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HomeMy WebLinkAbout23022_Chapel Hill Police Property_OAR_20140325LOON � I N LEKIIIN ENVIRONMENTAL SITE CHARACTERIZATION Chapel Hill Police Department Property 828 Martin Luther King Jr. Boulevard Chapel Hill, Orange County, NC ENVIRONMENTAL SITE CHARACTERIZATION Chapel Hill Police Department Property 828 Martin Luther King Jr. Boulevard Chapel Hill, Orange County, NC Prepared for: Town of Chapel Hill Chapel Hill Town Hall 405 Martin Luther King, Jr. Blvd. Chapel Hill, NC 27514 �CARO// Submitted by: Falcon Engineering, Inc. Q- '�y 1� 1210 Trinity Road • zz Suite 110 'AL Raleigh, North Carolina 27607 9 (919) 871-0800 www.falconengineers.com �0 Firm: C-3193 Falcon Project Number I El3047.00 March 25, 2014 TABLE OF CONTENTS Page Figures..................................................................................................................................................................iii Tables...................................................................................................................................................................iii Section1 1 Introduction...................................................................................................................................1 1.1 Site Location and Description....................................................................................................1 1.2 Project Objective and Scope of Work.....................................................................................2 1.3 Current Land Use..........................................................................................................................3 Section 2 1 Methods of Investigation............................................................................................................4 2.1 Monitoring Well Installation.........................................................................................................4 2.2 Groundwater Sampling...............................................................................................................5 2.3 Surface Water Sampling..............................................................................................................7 2.4 Composite Soil Sampling.............................................................................................................9 2.5 Geoprobe Soil Sampling........................................................................................................... l 1 Section 3 1 Site Geology and Hydrogeology............................................................................................17 3.1 Description of Soils......................................................................................................................17 3.2 Hydrogeologic Conditions ........................................................................................................17 Section 4 Summary of Findings.................................................................................................................18 Section 5 Recommendations....................................................................................................................20 AppendixA Figures...................................................................................................................................A-1 AppendixB Photographs..........................................................................................................................B-1 AppendixC Well RecordS........................................................................................................................C-1 AppendixD Laboratory Data.................................................................................................................D-1 k JF FIGURES Page Figure 1 1 General Site Location................................................................................................................A-2 Figure 2 1 Approximate Sampling Location Map..................................................................................A-3 TABLES Page Table 1 Groundwater Analytical Methods...............................................................................................5 Table 2 Summary of Groundwater Lab Results........................................................................................6 Table 3 Summary of Surface water Lab Results.......................................................................................8 Table 4 Summary of Composite Soil Sampling Lab Results.................................................................10 Table 5 Summary of Geoprobe Collected Data..................................................................................12 Table 6 Summary of Geoprobe Soil Sample Lab Results.....................................................................13 k JF SECTInN i INTRODUCTION Falcon Engineering, Inc. (Falcon) conducted an Environmental Site Characterization in general accordance with the January 2014 Inactive Hazardous Sites Program's Guidelines for Assessment and Cleanup. This assessment was performed on a property with the property identification number (PIN) 9789413949. Figure 1 (Appendix A) provides a general site location map of the subject property. Additional figures detailing sample locations are also provided in Appendix A of this report. 1.1 Site Location and Description The evaluated property is approximately a 10.24-acre property located along Martin Luther King Jr. Blvd. in Chapel Hill, North Carolina. The site is located to the east of Martin Luther King Jr. Blvd., with development primarily focused in the northwest corner. The property is located immediately north of Bolin Creek, beginning approximately 200 feet north of the centerline of Hillsborough Street. The property is currently developed with a 2 story structure approximately 35,000 square feet in size. There are also two parking lots and a few cargo containers used for storage present on site. The site is currently occupied by the Chapel Hill Police Department. The building is located in the northwest corner, with the majority of parking in the center of the site. The eastern and southern portions of the site are wooded. k JF 1.2 Project Objective and Scope of Work The Town of Chapel Hill retained Falcon to conduct this Environmental Site Characterization. The purpose of the investigation was to further delineate environmental conditions present at the site in regards to the former use as an ash landfill. Previous work conducted at the site is detailed below (Phase I ESA & Limited Phase 11) but is provided under a separate cover: The project goals of the Phase I were accomplished through the completion of the following tasks: Review of environmental databases and lists obtained from Federal, State, and local regulatory agencies including historic maps and directories of the site and the surrounding areas. • Visual inspection of the subject site, including photographic documentation of existing conditions and notation of adjacent property use and conditions. • Interviews with those knowledgeable of the site's history (as appropriate or required). The project goals of the Limited Phase II were accomplished through the completion of the following tasks: • Sediment and groundwater sampling to determine the existing conditions within identified areas on the subject property. Sampling included two sediment samples and 3 water samples. • Laboratory analyses of samples for chemicals of concern. • Comparison of analytical results to applicable criteria. Based on findings of those investigations NCDENR requested the lab results from two down gradient monitoring wells and additional composite samples of the ash landfill area. Falcon also conducted geoprobe drilling on site to better assess the extent of potential Coal Combustion Products (CCPs) on the subject property. 1.3 Current Land Use The subject property was generally undeveloped until the current police station was constructed after 1980. However, as discussed in the Historical Usage section, it appears the site was used as a borrow pit in the late 1950's through early 1960's then as a fill site from the mid- 1960's to mid- 1970's. The site has been the home of the Chapel Hill Police Station since the town acquired it in 1980. During the site reconnaissance, it became apparent that the site had significant amount of fill materials placed at one time. There is a steep slope along the southern portion of the property, where it was apparent that significant coal combustion products (CCPs) and debris were placed on the site. SECTION 2 METHODS OF INVESTIGATION 2.1 Monitoring Well Installation In previous investigative efforts, two (2) groundwater monitoring wells had been installed, MW-1 a permanent well and MW-2 a temporary well. MW-1 was installed adjacent to the southwest of the Police Station Building. MW-2 was installed between the subject property and Bolin Creek. Results from these sampling activities were provided in previously submitted reports to NC DENR. The first phase of this investigation involved the installation of two (2) down gradient groundwater monitoring wells on January 27, 2014. MW-3 was placed down gradient of the CCPs within the wooded area north of Bolin Creek Greenway Trail. MW-3 was located towards the western side of the subject property. MW-4 was placed downgradient of the CCPs, also within the wooded area north of Bolin Creek Greenway Trail. MW-4 was located toward the eastern side of the subject property. The installation depth of MW-3 was 11.0 ft below ground surface (bgs) and the installation depth of MW-4 was 9.2 ft bgs. Initial groundwater depths were recorded at 3.4 ft bgs for MW-3 and 4.1 ft bgs for MW-4. It should be noted that the shallow depths and auger refusal may have been due to the natural geology located in this area and the sites close proximity to Bolin Creek. Well Construction records are provided in Appendix C of this report. The installation of an additional well was attempted (MW-5) as an up -gradient well to determine background groundwater concentrations. This well was proposed to be placed on the north end of the property in the upper parking lot. Drilling was performed at this location until continued auger refusal was achieved due to onsite geologic conditions. Drilling completed at MW-5 at a final depth of 31.5 ft bgs. The augers were left for 12 hours to see if groundwater was present at these depths; however the well was observed to be dry and as a result filled in. Following installation of these wells, these wells were developed on January 29-30, 2014. Falcon utilized Region 4 EPA guidance document for the Design and Installation of Monitoring Wells. The method of purging the wells was by pumping and bailing. Per the established guidance, 24- 4 hours were allowed for the surface pad and protective casing to settle and at least 24-hours were allowed in between purging and sampling. Both wells recharged following adequate purging of at least three (3) well volumes or the wells being purged dry. 2.2 Groundwater Sampling Following installation, development and purging of these down gradient groundwater monitoring wells, environmental sampling was conducted. This sampling was performed on February 5, 2014 and was completed in accordance with the January 2014 Inactive Hazardous Sites Program's Guidelines for Assessment and Cleanup. Based upon this guidance, Table 1 provides the analytical methods that were used in the collection of these environmental samples. All analytical methods were performed by Prism Laboratories, Inc. (NC Certification