The URL can be used to link to this page

Home My WebLink About7407_Pitt_C&DLandfillInc_CDLF_Phase1_Phase2_June2021GW_FID1676959_20220518DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 DENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Smith Gardner, Inc. Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Seth C. Rickerts, P.G. E-mail: Seth@smithgardnerinc.com Phone: 919-828-0577 x 135 NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) C&D Disposal, Inc. 802 Recycling Lane. Greenville, NC 74-07 .0500 June 8-9 & 23-24, 2021 27834 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells ❑ Groundwater monitoring data from private water supply wells ❑ Leachate monitoring data El water monitoring data Methane gas monitoring data Corrective action data (specify) Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Seth C. Rickerts, P.G. Project Geologist 919-828-0577 x 135 gfiga% tative Name (Print) Title 5/18/2022 (Area Code) Telephone Number ,r_ QZV'A5 Affix NC Licensed/ Professional Geologist Seal Date 14 N. Boylan Ave. Raleigh, NC 27603 Facility Representative Address F-1370 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 June2021 Groundwater Monitoring Report COD Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-20016 7407- CDLF- 2009 Prepared for: CGD Disposal, Inc. 802 Recycling Lane Greenville, North Carolina 27834 May 2022 Prepared by: NCLIC.NO.F-1370 (ENGINEERING) SMITH+GARONER 14 N. Boylan Avenue, Raleigh NC 2?GO3 1919.828.057? PRINTED ON M. RECYCLED PAPER © 2022 Smith Gardner, Inc. This document is intended for the sole use of the client for which it was prepared and for the purpose agreed on by the client and Smith Gardner, Inc. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 June2021 Groundwater Monitoring Report COD Disposal, Inc. NC Solid Waste Permit 7407-CDLF-2001 O 7407- CDLF- 2009 Prepared For: COD Disposal, Inc. Greenville, North Carolina S+G Project No. EJERECYCLING-21-2 DocuSigned by: d�, G- ItZ >", E 3B8305C978EA4E6... Seth C. Rickerts, P.G. Project Geologist N CA p DocuSigned by: �Oc�lln Q. Swiq{%, O�� ENSlr� c y B9779EBA711F488... aS SEAL 5/1 / 22 Joan A, Smyth, P.G. 1369 Senior Hydrogeologist "p�0 Loy �� , May 2022 NCLIC.NO.F1370 (ENGINEERING) SMITH+GARONER 14 N. Boylan Avenue, Raleigh NC 2?683 1 919.828.0577 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 CRD Disposal, Inc. NC Solid Waste Permit No. 7407- CDLF- 2001 R 7407- CDLF- 2009 June2021 Groundwater Monitoring Report Table of Contents Page 1.0 INTRODUCTION...............................................................................................................1 2.0 SITE GEOLOGY.................................................................................................................1 3.0 SAMPLING LOCATIONS...................................................................................................1 4.0 SAMPLING PROCEDURES...............................................................................................2 5.0 FIELD & LABORATORY RESULTS....................................................................................2 5.1 Field Results........................................................................................................... 2 5.2 Laboratory Analysis................................................................................................ 2 5.3 Laboratory Results................................................................................................. 3 5.3.1 Inorganic Constituents................................................................................ 3 5.3.2 Organic Constituents.................................................................................. 3 5.3.3 Surface Water Results................................................................................ 4 6.0 GROUNDWATER CHARACTERIZATION ............................................................................4 7.0 CONCLUSIONS................................................................................................................4 FIGURE Figure 1 Groundwater Potentiometric Map TABLES Table 1 Groundwater Elevation Table 2 Field Parameters Table 3 Monitoring Results Table 4 Velocity and Conductivity Data APPENDICES Appendix A Well Logs Appendix B Laboratory Analytical Report Appendix C Time Vs. Concentration Graphs CSD Disposal, Inc. June 2021 Groundwater Monitoring Report May 2022 Table of Contents Page i DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 1.0 INTRODUCTION C&D Disposal, Inc., located at 802 Recycling Lane, Greenville, North Carolina, operates a C&D Landfill under Solid Waste Permit #7407- CDLF- 2001 and #7407- CDLF- 2009. The site is currently required to submit semi-annual groundwater monitoring reports to NCDEQ. The facility contains two unlined construction & demolition (C&D) landfill units. Phase 2 is currently active. Phase 1 has ceased accepting waste and is partially closed, with final closure planned for 2022. The Facility was developed in two non-contiguous footprints, Phases 1 and 2 approximately midway between US 264, i.e., a localized topographic divide, and Grindle Creek. The phases became operational in May 2001 and August 2009, respectively. Phase 1 was the regional repository for flood -damage debris after Hurricane Floyd in 1999. Phase 2 was a staging area, where flood -debris was stored temporarily. Both areas were used for agriculture, and a former railroad corridor traverses the site, including the Phase 2 footprint. This report presents the results from the semi-annual monitoring event conducted June 8-9 & 23-24, 2021 and includes a field procedure summary, laboratory analyses, summary tables and groundwater characterization. 2.0 SITE GEOLOGY Historical literature and available geologic maps indicate that C&D Landfill, Inc. sits within the NC Coastal Plain. The coastal plain is characterized as an eastward thickening wedge of sedimentary layers that alternate between sandy aquifers an aquitards. Information taken from The Geologic Map of North Carolina, 1985 shows that the C&D landfill is underlain by the Yorktown Formation, which is described as "fossillifferous clay with varying amounts of fine-grained sand, silty sand, sandy silt, silty clay, and blueish gray shell material". Groundwater in the upper -most aquifer generally flows through unconsolidated sediments. Recharge occurs generally in the northern portion of the site and is limited on slopes. Groundwater flows generally south where it discharges into tributaries of Grindle Creek. The groundwater potentiometric surface generally reflects a subdued expression of the surface topography. Local conditions are considered typical for the coastal plain region. Ground water depths generally range from 3 ft to 12 ft below ground surface (bgs) across the facility. There are minor seasonal variations in the flow pattern, but overall flow direction is consistent. 3.0 SAMPLING LOCATIONS The groundwater monitoring network consists of eighteen shallow and four deep wells totaling (22) groundwater monitoring wells. MW-IS (upgradient of phase I); MW-1D, MW-2D, MW-2S, MW-3D, MW-3S and MW-3A, MW-4, MW-5, MW-6, MW-7, and MW-8 (downgradient of phase 1); MW-9A, MW-16, and MW-17 (upgradient of phase 111; MW-10, MW-11, MW-12S, MW-13, MW-14D, MW-14S, and MW-15 (downgradient of phase II); the network also includes four surface water locations (SW-1, SW-2, SW-3, and SW-4). CSD Disposal, Inc. June 2021 Groundwater Monitoring Report May 2022 Pagel DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 Figure 1 illustrates sampling locations. Available well logs for the groundwater monitoring wells are included in Appendix A. 4.0 SAMPLING PROCEDURES Environment 1 personnel conducted the monitoring network sampling event June 9-10 & 23-24, 2021. Sampling methods followed the protocol outlined in the North Carolina Water Quality Monitoring Guidance Document for Solid Waste Facilities (DENR, DWM) and the approved site Water Quality Monitoring Plan'. The monitoring network includes wells: MW-1s, MW-1 d, MW-2s, MW-2d, MW-3A, MW-3s, MW-3d, MW-4, MW-5, MW-6, MW-7, MW-8m NW09a, MW-10, MW-11, MW-12s, MW-13, MW-14s, MW-14d, MW-15, MW-16 and MW-17, as well as surface water monitoring points SW-1 through SW-4. Monitoring wells MW-1s and MW-1d serve as the upgradient background locations for the site. Each well was gauged to determine groundwater depth and then purged three well volumes or until dry. Groundwater depth from this event, as well as other well details are presented in Table 1. Samples were collected by Environment 1, Inc. in laboratory prepared containers for the specified analytical procedures. Groundwater samples and quality control blanks, were properly preserved, placed on ice and transported to the laboratory facility within the specified hold times for each analysis. 5.0 FIELD B LABORATORY RESULTS 5.1 Field Results Temperature, pH, turbidity, specific conductance, ORP, and dissolved oxygen were measured in the field at the time of sampling via direct read instruments. Field results from this sampling event are presented in Table 2. All wells exhibited turbidities less than 10 NTUs except MW-3A which had 18 NTUs. 5.2 Laboratory Analysis Ground and surface water samples were transported to Environment 1, Inc., a North Carolina certified laboratory for metals and Appendix II VOC analysis. Samples were also analyzed for additional C&D inorganics, alkalinity, sulfide, chloride, total dissolved solids and tetrahydrofuran. The laboratory report including the full list of analytes tested for is presented as Appendix B. 1 Water Quality Monitoring Plan Amendment, C&D Landfill, Inc., CDLF (Phases 1 and 2) prepared for C&D Landfill, Inc., by David Garrett and Associates, Revised May 2008. CSD Disposal, Inc. June 2021 Groundwater Monitoring Report May 2022 Page 2 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 5.3 Laboratory Results Analytical results were compared to Rule 15A NCAC 2L.0200 (21- Standard) and/or the NC Groundwater Interim Maximum Allowable Concentration. Surface water results were compared with the NCAC 2B Standard for Class C waters (213 Standards). Most constituent concentrations were either below the method detection limit (MDL) or were reported as "J-values". J-values are identified by the laboratory as "estimated values between the MDL and the MRL". 5.3.1 Inorganic Constituents Five inorganic constituents were reported at concentrations above their 2L Standard this event. Antimony (MW-15); • Arsenic (MW-3S, MW-12S, MW-15, and MW-16); • Chromium (MW-3S, MW-8, MW-10, MW-12S, MW-15, and MW-16) • Copper (MW-3A, MW-3S, MW-6, MW-7, MW-8, MW-10, and MW-12S); • Iron (MW-1D, MW-1S, MW-2D, MW-2S, MW-3A, MW-3S, MW-4, MW-5, MW- 7, MW-8, MW-9A, MW-10, MW-11, MW-12S, MW-13, MW-14S, MW-15, MW- 16, and MW-17); and • Manganese (MW-1 D, MW-3A, MW-3S, MW-4, MW-5, MW-6, MW-7, MW-8, MW-9A, MW-10, MW-11, MW-12S, MW-14S, MW-15, MW-16, and MW-171. Three inorganic constituents were reported at concentrations above their GWP standard this event. • Cobalt (MW-3A, MW-3S, MW-6, MW-7, MW-8, MW-10, and MW-12S); and • Thallium (MW-2D, MW-3A, MW-9A, MW-10, and MW-15); and • Vanadium (MW-1D, MW-1S, MW-2D, MW-2S, MW-3A, MW-3S, MW-4, MW- 5, MW-6, MW-7, MW-8, MW-9A, MW-10, MW-11, MW-12S, MW-13, MW- 14S, MW-15, MW-16, and MW-17). As MW-1S and MW-1D are upgradient of Phase 1 and MW-17 is upgradient of Phase 2, exceedances in these wells indicate that detected constituents may be due to naturally occurring conditions. Detections are summarized in Table 3. 5.3.2 OrOanic Constituents Three organic constituents were detected above their 2L Standards during this sampling event. Detections are summarized in Table 3. CSD Disposal, Inc. June 2021 Groundwater Monitoring Report May 2022 Page 3 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 • 1,4-Dioxane (MW-IS, MW-2S, MW-3A, MW-3S, MW-5, MW-6, MW-7, MW- 8, MW-10, MW-11, MW-12S, MW-14S, MW-15S, and MW-16); • Benzene (MW-10, MW-12S, and MW-14S); and • Vinyl Chloride (MW-10 and MW-14S). 5.3.3 Surface Water Results No inorganic or organic constituents were detected above their NC213 standards in surface water samples collected this event. Surface water detections are provided on Table 3. 6.0 GROUNDWATER CHARACTERIZATION A potentiometric surface map was prepared from groundwater data from the most recent sampling event. The data indicates that groundwater is flowing generally south towards tributaries of Grindle Creek. This is consistent with groundwater flow patterns previously reported for the site. The potentiometric surface map is included as Figure 1. Groundwater flow velocities during the sampling event were calculated using the equation: V = Ki/n where: K = hydraulic conductivity i = groundwater gradient n = porosity Calculated groundwater velocities ranged from 0.00068 ft/day (MW-11) to 0.14591 ft/day (MW- 3A) averaging 0.06166 ft/day. Flow velocities and calculated gradients are included in Table 4. 7.0 CONCLUSIONS Analytical results are generally consistent with past sampling events. Iron, manganese, and vanadium were detected in most samples collected this event, including in background wells above their respective NC21- and NCGWP standards. Due to the low turbidity values, and the exceedances noted in upgradient wells, it is likely that some of these inorganic exceedances can be attributed to naturally occurring metals in the soil. 1,4-Dioxane, benzene, and vinyl chloride were detected in multiple monitoring wells above their NC21- standards this sampling event. Although not exceeding regulatory limits, once again 1,2- Dichloroethane and 1,2-cis-Dichloroethylene were present in multiple wells this event. The continued presence of these organochlorides as well as vinyl chloride provide some evidence that reductive dichlorination and natural attenuation may be occurring onsite. A corrective action plan is currently being drafted to further address these exceedances and will be submitted under a separate cover. CSD Disposal, Inc. June 2021 Groundwater Monitoring Report May 2022 Page 4 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 The next groundwater monitoring event is scheduled for Fall 2021. A report with laboratory analysis will be submitted to NCDEQ in accordance with 15A NCAC 13B .0544. CSD Disposal, Inc. June 2021 Groundwater Monitoring Report May 2022 Page 5 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 FIGURES June 2021 Groundwater Monitoring Report CEO Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 6 7407- CDLF- 2009 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 \ r i r_ y �. MW-17 �A TOC= 20.74 + s'� DTW= 6.57 '` • GWE= 14.17� ti 4� MW-16 TOC= 19.16 DTW= 6.6 SW-4 GWE= 12.56 l r RTWL L L © 2022 Smith Gardn , Inc. U'ir�rr�� fir;; MW-15AM TOC= 19.67 11tD= 5.4 = 14.27 ' MW-14SL� TOC= 16.60 DTW= 3.69 GWE= 12.91 ' r MW-13 TOC= 20.69 DTW= 8.2 GWE= 12.49 \1100olk/ MW-14D*M TOC= 17.45 DTW= 5.1 GWE= 12.35 ••t ►: A'% -V MW-9A � . TOC= 20.58 DTW= 5.12 GWE= 15.46 MW-12S TOC= 16.18 DTW= 4.03 GWE= 12.15 LEGEND NOTES EXISTING 10' CONTOUR 1. GROUNDWATER DATA COLLECTED BY ENVIRONMENT 1, INC. 950JUNE, 2021. (SEE REFERENCE 2) EXIS77NG 2' CONTOUR ' r (SEE REFERENCE 2) REFERENCES APPROXIMATE PROPERTY LINE 1. PARCEL BOUNDARIES FROM PITT COUNTY GIS DEPARTMENT. (SEE REFERENCE 1) 2. FLOOD HAZARD INFORMATION FROM NORTH CAROLINA FLOODPLAIN MAPPING PROGRAM, FEMA FIRM MAP NO. 3720562800L, EFFECTIVE .r FLOOD HAZARD AREAS ZONE AE DATE JUNE 19, 2020. ® (SEE REFERENCE 3) 3. AERIAL IMAGERY DATED 2016 FROM PITT COUNTY GIS DEPARTMENT APPROXIMATE GROUNDWATER SURFACE CONTOUR o 200' 400' . sW-1 SURFACEWATER MONITORING LOCATION INDICATES ELEVA77ON NOT {`, a M W-8* USED FOR CONTOURING ` r M W-1 A GROUNDWATER MONITORING WELL TOC TOP OF CASING ELEVATION • DTW DEPTH TO WATER i OWE GROUNDWATER ELEVAIION MW-1S 1� MW-10 . TOC= 20.91 TOC= 16.61 MW-1 D* DTW= 6.23 DTW= 2.54 TOC= 21.14 MW-4` GWE= 14.07" DTW= 8.16 '� GWE= 14.68 TOC= 18.42� 1 GWE= 12.98 r DTW= 6.45 4j GWE= 11.97. 1 MW-11 TOC= 14.49 DTW= 2.5 / GWE= 11.99� MW-8* TOC= 21.21 / DTW= 8.18 / GWE= 13.03 All / MW-3S TOC= 23.02 DTW= 10.51 •.L GWE= 12.51''' MW-311)* • ' "'�.� TOC=17.90 TOC= 22.83 MW-3A DTW= 4.82 MW-2D* � \ DTW= 12.12 TOC= 11..93 GWE= 13.08 TOC= 21.80 MW-2S TOC= 21.44 GWE= 10.71 DTW= 11.91 DTW= 9.3 \ GWE= 11.93 GWE= 9.89 \ GWE= 12.14 r \ MW-7 1 t TOC= 19.40 1 DTW= 7.3 GWE= 12.10 r .. MW-6 TOC= 20.03 DTW= 8.34 . ..- GWE= 11.69 �1 �4;P1w z w 1 MLj 0 0 J� z� Q o U o Z U o, T. e - c U m z CD m w w z Z w w J O Ln a o o W z W N N O � N T lD ►22 0- a - Z L7 W - z o Fu O L V W N z z_ z a J W o = Lw cja c� " 0 z o c L7 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This Page Intentionally Left Blank DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 TABLES June 2021 Groundwater Monitoring Report CEO Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 6 7407- CDLF- 2009 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 SMITH GARDNER Well Well Installation Date Well Diameter (inches) Total Well Depth (ft bgs) Ground Surface Elevation (ft amsl TOC Elevation (ft amsl) Depth toElevation Water (ft) Water Table (ft bgs) Screen Interval (feet bgs) M W-1 D 10/ 13/ 2000 2 33.75 17.4 1 21.14 8.16 12.98 40- 50 MW-1 S 5/2/2001 2 17.21 17.59 20.91 6.23 14.68 3-13 MW-2D 10/11/2000 2 38.17 17.97 21.8 11.91 9.89 39-49 MW-2S 5/3/2001 2 16.57 18.45 21.44 9.3 12.14 3-13 M W- 3A 8/ 10/ 2009 2 23.44 19.13 21.93 10 11.93 5- 20 MW-3D 10/13/2000 2 52.3 19.37 22.83 12.12 10.71 40-50 MW-3S 8/6/2007 2 22.24 19.37 23.02 10.51 12.51 8-18 MW-4 5/3/2001 2 15.98 14.83 18.42 6.45 11.97 3-13 M W- 5 11 / 19/ 2002 2 9.5 14.8 17.9 4.82 13.08 3-18 M W- 6 5/3/2001 2 16.65 16.87 20.03 8.34 11.69 3-13 M W- 7 5/3/2001 2 16.33 16.03 19.4 7.3 12.10 3-13 MW-8 11/5/2002 2 20.26 18.3 21.21 8.18 13.03 3-18 M W- 9A 8/ 7/ 2009 2 23.17 17.64 20.58 5.12 15.46 5- 20 M W-10 8/ 6/ 2009 2 22.73 14.16 16.61 2.54 14.07 5- 20 MW-11 8/6/2009 2 23.84 11.60 14.49 2.5 11.99 5-20 MW-12S 8/7/2009 2 22.93 1 13.72 16.18 4.03 12.15 5-20 M W-13 8/ 7/ 2009 2 20.68 18.12 20.69 8.2 12.49 5- 20 MW-14D 12/17/2002 2 41.92 14.54 17.45 5.1 12.35 35-40 M W-14S 12/ 18/ 2002 2 23.12 13.9 16.6 3.69 12.91 5- 20 M W-15 12/ 18/ 2002 2 22.14 13.9 19.67 5.4 14.27 5- 20 MW-16 6/16/2017 2 22.73 NA 19.16 6.6 12.56 NA M W-17 12/ 9/ 2002 2 22.25 18.18 20.74 6.57 14.17 5- 20 Note: 1. Well installation, depth, elevations, and screened interval from David Garrett Boring Logs M Rgeds\ GarrindaNtntoir# 23irrl&#aNt ntairUFperts\ EERydirrr, 3 SnTrE-2021 Srrrre-2321 EEbc,ydirgTaHe&dsx DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 SMITH GARDNER Ffdd Pawdas Well ID pH (SU) Temperature (OCelsius) Specific Conductivity (uMhos/cm) Dissolved Oxygen ORP (mv) Turbidity (NTU) M W-1 D 7.1 21 399 0.3 101 4.9 M W-1 S 6.5 21 493 0.6 57 3.9 MW-2D 7.5 22 451 0.5 101 7.3 MW-2S 6.3 22 410 1 99 5.9 M W- 3A 6.5 19 1155 0.7 136 18 MW-3D 7.8 21 528 4.8 111 <1 M W- 3S 6.7 22 3952 0.5 156 4 MW-4 6.2 20 526 0.7 101 9 MW-5 6.7 23 1017 0.8 103 5.4 MW-6 6.6 20 1380 2 92 2.7 M W- 7 6.5 21 748 0.7 105 7.8 MW-8 6.6 22 2265 1 146 6.1 M W- 9A 6.6 19 799 0.9 94 5.4 MW-10 6.4 20 2435 1.3 123 3.8 M W-11 6.7 21 1161 2.1 97 6.4 MW-12S 6.6 22 2423 0.7 129 2.7 MW-13 6.5 23 465 0.5 47 2.3 MW-14D 7.5 21 525 0.5 88 <1 MW-14S 6.6 22 1656 2.3 102 9.1 MW-15 6.2 20 1689 1.8 102 7.6 MW-16 6.2 23 1561 1.1 122 3.5 M W-17 5.6 21 214 0.4 56 6.1 SW-1 7 26 530 5.3 81 9.3 SW-2 NA NA NA NA NA NA SW-3 NA NA NA NA NA NA SW-4 6.6 26 162 8.2 56 10.2 Note: 1. Field Parameters measured by Environment 1 on 6/8-9, 23-24/2021. 