8002_Rowan_NeedmoreRoad_CelaneseFibers_Indus_May2021GW_Nov2021GW_FID1680265_20220601

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2021 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
CNA Holdings LLC
Irving, Texas
Project number: 60683034
May 2022
Delivering a better world

2021 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
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AECOM

2021 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
Table of Contents
AECOM Project number: 60683034
1.
Introduction...................................................................................................1
1.1
Site Background............................................................................................................................... 1
2.
Summary of Monitoring Activities ..................................... ............................2
3.
Summary of May 2021 and November 2021 Monitoring Results.................3
3.1
Groundwater Sampling Results....................................................................................................... 3
3.2
Groundwater Sampling Results....................................................................................................... 3
3.3
Ethylene Glycol................................................................................................................................ 3
3.3.1
1,4-Dioxane...................................................................................................................................... 4
3.3.2
DowTherm ATM................................................................................................................................. 4
3.4
Surface Water Sampling Results..................................................................................................... 4
3.5
Intermittent Seep Sampling Results................................................................................................. 5
3.6
Phytoremediation System and Landfill Cover Inspections............................................................... 5
4.
Conclusions..................................................................................................6
Tables
Table 1 May Groundwater and Surface Water Sampling Plan
Table 2 November Groundwater and Surface Water Sampling Plan
Table 3 Groundwater Elevations
Table 4 Groundwater Analytical Summary
Table 5 Surface Water Analytical Summary
Table 6 Intermittent Seep Water Analytical Summary
Table 7 Summary of Detected Constituents in Groundwater
Table 8 Time vs. Concentration Plots — Ethylene Glycol
Table 9 Time vs. Concentration Plots — 1,4-Dioxane
Table 10 Time vs. Concentration Plots — Diphenyl Ether
Figures
Figure 1
Site Location Map
Figure 2
Site Layout Map
Figure 3
Sample Location Map — May 2021
Figure 4
Sample Location Map — November 2021
Figure 5
Groundwater Elevation Data — November 2021
Figure 6
Ethylene Glycol Map — May 2021
Figure 7
Ethylene Glycol Map — November 2021
Figure 8
1,4-Dioxane Map — May 2021
Figure 9
1,4-Dioxane Map — November 2021
Figure 10
1,1-Biphenyl Map — November 2021
Figure 11
Diphenyl Ether Map — November 2021
AECOM

2021 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
Appendices
AECOM Project number: 60683034
Appendix A May 2021 and November 2021 Laboratory Analytical Reports
Appendix B Completed Inspection Forms for Landfill Cap and Phytoremediation System
Acronyms
CAP
Corrective Action Plan
IMAC
Interim Maximum Allowable Concentrations
mg/L
milligrams per liter
MNA
monitored natural attenuation
MSL
mean sea level
NC 2L
North Carolina Administrative Code, Title 15A, Subchapter 2L
NCDEQ
North Carolina Department of Environmental Quality
NPDES
National Pollutant Discharge Elimination System
NRLF
Needmore Road Landfill
VFA
Volatile Fatty Acid
AECOM

2021 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
1. Introduction
AECOM Project number: 60683034
This annual report has been prepared to present activities completed from January 2021 through
December 2021, and the sampling results for the May and November monitoring events for the
Needmore Road Landfill (NRLF) site. This report includes an updated summary of data and findings at
the site and presents the status of the monitored natural attenuation (MNA) and phytoremediation
programs established in the Corrective Action Plan (CAP).
1.1 Site Background
The NRLF site, located at 345 Messick Farm Road, Woodleaf, Rowan County, North Carolina, was used
until 1990 to dispose of by-products of polyester resin manufacturing from the former Hoechst Celanese
plant located on U.S. Route 70 near Salisbury, North Carolina. These by-products primarily included
waste materials containing ethylene glycol with some other impurities, including 1,4-dioxane, 1,1-
biphenyl, and diphenyl ether. There were four main disposal areas at this site, and they were referred to
as Taylor's Pit (0.6 acre), the 14-Acre Site, the 16-Acre Site, and the Secondary Site (2.6 acres). Taylor's
Pit was consolidated into the main part of the landfill prior to final landfill closure. The site consists of an
approximately 243-acre tract of land that is bounded by the South Yadkin River to the east. The current
North Carolina Department of Environmental Quality (NCDEQ) status of the site is "closed." A site
location map is included as Figure 1, and a site layout map is included as Figure 2.
The landfill lies within the central portion of the Charlotte Metamorphic Belt of the Piedmont Physiographic
Province. Bedrock in this area is composed of a complex series of meta -sedimentary, meta -volcanic, and
igneous intrusive rock types. This geologic matrix has undergone repeated cycles of folding, faulting,
metamorphism, and intrusions, which have resulted in regional northeasterly strike and southeasterly dip
directions.
A basic understanding of the geology at the landfill was established during several phases of work, during
which numerous monitoring and extraction wells were installed. Based on an evaluation of the
subsurface boring logs, the site is underlain by diorite, gabbro, and granite bedrock. Some localized
gneissic and schistose metamorphism was noted in several of the borings drilled at the site. These
profiles are generally well -weathered and occur in the zone above the competent rock.
Historic remedial activities at the landfill include the installation of an impermeable cover on the landfill,
regrading of the surface of the landfill (to improve surface water drainage), and the installation of
groundwater extraction wells. Groundwater was extracted and treated by a UV/peroxide oxidation
process and discharged under a National Pollutant Discharge Elimination System (NPDES) permit.
Groundwater extraction was suspended in June 2002 with NCDEQ approval. In 2004, modifications were
made to the drainage system and a phytoremediation system was initiated to address seepage at the toe
of the landfill. The phytoremediation system is positioned downgradient of the landfill face and upgradient
of the intermittent seep location.
Groundwater monitoring data in the reports submitted semiannually from November 2004 through 2007
demonstrated that the existing groundwater impact had been generally contained and was not expanding.
As such, a final CAP was established in 2007 defining a combination of MNA and phytoremediation as the
site remedy. Subsequent monitoring events have reported similarly successful results.
Biological degradation has been a significant component of natural attenuation of ethylene glycol and
DowTherm ATM components at the site. The original MNA parameters supplemented with the additional
sampling requested by NCDEQ indicate that biological degradation is occurring at the site to control the
AECOM
1

2021 Annual Report AECOM Project number: 60683034
Needmore Road Landfill
Salisbury, North Carolina
ethylene glycol and DowTherm ATM plume. Phytoremediation is currently being utilized to supplement the
MNA, treat the 1,4-dioxane plume through evapotranspiration, and to provide additional hydraulic control.
Groundwater monitoring, surface water monitoring, intermittent seep monitoring, and regular inspections
of the phytoremediation system and landfill cap have been ongoing at the site in accordance with the
schedule detailed in the CAP which was revised in early 2009. Based on the site understanding and
long-term data, the levels of impact in groundwater are not anticipated to exceed surface water quality
standards nor pose an unacceptable risk to the receptors. Based on these data, the reports support
continued MNA with phytoremediation as a viable remedy, as described in the CAP.
Because the primary constituents at the site have generally remained stable since 2007, and because the
MNA and phytoremediation systems have remained effective as designed, AECOM recommended in the
semiannual report submitted to NCDEQ in May 2014 that the monitoring continue to be conducted
semiannually in May and November and the reporting frequency be reduced from semiannual to annual.
The NCDEQ approved the reduction of the reporting frequency in a letter dated September 10, 2014, and
an annual site report has been prepared each year since May 2015.
2. Summary of Monitoring Activities
The ongoing MNA/phytoremediation activities for the NRLF site include:
• semiannual groundwater sampling and analysis;
• semiannual surface water sampling and analysis;
• semiannual sampling and analysis of intermittent seep at toe of landfill;
• continued ongoing maintenance and monthly inspection of the landfill cap; and
• continued ongoing maintenance and monthly inspections of the phytoremediation tree farm.
The May and November 2021 monitoring events were conducted using methodologies detailed in the
CAP. A reduced scope plan for the May events was approved in 2009 and is shown in Table 1. The
November events include the full sampling plan originally presented in the CAP, and the plan is shown in
Table 2. Prior to sampling, depths to groundwater were measured at the wells to be sampled. These
data are shown in Table 3 and are resolved to the groundwater elevations used to plot the site
potentiometric maps. The water levels in well B-22B had reached the top of well casing during the May
2021 sampling event, therefore, depth to water was not measured and groundwater elevation was not
calculated for this well.
The replacement of a Volatile Fatty Acids (VFAs) analysis with an acetic acid analysis was approved by
NCDEQ in 2010.
Sample location maps for the May and November monitoring events are included as Figure 3 and Figure
4, respectively. Laboratory analytical reports are included in Appendix A.
Completed monthly inspection forms for the phytoremediation system and landfill cap for January through
December 2021 are included in Appendix B.
AECOM
2

2021 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
AECOM Project number: 60683034
3. Summary of May 2021 and November
2021 Monitoring Results
Nine groundwater monitoring wells, one surface water location, and one intermittent seep location were
sampled during the May 2021 monitoring event. Fourteen groundwater monitoring wells and four surface
water locations were sampled during the November 2021 monitoring event. A sample was not collected
from the intermittent seep location CSW-2 in May 2021 and samples were not collected from intermittent
seep locations CSW-1 and CSW-2 in November 2021 due to the locations being dry during the monitoring
events. Laboratory analytical results are summarized in Table 4 (groundwater), Table 5 (surface water),
and Table 6 (intermittent seep). Complete analytical reports are included as Appendix A. Previous
reports identified that the primary constituents in groundwater are ethylene glycol, 1,4-dioxane,
1,1-biphenyl, and diphenyl ether. Monitoring updates for these constituents are presented in the following
sections.
3.1 Groundwater Sampling Results
During the May 2021 monitoring event, groundwater elevations ranged from approximately 655.70 feet
above mean sea level (MSL) at B-24A to approximately 707.75 feet above MSL at B-10. During the
November 2021 monitoring event, groundwater elevations ranged from approximately 657.09 feet above
MSL at B-12 to 716.25 feet above MSL at B-32B. The groundwater elevation data are presented in Table
3. The groundwater elevations in 2021 appear to be consistent with typical measurements from the
previous years.
The May 2021 and November 2021 groundwater elevation data are consistent with the groundwater flow
patterns established in the CAP (October 2007), which indicated that groundwater under the site
generally flows northeast toward the South Yadkin River. Groundwater elevations collected during the
November 2021 event were used to develop the potentiometric surface presented on Figure 5.
3.2 Groundwater Sampling Results
3.2.1 Ethylene Glycol
Historically, ethylene glycol remained below analytical reporting limits (non -detect) in samples collected
from 2007 to November 2012. Fluctuating concentrations of ethylene glycol have been detected at
several wells since May 2013, including B-01, B-09C, B-10, B-23A, and B-23B, and some detections
were above the North Carolina Administrative Code, Title 15A, Subchapter 2L (NC 2L) standard of 10
milligrams per liter (mg/L). During both the May 2021 monitoring event and November 2021 monitoring
event, ethylene glycol was not detected in any of the samples analyzed for ethylene glycol.
The low concentrations detected or non -detects results in the wells from 2007 to 2012 support the
ethylene glycol natural attenuation conclusions presented in the 2007 CAP. The landfill cap has
significantly reduced or eliminated the transport of ethylene glycol from the landfill into groundwater, and
the concentrations of ethylene glycol, which had entered the groundwater prior to the installation of the
cap, decreased or were attenuated (CAP, 2007). Since ethylene glycol is fully miscible in water and
mobile, ongoing occasional detections were anticipated in the 2007 CAP. Future fluctuations between
detections within historical ranges and non -detect results are expected as the remaining ethylene glycol
migrates and rapidly degrades. Detections do not suggest a deficiency in the landfill cover, and the
fluctuations back to non -detect continue to confirm MNA as an ongoing remedy. Ethylene glycol will
continue to be monitored.
Historic data summaries for ethylene glycol and other site parameters are presented in Table 7. Selected
trend plots of ethylene glycol concentrations over time are presented in Table 8. Ethylene glycol results
AECOM
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2021 Annual Report AECOM Project number: 60683034
Needmore Road Landfill
Salisbury, North Carolina
are shown on Figure 6 for the May 2021 monitoring event and Figure 7 for the November 2021 monitoring
event.
3.2.2 1,4-Dioxane
1,4-Dioxane has historically been detected in wells near the four former disposal sites. During the May
2021 and November 2021 monitoring events, 1,4-dioxane was detected at concentration higher than the
NC 2L standard of 0.003 mg/L in each sample analyzed for 1,4-dioxane. The highest 1,4-dioxane
concentrations were detected in well B-23A, at a concentration of 3.26 mg/L in May 2021 and 3.42 mg/L
in November 2021. The concentration trend plots presented in Table 9 indicate that 1,4-dioxane
concentrations in most wells are generally either stable or declining.
Data used to generate the plots in Table 9 can be found in Table 7. 1,4-Dioxane results are shown on
Figure 8 for the May 2021 monitoring event and Figure 9 for the November 2021 monitoring event.
3.2.3 DowTherm ATM
1,1-Biphenyl
1,1-Biphenyl results are presented in Table 4, and the 1,1-biphenyl results for the November 2021 event
are shown on Figure 10.
Since 2005, 1,1-biphenyl has been consistently detected only in samples collected from monitoring well
B-10. The result from B-10 was 0.127 mg/L in May 2021 and 0.11 mg/L in November 2021, similar to the
recent sampling results and below the NC 2L standard of 0.40 mg/L. Historic data for 1,1-biphenyl at B-
10 have typically remained below the 0.40 mg/L level but have occasionally exceeded this level. The
historic maximum 1,1-biphenyl detection of 0.461 mg/L was reported in 1999. 1,1-Biphenyl was not
detected in other wells analyzed for 1,1-biphenyl in 2021.
Diphenyl Ether
NCDEQ has not developed a 2L standard for diphenyl ether; therefore, the Interim Maximum Allowable
Concentration (IMAC) (0.10 mg/L, effective since April 2011) is used as the screening criteria for this
constituent at the site. Diphenyl ether has historically been detected at several wells located near the
former disposal sites and at the downgradient wells. Historically, diphenyl ether concentrations ranged
from approximately 1.1 to 4.5 mg/L, and concentrations detected in individual wells have demonstrated a
decreasing trend since December 2009. The May 2021 and November 2021 diphenyl ether data are
presented in Table 4. Diphenyl ether was detected in well B-10 in May 2021 and in wells B-01, B-09C, B-
10, B-22B, B-23A, B-23B, B-24A, and B-24B in November 2021. During the 2021 monitoring events,
concentrations detected ranged from 0.0091 mg/L in B-24A to 1.21 mg/L in B-10. The highest diphenyl
ether concentrations are consistently detected in B-10; however, the diphenyl ether concentrations
detected in B-10 demonstrate a decreasing trend since 2009. Diphenyl ether results for the November
2021 event are shown on Figure 11. Selected diphenyl ether trends are shown in Table 10.
The data continue to indicate that migration of 1,1-biphenyl and diphenyl ether is being controlled by the
landfill cap and through natural attenuation mechanisms.
3.3 Surface Water Sampling Results
Surface water monitoring was conducted at one location (SW-05) during the May 2021 monitoring event
and at four locations (SW-03, SW-05, SW-07, and SW-08) during the November 2021 event. The surface
water results are summarized in Table 5.
During both the May 2021 and November 2021 monitoring events, 1,4-dioxane, ethylene glycol, diphenyl
ether, or 1,1-biphenyl were not detected at any of the surface water monitoring locations.
AECOM
4

2021 Annual Report AECOM Project number: 60683034
Needmore Road Landfill
Salisbury, North Carolina
3.4 Intermittent Seep Sampling Results
CSW-1 and CSW-2 are monitoring locations associated with the intermittent seep, and both locations
have been dry for a substantial number of monitoring events since the phytoremediation program was
initiated. CSW-1 is located at the initial discharge point of the seep, and CSW-2 is located downstream in
the creek bed fed by the seep.
An intermittent seep sample was collected at one location (CSW-1) during the May 2021 monitoring
event, and 1,4-dioxane was detected at a concentration of 0.696 mg/L. Intermittent seep samples were
not collected at the two locations (CSW-1 and CSW-2) during the November 2021 monitoring event
because the locations were dry at the time of the monitoring event. The intermittent seep water results
are summarized in Table 6.
At CSW-1 and CSW-2, samples collected prior to construction of the phytoremediation system
concentrations of 1,4-dioxane were detected at CSW-1 at approximately 0.5 mg/L and lower
concentrations were detected at downgradient CSW-2. The 1,4-dioxane concentrations decreased after
the construction of the phytoremediation system and remained below 0.2 mg/L from 2012 through 2019,
indicating that the phytoremediation system continues to provide control of the 1,4-dioxane mass in the
treatment area. During the 2021 monitoring event, the 1,4-dioxane concentration in CSW-1 was higher
than in recent sampling results; however, the elevated 1,4-dioxane concentrations in the intermittent seep
may be temporary, and monitoring for 1,4-dioxane will continue in future monitoring events to evaluate the
concentration trends.
3.5 Phytoremediation System and Landfill Cover
Inspections
Monthly inspections of the phytoremediation system and landfill cap were conducted during the period of
January through December 2021 and are presented in Appendix B. Based on these inspections, the
cover remained in good condition and most of the trees remained in good health during this reporting
period.
The phytoremediation system was originally installed in 2004. A supplemental tree planting event was
conducted in 2012, including the removal of dead trees and planting of 30 new trees and 20 whips. After
the 2012 planting, some poplar trees were lost. The phytoremediation system status was evaluated in
2019, and another supplemental tree planting was conducted at the site in February and March 2020. A
total of 12 dead poplar trees were removed by mobile crane in February 2020. A total of 100 black willow
4-foot whips were planted in March 2020. The trees were planted in 6-inch diameter by 12-inch deep
holes, and the holes were backfilled with compost followed by fertilization. Five poplar trees appeared to
be dead in March 2021; all the new willow trees planted in 2020 are generally in good health through
2021.
The landfill cap has remained in good condition and permanent edge -of -waste markers were installed in
March 2021 per NCDEQ request.
The landfill cover has been in place since the early 1990s. The phytoremediation system was first
implemented in 2004 and has been upgraded and maintained consistently since that time. Groundwater
monitoring has consistently demonstrated that these systems remain effective and along with MNA
maintain stable to improving conditions.
Routine mowing and cover service will continue. Maintenance of the phytoremediation system will also
be continued. The maintenance will include periodic removal of trees based on damage, age, or
overcrowding, and additional trees will be installed as needed to continue meeting the objectives of the
CAP.
AECOM
5

2021 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
4. Conclusions
AECOM Project number: 60683034
The CAP was submitted in November 2007, and subsequent semiannual and annual reports describe
stable or declining concentrations and present the extent of the detections of primary constituents in
groundwater within the Needmore Road Landfill. This report describes the field activities from January to
December 2021 and the analytical results of the May 2021 and November 2021 monitoring events.
Semiannual monitoring and monthly inspections of the phytoremediation system were conducted during
this reporting period.
Ethylene glycol was not detected in any samples analyzed for ethylene glycol in 2021.
1,4-Dioxane was detected above the NC 2L standard, and concentrations remain stable or declining in
most wells.
1,1-Biphenyl has been consistently detected only at monitoring well B-10, and historical 1,1-biphenyl data
for B-10 indicate a decreasing trend since 2008. The highest diphenyl ether concentrations are
consistently detected in B-10; however, the diphenyl ether concentrations in the former disposal areas
have decreased or stabilized over time due to the natural attenuation processes.
The phytoremediation system and landfill cap remain in good condition. A total of 100 black willow 4-foot
whips were planted in March 2020 and remained generally in good health through 2021. Future
maintenance of the phytoremediation system, including pruning, removal, and/or installation of new trees,
will be continued as described in the CAP.
Semiannual monitoring of groundwater, surface water, and the intermittent seep will be continued in May
and November 2022 in accordance with the Sampling Plans presented in Tables 1 and 2, respectively. In
addition, monthly inspections of the phytoremediation system and landfill cap will be conducted during the
period of January through December 2022. The next annual report will be submitted in May 2023.
AECOM
6

2021 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
Tables
AECOM Project number: 60683034
AECOM

Table 1
May Groundwater and Surface Water Sampling Plan
CNA Holdings LLC — Needmore Road Landfill
AECOM Project No. 60683034
Location
1,4-Dioxane
DowTherm Alm
Ethylene
Glycol
VOCs*
MNA**
B-01
X
X
X
B-09C
X
X
X
B-10
X
X
X
X
B-12
X
X
X
B-17C
X
X
B-22B
X
X
B-23A
X
X
X
B-23B
X
X
X
B-24A
X
X
SW-5
X
X
X
CSW-1
X
CSW-2
X
Notes:
* VOCs to be analyzed annually (November only; revised from CAP schedule of May only)
** MNA: alkalinity, nitrate, phosphate, sulfate, DO, ORP, and ferrous iron
Page 1 of 1 5/10/2022

Table 2
November Groundwater and Surface Water Sampling Plan
CNA Holdings LLC — Needmore Road Landfill
AECOM Project No. 60683034
Location
1,4-Dioxane
DowTherm
A•M
Ethylene
Glycol
VOCs*
MNA**
Expanded
MNA***
B-01
X
X
X
X
X
X
B-09C
X
X
X
X
X
B-10
X
X
X
X
X
X
B-12
X
X
X
B-17B
X
X
X
X
B-17C
X
X
X
X
B-21 B
X
X
B-22A
X
X
X
X
X
B-22B
X
X
X
X
X
B-23A
X
X
X
X
X
X
B-23B
X
X
X
X
X
X
B-24A
X
X
X
X
B-24 B
X
X
X
X
B-32 B
X
X
X
X
X
CSW-1
X
CSW-2
X
SW-3
X
X
X
SW-5
X
X
X
SW-7
X
X
X
SW-8
I X
I X
I X
Notes:
* VOCs to be analyzed annually (November only; revised from CAP schedule of May only)
** MNA: alkalinity, nitrate, phosphate, sulfate, DO, ORP, and ferrous iron
*** Expanded MNA: TOC, ethane, ethene, methane, carbon dioxide, hydrogen, and volatile fatty acids
Page 1 of 1 5/10/2022

Table 3
Groundwater Elevations
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Well ID
Date
Gauged
Top of
Casing (TOC)
Depth to
Water
Groundwater
Elevation
MSL
Feet below
TOC
MSL
B-01
5/17/2021
756.55
56.45
700.10
11/30/2021
55.75
700.80
B-09C
5/17/2021
713.44
32.19
681.25
11/30/2021
36.30
677.14
B-10
5/17/2021
751.78
44.03
707.75
11/30/2021
44.98
706.80
B 12
5/17/2021
677.11
16.31
660.80
11 /29/2021
20.02
657.09
B-17B
11/30/2021
678.32
17.48
660.84
B-17C
5/17/2021
677.06
14.45
662.61
11 /29/2021
17.32
659.74
B-21 B
11/30/2021
676.73
11.40
665.33
B-22A
11/30/2021
661.66
4.04
657.62
B-22B
5/17/2021
660.15
NM
NC
11/30/2021
1.85
658.30
B-23A
5/17/2021
665.73
7.59
658.14
11 /29/2021
8.63
657.10
B-23B
5/17/2021
665.74
6.95
658.79
11 /29/2021
8.12
657.62
B-24A
5/17/2021
659.10
3.40
655.70
11 /29/2021
4.28
654.82
B-24B
11/29/2021
659.19
3.35
655.84
B-32B
11/30/2021
745.68
29.43
716.25
Notes:
MSL - mean sea level
NC -not calculated
NM - not measured
TOC - top of casing
Page 1 of 1 5/10/2022

Table 4
Groundwater Analytical Summary
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Location
B-01
5/17/2021
B-01-051721
B-01
11/30/2021
B-01-113021
B-09C
5/17/2021
B-09C-051721
B-09C
11/30/2021
B-09C-113021
B-09C
11/30/2021
B-99C-113021
B-10
5/11/2021
B-10-051721
B-10
511I12021
B-99-051721
B-10
11/30/2021
B-10-113021
Collection Date
Sample Name
Chemical Units NC 2L Standard
Organic: Compounds
1,1'-Biphenyl
mg/L
0.4
<0.0091
<0.0091
<O.0083
0.127
0.119
0.11
Diphenyl ether
mg/L
0.1 (IMAC)
0.0309
0.0212
0.0189
1.21
1.17
Ethylene Glycol
mg/L
10
<5.0
<5.0
<5.0
<25.0
<5.0
<5.0
<5.0
1,4-Dioxane
Acetone
mg/L
mg/L
0.003
6
1.61
1.65
0.703
0.852
0.909
3.46
0.956
3.52
0.193
0.181
<0.0250
2-Butanone
mg/L
4
0.33
0.548
0.583
<0.0050
Chlorobenzene
mg/L
0.05
<0.0025
<0.0125
<0.0100
<0.0010
Chloroethane
mg/L
3
0.0165
<0.0125
<0.0100
0.0356
1,1-Dichloroethane
mg/L
0.006
0.0102
<0.0125
<0.0100
0.0396
1,1-Dichloroethene
mg/L
0.35
<0.0025
<0.0125
<0.0100
<0.0010
4-Methyl-2-Pentanone
mg/L
0.0222
<0.0625
0.0958
<0.0050
1,4-Dichlorobenzene
mg/L
<0.0025
<0.0125
<0.0100
0.0039
cis-1,2-Dichloroethene
mg/L
<0.0025
0.0148
0.0143
<0.0010
Toluene
mg/L
<0.0025
<0.0125
<0.0100
0.0020
Vinyl chloride
mg/L
<0.0025
<0.0125
<0.0100
0.0021
MNA Parameters
Alkalinity
mg/L
1590
1300
2860
2500
475
420
Nitrate -as -nitrogen
mg/L
10
<0.040
<0.040
<0.040
<0.040
0.046
0.061
<0.040
Nitrite -as -nitrogen
mg/L
1
0.18
0.35
0.26
0.12
0.062
0.058
0.22
orthophosphate phosphorus
mg/L
1.3
0.83
0.27
0.74
0.34
0.39
0.22
Sulfate
mg/L
250
7.1
5.5
1.4
1.4
<1.0
<1.0
<1.0
Total organic carbon 1
mg/L
--
--
898
--
--
--
--
--
17.6
Total organic carbon 2
mg/L
--
--
916
--
--
--
--
--
18.2
Total organic carbon 3
mg/L
--
--
932
--
--
--
--
--
18.0
Total organic carbon 4
mg/L
--
--
919
--
--
--
--
--
18.1
Total organic carbon average
mg/L
--
--
916
--
--
--
--
--
18.0
Acetic Acid
mg/L
--
--
580
--
--
--
--
--
4.7
Methane
mg/L
--
--
15
--
--
--
--
--
17
Ethane
mg/L
--
--
<0.0010
--
--
--
--
--
<0.0010
Ethene
mg/L
<0.0010
<0.0010
Carbon dioxide
mg/L
--
--
399
--
--
--
--
--
264
Hydrogen
nM
--
--
--
--
--
--
--
--
--
Field Parameters
Dissolved Oxygen
mq/L
0.04
0.04
0.29
0.08
0.28
0.11
Iron, Ferrous
mq/L
5.6
3.8
6.4
4.2
3.2
2.6
ORP
mV
-108.3
-108.9
-111.4
-81.9
43.4
-57.3
pH
SU
5.67
6.31
6.09
6.41
5.40
6.21
Specific Conductance
umhos/cm
3066.0
2975.0
3133.0
4486.0
857.0
845.0
Temperature
degrees C
22.00
16.00
20.20
14.20
17.20
16.70
Turbidity
NTU
20.4
23.4
8.2
7.0
3.6
6.9
Notes:
IMAC- Interim Maximum Allowable Concentration
' site -specific target chemical
-- no standard specified under 15A NCAC 2L.0202
mg/L - milligrams per liter
mV - millivolts
SU - standard units
umhos/cm - micromhos per centimeter
degrees C - degrees Celsius
NTU - Nephelometric Turbidity Units
NA - Not Analyzed
Bold-Analyte detected by the laboratory
Bold and shaded - Concentration exceeds the NC 2L limit
J-: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample biased low.
Page 1 of 3 5/10/2022

Table 4
Groundwater Analytical Summary
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Location
B-12
5/17/2021
B-12-051721
B-12
11/29/2021
B-12-112921
B-17B
11/30/2021
B-17B-113021
B-17C
5/17/2021
B.17C-051721
B-17C
11/29/2021
B-17C-112921
B-21B
11/30/2021
B-216-113021
B-22A
11/30/2021
B-22A-113021
B-22B
5/17/2021
B-22B-051721
B-226
11/30/2021
B-221-113021
Collection Date
Sample Name
Chemical I Units I NC 2L Standard
Organic Compounds
1,1'-Biphenyl
mg/L
0.4
<0.0100
<0.0091
<0.0100
<0.0100
<0.0083
<0.0083
Diphenyl ether
mg/L
0.1 (IMAC)
<0.0100
<0.0091
<0.0100
<0.0100
<0.0083
0.0484
Ethylene Glycol
mg/L
10
--
--
--
--
--
--
--
--
--
1,4-Dioxane
Acetone
mg/L
mg/L
0.003
6
--
2.35
--
0.138
--
1.18
--
1.37
--
--
<0.0250
1.33
--
1.06
<0.0250
2-Butanone
mg/L
4
<0.0050
<0.0050
Chlorobenzene
mg/L
0.05
--
--
--
--
--
--
0.0049
--
0.0112
Chloroethane
mg/L
3
<0.0010
0.0189
1,1-Dichloroethane
mg/L
0.006
--
--
--
--
--
--
0.0037
--
<0.0010
1,1-Dichloroethene
mg/L
0.35
--
--
--
--
--
--
0.0024
--
<0.0010
4-Methyl-2-Pentanone
mg/L
--
--
--
--
--
--
--
<0.0050
--
<0.0050
1,4-Dichlorobenzene
mg/L
<0.0010
<0.0010
cis-1,2-Dichloroethene
mg/L
--
--
--
--
--
--
--
<0.0010
--
<0.0010
Toluene
mg/L
<0.0010
<0.0010
Vinyl chloride
mg/L
--
--
--
--
--
<0.0010
--
<0.0010
MNA Parameters
Alkalinity
mg/L
401
360
220
390
<5.0
250
470
797
920
Nitrate -as -nitrogen
mg/L
10
<0.040
<0.040
<0.040
<0.040
<0.040
<0.040
<0.040
<0.040
<0.040
Nitrite -as -nitrogen
mg/L
1
<0.040
<0.040
<0.040
<0.040
<0.040
<0.040
0.087
<0.040
0.041
orthophosphate phosphorus
mg/L
0.22
0.13
0.27
0.26
0.16
0.19
<0.050
0.22
0.33
Sulfate
mg/L
250
1.4
1.3
2.4
1.4
1.3
16.7
<1.0
<1.0
<1.0
Total organic carbon 1
mg/L
--
--
--
3.0
--
2.9
--
4.5
--
6.9
Total organic carbon 2
mg/L
--
--
--
2.3
--
3.0
--
4.3
--
6.8
Total organic carbon 3
mg/L
--
--
--
2.2
--
3.0
--
4.2
--
6.7
Total organic carbon 4
mg/L
--
--
--
2.2
--
3.0
--
4.1
--
6.6
Total organic carbon average
mg/L
--
--
--
2.4
--
3.0
--
4.3
--
6.8
Acetic Acid
mg/L
--
--
--
<0.50
--
1.9
--
<0.50
--
0.67
Methane
mg/L
--
--
--
0.045
--
0.072
--
0.052
--
25
Ethane
mg/L
--
--
--
<0.0010
--
<0.0010
--
0.0025
--
0.0022
Ethane
mg/L
<0.0010
<0.0010
<0.0010
<0.0010
Carbon dioxide
mg/L
--
--
--
163
--
129
--
265
--
299
Hydrogen
nM
--
--
--
7.7
--
<1.9
--
1.9
--
<1.9
Field Parameters
Dissolved Oxygen
mq/L
1.17
1.71
0.15
1.99
1.10
1.47
0.18
0.06
0.10
Iron, Ferrous
mq/L
0.0
0.0
1.6
0.0
1.0
0.4
4.0
3.6
3.5
ORP
mV
61.4
110.9
-33.8
52.6
60.2
36.8
-94.1
-81.0
-102.2
pH
SU
6.43
6.62
6.20
6.51
6.73
6.70
6.52
5.73
6.72
Specific Conductance
umhos/cm
691.0
637.0
423.9
702.0
671.0
481.0
968.0
1215.0
1035.0
Temperature
deqrees C
16.60
9.80
12.10
15.80
13.90
15.20
9.60
15.70
11.90
Turbidity
NTU
1.6
4.4
6.9
2.2
5.8
2.5
4.3
6.0
4.3
Notes:
IMAC- Interim Maximum Allowable Concentration
' site -specific target chemical
-- no standard specified under 15A NCAC 2L.0202
mg/L - milligrams per liter
mV - millivolts
SU - standard units
umhos/cm - micromhos per centimeter
degrees C - degrees Celsius
NTU - Nephelometric Turbidity Units
NA - Not Analyzed
Bold-Analyte detected by the laboratory
Bold and shaded - Concentration exceeds the NC 2L limit
J-: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample biased low.
Page 2 of 3 5/10/2022

Table 4
Groundwater Analytical Summary
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Location
B-23A
5/17/2021
B-23A-051721
B-23A
11/29/2021
B-23A-112921
B-23B
5/17/2021
B-2313-051721
B-23B
11/29/2021
B-2313-112921
B-24A
5/17/2021
B-24A-051721
B-24A
11/29/2021
B-24A-112921
B-24B
11/29/2021
B-246-112921
B32B
11/30/2021
B-32B-113021
Collection Date
Sample Name
Chemical Units I NC 2L Standard
Organic Compounds
1,1'-Biphenyl
mg/L
0.4
<0.0091
<0.0091
<0.0083
<0.0083
<0.0100
Diphenyl ether
mg/L
0.1(IMAC)
0.0479
0.0448
0.0091
0.0120
<0.0100
Ethylene Glycol
mg/L
10
<5.0
<25.0
<5.0
<25.0
<5.0
1,4-Dioxane
Acetone
mg/L
mg/L
0.003
6
3.42
5.86
2.69
3.00
3.56
0.226
<0.0250
<0.0250
2-Butanone
mg/L
4
0.836
0.504
<0.0050
<0.0050
Chlorobenzene
mg/L
0.05
<0.0250
<0.0100
<0.0010
<0.0010
Chloroethane
mg/L
3
<0.0250
0.0223
1 0.0039
0.0051
1,1-Dichloroethane
mg/L
0.006
0.0371
<0.0100
0.0074
<0.0010
1,1-Dichloroethene
mg/L
0.35
<0.0250
<0.0100
<0.0010
<0.0010
4-Methyl-2-Pentanone
mg/L
<0.125
<0.0500
<0.0050
<0.0050
1,4-Dichlorobenzene
mg/L
<0.0250
<0.0100
<0.0010
<0.0010
cis-1,2-Dichloroethene
mg/L
<0.0250
<0.0100
<0.0010
<0.0010
Toluene
mg/L
<0.0250
<0.0100
<0.0010
<0.0010
Vinyl chloride
mg/L
<0.0250
<0.0100
0.0016
0.0011
MNA Parameters
Alkalinity
mg/L
3390
3000
2060
2100
505
460
380
160
Nitrate -as -nitrogen
mg/L
10
0.041
<0.040
<0.040
<0.040
0.041
<0.040
<0.040
0.069
Nitrite -as -nitrogen
mg/L
1
<0.040
<0.040
0.12
0.11
<0.040
<0.040
<0.040
<0.040
orthophosphate phosphorus
mg/L
0.77
0.63
0.42
0.50
<0.062
0.36 J-
0.22 J-
<0.050
Sulfate
mg/L
250
4.8
5.9
3.8
5.4
<1.0
<1.0
<1.0
<1.0
Total organic carbon 1
mg/L
--
--
2710
--
1590
--
--
--
1.8
Total organic carbon 2
mg/L
--
--
2720
--
1640
--
--
--
1.4
Total organic carbon 3
mg/L
--
--
2730
--
1680
--
--
--
1.4
Total organic carbon 4
mg/L
--
--
2690
--
1630
--
--
--
1.3
Total organic carbon average
mg/L
--
--
2710
--
1640
--
--
--
1.5
Acetic Acid
mg/L
--
--
1400
--
980
--
--
--
<0.50
Methane
mg/L
--
--
4.1
--
7.5
--
--
--
2.4
Ethane
mg/L
--
--
<0.0010
--
<0.0010
--
--
--
<0.0010
Ethane
mg/L
<0.0010
<0.0010
<0.0010
Carbon dioxide
mg/L
--
--
463
--
568
--
--
--
54.4
Hydrogen
nM
--
--
2.5
--
2.9
--
--
--
--
Field Parameters
Dissolved Oxygen
mq/L
1.00
0.21
0.85
0.04
0.08
0.15
Iron, Ferrous
mq/L
3.2
3.0
3.2
4.2
2.8
3.0
ORP
mV
-103.0
-4.4
-66.1
-48.4
-104.8
-21.2
pH
SU
6.22
6.14
6.29
6.23
5.63
6.41
Specific Conductance
umhos/cm
5464.0
5286.0
438.0
4142.0
747.0
264.1
Temperature
decrees C
15.80
12.40
15.10
13.90
14.40
15.60
Turbidity
NTU
4.1
4.5
9.0
6.9
6.9
6.4
Notes:
IMAC - Interim Maximum Allowable Concentration
site -specific target chemical
-- no standard specified under 15A NCAC 2L.0202
mg/L - milligrams per liter
mV - millivolts
SU - standard units
umhos/cm - micromhos per centimeter
degrees C - degrees Celsius
NTU - Nephelomelric Turbidity Units
NA- Not Analyzed
Bold - Analyte detected by the laboratory
Bold and shaded - Concentration exceeds the NC 2L limit
J-: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample biased low.
Page 3 of 3 5/10/2022

Table 5
Surface Water Analytical Summary
CNA Holdings LLC — Needmore Road Landfill
AECOM Project No. 60683034
Location ID
SW-03
11/29/2021
SW-3-112921
SW-05
5/17/2021
SW-5-051721
SW-05
11/29/2021
SW-5-112921
SW-07
11/29/2021
SW-7-112921
SW-08
11/29/2021
SW-8-112921
Collection Date
Sample Name
Chemical Units
'Organic Compounds
1,1'-Biphenyl
mq/L
<0.0091
<0.0100
<0.0100
<0.0091
<0.0083
Di hen I ether
m /L
<0.0091
<0.0100
<0.0100
<0.0091
<0.0083
Ethylene Glycol
mq/L
<5.0
<5.0
<5.0
<5.0
<5.0
1,4-Dioxane
m /L
<0.0020
<0.0020
<0.0020
<0.0020
<0.0020
Field Parameters
Dissolved Oxygen
m /L
6.26
ORP
my
72.0
H
SU
6.98
Specific Conductance
umhos/cm
124.0
Temperature
degrees C
16.20
Turbidity
NTU
18.9
Notes:
mg/L — milligrams per liter
my — millivolts
SU — standard units
umhos/cm — micromhos per centimeter
degrees C — degrees Celsius
NTU — Nephelometric Turbidity Units
Page 1 of 1 5/10/2022