No. 402). Falcon utilized these parameters for the sampling of MW-3 and MW-4. Table 2 provides a summary of those constituents that were above the analytical reporting limits. A full laboratory report is provided in Appendix D of this report. TABLE 1 I GROUNDWATER ANALYTICAL METHODS Volatile Organic Compounds (VOC) 1,4-Dioxane Semi -volatile Organic Compounds (SVOC) Metals Hexavalent chromium SW 846 Method 8260 SW 846 Method 8260 SIM SW-846 Method 8270 USEPA method for detection limits below the 15A NCAC 2L standards USEPA Method 218.7 or 218.6 as modified by US EPA Region IV —75 TABLE 2 1 SUMMARY OF GROUNDWATER LAB RESULTS Mercury ug/I 1.4 BRL NS 1 Arsenic ug/I 1 140 1 BRL NS I EEEMMM Barium ug/I 1500 110 NS 700 Cadmium ug/I 1.7 BRL NS 2 Chromium ug/I 930 BRL NS 10 Lead ug/I 250 BRL NS 15 Selenium ug/I 99 BRL NS 20 NOTES: Values shown in BOLD are above the applicable standard BRL = Below Reporting Limit NS = Not Sampled * M W-5 was drilled to a depth of 31.5 ft bgs but no groundwater encountered 1 jF 2.3 Surface Water Sampling Bolin Creek runs adjacent to the subject property, bordering the southern property line. As the natural topography drains in the southern direction towards Bolin Creek, Falcon collected two grab samples from Bolin Creek to determine any potential impacts to this water body via groundwater or surface water runoff. The Bolin Creek samples, consisted of one downstream sample (BC-2) and one upstream sample (BC-1). This sampling method allowed for the collection of a background sample, via BC-1, prior to this water body encountering this property, and an impacted sample, via BC-2 after this water body would of seen surface runoff from this property. This sampling was performed on February 5, 2014 and was completed in accordance with the January 2014 Inactive Hazardous Sites Program's Guidelines for Assessment and Cleanup. The same analytical methods outlined in Table 1 above were also used for the analysis of these collected surface water samples. All analytical methods were performed by Prism Laboratories, Inc. (NC Certification No. 402). Table 3 provides a summary of those constituents that were above the analytical reporting limits. A full laboratory report is provided in Appendix D of this report. TABLE 3 1 SUMMARY OF SURFACE WATER LAB RESULTS NOTES: BRL = Below Reporting Limit ki 2.4 Composite Soil Sampling To determine the nature and extent of potentially contaminated soils, Falcon performed composite soil sampling at three locations along the southern property line. Sampling was conducted according to the January 2014 Inactive Hazardous Sites Program's Guidelines for Assessment and Cleanup and approved EPA sampling protocol for General Composite Sample Collection Procedures. Composite soil sample locations consisted of locations identified as S-5, S-6, and S-7. All three locations were in areas observed to be potentially exposed CCP. The samples were taken by auger and consisted of 4.0 feet of material just below removed leaf litter. The samples were then placed in large bags and thoroughly combined before sampling. This sampling was completed on January 31, 2014. Figure 2 provided in Appendix A provides a visually depiction of these sampling locations. The sampling figure denotes locations as well as pictures in Appendix B. Table 4 below provides a summary of sampling results that were above the established laboratory reporting limits. I JF TABLE 4 SUMMARY OF COMPOSITE SOIL SAMPLING LAB RESULTS Hexavalent Chromium mg/kg 1.3 Mercury mg/kg 0.3 Arsenic mg/kg 37 Barium mg/kg 2,800 Chromium mg/kg 21 Lead mg/kg 10 Selenium mg/kg 3.2 4-Isopropyltoluene mg/kg 0.051 Acetone mg/kg 0.14 Methyl Ethyl Ketone (2-Butanone) mg/kg BRL [Toxaphene mg/kg BRL NOTES: Values shown in BOLD are above the most stringent of the applicable MSCC BRL = Below Reporting Limit NA = Not applicable. No MSCC for this constituent 0.42 0.44 NA NA NA 43 44 NA NA NA I� 3,200 2,500 290 3,100 81,000 22 29 5.4 47 1,226 12 11 270 400 400 6.1 4.5 NA NA NA 1 ND 0.024 NA NA NA i 0.17 0.11 24 14,000 360,000 0.0086 BRL 16 9385 245,280 i BRL 0.17 NA NA NA 10 2.5 Geoprobe Soil Sampling To provide a preliminary delineation of potentially present CCPs, a geoprobe was mobilized to advance into the soils on the subject property. Troxler Geologic was contracted to provide these geoprobe services under the direction of Falcon staff. Falcon established a sampling grid across the horizontal extent of the subject property to determine the presence or absence of disposed CCPs. A visual depiction of these sampling locations can be found in Appendix A of this report. Table 5 below provides summary data for each of the geoprobed locations. This table includes location ID, final probed depths and approximate depths to which CCPs may be present. It should be noted that due to the consistency of CCPs, the material being compacted can give inaccurate portrayals of the depths of these materials. Falcon used its best judgment in determining the vertical extents of the material based on ease of drilling, recoveries, and site characteristics/gradient. It should also be noted that in some locations a layering of ash followed by a debris material or fill then back into an ash layer was observed. Field logs and pictures are provided in the Appendix for a more detailed description. Table 6 provides a summary of the analytical results for the collected geoprobe soil samples. This summary table provides only those constituents that were reported above the established laboratory reporting limits. Full detailed laboratory analysis can be found within Appendix D of this report. I JF TABLE 5 SUMMARY OF GEOPROBE COLLECTED DATA GP-1 14 35 9-12 5 - 30 8-12 T ^ "L ^^ GP-3 17 10 - 16 10 - 12 GP-4 20 3-16 10 - 12 GP-S-A 8 4-8 No Samples GP-5 12 4-8 Sampled 4 - 6 GP-6 26 1 1- 23 9- 1 1 GP-7 20 3-14 10 - 12 GP-8 17 5 - 15 11 - 15 GP-9 8 - No Samples GP-10 8 - No Samples GP-11 9 3-9 4-6 GP-12 12 2- 10 2-4 Refusal at 14 ft bgs into weathered rock Refusal at 35 ft bgs Refusal at 17 ft bgs due to possible landfill debris Into native soils at 17 ft bgs Refusal from wood debris at 8 ft bgs Refusal at 12 ft bgs Into native soils at 24 ft bgs Into native soils at 16 ft bgs Into native soils at 16 ft bgs Into native soils at 4 ft bgs / No ash observed Into native soils at 1 ft bgs / No ash observed Refusal at 9 ft bgs Into native soils at 11 ft bgs TABLE 6 SUMMARY OF GEOPROBE SOIL SAMPLE LAB RESULTS Mercury mg/kg 0.083 0.24 Arsenic mg/kg 3.5 41 Barium mg/kg 86 1,100 Chromium �_ mg/kg 8.8 19 Lead mg/kg 26 11 Seleniu� mg/kg BRL 4 Hexavalent Chromium I mg/kg I BRL BRL NOTES: Values shown in BOLD are above the most stringent of the applicable MSCC BRL = Below Reporting Limit NA = Not applicable. No MSCC for this constituent 0.42 NA NA NA 48 NA NA NA 1,200 290 3,100 81,000 23 5.4 47 1,226 39 270 400 400 BRL NA NA NA 0.53 5.4 47 1,226 13 TABLE b SUMMARY OF GEOPROBE SOIL SAMPLE LAB RESULTS (CONTINUED) NOTES: Values shown in BOLD are above the most stringent of the applicable MSCC BRL = Below Reporting Limit NA = Not applicable. No MSCC for this constituent 314 TABLE b SUMMARY OF GEOPROBE SOIL SAMPLE LAB RESULTS (CONTINUED) NOTES: Values shown in BOLD are above the most stringent of the applicable MSCC BRL = Below Reporting Limit NA = Not applicable. No MSCC for this constituent 315 TABLE 6 SUMMARY OF GEOPROBE SOIL SAMPLE LAB RESULTS (CONTINUED) Mercury mg/kg 0.28 Arsenic mg/kg 52 Barium mg/kg 2,000 Chromium mg/kg 19 Lead mg/kg 14 Selenium mg/kg 2.1 Hexavalent Chromium mg/kg i BRL NOTES: Values shown in BOLD are above the most stringent of the applicable MSCC BRL = Below Reporting Limit NA = Not applicable. No MSCC for this constituent NA NA NA NA NA NA 290 3,100 81,000 5.4 47 1,226 270 400 400 NA NA NA 5.4 47 11226 16 SECTION 3 SITE GEOLOGY AND HYDROGEOLOGY 3.1 Description of Soils The US Natural Resource Conservation Service's Orange County Soil Survey provides two (2) different native soil types on the subject site: TaE - Tatum Silt Loam Complex (15 to 25 percent slopes) - well drained soil derived from red saprolite (50% of the overall subject site). WmE - Wedowee Sandy Loam Complex (15 to 25 percent slopes) - well drained soil derived from red saprolite (50% of the overall subject site). 3.2 Hydrogeologic Conditions A review of the Chapel Hill, NC USGS 7.5-minute 1946 topographic map, which includes the project site, indicates that the site is located on varying elevations from 375 feet above mean sea level (msl) in the northwest corner of the site to 284 feet msl in the southeast corner where the site meets Bolin Creek. The 2010 Topographic Map from Orange County GIS indicates significantly different contours from the USGS maps. This data supports the filling and leveling of the site which would explain the soil/debris layers observed within the geoprobe soil profiles. The site is bounded on the north and west by paved streets, to the east by residential developed woodlands and to the south by Bolin Creek. The general site drainage is to the South via overland flow and along stormwater trenches aside Martin Luther King Jr. Blvd. All stormwater drains from this site into Bolin Creek. Very little, if any, surface water comes onto the site from offsite. 17 C Ct-T1 t1 Al SUMMARY OF FINDINGS Falcon Engineering, Inc. completed an Environmental Site Characterization at 828 Martin Luther King Jr. Boulevard located in Chapel Hill, North Carolina. The purpose of the investigation was to evaluate the on -site soils and groundwater for potential CCPs within the property boundaries. For this investigation, our scope of services consisted of the collection of composite soil samples, groundwater samples and surface water samples to determine the existing conditions present on the subject property. Sampling activities included the following: • Collection of three (3) composite soil samples via hand augered locations in the area of suspected CCP disposal. These sampling locations were identified as S-5, S-6, and S-7. • Collection of two (2) groundwater samples identified as MW-3 and MW-4. A duplicate sample was collected as a quality assurance sample from MW-3 and was identified as MW-3A. • Collection of two (2) surface water samples from Bolin Creek. BC-1 was collected as an up gradient grab sample and BC-2 was collected as a down gradient sample. In addition, Falcon advanced twelve (12) geoprobe borings into pre -defined locations throughout property to transect and attempt to delineate the vertical and horizontal extents of potential CCPs located at the subject property. Based upon our completed field activities and subsequent laboratory analysis Falcon was able to provide the following findings: 1. Composite soils sampled confirmed the presence of CCPs at the subject property. Laboratory results confirmed the presence of Arsenic, Barium, Chromium, Lead, and Selenium within the collected samples. Barium and Chromium were reported to be above the NC DENR Soil to Groundwater MSCCs. Only Barium was reported to be above the NC DENR Residential MSCCs on a few samples. I JF 2. Groundwater collected from MW-4 appears to have been impacted from the leaching of CCPs. Based upon laboratory data, levels of Mercury, Arsenic, Barium, Chromium, Lead and Selenium were all above the NC DENR 2L Groundwater Standard. 3. Groundwater collected from MW-3 showed reported concentrations of Barium within the sample, but was below the NC DENR 2L Groundwater Standard. 