2320B-2011 660430 92572199010 MW-11 SM 2320B-2011 660430 92572199011 MW-12 SM 2320B-2011 660077 92572199012 MW-13 SM 2320B-2011 660077 92572199013 MW-14 SM 2320B-2011 662075 92572199014 MW-15 SM 2320B-2011 660077 92572199015 SW-1 SM 2320E-2011 662075 92572199016 SW-3 SM 2320E-2011 660077 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Analytical Analytical Method Batch Page 175 of 185 laneAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR LANDFILL Pace Project No.: 92572199 Lab ID Sample ID QC Batch Method QC Batch 92572199017 SW-4 SM 2320E-2011 660077 92572199018 SW-2 SM 2320E-2011 660430 92572199019 EB-1 SM 2320B-2011 660077 92572199020 FB-1 SM 2320B-2011 660077 92572199001 MWA R SM 254OC-2015 660091 92572199002 MW-2R SM 2540C-2015 659745 92572199003 MW-3R SM 254OC-2015 660091 92572199004 MW-4R SM 2540C-2015 660562 92572199005 MW-5R SM 254OC-2015 660091 92572199006 MW-7 SM 2540C-2015 660562 92572199007 MW-8 SM 2540C-2015 660562 92572199008 MW-9 SM 254OC-2015 660091 92572199009 MW-10 SM 2540C-2015 659939 92572199010 MW-11 SM 2540C-2015 659939 92572199011 MW-12 SM 254OC-2015 659745 92572199012 MW-13 SM 254OC-2015 659745 92572199013 MW-14 SM 2540C-2015 660091 92572199014 MW-15 SM 254OC-2015 659745 92572199015 SW-1 SM 2540C-2015 660091 92572199016 SW-3 SM 254OC-2015 659745 92572199017 SW-4 SM 254OC-2015 659745 92572199018 SW-2 SM 2540C-2015 659939 92572199019 EB-1 SM 254OC-2015 659745 92572199020 FBA SM 254OC-2015 659745 92572199001 MWA R SM 4500-S2D-2011 659634 92572199002 MW-2R SM 4500-S2D-2011 659632 92572199003 MW-3R SM 4500-S2D-2011 659634 92572199004 MW-4R SM 4500-S2D-2011 660668 92572199005 MW-5R SM 4500-S2D-2011 659634 92572199006 MW-7 SM 4500-S2D-2011 660668 92572199007 MW-8 SM 4500-S2D-2011 660668 92572199008 MW-9 SM 4500-S2D-2011 659634 92572199009 MW-10 SM 4500-S2D-2011 659633 92572199010 MW-11 SM 4500-S2D-2011 659633 92572199011 MW-12 SM 4500-S2D-2011 659632 92572199012 MW-13 SM 4500-S2D-2011 659632 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Analytical Analytical Method Batch Page 176 of 185 laneAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR LANDFILL Pace Project No.: 92572199 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92572199013 MW-14 SM 4500-S2D-2011 659634 92572199014 MW-15 SM 4500-S2D-2011 659632 92572199015 SW-1 SM 4500-S2D-2011 659634 92572199016 SW-3 SM 4500-S2D-2011 659632 92572199017 SW-4 SM 4500-S2D-2011 659632 92572199018 SW-2 SM 4500-S2D-2011 659633 92572199019 EB-1 SM 4500-S2D-2011 659632 92572199020 FB-1 SM 4500-S2D-2011 659632 92572199001 MWA R EPA 300.0 Rev 2.1 1993 659676 92572199002 MW-2R EPA 300.0 Rev 2.1 1993 659676 92572199003 MW-3R EPA 300.0 Rev 2.1 1993 659676 92572199004 MW-4R EPA 300.0 Rev 2.1 1993 659676 92572199005 MW-5R EPA 300.0 Rev 2.1 1993 659676 92572199006 MW-7 EPA 300.0 Rev 2.1 1993 659676 92572199007 MW-8 EPA 300.0 Rev 2.1 1993 659676 92572199008 MW-9 EPA 300.0 Rev 2.1 1993 659676 92572199009 MW-10 EPA 300.0 Rev 2.1 1993 659677 92572199010 MW-11 EPA 300.0 Rev 2.1 1993 659677 92572199011 MW-12 EPA 300.0 Rev 2.1 1993 659677 92572199012 MW-13 EPA 300.0 Rev 2.1 1993 659677 92572199013 MW-14 EPA 300.0 Rev 2.1 1993 659677 92572199014 MWA5 EPA 300.0 Rev 2.1 1993 659677 92572199015 SW-1 EPA 300.0 Rev 2.1 1993 659677 92572199016 SW-3 EPA 300.0 Rev 2.1 1993 659677 92572199017 SW-4 EPA 300.0 Rev 2.1 1993 659677 92572199018 SW-2 EPA 300.0 Rev 2.1 1993 659677 92572199019 EB-1 EPA 300.0 Rev 2.1 1993 659677 92572199020 FB-1 EPA 300.0 Rev 2.1 1993 659677 92572199001 MWA R SM 4500-CI-E-2011 660538 92572199002 MW-2R SM 4500-CI-E-2011 660538 92572199003 MW-3R SM 4500-CI-E-2011 660538 92572199004 MW-4R SM 4500-CI-E-2011 660538 92572199005 MW-5R SM 4500-CI-E-2011 660538 92572199006 MW-7 SM 4500-CI-E-2011 660538 92572199007 MW-8 SM 4500-CI-E-2011 660538 92572199008 MW-9 SM 4500-CI-E-2011 660538 92572199009 MW-10 SM 4500-CI-E-2011 660538 92572199010 MWA1 SM 4500-CI-E-2011 660538 92572199011 MW-12 SM 4500-CI-E-2011 660538 92572199012 MW-13 SM 4500-CI-E-2011 661720 92572199013 MW-14 SM 4500-CI-E-2011 661720 92572199014 MWA5 SM 4500-CI-E-2011 661720 