Table 6
Intermittent Seep Water Analytical Summary
CNA Holdings LLC — Needmore Road Landfill
AECOM Project No. 60683034
Location ID
CSW-1
5/17/2021
CSW-1-051721
Collection Date
Sample Name
Chemical
Units
Organic Com ounds
1,4-Dioxane
mg/L
0.696
Field Parameters
Dissolved Oxygen
m /L
5.41
ORP
mV
33.7
pH
SU
7.14
Specific Conductance
umhos/cm
412.6
Temperature
degrees C
14.40
Turbidity
NTU
10.8
Notes:
mg/L — milligrams per liter
mV — millivolts
SU — standard units
Page 1 of 1 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-01
Jun-04
<0.05
4.07
<28
0.0723
Nov-04
<0.01
0.202
492
0.0211
May-05
<2.5
2.93
1160
<2.5
Nov-05
<0.01
3.69
<70
0.02
May-06
<0.02
2.75
93.9
0.0419
Nov-06
<0.01
4.68
2000
0.0446
May-07
<0.01
3.43
<140
0.0716
Nov-07
<0.04
3.01
<7
0.0662
May-08
<0.04
2.15
<7
0.0635
Nov-08
<0.01
3.31
<7
0.0565
May-09
NA
2.26
<7
NA
Dec-09
<0.01
3.54
<35
0.0423
May-10
NA
3.56
<35
NA
Nov-10
<0.01
3.24
<35
0.0811
May-11
NA
2.15
NA
NA
Nov-11
<0.01
3.25
<35
0.083
May-12
NA
3.85
NA
NA
Nov-12
<1
3.41
<14
<1
May-13
NA
3.07
254
NA
Nov-13
<0.1
2.74
38.5
<0.1
May-14
NA
1.96
796
NA
Nov-14
<0.01
3.27
648
0.0858
May-15
NA
2.89
<5.0
NA
Nov-15
<0.01
2.64
<50
0.122
May-16
NA
2.37
<50
NA
Nov-16
<0.1
2.18
751
<0.1
May-17
NA
0.242
266
NA
Nov-17
0.0101
1.86
198
0.132
May-18
NA
1.93
<10.0
NA
Nov-18
<0.0100
2.13
51.9
0.0223
May-19
NA
1.81
<5.0
NA
Nov-19
<0.0100
1.55
<50.0
0
May-20
N/A
1.51
<5.0
N/A
Nov-20
<0.0100
1.51
1 <5.0
1 0.0300
May-21
N/A
1.61
<5.0
N/A
Nov-21
<0.0091
1.65
<5.0
0.0309
Page 1 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-09C
Jun-04
<0.5
0.791
<70
<0.5
Nov-04
<0.05
1.04
1420
0.0545
May-05
<0.2
0.776
<70
<0.2
Nov-05
<0.01
1.31
363
0.0324
May-06
<0.02
0.668
85.8
0.0492
Nov-06
<0.01
1.29
2020
<0.01
May-07
<0.01
1.11
<140
0.0377
Nov-07
<0.01
0.995
<7
0.0352
May-08
<0.01
0.486
<7
0.0312
Nov-08
<0.01
1.11
<7
0.0438
May-09
NA
0.873
<7
NA
Dec-09
<0.01
1.15
<35
0.0581
May-10
NA
1.03
<35
NA
Nov-10
<0.01
0.951
<35
0.0542
May-11
NA
0.782
NA
NA
Nov-11
<0.01
1.1
<35
0.0451
May-12
NA
1.46
NA
NA
Nov-12
<0.01
1.15
<14
0.0255
May-13
NA
0.803
448
NA
Nov-13
<0.01
0.766
77
0.0272
May-14
NA
0.86
288
NA
Nov-14
<0.01
0.893
406
0.029
May-15
NA
0.972
<5.0
NA
Nov-15
<0.01
0.909
<500
0.0106
May-16
NA
0.954
<50
NA
Nov-16
<0.01
0.796
330
0.0157
May-17
NA
0.56
192
NA
Nov-17
<0.0100
0.906
122
0.0269
Nov-17
<0.0100
0.81
NA
0.026
May-18
NA
0.689
<10.0
NA
Nov-18
<0.0100
0.935
197
<0.0100
Nov-18
<0.0100
0.964
NA
<0.0100
May-19
NA
0.85
<5.0
NA
Nov-19
<0.0100
0.886
<50.0
0
Nov-19
<0.0100
0.848
NA
0
May-20
NA
0.756
<5.0
NA
Nov-20
<0.0100
0.743
<5.0
0.0255
Nov-20
<0.0100
1 0.686
1 NA
0.0244
5/17/2021
11 /30/2021
N/A
0.852
<5.0
N/A
<0.0091
0.909
<25.0
0.0212
Page 2 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-10
Jun-04
<1
0.723
<28
4.63
Nov-04
<0.4
0.592
354
3.33
May-05
0.02
0.419
647
0.193
Nov-05
0.31
0.62
57.5
3.62
May-06
0.29
0.328
<7
3.01
Nov-06
0.28
0.509
284
3.12
May-07
0.28
0.564
<28
3.26
Nov-07
0.31
0.413
<7
3.46
May-08
0.405
0.461
<7
3.22
Nov-08
0.352
0.481
<7
3.12
May-09
0.319
0.412
<7
3.09
Dec-09
0.391
0.649
<14
4.58
May-10
0.288
0.417
<14
2.91
Nov-10
0.25
0.39
<14
2.55
May-11
0.328
0.553
NA
3.34
Nov-11
0.3
0.306
<14
2.53
May-12
0.157
0.484
NA
1.45
Nov-12
0.165
0.546
<14
1.82
May-13
0.106
0.421
252
1.12
Nov-13
0.157
0.47
<35
1.69
May-14
0.0728
0.599
<10
0.73
Nov-14
0.169
0.508
<10
1.84
May-15
0.0828
0.511
<5.0
1.09
Nov-15
0.192
0.404
<50
2.11
May-16
0.0888
0.42
<50
1.16
Nov-16
0.104
0.33
403
1.08
May-17
0.137 J
0.275
<5
1.4 J
May-17
0.070 J
0.257
<5
0.735 J
Nov-17
0.231 J
0.327
<5.0
1.44
May-18
0.146
0.243
<10.0
1.46
May-18
0.178 J
0.261
<10.0
1.57
Nov-18
0.0321
0.267
41.3
0.31
May-19
0
0.328
<5.0
1
May-19
0
0.312
<5.0
1
Nov-19
0
0.222
<50.0
1
May-20
0.0711 J
0.219
<5.0
0.643 J
May-20
0.113 J
0.179
<5.0
1.01 J
Nov-20
0.0694
1 0.197
1 <5.0
1 0.698
May-21
0.127
0.193
<5.0
1.21
Nov-21
0.11
0.18
<5.0
1.14
Page 3 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-12
Feb-04
<0.01
0.315
<7
<0.01
May-04
<0.01
0.521
<7
<0.01
Jun-04
<0.01
0.775
<7
0.0102
Nov-04
<0.01
0.942
<7
0.0115
May-05
<0.01
0.222
<7
0.0108
Nov-05
<0.01
0.165
<7
<0.01
May-06
<0.01
0.151
NA
<0.01
Nov-06
<0.01
0.216
NA
<0.01
May-07
<0.01
0.118
NA
<0.01
Nov-07
<0.01
0.169
NA
<0.01
May-08
<0.01
0.121
<7
<0.01
Nov-08
<0.01
0.102
NA
<0.01
May-09
<0.01
0.105
NA
0.0108
Dec-09
<0.01
0.128
NA
0.0119
May-10
<0.01
0.11
NA
<0.01
Nov-10
<0.01
0.0946
NA
<0.01
May-11
<0.01
0.11
NA
<0.01
Nov-11
<0.01
0.0761
NA
<0.01
May-12
<0.01
0.13
NA
<0.01
May-12
<0.01
0.132
NA
<0.01
Nov-12
<0.01
3.68
NA
<0.01
May-13
<0.01
3.44
NA
<0.01
Nov-13
<0.01
3.24
NA
<0.01
May-14
<0.01
2.59
NA
<0.01
Nov-14
<0.01
3.27
NA
<0.01
May-15
<0.01
3.09
NA
<0.01
Nov-15
<0.01
2.9
NA
<0.01
May-16
<0.01
2.81
NA
<0.01
Nov-16
<0.01
2.91
NA
<0.01
May-17
<0.01
2.71
NA
<0.01
Nov-17
<0.0100
2.76
NA
<0.0100
May-18
<0.0100 UJ
2.89
NA
<0.0100 UJ
Nov-18
<0.0100
3.09
NA
<0.0100
May-19
<0.0100
2.5
NA
<0.0100
Nov-19
<0.0100
2.3
NA
<0.0100
May-20
<0.0100
2.13
NA
<0.0100
Nov-20
<0.0100
2.4
NA
<0.0100
May-21
I <0.0100
1 1.84
1 N/A
<0.0100
Nov-21
1 <0.0091
1 2.35
1 N/A
<0.0091
Page 4 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-17B
Feb-04
<0.01
2.98
<7
<0.01
May-04
<0.01
2.33
<7
0.0125
Jun-04
<0.01
4.96
<7
<0.01
Nov-04
<0.01
3.11
<7
<0.01
May-05
<0.01
2.83
<7
0.0102
Nov-05
<0.01
1.87
<7
0.0107
May-06
<0.01
2.42
NA
<0.01
Nov-06
<0.01
2.84
NA
<0.01
May-07
<0.01
2.62
NA
<0.01
Nov-07
<0.01
3.33
NA
<0.01
May-08
<0.01
3.52
<7
<0.01
Nov-08
<0.01
2.35
NA
<0.01
Dec-09
<0.01
2.54
NA
<0.01
Nov-10
<0.01
2.75
NA
<0.01
Nov-11
<0.01
2.59
NA
<0.01
Nov-12
<0.01
0.291
NA
<0.01
Nov-13
<0.01
0.113
NA
<0.01
Nov-14
<0.01
0.271
NA
<0.01
Nov-15
<0.01
0.135
NA
<0.01
Nov-16
<0.01
1.93
NA
<0.01
Nov-17
<0.0100
0.128
NA
<0.0100
Nov-18
<0.0100
0.0722
NA
<0.0100
Nov-19
<0.0100
0.259
NA
<0.0100
Nov-20
<0.0100
0.0786
NA
<0.0100
Nov-21
<0.0100
0.138
N/A
<0.0100
Page 5 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-17C
Feb-04
<0.01
3.29
<7
<0.01
May-04
<0.01
2.21
<7
<0.01
Jun-04
<0.01
3.01
<7
<0.01
Nov-04
<0.01
3.22
<7
0.0117
May-05
<0.01
2.51
<8.5
<0.01
Nov-05
<0.01
2.44
<7
<0.01
May-06
<0.01
2.68
NA
<0.01
Nov-06
<0.01
2.92
NA
<0.01
May-07
<0.01
2.93
NA
<0.01
Nov-07
<0.01
3.06
NA
<0.01
May-08
<0.01
2.90
<7
<0.01
Nov-08
<0.01
2.10
NA
<0.01
Dec-09
<0.01
2.40
NA
<0.01
May-10
NA
1.95
NA
NA
Nov-10
<0.01
2.39
NA
<0.01
May-11
NA
2.02
NA
NA
Nov-11
<0.01
2.15
NA
<0.01
May-12
NA
2.47
NA
NA
Nov-12
<0.01
3.18
NA
<0.01
May-13
NA
3.61
NA
NA
Nov-13
<0.01
3.1
NA
<0.01
May-14
NA
3.71
NA
NA
Nov-14
<0.01
2.42
NA
<0.01
May-15
NA
2.9
NA
NA
Nov-15
<0.01
1.81
NA
<0.01
May-16
<0.01
0.177
NA
<0.01
Nov-16
<0.01
0.177
NA
<0.01
May-17
NA
2.51
NA
NA
Nov-17
<0.0100
1.68
NA
<0.0100
May-18
NA
2.09
NA
NA
Nov-18
<0.0100
1.97
NA
<0.0100
May-19
NA
1.97
NA
NA
Nov-19
<0.0100
1.51
NA
<0.0100
May-20
NA
1.32
NA
NA
Nov-20
<0.0100
1.64
NA
<0.0100
May-21
N/A
1.18
N/A
N/A
Nov-21
<0.0100
1.37
N/A
<0.0100
Page 6 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC — Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-21 B
Jun-04
<0.01
0.0391
<7
<0.01
Nov-04
<0.01
0.047
<7
<0.01
May-05
<0.01
0.0338
<7
<0.01
Nov-05
<0.01
0.0477
<7
<0.01
May-06
NA
0.0348
NA
NA
Nov-06
NA
0.0507
NA
NA
May-07
NA
0.0511
NA
NA
Nov-07
NA
0.0686
NA
NA
May-08
NA
0.0557
<7
NA
Nov-08
NA
0.0598
NA
NA
Dec-09
NA
0.0698
NA
NA
Nov-10
NA
0.0534
NA
NA
Nov-11
NA
0.0573
NA
NA
Nov-12
NA
0.0811
NA
NA
Nov-13
NA
0.0665
NA
NA
Nov-14
NA
0.0832
NA
NA
Nov-15
NA
0.092
NA
NA
Nov-16
NA
0.0685
NA
NA
Nov-17
NA
0.071
NA
NA
Nov-18
NA
0.0703
NA
NA
Nov-19
NA
0
NA
NA
Nov-20
NA
0.0357
NA
NA
Nov-21
N/A
0.0372
N/A
N/A
Page 7 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-22A
Feb-04
<0.01
0.67
<7
0.0634
May-04
<0.01
0.322
<7
0.0514
Jun-04
<0.01
1.06
<7
0.0449
Nov-04
<0.01
0.895
<7
0.0427
May-05
<0.01
0.722
<7.9
0.0284
Nov-05
<0.01
0.572
<7
0.0268
May-06
<0.01
0.949
NA
0.025
Nov-06
<0.01
1.12
NA
0.0259
May-07
<0.01
1.13
NA
0.0186
Nov-07
<0.01
1.3
NA
0.0213
May-08
<0.01
1.18
<7
0.0242
Nov-08
<0.01
1.04
NA
0.0214
Dec-09
<0.01
1.25
NA
0.0141
Nov-10
<0.01
1.74
NA
<0.01
Nov-11
<0.01
1.22
NA
<0.01
Nov-12
<0.01
2.05
NA
<0.01
Nov-13
<0.01
1.71
NA
<0.01
Nov-14
<0.01
1.64
NA
<0.01
Nov-15
<0.01
1.69
NA
<0.01
Nov-16
<0.01
1.48
NA
<0.01
Nov-17
<0.0100
1.35
NA
<0.0100
Nov-18
<0.0100
0.767
NA
<0.0100
Nov-19
<0.0100
1.44
NA
<0.0100
Nov-20
<0.0100
1.27
NA
<0.0100
Nov-21
<0.0083
1.2
N/A
<0.0083
Page 8 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-22B
Feb-04
<0.01
2.64
<7
0.0323
May-04
<0.01
1.9
<7
0.0346
Jun-04
<0.01
2.78
<7
0.033
Nov-04
<0.01
2.72
<7
0.0362
May-05
<0.01
2.32
<10.8
0.0351
Nov-05
<0.01
1.22
<7
0.0365
May-06
<0.01
2.46
NA
0.0329
Nov-06
<0.01
2.33
NA
0.028
May-07
<0.01
2.79
NA
0.0284
Nov-07
<0.01
2.62
NA
0.0295
May-08
<0.01
2.42
<7
0.023
Nov-08
<0.01
1.87
NA
0.0236
May-09
NA
2.39
NA
NA
Dec-09
<0.01
2.14
NA
0.0265
May-10
NA
2.01
NA
NA
Nov-10
<0.01
2.14
NA
0.0316
May-11
NA
1.75
NA
NA
Nov-11
<0.01
1.5
NA
0.0251
May-12
NA
1.95
NA
NA
Nov-12
<0.01
2.08
NA
0.0243
Nov-12
<0.01
2.2
NA
0.0227
May-13
NA
1.88
NA
NA
Nov-13
<0.01
1.69
NA
0.0222
May-14
NA
2.05
NA
NA
Nov-14
<0.01
2.8
NA
0.0202
May-15
NA
1.73
NA
NA
Nov-15
<0.01
1.72
NA
0.0117
May-16
<0.01
1.39
NA
0.0119
Nov-16
NA
1.62
NA
NA
May-17
NA
1.87
NA
NA
Nov-17
<0.0100
1.62
NA
0.0367
May-18
NA
1.63
NA
NA
Nov-18
<0.0100
1.51
NA
0.0163
May-19
NA
1.71
NA
NA
Nov-19
<0.0100
1.41
NA
0
Nov-20
NA
1.33
NA
NA
May-20
<0.0100
1.35
NA
0.0312
May-21
I N/A
1.33
N/A
N/A
Nov-21
1 <0.0083
1.06
N/A
0.0484
Page 9 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-23A
Feb-04
<0.01
1.5
<7
0.115
May-04
<0.01
1.21
<7
0.0928
Jun-04
<0.01
2.03
<7
0.0911
Nov-04
<0.01
1.45
227
0.0769
May-05
<0.01
1.41
278
0.0108
Nov-05
<0.01
1.29
<70
0.0919
May-06
<0.01
0.711
286
0.0823
Nov-06
<0.01
2.01
255
0.0791
May-07
<0.01
1.51
<70
0.0768
Nov-07
<0.01
1.45
<7
0.112
May-08
<0.01
1.91
NA
0.0936
Nov-08
<0.01
1.97
<7
0.0711
May-09
NA
1.34
<7
NA
Dec-09
<0.01
1.84
<7
0.131
May-10
NA
1.96
<7
NA
Nov-10
<0.01
1.81
<7
0.1
May-11
NA
1.3
NA
NA
Nov-11
<0.01
2.41
<7
0.0884
May-12
NA
2.45
NA
NA
Nov-12
<0.01
3.35
<7
0.0772
May-13
NA
2.82
120
NA
Nov-13
<0.01
2.76
146
0.0755
May-14
NA
3.06
<100
NA
Nov-14
<0.01
3.54
329
0.0708
May-15
NA
3.24
<5.0
NA
Nov-15
<0.1
3.35
<50
<0.1
May-16
NA
3.11
<50
NA
Nov-16
<0.01
2.52
189
0.0349
May-17
NA
3.04
393
NA
Nov-17
<0.0100 UJ
2.99
244
0.0696 J
May-18
NA
2.76
<50.0
NA
Nov-18
<0.0100
3.54
192
0.0257
May-19
NA
2.65
<5.0
NA
Nov-19
<0.0100
3.09
<50.0
0
May-20
NA
2.92
<50.0
NA
Nov-20
<0.0100
3.47
<50.0
0.0431
May-21
N/A
3.26
<5.0
N/A
Nov-21
<0.0091
3.42
<25.0
0.0479
Page 10 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-23B
Feb-04
<0.01
1.67
594
0.124
May-04
<0.01
1.14
<7
0.115
Jun-04
<0.01
1.76
<35
0.101
Nov-04
<0.01
1.82
393
0.0857
May-05
<0.2
1.29
<35
<0.2
Nov-05
<0.01
1.33
<35
0.129
May-06
<0.01
0.891
51.9
0.116
Nov-06
<0.02
1.7
907
0.128
May-07
<0.02
2.29
<70
0.0973
Nov-07
<0.01
1.94
<7
0.128
May-08
<0.01
2.31
<7
0.123
Nov-08
<0.01
2.54
<7
0.112
May-09
NA
1.77
<7
NA
Dec-09
<0.01
2.46
<7
0.183
May-10
NA
2.14
<7
NA
Nov-10
<0.01
2.02
<7
0.0768
May-11
NA
2.15
NA
NA
Nov-11
<0.01
2.49
<7
0.0982
May-12
NA
2.39
NA
NA
Nov-12
<0.01
3.52
<7
0.0811
May-13
NA
2.72
120
NA
Nov-13
<0.01
2.88
82.3
0.0759
May-14
NA
3.01
381
NA
Nov-14
<0.0111
3.4
542
0.103
May-15
NA
2.78
<5.0
NA
Nov-15
<0.01
3.33
<50
<0.01
May-16
NA
2.73
<50
NA
Nov-16
<0.01
2.71
516
0.0275
May-17
NA
2.62
512
NA
Nov-17
<0.0100
2.63
<5.0
0.103
May-18
NA
2.53
<50.0
NA
Nov-18
<0.0100
3.04
74
0.0322
May-19
NA
3.4
<5.0
NA
Nov-19
<0.0100
3.08
<50.0
0
May-20
NA
2.63
<50.0
NA
Nov-20
<0.0100
3.15
<50.0
0.0696
May-21
N/A
2.69
<5.0
N/A
Nov-21
<0.0091
3
<25.0
0.0448
Page 11 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-24A
Feb-04
<0.01
0.0548
7.8
<0.01
May-04
<0.01
0.022
<7
<0.01
Jun-04
<0.01
0.0625
<7
<0.01
Nov-04
<0.01
0.0796
<7
<0.01
May-05
<0.01
0.0885
<7
<0.01
Nov-05
<0.01
0.0726
<7
0.0111
May-06
<0.01
0.105
NA
0.0102
Nov-06
<0.01
0.158
NA
0.0126
May-07
<0.01
0.141
NA
<0.01
Nov-07
<0.01
0.161
NA
0.0124
May-08
<0.01
0.159
<7
<0.01
Nov-08
<0.01
0.125
NA
0.0124
May-09
NA
0.113
NA
NA
Dec-09
<0.01
0.15
NA
0.0169
May-10
NA
0.135
NA
NA
Nov-10
<0.01
0.133
NA
0.01
May-11
NA
0.102
NA
NA
Nov-11
<0.01
0.132
NA
0.0118
Nov-12
<0.01
0.218
NA
0.011
May-13
NA
0.126
NA
NA
Nov-13
<0.01
0.158
NA
<0.01
May-14
NA
0.189
NA
NA
Nov-14
<0.01
0.23
NA
0.0124
May-15
NA
0.103
NA
NA
Nov-15
NA
NA
NA
NA
May-16
<0.01
0.188
NA
<0.01
Nov-16
<0.01
0.155
NA
<0.01
Ma -17
NA
0.0437
NA
NA
Nov-17
<0.0100
0.198
NA
0.013
Ma -18
NA
0.158
NA
NA
Nov-18
<0.0100
0.0313
NA
<0.0100
Ma -19
NA
0.231
NA
NA
Nov-19
<0.0100
0.214
NA
<0.0100
May-20
NA
0.162
NA
NA
Nov-20
<0.0100
0.182
NA
<0.0100
May-21
N/A
0.226
N/A
N/A
Nov-21
<0.0083
0.248
N/A
0.0091
Page 12 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-24B
Feb-04
<0.01
0.0586
<7
0.0184
Ma -04
<0.01
0.0439
<7
0.0178
Jun-04
<0.01
0.0892
<7
0.0146
Nov-04
<0.01
0.082
<7
0.0181
May-05
<0.01
0.0722
<7
0.0194
Nov-05
<0.01
0.0591
<7
0.0165
May-06
<0.01
0.0746
NA
0.0178
Nov-06
<0.01
0.101
NA
0.018
May-07
<0.01
0.0962
NA
0.015
Nov-07
<0.01
0.102
NA
0.0158
May-08
<0.01
0.113
<7
0.0151
Nov-08
<0.01
0.0877
NA
0.0178
Dec-09
<0.01
0.0931
NA
0.0226
Nov-10
<0.01
0.0896
NA
0.0151
Nov-11
<0.01
0.0874
NA
0.0144
Ma -12
NA
0.103
NA
NA
Nov-12
<0.01
0.118
NA
0.0136
Nov-13
<0.01
0.0918
NA
<0.01
Nov-14
<0.01
0.103
NA
0.0101
Nov-15
NA
NA
NA
NA
May-16
<0.01
0.0998
NA
<0.01
Nov-16
<0.01
0.122
NA
0.0102
Nov-17
<0.0100
0.104
NA
0.0178
Nov-18
<0.0100
0.0485
NA
<0.0100
Nov-19
<0.0100
0
NA
0
Nov-20
<0.0100
0.103
NA
0.0104
Nov-21
<0.0083
0.12
N/A
0.012
Page 13 of 14 5/10/2022

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-32B
Jun-04
<0.01
0.176
<28
0.0577
Nov-04
<0.01
0.198
162
0.0575
Ma -05
<0.2
0.115
<14
<0.2
Nov-05
<0.01
0.072
<14
0.0416
Ma -06
<0.01
0.0818
27.6
0.0617
Nov-06
<0.01
0.0996
344
0.0558
Ma -07
<0.01
0.149
<35
0.0414
Nov-07
<0.01
0.117
<7
0.0816
Ma -08
<0.01
0.0796
<7
0.0329
Nov-08
<0.01
0.173
<7
0.0816
Dec-09
<0.01
0.104
<7
0.0621
Nov-10
<0.01
0.144
<7
0.0566
Nov-11
<0.01
0.0988
<7
0.0399
Nov-12
<0.01
0.0755
<7
<0.01
Nov-13
<0.01
0.0275
<7
0.0106
Nov-14
<0.01
0.0178
<10
<0.01
Nov-15
<0.01
0.0183
<50
<0.01
Nov-16
<0.01
0.0123
<5
<0.01
Nov-17
<0.0100
0.0152
246
<0.0100
Nov-18
<0.0100
0.0033
<50.0
<0.0100
Nov-19
<0.0100
0.0041
<5.0
<0.0100
Nov-20
<0.0100
.0034
<5.0
<0.0100
Nov-21
<0.0100HO(.0032
<5.0
<0.0100
Notes:
mg/L - milligrams per liter
NA - Not Analyzed
PQL - Practical Quantitation Limit
Page 14 of 14 5/10/2022

Ethylene Glycol (B-01)
J
OI
c
c
c
U
pb 0 p6
Date
B-01 f NC 2L Standard
Table 8
Time vs. Concentration Plots - Ethylene Glycol
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Ethylene Glycol (B-09C)
O)
E
c
0
.c
c
U
Date
tB-09C tNC2LStandard
Ethylene Glycol (B-23A)
_ 450
J 400
W
E aso
300
° 250
200
y 150
C 100
tj 50
0
Date
tB-23A t-NC 2L Standard
i -
Ethylene Glycol(B-10)
J 1000
� 800
.io soo
� 400
m
c zoo
O
U
0
Date
tB-10 tNC2LStandard
Ethylene Glycol (B-23B)
loon
J_
� 800
E
`o soa
.q
C 400
C200
U
0
Date
t B-236 f NC 2L Standard
Page 1 of 1 5/10/2022

s
4
3
2
1
0
1,4-Dioxane (B-01)
Date
B-01 f NC 2L Standard
1,4-Dioxane (B-12)
J 5
£ 4
c 3
O
m 2
c 1
0
v )Jc )Jc )Jc )JJ )Jc )JJ )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc
5
4
3
2
1
0
Date
—*—B-12 tNC2LStandard
1,4-Dioxane(B-23A)
Date
tB-23A f NC 2L Standard
Table 9
Time vs. Concentration Plots — 1,4-Dioxane
CNA Holdings LLC — Needmore Road Landfill
5
4
3
2
0
AECOM Project No. 60683034
1,4-Dioxane (B-09C)
Date
t B-09C f NC 2L Standard
1,4-Dioxane (B-17C)
J 5
01 4
t=
c 3
O
2
R
C 1
U O
O
U )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc )Jc
Date
tB-1X tNC2LStandard
1,4-Dioxane(B-23B)
5
4
3
2
1
0
)J�d 05 OA6 O'" ,O0 Oa c^o O,� O^ry ,^1 O,�a 0,�l O^0 o^' ,^0 O0 coo K,�
)J )J )J )J )J )J )J )J )J )J )J )J )J )J )J )J )J
Date
t B-23B t NC 2L Standard
1,4-Dioxane (B-10)
5
4
3
2
1
0
)JC )JC )JJ )JJ )JJ )JJ )JC )JC )JK )JK )JK )JC )JC )JC )JC )JC )JC )JC
Date
B-10 f NC 2L Standard
1,4-Dioxane (B-22B)
J 5
a 4
E 3
C
O 2
C 1
u 0
Ca
)J )J )J )J )J )J )J )J )J )J )J )J )J )J )J )J )J )J
0.3
0.25
0.2
0.15 Jh
0.1
0.05
0
Date
--*--- B-22B f NC 2L Standard
1,4-Dioxane (B-24A)
Date
tB-24A ANC 2L Standard
Page 1 of 1
5/10/2022

Diphenyl Ether(B-01)
0.5
J
0.4
0.3
O
0.2
0.1
U
C 0
U
Date
tB-01 tNC 2L Standard
0.5
J
07 0.4
E
= 0.3
O
.q
0.2
Table 10
Time vs. Concentration Plots - Diphenyl Ether
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60683034
Diphenyl Ether (B-12)
J 0.12
0.1
0.08
O 0.06
i 0.04
0.02
C 0
O Ob 00 06 01 06 O°j ,�O ^'� ,�`L ^3 ^b ^6 ,�6 ^A
U S§c ��3c �S§c �� ��c ��c ��c ��c ��c ��c ��c ��c ��
Diphenyl Ether (B-23A)
Date
F B-12 f NC 2L Standard
c 0.1
C 0
O Ob pg 06 p� 09 poi O ^^ ry ^- qb ^5 q6 NA q0
V 'c -o �c �c �c �c �c s §c "c .c -, �, -, �c -,, ��c
> > > > > > > > > > > > > > > > > >
Date
+B-23A tNC 2L Standard
J 0.5
07 0.4
E
= 0.3
O
.q
0.2
Diphenyl Ether (B-10)
s
J
E 4
� 3
O
i 2
c
V
C 0
O
U c . . . . . . . c . c . c . c .
Diphenyl Ether (B-23B)
Date
tB-10 tNC2LStandard
c 0.1
8 0
CO Ob d, 06 01 00 Z§b NO ^N Nil Nb Nb ^`o N. ^'1 N. ^A rp rah
V Jc s -c -, sc �c �c �c sc �c sc �l sc �l
> > > > > > > > > > > > > > > > > >
Date
+B-23B t NC 2L Standard
Page 1 of 1 5/10/2022

2021 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
Figures
AECOM Project number: 60683034
AECOM

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FIGURE 1
SITE LOCATION MAP
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
MAY 2022 60683034

r'
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a
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SITE
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8
14-ACRE SITE j
L=com
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0. 400' 800'
SCALE
FIGURE 2
SITE LAYOUT MAP
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
6068303,
C\Users\splawnm\OneDrive - AECOM\Desktop\Projects\Salisbury\60313404_031 Site Layout Map_Nov2021.dwg, 4/11/20224:51:31 PM, DWG To PDF.pc3

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a
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a
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SURFACE WATER SAMPLING LOCATIONS
INTERMITTENT SEEP SAMPLING LOCATION
CSW-2 WAS DRY AND THEREFORE NOT SAMPLED.
7 ld�w
I
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,70
I
4 I
1, 6 0. 400' 800'
SCALE
FIGURE 3
SAMPLE LOCATION MAP
MAY 2021
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2022 60683034
C:\Users\splawnm\OneDrive - AECOM\Desktop\Projects\Salisbury\60313404_029 Sample Location Map_May2021.dwg, 4/11/2022 4:41:46 PM, DWG To PDF.pc3

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SURFACE WATER SAMPLING
LOCATIONS
INTERMITTENT SEEP SAMPLING LOCATIONS
-17 SW 5
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m
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FIGURE 4
SAMPLE LOCATION MAP
NOVEMBER 2021
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2022 60683034
C:\Users\splawnm\OneDrive - AECOM\Desktop\Projects\Salisbury\60313404_030 Sample Location Map_Nov2021.dwg, 4/11/20224:41:23 PM, DWG To PDF.pc3

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`1
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[658.301
B-22A
[657.62]
B-23 B
[657.62]
B-23A
[657.101
B-24B
[655.84]
B-24A
1654.821
L=com
LEGEND
MONITORING WELL LOCATION
GROUNDWATER CONTOUR
(DASHED WHERE INFERRED)
MAY 202
0 P.00 400 800
SC4LE I% FEET
FIGURE 5
GROUNDWATER ELEVATION DATA
NOVEMBER 2021
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
2
606830341
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B-23B
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<5.0
B-10
<5.0 /<5.0 /
P"=COM
LEGEND
® MONITORING WELL LOCATION
SURFACE WATER SAMPLING LOCATION
<5.0 ETHYLENE GLYCOL CONCENTRATION (mg/L)
NOTE: Locations not sampled or analyzed for ethylene
glycol are not shown.
I
N
o7
I
4 I
1, 6 0. 400' 800'
SCALE
FIGURE 6
ETHYLENE GLYCOL MAP
MAY 2021
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2022 60683034
C:\Users\splawnnn\OneDrive - AECOM\Desktop\Projects\Salisbury\60313404_023 Ethylene Glycol Map_May2021 Data.dwg, 4/11/2022 4:34:13 PM, DWG To PDF.pc3

c
I 0 o B 09C
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SLIGHTLY UPSTREAM
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Q
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B-23B
<25.0 \
° ss
-23A
<25.0
0
5
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<5.0
B-10
<5.0 /
L=COM
LEGEND
® MONITORING WELL LOCATION
SURFACE WATER SAMPLING LOCATION
<5.0 ETHYLENE GLYCOL CONCENTRATION (mg/L)
NOTE: Locations not sampled or analyzed for ethylene
glycol are not shown.
i
SW-8 <5.0 —
± 1000 FT DOWN STREAM
OF COOLEEMEE WEIR
SW-7
—_�5.0
I
0
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I
ti I
01 400' 800'
I
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FIGURE 7
ETHYLENE GLYCOL MAP
NOVEMBER 2021
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2022 60683034
C:\Users\splawnm\OneDrive - AECOM\Desktop\Projects\Salisbury\60313404_024 Ethylene Glycol Map_Nov2021 Data.dwg, 4/11/20224:34AO PM, DWG To PDF.pc3

m 1 O W
Q B-09C
0 0.8. o
0
C3
LEGEND
\ ® MONITORING WELL LOCATION
J LJ SURFACE WATER SAMPLING LOCATION
® INTERMITTENT SEEP SAMPLING LOCATION
1.18 1,4-DIOXANE CONCENTRATION (mg/L)
J
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W-5
®< .0020
B-22B
1.33
B-63B
o \
B-23A
3.26
m
B-24A
.226
0
B-01
01.61
B-10
0.193/0.181
P"=COM
NOTES:
Locations not sampled or analyzed for 1,4-dioxane are not shown.
I
N
o7
I
4 I
1, 6 0. 400' 800'
SCALE
FIGURE 8
1,4-DIOXANE MAP
MAY 2021
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2022 60683034
C:\Users\splawnrn\OneDrwe - AECOM\Desktop\Projects\Salisbury\60313404_025 1-4 Dioxane Map May2021 Data.dwg, 4/11/2022 4:34:53 PM, DWG To PDF.pc3

a
11 b
I
B-09C
0.909/0.956 69
B-2'
®0.00
°
1ti .35
1 C3
SW-3 <0.0020
SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
J
37 C S 0
020
° 1.06
2A
1.
1.2
° B-23B
° 3 \
23A
.42
B-24B
0.12
s� 6AA
.248 SW-7
<0 20
LEGEND
0 MONITORING WELL LOCATION
SURFACE WATER SAMPLING LOCATION
INTERMITTENT SEEP SAMPLING LOCATIONS
1.37 1,4-DIOXANE CONCENTRATION (mg/L)
NOTE: Locations not sampled or analyzed for 1,4-dioxane
are not shown.
SW-8 <0.0020
000 FT DOWN STREAM
,F COOLEEMEE WEIR
gg o
®1.65
B-10 1
0.18 1°
1 6
® 70
0A I� 71
4 I
1� V
1 1,
1 6 01 400' 800,
SCALE
FIGURE 9
1,4-DIOXANE MAP
P"=COM NOVEMBER 2021
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2022 60683034
C:\Users\splawnm\OneDrive - AECOM\Desktop\Projects\Salisbury\60313404_0261-4 Dwane Map_Nov2021 Data.dwg, 4/11/20224:35:27 PM, DWG To PDF.pc3

1 Q `^
a
b
Q o Ce
<0.0091 /< . 0 e°
0
1ti B-1
SW-3 <0.0091
SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
LEGEND
® MONITORING WELL LOCATION
0 SURFACE WATER SAMPLING LOCATION
J<0.01 1,1-BIPHENYL CONCENTRATION (mg/L)
NOTE:
Locations not sampled or analyzed for 1,1-biphenyl are not shown.
I S -5
1 B 0 00< .01
83
\� BO 0083
\ � o
\ 0.0091\
- 3A
00091
B-24B
<0.008
-24A
\ 0.0083 SW-7
L=COM
SW-8 <0.0083
1000 FT DOWN STREAM
DF COOLEEMEE WEIR
I�
Gl
I
I
01 400' 800'
SCALE
FIGURE 10
1,1-BIPHENYL MAP
NOVEMBER 2021
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
2022
60683034
C:\Users\splawnm\OneDrive - AECOM\Desktop\Projects\Salisbury\60313404_027 1-1 Biphenyl Map_Nov2021 Data.dwg, 4/11/20224:33:51 PM, DWG To PDF.pc3

i � @bpi Ali l
i<
ISW-3 <0.0091
SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
/ J LEGEND
® MONITORING WELL LOCATION
SURFACE WATER SAMPLING LOCATION
J0.0448 DIPHENYL ETHER CONCENTRATION (mg/L)
NOTES:
Locations not sampled or analyzed for diphenyl ether
are not shown.
<0'71 B-22B 0.01
.0484
0.0B-22A
< 171 <0.0083
SW-8 <0.0083
0.0448 ± 1000 FT DOWN STREAM
.044\ OF COOLEEMEE WEIR
s
- 3A
479
B-24B
0.0120
B-24A SW_
0.0091 091
v
ggppo
® 0.0309
75 I N
.1 1 �
1"
1 6
® 70
� 71
4 I
1� V
1 1,
0. 400' 800'
SCALE
FIGURE 11
DIPHENYL ETHER MAP
P"=COM NOVEMBER 2021
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2022 60683034
C\Users\splawnm\OneDrive - AECOM\Desktop\Projects\Salisbury\60313404_028 Diphenyl Ether Map_Nov2021 Data.dwg, 4/11/2022 4:49:39 PM, DWG To PDF.pc3

2021 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
Appendix A
May 2021 and November 2021
Laboratory Analytical Reports
AECOM Project number: 60683034
AECOM

lceAnalyilcal®
www.pacelabs.cem
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
May 28, 2021
Jing Zhou
AECOM
1000 Abernathy Road
Building 400, Suite 900
Atlanta, GA 30328
RE: Project: NRLF
Pace Project No.: 92539166
Dear Jing Zhou:
Enclosed are the analytical results for sample(s) received by the laboratory on May 17, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Indianapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
1(704)875-9092
Project Manager
Enclosures
cc: Rob Davis, AECOM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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Greenwood, SC 29649
[phone]
Project: NRLF
Pace Project No.: 92539166
Pace Analytical Services Indianapolis
7726 Moller Road, Indianapolis, IN 46268
Illinois Accreditation #: 200074
Indiana Drinking Water Laboratory #: C-49-06
Kansas/TNI Certification #: E-10177
Kentucky UST Agency Interest #: 80226
Kentucky WW Laboratory ID M 98019
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Michigan Drinking Water Laboratory #9050
Ohio VAP Certified Laboratory #: CL0065
Oklahoma Laboratory #: 9204
Texas Certification #: T104704355
Wisconsin Laboratory #: 999788130
USDA Soil Permit #: P330-19-00257
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 34

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816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
NRLF
92539166
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92539166001
B-12-051721
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
NGP
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92539166002
B-10-051721
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
NGP
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92539166003
B-99-051721
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
NGP
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92539189001
B-01-051721
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
NGP
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92539189002
B-09C-051721
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
NGP
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92539189003
B-23A-051721
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
NGP
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project:
NRLF
Pace Project No.:
92539166
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 9056A
CDC
1
PASI-A
92539189004
13-2313-051721
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
NGP
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92539189005
B-17C-051721
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
NGP
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92539189006
13-2213-051721
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
NGP
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92539189007
B-24A-051721
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
NGP
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92539189008
SW-5-051721
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92539189009
CSW-1-051721
EPA 8260DMod.
LMB
3
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-I = Pace Analytical Services - Indianapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: B-12-051721 Lab ID: 92539166001 Collected: 05/17/21 13:03 Received: 05/17/21 15:09 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
10.0
1
05/19/21 11:55
05/20/21 15:50
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L
10.0
1
05/19/21 11:55
05/20/21 15:50
101-84-8
Surrogates
Nitrobenzene-d5 (S)
82 %
10-144
1
05/19/21 11:55
05/20/21 15:50
4165-60-0
2-Fluorobiphenyl (S)
68 %
10-130
1
05/19/21 11:55
05/20/21 15:50
321-60-8
Terphenyl-d14 (S)
146 %
34-163
1
05/19/21 11:55
05/20/21 15:50
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1840 ug/L
100
50
05/18/21 01:20
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
96 %
70-130
50
05/18/21 01:20
17060-07-0
Toluene-d8 (S)
116 %
66-133
50
05/18/21 01:20
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
401 mg/L
5.0
1
05/24/21 21:40
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
05/18/21 10:40
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/18/21 10:40
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.22 mg/L
0.050
1
05/18/21 02:48
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.4 mg/L
1.0
1
05/19/2104:47
14808-79-8
Date: 05/28/2021 10:38 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
M1
Page 5 of 34

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: B-10-051721 Lab ID: 92539166002 Collected: 05/17/21 13:40 Received: 05/17/21 15:09 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
5.0
1
05/24/21 16:59
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA
3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
127 ug/L
100
10
05/19/21 11:55
05/21/21 10:32
92-52-4
Diphenyl ether (Phenyl ether)
1210 ug/L
100
10
05/19/21 11:55
05/21/21 10:32
101-84-8
Surrogates
Nitrobenzene-d5 (S)
110 %
10-144
1
05/19/21 11:55
05/20/21 16:15
4165-60-0
2-Fluorobiphenyl (S)
89 %
10-130
1
05/19/21 11:55
05/20/21 16:15
321-60-8
Terphenyl-d14 (S)
130 %
34-163
1
05/19/21 11:55
05/20/21 16:15
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
193 ug/L
10.0
5
05/18/21 01:39
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
98 %
70-130
5
05/18/21 01:39
17060-07-0
Toluene-d8 (S)
113 %
66-133
5
05/18/21 01:39
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
475 mg/L
5.0
1
05/24/21 13:34
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.046 mg/L
0.040
1
05/18/21 10:41
14797-55-8
Nitrogen, Nitrite
0.062 mg/L
0.040
1
05/18/21 10:41
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.34 mg/L
0.084
1.67
05/18/21 02:48
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/19/2105:01
14808-79-8
Date: 05/28/2021 10:38 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: B-99-051721 Lab ID: 92539166003 Collected: 05/17/21 13:45 Received: 05/17/21 15:09 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
5.0
1
05/24/21 17:08
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
119 ug/L
100
10
05/19/21 11:55
05/21/21 10:58
92-52-4
Diphenyl ether (Phenyl ether)
1170 ug/L
100
10
05/19/21 11:55
05/21/21 10:58
101-84-8
Surrogates
Nitrobenzene-d5 (S)
96 %
10-144
1
05/19/21 11:55
05/20/21 16:40
4165-60-0
2-Fluorobiphenyl (S)
76 %
10-130
1
05/19/21 11:55
05/20/21 16:40
321-60-8
Terphenyl-d14 (S)
109 %
34-163
1
05/19/21 11:55
05/20/21 16:40
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
181 ug/L
10.0
5
05/18/21 01:58
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
100 %
70-130
5
05/18/21 01:58
17060-07-0
Toluene-d8 (S)
111 %
66-133
5
05/18/21 01:58
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
473 mg/L
5.0
1
05/24/21 13:46
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.061 mg/L
0.040
1
05/18/21 10:42
14797-55-8
Nitrogen, Nitrite
0.058 mg/L
0.040
1
05/18/21 10:42
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.39 mg/L
0.050
1
05/18/21 02:49
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/19/2106:11
14808-79-8
Date: 05/28/2021 10:38 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: B-01-051721
Lab ID: 92539189001 Collected: 05/17/21
12:41
Received: 05/17/21 13:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/24/21 16:22
107-21-1
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1610 ug/L 50.0
25
05/18/21 02:17
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
96 % 70-130
25
05/18/21 02:17
17060-07-0
Toluene-d8 (S)
114 % 66-133
25
05/18/21 02:17
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
1590 mg/L 5.0
1
05/24/21 14:53
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L 0.040
1
05/18/21 10:37
14797-55-8
Nitrogen, Nitrite
0.18 mg/L 0.040
1
05/18/21 10:37
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
1.3 mg/L 0.25
5
05/18/21 02:47
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
7.1 mg/L 1.0
1
05/19/2106:25
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: B-09C-051721
Lab ID: 92539189002 Collected: 05/17/21
11:43
Received: 05/17/21 13:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/24/21 18:04
107-21-1
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
852 ug/L 20.0
10
05/18/21 02:36
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
100 % 70-130
10
05/18/21 02:36
17060-07-0
Toluene-d8 (S)
111 % 66-133
10
05/18/21 02:36
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
2860 mg/L 5.0
1
05/24/21 15:30
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L 0.040
1
05/18/21 10:34
14797-55-8
Nitrogen, Nitrite
0.26 mg/L 0.040
1
05/18/21 10:34
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.27 mg/L 0.25
5
05/18/21 02:45
M1,R1
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.4 mg/L 1.0
1
05/19/2106:39
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 34