4. Surface water sampled from Bolin Creek did not exhibit results indicative of environmental contamination above established NC DENR Surface Water Standards for water supply sources or freshwater aquatic life. I JF SECTION 5 RECOMMENDATIONS In response to this investigation, The Town of Chapel Hill has authorized Falcon to restrict public access via the installation of fencing along the south portions of the property in which the CCPs is visibly exposed. The Town of Chapel Hill has also authorized Falcon to install silt fencing along this southern property line to mitigate the potential for these CCPs to migrate offsite as a result of stormwater run-off. Additional silt fencing was also installed along the toe of the hill along this southern property to prevent further erosion and migration of these materials from the hillside. These measures are prudent cautionary measures to prevent CCPs from leaving the site and to deter public access into these identified areas. Falcon recommends that these results be submitted to NC DENR for further review and consultation. Additional sampling of the installed groundwater monitoring wells can be performed on a routine schedule as dictated by NC DENR or desired by the Town of Chapel Hill. It is recommended that this area be inspected on a quarterly basis to ensure the preventative measures are remaining in proper functional order. While these preventative measures provide an adequate short-term mitigation, a more permanent solution should be considered following consultations with NC DENR. Falcon is available to provide additional consultation and recommended courses of action for these solutions. _�720 APPENDIX A FIGURES FIGURE 1 I GENERAL SITE LOCATION JF FIGURE 2 1 APPROXIMATE SAMPLING LOCATION MAP 3A-3 40 86 Z 501 c _ 15 cn 41 40 Z ESTES DR P� o"*SITE N HILLSBOROU(GH ST 15 86 \ S� 501 40 /�FgPNRALEIGH RD VICINITY MAP SN Ezo o� (NOT TO SCALE) GENERAL NOTES 1) THE PURPOSE OF THIS PLAT IS TO SHOW MONITORING WELLS AND BUILDINGS IN RELATION TO THE CONTROL LINE ESTABLISHED FOR THIS SURVEY. 2) ALL BEARINGS, DISTANCES, AND COORDINATES SHOWN HEREON ARE BASED UPON THE NORTH CAROLINA STATE PLANE COORDINATE SYSTEM, NAD 83 (2011), WITH NAVD88 (GEOID 12) ELEVATIONS, PER A GPS SURVEY PERFORMED BY TAYLOR WISEMAN AND TAYLOR ON FEBRUARY 25, 2014. THE N.C. STATE PLANE COORDINATE SYSTEM SHOWN FOR CONTROL POINTS HEREON WERE ESTABLISHED UTILIZING GLOBAL POSITIONS SYSTEMS (GPS) IN CONJUNCTION WITH THE NORTH CAROLINA GEODETIC SURVEY'S VIRTUAL REFERENCE SYSTEM (VRS), WHICH IS BASED UPON THE CONTINUALLY OPERATING REFERENCE STATIONS (CORS). 3) PROPERTIES SHOWN HEREON ARE SUBJECT TO EASEMENTS AND RESTRICTIONS OF RECORD THAT WOULD BE REVEALED BY A THOROUGH TITLE SEARCH. THIS PLAT SHOULD NOT BE RELIED UPON AS A COMPLETE RECORD OF ALL EASEMENTS THAT MAY EFFECT THESE PROPERTIES. 4) THIS MAP DOES NOT REPRESENT A BOUNDARY SURVEY. PROPERTY LINES, STREAM CENTERLINES AND PLANIMETRIC INFORMATION SHOWN HEREON WERE TAKEN FROM THE ORANGE COUNTY GIS DATABASE ON MARCH 03, 2014 AND THIS INFORMATION HAS BEEN SHOWN HEREON FOR REFERENCE PURPOSES ONLY. NO TRANSLATION, ROTATION OR SCALING WAS PERFORMED ON THE GIS DATA. IT WAS INSERTED INTO OUR DRAWING FILE AS PROVIDED. NO ACCURACY OR POSITIONAL TOLERANCE IS GUARANTEED BY THIS SURVEY AS TO HOW THE SURVEYED FEATURES TRULY RELATE TO THE GIS INFORMATION SHOWN HEREON. 5) ALL DISTANCES AND COORDINATES SHOWN HEREON ARE LOCALIZED, GROUND INFORMATION, UNLESS SPECIFICALLY NOTED AS "GRID". FEATURE TABLE ID NORTHING EASTING TOP CASE ELEV GROUND ELEV MW-1 792206.53 1984238.25 346.12 346.52 MW-3 791897.55 1984360.36 304.95 301.47 MW-4 1 791819.55 1 1984508.46 1 301.42 1 297.79 MW-5 792377.87 1984299.80 - 362.76 1 *NOTE* MW-5'S LOCATION IS AT GROUND ELEVATION MW-5 WAS DRILLED, BUT NOT SET ABBREVIATIONS BLVD BOULEVARD DR DRIVE ELEV ELEVATION ST STREET W W E S NC Grid - NAD 83 (2011) SYMBOL LEGEND Q MONITORING WELL (51 SURVEY CONTROL POINT I, CHAD T. HOWARD, CERTIFY THAT THIS MAP WAS DRAWN UNDER MY SUPERVISION, FROM AN ACTUAL GROUND (CONVENTIONAL) AND GPS SURVEY MADE UNDER MY SUPERVISION; THAT THE GPS SURVEY INFORMATION (METADATA) HAS BEEN REPORTED HEREON UNDER THE "SURVEY CONTROL J GRID TIE NOTES"; THAT THE BOUNDARIES NOT SURVEYED ARE CLEARLY INDICATED AS SUCH AND ARE BASED UPON THE DEEDS AND PLATS REPORTED HEREON; THAT THE RATIO OF PRECISION OR POSITIONAL ACCURACY HAS BEEN REPORTED HEREON. WITNESS MY ORIGINAL SIGNATURE, REGISTRATION NUMBER AND SEAL THIS 4th DAY OF MARCH, IN THE YEAR OF OUR LORD 2014. ° A4 iz-() 4 4 � -, � � � ==off �o, • ° SEAL g 8 L-4220 0ol 9 o. %° °° 4 oo CHAD T. HOWARD LICENSE NO. L 4220 ,,* T/j{{ l O ° GRAPHIC SCALE 60 0 30 60 120 240 1"=60' 0 0 A w w a w D U) U) Zo ® E u i wi 00 ti O (n V p M J Z o 0 >-���(9 W W U N W w Z N yWLu . Lu Z Q 00�=3"-Z Lu Q o -� U Y rn Z ® CZ-7 N W Z f-- Q = IX Q w Q' Z o M W F— W J Z Z�-7= 0 a Z LLI W _ V Q OW�U JUW 1 0 - i- J O J Z U Z � U 0CL4z E— Q 00 0(.) 00 2 REVISIONS: DATE OF SURVEY: 02/26/2014 SCALE: 1" = 69 DRAWN BY: J. REYNOLDS CHECKED BY: C. HOWARD PROJECT: 70616.6007.00 SHEET: 1/1 q: \CAD\70616 \70616.6007. 00\dwg \ 70616.6007. 00-BASE. dwg APPENDIX B PHOTOGRAPHS PJF NA '4 Y 'Y !r" � r; � . �'S. y®`°i�xk. �'q f!e �' ' .A. si M� y��j♦ �, I ' , ii �° � 1 � _ - b � �/ ''t s, 'F c�'il� v'C'gi [ � v 1 �� � 'i.` • d q }p F� f � � 1� r -+�* 14 n14s t a ti�1 '' r�pl 1, Ty v 9 ;➢ �k� 1 j.. fi 1(f -'1� - 8- L "• 1�KI V1,'!' G= ♦ ° 1 tl r �'��-�'.� *��. a; �+ �' "_i �'t - f � atC`".,t,' � r.., - a" - �OP� 5 r 5F % fr f7W ,tea ,. . Q: � r - :3• RQl jrmT• Attempted location for MW-5 in north Encountered soils at MW-5 location ,t z2 71, IVS PMW-.-- A J. gq F J �_ • f-�yFFi1l� `�s� GYP S a f �:/ Y�a'Wl � 110 �r � .r► - sv g a Do oA lot 171 fmmlff---�k- t�j i rk-77=4 'Ott" 17 Jq N � ' 41; x - b. A �'w�- View of water purging activities at MW-4 k 4 Typical of initial water clarity of purged water r�3 v MAL1 V MW-3 well location Bolin Creek sample location for downstream BC-2 * J i 4 L, View of drainage southeast of site View towards site from drainage southeast of site Geoprobe location 1 GP-1 Soil profile GP-1 Soil Profile Geoprobe location 2 Geoprobe location 2 GP-2 soil profile GP-2 soil profile GP-3 drill location Geoprobe location 3 GP-3 soil profile GP-3 soil profile pw, ip 5,54 Geoprobe location 4 GP-4 soil profile GP-4 soil profile M GP-5 soil profile GP-5 soil profile GP-5 soil profile GP-5-A soil profile (shallow refusal) fir - - � � ` J � j V GP7 49 f..-. I� 115 1 �.�r: �`� _ _ � � �.'1� �• _ � � ter. I I III Il �� MAU I AL • 1 Ry drill location l ' i Ogg fffy � P_ r s GP-10 drill location GP-10 soil profile GP-10 soil profile GP-10 soil profile GP-11 geoprobe location GP-11 soil profile SUBJECT: ALCON PROJECT: PREPARED ffY' le GP-11 soil profile CHECKED BY: GP-12 sample GP-12 soil profile GP-12 soil profile GP-12 soil profile APPENDIX C WELL RECORDS �n4,;cstATFw �y NONRESIDENTIAL WELL CONSTRUCTION RECORD x� North Carolina Department of Environment and Natural Resources- Division of Water Quality /""`'"' WELL CONTRACTOR CERTT'ICAITON-# 1. WELLCONTMCTOR: Well Contractor (individual) Name �%%1-f Gy�J l� 1yPJd�-TIrJ1`� Well Contractor Company Name S-Cd /f%Ar- Street Address. City or Town State. Zip Code 3L I1 y 5`1�-3- ///5r Area code Phone number 2. WELL INFORMATION: WELL CONSTRUCTION PERMIT# OTHER ASSOCIATED PERMIT#(if applicable) SITE WELL ID #(if applicable). M W 3. WELL USE (Check One Box) Monitoringe MunloipallPublic ❑ Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection ❑ irrigation❑ Other p (list use) DATE DRILLED f - 2-`? • t `7 4. WELL LOCATION: (Street Name. Numbers, Community, Subdivision, Lot Nd., Parcel, Zip Code) CITY: ahA-p e-/ Itf // COUNTY TOPOGRAPHIC / LAND SETTING: (check appropriate box) ❑Slope QVal(ey CKa-t ❑Ridge ❑other LATITUDE 35 "�' " DMS OR-3X.X)WoaoOc)C DID LONGITUDE B0 " DMS OR 7X.KK_!Lc XXX DD Latitude/longitude source: ❑3PS Dropographic map (locatlon of well ,must be shown on a USGS topo map andattached to this fofm if not using CPS) 5. FACILITY (Name of the business where the well is Jocated.) Facile , Faclity ID# (Jf applicable) Zss / -'+. 't L"fk' Street Address City or Town T State ZJp Code Contact Name Mailing Address City or Town State ZIp Code Area code Phone number 6. WELL DETAILS: a. TOTAL DEPTH: b. DOES WELL REPLACE EXISTING: WELL? YES Q NO c. WATER LEVEL Below Top of Casing: 7, FT. (Use "+" if Above Top of Casing) : ct, TOP OF CASING IS 2' S— FT. Above Land Surface 'Top of casing terminated atlor below land surface may require a variance in accordance with 15A NCAC 2C .0118. e. YIELD (gpm): METHOD OF TEST = f. DISINFECTION: Type Amount g. WATER ZONES (depth): Top Bottom Top Bottom :Top— Bottom Top Bottom Top Bottom Top Bottom Thickness/ 7. CASING: Depth r� Diameter Weight Material Top �'2 Bottom 9� Ft. 5k4 qO Top Bottom Ft Top . Bottom Ft. 8_ GROUT: Depth Material Method : Top Bottom z rr Ft. kcl,(— Top Bottom Ft. = Top Bottom Ft. = 9. SCREEN: Depth Diameter Slot Size Material Top y'z Bottom �r Ft. �p in. t y� in. C_ Top Bottom Ft. in. in. Top Bottom Ft. in. in. 10. SANDIGRAVEL PACK: s Top �1 Depth r N Bottom Z Size Ft_,�ff__ Material Tap Bottom Ft. Top Bottom Ft_ 11, DRILLING LOG Top Bottom 1 I : 12. REMARKS: Formation Description I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS = RECORD HAS BEEN PROVIDED TO THE WELL OWNER. : SIGNATURE OF CERTIFIED �W/ELL CONTRACTOR DATE IF I DO Fk1NL 4— PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit within 30 clays of completion to: Division of Water Quality Information Processing, Form G1N-1n P � ' � Rev. 2/09 1617 Mail Service Center, Raleigh, NG 27699-161, Phone , t919) 807-6300 d s", NONRESIDENTIAL WELL CONSTRUCTION RECORD Nora, Carolina Departtnent of Environment and Natural Resources- Division of Water Quality WELL CONTRACTOR CERTIFICATION # u' 7 q- 1. WELL CONTRACTOR: _ `' w (t� - Well Contractor (individual) Name Well Contractor Compa y Nor Name 5tO rrv�r�,r7ct.4r' ArtJ Street Address 6/'& rV axo �C. Z7 9b(, City or Town State, Zip Code t. 4ri" -fits` . Area code Phone number d. TOP OF CASING IS 2+ FT. Above Land Surface* 'Top of casing terminated atlor below land surface may require a variance In accordance with 15A NCAC 2C .0118, e_ YIELD (gpm): METHOD OF TEST f. DISINFECTION: Type Amount g. WATER ZONES (depth): Top Bottom Top Bottom = Top Bottom Top Bottom Top Bottom Top Bottom 2. WELL INFORMATION: A : 7. CASING: Depth Diameter WELL CONSTRUCTION PERMIT# j A : Top Bottom Ft. Z�� OTHER ASSOCIATED PERMIT#(if applicable) SITE WELL ID #(if applicable) Mr - _- 3, WELL 115E (Check One Box) Monitoring P MunicipaUPubllc Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection no Irrigation❑ ether ❑ (list use) DATE DRILLED 1 C WELL LOCATION: q l-V M,� 1 L� lt; t $ � 27S y (Street Name, Numbers, Community, Subc!Mslon, tmt No., Parcel, Zrp Code) CITY: C�+4- )filr� COUNTY a►�`-- TOPOGRAPHIC / LAND SETTING: (check appropriate box) ❑Slope pValley Flat ❑Rldge ❑Other LATITUDE; 35 °_' " DMS OR 3X.XXWMXX DD LONGITUDE ao °� ° OMS OR 7X.XXXXXXXXX DD Latitudellongitude source: BPS Qfopographic map {locaffon of well must be shown on a USGS topo map andattached to this form if not using GPS) S. FACILITY (Name of ttte business where the well is located.) Facility f4ame LA#4, S Facility ID# if applicable) :sZ�S AM�4�1 Iris,;gy ge Street Address C'h,rJ � A1C z7r-) I City or own State zip Code Contact Name Melling Address City or Town State Zip Code L`) Area, code Phone number 6. WELL DETAILS: a. TOTAL DEPTH: l b. DOES WELL REPLACE EXISTING WELL? YES rl NO l5/ c. WATER LEVEL Below Top of Casing_ FT. (Use "+° IfAbove Top of Casing) Thicknesst Weight Material Yu P Top Bottom Ft. Top Bottom Ft.