92572199015 SW-1 SM 4500-CI-E-2011 661720 92572199016 SW-3 SM 4500-CI-E-2011 661720 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/02/2021 09:16 AM without the written consent of Pace Analytical Services, LLC. Page 177 of 185 laneAnalj&al www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LANDFILL 92572199 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92572199017 SW-4 SM 4500-CI-E-2011 661720 92572199018 SW-2 SM 4500-CI-E-2011 661720 92572199019 EB-1 SM 4500-CI-E-2011 661720 92572199020 FB-1 SM 4500-CI-E-2011 661720 92572199001 MWA R SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199002 MW-2R SM 4500-CN-E-2016 660374 SM 4500-CN-E-2016 660571 92572199003 MW-3R SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199004 MW-411 SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199005 MW-5R SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199006 MW-7 SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199007 MW-8 SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199008 MW-9 SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199009 MW-10 SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199010 MW-11 SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199011 MW-12 SM 4500-CN-E-2016 660374 SM 4500-CN-E-2016 660571 92572199012 MW-13 SM 4500-CN-E-2016 660374 SM 4500-CN-E-2016 660571 92572199013 MW-14 SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199014 MW-15 SM 4500-CN-E-2016 660374 SM 4500-CN-E-2016 660571 92572199015 SW-1 SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199016 SW-3 SM 4500-CN-E-2016 660374 SM 4500-CN-E-2016 660571 92572199017 SW-4 SM 4500-CN-E-2016 660374 SM 4500-CN-E-2016 660571 92572199018 SW-2 SM 4500-CN-E-2016 659812 SM 4500-CN-E-2016 660107 92572199019 EB-1 SM 4500-CN-E-2016 660377 SM 4500-CN-E-2016 660573 92572199020 FB-1 SM 4500-CN-E-2016 660377 SM 4500-CN-E-2016 660573 Date: 12/02/2021 09:16 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 178 of 185 Document Name: Document Revised: October 28, 2020 217ceAnalytical- Sample Condition Upon Recei t(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville [I Raleigh[] Mechanicsville[] Atlanta[] Kernersville❑ ConditionSample Upon Receipt Client Name: ProjectWO#� ; 92572199 Courier: ❑Fed Ex ❑UPS ❑US?5 ❑Client ❑ Commercial ❑Pace ❑Other: Il925723 89 Custody Seal Present? Dyes ❑No Seals Intact? ❑Yes ❑No t Dge/InHiais Person Examining Contents: � 1'1 Z _Z 1 Packing Material: ❑Bubble Wrap ❑Bubble Sags ❑None ❑ Other Biological Tissue Frozen? .Vno Thermometer: ❑Yes []No []N/A ❑wet []Blue[]Noneype a ce: 14,7 1, 61 z, z+/ Correction Factor: Cooler Temp: _ Add/Subtract Add/Subtt ('C) 0 Temp should be above frtiezing to VC 7•`3 �. �� ��j.z��(, ❑Samples out of temp criteria. Samples on ice. cooling process Cooler Temp Carrected {'Cj: �{ • 7 1, 0 z,�j/� ,5�, 3ll �/3 ��% has btgun USDA Regulated Soil (❑ N/A, water sample) L(+L Did samples originate in a quarantine zone within the United States: CA. NY. or SC (check mans)? Did samdes on¢fnate From a foreien source (Internationally. []Yes ❑No inciudingHawall and Puerto Rico)? ❑Yes ❑No Comments/Discrepancy: Chain of Custody Present? ❑Yes []No []NIA 1. Samples Arrived within Hold Time? []Yes__ ❑Iva ❑N/A 2. Short Hold Time Analysis 02 hr.)? ❑Yes ❑No ❑NIA 3. Rush Turn Around Time Requested? \ 1 I-;IRYgs Na ❑NIA 4. Sufficient Volume? ❑Yes ❑Na ❑NIA S. Correct Containers Used? -Pace Containers used? ❑Yes [:]Yes []No []No ❑N/A ❑N/A 6. Containers Intact? ❑Yes ❑No ❑N/A 7. Dissolved analysis: Samples Field Filtered? []Yes []No ❑N/A 8. Sample Label$ Match COC? -Includes Uate/Time/IO/Analysis Matrix: ❑Yes l I []No ❑N/A 9. Headspace in VOA Vials (>5-6mm)? []Yes ❑No []N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ❑No ❑No ❑N/A ❑N/A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of spat containers: CLIENT NOTIFICATION/RESOLUTION -Person-cont-acted. Dater Project Manager SCURF Review: Date: Project Manager 5RF Review: Qate: Field Data Required? []Yes []NO Page 179 of 185 �f"d4t"JrSlfitly{lL�iif Document No.: Issuing Authority: fF _ F•CM-CS-033-f1ev.07 Pace Carolinas Quality Offce. *Check mark top half of box if pH and/or dechlorination is Project ' verified and within the acceptance range for preservation WQ# : 92572199 - - - ---- samples.