3. Bold indicates a turbidity exceeding 10 NTU. M Rgeds\ GarrindaNtntc ir# 23irrl&#aNt ntairUFperts\ EERrydirrr, 3 Sxrrre-2021 Srrrre-2321 EERx,ydirgTaJe&k x DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 SMITH GARDNER Tade3 W tairgFesJts EffbcydingLa-dll Axe&9,2324,2021 Monitoring Results W.W Dte 05 6 m Station Name Units NC2L NCCWP NC28 NC2B-P MW-11D MW-1S MW-21D MW-2S MW-3A MW-3D MW-3S MW-4 MW-5 MW-6 MW-7 MW-8 MW-9A MW-10 MW-11 MW-12S Sample Date 6/8/2021 6/8/2021 6/8/2021 6/8/2021 6/8/2021 6/8/2021 6/8/2021 6/8/2021 6/9/2021 6/9/2021 6/9/2021 6/9/2021 6/23/2021 6/23/2021 6/23/2021 6/23/2021 Furans Tetrahydrofuran ug/I NE 2000 NE NE 4.13 5.77 24.8 1.48 2.82 3.5 10.9 19.5 23 5.32 13.7 Metals Antimony ug/I 1 1 NE 5300 0.09 J 0.49 J 0.12 J 0.09 J 0.21 J 0.09 J 0.35 J 0.09 J 0.34 J 0.21 J 0.14 J 0.24 J 0.24 J 0.14 J 0.111 0.54 J Arsenic ug/I 10 NE NE NE 1 J 1.3J 0.54J 0.71 J 8.8 0.22J 18.8 1.2J 1.7J 1.11 1.11 7.9 0.7J 5.2 6.7 17 Barium ug/I 700 NE NE NE 24.1 31.9 17.6 69.3 152 10.3 705 168 204 308 180 340 83.8 344 77 371 Beryllium ug/I 4 4 6.5 NE 0.02 J 0.04 J 0.05 J 0.02 J 0.09 J 0.02 J 0.08 J 0.05 J 0.04 J 0.02 J 0.04 J 0.04 J Cadmium ug/I 2 NE NE NE 0.08J 0.05J 0.16J 0.05J 0.06J Chromium ug/I 10 NE NE NE 0.29J 0.39J 0.52J 0.51 J 5.6 0.14J 28.5 2.1 J 3.2J 2J 3.2J 11.4 0.6J 15 1.6J 18 Cobalt ug/I 1 1 NE 4 0.06 J 0.08 J 0.11 0.28 J 2.5 5.7 0.26 J 1 1.8 1.6 3.6 0.16 J 1.4 0.8 J 1.5 Copper ug/I 1000 NE NE NE 0.79J 2.2J 0.42J 0.75J 0.551 0.2J 0.48J 0.14J 1.6J 1.51 1.2J 1.3J 0.48J 0.16J 0.11 0.26J Iron ug/11 300 NE NE NE 834 920 367 305 10145 8 J 18545 7317 1511 266 2111 8131 3144 1635 18403 7459 Lead ug/I 15 NE 25 NE 0.11 0.62J 0.191 0.28J 0.24J 0.28J 0.15J 0.16J 0.06J 0.16J 0.11 0.21 J 0.11 0.04J 0.11 Manganese ug/11 50 NE NE NE 91 5J 13 28 418 1 599 86 111 452 76 469 153 304 219 616 Mercury ug/I 1 NE NE NE 0.05 J 0.05 J 0.05 J 0.05 J 0.06 J Nickel ug/I 100 NE 88 NE 0.41 J 0.5J 0.36J 0.45J 1.2J 0.16J 2.2J 0.24J 1.4J 1.11 0.76J 1.6J 0.55J 1.4J 0.75J 2.3J Selenium ug/I 20 NE 5 NE 0.21 J 0.7J 0.18J 0.26J 0.39J 1.5J 0.62J 0.4J 0.44J 0.39J 1.11 0.12J 1.2J 0.58J 0.86J Silver ug/I 20 NE NE NE 0.24 J 0.22 J Thallium ug/I 2 0.2 0.47 NE 0.04 J 0.25 J 0.1 J 0.32 J 0.02 J 0.02 J 0.08 J 0.11 0.06 J 0.11 J 0.29 J 0.34 J 0.06 J 0.02 J Tin u g/ I 2000 2000 NE NE 0.14 J 0.05 J 0.111 0.09 J 0.49 J 0.11 Vanadium ug/I 7 0.3 NE NE 0.39J 1.9 0.39J 0.55J 2.3 8.8 2.2 1.1 1.1 1.1 1.4 1 8 0.991 11 Zinc ug/I 1000 NE 81 NE 4J 2.3J 10.6 3.4J 1.9J 1.2J 1.4J 3.4J 2.2J 1.2J 1.4J 1.8J 4.1 J 1.4J 1.2J 1.3J Nutrients Nitrite (as N) mg/I NE NE NE NE 0.11 0.47 0.76 0.33 7.18 2.35 31.6 0.23 Other 1,2-cis-Dichloroethylene ug/I 70 NE NE NE 1,2-Dichloroethane ug/I 0.4 NE NE NE 0.05 J 0.09 J 0.02 J 0.21 0.04 J 0.11 1,2-Dichloropropane ug/I 0.6 NE NE NE 0.04 J 0.15 J 0.06 J 1,4-Dioxane ug/I 3 NE NE NE 4.48 3.99 41.1 142 16.8 19.7 3.53 78 9.32 5.76 11.1 Acenaphthene ug/I 80 NE NE NE 6.92 J Acetone ug/I 6000 NE NE NE 9.72 J Alkalinity, Total (as CaCO3) mg/I NE NE NE NE 162 162 184 78 500 242 1620 200 312 665 275 808 192 950 340 740 Benzene ug/I 1 NE NE NE 0.83 J 2.12 0.34 J 1.13 Carbon Disulfide ug/I 700 NE NE NE Chloride mg/I 250 NE NE NE 14 15 12 18 49 21 206 15 37 23 19 106 21 60 19 100 Ethyl benzene ug/I 600 NE NE NE Methyl Ethyl Ketone (2-Butanone) ug/I 4000 NE NE NE Naphthalene ug/I 6 NE NE NE 2.02 J Sulfate mg/I 250 NE NE NE 24.8 87.7 29.8 53.8 56.6 38.4 65.7 165 69.4 39 176 198 348 302 585 Sulfide ug/I NE NE NE NE 221 J 169 J Toluene ug/I 600 NE NE NE Total Dissolved Solids mg/I I NE NE NE NE 2000 Vinyl chloride ug/I 1 0.03 NE NE NE I 1 0.55 NOTES: ug/L = micrograms per liter BOLD = Constituent exceeds NCACO2L or GWP regulatory limits BCLD = Constituent exceeds NCACO2B or 2B Protection regulatory limits J = Lab estimated concentration BDL = constituent is below laboratory detection limits NA = Not Analyzed MRged6l OwbAdErWitcnro20anJndaMritargF4ats1EEFa)dirj,33mrEr f,9rmaMEBbydirgTEiesAEx DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 SMITH GARDNER Tade3 W tairgPesdts EffbcydingLaldill Axe&9,2324,2021 Monitoring Results Station Name Units NC2L NCGWP NC2B NC2B-P MW-13 MW-14D MW-14S MW-15 MW-16 MW-17 SW-1 SW-4 Sample Date 6/23/2021 6/24/2021 6/24/2021 6/24/2021 6/24/2021 6/24/2021 6/9/2021 6/9/2021 Furans Tetrahydrofuran ug/I NE 2000 NE NE 12.9 6.82 2.8 3.62 Metals Antimony ug/I 1 1 NE 5300 0.2 J 0.19 J 1.6 0.25 J 0.11 0.2 J 0.08 J Arsenic ug/I 10 NE NE NE 3J 0.43J 2.3J 26 14 0.44J 2.3J 0.551 Barium ug/I 700 NE NE NE 36.8 10.5 267 507 357 38 123 103 Beryllium ug/I 4 4 6.5 NE 0.02J 0.12J 0.06J 0.06J 0.02J 0.14J Cadmium ug/I 2 NE NE NE 0.051 Chromium ug/I 10 NE NE NE 0.39 J 0.21 J 6.4 38 16 1.1 J 3.6 J 0.9 J Cobalt ug/I 1 1 NE 4 0.43 J 0.99 J 0.69 J 0.96 J 0.11 0.36 J 0.74 J Copper ug/I 1000 NE NE NE 0.43J 0.111 0.28J 1.91 0.18J 0.2J 0.82J 0.46J Iron u g/ I 300 NE NE NE 3330 58 16181 9476 57833 2670 Lead ug/I 15 NE 25 NE 0.511 0.051 0.24J 2.4J 0.2J 0.18J 0.34J 0.51 Manganese ug/ I 50 NE NE NE 21 4 J 1332 323 364 106 Mercury ug/I 1 NE NE NE Nickel ug/I 100 NE 88 NE 0.28J 0.151 0.76J 2.5J 1.3J 0.56J 0.68J 0.551 Selenium ug/I 20 NE 5 NE 0.44J 0.06J 0.61 J 1.3J 1.6J 0.191 0.151 0.191 Silver ug/I 20 NE NE NE Thallium ug/I 2 0.2 0.47 NE 0.04J 0.18J 0.22J 0.08J 0.04J 0.11 0.11 Tin ug/I 2000 2000 NE NE 0.16J 0.051 Vanadium ug/I 7 0.3 NE NE 5 0.14 J 2 10 11 2 1.4 1.4 Zinc ug/I 1000 NE 81 NE 2.3J 2.2J 1.7J 29 1.51 4.1 J 3.1 J 2.4J Nutrients Nitrite (as N) mg/I NE NE NE NE 0.3 0.1 0.04 Other 1,2-cis-Dichloroethylene ug/I 70 NE NE NE 0.54J 1,2-Dichloroethane ug/I 0.4 NE NE NE 0.08J 0.03J 0.191 1,2-Dichloropropane ug/I 0.6 NE NE NE 0.11 1,4-Dioxane ug/I 3 NE NE NE 5.33 5.18 54.4 Acenaphthene ug/I 80 NE NE NE Acetone ug/I 6000 NE NE NE 26.6J Alkalinity, Total (as CaCO3) mg/I NE NE NE NE 196 244 690 205 342 10 Benzene ug/I 1 NE NE NE 1.19 0.25J Carbon Disulfide ug/I 700 NE NE NE 0.27J Chloride mg/I 250 NE NE NE 5 16 34 86 82 Ethylbenzene ug/I 600 NE NE NE 0.28J Methyl Ethyl Ketone(2-Butanone) ug/I 4000 NE NE NE 2.73J Naphthalene ug/I 6 NE NE NE Sulfate mg/I 250 NE NE NE 16.4 188 542 314 76.1 Sulfide ug/I NE NE NE NE 661 J 184 J Toluene ug/I 600 NE NE NE 0.31 J Total Dissolved Solids mg/I NE NE NE NE MnA chloride ug/I 0.03 NE NE NE 1.19 NOTES: ug/L = micrograms per liter BOLD = Constituent exceeds N CACO2L or GNP regulatory limits BCLD = Constituent exceeds NCACO2B or 2B Protection regulatory limits J = Lab estimated concentration BDL =constituent is below laboratory detection limits NA= Not Analyzed EV.93 Dteo5 6'm MRged6l OwbAdErWitcnro20anJndaMritargF4ats1EEFac dirj,38rrrrErMSrmaMEt3R-.}dirgIldesAEx DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 SMITH GARDNER Hydraulic Hydraulic Velocity Effective Weil Conductivity Gradient v Porosity n (feet/day) i (feet/day) M W- 3A 0.805 0.08 0.015 0.14591 M W-10 0.116 0.05 0.004 0.00882 MW-11 0.009 0.04 0.003 0.00068 MW-12S 0.322 0.06 0.017 0.09123 Note: 1. Hydraulic conductivity and effective porosity values from historical Wood Inc. groundwater monitoring reports 2. Velocity calculated based on the modified Darcyequation: v=(KI)/n W.3j ate 05' 15 MRgedslOaxr%M1EtErItch#2GanJAdErMntcrirgRpotslEEFt,ydir#a mre'2C 3mra'2 L1EB.ydirgTdies*x DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 AppendixA Well Logs June 2021 Groundwater Monitoring Report CEO Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 6 7407- CDLF- 2009 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P. G., P.E. Boring No. AlfW-I d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 17.40 �t Equipment CME 750 Drilling Method 3-114" Hollow AugeisNater Level, TOB NA sz Date Started iom2100 Date Ended 10/13/00 Water Level, 24 Hr. 4.8 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.8 Comments Plowed field. cool sunny weather Total Depth mo Date of Observation 1omwoo Elegy. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Medium dense buff -white, slightly silty, I I I I I I I I I I I I I I I moist 16,00 I I I I I I I I I I I I - - 14.00 I I I I I I I I 1 I I l I I I - - - 3.5 3 i i I i I i S i I 4.0 SAND: Loose, green -gray, silty and clayey, wet 4 SM 5 I I I I I I I I I I -- - 12.00 t I I I I I I I I i S t I I I I I I I I I 7.5 - - 10.00 ' I I ' ' ' —Y SILT: Medium stiff, gray -green, fine sandy and clayey, with heavy shell hash (turritellas) wet, 8.5 2 i i i i ; —_ medium plasticity 1 SM 8.00 i i i i i — 1 I I— I I I I I i I I I I — 6.00 4WV I I I I I I I I I I I S ! S 5 t I I I I I I I I I I — - — 4.00 1 I I I I I I I I t I I I 1 1 I I I I I I — 13.5 3 I I I I — 4 s I I I I — M L- 1 I I 1 I C L 2,00 1 I I I I — — 0.00 3 I S I I I I 1 I 1 I I I I I I I I I I I I I I I — — — — I I I I 1 I I I I I I 18.5 — 18,5 4 ♦ CLAY: Medium stiff, gray -green, plastic gumbo -2.00 4 clay, moist CL 6 I I I I 1 I I I I I I I I I I I I I I I 4 00 I I I I I I I 1 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I M I I I I I I I 1 I I I I I I I I I I 1 I 23.5 4 I I I 5 I I ' I I ' I CL 7 I I I I I I I I DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P. G., P.E. Boring No. A4W--1 d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 2 Client and Project CSD Landfill, Inc. (Pitt County) Ground Elevation 17.40 Equipment CME 750 Drilling Method 3-114" Hollow AugelhlVater Level, TOB NA Date Started 10/12/00 Date Ended 10/13/00 Water Level, 24 Hr. 4.8 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.8 r.nmmPntG Pinwed field- cool sunnv weather Total DeDth sox Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction -8.00 i i ; i CLAY: Medium stiff, gray -green, plastic gumbo 'ANNULUS GROUTED i f S I I I I I I I 1 I I I I I day, moist -10.00 I I I I I I 1 1 I I I I I I I I I I I I I I I I I I 28.5 3CL I I I I I I I I I I 1 3 -12.00 I I I I 1 I I I I I I I 1 I I I I I I I I 1 I I I 31.5 -14.00 SILTYSAND: Dense, partly cemented, black- - ' ' green speckled, variably clayey, silty, moist, hard — ' layer at 36 to 38 feet, very hard below 45 feet -16.00 I 1 I I I I s -7. -• 33.5 6 22 I I I I ! — SM Bentonite 18 I I I r I I Seal -18.00 I I I 7 I I I I I I I ! t S I I I I I 1 1 I I I I I - - -20.00 3 I 1 f t I I I I I I I I I I I I I I I 1 I I I I I I I I I I I - - 38.5 31 I I I 1 I I I 15 I - SM -22.00 I - 24 I I I I I I I I I I I I I I I 1 I - -24.007. I I I I I I I I I I 1 I - I I I I I I I I 1 1 I l I I I I - Sand Pack I - SM -26.00 1 43.5 501.1— I I ! I I I - I I 1 I I 1 I I I I I 1 I I I 77 0.010" 28.00 i i i i i Slotted I I I 7 I I I I I I Screen -30.00 .JII W I I I i ! I I I I I I I I I I t 48.5 501.5 I I I I I I I I I S 7. SM -32.00 — ' I I I ' I t Boring Terminated at 50 feet DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P. G., P.E. Boring No. MW-1 s Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of i Client and Project C8D Landfill, Inc. (Pitt County) Ground Elevation 17.59 Equipment CME 75 Drilling Method 4.11NO ID HSA Water Level, TOB NA sz Date Started 05102/01 Date Ended 05/02/01 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 5.59 s Comments Lockino cover with 3.32' stickup Total Depth 13.0 Date of Observation 5/116/01 Elev. SPT Data and Strata Depths. Lithology Description and USCS Code Piez. Construction 1 I I I ! SILTY SAND: Loose, tan -brown, moist [ I I , - Concrete I i I I I pad 16.00 I t I I I • I I I I I SM Bentonite I I I I 1 - Seal 14.00 I I I I I I I I I I I I I I f I I I I I ] i I 1 I - - 12.00— I I I I I I I l } ! I I I I I I I • = - I I I I I I I 3 ! S I I I I I I - - 10.00 I I I I 1 I 8.0 - 0.010" . • . SAND: Loose, tan, fine to medium Slotted 1 Screen I I ! ! $W g.00 ! I 3 I I I I 1 I ! I ! - 6.00 3 5 ! I I I I 1 1 I 1 I I I I I I I I I I I I I I 1 I I I 1 I I I I I I I Boring Terminated at 13 feet DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 3 Client and Project C&D Landfill, inc. (Pitt County) Ground Elevation 17.97 Equipment CME 750 Drilling Method 3-718" rotary -mud Water Level, TOB 6.6 a Date Started 1019100 Date Ended 10111100 Water Level, 24 Hr. 7.9 Drilling Firm Bore & core Logged by David Garrett Stabilized Level 7.9 Comments Plowed field. cool sunnv weather Total Degth 70.o Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction F I I I I . ' . • - SAND: Loose, tan -yellow, variably silty sand 16.00 { I I I I I I 1 1 I I I I I I I I I I I I I I I I - I I I I I I I I I I 1 3.5 14.00 3.5 16 ' ' CLAY: Medium stiff, tan range, very sandy, silty, e ; slightly plastic, moist, crumbly CL 8 I i I I i I I i 1 I i I I i I I SM 12.00 I I I l I I I ' I I I I I I I 1 1 I I I I I I I i I 75 i D.00 ' SAND: Medium dense, tan, subangular, f - c well ; graded (boring collapsed at 13.6 feet when casing Bentonite- 8.5 5 i pulled, redrilled with 41l4" hollow stem auger) Cement 6 I f I I I � $p- Grout 8 SM 8.00 I I 1 ! I I I I I I - 6.00 I I I I I I 1 I I I I I I I I I I I I I I I S F E 12.5 - �- -, CLAYEY SILT: Medium stiff, gray -green, fine — sandy, with heavy shell hash (whole turritellas), 13.5 3 — moist, moderately plastic 4 00 3 � I I r I I �— CL- 4 I I I I I ML I I I I 1 t I I I I \— I I I I { I I I I I \- 2.00 I I 1 I \ I I ! I I \ — I I I I I 0.00 i I r I I I I I I 1 1 t I I I \— I I I 1 I 16.5 2 a I I 1 I 2 , I i I i I i I i \— iiL- ML -2.00 3 , I I I I I \— I I 1 I I I I I I I \— I I 1 1 I I I I I I �— I I 1 I I I I I I I \ µ -4.00 I 1 I I I 22.5 CLAY: Medium stiff, gray -green, plastic gumbo I I I I I I I I I I clay, moist 23.5 2 -6.00 2 ' I ' I I I I CL 4 I I I I I DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 3 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 17.97 n Equipment CME 750 Drilling Method 3-7/8" rotarrmud Water Level, TOB 6.6 a Date Started 1o/woo Date Ended 10/11/00 Water Level, 24 Hr. 7.9 Drilling Firm Bore & core Logged by David Garrett Stabilized Level 7.9 Comments Plowed field. cool sunnv weather Total Depth 70A Date of Observation 1of16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code PEez. Construction 1 I I I CLAY: Medium stiff, gray -green, plastic gumbo i f i i i day, moist -8.00 I I I I i I I I I I I I I I I I I I I I -10.00 I I I I I I I I I I I I I I I I f 7 f f 1 28.5 2 I I I I l I I ' I I 2 , I I 1 I I CL 3 I I I I I I I I -12.00 I I I I I I 1 I [ I I I I I I I I I I I I I I l ? i i I I I I I I I I -14.00 I I I I l S i I I I I I I I I I I E S I I I I I I 33.5 _3604 33.5 1 I 1 I 1 I i I i = SILT: Stiff, gray -green, fine sandy, clayey, fi I I I I — - interlayered with sand SM 8 I I I I I — I _- Bentonite — Seal -18.00 7 I I I I I I I I I I - - i 37.0 _ 1 I I I I I , Sand Pack = — SILT: Hard, black -green speckled, clayey, fine ' — sandy, moist, moderately plastic, scattered -20.00 ; I i I i I i I i I — - pelecypod shell hash 38.5 5 ' — ' ' ' — 4 I 1 I I I ML 29 -22.00 I I I I I I I 1 I I I I I I I I 1 I I I - - - - -24 00 I I I I I I I I I I I I I I I I 1 - - = I I I I I I I I I 1 - 0.01 a' - Slotted Screen MIL 43.5 10 26.00 20- 27 I I I I I I I I 1 1 — - -28 00 I I I I I I I I 1 I I I I I I I I I I I I I I I 1 I - = - -30.00 I I I I I I I I I I I I I I I I I I I I 1 I 1 I I _- - — - - 48.5 22 I I I I I I I I I 1 49.038 - 5M Bentonite SAND: Very dense (partly cemented), black -green 501.2 i i i i i speckled, clayey, silty, fine glauconite nodules Seal DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 3 of 3 Client and Project C&D Landfill, Inc, (Pitt County) Ground Elevation 17.97 Equipment CME 750 Drilling Method 3-7/8" rotary -mud Water Level, TOB 6.6 Date Started iomoo Date Ended 10/11100 Water Level, 24 Hr. 7.9 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 7.9 z Comments Plowed field. cool sunny weather Total Depth 70.o Date of Observation 10M6100 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Very dense (partly cemented), black -green 1 I I I I I E I I I I - speckled, clayey, silty, fine glauconite nodules -3-4.00 I 1 I I I I I I I I 53.5 50/ t I i 36.00 i I i - SM -38.00 I I ! I I I - I I I I I I I I I I I I I I I I I r I 1 57.4 - - ' SAND: Medium dense, green -black speckled, 40.00 i i i i i silty, clayey, fine grained, wet 58.5 6 I I I I I I I I F 7 I I I i 8C 7 42.00 I I I I I I I I Boring .• collapsed below50 I r I 61.5 , ' . feet CLAY: Medium stiff to very hard, gray -green, fine -44.00 i i i I I I I I I I r i ! I I I I I I I sandy, silty, moderately plastic 63.5 5 I I I I I I r s I I I I I -46.00 6 I I I ° I I I CL 5 I I I I I I i l I I I I I i I -48 00 I I I I I I I I I I I I I 7 r r ! F I I I I I I i I I i I I -_^•� I I I I I I I I I I I l k t ! I I I 1 I I I I I I 68.5 40 38 ; CL -s7 nn 501.5 I I t r I I Boring Terminated at 70 feet DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P. G., P.E. Boring No. MW-2s Engineering and Geology Depths in feet, referenced 6.g.s. Page 1 of i Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 1 s.45 Equipment CME 75 Drilling Method 4114" ID HSA Water Level, TOB NA Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Finn Bore & core Logged by David Garrett Stabilized Level 7.91 Comments Locking cover with 2.99' stickup Total Depth 13.o Date of Observation 5116101 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction 18.00 i i i i i - • - SILTY SAND. Loose, tan -brown, moist Concrete I I i I I I I I I I Prdut l I I I I ! I I I I t — SM Bentonite 16.00 I I I ' I I ' ! I I 1 I I .. - Sea[ 14.00 l 3 I I I I 1 I I I I I 1 I I I I I I 1 - 12.00 I I I I I I I I I I I I ' 1 t I - I I I I I I I I I I 7.0 - SAND: Loose, tan, fine to medium, wet I I 1 I I I I 1 i I . ' 0.019, 10.00 I I Slotted 1 I I I I I I ! 