- S. GROUT: Depth Material Method Top _ Bottom Ft t— Top Bottom Ft. Top Bottom Ft. = 9. SCREEN: Depth Diameter Slot Size Material Top 6 Bottom jtf Ft 'Z in. + 10 in. PUC_ Top Bottom FL in. in, Top Bottom Ft - in. in. 10. SANDIGRAVEL PACK: Depth Sae Material Top y Sottom 11 Ft. — Top Bottom Ft. Top Bottom Ft.. 11. DRILLING LOG Top Bottom Formation Description 1 i _ r .1 I : 1Z. REMARKS: i DO HEREBY CERTIFY THATTHIs WELL WAS CONSTRUCTED 1N ACCORDANCE W ITN 15A NCAG 2C, WSLL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS __,PEEN AROYEOI D F 7HE WELL OWNER SIGNATURE OF CERTIFIED WELL CONT C- OAR DATE : PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit within 30 days of completion to. Division of Water Quality - Information Processing, Form GW-1bRev. 2109 1617 Mail Service Center, Raleigh, NC 27699-161, Phone (919) $07-6300 APPENDIX D LABORATORY DATA UF RIS Full -Service Analytical Environmental Solutions /PM 1W_Z1�, LABOFATOAIES.INC. Falcon Engineering Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 NC Certification No. 402 SC Certification No. 99012 NC Drinkinq Water Cent No. 37735 VA Certification No. 460211 DoD ELAP: L-A-B Accredited Certificate No. L2307 ISO/IEC 17025: L-A-B Accredited Certificate No. L2307 Project: 828 Martin Luther King Jr Blvd. Lab Submittal Date: 01/31/2014 Prism Work Order: 4020008 Case Narrative 02/18/2014 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a ----I Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference: Reviewed By Angela D. Overcash VP Laboratory Services A Result should be considered as estimated concentration. CCV result was below established QC limits. Aa Surrogate recovered below established QC limits. Sample from this project selected for re -extraction for confirmational purpose. Similar results for extraction surrogates were obtained. Original results were reported. Matrix interference is suspected. CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. D RPD value outside of the control limits. ICV ICV result is above the control limits. Analyte not detected in the sample. No further action taken. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). LH High LCS recovery. Analyte not detected in the sample(s). No further action taken. SR Surrogate recovery outside the QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 35 bnRISM Fullironm n Analyticals-' Environmental Solutions �Ili —a ATIEs,ING Sample Receipt Summary 02/18/2014 Prism Work Order: 4020008 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received S-5 4020008-01 Solid 01/31/14 01/31/14 S-6 4020008-02 Solid 01/31/14 01/31/14 S-7 4020008-03 Solid 01/31/14 01/31/14 Samples were received in good condition at 5.3 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 35 ® P R I S M Full -Service Analytical Environmental ronenfal Solutions Summary of Detections 02/18/2014 Prism Work Order: 4020008 Prism ID Client ID Parameter Method Result Units 4020008-01 S-5 Hexavalent Chromium '7196A 1.3 mg/kg dry 4020008-01 S-5 Mercury *7471B 0.30 mg/kg dry 4020008-01 S-5 Arsenic '6010C 37 mg/kg dry 4020008-01 S-5 Barium `6010C 2800 mg/kg dry 4020008-01 S-5 Chromium '6010C 21 mg/kg dry 4020008-01 S-5 Lead "6010C 10 mg/kg dry 4020008-01 S-5 Selenium '6010C 3.2 mg/kg dry 4020008-01 S-5 4-Isopropyltoluene 8260E 0.051 mg/kg dry 4020008-01 S-5 Acetone 8260E 0.14 mg/kg dry 4020008-02 S-6 Hexavalent Chromium *7196A 2.7 mg/kg dry 4020008-02 S-6 Mercury `7471B 0.42 mg/kg dry 4020008-02 S-6 Arsenic '6010C 43 mg/kg dry 4020008-02 S-6 Barium "6010C 3200 mg/kg dry 4020008-02 S-6 Chromium '6010C 22 mg/kg dry 4020008-02 S-6 Lead `6010C 12 mg/kg dry 4020008-02 S-6 Selenium "6010C 6.1 mg/kg dry 4020008-02 S-6 Acetone 8260B 0.17 mg/kg dry 4020008-02 S-6 Methyl Ethyl Ketone (2-Butanone) 8260E 0.0086 .1 mg/kg dry 4020008-03 S-7 Hexavalent Chromium *7196A 1.4 mg/kg dry 4020008-03 S-7 Toxaphene 8081 B 0.17 mg/kg dry 4020008-03 S-7 Mercury `7471B 0.44 mg/kg dry 4020008-03 S-7 Arsenic '6010C 44 mg/kg dry 4020008-03 S-7 Barium "6010C 2500 mg/kg dry 4020008-03 S-7 Chromium '6010C 29 mg/kg dry 4020008-03 S-7 Lead `6010C 11 mg/kg dry 4020008-03 S-7 Selenium '6010C 4.5 mg/kg dry 4020008-03 S-7 4-Isopropyltoluene 8260B 0.024 mg/kg dry 4020008-03 S-7 Acetone 8260B 0.11 mg/kg dry This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Sample Matrix: Solid Client Sample ID: S-5 Prism Sample ID: 4020008-01 Prism Work Order: 4020008 Time Collected: 01/31/14 10:00 Time Submitted: 01/31/14 18:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 63.1 % by 0.100 0.100 1 *SM2540 G 2/3/14 15:15 JAB P4130021 Weight Hexavalent Chromium 1.3 mg/kg dry 0.63 0.24 1 *7196A 215114 17:00 CDE P4130057 Organochlorine Pesticides by GC/ECD 4,4'-DDD BRL mg/kg dry 0.0032 0.00074 1 8081B 2/7/14 13:32 JMV P4130032 4,4'-DDE BRL mg/kg dry 0.0032 0.00057 1 8081B 2/7/14 13:32 JMV P4130032 4,4'-DDT BRL mg/kg dry 0.0048 0.0010 1 8081B 2/7/14 13:32 JMV P4130032 Aldrin BRL mg/kg dry 0.0032 0.00073 1 8081B 2/7/14 13:32 JMV P4130032 alpha-BHC BRL mg/kg dry 0.0032 0.00045 1 8081B 2/7/14 13:32 JMV P4130032 cis -Chlordane BRL mg/kg dry 0.0032 0.00062 1 8081B 2/7/14 13:32 JMV P4130032 beta-BHC BRL mg/kg dry 0.0032 0.00061 1 8081B 2/7/14 13:32 JMV P4130032 Chlordane BRL mg/kg dry 0.079 0.0084 1 8081B 2/7/14 13:32 JMV P4130032 delta-BHC BRL mg/kg dry 0.0032 0.00049 1 8081B 2/7/14 13:32 JMV P4130032 Dieldrin BRL mg/kg dry 0.0032 0.00056 1 8081B 2/7/14 13:32 JMV P4130032 Endosulfan I BRL mg/kg dry 0.0032 0.00070 1 8081B 2/7/14 13:32 JMV P4130032 Endosulfan 11 BRL mg/kg dry 0.0032 0.00076 1 8081B 2/7/14 13:32 JMV P4130032 Endosulfan Sulfate BRL mg/kg dry 0.0032 0.0010 1 8081B 2/7/14 13:32 JMV P4130032 Endrin BRL mg/kg dry 0.0032 0.00070 1 8081B 2/7/14 13:32 JMV P4130032 Endrin Aldehyde BRL mg/kg dry 0.0032 0.00087 1 8081B 2/7/14 13:32 JMV P4130032 Endrin Ketone BRL mg/kg dry 0.0032 0.00079 1 8081B 2/7/14 13:32 JMV P4130032 gamma-BHC BRL mg/kg dry 0.0032 0.00061 1 8081B 2/7/14 13:32 JMV P4130032 trans -Chlordane BRL mg/kg dry 0.0032 0.00085 1 8081B 2/7/14 13:32 JMV P4130032 Heptachlor BRL mg/kg dry 0.0032 0.0010 1 8081B 2/7/14 13:32 JMV P4130032 Heptachlor Epoxide BRL mg/kg dry 0.0032 0.00088 1 8081B 2/7/14 13:32 JMV P4130032 Methoxychlor BRL mg/kg dry 0.0032 0.0018 1 8081B 2/7/14 13:32 JMV P4130032 Toxaphene BRL mg/kg dry 0.079 0.0049 1 8081B 2/7/14 13:32 JMV P4130032 Surrogate Recovery Control Limits Decachlorobiphenyl 136 % 26-204 Tetrachloro-m-xylene 91 % 40-162 Polychlorinated Biphenyls (PCBs) by GC/ECD Aroclor 1016 BRL mg/kg dry 0.079 0.014 1 8082A 2/5/14 4:36 JMV P4130033 Aroclor 1221 BRL mg/kg dry 0.16 0.063 1 8082A 2/5/14 4:36 JMV P4130033 Aroclor 1232 BRL mg/kg dry 0.16 0.021 1 8082A 2/5/14 4:36 JMV P4130033 Aroclor 1242 BRL mg/kg dry 0.079 0.021 1 8082A 2/5/14 4:36 JMV 134130033 Aroclor 1248 BRL mg/kg dry 0.079 0.016 1 8082A 2/5/14 4:36 JMV P4130033 Aroclor 1254 BRL mg/kg dry 0.079 0.020 1 8082A 2/5/14 4:36 JMV P4130033 Aroclor 1260 BRL mg/kg dry 0.079 0.011 1 8082A 2/5/14 4:36 JMV P4130033 Surrogate Recovery Control Limits Tetrachloro-m-xylene 100 % 36-182 Decachlorobiphenyl 78 % 34-182 Semivolatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: S-5 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020008-01 1210 Trinity Road Prism Work Order: 4020008 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 01/31/14 10:00 Time Submitted: 01/31/14 18:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,2,4-Trichlorobenzene BRL mg/kg dry 0.52 0.19 1 8270D 2/4/14 16:06 KC P4130016 1,2-Dichlorobenzene BRL mg/kg dry 0.52 0.17 1 8270D 2/4/14 16:06 KC P4130016 1,3-Dichlorobenzene BRL mg/kg dry 0.52 0.18 1 8270D 2/4/14 16:06 KC P4130016 1,4-Dichlorobenzene BRL mg/kg dry 0.52 0.17 1 8270D 2/4/14 16:06 KC P4130016 1-Methyl naphthalene BRL mg/kg dry 0.52 0.12 1 8270D 2/4/14 16:06 KC P4130016 2,4,6-Trichlorophenol BRL mg/kg dry 0.52 0.17 1 8270D 2/4/14 16:06 KC P4130016 2,4-Dichlorophenol BRL mg/kg dry 0.52 0.19 1 8270D 2/4/14 16:06 KC P4130016 2,4-Dimethyl phenol BRL mg/kg dry 0.52 0.22 1 8270D 2/4/14 16:06 KC P4130016 2,4-Dinitrophenol BRL mg/kg dry 0.52 0.082 1 8270D 2/4/14 16:06 KC P4130016 2,4-Dinitrotoluene BRL mg/kg dry 0.52 0.089 1 8270D 2/4/14 16:06 KC P4130016 2,6-Dinitrotoluene BRL mg/kg dry 0.52 0.079 1 8270D 2/4/14 16:06 KC P4130016 2-Chloronaphthalene BRL mg/kg dry 0.52 0.18 1 8270D 2/4/14 16:06 KC P4130016 2-Chlorophenol BRL mg/kg dry 0.52 0.20 1 8270D 2/4/14 16:06 KC P4130016 2-Methyl naphthalene BRL mg/kg dry 0.52 0.19 1 8270D 2/4/14 16:06 KC P4130016 2-Methylphenol BRL mg/kg dry 0.52 0.18 1 8270D 2/4/14 16:06 KC P4130016 2-Nitrophenol BRL mg/kg dry 0.52 0.19 1 8270D 2/4/14 16:06 KC P4130016 3,3'-Dichlorobenzidine BRL mg/kg dry 0.52 0.087 1 8270D 2/4/14 16:06 KC P4130016 3/4-Methyl phenol BRL mg/kg dry 0.52 0.15 1 8270D 2/4/14 16:06 KC P4130016 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.52 0.056 1 8270D 2/4/14 16:06 KC P4130016 4-Bromophenyl phenyl ether BRL mg/kg dry 0.52 0.12 1 8270D 2/4/14 16:06 KC P4130016 4-Chloro-3-methylphenol BRL mg/kg dry 0.52 0.19 1 8270D 2/4/14 16:06 KC P4130016 4-Chloroaniline BRL mg/kg dry 0.52 0.18 1 8270D 2/4/14 16:06 KC P4130016 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.52 0.15 1 8270D 2/4/14 16:06 KC P4130016 4-Nitrophenol BRL mg/kg dry 0.52 0.065 1 8270D 2/4/14 16:06 KC P4130016 Acenaphthene BRL mg/kg dry 0.52 0.16 1 8270D 2/4/14 16:06 KC P4130016 Acenaphthylene BRL mg/kg dry 0.52 0.17 1 8270D 2/4/14 16:06 KC P4130016 Anthracene BRL mg/kg dry 0.52 0.10 1 8270D 2/4/14 16:06 KC P4130016 Azobenzene BRL mg/kg dry 0.52 0.12 1 8270D 2/4/14 16:06 KC P4130016 Benzo(a)anthracene BRL mg/kg dry 0.52 0.11 1 8270D 2/4/14 16:06 KC P4130016 Benzo(a)pyrene BRL mg/kg dry 0.52 0.098 1 8270D 2/4/14 16:06 KC P4130016 Benzo(b)fluoranthene BRL mg/kg dry 0.52 0.071 1 8270D 2/4/14 16:06 KC P4130016 Benzo(g,h,i)perylene BRL mg/kg dry 0.52 0.17 1 8270D 2/4/14 16:06 KC P4130016 Benzo(k)fluoranthene BRL mg/kg dry 0.52 0.15 1 8270D 2/4/14 16:06 KC P4130016 Benzoic Acid BRL mg/kg dry 0.52 0.069 1 8270D 2/4/14 16:06 KC P4130016 Benzyl alcohol BRL mg/kg dry 0.52 0.17 1 8270D 2/4/14 16:06 KC P4130016 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.52 0.27 1 8270D 2/4/14 16:06 KC P4130016 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.52 0.19 1 8270D 2/4/14 16:06 KC P4130016 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.52 0.21 1 8270D 2/4/14 16:06 KC P4130016 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.52 0.10 1 8270D 2/4/14 16:06 KC P4130016 Butyl benzyl phthalate BRL mg/kg dry 0.52 0.12 1 8270D 2/4/14 16:06 KC P4130016 Chrysene BRL mg/kg dry 0.52 0.12 1 8270D 2/4/14 16:06 KC P4130016 Dibenzo(a,h)anthracene BRL mg/kg dry 0.52 0.17 1 8270D 2/4/14 16:06 KC P4130016 Dibenzofuran BRL mg/kg dry 0.52 0.15 1 8270D 2/4/14 16:06 KC P4130016 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: S-5 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020008-01 1210 Trinity Road Prism Work Order: 4020008 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 01/31/14 10:00 Time Submitted: 01/31/14 18:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diethyl phthalate BRL mg/kg dry 0.52 0.094 1 8270D 2/4/14 16:06 KC P4130016 Dimethyl phthalate BRL mg/kg dry 0.52 0.098 1 8270D 2/4/14 16:06 KC P4130016 Di-n-butyl phthalate BRL mg/kg dry 0.52 0.12 1 8270D 2/4/14 16:06 KC P4130016 Di-n-octyl phthalate BRL mg/kg dry 0.52 0.12 1 8270D 2/4/14 16:06 KC P4130016 Fluoranthene BRL mg/kg dry 0.52 0.11 1 8270D 2/4/14 16:06 KC P4130016 Fluorene BRL mg/kg dry 0.52 0.12 1 8270D 2/4/14 16:06 KC P4130016 Hexachlorobenzene BRL mg/kg dry 0.52 0.087 1 8270D 2/4/14 16:06 KC P4130016 Hexachlorobutadiene BRL mg/kg dry 0.52 0.20 1 8270D 2/4/14 16:06 KC P4130016 Hexachlorocyclopentadiene BRL ICV mg/kg dry 0.52 0.16 1 8270D 2/4/14 16:06 KC P4130016 Hexachloroethane BRL mg/kg dry 0.52 0.17 1 8270D 2/4/14 16:06 KC P4130016 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.52 0.14 1 8270D 2/4/14 16:06 KC P4130016 Isophorone