---- _`.—..__----- --= ---.._ --- ' - - -- Exceptions: V0A, Conform, TCC, oil and Grease, ORo(8615 (watery 4pC, tLHg PM: ATF Due Date: 11 /30121 "Bottom half of box is td list number of bottles > � ` � � CLIENT: 92-HOR Q i d d N a Q v 2 N a ¢ y N a v v T v x V O v z O S r O °6 «RR N Q H U n s Y O. Z O v V " 71 c n V S a _u ¢ � v VI V c N ° G O N. v z 4 4 vt s Q u x 2 y Q _V Z 0 Z CL t w Y m .. N r I Z I z n :: v 0 N N ? r to 2 L N o z N } z y� L - a J E - O m a .+ C Pf m a Jr ` N m 1 u - 'f m a J C n - p" m J E N -M In a Jr E: rN-I a_ A a J is N O m �77 ? (� E Q L ,•� '� C Q L r'I ¢ _e[ G N nl c Q M •i r E' tR N NI N r Q �1 O } J Q M O } J O S D a } J d M E O J 0- .1 Y a e a Q > s T i7 J ry N fy Yl d C NC N N H 9 i E in n m a E < e61 C I � O a E u J O N i J O c ?r a Note-Nhenererthere;sadiscrepancyaffectingNar;h{arttCnaeflmpiiane¢seaxPILL s�sapya€thisfemxill�e j�}�yg,�ro�na-0FkNALertif>saflaaDce{I,�, — x Out of hold, Ircerrect pvesetAtive, out of temp, incorrect containers. 3 Page 180 of T85 rdrytnUel Document uo.: Issuing Authority; ARCS-033 Aev.07 Pace Caralinas Quallty office. *Check mark top half of box if pH and/or dechiorination is verified and within the acceptance range for preservation _ - --samples - Exceptions: VOA, Coliform, TOC, Oil and Grease, DROINIS (water] DOC, LLHg "Bottom ha If of box is to list number of bottles Project # v ? a z Z 2 o 2 N m o : a a. i m z it Z is L N Y v AI A C 7 L 2 n E1 9 (: M Y N v V = Q ? 2 x 9 1 I Q m 71 -3 ticc Z } N G m 2 Y .a. 1♦ z 4 is a fd v L 2 A— T. Q Z z v ;� en m ¢ \ Z a y 7 a n m a e u a e n C m a ry z Q N v a a y a G a O ut ' y O Z t w 3 3 3. Z M N 2 v _ e�,r 2 Q `" a > y Z 7 e c J J d a J 4 s Q a Q °,� ~ ¢ a Q Q o C o aCL n" E J c vi a G o _w E o in E ' _ ° m v a n E �j E > E °� c i is E n E o ,n s J m N a ., N N g ❑ = ZR o a 3 7 N ] - .-- rr _ ui_ 2 µ U .. LL 19 7 .4 = w 7 M elf A en M � 2 of m 7 of 1 = Q X- V a m m m m m m m m Q a 4 Q �. Q �7 Q l7 O G7 > l7 ? a )] in d N a 4 ^J .Y�i L9 N vt a 4 > d - �_ j NK, A T7 5V � v . 4 y 6 4 X��� t , \ \ \� I N X X, N\ \�XN N ,.z z pH Adjustment Log for Preserved Sampis Sample M Type of Preservative: pH upon receipt Date preservation adiusted Time preserv4p Amount of Preservative adjusted added Lot 3 Isote.-'lVheneverthere�s-a-discrepancy-atfetting�Narth-Cara ina-mrnpIlanee-%fnples a�apy-0f this farrt�;vilRhe v� }�iio ,6araiina�SHNR Carhflcatios{ Gffice {I, a, aut of hold, Incorrect preservative, out of temp, incorrect containers. 's } Page 181 of t185 Condition Upon Receipt(SCUR) Page 2 of 2 Document No.; Issuing ALthonty: F-CAR-0-033-Rev.07 Pace Caroinas Quality Office. "Check mark top half of box if pH and/'or dechlor(nation is Project # verified and within the acceptance range for preservation - - - - - santplis,---- _ — -- — - - - .Exceptions: VOA, Coliform, 7OC, Oil and Grease, DRO/901S (water) Doc, LLHg "Bottom half of box is tb list number of battles PG�� — " d Y z a. a ai m N z m u ay ry 'tl m ry u. Z ? Z Z C L v S V m ^ d ? V x Y I Q z N ; ? a a a v v v�i a 4 z ti N ° v a a a m C O M " _ m S a a v y A m z L In u v ° c c vi (] a O. a a 0 v0r p T ry a a a 2 _ V 3 ry x Q 2 a N ] A = C C a V V W ] = U M L 7 x ti =.'a d 2 o c 7 _ U V u y U G n = ° v b a o a o E a E ¢ d ¢ t a a a 'a E a O O .+ J J J Q ¢ J- Q n > j n a ys H a W E E E E E E E a °�`+ u a E ° a E E H en E E E c E E E N N �uy� _ 1�7C o >c _. Yet r� ti a :i 7 `a ~ N `ti N IT Y I r M - M A In N Q - 3 7 3 2 LJ 7 = u1 T 7 a In m - 1 N rL - •i A y q rl en d Rr M a a a .r l7 et l7 M 0 ,� l9 M l7 l7 fi L7 � h tl Q C u~1 P. m O cn rn m m. m m m m m 3 a a a a . a < n [7 } l9 y o > = s a. a - j A a C Nl� I 3 I \d\N, N l 4 -? \\N L 5 N N\�\I 6 1\\\\� 1\ N\N -T--\\ 1 N N N�S\--I- I I 9 I \N\ N. N- YO I NNN\ N N\' 11 1Z —�LL \—NN\ pH Adjustment Log for Preserved Sampes Sample ID Type of Peeservative pH upon receipt Date preservation adjusted Time areserAin Amount of Preservative