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816 Durst Avenue East
Greenwood, SC 29649
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ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: B-23A-051721
Lab ID: 92539189003 Collected: 05/17/21 10:46
Received: 05/17/21 13:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/24/21 16:41
107-21-1
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
3260 ug/L 100
50
05/18/21 02:55
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
100 % 70-130
50
05/18/21 02:55
17060-07-0
Toluene-d8 (S)
113 % 66-133
50
05/18/21 02:55
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
3390 mg/L 5.0
1
05/24/21 16:18
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.041 mg/L 0.040
1
05/18/21 10:32
14797-55-8
Nitrogen, Nitrite
ND mg/L 0.040
1
05/18/21 10:32
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.77 mg/L 0.25
5
05/18/21 02:44
F6
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
4.8 mg/L 1.0
1
05/19/2106:53
14808-79-8
Date: 05/28/2021 10:38 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 34

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ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: 13-2313-051721
Lab ID: 92539189004 Collected: 05/17/21 11:35
Received: 05/17/21 13:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/24/21 16:50
107-21-1
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
2690 ug/L 100
50
05/18/21 03:14
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
98 % 70-130
50
05/18/21 03:14
17060-07-0
Toluene-d8 (S)
111 % 66-133
50
05/18/21 03:14
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
2060 mg/L 5.0
1
05/24/21 17:33
M1
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L 0.040
1
05/18/21 10:33
14797-55-8
Nitrogen, Nitrite
0.12 mg/L 0.040
1
05/18/21 10:33
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.42 mg/L 0.25
5
05/18/21 02:45
F6
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
3.8 mg/L 1.0
1
05/19/2107:07
14808-79-8
Date: 05/28/2021 10:38 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 34

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Greenwood, SC 29649
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ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: B-17C-051721
Lab ID: 92539189005 Collected:
05/17/21 12:26
Received: 05/17/21 13:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1180 ug/L
50.0
25
05/18/21 03:33
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
93 %
70-130
25
05/18/21 03:33
17060-07-0
Toluene-d8 (S)
111 %
66-133
25
05/18/21 03:33
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
390 mg/L
5.0
1
05/24/21 21:49
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
05/18/21 10:36
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/18/21 10:36
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.26 mg/L
0.050
1
05/18/21 02:47
F6
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.4 mg/L
1.0
1
05/19/2107:21
14808-79-8
Date: 05/28/2021 10:38 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: 13-2213-051721
Lab ID: 92539189006 Collected:
05/17/21 10:37
Received: 05/17/21 13:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1330 ug/L
40.0
20
05/18/21 03:51
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92 %
70-130
20
05/18/21 03:51
17060-07-0
Toluene-d8 (S)
112 %
66-133
20
05/18/21 03:51
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
797 mg/L
5.0
1
05/24/21 22:00
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
05/18/21 10:31
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/18/21 10:31
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.22 mg/L
0.050
1
05/18/21 02:42
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/19/2107:35
14808-79-8
Date: 05/28/2021 10:38 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: B-24A-051721
Lab ID: 92539189007 Collected:
05/17/21 09:48
Received: 05/17/21 13:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
226 ug/L
5.0
2.5
05/18/21 04:10
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92 %
70-130
2.5
05/18/21 04:10
17060-07-0
Toluene-d8 (S)
110 %
66-133
2.5
05/18/21 04:10
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
505 mg/L
5.0
1
05/24/21 19:52
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.041 mg/L
0.040
1
05/18/21 10:30
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/18/21 10:30
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
ND mg/L
0.062
1.25
05/18/21 02:40
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/19/2107:49
14808-79-8
Date: 05/28/2021 10:38 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: SW-5-051721
Lab ID: 92539189008 Collected: 05/17/21
08:15
Received: 05/17/21 13:00 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/24/21 16:13
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 10.0
1
05/20/21 08:32
05/25/21 09:41
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 10.0
1
05/20/21 08:32
05/25/21 09:41
101-84-8
Surrogates
Nitrobenzene-d5 (S)
61 % 10-144
1
05/20/21 08:32
05/25/21 09:41
4165-60-0
2-Fluorobiphenyl (S)
43 % 10-130
1
05/20/21 08:32
05/25/21 09:41
321-60-8
Terphenyl-d14 (S)
62 % 34-163
1
05/20/21 08:32
05/25/21 09:41
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
05/18/21 01:01
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
96 % 70-130
1
05/18/21 01:01
17060-07-0
Toluene-d8 (S)
115 % 66-133
1
05/18/21 01:01
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92539166
Sample: CSW-1-051721
Lab ID: 92539189009 Collected:
05/17/21
09:02
Received: 05/17/21 13:00 Matrix: Water
Parameters
Results Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
696 ug/L
20.0
10
05/18/21 04:29
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
93 %
70-130
10
05/18/21 04:29
17060-07-0
Toluene-d8 (S)
110 %
66-133
10
05/18/21 04:29
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92539166
QC Batch: 622490 Analysis Method: EPA 8015 Alcohol -Glycol
QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified
Laboratory: Pace Analytical Services - Indianapolis
Associated Lab Samples: 92539166002, 92539166003, 92539189001, 92539189002, 92539189003, 92539189004, 92539189008
METHOD BLANK: 2868778 Matrix: Water
Associated Lab Samples: 92539166002, 92539166003, 92539189001, 92539189002, 92539189003, 92539189004, 92539189008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ethylene glycol mg/L ND 5.0 05/24/21 16:04
LABORATORY CONTROL SAMPLE: 2868779
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Ethylene glycol mg/L 25 35.2 141 39-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2868780 2868781
MS MSD
92539189008 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mg/L ND 25 25 37.9 40.5 150 160 36-158 7 MO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC.
Page 17 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92539166
QC Batch: 620969 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92539166001, 92539166002, 92539166003, 92539189001
METHOD BLANK: 3267380
Matrix:
Water
Associated Lab Samples:
92539166001, 92539166002, 92539166003, 92539189001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
05/17/21 19:21
1,2-Dichloroethane-d4 (S)
%
94
70-130
05/17/21 19:21
Toluene-d8 (S)
%
116
66-133
05/17/21 19:21
LABORATORY CONTROL SAMPLE: 3267381
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 19.3 96 70-130
1,2-Dichloroethane-d4 (S) % 93 70-130
Toluene-d8(S) % 116 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3267382
3267383
MS
MSD
92539189001 Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 1610 500
500
2080
2050 94
88
64-141 1
1,2-Dichloroethane-d4 (S)
%
96
92
70-130
Toluene-d8(S)
%
110
110
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92539166
QC Batch: 620971 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92539189002, 92539189003, 92539189004, 92539189005, 92539189006, 92539189007, 92539189008,
92539189009
METHOD BLANK: 3267388
Matrix:
Water
Associated Lab Samples:
92539189002, 92539189003, 92539189004, 92539189005, 92539189006,
92539189007, 92539189008,
92539189009
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
05/17/21 19:40
1,2-Dichloroethane-d4 (S)
%
91
70-130
05/17/21 19:40
Toluene-d8 (S)
%
117
66-133
05/17/21 19:40
LABORATORY CONTROL SAMPLE: 3267389
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 18.8 94 70-130
1,2-Dichloroethane-d4 (S) % 90 70-130
Toluene-d8(S) % 115 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3267390
3267391
MS
MSD
92539189009 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 696 200
200 897
887 101
96
64-141 1
1,2-Dichloroethane-d4 (S)
%
92
88
70-130
Toluene-d8(S)
%
112
109
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92539166
QC Batch: 621428
Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C
Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92539166001, 92539166002,
92539166003, 92539189008
METHOD BLANK: 3269633
Matrix: Water
Associated Lab Samples: 92539166001, 92539166002,
92539166003, 92539189008
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Biphenyl (Diphenyl)
ug/L
ND 10.0
05/20/21 11:15
Diphenyl ether (Phenyl ether)
ug/L
ND 10.0
05/20/21 11:15
2-Fluorobiphenyl (S)
%
92 10-130
05/20/21 11:15
Nitrobenzene-d5 (S)
%
118 10-144
05/20/21 11:15
Terphenyl-d14 (S)
%
145 34-163
05/20/21 11:15
LABORATORY CONTROL SAMPLE:
3269634
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Biphenyl (Diphenyl)
ug/L
50 42.3
85 31-130
Diphenyl ether (Phenyl ether)
ug/L
50 43.1
86 25-130
2-Fluorobiphenyl (S)
%
79 10-130
Nitrobenzene-d5 (S)
%
98 10-144
Terphenyl-d14 (S)
%
120 34-163
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3269635 3269636
MS MSD
92539018005
Spike Spike MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Biphenyl (Diphenyl)
ug/L ND
50 50 54.0
28.0 108 56
17-130 63 R1
Diphenyl ether (Phenyl ether)
ug/L ND
50 50 55.8
27.8 112 56
16-130 67 R1
2-Fluorobiphenyl (S)
%
98 46
10-130
Nitrobenzene-d5 (S)
%
108 61
10-144
Terphenyl-d14 (S)
%
132 105
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 34

lreAnalyilcal®
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92539166
QC Batch: 622414 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92539166001,92539166002,92539166003,92539189001,92539189002,92539189003,92539189004,
92539189005,92539189006,92539189007
METHOD BLANK: 3274648 Matrix: Water
Associated Lab Samples: 92539166001,92539166002,92539166003,92539189001,92539189002,92539189003,92539189004,
92539189005,92539189006,92539189007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Alkalinity, Total as CaCO3 mg/L ND 5.0 05/24/21 12:40
LABORATORY CONTROL SAMPLE: 3274649
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 mg/L 50 52.2 104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3274650 3274651
MS MSD
92539166001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 401 50 50 419 423 37 44 80-120 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3274652 3274653
MS MSD
92539189004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 2060 50 50 2080 2080 41 43 80-120 0 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC.
Page 21 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92539166
QC Batch: 621031 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92539166001,92539166002,92539166003,92539189001,92539189002,92539189003,92539189004,
92539189005,92539189006,92539189007
METHOD BLANK: 3267495 Matrix: Water
Associated Lab Samples: 92539166001,92539166002,92539166003,92539189001,92539189002,92539189003,92539189004,
92539189005,92539189006,92539189007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.040 05/18/21 10:13
Nitrogen, Nitrite mg/L ND 0.040 05/18/21 10:13
LABORATORY CONTROL SAMPLE: 3267496
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 101 90-110
Nitrogen, Nitrite mg/L 1 1.0 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3267497
3267498
MS
MSD
92539163004 Spike
Spike MS
MSD MS
MSD % Rec
Parameter
Units
Result Conc.
Conc. Result
Result % Rec
% Rec Limits RPD Qual
Nitrogen, Nitrate
mg/L
6.3 1.5
1.5 7.8
7.7 95
95 90-110 0
Nitrogen, Nitrite
mg/L
0.089 1
1 1.0
0.99 91
90 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3267499
3267500
MS
MSD
92539163005 Spike
Spike MS
MSD MS MSD % Rec
Parameter
Units
Result Conc.
Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate
mg/L
0.82 1.5
1.5 2.3
2.3 97 96 90-110 0
Nitrogen, Nitrite
mg/L
0.020J 1
1 1.0
1.0 98 99 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC.
Page 22 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92539166
QC Batch: 621003 Analysis Method: SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011 Analysis Description: SM450OP-E Phosphorus, Ortho
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92539166001,92539166002,92539166003,92539189001,92539189002,92539189003,92539189004,
92539189005,92539189006,92539189007
METHOD BLANK: 3267457 Matrix: Water
Associated Lab Samples: 92539166001,92539166002,92539166003,92539189001,92539189002,92539189003,92539189004,
92539189005,92539189006,92539189007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Orthophosphate as P mg/L ND 0.050 05/18/21 02:36
LABORATORY CONTROL SAMPLE: 3267458
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Orthophosphate as P mg/L 0.25 0.25 102 49-145
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3267459 3267460
MS MSD
92539189007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Orthophosphate as P mg/L ND 0.31 0.31 0.30 0.30 97 96 90-110 0 F6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3267461 3267462
MS MSD
92539189002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Orthophosphate as P mg/L 0.27 0.25 0.25 1.4 1.2 447 360 90-110 17 F6,M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC.
Page 23 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92539166
QC Batch: 621093 Analysis Method: EPA 9056A
QC Batch Method: EPA 9056A Analysis Description: 9056 IC anions 28 Days
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92539166001,92539166002,92539166003,92539189001,92539189002,92539189003,92539189004,
92539189005,92539189006,92539189007
METHOD BLANK: 3267764 Matrix: Water
Associated Lab Samples: 92539166001,92539166002,92539166003,92539189001,92539189002,92539189003,92539189004,
92539189005,92539189006,92539189007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfate mg/L ND 1.0 05/18/2122:25
LABORATORY CONTROL SAMPLE: 3267765
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfate mg/L 50 50.2 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3267766 3267767
MS MSD
92538487021 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 121 50 50 166 172 91 102 90-110 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3267768 3267769
MS MSD
92539166002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L ND 50 50 51.2 51.6 102 103 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC.
Page 24 of 34

lreAnalyilcal®
www.pacelabs.cem
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALIFIERS
Project: NRLF
Pace Project No.: 92539166
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 92539189001
Ill Client informed the Orthophosphorus samples were field filtered.
Sample: 92539189002
Ill Client informed the Orthophosphorus samples were field filtered.
Sample: 92539189003
Ill Client informed the Orthophosphorus samples were field filtered.
Sample: 92539189004
Ill Client informed the Orthophosphorus samples were field filtered.
Sample: 92539189005
Ill Client informed the Orthophosphorus samples were field filtered.
Sample: 92539189006
Ill Client informed the Orthophosphorus samples were field filtered.
Sample: 92539189007
Ill Client informed the Orthophosphorus samples were field filtered.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 34

lreAnalyilcal®
www.pacelabs.cem
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALIFIERS
Project: NRLF
Pace Project No.: 92539166
ANALYTE QUALIFIERS
F6 Sample was not filtered within 15 minutes of collection and does not meet sampling and/or regulatory requirements.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 34

lreAnalyilcal®
www.pacelabs.cem
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NRLF
Pace Project No.: 92539166
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92539166002
B-10-051721
EPA 8015
Alcohol -Glycol
622490
92539166003
B-99-051721
EPA 8015
Alcohol -Glycol
622490
92539189001
B-01-051721
EPA 8015
Alcohol -Glycol
622490
92539189002
B-09C-051721
EPA 8015
Alcohol -Glycol
622490
92539189003
B-23A-051721
EPA 8015
Alcohol -Glycol
622490
92539189004
B-23B-051721
EPA 8015
Alcohol -Glycol
622490
92539189008
SW-5-051721
EPA 8015
Alcohol -Glycol
622490
92539166001
B-12-051721
EPA 3510C
621428
EPA 8270E 621686
92539166002
B-10-051721
EPA 3510C
621428
EPA 8270E 621686
92539166003
B-99-051721
EPA 3510C
621428
EPA 8270E 621686
92539189008
SW-5-051721
EPA 3510C
621428
EPA 8270E 621686
92539166001
B-12-051721
EPA 8260D Mod.
620969
92539166002
B-10-051721
EPA 8260D Mod.
620969
92539166003
B-99-051721
EPA 8260D Mod.
620969
92539189001
B-01-051721
EPA 8260D Mod.
620969
92539189002
B-09C-051721
EPA 8260D Mod.
620971
92539189003
B-23A-051721
EPA 8260D Mod.
620971
92539189004
B-23B-051721
EPA 8260D Mod.
620971
92539189005
B-17C-051721
EPA 8260D Mod.
620971
92539189006
B-22B-051721
EPA 8260D Mod.
620971
92539189007
B-24A-051721
EPA 8260D Mod.
620971
92539189008
SW-5-051721
EPA 8260D Mod.
620971
92539189009
CSW-1-051721
EPA 8260D Mod.
620971
92539166001
B-12-051721
SM 2320B-2011
622414
92539166002
B-10-051721
SM 2320B-2011
622414
92539166003
B-99-051721
SM 2320B-2011
622414
92539189001
B-01-051721
SM 2320B-2011
622414
92539189002
B-09C-051721
SM 2320B-2011
622414
92539189003
B-23A-051721
SM 2320B-2011
622414
92539189004
B-23B-051721
SM 2320B-2011
622414
92539189005
B-17C-051721
SM 2320B-2011
622414
92539189006
B-22B-051721
SM 2320B-2011
622414
92539189007
B-24A-051721
SM 2320B-2011
622414
92539166001
B-12-051721
EPA 353.2 Rev 2.0 1993
621031
92539166002
B-10-051721
EPA 353.2 Rev 2.0 1993
621031
92539166003
B-99-051721
EPA 353.2 Rev 2.0 1993
621031
92539189001
B-01-051721
EPA 353.2 Rev 2.0 1993
621031
92539189002
B-09C-051721
EPA 353.2 Rev 2.0 1993
621031
92539189003
B-23A-051721
EPA 353.2 Rev 2.0 1993
621031
92539189004
B-23B-051721
EPA 353.2 Rev 2.0 1993
621031
92539189005
B-17C-051721
EPA 353.2 Rev 2.0 1993
621031
92539189006
B-22B-051721
EPA 353.2 Rev 2.0 1993
621031
92539189007
B-24A-051721
EPA 353.2 Rev 2.0 1993
621031
92539166001
B-12-051721
SM 4500-P E-2011
621003
92539166002
B-10-051721
SM 4500-P E-2011
621003
92539166003
B-99-051721
SM 4500-P E-2011
621003
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2021 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 34

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NRLF
Pace Project No.: 92539166
Lab ID Sample ID QC Batch Method QC Batch
92539189001
B-01-051721
SM
4500-P
E-2011
621003
92539189002
B-09C-051721
SM
4500-P
E-2011
621003
92539189003
B-23A-051721
SM
4500-P
E-2011
621003
92539189004
B-23B-051721
SM
4500-P
E-2011
621003
92539189005
B-17C-051721
SM
4500-P
E-2011
621003
92539189006
B-22B-051721
SM
4500-P
E-2011
621003
92539189007
B-24A-051721
SM
4500-P
E-2011
621003
92539166001
B-12-051721
EPA 9056A
621093
92539166002
B-10-051721
EPA 9056A
621093
92539166003
B-99-051721
EPA 9056A
621093
92539189001
B-01-051721
EPA 9056A
621093
92539189002
B-09C-051721
EPA 9056A
621093
92539189003
B-23A-051721
EPA 9056A
621093
92539189004
B-23B-051721
EPA 9056A
621093
92539189005
B-17C-051721
EPA 9056A
621093
92539189006
B-22B-051721
EPA 9056A
621093
92539189007
B-24A-051721
EPA 9056A
621093
Date: 05/28/2021 10:38 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 28 of 34

Document Name:
Document Revised: October 28, 2020
i aCEAfIaoical�
Sample Condition Upon Receipt(SCUR) -
- -Page oaf-2-.. -- —
Document No.:
F-CAR-CS-033-Rev.07
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville M Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
Sample Condition Client Name: �n Project f WO# : 92539166
Upon Receipt. lI r u■ ur■ilt I n u l oil
❑ Commercial ❑Pace ❑Other: 11 ■ ii■ nr■ni 1 n 1111 all
92539166
Custody Seal Present? ❑Yes 5N_ Seals Intact? ❑Yes &lo
- ....._ .-_ -6 r' .
Date/Initials Personmrnirng tu`ntents:
Packing Material: (Bubble Wrap OJ3ubbie Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: [:]Yes [:]No BN/A
I�IRGuniD: Wet ❑Blue ❑None
92TO64 Type of Ice:
Correction Factor:
Cooler Temp: Add/Subtract (°C) _0,1 Temp shou Id be above freezing to 6'C
(� l ❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected(' ): i �`j has begun
USDA Regulated Soil ( N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
i-4.... = _ i­ I...ffno 14na -jnii And Pnprtn Ritnl7 Fl Yp; it No
Comments/Discrepa ncy:
Chain of Custody Present?
'g%es
[!]NO
❑N/A
1.
Samples Arrived within Bold Time?
B �
❑No
❑N/A
2,
Short Hold Time Analysis (<72 hr.)?
[` yes
[:]NO.
❑N/A
3. - f CJ/}(2 r e 1- U f_it�
Rush Turn Around Time Requested?
❑Yes
� o
❑N/A
4.
Sufficient Volume?
- Yes
❑No
❑N/A
5.
Correct Containers Used?
`gYes
[:]No
❑N/A
6.
-Pace Containers Used?
C(fies
❑No
❑N/A
Containers Intact?
EKES
❑No
[]NIA
7,
Dissolved analysis: Samples Field Filtered?
❑Yes
[30o
❑N/A
8.
Sample Labels Match COC?
Ves
❑No
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
❑Yes
r7No
❑N/A
10.
Trip Blank Present?
❑Yes
lja'elo
❑N/A
11,
Trip Blank Custody Seals Present?
❑Yes
ZNo-
❑N/A
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Lot lD of split containers:
Date:
Date:
Field Data Required? Dyes ❑No
Page 29 of 34

Document Name:
-Sample Condition Upon Receii
%.�aceAnalytical Document No.:
F-CAR-CS-033-Rev.07
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Document Revised: October 28, 2020
-- — Page-2-of 2
Issuing Authority:
Pace Carolinas Quality Office
Project W0# ; 92539166
PM: KRG Due Date: 05/26/21
CLIENT: 97-CNA
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adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
out of hold, incorrect preservative, out of temp, incorrect containers.
Page 30 of 34

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Document Name:
Document Revised: October 28, 2020
_ ...__....�
aceAnalytical
Sample Condition —Upon Receipt(SCUR)
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.07
Pace Carolinas Quality Office
Laboratory receiving samples-,
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [! Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
❑
Commercial
Client Name: WO# : 92539189
jn}- _ Project #:
CC
❑Other: it II! 1�1
92539189
Custody Seal Present? ❑Yes L�Go Seals Intact? Dyes Wo
Date/ rmtia s erson xamini"�`ning i~antents:
Packing Material: VBubble Wrap L>SBubble Bags LJNone LJ Other Biological Tissue Frozen?
Thermometer: ❑Yes ❑No `QN/A
IR Gun ID: 92TO64 Type of Ice: QWet []Blue ❑None
Correction Factor:
Cooler Tamp: � � Add/Subtract (°C) -0,1 Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (*Q L r _ has begun
USDA Regulated Soil { N/A, water sample]
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
MY.-, l—IN. including Hawaii and Puerto Rico)? RYes nNo
Comments/Discrepancy:
Chain of Custody Present?
Yes
[:]NO
❑N/A
1.
Samples Arrived within Hold Time?
-es
[:]NO
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
Ry.es
❑No
❑N/A
3. 0`0Ur1 f-e S
Rush Turn Around Time Requested?
❑Yes
®No
❑N/A
4.
Sufficient Volume?
LOYes
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
V es
Rles
[]No
❑No
❑N/A
❑N/A
6.
Containers Intact?
®Yes
[]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered? []Yes
t[�No
❑N/A
S.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis
AYes
1 e
Matrix:
❑No
I—] N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
jgNo
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
[�JNo
Mo
[]N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Date/Time:
Lot 10 ofscHtcontainers:
Date:
Field Data Required? []Yes ❑No
Project Manager SRF Review: Date:
Page 32 of 34

Document Name:
Document Revised: October 28, 2020
- -
,.- EeMaVical
- Sample Condition Upon Receipt(S€UR)
- - - -Page-2 of 2 — --
Document No.:
F-CAR-05-o33-Rev.D7
Issuing Authority:
Pace Carolinas Quahty Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water} DOC, LLHg
"Bottom half of box is to list number of bottles
Project f WQ# : 92539189
PM: KRG Due Date: 05/26/21
CLIENT: 97—CNA
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Lot #
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy or mis rorm win ee sent to the worth Carolina utHPJK Certmrication unice (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 33 of 34

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Page 34 of 34

/" .=CQM AECOM 404.965.9600 tel
One Midtown Plaza 404.965.9605 fax
1360 Peachtree St. N.E.
Suite 500
Atlanta, GA 30309
Memorandum
To Jing Zhou — AECOM Atlanta Page 1 of 4
CC
Subject Level 2 Data Validation for Needmore Road Landfill
From Robert Davis — AECOM Atlanta
Date March 11, 2022
Limited validation of the analytical data for the water samples was performed on one data package
received from Pace Analytical Services, Inc. in Greenwood, South Carolina. The samples were
collected on May 17, 2021, at the Needmore Road Landfill in North Carolina.
The data were reviewed for conformance to method specifications and the project guidance
document: Supplemental Characterization and Long -Term Monitoring (AECOM, July 2010 Revision
2). Data qualifiers were applied in accordance with the validation criteria set forth in USEPA
Contract Laboratory Program (CLP) National Functional Guidelines for Organic Superfund Methods
Data Review EPA-540-R-20-005, November 2020 and USEPA National Functional Guidelines for
Inorganic Superfund Methods Data Review, EPA-542-R-20-006, November 2020, as they apply to
the analytical methods employed.
Field duplicate relative percent difference (RPD) review and applicable control limits were taken
from the USEPA Region 1, New England Data Validation Functional Guidelines for Evaluating
Environmental Analyses, December 1996.
The following methods were requested on the chain -of -custody (COC) records:
• Method 8260D SIM — Volatiles by Gas Chromatography/Mass Spectrometry (GC/MS) in
SIM mode;
• Method 8270E
— Semivolatiles by GC/MS;
• Method 8015M
— Ethylene Glycol by GC;
• Method 2320B
— Alkalinity;
• Method 353.2 —
Nitrate and Nitrite;
• SM450OP-E — Orthophosphate; and
• Method 9056A
— Sulfate by Ion Chromatography (IC).

AECOM
2
Review Elements
Sample data were reviewed for the following quality control parameters:
• Agreement of analyses conducted with COC requests;
• Holding times and sample preservation;
• GC/MS hardware tunes, initial and continuing calibrations;
• Method blanks/trip blanks;
• Surrogate recoveries;
• Laboratory control sample (LCS) recoveries;
• Matrix spike/matrix spike duplicate (MS/MSD) recoveries; and
• Field duplicate precision results.
Samples
Environmental Field Management (EFM) personnel collected the following water samples from the
Needmore Road Landfill in North Carolina, as reported under the Pace Analytical Services, Inc. job
number:
92539166
Lab ID
Sample ID
Lab ID
Sample ID
92539166001
B-12-051721
90539189004
B-23B-051721
92539166002
B-10-051721
90539189005
B-17C-051721
92539166003
B-99-051721
90539189006
B-22B-051721
90539189001
B-01-051721
90539189007
B-24A-051721
90539189002
B-09C-051721
90539189008
SW-5-051721
90539189003
B-23A-051721
90539189009
CSW-1-051721
Analytical Results
In general, the data results are valid as reported and may be used for decision -making purposes.
None of the samples required data qualification.
DISCUSSION
Agreement of Analyses Conducted with Chain -of -Custody (COC) Requests
Sample reports were checked to verify agreement with the COC request. No discrepancies were
noted.
Holding Times and Sample Preservation
All samples were analyzed within the holding times required by the methods.
All coolers were received within the optimal range of 4±2 degrees Celsius (°C).
All samples were properly preserved as specified by the methods.

AECOM
GC/MS Tunes, Initial and Continuing Calibrations
GUMS tuning and calibration summaries were not submitted for validation in this Level II data
package.
Method Blanks/Trip Blanks
No analytes were detected at concentrations exceeding the reporting limits for the method blanks.
Trip blanks were not submitted with sample set. Contamination picked up in storage or transit could
not be evaluated.
Surrogate Recoveries
The surrogate recoveries were acceptable for all analyses.
Laboratory Control Sample (LCS) Recoveries
LCS recoveries for all of the analyses were within the quality control limits.
Matrix Spike/Matrix Spike Duplicate (MS/MSD) Recoveries
MS/MSDs that were performed on non -project samples were not evaluated because matrix
similarity to project samples could not be assumed.
The MS/MSD recoveries on client samples were all within the advisory limits with the following
exception:
• Method SM 2320B-2011: The alkalinity recovery MS/MSD recoveries were outside of the
quality control limits in sample B-12-051721. The spike amount was less than 25% of the
sample concentration; therefore, data qualification was not required.
Field Duplicate Precision Results
A field duplicate was collected on sample B-10-051721. See Table 1 for the calculated RPDs for all
compounds for which there were detections. The RPDs between the original and field duplicate
were all within the advisory limits of 0-30%. Field sampling/laboratory precision and sample
homogeneity were acceptable. No data qualifications were required.

AECOM
Table 1
Field Precision
Method
Compound
B-10-051721
B-99-051721
Units
% RPD
8270E
Biphenyl
127
119
pg/L
6.5
8270E
Diphenyl ether
1210
1170
pg/L
3.4
8260D
1,4-Dioxane
193
181
pg/L
6.4
2320B
Alkalinity
475
473
mg/L
0.42
353.2
Nitrate
0.046
0.061
mg/L
28
353.2
Nitrite
0.062
0.058
mg/L
6.7
SM450OP-E
Orthophosphate
0.34
0.39
mg/L
14
Notes:
% RPD: Relative percent difference between the primary sample result and the sample duplicate result.
pg/L: micrograms per liter
mg/L: milligrams per liter

lceAnalyilcal®
www.pacelabs.cem
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
December 21, 2021
Jing Zhou
AECOM
1360 Peachtree St.
Suite 500
Atlanta, GA 30309
RE: Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Dear Jing Zhou:
Enclosed are the analytical results for sample(s) received by the laboratory on November 30, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Gulf Coast
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
• Pace Analytical Services - Indianapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
-�Jax
Bonnie Vang
[e-mail]
[phone]
Project Manager
Enclosures
cc: Rob Davis. AECOM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 93

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Pace Analytical Services Indianapolis
7726 Moller Road, Indianapolis, IN 46268
Illinois Accreditation #: 200074
Indiana Drinking Water Laboratory #: C-49-06
Kansas/TNI Certification #: E-10177
Kentucky UST Agency Interest #: 80226
Kentucky WW Laboratory ID M 98019
CERTIFICATIONS
Michigan Drinking Water Laboratory #9050
Ohio VAP Certified Laboratory #: CL0065
Oklahoma Laboratory #: 9204
Texas Certification #: T104704355
Wisconsin Laboratory #: 999788130
USDA Soil Permit #: P330-19-00257
Pace Analytical Gulf Coast
7979 Innovation Park Drive, Baton Rouge, LA 70820
North Dakota Certification #: R-195
Arkansas Certification #: 88-0655
Oklahoma Certification #: 2019-101
DoD ELAP Certification #: L18-597
South Carolina Certification #: 73006001
Florida Certification #: E87854
Texas Certification #: T104704178-19-11
Illinois Certification #: 004585
USDA Soil Permit # P330-19-00209
Kansas Certification #: E-10354
Virginia Certification #: 460215
Louisiana/LELAP Certification M 01955
Washington Certification #: C929
North Carolina Certification #: 618
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Drinking Water Cert. #: 99006003
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Louisiana DoH Drinking Water #: LA029
South Carolina Laboratory ID: 99006
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
South Carolina Laboratory ID: 99030
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 40
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification #: 37738
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
NRLF-NOVEMBER 2021
92574833
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92574833001
TRIP BLANK-01-112921
EPA 8260D
CL
53
PASI-C
92574833002
SW-7-112921
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
8
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92574833003
SW-5-112921
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92574833004
SW-3-112921
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92574833005
SW-8-112921
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92574833006
B-24B-112921
SM 4500-P E-2011
MWF
1
PASI-E
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
EPA 9056A
CDC
1
PASI-A
92574833007
B-24A-112921
SM 4500-P E-2011
MWF
1
PASI-E
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
EPA 9056A
CDC
1
PASI-A
92574833008
B-23A-112921
SM 4500-P E-2011
MWF
1
PASI-E
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
AWE
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
SAS
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MDW
5
PASI-A
AM23G
SLL2
1
GCLA
92574833009
B-23B-112921
SM 4500-P E-2011
MWF
1
PASI-E
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
AWE
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
SAS
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MDW
5
PASI-A
AM23G
SLL2
1
GCLA
92574833010
B-17C-112921
SM 4500-P E-2011
MWF
1
PASI-E
RSK-175
AWE
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MDW
5
PASI-A
AM23G
SLL2
1
GCLA
92574833011
B-12-112921
SM 4500-P E-2011
MWF
1
PASI-E
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
EPA 9056A
CDC
1
PASI-A
92574833012
B-22B-113021
SM 4500-P E-2011
MWF
1
PASI-E
RSK-175
AWE
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MDW
5
PASI-A
AM23G
SLL2
1
GCLA
92574833013
B-17B-113021
SM 4500-P E-2011
MWF
1
PASI-E
RSK-175
AWE
3
GCLA
RSK-175
BMR
1
GCLA
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
NRLF-NOVEMBER 2021
92574833
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MDW
5
PASI-A
AM23G
SLL2
1
GCLA
92574833014
B-22A-113021
SM 4500-P E-2011
MWF
1
PASI-E
RSK-175
AWE
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MDW
5
PASI-A
AM23G
SLL2
1
GCLA
92574833015
B-09C-113021
SM 4500-P E-2011
MWF
1
PASI-E
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D
SAS
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
EPA 9056A
CDC
1
PASI-A
92574833016
B-21B-113021
SM 4500-P E-2011
MWF
1
PASI-E
EPA 8260D Mod.
LMB
3
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
EPA 9056A
CDC
1
PASI-A
92574833017
B-99C-113021
EPA 8270E
PKS
5
PASI-C
EPA 8260D
SAS
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92574833018
B-23A-112921 H2
AM20GAX
CWB
1
GCLA
92574833019
B-23B-112921 H2
AM20GAX
CWB
1
GCLA
92574833020
B-17C-112921 H2
AM20GAX
CWB
1
GCLA
92574833021
B-22B-113021 H2
AM20GAX
CWB
1
GCLA
92574833022
B-17B-113021 H2
AM20GAX
CWB
1
GCLA
92574833023
B-22A-113021 H2
AM20GAX
CWB
1
GCLA
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
GCLA =
Pace Analytical Gulf Coast
PASI-A
= Pace Analytical Services - Asheville
PASI-C
= Pace Analytical Services - Charlotte
PASI-E
= Pace Analytical Services - Eden
PASI-I =
Pace Analytical Services - Indianapolis
REPORT OF LABORATORY ANALYSIS
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Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: TRIP BLANK-01-112921
Parameters
8260D MSV Low Level Landfill
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene (Cumene)
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
ANALYTICAL RESULTS
Lab ID: 92574833001 Collected: 11/29/21 00:00 Received: 11/30/21 12:10 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
12/03/2105:50
67-64-1
ND
ug/L
1.0
1
12/03/2105:50
71-43-2
ND
ug/L
1.0
1
12/03/2105:50
74-97-5
ND
ug/L
1.0
1
12/03/2105:50
75-27-4
ND
ug/L
1.0
1
12/03/2105:50
75-25-2
ND
ug/L
2.0
1
12/03/2105:50
74-83-9
ND
ug/L
5.0
1
12/03/2105:50
78-93-3
ND
ug/L
2.0
1
12/03/2105:50
75-15-0
ND
ug/L
1.0
1
12/03/2105:50
56-23-5
ND
ug/L
1.0
1
12/03/2105:50
108-90-7
ND
ug/L
1.0
1
12/03/2105:50
75-00-3
ND
ug/L
1.0
1
12/03/2105:50
67-66-3
ND
ug/L
1.0
1
12/03/2105:50
74-87-3
ND
ug/L
1.0
1
12/03/2105:50
110-82-7
ND
ug/L
2.0
1
12/03/2105:50
96-12-8
ND
ug/L
1.0
1
12/03/2105:50
124-48-1
ND
ug/L
1.0
1
12/03/2105:50
106-93-4
ND
ug/L
1.0
1
12/03/2105:50
95-50-1
ND
ug/L
1.0
1
12/03/2105:50
541-73-1
ND
ug/L
1.0
1
12/03/2105:50
106-46-7
ND
ug/L
1.0
1
12/03/2105:50
75-71-8
ND
ug/L
1.0
1
12/03/2105:50
75-34-3
ND
ug/L
1.0
1
12/03/2105:50
107-06-2
ND
ug/L
1.0
1
12/03/2105:50
75-35-4
ND
ug/L
1.0
1
12/03/2105:50
156-59-2
ND
ug/L
1.0
1
12/03/2105:50
156-60-5
ND
ug/L
1.0
1
12/03/2105:50
78-87-5
ND
ug/L
1.0
1
12/03/2105:50
10061-01-5
ND
ug/L
1.0
1
12/03/2105:50
10061-02-6
ND
ug/L
1.0
1
12/03/2105:50
100-41-4
ND
ug/L
5.0
1
12/03/2105:50
591-78-6
ND
ug/L
1.0
1
12/03/2105:50
98-82-8
ND
ug/L
10.0
1
12/03/2105:50
79-20-9
ND
ug/L
10.0
1
12/03/2105:50
108-87-2
ND
ug/L
5.0
1
12/03/2105:50
75-09-2
ND
ug/L
5.0
1
12/03/2105:50
108-10-1
ND
ug/L
1.0
1
12/03/2105:50
1634-04-4
ND
ug/L
1.0
1
12/03/2105:50
100-42-5
ND
ug/L
1.0
1
12/03/2105:50
79-34-5
ND
ug/L
1.0
1
12/03/2105:50
127-18-4
ND
ug/L
1.0
1
12/03/2105:50
108-88-3
ND
ug/L
1.0
1
12/03/2105:50
87-61-6
ND
ug/L
1.0
1
12/03/2105:50
120-82-1
ND
ug/L
1.0
1
12/03/2105:50
71-55-6
ND
ug/L
1.0
1
12/03/2105:50
79-00-5
ND
ug/L
1.0
1
12/03/2105:50
79-01-6
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: TRIP BLANK-01-112921
Parameters
Lab ID: 92574833001 Collected: 11/29/21 00:00
Results Units Report Limit DF
Received: 11/30/21 12:10 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Trichlorofluoromethane
ND ug/L
1.0
1
12/03/21 05:50
75-69-4
1,1,2-Trichlorotrifluoroethane
ND ug/L
1.0
1
12/03/21 05:50
76-13-1
Vinyl chloride
ND ug/L
1.0
1
12/03/21 05:50
75-01-4
Xylene (Total)
ND ug/L
1.0
1
12/03/21 05:50
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
12/03/21 05:50
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
12/03/21 05:50
17060-07-0
Toluene-d8(S)
100 %
70-130
1
12/03/21 05:50
2037-26-5
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: SW-7-112921 Lab ID: 92574833002 Collected: 11/29/21 12:00 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015M Glycols in water Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol ND mg/L 5.0 1
8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 12/21 /2021 11:18 AM
12/06/21 15:42 107-21-1
ND
ug/L
9.1
1
12/01/2105:25
12/01/2117:48
92-52-4
ND
ug/L
9.1
1
12/01/2105:25
12/01/2117:48
101-84-8
48
%
10-144
1
12/01 /21 05:25
12/01 /21 17:48
4165-60-0
42
%
10-130
1
12/01 /21 05:25
12/01 /21 17:48
321-60-8
70
%
34-163
1
12/01 /21 05:25
12/01 /21 17:48
1718-51-0
18
%
10-130
1
12/01 /21 05:25
12/01 /21 17:48
13127-88-3
14
%
10-130
1
12/01/2105:25
12/01/2117:48
367-12-4
21
%
10-144
1
12/01 /21 05:25
12/01 /21 17:48
118-79-6
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L 2.0 1
114 % 70-130 1
119 % 66-133 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
12/01 /21 00:42 123-91-1
12/01 /21 00:42 17060-07-0
12/01 /21 00:42 2037-26-5
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ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: SW-5-112921
Lab ID: 92574833003 Collected: 11/29/21
12:19
Received: 11/30/21 12:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
12/06/21 15:51
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 10.0
1
12/01/21 05:25
12/01/21 19:03
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 10.0
1
12/01/21 05:25
12/01/21 19:03
101-84-8
Surrogates
Nitrobenzene-d5(S)
88 % 10-144
1
12/01/21 05:25
12/01/21 19:03
4165-60-0
2-Fluorobiphenyl (S)
73 % 10-130
1
12/01/21 05:25
12/01/21 19:03
321-60-8
Terphenyl-d14 (S)
84 % 34-163
1
12/01/21 05:25
12/01/21 19:03
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
12/01/21 01:01
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
117 % 70-130
1
12/01/21 01:01
17060-07-0
Toluene-d8 (S)
120 % 66-133
1
12/01/21 01:01
2037-26-5
REPORT OF LABORATORY ANALYSIS
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Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 93

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ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: SW-3-112921
Lab ID: 92574833004 Collected: 11/29/21
12:34
Received: 11/30/21 12:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
12/06/21 16:00
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 9.1
1
12/01/21 05:25
12/01/21 19:29
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 9.1
1
12/01/21 05:25
12/01/21 19:29
101-84-8
Surrogates
Nitrobenzene-d5(S)
81 % 10-144
1
12/01/21 05:25
12/01/21 19:29
4165-60-0
2-Fluorobiphenyl (S)
71 % 10-130
1
12/01/21 05:25
12/01/21 19:29
321-60-8
Terphenyl-d14 (S)
97 % 34-163
1
12/01/21 05:25
12/01/21 19:29
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
12/01/21 01:21
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
115 % 70-130
1
12/01/21 01:21
17060-07-0
Toluene-d8 (S)
119 % 66-133
1
12/01/21 01:21
2037-26-5
REPORT OF LABORATORY ANALYSIS
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[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: SW-8-112921
Lab ID: 92574833005 Collected: 11/29/21
13:10
Received: 11/30/21 12:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
12/06/21 16:09
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 8.3
1
12/01/21 05:25
12/01/21 19:54
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 8.3
1
12/01/21 05:25
12/01/21 19:54
101-84-8
Surrogates
Nitrobenzene-d5(S)
80 % 10-144
1
12/01/21 05:25
12/01/21 19:54
4165-60-0
2-Fluorobiphenyl (S)
63 % 10-130
1
12/01/21 05:25
12/01/21 19:54
321-60-8
Terphenyl-d14 (S)
92 % 34-163
1
12/01/21 05:25
12/01/21 19:54
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
12/01/21 01:40
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
115 % 70-130
1
12/01/21 01:40
17060-07-0
Toluene-d8 (S)
119 % 66-133
1
12/01/21 01:40
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 93