BRL mg/kg dry 0.52 0.19 1 8270D 2/4/14 16:06 KC P4130016 Naphthalene BRL mg/kg dry 0.52 0.20 1 8270D 2/4/14 16:06 KC P4130016 Nitrobenzene BRL mg/kg dry 0.52 0.18 1 8270D 2/4/14 16:06 KC P4130016 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.52 0.18 1 8270D 2/4/14 16:06 KC P4130016 N-Nitrosodiphenylamine BRL mg/kg dry 0.52 0.11 1 8270D 2/4/14 16:06 KC P4130016 Pentachlorophenol BRL mg/kg dry 0.52 0.043 1 8270D 2/4/14 16:06 KC P4130016 Phenanthrene BRL mg/kg dry 0.52 0.092 1 8270D 2/4/14 16:06 KC P4130016 Phenol BRL mg/kg dry 0.52 0.19 1 8270D 2/4/14 16:06 KC P4130016 Pyrene BRL mg/kg dry 0.52 0.14 1 8270D 2/4/14 16:06 KC P4130016 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 28 % 37-131 SR 2-Fluorobiphenyl 128 % 47-130 2-Fluorophenol 18 % 44-117 SR Nitrobenzene-d5 130 % 45-121 SR Phenol-d5 17 % 37-127 SR Terphenyl-d14 120 % 38-135 Total Metals Mercury 0.30 mg/kg dry 0.032 0.011 1 *7471B 214/14 14:20 MEH P4130029 Arsenic 37 mg/kg dry 0.40 0.059 1 *6010C 214114 19:18 BGM P4130025 Barium 2800 mg/kg dry 80 4.0 100 *6010C 2/5/14 20:32 BGM P4130025 Cadmium BRL mg/kg dry 0.40 0.0038 1 *6010C 2/4/14 19:18 BGM P4130025 Chromium 21 mg/kg dry 0.40 0.13 1 *6010C 2/4/14 19:18 BGM P4130025 Lead 10 mg/kg dry 0.40 0.047 1 *6010C 2/4/14 19:18 BGM P4130025 Selenium 3.2 mg/kg dry 0.80 0.097 1 *6010C 2/4/14 19:18 BGM P4130025 Silver BRL mg/kg dry 0.40 0.0064 1 *6010C 2/4/14 19:18 BGM P4130025 Volatile Organic Compounds by GC/MS 1,1,1-Trichloroethane BRL mg/kg dry 0.0074 0.00024 1 8260B 2/12/14 4:28 CGP P4130152 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0074 0.0012 1 8260B 2/12/14 4:28 CGP P4130152 1,1,2-Trichloroethane BRL mg/kg dry 0.0074 0.00062 1 8260B 2/12/14 4:28 CGP P4130152 1,1-Dichloroethane BRL mg/kg dry 0.0074 0.00062 1 8260B 2/12/14 4:28 CGP P4130152 1,1-Dichloroethylene BRL mg/kg dry 0.0074 0.00045 1 8260B 2/12/14 4:28 CGP P4130152 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: S-5 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020008-01 1210 Trinity Road Prism Work Order: 4020008 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 01/31/14 10:00 Time Submitted: 01/31/14 18:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1-Dichloropropylene BRL mg/kg dry 0.0074 0.00078 1 8260B 2/12/14 4:28 CGP P4130152 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0074 0.00055 1 8260B 2/12/14 4:28 CGP P4130152 1,2,3-Trichloropropane BRL mg/kg dry 0.0074 0.0011 1 8260B 2/12/14 4:28 CGP P4130152 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0074 0.00043 1 8260B 2/12/14 4:28 CGP P4130152 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0074 0.0015 1 8260B 2/12/14 4:28 CGP P4130152 1,2-Dibromoethane BRL mg/kg dry 0.0074 0.00085 1 8260B 2/12/14 4:28 CGP P4130152 1,2-Dichlorobenzene BRL mg/kg dry 0.0074 0.00033 1 8260B 2/12/14 4:28 CGP P4130152 1,2-Dichloroethane BRL mg/kg dry 0.0074 0.0012 1 8260B 2/12/14 4:28 CGP P4130152 1,2-Dichloropropane BRL mg/kg dry 0.0074 0.00047 1 8260B 2/12/14 4:28 CGP P4130152 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0074 0.00035 1 8260B 2/12/14 4:28 CGP P4130152 1,3-Dichlorobenzene BRL mg/kg dry 0.0074 0.00010 1 8260B 2/12/14 4:28 CGP P4130152 1,3-Dichloropropane BRL mg/kg dry 0.0074 0.00080 1 8260B 2/12/14 4:28 CGP P4130152 1,4-Dichlorobenzene BRL mg/kg dry 0.0074 0.00054 1 8260B 2/12/14 4:28 CGP P4130152 2,2-Dichloropropane BRL mg/kg dry 0.0074 0.00047 1 8260B 2/12/14 4:28 CGP P4130152 2-Chlorotoluene BRL mg/kg dry 0.0074 0.00045 1 8260B 2/12/14 4:28 CGP P4130152 4-Chlorotoluene BRL mg/kg dry 0.0074 0.00035 1 8260B 2/12/14 4:28 CGP P4130152 4-Isopropyltoluene 0.051 mg/kg dry 0.0074 0.00047 1 8260B 2/12/14 4:28 CGP P4130152 Acetone 0.14 mg/kg dry 0.074 0.0039 1 8260B 2/12/14 4:28 CGP P4130152 Benzene BRL mg/kg dry 0.0044 0.00045 1 8260B 2/12/14 4:28 CGP P4130152 Bromobenzene BRL mg/kg dry 0.0074 0.00031 1 8260B 2/12/14 4:28 CGP P4130152 Bromochloromethane BRL mg/kg dry 0.0074 0.0011 1 8260B 2/12/14 4:28 CGP P4130152 Bromodichloromethane BRL mg/kg dry 0.0074 0.00034 1 8260B 2/12/14 4:28 CGP P4130152 Bromoform BRL mg/kg dry 0.0074 0.0013 1 8260B 2/12/14 4:28 CGP P4130152 Bromomethane BRL mg/kg dry 0.015 0.0021 1 8260B 2/12/14 4:28 CGP P4130152 Carbon Tetrachloride BRL mg/kg dry 0.0074 0.00040 1 8260B 2/12/14 4:28 CGP P4130152 Chlorobenzene BRL mg/kg dry 0.0074 0.00034 1 8260B 2/12/14 4:28 CGP P4130152 Chloroethane BRL mg/kg dry 0.015 0.0056 1 8260B 2/12/14 4:28 CGP P4130152 Chloroform BRL mg/kg dry 0.0074 0.00031 1 8260B 2/12/14 4:28 CGP P4130152 Chloromethane BRL mg/kg dry 0.0074 0.0038 1 8260B 2/12/14 4:28 CGP P4130152 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0074 0.00060 1 8260B 2/12/14 4:28 CGP P4130152 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0074 0.00037 1 8260B 2/12/14 4:28 CGP P4130152 Dibromochloromethane BRL mg/kg dry 0.0074 0.00050 1 8260B 2/12/14 4:28 CGP P4130152 Dichlorodifluoromethane BRL mg/kg dry 0.0074 0.00079 1 8260B 2/12/14 4:28 CGP P4130152 Ethylbenzene BRL mg/kg dry 0.0074 0.00048 1 8260B 2/12/14 4:28 CGP P4130152 Isopropyl Ether BRL mg/kg dry 0.0074 0.00032 1 8260B 2/12/14 4:28 CGP P4130152 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0074 0.00037 1 8260B 2/12/14 4:28 CGP P4130152 m,p-Xylenes BRL mg/kg dry 0.015 0.00095 1 8260B 2/12/14 4:28 CGP P4130152 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.074 0.0015 1 8260B 2/12/14 4:28 CGP P4130152 Methyl Ethyl Ketone (2-Butanone) BRL A mg/kg dry 0.15 0.0026 1 8260B 2/12/14 4:28 CGP P4130152 Methyl Isobutyl Ketone BRL mg/kg dry 0.074 0.0020 1 8260B 2/12/14 4:28 CGP P4130152 Methylene Chloride BRL mg/kg dry 0.0074 0.00054 1 8260B 2/12/14 4:28 CGP P4130152 Methyl-tert-Butyl Ether BRL mg/kg dry 0.015 0.00057 1 8260B 2/12/14 4:28 CGP P4130152 Naphthalene BRL mg/kg dry 0.015 0.00054 1 8260B 2/12/14 4:28 CGP P4130152 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: S-5 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020008-01 1210 Trinity Road Prism Work Order: 4020008 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 01/31/14 10:00 Time Submitted: 01/31/14 18:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID n-Butylbenzene BRL mg/kg dry 0.0074 0.00033 1 8260B 2/12/14 4:28 CGP P4130152 n-Propylbenzene BRL mg/kg dry 0.0074 0.00042 1 8260B 2/12/14 4:28 CGP P4130152 o-Xylene BRL mg/kg dry 0.0074 0.00047 1 8260B 2/12/14 4:28 CGP P4130152 sec-Butylbenzene BRL mg/kg dry 0.0074 0.00030 1 8260B 2/12/14 4:28 CGP P4130152 Styrene BRL mg/kg dry 0.0074 0.00032 1 8260B 2/12/14 4:28 CGP P4130152 tert-Butylbenzene BRL mg/kg dry 0.0074 0.00038 1 8260B 2/12/14 4:28 CGP P4130152 Tetrachloroethylene BRL mg/kg dry 0.0074 0.00051 1 8260B 2/12/14 4:28 CGP P4130152 Toluene BRL mg/kg dry 0.0074 0.00044 1 8260B 2/12/14 4:28 CGP P4130152 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0074 0.00086 1 8260B 2/12/14 4:28 CGP P4130152 trans- 1,3-Dichloropropylene BRL mg/kg dry 0.0074 0.00036 1 8260B 2/12/14 4:28 CGP P4130152 Trichloroethylene BRL mg/kg dry 0.0074 0.00068 1 8260B 2/12/14 4:28 CGP P4130152 Trichlorofluoromethane BRL mg/kg dry 0.0074 0.00060 1 8260B 2/12/14 4:28 CGP P4130152 Vinyl acetate BRL mg/kg dry 0.037 0.0021 1 8260B 2/12/14 4:28 CGP P4130152 Vinyl chloride BRL mg/kg dry 0.0074 0.00096 1 8260B 2/12/14 4:28 CGP P4130152 Xylenes, total BRL mg/kg dry 0.022 0.0014 1 8260B 2/12/14 4:28 CGP P4130152 Surrogate Recovery Control Limits 4-Bromofluorobenzene 168 % 70-130 SR Dibromofluoromethane 105 % 84-123 Toluene-d8 90 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Sample Matrix: Solid Client Sample ID: S-6 Prism Sample ID: 4020008-02 Prism Work Order: 4020008 Time Collected: 01/31/14 10:30 Time Submitted: 01/31/14 18:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 60.1 % by 0.100 0.100 1 *SM2540 G 2/3/14 15:15 JAB P4130021 Weight Hexavalent Chromium 2.7 mg/kg dry 0.67 0.26 1 *7196A 215114 17:00 CDE P4130057 Organochlorine Pesticides by GC/ECD 4,4'-DDD BRL mg/kg dry 0.0033 0.00077 1 8081B 2/7/14 14:14 JMV P4130032 4,4'-DDE BRL mg/kg dry 0.0033 0.00060 1 8081B 2/7/14 14:14 JMV P4130032 4,4'-DDT BRL mg/kg dry 0.0050 0.0010 1 8081B 2/7/14 14:14 JMV P4130032 Aldrin BRL mg/kg dry 0.0033 0.00077 1 8081B 2/7/14 14:14 JMV P4130032 alpha-BHC BRL mg/kg dry 0.0033 0.00047 1 8081B 2/7/14 14:14 JMV P4130032 cis -Chlordane BRL mg/kg dry 0.0033 0.00065 1 8081B 2/7/14 14:14 JMV P4130032 beta-BHC BRL mg/kg dry 0.0033 0.00064 1 8081B 2/7/14 14:14 JMV P4130032 Chlordane BRL mg/kg dry 0.083 0.0088 1 8081B 2/7/14 14:14 JMV P4130032 delta-BHC BRL mg/kg dry 0.0033 0.00052 1 8081B 2/7/14 14:14 JMV P4130032 Dieldrin BRL mg/kg dry 0.0033 0.00059 1 8081B 2/7/14 14:14 JMV P4130032 Endosulfan I BRL mg/kg dry 0.0033 0.00073 1 8081B 2/7/14 14:14 JMV P4130032 Endosulfan 11 BRL mg/kg dry 0.0033 0.00080 1 8081B 2/7/14 14:14 JMV P4130032 Endosulfan Sulfate BRL mg/kg dry 0.0033 0.0011 1 8081B 2/7/14 14:14 JMV P4130032 Endrin BRL mg/kg dry 0.0033 0.00074 1 8081B 2/7/14 14:14 JMV P4130032 Endrin Aldehyde BRL mg/kg dry 0.0033 0.00091 1 8081B 2/7/14 14:14 JMV P4130032 Endrin Ketone BRL mg/kg dry 0.0033 0.00082 1 8081B 2/7/14 14:14 JMV P4130032 gamma-BHC BRL mg/kg dry 0.0033 0.00064 1 8081B 2/7/14 14:14 JMV P4130032 trans -Chlordane BRL mg/kg dry 0.0033 0.00089 1 8081B 2/7/14 14:14 JMV P4130032 Heptachlor BRL mg/kg dry 0.0033 0.0011 1 8081B 2/7/14 14:14 JMV P4130032 Heptachlor Epoxide BRL mg/kg dry 0.0033 0.00093 1 8081B 2/7/14 14:14 JMV P4130032 Methoxychlor BRL mg/kg dry 0.0033 0.0019 1 8081B 2/7/14 14:14 JMV P4130032 Toxaphene BRL mg/kg dry 0.083 0.0051 1 8081B 2/7/14 14:14 JMV P4130032 Surrogate Recovery Control Limits Decachlorobiphenyl 134 % 26-204 Tetrachloro-m-xylene 84 % 40-162 Polychlorinated Biphenyls (PCBs) by GC/ECD Aroclor 1016 BRL mg/kg dry 0.083 0.015 1 8082A 2/5/14 5:19 JMV P4130033 Aroclor 1221 BRL mg/kg dry 0.17 0.066 1 8082A 2/5/14 5:19 JMV P4130033 Aroclor 1232 BRL mg/kg dry 0.17 0.022 1 8082A 2/5/14 5:19 JMV P4130033 Aroclor 1242 BRL mg/kg dry 0.083 0.022 1 8082A 2/5/14 5:19 JMV 134130033 Aroclor 1248 BRL mg/kg dry 0.083 0.017 1 8082A 2/5/14 5:19 JMV P4130033 Aroclor 1254 BRL mg/kg dry 0.083 0.021 1 8082A 2/5/14 5:19 JMV P4130033 Aroclor 1260 BRL mg/kg dry 0.083 0.011 1 8082A 2/5/14 5:19 JMV P4130033 Surrogate Recovery Control Limits Tetrachloro-m-xylene 99 % 36-182 Decachlorobiphenyl 77 % 34-182 Semivolatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: S-6 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020008-02 1210 Trinity Road Prism Work Order: 4020008 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 01/31/14 10:30 Time Submitted: 01/31/14 18:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,2,4-Trichlorobenzene BRL mg/kg dry 0.55 0.20 1 8270D 2/4/14 16:28 KC P4130016 1,2-Dichlorobenzene BRL mg/kg dry 0.55 0.18 1 8270D 2/4/14 16:28 KC P4130016 1,3-Dichlorobenzene BRL mg/kg dry 0.55 0.18 1 8270D 2/4/14 16:28 KC P4130016 1,4-Dichlorobenzene BRL mg/kg dry 0.55 0.17 1 8270D 2/4/14 16:28 KC P4130016 1-Methyl naphthalene BRL mg/kg dry 0.55 0.13 1 8270D 2/4/14 16:28 KC P4130016 2,4,6-Trichlorophenol BRL mg/kg dry 0.55 0.18 1 8270D 2/4/14 16:28 KC P4130016 2,4-Dichlorophenol BRL mg/kg dry 0.55 0.19 1 8270D 2/4/14 16:28 KC P4130016 2,4-Dimethyl phenol BRL mg/kg dry 0.55 0.23 1 8270D 2/4/14 16:28 KC P4130016 2,4-Dinitrophenol BRL mg/kg dry 0.55 0.086 1 8270D 2/4/14 16:28 KC P4130016 2,4-Dinitrotoluene BRL mg/kg dry 0.55 0.094 1 8270D 2/4/14 16:28 KC P4130016 2,6-Dinitrotoluene BRL mg/kg dry 0.55 0.083 1 8270D 2/4/14 16:28 KC P4130016 2-Chloronaphthalene BRL mg/kg dry 0.55 0.19 1 8270D 2/4/14 16:28 KC P4130016 2-Chlorophenol BRL mg/kg dry 0.55 0.21 1 8270D 2/4/14 16:28 KC P4130016 2-Methyl naphthalene BRL mg/kg dry 0.55 0.20 1 8270D 2/4/14 16:28 KC P4130016 2-Methylphenol BRL mg/kg dry 0.55 