tot R adjusted added —Noce—Whenewthereis-a fire ancy affecting,Yarth 6araiina c9mp11anEe sameles a�eov-0i rhis faxm�vill t;e sod p Out of held, Interred preservative, out of temp, Incorrect contMners. :e-�sAh:�aral�na�DF,FiNR-Cert�flcahon-g0ice-{I, a,--� i Page 182 of 186 L CHAIN -OF -CUSTODY 1 Analytical Request ao I!Z,ftal• : nn.rurwico• Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields be t° Submitting a sample via this chain of custody constitutes acknowledgment must completed accurately. and acceptance the Section A Section B of Pace Terms and Conditions found at hftps://info.pacelabs.com/hubfslpas-standard-erms.pdf. U Required Client information: F Required Project Section C Invoice Information: M 1L Company: HEIR Engineering Report To: Mark Fi;ardi Attenticrt ' Page 1 �f ' � Address: 440 S. Church SI Copy To: Company Name Charlotte. NC 28202 Address: Email: mark. filardi hdrinc.com PurchaseOrderk Paco Quote: ft ulato A Phone: (704)33M787 JFaX Project Name: OSR Landfill Pare Project Manager tyler.Forney pacelabs.com, Requested Due date: Project 9: Paco Profile 9: 95gg..q State 1 Location I SAMPLE ID One Character per box. (A-Z, 0-9 1, -) Sample Ids must be unique W 1- 7 MW-1R 2 MW-2H 3 MVy-3R 4 MWAR 5 MW-SR 7 MW-8 8 Mw-9 9 MW10 10 Nlw-11 ADDITIONAL COMMENTS MATRIX cnbE D[Vnkim Wain ON ro m 4 aU wmm WT S U Waste Wale, WW a _ m Q Produtl P So.Ilsoha SL Il on OL ? START Wlpe WP A, AR o a} Q hrr OT V Ti.. TS >< F w n nATF T COLT-Fr`TED wT I "INer1 (I q0 WT /zt � 5tic wT �trl��2ilt?`{S y 0 1 L t-ICJCIVtl�IyCJ r U w JI END p a q c W � CI O N Z C N m O m v c ` n U m O DATE TIME h=IJ IX, /, 133 vYr t�ca%x O S f %Y0Wr tJ rt— 1Y20 rt�l°. Q14 wr I /y/11 t. r e�y{ wr lOtxs _ wr MUP!OU48HEDR (AFFILIATION " 9 11 k 1 DATE I TIME x IX"Iz ix Ix tr ACCEPTED BY) AFFIL[ATIOH DATE TIME SAMPLE CONDITioNS NAME AND SIGNATURE Name of MpLI=R: c� 0 � m iSlof SAMPLER; a o p a — Dz- ATc Signed z z E z i ceMalytical� � xw esuue: cox Section A Submitting a sample Via this -� C HA I' 1 _O C_ 'l CHAIN-OF-CUSTODY r pDSTODY /Anal O Required Clientlnformation: chain of custody constitutes acknowledgment Section $ in The C ain of -Custody is a LEGAL D0 ytical Rege��St po gment and acre CUMEN-F, q}I cument ptanr� ompany: q En address Required Project Info information- re}evant {ieids iNUst be CORipleled a Section C CCuratefy, Dt the Pace Terms and Conditions found ai h'lPs:"ino.Pacelabs.com/hubfs/pas-standard-terms G 440 5. Church S[ Church St 'harlotte, NC 28202 Rep°rt T°� Mark Filartli COPY To; Pacelabs.com/hubfs/pas-standard-terms. Of Invoice info Information.- tl - :mail: mark.MarM hdrinc com 'hone: Atlenii°n� Company Name: (704)338�767 Fax Purchase Order#: Address: .equested Due Date. Project Name: 2-SR Lantlfill 0...:.. -... Pace Owe: L SAMPLE 11) One Character per box. 3t IA-Z, 0-91, -} Sampte ids must be unique iU F- 13 Mw-14 14 15 , SW-1 1s sw_2 17 SW3 18 SW-t 19 20 21 r 22 r/1 23 z4 ADDITIONALCOMMENTS Pa 4 ce Profile #� -yrcr-lorney 2 568 pacelabs.com _ d State! -eau MATRtx D.'"xr�y War' DW E { COLLECTED Re uested Anal sis Fite r rod Y!N NC Wmer wr Was te Naeer yryy m z � Preservatives z }` PrOAvd S.IVSGIId r SL - G J Oil w Ar wa as START EN➢ o U +1I Oni"r Trsue T5 L) a w ¢ w = 2 + f U f' p [ $ i} r a w = m in r" TIME DATE TI a o q oDATE o z io o o C A o U wT ; rt1 fZaG r!%rrr fz f I t /' } � N VV-f 'J r��/Z; 11JU �7�< <rs�: A x x x m a x x x x x wT tl t 23c, ((16 VVT '163/� left tY x wT x x x x x x x v l i�og 17r,'t �12 ? x x x x x x x x - r r� RELIIVQU,� ED B"AFFILIATION DATE TIME ACCEPTED BY !AFFILIATION / i DATE TIME SAMPt_E CONDITIONS t r fiJ 7 ti SAMPLER NAME AND SIGNATURt PRINT Name Of SAMPLER: SIGJ -LER: c Ot SAMP � ° — - - - DATE Si _ Qned;� a a ?' m z U U rn c !