1 I I I SVV Screen 6 W00 V 1 t I I I t I I I ! I I I I I I I I I I I I I I I I I I I [ • 6'00 I I I I i i Boring Terminated at 131eet DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P. G., P.E. Boring No. M 3d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 19.37 Equipment CME 750 Drilling Method 4-1v4" Hollow AugaiNater Level, TOB 3.0 Q Date Started 10112l00 Date Ended 10/13/00 Water Level, 24 Hr. 4.5 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.5 Comments Plowed field. cool sunnv weather Total Depth 50.0 Date of Observation 10/16/00 Elev, SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I I r I CLAY: Stiff, bright yellow -orange, fine sandy, silty, 1 I I I S I moist I I I S I 18.00 I 1 I I I I I I I 1 I I I I I I I I I I I i ! i I I I I i I I I I I I I Caved 16.00 3.5 4 + I i i i 4.0 SAND: Medium dense, tan -yellow, silty, trace of 4 I i I i I i I i I CL M 6 I I I I I f day, moist 14.00 I I I I I I I I f i I I I I I I I I 1 i 7.0 ' 12 00 I I SAND: Medium dense, tan -buff, well graded fine I to coarse, wet I I I I 4 S I I I 6.5 4 I I I I I I 10.00 5 * I i I i I i I i SW I I i 3 I I I I I I I I I I 1 1 I I I I 8.00 1 I ! ! I I I I I I I I I I I I I I I I 6.00 I I I 1 I 1 I I I I I I I I I 13.5 2 ' ' 14.0 - I I I I SILT: Stiff, gray -green, fine sandy and clayey, with 4 I M L- 4 I i i I i i — - rr heavy shell hash (tuitellas) wet, medium plastic CL 4.00 I I I I I I I I I I I I I I I I 1 1 1 1 — - - 2,00 I I I I I I I I I I I I I I I I I 1 I I I i 16.5 2 I I I I I 1 I I I I - 0•DD 2 CL 4 I I I I I I 1 I I I I I I I I — - - - -2.00 I I I I I I I I I I I I I 1 I I 1 1 I 1 I I I I r I I I I I I I I I - - - - - -4.00 I i I i 1 i I i I i 23.5 — CLAY: Medium stiff, gray -green, plastic gumbo 23.5 2 5 Gay, moist CL 7 I I I I 1 1 I I I I I DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P.G., P.E. Boring No. MW-3d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 19.37 r `1 Equipment CME 750 Drilling Method 4-114" Hollow AugekWater Level, TOB 3.0 a Date Started 10/12/00 Date Ended 10/13/00 Water Level, 24 Hr. 4.5 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.5 Y Comments Plowed field, cool sunny weather Total Depth 50.0 Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez, Construction _g 00 ' CLAY: Medium stiff, gray -green, plastic gumbo Bentonite- : day, moist Cement I I I I I r i I I I I I Grout -8.00 I I I I I I ! I I I I 27.5 - - SILTYSAND: Medium dense to dense, partly .. cemented, black -green speckled, variably clayey, 28.5 3 - silty, moist, very hard drilling (cemented) below 38 6 * i i i i feet, glauconitic SM -10.00 5 ! 3 1 I I I I I I I I I -- 12.00 F I I I I I 1 I I 1 I I I I I I I I I I I I I I I 77 - - -14.00 I I I I I I I I I I I I I I I I I I I I I I 33.5 5 I I I I I 18 I I I I I I SM 20 I I I ' - - _18.00 I I I I I _ Bentonite I I I I I I I I I I I I I I I I I I I I - Seal -18.00 I I I I I I I I I I I I 1 I 1 I I I I I I I I I I 38.5 15 I I I I I I I 1 1 1 I I 1 I I I - -20.00 501.3 i I I i I I i 1 1 i l r i I I _ - - SM I I I 1 s f I I - .. -22.00 I I I s I I I 1 I l I I - - Sand Pack -24.00 I I 1 I I 1 1 3 F I SM 43.5 501.5 I 1 I I 1 I f 1 I I -26.00 I 1 1 I I I I I 1 ! ! I I I 0.010" I I I I I Slotted 1 1 1 I r I 1 ! 1 1 I I - -- - Screen V W 1 1 I I I I I I I I 3 f I I I I - - 48,gyp .5 2943 1 I 1 I r I I I I 1 1 1 I I I -30.00 1 ! SM 501.5 Boring Terminated at 50 feet DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P.G., P.E. Boring No. MW-3s Engineering and Geology Depths in feet, referenced b.g.s- Page 1 of 1 Client and Project CAD Landfill, Inc. (Pitt County) Ground Elevation 19.37 Equipment CME 750 Drilling Method 4-11,V Hollow AugeliNater Level, TOB 3.9 s Date Started 815107 Date Ended 815107 Water Level, 24 Hr. NA Drilling Firm Bore A Core Logged by Aaron Hill Stabilized Level NA Comments Renlaces former MW-9s Total Depth 20.o Date of Observation NA Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I t ' SILTY CLAY: St'df, bright yellow -orange, fine 1 I I I 1.2 sandy, silty. moist 18.00 1.0 12 + Bentonite- — 16 i i i i — SILTY SAND: Med. dense, brown w! orange ML_ Cement I .. mottle, fine -medium texture CL Grout 21 I I I I I - I I I I I I 33 — Bentonite 16.00 3.5 14 ' i ' i ' i i ' i SAND: Tan, silty, fine texture, moist Seal 11 i i i i i SM- 11 I I I I 1 ML 14.00 I I I I I - 6.0 7 I I i I i I i I i • Sand Pack 11 i i i i 7.1 SM 12.00 11 ; SAND: Medium dense, tan -gray, well graded fine ' to medium texture, wet '• 0.010" 8.5 4 Slotted 4 SW Screen 10.00 4 I I i ! I i I I i I I i I t sM 8 00 I I I 1 1 I I I I I I I I I 7 ! I - I I I I I I I I I I I I r t S 12.9 - I I i I i I i t i CLAYEY SILT: Stiff, gray -green, fine sandy and 6.00 13.5 2 1 _ _ clayey, with heavy shell hash (turritellas) wet, 3 medium plasticity SM 3 I I I S I I 4.00 I I I I I I I I I I \ W I I E I I I I I i I I I I I I I I i t I 2.00 I I I I I \- I I 5 I I 18.5 4 I I ! I I — 5 I \ CL_ 0.� 5 I I F I I I _ Boring Terminated at 20 feet MIL r-111 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/10/09 Date Ended 08/10/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 21.93 Total Depth 20.0 Boring No. MW-3A Page 1 of 1 Ground Elevation 19.13 Water Level, TOB 5.9 Water Level, 24 Hr. NA Stabilized Level 11.4 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -18 -16 -14 -12 Eli] -8 -6 -4 -2 -0 N = 0 20 40 60 80 100 BPF CLAYEY SAND: Topsoil with roots Bentonite- 1.0 3 1.6 Cement Grout 5 SM 0 - 3' SILTY SAND: Loose orange sli. clayey, fine - medium, trace of roots, sli. moist 3.5 4 - Bentonite Seal 4 -_ SM 3-4' 5 SZ 6.0 7 SM 7 8.5 SAND: Medium dense, tan -buff, 8.5 5 s well graded fine to coarse, SW moist -wet Sand Pack 4-20' 12.9 :. . — �- SILTY CLAY: Stiff, gray -green, 13.5 3 fine sandy, with heavy shell \- hash (turritellas) wet, medium ML- 4 plasticity CL 0.010" Slotted Screen 5 - 20' �- 18.5 2 \- M L- 2 — �— Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P. G., P.E. Boring No. MW-4 Engineering and Geology Depths in feet, referenced b.g.s. Page i of i Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 14.83 Equipment CME 75 Drilling Method 4-114~ ID HSA Water Level, TOB NA s Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm sore & core Logged by David Garrett Stabilized Level 3.35 Comments leckinn cover with 3.59'stickuo Total Der)th 13.o Date of Observation wiwo1 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction _ .. - SILTY SAND: Loose, tan -brown, moist Concrete I I I I I .. Pad 14.00 ' ' ' ' ' — I I I I I I I Grout I I 1 I I I - — SM Bentonite I Seal 12.00 I I .. I I I I I I I I 1 I I l I I I — 10.00 I I I I I I I I I 1 1 1 I I I l I I I I — I I I I I I I I 1 I I 6.0 — SAND: Loose, tan, fine to medium, wet i i $.00 I 1 I I I I I ! f I I - - 1 t I 1 t I I 1 I I I 0.010" Slotted 6.00 W Screen I I I i i I I I I I I I I I I • SW 4.00 I I I I I I I I I I I I ! I I - 2.00 I I I I I I Boring Terminated at 13 feet DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P. G., P.E. Boring No. MW-5 Engineering and Geology Depths in feet, referenced b.g.s_ Page 1 of 1 Client and Project C&D Landfill, Inc. (Phase 1) Ground Elevation 14,.80 Equipment Mobile 6-53 ATUrilling Method 4-1147 Hollow AugeidVater Level, TOB 3.6 Date Started 11M9102 Date Ended 11/19/02 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 3.9 Comments wooded area, cool sunny weatherTotal Depth 20.o Date of Observation 11/27/02 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Loose, tan, silty, fine to medium, dry ` Bentonite- I Cement 14.00 i ; i i Grout 1.0 4 4 i i i i SM 6 S I I I I I I Bentonite 2.9 Seal 12.00 i i i i i SAND: Medium dense, tan -buff, medium to 3.5 9 I I I 1 coarse, wet (fluvial) 3V ' I � 14 i i i i SW 10.00 16 I I I I I I I I I I S I 5.6 ' SAND: Loose to medium dense, tan -buff, fine to 6.1) 9 coarse, wet, trace of silt (fluvial) $.00 9 i i i i sM 4 I k I I I I I 3 t I I I I I I 8.1 Sand Pack I CLAYEY SAND: Loose, green -gray, silty, wet, 6.00 8.5 4 3 I . � sampled as distinct sand layers with plastic clay lenses (channel or near -shore deposits) SC 4 I \- I I ! I I \ \- I �- 4'00\- 0.01 a, \- ••• Slotted l I I I I Screen 2•00 3 I I I I 1 13.5 3 I i i i ....... .\- 4 i i i i \-\- SC 0.00 4\-\- i-- * Locking steel cover w! 3 foot \- •\ stickup �, -2.00 I I I I I I I I 1 I \- I I 1 I I I I I I I 18.4 Deep SILTY CLAY: Stiff, gray -green, var. sandy, shell 4.00 18.5 3 i i i i i marine 4 1 i i i i hash, moist, plastic ** CL_ deposits (Yorktown 6 i i i Boring Termat 20 feet CHinated Grp.) DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P. G., P.E. Boring No. MW-6 Engineering and Geology Depths in feet, referenced b.g-s. Page 1 of 1 Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 16"87 Equipment CME 75 Drilling Method 411,C ID HSA Water Level, TOB NA Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 6.68 Comments Lockina cover with 3.16" stickup Total Depth 13.o Date of Observation 5116/01 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I SILTY SAND: Loose, tan, moist Concrete pad 16.00 I — I I ! I I I - - Grout I I f I I SM Bentonite — Seal 14.00 I l f I I I I I I I 1 I I I I - 12.00 3 1 I I I I ! I I I . . — I I 1 ! I I I I I 1 6.0 - SAND: Loose, tan, fine to medium, wet I I I I I i 0.00 I I I I I 1 I I ! I • I I I I I 1 I I I I • 0.010" ' Slotted 8.00 i i i r i Screen I 1 1 I I I I I I I F I 1 I I I - SVj b 00 I I I I I I I - 1 I l I I I I I I I - 1 1 I I I I - Boring Terminated at 13 feet 4.00 - DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P.G., P.E. Boring No. AM-7 Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of i Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 16.03 Equipment CME 75 Drilling Method 4-1►47 ID HSA Water Level, TOB NA s Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm sore & core Logged by David Garrett Stabilized Level 5.29 ('nmmAntS Lne-kinn cover with 3.37' stickup Total Depth 13.o Date of Observation 5/16/01 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SILTY SAND: Loose, tan, moist Concrete I I I I I •• P I I I I I — Grout 14.00 1 ; r ; I ; I ; I ;77 SM Bentonfte I I I E I I I I I i Seal 12.00 I I I I I I I I I I I I I I I I S 5 1 i - I I I I ! I I I I 5.0 - - I SAND: Loose, tan, fine to medium, wot 10.00 I I S ! t I I I I I I 1 I I I I I 1 I I I I I I I I I 1 I I I I I I I 0.010" I I I I 1 Slotted Screen I SW 6.00 I 1 I I 1 I I 4D0 I 1 I I I I 1 i I I Boring Terminated at 13 feet DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 David Garrett, P. G., P.E. Boring .No. AM-8 Engineering and Geology Depths in feet, referenced b-g.s. Page 1 of 1 Client and Project CSD Landfill, Inc. (Phase 1) Ground Elevation 18.30 Equipment Mobile 13-53 ATDrilling Method 4-114" Hollow AugeliJVater Level, TOB 7.3 s Date Started 11/18/02 Date Ended 11/18/02 Water Level, 24 Hr. 7.3 Drilling Firm Bore S Core Logged by David Garrett Stabilized Level 7.3 ('OMMentS wooded area- cool sunny weatherTotal ❑eoth 20.o Date of Observation 11/27/02 Elegy. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction 18.00 SAND: Loose, tan, slightly silty, fine to medium, ` Bentonite- ' dry Cement Grout - 2 i i r i SW 16.00 3 I , I I , f I I , I I , I I , I - Bentonite Seal 3.5 3 I s I I I I 14.00 3 i i i i t - SW 4 I I I I I I I I I I I I I 1 f - I I I I I 6.3 ' 12.00 6.0 4 �' 4 SAND: Medium dense, tan -buff, medium to SW 4 I I I I f I I I :. coarse, wet 10.00 i ! i I i I i I i I 8 4 Sand Pack _ . • SAND: Loose to medium dense, tan -buff, fine to 8.5 7 8 I I i I i I i I , ' ' coarse, wet, trace of slit Sw 8.00 I 1 I I I - I I I I I Slotted I I I I 1 Screen W 6.00 I I I I I I I I I I I I 1 1 1 • 13.5 4 I I I 1 I I I - 4.00 4 I i i i i SW 4 I I 1 I I I Locking I , , , , • steel cover _ wl 3 foot 2.00 I I I : = I stickup I i I I i I 1 i I I s i I i I 17.6 ." SILTY CLAY: Mod. stiff, gray -green, var. sandy, 0.00 i i i heavy shell hash (turritellas) moist, plastic '• CL- " Deep 18.5 3 l• ; I i I i I i I CH marine deposits 4 I I 1 I I 1 I (Ye rkiown 6 Boring Terminated at 20 feet Fm.) DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 20.58 Total Depth 20.0 Boring No. MW-9A Page 1 of 1 Ground Elevation 17.64 Water Level, TOB 3.1 Water Level, 24 Hr. NA Stabilized Level 4.8 Observation Date o8M o/og Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -16 -14 -12 -10 -8 -6 -4 -2 -0 -2 N = 0 20 40 60 80 100 BPF 77 SILTY SAND: FILL with brick 1.0 3 77 and concrete fragments Bentonite- Cement Grout 4 2.1 SM 0-3' 5 XX CLAY: Med. stiff, orange -tan - gray (mottled), fine sandy, very 3.5 10 moist Bentonite Seal 12 CIL 3 - 4' 13 Ir 5.9 SAND: Medium dense, light 6.0 5 ♦ 5 gray -buff, sli. silty, well graded SW- 6 fine to medium, wet SM 85 4 5 SW- 5 SM Sand Pack 4-20' 13.5 4 13.7 _ 4 — SILTY CLAY: Med. stiff, gray- ML- 5 green, sli. fine sandy, with CL �- heavy shell hash (turritellas) 0.010" Slotted — wet, medium plasticity Screen 5 - 20' �- Artesian water press. at 12 feet 18.5 2 \- M L- 2 — Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/06/09 Date Ended 08/06/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 16.61 Total Depth 20.0 Boring No. MW-10 Page 1 of 1 Ground Elevation 14.16 Water Level, TOB 2.7 Water Level, 24 Hr. NA Stabilized Level 4.8 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -14 -12 -10 -8 -6 -4 W -0 -2 -4 N = 0 20 40 60 80 100 BPF SILT: Soft, dark brown, fine 1 sandy, organic, very moist Bentonite- 1.0 Cement Grout 1 2.1 ML 0-3' 5 SAND: Med. dense, tan -buff, uniform fine grained, wet t t 3.5 9 Bentonite Seal 13 SP 3-4' 12 Ir 6.0 9 12 7.1 SW 2 8.0 SAND: Loose, tan -buff, sli. silty —_ SILTY CLAY: Soft, gray -green, 8.5 3 sli. fine sandy, with heavy shell 2ML- \ hash (turritellas) wet, distict CL sand and clay layers Sand Pack 4-20' 13.5 3 �- 2 — M L- 3 CL \- 0.010" Slotted Screen 5 - 20' �- 18.5 3 \- M L- 3 — Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/06/09 Date Ended 08/06/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 14.49 Total Depth 20.0 Boring No. MW-11 Page 1 of 1 Ground Elevation 11.60 Water Level, TOB 6.1 Water Level, 24 Hr. NA Stabilized Level 3.1 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data M -8 -6 -4 -2 -o -2 -4 -6 -8 N = 0 20 40 60 80 100 BPF SAND: Loose, dark brown, silty, 2 fine - medium, tr. clay, moist Bentonite- 1.0 Cement Grout 2 SM >0-3' 3 2.9 CLAY: Very soft, green -gray, 3.5 1 silty, fine sandy, w/ turritella Bentonite Seal shell hash, wet ��- 3 - 4' o 5.5 CLAY: Soft - med. stiff, gray- 6.0 2 Sz 3 green, fine sandy, very silty, ML- 2 with shell hash (turritellas) wet, CL very sandy layer w/ large shell fragments at 9.5 - 10 feet 8.5 4 5 SC- 6 CL Sand Pack 4-20' 13.5 5 5 14.5 MH- $ SILTY CLAY: Med. stiff, gray- CH — green, sli. fine sandy, wet, very 0.010" Slotted plastic Screen 5 - 20' 18.5 5 \- M H- Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 16.18 Total Depth 20.0 Boring No. MW-12S Page 1 of 1 Ground Elevation 13.72 Water Level, TOB 2.1 Water Level, 24 Hr. NA Stabilized Level 5.3 Observation Date o8M o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -10 -8 -6 -4 -2 -0 -2 -4 z. N = 0 20 40 60 80 100 BPF SAND: FILL, Loose, brown, 1.0 1 silty, moist (drilling pad) Bentonite- Cement Grout 2 2 0 SM sz 0 - 3' SAND: Loose, tan -gray. sli. 5 silty, fine -medium, black 3.5 10 decayed organic debris, wet Bentonite Seal 12 SW- 3-4' 13 SM 7W 6.0 5 9 SW 10 SM 8.5 5 Loose, white, clean "sugar sand" 7 9.5 SP 3 10.0 �- SILTY CLAY: Med. stiff, gray- Sand Pack green, sli. fine sandy, moist, w/ 4 - 20' _— shells, very plastic 13.5 3 5 CH \- 0.010" Slotted Screen 5 - 20' �- 18.5 5 \- M H- Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 20.69 Total Depth 20.0 Boring No. MW-13 Page 1 of 1 Ground Elevation 18.12 Water Level, TOB 5.1 Water Level, 24 Hr. NA Stabilized Level 8.8 Observation Date o8M o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -18 -16 -14 -12 -10 -8 -6 -4 -2 -0 N = 0 20 40 60 80 100 BPF SILTY SAND: Loose, brown, 1.0 2 fine -medium, w/ clay, roots, dry Bentonite- 3 (perimeter embankment fill) gW_ Cement Grout0 - 3' 3 - SM 3.5 3 4.0 Bentonite Seal CLAYEY SAND: Loose, tan, SC 3 - 4' 5 fine -medium, w/ wood, moist 5.7 - SILTY SAND: Very loose, tan- 6.0 1 1 brown, w/ tr. clay, wood sM 1 _ 8.1 �_ SILTY CLAY: Stiff, green -gray, 8.5 7 9 _— sli. fine sand w/wood Y, ML- 10 C L \_ Sand Pack — 4-20' 12.5 �- �- SILTY CLAY: Stiff, gray -green, 13.5 5 sli. fine sandy, w/ heavy shell 6 — hash (turritellas), moist, very MH- 6 plastic CH \- 0.010" Slotted Screen 5 - 20' �- 18.5 4 \- M H- 5 Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/17/02 Date Ended 12/17/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 17.45 Total Depth 40.0 Boring No. MW-14D Page 1 of 2 Ground Elevation 14.54 Water Level, TOB 2.9 Water Level, 24 Hr. 3.0 Stabilized Level 4.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -14 -12 -10 -8 -6 -4 -2 -0 W -4 -6 -8 -10 N = 0 20 40 60 80 100 BPF . SILTY SAND: Medium dense 1.0 ♦ tan -brown, fine to medium Convertedfrom 5 SM piezometer 5 B-23d 3.1 3.5 6 SAND: Medium dense, tan, 10 medium to coarse SP 9 6.0 7 10 SW 7 7.9 X. CLAYEY SAND: Medium 8.5 4 • dense, dark gray 3 _I SC 5 12.7 Bentonite- Cement Grout �- SILTY CLAY: Stiff, dark gray, 13.5 4 l \- fine sand layers, shell layers, 0-32' 5 — becomes sandy with shell hash ML- 6 below 28.4 feet CL 18.5 4 * �_ 6 CH 23.5 5 CH 6 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/17/02 Date Ended 12/17/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 17.45 Total Depth 40.0 Boring No. MW-14D Page 2 of 2 Ground Elevation 14.54 Water Level, TOB 2.9 Water Level, 24 Hr. 3.0 Stabilized Level 4.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -14 -16 -18 - 20 - 22 - 24 N = 0 20 40 60 80 100 BPF \- SILTY CLAY: Stiff, dark gray, fine sand layers, shell layers, becomes sandy with shell hash below 28.4 feet 28.5 21 : \- 16 CL Bentonite Seal 32-33' 32.8 �- SAND: Very dense, dark gray, 33.5 50/A silty, glauconitic, shell hash SM Sand Pack 33-40' 0.0101, Slotted Screen 35-40' 29 38.5 50/.5 Boring Terminated at 40.0 feet SM DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/18/02 Date Ended 12/18/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 16.60 Total Depth 20.0 Boring No. MW-14S Page 1 of 1 Ground Elevation 13.90 Water Level, TOB 3.0 Water Level, 24 Hr. 2.2 Stabilized Level 2.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -10 -8 -6 -4 -2 -0 -2 -4 -6 N = 0 20 40 60 80 100 BPF SILTY SAND: Medium dense Convertedfrom 1.0 tan -brown, fine to medium piezometer B-23s 5 SM 5 Bentonite- 3.1 _ sz Cement Grout SAND: Medium dense, tan, 3.5 6 0-1' 10 medium to coarse SP Bentonite Seal 9 1-3' 6.0 7 10 SW 7 7.9 X. CLAYEY SAND: Medium 8.5 4 dense, dark gray 3 Sc 5 12.7 Sand Pack 3-20' -- SILTY CLAY: Stiff, dark gray, 13.5 4 l \— fine sand layers, shell layers, 5 — becomes sandy with shell hash ML- 6 below 28.4 feet CL \- 0.010" Slotted Screen 5-20' 18.5 4 \— s ? Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett, P.G., P.E. MW-15s (OLD B-23s) Engineering and Geology Page 1 of 1 Client and Project CAD Landfill, Inc. (Phase 2) Ground Elevation 13.90 Equipment Detrich 0-10 Drilling Method 3-114" HSA Water Level, TOB 3.0 Date Started 12/18/02 Date Ended 12 I8102 Water Level, 24 Hr. 2.2 Drilling Firm Bare & care, inc. Logged by David Garrett Stabilized Level 1.4 Comments Lagged area, cool sunny weather Total Depth 20.0 Date of Observation 1116103 All deaths are given in feet and referenced b.a.s. Depth and Elev. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezometer Constuction Data -0 - 2 12.00 - 4 10.00 - g 8.00 - 8 6.00 - 10 4.00 - 12 2.00 - 14 0.00 - 16 -2.00 - 18 -4.00 — 20 -6.00 i I l i i i i + � I i i I i i i i i BLANK: No samples taken - please see log fpr &23d sz Bentonite- Cement Grout Bentonite Seal ' i I I i i Sand Pack 3 ' 0.0101, (} t E F e ! i i Slotted Screen DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett, P.G., P.E. MW-17 (OLD B-20) M I I I Engineering and Geology Page I of 1 Client and Project C&D Landfill, Inc. (Phase 2) Ground Elevation 18.18 Equipment Detrich D•10 Drilling Method 3-1/4" NSA Water Level, TOB 3.7" Date Started 12/09/02 Date Ended 12109/02 Water Level, 24 Hr. 3.9 Drilling Firm sore & Core, Inc. Logged by David Garrett Stabilized Level 4.1 Comments Logged area, cool Manny weather Total Depth 20.0 Date of Observation 1115103 All depths are given in feet and referenced b.g.s. Depth and Elev.1. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezometer Constuction Data - a 1 B_oa — 16.00 — 14.00 — 6 12.00 — 8 10.00 — 10 8.00 — 12 6.00 — 14 4.00 — 16 2.00 = 18 0.00 - 20 .. SILTY SAND: Medium Sentonite- ; i dense, dark brown, fine Cement Grout 3 grained SM 5 1 — Bentonite Seal � SAND: Medium dense to dense, tan -brown, SW 19 I i fine to medium 8 14 0i ! i i ! SW 21 ! I 9 12 SW 14 I f � I i Sand Pack 3 SW SAND: Medium dense, [ fine to medium, trace of i { silt E f f� �{ 0.01 01, I I i Slotted Screen 3 a E f ! ! SILTY CLAY: Medium 5 I stiff, trace of shells ML-CL DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 D SOIL CLASSIFICATION P .AND REMARKS T H SEE KEY SYMBOL SHEET FOR EXPLANATION OF (ft) SYMBOLS AND ABBREVIATIONS BELOW. 0 Sandy topsoilirootmat Landfill debris/gravel and sand ------------------------ COASTAL PLAIN: Orange -tan to gray, dry to moist, clayey and silty SAND (SM) C-OAST-AT P-1-Tan--a-a-nd -wh-t-m-ist-to-sa-tur-ate-d- L E SAMPLES PL (%) NM.(%) LL (%) E L I (Rec") G E D T N-COUNT ♦ FINES (%) E V E Y or N N P Rcc%MQD% SPT (bpf) D (ft) T E 6"- 6"- 6"- 6" 10 20 30 40 50 60 70 80 90 100 15.0 5 slightly silty, tine to coarse SAND (SP) with trace rounded 10.0 fine gravel 1 . 10 5.0 15 YORKTOWN FORMATION: Dark gray to gray -green,- 0.0 saturated, silty, fine to medium SAND (SM) with thin (0,1-0.2) lenses and layers of dark gray -green, fat CLAY (CH) 20 Boring terminated at 20.0 feet. -5.0 G n :7 a 3 25 0.0 d .a a a a n 30 15.0 35 -1 1 �- -20.0 40 -1 1 F- -25.0 45 -30.0 CONTRACTOR: Regional Probing Services -Larry Opper LOGGED BY: M. Lear EQUIPMENT: Geoprobe 5410 DRILL METHOD: Direct Push HOLE DIAMETER: 4" WELL: Stickup 2.9' Size 2" CLOSURE METHOD: Installed Monitering Well MW-16. REMARKS: Well developed by purging approximately 3 well volumes via bailer and pump. Static water level measured at 7,45 ft below TOC. 0 10 20 30 40 50 60 70 80 90 100 GEOTECHNICAL BORING RECORD BORING NO.: MW-16 PROJECT: EJE Recycling LOCATION: Greenville, NC DRILLED: June 16, 2017 PROJECT NO.: 6468-17-7070 PAGE 1 OF 1 IEWED BY: amec faster wheeler ► DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 David Garrett, P.G., P.E. Engineering and Geology .,Client and Project C&D Landfill, Inc. (phases 3 and 4) Equipment CIVIE 450 Drilling Method 4 1vvv H$A Date Started 12114101 Date Ended 12/14/01 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments :.iamg2u aiea5 cioal rarliny weather Total Depth 15.0 All dent :- are ,;:al: ,l__� _s_..__i.td r � � �kl iT.CI pelf l�if�rl'�.��YV`ii N.w.sx OLD B-Is (BG) Page 1 of 1 Ground Elevation 17.19 Water Level, TOE 1.5 Water Level, 24 Hr. 1.4 Stabilized Level 1.6 Date of Observation 12/27/01 Depth and Elegy. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezom2ter Constuction Data 0 r 16.00 2 14.00 4 12.00 6 10.00 8 8.00 10 6.00 12 4.00 14 SAND: Loose, gray- 2 I I I - brown, variably silty, 3 4 moist, trace of clay and a i ! . organics SM I Bentonite- s 6 ' SP- Cement Grout 7 i I SM 2 SILT: Soft, dark bra.,.n, 2 clayey, decayed 2 — organics (channel Bentonite Seal -= deposits) 2 I — 1 I i ML 2 — Sand Pack 0.0101, 2 i I i i - - — ML Slotted Screen DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 Appendix Laboratory Analytical Report June 2021 Groundwater Monitoring Report CEO Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 6 7407- CDLF- 2009 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 L1LILl��®LlL1LILJULiU 4JQ ��a��1� Drinking Water IDs 37715 4 wastewater YD1 10 114 OAKMONT DRIVE GnEE NVILLE, N C. 27858 CLIENT: C & D DISPOSAL, INC. MR, MMSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: ~ LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHON (252) 756.62A8 FAX (252) 756-0633 CLIENT ID: 6003 E ANALYST: JAP DATE COLLECTED: 06/08/21 Page: 1 DATE ANALYZED: 06/12/21 DATE REPORTSD: 11/12/21 PARAMETEH8, u9/1 MDL MRL Mw-4 1. Chloromethane 0.71 3.000 V 2. Vinyl Chloride 0.22 0.200 ••• U 3. Bromomethane 0.67 10,000 --- U 4. Chloxoethana 0.40 10.000 U S. Trichlora[lUoromethane 0.24 1.000 --- U 6, 1,1-Dichloroethene 0.17 5.000 --- U 7. Acetone 9.06 100.000 --- U B. Iod4methane 0.29 1O.00D --- U 9. CArb" Disulfide 0.23 100.006 --- U 10, methylene Chloride 0.44 1.000 --- U 11. trans-1,2-Dichloroethene 0.23 5,000 --- U 12. 1,1-Dichioxoethane 0.20 5.000 --- U 13, vinyl Acetate 0.20 50.060 --- U 14. Cie-1,2-Dichloroethene 0.25 5.000 •-- U I$, 2-Butanons 2,21 100.000 --- U 16. Bromochloromethane 0.27 3.000 - U 17, Chloroform 0.25 $,000 --- U 18. 1,1,1-Trichloroethane 0.19 1.000 --- U 15, Carhon 'tetrachloride 0.04 0.200 --- U 20. Sansone 0.24 1.000 --- U 21. 1,2-D1chlarOeth*n* 0.02 6.200 --- U 22. Triahloroethene 0.23 1.000 ••• U 23. 1,2-1)1chloroprppane 0.04 0.200 --- U 24, Bromodichlorom*thOne 0.04 0,200 ••• U 25. Cis-1,3-Dichloropropens 0.06 0.200 --- U 26. 4-Methyl-2-Pentanane 1.19 100.000 --- U 27. Toluene 0.23 1.000 --- U 2B. trans-1,3-Diahlorvprvpene 0.04 0.200 --- U 29. 1,1,2-Trich2aroethane 0.03 0,�00 --- U 30. T.trechlcraethene 0.10 0.200 --- U 31. 2-Hexanone 1.57 50,000 --- U 32. Dibromochloromethane 0.03 0.200 --- U 33. 1,2-Dibromoethane 0.03 0.200 --- U 34, Chlorobenzene 0.30 3.000 --- U 35. 1,1,1,2-Tetraehloroethane 0.22 1,000 --- U 35. Ethylbenaene 0.21 1.000 --- U 37. Xylenes 0.59 S•OOD --- U 38. Dlbromamethene 0.28 10.000 --- U 39, gtyrene 0.19 1.000 --- U 40. Bromform 0,20 3.000 --- U 41. 1,2,2,2-Tytrachloroethane 0.03 0.200 --- U 42. 1,2,3-Trichloroprvpene 0.09 0.200 --- U 43. 1,4-Dichlorobenzene 0.39 1.000 --- U 44. 1,2-Dich2arobenrene 0.32 5.000 --- U 45, 1,2-Dibromo-3-Chlarogrop*no 0.07 0.200 --- U 46. Acrylonitrile 2.72 200.000 --- U 47. trana-LA-Dichloro-2--Rutene 0.42 100.000 --- U 40. Aeralein 1.97 4.000 - U j • Eatimated value between the NVL and MRL, U - Below ALL Uuantitation Limits. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 o u k000Too d od Drinking water XD: 37715 waptewataY ID: 10 114 OAKMONT DRIVE PHONE (252) 756.6208 GRE�NVILLE, N.C. 27W5 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 F MR. J'UDSON WHITEHURST 602 RECYCLING LANE ANALYST: J'AP GREENVILLE, NC 27834 DATE COLLECTED: 06/08/21 Page: 2 DATE ANALYZED: 06/12/21 4 DATE REPORTED: 11/12/21 REVIEWED BY: — LANDFILL APPgNDTX II EPA METHOD 8260D R4(18) PARAMETERS, ug/1 MDL MRL Mw-4 49, Allyl Chlorid• 0.20 10.000 --- u 50. Chloropreno 0.21 20.000 --- u 51, 1,3-DichlorobbnXane 0.41 5.000 --- u 52. Dichlorodiflunromethane 0,51 5.000 --- u 53, 1,3-DichlorOprOpane 0.29 1.000 --- ❑ 54. 2,2-Dichloxopropaae 1 0.17 15.000 --- u 55, 1,1-Dichlaropropene 0.22 5.600 --- u 56. Ethyl Mothaerylate 0.16 10.000 --- u 57, Hexachlarobutadiene 0.10 0.200 --- u 50. I84butyl Alcohol 12.00 100.000 --- ❑ 59. Methacrylaai.trile 1.93 100.D00 --- D 60. Methyl mathacrylate 0.25 30.000 --- ❑ 61. Naphthalene 0,47 6.000 --- u 62, Propionitrild 3.26 150.000 --- 63. 1,2,4-TrichlorobentOnt 6.50 10,000 --- u fig. Acetonitril• 36.29 55.000 --- 65. Tetrahydrofuran 0.39 11000 --- u 66. 1,4-%oxane 2.71 3.000 --- u a . Estimated value between the MDL and MRL, Q r yelaw ALL Quantitatiorl Limita. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63'd prinking Water ID, 37715 Waatswttox 1Pt 10 114 OAKMONT DRIVE GREENVILLE, N.G. 27858 C & D DISPOSAL, INC. MR. JUrDSON WHITEHURST 802 99CY'CLING LANE GREENVILLE, NC 27834 PHONE /bb-6208 FAX (252) 756-0633 ID#: 6003 DATE COLLECTED: 06/08/21. DATE REPORTED : 07/02/21 REVIEWED BY: 1 b5W-4 Analysis Method PARAMETERS MDL MRL Date ApAlyst coda PH (fiold measurement), Units 6.2 06/08/21 PJC 4500HB-11 Nitrate*Nitrite am N, mg/l 0,04 C.04 --- u 06/09/21 RSS 351.2 R2-93 Alkalinity (t4 pH 4.5), mg CaCO3/ 1 1.0 1.0 200 06/14/21 Dld 232OD-11 Chloride, mg/1 5.0 5.0 15 06/14/21 JMS 4500CLB-11 TQLoL piAaOlved Residue, mg/1 1.0 10 M 120 09/10/21 CAW D5907-13 Sulfate, mg/1 5.0 5.0 65.7 06/14/21 LFJ 45003042ELI Antimony, ug/1 0101 1.0 O,D97 06/14/21 HMM EPA200.6 Arsenic, µg/1 0.D9 5.0 1.2 J 06/14/21 HMM 6PA200.9 Barium, ug/1 0.04 10.0 166 06/14/21 HMM EPA2DO.8 Beryllium, ug/1 0.02 1.0 0.09 J 06/14/21 HMM EPA200.8 Cadmium, ug/1 0,04 1.0 - -- U 06/14/21 HMM &PA2DO.0 Cobalt, ug/l 0.02 1.0 0.26 J 06/14/21 HMM EPA200.8 Total Chromium, ug/l 0.12 5.0 2.11 06/14/21 HMM EPA200.8 copper, ug/l 0.04 10.0 0.14 J 06/14/21 HMM EPA200.8 Iran, ug/l 4.96 50.0 7317 06/17/21 LFJ 9PA200.7 Manganese, hq/1 0.31 10.0 B6 06/17/21 LFJ EPA200.1 Lead, uq/l 0.03 5.0 0.1$ J 06/14/21 RMM EPA200.B mev; 'y, UY/1 0.05 0.20 --- U 06/11/21 MTM 245.1 R3-94 Nickel, ug/l 0.01 10.0 0.24 J 06/14/21 HMM EPA200.9 selenium, ug/1 0.05 10.0 0.62 J 06/14/21 HMM sPA200,0 silver, 09/1 0.22 5.0 --- U 06/14/21 HMM HPA200.9 Thallium, ug/l 0.02 1.0 0.02 J 06/14/21 HMM EPA200,8 Tin, µg/l 0.05 100.0 --- U 0$/14/21 HMM EPA200.8 Vanadium, ug/1 0.04 1.0 2.2 06/14/21 HMM EPA200,9 zinc, ug/1 0.17 10.0 $.4 J 04/14/21 HMM EPA200.8 Sulfide, ug/1 100 1000 --- U 06/10/21 LFJ 450082p-11 Conductivity (at 25C), nMhcs/Ca 1.0 1.0 $2$ 0$/08/21 SEB 25105-11 Diaaolved oxygen, mg/l 0.1 0.1 0.7 05/08/21 PJC 450000-11 Temperature, °C 20 06/00/21 PJC 2550E-10 Static Water Level, feet 6.45 06/08/21 PJC Well Pepth, eeet 15.98 06/OB/21 PJC 4RR, my 4.101 06/09/21 PJC 2580E-11 Turbidity (Field), NTU 1.0 2.0 9.0 D6/09/21 PJC 2130E-11 J - Estimated value between the MDL and MRL, U . Below ALL puxntitativn Limito. All QC requiremenK6 not met: M - Method blank exceeded method constant weighl eriteriR. DocufS�ilgL}nREf�nfv�elnopfe ID: �6F6DlF1B-6/131D-1i4f6�1D(2--]97755AIII^^^-Ff7�"SDCCAff78CDo1DE63 LI1JLJllLI VUL�LJLILI LIU u� LILILI+JV IiJ W Drinking Wator ZD: 37715 L] wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE CREENVILLE, NC 27834 REVIEWED BY: BASE/NEUTRAL COMPOUNDS EPA METHOD 8270E R6(1.8) PHONE (252) 756-6206 FAX (252) 756-0633 CLIENT ID! 6003 ANALYST- HIC DATE COLLECTED: 06/08/21 DATE EXTRACTED: 06/10/21 DATE ANALYZED: 06/15/21 DATE REPORTED: 07/02/21 PARAMETRRE, ug/l MDL MRL MW-4 1. Aaenaghkhene 2.66 10.000 - U a - Estimated value between the MDL and MRL, U - $elaW ALL Uuantjt4t,an Limits, DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 -p � Cn Cn in W .. rn n o: v Cn Of o .. A A rn v : mo `o . EP `> z CD C N : : CD N E CD .. ,. U` m CA 93 a CD. s. tr o U e ;, c: CD: 3 O 0 Cn (D J t E � O N E RD ,..� 'r' 0 CD d z .. M �vav, �o.., . a... rz ,,: 0040 0 . 00• ems: m m TOTAL CHLORINE; ingil ' C7 ; :. ':• `.:: '; OR AT COLLECTION ug/I N TE0LRAtURE,°C: ATCOLLECTfON; : ;, .. OF CONTAINERS. m ......., WA •, • . rat&NiErife: Chloride:•:•,'' { ` � � ' <� .`' Sulfate �. �: ; �:.� . • . 0: f � ; � Sulfide''. F>� ¢•,:� 's:: :�i :' Tetni' erature,:.::: 8270E Du '. I:: ' } ' 8270E Dup: # 8270E Dup. 3:, 1 .. o 1 Fn _ rr1 Q ■■J �'' l N cn "A^ Q Crr1�7 Z a [A r n VCi Q Y .. 6. �E cn Z b a � ' •� �'� z "s 3r n n � o 7C � � D o rn 0 _ c rn Do 9 o Z W � : 8260D PARAMETERS/TESTS ' i c, by b c�c' 93 m O �y ay n � o z m v = r zn = O n Z a z a 0 s [ k � i § J ( | % z � ...� ?co § 7 I1E CD P/ ®. \m / \ƒ�P E _ 0 \ k ƒ \ \ \/ \ \ \ / \2 \� / / \ & _� C \ _ r n 0 \ - . .. mUBETBS S2 o n ? 2 B n / o f = 2 ztj o 2 r \ � \ \ k k k & ¢ 2 ± m S j � DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 k2wimmum M] G� 00 V pa 00 114 OAKMONT DRIVE GREENVILLE. N.0 27868 C & D DISPOSAL, INC. N.Z. JUDSON WHZTEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 Drinking water IDj 37715 IF- MEME1060" PHONE (252) 756-0208 FAX (252) 756.063.1 in#: 6003 A DATE COLLECTED: 06/08/21 DATE REPORTED : 11/12/21 REVIEWED 8Y MW-19 MW-iD MW-2s Mw-2D Mw-1.9 Analysis Method PARAMETERS MDL MRL Date Analyst Code 6.5 7.1 6.3 7.5 6.7 06/09/21 FJC 450OH8 pH (field measurement), Unite 0.47 4.11 --- U 06/09/21 XEs 353.2 Nitrate+Nitrite as N, mg/l 0.04 0.04 --- U --- U Alkalinity {to pH 4.5j, mg C&CO3/1 1.0 1.0 162 162 70 124 1620 06/14/21 D1J 23208- 5.0 5.0 15 14 19 12 206 06/14/21 JM$ 4500CL Chloride, mg/l Total Dissolved Residue, my/l 1.0 10 M 320 M 219 M 210 H 260 09/10/21 CAW D5907- 2000 06/14/21 BLV D5907- Total Dissolved Rsaidus, mg/l 1,0 10 rag/1 5.0 5.0 87.7 2410 29.9 06/14/21 LFJ 45009C eulfato, 53.0 38.4 06/16/21 Lrd 45009C sulfate, mg/1 $.0 5.0 AntimOny, ug/l 0.03 1.0 0.is J a.09 J 0.09 J 0.12 J 0.35 J 06/14/21 HMM EPA20C Arsenic, ug/1 0.08 5.0 1.3 J 1.0 J 0.71 J 0.54 J 18.8 06/14/31 HMM SPA2c0 ug/l 0.04 10.0 31.9 24.1 69.3 17.6 705 06/14/21 HMM EPA20C Barium, 0.02 1.0 D.02 J --- U 0.04 J --- U 0,02 J 06/14/21 HMM EPA20( Beryllium, ug/l U 0.08 J - U --- U 06/14/21 HMM ERA20C Cadmium. ug/1 0.04 1.0 --- U --- cobalt, mg/1 0,02 1.0 0.08 J 0.06 J 0.2s J 0.10 J 5.7 06/14/21 HMM 6PAZU( Total Chromium, ug/l 0.12 5.0 0.39 J 0,29 J 0.51 J 0.52 J 28.5 06/14/21 HMM HPA20( Copper, u9/1 0.04 10.0 2.2 J 0.79 J 0.75 J 0.42 J 0.413 J 06/14/21 HMM PPA20C 4.96 50.0 920 014 3D5 367 10545 06/17/21 LFJ HPA20( frig+, ug/1 91 29 13 599 06/17/21 LFJ EPA20( Manganese, ug/l 0.31 10.0 5 J 0.62 J 0.10 J 0.20 J 0.19 J 0.28 J 06/14/21 HMM HPA20( Lead, ug/1 0.03 5.0 Mercury, ug/l 0.05 0.20 0.05 J 0.05 J --- U --- U --- U 06/21/21 MTN 245.1 0.03 10.0 0.50 a 0.41 J 0.45 J 0.36 J 2.2 1 OW4/21 HMM OP4201 Ni¢kel, ug/1 0.05 10.0 9.70 J 0.21 J 0,26 J 0,18 J 1.5a 06/14/21 HMM EPA2D1 gelanium, ug/1 --- U --- U --- U --- U 06/14/21 H9X EPA201 silver, u9/1 0,22 5.0 --- U Thallium, ug/l 0.02 1.D 0.04 J --- U D.10 J 0.25J 0,92 J 06/14/21 RMM EPA201 Tin, ug/1 O.DS 100.0 --- U 0.14 J --- U O.D5 J --- 11 06/14/21 HMM EPA201 Vanadium, ug/1 0.04 1.0 1.9 0.39 J 0.55 J 0.39 1 8.a 06/14/21 HMM aFA20, 0.17 10.0 2.$ J 4.0 J 3.4 J 10.6 1.4 J 06/14/21 HMM EPA20, Zinc, ug/l 0 --- U --- U --- U 06/10/21 LFJ 45008 Sulfide, u7/1 100 1000 --- U --- Conductivity (At 25C5, uMhOd/om 1.0 1.0 493 399 410 451 3952 06/08/21 sEB 251DB Dissolved 0%ygen, mg/1 0.1 0.1 0.5 0.3 1.0 0.5 0.5 06/0$/21 PJC 45000- 21 71. 22 27. 22 09/08/21 PJC 25508 TempeYGCure, °C 6,23 8.16 9.30 11.91 10.51 06/00/21 PJC Static Water Level, feet 17.21 33,75 26.57 38.17 22.24 06/08/21 PJc well Depth, feet +57 +101 +99 +101 +156 06/08/21 PJC 259DH Q(aP, my Turbidity (aField), NTU 1.0 1.0 3.9 4.9 5.9 7,3 4-0 06/00/21 PJC 2230D All QC requirements were not met, M glank result exceeded method constant weight Criteria. J . estimated value between the MDL and MRL, u . 9olow ALL Quantitration Limits+ All QC requirements not ntet: M - MellHid blank exceeded mcihUd constant weight criteria. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 L � oWoIm[[a ° N lln(�a ip0��i��r�1 * 114 OAKMONT DRIVE 3REf=NVILLE, N-C. 27658 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 Drinking Water TDB 37715 Wastewater 1p: 10 FAX (252) 756.0633 ID#: 6003 A DATE COLLECTED: 06/06/21 DATE REPORTED : 11/12/21 REVIEWED BY: MW-3D KW-3A Trip Analysis Hathod PARAMRTERS MDL MRI4 blank Date Analyst Code PH (field measurement), Unite 7.9 6.5 06/00/21 PJC 4500HB-11 Nitrate+Nitrite as N, mg/1 0.04 0.04 0.31 0.76 06/09/21 xi:8 353.2 R2-93 Alkalinity (to PH 4.5), mg C4C43/1 1.0 1.0 242 SOD 06/14/21 DIJ 2320D-21 Chloride, mg/l 5A 5.0 21 49 06/14/21 JM8 A500CLB-ll Total Dissolved Residue, mg/l 1.0 10 M 310 M 570 06/10/21 CAW D5907-13 sulfate, mg/l $.0 5.0 --- U 56.9 06/14/22 LFJ 45009042311 Antimony, ug/1 0.03 1.0 0,00 J 0.21 S 06/14/21 HMH EPA200.8 Arsenic, u9/1 0.08 5.0 0.22 J 8.8 06/14/21 HMM RPA200.8 barium, ug/1 0.04 10.0 10.3 162 09/14/21 HMM EPA200.8 Beryllium, ug/l 0.02 1.0 --- U 0.05 J 06/14/21 HMM bPA200.8 Cadmfum, ug/l 0.04 1.0 --- U --- U 06/14/21 HHM EPA200.2 Cobalt, u9/1 D.02 1.0 --- V 2.5 06/14/21 HMM EPA200.8 Total chromium, ug/l 0.12 5.0 0.14 J 5.6 06/14/21 HMM EPA200.0 Capper, Vg/l 0,og 10.0 0.20 J 0.55 S 06/14/21 HMM EPA200.8 iron, ug/1 4.96 50.0 8 J 06/10/21 LP.T EPA200.7 Iron, u4/l 4.96 50.0 10145 06/17/21 LFJ EPA200.7 MAngansee, ug/1 0.31 10.0 --- V 410 D6/17/21 LFJ SPA200.7 Load, ug/l 0.03 5.0 --- U 0.24 J 06/19/21 HHH IRPA200.0 Mercury, ug/I 0.05 0.20 0.05 J .-- U 06/21/21 MTM 245.1 R3-94 Nickel, ug/1 0.03 10.0 0.16 J 1.2 J 06/14/21 HMM HPA200.6 Selenium, ug/1 0105 10.0 --- V 0.39 J 06/14/21 HMM SFA200.8 silver, Ug/1 0.22 5.0 --- U --- U 06/14/22 HMM EPA200.0 Thallium, u9/1 0.02 1.0 --- U 0.32 J 06/14/21 HMM EPA200.$ Tin, u1j/1 0.05 100,0 0.11 J --- V 06/14/21 HASM EPA200.8 Vanadium, ug/1 0.04 1.0 --- U 2.3 06/14/21 RMM SPA200,8 zing, ug/1 0.17 10.0 1.2 J 1.9 J 06/14/21 HMM EPA200.8 Sulfide, u9/1 1D0 1000 --- U --- U 04/10/21 LFJ 450092D-11 Conductivity (at 25c), uMhae/Cm 1.0 1.0 528 1155 06/0$/21 SEE 25108-11 Dissolved oxygen, mg/I 0.1 0.1 4.8 0.7 06/00/21 PJC 450000-12 Temperature, 'C 21 19 06/08/21 PJC 255OR-10 Static water Level, feet 12.12 10.00 06/08/21 PJC Well Depth, feet 92.30 23.44 06/00/21 PJC oRP, my +111 +136 06/o$/21 PJe 25808-11 Turbidity (Field). NTV 1.0 i.D --- Ti 10.0 06/08/21 PJC 2130E-11 J . notimated value betwoan tho MDL and MRL, U • B81OW ALL Quantitatiea Limits. Ail QC requirements not mot: M - Method blank exceeded method constant weight criteria. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 Drinking Water iDs 37715 WaatawAtax ID; In 114 OAKMONT DRIVE GREENVILLE, N.C. 2785i CLIENT: C & D DISPOSAL, INC. CLIENT TD: MR. JUDSON WHITEHURST PHONE (252) 756-6208 FAX (252) 756-0633 6003 A 802 RECYCLING LANE ANALYST: HIC CREENVILLE, NC 27834 DATE COLLECTED: 06/08/21 Berge: 1 DATE EXTRACTED: 06/10/21 DATE REPORTED: 11 / 12 / 21 REVIEWED BY: BASE/NEUTRAL COMPOUNDS EPA METHOD 8270E R6(18) Date Analya4d• 06/25/21 06/15/21 mW-1s NW -ID PARAMETRR9, u9/1 MDL MRL 1. Aclbraghthene 2.649 30.000 --- V --- U J . 2eCimat*d value between th* MDL and MRL, V - B¢18W ALL Quantitation Limits. os/1s/21 I o6/ls/ai I ��/�s/ai Mw as } taw.= ` MW-30 --- U I --- U 1 6.92 J DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F�7DCA78DDE63 L'"u W U�IVJ O,�I Drinking water 1D! 37715 Wantawater In: to 114 OAKMONT DRIVE PHONE (262) i5b-62uo GRELNVILLE, N.O. 27858 FAX (262) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: HIC GREENVILLE, NC 27634 DATE COLLECTED: 06/08/21 Page: 2 DATE EXTRACTED: 06/10/21 REVIEWED BY: DATE REPORTED: 11/12/21 BASE/NEUTRAL COMPOUNDS EPA METHOD 8270E R6(18) Data Armlyxed 06/16/21 06/15/21 MW-�D MW-3A PARAMET6R8, ug/1 HDL MRL 1. Acenaphthenm 2.66 10.000 --- u •• u J - Eatimated 'value between the MDL and MRL, U . Below ALL ¢uantitation Limitb. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-Fj7}DCA78DDE63 Ij D�� Drinking Water IDi 27715 �aAxs�rRCeF IDi j,0 114 OAKNION i UIiiVt PHONE (252) 756-6208 GREENVILLE. N.C. 2785E FAX (252) 756.0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JA,P GREENVILLE, NC 27834 DATE COLLECTED: 06/013/21 Page: 1 DATE REPORTED: 11 / 12 / 21 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 82601) R4(18) Date Analyldd 06/11/21 06/16/21 06/11/21 06/11/21 46/10/2} MW-16 KW-1D MW-25 MW-2D MW-35 PARAMETERS, ug/l NDL HIM 1, Chloromethans 0.77 3.000 --- U --- U --- V --- U --- U 2. vinyl Chloride 0.12 0.200 --- U --- U --- T3 --- U --- U 3, eromomethnne 0.67 10.000 --- V --- U --- U --- V U 4. Chloroethane 0.49 10.000 U --- U --- U •-- U --- U 5, Trichlorofluoramethane 0.24 1.000 --- U --- U '•" U --- U --- U 6. 1,1-Dichloroetharts 0117 5.000 --- U-- U -'- U --- U --' U 1, Acetone 9.09 10D,000 9.72 7 --- U ••• U --• U --- U 8. Iodomethans 0.26 10.000 --- ❑ --- U --- U --- U •-• U 9. Carbon Di0ulfids 0.23 100.000 --- U --- U --- U --• U --- U 10. methylens Chloride 0.64 11000 --- U --- U --- U - U •-- U 11. kYirie-1,2-DiohlorosChella 0.23 5.000 --- U V --- V -•-U -- U 12. 1,1-Dich2oroethane 0120 5,000 --- U --- a --- U U V 23. Vinyl Acetate 0.20 50.000 --- U --- U --- U '-- U -"- U 14. Ci9-1,2-Dichloraethene D.25 $.000 --- U --- U --- U -- U --- V 15. 2-Eutanons 2.21 200.000 --- U `-" U --- U '"' U " " U 16. Broma4hloromethans 0.21 3.000 --- V -^- V --- U --- U --- U j1, Chloroform 0.25 5.000 --- V --- U --- U --- U ... U 10, 1,1,1-Trichloroathans 0119 1.000 --- U ^-- V --- V --- U --- U 19. Carbon Tetrachloride 0.04 0.200 --- U --- U --- U --- U --- U 20. Beameae 0.24 1.000 --- U -^- U --- U --• U 0.03 .7 21, 1,2-Dichlaroathane 0.02 0,200 --- U --- U --- U --- U 0.09 J 22. Trichloroethene 0,23 1.000 -`- V --^ U --- U '"' V --- U 23. 1,2-Dichloropropana 0.04 0.200 --- U --- U --- U V 0.04 J 24. Eromodichloromsthane 0.04 0.200 --- u --- V --- U " ' U --- U 25. Cie-1,3-Dichloropropens 0.06 0.200 --- V --- U --- U --- U --- U 26. 4-Methy1-2-F4ntenane 1.19 100.000 --- U ,-_ U -__ V --- U --- U 27. Toluene 0.23 1.000 --- V --- U --- U --- V --- U 26, trans-2,3-DAahloropropens 0,D4 D,200 --- U --- v --- u --- V --- U 29, 1,3,2-Trichlorosthana 0.03 D.200 --- U _ V _-- V _ U U 30. TBtriohloroethsne 0110 0.20D --- U ••- U --- U --- U 31, 2-Hexanond 1.57 50.00D --- U --- U •'- V --- U ."` U 32. Dibromochloromethans D,03 0.200 --- U --- U --- U -"- U --- V 33, 1,2-Dibromcethana 0.03 0.200 --- U --- U --- U --- V --- U 34. Chlorabenzene 0,30 3.000 --- t7 - '0 ••- V •-• U --^ V 35. 1,1,1,2-Tatrachlorosthsne 0.22 1,000 --- U --- U --- U --- V --- U 36. Ethylbanren• 0.21 1.000 ___ U -_- U --- U __ U _-_ U 37. nylenes 0.8$ 5.000 --- U --- U ... V --- V --• U Is. nibromomethana 0.28 10,000 --- V --- U --- U U -t- U 39. Styrene 0,19 1.000 --- U --- U ... U --- U --- U 40. Bromoform 0.20 3.000 --- V --- U --- U •^- V ••- U 41, 1.1,2,2-Tetrachloroathane 0.03 0.200 --- U --- U -" U --` U --- U 42, 1,2,3-TrichloroproPASe 0�09 0.200 --- V --• U `"` V --- U --- V 43, 1,4-Dichlorohnnrans 0.39 1.000 --- U --- U --- U --- U --- U 44, 1,2-Dichlorobontene 0.32 5.000 --- U --- U •-- V --• U --- V 45. 1,2-Dibromo-3-Chloropropene 9.97 0.200 -_- V ••- U -" U " - U -•- U 46, Acrylonitrile 2.72 200,000 --- U U --- U _•_ U --- U 47, trans-1,4-Dichloro-2-eutene 0.42 100.000 --- U --- U -•- U --- U --- U s . satimated value between the NDL and MAL, U r Below ALL Guantitetion Limits. NOTE; EPA METHOD 8260D R4 (18): MW-35 received at pH >2. DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 4 �NLkJJDrinking Water IDt 37725 is 114 OAKMONT DR1VE GREENVILLE, N.C. 27851� CLIENT: C & A DISPOSAL, INC. MR. JLMSON WHIT5HURST $02 RECYCLING LANE GREENV'TLLE, NC 27834 REVIEWED BY; LANDFILL APPENDIX Y7 EPA METHOD 82 6 Oil R4 (18 ) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT Xn: 6003 A ANALYST: JAP DATE COLLECTED: 06/08/21 loge:: 2 DATE REPORTED: 11/12/21 Dot■ Analyzed 06/11/21 04/16/21 06/11/21 06/11/21 06/16/22 Mw-18 HW-1A taw-29 MW-2n MW-39 PARAMETERS, UV/l MVL MRL 49. Aarolsin 1,97 4.000 --- V --- u --- u --- u •-- u 49. Allyl Ctlloride 0.20 10.000 - V --- u `-. a --" u - V 50, Chloxoprene 0,21 20.000 --- V --- u -- u --- V u 51, 1,3-Diohl4robenaene 0.41 5.000 --- V '-- u "-- V •'"" V --- u 52. TichlorodiflUoremethaao 0.51 3.000 --- V --- V --- u --- V u 53. 1,3-Dichloropaopane 0.28 1.000 --- V --- u --- a --- u d 34. 2,2-nichloropxopaae 0.17 15.000 -"' u "'- V --- V - - 0 --- u 55. 1,1-Diohloropropane 0.22 5.000 --- u --- u --- u -- _ D -"- V 56. Ethyl Mathacrylate 0.16 10.000 --- u "- u " ' V -- V --- u $7. Bexachlorobutadiene 0.10 0.200 --- a -- u --- u --- u u so, loobutyl Alcohol 12.80 1001000 --- U --- u --- u --- V --- o $9• MathaCrylpnitrila 1.93 160.000 --- u --- V 60. Nothyl Methacxylahe 0.25 30.000 --- D --- V --- V -'- V --- u 91. Naphthalene 0.47 6.000 --- u --- V --- D --- V 2,02 J 62, Propionitrile 3.26 150.000 --` V --- u --- a _.. V - u 63. 1,2,4-Trichlorobenzens 0.50 10.000 --- u --- V --- V --- u --- u 64. ACatOnitrile 36,29 $5.000 -- u --- V --" u V u 95. Tetrahydroeuran 0.39 1,000 --- u 4.13 V --- u 24.90 66. 1,4-Dioxane 2.71 3.004 4.48 --- u 3.99 --- u 142.00 J ■ Estimated ValUe between rha MDL and MRL, V - Below ALL puantihation Limits. NOTE: EPA METHOD 8260D R4 (l 9): MW-3S received at pH >2. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 ,R]Vfl C [ mI 1JC lid L(n Drinking Water M 37715 wastewater IPz 10 114 OAKMONT DRIVE GREENVILLE. N.C. 2785F, CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY; PHONE (262) 756-6208 r"AX (252) 756-0633 CLIENT ID: 6003 A ANALYST; JAP DATE COLLECTED: 06/08/21 Page; 3 DATE REPORTED: 11/12/21 LANDFILL APPENDIX 11 EPA METHOD 8260D R4(18) Pete Analyzed 06/12/21 06/16/21 06/11/21 :4w-3n MW-2A Trip PARAMST6FS5r U9I1 MDL MRL Blank 1• Chloromethahe 0,77 3.000 --- U "-" V --- U 2. Vinyl Chloride 0.12 0.200 --- U -` U --" U 3. Bromometbane 0.57 10.000 U "'- u --- U 4. Chloroethane 0.49 10.000 --• U `.. U --- U S. Triehlorofluoromethana 0.24 1.000 --- U --- U --- U 6. 1,1-Dichloroethena 0.17 5.000 ••- U --- U ••" U 7. Acotbhe 9.06 100,000 --- U --' U --' U 8, Iodomethmne 0.26 20.000 ^- V ^^- U --' V 9. carbon Disulfide 0.23 100.000 --- 0 --- U '•" U 10. methylene Chloride 0.64 1.000 ^-- U --- U --- U 11, trans-1,2-Dichlorcethene 0.23 5.000 --- U -•• U •-- U 12. 1,1-Dichloroethane 0.20 5.000 --- U --- U --- U 13, vinyl Acetate 0.20 50.000 ••- U --- U --- U 14. Cis-1.2-Dichlor4ettfens 0.25 5.000 --- U --` U --- U 15, 2-Butmnono 2.21 100.D00 ... U -•- U --- U 16. Bromochloromethahe 0.27 3,000 --- U --- U --- U 27, Chloroform 0,25 5.000 --- U -•• U -•- U 18. 1,1,1-Trichlcroothbhe 0.19 1,000 --- U --- U '-- U 19, Carbon Tetrachloride 0,04 0.200 --- U "•• U 20. Donxene 0.24 1.000 --- U --- U --- U 21. 1,2-Dichloroethane 0.02 0.200 --- U 0.05 J --- U 22, Trichloroathene 0.23 1.000 U --- U --- U 23. 1,2-pichloroproptne 0.04 0,200 --- U "-- U --- U 24. Bromodichloromethane 0.04 0.200 - U --• U --- U 25, Cie-1,3-nich2oropropene 0.06 0.200 --- U --- U '-" U 26. 4-Methyl-2-Pentanone 1.19 100.000 •-- V -^^ U " - U 27, Toluene 0.23 1.000 -•- U -`- U •-• U 28. trans-1,3-Dichloroprcpene 0.04 0.200 -•- V "- V --- U 29, 1,1,2-Trichlorcethane 0.03 0.200 --- U --- U ••. U 30. Tetrachlcroethene 0.10 0,200 --- U --- U --- U 9y 2-Bexanone 1.57 50.000 ••• V U - U 32. Dibromochl .6thena 0.03 0.200 --- U --- U --- U 33. 1,2-Dibromvethane 0.03 O.Y00 --- U ... V - U 34. Chlorobenzene 0.30 3.000 --- U --- U '-- U 35. 1,1,1,2-Tetraohloroeth0Lha 0.22 1.000 u •^- u - U 36. Ethylbenzehe 0,21 1.000 --- U --- U ... U 37. Rylonaa 0.66 5,000 --- U --- U ___ ly 18. DibromOM*thane 0,20 10.000 --- U ••- U --- U 39. 6tyrene 0.19 1.000 --• U -•- U - -• U 40. 6romoform 0.20 3.000 --- U --- U --- U 41. 1,1,2,2-T4trachlorcethana 0.03 0.200 ••- U ••. U •-- V 42, 1,2,3-Trichloropccpane 0.09 0.200 --- U --- U ••. U 43. 1,4-Dichlorobanzene 0.39 1,000 ... V --- U --- U 44. 1,2-oichlorobenzene 0.32 5.000 ... U --- U --- V 45, 1,2-nibromo-3-Chlcrcpropane 0.07 0.200 --- U --• U --- V 46. Acrylonitrile 2.72 200,000 --- U --^ V --- V 47, trana•1,4-Pichloro-2-butane 0,42 100.000 ... U ... U -"- U ,1 . Matimated value between the MDL and MRL, U - Below ALL 0uantitation Limits. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 Drinking Wator ID: 37715 WsatGW9t6r ID, 10 114 OAKMONT DRIVE G RELNVILLE, N.C. 27858 CLIENT: C & D DISP08AL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (2521 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: JAP DATE COLLECTED: 06/08/21 Page: 4 DATE REPORTED: 11/12/21 PARAMETERS, ug/1 Date NDL Analy%*d MRL 06/12/21 MW-3D 06/16/21 MW-3A 06/11/21 Trip 81aAk 48. Acrolein 1.97 6.000 --- u -•- t1 --- u 49. Allyl Chloride 0.20 10.000 --- V --- V --- u 50, Chloroprene 0.21 20.000 --- u --- u --- u 51, 1,3-Dichlorobensene 0.41 5.000 u --- u " ' u 52, Diehiorod itIuoram6thA40 0.51 5,000 --- u --- u --- u 53. 1,3-DiChlotaprapana 0.28 1.000 --- u --- u --- u 54. 2,2-DichlorapropAnt 0.17 15,000 --- U ... u --- u 55, 1,1-Dichloropropene 0.22 5.000 --- u --- u --- u 56. Ethyl Nethacrylite 0.16 16.000 --- u --- u --' u 57. HemachlorQbutadiene 0.10 0.200 u --- u --- U 58. laobutyl Alcohol 12,80 100.000 --- u --- u '-- U 59, MOtnacxylonitrile 1.93 100.000 '-- u --- u --- D 60. Methyl Methacrylate 0.25 30.000 --- u --- u --- u 61, Naphthalene 0,47 6.000 u --- u --- V 62. AropioAiteile 3.26 150.000 --- u --- u --- u 63. 1,2,4-Trichlarobenmane 0,50 10.000 --- u --- u -•• u 64. Aoetor+itrile 36.29 55.066 --- u — 65• Tetrahydraturan 0.39 1.000 --- u 5.77 --- u 66. 1,4-Dioxane 2.71 3.000 --- U 41.10 --- u J . Ratimated valµe between the MDL and MRL, U • Below ALL puantitation Llmita- DocuSi 0 r-. { i6 63 co CL co z r.i gn Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 ° i tr C F _Ru{ i aoQ l �4 p7 w sN wn e:F r'M cn t-n C7 , ' 9 T a- o a a m 77 C Q�l mw m m TOTAL CHLORWE, mg11 C7 m m OR uyll AT COLLECTION CC O Q - r N lam+ N cJ TEMPERATURE,°C C m I AT COLLECTION D rn # OF CONTAINERS w .l f11.� 111 Field i + INi Nitrate-Nitrite ;'s{';`, •,i# • of N`{, rs- ;.�';� :::,r ar �:;,;}. rr:Alkglvlity >ro ' Chloride"C ,i• t}f ri4 ti[•.i �r,s.ns S�lif[:'ly. 3Ff: ::;f: "{I 1'IY:a:, . f"9v,` Y i�;:.it:: .. . r� DS l�l/w7 {.r inlr[ '}'1jVl W. Sulfate Y 's1 m m met is � "d 'r>+ �r ;,f.Hi• ..•,.f .' •ti ref{:u �•�'„ :�v y:"}.' :3;, ,.fig. : 5, `'Ff Sulfide 'Ti zi Couductivity C-d DO > ro Temperature 21.} s F'ield Parameter ;:„ :::s '',.'s":' is ,;:. s :her,: §?'s,' ` 8270E Du 1 47 v Irf:{i 8270E Dup. 2 C� ?; 8270E Dup. 3 > C} a:i{.: {,, # ;r; ha #g'a'r##: •. 8260D App. 11 a PARAMETER51TE6TS � IL z am "14�/7 C7 m = o _ L m { rn a z �j N G5 F u1 p A i DocuSi 8 Ei m 0 m G5 z f�1 gn Envelope ID: If \6\F6D1F1B-631D-46D2-975A-F7D�CA78DDE63 ° Cl n -0 n y4 r 4 On m m 4 C17 2 C) r µ all U f4 l C7 p {n rn TOTAL CHLORINE, mgll OR ug11 AT COLLECTION U L L C7 .•r h•1 { ' � 4 n -- [`# �" N C� N C� TEMPERATURE, °C < — N t-} N — AT COLLECTION 4 " G-' # OF CONTAINERS M,}: 8260D App. 112 n C� i7r 8264D Am . 11 3ORP Cs }� hrrl V s r ^k ;. • s'i f` 827UF' B/N G) m m •.. m 9 a t •q � C � O n $ c, _am PARAMETERSITE5T5 U L L 4 J T m 9 G7 ( o m r} D m =o „ m F � � -i ,� ¢ � rrn^• � Cj Ci o rjA w DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 EIM201MR010 % J1M9@rP@T&"d GREENVILLE, N.C. 27858 C & D D19POSAL, INC. MR, JUDSON WHITZHURST 802 RECYCLING LANE GREENVILLE, NC 27834 Drinking Water ID, 37715 Wastewdtr4r ID: 10 Yp#: 6003 DATE COLLECT$D: 06/09/21 DATE REPORTED : 11/12/21 REVIEWED BY: MW-5 MW-6 KW-7 NW-8 'Trip Analysis Method Blank D&te Analyst Cade PARANSTSRS MDL MRL 6,6 6.$ 6.6 05/09/21 SEE 4500HR PH (field measurement), Unite 6.7 2.35 31.60 06/11/21 Ras 353.2 Nitratm+Nitrits as N, Mg/1 0,04 0.04 --- U 7.10 008 06/14/21 DIS 232D8- Alkalinity (to pH 4,S), mg CaCO3/2 1.0 1.0 312 665 275 106 06/14/21 JMa 4500C1 Chloride, mg/1 5.0 5.0 37 23 19 M 390 M 1400 ❑$/10/21 CAW D5997- Total niesalvsd Residua, mg/ 1 1.0 10 M 6D0 M 810 176 06/16/21 LYJ 45048( sul4sfke, mg/1 $.0 5.9 165 64.4 39.0 0.14 7 0,74 J 09/14/21 HMM EPA20f Antimony, ug/l 0.03 1.0 0.34 J 0.21 J 1-1 J 7.9 Arsenic, u9/1 0.06 5.0 1.7 J 1.1 J 180 340 06/14/21 HMM EPA20( Earidm, u9/1 0,04 10.0 264 309 0.0$ J 0.04 J 05/14/21 HKN HPA201 Beryllium, ug/1 0.02 1,0 0,02 J a.08 J 0.06 J 06/14/21 HMM BPA201 Cadmium, ug/1 0.44 1.0 0.05 J 4,16 J 0.05 J 3.6 06/14/21 HMM 911A201 Cobalt, mg/1 0.02 1.4 1.0 1.9 1.6 11,4 06/14/21 HMM F-PA20, TotalChromium, u9/1 0.12 5.0 3,2J 2.0.7 3.2J 1.3 J 06/14/21 HNM 9PA24 copper, rs ug/1 4.44 10.0 1.6 J 1.5 J 1.211 8131 06/17/21 LFJ BPA20 Iron, ug/1 4,96 50.0 1511 266 2111 16 469 06/17/21 LSJ EFA20 NanganRser ug/1 0.31 10,6 ill 452 0.06 J 0.16 J 0.10 J 06/14/2l HMM EPA20 Lead, ug/1 0.03 4.0 0.26 J 0.46.7 - U 06/21/21 MTM 245.1 Mercury, 4.45 0.30 --- V 0.051 1,1 J 0.76 J 1.61 / /21 HMM 06 14 SPA20 sr/l Nickel, ug/1 0.03 10.O J 4.39 J 1.1J Ofi/14/21 HNM gPA24 selenium, ug/1 0.05 1d.6 0.40 J .40 0.49 J U 06/14/21 HMM EPA20 Silver, ug/l 0.22 5.0 --- ❑ ,-_ U 0.10 J --- D 0.06 J --- 0.111 06/14/21 HMM 2PA20 Thallium, 49/1 0.02 1,0 0.08 J U 06/14/21 RXM EPA20 Tin, u9/1 0.05 100.0 --- U --- V --- V 1.1 --- 1.4 06/14/31 HMM F*PA20 Vanadium, u9/1 0.04 1.0 1.1 1.1 1.4 J 1.$ J 06/14/21 HMM HFA20 zinc, ug/1 0.17 10.0 2.2 1 1.2 J U 06/10/21 LFT 45DOE 8ulCide, u9/1 200 1000 --- D --- U 1380 --- ❑ 74B --- 2265 06I09/21 SHa 2514R Conductivity (at 250), uMhod/cm 1,0 1.0 1027 0.7 1.D 06/09/21 6RD 4500C Dissolved Oxygen, mg/1 0.1 0.1 0.8 2.0 22 06/09/21 SHE 2550E Temperature, °C 23 4,82 20 9.34 21 7.36 8.1B 06/09/21 6S8 Stater ware, Level, Peet 9,50 16.65 16.33 20.20 06/09/21 SHE Well Depth, feet fi105 +146 46/09/21 fists 25841 ORR, my +103 +92 2.7 7.9 6.1 06/09/21 SES 21307 Turbidity (PLuld), NTV 1.0 1.0 5.4 .7 . Sstimated Value between the MDL and MRF., V + Below ALI, Quantitation Limits - All QC rc(luiremenls not Hlet: M - Method bland: exceeded method constant weight criteria. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 wa.esvi�Ae.r ia� 1Q 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID; 6003 MR. JUDSON WHITEHURST $02 RECYCLING LANE ,ANALYST: HIC GREENVILLE, NC 27834 DATE COLLECTED: 06/09/21 DATE EXTRACTED: 06/10/21 � DATE REPORTED: 11/12/21 REVIEWED BY; BASE/NEUTRAL COMPOUNDS EPA METHOD 8270E R6(18) Date Analysed: 06/15/21 D6/16/21 06/16/21 06/16/21 MW-5 Mw-6 MW-7 MW-8 PARAMETERS, ug/l MDL MRL 1, Acenaphthane 2.6E 10.000 --- u --- u " ' U --- u J . Datimated value hr.rwuon tlic MDL and MRL, U - Eel,dry ALL QURntltat14n Limita. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 Euwkoo Iffold % h(ompamU4 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. ,7LIDSON WHITERURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY; LANDFILL Z,PPENDIX 11 EPA METHOD 8260D R4(18) "07-:R '.PTV • PHONE (252) 756.6208 FAX (252) 756-O633 CLIENT 1D: 6003 ANALYST; TAP DATE COLLECTED; 06/09/21. Page: 1 DATE REPORTED: 11/12/21 PhRAMETERS, ug/l ante MDL Analyzed MRL 06/12/21 Mw-5 06/l2/21 NW-6 06/12/21 MW-7 06/16/21 MA'-8 06/11/21 Trip Blank 1, Chloromethane D.77 3.000 --- U --- U --- U --• U -^- U 2. Vinyl C1110ride 0.12 0.200 --- U -_- U - U --- U --- U 1, Brpmomethane 0,97 10.000 _- U -•- U --- U ••. U --- V 4. Chloroathane 0.4B 10.000 --- U --- U --- U --- ❑ --- U $. Trichlarcfluoromethane 0,24 1.000 =-- U --- U --- U ^-- U --- V 6. 1,1-nichloroathene 0.17 5.000 --- U --- U •-- V --- U --- U 7. Acetone 9.06 100.000 --- U --- U --• U --- U --- U S. Iodomekhane 0.26 10-000 --- U --- U ••• U -" U --- U 9. Carbon Dieultide 0.23 100.000 --- U -•- V -•- U --- U -'- U 10. Methylene Chlorid9 0.64 1,000 --- U --- U ••- U --- U --- U 11. trans-1,2-Dich1oroethene 0121 S.DOD --- U •-- U --- U --- U --- V 12. l,l-Diehloroethane 0.20 5.000 --- U --- U ••• U --- V --- U 13. vinyl Acetatia 0,20 50.000 --- Ti ... U --- U --- U --- U 14, Cie-1,2-Dichlorvsthene D.25 5,000 --- U --- U --- U --- U --- U 15. 2-Butanan■ 2,21 100.000 --- U ••. U --- ❑ __- U .-- U 16, Bromochlorvmethant 0.27 3,000 --- U --- U " ' U --- u --- U 17. Chloroform 0.29 5.000 --- U --- U -•• U --- U `-` U 19. 1.1,1-Trichl9r0atR4ne 0.19 1.000 --- U --- U --- U --- U --- U 19. Carbon Tetrachloride 0.04 0.200 -• U V --- U --- U -" U 20. Benzene 0.24 1.000 --- V --- U --- U --- U --- U 21, ;,2-Dichloroethane 0.02 0.200 --- U --- V --- U 0.02 d ••• U 22. Trichlorosthene 0.23 1.0D0 --- V --- U --- U --- U --- U 23, 1,2-Diohlaropropane 0.04 0.200 --- U --- V --- U --- U ••. U 24. BrpmodiLchloromethane 0.04 0.200 --- U --- U --- U --- U --- U 25, Cie-1,3-Dichloroprvpene 0.06 0,200 --- U --- U --- U --- u -•• U 26. 4-Methyl-2-Pentanone 1.19 100.000 --- U --- U --- U --- V --- U 27. Toluene 9.23 1.000 --- U --- U ^-- U --- U --- V 28. tra-na-1,3-Diehlvcvpropene 0.04 0.200 --- U --- U --- U "•- U --- U 29. 1,1,2-Trichloroethane 0.03 5,200 --- U --- U •-- U --- U --- V 30, Tetrachloroethene 0.10 0.200 --- a -" U --- U --• U --- U 11. 2-Hexanone 1.57 50.000 --- U --- U --- V --- U -'- V 32. Dibromcchloromethag0 0.03 0.200 --- U --^ U --- U --^ U --- U 33. 1,2-Dibromoethane 0.01 0.200 --- U --- U ••- V --- U ^-- U 34. Chlorobenzene 0.30 3.060 .-- U --- V •-- U -_- U --- U 35. 