0.19 1 8270D 2/4/14 16:28 KC P4130016 2-Nitrophenol BRL mg/kg dry 0.55 0.20 1 8270D 2/4/14 16:28 KC P4130016 3,3'-Dichlorobenzidine BRL mg/kg dry 0.55 0.092 1 8270D 2/4/14 16:28 KC P4130016 3/4-Methyl phenol BRL mg/kg dry 0.55 0.15 1 8270D 2/4/14 16:28 KC P4130016 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.55 0.059 1 8270D 2/4/14 16:28 KC P4130016 4-Bromophenyl phenyl ether BRL mg/kg dry 0.55 0.12 1 8270D 2/4/14 16:28 KC P4130016 4-Chloro-3-methylphenol BRL mg/kg dry 0.55 0.19 1 8270D 2/4/14 16:28 KC P4130016 4-Chloroaniline BRL mg/kg dry 0.55 0.19 1 8270D 2/4/14 16:28 KC P4130016 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.55 0.16 1 8270D 2/4/14 16:28 KC P4130016 4-Nitrophenol BRL mg/kg dry 0.55 0.068 1 8270D 2/4/14 16:28 KC P4130016 Acenaphthene BRL mg/kg dry 0.55 0.17 1 8270D 2/4/14 16:28 KC P4130016 Acenaphthylene BRL mg/kg dry 0.55 0.17 1 8270D 2/4/14 16:28 KC P4130016 Anthracene BRL mg/kg dry 0.55 0.11 1 8270D 2/4/14 16:28 KC P4130016 Azobenzene BRL mg/kg dry 0.55 0.13 1 8270D 2/4/14 16:28 KC P4130016 Benzo(a)anthracene BRL mg/kg dry 0.55 0.11 1 8270D 2/4/14 16:28 KC P4130016 Benzo(a)pyrene BRL mg/kg dry 0.55 0.10 1 8270D 2/4/14 16:28 KC P4130016 Benzo(b)fluoranthene BRL mg/kg dry 0.55 0.075 1 8270D 2/4/14 16:28 KC P4130016 Benzo(g,h,i)perylene BRL mg/kg dry 0.55 0.17 1 8270D 2/4/14 16:28 KC P4130016 Benzo(k)fluoranthene BRL mg/kg dry 0.55 0.16 1 8270D 2/4/14 16:28 KC P4130016 Benzoic Acid BRL mg/kg dry 0.55 0.073 1 8270D 2/4/14 16:28 KC P4130016 Benzyl alcohol BRL mg/kg dry 0.55 0.18 1 8270D 2/4/14 16:28 KC P4130016 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.55 0.28 1 8270D 2/4/14 16:28 KC P4130016 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.55 0.20 1 8270D 2/4/14 16:28 KC P4130016 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.55 0.22 1 8270D 2/4/14 16:28 KC P4130016 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.55 0.11 1 8270D 2/4/14 16:28 KC P4130016 Butyl benzyl phthalate BRL mg/kg dry 0.55 0.12 1 8270D 2/4/14 16:28 KC P4130016 Chrysene BRL mg/kg dry 0.55 0.12 1 8270D 2/4/14 16:28 KC P4130016 Dibenzo(a,h)anthracene BRL mg/kg dry 0.55 0.18 1 8270D 2/4/14 16:28 KC P4130016 Dibenzofuran BRL mg/kg dry 0.55 0.15 1 8270D 2/4/14 16:28 KC P4130016 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: S-6 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020008-02 1210 Trinity Road Prism Work Order: 4020008 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 01/31/14 10:30 Time Submitted: 01/31/14 18:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diethyl phthalate BRL mg/kg dry 0.55 0.099 1 8270D 2/4/14 16:28 KC P4130016 Dimethyl phthalate BRL mg/kg dry 0.55 0.10 1 8270D 2/4/14 16:28 KC P4130016 Di-n-butyl phthalate BRL mg/kg dry 0.55 0.13 1 8270D 2/4/14 16:28 KC P4130016 Di-n-octyl phthalate BRL mg/kg dry 0.55 0.12 1 8270D 2/4/14 16:28 KC P4130016 Fluoranthene BRL mg/kg dry 0.55 0.12 1 8270D 2/4/14 16:28 KC P4130016 Fluorene BRL mg/kg dry 0.55 0.13 1 8270D 2/4/14 16:28 KC P4130016 Hexachlorobenzene BRL mg/kg dry 0.55 0.092 1 8270D 2/4/14 16:28 KC P4130016 Hexachlorobutadiene BRL mg/kg dry 0.55 0.21 1 8270D 2/4/14 16:28 KC P4130016 Hexachlorocyclopentadiene BRL ICV mg/kg dry 0.55 0.17 1 8270D 2/4/14 16:28 KC P4130016 Hexachloroethane BRL mg/kg dry 0.55 0.18 1 8270D 2/4/14 16:28 KC P4130016 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.55 0.15 1 8270D 2/4/14 16:28 KC P4130016 Isophorone BRL mg/kg dry 0.55 0.20 1 8270D 2/4/14 16:28 KC P4130016 Naphthalene BRL mg/kg dry 0.55 0.21 1 8270D 2/4/14 16:28 KC P4130016 Nitrobenzene BRL mg/kg dry 0.55 0.18 1 8270D 2/4/14 16:28 KC P4130016 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.55 0.19 1 8270D 2/4/14 16:28 KC P4130016 N-Nitrosodiphenylamine BRL mg/kg dry 0.55 0.11 1 8270D 2/4/14 16:28 KC P4130016 Pentachlorophenol BRL mg/kg dry 0.55 0.045 1 8270D 2/4/14 16:28 KC P4130016 Phenanthrene BRL mg/kg dry 0.55 0.097 1 8270D 2/4/14 16:28 KC P4130016 Phenol BRL mg/kg dry 0.55 0.20 1 8270D 2/4/14 16:28 KC P4130016 Pyrene BRL mg/kg dry 0.55 0.15 1 8270D 2/4/14 16:28 KC P4130016 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 9 % 37-131 Aa 2-Fluorobiphenyl 80 % 47-130 2-Fluorophenol 10 % 44-117 Aa Nitrobenzene-d5 83 % 45-121 Phenol-d5 6 % 37-127 Aa Terphenyl-d14 74 % 38-135 Total Metals Mercury 0.42 mg/kg dry 0.036 0.012 1 *7471B 214/14 14:25 MEH P4130029 Arsenic 43 mg/kg dry 0.42 0.062 1 *6010C 214114 19:26 BGM P4130025 Barium 3200 mg/kg dry 84 4.2 100 *6010C 2/5/14 20:37 BGM P4130025 Cadmium BRL mg/kg dry 0.42 0.0040 1 *6010C 2/4/14 19:26 BGM P4130025 Chromium 22 mg/kg dry 0.42 0.14 1 *6010C 2/4/14 19:26 BGM P4130025 Lead 12 mg/kg dry 0.42 0.049 1 *6010C 2/4/14 19:26 BGM P4130025 Selenium 6.1 mg/kg dry 0.84 0.10 1 *6010C 2/4/14 19:26 BGM P4130025 Silver BRL mg/kg dry 0.42 0.0068 1 *6010C 2/4/14 19:26 BGM P4130025 Volatile Organic Compounds by GC/MS 1,1,1-Trichloroethane BRL mg/kg dry 0.0086 0.00028 1 8260B 2/12/14 23:04 MSC P4130223 1,1,2,2-Tetrachloroethane BRL CCV mg/kg dry 0.0086 0.0014 1 8260B 2/12/14 23:04 MSC P4130223 1,1,2-Trichloroethane BRL mg/kg dry 0.0086 0.00073 1 8260B 2/12/14 23:04 MSC P4130223 1,1-Dichloroethane BRL mg/kg dry 0.0086 0.00073 1 8260B 2/12/14 23:04 MSC P4130223 1,1-Dichloroethylene BRL mg/kg dry 0.0086 0.00052 1 8260B 2/12/14 23:04 MSC P4130223 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: S-6 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020008-02 1210 Trinity Road Prism Work Order: 4020008 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 01/31/14 10:30 Time Submitted: 01/31/14 18:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1-Dichloropropylene BRL mg/kg dry 0.0086 0.00091 1 8260B 2/12/14 23:04 MSC P4130223 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0086 0.00064 1 8260B 2/12/14 23:04 MSC P4130223 1,2,3-Trichloropropane BRL CCV mg/kg dry 0.0086 0.0013 1 8260B 2/12/14 23:04 MSC P4130223 1,2,4-Trichlorobenzene BRL CCV mg/kg dry 0.0086 0.00051 1 8260B 2/12/14 23:04 MSC P4130223 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0086 0.0017 1 8260B 2/12/14 23:04 MSC P4130223 1,2-Dibromoethane BRL mg/kg dry 0.0086 0.00099 1 8260B 2/12/14 23:04 MSC P4130223 1,2-Dichlorobenzene BRL mg/kg dry 0.0086 0.00039 1 8260B 2/12/14 23:04 MSC P4130223 1,2-Dichloroethane BRL mg/kg dry 0.0086 0.0014 1 8260B 2/12/14 23:04 MSC P4130223 1,2-Dichloropropane BRL mg/kg dry 0.0086 0.00055 1 8260B 2/12/14 23:04 MSC P4130223 1,3,5-Trimethyl benzene BRL CCV mg/kg dry 0.0086 0.00041 1 8260B 2/12/14 23:04 MSC P4130223 1,3-Dichlorobenzene BRL mg/kg dry 0.0086 0.00012 1 8260B 2/12/14 23:04 MSC P4130223 1,3-Dichloropropane BRL mg/kg dry 0.0086 0.00093 1 8260B 2/12/14 23:04 MSC P4130223 1,4-Dichlorobenzene BRL mg/kg dry 0.0086 0.00063 1 8260B 2/12/14 23:04 MSC P4130223 2,2-Dichloropropane BRL mg/kg dry 0.0086 0.00054 1 8260B 2/12/14 23:04 MSC P4130223 2-Chlorotoluene BRL CCV mg/kg dry 0.0086 0.00053 1 8260B 2/12/14 23:04 MSC P4130223 4-Chlorotoluene BRL mg/kg dry 0.0086 0.00040 1 8260B 2/12/14 23:04 MSC P4130223 4-Isopropyltoluene BRL mg/kg dry 0.0086 0.00055 1 8260B 2/12/14 23:04 MSC P4130223 Acetone 0.17 mg/kg dry 0.086 0.0046 1 8260B 2/12/14 23:04 MSC P4130223 Benzene BRL mg/kg dry 0.0052 0.00052 1 8260B 2/12/14 23:04 MSC P4130223 Bromobenzene BRL CCV mg/kg dry 0.0086 0.00037 1 8260B 2/12/14 23:04 MSC P4130223 Bromochloromethane BRL mg/kg dry 0.0086 0.0013 1 8260B 2/12/14 23:04 MSC P4130223 Bromodichloromethane BRL mg/kg dry 0.0086 0.00040 1 8260B 2/12/14 23:04 MSC P4130223 Bromoform BRL mg/kg dry 0.0086 0.0015 1 8260B 2/12/14 23:04 MSC P4130223 Bromomethane BRL mg/kg dry 0.017 0.0024 1 8260B 2/12/14 23:04 MSC P4130223 Carbon Tetrachloride BRL mg/kg dry 0.0086 0.00047 1 8260B 2/12/14 23:04 MSC P4130223 Chlorobenzene BRL mg/kg dry 0.0086 0.00040 1 8260B 2/12/14 23:04 MSC P4130223 Chloroethane BRL mg/kg dry 0.017 0.0065 1 8260B 2/12/14 23:04 MSC P4130223 Chloroform BRL mg/kg dry 0.0086 0.00036 1 8260B 2/12/14 23:04 MSC P4130223 Chloromethane BRL mg/kg dry 0.0086 0.0044 1 8260B 2/12/14 23:04 MSC P4130223 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0086 0.00070 1 8260B 2/12/14 23:04 MSC P4130223 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0086 0.00043 1 8260B 2/12/14 23:04 MSC P4130223 Dibromochloromethane BRL mg/kg dry 0.0086 0.00059 1 8260B 2/12/14 23:04 MSC P4130223 Dichlorodifluoromethane BRL mg/kg dry 0.0086 0.00092 1 8260B 2/12/14 23:04 MSC P4130223 Ethylbenzene BRL mg/kg dry 0.0086 0.00055 1 8260B 2/12/14 23:04 MSC P4130223 Isopropyl Ether BRL mg/kg dry 0.0086 0.00037 1 8260B 2/12/14 23:04 MSC P4130223 Isopropylbenzene (Cumene) BRL CCV mg/kg dry 0.0086 0.00043 1 8260B 2/12/14 23:04 MSC P4130223 m,p-Xylenes BRL mg/kg dry 0.017 0.0011 1 8260B 2/12/14 23:04 MSC P4130223 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.086 0.0018 1 8260B 2/12/14 23:04 MSC P4130223 Methyl Ethyl Ketone (2-Butanone) 0.0086 J mg/kg dry 0.17 0.0031 1 8260B 2/12/14 23:04 MSC P4130223 Methyl Isobutyl Ketone BRL mg/kg dry 0.086 0.0023 1 8260B 2/12/14 23:04 MSC P4130223 Methylene Chloride BRL mg/kg dry 0.0086 0.00063 1 8260B 2/12/14 23:04 MSC P4130223 Methyl-tert-Butyl Ether BRL mg/kg dry 0.017 0.00066 1 8260B 2/12/14 23:04 MSC P4130223 Naphthalene BRL mg/kg dry 0.017 0.00063 1 8260B 2/12/14 23:04 MSC P4130223 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 35 /P R I S M Full -Service Analytical Environmental Solutions LA6pAATOA I E6 - Laboratory Report 02/18/2014 Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Sample Matrix: Solid Client Sample ID: S-6 Prism Sample ID: 4020008-02 Prism Work Order: 4020008 Time Collected: 01/31/14 10:30 Time Submitted: 01/31/14 18:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID n-Butylbenzene BRL mg/kg dry 0.0086 0.00038 1 8260B 2/12/14 23:04 MSC P4130223 n-Propylbenzene BRL mg/kg dry 0.0086 0.00049 1 8260B 2/12/14 23:04 MSC P4130223 o-Xylene BRL mg/kg dry 0.0086 0.00055 1 8260B 2/12/14 23:04 MSC P4130223 sec-Butylbenzene BRL CCV mg/kg dry 0.0086 0.00035 1 8260B 2/12/14 23:04 MSC P4130223 Styrene BRL mg/kg dry 0.0086 0.00038 1 8260B 2/12/14 23:04 MSC P4130223 tert-Butylbenzene BRL CCV mg/kg dry 0.0086 0.00045 1 8260B 2/12/14 23:04 MSC P4130223 Tetrachloroethylene BRL mg/kg dry 0.0086 0.00060 1 8260B 2/12/14 23:04 MSC P4130223 Toluene BRL mg/kg dry 0.0086 0.00051 1 8260B 2/12/14 23:04 MSC P4130223 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0086 0.0010 1 8260B 2/12/14 23:04 MSC P4130223 trans- 1,3-Dichloropropylene BRL mg/kg dry 0.0086 0.00042 1 8260B 2/12/14 23:04 MSC P4130223 Trichloroethylene BRL mg/kg dry 0.0086 0.00080 1 8260B 2/12/14 23:04 MSC P4130223 Trichlorofluoromethane BRL mg/kg dry 0.0086 0.00070 1 8260B 2/12/14 23:04 MSC P4130223 Vinyl acetate BRL mg/kg dry 0.043 0.0024 1 8260B 2/12/14 23:04 MSC P4130223 Vinyl chloride BRL mg/kg dry 0.0086 0.0011 1 8260B 2/12/14 23:04 MSC P4130223 Xylenes, total BRL mg/kg dry 0.026 0.0016 1 8260B 2/12/14 23:04 MSC P4130223 Surrogate Recovery Control Limits 4-Bromofluorobenzene 83 % 70-130 Dibromofluoromethane 116 % 84-123 Toluene-d8 122 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Sample Matrix: Solid Client Sample ID: S-7 Prism Sample ID: 4020008-03 Prism Work Order: 4020008 Time Collected: 01/31/14 11:00 Time Submitted: 01/31/14 18:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 61.1 % by 0.100 0.100 1 *SM2540 G 2/3/14 15:15 JAB P4130021 Weight Hexavalent Chromium 1.4 mg/kg dry 0.65 0.25 1 *7196A 215114 17:00 CDE P4130057 Organochlorine Pesticides by GC/ECD 4,4'-DDD BRL mg/kg dry 0.0033 0.00076 1 8081B 2/7/14 14:57 JMV P4130032 4,4'-DDE BRL mg/kg dry 0.0033 0.00059 1 8081B 2/7/14 14:57 JMV P4130032 4,4'-DDT BRL mg/kg dry 0.0049 0.0010 1 8081B 2/7/14 14:57 JMV P4130032 Aldrin BRL mg/kg dry 0.0033 