_ �a'ceA,aryrrcar' CHAIN -OF -CUSTODY 1 Analytical Request Document Submitting a sample Section via this chain of custody constitutes acknowledgment The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed A Required Section B accurately. and acceptance of the Pace Terms and Conditions found at https:!lrnfo.pacelabs_com/hubfs/pas-standard-terms Client Information; Required Project fnformation: Section C df. p Company: HDR Report Td Ben Weiserbs Invoice Information,- d Address � 440 S. Churrh 51 Copy 7a: Attention: Pa e ; T Of t Suite 900, Charlotte, NC 28202 Company Name: Email: Purchase Orde Address: Phone: )-x Protect Name OSR Landfill Pace Quo[e: Reaulato Agency Requested Due Date, Prolecl # - Pace ProjectManager, _tyler_torney .pace labs. com Pace Profile #. 4E89-q State f Lccatian a Ra uestad Anal sis Filtered Y!N NC MATRIX Dnnking water OW — O U V COLLECTED Z Z Preservatives r Wolcr YT, Wt., WT m SAMPLE ID Prndud so,usol,b WW P b_ ¢ U One Character per box. On Wi" 54 pt„' WP t? START END o w Go z } AR o w w m ti Sample Ids must be unique T ur o o s X a w w Q z 2 o _ m v q ° g b X a 3 ti vi DATE 71 ¢ o D c c�v 2 = t� o U m z Q o c a o p o m 2 m -o `6 ME DATE TIME 0 z 2 3 1 • ti 5 6 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY! AFFILIATION DATE TIME ACCEPTED BY! AFFILIATION DATE TIME SAMPLE CONDITSONS SAMPLER NAME AND SIGNATURE PINT Name of -SAMPLER' c SIGNATU of SAMPLE . 0 Signed: Y C i F tr Z a'} g m o Z '�U } n v} cz This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix C - Field Data t r- Appendix C — Field Data Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix C — Field Data This page intentionally left blank. DEPTH TO WATER AND GAS READINGS Project Name: OSR LandRll Locaiton: Winston-Salem, NC Time Started: � - personnel C / ,` l 11VAMNI MW-2R ti Date: Aber w 10243102 projec Time Finished: Signature: ii, R,na.,w. Sheet I of 01 Groundwater Sampling Form Sample ID: MW-iR Site Information to Name: OSR landfill Project Number: 10243202 Site Location: Winston Salem, NC Sampling Personnel: cr Date' H %7n Weather:r7 Well Information Well Diameter (In): 2" Purge Equipment: Geotech Screened Interval (ft): 4S' - 60' Pump Type: Dedicated Bladder Pump Well Depth (ft); 60' Pump Depth (ft-bTOt): Depth -to -Water (11.11 C): 7(::� Tubing Diameter (in): 3/8" %1/2" Water Column Thickness (ft): Well Volume (ftA3): 1 well Volume=(Total Depth -static Water Le ll•Well Capacity Well capacity(gallons Per feet): 0.75"=0,02; 1"=0.04; 125'=0.06; 2'=0.16; T=10.37; 4"=0.65; 5"=142; 6"=147 ,elms tnFnrmafin Parameter Instrument(.): Hanna, YSl VOLUME TIME PURGED IUl CUMULATIVE VOLUME PURGED (Laars) PURGE RATE ImL/min) DEPTH TO WATER (f,bTOC) PH (SU) Ip_ll TEMP. ICI COND. Iµ5/un) (5%1 DISSOLVED OKKGFN Img/L) (10x1' ORP fflual W COLOR/ (mV) IMU51 (510 ODOR (]20mV) or 10%) (EesulbU 41 32, F 99 1 1 -It 2122 1, O 4 can 53 • A(.�3 16 .+Pl. 3 3,fJ 1?.12-7 ff, ,Ct 20 GS.7 KZI-z.l rtl 3. ,941 y 33.)4 4 6.9 �_ crD 9 -CeD, 3 2 400 S 20 . /64•t 11 4m ,2 cx5 .6 r-l73.2 � • DD below 2.0 mg/L a Deree at f0.2 m./L; W below 0 5 mg/l :name Sample Number ColleRae Parameter ime MW-1R Notes: Pumprate= .fit/lE4e�% : £3 Sow Container 1 Preumev. N ex Sheet I of I ?� Gm,'ndWBte►sampling Form .r.e,.n.a.. Diameter N: 2' � ~r :raid IntM'�1}t�; F 7i 1 RimlLlflM�'�CUMU�RiIVE PURGE y TML R;ypLUMf yO'UM[ RATE Itl. 11 i�U l ImUmIA i mnempR ynpe A.>'M1e' Trme (Tntal (Dept Water Level)' Well Capacity 1^:0.04; 1.25"=006; 2-0.16; T-0.37; 4" Sample ID: MW-ZR 5" = 102; 6" = 147 Oi550LVE0 ORP L�1151.0,j"COEOP/ [ONO. OXYGENTEMP. IrrVIOR9 UI) ODOR ISUI IpGocov 1.30mv1 IC•1 (s%1 (mg/q ,tae:.ribe parameter -jr -,5,7(4j� g 40e///sEV �1 sr � C.rta,rer I P'..Kve 2-1nc�,,L � 6 M MGn� 2-ILAv,4G Gmw4+a w swnprmr4 Fam eewea kenah F_ 12 - Z7 sNeet '_. d 1 s.NvAe m: %A* ,u I:•, :TAE- ='d Jpt`-4a:. Ma<.:e.N `�W ia. a;\ •2�=,X r=-6 3_^3- J65 CI6 4 —^+T �iQnliUgl r A�!•4 :�V-J-h JEs_ TVA f1PCiJ >JC'J 4- rS_ 3W JD'uES 46t�1 Oi= .�iR.n�-•, J'.Ji; `JJJF rx4! ,_y__ •:-= r,- :. (�, i-.N 141..9 S:J / vEc �r - 4!- 7 _ci ow - 19 .41 0 17r%o N.8 I 40 - ?.�f 2 8 "� !- �! -52.7 c +L! Od 171c! 6 39 2.0 -s�_2 1 4A s3.3z,=r •WMma2Amg/lKvable c-g ar�amsli n:-. h'i-z._.s rase 1 6aR4k Number I ��ieA I Parameter Tmte Container Presemtive MW-3R Pumprate= rgz7O �►sc r-�Cl� I2Sµ1-R 12 2-r�..