1,1,1,2-Tetrachlorouthane 0.22 1.000 --- a ... V --- U --- U --- U 36. Bthylbenk;tMe 0121 1.000 U --- U •-- V U U 37. %ylenes 0.69 5.000 --- U --- U --- U -_- U --- U 39, Pibrpmomethane 0.28 10,000 U ... U - U --- U --- U 39. styrene 0.19 1.000 --• U --- U --- U --- U --- U 40. Bromoform 0.20 3,V00 --• U --- V --` U --- U --- U 41, 1,1,2,2-Tetrachlaroetihaae 0.03 0.200 --- U --- U --- U ... V '-- U 42. 1,2,3-Trichloropropene 0.09 0.200 --- U --- U --^ U --- U ••• V 43. 1,4-Dichlvrvbenrarie 0.39 1.000 --- U =-- U --` U •-- U --- U 44, 1,2-DichlDrobenzena 0.32 5.000 --- U --- U --- U --- U --- U 45. 1,2-Cib.CQMQ-3-Ch10ropr9Pane 0.07 0,200 --- U --- U ••- U - U _ ❑ 46, Acrylonitrile 2.72 200,000 --- U --- U --- U --- U --- U 47. trans-1,4-Gichloro-2-Butene 0.42 100.000 --- U --- U -•- 0 =-- V --• U a + Estimated value between the NDL and MRL, U - Below ALL 4uantitation LimitR. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 km'kubif &N� % k�@Tpo 9- T as, hd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 v REVIEWED BY: LANDFILL APPENDIX 11 EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: JAP DATE COLLECTED. 06/09/21 Page: 2 DATE REPORTED: 11/12/21 PARAMETERS, ug/l Date MDL Analyzed NRL 06/12/21 MW-5 06/12/21 MW-6 06/12/21 MW-7 06/16/21 MW-8 06/11/21 Trip Blank 48. Acrolein 1.97 4.000 --- U --- U --- U --- V - U 4B, a11yl Chluride 0.20 10.00D --- U --• 0 --- V --- U --- U 50, Chloroprene 0.21 20,000 -`- U --- U ••. U --- U ... U 51. 1,3-Dichlorobenaane 0.41 5.000 --- U ••• U --- V --- U --- U 52. DighIcrodifIuoYvmetnane 0.51 5,000 --- U --- U --- U --- v --- U 93, 1,3-Dlghlargprapane 0.28 2.000 --- U -•- U --- U -^- U --- U 54. 2,2•Dichloraprapane D.17 15.000 --- V .-- U --- U --- U --- U 55, 1,1-nichloropropene 0.22 5.000 --- U --- U --- U --- U ••• U 56. Ethyl Mrthherylate 0.16 10.000 --- V ... U --- U --- U ^-- V 57, KeXaghlorobutmdieee 0.10 0.200 --- U --- U "-- U --- U ••• U 50. laobutyl Alcohol 12.80 100.000 --- U --- U --- U --- U --- U 59, Q'athacrylonitrils 1.93 100.000 --- U --- U --- U --- U •-• U 60. Methyl Methacrylate 0.25 3D.000 --- U --- U --- U ^-^ V --- U $1, Naphthalene 0,47 6,000 --• U --- U .-- U --- U -•• U 62. Propiandtrile 1.26 150.000 --- U --- U --- U •^- U --- U 63, 1,2,4-Trichlorobenxene 0.50 10,000 U --- U --- U U --- U 64. Acetanitrile 36.29 55.000 --- U --- U --- U """ U --- U $5. Tetrahydrofurat7 0.39 1.000 1.40 2.$2 3.50 10.90 --• U 66, 1,4-Dioxane 2.71 3.000 16.60 19.70 3.53 79.0U --- U S - Estimated value between the MDL And MRL, U - below ALL Quarttitatd6n Limits. In Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 C, r ]Fn 1 ' da44 4N inzi en 2 0(� 0 w❑ 4 J) Q o -� a W z ifr � es m -a �o xJ TOTAL CHLORINE, mgll d OR ugll AT COLLECTION �••` rn m IM z G r7 M TEMPERATURE,°C o � T m AT COLLECTION m n G' P 4 OF CONTAINERS m z 4 w w w cn 0} ,6 s},' Field 01 b Nitrate-Nitrite ME,Y S} Ir V Q Chloride f m m 'I'd m vrs> s'€:;;` ..,. Sulfate Metals 11 WIN 0 s iF1.Sulfide ifit�Y##•ki ;?:} `;.: cpndUetivitV Fes) rn smwd #:1 j° DO gv Temperature > `b Z3$3 r h' i ii:f{ a =:Y,,, Sr , s� Fie Id Parameter 5� 3r#i cr�,;sr. :,; u8270E Dup. 1 _ 8270F, Dup. 2 G� .' 8270E Dup. 3 > .: u zlr ; €: s5 a:s •`# 8260D App. II �*► n PARAMETERSITESTS, e, rn , Fn 1I n m c� z Crn7 � CD PR �f ' A cT, I..r' r�7 p An �y rn I w C-} �' lI � [rs 2 m � Co SiFH Z 4 2 O M a DocuSign Ern elope ID: 6F6D1F1B-631D-, N 2 o m 0 n m I'm m 46D2-975A-F7DU 78DD E63 �E WEEMEMEMEMMEM t u L T c� mz M m 1N � p a cn Crj P-t [ r 0 eb W CA C�7 i�i d RZ ry O LQ r�0 y J a � c. w m Z w m TOTAL CHLORINE, mgJ j� v OF ugll AT COLLECTION TEMPERATURE,'C O AT COLLECTION #OFCONTAINERS z 8260D App. 8260D AppAl 3 CC� 8264D APP. iI 4 G3 O RP 'tl 8270E BIN' C7 C PARAMETERSITESTS 0 'o L Q �u C7 co z m m m rn G7 m Q iF Z � aC N O DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 �L 114 OAKMONT DNIVE GREENVILLE, N.C. 27858 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE CREENVILLE, NC 27834 Drinking Water IDr 37715 WaBtew¢ter I,D: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 6003 c DATE COLLECTED: 06/09/21 DATE REPORTED : 11/12/21 REiiIEWEU BY: SW-1 SW-2 9w-3 SW-4 Trip Analysis Method PARAMETERS MDL MRL clank Late Analyst Cade PH (field measurement), Units 7.0 MISSING MISSING 6.6 o6/09/21 SEE 4500HB-11 Antimony, ug/1 0.03 1.0 0.20 J MISSING MISSING 3.08 J 09/14/21 HMM SPA200.8 Arsenic, ug/1 0.0E 5.0 2,3 J MISSING MISSING 0.55 J 06/14/21 HMM EPA200.8 DArium, ug/1 0.04 10,0 123 MISSING MISSING 103 06/14/21 HMM aPA200.9 Beryllium, u9/1 0.02 1.0 0,01 J M1218ING MISSING 0.14 J 06/24/21 HMM EPA200.8 Cadmium, ug/1 0.04 1.0 --- U MISSING MISSING --- D 06/14/21 HMM 9PA200,6 Cobalt, u9/1 p.02 1.0 0.36 J xiaSING MISSING 0,74 J 06/14/21 HMM EPA200.B Total chromium, u9/1 0.12 5.0 3.51 MISSING MISSING 0.90.7 04/14/21 HMM SPA200,9 Capper, ug/l 0.04 10.0 0.82.7 MISSING MISSING 0.45 J 06/14/21 HMM EPA200.8 Lead, ug/l 0.03 5.0 0.34 J MISSING MISSING 0.50.1 06/14/21 HMM EPA200.S Hiekel, ug/l 0.03 30.0 0.6B J MISSIN4 MISSING 0,55 J 06/14/21 HMM EPA200.8 Selenium, ug/l 6.05 10.0 0,15 J MISSING MISSING 0.19 J 06/14/21 HMM EPA200-$ Silver, ug/l 0.22 5.0 --- V MISSING MISSING --- V 06/14/21 HMM EPA200.0 Thallium, u5/1 6.02 1.0 0,10 J MISSING MISSING 0.10 J 06/14/21 HMM HPA200•a vanadium, ug/1 0.04 1.0 1.4 MISSING MIBSTNG 1.4 06/14/21 HMM EPA200.8 Zino, ug/l 0.17 10.0 3.1 J MISSING MISSING 2.4 J 06/14/21 HMM EPA200.B Conductivity fat 25C), uMhee/cm 1.0 1.0 530 MISSING MISSING 162 06/09/21 San 25106-11 Dissolved oxygen, mg/1 0.1 0.1 5.3 MISSING MISSING 6.2 06/09/21 SEE 45000G-11 Temperature, 'C 26 MISSING HISSING 26 06/09/21 SHU 2550E-10 E250 (duplicate) MISSING MISSING 9260 (duplicate) MISSING MISSING ORP, my +01 MISSING MISSING +56 06/05/21 SEE 25B0B-11 Turbidity (Fields, NTU 1.0 1.0 9.3 M1891NG MISSING 10.2 06/09/21 BOB 21308-11 All QC requirements were not met% M Blank result excooded method constant woight criteria. J • Estimated value betWoon the+ MDL and MRL, U . Below ALL puantitatiOn Limits. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 �[Nmwpo' 00 �mi"&do Drinking Water TD: 37715 Waet;ewatex ID: 10 i14 OAKNIONT ❑RIVE GREENVILLE, N.C. 27858 CLIENT- C & D DISPOSAL, INC. MR. JUDSON WHITEHUR8T 802 RECYCLING LANE GREENVILLE, NC 27834 w.. REVIEWED BY; LANDFILL APPENDIX ZI EPA METHOD] 826 0D R4 (18 ) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 C ANALYST: JAP DATE COLLECTED: 06/09/21 Page; 1 DATE REPORTED: 11/12/21 ❑ate Analysed 06/12/21 05/12/21 06/11/21 sW-1 9W-4 Trip PARAMETERS, a$/l MUL MRL Blank 1. Chloromethans 0.77 3.000 --- u --- u '-- u 2. Vinyl Chloride 0.12 0.200 --- u --- u --- V 3. Bromomethmne 0.67 10,000 u --- u -- u 4. Chloroethaae 0.42 10.000 --- u --- u " - V S. Trichlarofluoromethane 0.24 1.000 --- u --- u --- u 5. 1,1-Dichloroethane 0.17 5.000 --- u --- V --- t) 7. Acetone 9,06 100.000 --- u --- a --- u 9. 14domethans 0.26 10.000 --- u --- u --- u S. Carbon Dis171Pide 0.23 100.000 --- u --- a --' u 10, Methylene Chloride 0.64 1.000 --- u --- a --- u 11. trans-1,2-Dichloroethen■ 0,33 5.000 --- u --- U --- u 12, J,1-Dichloroethane 0.20 5.000 --- u --- u --- u 13. Vinyl Acetate 0,20 50.000 --- u --- u --- u 14. Cia-1,2-0ich2oroethane 0.25 5,000 --- a --- u --- u 15. 2-Butanone 2,21 100.000 --- u --- u --- u 16. Hromochloromethane 0.27 3.000 --- u --- u --- u 17. Chloroform 0,25 3.ODO --- u --- u --- V 1$. 1,1,1-Trichloroethane 0.19 1.000 --- V --- u --- u 19. Carbon Tetrar111oride 0.04 0.200 --- u --- u -- u 20. gengans 0.24 1.000 -- a --- u -'- u 21. 1,2-Dichloroethane 0.02 0.200 -- u --- u `"- u 22. TWLChlproethene 0.23 1.000 --- a --- u ^- u 23. 1,2-Dichloropropana 0.04 0.200 -- u --- u --- u 24. BrpmodichloromathAne 0.04 0.200 --- u -"- u '- u 25. Cis-1,3-Pichloropropene 0.06 0.200 --- V --- u --- u 26, 4-methyl-2-Pantanone 1.19 100.000 --- u '-- u --- ❑ 27. TolU•YYR 0.23 1.000 --- u --- u --- u 2$, trans-1,3-Dichloropropene 0.04 0.800 --- u --- tl --- u 29. 1,1,2-Trichloraethsne 0.03 0.200 --- D --- u --- u 10. Tetrachloroethene 0.1D 0.200 --- u --- u -- u 31, 2-HBXanane 1,57 50.000 --- u --- u --- u 12. DibromochIoromethane 0.03 0,200 --- u --- u --- u 33. 1,2-Dibromoathane 0,01 0.200 --- u --- V --- u 34. Chlorobenzens 0.30 3.000 --- V --- u -'" u 35. 1,1,1,2-Tetrachloroetbane 0.22 1.000 --- u --- t7 --- u 36. 8thylbanzene 0,21 1.000 --- u --- u --- u 37, 8ylenes 0.68 5.000 --- u --- u u 38. D4bromamethans 0.28 10.000 - u --- u --- u 39, styrene 0.19 1.000 =»- u --- V --- u 40. Hromoiorm 0.20 3,000 --- u --- V --` u 41. 1,1,2,2-Tetrachloroethane 0.03 0.200 --- u u --- u 42. 1,2,3-Triehloropropans 0.09 0.200 --- u --- u --- u 43. 1,4-Dichlorobenzens 0.39 1,000 --- u " ' u --- u 44, 1,2-Dichlorobenzene 0.32 5.000 --- u --- u '^' u 45, 1,2-Dibromo-3-Ch1orop9opaRe 0.07 0.200 --- u --- u --- u 46. AcrylonitrL20 2.72 2DO.000 --- u --- u --- u 47. Crane-1.4-Dichloro-2-B0tena 0.42 100.000 --- u --- u --- u 7 a Unmated value bitWee4 the MDL and MRL, v - eelaw ALL Ouantitation Limits. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 L Gd� `gyp �1 (Q oTb Drinking Water IDs J7715 Wastewater ID: 10 114 OAKMONT UMVE PHONE (252) 756-6208 GREENVILLE. N.C. 2785P FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 C MR. JUDSON WHITEHURST 802 RECYCLI14G LANE ANALYST: JAP GRgnNVILLE, NC 27834 DATE COLLECTED: 06/09/21 Page: 2 DATE REPORTED: 11/12/21 REVIEWED BY: LANDFILL APPENDIX 11 EPA METHOD 8260D R4(18) Datt Analysed 06/12/21 06/12/21 06/11/21 aw-1 9W-4 Trip PARAMRTBRB, ug/l KDL MRL Blank 4$, Acrolein 1.97 4.000 --- u --- u --- u 49. Allyl Chloride 0.20 10.000 --- u --- u --- u 50, Chloraprane 0.21 26,000 --- u --- u --- u 51. 1,3-DiQhlDrobanmeri# 0.41 5.000 --- a --- u --- u 52. Dichloredilluoromethana 1 0.51 5.000 --- u --- u '-" u 53. 1,3-Dioh1DrupYcn4ne 1.29 1.000 --- ❑ --- u " - D $4. 2,2-Dichloropropans 0.17 15.000 --- u --- u """ u 55. 1,1-Dich2ur4propene 0.22 5,000 --` it --- u --- u 56. sthyl methacrylata 0.16 10.000 --- u --- u --- u 57. Nexachlorobutadiena 0.10 0.200 --- u — u u 59. IiOk�Utyl AldohOl 12.80 100,000 --- u --- V --- u 59. Metht9ryl4nitrile 1198 100.000 --- u --- u --- u 50, WCthyl methacrylate 0.25 30,000 --- Ti — a 61. Naphthalene 0,47 6.000 --- u --- u --- u 62, Prepionitrile 3.26 150.000 --- u --- D --- u 63. 1,2,4-Trichlorobanxene 0.50 10.000 --- u --- u --- u $4. Acetonitrile 36.29 55.000 --- u --- u --- u 65, Tatrahydrofuran 0.39 1.000 --- u --- u --- u 66, 1,4-Dioxane 2.71 3.400 --- u --- ❑ --- u J r Eetimatad valVa between the MDL and mRL, C r gelaw ALL 0vantitaticn Limita. DocuSi( M s a Cr (D �o w m W z 10 c) `O him 0o In Envelope m ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 m �? ��CC ' n � � c P° `� D { c CIS (A t� f! 0-4 c r.. Fri �` o x t"f1C) o-,a tR rp Cr19 Z LA29 � • ( a '7:�j�� r � yi x 1 � N m m' m- w ' Cy m m rn m TOTAL CHLORIDE, Yrgll Q m rn OR ug/l AT COLLECTION `7 TEMPERATURE, C Q [ x l m ATCOLLECTION t �' '' v9 in ' EE Q # OF CONTAINERS � wl Y � yr Field pH � b etals 71 Conductivity "A?': 1'L'lll 1CCat1YrC zi i; 2f7t1 Dup. 182 rr.-. 1J 8260 Dup. 3 8260 Dup. 4 m � 82601) App. 11 $260D App. 112 C� C f ' ' 8260D App, 113 ORP 'C Field Parameter 1 [n c� L PARAMETERS/TESTS y n o m [? m A Ca m 22 M ty 7O M S Z m m m m ' z m p n C, 4 r� Z In 4iS T M O 1T� = T, _ 2 rh m Z n l r DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 -114 OAKMONT DRIVE GREENVILLE, N.C. 2785P CLIENT: C6D DISPOSAL, INC. CLIENT ID; MR. 7=SON WHITEHURST 802 RECYCLING LAME ANALYST; GREENVILLE, NC 27834 DATE COLLECTED DATE ANALYZED: DATE REPORTED: REVIEWED BY:t� _ VOLATILE ORGANICS EPA METHOD 9260D R4 (18) METHOD BLANK RESULTS PHONE (252) 756-6208 FAX (252) 756-0633 6003 A,C ip 06/08/21 - 06/09/21 06/11/21 - 06/12/21 11/12/21 PARAMETERS, u9/1 1. Chloromethana MIDI, XPL Concentration 0.77 3.00 --- U 2. V:Lnyl Chloride 0.12 0.20 --- u 3. Bromomethane 0.67 0.48 10.00 --- u 4. Chloroathane 10,00 --- u 5. Trichlorofluoromethane 0.24 1.00 --- u 6. 1,1-Diohloroethane 0,17 5.00 --- u 7. Acetone 9.a6 100.00 --- u 8. Iodomethana 0.26 10.00 --- u 9. Carbon Disulfide 0.23 100.00 --- U 10. Mathylene chloride 0.64 1.00 --- u 11. trans-1,2-Dichloroethene 0.23 5,00 ---lu 12. 1,1-Dichloroathana 0,20 5.00 --- u 13. Vin 1 Acetate 0.20 50.00 I --- Ti 14. cis-1,2-Dichlorcethana 0.25 5,00 --- u 15. 2-Butsnone 2.21 100.00 --- tT 16, Hzomochloromethana 0.27 3.00 --- u 17. Chloroform 0.25 5.00 --- u 18, 1,1,1-Trichloroathane 0.19 1.00 ---- u 19, Carbon Tatrachlorids 0.04 0.20 --- u 20. Benzene 0.24 1.00 --- u 21. 1,2-Dichloroathane 0.02 0.20 --- tl 22. Trichloroethene 0.23 1.00 --- u 23. 1,2-Dichloropropane 0.04 0.20 --- u 24. Sromodichloromethane 0.04 0.20 --- U 25. cia-1,3-Dichloropropane 0.06 0.20 --- u 26. 4-methyl-2-Pentanone 1.19 100.00 --- V 27. Taivane 0.23 1.00 --- U 28. trans-1,3-Dichloropro ene 0.04 0.20 ---- u 29, 1,1,2-Trichloroathane 0.03 0.20 --- u 30. Totrachloroathana 0.10 0.20 --- u 31. 2-Hexanone 1.57 40.00 --- u 32. Dibromochlorom®thane 0.03 0.20 --- U 33. 1,2-Dibromaathane 0.03 0.20 --- u 34. Chlorobanzene 0.30 3.00 --- u 35. 1,1,1,2 'Tetrachloroethane 0.22 1.00 --- u 36. Ethylbenxere 0,71 1.00 --- u 37. Xylenes 0.68 5100 --- u 38. Dibromomethane 0.28 10.00 -- u 39. Styrene 0.19 1.00 --- Ti 40. nromoform 0.20 3.00 --- V 41. 1,1,2,2-Tetraahloroethana 0.03 0.20 =- 42, 1,2,3-Trichloropropane 0.09 0.20 --- V 43. 1,4-Dichlorabsnzana 0.39 1.00 --- u 44. 1,2-Dichlorobanzane 0.32 5.00 --- u 45. 1,2-Dibromo-3-Chloropropane 0.07 0.20 --- V 46, Acrylonitrila 2.72 200.00 --- u 47. trans-1,4-D14hlaro-2-Butene 0.42 100.00 --- i7 48. Acrolain 1.97 4.00 --- u 49. Allyl chloride 0.20 10.00 --- u 50. Chloroprane 0.21 20.00 - V DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 �HWAI �� oFpco nw,W 114 OAKMONT DRIVE GREENVILLE, Id.C. 2785E CLIENT: C&D DISPOSAL, INC. MR. JuDSON WKITEHURST 802 RECYCLING LANE GREENVILLE, NO 27834 REVIEWED BY' CLIENT ID: ANALYST: DATE COLLECTED: DATE ANALYZED: DATE REPORTED: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS (continued) PHONE (252) 756-6208 FAX (252) 756-0633 6003 A,C up 06/08/21 - 06/09/21 06/11/21 - 06/12/21 11/12/21 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 L �do�o� Flo hwqoowt d 114 O AKMONT DRIVE GREENVILLE, N.C. 2785r1 CLIENT., CSA DISPOSAL, INC. CLIENT YD: MR. JUDSON WHITEHUR5T 802 RECYCLING LANE ANALYST: GREENVILLE, NC 27834 DATE COLLECTED: DATE ANALYZED: LSp,,TE REPORTED: REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) METHOD BLANK RESULTS PHONE (252) 756-6208 FAX (252) 756-0633 6003 A JP 06/08/21 - 06/09/21 ❑6/16/21 7.1/12/21 PARAMETERS, ug/1 MDL MRL Concentration 1. Chloromethana 0.77 3.00 --- U 2. Vinyl Chlorida 0.12 0.20 ---- ❑ 3. Bromomathana 0.67 10.00 --- Y7 4. Chloroathano 0.48 10.00 --- U S. Trichlorofluoromothane 0.24 1.00 --- u 6. 1,1-Dichloroathene 0.17 5.00 --- U 7. Acetone 9.06 100.00 --- v S. iodomethane 0.26 10.00 µ-- U 9, Carbon Disulfide 0.23 100.00 --- U 10. methylane Chloride 0.64 1.00 -- U 11. trans-1,2-niehloroathana 0.23 5,00 --- Tt 12. 1,1-D3ohloroethaYne 0.20 5.00 --- U 13. Vinyl Acetate 0.20 50.00 --- U 14. cis-1,2-Dichlorcathsna 0.25 5.00 ---- C1 15. 2-Butanona 2.21 1.00.00 --- U 16. Bromochloromathana 0.27 3.00 y-- Ti 17. chloroform 0.25 5.00 -- U 18. 1,1,1-Trichloroethana 0,19 1.00 --- U 19, Carbon Tetrachloride 0.04 0.20 --- U 20. Benzene 0.24 1.00 --- U 21, 1,2-1)ichloroethana 0.02 0.20 --- U 22, TrlLchiproathana 0.23 1.00 --- V 23. 1,2-Dichloropropana 0.04 0.20 --- U 24. Hromedichloromethana 0.04 0.20 --- U 25. oia-1,3-0ichloropropene 0.06 0.20 --- U 26. 4-methyl-2-Fentanona 1.19 100.00 --- U 27. Toluene 0.23 1.00 --- U 28. trans-1,3-DJchloropropene 0.04 0.20 --- u 29. 1,1,2-Trichloroethana 0.03 0.20 --- U 30. Tatrachloroathene 0.10 0.20 -- ❑ 31. 2-Hexanone 1.57 40.00 --- Ti 32. Dibromoehloromathane 0.03 0.20 --- U 33. 1,2-Dibromaethans 0.03 0.20 ---- u 34. Chlorobenzene 0.30 3.00 --- U 35. 1,1,1,2-Tatrachloroethana 0.22 1.00 - - U 36. Ethylbenzens 0.21 1.00 --- u 37. xylanes 0.68 5.00 --- U 38. Dibromomathano 0.26 10.00 --- u 39. Styrene 0.19 1.00 --- U 40. Sromoform 0,20 3.00 --- U 41. 1,1,2,2-Tatrachloroethane 0.03 0.20 --- i) 42. 1,2,3-Trichloropropane 0.09 0.20 --- U 43. 1,4-Dichlorobenzene 0,39 1.00 --- U 44. 1,2-Dichlorebenzene 0.32 5.00 --- U 45. 1,2-Dibromo-3-Chlora ropans 0.07 0.20 --- U 46. Acrylonitrile 2.72 200.00 --- U 47. tzana-1,4-11)iehlcro-2-Butena 0.42 100.00 --- U 48. Aorolein 1.97 4.00 --- U 49. A11 1 chloride 0.20 10.00 --- U 50. Chlozoprana 0.21 20.00 --- U DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 J MTOO fla@-O)m� 'd, Ago 00 mW 114 OAKMONT DRIVE GREENVILLE, N.C. 2785E CLIENT: C&D DISPOSAL, INC. CLIENT ID: M, ,JLMSON WHZTEHURST 802 RECYCLING LANE ANALYST: GREENVILLE, NC 27934 DATE COLLECTED: DATE ANALYZED: DATE REPORTED; REVIEWED BY, VOLATILE ORGANICS EPA METHOD 8260D R4 (19) METHOD BLANK REST ITS (continued) PHONE (252) 756-6208 FAX (252) 756-0633 6003 A JP 06/08/21 - 06/09/21 06/16/21 11/12/21 PAPI*MTERS, u7/1 MDL MRL Concentration St. 1,3 Dichlorobenzene 0.41 5.00 --- U 52, nichlorodifluoromethane 0.51 5.00 --- u 53. 1,3-nichloropropane 0.28 1,00 --- U 54. 2,2-pichloropropane 0.17 15.00 - - U 55, 1,1-Diahloropra ens 0.22 5.00 '"" U 56. Ethyl Msthaorylate 0.16 10.00 --- U 57. Hsxachlorobutadisne 0.10 0.20 --- U 58. Iaobutyl Alcohol 12.80 100.00 --- U 59. Methac lonitrile 1.93 100.00 60, Methyl Methacrylats 0.25 30.00 --- U 61. Na hthalsne 0.47 6.00 --- U 62. PrOpienitrils 3.26 150.00 --- V 63. 1,2,4-Trichlorobsnzsne 0.50 10.00 --- U 64. ACatonitrile 36.29 55,00 --- U 65. Tstrahydrofuran 0.39 1.00 --- U 66. 