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-24B-112921 Lab ID: 92574833006 Collected: 11/29/21 09:48 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.22 mg/L
0.050
1
12/01/21 13:44
H3
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
8.3
1 12/01/21 05:25
12/01/21 17:59
92-52-4
Diphenyl ether (Phenyl ether)
12.0 ug/L
8.3
1 12/01/21 05:25
12/01/21 17:59
101-84-8
Surrogates
Nitrobenzene-d5(S)
78 %
10-144
1 12/01/21 05:25
12/01/21 17:59
4165-60-0
2-Fluorobiphenyl (S)
66 %
10-130
1 12/01/21 05:25
12/01/21 17:59
321-60-8
Terphenyl-d14 (S)
86 %
34-163
1 12/01/21 05:25
12/01/21 17:59
1718-51-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
12/03/21 12:30
67-64-1
Benzene
ND ug/L
1.0
1
12/03/21 12:30
71-43-2
Bromochloromethane
ND ug/L
1.0
1
12/03/21 12:30
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
12/03/21 12:30
75-27-4
Bromoform
ND ug/L
1.0
1
12/03/21 12:30
75-25-2
Bromomethane
ND ug/L
2.0
1
12/03/21 12:30
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
12/03/21 12:30
78-93-3
Carbon disulfide
ND ug/L
2.0
1
12/03/21 12:30
75-15-0
Carbon tetrachloride
ND ug/L
1.0
1
12/03/21 12:30
56-23-5
Chlorobenzene
ND ug/L
1.0
1
12/03/21 12:30
108-90-7
Chloroethane
5.1 ug/L
1.0
1
12/03/21 12:30
75-00-3
Chloroform
ND ug/L
1.0
1
12/03/21 12:30
67-66-3
Chloromethane
ND ug/L
1.0
1
12/03/21 12:30
74-87-3
Cyclohexane
ND ug/L
1.0
1
12/03/21 12:30
110-82-7
1,2-Dibromo-3-chloropropane
ND ug/L
2.0
1
12/03/21 12:30
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
12/03/21 12:30
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
12/03/21 12:30
106-93-4
1,2-Dichlorobenzene
ND ug/L
1.0
1
12/03/21 12:30
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
12/03/21 12:30
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
12/03/21 12:30
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
12/03/21 12:30
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
1
12/03/21 12:30
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
12/03/21 12:30
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
12/03/21 12:30
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
12/03/21 12:30
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
12/03/21 12:30
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
12/03/21 12:30
78-87-5
cis-1,3-Dichloropropene
ND ug/L
1.0
1
12/03/21 12:30
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
12/03/21 12:30
10061-02-6
Ethylbenzene
ND ug/L
1.0
1
12/03/21 12:30
100-41-4
2-Hexanone
ND ug/L
5.0
1
12/03/21 12:30
591-78-6
Isopropylbenzene (Cumene)
ND ug/L
1.0
1
12/03/21 12:30
98-82-8
Methyl acetate
ND ug/L
10.0
1
12/03/21 12:30
79-20-9
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM
without the written consent of Pace Analytical Services, LLC.
Page 13 of 93

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: 13-2413-112921 Lab ID: 92574833006 Collected: 11/29/21 09:48 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Methylcyclohexane
ND ug/L
10.0
1
12/03/21 12:30
108-87-2
Methylene Chloride
ND ug/L
5.0
1
12/03/21 12:30
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
12/03/21 12:30
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
12/03/21 12:30
1634-04-4
Styrene
ND ug/L
1.0
1
12/03/21 12:30
100-42-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
12/03/21 12:30
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
12/03/21 12:30
127-18-4
Toluene
ND ug/L
1.0
1
12/03/21 12:30
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
12/03/21 12:30
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
12/03/21 12:30
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
12/03/21 12:30
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
12/03/21 12:30
79-00-5
Trichloroethene
ND ug/L
1.0
1
12/03/21 12:30
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
12/03/21 12:30
75-69-4
1,1,2-Trichlorotrifluoroethane
ND ug/L
1.0
1
12/03/21 12:30
76-13-1
Vinyl chloride
1.1 ug/L
1.0
1
12/03/21 12:30
75-01-4
Xylene (Total)
ND ug/L
1.0
1
12/03/21 12:30
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
12/03/21 12:30
460-00-4
1,2-Dichloroethane-d4 (S)
100 %
70-130
1
12/03/21 12:30
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
12/03/21 12:30
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
120 ug/L
4.0
2
12/01/21 02:38
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
114 %
70-130
2
12/01/21 02:38
17060-07-0
Toluene-d8(S)
114 %
66-133
2
12/01/21 02:38
2037-26-5
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
12/01/21 00:50
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
12/01/21 00:50
14797-65-0
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
12/01/2120:33
14808-79-8
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 93

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-24A-112921 Lab ID: 92574833007 Collected: 11/29/21 10:30 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.36 mg/L
0.050
1
12/01/21 13:44
H3
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
8.3
1 12/01/21 05:25
12/01/21 18:27
92-52-4
Diphenyl ether (Phenyl ether)
9.1 ug/L
8.3
1 12/01/21 05:25
12/01/21 18:27
101-84-8
Surrogates
Nitrobenzene-d5(S)
84 %
10-144
1 12/01/21 05:25
12/01/21 18:27
4165-60-0
2-Fluorobiphenyl (S)
74 %
10-130
1 12/01/21 05:25
12/01/21 18:27
321-60-8
Terphenyl-d14 (S)
87 %
34-163
1 12/01/21 05:25
12/01/21 18:27
1718-51-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
12/03/21 12:48
67-64-1
Benzene
ND ug/L
1.0
1
12/03/21 12:48
71-43-2
Bromochloromethane
ND ug/L
1.0
1
12/03/21 12:48
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
12/03/21 12:48
75-27-4
Bromoform
ND ug/L
1.0
1
12/03/21 12:48
75-25-2
Bromomethane
ND ug/L
2.0
1
12/03/21 12:48
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
12/03/21 12:48
78-93-3
Carbon disulfide
ND ug/L
2.0
1
12/03/21 12:48
75-15-0
Carbon tetrachloride
ND ug/L
1.0
1
12/03/21 12:48
56-23-5
Chlorobenzene
ND ug/L
1.0
1
12/03/21 12:48
108-90-7
Chloroethane
3.9 ug/L
1.0
1
12/03/21 12:48
75-00-3
Chloroform
ND ug/L
1.0
1
12/03/21 12:48
67-66-3
Chloromethane
ND ug/L
1.0
1
12/03/21 12:48
74-87-3
Cyclohexane
ND ug/L
1.0
1
12/03/21 12:48
110-82-7
1,2-Dibromo-3-chloropropane
ND ug/L
2.0
1
12/03/21 12:48
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
12/03/21 12:48
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
12/03/21 12:48
106-93-4
1,2-Dichlorobenzene
ND ug/L
1.0
1
12/03/21 12:48
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1
12/03/21 12:48
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
12/03/21 12:48
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
1
12/03/21 12:48
75-71-8
1,1-Dichloroethane
7.4 ug/L
1.0
1
12/03/21 12:48
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
1
12/03/21 12:48
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
1
12/03/21 12:48
75-35-4
cis-1,2-Dichloroethene
ND ug/L
1.0
1
12/03/21 12:48
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
12/03/21 12:48
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1
12/03/21 12:48
78-87-5
cis-1,3-Dichloropropene
ND ug/L
1.0
1
12/03/21 12:48
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
12/03/21 12:48
10061-02-6
Ethylbenzene
ND ug/L
1.0
1
12/03/21 12:48
100-41-4
2-Hexanone
ND ug/L
5.0
1
12/03/21 12:48
591-78-6
Isopropylbenzene (Cumene)
ND ug/L
1.0
1
12/03/21 12:48
98-82-8
Methyl acetate
ND ug/L
10.0
1
12/03/21 12:48
79-20-9
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM
without the written consent of Pace Analytical Services, LLC.
Page 15 of 93

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-24A-112921 Lab ID: 92574833007 Collected: 11/29/21 10:30 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Methylcyclohexane
ND ug/L
10.0
1
12/03/21 12:48
108-87-2
Methylene Chloride
ND ug/L
5.0
1
12/03/21 12:48
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
1
12/03/21 12:48
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
1
12/03/21 12:48
1634-04-4
Styrene
ND ug/L
1.0
1
12/03/21 12:48
100-42-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
12/03/21 12:48
79-34-5
Tetrachloroethene
ND ug/L
1.0
1
12/03/21 12:48
127-18-4
Toluene
ND ug/L
1.0
1
12/03/21 12:48
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
1
12/03/21 12:48
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
1
12/03/21 12:48
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
1
12/03/21 12:48
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
12/03/21 12:48
79-00-5
Trichloroethene
ND ug/L
1.0
1
12/03/21 12:48
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
12/03/21 12:48
75-69-4
1,1,2-Trichlorotrifluoroethane
ND ug/L
1.0
1
12/03/21 12:48
76-13-1
Vinyl chloride
1.6 ug/L
1.0
1
12/03/21 12:48
75-01-4
Xylene (Total)
ND ug/L
1.0
1
12/03/21 12:48
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100 %
70-130
1
12/03/21 12:48
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
12/03/21 12:48
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
12/03/21 12:48
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
248 ug/L
5.0
2.5
12/01/21 02:58
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
109 %
70-130
2.5
12/01/21 02:58
17060-07-0
Toluene-d8 (S)
112 %
66-133
2.5
12/01/21 02:58
2037-26-5
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
12/01/21 00:56
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
12/01/21 00:56
14797-65-0
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
12/01/2121:19
14808-79-8
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 93

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-23A-112921 Lab ID: 92574833008 Collected: 11/29/21 14:14 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
8015M Glycols in water
Ethylene glycol
Biodegradation Indicator Gases
Methane
Ethane
Ethene
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV Low Level Landfill
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
Date: 12/21 /2021 11:18 AM
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
0.63 mg/L
0.12
2.5
12/01 /21 14:12
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
ND mg/L
25.0
5
12/07/2114:57
107-21-1 D3
Analytical Method: RSK-175
Pace Analytical Gulf Coast
4100 ug/L
5.0
1
12/06/21 19:39
74-82-8
ND ug/L
1.0
1
12/06/2119:39
74-84-0
ND ug/L
1.0
1
12/06/2119:39
74-85-1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
463000 ug/L
45000
50
12/10/2112:29
124-38-9
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
ND ug/L
9.1
1
12/01/2105:25
12/01/2118:56
92-52-4
47.9 ug/L
9.1
1
12/01/2105:25
12/01/2118:56
101-84-8
62 %
10-144
1
12/01 /21 05:25
12/01 /21 18:56
4165-60-0
131 %
10-130
1
12/01 /21 05:25
12/01 /21 18:56
321-60-8 SO
83 %
34-163
1
12/01 /21 05:25
12/01 /21 18:56
1718-51-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
5860 ug/L
625
25
12/04/2107:19
67-64-1
ND ug/L
25.0
25
12/04/2107:19
71-43-2
ND ug/L
25.0
25
12/04/2107:19
74-97-5
ND ug/L
25.0
25
12/04/2107:19
75-27-4
ND ug/L
25.0
25
12/04/2107:19
75-25-2
ND ug/L
50.0
25
12/04/2107:19
74-83-9
836 ug/L
125
25
12/04/2107:19
78-93-3
ND ug/L
50.0
25
12/04/2107:19
75-15-0
ND ug/L
25.0
25
12/04/2107:19
56-23-5
ND ug/L
25.0
25
12/04/2107:19
108-90-7
ND ug/L
25.0
25
12/04/2107:19
75-00-3
ND ug/L
25.0
25
12/04/2107:19
67-66-3
ND ug/L
25.0
25
12/04/2107:19
74-87-3
ND ug/L
25.0
25
12/04/2107:19
110-82-7
ND ug/L
50.0
25
12/04/2107:19
96-12-8
ND ug/L
25.0
25
12/04/2107:19
124-48-1
ND ug/L
25.0
25
12/04/2107:19
106-93-4
ND ug/L
25.0
25
12/04/2107:19
95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 93

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-23A-112921 Lab ID: 92574833008 Collected: 11/29/21 14:14 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/L
25.0
25
12/04/21 07:19
541-73-1
1,4-Dichlorobenzene
ND
ug/L
25.0
25
12/04/21 07:19
106-46-7
Dichlorodifluoromethane
ND
ug/L
25.0
25
12/04/21 07:19
75-71-8
1,1-Dichloroethane
37.1
ug/L
25.0
25
12/04/21 07:19
75-34-3
1,2-Dichloroethane
ND
ug/L
25.0
25
12/04/21 07:19
107-06-2
1,1-Dichloroethene
ND
ug/L
25.0
25
12/04/21 07:19
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
25.0
25
12/04/21 07:19
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
25.0
25
12/04/21 07:19
156-60-5
1,2-Dichloropropene
ND
ug/L
25.0
25
12/04/21 07:19
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
25.0
25
12/04/21 07:19
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
25.0
25
12/04/21 07:19
10061-02-6
Ethylbenzene
ND
ug/L
25.0
25
12/04/21 07:19
100-41-4
2-Hexanone
ND
ug/L
125
25
12/04/21 07:19
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
25.0
25
12/04/21 07:19
98-82-8
Methyl acetate
ND
ug/L
250
25
12/04/21 07:19
79-20-9
Methylcyclohexane
ND
ug/L
250
25
12/04/21 07:19
108-87-2
Methylene Chloride
ND
ug/L
125
25
12/04/21 07:19
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
125
25
12/04/21 07:19
108-10-1
Methyl-tert-butyl ether
ND
ug/L
25.0
25
12/04/21 07:19
1634-04-4
Styrene
ND
ug/L
25.0
25
12/04/21 07:19
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
25.0
25
12/04/21 07:19
79-34-5
Tetrachloroethene
ND
ug/L
25.0
25
12/04/21 07:19
127-18-4
Toluene
ND
ug/L
25.0
25
12/04/21 07:19
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
25.0
25
12/04/21 07:19
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
25.0
25
12/04/21 07:19
120-82-1
1,1,1-Trichloroethane
ND
ug/L
25.0
25
12/04/21 07:19
71-55-6
1,1,2-Trichloroethane
ND
ug/L
25.0
25
12/04/21 07:19
79-00-5
Trichloroethene
ND
ug/L
25.0
25
12/04/21 07:19
79-01-6
Trichlorofluoromethane
ND
ug/L
25.0
25
12/04/21 07:19
75-69-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
25.0
25
12/04/21 07:19
76-13-1
Vinyl chloride
ND
ug/L
25.0
25
12/04/21 07:19
75-01-4
Xylene (Total)
ND
ug/L
25.0
25
12/04/21 07:19
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
105
%
70-130
25
12/04/21 07:19
460-00-4
1,2-Dichloroethane-d4 (S)
105
%
70-130
25
12/04/21 07:19
17060-07-0
Toluene-d8(S)
103
%
70-130
25
12/04/21 07:19
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
3420
ug/L
100
50
12/01/21 03:17
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
113
%
70-130
50
12/01/21 03:17
17060-07-0
Toluene-d8(S)
112
%
66-133
50
12/01/21 03:17
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-23A-112921
Lab ID: 92574833008 Collected:
11/29/21 14:14
Received: 11/30/21 12:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
12/01/21 00:58
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
12/01/21 00:58
14797-65-0
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
5.9 mg/L
1.0
1
12/01/2122:05
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
2710 mg/L
250
250
12/01/21 21:51
7440-44-0
Total Organic Carbon
2720 mg/L
250
250
12/01/21 21:51
7440-44-0
Total Organic Carbon
2730 mg/L
250
250
12/01/21 21:51
7440-44-0
Total Organic Carbon
2690 mg/L
250
250
12/01/21 21:51
7440-44-0
Mean Total Organic Carbon
2710 mg/L
250
250
12/01/21 21:51
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
1400 mg/L
250
500
12/13/21 17:40
64-19-7
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-2313-112921 Lab ID: 92574833009 Collected: 11/29/21 15:46 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
8015M Glycols in water
Ethylene glycol
Biodegradation Indicator Gases
Methane
Ethane
Ethene
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV Low Level Landfill
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
Date: 12/21 /2021 11:18 AM
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
0.50 mg/L
0.25
5
12/01 /21 14:23
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
ND mg/L
25.0
5
12/07/2115:16
107-21-1 D3
Analytical Method: RSK-175
Pace Analytical Gulf Coast
7500 ug/L
5.0
1
12/06/21 19:50
74-82-8
ND ug/L
1.0
1
12/06/2119:50
74-84-0
ND ug/L
1.0
1
12/06/2119:50
74-85-1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
568000 ug/L
45000
50
12/10/2112:36
124-38-9
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND ug/L
9.1
1
12/01/2105:25
12/01/2119:25
92-52-4
44.8 ug/L
9.1
1
12/01/2105:25
12/01/2119:25
101-84-8
74 %
10-144
1
12/01/2105:25
12/01/2119:25
4165-60-0
108 %
10-130
1
12/01 /21 05:25
12/01 /21 19:25
321-60-8
74 %
34-163
1
12/01 /21 05:25
12/01 /21 19:25
1718-51-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
3560 ug/L
250
10
12/04/2107:37
67-64-1
ND ug/L
10.0
10
12/04/2107:37
71-43-2
ND ug/L
10.0
10
12/04/2107:37
74-97-5
ND ug/L
10.0
10
12/04/2107:37
75-27-4
ND ug/L
10.0
10
12/04/2107:37
75-25-2
ND ug/L
20.0
10
12/04/2107:37
74-83-9
504 ug/L
50.0
10
12/04/2107:37
78-93-3
ND ug/L
20.0
10
12/04/2107:37
75-15-0
ND ug/L
10.0
10
12/04/2107:37
56-23-5
ND ug/L
10.0
10
12/04/2107:37
108-90-7
22.3 ug/L
10.0
10
12/04/2107:37
75-00-3
ND ug/L
10.0
10
12/04/2107:37
67-66-3
ND ug/L
10.0
10
12/04/2107:37
74-87-3
ND ug/L
10.0
10
12/04/2107:37
110-82-7
ND ug/L
20.0
10
12/04/2107:37
96-12-8
ND ug/L
10.0
10
12/04/2107:37
124-48-1
ND ug/L
10.0
10
12/04/2107:37
106-93-4
ND ug/L
10.0
10
12/04/2107:37
95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: 13-2313-112921 Lab ID: 92574833009 Collected: 11/29/21 15:46 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/L
10.0
10
12/04/21 07:37
541-73-1
1,4-Dichlorobenzene
ND
ug/L
10.0
10
12/04/21 07:37
106-46-7
Dichlorodifluoromethane
ND
ug/L
10.0
10
12/04/21 07:37
75-71-8
1,1-Dichloroethane
ND
ug/L
10.0
10
12/04/21 07:37
75-34-3
1,2-Dichloroethane
ND
ug/L
10.0
10
12/04/21 07:37
107-06-2
1,1-Dichloroethene
ND
ug/L
10.0
10
12/04/21 07:37
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
10.0
10
12/04/21 07:37
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
10.0
10
12/04/21 07:37
156-60-5
1,2-Dichloropropene
ND
ug/L
10.0
10
12/04/21 07:37
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
10.0
10
12/04/21 07:37
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
10.0
10
12/04/21 07:37
10061-02-6
Ethylbenzene
ND
ug/L
10.0
10
12/04/21 07:37
100-41-4
2-Hexanone
ND
ug/L
50.0
10
12/04/21 07:37
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
10.0
10
12/04/21 07:37
98-82-8
Methyl acetate
ND
ug/L
100
10
12/04/21 07:37
79-20-9
Methylcyclohexane
ND
ug/L
100
10
12/04/21 07:37
108-87-2
Methylene Chloride
ND
ug/L
50.0
10
12/04/21 07:37
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
50.0
10
12/04/21 07:37
108-10-1
Methyl-tert-butyl ether
ND
ug/L
10.0
10
12/04/21 07:37
1634-04-4
Styrene
ND
ug/L
10.0
10
12/04/21 07:37
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
10.0
10
12/04/21 07:37
79-34-5
Tetrachloroethene
ND
ug/L
10.0
10
12/04/21 07:37
127-18-4
Toluene
ND
ug/L
10.0
10
12/04/21 07:37
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
10.0
10
12/04/21 07:37
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
10.0
10
12/04/21 07:37
120-82-1
1,1,1-Trichloroethane
ND
ug/L
10.0
10
12/04/21 07:37
71-55-6
1,1,2-Trichloroethane
ND
ug/L
10.0
10
12/04/21 07:37
79-00-5
Trichloroethene
ND
ug/L
10.0
10
12/04/21 07:37
79-01-6
Trichlorofluoromethane
ND
ug/L
10.0
10
12/04/21 07:37
75-69-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
10.0
10
12/04/21 07:37
76-13-1
Vinyl chloride
ND
ug/L
10.0
10
12/04/21 07:37
75-01-4
Xylene (Total)
ND
ug/L
10.0
10
12/04/21 07:37
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
106
%
70-130
10
12/04/21 07:37
460-00-4
1,2-Dichloroethane-d4 (S)
110
%
70-130
10
12/04/21 07:37
17060-07-0
Toluene-d8(S)
104
%
70-130
10
12/04/21 07:37
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
3000
ug/L
100
50
12/01/21 03:37
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
113
%
70-130
50
12/01/21 03:37
17060-07-0
Toluene-d8(S)
111
%
66-133
50
12/01/21 03:37
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 93

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: 13-2313-112921
Lab ID: 92574833009 Collected:
11/29/21 15:46
Received: 11/30/21 12:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
12/01/21 00:59
14797-55-8
Nitrogen, Nitrite
0.11 mg/L
0.040
1
12/01/21 00:59
14797-65-0
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
5.4 mg/L
1.0
1
12/01/2122:21
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
1590 mg/L
250
250
12/01/21 22:45
7440-44-0
Total Organic Carbon
1640 mg/L
250
250
12/01/21 22:45
7440-44-0
Total Organic Carbon
1680 mg/L
250
250
12/01/21 22:45
7440-44-0
Total Organic Carbon
1630 mg/L
250
250
12/01/21 22:45
7440-44-0
Mean Total Organic Carbon
1640 mg/L
250
250
12/01/21 22:45
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
980 mg/L
250
500
12/13/21 18:15
64-19-7
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-17C-112921 Lab ID: 92574833010 Collected: 11/29/21 14:00 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Biodegradation Indicator Gases
Methane
Ethane
Ethene
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
9056 IC anions 28 Days
Sulfate
Total Organic Carbon,Asheville
Total Organic Carbon
Total Organic Carbon
Total Organic Carbon
Total Organic Carbon
Mean Total Organic Carbon
Date: 12/21 /2021 11:18 AM
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
0.16 mg/L
0.050
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
72 ug/L
5.0
1
ND ug/L
1.0
1
ND ug/L
1.0
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
129000 ug/L
45000
50
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
12/01/21 13:45
12/06/21 20:02 74-82-8
12/06/21 20:02 74-84-0
12/06/21 20:02 74-85-1
12/ 10/21 12:41 124-38-9
ND ug/L
10.0
1
12/01/2105:25
12/02/2113:33
92-52-4
ND ug/L
10.0
1
12/01/2105:25
12/02/2113:33
101-84-8
68 %
10-144
1
12/01/2105:25
12/02/2113:33
4165-60-0
58 %
10-130
1
12/01/2105:25
12/02/2113:33
321-60-8
75 %
34-163
1
12/01/2105:25
12/02/2113:33
1718-51-0
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1370 ug/L
50.0
25
12/01/2103:56
123-91-1
108 %
70-130
25
12/01/2103:56
17060-07-0
108 %
66-133
25
12/01/21 03:56
2037-26-5
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L
0.040
1
12/01/2100:57
14797-55-8
ND mg/L
0.040
1
12/01/2100:57
14797-65-0
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
1.3 mg/L
1.0
1
12/01/21 22:36
14808-79-8
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
2.9 mg/L
1.0
1
12/01/21 23:02
7440-44-0
3.0 mg/L
1.0
1
12/01/21 23:02
7440-44-0
3.0 mg/L
1.0
1
12/01/21 23:02
7440-44-0
3.0 mg/L
1.0
1
12/01/21 23:02
7440-44-0
3.0 mg/L
1.0
1
12/01/21 23:02
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 93

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-17C-112921 Lab ID: 92574833010 Collected: 11/29/21 14:00 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Low Level Volatile Fatty Acids Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid 1.9 mg/L 0.50 1 12/10/21 22:52 64-19-7
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 24 of 93

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-12-112921 Lab ID: 92574833011 Collected: 11/29/21 16:00 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.13 mg/L
0.050
1
12/01/21 13:47
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
9.1
1
12/01/21 05:25
12/02/21 13:58
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L
9.1
1
12/01/21 05:25
12/02/21 13:58
101-84-8
Surrogates
Nitrobenzene-d5(S)
70 %
10-144
1
12/01/21 05:25
12/02/21 13:58
4165-60-0
2-Fluorobiphenyl (S)
61 %
10-130
1
12/01/21 05:25
12/02/21 13:58
321-60-8
Terphenyl-d14(S)
68 %
34-163
1
12/01/21 05:25
12/02/21 13:58
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
2350 ug/L
100
50
12/01/21 04:15
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
110 %
70-130
50
12/01/21 04:15
17060-07-0
Toluene-d8(S)
108 %
66-133
50
12/01/21 04:15
2037-26-5
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
12/01/21 01:00
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
12/01/21 01:00
14797-65-0
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.3 mg/L
1.0
1
12/01/2122:52
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 93

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-2213-113021 Lab ID: 92574833012 Collected: 11/30/21 07:57 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Biodegradation Indicator Gases
Methane
Ethane
Ethene
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV Low Level Landfill
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
Date: 12/21 /2021 11:18 AM
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
0.33 mg/L
0.050
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
25000 ug/L
10
2
2.2 ug/L
1.0
1
ND ug/L
1.0
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
299000 ug/L
45000
50
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
12/01/21 13:47
12/09/21 19:59 74-82-8
12/06/21 20:13 74-84-0
12/06/2120:13 74-85-1
12/ 10/21 12:48 124-38-9
ND
ug/L
8.3
1
12/01/2105:25
12/02/2114:23
92-52-4
48.4
ug/L
8.3
1
12/01/2105:25
12/02/2114:23
101-84-8
89
%
10-144
1
12/01/2105:25
12/02/2114:23
4165-60-0
76
%
10-130
1
12/01/2105:25
12/02/2114:23
321-60-8
91
%
34-163
1
12/01/2105:25
12/02/2114:23
1718-51-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
12/03/2113:06
67-64-1
ND
ug/L
1.0
1
12/03/2113:06
71-43-2
ND
ug/L
1.0
1
12/03/2113:06
74-97-5
ND
ug/L
1.0
1
12/03/2113:06
75-27-4
ND
ug/L
1.0
1
12/03/2113:06
75-25-2
ND
ug/L
2.0
1
12/03/2113:06
74-83-9
ND
ug/L
5.0
1
12/03/2113:06
78-93-3
ND
ug/L
2.0
1
12/03/2113:06
75-15-0
ND
ug/L
1.0
1
12/03/2113:06
56-23-5
11.2
ug/L
1.0
1
12/03/2113:06
108-90-7
18.9
ug/L
1.0
1
12/03/21 13:06
75-00-3
ND
ug/L
1.0
1
12/03/2113:06
67-66-3
ND
ug/L
1.0
1
12/03/2113:06
74-87-3
ND
ug/L
1.0
1
12/03/2113:06
110-82-7
ND
ug/L
2.0
1
12/03/2113:06
96-12-8
ND
ug/L
1.0
1
12/03/2113:06
124-48-1
ND
ug/L
1.0
1
12/03/2113:06
106-93-4
ND
ug/L
1.0
1
12/03/2113:06
95-50-1
ND
ug/L
1.0
1
12/03/2113:06
541-73-1
ND
ug/L
1.0
1
12/03/2113:06
106-46-7
ND
ug/L
1.0
1
12/03/2113:06
75-71-8
ND
ug/L
1.0
1
12/03/2113:06
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 26 of 93

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: 13-2213-113021 Lab ID: 92574833012 Collected: 11/30/21 07:57 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene (Cumene)
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 12/21 /2021 11:18 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND ug/L
1.0
1
12/03/21 13:06
107-06-2
ND ug/L
1.0
1
12/03/21 13:06
75-35-4
ND ug/L
1.0
1
12/03/21 13:06
156-59-2
ND ug/L
1.0
1
12/03/21 13:06
156-60-5
ND ug/L
1.0
1
12/03/21 13:06
78-87-5
ND ug/L
1.0
1
12/03/21 13:06
10061-01-5
ND ug/L
1.0
1
12/03/21 13:06
10061-02-6
ND ug/L
1.0
1
12/03/21 13:06
100-41-4
ND ug/L
5.0
1
12/03/21 13:06
591-78-6
ND ug/L
1.0
1
12/03/21 13:06
98-82-8
ND ug/L
10.0
1
12/03/21 13:06
79-20-9
ND ug/L
10.0
1
12/03/21 13:06
108-87-2
ND ug/L
5.0
1
12/03/21 13:06
75-09-2
ND ug/L
5.0
1
12/03/21 13:06
108-10-1
ND ug/L
1.0
1
12/03/21 13:06
1634-04-4
ND ug/L
1.0
1
12/03/21 13:06
100-42-5
ND ug/L
1.0
1
12/03/21 13:06
79-34-5
ND ug/L
1.0
1
12/03/21 13:06
127-18-4
ND ug/L
1.0
1
12/03/21 13:06
108-88-3
ND ug/L
1.0
1
12/03/21 13:06
87-61-6
ND ug/L
1.0
1
12/03/21 13:06
120-82-1
ND ug/L
1.0
1
12/03/21 13:06
71-55-6
ND ug/L
1.0
1
12/03/21 13:06
79-00-5
ND ug/L
1.0
1
12/03/21 13:06
79-01-6
ND ug/L
1.0
1
12/03/21 13:06
75-69-4
ND ug/L
1.0
1
12/03/21 13:06
76-13-1
ND ug/L
1.0
1
12/03/21 13:06
75-01-4
ND ug/L
1.0
1
12/03/21 13:06
1330-20-7
99 %
70-130
1
12/03/21 13:06
460-00-4
98 %
70-130
1
12/03/21 13:06
17060-07-0
100 %
70-130
1
12/03/21 13:06
2037-26-5
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1060 ug/L
40.0
20
12/01/2104:35
123-91-1
107 %
70-130
20
12/01/2104:35
17060-07-0
107 %
66-133
20
12/01/21 04:35
2037-26-5
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L
0.040
1
12/01/2101:04
14797-55-8
0.041 mg/L
0.040
1
12/01 /21 01:04
14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 93

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: 13-2213-113021
Lab ID: 92574833012 Collected:
11/30/21 07:57
Received: 11/30/21 12:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
12/01/2123:07
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
6.9 mg/L
1.0
1
12/01/21 23:20
7440-44-0
Total Organic Carbon
6.8 mg/L
1.0
1
12/01/21 23:20
7440-44-0
Total Organic Carbon
6.7 mg/L
1.0
1
12/01/21 23:20
7440-44-0
Total Organic Carbon
6.6 mg/L
1.0
1
12/01/21 23:20
7440-44-0
Mean Total Organic Carbon
6.8 mg/L
1.0
1
12/01/21 23:20
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
0.67 mg/L
0.50
1
12/10/21 23:27
64-19-7
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 28 of 93

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-1713-113021 Lab ID: 92574833013 Collected: 11/30/21 08:34 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Biodegradation Indicator Gases
Methane
Ethane
Ethene
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
9056 IC anions 28 Days
Sulfate
Total Organic Carbon,Asheville
Total Organic Carbon
Total Organic Carbon
Total Organic Carbon
Total Organic Carbon
Mean Total Organic Carbon
Date: 12/21 /2021 11:18 AM
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
0.27 mg/L
0.050
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
45 ug/L
5.0
1
ND ug/L
1.0
1
ND ug/L
1.0
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
163000 ug/L
45000
50
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
12/01/21 13:51
12/06/21 20:24 74-82-8
12/06/21 20:24 74-84-0
12/06/21 20:24 74-85-1
12/ 10/21 12:57 124-38-9
ND ug/L
10.0
1
12/01/2105:25
12/02/21 14:49
92-52-4
ND ug/L
10.0
1
12/01/2105:25
12/02/21 14:49
101-84-8
81 %
10-144
1
12/01/2105:25
12/02/21 14:49
4165-60-0
69 %
10-130
1
12/01 /21 05:25
12/02/21 14:49
321-60-8
87 %
34-163
1
12/01 /21 05:25
12/02/21 14:49
1718-51-0
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
138 ug/L
5.0
2.5
12/01/2116:11
123-91-1
102 %
70-130
2.5
12/01/2116:11
17060-07-0
102 %
66-133
2.5
12/01/2116:11
2037-26-5
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L
0.040
1
12/01/2101:06
14797-55-8
ND mg/L
0.040
1
12/01/2101:06
14797-65-0
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
2.4 mg/L
1.0
1
12/01 /21 23:23
14808-79-8
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
3.0 mg/L
1.0
1
12/01 /21 23:37
7440-44-0
2.3 mg/L
1.0
1
12/01 /21 23:37
7440-44-0
2.2 mg/L
1.0
1
12/01 /21 23:37
7440-44-0
2.2 mg/L
1.0
1
12/01 /21 23:37
7440-44-0
2.4 mg/L
1.0
1
12/01 /21 23:37
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 29 of 93

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-17B-113021 Lab ID: 92574833013 Collected: 11/30/21 08:34 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Low Level Volatile Fatty Acids Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid ND mg/L 0.50 1 12/11/2100:02 64-19-7
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 30 of 93

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-22A-113021 Lab ID: 92574833014 Collected: 11/30/21 09:40 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Biodegradation Indicator Gases
Methane
Ethane
Ethene
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV Low Level Landfill
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
Date: 12/21 /2021 11:18 AM
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
ND mg/L
0.050
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
52 ug/L
5.0
1
2.5 ug/L
1.0
1
ND ug/L
1.0
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
265000 ug/L
45000
50
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
12/01/21 13:52
12/06/21 20:36 74-82-8
12/06/21 20:36 74-84-0
12/06/21 20:36 74-85-1
12/ 10/21 13:15 124-38-9
ND
ug/L
8.3
1
12/01/2105:25
12/02/21 15:14
92-52-4
ND
ug/L
8.3
1
12/01/2105:25
12/02/21 15:14
101-84-8
44
%
10-144
1
12/01/2105:25
12/02/21 15:14
4165-60-0
37
%
10-130
1
12/01 /21 05:25
12/02/21 15:14
321-60-8
55
%
34-163
1
12/01 /21 05:25
12/02/21 15:14
1718-51-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
12/03/2113:25
67-64-1
ND
ug/L
1.0
1
12/03/2113:25
71-43-2
ND
ug/L
1.0
1
12/03/2113:25
74-97-5
ND
ug/L
1.0
1
12/03/2113:25
75-27-4
ND
ug/L
1.0
1
12/03/2113:25
75-25-2
ND
ug/L
2.0
1
12/03/2113:25
74-83-9
ND
ug/L
5.0
1
12/03/2113:25
78-93-3
ND
ug/L
2.0
1
12/03/2113:25
75-15-0
ND
ug/L
1.0
1
12/03/2113:25
56-23-5
4.9
ug/L
1.0
1
12/03/2113:25
108-90-7
ND
ug/L
1.0
1
12/03/2113:25
75-00-3
ND
ug/L
1.0
1
12/03/2113:25
67-66-3
ND
ug/L
1.0
1
12/03/2113:25
74-87-3
ND
ug/L
1.0
1
12/03/2113:25
110-82-7
ND
ug/L
2.0
1
12/03/2113:25
96-12-8
ND
ug/L
1.0
1
12/03/2113:25
124-48-1
ND
ug/L
1.0
1
12/03/2113:25
106-93-4
ND
ug/L
1.0
1
12/03/2113:25
95-50-1
ND
ug/L
1.0
1
12/03/2113:25
541-73-1
ND
ug/L
1.0
1
12/03/2113:25
106-46-7
ND
ug/L
1.0
1
12/03/2113:25
75-71-8
3.7
ug/L
1.0
1
12/03/21 13:25
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-22A-113021 Lab ID: 92574833014 Collected: 11/30/21 09:40 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene (Cumene)
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 12/21 /2021 11:18 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND ug/L
1.0
1
12/03/21 13:25
107-06-2
2.4 ug/L
1.0
1
12/03/21 13:25
75-35-4
ND ug/L
1.0
1
12/03/21 13:25
156-59-2
ND ug/L
1.0
1
12/03/21 13:25
156-60-5
ND ug/L
1.0
1
12/03/21 13:25
78-87-5
ND ug/L
1.0
1
12/03/21 13:25
10061-01-5
ND ug/L
1.0
1
12/03/21 13:25
10061-02-6
ND ug/L
1.0
1
12/03/21 13:25
100-41-4
ND ug/L
5.0
1
12/03/21 13:25
591-78-6
ND ug/L
1.0
1
12/03/21 13:25
98-82-8
ND ug/L
10.0
1
12/03/21 13:25
79-20-9
ND ug/L
10.0
1
12/03/21 13:25
108-87-2
ND ug/L
5.0
1
12/03/21 13:25
75-09-2
ND ug/L
5.0
1
12/03/21 13:25
108-10-1
ND ug/L
1.0
1
12/03/21 13:25
1634-04-4
ND ug/L
1.0
1
12/03/21 13:25
100-42-5
ND ug/L
1.0
1
12/03/21 13:25
79-34-5
ND ug/L
1.0
1
12/03/21 13:25
127-18-4
ND ug/L
1.0
1
12/03/21 13:25
108-88-3
ND ug/L
1.0
1
12/03/21 13:25
87-61-6
ND ug/L
1.0
1
12/03/21 13:25
120-82-1
ND ug/L
1.0
1
12/03/21 13:25
71-55-6
ND ug/L
1.0
1
12/03/21 13:25
79-00-5
ND ug/L
1.0
1
12/03/21 13:25
79-01-6
ND ug/L
1.0
1
12/03/21 13:25
75-69-4
ND ug/L
1.0
1
12/03/21 13:25
76-13-1
ND ug/L
1.0
1
12/03/21 13:25
75-01-4
ND ug/L
1.0
1
12/03/21 13:25
1330-20-7
99 %
70-130
1
12/03/21 13:25
460-00-4
99 %
70-130
1
12/03/21 13:25
17060-07-0
101 %
70-130
1
12/03/21 13:25
2037-26-5
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1200 ug/L
40.0
20
12/01/2104:54
123-91-1
104 %
70-130
20
12/01/2104:54
17060-07-0
106 %
66-133
20
12/01/21 04:54
2037-26-5
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L
0.040
1
12/01/2101:11
14797-55-8
0.087 mg/L
0.040
1
12/01 /21 01:11
14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 32 of 93

lreAnalyilcal®
www.pacelabs.cem
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-22A-113021
Lab ID: 92574833014 Collected:
11/30/21 09:40
Received: 11/30/21 12:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
12/01/2123:38
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
4.5 mg/L
1.0
1
12/01/21 23:55
7440-44-0
Total Organic Carbon
4.3 mg/L
1.0
1
12/01/21 23:55
7440-44-0
Total Organic Carbon
4.2 mg/L
1.0
1
12/01/21 23:55
7440-44-0
Total Organic Carbon
4.1 mg/L
1.0
1
12/01/21 23:55
7440-44-0
Mean Total Organic Carbon
4.3 mg/L
1.0
1
12/01/21 23:55
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
ND mg/L
0.50
1
12/11/2100:36
64-19-7
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 33 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-09C-113021 Lab ID: 92574833015 Collected: 11/30/21 10:05 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.74 mg/L
0.25
5
12/01/21 14:23
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
25.0
5
12/07/21 15:34
107-21-1 D3
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
9.1
1 12/01/21 05:25
12/02/21 15:39
92-52-4
Diphenyl ether (Phenyl ether)
21.2 ug/L
9.1
1 12/01/21 05:25
12/02/21 15:39
101-84-8
Surrogates
Nitrobenzene-d5(S)
86 %
10-144
1 12/01/21 05:25
12/02/21 15:39
4165-60-0
2-Fluorobiphenyl (S)
74 %
10-130
1 12/01/21 05:25
12/02/21 15:39
321-60-8
Terphenyl-d14 (S)
78 %
34-163
1 12/01/21 05:25
12/02/21 15:39
1718-51-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
3460 ug/L
312
12.5
12/04/21 07:02
67-64-1
Benzene
ND ug/L
12.5
12.5
12/04/21 07:02
71-43-2
Bromochloromethane
ND ug/L
12.5
12.5
12/04/21 07:02
74-97-5
Bromodichloromethane
ND ug/L
12.5
12.5
12/04/21 07:02
75-27-4
Bromoform
ND ug/L
12.5
12.5
12/04/21 07:02
75-25-2
Bromomethane
ND ug/L
25.0
12.5
12/04/21 07:02
74-83-9
2-Butanone (MEK)
548 ug/L
62.5
12.5
12/04/21 07:02
78-93-3
Carbon disulfide
ND ug/L
25.0
12.5
12/04/21 07:02
75-15-0
Carbon tetrachloride
ND ug/L
12.5
12.5
12/04/21 07:02
56-23-5
Chlorobenzene
ND ug/L
12.5
12.5
12/04/21 07:02
108-90-7
Chloroethane
ND ug/L
12.5
12.5
12/04/21 07:02
75-00-3
Chloroform
ND ug/L
12.5
12.5
12/04/21 07:02
67-66-3
Chloromethane
ND ug/L
12.5
12.5
12/04/21 07:02
74-87-3
Cyclohexane
ND ug/L
12.5
12.5
12/04/21 07:02
110-82-7
1,2-Dibromo-3-chloropropane
ND ug/L
25.0
12.5
12/04/21 07:02
96-12-8
Dibromochloromethane
ND ug/L
12.5
12.5
12/04/21 07:02
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
12.5
12.5
12/04/21 07:02
106-93-4
1,2-Dichlorobenzene
ND ug/L
12.5
12.5
12/04/21 07:02
95-50-1
1,3-Dichlorobenzene
ND ug/L
12.5
12.5
12/04/21 07:02
541-73-1
1,4-Dichlorobenzene
ND ug/L
12.5
12.5
12/04/21 07:02
106-46-7
Dichlorodifluoromethane
ND ug/L
12.5
12.5
12/04/21 07:02
75-71-8
1,1-Dichloroethane
ND ug/L
12.5
12.5
12/04/21 07:02
75-34-3
1,2-Dichloroethane
ND ug/L
12.5
12.5
12/04/21 07:02
107-06-2
1,1-Dichloroethene
ND ug/L
12.5
12.5
12/04/21 07:02
75-35-4
cis-1,2-Dichloroethene
14.8 ug/L
12.5
12.5
12/04/21 07:02
156-59-2
trans-1,2-Dichloroethene
ND ug/L
12.5
12.5
12/04/21 07:02
156-60-5
1,2-Dichloropropane
ND ug/L
12.5
12.5
12/04/21 07:02
78-87-5
cis-1,3-Dichloropropene
ND ug/L
12.5
12.5
12/04/21 07:02
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 12/21 /2021 11:18 AM
without the written consent of Pace Analytical
Services, LLC.
Page 34 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-09C-113021 Lab ID: 92574833015 Collected: 11/30/21 10:05 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
trans- 1,3-Dichloropropene
ND ug/L
12.5
12.5
12/04/21 07:02
10061-02-6
Ethylbenzene
ND ug/L
12.5
12.5
12/04/21 07:02
100-41-4
2-Hexanone
ND ug/L
62.5
12.5
12/04/21 07:02
591-78-6
Isopropylbenzene (Cumene)
ND ug/L
12.5
12.5
12/04/21 07:02
98-82-8
Methyl acetate
ND ug/L
125
12.5
12/04/21 07:02
79-20-9
Methylcyclohexane
ND ug/L
125
12.5
12/04/21 07:02
108-87-2
Methylene Chloride
ND ug/L
62.5
12.5
12/04/21 07:02
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
62.5
12.5
12/04/21 07:02
108-10-1
Methyl-tert-butyl ether
ND ug/L
12.5
12.5
12/04/21 07:02
1634-04-4
Styrene
ND ug/L
12.5
12.5
12/04/21 07:02
100-42-5
1,1,2,2-Tetrachloroethane
ND ug/L
12.5
12.5
12/04/21 07:02
79-34-5
Tetrachloroethene
ND ug/L
12.5
12.5
12/04/21 07:02
127-18-4
Toluene
ND ug/L
12.5
12.5
12/04/21 07:02
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
12.5
12.5
12/04/21 07:02
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
12.5
12.5
12/04/21 07:02
120-82-1
1,1,1-Trichloroethane
ND ug/L
12.5
12.5
12/04/21 07:02
71-55-6
1,1,2-Trichloroethane
ND ug/L
12.5
12.5
12/04/21 07:02
79-00-5
Trichloroethene
ND ug/L
12.5
12.5
12/04/21 07:02
79-01-6
Trichlorofluoromethane
ND ug/L
12.5
12.5
12/04/21 07:02
75-69-4
1,1,2-Trichlorotrifluoroethane
ND ug/L
12.5
12.5
12/04/21 07:02
76-13-1
Vinyl chloride
ND ug/L
12.5
12.5
12/04/21 07:02
75-01-4
Xylene (Total)
ND ug/L
12.5
12.5
12/04/21 07:02
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
106 %
70-130
12.5
12/04/21 07:02
460-00-4
1,2-Dichloroethane-d4 (S)
108 %
70-130
12.5
12/04/21 07:02
17060-07-0
Toluene-d8 (S)
101 %
70-130
12.5
12/04/21 07:02
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
909 ug/L
20.0
10
12/01/21 05:14
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
106 %
70-130
10
12/01/21 05:14
17060-07-0
Toluene-d8(S)
106 %
66-133
10
12/01/21 05:14
2037-26-5
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
12/01/21 01:14
14797-55-8
Nitrogen, Nitrite
0.12 mg/L
0.040
1
12/01/21 01:14
14797-65-0
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.4 mg/L
1.0
1
12/01/2123:54
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 93