��^6 c Ai —IL ,a,,6 0� Sheet _ of _ Groundwater Sampling Form Sample ID: MWAR Well Information Well Diameter In): 2" Purge Equipment: Geotech Screened Interval (R): S' - 20' Pump Type: Dedicated Bladder Pump Well Depth (R): 20' Pump Depth (R-bTOC): Depth -to -Water (R-bTOC). r .r7 Tubing Diameter (in): 3/8" X 1/2" stet Column Thickness (R): Well Volume (k^3): l WellGoadty 1 Well Volume = (Total Depth - Static Water level) • Well Capacity - ... __. parameter instrumeMt( s): Hanna. YSI Purging Information MIN «' ����I�Mvm— r— L'SI�:1111MIlt 7 ''►r, ir�7L Y7® 1 AMON a-TMMrM1v!*.7rly3iiC�?G'iyF�lE�C7C ✓1i ®6 PTO PW"r sI a aCrl Mroa �TTrr� rr PAIMPOOMFMI , tm MA►MMGsMAMMM 7"7 Information I Sample Number I colle lion I Parameter I I 1 nm container P.e:ervatrve MW-4R Notes: Pumprate= Sheet L of -- �r ` Groundwater Sampling Farm sample 10: MW-Slt 30' Column Well C -M 1 Well Volume = (Total Depth - StabC Water LeveO' Well CapacitY �t1:a 7s"=0.02; 1"=- D04, 1.25"=0.06; 2"=0.16; 3'=0.37; C CUMULATIVE DEPiH COND. VOLUME PURGE SU TEMP. OXYGEN TIME PURGE 0 VOLUME RATE TO toA IC.) (V(5%) Jim)- (Utersl PURGED (PURGE f-11 ATER (toll (5%1 I10%I' O Collection I Parameter Sample Number Time MW-SR Notes: Pumprate7K5/L.,I_V,e 8�sr 5" = 102; 6" = 147 ORP TUR61017V COLOR/ Imv) (NTUij (slo DDOR 1220mV) or10%) (de¢nbel Container Preservative k Groundwatersampling Form Ate 44" OSR I ell p sit, 1 h t°DatlpL\. Wmslon Salem, NC Site I lormaElon P l et N b . 1/143102 Sampling Personnel: �. [_. c I Sample ID: NIW 9 R VOLUME CUMULATIVE VOLUME PURGE OEPTN TO PN TEMP. COND. DISSOLVED OyyGEN OPP (mVl TURBIORT INT.0 (510 �DOOP THE PURGED PURGED RATE WATER Du) IC.I IPS/[ml (mgnl 420MV1 or 10%) Ides[rlbel Iutey ltttersl ImL/mint0.11 I (N-blotl Ig% pa%)• 3360 < /fCL'n 31.4 4 1 .,3 i-17 %r lI q r4S 1 5-2 3 . f ev o (op 3<D 3.2 5. 2 Is. I ss v ,. —,..,..,mg,Lu, Vme.,=.,mg,tD0., ....mg,. Sample Number Calleetion Parameter Container I preservative Time M W-7 Notes: Pumprate= Sheet L of fJ` Groundwater Sampling Form Sample ID: MW-B Site Name: 01111 "dhll Site Information Site t outltm: WmstomSalenl NC Project Number: 10243102 Date; 2 Samplln Personnel: /', r / Weather: V Well Diameter In): 2" Well Information Screened Interval (h): 12' Purge Equipment: Geotech 27' WeII to (h). 77 Pump Type: Dedicated Bladder Pump Depth -to -Water (h-bTOC): 3 Pump Depth (ft-bTOC): 2•% Water Column Thickness (ft): Tubing Diameter (in): 3/8" X 1/2" O, Well Volume (ft^3): 1 .7 1 Well Volume = (Total Depth - Static Water LeVei) - Well Capacity We" Capadty(111ons Der feetl n7,-n m. .••_,. ,... P ging Information Parameter Instrument(s): Hanna, ySl NMUI TIVE VOLUME PURGED literal PURGE RATE (mVminl DEPTH TO WATER(h bTOC) pH (SU) Ii0.11 TEMP. (Cl CONO. DISSOLVED ORP TURRHDM COLOR/ O%VGEN LOA,l 1.1 (wuU) (510 ODOR Ll 15%) h , (t30mV) or 10%) (describe) • d70 1?36 5.24t (5.41 L O'G 33-31 7_S 5,r8 t5_3 1 3o9.f 35.1 9 2 / _2 .24 5- L(Ute�j 40 ? 25 r5_3 )7, .71 a -NA 4 ,75 5, L r-t r7. 3 2�- r7,9t ,23 /S-2 ,i •r T 0-22 c N s_ o r •� sz 1s_ p, rS-I 3 32�r.236,7t C&uA/.4 ' w,.emw co mg/us stable at S0.2 mg/L: 00 below 0.5 mg/L is stable ) I Sample Number I Collimection I Parameter I Container I Preservaw.I Te MW-8 Notes: Pumprate=G(<Z)w,r r Sd (Fine Q275 $041 /4dg2 gt sl , lft gv I Time: MW-9 Groundwater Sampling Form Sample ID: OCR Well Volume=(TP[al Oeplb- Static Water Level)' Well Capac$w I4J OJS" = 001: 1" = 0.00: 1.25" = 0.06; 2" = 16' 3' = 0 37 4" = 0.65' S" =1.02; 6" _ r�ME VOLUME PUflGfO (LA, CUMULATIVE VOLUME PURGED ILke6 PURGE flRTF (mI/mml DEPTH TO (WATER PH (5U) IY0.1) TEMP. lC) CONO. lµ5/cml (5%) DISSULveu OY (mg/1.) �L) (10%1- GRP lm`/) U20mV) NRBID)R'E1530 ImtlsR oe 10%1 Itleu,�bel .�� .6 5, 4 I • I,b _ 5.10 r _ 259.1 4. �L 4 160- ` J-z f.0 5, 78 21 A "f 2, _7 5,�13 ��37: > f i �raao yg 4 t 3.Sf � G • z ', . DO below 2.0 mg/L is i1a the a[z-I TV c, u1-1— v --..._., I i M Cpllettion CUn(amer Preservauv Sample Number Parameter Time M W-9 Time: Notes: Pumprate= Sheet Cot 3 N._ o,oan e I_Yz Sample ID: MW-lo Groundwater Sampling Form Interval (ft) h (R): 21.0' X 1 Well Volume - (Total Depth Static Water Level) -Well Capacity Well QPactV(gallons per feet): 0.7V-0.02; 1"=0.00; 1.25"=O.W; 2"=0.16; 3'=0.3); 4"=065- 5" 02; 6"=14) Hanna. VOLUME CUMULATIVE VOLUME - PURGE -RATE D H TO pN TEMP. COND ' D155OLVE0 OXYGEN ORp TU"aDn" COIU^r (..V, (NTUs) (510 OOOP TIME PURGED PURGED WATER (SU) YGl) (C) (IS)[m) IS%1 Img/Ll (.20mV1 ar 10%1 l4escPlwl (Liters) lure") (mVmin) y� (fCbTOC) 6.36 1 . l601 _47 -32.2 45. 