0.00075 1 8081B 2/7/14 14:57 JMV P4130032 alpha-BHC BRL mg/kg dry 0.0033 0.00046 1 8081B 2/7/14 14:57 JMV P4130032 cis -Chlordane BRL mg/kg dry 0.0033 0.00064 1 8081B 2/7/14 14:57 JMV P4130032 beta-BHC BRL mg/kg dry 0.0033 0.00063 1 8081B 2/7/14 14:57 JMV P4130032 Chlordane BRL mg/kg dry 0.082 0.0086 1 8081B 2/7/14 14:57 JMV P4130032 delta-BHC BRL mg/kg dry 0.0033 0.00051 1 8081B 2/7/14 14:57 JMV P4130032 Dieldrin BRL mg/kg dry 0.0033 0.00058 1 8081B 2/7/14 14:57 JMV P4130032 Endosulfan I BRL mg/kg dry 0.0033 0.00072 1 8081B 2/7/14 14:57 JMV P4130032 Endosulfan 11 BRL mg/kg dry 0.0033 0.00078 1 8081B 2/7/14 14:57 JMV P4130032 Endosulfan Sulfate BRL mg/kg dry 0.0033 0.0011 1 8081B 2/7/14 14:57 JMV P4130032 Endrin BRL mg/kg dry 0.0033 0.00073 1 8081B 2/7/14 14:57 JMV P4130032 Endrin Aldehyde BRL mg/kg dry 0.0033 0.00089 1 8081B 2/7/14 14:57 JMV P4130032 Endrin Ketone BRL mg/kg dry 0.0033 0.00081 1 8081B 2/7/14 14:57 JMV P4130032 gamma-BHC BRL mg/kg dry 0.0033 0.00063 1 8081B 2/7/14 14:57 JMV P4130032 trans -Chlordane BRL mg/kg dry 0.0033 0.00088 1 8081B 2/7/14 14:57 JMV P4130032 Heptachlor BRL mg/kg dry 0.0033 0.0010 1 8081B 2/7/14 14:57 JMV P4130032 Heptachlor Epoxide BRL mg/kg dry 0.0033 0.00091 1 8081B 2/7/14 14:57 JMV P4130032 Methoxychlor BRL mg/kg dry 0.0033 0.0019 1 8081B 2/7/14 14:57 JMV P4130032 Toxaphene 0.17 mg/kg dry 0.082 0.0051 1 8081B 2/7/14 14:57 JMV P4130032 Polychlorinated Biphenyls (PCBs) by GC/ECD Surrogate Decachlorobiphenyl Tetrachloro-m-xylene Recovery 127 % 80 % Control Limits 26-204 40-162 Aroclor 1016 BRL mg/kg dry 0.082 0.015 1 8082A 2/5/14 6:03 JMV P4130033 Aroclor 1221 BRL mg/kg dry 0.16 0.065 1 8082A 2/5/14 6:03 JMV P4130033 Aroclor 1232 BRL mg/kg dry 0.16 0.021 1 8082A 2/5/14 6:03 JMV P4130033 Aroclor 1242 BRL mg/kg dry 0.082 0.022 1 8082A 2/5/14 6:03 JMV P4130033 Aroclor 1248 BRL mg/kg dry 0.082 0.016 1 8082A 2/5/14 6:03 JMV P4130033 Aroclor 1254 BRL mg/kg dry 0.082 0.020 1 8082A 2/5/14 6:03 JMV P4130033 Aroclor 1260 BRL mg/kg dry 0.082 0.011 1 8082A 2/5/14 6:03 JMV P4130033 Surrogate Recovery Control Limits Tetrachloro-m-xylene 96 % 36-182 Decachlorobiphenyl 72 % 34-182 Semivolatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: S-7 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020008-03 1210 Trinity Road Prism Work Order: 4020008 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 01/31/14 11:00 Time Submitted: 01/31/14 18:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,2,4-Trichlorobenzene BRL mg/kg dry 0.54 0.20 1 8270D 2/4/14 16:49 KC P4130016 1,2-Dichlorobenzene BRL mg/kg dry 0.54 0.18 1 8270D 2/4/14 16:49 KC P4130016 1,3-Dichlorobenzene BRL mg/kg dry 0.54 0.18 1 8270D 2/4/14 16:49 KC P4130016 1,4-Dichlorobenzene BRL mg/kg dry 0.54 0.17 1 8270D 2/4/14 16:49 KC P4130016 1-Methyl naphthalene BRL mg/kg dry 0.54 0.13 1 8270D 2/4/14 16:49 KC P4130016 2,4,6-Trichlorophenol BRL mg/kg dry 0.54 0.18 1 8270D 2/4/14 16:49 KC P4130016 2,4-Dichlorophenol BRL mg/kg dry 0.54 0.19 1 8270D 2/4/14 16:49 KC P4130016 2,4-Dimethyl phenol BRL mg/kg dry 0.54 0.22 1 8270D 2/4/14 16:49 KC P4130016 2,4-Dinitrophenol BRL mg/kg dry 0.54 0.085 1 8270D 2/4/14 16:49 KC P4130016 2,4-Dinitrotoluene BRL mg/kg dry 0.54 0.092 1 8270D 2/4/14 16:49 KC P4130016 2,6-Dinitrotoluene BRL mg/kg dry 0.54 0.082 1 8270D 2/4/14 16:49 KC P4130016 2-Chloronaphthalene BRL mg/kg dry 0.54 0.19 1 8270D 2/4/14 16:49 KC P4130016 2-Chlorophenol BRL mg/kg dry 0.54 0.20 1 8270D 2/4/14 16:49 KC P4130016 2-Methyl naphthalene BRL mg/kg dry 0.54 0.20 1 8270D 2/4/14 16:49 KC P4130016 2-Methylphenol BRL mg/kg dry 0.54 0.19 1 8270D 2/4/14 16:49 KC P4130016 2-Nitrophenol BRL mg/kg dry 0.54 0.20 1 8270D 2/4/14 16:49 KC P4130016 3,3'-Dichlorobenzidine BRL mg/kg dry 0.54 0.090 1 8270D 2/4/14 16:49 KC P4130016 3/4-Methyl phenol BRL mg/kg dry 0.54 0.15 1 8270D 2/4/14 16:49 KC P4130016 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.54 0.058 1 8270D 2/4/14 16:49 KC P4130016 4-Bromophenyl phenyl ether BRL mg/kg dry 0.54 0.12 1 8270D 2/4/14 16:49 KC P4130016 4-Chloro-3-methylphenol BRL mg/kg dry 0.54 0.19 1 8270D 2/4/14 16:49 KC P4130016 4-Chloroaniline BRL mg/kg dry 0.54 0.19 1 8270D 2/4/14 16:49 KC P4130016 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.54 0.16 1 8270D 2/4/14 16:49 KC P4130016 4-Nitrophenol BRL mg/kg dry 0.54 0.067 1 8270D 2/4/14 16:49 KC P4130016 Acenaphthene BRL mg/kg dry 0.54 0.17 1 8270D 2/4/14 16:49 KC P4130016 Acenaphthylene BRL mg/kg dry 0.54 0.17 1 8270D 2/4/14 16:49 KC P4130016 Anthracene BRL mg/kg dry 0.54 0.11 1 8270D 2/4/14 16:49 KC P4130016 Azobenzene BRL mg/kg dry 0.54 0.12 1 8270D 2/4/14 16:49 KC P4130016 Benzo(a)anthracene BRL mg/kg dry 0.54 0.11 1 8270D 2/4/14 16:49 KC P4130016 Benzo(a)pyrene BRL mg/kg dry 0.54 0.10 1 8270D 2/4/14 16:49 KC P4130016 Benzo(b)fluoranthene BRL mg/kg dry 0.54 0.074 1 8270D 2/4/14 16:49 KC P4130016 Benzo(g,h,i)perylene BRL mg/kg dry 0.54 0.17 1 8270D 2/4/14 16:49 KC P4130016 Benzo(k)fluoranthene BRL mg/kg dry 0.54 0.16 1 8270D 2/4/14 16:49 KC P4130016 Benzoic Acid BRL mg/kg dry 0.54 0.071 1 8270D 2/4/14 16:49 KC P4130016 Benzyl alcohol BRL mg/kg dry 0.54 0.18 1 8270D 2/4/14 16:49 KC P4130016 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.54 0.28 1 8270D 2/4/14 16:49 KC P4130016 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.54 0.20 1 8270D 2/4/14 16:49 KC P4130016 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.54 0.21 1 8270D 2/4/14 16:49 KC P4130016 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.54 0.10 1 8270D 2/4/14 16:49 KC P4130016 Butyl benzyl phthalate BRL mg/kg dry 0.54 0.12 1 8270D 2/4/14 16:49 KC P4130016 Chrysene BRL mg/kg dry 0.54 0.12 1 8270D 2/4/14 16:49 KC P4130016 Dibenzo(a,h)anthracene BRL mg/kg dry 0.54 0.18 1 8270D 2/4/14 16:49 KC P4130016 Dibenzofuran BRL mg/kg dry 0.54 0.15 1 8270D 2/4/14 16:49 KC P4130016 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: S-7 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020008-03 1210 Trinity Road Prism Work Order: 4020008 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 01/31/14 11:00 Time Submitted: 01/31/14 18:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diethyl phthalate BRL mg/kg dry 0.54 0.097 1 8270D 2/4/14 16:49 KC P4130016 Dimethyl phthalate BRL mg/kg dry 0.54 0.10 1 8270D 2/4/14 16:49 KC P4130016 Di-n-butyl phthalate BRL mg/kg dry 0.54 0.13 1 8270D 2/4/14 16:49 KC P4130016 Di-n-octyl phthalate BRL mg/kg dry 0.54 0.12 1 8270D 2/4/14 16:49 KC P4130016 Fluoranthene BRL mg/kg dry 0.54 0.11 1 8270D 2/4/14 16:49 KC P4130016 Fluorene BRL mg/kg dry 0.54 0.13 1 8270D 2/4/14 16:49 KC P4130016 Hexachlorobenzene BRL mg/kg dry 0.54 0.090 1 8270D 2/4/14 16:49 KC P4130016 Hexachlorobutadiene BRL mg/kg dry 0.54 0.20 1 8270D 2/4/14 16:49 KC P4130016 Hexachlorocyclopentadiene BRL ICV mg/kg dry 0.54 0.16 1 8270D 2/4/14 16:49 KC P4130016 Hexachloroethane BRL mg/kg dry 0.54 0.18 1 8270D 2/4/14 16:49 KC P4130016 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.54 0.14 1 8270D 2/4/14 16:49 KC P4130016 Isophorone BRL mg/kg dry 0.54 0.20 1 8270D 2/4/14 16:49 KC P4130016 Naphthalene BRL mg/kg dry 0.54 0.21 1 8270D 2/4/14 16:49 KC P4130016 Nitrobenzene BRL mg/kg dry 0.54 0.18 1 8270D 2/4/14 16:49 KC P4130016 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.54 0.18 1 8270D 2/4/14 16:49 KC P4130016 N-Nitrosodiphenylamine BRL mg/kg dry 0.54 0.11 1 8270D 2/4/14 16:49 KC P4130016 Pentachlorophenol BRL mg/kg dry 0.54 0.044 1 8270D 2/4/14 16:49 KC P4130016 Phenanthrene BRL mg/kg dry 0.54 0.095 1 8270D 2/4/14 16:49 KC P4130016 Phenol BRL mg/kg dry 0.54 0.20 1 8270D 2/4/14 16:49 KC P4130016 Pyrene BRL mg/kg dry 0.54 0.15 1 8270D 2/4/14 16:49 KC P4130016 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 9 % 37-131 SR 2-Fluorobiphenyl 79 % 47-130 2-Fluorophenol 14 % 44-117 SR Nitrobenzene-d5 80 % 45-121 Phenol-d5 15 % 37-127 SR Terphenyl-d14 67 % 38-135 Total Metals Mercury 0.44 mg/kg dry 0.034 0.011 1 *7471B 214/14 14:29 MEH P4130029 Arsenic 44 mg/kg dry 0.42 0.061 1 *6010C 214114 19:34 BGM P4130025 Barium 2500 mg/kg dry 83 4.2 100 *6010C 2/5/14 20:42 BGM P4130025 Cadmium BRL mg/kg dry 0.42 0.0040 1 *6010C 2/4/14 19:34 BGM P4130025 Chromium 29 mg/kg dry 0.42 0.13 1 *6010C 2/4/14 19:34 BGM P4130025 Lead 11 mg/kg dry 0.42 0.049 1 *6010C 2/4/14 19:34 BGM P4130025 Selenium 4.5 mg/kg dry 0.83 0.10 1 *6010C 2/4/14 19:34 BGM P4130025 Silver BRL mg/kg dry 0.42 0.0067 1 *6010C 2/4/14 19:34 BGM P4130025 Volatile Organic Compounds by GC/MS 1,1,1-Trichloroethane BRL mg/kg dry 0.0081 0.00026 1 8260B 2/12/14 23:35 MSC P4130223 1,1,2,2-Tetrachloroethane BRL CCV mg/kg dry 0.0081 0.0013 1 8260B 2/12/14 23:35 MSC P4130223 1,1,2-Trichloroethane BRL mg/kg dry 0.0081 0.00068 1 8260B 2/12/14 23:35 MSC P4130223 1,1-Dichloroethane BRL mg/kg dry 0.0081 0.00068 1 8260B 2/12/14 23:35 MSC P4130223 1,1-Dichloroethylene BRL mg/kg dry 0.0081 0.00049 1 8260B 2/12/14 23:35 MSC P4130223 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 35 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/18/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: S-7 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020008-03 1210 Trinity Road Prism Work Order: 4020008 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 01/31/14 11:00 Time Submitted: 01/31/14 18:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID 1,1-Dichloropropylene BRL mg/kg dry 0.0081 0.00085 1 8260B 2/12/14 23:35 MSC P4130223 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0081 0.00060 1 8260B 2/12/14 23:35 MSC P4130223 1,2,3-Trichloropropane BRL CCV mg/kg dry 0.0081 0.0012 1 8260B 2/12/14 23:35 MSC P4130223 1,2,4-Trichlorobenzene BRL CCV mg/kg dry 0.0081 0.00047 1 8260B 2/12/14 23:35 MSC P4130223 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0081 0.0016 1 8260B 2/12/14 23:35 MSC P4130223 1,2-Dibromoethane BRL mg/kg dry 0.0081 0.00093 1 8260B 2/12/14 23:35 MSC P4130223 1,2-Dichlorobenzene BRL mg/kg dry 0.0081 0.00036 1 8260B 2/12/14 23:35 MSC P4130223 1,2-Dichloroethane BRL mg/kg dry 0.0081 0.0013 1 8260B 2/12/14 23:35 MSC P4130223 1,2-Dichloropropane BRL mg/kg dry 0.0081 0.00051 1 8260B 2/12/14 23:35 MSC P4130223 1,3,5-Trimethyl benzene BRL CCV mg/kg dry 0.0081 0.00039 1 8260B 2/12/14 23:35 MSC P4130223 1,3-Dichlorobenzene BRL mg/kg dry 0.0081 0.00011 1 8260B 2/12/14 23:35 MSC P4130223 1,3-Dichloropropane BRL mg/kg dry 0.0081 0.00087 1 8260B 2/12/14 23:35 MSC P4130223 1,4-Dichlorobenzene BRL mg/kg dry 0.0081 0.00059 1 8260B 2/12/14 23:35 MSC P4130223 2,2-Dichloropropane BRL mg/kg dry 0.0081 0.00051 1 8260B 2/12/14 23:35 MSC P4130223 2-Chlorotoluene BRL CCV mg/kg dry 0.0081 0.00049 1 8260B 2/12/14 23:35 MSC P4130223 4-Chlorotoluene BRL mg/kg dry 0.0081 0.00038 1 8260B 2/12/14 23:35 MSC P4130223 4-Isopropyltoluene 0.024 mg/kg dry 0.0081 0.00051 1 8260B 2/12/14 23:35 MSC P4130223 Acetone 0.11 mg/kg dry 0.081 0.0043 1 8260B 2/12/14 23:35 MSC P4130223 Benzene BRL mg/kg dry 0.0048 0.00049 1 8260B 2/12/14 23:35 MSC P4130223 Bromobenzene BRL CCV mg/kg dry 0.0081 0.00034 1 8260B 2/12/14 23:35 MSC P4130223 Bromochloromethane BRL mg/kg dry 0.0081 0.0012 1 8260B 2/12/14 23:35 MSC P4130223 Bromodichloromethane BRL mg/kg dry 0.0081 0.00037 1 8260B 2/12/14 23:35 MSC P4130223 Bromoform BRL mg/kg dry 0.0081 0.0014 1 8260B 2/12/14 23:35 MSC P4130223 Bromomethane BRL mg/kg dry 0.016 0.0023 1 8260B 2/12/14 23:35 MSC P4130223 Carbon Tetrachloride BRL mg/kg dry 0.0081 0.00044 1 8260B 2/12/14 23:35 MSC P4130223 Chlorobenzene BRL mg/kg dry 0.0081 0.00038 1 8260B 2/12/14 23:35 MSC P4130223 Chloroethane BRL mg/kg dry 0.016 0.0061 1 8260B 2/12/14 23:35 MSC P4130223 Chloroform BRL mg/kg dry 0.0081 0.00034 1 8260B 2/12/14 23:35 MSC P4130223 Chloromethane BRL mg/kg dry 0.0081 0.0041 1 8260B 2/12/14 23:35 MSC