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-21B-113021
Lab ID: 92574833016 Collected:
11/30/21 11:24
Received: 11/30/21 12:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.19 mg/L
0.050
1
12/01/21 13:53
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
37.2 ug/L
2.0
1
12/01/21 02:00
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
117 %
70-130
1
12/01/21 02:00
17060-07-0
Toluene-d8 (S)
118 %
66-133
1
12/01/21 02:00
2037-26-5
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
12/01/21 01:26
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
12/01/21 01:26
14797-65-0
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
16.7 mg/L
1.0
1
12/02/2117:41
14808-79-8
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 36 of 93

lreAnalyilcal®
www.pacelabs.cem
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-99C-113021 Lab ID: 92574833017 Collected: 11/30/21 10:10 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Biphenyl (Diphenyl)
ND
ug/L
8.3
1
12/01/21 05:25
12/02/21 16:04
92-52-4
Diphenyl ether (Phenyl ether)
18.9
ug/L
8.3
1
12/01/21 05:25
12/02/21 16:04
101-84-8
Surrogates
Nitrobenzene-d5(S)
83
%
10-144
1
12/01/21 05:25
12/02/21 16:04
4165-60-0
2-Fluorobiphenyl (S)
75
%
10-130
1
12/01/21 05:25
12/02/21 16:04
321-60-8
Terphenyl-d14 (S)
79
%
34-163
1
12/01/21 05:25
12/02/21 16:04
1718-51-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
3520
ug/L
250
10
12/04/21 06:44
67-64-1
Benzene
ND
ug/L
10.0
10
12/04/21 06:44
71-43-2
Bromochloromethane
ND
ug/L
10.0
10
12/04/21 06:44
74-97-5
Bromodichloromethane
ND
ug/L
10.0
10
12/04/21 06:44
75-27-4
Bromoform
ND
ug/L
10.0
10
12/04/21 06:44
75-25-2
Bromomethane
ND
ug/L
20.0
10
12/04/21 06:44
74-83-9
2-Butanone (MEK)
583
ug/L
50.0
10
12/04/21 06:44
78-93-3
Carbon disulfide
ND
ug/L
20.0
10
12/04/21 06:44
75-15-0
Carbon tetrachloride
ND
ug/L
10.0
10
12/04/21 06:44
56-23-5
Chlorobenzene
ND
ug/L
10.0
10
12/04/21 06:44
108-90-7
Chloroethane
ND
ug/L
10.0
10
12/04/21 06:44
75-00-3
Chloroform
ND
ug/L
10.0
10
12/04/21 06:44
67-66-3
Chloromethane
ND
ug/L
10.0
10
12/04/21 06:44
74-87-3
Cyclohexane
ND
ug/L
10.0
10
12/04/21 06:44
110-82-7
1,2-Dibromo-3-chloropropane
ND
ug/L
20.0
10
12/04/21 06:44
96-12-8
Dibromochloromethane
ND
ug/L
10.0
10
12/04/21 06:44
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
10.0
10
12/04/21 06:44
106-93-4
1,2-Dichlorobenzene
ND
ug/L
10.0
10
12/04/21 06:44
95-50-1
1,3-Dichlorobenzene
ND
ug/L
10.0
10
12/04/21 06:44
541-73-1
1,4-Dichlorobenzene
ND
ug/L
10.0
10
12/04/21 06:44
106-46-7
Dichlorodifluoromethane
ND
ug/L
10.0
10
12/04/21 06:44
75-71-8
1,1-Dichloroethane
ND
ug/L
10.0
10
12/04/21 06:44
75-34-3
1,2-Dichloroethane
ND
ug/L
10.0
10
12/04/21 06:44
107-06-2
1,1-Dichloroethene
ND
ug/L
10.0
10
12/04/21 06:44
75-35-4
cis-1,2-Dichloroethene
14.3
ug/L
10.0
10
12/04/21 06:44
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
10.0
10
12/04/21 06:44
156-60-5
1,2-Dichloropropane
ND
ug/L
10.0
10
12/04/21 06:44
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
10.0
10
12/04/21 06:44
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
10.0
10
12/04/21 06:44
10061-02-6
Ethylbenzene
ND
ug/L
10.0
10
12/04/21 06:44
100-41-4
2-Hexanone
ND
ug/L
50.0
10
12/04/21 06:44
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
10.0
10
12/04/21 06:44
98-82-8
Methyl acetate
ND
ug/L
100
10
12/04/21 06:44
79-20-9
Methylcyclohexane
ND
ug/L
100
10
12/04/21 06:44
108-87-2
Methylene Chloride
ND
ug/L
50.0
10
12/04/21 06:44
75-09-2
4-Methyl-2-pentanone (MIBK)
95.8
ug/L
50.0
10
12/04/21 06:44
108-10-1
Methyl-tert-butyl ether
ND
ug/L
10.0
10
12/04/21 06:44
1634-04-4
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-99C-113021 Lab ID: 92574833017 Collected: 11/30/21 10:10 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 12/21 /2021 11:18 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
10.0
10
12/04/2106:44
100-42-5
ND
ug/L
10.0
10
12/04/2106:44
79-34-5
ND
ug/L
10.0
10
12/04/2106:44
127-18-4
ND
ug/L
10.0
10
12/04/2106:44
108-88-3
ND
ug/L
10.0
10
12/04/2106:44
87-61-6
ND
ug/L
10.0
10
12/04/2106:44
120-82-1
ND
ug/L
10.0
10
12/04/2106:44
71-55-6
ND
ug/L
10.0
10
12/04/2106:44
79-00-5
ND
ug/L
10.0
10
12/04/2106:44
79-01-6
ND
ug/L
10.0
10
12/04/2106:44
75-69-4
ND
ug/L
10.0
10
12/04/2106:44
76-13-1
ND
ug/L
10.0
10
12/04/2106:44
75-01-4
ND
ug/L
10.0
10
12/04/2106:44
1330-20-7
104
%
70-130
10
12/04/2106:44
460-00-4
106
%
70-130
10
12/04/2106:44
17060-07-0
103
%
70-130
10
12/04/2106:44
2037-26-5
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
956
ug/L
25.0
12.5
12/01/2105:33
123-91-1
108
%
70-130
12.5
12/01/2105:33
17060-07-0
105
%
66-133
12.5
12/01/2105:33
2037-26-5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-23A-112921 H2 Lab ID: 92574833018 Collected: 11/29/21 15:10 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen 2.5 nM 1.9 1 12/08/2110:52 1333-74-0
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
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Page 39 of 93

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ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: 13-2313-112921 H2 Lab ID: 92574833019 Collected: 11/29/21 16:20 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen 2.9 nM 1.9 1 12/08/2111:14 1333-74-0
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-17C-112921 H2 Lab ID: 92574833020 Collected: 11/29/21 14:40 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen ND nM 1.9 1 12/08/2111:34 1333-74-0
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
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Page 41 of 93

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Pace Analytical Services, LLC
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ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: 13-2213-113021 H2 Lab ID: 92574833021 Collected: 11/30/21 08:40 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen ND nM 1.9 1 12/08/2111:49 1333-74-0
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 42 of 93

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Pace Analytical Services, LLC
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Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-17B-113021 H2 Lab ID: 92574833022 Collected: 11/30/21 09:12 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen 7.7 nM 1.9 1 12/08/2112:03 1333-74-0
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 43 of 93

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Sample: B-22A-113021 H2 Lab ID: 92574833023 Collected: 11/30/21 10:30 Received: 11/30/21 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2 Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen 1.9 nM 1.9 1 12/08/2112:16 1333-74-0
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 44 of 93

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Pace Analytical Services, LLC
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Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 663113 Analysis Method: SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011 Analysis Description: SM450OP-E Phosphorus, Ortho
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92574833006,92574833007,92574833008,92574833009,92574833010,92574833011,92574833012,
92574833013,92574833014,92574833015,92574833016
METHOD BLANK: 3473618 Matrix: Water
Associated Lab Samples: 92574833006,92574833007,92574833008,92574833009,92574833010,92574833011,92574833012,
92574833013,92574833014,92574833015,92574833016
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Orthophosphate as P mg/L ND 0.050 12/01/21 13:42
LABORATORY CONTROL SAMPLE: 3473619
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Orthophosphate as P mg/L 0.25 0.26 105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3474276 3474277
MS MSD
92574936002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Orthophosphate as P mg/L 0.60 0.25 0.25 0.85 0.86 100 102 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3474278 3474279
MS MSD
92575044003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Orthophosphate as P mg/L ND 0.25 0.25 0.27 0.28 99 99 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 653917 Analysis Method: EPA 8015 Alcohol -Glycol
QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified
Laboratory: Pace Analytical Services - Indianapolis
Associated Lab Samples: 92574833002, 92574833003, 92574833004, 92574833005, 92574833008, 92574833009, 92574833015
METHOD BLANK: 3014240 Matrix: Water
Associated Lab Samples: 92574833002, 92574833003, 92574833004, 92574833005, 92574833008, 92574833009, 92574833015
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ethylene glycol mg/L ND 5.0 12/06/21 15:06
LABORATORY CONTROL SAMPLE: 3014241
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Ethylene glycol mg/L 25 20.6 82 39-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3014242 3014243
MS MSD
92574833002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mg/L ND 25 25 24.2 27.4 96 109 36-158 12
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
Page 46 of 93

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 728838 Analysis Method: AM20GAX
QC Batch Method: AM20GAX Analysis Description: Indicator Gases Bubble Strip H2
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92574833018, 92574833019, 92574833020, 92574833021, 92574833022, 92574833023
METHOD BLANK: 2282833 Matrix: Air
Associated Lab Samples: 92574833018, 92574833019, 92574833020, 92574833021, 92574833022, 92574833023
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Hydrogen nM ND 1.9 12/08/2110:40
LABORATORY CONTROL SAMPLE & LCSD: 2282834 2282835
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Hydrogen nM 12 10 10 86 86 70-130 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
Page 47 of 93

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Pace Analytical Services, LLC
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QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 728703 Analysis Method: RSK-175
QC Batch Method: RSK-175 Analysis Description: Biodegradation Indicator Gases
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92574833008, 92574833009, 92574833010, 92574833012, 92574833013, 92574833014
METHOD BLANK: 2282093
Matrix: Water
Associated Lab Samples:
92574833008, 92574833009, 92574833010, 92574833012, 92574833013,
92574833014
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Methane
ug/L
ND 5.0
12/06/2118:10
Ethane
ug/L
ND 1.0
12/06/2118:10
Ethene
ug/L
ND 1.0
12/06/2118:10
LABORATORY CONTROL SAMPLE & LCSD:
2282094
2282095
Spike
LCS
LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD RPD Qualifiers
Methane
ug/L
380
360
360
95 95
70-130 0 30
Ethane
ug/L
97
100
100
107 106
70-130 1 30
Ethene
ug/L
120
130
130
108 108
70-130 1 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
Page 48 of 93

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 729060 Analysis Method: RSK-175
QC Batch Method: RSK-175 Analysis Description: Biodegradation Indicator Gases
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92574833012
METHOD BLANK: 2284245
Associated Lab Samples: 92574833012
Parameter Units
Methane ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 12/09/21 17:08
LABORATORY CONTROL SAMPLE & LCSD: 2284538 2284539
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Methane ug/L 380 370 370 96 97 70-130 1 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 729093 Analysis Method: RSK-175
QC Batch Method: RSK-175 Analysis Description: EPA RSK 175 CO2
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92574833008, 92574833009, 92574833010, 92574833012, 92574833013, 92574833014
METHOD BLANK: 2284464 Matrix: Water
Associated Lab Samples: 92574833008, 92574833009, 92574833010, 92574833012, 92574833013, 92574833014
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Carbon dioxide ug/L ND 900 12/10/21 09:54
LABORATORY CONTROL SAMPLE & LCSD: 2284465 2284466
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Carbon dioxide ug/L 8700 8630 8130 99 93 38-147 6 40
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 663537 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92574833001, 92574833006, 92574833007, 92574833012, 92574833014
METHOD BLANK: 3475930 Matrix: Water
Associated Lab Samples: 92574833001, 92574833006, 92574833007, 92574833012, 92574833014
Blank Reporting
Parameter Units Result Limit Analyzed
1,1,1-Trichloroethane
ug/L
ND
1.0
12/03/21 05:14
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/03/21 05:14
1,1,2-Trichloroethane
ug/L
ND
1.0
12/03/21 05:14
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
12/03/21 05:14
1,1-Dichloroethane
ug/L
ND
1.0
12/03/21 05:14
1,1-Dichloroethene
ug/L
ND
1.0
12/03/21 05:14
1,2,3-Trichlorobenzene
ug/L
ND
1.0
12/03/21 05:14
1,2,4-Trichlorobenzene
ug/L
ND
1.0
12/03/21 05:14
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/03/21 05:14
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/03/21 05:14
1,2-Dichlorobenzene
ug/L
ND
1.0
12/03/21 05:14
1,2-Dichloroethane
ug/L
ND
1.0
12/03/21 05:14
1,2-Dichloropropane
ug/L
ND
1.0
12/03/21 05:14
1,3-Dichlorobenzene
ug/L
ND
1.0
12/03/21 05:14
1,4-Dichlorobenzene
ug/L
ND
1.0
12/03/21 05:14
2-Butanone (MEK)
ug/L
ND
5.0
12/03/21 05:14
2-Hexanone
ug/L
ND
5.0
12/03/21 05:14
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/03/21 05:14
Acetone
ug/L
ND
25.0
12/03/21 05:14
Benzene
ug/L
ND
1.0
12/03/21 05:14
Bromochloromethane
ug/L
ND
1.0
12/03/21 05:14
Bromodichloromethane
ug/L
ND
1.0
12/03/21 05:14
Bromoform
ug/L
ND
1.0
12/03/21 05:14
Bromomethane
ug/L
ND
2.0
12/03/21 05:14
Carbon disulfide
ug/L
ND
2.0
12/03/21 05:14
Carbon tetrachloride
ug/L
ND
1.0
12/03/21 05:14
Chlorobenzene
ug/L
ND
1.0
12/03/21 05:14
Chloroethane
ug/L
ND
1.0
12/03/21 05:14
Chloroform
ug/L
ND
1.0
12/03/21 05:14
Chloromethane
ug/L
ND
1.0
12/03/21 05:14
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/03/21 05:14
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/03/21 05:14
Cyclohexane
ug/L
ND
1.0
12/03/21 05:14
Dibromochloromethane
ug/L
ND
1.0
12/03/21 05:14
Dichlorodifluoromethane
ug/L
ND
1.0
12/03/21 05:14
Ethylbenzene
ug/L
ND
1.0
12/03/21 05:14
Isopropylbenzene (Cumene)
ug/L
ND
1.0
12/03/21 05:14
Methyl acetate
ug/L
ND
10.0
12/03/21 05:14
Methyl-tert-butyl ether
ug/L
ND
1.0
12/03/21 05:14
Methylcyclohexane
ug/L
ND
10.0
12/03/21 05:14
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 51 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
METHOD BLANK: 3475930 Matrix: Water
Associated Lab Samples: 92574833001, 92574833006, 92574833007, 92574833012, 92574833014
Blank Reporting
Parameter Units Result Limit Analyzed
Methylene Chloride
ug/L
ND
5.0
12/03/21 05:14
Styrene
ug/L
ND
1.0
12/03/21 05:14
Tetrachloroethene
ug/L
ND
1.0
12/03/21 05:14
Toluene
ug/L
ND
1.0
12/03/21 05:14
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/03/21 05:14
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/03/21 05:14
Trichloroethene
ug/L
ND
1.0
12/03/21 05:14
Trichlorofluoromethane
ug/L
ND
1.0
12/03/21 05:14
Vinyl chloride
ug/L
ND
1.0
12/03/21 05:14
Xylene (Total)
ug/L
ND
1.0
12/03/21 05:14
1,2-Dichloroethane-d4 (S)
%
95
70-130
12/03/21 05:14
4-Bromofluorobenzene (S)
%
99
70-130
12/03/21 05:14
Toluene-d8 (S)
%
100
70-130
12/03/21 05:14
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3475931
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1-Trichloroethane
ug/L
50
49.6
99
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.7
105
70-130
1,1,2-Trichloroethane
ug/L
50
49.4
99
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
52.5
105
70-130
1,1-Dichloroethane
ug/L
50
50.0
100
70-130
1,1-Dichloroethene
ug/L
50
50.6
101
70-132
1,2,3-Trichlorobenzene
ug/L
50
53.4
107
70-134
1,2,4-Trichlorobenzene
ug/L
50
52.6
105
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
55.5
111
70-132
1,2-Dibromoethane (EDB)
ug/L
50
52.2
104
70-130
1,2-Dichlorobenzene
ug/L
50
50.8
102
70-130
1,2-Dichloroethane
ug/L
50
49.3
99
70-130
1,2-Dichloropropane
ug/L
50
51.7
103
70-130
1,3-Dichlorobenzene
ug/L
50
50.7
101
70-130
1,4-Dichlorobenzene
ug/L
50
51.2
102
70-130
2-Butanone (MEK)
ug/L
100
101
101
70-133
2-Hexanone
ug/L
100
110
110
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
105
105
70-130
Acetone
ug/L
100
101
101
70-144
Benzene
ug/L
50
49.4
99
70-130
Bromochloromethane
ug/L
50
49.5
99
70-130
Bromodichloromethane
ug/L
50
50.5
101
70-130
Bromoform
ug/L
50
50.5
101
70-131
Bromomethane
ug/L
50
55.9
112
30-177
Carbon disulfide
ug/L
50
50.8
102
70-133
Carbon tetrachloride
ug/L
50
49.8
100
70-130
Chlorobenzene
ug/L
50
51.5
103
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 52 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
LABORATORY CONTROL SAMPLE:
Parameter
3475931
Units
Spike LCS
Conc. Result
Chloroethane
ug/L
50
Chloroform
ug/L
50
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Cyclohexane
ug/L
50
Dibromochloromethane
ug/L
50
Dichlorodifluoromethane
ug/L
50
Ethylbenzene
ug/L
50
Isopropylbenzene (Cumene)
ug/L
50
Methyl acetate
ug/L
50
Methyl-tert-butyl ether
ug/L
50
Methylcyclohexane
ug/L
50
Methylene Chloride
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
47.0
94
46-131
48.9
98
70-130
50.5
101
49-130
50.4
101
70-130
49.6
99
70-130
53.0
106
70-131
53.0
106
70-130
54.8
110
52-134
52.4
105
70-130
54.6
109
70-130
51.8
104
70-131
48.8
98
70-130
51.6
103
70-130
47.4
95
68-130
53.6
107
70-130
50.3
101
70-130
49.5
99
70-130
50.6
101
70-130
49.6
99
70-130
49.2
98
70-130
49.0
98
61-130
53.7
107
59-142
157
105
70-130
96
70-130
103
70-130
100
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3475932
MS
92575056002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3475933
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
20
20
20.5
20.3
102
102
70-148
1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.2
21.0
106
105
70-131
1
1,1,2-Trichloroethane
ug/L
ND
20
20
20.8
20.5
104
102
70-136
1
1,1,2-Trichlorotrifluoroethane
ug/L
ND
20
20
22.4
21.0
112
105
70-154
6
1,1-Dichloroethane
ug/L
ND
20
20
20.5
20.4
103
102
70-147
1
1,1-Dichloroethene
ug/L
ND
20
20
19.8
20.1
99
101
70-158
2
1,2,3-Trichlorobenzene
ug/L
ND
20
20
22.1
21.6
110
108
68-140
2
1,2,4-Trichlorobenzene
ug/L
ND
20
20
22.1
21.8
111
109
70-139
1
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.2
21.4
106
107
69-136
0
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.3
21.3
107
106
70-137
0
1,2-Dichlorobenzene
ug/L
ND
20
20
22.0
21.5
110
108
70-133
2
1,2-Dichloroethane
ug/L
ND
20
20
18.9
18.9
94
95
67-138
0
1,2-Dichloropropane
ug/L
ND
20
20
21.6
21.5
108
107
70-138
1
1,3-Dichlorobenzene
ug/L
ND
20
20
21.9
21.8
110
109
70-133
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
Page 53 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3475932
3475933
MS
MSD
92575056002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
20
20
22.3
21.8
112
109
70-133
2
2-Butanone (MEK)
ug/L
ND
40
40
35.4
35.6
88
89
61-147
1
2-Hexanone
ug/L
ND
40
40
40.1
39.2
100
98
67-139
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
38.7
38.7
97
97
67-136
0
Acetone
ug/L
ND
40
40
35.7
35.3
89
88
55-159
1
Benzene
ug/L
ND
20
20
21.8
21.4
109
107
67-150
2
Bromochloromethane
ug/L
ND
20
20
20.4
20.0
102
100
70-146
2
Bromodichloromethane
ug/L
ND
20
20
20.9
21.0
105
105
70-138
0
Bromoform
ug/L
ND
20
20
19.7
19.6
99
98
57-138
1
Bromomethane
ug/L
ND
20
20
18.9
18.6
94
93
10-200
2 v3
Carbon disulfide
ug/L
ND
20
20
20.4
19.9
102
100
70-152
3
Carbon tetrachloride
ug/L
ND
20
20
21.8
22.0
109
110
70-147
1
Chlorobenzene
ug/L
ND
20
20
22.1
21.9
110
110
70-137
1
Chloroethane
ug/L
ND
20
20
21.1
20.4
105
102
51-166
4 v3
Chloroform
ug/L
ND
20
20
19.3
19.0
97
95
70-144
2
Chloromethane
ug/L
ND
20
20
21.0
20.6
105
103
24-161
2
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.1
20.0
100
100
67-148
0
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.0
20.8
105
104
70-142
1
Cyclohexane
ug/L
ND
20
20
20.9
21.1
104
105
70-151
1
Dibromochloromethane
ug/L
ND
20
20
20.9
20.9
104
104
68-138
0
Dichlorodifluoromethane
ug/L
ND
20
20
21.7
21.2
108
106
43-155
2
Ethylbenzene
ug/L
ND
20
20
22.4
22.2
112
111
68-143
1
Isopropylbenzene (Cumene)
ug/L
ND
20
20
23.1
22.9
115
114
70-136
1
Methyl acetate
ug/L
ND
20
20
19.1
19.3
95
96
55-149
1
Methyl-tert-butyl ether
ug/L
ND
20
20
19.5
19.0
97
95
59-156
3
Methylcyclohexane
ug/L
ND
20
20
22.0
21.9
110
109
70-142
1
Methylene Chloride
ug/L
ND
20
20
19.3
19.0
97
95
64-148
2
Styrene
ug/L
ND
20
20
21.8
21.3
109
107
70-136
2
Tetrachloroethene
ug/L
ND
20
20
22.0
22.0
110
110
70-139
0
Toluene
ug/L
ND
20
20
21.3
21.3
107
106
47-157
0
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.5
20.6
107
103
70-149
4
trans- 1,3-Dichloropropene
ug/L
ND
20
20
20.5
20.2
103
101
70-138
2
Trichloroethene
ug/L
ND
20
20
21.9
21.4
109
107
70-149
2
Trichlorofluoromethane
ug/L
ND
20
20
18.0
17.9
90
89
61-154
1
Vinyl chloride
ug/L
ND
20
20
22.4
22.2
112
111
55-172
0
Xylene (Total)
ug/L
ND
60
60
67.1
66.2
112
110
66-145
1
1,2-Dichloroethane-d4 (S)
%
83
84
70-130
4-Bromofluorobenzene (S)
%
99
99
70-130
Toluene-d8(S)
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
Page 54 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 663751 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92574833008, 92574833009, 92574833015, 92574833017
METHOD BLANK: 3476861 Matrix: Water
Associated Lab Samples: 92574833008, 92574833009, 92574833015, 92574833017
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
1.0
12/03/21 22:44
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/03/21 22:44
1,1,2-Trichloroethane
ug/L
ND
1.0
12/03/21 22:44
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
12/03/21 22:44
1,1-Dichloroethane
ug/L
ND
1.0
12/03/21 22:44
1,1-Dichloroethene
ug/L
ND
1.0
12/03/21 22:44
1,2,3-Trichlorobenzene
ug/L
ND
1.0
12/03/21 22:44
1,2,4-Trichlorobenzene
ug/L
ND
1.0
12/03/21 22:44
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/03/21 22:44
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/03/21 22:44
1,2-Dichlorobenzene
ug/L
ND
1.0
12/03/21 22:44
1,2-Dichloroethane
ug/L
ND
1.0
12/03/21 22:44
1,2-Dichloropropane
ug/L
ND
1.0
12/03/21 22:44
1,3-Dichlorobenzene
ug/L
ND
1.0
12/03/21 22:44
1,4-Dichlorobenzene
ug/L
ND
1.0
12/03/21 22:44
2-Butanone (MEK)
ug/L
ND
5.0
12/03/21 22:44
2-Hexanone
ug/L
ND
5.0
12/03/21 22:44
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/03/21 22:44
Acetone
ug/L
ND
25.0
12/03/21 22:44
Benzene
ug/L
ND
1.0
12/03/21 22:44
Bromochloromethane
ug/L
ND
1.0
12/03/21 22:44
Bromodichloromethane
ug/L
ND
1.0
12/03/21 22:44
Bromoform
ug/L
ND
1.0
12/03/21 22:44
Bromomethane
ug/L
ND
2.0
12/03/21 22:44
Carbon disulfide
ug/L
ND
2.0
12/03/21 22:44
Carbon tetrachloride
ug/L
ND
1.0
12/03/21 22:44
Chlorobenzene
ug/L
ND
1.0
12/03/21 22:44
Chloroethane
ug/L
ND
1.0
12/03/21 22:44
Chloroform
ug/L
ND
1.0
12/03/21 22:44
Chloromethane
ug/L
ND
1.0
12/03/21 22:44
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/03/21 22:44
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/03/21 22:44
Cyclohexane
ug/L
ND
1.0
12/03/21 22:44
Dibromochloromethane
ug/L
ND
1.0
12/03/21 22:44
Dichlorodifluoromethane
ug/L
ND
1.0
12/03/21 22:44
Ethylbenzene
ug/L
ND
1.0
12/03/21 22:44
Isopropylbenzene (Cumene)
ug/L
ND
1.0
12/03/21 22:44
Methyl acetate
ug/L
ND
10.0
12/03/21 22:44
Methyl-tert-butyl ether
ug/L
ND
1.0
12/03/21 22:44
Methylcyclohexane
ug/L
ND
10.0
12/03/21 22:44
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 55 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
METHOD BLANK: 3476861 Matrix: Water
Associated Lab Samples: 92574833008, 92574833009, 92574833015, 92574833017
Blank Reporting
Parameter Units Result Limit
Analyzed
Methylene Chloride
ug/L
ND
5.0
12/03/21 22:44
Styrene
ug/L
ND
1.0
12/03/21 22:44
Tetrachloroethene
ug/L
ND
1.0
12/03/21 22:44
Toluene
ug/L
ND
1.0
12/03/21 22:44
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/03/21 22:44
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/03/21 22:44
Trichloroethene
ug/L
ND
1.0
12/03/21 22:44
Trichlorofluoromethane
ug/L
ND
1.0
12/03/21 22:44
Vinyl chloride
ug/L
ND
1.0
12/03/21 22:44
Xylene (Total)
ug/L
ND
1.0
12/03/21 22:44
1,2-Dichloroethane-d4 (S)
%
103
70-130
12/03/21 22:44
4-Bromofluorobenzene (S)
%
105
70-130
12/03/21 22:44
Toluene-d8 (S)
%
102
70-130
12/03/21 22:44
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3476862
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1-Trichloroethane
ug/L
50
43.4
87
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.8
100
70-130
1,1,2-Trichloroethane
ug/L
50
49.7
99
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
43.6
87
70-130
1,1-Dichloroethane
ug/L
50
48.1
96
70-130
1,1-Dichloroethene
ug/L
50
44.5
89
70-132
1,2,3-Trichlorobenzene
ug/L
50
44.4
89
70-134
1,2,4-Trichlorobenzene
ug/L
50
44.2
88
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
45.8
92
70-132
1,2-Dibromoethane (EDB)
ug/L
50
47.7
95
70-130
1,2-Dichlorobenzene
ug/L
50
46.6
93
70-130
1,2-Dichloroethane
ug/L
50
48.6
97
70-130
1,2-Dichloropropane
ug/L
50
52.3
105
70-130
1,3-Dichlorobenzene
ug/L
50
45.3
91
70-130
1,4-Dichlorobenzene
ug/L
50
46.6
93
70-130
2-Butanone (MEK)
ug/L
100
104
104
70-133
2-Hexanone
ug/L
100
105
105
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
115
115
70-130
Acetone
ug/L
100
109
109
70-144
Benzene
ug/L
50
48.7
97
70-130
Bromochloromethane
ug/L
50
44.6
89
70-130
Bromodichloromethane
ug/L
50
48.7
97
70-130
Bromoform
ug/L
50
43.6
87
70-131
Bromomethane
ug/L
50
47.3
95
30-177
Carbon disulfide
ug/L
50
45.8
92
70-133
Carbon tetrachloride
ug/L
50
45.1
90
70-130
Chlorobenzene
ug/L
50
46.1
92
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 56 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
LABORATORY CONTROL SAMPLE:
Parameter
3476862
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Chloroethane
ug/L
50
54.7
109
46-131
Chloroform
ug/L
50
47.1
94
70-130
Chloromethane
ug/L
50
47.8
96
49-130
cis-1,2-Dichloroethene
ug/L
50
47.9
96
70-130
cis-1,3-Dichloropropene
ug/L
50
50.8
102
70-130
Cyclohexane
ug/L
50
47.9
96
70-131
Dibromochloromethane
ug/L
50
44.3
89
70-130
Dichlorodifluoromethane
ug/L
50
46.3
93
52-134
Ethylbenzene
ug/L
50
47.0
94
70-130
Isopropylbenzene (Cumene)
ug/L
50
47.5
95
70-130
Methyl acetate
ug/L
50
47.1
94
70-131
Methyl-tert-butyl ether
ug/L
50
46.8
94
70-130
Methylcyclohexane
ug/L
50
52.1
104
70-130
Methylene Chloride
ug/L
50
48.4
97
68-130
Styrene
ug/L
50
47.5
95
70-130
Tetrachloroethene
ug/L
50
41.8
84
70-130
Toluene
ug/L
50
49.2
98
70-130
trans-1,2-Dichloroethene
ug/L
50
48.8
98
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.9
100
70-130
Trichloroethene
ug/L
50
45.0
90
70-130
Trichlorofluoromethane
ug/L
50
42.7
85
61-130
Vinyl chloride
ug/L
50
47.7
95
59-142
Xylene (Total)
ug/L
150
140
93
70-130
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
103
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3476863
MS
92574833009 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3476864
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
200
200
208
203
104
102
70-148
2
1,1,2,2-Tetrachloroethane
ug/L
ND
200
200
201
205
101
102
70-131
2
1,1,2-Trichloroethane
ug/L
ND
200
200
206
210
103
105
70-136
2
1,1,2-Trichlorotrifluoroethane
ug/L
ND
200
200
202
197
101
98
70-154
3
1,1-Dichloroethane
ug/L
ND
200
200
230
221
115
111
70-147
4
1,1-Dichloroethene
ug/L
ND
200
200
215
210
108
105
70-158
3
1,2,3-Trichlorobenzene
ug/L
ND
200
200
176
213
88
106
68-140
19
1,2,4-Trichlorobenzene
ug/L
ND
200
200
170
205
85
103
70-139
19
1,2-Dibromo-3-chloropropane
ug/L
ND
200
200
177
214
89
107
69-136
19
1,2-Dibromoethane (EDB)
ug/L
ND
200
200
199
202
99
101
70-137
2
1,2-Dichlorobenzene
ug/L
ND
200
200
192
239
96
119
70-133
22
1,2-Dichloroethane
ug/L
ND
200
200
221
216
110
108
67-138
2
1,2-Dichloropropane
ug/L
ND
200
200
239
235
119
118
70-138
2
1,3-Dichlorobenzene
ug/L
ND
200
200
191
187
96
93
70-133
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
Page 57 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3476863
3476864
MS
MSD
92574833009
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
200
200
202
193
101
97
70-133
5
2-Butanone (MEK)
ug/L
504
400
400
983
960
120
114
61-147
2
2-Hexanone
ug/L
ND
400
400
430
469
108
117
67-139
9
4-Methyl-2-pentanone (MIBK)
ug/L
ND
400
400
501
505
117
118
67-136
1
Acetone
ug/L
3560
400
400
4050
4020
121
114
55-159
1 E
Benzene
ug/L
ND
200
200
228
224
112
109
67-150
2
Bromochloromethane
ug/L
ND
200
200
209
204
104
102
70-146
2
Bromodichloromethane
ug/L
ND
200
200
210
210
105
105
70-138
0
Bromoform
ug/L
ND
200
200
174
180
87
90
57-138
3
Bromomethane
ug/L
ND
200
200
112
149
56
75
10-200
28
Carbon disulfide
ug/L
ND
200
200
209
202
104
101
70-152
3
Carbon tetrachloride
ug/L
ND
200
200
203
200
102
100
70-147
2
Chlorobenzene
ug/L
ND
200
200
198
195
99
98
70-137
1
Chloroethane
ug/L
22.3
200
200
266
267
122
122
51-166
0
Chloroform
ug/L
ND
200
200
206
206
103
103
70-144
0
Chloromethane
ug/L
ND
200
200
219
223
110
111
24-161
1
cis-1,2-Dichloroethene
ug/L
ND
200
200
218
213
109
107
67-148
2
cis-1,3-Dichloropropene
ug/L
ND
200
200
203
206
102
103
70-142
1
Cyclohexane
ug/L
ND
200
200
226
214
113
107
70-151
5
Dibromochloromethane
ug/L
ND
200
200
187
189
94
94
68-138
1
Dichlorodifluoromethane
ug/L
ND
200
200
210
203
105
102
43-155
3
Ethylbenzene
ug/L
ND
200
200
206
205
103
103
68-143
0
Isopropylbenzene (Cumene)
ug/L
ND
200
200
200
206
100
103
70-136
3
Methyl acetate
ug/L
ND
200
200
207
204
103
102
55-149
1
Methyl-tert-butyl ether
ug/L
ND
200
200
198
188
99
94
59-156
5
Methylcyclohexane
ug/L
ND
200
200
229
222
114
111
70-142
3
Methylene Chloride
ug/L
ND
200
200
264
257
109
106
64-148
3
Styrene
ug/L
ND
200
200
198
202
99
101
70-136
2
Tetrachloroethene
ug/L
ND
200
200
184
183
92
91
70-139
1
Toluene
ug/L
ND
200
200
226
223
109
107
47-157
1
trans-1,2-Dichloroethene
ug/L
ND
200
200
209
214
104
107
70-149
3
trans- 1,3-Dichloropropene
ug/L
ND
200
200
196
199
98
100
70-138
2
Trichloroethene
ug/L
ND
200
200
205
203
102
101
70-149
1
Trichlorofluoromethane
ug/L
ND
200
200
199
194
100
97
61-154
3
Vinyl chloride
ug/L
ND
200
200
227
224
113
112
55-172
1
Xylene (Total)
ug/L
ND
600
600
621
608
104
101
66-145
2
1,2-Dichloroethane-d4 (S)
%
101
100
70-130
4-Bromofluorobenzene (S)
%
101
103
70-130
Toluene-d8(S)
%
103
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
Page 58 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 662966 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92574833002, 92574833003, 92574833004, 92574833005, 92574833006, 92574833007, 92574833008,
92574833009,92574833010,92574833011,92574833012,92574833014,92574833015,92574833016,
92574833017
METHOD BLANK: 3473016 Matrix: Water
Associated Lab Samples: 92574833002, 92574833003, 92574833004, 92574833005, 92574833006, 92574833007, 92574833008,
92574833009,92574833010,92574833011,92574833012,92574833014,92574833015,92574833016,
92574833017
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,4-Dioxane (p-Dioxane) ug/L ND 2.0 12/01/21 00:23
1,2-Dichloroethane-d4 (S) % 119 70-130 12/01/21 00:23
Toluene-d8 (S) % 121 66-133 12/01/21 00:23
LABORATORY CONTROL SAMPLE: 3473017
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 18.3 91 70-130
1,2-Dichloroethane-d4 (S) % 114 70-130
Toluene-d8(S) % 121 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3473018
3473019
MS
MSD
92574833002 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 19.2
19.0 96
95
64-141 1
1,2-Dichloroethane-d4 (S)
%
106
102
70-130
Toluene-d8(S)
%
104
104
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 59 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 663156 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92574833013
METHOD BLANK: 3473881
Matrix:
Water
Associated Lab Samples: 92574833013
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
12/01/21 15:13
1,2-Dichloroethane-d4 (S)
%
100
70-130
12/01/21 15:13
Toluene-d8 (S)
%
102
66-133
12/01/21 15:13
LABORATORY CONTROL SAMPLE: 3473882
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 20.5 102 70-130
1,2-Dichloroethane-d4 (S) % 101 70-130
Toluene-d8(S) % 102 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3473883
3473884
MS
MSD
92574833013 Spike
Spike MS MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 138 50
50 183 178 90
79
64-141 3
1,2-Dichloroethane-d4 (S)
%
102
101
70-130
Toluene-d8(S)
%
102
103
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 60 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 663000 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92574833002, 92574833003, 92574833004, 92574833005, 92574833006, 92574833007, 92574833008,
92574833009,92574833010,92574833011,92574833012,92574833013,92574833014,92574833015,
92574833017
METHOD BLANK: 3473090 Matrix: Water
Associated Lab Samples: 92574833002, 92574833003, 92574833004, 92574833005, 92574833006, 92574833007, 92574833008,
92574833009,92574833010,92574833011,92574833012,92574833013,92574833014,92574833015,
92574833017
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Biphenyl (Diphenyl)
ug/L
ND
10.0
12/01/21 10:15
Diphenyl ether (Phenyl ether)
ug/L
ND
10.0
12/01/21 10:15
2,4,6-Tribromophenol (S)
%
71
10-144
12/01/21 10:15
2-Fluorobiphenyl (S)
%
55
10-130
12/01/21 10:15
2-Fluorophenol (S)
%
46
10-130
12/01/21 10:15
Nitrobenzene-d5 (S)
%
66
10-144
12/01/21 10:15
Phenol-d6 (S)
%
34
10-130
12/01/21 10:15
Terphenyl-d14 (S)
%
77
34-163
12/01/21 10:15
LABORATORY CONTROL SAMPLE:
Parameter
3473091
Units
Spike LCS LCS
Conc. Result % Rec
% Rec
Limits Qualifiers
Biphenyl (Diphenyl)
ug/L
50 30.3 61
31-130
Diphenyl ether (Phenyl ether)
ug/L
50 31.2 62
25-130
2,4,6-Tribromophenol (S)
%
86
10-144
2-Fluorobiphenyl (S)
%
65
10-130
2-Fluorophenol(S)
%
49
10-130
Nitrobenzene-d5 (S)
%
72
10-144
Phenol-d6 (S)
%
37
10-130
Terphenyl-d14 (S)
%
80
34-163
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3473092
3473093
MS
MSD
92574833002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Biphenyl (Diphenyl)
ug/L
ND
90.9
90.9
83.9
65.8
92
72
17-130 24
Diphenyl ether (Phenyl ether)
ug/L
ND
90.9
90.9
83.0
64.9
91
71
16-130 24
2,4,6-Tribromophenol (S)
%
103
95
10-144
2-Fluorobiphenyl (S)
%
82
67
10-130
2-Fluorophenol(S)
%
76
62
10-130
Nitrobenzene-d5(S)
%
91
74
10-144
Phenol-d6 (S)
%
66
54
10-130
Terphenyl-d14(S)
%
84
86
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
Page 61 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 662970 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92574833006,92574833007,92574833008,92574833009,92574833010,92574833011,92574833012,
92574833013,92574833014,92574833015
METHOD BLANK: 3473033 Matrix: Water
Associated Lab Samples: 92574833006,92574833007,92574833008,92574833009,92574833010,92574833011,92574833012,
92574833013,92574833014,92574833015
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.040 12/01/21 00:43
Nitrogen, Nitrite mg/L ND 0.040 12/01/21 00:43
LABORATORY CONTROL SAMPLE: 3473034
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 101 90-110
Nitrogen, Nitrite mg/L 1 1.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3473035
3473036
MS
MSD
92574833006 Spike
Spike MS
MSD MS
MSD % Rec
Parameter
Units
Result Conc.
Conc. Result
Result % Rec
% Rec Limits RPD Qual
Nitrogen, Nitrate
mg/L
ND 1.5
1.5 1.5
1.4 97
96 90-110 0
Nitrogen, Nitrite
mg/L
ND 1
1 0.98
0.98 96
96 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3473037
3473038
MS
MSD
92574833011 Spike
Spike MS
MSD MS MSD
% Rec
Parameter
Units
Result Conc.
Conc. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate
mg/L
ND 1.5
1.5 1.5
1.5 102 103
90-110 1
Nitrogen, Nitrite
mg/L
ND 1
1 1.0
1.0 104 104
90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
Page 62 of 93