40 �/ .8 1 3W 1 .6 17 1.92 35.2 7 !cN .f! 57.36 o . v !61 .5 -3 55 , si 2 _o S'on ! 6-34 .6 (60 !O 4/ S. cC, 1/. s 6.34 6. I 3 3_8�'g�?•7 ( `� 1 73. l/ tl 4. //. 5 31^ /6 4/3. 156.5 . = mg,.iss.ae,ein... mg,.;—..,—... II Collection I Parameter I Container ' Preservative ' Sample Number Time M W-10 Notes:: Pump/rate= r-ICU..r.d1rd. UiScGr c�(S� ' S Sheet Hof '3 � t ���•/����.��IMM=���d-1J�,�J�IJ �.KIM ' DO below 2 0 mg/L is stable at t0.2 mg/L; DO below u I mWI �� °•�0"°S° Sheet of Sample ID: MIl" t0 •r, Purging Information Parameter Instrumenl Hanna, YSI -YG VOWME CUMULATIVE PURGE DEPTH TO pN TEMP. COND. DISSOLVED OIttGEN.+3, ORP TUP810RY COOR/< ODOR TIME pURGEO VOLUME PURGRO PATE WATER ISD) ICi lus/<m) (mg/LI (mVI 1_20,V) INTUsI (510 or 10%1 (deunhe) IUten) (Lite6l (mt/min) (k-bTOCI 08os _ .c/ og ,ON 6 13-7 5.7 S- 6 I5- �• S Qrn• !q7.-3 -5. r g 5. 5 23.7 2$ to 1-9.5 I Z76,31.53 2S •' 2-O Noo 4.7m 6/1)-5.2 1 M9 1 a. cir I. yc3. .v 2,1/ Jail JQ.20 1,5.67 115.2 j2-X,(aln.,Q5(5- 5/2. v yoo v. z0 G 5_ 277-6 ES 2 Sos, f 8a .`� tioo S.6`I �3 Z99• O.Yg �1H3_( .l 277. I .3 $ 7S7 afSS ti y,�v 00 1 `/.z I 1 5-43 1 U.41 1777, 61 C."28 16. 2 89 • DO below 2.0 mg/L is stable At±01 mg/4 DO below 05 mg/L is stable Sample Number I Collection I Parameter I Container 1Dreservabve me MW-11 Time: Notes: Pumprate= Groundwater Sampling Form w: Yr ry.M.l -• r V�. qn P{l r0 TI II MP rrlpry IiP:inllp •M �5"'�� q.hd:r I Wp11q 15111 Iu\/rml pdr�W sneee� Sample 1O: MW.11 MP fpP9.Ullr � ImVI 1•rtoq 1;1 ca 9a/ ��1/�■M �i7��}a��tel�Ll.�ea���� � ��j,i� DO below 20 mg/L is sta a at i .a M . Sheet L Of L KRGroundwater Sampling Form OSR 5.58' - Well 1 Well Volume = (Total Oep[h -Static Water LeveQ' Weli Capaci3y Well Capacity (gallon, per feet): 0.75"=0.02; 1"=0.04; 1.25"=0.06; 2"=0.16; 3'=0.37; 4" Hanna. Sample ID: MW-12 5" =1.02; 6" = 1.47 VOLUME CUMULATIVE PURGE DEPTH PH COND. DISSOLVED ORP TURBIDITY COLOR/ ODOP nME PURGED VOLUME RATE TO (SU) TEMP. ('skm) O%VGEN (mg/LI V (m 1 ryNsl I530 (descrihe) lUbo, PURGED (mUmin) WATER IE0.11 (C) 15%) (10%)• U2GmV) ILilen) (R-bTOC) S ti SlO£3 c o s 2--% 13.12 1 5 2 a 8 0.0 l c y ,5 7'15 I -1 �7 c( , .P1..[. m&LU..lean S.t mGlq Woeiow u.�ni6l•oa."�i� Collection Sample Number r M W-12 Parameter Container I Pre '.t'Ve 1. A G ao6 G A* Sheet -L Of —L Groundwater Sampling Form Name: Sample ID: Mw-13 VOLUME CUMULATIVE VOLUME PURGE DEPTH TD PH TEMP. COND. DISSOLVED OXYGEN ORp (mVl TURBIDITY INTUs) 510 w"'^r ODOR TIME PURGED PURGED RATE WATER (Sul IC') IPR�cm) (5%) (mg/LI Y30mV) of 10%) (deienbe) (VIersI (Lite.) (mVminl (k-0iOC) (aD�1 n.o y. s.v a Sv 40o qYS 5.1N (G. az 5_06 264,0 5 " Iu mil a8 .cl /ruA Y.a7 5.Ic1 16,8 He a 3 cI.OU rV 2.-1 l 7 396: 3 2_ 4_52 a9 Ell E '' W bNow 3.0 mg/L Is table at l .i TEVL; 00 below OS MVL IS stable J I Sample Number I Colledicm I Parameter I CbebibeT I Preservative I ime I M W-13 Pumprate= [.�S�CSrc �: 2 ') . 7 Sa 5ulvie 5270 pogv c 2 Time: 12-km ZPL -rZti z.t 05' ate N� vy r v,.ar,n h lIXlnan N lu.. Wnm Ipl O'a!rgNr (Inl. l T'eata0 Imeaal (NI: 1i=f ] elI OePtb (R):: Groundwater Ssmplln/ form U In nrmatlnn __ Pro KI Numbrr 101e1101 L We, = (Total DePr6' SMM Water Le Well Caaac q - _. -.... _nne r]5'=006: 3"="' 3' : =031, N TUK LQUMF PURGE VOIUMF TO P a„mtn vu0.GE0 (mMn mm wa;Efl, f.aVtl Gr Street 0f / 'tJ' !z{ Sampta lo: rs"" _ 6.. _ OflP `:V)Mq COL0V 8aI 100x1(Tl Y M N0. TUU NToflrz D00.0./ Ic•1 IP5/cml ; (t20. (aube) Isxl n0EDre � 1• - , I Sample0 .leer I Collectlpn I Parameter I Cantamer I Preservative I Time MW-8 Notes: NC Groundwater Sampling Form ESP Sheet r of Sample to: MW-15 .