1,4-Dioxane 2.71 3.00 --- U DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CLIENT: C&D DISPOSAL, INC, CLIENT ID: 6003 A,C MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JP GREENVILLE, NC 27834 DATE COLLECTED: 06/08/21 - 06/09/21 DATE ANALYZED, 06/11/21 06/12/21 DATE REPORTED: 11/12/21 REVIEWED BY: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) SURROGATE RECOVERY RESULTS Sample Name Limits 1,2-DCA-d4 T01U0na-d8 4-SEB ( recovery) (% recovery) (% recovery) recovery) Continuing Calibration std. 70-130 95.3 98.9 101 Method Blank 70-130 108 102 94.8 MW-lg 70-130 107 101 97.3 MW-2g 70-130 106 100 98.4 taw-2D 70-130 107 101 97.0 Mw-30 70-130 108 101 98.5 Trip blank (A) 70-130 106 98.6 98.5 MW-4 70-130 109 100 97.5 W-5 70-130 107 99.4 97.8 pg7-6 70-130 108 100 96.5 MW-7 70-130 108 100 97.5 Trip blank 70-130 103 9914 97.2 Sw-1 70-130 107 100 i 96.8 SW-4 70-130 106 98.5 97.5 Trip blank (C) 70-130 108 102 57.6 6003 MW-4 M.S. 70-130 97.8 101 103 5003 MW-4 M.S.D. 70-130 9819 99.4 103 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 klaw'UMER910 I boUpmud 114 OAKMONT DRIVE GREENVILLE. N.C. 27858 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: CLIENT ID ANALY$T: DATE COLLECTED: DATE ANALYZED: DATE REPORTED: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) SURROGATE RECOVERY RESULTS PHONE (252) 756-6208 FAX (252) 756-0633 6003 A I7P 06/08/21 — 06/09/21 06/16/21 11/12/21 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 EIMHUME� (d17 114 OAKMONT DR3VE GREENVILLE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WrHITEHURST B02 RECYCLING, LANE GREENVILLE, NC 27834 REVIEWED BY: CLIENT ID: ANALYST: DATE COLLECTED: DATE ANALYZED: DATE REPORTED: VOLATILE ORGANICS EPA METHOD 8260D R4 (18) MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULTS PHONE (252) 756-6206 FAX (252) 756-0633 6003 A,C JP 06/08/21 - 06/09/21 06/11/21 - 06/12/21 11/12/21 Sample Spiked: Spike Sample Spike Spike Spike Dup. Spike Dup. MS/MSD (6003) AmOuftt Result Result Recovery Result Recovery RFD MW-4 ag/l ug/l Ug/1 (70-130%) Ug/1 (70-130%) (20%) 1,1-Dichloroethene 20.0 --- U 18.15 90.8 19.78 98.9 0.6 Benzene 20.0 --- U 19.05 95.3 20.46 102 7.1 Tr±ohloroethene 20.0 --- U 18.96 94.8 24.34 102 7.0 Toluene 20.0 --- U 19,26 1 96.3 1 20.96 105 8.5 Chlorobenxene 20.0 --- U 1 18.81 1 94.1 1 20.26 1 101 1.4 LABORATORY CONTROL SAMPLE RESULTS Sample Compound: 9pi,ka Amount Ug/1 Spike Result Ti/1 Spike Recovery (70-1g0%) 1,1-Diehloroethene 20.00 21.28 106 Benzene 20.00 21.45 107 Trichloroethene 20.00 20.59 103 Toluene 20.0 1 1,44 107 Chlorobenxene 20.00 1 21.91 1 110 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 114 OAKMONT DRIVE GREENVIUE, N.C. 27858 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WHITEHURST 302 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: CLIENT ID ANALYST: DATE COLLECTED DATE ANALYZED: DATE REPORTED: VOLATILE ORGANICS EPA METHOD 0260D R4 (18) MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULTS LABORATORY CONTROL SAMPLE RESULTS Sample Compound: Spike Amount -Ug/l Spike Result Ug/1 spike Recovery (70-130%) 1,1-Diahloxoethene 20,00 20.13 101 Benzene 20.00 20.49 102 Trichloroethene 20.00 20.77 104 xcluexte 20.00 20.72 104 Chlorohenzene 20.00 20.59 103 PHONE (252) 756-6208 FAX (252) 756-0633 6003 A JP 06/08/21 — 06/09/21 06/16/21 11/12/21 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 � OC�'Q��[ g1W, `d� �r�.o Drinking Water IDi 31715 114 OAKMONT DRIVE GREENVILLE, N.G 27858 C & D DISPOSAL, INC. MR. JUDSON WHITERURST 802 RECYCLING, LANE GREMVILLE, NC 27834 PHONE (252') 756-6208 FAX (252) 756-063 i ID#: 6003 e DATE COLLECTED: 06/23/21. DATE REPORTED : 11/12/21 l REVIEWED BY: MW-9A 14w-10 bsw-11 MW-13 Nw-12a Analysis method FARAMSTEAB NDL MRL Date Analyst Code pH (field measursment), [mite 6.6 6.4 6.7 6.5 6.6 06/23/21 SEE 4500RB Nitrata+Nitrite as N, mg/1 0.04 0104 --- 0 --- U 0.23 --- U --- U 06/24/21 DTL 3S3,2 Alkalinity (to PH 4,5), mg CRC03/1 1-0 1.0 192 990 340 296 740 06/29/21 JM9 212OB- Chlorida, mg/1 5.0 5,0 21 60 19 5 200 06/28/21 CAW 45DUCL Total Dissolved Residue, mg/1 1.0 10 N 550 M 2600 N 130 M 310 m 1600 06/24/21 DNS D5901- 9ulfate, mg/i 5.0 5.0 190 340 30? 16.4 585 06/25/21 LFJ 450090 Antimony, ug/1 0.03 1.0 0.24 J 0.14 J 0.11 J 0.20 J 0.54 J 06/29/21 NAB EPA200 Arsenic, ug/l 0.08 5.0 0.70 J 5.2 6.7 3.0 J 17 07/13/21 NAB SPA200 Barium, U9/1 O.D4 10.0 83.0 344 77.0 31A 371 06/29/21 NAB EPA200 Beryllium, ug/1 0.02 1.0 0.02 J 0.04 J 0,04 J --- U --- U 06/29/21 NAB EPA200 Cadmium, ug/1 0.04 1.D --- [J --- U --- U --- U --- U 96/30/21 NAB EPA200 Cobalt, ug/1 0.02 1.0 0.16 J 1.4 0.80 J 0.43 J 1.5 06/30/21 NAB SPA200 TPtPl Chromium, ug/l 0.12 5.0 0.60 J 15 1.6 J 0.39 J 18 06/30/21 NAB RPA200 Capper, u9/1 0.04 10.0 0.48 J 0.16 J 0.10 J 0.43 J 0,26 J 06/30/21 NAB EPA200 Iran, ug/l 4.96 50.0 3144 1635 18403 3330 7459 06/25/21 LFJ EPA200 manganess' U9/1 0.31 10.0 %53 304 219 21 615 09/25/21 LFJ 9PA200 Lead, ug/1 0.03 5.0 D.21 J 0,10 J 0.04 J 0.51 J 0.20 J 05/29/21 NAB EPA20C D4QrcurYr ug/1 0.05 0.70 --- U --- U --- U --- U --- U 07/12/21 b4TM 245.1 Nickel, ugfl 0.61 10.0 0.55 J 1.4 J 0.75 J 0.20 J 2.3 J 06/30/21 NAB EPA20C Selenium, ug/1 0.05 10.9 0.12,7 1.2 J 0.50 J 0.44 J 0.86,T 07/13/21 NAB EPA20C silver, ug/l 0,22 5.0 0.24 J 0.22 J --- u --- v --- U 06/30/21 NAB BPA20C Thallium, ug/l 0.02 1.0 0.29 J 0.34 .7 0.06 J 0.04 J 0.02 J 06/30/21 NA8 EPA2CC Tin, U9/1 0.05 100.0 0.09 J --- U 014P J --- U 0.10 J 01/13/21 NAB 9PA20C vanadium, ug/1 0.04 1.0 1 8 0.39 J 5 11 06/30/21 NAB HPA201 Zinc. ug/l 0.17 1D.9 4.1 J 1.4 J 1,2 J 2.3 J 1,3 J 06/30/21 NAB APA20C sulfide, ug/1 160 1000 --- V 221 J --- U --- U 169 J 06/2S/21 ;,FJ 4$DD5: Conductivity (at 250). uMhce/cm 1.0 1.0 799 2435 1161 465 2421 06/23/21 866 2510B• Dissolved Oxygen, mg/1 0.1 0.1 0.9 1.3 2.1 0.5 0.7 06/23/21 SEE 45000C Temperature, 'C 19 20 21 23 22 06/23/21 BBB 25506- Statia Water Level, feet 5112 2.54 2.50 6.20 4.03 06/23/21 SEE Well Depth, E9et 23.17 22.73 23.84 20.60 22.93 06/23/21 886 ORPI rev +94 +123 +97 +47 +129 06/23/21 SEE 25BOB- Turbidity (Field), NTU 1.0 1.0 5.4 318 6.4 2,3 2.7 06/23/21 BED 313DE, All QC requirements were not met: N Blank regult exceeded method constant weight criteria. J + Estimated value between the MDL and MRL, U - Be1DW ALL Quantitetion Limits. All QC requirements not mct: M - Method blank exceeded method constant weight Criteria. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 r' I va i1a Q 00 ,� b �N orinking Water ID, 37715 WautewatuE SD: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27W1 CLIENT- C & D DISPOSAL INC. CLIENT SD: PHONE (252) 756-6208 FAX {252) 756-0633 6003 a F MR. JUDSON WHZTEHURST 802 RECYCLING LANE ANALYST: HIC GREE1+]VILLE, NC 27034 ]SATE COLLECTED: 06/23/21 DATE EXTRACTED: 0 6 / 2 9 / 21 DATE ANALYZED: 06/29/21 REVIEWED BY; DATE REPORTED: 11/12/21 SASE/NEUTRAL COMPOUNDS EPA METHOD 6270E 96(18) MW-9A I MW-10 PARAMETHR9, uJ%1 1, Aeenaphthone MDL MRL 2.56 1 10.000 u 3 a Estimated value between the MDL and MRL, v . nalow ALL ¢uantitation Limite. MW-11 I MW-13 1 Mw-12e --- D I .-- u I u DloccuSign EnvelopeID: 6F6D�1`FIB-631D-46D2-975A-F7DCA78DDE63 LLL111111JJJ LLLIII Drinking WatOK IDI 37715 L7 1J IJ IJ l3 LLL!lI LLL!l1111111 LLLSSS W60kOw}p4F 1C7 lfl 114 0AKM0NT DRIVE GREENVILLE, N.0 27858 PHONE (252) 756,6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 B MR. JUDSON WHITEHURST 802 RECYCLTNG LANE ANALYST: JAP GREENVILLE, IRC 27834 DATE COLLECTED: 06/23/21 Page; 1 DATE ANALYZED: 07/02/21 DATE REPORTED: 11/12/21 REVIEWED BY: LANDFILL APPENDIX 11 EPA METHOD 8260D R.4(18) MW-BA RW-10 MW-11 Mw-13 MW-12e (PARAMETERS, ug/1 MDL MRL 1. Chloromethane 0.77 3.000 --- U '-- U --` u - U - u 2, vinyl Chloride 0.12 0,200 - - t! 0,55 --- ❑ - U V 3. BrOMQmethane 0.67 10.000 u --- v --- V -"- u --• U 4. Chiggoethane 0.4$ 10.000 --- u --- --- u --- a --- u 5. TrichlorvEl"romethane 0.24 1.000 --- u --• U --• V --' u ••- u 6. 1,1-Dichloroethene 0.17 5.000 --- V --- u --- u --- u --• u 7. Acetone 9.06 100.000 ___ U --- V ••- U U _'. U H. SOdomethane 0,26 10,000 •-- u --- u --- u --` v --` u 9. carbon nieUlfide 0.23 100,000 --- V ••. u •- u - u - V 10. Methylene Chloride 0,64 1.000 --- V --- u --• IT --• u --- u 11. tran4q-1,2-D1chloroethena 0.23 5.000 --• u --- V •" U --- u --- u 22. 1,1-nichloroathane 0.20 5.000 --- u --- v --- U --- V -•- V l3• Vinyl ACOtatA 0.20 50.000 - u --- V ... U _._ V :- u 14, CiA-1,2-uichloroathene 0.25 5.000 --- U --- u --- U V - - u 15, 2-Euranone 2.21 100.ODD -•- u --- V --- ❑ --- u --- u 26, BVomochloromethane 0.27 3.000 --- u --- u --` U "-- V ••• V 11. Chloroform 0.25 5.000 -•• u -"" V 10, 1,1,1-Trichloroethana 0.19 11000 --- u --- u --- V -•• V "L^ u i9. Carbon Tetrachlorid0 0.04 0.200 --- V --- V u u u 0.24 1,000 --- u 2.12 0.34 S ••• V 1.13 20, Ednzene 0.02 0.200 --- U 0.21 0,64 .7 --- u 0.10 1 21. 1,Z-Diahloroethatsa u - U 22, Trichloroothene D.23 1.040 --- u --- V u 23. 1,2-Dichlarvprppane 0.04 0,200 --- u 0,1$ J --- V --- V 0.06 1 24, Sromodichloromethan0 0.04 0.200 --- u --- U --- u v u 25. Cia-1,3•Djohloropropene 0.06 0.200 "-- u --- U --- V -•• U --" u 26, 4-Mothyl-2-Fentanane 1.18 100.000 --- V --- U u --- u --- u 27. Toluene 0.23 1.000 --- u '-' V -'• V -.- U -^_ U 28. tYansp-1.3-bichlorvpropenu 0.04 D.200 •-- U ^'- u --- U --- V --• u 29. 1,1,2-Trichloroethane 0.03 0.200 --- u --- V ••. U --- u --- u 30, Tetrachloroothene 0.10 0.200 --- U --- u --- u -" u "•• u 31. 2-Hexanbna 1.57 50.000 --- U --- U --- U " - u --- u 32, Dihromochloromethane 0.03 0.200 --- Q 33. 1,2-Dibromoethane 0.03 01200 --- V --- V 34. Ghlorobenzene 0.30 3.000 --- u --- u --• u --- V •-' U 35. 1,1,1,2-Tetrauhloecathane 0.22 1.000 --- u ••. V '-- V "-- u --- u 36, Ethylbenzene 0.22 1,000 --- u --- u --- u -•" V - " U 37, %ylanea 0.68 5.000 ".. V ___ u - u -- u ._- U 39. Dibromomathane D.28 10.000 --- V �•• V •-- u ••• V- u 39. Styrene 0.19 1.000 --- u --- u --- u --- V -•. V 40. Bromoform 0,20 3.000 ... V --- u --- u --- u --- u 4 1,1,Z,2-Tatrachlorpathane 0.43 0.24D --- v -• tr u u1. 42, 1,2,3-TriCh1oroprapane 0.09 0,200 --- u -- u _ -- u -- - V - V 43. 1,4-nichlcrobenzene 0.35 1.000 ••• V •-- u --- u '-- D - u 44, 1,2-DiChl4robenzene 0.32 5,000 --- v --• a --• V -•- u -^- u 45. 1,2-Dibromo-3-chloraprOpane 0.07 0.200 U --- V --- u --- u --- U 46. Acrylonitrila 2.72 200.000 "-- V --- u " - U --- u ::-tene u 47, trans-1,4-Diohloro-Z-9u 0.42 100.000 --- u --- tt -`" U "- V - U 48. Acrolein 1.@7 4.000 --- U --- U "- U --- u --- u .; . Estimated value bltween the MDL and MRL, V • 8614w ALL quantitmtian Limits. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 Drinking WaL-er IDS 37715 WQetewatea Ias 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 R8VTEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID; 6003 B ANALYST; JAP DATE COLLECTED: 06/23/21 Page: 2 DATE ANALYZED; 07/02/21 DATE REPORTED: 11/12/21 KW-9n MW-10 KW-11 H➢7-13 HW-128 PARANSTMR8, ug/l HDL MRL 49, Allyl Chloride 0.20 10.000 --- U --- U --- U --- U "-- Tr 50. Chloreprene 0.21 20.000 --- U --- U --- U "" U '-' U 51, 1,3-Dichlorebenaene 0.41 $.000 --- U --- U --- U --- U --- U 52. Dichlorodi41uoromathane 0.51 5.000 --- U ..__ U --- U --- U •-- U 53, 1.3-bichlcropropane 0.28 1.000 --- U --, V --- U --- U U 54. 2,2-Di4hloropropan■ 0.17 15.000 --- U '-- U """ U--- $5, 1,1-Dichloropropene 0.32 5.000 --- U - U '-- U ••' U L 56, Ethyl Methacrylata 0.16 10.000 •-- U __- U --- U 57. Hexaehlorebutadiene 0.10 0.200 --- U--- U _-- U _-- p -•- U 59, Iaobutyl Alcohol 12.00 100.000 --- U --- U --- U --- U -` U 59. Methacrylonitrila 1.93 100.000 --- U --- U --' U --- U -`- U 60, Methyl HothaCrylate 0.25 30.000 - U ^-- U --- ❑ --- U --- U 61. Naphthalene 0.47 6.000 ___ U --- U --- U --- u --- Ti fit. Prcpicnttrile 3.26 150.000 --- u --- U --- U --- TJ -• U 63, 1,2,4-Trichlbrcbenaene 0.50 14.000 --- U --- U --- U -_- U --- U 64. Aoetonitrlle 36,29 55.000 U --" U --- U --- U ". U 65. TetrmhydrOturan 0.39 1,000 19.50 23.00 5.32 "-- U 13,70 66, 1,4-nioxane 2.71 3.000 --- U 9.32 5.76 --- U 11.10 J = Roti.mated value between the MDL grid MRL, U - Below ALL quahtitAti4n Limits. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 u i1 Wuv oL1 lUJll�1l11JUl5LJ " f llu Amo wvwbu R(W o Drinking Water ins 37715 W&APtewatax SD: 10 114 OAKMONT DHIVE GREENVILLE, N.C. 27858 FAX (252) 758-0633 CLIENT: C & D DISPOSAL, INC- CLIENT ID: 6003 B MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: aAP GREENVILLE, NC 27834 MATE COLLECTED: 06/23/21 DATE ANALYZED: 07/02/21 DATE REPORTED: 11/12/21 REVIEWED BY: � " `~ LANDFILL EPA METHOD APPENDIX TT 8260D R4(18) Trip PARAMETERS, U9/1 MDL EARL 81ank 1. Chlaromethane 0.77 1.000 --- D 2. Vinyl Chloride 0,12 0.200 --- U 3. gromomethane 0.67 10.00D --- U 4, ChloroethMne 0.40 10.006 --- U 5, TrlChlarcflucroMOthane D,24 1.D00 U 6. 1,1-Dichloroothene 0.17 5,000 - U 7, A4etone 9.06 10D.000 •-- U 9. Iodomethane 0.26 10,000 --- U 9, Cerhoa Disulfide 0,23 100,000 -•• U la. Methylene Chloride 0.64 1,000 --- U 11, ttans-1,2-Dichloraethena 0.23 5.000 -•• U 12. 1,1-Dichloroathane D•20 5,000 --- U 13, Vinyl Acetate 0.20 50.000 --- V 14. Cie-1,2-Dichloroethens 0.25 5.000 --- U 15. 2-Eutanone 2.21 100,00a --- U 16. BromochloromethaAe 0.27 3.000 --- U 17. Chloroform 0,25 S,acD --- U 28. 1,1,1-Trichloroethane 0.19 1.000 --^ U 19. Carbon Tatrachlvride 0.04 0.200 --- U 20. Benzene 0.24 1.000 --- U 21. 1,2-Dichloreethane 0.02 0.200 ••• U 22, Trichlorosehane 0.23 1,006 --- U 23, 1,2-Dichloroprbgane 0.04 0.200 V 24. Bromodieh1promethane D.04 0.200 --• U 25, Cis-1,3-Dichlormpropens 0.06 0.200 •^• ❑ 26. 4•MettAy1-2-Pentanone 1.29 100,000 --- U 27, Toluene 0,23 1.000 --- U 2B. tram-A,]-nichloropropene 0.04 a.200 --- D 29. 1,1,2-Trichlornethane 0,01 0.200 ••• U 30. Tetrachlorosthene 0.10 4D.200 --- U 31, 2-Hexanone 1.57 50.000 ^ - V 32. Dlbromochloromethane 0.D3 0,200 --- U 33. 1,2-Dibromoethane 0.03 0.200 --- U 34, ChlorobenzOnC 0.30 3.000 --- U 35. 1,1,1,2-Tatrachloroathane 0.22 1.000 --- U 36. Ethylben%ehe 0.21 1.000 --- U 37. Sylenes 0168 5.000 --- U 38. DibrDmomethane 0.28 10.000 --- U 39. Styrene 0.19 1.000 --- V 40, Aromoform 0,20 3.000 -•• U 41. 1,1,A,2-Tetrachlaroethane 0.03 0.200 --- U 42, 1,2,3-Trichloropropan■ 0.09 0.200 •^- U 43, 1,4-nichlorobenaane 0.30 1,000 --• U 44. 1,2-Dichlorobenzane 0.32 5,000 --- U 45. 1,2-bibromo-3-Cbloropr0vane 0107 0.20e ••• U 46. Acrylonitrile 2.72 200.ODD --- U 47, trana-1,4-Dichloro-2-BUtone 0.42 100.000 --- U 49. Acralein 1,97 4.000 --- U a . EaCimatad value between the KDL and MRL, V . Below ALL quantitation Limit". Page: 3 DioccuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 'r�j�MnT0nf a100,jlll� CII� 6� vrinking 'Water IDi 31715 LL55ULl 11 11 \J LIIJIJ LuJIIJJ l� LI 4 p' Wastav&ter Yd; 10 114 OAKMONT DRIVE GREENVILLE. N.C. 27868 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY:� LANDFILL APPENDIX IZ EPA METHOD 8260D R4(18) PHONE (25,') t 56-6208 FAX (252) 756-0633 CLIENT ID: 6003 B ANALYST, JAP DATE COLLECTED: 06/23/21 Page: 4 DATE ANALYZED: 07/02/21 DATE REPORTED: 11/12/21 PARAMBTSRB, u5/1 DEAL MRL Trip Blank 49, Allyl Chloride 0,20 10.000 --- U 50. Chloroprene 0.21 20.060 --• U 51, 1,3-Dichlorobenaene 0.41 5.000 --- V 52. Dichlorodifluoromethane 0.51 5.000 --- U 53. 1,3-Dichloropropane 0.20 1.000 --- u 54, 2,a-Dichlcropropane 0,11 15.000 --- U $5. 1,1-Dichloropropane 0.22 5.000 --- U 5$, Ethyl Methacrylate 0.16 10,000 U 57. 8exachlorobutadione 0.10 0.200 U 5$, ieobutyl Alcohol 12.80 100,000 --- D 59. Methacrylonitrils 1.93 100.000 --- U 80. Methyl Methacrylate 0.25 30,000 --- u 61. Naphthalene 0,47 6.000 --- U 62. Propionitrile 3.26 150.D00 --- U 63, 1,2,4-Trichiorob anrene 0.50 10.000 --- U 64, Ac4tonitrile 36.29 55.000 --- U 6$. TetrohydrOfuran 0.39 1.000 --- C 66. 1,4-Dioxane 2.71 3.000 --- v J . Matimated value betw"n the MDL and MRL, u - Below ALL 4uantitatiOn [,imite. In Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 o n b a m � lf`aJ O 8 B a -- r� m LON f nkj r nc7Nia aa� CJ �3 ago ) 4 m m w m TOTAL CHLORINE, mg1l m OR ug/I AT COLLECTION TEMPERATURE, "C D C -� ATCOLLECTION t OF CONTAINERS rn :'h N field H a a; € 02. :tv ? ''ss Nitrate -Nitrite C] Alkalinityp <„1�1'. 1s I Chloride TDS`d ffi -7�r rn ��' �;. hg :�,.,r � � s } � Sulfate '° Q aLa ' :€ s:.#?3 ` :, Metals a,, Cs7 Sulfide Conduttivit > DO 'Temperature b .•s^ra U >' ¢ ?' :fir' j}f Field Parameter 8270E Du 1 > GJ V ti i} ti iii} 8274E Dup. 2 :} 8274E Dup. 3 > sE.fYF; '+.S}{'i r111i �� .�rd '�k"md ;' vA', 82601) App. 11 PARANIETEflS1T1:575 rrb A. L L m m ry n v z r- �j 2 p m rn � m � S rn Co z rl zu rn Q � �DocuSi Lh U7 0 CG CO [b CL ca N gn Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 U7 i-+ L•i4' C i ~ p Q v Z C)«- m [=7 F z G7 .,5 G7 r. W 4 � ��yrri Cq oho S o w m m 9j m rn TOTAL CHLORINE, mg/l m R n OR ugll AT COLLECTION a z n Z o U N TEMPERATURE.°C ATCOUECTION rn n FP - co [n z t� z # OF CONTAINERS w 8260D A . 11 2 C�1 82601) App. IC 3 01 m m r m --TT1 PARAMETERSITESTS P' G L Li LD [? a7 2 m E3 m v` ` _= o m x m z 'T' 7 c� cn z a n m m "' �Q — Gi ^ m o W o rL f m L> �N77 m p z o as C w DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 knTwoo nuodn Drinking Water ID: 37715 114 OAKMONT DRIVE GFIF-ENVILLE. N.0 27858 C & D DISPOSAL, INC. MR, JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 PARAMETERB Pk (field meanuremeet), Units Nitrats+Nitrite as N, 149/1 Alkalinity (to pH 4.5), mg CaC43/1 Chloride, mg/l Total Dissolved Residue, mg/1 Total Dissolved Residua, mg/l Sulfate, mg/l Antimony, ug/1 Arsenio. ug/1 Barium, ug/l Beryllium, ug/1 Cadmium, ug/l Cobalt, ug/l Cobalt, Vg/l Total Chromiµm, ug/l Capper, u9/l Copper, ug/l Iran, ug/1 Iron, ug/l Manganese, ug/1 Manganese, ug/1 Lead, ug/l Mercury, ug/1 Nickel, ug/l Nickel, ug/l selenium, µg/1 silver, ug/l 'thallium, ug/1 Tin, ug/l Vanadium, u9/1 zinc, u9/1 Sulfide, ug/1 CohdUetivity (at 250), uMhoe/Cm Dissolved Oxygen, mg/1 T9Ngerature, °C static Water Level, feet Well Depth, feet ORP, my Turbidity (Field), NTU NW-15 MDL MEL 0.04 1.0 5.b 1.0 1.0 5.0 0.02 0.48 0.44 0.43 aloe q.42 0.02 0.12 0.04 0.04 4.96 4.96 Q.31 0.31 0.03 0.05 0.03 0.03 a.05 0.22 0.02 0.05 0.04 0,17 10Q 1.0 0.1 aloe 1.4 5-4 10 1q s.4 l.0 5.4 xa.o 1.0 1,4 1.0 i.o 5.4 10.0 10.0 50.0 50.0 10.0 10.0 5.0 0.20 10.0 10.0 10.0 5.0 1,0 100.0 1.0 10.0 1000 1.0 a.1 KW-16 PHONE (252) 756-6208 FAX (252) 756-8633 ID#: 6003 D DATE COLLECTED: 06/24/21 DATE REPORT= : 11. / 12 / 21 REVIEWED HX: MW-17 MW-14s taw-14D Analysis Method 612 612 5,6 6.6 0.10 --- U 0.04 -•- U 205 $42 10 $90 06 62 --- U 34 M x140 N 1100 N 160 M 1100 542 314 76.1 las 1.6 0.25 J 0.10 J --- U 26 14 0,44 J 2.3 J 507 357 30.0 267 0.12 d 0.06 1 0.06 1 0.02 17 0,051 --- U --- U --- U 4.69 J 0.96 J 0,10 J 0.99 J 30 16 1.1 J 5.4 1.9J 0,18J 0.2J 0.29 J 9476 16181 57833 2670 323 1332 164 106 2.4a 0.20J 0.18J 0.24 J U--- U --- U 1.3 J 0.56 J 0,78 i 1.3 J 1. 6 J 0. 19 J 0. 61 J --- U --- U --- U '-- U 0,23J aloes 0.04J •-- U 0.16 J a.05,7 --- U --- U 10 11 2 2 29 1.517 4.11 1.71 661 J --- U 164 .i --- U 2695 2561 224 1656 1.8 1.1 0.4 2.3 20 23 21 22 5.40 6.50 6.57 1.69 22.14 22.73 22.25 23.12 +102 +122 +56 +202 7,6 3.5 6.1 9.1 All QC requirements WOVO not mats M Blank result Oxceeded method constant weight criteria. J e Estimated value b8tween the MDL and MEL, V + Below ALL Quantitatiad Limits. Date Analyst Code 7.5 06/24/21 PJC 4500H5-11 0.30 06/28/21 TLH 3$3.2 R2-9 244 06/28/21 SMs 232OR-11 16 06/26/22 CAW 4500CLB-11 07/01/21 CAW D5907-13 M 310 06/29/21 DNS D5307-13 --- D 07/02/21 LF.i 4500S042E1 0.19 J 06/29/21 NAB EPA200.8 0.43 1 07/13/21 NAB 8PA200.8 10.5 06/29/21 NAB EPA200,6 --- U 06/29/21 NAB 8PA200.8 V 06/36/21 NAB EPA200.