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 662971
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92574833016
METHOD BLANK: 3473039
Matrix: Water
Associated Lab Samples: 92574833016
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L
ND 0.040 12/01/21 01:15
Nitrogen, Nitrite mg/L
ND 0.040 12/01/21 01:15
LABORATORY CONTROL SAMPLE: 3473040
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L
1.5 1.5 97 90-110
Nitrogen, Nitrite mg/L
1 0.95 95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3473041 3473042
MS MSD
92574796002
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate mg/L 3.3
1.5 1.5 5.1 5.5 119 147
90-110 8
Nitrogen, Nitrite mg/L ND
1 1 1.0 1.0 103 102
90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
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[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 663096 Analysis Method: EPA 9056A
QC Batch Method: EPA 9056A Analysis Description: 9056 IC anions 28 Days
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92574833006,92574833007,92574833008,92574833009,92574833010,92574833011,92574833012,
92574833013,92574833014,92574833015
METHOD BLANK: 3473539 Matrix: Water
Associated Lab Samples: 92574833006,92574833007,92574833008,92574833009,92574833010,92574833011,92574833012,
92574833013,92574833014,92574833015
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfate mg/L ND 1.0 12/01/2116:26
LABORATORY CONTROL SAMPLE: 3473540
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfate mg/L 50 49.6 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3473541 3473542
MS MSD
92574624001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 2.2 50 50 51.5 53.9 99 103 90-110 4
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3473543 3473544
MS MSD
92574833006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L ND 50 50 49.9 51.1 100 102 90-110 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
816 Durst Avenue East
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[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 663104 Analysis Method: EPA 9056A
QC Batch Method: EPA 9056A Analysis Description: 9056 IC anions 28 Days
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92574833016
METHOD BLANK: 3473583
Associated Lab Samples: 92574833016
Parameter Units
Sulfate mg/L
LABORATORY CONTROL SAMPLE: 3473584
Parameter Units
Sulfate mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 12/02/21 00:09
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
50 49.8 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3473585 3473586
MS MSD
92574749001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 0.911 50 50 51.8 53.4 102 105 90-110 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
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[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 663123 Analysis Method: EPA 9060A
QC Batch Method: EPA 9060A Analysis Description: 9060 TOC, AVL
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92574833008, 92574833009, 92574833010, 92574833012, 92574833013, 92574833014
METHOD BLANK: 3473693
Matrix:
Water
Associated Lab Samples: 92574833008, 92574833009, 92574833010, 92574833012, 92574833013,
92574833014
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mean Total Organic Carbon
mg/L
ND
1.0
12/01/21 15:51
Total Organic Carbon
mg/L
ND
1.0
12/01/21 15:51
Total Organic Carbon
mg/L
ND
1.0
12/01/21 15:51
Total Organic Carbon
mg/L
ND
1.0
12/01/21 15:51
Total Organic Carbon
mg/L
ND
1.0
12/01/21 15:51
LABORATORY CONTROL SAMPLE:
3473694
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Mean Total Organic Carbon
mg/L
25
26.6
106
75-125
Total Organic Carbon
mg/L
25
25.9
104
75-125
Total Organic Carbon
mg/L
25
26.5
106
75-125
Total Organic Carbon
mg/L
25
27.0
108
75-125
Total Organic Carbon
mg/L
25
26.8
107
75-125
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3473695
3473696
MS
MSD
92574554002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Mean Total Organic Carbon
mg/L
ND
25
25
27.0
27.1
107
107
75-125
1
Total Organic Carbon
mg/L
ND
25
25
26.8
27.1
106
107
75-125
1
Total Organic Carbon
mg/L
ND
25
25
27.2
27.2
108
108
75-125
0
Total Organic Carbon
mg/L
ND
25
25
26.5
26.7
105
105
75-125
1
Total Organic Carbon
mg/L
ND
25
25
27.4
27.4
108
109
75-125
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3473697
3473698
MS
MSD
92573383001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Mean Total Organic Carbon
mg/L
ND
25
25
26.9
27.3
106
108
75-125
1
Total Organic Carbon
mg/L
ND
25
25
27.1
27.3
106
107
75-125
1
Total Organic Carbon
mg/L
ND
25
25
27.0
27.4
107
108
75-125
2
Total Organic Carbon
mg/L
ND
25
25
26.4
27.0
104
106
75-125
2
Total Organic Carbon
mg/L
ND
25
25
27.2
27.7
107
109
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 729099 Analysis Method: AM23G
QC Batch Method: AM23G Analysis Description: Low Level Volatile Fatty Acids
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92574833010, 92574833012, 92574833013, 92574833014
METHOD BLANK: 2284479 Matrix: Water
Associated Lab Samples: 92574833010, 92574833012, 92574833013, 92574833014
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Acetic Acid mg/L ND 0.50 12/10/2114:13
LABORATORY CONTROL SAMPLE & LCSD: 2284480 2284481
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Acetic Acid mg/L 2 1.9 1.8 97 92 70-130 5 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
QC Batch: 729475 Analysis Method: AM23G
QC Batch Method: AM23G Analysis Description: Low Level Volatile Fatty Acids
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92574833008, 92574833009
METHOD BLANK: 2286470 Matrix: Water
Associated Lab Samples: 92574833008, 92574833009
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Acetic Acid mg/L ND 0.50 12/14/2110:17
LABORATORY CONTROL SAMPLE & LCSD: 2286471 2286487
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Acetic Acid mg/L 2 1.7 1.8 85 90 70-130 5 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC.
Page 68 of 93

Pace Analytical Services, LLC
ceAnalXical ® Greenwood,urst SC 2 East
Grenwood, SC 29649
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QUALIFIERS
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
H3 Sample was received or analysis requested beyond the recognized method holding time.
SO Surrogate recovery outside laboratory control limits.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
NRLF-NOVEMBER 2021
92574833
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method Batch
92574833006
B-24B-112921
SM 4500-P E-2011
663113
92574833007
B-24A-112921
SM 4500-P E-2011
663113
92574833008
B-23A-112921
SM 4500-P E-2011
663113
92574833009
B-23B-112921
SM 4500-P E-2011
663113
92574833010
B-17C-112921
SM 4500-P E-2011
663113
92574833011
B-12-112921
SM 4500-P E-2011
663113
92574833012
B-22B-113021
SM 4500-P E-2011
663113
92574833013
B-17B-113021
SM 4500-P E-2011
663113
92574833014
B-22A-113021
SM 4500-P E-2011
663113
92574833015
B-09C-113021
SM 4500-P E-2011
663113
92574833016
B-21B-113021
SM 4500-P E-2011
663113
92574833002
SW-7-112921
EPA 8015 Alcohol -Glycol
653917
92574833003
SW-5-112921
EPA 8015 Alcohol -Glycol
653917
92574833004
SW-3-112921
EPA 8015 Alcohol -Glycol
653917
92574833005
SW-8-112921
EPA 8015 Alcohol -Glycol
653917
92574833008
B-23A-112921
EPA 8015 Alcohol -Glycol
653917
92574833009
B-23B-112921
EPA 8015 Alcohol -Glycol
653917
92574833015
B-09C-113021
EPA 8015 Alcohol -Glycol
653917
92574833018
B-23A-112921
H2
AM20GAX
728838
92574833019
B-23B-112921
H2
AM20GAX
728838
92574833020
B-17C-112921
H2
AM20GAX
728838
92574833021
B-22B-113021
H2
AM20GAX
728838
92574833022
B-17B-113021
H2
AM20GAX
728838
92574833023
B-22A-113021
H2
AM20GAX
728838
92574833008
B-23A-112921
RSK-175
728703
92574833009
B-23B-112921
RSK-175
728703
92574833010
B-17C-112921
RSK-175
728703
92574833012
B-22B-113021
RSK-175
728703
92574833012
B-22B-113021
RSK-175
729060
92574833013
B-17B-113021
RSK-175
728703
92574833014
B-22A-113021
RSK-175
728703
92574833008
B-23A-112921
RSK-175
729093
92574833009
B-23B-112921
RSK-175
729093
92574833010
B-17C-112921
RSK-175
729093
92574833012
B-22B-113021
RSK-175
729093
92574833013
B-17B-113021
RSK-175
729093
92574833014
B-22A-113021
RSK-175
729093
92574833002
SW-7-112921
EPA 3510C
663000
EPA 8270E 663056
92574833003
SW-5-112921
EPA 3510C
663000
EPA 8270E 663056
92574833004
SW-3-112921
EPA 3510C
663000
EPA 8270E 663056
92574833005
SW-8-112921
EPA 3510C
663000
EPA 8270E 663056
92574833006
B-24B-112921
EPA 3510C
663000
EPA 8270E 663056
92574833007
B-24A-112921
EPA 3510C
663000
EPA 8270E 663056
92574833008
B-23A-112921
EPA 3510C
663000
EPA 8270E 663056
92574833009
B-23B-112921
EPA 3510C
663000
EPA 8270E 663056
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
Date: 12/21 /2021
11:18 AM
without the written consent of Pace Analytical Services, LLC.
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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
NRLF-NOVEMBER 2021
Pace Project No.:
92574833
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method Batch
92574833010
B-17C-112921
EPA 3510C
663000
EPA 8270E 663056
92574833011
B-12-112921
EPA 3510C
663000
EPA 8270E 663056
92574833012
B-2213-113021
EPA 3510C
663000
EPA 8270E 663056
92574833013
B-17B-113021
EPA 3510C
663000
EPA 8270E 663056
92574833014
B-22A-113021
EPA 3510C
663000
EPA 8270E 663056
92574833015
B-09C-113021
EPA 3510C
663000
EPA 8270E 663056
92574833017
B-99C-113021
EPA 3510C
663000
EPA 8270E 663056
92574833001
TRIP BLANK-01-112921
EPA 8260D
663537
92574833006
B-2413-112921
EPA 8260D
663537
92574833007
B-24A-112921
EPA 8260D
663537
92574833008
B-23A-112921
EPA 8260D
663751
92574833009
B-2313-112921
EPA 8260D
663751
92574833012
B-2213-113021
EPA 8260D
663537
92574833014
B-22A-113021
EPA 8260D
663537
92574833015
B-09C-113021
EPA 8260D
663751
92574833017
B-99C-113021
EPA 8260D
663751
92574833002
SW-7-112921
EPA 8260D Mod.
662966
92574833003
SW-5-112921
EPA 8260D Mod.
662966
92574833004
SW-3-112921
EPA 8260D Mod.
662966
92574833005
SW-8-112921
EPA 8260D Mod.
662966
92574833006
B-2413-112921
EPA 8260D Mod.
662966
92574833007
B-24A-112921
EPA 8260D Mod.
662966
92574833008
B-23A-112921
EPA 8260D Mod.
662966
92574833009
B-2313-112921
EPA 8260D Mod.
662966
92574833010
B-17C-112921
EPA 8260D Mod.
662966
92574833011
B-12-112921
EPA 8260D Mod.
662966
92574833012
B-2213-113021
EPA 8260D Mod.
662966
92574833013
B-17B-113021
EPA 8260D Mod.
663156
92574833014
B-22A-113021
EPA 8260D Mod.
662966
92574833015
B-09C-113021
EPA 8260D Mod.
662966
92574833016
B-21 B-113021
EPA 8260D Mod.
662966
92574833017
B-99C-113021
EPA 8260D Mod.
662966
92574833006
B-2413-112921
EPA 353.2 Rev 2.0 1993
662970
92574833007
B-24A-112921
EPA 353.2 Rev 2.0 1993
662970
92574833008
B-23A-112921
EPA 353.2 Rev 2.0 1993
662970
92574833009
B-2313-112921
EPA 353.2 Rev 2.0 1993
662970
92574833010
B-17C-112921
EPA 353.2 Rev 2.0 1993
662970
92574833011
B-12-112921
EPA 353.2 Rev 2.0 1993
662970
92574833012
B-2213-113021
EPA 353.2 Rev 2.0 1993
662970
92574833013
B-17B-113021
EPA 353.2 Rev 2.0 1993
662970
92574833014
B-22A-113021
EPA 353.2 Rev 2.0 1993
662970
92574833015
B-09C-113021
EPA 353.2 Rev 2.0 1993
662970
92574833016
B-21 B-113021
EPA 353.2 Rev 2.0 1993
662971
92574833006
B-2413-112921
EPA 9056A
663096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/21 /2021 11:18 AM without the written consent of Pace Analytical Services, LLC. Page 71 of 93

lreAnalyilcal®
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Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NRLF-NOVEMBER 2021
Pace Project No.: 92574833
Lab ID Sample ID QC Batch Method QC Batch
92574833007
B-24A-112921
EPA 9056A
663096
92574833008
B-23A-112921
EPA 9056A
663096
92574833009
B-23B-112921
EPA 9056A
663096
92574833010
B-17C-112921
EPA 9056A
663096
92574833011
B-12-112921
EPA 9056A
663096
92574833012
B-22B-113021
EPA 9056A
663096
92574833013
B-17B-113021
EPA 9056A
663096
92574833014
B-22A-113021
EPA 9056A
663096
92574833015
B-09C-113021
EPA 9056A
663096
92574833016
B-21B-113021
EPA 9056A
663104
92574833008
B-23A-112921
EPA 9060A
663123
92574833009
B-23B-112921
EPA 9060A
663123
92574833010
B-17C-112921
EPA 9060A
663123
92574833012
B-22B-113021
EPA 9060A
663123
92574833013
B-17B-113021
EPA 9060A
663123
92574833014
B-22A-113021
EPA 9060A
663123
92574833008
B-23A-112921
AM23G
729475
92574833009
B-23B-112921
AM23G
729475
92574833010
B-17C-112921
AM23G
729099
92574833012
B-22B-113021
AM23G
729099
92574833013
B-17B-113021
AM23G
729099
92574833014
B-22A-113021
AM23G
729099
Date: 12/21 /2021 11:18 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 72 of 93

Document Name: Document Revised: November 15, 2021
Sample Condition Upon Receipt (SCUR) Page I of 2
Are YAC31 Document No.: Issuing Authority:
F-CAR-CS-033-Rev.08 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville&] Raleigh❑ MechaniMechanicsville[]Atlanta[]Kernersville❑
SampleClient Name: WO# : 92574833
• .. , ,� l_ (J/J� Project — A41,; n�. U�k ti:
Courier: ❑Fed Ex ❑UPS ❑U5P5 []client
❑ Commercial `[Pace ❑Other: 92574833
Custody Seal Present? ❑Yes E3No Seats Intact? ❑Yes ❑No
Date/Initials Person Examining Contents: YY�)
Packing Material: 198ubble Wrap '91Bubble Bags []None ❑ other Biological Tissue Frozen?
Thermorgeter; []Yes []No QN/A
�� � (:)6- []Wet []Blue []None
IR Gun ID: c.. Vli Type of Ice:
Correction Factor:
Cooler Temp: �' Add/Subtract (°C) % Temp should be above freezing to VC
L 1 ❑Samples out of temp criteria.53mples on ice, cooling process
Coal er-Temp-Corrected-('C-)- b gu
USDA Regulated Soil (`gN/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
[]Yes ❑Na including Hawaii and Puerto Rico)? []Yes [:]No
Comm ents/DIscreo ancy,
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (c72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match COL?
-Includes Date/Time/ID/Analysis Mat
Headspace In VOA Vials (>S-6mm)?
Trip Blank Present?
Trip Blank Custody Seals present?
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted;
Project Manager SCURF Review:
Project Manager5RF Review:
©Yes ❑Na ❑N/A 11.
Yes
❑No
N/A
2.
®Yes
[]No
N/A
3.
❑Yes
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[:]No
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No
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`Yes ❑No ❑N/A 9,
❑Yes tjNo ❑N/A 10.
} yes ❑No ❑N/A 11.
Date/Time:
Lot 10 of split containers:
Date:
Date;
Field Data Required? ❑Yes []No
Page 73 of 93

Document Name:
Document Revised: November 15, 2021
aceAnalytical
Sample Condition Upon Receipt (SCUR)
Page 2 of 2
Document No.:
Issuing Authority:
F-CAR-CS.033-Rev.09
Pace Carolinas quality Office
*Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Conform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHS
* *Bottom half of box is to list number of Mottles
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Sample ID
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pH upon receipt
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Time preservation
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adjusted
added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (I.e.
out of hold, incorrect preservative, out of temp, incorrect containers.
Page 74 of 93

Document Name: Cocument Revised: November IS, 2021
ace�4rlafyticaln Sample Condition Upon Receipt (SCUR) Page 2 of 2
Document Nn.; Issuing Authority:
F•CAR-0-033-Rev.08 Pace Carolinas Quality Office
*Check mark top half of box if AM and/or dechlorination is Projec WC)# : 92574833
verified and within the acceptance range for preservation —
samples, PM: BV Due Date: 12/09/21
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 {water) DOC, LLHg CLIENT: 97—CNA
**Bottom half of box is to list number of battles
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Page 75 of 93

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93

urofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins TestAmerica, Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-208195-1
Client Project/Site: 92574833/NRLF-November 2021
Pace Analytical Services, LLC
9800 Kincey Avenue, Suite 100
Huntersville, North Carolina 28078
Attn: Bonnie Vang
Authorized for release by.
121912021 5:10:31 PM
Sheila Hoffman, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory. page 78 of 93

Sample Summary C
Client: Pace Analytical Services, LLC Job ID: 680-208195-1
Project/Site: 92574833/NRLF-November 2021
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
680-208195-1
13-2413-112921
Water
11/29/2109:48
12/02/21 11:00
680-208195-2
B-24A-112921
Water
11/29/2110:30
12/02/21 11:00
680-208195-3
B-23A-112921
Water
11/29/2114:14
12/02/21 11:00
680-208195-4
B-23B-112921
Water
11/29/2115:46
12/02/21 11:00
680-208195-5
B-17C-112921
Water
11/29/2114:00
12/02/21 11:00
680-208195-6
B-12-112921
Water
11/29/2116:00
12/02/21 11:00
680-208195-7
B-22-113021
Water
11/30/2107:57
12/02/21 11:00
680-208195-8
B-17B-113021
Water
11/30/21 08:34
12/02/21 11:00
680-208195-9
B-22A-113021
Water
11/30/21 09:40
12/02/21 11:00
680-208195-10
B-09C-113021
Water
11/30/2110:05
12/02/21 11:00
680-208195-11
B-21B-113021
Water
11/30/21 11:24
12/02/21 11:00
Eurofins TestAmericBPfta grOgli
Page 2 of 16 12/9/2021

Method Summary
Client: Pace Analytical Services, LLC
Project/Site: 92574833/NRLF-November 2021
F
Job ID: 680-208195-1
U
Method Method Description Protocol Laboratory
2320B-2011 Alkalinity, Total SM TAL SAV
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins TestAmerica, Savannah
Page 80 of 93
Page 3 of 16 12/9/2021

Definitions/Glossary
Client: Pace Analytical Services, LLC
Project/Site: 92574833/NRLF-November 2021
Qualifiers
General Chemistry
Qualifier Qualifier Description
U Indicates that the compound was analyzed for but not detected.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
c Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
oil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Lever'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MOIL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
F
Job ID: 680-208195-1
Page 4 of 16
Eurofins TestAmerica, Savannah
Page 81 of 93
12/9/2021

Case Narrative
Client: Pace Analytical Services, LLC
Project/Site: 92574833/NRLF-November 2021
Job ID: 680-208195-1
Laboratory: Eurofins TestAmerica, Savannah
Narrative
CASE NARRATIVE
Job ID: 680-208195-1
Client: Pace Analytical Services, LLC
Project: 92574833/NRLF-November 2021 C
Report Number: 680-208195-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 12/02/2021; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 1.4 C.
ALKALINITY
Samples 13-246-112921 (680-208195-1), B-24A-112921 (680-208195-2), B-23A-112921 (680-208195-3), 13-236-112921 (680-208195-4),
B-17C-112921 (680-208195-5), B-12-112921 (680-208195-6), B-22-113021 (680-208195-7), B-176-113021 (680-208195-8),
B-22A-113021 (680-208195-9), B-09C-113021 (680-208195-10) and B-21 B-113021 (680-208195-11) were analyzed for alkalinity in
accordance with SM 2320B. The samples were analyzed on 12/07/2021, 12/08/2021 and 12/09/2021.
Sample B-23A-112921 (680-208195-3)[1 OX] required dilution prior to analysis. The reporting limits have been adjusted accordingly.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins TestAmerica?g&gh
Page 5 of 16 12/9/2021

Client Sample Results
Client: Pace Analytical Services, LLC
Project/Site: 92574833/NRLF-November 2021
Client Sample ID: B-24B-112921
Date Collected: 11/29/21 09:48
Date Received: 12/02/21 11:00
F
Job ID: 680-208195-1
Lab Sample ID: 680-208195-1
Matrix: Water
General Chemistry
Analyte
Result Qualifier
PQL
MDL
Unit
D
Prepared Analyzed Dil Fac
Alkalinity
380
5.0
5.0
mg/L
-
12/07/21 14:59 1
Bicarbonate Alkalinity
380
5.0
5.0
mg/L
12/07/21 14:59 1
Carbonate Alkalinity
5.0 U
5.0
5.0
mg/L
12/07/21 14:59 1
Client Sample ID: B-24A-112921
Lab Sample ID: 680-208195-2
Date Collected: 11/29/21 10:30
Matrix: Water
E:
Date Received: 12/02/21 11:00
General Chemistry
F
Analyte
Result Qualifier
PQL
MDL
Unit
D
Prepared Analyzed Dil Fac
Alkalinity
460
5.0
5.0
mg/L
12/07/21 14:59 1
Bicarbonate Alkalinity
450
5.0
5.0
mg/L
12/07/21 14:59 1
Carbonate Alkalinity
5.0 U
5.0
5.0
mg/L
12/07/21 14:59 1
Client Sample ID: B-23A-112921
Lab Sample ID: 680-208195-3
Date Collected: 11/29/21 14:14
Matrix: Water
Date Received: 12/02/21 11:00
General Chemistry
Analyte
Result Qualifier
PQL
MDL
Unit
D
Prepared Analyzed Dil Fac
Alkalinity
3000
50
50
mg/L
12/09/21 12:12 10
Bicarbonate Alkalinity
3000
50
50
mg/L
12/09/21 12:12 10
Carbonate Alkalinity
50 U
50
50
mg/L
12/09/21 12:12 10
Client Sample ID: 13-236-112921
Lab Sample ID: 680-208195-4
Date Collected: 11/29/21 15:46
Matrix: Water
Date Received: 12/02/21 11:00
General Chemistry
Analyte
Result Qualifier
PQL
MDL
Unit
D
Prepared Analyzed oil Fac
Alkalinity
2100
5.0
5.0
mg/L
12/07/21 14:59 1
Bicarbonate Alkalinity
2100
5.0
5.0
mg/L
12/07/21 14:59 1
Carbonate Alkalinity
5.0 U
5.0
5.0
mg/L
12/07/21 14:59 1
Client Sample ID: 13-17C-112921
Lab Sample ID: 680-208195-5
Date Collected: 11/29/21 14:00
Matrix: Water
Date Received: 12/02/21 11:00
General Chemistry
Analyte
Result Qualifier
PQL
MDL
Unit
D
Prepared Analyzed Dil Fac
Alkalinity
5.0 U
5.0
5.0
mg/L
12/07/21 14:59 1
Bicarbonate Alkalinity
5.0 U
5.0
5.0
mg/L
12/07/21 14:59 1
Carbonate Alkalinity
5.0 U
5.0
5.0
mg/L
12/07/21 14:59 1
Client Sample ID: B-12-112921
Lab Sample ID: 680-208195-6
Date Collected: 11/29/21 16:00
Matrix: Water
Date Received: 12/02/21 11:00
General Chemistry
Analyte
Result Qualifier
PQL
MDL
Unit
D
Prepared Analyzed Dil Fac
Alkalinity
360
5.0
5.0
mg/L
12/08/2113:55 1
Bicarbonate Alkalinity
360
5.0
5.0
mg/L
12/08/21 13:55 1
Eurofins TestAmerica, Savannah
Page 83 of 93
Page 6 of 16
12/9/2021

Client: Pace Analytical Services, LLC
Project/Site: 92574833/NRLF-November 2021
Client Sample ID: B-12-112921
Date Collected: 11/29/21 16:00
Date Received: 12/02/21 11:00
General Chemistry (Continued)
Analyte
Carbonate Alkalinity
Client Sample ID: B-22-113021
Date Collected: 11/30/21 07:57
Date Received: 12/02/21 11:00
Client Sample Results
Result Qualifier PQL
5.0 U 5.0
F
Job ID: 680-208195-1
Lab Sample ID: 680-208195-6
Matrix: Water
MDL
Unit
D Prepared Analyzed
Dil Fac
5.0
mg/L
12/08/21 13:55
1
General Chemistry
Analyte Result Qualifier PQL MDL Unit
Alkalinity 920 5.0 5.0 mg/L
Bicarbonate Alkalinity 920 5.0 5.0 mg/L
Carbonate Alkalinity 5.0 U 5.0 5.0 mg/L
Client Sample ID: B-176-113021
Date Collected: 11/30/21 08:34
Date Received: 12/02/21 11:00
General Chemistry
Analyte
Alkalinity
Bicarbonate Alkalinity
Carbonate Alkalinity
Client Sample ID: B-22A-113021
Date Collected: 11/30/21 09:40
Date Received: 12/02/21 11:00
General Chemistry
Analyte
Alkalinity
Bicarbonate Alkalinity
Carbonate Alkalinity
Client Sample ID: B-09C-113021
Date Collected: 11/30/21 10:05
Date Received: 12/02/21 11:00
General Chemistry
Analyte
Alkalinity
Bicarbonate Alkalinity
Carbonate Alkalinity
Client Sample ID: B-21 B-113021
Date Collected: 11/30/21 11:24
Date Received: 12/02/21 11:00
General Chemistry
Analyte
Alkalinity
Bicarbonate Alkalinity
Carbonate Alkalinity
Result Qualifier PQL MDL Unit
220 5.0 5.0 mg/L
220 5.0 5.0 mg/L
5.0 U 5.0 5.0 mg/L
Lab Sample ID: 680-208195-7
Matrix: Water
D Prepared Analyzed Dil Fac
12/08/21 13:55 1
12/08/21 13:55 1
12/08/21 13:55 1
Lab Sample ID: 680-208195-8
Matrix: Water
D Prepared Analyzed Dil Fac
12/08/21 13:55 1
12/08/21 13:55 1
12/08/21 13:55 1
Lab Sample ID: 680-208195-9
Matrix: Water
Result Qualifier
PQL
MDL
Unit
D Prepared Analyzed
Dil Fac
470
5.0
5.0
mg/L
12/08/21 13:55
1
470
5.0
5.0
mg/L
12/08/21 13:55
1
5.0 U
5.0
5.0
mg/L
12/08/21 13:55
1
Lab Sample ID: 680-208195-10
Matrix: Water
Result Qualifier
PQL
MDL
Unit
D Prepared Analyzed Dil Fac
2500
5.0
5.0
mg/L
12/08/21 13:55 1
2500
5.0
5.0
mg/L
12/08/21 13:55 1
5.0 U
5.0
5.0
mg/L
12/08/21 13:55 1
Lab Sample ID: 680-208195-11
Matrix: Water
Result Qualifier
PQL
MDL
Unit
D Prepared Analyzed Dil Fac
250
5.0
5.0
mg/L
12/08/21 13:55 1
250
5.0
5.0
mg/L
12/08/21 13:55 1
5.0 U
5.0
5.0
mg/L
12/08/21 13:55 1
Eurofins TestAmerica, Savannah
Page 84 of 93
Page 7 of 16 12/9/2021

QC Sample Results
Client: Pace Analytical Services, LLC
Project/Site: 92574833/NRLF-November 2021
Job ID: 680-208195-1
Method: 2320B-2011 - Alkalinity, Total
Lab Sample ID: MB 680-697833/8 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 697833
MB MB
Analyte Result Qualifier
Alkalinity 5.0 U
Bicarbonate Alkalinity 5.0 U
Carbonate Alkalinity 5.0 U
Lab Sample ID: LCS 680-697833/10
Matrix: Water
Analysis Batch: 697833
Analyte
Alkalinity
Lab Sample ID: LCSD 680-697833/36
Matrix: Water
Analysis Batch: 697833
Analyte
Alkalinity
Lab Sample ID: MB 680-697941/8
Matrix: Water
Analysis Batch: 697941
MB MB
Analyte Result Qualifier
Alkalinity 5.0 U
Bicarbonate Alkalinity 5.0 U
Carbonate Alkalinity 5.0 U
Lab Sample ID: LCS 680-697941/10
Matrix: Water
Analysis Batch: 697941
Analyte
Alkalinity
Lab Sample ID: LCSD 680-697941/34
Matrix: Water
Analysis Batch: 697941
Analyte
Alkalinity
Lab Sample ID: MB 680-698176/8
Matrix: Water
Analysis Batch: 698176
MB MB
Analyte Result Qualifier
Alkalinity 5.0 U
Bicarbonate Alkalinity 5.0 U
Carbonate Alkalinity 5.0 U
PQL
MDL Unit
D Prepared Analyzed Dil Fac
5.0
5.0 mg/L
12/07/2114:59 1
5.0
5.0 mg/L
12/07/2114:59 1
5.0
5.0 mg/L
12/07/2114:59 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec.
Added
Result
Qualifier
Unit D %Rec Limits
250
250
mg/L 100 90 - 112
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD
LCSD
%Rec. RPD
Added
Result
Qualifier
Unit D %Rec Limits RPD Limit
250
252
mg/L 101 90 - 112 1 30
Client Sample ID: Method Blank
Prep Type: Total/NA
PQL
MDL Unit
D Prepared Analyzed Dil Fac
5.0
5.0 mg/L
12/08/2113:55 1
5.0
5.0 mg/L
12/08/2113:55 1
5.0
5.0 mg/L
12/08/2113:55 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec.
Added
Result
Qualifier
Unit D %Rec Limits
250
249
mg/L 100 90 - 112
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD
LCSD
%Rec. RPD
Added
Result
Qualifier
Unit D %Rec Limits RPD Limit
250
270
mg/L 108 90 - 112 8 30
Client Sample ID: Method Blank
Prep Type: Total/NA
PQL MDL Unit D Prepared Analyzed Dil Fac
5.0 5.0 mg/L 12/09/2111:31 1
5.0 5.0 mg/L 12/09/2111:31 1
5.0 5.0 mg/L 12/09/2111:31 1
Page 8 of 16
Eurofins TestAmerica, Savannah
Page 85 of 93
12/9/2021

QC Sample Results
Client: Pace Analytical Services, LLC
Job ID: 680-208195-1
Project/Site: 92574833/NRLF-November 2021
Method: 2320B-2011 - Alkalinity, Total (Continued)
Lab Sample ID: LCS 680-698176/10
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 698176
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit D %Rec Limits
Alkalinity
250
250
mg/L 100 90 - 112
Lab Sample ID: LCSD 680-698176/35
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 698176
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit D %Rec Limits RPD Limit
Alkalinity
250
270
mg/L 108 90 - 112 8 30
Page 9 of 16
Eurofins TestAmerica, Savannah
Page 86 of 93
12/9/2021

QC Association Summary
Client: Pace Analytical Services, LLC
Project/Site: 92574833/NRLF-November 2021
General Chemistry
Analysis Batch: 697833
Lab Sample ID
Client Sample ID
680-208195-1
B-24B-112921
680-208195-2
B-24A-112921
680-208195-4
B-23B-112921
680-208195-5
B-17C-112921
MB 680-697833/8
Method Blank
LCS 680-697833/10
Lab Control Sample
LCSD 680-697833/36
Lab Control Sample Dup
Analysis Batch: 697941
Lab Sample ID
Client Sample ID
680-208195-6
B-12-112921
680-208195-7
B-22-113021
680-208195-8
B-17B-113021
680-208195-9
B-22A-113021
680-208195-10
B-09C-113021
680-208195-11
B-21B-113021
MB 680-697941/8
Method Blank
LCS 680-697941/10
Lab Control Sample
LCSD 680-697941/34
Lab Control Sample Dup
Analysis Batch: 698176
Lab Sample ID
Client Sample ID
680-208195-3
B-23A-112921
MB 680-698176/8
Method Blank
LCS 680-698176/10
Lab Control Sample
LCSD 680-698176/35
Lab Control Sample Dup
F
Job ID: 680-208195-1
Prep Type
Matrix
Method
Total/NA
Water
2320B-2011
Total/NA
Water
2320B-2011
Total/NA
Water
2320B-2011
Total/NA
Water
2320E-2011
Total/NA
Water
2320E-2011
Total/NA
Water
2320E-2011
Total/NA
Water
2320E-2011
Prep Type
Matrix
Method
Total/NA
Water
2320B-2011
Total/NA
Water
2320B-2011
Total/NA
Water
2320B-2011
Total/NA
Water
2320B-2011
Total/NA
Water
2320B-2011
Total/NA
Water
2320B-2011
Total/NA
Water
2320E-2011
Total/NA
Water
2320E-2011
Total/NA
Water
2320E-2011
Prep Type
Matrix
Method
Total/NA
Water
2320B-2011
Total/NA
Water
2320B-2011
Total/NA
Water
2320B-2011
Total/NA
Water
2320B-2011
Prep Batch
L
0
E:
Prep Batch F
Prep Batch
Page 10 of 16
Eurofins TestAmerica, Savannah
Page 87 of 93
12/9/2021

Lab Chronicle
Client: Pace Analytical Services, LLC
Job ID: 680-208195-1
Project/Site: 92574833/NRLF-November 2021
Client Sample ID: B-24B-112921
Lab Sample ID: 680-208195-1
Date Collected: 11/29/21 09:48
Matrix: Water
Date Received: 12/02/21 11:00
Batch Batch
Dil
Initial Final
Batch
Prepared
Prep Type Type Method
Run
Factor
Amount Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 2320B-2011
1
697833
12/07/21 14:59 ALG TAL SAV
Instrument ID: NOEQUIP
Client Sample ID: B-24A-112921
Lab Sample ID: 680-208195-2
Date Collected: 11/29/21 10:30
Matrix: Water
Date Received: 12/02/21 11:00
Batch Batch
Dil
Initial Final
Batch
Prepared
Prep Type Type Method
Run
Factor
Amount Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 2320B-2011
1
697833
12/07/21 14:59 ALG TAL SAV
Instrument ID: NOEQUIP
Client Sample ID: B-23A-112921
Lab Sample ID: 680-208195-3
Date Collected: 11/29/21 14:14
Matrix: Water
Date Received: 12/02/21 11:00
Batch Batch
Dil
Initial Final
Batch
Prepared
Prep Type Type Method
Run
Factor
Amount Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 232OB-2011
10
698176
12/09/21 12:12 DR TAL SAV
Instrument ID: MANTECH 2
Client Sample ID: 13-2313-112921
Lab Sample ID: 680-208195-4
Date Collected: 11/29/21 15:46
Matrix: Water
Date Received: 12/02/21 11:00
Batch Batch
Dil
Initial Final
Batch
Prepared
Prep Type Type Method
Run
Factor
Amount Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 2320B-2011
1
697833
12/07/21 14:59 ALG TAL SAV
Instrument ID: NOEQUIP
Client Sample ID: 13-17C-112921
Lab Sample ID: 680-208195-5
Date Collected: 11/29/21 14:00
Matrix: Water
Date Received: 12/02/21 11:00
Batch Batch
Dil
Initial Final
Batch
Prepared
Prep Type Type Method
Run
Factor
Amount Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 2320B-2011
1
697833
12/07/21 14:59 ALG TAL SAV
Instrument ID: NOEQUIP
Client Sample ID: B-12-112921
Lab Sample ID: 680-208195-6
Date Collected: 11/29/21 16:00
Matrix: Water
Date Received: 12/02/21 11:00
Batch Batch
Dil
Initial Final
Batch
Prepared
Prep Type Type Method
Run
Factor
Amount Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 2320B-2011
1
697941
12/08/21 13:55 DR TAL SAV
Instrument ID: NOEQUIP
Eurofins TestAmerica, Savannah
Page 88 of 93
Page 11 of 16 12/9/2021

Lab Chronicle
Client: Pace Analytical Services, LLC
Job ID: 680-208195-1
Project/Site: 92574833/NRLF-November 2021
Client Sample ID: B-22-113021
Lab Sample ID: 680-208195-7
Date Collected: 11/30/21 07:57
Matrix: Water
Date Received: 12/02/21 11:00
Batch Batch
Dil
Initial Final
Batch
Prepared
Prep Type Type Method
Run
Factor
Amount Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 2320B-2011
1
697941
12/08/21 13:55 DR TAL SAV
Instrument ID: NOEQUIP
Client Sample ID: B-17B-113021
Lab Sample ID: 680-208195-8
Date Collected: 11/30/21 08:34
Matrix: Water
Date Received: 12/02/21 11:00
Batch Batch
Dil
Initial Final
Batch
Prepared
Prep Type Type Method
Run
Factor
Amount Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 2320B-2011
1
697941
12/08/21 13:55 DR TAL SAV
Instrument ID: NOEQUIP
Client Sample ID: B-22A-113021
Lab Sample ID: 680-208195-9
Date Collected: 11/30/21 09:40
Matrix: Water
Date Received: 12/02/21 11:00
Batch Batch
Dil
Initial Final
Batch
Prepared
Prep Type Type Method
Run
Factor
Amount Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 232OB-2011
1
697941
12/08/21 13:55 DR TAL SAV
Instrument ID: NOEQUIP
Client Sample ID: 13-09C-113021
Lab Sample ID: 680-208195-10
Date Collected: 11/30/21 10:05
Matrix: Water
Date Received: 12/02/21 11:00
Batch Batch
Dil
Initial Final
Batch
Prepared
Prep Type Type Method
Run
Factor
Amount Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 2320B-2011
1
697941
12/08/21 13:55 DR TAL SAV
Instrument ID: NOEQUIP
Client Sample ID: B-216-113021
Lab Sample ID: 680-208195-11
Date Collected: 11/30/21 11:24
Matrix: Water
Date Received: 12/02/21 11:00
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis 2320B-2011 1 697941 12/08/21 13:55 DR TAL SAV
Instrument ID: NOEQUIP
Laboratory References:
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Page 12 of 16
Eurofins TestAmerica, Savannah
Page 89 of 93
12/9/2021

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Page 90 of 93
12/9/2021

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Page 14 of 16
Page 91 of 93
12/9/2021

Login Sample Receipt Checklist
Client: Pace Analytical Services, LLC
Job Number: 680-208195-1
Login Number: 208195
List Number: 1
Creator: Hartley, Tyler
Question
List Source: Eurofins TestAmerica, Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True m
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins TestAmerica, Savannah Page 92 of 93
Page 15 of 16 12/9/2021

Accreditation/Certification Summary
Client: Pace Analytical Services, LLC
Job ID: 680-208195-1
Project/Site: 92574833/NRLF-November 2021
Laboratory: Eurofins TestAmerica, Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program
Identification Number
Expiration Date
North Carolina (WW/SW) State
269
12-31-21
South Carolina State
98001
06-30-22
Virginia N ELAP
10509
06-29-22
F
F
M
Eurofins TestAmerica, Savannah
Page 93 of 93
Page 16 of 16
12/9/2021

lceAnalyilcal®
www.pacelabs.cem
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
December 23, 2021
Jing Zhou
AECOM
1360 Peachtree St.
Suite 500
Atlanta, GA 30309
RE: Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Dear Jing Zhou:
Enclosed are the analytical results for sample(s) received by the laboratory on December 01, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Gulf Coast
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
• Pace Analytical Services - Indianapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
-�Jax
Bonnie Vang
[e-mail]
[phone]
Project Manager
Enclosures
cc: Rob Davis. AECOM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 49

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Pace Analytical Services Indianapolis
7726 Moller Road, Indianapolis, IN 46268
Illinois Accreditation #: 200074
Indiana Drinking Water Laboratory #: C-49-06
Kansas/TNI Certification #: E-10177
Kentucky UST Agency Interest #: 80226
Kentucky WW Laboratory ID M 98019
CERTIFICATIONS
Michigan Drinking Water Laboratory #9050
Ohio VAP Certified Laboratory #: CL0065
Oklahoma Laboratory #: 9204
Texas Certification #: T104704355
Wisconsin Laboratory #: 999788130
USDA Soil Permit #: P330-19-00257
Pace Analytical Gulf Coast
7979 Innovation Park Drive, Baton Rouge, LA 70820
North Dakota Certification #: R-195
Arkansas Certification #: 88-0655
Oklahoma Certification #: 2019-101
DoD ELAP Certification #: L18-597
South Carolina Certification #: 73006001
Florida Certification #: E87854
Texas Certification #: T104704178-19-11
Illinois Certification #: 004585
USDA Soil Permit # P330-19-00209
Kansas Certification #: E-10354
Virginia Certification #: 460215
Louisiana/LELAP Certification M 01955
Washington Certification #: C929
North Carolina Certification #: 618
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Drinking Water Cert. #: 99006003
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Louisiana DoH Drinking Water #: LA029
South Carolina Laboratory ID: 99006
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
South Carolina Laboratory ID: 99030
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 40
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification #: 37738
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 49