>•ev..acer IR-o2oc(: iY I Tubing Diameter (in): 3/8" X 1/2" at" Column Thickness (ft): [/ Well Volume (f -3): I Well Volume = (Total Depth - Static Water Level) . Well Capaow WNl hpa<ity (gallons per feet):O]5"=0.02; 1"=O.Da; 115"=0.06; 2"=0.16; 3'=0.31; 4"=0.65; 5"=102; 6"=14] Purgi g Informatio Parameter Itutn2mentlsl: Hanna Vcl VOLUME CUMULATIVE nME PURGE. PURGE VOLUME RATE (LRers7 PURGED Wren) fmL/min) DEPTH TO WATER (k-PTOC) pN ISDI ltot) TEMP. IC.I COND. luslunj 0%) DISSOLVED OXYGEN mg/L) (mg/L) (10%j• OAP ImVI IT20mV1 TURBIDITY COLON INTL'I (510 ODOR or 10%) Inesrnbel f055 •y Oo 39,39 _ 5 (7.7 •1/ NG<::) IlG3 4 �` 7,3'-/ 3.1.3L N q /4,0 20.1 39z3 V 1 2-7 .79 !• L/ •�I 37. 35 4,41n 14. 379Hl 1-72 109.7 22 1 T 34.3 4. 372. 1 5 _O 3 . 1.6(1 NQ f Sample Number I Collection I I I I Time Parameter Container Preservative I MW-15 Notes: Pumprate= �N f l 3 o S �Gl�e z7 o vogfl'2 *-1612�6/'A-s Zs �.c P1, IUApH t Z.. 2-1 L �.�G N—. n/Whb Sheet —_ Of — .../// + lSample ID: `SW-1 ` Groundwater Sampling Form � Well Information well DlamelW in(: N/A purge Equipment: N/A ScreeneNl Interval (ft): N/A Pump Type: N/A Well Depth (-1: N/A Pump Depth Depth -to -Water (k-hTOCJ: N/A Tat Diameter (in(: N/A ater CWumn Thickness (k(: N/A Well Volume (ft^3(: N/A 1 I Well Volume = (Total Depth-Statle Water Level)' Well Capacity I l W-I1G 'ty(g 11 p feet): O75 002 1 004 125 006 2 016 3 0374--065- 5"=302' 6"=1.4] Hanna, aLIRUD ®�F-�® "IMEN DO bNow 2.D mg/L k stebk at ID.2 mg/L DO below 0.5 mg/L isstable ' Sampk Number I Collection I parameter I Cantamr IPresemativel Time Sheet _ of Groundwater Sampling Form Sample ID: SW-2 Vs ',ton Salem. _ Well Information Iven I)•a "tor In : NIA Purge Equipment: N/A Screened Interval (it): N/A Pump Type: NIA NI Depth (R): N/A Pump Depth (ft-bTOC): N/A DepM-to-Water (ft-taTOC): NIA Tubing Diameter (in): N/A ,ter Column Thickness (k): N/A Well Volume (ft^- N/A 1 Well Volume = (Total Depth - Static Water Level) • Well Capacity Well Cac4 ity(gallons per feet): 0J5"=0.02; 1"=0.04; 1.25"=0.06; 2"-0. 16; 3'=0.37; 4"=0.65; 5"=1.02; 6"=1.67 Para Purging Information meter Instrument(,): Hanna, V51 VOi CUMULATIVE TIME PURGED VOWME lu2ers1 PUtbrO PURGE Im4minl r'/m DEPTH TO WATER (k-bT0[)- PR (SulTEMP. ImD1Ic•1 sot IIS%) COND. IP(5%) OISSOLVEO MCOLOR/ O%YGEN Us)0000. Ime/qtiters) IM,(describe) wmOm'[.Umg/L ms bleM�,2mg/g00below C.5mg/Lisstable 1 I Sample Number I Collection I Parameter I Container I preservative I Time SW-2 Notes: r>r Sample 11). SW-3 L17 Groundwater Sampling Form -� hame4er )"t• to Wall rer n arva.F w•• yyelivolume (ftA3): N/A Ma!n Column TIIdowss (R): N/A - Static Water Eeveli - Well6PaCl a, B"' 1 41 - 1 W ell VPWme - li OMI Depth 0.37; _ ObS; 5" =102; WMIC.Pac,Nflallon,P-1110'075=002: 1"=0.04; 1.25-0.062"=0.16; ; 3'= Purging Information ararneter lnstrumentls): Hanna. V5 ruaelom' COLOR/ WtUME CUMUNnV[ PUFGE OEPiH To PN CONO. TEMP. rn5S01vE0 OLyGEN oar y INTUO 1510 I OOP VOIUME TWR PURGED PURGED RATE WATER IVS/cm) (SUI ICI Im6/L) I]20mV) or 10%I 20 I4eXnbe) 111—) .._ (mUminl �.. ....�. inO Tj IS%I n0%1 Sampe Number I Collection Time SW-3 Parameter Container 12C0d 3-LrC�,L Preu.ba . Sheet —L of 1 Groundwater Sampling Form Sample ID: 5WA rarameter (nstrumentfsf: Hanna, YSI . _. e...e ....�....a..a.. VOLUME CUMULATIVE DEPTH TIME VOLUME PURGE PH CORD. DISSOLVED ORP TURBIDITY CGLOR/ PURGED PURGED RATE TD (SUI TEMP I45/cm O%VGER (Li4rs1 ImVmin) WATER (D•) 1 Im8/q (,o IMUs) I51G ODOR (liters) (tt-bTOC) (•-D'LI (5%1 ('20rrV1 or tG%1 (descnbO 0%1• kq,0 033 6_09 -5"1 120,0 Clt�.i l4 f UU bn. 2.0 m8/L m sable at 1U.2 mg/L; DO W.0.5 ma/L is stable ( I Sample Number I Collection I Parameter I Ca M,.r I Preservative I ime SW-4 ... is: Pumprate=1-(Cn"//'"/, 92C...L�, 3.�G(Ci..L �n. (j � L This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix D — Electronic Files (Paper Copies Only) f 1 Appendix D —Electronic Files (Paper Copies Only) Portable document format (PDF) of this report Electronic data deliverable (EDD) of Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix D — Electronic Files (Paper Copies Only) This page intentionally left blank. HDR Engineering, Inc. of the Carolinas 440 S Church Street, Suite 1200 Charlotte, NC 28202-2075 704.338.6700 NC License F0116 hdrinc.com © 2022 HDR, Inc., all rights reserved