@ -- U 01/13/21 NAB BPA200.B 06/30/21 NAB 6PA200,8 0.21 J 06/10/21 NAB EPA200.8 u.li J 07/14/21 NAB EPA700,9 06/30/21 NAB EPA200.0 06/25/21 LFJ EPA200,7 58 07/06/21 LFJ EPA200.7 06/25/21 LFJ EPA200.7 4 J 07/06/21 LFJ 10eA200.7 0.05J 06/29/21 NAB MPA200.9 --- D 07/17/21 MTM 245.1 R3.9 0.15 J 07/13/21 NAB EPA700,8 06/30/21 NAE NPA200.8 0.06 J 01/13/21 NAB EPA200,8 --- U 06/30/71 NAB 11PA200.9 0.18 J 06/10/21 14AD BPA200.8 --- D 07/13/21 NAB EPA2D0.9 0.14 J 06/10/21 NAB EPA200.8 2.2U 05/30/21 NAB EPA200,6 --- U 06/28/31 LFJ 450052D-11 525 06/24/21 PJC 2510E-11 0,8 06/24/21 PJC 450000.11 21 06/24/21 PJC 2550E-10 5.10 06/24/21 PJC 41.92 06/24/21 PJC +88 06/24/21 PJC 2590E-11 - U 06/24/21 PJC 213OD-11 All QC requirements not met; M - Method blank exceeded method Constant weight critcria. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 Eow'u' Too fi m' IInwp0m. LlAd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 4 REVIEWED BY: PARAMETERS, ug/1 1. Ao*naphthene Drinking water It: 37715 WaatBwAtcr IDi }O a PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: HIC DATE COLLECTED: 06/24/21 DATE EXTRACTED: 06/29/21 DATE ANALYZED: 06/29/21 DATE REPORTED: 11/12/21 BASE/NEUTRAL COMPOUNDS EPA METHOD 8270E W 16) LMW-1S tdW-16 MDL MR 2.66 14.404 --- a --- u J - Retimated value between the MDL and MRL, U - Below ALL RUantitatian Limits. mw-11 1 Mw-14S 1 MW-14I1 ... u I ... u I --- u DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 ,oqm Drinl,ing Water XA; 37715 wastawttor ID: 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GFREENVILLE, N.0 2785P FAX (252) 756-0633 CLIENT; C & D DISPOSAL, INC. CLIENT ID: 6003 D MR. JUDSON WHI"TEHURST B02 RECYCLING LANE ANALYST: TAP GREENVILLE, NC 27B34 DATE COLLECTED: 06/24/21 Page: 1 DATE ANALYZED: 07/02/21 DATE REPORTED: 11/12/21 REVIEWED BY: LADTAFILL APPENDIX II EPA METHOD 8260D R4(18) KW-15 Mw-jr, NW-17 Mw-14r MW-143) PARAMETERS, uj/X MDL MRL 1. Chloromethane 0.77 31000 --- U --- U --- U --- U --- U 2, Vinyl Chloride 0.12 01200 --- U =_- U 3, aromomathane 0.67 10.000 --- U --- V --- D - U - it 4. Chloroothans 0,48 10,000 -- U --' U -"- U --- U , U 5, Trichlorofluoromsth4nO 0.24 1.000 --- U --- U --- tl --- V -- U S. 1,1-Dlghloroethene 0.17 5.000 --- U --- U ___ U --- U --- U 7, Acetone 9.06 100.000 26.60 1 --- U --- V --- V `-- U 0. Iodomethans 0.26 10.000 --- U --- V 9, Uarbon Disulfids 0,23 10o.000 0.27 1 --- V --- U --- U --- U 10. Ha thylene Chloride 0.64 1.000 --- U --- U --- U -•• U - U 11, trans-1,2-Die hlox0*tJlefke 0123 5.000 --- U - " U --- U - U U 12. 1,1-Diehloraoth¢ne 0.20 5.000 --- U -- U --- U --- U --- U 13. vinyl Acetate 0,20 50.000 --- U --- V --- U - V --- U 14. Cis-1,2-Dichloraathens 0.25 5.000 --- U 0.54 1 --- U --- U - U 15. 2-13utanone 2,21 100,000 2.73 J --- U --- U --- 16. Hxgmochl0YOro4thane 0.27 3,000 --- U - U - U U U 17. Chloroform 0.25 5.000 --- U --- U 26, 1,1,1-Triohlorosthane 0.19 1.000 --- U --- U 19, Carbon Tetrachloride 0.04 0.200 --- U -__ U -__ U 20. Benzene 0.24 1.000 --- U 0.25 1 --- U 1.18 U 21, i,2-Dichlaraethane 0.02 0,200 0.03 1 0.19 1 --- U 0.08 1 --- U 22. Trichlorcathans 0.23 1.000 --- U --- U " ' U --- B --- U 23, i,2-Dich2oropropans 0.04 0.200 --- U 0.10 1 --- U --" U 24. br*Mo dithlarom*thane 0.04 0.200 --- U --- U -- -- 9 v 95. cis-1,3-Dichloropr0p*n* 0.06 0.200 --- U --- U --- U "-- U -- U 26. 4-Mathy1-2-Pentanone 1119 100,000 --- U -"- U --- U --- V --- U 27• Toluene 0.23 1.000 0,31 1 --- 1i '-- U --- U --- U 20. trans-1,3-Dichloropropene 0.04 0.200 --- U --- U --- U -'" V --- U 29. 1,1,2-Trichloroethnne 0103 0.20D --- V --- V -'- U --- U --- U 30. Tstrachloxoeth*n$ 0.10 0.200 31. 2-Hexanone 1.57 50.000 --- U --- U -"- U 32. Dibromochloromethane 0.03 0,200 --- U --- U ___ U - U U 31. 1,2-Dibromoethsne 0.03 0.200 --- U --- U --_ U U U 34. ChlorobsnR*ne 0.30 3,000 --- U --- U ___ U ___ U ___ U 15, 1,1,1,2-TstrmChlgroethmne 0.22 1.000 --- U --- U --- U --- V --- V 36, Ethylb*nzene 0.21 1.000 --- U 0.28 d --- U --" U U 37, Xylenes 0.68 5.000 --- V --- U --" 38. Dibromomethans 0.29 10.000 --- U --- U --- V --- U --- U 34. Styrafts D.19 1.000 --- U --- U ___ U --- U --- V 40. Itcemoform 0.20 3.000 --- U --- U - U --- V --- U 41. 1,1,2,2-TeCrachlorpethane 0.03 0.200 --- V --^ U --- U --- U "' U 42. 1,2,3-TrichloroprOpane 0.09 0,200 --- U --- U --- V "-" U --- U 43, 1,4-Dichlorobsnzana 0.39 1.000 -^ V 44. 1,2-Dichlorobenzene 0.33 5.000 --- U --- U 45. 1,2-DibYpmO-3-Chloroyropaee 6.07 0,200 --- U 46. Acrylonitrile 2.72 200.000 --- U --- U --- U --- U "- U 47. trana-1,4-Dichloro-2-butene 0.42 200.000 --- U --- U --- U --- U - U 40. Acrol*in 1.91 4.000 --- U --- U -'- U ... V U j . Estimated valve between the MD1, Arid XRL, U - below ALL Quantitatiaa Limits, DocuSig[�n�71E,n�vlelop`ee IrD:: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 � �y�llll ®IIIIli1111 i � �WooMOW6�� Drinking Water M 3771S # - - lll�� ti! [[[JJJ LLII `llllll llllll LLLJJJ LL�JJ LLLIII -- - - _ -� . V � ` 114 OAKMONT DRIVE PHONE (252) 756-6208 GFIEENVILLE, N.0 27856 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 D MR. J'UDSON WHITEHURST 802 RECYCLING LANE ANALYST, TAP GREENVILLE, NC 27834 DATE COLLECTED: 06/24/21 Page: 2 DATE ANALYZED: 07/02/21 DATE REPORTED?: 11/12/21 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) sew-15 Mw-16 MW-17 04w-14s Mw-i4n PARaM'BTERB , u4/1 MDL �RBL 49. Allyl Chl4rdde 0.20 10.000 =-- U --• u --- U -"- U --" u $0. Chloroprene 0.21 20.000 --- U --- U -'- D --- U - V 51. 1.3-Dich14robanaans 0.42 5,000 U --- u --- u --- U --- u 52. DichlorodiflubroMethane 0.51 5.000 --- U --- u --- u --' u --" u 53. 1,3-Dich2oropropans 0.29 1.000 --- U --- u --- u "-- 13 -_- u 54, 2,2-Di4hlot0Vr0Pane 0,17 25.000 --- u --- 0 --- u --- u --- u 55, 1,1-Diahlorppropene 0.22 5.000 --- u --- U -- u - U --- u 56, Ethyl Methacrylate 0,16 10,000 =-- U --- U --- u --- u --- ❑ 57. Hexaehlorahutadiene 0.10 0.200 --- u --- u --- U --- U --- V 58. Imobutyl Alcohol 12.80 100.000 --- u ._. U .." U --- U ••_ U $9. Mathaorylonitril■ 1.93 100.000 --- u _ u _ - u a ^- u 60. methyl Mathacrylate 0.25 30.000 --- t1 --- U ""- u --- U - u 61. Naphthalene 0.47 6.099 .._ U --- D --' T1 ..` U u 62, Prppionitrile 3.26 150,000 --- U --" u --- u V _-- U 63. 1.2,4-Triahloxobenaens 0.50 10.000 --- u --- ❑ --" U - U u 64, ACatonitrile 36.29 55,000 --- u --- U --- u --- ❑ --- u 65. TetrahydrofuxaA 0.39 1.000 6.82 2,ep 3,62 12.90 •-- u 66. 1,4-Diaxane 2.71 3.000 5.19 54.40 --- u U . Estimated value between the MDL and MAL, U . Below ALL Quantitation Limits. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 Em'HOMSM �fj 4NQ 00 0 Drinking Water lDt 37715 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVI►.LE, N.C. 27858 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 D MR. JTMSON WHITEHURST 802 RECYCLING LANE ANALYST: J'AP GREENVILLE, NC 27834 DATE COLLECTEA: 06/24/21 Page: 3 DATE ANALYZED: 07/02/21 DATE REPORTED: 11/12/21 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4 (18) PARAMETERS, ag/l MDT, MRL Trip 91Ank 1, chloromethane 0.77 3,000 --• V 2. Vinyl Chloride 0.12 0.200 --- U 3. Eromamethana 0.0 10.000 U 4. Chloroethane 0.40 10,000 •-- U 5, Trichlarofluonomethans 0.24 1.000 --- U 6. 1,1-Diehlaroethsne 0.17 5.000 --- U 1. Acetone 9.06 100.000 --- U B. IOdomethane D.26 10,000 --- U 9. Carbon Disulfide 0.23 100.000 --- U 10, Methylene Chloride 0,64 1.D00 --- u 11. trono-1,2-Dichlaroethene 0.23 5.000 --- U 12. 1,1-DiCh14roeth8ne 0.20 5.000 --- U 13. Vtr?yl Acetate 0.20 50.000 --- U 14. Cie-1,2-Dichloroethane 0.25 5.000 --- U 15, 2-Eutanone 2.21 100.00D --- U 16. @romOChloromethana 0.27 3.000 --- U 11, chloroform 0.25 5.000 --- U 10, 1,1,1-Trichloroethane 0.19 1,000 --- V 19. Carbon Tetrachloride 0,04 0.200 --- U 20. Eenxens 0.24 1.000 --- U 21. 1,2-Dichloroethane 0.02 D.200 --- U 22, TrichlorusthOAe 0.23 11000 --- U 23. 1,2-Diehloropropans 0.04 0.200 --- U 24, Bromodichlorcmothans 0.04 0.200 --, U 25. Cia-1,3-DichloroprOpsne 0.06 0.200 --- U 26. 4-Methyl-2-pomtanone 1.19 100.000 -•- U 27, Toluene 0.23 1.000 .•• U 20. trans-1,3-Dichloropropsna 0.04 0.200 --- U 29, 1,1,2-Trichloroathane 0.03 0,200 U 30. TSCraohlcroethens 0.10 0.200 --- U 31. 2-HexanoAe 1.57 50.000 --- U 32, Dibromochloromethana 0.03 0.200 --- U 33. 1,2-Dibromoethans 0.03 0.200 --- U 34. phlorobanzene 0.30 3.000 --- U 35. 1,1,1,2-Tstrauhlorosthane 0,22 1.000 --- U 36, Ethylbenzene 0.21 1.000 --- U 37, xylonea 0.69 5.000 --- U 38. Dibromomethane 0.2a 10.DOD --- u 39. Styrene 0.19 1.000 •-- U 40. BxOmolorm 0.20 3.000 --- U 41. 1,1,2,2-Totrachloroethans 0,03 0.200 --- U 42, x,2,3-Trichloropr0pem0 0.05 0.200 --- U 43. 1,4-Dichlorobentens 0.39 1.000 --- U 44. 1,2-Dichlorobsri2ene 0.32 5.000 --- U 45. 1,2-Dibromc-3-Chloropropane 0.07 0.200 --- U 46. kcrylonitrile 2.72 a00,000 --- U 47. trans-1,4-Dichloro-2-Butene 0.42 100.000 ••. U 4E. Acrolein 1,97 4.000 --- U J . Estimated Value between the MPL and MRL, V - Below ALL QuantitatiOn Limitg. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 . J U 1 j' - I � Y p I (�'1 fl �}j ` nl r��r�j�1 11 II� III[II{[� UU U i� U @R0 Drinking Water IDS 37715 LLl1LLII L! ULI lJ LJLILI uuuuuulll��1 LLU uuuuuv v wastewater 1D: la 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. =SON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PRONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: JAP DATE COLLECTED: 06/24/21 Page: 4 DATE ANALYZED; 07/02/21 DATE REPORTED: 11/12/21 PARAMETERS, u911 MDL MR71 Trip Blank 49. Allyl Chloride 0.20 10,000 --- U 50, Chloroprsne 0.21 20.000 --- U 51. 1,3-Aichlorohansene 0.41 5.000 --- U 52, nichlarodifluoromethane 0.51 5.000 -•- U 53. 1,3-Piehloropropane 0.25 1.000 --- U 54. 2,2-Dinhloropropane 0.17 15.000 --- U 35. 1,3-Dichlorapropene 0.22 5.000 --- U $6. Ethyl Methaerylate 0,16 10,000 --- U 57, Hexachlorobutadiene 0.10 0.200 --- U 5$. isabutyl Alcohol 12.00 100,000 --- U 59. nmethaerylonitrile 1.93 100.000 --- U 60. Methyl Methaerylat* 0.25 30.000 --- U 61. Naphthalsne 0.47 6.000 --- U 62. Propionitrile 3,26 150.000 --- U 63. 1,2,4-Trichlorobenaens 0,50 10.000 U 64, ACetoditrile 36.29 55.000 U $5. Tetrahydt0fvran 0.39 1.000 --- U 66, 1,4-Dioxane 2.71 1.000 --- U 3 + Setimated value between the MDL and MRL, U • Below ALL Quantitation Limits• GDocuSi m m 44 z U7 00 gn Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 o - %' n -0 G C Ell ur C in cn � cry � �0' G7 � > a a n y _ i N Ct m m m rn m mTdTAL CHLORINE, mgll j� v 1.� 11..�� rn m_ m ❑R ugll AT COLLECTQN v� Q � Q TEMPERATURE, °C 9-! 0. Q� ATCOLLECTION cn m z ., fi OF CONTAINERS Ail a w w -4 :3:,{�., Fie Nitrate -Nitrite A linity Chloride >;, # 7 DS x* ro mm m Sulfate Sulfide b }Fr ` `' ` rf Conductivity 'C ' DO PV Temperature 8¢r�; '. }.• „#,,�, �;3;a: Field Parameter 8260 Dup. 2 827OU Dup, 1 Y Ga ?° 8270E Dup. 2 Gk xr' s 8270E Dup. 3 Y PARAMETERMESTS L Fn w, fn c G U L L Ci m m s r7-1 c i z m {� n m m V [ l`Vll Yl p Z V] �O w m m (n m m = m�'7 > L" y CS C? 33 o z o DocuSi 0 0 CL cu M w gn Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 gyp' C C m UJ co m C qWq ��a y �� fa m m 6 A ° 4, Q2 -4 � U� m Nr'y� W t'jo P7, O c �. DD t+� m m7, m m fn m TOTAL CHLORINE, mgll Cj rn OR ugll AT COLLECTION L� O q ] >,J 1 X3 TEMPERATURE, °C °° b ATCOLLECTION cn Uy vs C) # OF CONTAINERS 8260D App. 11 G� 8260D A s , 112 ,., 2GUD Aim. 1I s s C] lT7 C,7 9260D App. 114 mp +::f;;} s $x ;:'s : Mks f J{: ; ri rf !' „cs:s 827U> Iilh1 !r YYJ m S m n m m m s f� u, n b PARAMETERSITESTSam , CO pr m - a T m m ri f cn a m m 2 O m m m m co cn c 1�r m m E5 r, m rr 0 O n d :t w DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 Euflw'0n[MH@M % h(nTpughd 114 OAKMONT L)RIVE GREENVILL.E, N.C. 27858 CLIENT: C&D DISPOSAL, INC. CLIENT ID: MR- JUDSON WHITEHURST B02 RECYCLING LANE ANALYST: GREENVILLE, NC 27834 DATE COLLECTED: DATE ANALYZED: DATE REPORTED: REVIEWED BY: y VOLATILE ORGANICS EPA METHOD 8260n R4 (19) METHOD BLANK RESULTS PRONE (252) 756-6208 FAX (252) 7.56-0633 6003 a,D JF 06/23/21 -- 06/24/21 07/02/21 11/12/21 PARAOMTERS, u /1 -- HDL MEL Concentration 1. Chloromethane 0.77 3.00 --- u 2. Vinyl Chloride 0.12 0.20 - u 3. eromomathane 0.67 10.00 --- u 4. Chloroathans 0,48 10.00 --- u S. Tirichlorofluoromathane 0.24 1.00 --- u 6, 1,1-Dichloroethene 0.17 5.00 --- u 7. Acetone 9.06 100.00 --- U e. mdomethaae o.26 10.00 --- u 9. Carbon Disulfide 4.23 100,00 --- u 10. Methylene Chloride 0.64 1.00 --- u 11, trans-1,2-Dichloroathana 0.23 5.00 --- U 12. 1,1-Dichloroethane 0.20 5.00 --- u 13. Vinyl Acatate 0.20 50.00 --- u 14. cis-1,2-nichloroathane 0.25 5.00 --- u 15. 2-Eutanone 2.21 100.00 ,-- Ti 16, Bromoohloromethane 0,27 3,00 ---- L1 17. Chloroform 0.25 5.00 --- u 18. 1,1,1-Trichloroethans 0.19 1.00 -- u 19. Carbon Tetrachloride 0.04 0.20 --- U 20. Benzene 0.24 1.00 --- U 21. 1,2-Dichloroethane 0.02 0.20 --- V 22. Trichloroethene 0.23 1.00 ---,u 23. 1,2-Dichloropropane 0.04 0.20 --- U 24. Hromodichloromethane 0.04 0.20 `-- u 25. cis-1,3-Diahloro rapene 0.06 0.20 --- u 26, 4--meth 1-2-Pentanone 1.19 100.00 --- U 27. Toluene 0.23 1.00 --- u 28. trans-1,3-1)iah1oro ropans- 0.04 0.20 --- u 29, 1,1,2-Trichloroethane 0.03 0.20 --- [7 30. Tatzachloroathene 0.10 0.20 --- u 31. 2-Hexanone 1.57 40.00 --- u 32. Dibromochloromathane 0,03 0.20 - - - Ti 33. 1,2-Dibromoathans 0.03 0.20 --- u 34, Chlorobenzene 0.30 3.00 --- u 35. 1,1,1,2-Tetrachloroethane 0.22 1.00 --- u 36. Ethylbanzane 0.21 37, xyianaw 0.68 5.00 -yy u 30. Dibromomathane 0.28 10.00 --- iY 39. Styrene 0.19 1.00 --- u 40. Sromoform 0.20 3.00 u 41. 1,1,2,2-Tetrach1oroethane 0.03 0.20 --- u 42. 1,2,3-Trichloropropans 0.09 0.20 u 43. 1,4-Dichlorobenzene 0.39 1.00 --- V 44. 1,2-Dichlorobenzana 0.32 5.00 --- u 45. 1,2-Dibromo-3-Chloxo ro ana 0.07 0.20 --- V 46. Acrylonitrils 2.72 200.00 --- U 47. trans-1,4-Dlohloro-2-Sutene 0.42 100.00 --- u 48. Acrolain 1.57 1 4.00 --- D 49. Allyl Chloride 0,20 1 10.00 --- V .0. Chloroprene 0.23. 1 20,00 1 --- u DocuSign Envelope ID: 6F6D1 F1 B-631 D-46D2-975A-F7DCA78DDE63 Emu - H&CM `�o 4964(jo Mai`A 0 114 OAKMONT DRIVE GREENVILLE. N.C. 2785E CLIENT: C&D DISPOSAL, INC, MR. J=80N WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED 6Y CLIENT ID ANALYST: DATE COLLECTED DATE ANALYZED DATE REPORTED VOLATILE ORGANICS EPA MT134D 8260D R4 (18) METHOD BLANK RESULTS (continued) PHONE (252) 756-6208 FAX (252) 756-0633 6003 S,D JP 06/23/21 -- 06/24/21 07/02/21 11/12/21 PARAMETERS, u /1 NIDL MRL Concentration 51. 1,3-Dichlorobenzene 0.41 5.00 --- U 52, DichlorodiEluoromethane 0.51 5.00 --- u 53. 1,3-Dichloro ropane 0.28 1.00 --- U 54. 2,2-Dichloxopropane 0,17 15.00 --- U 55, 1,1-Dichloropxap9rie 0.22 5.00 --- U 56. Ethyl Methacrylate 0.16 10.00 ---u 57. Hexachlorobutadi.ene 0.10 0.20 --- U 58. Iaobut 1 Alcohol 12 880 100.00 --- U 59. Mathacr'ylonitrila 1.93 100,00 --- U 60. methyl Mothacryiate 0.25 30.00 --- u 61. Naphthalene 0.47 6.00 ---- U 62. Propionitrile 3.26 150.00 --- U 63. 1,2,4-Triehlorobanzene 0.50 10.00 --- U 64. Acetonitrile 36.29 55.00 --- 0 65, Tetrahydrofuran 0.39 1.00 --- U 66. 1,4-11ioxane 2.71 3.00 --- U DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 ERAT(olimmid % kkr-iLa@TR(m%d 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C&D niSPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: �+ PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 B,D ANALYST: JP DATE COLLECTED: 06/23/21 - 06/24/21 DATE ANALYZED: 07/02/21 DME REPORTED: 11/12/21 VOLATILE ORGANICS EPA METHOD 8260D R4 (18) SURROGATE RECOVERY RESULT$ Sample Name LimitS (�h recovery) 1,2-DCA-d4 recovery) TclUana-d8 raoovery) 4-BFB (Pd recovery) continuing Calibration std. 70-130 98.6 58.2 103 Method Blank 70-130 101 98.4 98.8 MW--9A 70-130 98.2 97.6 93.9 Mw-10 70-130 98.8 99.2 94.1 Mw-11 70-130 96.4 100 95.5 Mw-13 70-130 98.6 100 99.6 Mw-128 70-130 97.3 98.1 96.4 Tri blank (3) 70-130 97,4 99.8 95.1 MW-15 70-130 98.5 99.6 97.5 MW-16 70-130 98.9 99.9 98.5 MW-17 70-130 98.3 99.6 97.3 MW-14S 70-130 100 103 96.6 Mw-14D 70-130 97.9 99.6 95.0 Trip Blank (D) 70-130 98.1 102 1 93.4 6003D MW-15 M.S. 70-130 99.5 101 1 101 6003D Mw-15 M.S.D. 70-130 98.3 100 1 101 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 Elow 114 OAKMONT DRIVE GREENVILLE, N.C. 27868 CLIENT: C&D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 f ` V REVIEWED BY: �✓% ANALYST; DATE COLLECTED: DATE ANALYZED DATE REPORTED VOLATILE ORGANICS EPA METHOD 8260D R4 (18) MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULTS PHONE (252) 756-6268 FAX (252) 756-0633 6003 B,D .7P 06/23/21 - 06/24/21 07/02/21 11/12/21 Sample Spiked: (6003D) MW-15 Spike Amount Ug/1 Sample Result Og/l Spike Result U9/1 Spike Recovery (70-13096) spike ➢up. Reault ug/1 $pike Dup. ROOOvery (70-130%) HS/MSA RPD (20%) 1,1-Dichloroethene 20.0 --- u 19.61 98.1 21.16 106 7.6 Benzene 20.0 --- U 19.51 97.6 20.92 105 7.0 Trichloroethene 20.0 --- U 19.18 95.9 21.49 107 11.4 Toluene 20.0 1 0.31 J 19.98 98.4 1 21.95 L09 9.4 ChlOrabenzene 20.0 t ---- T7 18.92 94.6 1 20.46 1 102 1 7.8 LABORATORY CONTROL SAMPLE RESULTS Sample Compound: Spike Amount V /1 Spike Result ug/1 Spike Recovery (70-130�) 1,1-Dichloroethono 20.00 20.25 101 Benzene 20.00 20.48 102 Trichloraethene 20.00 20.84 104 Toluene 20.00 1 20.61 1 103 Chlorobenzene 1 0.00 1 20.50 1 103 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 Appendix C Time vs. Concentration Graphs June 2021 Groundwater Monitoring Report CEO Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 6 7407- CDLF- 2009 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 This page intentionally left blank. DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 2.5 2 0 v 0 u 1 0.5 0 Jul-09 BE MW-3S Organochlorides Nov-10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 Mar-23 tTetrachloroethene (CAS 127-18-4) tTrichloroethene (CAS 79-01-6) +1,2-Dichloroethane +cis-1,2-Dichloroethene --*--Vinyl chloride DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 BE MW-3A Organochlorides -23 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 1.6 1.4 1.2 1 0 u 0.6 0.4 0.2 0 Jul-09 BE MW-8 Organochlorides Nov 10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 Mar-23 tTetrachloroethene (CAS 127-18-4) tTrichloroethene(CAS 79-01-6) t 1,2-Dichloroethane cis-1,2-Dichloroethene Vinyl chloride DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 EJE MW-10 Organochlorides -23 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 EJE MW-11 Organochlorides :-21 Mar-23 DocuSign Envelope ID: 6F6D1F1B-631D-46D2-975A-F7DCA78DDE63 EJE MW-12S Organochlorides 9 8 7 6 c — S c 0 w 4 0 u 3 — 2 — 0 0' V i — 0 ti • i • • 1 4 • • • r—i Jul-09 Nov-10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 Mar-23 t Tetrachloroethene (CAS 127-18-4) tTrichloroethene (CAS 79-01-6) t 1,2-Dichloroethane +cis-1,2-Dichloroethene +Vinyl chloride