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92575044001
B-01-113021
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
MWF
1
PASI-E
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
AWE
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
SAS
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MDW
5
PASI-A
AM23G
SLL2
1
GCLA
92575044002
B-10-113021
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
MWF
1
PASI-E
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
AWE
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MDW
5
PASI-A
AM23G
SLL2
1
GCLA
92575044003
B-3213-113021
EPA 353.2 Rev 2.0 1993
SRS
3
PASI-E
SM 4500-P E-2011
MWF
1
PASI-E
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
AWE
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
EPA 9056A
CDC
1
PASI-A
EPA 9060A
MDW
5
PASI-A
AM23G
SLL2
1
GCLA
92575044007
TRIP BLANK 02-113021
EPA 8260D
CL
53
PASI-C
GCLA = Pace Analytical Gulf Coast
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 49

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
PASI-I = Pace Analytical Services - Indianapolis
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 49

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Sample: B-01-113021 Lab ID: 92575044001 Collected: 11/30/21 11:40 Received: 12/01/21 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
0.049 mg/L
0.040
1
12/02/21 09:05
Nitrogen, Nitrate
ND mg/L
0.040
1
12/02/21 09:05
14797-55-8
Nitrogen, Nitrite
0.35 mg/L
0.040
1
12/02/21 09:05
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.83 mg/L
0.084
1.67
12/01/21 17:26
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
5.0
1
12/08/21 18:46
107-21-1
Biodegradation Indicator Gases
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Methane
15000 ug/L
5.0
1
12/06/2120:47
74-82-8
Ethane
ND ug/L
1.0
1
12/06/2120:47
74-84-0
Ethene
ND ug/L
1.0
1
12/06/2120:47
74-85-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
399000 ug/L
45000
50
12/10/21 13:28
124-38-9
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA
3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L
9.1
1
12/03/21 04:33
12/03/21 10:37
92-52-4
Diphenyl ether (Phenyl ether)
30.9 ug/L
9.1
1
12/03/21 04:33
12/03/21 10:37
101-84-8
Surrogates
Nitrobenzene-d5(S)
64 %
10-144
1
12/03/21 04:33
12/03/21 10:37
4165-60-0
2-Fluorobiphenyl (S)
52 %
10-130
1
12/03/21 04:33
12/03/21 10:37
321-60-8
Terphenyl-d14 (S)
53 %
34-163
1
12/03/21 04:33
12/03/21 10:37
1718-51-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
703 ug/L
62.5
2.5
12/04/21 06:26
67-64-1
Benzene
ND ug/L
2.5
2.5
12/04/21 06:26
71-43-2
Bromochloromethane
ND ug/L
2.5
2.5
12/04/21 06:26
74-97-5
Bromodichloromethane
ND ug/L
2.5
2.5
12/04/21 06:26
75-27-4
Bromoform
ND ug/L
2.5
2.5
12/04/21 06:26
75-25-2
Bromomethane
ND ug/L
5.0
2.5
12/04/21 06:26
74-83-9
2-Butanone (MEK)
330 ug/L
12.5
2.5
12/04/21 06:26
78-93-3
Carbon disulfide
ND ug/L
5.0
2.5
12/04/21 06:26
75-15-0
Carbon tetrachloride
ND ug/L
2.5
2.5
12/04/21 06:26
56-23-5
Chlorobenzene
ND ug/L
2.5
2.5
12/04/21 06:26
108-90-7
Chloroethane
16.5 ug/L
2.5
2.5
12/04/21 06:26
75-00-3
Chloroform
ND ug/L
2.5
2.5
12/04/21 06:26
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 49

lreAnalyilcal®
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816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Sample: B-01-113021 Lab ID: 92575044001 Collected: 11/30/21 11:40 Received: 12/01/21 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Chloromethane
ND
ug/L
2.5
2.5
12/04/21 06:26
74-87-3
Cyclohexane
ND
ug/L
2.5
2.5
12/04/21 06:26
110-82-7
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
2.5
12/04/21 06:26
96-12-8
Dibromochloromethane
ND
ug/L
2.5
2.5
12/04/21 06:26
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
2.5
2.5
12/04/21 06:26
106-93-4
1,2-Dichlorobenzene
ND
ug/L
2.5
2.5
12/04/21 06:26
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.5
2.5
12/04/21 06:26
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.5
2.5
12/04/21 06:26
106-46-7
Dichlorodifluoromethane
ND
ug/L
2.5
2.5
12/04/21 06:26
75-71-8
1,1-Dichloroethane
10.2
ug/L
2.5
2.5
12/04/21 06:26
75-34-3
1,2-Dichloroethane
ND
ug/L
2.5
2.5
12/04/21 06:26
107-06-2
1,1-Dichloroethene
ND
ug/L
2.5
2.5
12/04/21 06:26
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.5
2.5
12/04/21 06:26
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.5
2.5
12/04/21 06:26
156-60-5
1,2-Dichloropropene
ND
ug/L
2.5
2.5
12/04/21 06:26
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.5
2.5
12/04/21 06:26
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
2.5
2.5
12/04/21 06:26
10061-02-6
Ethylbenzene
ND
ug/L
2.5
2.5
12/04/21 06:26
100-41-4
2-Hexanone
ND
ug/L
12.5
2.5
12/04/21 06:26
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
2.5
2.5
12/04/21 06:26
98-82-8
Methyl acetate
ND
ug/L
25.0
2.5
12/04/21 06:26
79-20-9
Methylcyclohexane
ND
ug/L
25.0
2.5
12/04/21 06:26
108-87-2
Methylene Chloride
ND
ug/L
12.5
2.5
12/04/21 06:26
75-09-2
4-Methyl-2-pentanone (MIBK)
22.2
ug/L
12.5
2.5
12/04/21 06:26
108-10-1
Methyl-tert-butyl ether
ND
ug/L
2.5
2.5
12/04/21 06:26
1634-04-4
Styrene
ND
ug/L
2.5
2.5
12/04/21 06:26
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
2.5
2.5
12/04/21 06:26
79-34-5
Tetrachloroethene
ND
ug/L
2.5
2.5
12/04/21 06:26
127-18-4
Toluene
ND
ug/L
2.5
2.5
12/04/21 06:26
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.5
2.5
12/04/21 06:26
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.5
2.5
12/04/21 06:26
120-82-1
1,1,1-Trichloroethane
ND
ug/L
2.5
2.5
12/04/21 06:26
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.5
2.5
12/04/21 06:26
79-00-5
Trichloroethene
ND
ug/L
2.5
2.5
12/04/21 06:26
79-01-6
Trichlorofluoromethane
ND
ug/L
2.5
2.5
12/04/21 06:26
75-69-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
2.5
2.5
12/04/21 06:26
76-13-1
Vinyl chloride
ND
ug/L
2.5
2.5
12/04/21 06:26
75-01-4
Xylene (Total)
ND
ug/L
2.5
2.5
12/04/21 06:26
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
104
%
70-130
2.5
12/04/21 06:26
460-00-4
1,2-Dichloroethane-d4 (S)
105
%
70-130
2.5
12/04/21 06:26
17060-07-0
Toluene-d8 (S)
101
%
70-130
2.5
12/04/21 06:26
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
1650
ug/L
50.0
25
12/02/21 21:55
123-91-1
REPORT OF LABORATORY ANALYSIS
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Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 49

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Sample: B-01-113021 Lab ID: 92575044001 Collected: 11/30/21 11:40 Received: 12/01/21 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV SIM Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
9056 IC anions 28 Days
Sulfate
Total Organic Carbon,Asheville
Total Organic Carbon
Total Organic Carbon
Total Organic Carbon
Total Organic Carbon
Mean Total Organic Carbon
Low Level Volatile Fatty Acids
Acetic Acid
Date: 12/23/2021 10:34 AM
105 %
70-130
25
12/02/2121:55
17060-07-0
105 %
66-133
25
12/02/21 21:55
2037-26-5
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
5.5 mg/L
1.0
1
12/04/2111:28
14808-79-8
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
898 mg/L
50.0
50
12/08/2110:00
7440-44-0
M1
916 mg/L
50.0
50
12/08/2110:00
7440-44-0
M1
932 mg/L
50.0
50
12/08/2110:00
7440-44-0
M1
919 mg/L
50.0
50
12/08/2110:00
7440-44-0
M1
916 mg/L
50.0
50
12/08/2110:00
7440-44-0
M1
Analytical Method: AM23G
Pace Analytical Gulf Coast
580 mg/L
50
100
12/14/21 17:58
64-19-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 49

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Sample: B-10-113021 Lab ID: 92575044002 Collected: 11/30/21 13:40 Received: 12/01/21 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, NO2 plus NO3
0.060 mg/L
0.040
1
12/02/21 09:06
Nitrogen, Nitrate
ND mg/L
0.040
1
12/02/21 09:06
14797-55-8
Nitrogen, Nitrite
0.22 mg/L
0.040
1
12/02/21 09:06
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
Orthophosphate as P
0.22 mg/L
0.050
1
12/01/21 17:28
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
5.0
1
12/08/21 18:55
107-21-1
Biodegradation Indicator Gases
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Methane
17000 ug/L
5.0
1
12/06/2120:58
74-82-8
Ethane
ND ug/L
1.0
1
12/06/2120:58
74-84-0
Ethene
ND ug/L
1.0
1
12/06/2120:58
74-85-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
264000 ug/L
45000
50
12/10/21 13:34
124-38-9
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
110 ug/L
9.1
1
12/03/21 04:33
12/03/21 11:02
92-52-4
Diphenyl ether (Phenyl ether)
1140 ug/L
90.9
10
12/03/21 04:33
12/03/21 15:40
101-84-8
Surrogates
Nitrobenzene-d5(S)
90 %
10-144
1
12/03/21 04:33
12/03/21 11:02
4165-60-0
2-Fluorobiphenyl (S)
75 %
10-130
1
12/03/21 04:33
12/03/21 11:02
321-60-8
Terphenyl-d14 (S)
76 %
34-163
1
12/03/21 04:33
12/03/21 11:02
1718-51-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
12/03/21 14:01
67-64-1
Benzene
ND ug/L
1.0
1
12/03/21 14:01
71-43-2
Bromochloromethane
ND ug/L
1.0
1
12/03/21 14:01
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
12/03/21 14:01
75-27-4
Bromoform
ND ug/L
1.0
1
12/03/21 14:01
75-25-2
Bromomethane
ND ug/L
2.0
1
12/03/21 14:01
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
12/03/21 14:01
78-93-3
Carbon disulfide
ND ug/L
2.0
1
12/03/21 14:01
75-15-0
Carbon tetrachloride
ND ug/L
1.0
1
12/03/21 14:01
56-23-5
Chlorobenzene
ND ug/L
1.0
1
12/03/21 14:01
108-90-7
Chloroethane
35.6 ug/L
1.0
1
12/03/21 14:01
75-00-3
Chloroform
ND ug/L
1.0
1
12/03/21 14:01
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 49

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Sample: B-10-113021 Lab ID: 92575044002 Collected: 11/30/21 13:40 Received: 12/01/21 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Chloromethane
ND
ug/L
1.0
1
12/03/21 14:01
74-87-3
Cyclohexane
ND
ug/L
1.0
1
12/03/21 14:01
110-82-7
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/03/21 14:01
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/03/21 14:01
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/03/21 14:01
106-93-4
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/03/21 14:01
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
12/03/21 14:01
541-73-1
1,4-Dichlorobenzene
3.9
ug/L
1.0
1
12/03/21 14:01
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
12/03/21 14:01
75-71-8
1,1-Dichloroethane
39.6
ug/L
1.0
1
12/03/21 14:01
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/03/21 14:01
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/03/21 14:01
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/03/21 14:01
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/03/21 14:01
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/03/21 14:01
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/03/21 14:01
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/03/21 14:01
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/03/21 14:01
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/03/21 14:01
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
1.0
1
12/03/21 14:01
98-82-8
Methyl acetate
ND
ug/L
10.0
1
12/03/21 14:01
79-20-9
Methylcyclohexane
ND
ug/L
10.0
1
12/03/21 14:01
108-87-2
Methylene Chloride
ND
ug/L
5.0
1
12/03/21 14:01
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/03/21 14:01
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
12/03/21 14:01
1634-04-4
Styrene
ND
ug/L
1.0
1
12/03/21 14:01
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/03/21 14:01
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/03/21 14:01
127-18-4
Toluene
2.0
ug/L
1.0
1
12/03/21 14:01
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
1
12/03/21 14:01
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
1
12/03/21 14:01
120-82-1
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/03/21 14:01
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/03/21 14:01
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/03/21 14:01
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/03/21 14:01
75-69-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
1.0
1
12/03/21 14:01
76-13-1
Vinyl chloride
2.1
ug/L
1.0
1
12/03/21 14:01
75-01-4
Xylene (Total)
2.1
ug/L
1.0
1
12/03/21 14:01
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
12/03/21 14:01
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
12/03/21 14:01
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
12/03/21 14:01
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
180
ug/L
8.0
4
12/02/21 22:14
123-91-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 49

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816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Sample: B-10-113021 Lab ID: 92575044002 Collected: 11/30/21 13:40 Received: 12/01/21 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV SIM Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
9056 IC anions 28 Days
Sulfate
Total Organic Carbon,Asheville
Total Organic Carbon
Total Organic Carbon
Total Organic Carbon
Total Organic Carbon
Mean Total Organic Carbon
Low Level Volatile Fatty Acids
Acetic Acid
Date: 12/23/2021 10:34 AM
108 %
70-130
4
12/02/2122:14
17060-07-0
105 %
66-133
4
12/02/2122:14
2037-26-5
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
ND mg/L
1.0
1
12/04/2112:11
14808-79-8
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
17.6 mg/L
1.0
1
12/08/21 10:55
7440-44-0
18.2 mg/L
1.0
1
12/08/21 10:55
7440-44-0
18.0 mg/L
1.0
1
12/08/21 10:55
7440-44-0
18.1 mg/L
1.0
1
12/08/21 10:55
7440-44-0
18.0 mg/L
1.0
1
12/08/21 10:55
7440-44-0
Analytical Method: AM23G
Pace Analytical Gulf Coast
4.7 mg/L
0.50
1
12/12/2104:56
64-19-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 49

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816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Sample: B-3213-113021 Lab ID: 92575044003 Collected: 11/30/21 14:54 Received: 12/01/21 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 NO2/NO3 unpres EDN
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
8015M Glycols in water
Ethylene glycol
Biodegradation Indicator Gases
Methane
Ethane
Ethene
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
9056 IC anions 28 Days
Sulfate
Total Organic Carbon,Asheville
Total Organic Carbon
Date: 12/23/2021 10:34 AM
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
0.069 mg/L
0.040
1
12/02/2109:07
0.069 mg/L
0.040
1
12/02/2109:07
14797-55-8
ND mg/L
0.040
1
12/02/2109:07
14797-65-0
Analytical Method: SM 4500-P E-2011
Pace Analytical Services - Eden
ND mg/L
0.050
1
12/01/2117:29
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
ND mg/L
5.0
1
12/08/2119:04
107-21-1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
2400 ug/L
5.0
1
12/06/2121:10
74-82-8
ND ug/L
1.0
1
12/06/2121:10
74-84-0
ND ug/L
1.0
1
12/06/2121:10
74-85-1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
54400 ug/L
45000
50
12/10/2113:39
124-38-9
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
ND ug/L
10.0
1
12/03/2104:33
12/03/2111:28
92-52-4
ND ug/L
10.0
1
12/03/2104:33
12/03/2111:28
101-84-8
66 %
10-144
1
12/03/2104:33
12/03/2111:28
4165-60-0
57 %
10-130
1
12/03/2104:33
12/03/2111:28
321-60-8
66 %
34-163
1
12/03/2104:33
12/03/2111:28
1718-51-0
Analytical Method: EPA 8260D Mod
Pace Analytical Services - Charlotte
3.2 ug/L
2.0
1
101 %
70-130
1
104 %
66-133
1
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
ND mg/L
1.0
1
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
1.8 mg/L
1.0
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
12/02/21 18:02 123-91-1
12/02/21 18:02 17060-07-0
12/02/21 18:02 2037-26-5
12/04/21 13:09 14808-79-8
i1111011PAEifiRiRiZ5[aLCgo]
Page 11 of 49

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Sample: B-32B-113021
Parameters
Lab ID: 92575044003 Collected: 11/30/21 14:54
Results Units Report Limit DF
Received: 12/01/21 08:00 Matrix: Water
Prepared Analyzed CAS No. Qual
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
1.4 mg/L
1.0
1
12/08/21 11:13
7440-44-0
Total Organic Carbon
1.4 mg/L
1.0
1
12/08/21 11:13
7440-44-0
Total Organic Carbon
1.3 mg/L
1.0
1
12/08/21 11:13
7440-44-0
Mean Total Organic Carbon
1.5 mg/L
1.0
1
12/08/21 11:13
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
ND mg/L
0.50
1
12/12/21 05:30
64-19-7
Date: 12/23/2021 10:34 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 49

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Sample: TRIP BLANK 02-113021 Lab ID: 92575044007 Collected: 11/30/21 00:00 Received: 12/01/21 08:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/03/21 06:09
67-64-1
Benzene
ND
ug/L
1.0
1
12/03/21 06:09
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/03/21 06:09
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/03/21 06:09
75-27-4
Bromoform
ND
ug/L
1.0
1
12/03/21 06:09
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/03/21 06:09
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/03/21 06:09
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/03/21 06:09
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/03/21 06:09
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/03/21 06:09
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/03/21 06:09
75-00-3
Chloroform
ND
ug/L
1.0
1
12/03/21 06:09
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/03/21 06:09
74-87-3
Cyclohexane
ND
ug/L
1.0
1
12/03/21 06:09
110-82-7
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/03/21 06:09
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/03/21 06:09
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/03/21 06:09
106-93-4
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/03/21 06:09
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
12/03/21 06:09
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/03/21 06:09
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
12/03/21 06:09
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
1
12/03/21 06:09
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/03/21 06:09
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/03/21 06:09
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/03/21 06:09
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/03/21 06:09
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/03/21 06:09
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/03/21 06:09
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/03/21 06:09
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/03/21 06:09
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/03/21 06:09
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
1.0
1
12/03/21 06:09
98-82-8
Methyl acetate
ND
ug/L
10.0
1
12/03/21 06:09
79-20-9
Methylcyclohexane
ND
ug/L
10.0
1
12/03/21 06:09
108-87-2
Methylene Chloride
ND
ug/L
5.0
1
12/03/21 06:09
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/03/21 06:09
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
12/03/21 06:09
1634-04-4
Styrene
ND
ug/L
1.0
1
12/03/21 06:09
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/03/21 06:09
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/03/21 06:09
127-18-4
Toluene
ND
ug/L
1.0
1
12/03/21 06:09
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
1
12/03/21 06:09
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
1
12/03/21 06:09
120-82-1
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/03/21 06:09
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/03/21 06:09
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/03/21 06:09
79-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 49

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816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
Sample: TRIP BLANK 02-113021
Parameters
Lab ID: 92575044007 Collected: 11/30/21 00:00
Results Units Report Limit DF
Received: 12/01/21 08:00 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Trichlorofluoromethane
ND ug/L
1.0
1
12/03/21 06:09
75-69-4
1,1,2-Trichlorotrifluoroethane
ND ug/L
1.0
1
12/03/21 06:09
76-13-1
Vinyl chloride
ND ug/L
1.0
1
12/03/21 06:09
75-01-4
Xylene (Total)
ND ug/L
1.0
1
12/03/21 06:09
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
12/03/21 06:09
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
12/03/21 06:09
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
12/03/21 06:09
2037-26-5
Date: 12/23/2021 10:34 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 49

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[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 663324 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92575044001, 92575044002, 92575044003
METHOD BLANK: 3474712
Matrix:
Water
Associated Lab Samples:
92575044001, 92575044002, 92575044003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/L
ND
0.040
12/02/21 09:02
Nitrogen, Nitrite
mg/L
ND
0.040
12/02/21 09:02
Nitrogen, NO2 plus NO3
mg/L
ND
0.040
12/02/21 09:02
LABORATORY CONTROL SAMPLE: 3474713
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.4 95 90-110
Nitrogen, Nitrite mg/L 1 0.99 99 90-110
Nitrogen, NO2 plus NO3 mg/L 2.5 2.4 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3474714
3474715
MS
MSD
92575013001 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Nitrogen, Nitrate
mg/L
1.7 1.5
1.5
3.1
3.1
89
89
90-110 0
Nitrogen, Nitrite
mg/L
ND 1
1
1.0
1.0
100
101
90-110 1
Nitrogen, NO2 plus NO3
mg/L
1.7 2.5
2.5
4.1
4.1
94
94
90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 49

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[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 663113 Analysis Method: SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011 Analysis Description: SM450OP-E Phosphorus, Ortho
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92575044001, 92575044002, 92575044003
METHOD BLANK: 3473618
Matrix:
Water
Associated Lab Samples: 92575044001, 92575044002, 92575044003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Orthophosphate as P
mg/L
ND
0.050
12/01/21 13:42
LABORATORY CONTROL SAMPLE:
3473619
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Orthophosphate as P
mg/L
0.25
0.26
105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3474276 3474277
MS MSD
92574936002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Orthophosphate as P mg/L 0.60 0.25 0.25 0.85 0.86 100 102 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3474278 3474279
MS MSD
92575044003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Orthophosphate as P mg/L ND 0.25 0.25 0.27 0.28 99 99 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 16 of 49

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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 653919 Analysis Method: EPA 8015 Alcohol -Glycol
QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified
Laboratory: Pace Analytical Services - Indianapolis
Associated Lab Samples: 92575044001, 92575044002, 92575044003
METHOD BLANK: 3014249
Matrix:
Water
Associated Lab Samples: 92575044001, 92575044002, 92575044003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Ethylene glycol
mg/L
ND
5.0
12/08/21 15:19
LABORATORY CONTROL SAMPLE:
3014250
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Ethylene glycol
mg/L
25
21.6
86 39-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3014251 3014252
MS MSD
5283799001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mg/L ND 25 25 26.9 28.7 107 114 36-158 6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 17 of 49

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 728703 Analysis Method: RSK-175
QC Batch Method: RSK-175 Analysis Description: Biodegradation Indicator Gases
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92575044001, 92575044002, 92575044003
METHOD BLANK: 2282093
Matrix: Water
Associated Lab Samples:
92575044001, 92575044002, 92575044003
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Methane
ug/L
ND 5.0
12/06/2118:10
Ethane
ug/L
ND 1.0
12/06/2118:10
Ethene
ug/L
ND 1.0
12/06/2118:10
LABORATORY CONTROL SAMPLE & LCSD:
2282094
2282095
Spike
LCS
LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD RPD Qualifiers
Methane
ug/L
380
360
360
95 95
70-130 0 30
Ethane
ug/L
97
100
100
107 106
70-130 1 30
Ethene
ug/L
120
130
130
108 108
70-130 1 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 729093 Analysis Method: RSK-175
QC Batch Method: RSK-175 Analysis Description: EPA RSK 175 CO2
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92575044001, 92575044002, 92575044003
METHOD BLANK: 2284464 Matrix: Water
Associated Lab Samples: 92575044001, 92575044002, 92575044003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Carbon dioxide ug/L ND 900 12/10/21 09:54
LABORATORY CONTROL SAMPLE & LCSD: 2284465 2284466
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Carbon dioxide ug/L 8700 8630 8130 99 93 38-147 6 40
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 19 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 663537 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92575044002, 92575044007
METHOD BLANK: 3475930
Associated Lab Samples: 92575044002, 92575044007
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
1.0
12/03/21 05:14
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/03/21 05:14
1,1,2-Trichloroethane
ug/L
ND
1.0
12/03/21 05:14
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
12/03/21 05:14
1,1-Dichloroethane
ug/L
ND
1.0
12/03/21 05:14
1,1-Dichloroethene
ug/L
ND
1.0
12/03/21 05:14
1,2,3-Trichlorobenzene
ug/L
ND
1.0
12/03/21 05:14
1,2,4-Trichlorobenzene
ug/L
ND
1.0
12/03/21 05:14
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/03/21 05:14
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/03/21 05:14
1,2-Dichlorobenzene
ug/L
ND
1.0
12/03/21 05:14
1,2-Dichloroethane
ug/L
ND
1.0
12/03/21 05:14
1,2-Dichloropropane
ug/L
ND
1.0
12/03/21 05:14
1,3-Dichlorobenzene
ug/L
ND
1.0
12/03/21 05:14
1,4-Dichlorobenzene
ug/L
ND
1.0
12/03/21 05:14
2-Butanone (MEK)
ug/L
ND
5.0
12/03/21 05:14
2-Hexanone
ug/L
ND
5.0
12/03/21 05:14
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/03/21 05:14
Acetone
ug/L
ND
25.0
12/03/21 05:14
Benzene
ug/L
ND
1.0
12/03/21 05:14
Bromochloromethane
ug/L
ND
1.0
12/03/21 05:14
Bromodichloromethane
ug/L
ND
1.0
12/03/21 05:14
Bromoform
ug/L
ND
1.0
12/03/21 05:14
Bromomethane
ug/L
ND
2.0
12/03/21 05:14
Carbon disulfide
ug/L
ND
2.0
12/03/21 05:14
Carbon tetrachloride
ug/L
ND
1.0
12/03/21 05:14
Chlorobenzene
ug/L
ND
1.0
12/03/21 05:14
Chloroethane
ug/L
ND
1.0
12/03/21 05:14
Chloroform
ug/L
ND
1.0
12/03/21 05:14
Chloromethane
ug/L
ND
1.0
12/03/21 05:14
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/03/21 05:14
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/03/21 05:14
Cyclohexane
ug/L
ND
1.0
12/03/21 05:14
Dibromochloromethane
ug/L
ND
1.0
12/03/21 05:14
Dichlorodifluoromethane
ug/L
ND
1.0
12/03/21 05:14
Ethylbenzene
ug/L
ND
1.0
12/03/21 05:14
Isopropylbenzene (Cumene)
ug/L
ND
1.0
12/03/21 05:14
Methyl acetate
ug/L
ND
10.0
12/03/21 05:14
Methyl-tert-butyl ether
ug/L
ND
1.0
12/03/21 05:14
Methylcyclohexane
ug/L
ND
10.0
12/03/21 05:14
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 49

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
METHOD BLANK: 3475930
Associated Lab Samples: 92575044002, 92575044007
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Methylene Chloride
ug/L
ND
5.0
12/03/21 05:14
Styrene
ug/L
ND
1.0
12/03/21 05:14
Tetrachloroethene
ug/L
ND
1.0
12/03/21 05:14
Toluene
ug/L
ND
1.0
12/03/21 05:14
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/03/21 05:14
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/03/21 05:14
Trichloroethene
ug/L
ND
1.0
12/03/21 05:14
Trichlorofluoromethane
ug/L
ND
1.0
12/03/21 05:14
Vinyl chloride
ug/L
ND
1.0
12/03/21 05:14
Xylene (Total)
ug/L
ND
1.0
12/03/21 05:14
1,2-Dichloroethane-d4 (S)
%
95
70-130
12/03/21 05:14
4-Bromofluorobenzene (S)
%
99
70-130
12/03/21 05:14
Toluene-d8 (S)
%
100
70-130
12/03/21 05:14
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3475931
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1-Trichloroethane
ug/L
50
49.6
99
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.7
105
70-130
1,1,2-Trichloroethane
ug/L
50
49.4
99
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
52.5
105
70-130
1,1-Dichloroethane
ug/L
50
50.0
100
70-130
1,1-Dichloroethene
ug/L
50
50.6
101
70-132
1,2,3-Trichlorobenzene
ug/L
50
53.4
107
70-134
1,2,4-Trichlorobenzene
ug/L
50
52.6
105
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
55.5
111
70-132
1,2-Dibromoethane (EDB)
ug/L
50
52.2
104
70-130
1,2-Dichlorobenzene
ug/L
50
50.8
102
70-130
1,2-Dichloroethane
ug/L
50
49.3
99
70-130
1,2-Dichloropropane
ug/L
50
51.7
103
70-130
1,3-Dichlorobenzene
ug/L
50
50.7
101
70-130
1,4-Dichlorobenzene
ug/L
50
51.2
102
70-130
2-Butanone (MEK)
ug/L
100
101
101
70-133
2-Hexanone
ug/L
100
110
110
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
105
105
70-130
Acetone
ug/L
100
101
101
70-144
Benzene
ug/L
50
49.4
99
70-130
Bromochloromethane
ug/L
50
49.5
99
70-130
Bromodichloromethane
ug/L
50
50.5
101
70-130
Bromoform
ug/L
50
50.5
101
70-131
Bromomethane
ug/L
50
55.9
112
30-177
Carbon disulfide
ug/L
50
50.8
102
70-133
Carbon tetrachloride
ug/L
50
49.8
100
70-130
Chlorobenzene
ug/L
50
51.5
103
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 49

lreAnalyilcal®
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Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
LABORATORY CONTROL SAMPLE:
Parameter
3475931
Units
Spike LCS
Conc. Result
Chloroethane
ug/L
50
Chloroform
ug/L
50
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Cyclohexane
ug/L
50
Dibromochloromethane
ug/L
50
Dichlorodifluoromethane
ug/L
50
Ethylbenzene
ug/L
50
Isopropylbenzene (Cumene)
ug/L
50
Methyl acetate
ug/L
50
Methyl-tert-butyl ether
ug/L
50
Methylcyclohexane
ug/L
50
Methylene Chloride
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
47.0
94
46-131
48.9
98
70-130
50.5
101
49-130
50.4
101
70-130
49.6
99
70-130
53.0
106
70-131
53.0
106
70-130
54.8
110
52-134
52.4
105
70-130
54.6
109
70-130
51.8
104
70-131
48.8
98
70-130
51.6
103
70-130
47.4
95
68-130
53.6
107
70-130
50.3
101
70-130
49.5
99
70-130
50.6
101
70-130
49.6
99
70-130
49.2
98
70-130
49.0
98
61-130
53.7
107
59-142
157
105
70-130
96
70-130
103
70-130
100
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3475932
MS
92575056002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3475933
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
20
20
20.5
20.3
102
102
70-148
1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.2
21.0
106
105
70-131
1
1,1,2-Trichloroethane
ug/L
ND
20
20
20.8
20.5
104
102
70-136
1
1,1,2-Trichlorotrifluoroethane
ug/L
ND
20
20
22.4
21.0
112
105
70-154
6
1,1-Dichloroethane
ug/L
ND
20
20
20.5
20.4
103
102
70-147
1
1,1-Dichloroethene
ug/L
ND
20
20
19.8
20.1
99
101
70-158
2
1,2,3-Trichlorobenzene
ug/L
ND
20
20
22.1
21.6
110
108
68-140
2
1,2,4-Trichlorobenzene
ug/L
ND
20
20
22.1
21.8
111
109
70-139
1
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.2
21.4
106
107
69-136
0
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.3
21.3
107
106
70-137
0
1,2-Dichlorobenzene
ug/L
ND
20
20
22.0
21.5
110
108
70-133
2
1,2-Dichloroethane
ug/L
ND
20
20
18.9
18.9
94
95
67-138
0
1,2-Dichloropropane
ug/L
ND
20
20
21.6
21.5
108
107
70-138
1
1,3-Dichlorobenzene
ug/L
ND
20
20
21.9
21.8
110
109
70-133
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 22 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3475932
3475933
MS
MSD
92575056002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
20
20
22.3
21.8
112
109
70-133
2
2-Butanone (MEK)
ug/L
ND
40
40
35.4
35.6
88
89
61-147
1
2-Hexanone
ug/L
ND
40
40
40.1
39.2
100
98
67-139
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
38.7
38.7
97
97
67-136
0
Acetone
ug/L
ND
40
40
35.7
35.3
89
88
55-159
1
Benzene
ug/L
ND
20
20
21.8
21.4
109
107
67-150
2
Bromochloromethane
ug/L
ND
20
20
20.4
20.0
102
100
70-146
2
Bromodichloromethane
ug/L
ND
20
20
20.9
21.0
105
105
70-138
0
Bromoform
ug/L
ND
20
20
19.7
19.6
99
98
57-138
1
Bromomethane
ug/L
ND
20
20
18.9
18.6
94
93
10-200
2 v3
Carbon disulfide
ug/L
ND
20
20
20.4
19.9
102
100
70-152
3
Carbon tetrachloride
ug/L
ND
20
20
21.8
22.0
109
110
70-147
1
Chlorobenzene
ug/L
ND
20
20
22.1
21.9
110
110
70-137
1
Chloroethane
ug/L
ND
20
20
21.1
20.4
105
102
51-166
4 v3
Chloroform
ug/L
ND
20
20
19.3
19.0
97
95
70-144
2
Chloromethane
ug/L
ND
20
20
21.0
20.6
105
103
24-161
2
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.1
20.0
100
100
67-148
0
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.0
20.8
105
104
70-142
1
Cyclohexane
ug/L
ND
20
20
20.9
21.1
104
105
70-151
1
Dibromochloromethane
ug/L
ND
20
20
20.9
20.9
104
104
68-138
0
Dichlorodifluoromethane
ug/L
ND
20
20
21.7
21.2
108
106
43-155
2
Ethylbenzene
ug/L
ND
20
20
22.4
22.2
112
111
68-143
1
Isopropylbenzene (Cumene)
ug/L
ND
20
20
23.1
22.9
115
114
70-136
1
Methyl acetate
ug/L
ND
20
20
19.1
19.3
95
96
55-149
1
Methyl-tert-butyl ether
ug/L
ND
20
20
19.5
19.0
97
95
59-156
3
Methylcyclohexane
ug/L
ND
20
20
22.0
21.9
110
109
70-142
1
Methylene Chloride
ug/L
ND
20
20
19.3
19.0
97
95
64-148
2
Styrene
ug/L
ND
20
20
21.8
21.3
109
107
70-136
2
Tetrachloroethene
ug/L
ND
20
20
22.0
22.0
110
110
70-139
0
Toluene
ug/L
ND
20
20
21.3
21.3
107
106
47-157
0
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.5
20.6
107
103
70-149
4
trans- 1,3-Dichloropropene
ug/L
ND
20
20
20.5
20.2
103
101
70-138
2
Trichloroethene
ug/L
ND
20
20
21.9
21.4
109
107
70-149
2
Trichlorofluoromethane
ug/L
ND
20
20
18.0
17.9
90
89
61-154
1
Vinyl chloride
ug/L
ND
20
20
22.4
22.2
112
111
55-172
0
Xylene (Total)
ug/L
ND
60
60
67.1
66.2
112
110
66-145
1
1,2-Dichloroethane-d4 (S)
%
83
84
70-130
4-Bromofluorobenzene (S)
%
99
99
70-130
Toluene-d8(S)
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 23 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 663751 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92575044001
METHOD BLANK: 3476861
Associated Lab Samples: 92575044001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
1.0
12/03/21 22:44
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/03/21 22:44
1,1,2-Trichloroethane
ug/L
ND
1.0
12/03/21 22:44
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
12/03/21 22:44
1,1-Dichloroethane
ug/L
ND
1.0
12/03/21 22:44
1,1-Dichloroethene
ug/L
ND
1.0
12/03/21 22:44
1,2,3-Trichlorobenzene
ug/L
ND
1.0
12/03/21 22:44
1,2,4-Trichlorobenzene
ug/L
ND
1.0
12/03/21 22:44
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/03/21 22:44
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/03/21 22:44
1,2-Dichlorobenzene
ug/L
ND
1.0
12/03/21 22:44
1,2-Dichloroethane
ug/L
ND
1.0
12/03/21 22:44
1,2-Dichloropropane
ug/L
ND
1.0
12/03/21 22:44
1,3-Dichlorobenzene
ug/L
ND
1.0
12/03/21 22:44
1,4-Dichlorobenzene
ug/L
ND
1.0
12/03/21 22:44
2-Butanone (MEK)
ug/L
ND
5.0
12/03/21 22:44
2-Hexanone
ug/L
ND
5.0
12/03/21 22:44
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/03/21 22:44
Acetone
ug/L
ND
25.0
12/03/21 22:44
Benzene
ug/L
ND
1.0
12/03/21 22:44
Bromochloromethane
ug/L
ND
1.0
12/03/21 22:44
Bromodichloromethane
ug/L
ND
1.0
12/03/21 22:44
Bromoform
ug/L
ND
1.0
12/03/21 22:44
Bromomethane
ug/L
ND
2.0
12/03/21 22:44
Carbon disulfide
ug/L
ND
2.0
12/03/21 22:44
Carbon tetrachloride
ug/L
ND
1.0
12/03/21 22:44
Chlorobenzene
ug/L
ND
1.0
12/03/21 22:44
Chloroethane
ug/L
ND
1.0
12/03/21 22:44
Chloroform
ug/L
ND
1.0
12/03/21 22:44
Chloromethane
ug/L
ND
1.0
12/03/21 22:44
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/03/21 22:44
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/03/21 22:44
Cyclohexane
ug/L
ND
1.0
12/03/21 22:44
Dibromochloromethane
ug/L
ND
1.0
12/03/21 22:44
Dichlorodifluoromethane
ug/L
ND
1.0
12/03/21 22:44
Ethylbenzene
ug/L
ND
1.0
12/03/21 22:44
Isopropylbenzene (Cumene)
ug/L
ND
1.0
12/03/21 22:44
Methyl acetate
ug/L
ND
10.0
12/03/21 22:44
Methyl-tert-butyl ether
ug/L
ND
1.0
12/03/21 22:44
Methylcyclohexane
ug/L
ND
10.0
12/03/21 22:44
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
METHOD BLANK: 3476861
Associated Lab Samples: 92575044001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Methylene Chloride
ug/L
ND
5.0
12/03/21 22:44
Styrene
ug/L
ND
1.0
12/03/21 22:44
Tetrachloroethene
ug/L
ND
1.0
12/03/21 22:44
Toluene
ug/L
ND
1.0
12/03/21 22:44
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/03/21 22:44
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/03/21 22:44
Trichloroethene
ug/L
ND
1.0
12/03/21 22:44
Trichlorofluoromethane
ug/L
ND
1.0
12/03/21 22:44
Vinyl chloride
ug/L
ND
1.0
12/03/21 22:44
Xylene (Total)
ug/L
ND
1.0
12/03/21 22:44
1,2-Dichloroethane-d4 (S)
%
103
70-130
12/03/21 22:44
4-Bromofluorobenzene (S)
%
105
70-130
12/03/21 22:44
Toluene-d8 (S)
%
102
70-130
12/03/21 22:44
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3476862
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1-Trichloroethane
ug/L
50
43.4
87
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.8
100
70-130
1,1,2-Trichloroethane
ug/L
50
49.7
99
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
43.6
87
70-130
1,1-Dichloroethane
ug/L
50
48.1
96
70-130
1,1-Dichloroethene
ug/L
50
44.5
89
70-132
1,2,3-Trichlorobenzene
ug/L
50
44.4
89
70-134
1,2,4-Trichlorobenzene
ug/L
50
44.2
88
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
45.8
92
70-132
1,2-Dibromoethane (EDB)
ug/L
50
47.7
95
70-130
1,2-Dichlorobenzene
ug/L
50
46.6
93
70-130
1,2-Dichloroethane
ug/L
50
48.6
97
70-130
1,2-Dichloropropane
ug/L
50
52.3
105
70-130
1,3-Dichlorobenzene
ug/L
50
45.3
91
70-130
1,4-Dichlorobenzene
ug/L
50
46.6
93
70-130
2-Butanone (MEK)
ug/L
100
104
104
70-133
2-Hexanone
ug/L
100
105
105
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
115
115
70-130
Acetone
ug/L
100
109
109
70-144
Benzene
ug/L
50
48.7
97
70-130
Bromochloromethane
ug/L
50
44.6
89
70-130
Bromodichloromethane
ug/L
50
48.7
97
70-130
Bromoform
ug/L
50
43.6
87
70-131
Bromomethane
ug/L
50
47.3
95
30-177
Carbon disulfide
ug/L
50
45.8
92
70-133
Carbon tetrachloride
ug/L
50
45.1
90
70-130
Chlorobenzene
ug/L
50
46.1
92
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
LABORATORY CONTROL SAMPLE:
Parameter
3476862
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Chloroethane
ug/L
50
54.7
109
46-131
Chloroform
ug/L
50
47.1
94
70-130
Chloromethane
ug/L
50
47.8
96
49-130
cis-1,2-Dichloroethene
ug/L
50
47.9
96
70-130
cis-1,3-Dichloropropene
ug/L
50
50.8
102
70-130
Cyclohexane
ug/L
50
47.9
96
70-131
Dibromochloromethane
ug/L
50
44.3
89
70-130
Dichlorodifluoromethane
ug/L
50
46.3
93
52-134
Ethylbenzene
ug/L
50
47.0
94
70-130
Isopropylbenzene (Cumene)
ug/L
50
47.5
95
70-130
Methyl acetate
ug/L
50
47.1
94
70-131
Methyl-tert-butyl ether
ug/L
50
46.8
94
70-130
Methylcyclohexane
ug/L
50
52.1
104
70-130
Methylene Chloride
ug/L
50
48.4
97
68-130
Styrene
ug/L
50
47.5
95
70-130
Tetrachloroethene
ug/L
50
41.8
84
70-130
Toluene
ug/L
50
49.2
98
70-130
trans-1,2-Dichloroethene
ug/L
50
48.8
98
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.9
100
70-130
Trichloroethene
ug/L
50
45.0
90
70-130
Trichlorofluoromethane
ug/L
50
42.7
85
61-130
Vinyl chloride
ug/L
50
47.7
95
59-142
Xylene (Total)
ug/L
150
140
93
70-130
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
103
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3476863
MS
92574833009 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3476864
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
200
200
208
203
104
102
70-148
2
1,1,2,2-Tetrachloroethane
ug/L
ND
200
200
201
205
101
102
70-131
2
1,1,2-Trichloroethane
ug/L
ND
200
200
206
210
103
105
70-136
2
1,1,2-Trichlorotrifluoroethane
ug/L
ND
200
200
202
197
101
98
70-154
3
1,1-Dichloroethane
ug/L
ND
200
200
230
221
115
111
70-147
4
1,1-Dichloroethene
ug/L
ND
200
200
215
210
108
105
70-158
3
1,2,3-Trichlorobenzene
ug/L
ND
200
200
176
213
88
106
68-140
19
1,2,4-Trichlorobenzene
ug/L
ND
200
200
170
205
85
103
70-139
19
1,2-Dibromo-3-chloropropane
ug/L
ND
200
200
177
214
89
107
69-136
19
1,2-Dibromoethane (EDB)
ug/L
ND
200
200
199
202
99
101
70-137
2
1,2-Dichlorobenzene
ug/L
ND
200
200
192
239
96
119
70-133
22
1,2-Dichloroethane
ug/L
ND
200
200
221
216
110
108
67-138
2
1,2-Dichloropropane
ug/L
ND
200
200
239
235
119
118
70-138
2
1,3-Dichlorobenzene
ug/L
ND
200
200
191
187
96
93
70-133
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 26 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3476863
3476864
MS
MSD
92574833009
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
200
200
202
193
101
97
70-133
5
2-Butanone (MEK)
ug/L
504
400
400
983
960
120
114
61-147
2
2-Hexanone
ug/L
ND
400
400
430
469
108
117
67-139
9
4-Methyl-2-pentanone (MIBK)
ug/L
ND
400
400
501
505
117
118
67-136
1
Acetone
ug/L
3560
400
400
4050
4020
121
114
55-159
1 E
Benzene
ug/L
ND
200
200
228
224
112
109
67-150
2
Bromochloromethane
ug/L
ND
200
200
209
204
104
102
70-146
2
Bromodichloromethane
ug/L
ND
200
200
210
210
105
105
70-138
0
Bromoform
ug/L
ND
200
200
174
180
87
90
57-138
3
Bromomethane
ug/L
ND
200
200
112
149
56
75
10-200
28
Carbon disulfide
ug/L
ND
200
200
209
202
104
101
70-152
3
Carbon tetrachloride
ug/L
ND
200
200
203
200
102
100
70-147
2
Chlorobenzene
ug/L
ND
200
200
198
195
99
98
70-137
1
Chloroethane
ug/L
22.3
200
200
266
267
122
122
51-166
0
Chloroform
ug/L
ND
200
200
206
206
103
103
70-144
0
Chloromethane
ug/L
ND
200
200
219
223
110
111
24-161
1
cis-1,2-Dichloroethene
ug/L
ND
200
200
218
213
109
107
67-148
2
cis-1,3-Dichloropropene
ug/L
ND
200
200
203
206
102
103
70-142
1
Cyclohexane
ug/L
ND
200
200
226
214
113
107
70-151
5
Dibromochloromethane
ug/L
ND
200
200
187
189
94
94
68-138
1
Dichlorodifluoromethane
ug/L
ND
200
200
210
203
105
102
43-155
3
Ethylbenzene
ug/L
ND
200
200
206
205
103
103
68-143
0
Isopropylbenzene (Cumene)
ug/L
ND
200
200
200
206
100
103
70-136
3
Methyl acetate
ug/L
ND
200
200
207
204
103
102
55-149
1
Methyl-tert-butyl ether
ug/L
ND
200
200
198
188
99
94
59-156
5
Methylcyclohexane
ug/L
ND
200
200
229
222
114
111
70-142
3
Methylene Chloride
ug/L
ND
200
200
264
257
109
106
64-148
3
Styrene
ug/L
ND
200
200
198
202
99
101
70-136
2
Tetrachloroethene
ug/L
ND
200
200
184
183
92
91
70-139
1
Toluene
ug/L
ND
200
200
226
223
109
107
47-157
1
trans-1,2-Dichloroethene
ug/L
ND
200
200
209
214
104
107
70-149
3
trans- 1,3-Dichloropropene
ug/L
ND
200
200
196
199
98
100
70-138
2
Trichloroethene
ug/L
ND
200
200
205
203
102
101
70-149
1
Trichlorofluoromethane
ug/L
ND
200
200
199
194
100
97
61-154
3
Vinyl chloride
ug/L
ND
200
200
227
224
113
112
55-172
1
Xylene (Total)
ug/L
ND
600
600
621
608
104
101
66-145
2
1,2-Dichloroethane-d4 (S)
%
101
100
70-130
4-Bromofluorobenzene (S)
%
101
103
70-130
Toluene-d8(S)
%
103
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 27 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 663547 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92575044001, 92575044002, 92575044003
METHOD BLANK: 3475994
Matrix:
Water
Associated Lab Samples:
92575044001, 92575044002, 92575044003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
12/02/21 17:23
1,2-Dichloroethane-d4 (S)
%
101
70-130
12/02/21 17:23
Toluene-d8 (S)
%
103
66-133
12/02/21 17:23
LABORATORY CONTROL SAMPLE: 3475995
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 18.6 93 70-130
1,2-Dichloroethane-d4 (S) % 100 70-130
Toluene-d8 (S) % 102 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3475996
3475997
MS
MSD
92575044003 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L 3.2 20
20 23.4
22.3 101
95
64-141 5
1,2-Dichloroethane-d4 (S)
%
104
109
70-130
Toluene-d8(S)
%
104
106
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 663297
Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C
Analysis Description: 8270E Water MSSV
RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92575044001, 92575044002,
92575044003
METHOD BLANK: 3474659
Matrix: Water
Associated Lab Samples: 92575044001, 92575044002,
92575044003
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
2,4,6-Tribromophenol (S)
%
46 10-144
12/02/21 09:21
2-Fluorobiphenyl (S)
%
72 10-130
12/02/21 09:21
2-Fluorophenol(S)
%
44 10-130
12/02/21 09:21
Nitrobenzene-d5 (S)
%
77 10-144
12/02/21 09:21
Phenol-d6 (S)
%
40 10-130
12/02/21 09:21
Terphenyl-d14 (S)
%
76 34-163
12/02/21 09:21
LABORATORY CONTROL SAMPLE:
3474660
Spike LCS
LCS %
Rec
Parameter
Units
Conc. Result
% Rec Limits
Qualifiers
2,4,6-Tribromophenol (S)
%
69
10-144
2-Fluorobiphenyl (S)
%
50
10-130
2-Fluorophenol(S)
%
37
10-130
Nitrobenzene-d5 (S)
%
56
10-144
Phenol-d6 (S)
%
31
10-130
Terphenyl-d14 (S)
%
68
34-163
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3474661 3474662
MS MSD
92573910005
Spike Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Biphenyl (Diphenyl)
ug/L ND
50 50 34.6
37.4
69 75
17-130 8
Diphenyl ether (Phenyl ether)
ug/L ND
50 50 34.4
37.0
69 74
16-130 7
2,4,6-Tribromophenol (S)
%
86 87
10-144
2-Fluorobiphenyl (S)
%
68 74
10-130
2-Fluorophenol(S)
%
53 59
10-130
Nitrobenzene-d5 (S)
%
75 81
10-144
Phenol-d6 (S)
%
40 47
10-130
Terphenyl-d14 (S)
%
73 72
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 29 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 663809 Analysis Method: EPA 9056A
QC Batch Method: EPA 9056A Analysis Description: 9056 IC anions 28 Days
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92575044001, 92575044002, 92575044003
METHOD BLANK: 3477215
Matrix:
Water
Associated Lab Samples: 92575044001, 92575044002, 92575044003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Sulfate
mg/L
ND
1.0
12/04/2110:59
LABORATORY CONTROL SAMPLE:
3477216
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Sulfate
mg/L
50
47.3
95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3477217 3477218
MS MSD
92575044001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 5.5 50 50 51.0 51.6 91 92 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 30 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 664543 Analysis Method: EPA 9060A
QC Batch Method: EPA 9060A Analysis Description: 9060 TOC, AVL
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92575044001, 92575044002, 92575044003
METHOD BLANK: 3481125
Matrix:
Water
Associated Lab Samples: 92575044001, 92575044002, 92575044003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mean Total Organic Carbon
mg/L
ND
1.0
12/08/21 09:24
Total Organic Carbon
mg/L
ND
1.0
12/08/21 09:24
Total Organic Carbon
mg/L
ND
1.0
12/08/21 09:24
Total Organic Carbon
mg/L
ND
1.0
12/08/21 09:24
Total Organic Carbon
mg/L
ND
1.0
12/08/21 09:24
LABORATORY CONTROL SAMPLE:
3481126
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Mean Total Organic Carbon
mg/L
25
26.7
107
75-125
Total Organic Carbon
mg/L
25
25.9
104
75-125
Total Organic Carbon
mg/L
25
26.6
106
75-125
Total Organic Carbon
mg/L
25
27.2
109
75-125
Total Organic Carbon
mg/L
25
27.0
108
75-125
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3481127
3481128
MS
MSD
92575044001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Mean Total Organic Carbon
mg/L
916
25
25
912
911
-18
-20
75-125
0 M1
Total Organic Carbon
mg/L
898
25
25
895
897
-12
-4
75-125
0 M1
Total Organic Carbon
mg/L
916
25
25
908
904
-30
-50
75-125
1 M1
Total Organic Carbon
mg/L
919
25
25
914
921
-20
8
75-125
1 M1
Total Organic Carbon
mg/L
932
25
25
930
924
-10
-32
75-125
1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 31 of 49

lreAnalyilcal®
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
QC Batch: 729535 Analysis Method: AM23G
QC Batch Method: AM23G Analysis Description: Low Level Volatile Fatty Acids
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92575044001
METHOD BLANK: 2286612
Associated Lab Samples: 92575044001
Parameter Units
Acetic Acid mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.50 12/14/2117:23
LABORATORY CONTROL SAMPLE & LCSD: 2286613 2286661
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Acetic Acid mg/L 2 2.0 2.0 99 99 70-130 0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC.
Page 32 of 49

Pace Analytical Services, LLC
ceAnalXical ® Greenwood,urst SC 2 East
Grenwood, SC 29649
www.pacelabs.com [phone]
QUALIFIERS
Project: NRLF NOVEMBER 2021
Pace Project No.: 92575044
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
WORKORDER QUALIFIERS
WO: 92575044
[1] Project Manager Comments - On 12/14, the analyst emailed that the samples assigned Hydrogen analyses could not be
located. There was nothing noted during sample receipt about any problems with the shipment. Receiving checked on
12/15 and 12/16 throughout the laboratory areas and was unable to locate the Hydrogen vials. These analyses were
canceled from the project. (Ruth Welsh(Do Not 12/17/2021 10:42)
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/23/2021 10:34 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 49

lreAnalyilcal®
www.pacelabs.cem
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
NRLF NOVEMBER 2021
92575044
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method Batch
92575044001
B-01-113021
EPA 353.2 Rev 2.0 1993
663324
92575044002
B-10-113021
EPA 353.2 Rev 2.0 1993
663324
92575044003
B-3213-113021
EPA 353.2 Rev 2.0 1993
663324
92575044001
B-01-113021
SM 4500-P E-2011
663113
92575044002
B-10-113021
SM 4500-P E-2011
663113
92575044003
B-3213-113021
SM 4500-P E-2011
663113
92575044001
B-01-113021
EPA 8015 Alcohol -Glycol
653919
92575044002
B-10-113021
EPA 8015 Alcohol -Glycol
653919
92575044003
B-3213-113021
EPA 8015 Alcohol -Glycol
653919
92575044001
B-01-113021
RSK-175
728703
92575044002
B-10-113021
RSK-175
728703
92575044003
B-3213-113021
RSK-175
728703
92575044001
B-01-113021
RSK-175
729093
92575044002
B-10-113021
RSK-175
729093
92575044003
B-3213-113021
RSK-175
729093
92575044001
B-01-113021
EPA 3510C
663297
EPA 8270E 663318
92575044002
B-10-113021
EPA 3510C
663297
EPA 8270E 663318
92575044003
B-3213-113021
EPA 3510C
663297
EPA 8270E 663318
92575044001
B-01-113021
EPA 8260D
663751
92575044002
B-10-113021
EPA 8260D
663537
92575044007
TRIP BLANK 02-113021
EPA 8260D
663537
92575044001
B-01-113021
EPA 8260D Mod.
663547
92575044002
B-10-113021
EPA 8260D Mod.
663547
92575044003
B-3213-113021
EPA 8260D Mod.
663547
92575044001
B-01-113021
EPA 9056A
663809
92575044002
B-10-113021
EPA 9056A
663809
92575044003
B-3213-113021
EPA 9056A
663809
92575044001
B-01-113021
EPA 9060A
664543
92575044002
B-10-113021
EPA 9060A
664543
92575044003
B-3213-113021
EPA 9060A
664543
92575044001
B-01-113021
AM23G
729535
92575044002
B-10-113021
AM23G
729173
92575044003
B-3213-113021
AM23G
729173
Date: 12/23/2021 10:34 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 34 of 49

Document Name: J Document
Corufition U on Recee t (SCUR1
Document No.; T�T
F CAR-CS-033-Rev.03 Pace Carolinas Qua!R Office
laharatary receiving sa les:
Asheville ❑ EdenV1 Greenwood ❑ Huntersvllle ❑ Raleigh[] Mechanlesville❑ Atlanta❑ Omersv(lle❑
OieneNante:
Rrojeet g WO# a 9:2575044
�
CouWer: ❑ ace x UPS ❑
Commercial r ❑Client II IIII ICI I IIIII II I III
❑
92575044
Custody Seal Present? ❑Yes O Seats Intact? ❑Yes ❑No �l ► �,�
oaiaJInitiafs Persoo Exurninind Contui[s�, i1l 1 1 ! 1
packing Material: ❑Bubble Wrap []Bubble Bags ❑None ❑ other BlologfcalTissue Frozen?
Thermometer. []Yes❑No ❑N/A
�!R Gun !D:p$3 Type of ice: ❑wet ❑Blue ❑Hone
Correction Factor:
Canter Temp: u • C9 Add/Subtract (,Q Temp should be above freezing to 6'C
13sempits outof tamp riiteris.$amples on fee, coomi;Process
Cooler Tamp Corrected (°C� . hasbalun
USDARegulated Soft (PN/A, water sample)
Did samples ofigivate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Old sarrpfesorlsM to from a foreign source (Into tationft
Yes No Including Hawaii and Puerto Rico)? []Yes f Fla
i-na1(1QTV.U5TQffYrmsentf
Jdym
Ofto
QNIA
1 I.
Samples Arrived within Hold Time?
2f,
No
N/A
1 Z,
Short hold Time Analysis <n hr.?
Yes
Ne
A
3.
Rush Turn Around Time uested7
yes
a
N/A
4.
SufficlentVolume?Pry6s
ONO
ONIA
5.
Correct Containers Used?
pN1,
pN/A
6.
-Pace Container3 Used?
Yes
Na
ONA
Containers Intact?
Yes
ONO
EIN/A
7.
Sample Labels Irlatch CAC? , _ �jfYes ©Na (IN/A 19.
Heads ace In VOAVlafs �S-6mrn ? YesMo EINIA 10.
Trip Blank Present? ����as ©No CIN/A 1L
Trip Blank Custody Seats Present? De. IiNe f-ltila
COMMENTS/SAMPLE DISCREPANCY
Lot 1O of split containers:
CLIENT NOT(FICATION/RESOLUTION
Field Data RaquIrad? []Yes
Person contacted: Oate/Pime:
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date: C/ ti

Document flame:
Document No.:
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Fxceptlons: VOA, Collform, MO Oil and Grease, DRO/8015 (water) DOC, U.Hi;
**Bottom half of box is to list number of bodes
Document Revlsed: November 15, 2021
Project WaL ; g;257F044
PM: 9V Due Date: 12/10/21
CLIENT: 97—CNA
.rrt
a
a a a o
s a a a
3i q� a a p 3 y
£ E x q. 7 s aTi a 3
a. gL
Ewil
£
1 O S
l 2
9
it
12
pH Adjustment
Log for Preserved Samples
$ample iD
Type of Preservative
pH upon receipt
date preservation adjusted
Time prenration
adjusted
Amount of Preservative
added
Lpt N
Note: Whenever there Is a discrepancy affecting North Caroirea compliance samples, a copy or mrs rorm wou ae senr w the north 9.131`011na ur[MMA LemncapOn uflrte the.
Out of hold, Incorrect preservative, out of temp, Incorrect containers.

;y
-n�
t•
���, � aaa■�lwwa��e�r� -
MMMME■!wUCIUM
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MMIMMEMMMMIRMOMMEME
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ON
ENNOMMMMUMIUM
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�•,I � PP.byµ; �� ;'• � i
w �

urofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins TestAmerica, Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-208261-1
Client Project/Site: 92575044/NRLF November 2021
Pace Analytical Services, LLC
9800 Kincey Avenue, Suite 100
Huntersville, North Carolina 28078
Attn: Bonnie Vang
Authorized for release by.
121912021 3:36:04 PM
Sheila Hoffman, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory. page 38 of 49

Sample Summary
Client: Pace Analytical Services, LLC
Project/Site: 92575044/NRLF November 2021
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
680-208261-1
B-01-113021
Water
11/30/21 11:40
12/03/21 10:55
680-208261-2
B-10-113021
Water
11/30/21 13:40
12/03/21 10:55
680-208261-3
B-3213-113021
Water
11/30/2114:54
12/03/21 10:55
F
Job ID: 680-208261-1
U
Eurofins TestAmeric0aft3grOAH
Page 2 of 12 12/9/2021

Method Summary
Client: Pace Analytical Services, LLC
Project/Site: 92575044/NRLF November 2021
F
Job ID: 680-208261-1
U
Method Method Description Protocol Laboratory
2320B-2011 Alkalinity, Total SM TAL SAV
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins TestAmerica, Savannah
Page 40 of 49
Page 3 of 12 12/9/2021

Definitions/Glossary
Client: Pace Analytical Services, LLC
Project/Site: 92575044/NRLF November 2021
Qualifiers
General Chemistry
Qualifier Qualifier Description
U Indicates that the compound was analyzed for but not detected.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
c Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
oil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Lever'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MOIL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
F
Job ID: 680-208261-1
Page 4 of 12
Eurofins TestAmerica, Savannah
Page 41 of 49
12/9/2021

Case Narrative
Client: Pace Analytical Services, LLC
Project/Site: 92575044/NRLF November 2021
Job ID: 680-208261-1
Laboratory: Eurofins TestAmerica, Savannah
Narrative
CASE NARRATIVE
Job ID: 680-208261-1
Client: Pace Analytical Services, LLC
Project: 92575044/NRLF November 2021 C
Report Number: 680-208261-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 12/03/2021; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 1.5 C.
ALKALINITY
Samples B-01-113021 (680-208261-1), B-10-113021 (680-208261-2) and 13-3213-113021 (680-208261-3) were analyzed for alkalinity in
accordance with SM 2320B. The samples were analyzed on 12/08/2021.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins TestAmerical g&g&A"A8
Page 5 of 12 12/9/2021

Client Sample Results
Client: Pace Analytical Services, LLC
Project/Site: 92575044/NRLF November 2021
Client Sample ID: B-01-113021
Date Collected: 11/30/21 11:40
Date Received: 12/03/21 10:55
F
Job ID: 680-208261-1
Lab Sample ID: 680-208261-1
Matrix: Water
General Chemistry
Analyte
Result Qualifier
PQL
MDL
Unit
D Prepared Analyzed Dil Fac
Alkalinity
1300
5.0
5.0
mg/L
—
12/08/21 13:55 1
Bicarbonate Alkalinity
1300
5.0
5.0
mg/L
12/08/21 13:55 1
Carbonate Alkalinity
5.0 U
5.0
5.0
mg/L
12/08/21 13:55 1
Client Sample ID: B-10-113021
Lab Sample ID: 680-208261-2
Date Collected: 11/30/21 13:40
Matrix: Water
E:
Date Received: 12/03/21 10:55
General Chemistry
F
Analyte
Result Qualifier
PQL
MDL
Unit
D Prepared Analyzed Dil Fac
Alkalinity
420
5.0
5.0
mg/L
12/08/21 13:55 1
Bicarbonate Alkalinity
420
5.0
5.0
mg/L
12/08/21 13:55 1
Carbonate Alkalinity
5.0 U
5.0
5.0
mg/L
12/08/21 13:55 1
Client Sample ID: 13-3213-113021
Lab Sample ID: 680-208261-3
Date Collected: 11/30/21 14:54
Matrix: Water
Date Received: 12/03/21 10:55
General Chemistry
Analyte
Result Qualifier
PQL
MDL
Unit
D Prepared Analyzed Dil Fac
Alkalinity
160
5.0
5.0
mg/L
12/08/21 13:55 1
Bicarbonate Alkalinity
160
5.0
5.0
mg/L
12/08/21 13:55 1
Carbonate Alkalinity
5.0 U
5.0
5.0
mg/L
12/08/21 13:55 1
Eurofins TestAmerica, Savannah
Page 43 of 49
Page 6 of 12 12/9/2021

QC Sample Results
Client: Pace Analytical Services, LLC
Job ID: 680-208261-1
Project/Site: 92575044/NRLF November 2021
Method: 2320B-2011 - Alkalinity, Total
Lab Sample ID: MB 680-697941/8
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 697941
MB
MB
Analyte Result
Qualifier
PQL
MDL Unit
D Prepared Analyzed Dil Fac
Alkalinity 5.0
U
5.0
5.0 mg/L
12/08/21 13:55 1
Bicarbonate Alkalinity 5.0
U
5.0
5.0 mg/L
12/08/21 13:55 1
Carbonate Alkalinity 5.0
U
5.0
5.0 mg/L
12/08/21 13:55 1
Lab Sample ID: LCS 680-697941/10
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 697941
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit D %Rec Limits
Alkalinity
250
249
mg/L 100 90 - 112
Lab Sample ID: LCSD 680-697941/34
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 697941
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit D %Rec Limits RPD Limit
Alkalinity
250
270
mg/L 108 90 - 112 8 30
Page 7 of 12
Eurofins TestAmerica, Savannah
Page 44 of 49
12/9/2021

QC Association Summary
Client: Pace Analytical Services, LLC
Project/Site: 92575044/NRLF November 2021
General Chemistry
Analysis Batch: 697941
Lab Sample ID
Client Sample ID
680-208261-1
B-01-113021
680-208261-2
B-10-113021
680-208261-3
B-32B-113021
MB 680-697941/8
Method Blank
LCS 680-697941/10
Lab Control Sample
LCSD 680-697941/34
Lab Control Sample Dup
Prep Type
Matrix
Total/NA
Water
Total/NA
Water
Total/NA
Water
Total/NA
Water
Total/NA
Water
Total/NA
Water
Job ID: 680-208261-1
Method
2320B-2011
2320B-2011
2320B-2011
2320E-2011
2320E-2011
2320E-2011
Prep Batch
Page 8 of 12
Eurofins TestAmerica, Savannah
Page 45 of 49
12/9/2021

Lab Chronicle
Client: Pace Analytical Services, LLC
Job ID: 680-208261-1
Project/Site: 92575044/NRLF November 2021
Client Sample ID: B-01-113021
Lab Sample ID: 680-208261-1
Date Collected: 11/30/21 11:40
Matrix: Water
Date Received: 12/03/21 10:55
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 2320B-2011
1
697941
12/08/21 13:55 DR TAL SAV
Instrument ID: NOEQUIP
Client Sample ID: B-10-113021
Lab Sample ID: 680-208261-2
Date Collected: 11/30/21 13:40
Matrix: Water
Date Received: 12/03/21 10:55
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 2320B-2011
1
697941
12/08/21 13:55 DR TAL SAV
Instrument ID: NOEQUIP
Client Sample ID: 13-3213-113021
Lab Sample ID: 680-208261-3
Date Collected: 11/30/21 14:54
Matrix: Water
Date Received: 12/03/21 10:55
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 232OB-2011
1
697941
12/08/21 13:55 DR TAL SAV
Instrument ID: NOEQUIP
Laboratory References:
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA
31404, TEL [phone]
Eurofins TestAmerica, Savannah
Page 46 of 49
Page 9 of 12 12/9/2021

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Login Sample Receipt Checklist
Client: Pace Analytical Services, LLC
Job Number: 680-208261-1
Login Number: 208261
List Number: 1
Creator: Hartley, Tyler
Question
List Source: Eurofins TestAmerica, Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True m
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins TestAmerica, Savannah Page 48 of 49
Page 11 of 12 12/9/2021

Accreditation/Certification Summary
Client: Pace Analytical Services, LLC
Job ID: 680-208261-1
Project/Site: 92575044/NRLF November 2021
Laboratory: Eurofins TestAmerica, Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program
Identification Number
Expiration Date
North Carolina (WW/SW) State
269
12-31-21
South Carolina State
98001
06-30-22
Virginia N ELAP
10509
06-29-22
F
F
M
Eurofins TestAmerica, Savannah
Page 49 of 49
Page 12 of 12
12/9/2021

/" .=CQM AECOM 404.965.9600 tel
One Midtown Plaza 404.965.9605 fax
1360 Peachtree St. N.E.
Suite 500
Atlanta, GA 30309
Memorandum
To Jing Zhou — AECOM Atlanta Page 1 of 4
CC
Subject Level 2 Data Validation for Needmore Road Landfill
From Robert Davis — AECOM Atlanta
Date March 14, 2022
Limited validation of the analytical data for the water samples was performed on two data packages
received from Pace Analytical Services, Inc. in Greenwood, South Carolina. The samples were
collected on November 29-30, 2021, at the Needmore Road Landfill in North Carolina.
The data were reviewed for conformance to method specifications and the project guidance
document: Supplemental Characterization and Long -Term Monitoring (AECOM, July 2010 Revision
2). Data qualifiers were applied in accordance with the validation criteria set forth in USEPA
Contract Laboratory Program (CLP) National Functional Guidelines for Organic Superfund Methods
Data Review EPA-540-R-20-005, November 2020 and USEPA National Functional Guidelines for
Inorganic Superfund Methods Data Review, EPA-542-R-20-006, November 2020, as they apply to
the analytical methods employed. Field duplicate relative percent difference (RPD) review and
applicable control limits were taken from the USEPA Region 1, New England Data Validation
Functional Guidelines for Evaluating Environmental Analyses, December 1996.
The following methods were requested on the chain -of -custody (COC) records:
• Method 8260D — Volatiles by Gas Chromatography/Mass Spectrometry (GC/MS);
• Method 8260D SIM — Volatiles by GC/MS in SIM mode;
• Method 8270E — Semivolatiles by GC/MS;
• Method 8015M — Ethylene Glycol by GC;
• Method 2320B — Alkalinity;
• Method 353.2 — Nitrate and Nitrite;
• SM450OP-E — Orthophosphate;
• Method 9056A — Sulfate by Ion Chromatography (IC);
• Method AM23G — Volatile Fatty Acids;
• Method AM20GAX — Hydrogen;
• Method AM20GAX — Dissolved Gases (MEE); and
• Method RSK-175 —Carbon Dioxide.

AECOM
2
Review Elements
Sample data were reviewed for the following quality control parameters:
• Agreement of analyses conducted with COC requests;
• Holding times and sample preservation;
• GC/MS hardware tunes, initial and continuing calibrations;
• Method blanks/trip blanks;
• Surrogate recoveries;
• Laboratory control sample (LCS) recoveries;
• Matrix spike/matrix spike duplicate (MS/MSD) recoveries; and
• Field duplicate precision results.
Samples
Environmental Field Management (EFM) personnel collected the following water samples from the
Needmore Road Landfill in North Carolina, as reported under the Pace Analytical Services, Inc. job
number:
Lab ID
Sample ID
Lab ID
Sample ID
92574833001
TRIP BLANK-01-112921
92574833013
B-1713-113021
92574833002
SW-7-112921
92574833014
B-22A-113021
92574833003
SW-5-112921
92574833015
B-09C-113021
92574833004
SW-3-112921
92574833016
B-21 B-113021
92574833005
SW-8-112921
92574833017
B-99C-113021
92574833006
B-24B-112921
92574833018
B-23A-112921 H2
92574833007
B-24A-112921
92574833019
B-2313-112921 H2
92574833008
B-23A-112921
92574833020
B-17C-112921 H2
92574833009
B-23B-112921
92574833021
B-2213-113021 H2
92574833010
B-17C-112921
92574833022
B-1713-113021 H2
92574833011
B-12-112921
92574833023
B-22A-113021 H2
92574833012
B-2213-113021
92575044
Lab ID
Sample ID
Lab ID
Sample ID
92575044001
B-01-113021
92575044003
B-32B-113021
92575044002
B-10-113021
92575044007
TRIP BLANK 02-113021
Analytical Results
In general, the data results are valid as reported and may be used for decision -making purposes.
Sample data were qualified with "J-" (estimated, biased low). See Table 1.

AECOM
DISCUSSION
Agreement of Analyses Conducted with Chain -of -Custody (COC) Requests
Sample reports were checked to verify agreement with the COC request. No discrepancies were
noted.
Holding Times and Sample Preservation
All samples were analyzed within the holding times required by the methods with the following
exceptions:
• Method SM4500P-E: Several samples were outside of the holding time for orthophosphate.
The orthophosphate results were qualified. See Table 1.
All coolers were received within the optimal range of 4±2 degrees Celsius (°C).
All samples were properly preserved as specified by the methods.
GUMS Tunes, Initial and Continuing Calibrations
GC/MS tuning and calibration summaries were not submitted for validation in this Level II data
package.
Method Blanks/Trip Blanks
No analytes were detected at concentrations exceeding the reporting limits for the method blanks or
trip blanks.
Surrogate Recoveries
The surrogate recoveries were acceptable for all analyses with the following exception:
• Method 8270E: Surrogate 2-fluorobiphenyl was outside of the quality control limits biased
high in sample B-23A-112921. Based on the National Functional Guidelines, one acid and
one base can be outside of the quality control limits for method 8270. Data qualification
was not required.
Laboratory Control Sample (LCS) Recoveries
LCS recoveries for all of the analyses were within the quality control limits.
Matrix Spike/Matrix Spike Duplicate (MS/MSD) Recoveries
MS/MSDs that were performed on non -project samples were not evaluated because matrix
similarity to project samples could not be assumed.
The MS/MSD recoveries on client samples were all within the advisory limits with the following
exception:
• Method 906OA: The total organic carbon (TOC) MS/MSD recoveries were outside of the
quality control limits in sample B-01-113021. The spike amounts were less than 25% of the
sample concentrations; therefore, data qualification was not required.
Field Duplicate Precision Results
A field duplicate was collected on sample B-09C-113021. See Table 2 for the calculated RPDs for
all compounds for which there were detections. The RPDs between the original and field duplicate
were all within the advisory limits of 0-30%. Field sampling/laboratory precision and sample
homogeneity were acceptable. No data qualifications were required.

AECOM
Table 1
Qualified Analytical Data
Lab
Lab
Validated
Validation
Reason
Sample ID
Method
Analyte
Result
Qual
Result
Qualifier
Units
Codes
B-2413-112921
SM450OP-E
Orthophosphate
0.22
0.22
J-
m /L
HT
B-24A-112921
SM450OP-E
Orthophosphate
0.36
0.36
J-
m /L
HT
1: USEPA-defined data validation qualifiers applied in this data evaluation:
J-: The associated numerical value is the approximate concentration of the compound in the sample biased low.
Z: Reason Codes:
HT: The holding time was exceeded.
Notes:
mg/L: milligrams per liter
Table 2
Field Precision
Method
Compound
B-09C-113021
B-99C-113021
Units
% RPD
8270E
Diphenyl ether
21.2
18.9
pg/L
11
8260D
Acetone
3460
3520
pg/L
1.7
8260D
2-Butanone
548
583
pg/L
6.2
8260D
cis- 1,2-Dichloroethene
14.8
14.3
pg/L
3.4
8260D
MIBK
ND
95.8
pg/L
NC*
8260D
1,4-Dioxane
909
956
pg/L
5.0
Notes:
% RPD: Relative percent difference between the original sample result and the sample duplicate result.
* The original sample and the duplicate sample are <5X the reporting limit (RL) (including non -detects), and the
absolute difference between the sample and the duplicate is < the RL (using the RL value for non -detects). Data
qualification is not required.
pg/L: micrograms per liter
ND: Not detected
NC: Not calculated

2021 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
AECOM Project number: 60683034
Appendix B
Completed Inspection Forms for Landfill
Cap and Phytoremediation System
AECOM

1`�C`1►11
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
1/29/2021
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet
X I Weather: rain
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
1/ 1 /2021
1 /8/2021
1 /15/2021
1 /22,29/2021
Reading
0.7
0.8
0.2
0,1.6
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed:
❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3
R8T3 R9T6 R13T8
Trunk Size (inches circ.) 37.5 N/A
19.25 14
Approx Tree Height 30'+ N/A
20'+ 20'+
Foliage Condition N/A N/A
N/A N/A
Other Observations: Leaves have fallen, R8T3 too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Photos Taken:
Yes
Yes
❑
No
No
Tree Growth Audit by Others:
Yes
Ej
No
X
PI/

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: none
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

1`�C`1►11
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
2/26/2021
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet X I
Weather:
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
2/5/2021
2/12/2021
2/19/2021
2/26/2021
Reading
0.8
1.3
2.7
0.9
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3
R9T6 R13T8
Trunk Size (inches circ.) 37.5 N/A
19.5 14.25
Approx Tree Height 30'+ N/A
20'+ 20'+
Foliage Condition N/A N/A
N/A N/A
Other Observations: Leaves have fallen, R8T3 too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired ❑
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Yes
No
Photos Taken: Yes F1 No
Tree Growth Audit by Others:
Yes
No
X
PI/

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
11-andfill Cap Observation: good condition
11-andfill Cap Maintenance Activities: none
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

1`�C`1►11
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE: 3/25/2022
CLIENT: CNA INSPECTED BY: L.Brooks
General Site Conditions
Site Conditions: Dry Wet X Weather: rain
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
3/4/2022
3/11 /2022
3/18/2022
3/25/2022
Reading
1.2
0.3
0.1
2.2
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive E Declining ED No Change
Area of Declining Health (if any): The poplars from last year that were showing declining foilage
have delaminating of bark and appear to have died.
Tree Status: Tree Identification: R2T3 R8T3 R9T6 R13T8
Trunk Size (inches circ.) 37.55 1 20.25 15.5
Approx Tree Height 30'+ 6.5 20'+ 20'+
Foliage Condition dormant budding budding budding
Other Observations: Willows are budding.
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired ❑
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Yes
No
Photos Taken: Yes F1 No
Tree Growth Audit by Others:
Yes
No
X
PI/

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
11-andfill Cap Observation: good condition
11-andfill Cap Maintenance Activities: none
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

AZCOM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE: 4/30/2021
CLIENT: CNA
INSPECTED BY: L.Brooks
General Site Conditions
Site Conditions: Dry
Wet X I Weather: rain
Water Flow From Culvert: Yes X
No
Rain Gauge Readings (unit in inches)
Date
4/2/2021
4/9/2021
4/16/2021
4/23,30/2021
Reading
0.9
0
0.4
0,1.1
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive E Declining 0 No Change
Area of Declining Health (if any):
the 5 poplars with delaminating bark appear dead
all willows are healthy
Tree Status: Tree Identification:
R2T3 R8T3 R9T6 R13T8
Trunk Size (inches circ.)
37.5 N/A 19.5 14.25
Approx Tree Height 30'+
N/A 20'+ 20'+
Foliage Condition N/A
N/A N/A N/A
Other Observations: Leaves budding, R8T3
too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree:
Yes
X
No
17/17/17
P
Site Irrigation:
Yes
No
F—xl
Apply Herbicide:
Yes
No
Generic Round up
Tree Prune:
Yes
No
El
Fence Condition:
Intact
X�
Damaged
Repaired ❑
Evidence of Grazing:
Yes
No
Photos Taken: Yes No
Tree Growth Audit by Others:
Yes
El
No
X
PI/

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
11-andfill Cap Observation: good condition
11-andfill Cap Maintenance Activities: none
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

1`�C`1►11
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
5/28/2021
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry X Wet
Weather:
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
5/7/2021
5/14/2021
5/21 /2021
5/28/2021
Reading
0
0
0
0
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: N Improving/Positive ❑ Declining 0 No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3
R9T6 R13T8
Trunk Size (inches circ.) 37.5 1
19.75 14.5
Approx Tree Height 30'+ 5'
20'+ 20'+
Foliage Condition good good
good good
Other Observations: full foilage
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
X
No
X
Fertilize the Tree: Yes No
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No
X
Tree Prune:
Yes
No
X
Fence Condition:
Intact
X�
Damaged
Repaired ❑
Evidence of Grazing:
Yes
No
Photos Taken: Yes F1 No
x
Tree Growth Audit by Others:
Yes
El
No
X
PI/

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
11-andfill Cap Observation: good condition
11-andfill Cap Maintenance Activities: Mowing
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

1`�C`1►11
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
6/25/2021
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry X Wet
Weather:
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
6/4/2021
6/11 /2021
6/18/2021
6/25/2021
Reading
0
0
0
0
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: N Improving/Positive ❑ Declining 0 No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3
R9T6 R13T8
Trunk Size (inches circ.) 37.5 1
19.75 15
Approx Tree Height 30'+ 6'
20'+ 20'+
Foliage Condition good good
good good
Other Observations: full foilage
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
X
Fertilize the Tree: Yes No
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No
X
X
Tree Prune: Yes No
Fence Condition:
Intact
X�
Damaged
Repaired ❑
Evidence of Grazing:
Yes
No
Photos Taken: Yes F1 No
x
Tree Growth Audit by Others:
Yes
No
X
PI/

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
11-andfill Cap Observation: good condition
11-andfill Cap Maintenance Activities: none
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

1`�C`1►11
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
7/30/2021
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry
Wet X I Weather:
Water Flow From Culvert: Yes X
No
Rain Gauge Readings (unit in inches)
Date
7/2/2021
7/9/2021
7/16/2021
7/23,30/2021
Reading
0.8
0.7
2.3
1.9,0.4
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive E Declining ED No Change
Area of Declining Health (if any):
Leaf canopy diminishing on all of the original planted poplars
Willows continue to do well
Tree Status: Tree Identification:
R2T3 R8T3 R9T6 R13T8
Trunk Size (inches circ.)
37.5 1 19.75 15
Approx Tree Height
30'+ 6' 20'+ 20'+
Foliage Condition
good good good good
Other Observations: full foilage
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired ❑
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Yes
No
Photos Taken: Yes F1 No
Tree Growth Audit by Others:
Yes
No
X
PI/

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
11-andfill Cap Observation: good condition
11-andfill Cap Maintenance Activities: mowing
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

1`�C`1►11
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE: 8/27/2021
CLIENT: CNA
INSPECTED BY: L.Brooks
General Site Conditions
Site Conditions: Dry
X Wet Weather:
Water Flow From Culvert: Yes X
No
Rain Gauge Readings (unit in inches)
Date
8/6/2021
8/13/2021
8/20/2021
8/27/2021
Reading
1.2
1.3
1.4
0
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive 0 Declining ED No Change
Area of Declining Health (if any):
the original planted poplars continue to decline
Tree Status: Tree Identification:
R2T3 R8T3 R9T6 R13T8
Trunk Size (inches circ.)
37.5 1 20 15
Approx Tree Height
30'+ 6.5 20'+ 20'+
Foliage Condition
declining good good good
Other Observations:
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired ❑
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Yes
No
Photos Taken: Yes F1 No
Tree Growth Audit by Others:
Yes
No
X
PI/

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
11-andfill Cap Observation: good condition
11-andfill Cap Maintenance Activities: none
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

1`�C`1►11
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
9/24/2021
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet
X Weather: rain
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
9/3/2021
9/10/2021
9/17/2021
9/24/2021
Reading
1.1
0.1
0
3.2
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed:
❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3 R9T6 R13T8
Trunk Size (inches circ.) 37.5
1 20 15
Approx Tree Height 30'+
6.5 20'+ 20'+
Foliage Condition no change good
good good
Other Observations: full foilage
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired ❑
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Yes
No
Photos Taken: Yes F1 No
Tree Growth Audit by Others:
Yes
No
X
PI/

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
11-andfill Cap Observation: good condition
11-andfill Cap Maintenance Activities: mowing
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

AZCOM PAGE 1 of 2
IROJECT:
Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER:
AECOM - 60135443
.00ATION:
Salisbury, NC
DATE:
1 10/29/2021
:LIENT:
CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet L XI Weather: rain I
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date 10/1 /2021 10/8/2021 10/15/2021 10/22,29/2021
Reading 0 2 0 0,1.8
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Status:
Tree Identification:
R2T3
R8T3
R9T6
R13T8
Trunk Size (inches circ.)
37.5
1
20
15
Approx Tree Height
30'+
6.5
20'+
20'+
Foliage Condition
fallen
good
good
good
Other Observations: Leaves falling. Large tree fell onto fence and damaged it in multiple
(attach additional
pages if needed) Tree also damaged multiple new willows.
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree:
Yes
No
X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
F x] Repaired ❑
Fence Condition: Intact Damaged
Evidence of Grazing:
Yes
No
Photos Taken: Yes F1 No
Tree Growth Audit by Others:
Yes
No
X
I-ejoll

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
11-andfill Cap Observation: good condition
11-andfill Cap Maintenance Activities: none
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

1`�C`1►11
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
11/26/2021
CLIENT: CNA INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet X I Weather: cloudy
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
11 /5/2021
11 / 12/2021
11 /19/2021
11 /26/2021
Reading
0
0.3
0
0.1
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3 R9T6 R13T8
Trunk Size (inches circ.) 37.5 1 20.25 15.5
Approx Tree Height 30'+ 6.5 20'+ 20'+
Foliage Condition fallen good good good
Other Observations: Leaves falling. Fallen tree from last month removed.
(attach additional
pages if needed) Evidence of deer rubbing willows. Fence repair scheduled.
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired ❑
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Yes
No
Photos Taken: Yes F1 No
Tree Growth Audit by Others:
Yes
No
X
PI/

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
11-andfill Cap Observation: good condition
11-andfill Cap Maintenance Activities: mowing
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

1`�C`1►11
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
12/31/2021
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet X I
Weather: rain
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
12/3/2021
12/ 10/2021
12/17/2021
12/24, 31 /2021
Reading
0
1
1.2
0'.9
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3
R9T6 R13T8
Trunk Size (inches circ.) 37.55 1
20.25 15.5
Approx Tree Height 30'+ 6.5 20'+ 20'+
Foliage Condition dormant dormant
dormant dormant
Other Observations: Trees are dormant. Fence repair complete.
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired ❑
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Yes
No
Photos Taken: Yes F1 No
Tree Growth Audit by Others:
Yes
No
X
PI/

1`�C`1►11
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
11-andfill Cap Observation: good condition
11-andfill Cap Maintenance Activities: none
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

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