P4130223 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0081 0.00065 1 8260B 2/12/14 23:35 MSC P4130223 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0081 0.00040 1 8260B 2/12/14 23:35 MSC P4130223 Dibromochloromethane BRL mg/kg dry 0.0081 0.00055 1 8260B 2/12/14 23:35 MSC P4130223 Dichlorodifluoromethane BRL mg/kg dry 0.0081 0.00087 1 8260B 2/12/14 23:35 MSC P4130223 Ethylbenzene BRL mg/kg dry 0.0081 0.00052 1 8260B 2/12/14 23:35 MSC P4130223 Isopropyl Ether BRL mg/kg dry 0.0081 0.00035 1 8260B 2/12/14 23:35 MSC P4130223 Isopropylbenzene (Cumene) BRL CCV mg/kg dry 0.0081 0.00040 1 8260B 2/12/14 23:35 MSC P4130223 m,p-Xylenes BRL mg/kg dry 0.016 0.0010 1 8260B 2/12/14 23:35 MSC P4130223 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.081 0.0017 1 8260B 2/12/14 23:35 MSC P4130223 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.16 0.0029 1 8260B 2/12/14 23:35 MSC P4130223 Methyl Isobutyl Ketone BRL mg/kg dry 0.081 0.0021 1 8260B 2/12/14 23:35 MSC P4130223 Methylene Chloride BRL mg/kg dry 0.0081 0.00059 1 8260B 2/12/14 23:35 MSC P4130223 Methyl-tert-Butyl Ether BRL mg/kg dry 0.016 0.00062 1 8260B 2/12/14 23:35 MSC P4130223 Naphthalene BRL mg/kg dry 0.016 0.00059 1 8260B 2/12/14 23:35 MSC P4130223 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 35 /P R I S M Full -Service Analytical Environmental Solutions LA6pAATOA I E6 - Laboratory Report 02/18/2014 Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Sample Matrix: Solid Client Sample ID: S-7 Prism Sample ID: 4020008-03 Prism Work Order: 4020008 Time Collected: 01/31/14 11:00 Time Submitted: 01/31/14 18:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID n-Butylbenzene BRL mg/kg dry 0.0081 0.00036 1 8260B 2/12/14 23:35 MSC P4130223 n-Propylbenzene BRL mg/kg dry 0.0081 0.00046 1 8260B 2/12/14 23:35 MSC P4130223 o-Xylene BRL mg/kg dry 0.0081 0.00051 1 8260B 2/12/14 23:35 MSC P4130223 sec-Butylbenzene BRL CCV mg/kg dry 0.0081 0.00033 1 8260B 2/12/14 23:35 MSC P4130223 Styrene BRL mg/kg dry 0.0081 0.00035 1 8260B 2/12/14 23:35 MSC P4130223 tert-Butylbenzene BRL CCV mg/kg dry 0.0081 0.00042 1 8260B 2/12/14 23:35 MSC P4130223 Tetrachloroethylene BRL mg/kg dry 0.0081 0.00056 1 8260B 2/12/14 23:35 MSC P4130223 Toluene BRL mg/kg dry 0.0081 0.00048 1 8260B 2/12/14 23:35 MSC P4130223 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0081 0.00093 1 8260B 2/12/14 23:35 MSC P4130223 trans- 1,3-Dichloropropylene BRL mg/kg dry 0.0081 0.00039 1 8260B 2/12/14 23:35 MSC P4130223 Trichloroethylene BRL mg/kg dry 0.0081 0.00075 1 8260B 2/12/14 23:35 MSC P4130223 Trichlorofluoromethane BRL mg/kg dry 0.0081 0.00066 1 8260B 2/12/14 23:35 MSC P4130223 Vinyl acetate BRL mg/kg dry 0.040 0.0023 1 8260B 2/12/14 23:35 MSC P4130223 Vinyl chloride BRL mg/kg dry 0.0081 0.0010 1 8260B 2/12/14 23:35 MSC P4130223 Xylenes, total BRL mg/kg dry 0.024 0.0015 1 8260B 2/12/14 23:35 MSC P4130223 Surrogate Recovery Control Limits 4-Bromofluorobenzene 114 % 70-130 Dibromofluoromethane 125 % 84-123 SR Toluene-d8 138 % 76-129 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 35 P R I S M FullAnalytical Environmental tal Solutions LA6-QRIES INC. Level II QC Report 2/18/14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020008 Attn: Josh Dunbar Time Submitted: 1/31/2014 6:10:OOPM 1210 Trinity Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4BO152 - 5035 Blank (P460152-BLK1) Prepared & Analyzed: 02/11/14 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1,1,2,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,2-Trichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,3-Trichloropropane BRL 0.0050 mg/kg wet 1,2,4-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,4-Trimethyl benzene BRL 0.0050 mg/kg wet 1,2-Dibromoethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0.0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Trimethyl benzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0.0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chlorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.050 mg/kg wet Benzene BRL 0.0030 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromoform BRL 0.0050 mg/kg wet Bromomethane BRL 0.010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chloroethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethane BRL 0.0050 mg/kg wet cis-1,2-Dichloroethylene BRL 0.0050 mg/kg wet cis-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodifluoromethane BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbenzene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.050 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0.10 mg/kg wet Methyl Isobutyl Ketone BRL 0.050 mg/kg wet Methylene Chloride BRL 0.0050 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 35 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/18/14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020008 Attn: Josh Dunbar Time Submitted: 1/31/2014 6:10:OOPM 1210 Trinity Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4BO152 - 5035 Blank (P4B0152-BLK1) Prepared & Analyzed: 02/11/14 Methyl-tert-Butyl Ether BRL 0.010 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet sec-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butylbenzene BRL 0.0050 mg/kg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet trans-1,2-Dichloroethylene BRL 0.0050 mg/kg wet trans-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichloroethylene BRL 0.0050 mg/kg wet Trichlorofluoromethane BRL 0.0050 mg/kg wet Vinyl acetate BRL 0.025 mg/kg wet Vinyl chloride BRL 0.0050 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate: 4-Bromofluorobenzene 0.0592 mg/kg wet 0.05000 118 70-130 Surrogate: Dibromofluoromethane 0.0507 mg/kg wet 0.05000 101 84-123 Surrogate: Toluene-d8 0.0511 mg/kg wet 0.05000 102 76-129 LCS (P41130152-113SI) Prepared & Analyzed: 02/11/14 1,1-Dichloroethylene 0.0457 0.0050 mg/kg wet 0.05000 91 67-149 Benzene 0.0504 0.0030 mg/kg wet 0.05000 101 74-127 Chlorobenzene 0.0520 0.0050 mg/kg wet 0.05000 104 74-118 Toluene 0.0517 0.0050 mg/kg wet 0.05000 103 71-129 Trichloroethylene 0.0484 0.0050 mg/kg wet 0.05000 97 75-133 Surrogate: 4-Bromofluorobenzene 0.0529 mg/kg wet 0.05000 106 70-130 Surrogate: Dibromofluoromethane 0.0477 mg/kg wet 0.05000 95 84-123 Surrogate: Toluene-d8 0.0498 mg/kg wet 0.05000 100 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 35 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� ueoAAroAiEs iN� Level II QC Report 2/18/14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020008 Attn: Josh Dunbar Time Submitted: 1/31/2014 6:10:OOPM 1210 Trinity Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4BO152 - 5035 LCS Dup (P4B0152-BSD1) Prepared & Analyzed: 02/11/14 1,1-Dichloroethylene 0.0385 0.0050 mg/kg wet 0.05000 77 67-149 17 20 Benzene 0.0482 0.0030 mg/kg wet 0.05000 96 74-127 5 20 Chlorobenzene 0.0487 0.0050 mg/kg wet 0.05000 97 74-118 7 20 Toluene 0.0517 0.0050 mg/kg wet 0.05000 103 71-129 0.02 20 Trichloroethylene 0.0444 0.0050 mg/kg wet 0.05000 89 75-133 8 20 Surrogate: 4-Bromofluorobenzene 0.0637 mg/kg wet 0.05000 127 70-130 Surrogate: Dibromofluoromethane 0.0454 mg/kg wet 0.05000 91 84-123 Surrogate: Toluene-d8 0.0487 mg/kg wet 0.05000 97 76-129 Batch P4BO223 - 5035 Blank (P460223-131-K1) Prepared & Analyzed: 02/12/14 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1,1,2,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,2-Trichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,3-Trichloropropane BRL 0.0050 mg/kg wet 1,2,4-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,4-Trimethyl benzene BRL 0.0050 mg/kg wet 1,2-Dibromoethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0.0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Trimethyl benzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0.0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chlorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.050 mg/kg wet Benzene BRL 0.0030 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromoform BRL 0.0050 mg/kg wet Bromomethane BRL 0.010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chloroethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethane BRL 0.0050 mg/kg wet cis-1,2-Dichloroethylene BRL 0.0050 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 of 35 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/18/14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020008 Attn: Josh Dunbar Time Submitted: 1/31/2014 6:10:OOPM 1210 Trinity Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4BO223 - 5035 Blank (P4B0223-BLK1) Prepared & Analyzed: 02/12/14 cis-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodifluoromethane BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbenzene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.050 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0.10 mg/kg wet Methyl Isobutyl Ketone BRL 0.050 mg/kg wet Methylene Chloride BRL 0.0050 mg/kg wet Methyl-tert-Butyl Ether BRL 0.010 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet sec-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butylbenzene BRL 0.0050 mg/kg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet trans-1,2-Dichloroethylene BRL 0.0050 mg/kg wet trans-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichloroethylene BRL 0.0050 mg/kg wet Trichlorofluoromethane BRL 0.0050 mg/kg wet Vinyl acetate BRL 0.025 mg/kg wet Vinyl chloride BRL 0.0050 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate: 4-Bromofluorobenzene 0.0610 mg/kg wet 0.05000 122 70-130 Surrogate: Dibromofluoromethane 0.0517 mg/kg wet 0.05000 103 84-123 Surrogate: Toluene-d8 0.0507 mg/kg wet 0.05000 101 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 35 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/18/14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020008 Attn: Josh Dunbar Time Submitted: 1/31/2014 6:10:OOPM 1210 Trinity Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4BO223 - 5035 LCS (P4130223-13SI) Prepared & Analyzed: 02/12/14 1,1-Dichloroethylene 0.0575 0.0050 mg/kg wet 0.05000 115 67-149 Benzene 0.0499 0.0030 mg/kg wet 0.05000 100 74-127 Chlorobenzene 0.0523 0.0050 mg/kg wet 0.05000 105 74-118 Toluene 0.0539 0.0050 mg/kg wet 0.05000 108 71-129 Trichloroethylene 0.0544 0.0050 mg/kg wet 0.05000 109 75-133 Surrogate: 4-Bromofluorobenzene 0.0528 mg/kg wet 0.05000 106 70-130 Surrogate: Dibromofluoromethane 0.0485 mg/kg wet 0.05000 97 84-123 Surrogate: Toluene-d8 0.0526 mg/kg wet 0.05000 105 76-129 LCS Dup (P41130223-13SD1) Prepared & Analyzed: 02/12/14 1,1-Dichloroethylene 0.0508 0.0050 mg/kg wet 0.05000 102 67-149 12 20 Benzene 0.0495 0.0030 mg/kg wet 0.05000 99 74-127 0.8 20 Chlorobenzene 0.0519 0.0050 mg/kg wet 0.05000 104 74-118 0.8 20 Toluene 0.0600 0.0050 mg/kg wet 0.05000 120 71-129 11 20 Trichloroethylene 0.0535 0.0050 mg/kg wet 0.05000 107 75-133 2 20 Surrogate: 4-Bromofluorobenzene 0.0579 mg/kg wet 0.05000 116 70-130 Surrogate: Dibromofluoromethane 0.0468 mg/kg wet 0.05000 94 84-123 Surrogate: Toluene-d8 0.0474 mg/kg wet 0.05000 95 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 of 35 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� ueoAAroAiEs iN� Level II QC Report 2/18/14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020008 Attn: Josh Dunbar Time Submitted: 1/31/2014 6:10:OOPM 1210 Trinity Road Raleigh, NC 27607 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0016 - 3550C MS Blank (P4B0016-BLK1) Prepared: 02/03/14 Analyzed: 02/04/14 1,2,4-Trichlorobenzene BRL 0.33 mg/kg wet 1,2-Dichlorobenzene BRL 0.33 mg/kg wet 1,3-Dichlorobenzene BRL 0.33 mg/kg wet 1,4-Dichlorobenzene BRL 0.33 mg/kg wet 1-Methyl naphthalene BRL 0.33 mg/kg wet 2,4,6-Trichlorophenol BRL 0.33 mg/kg wet 2,4-Dichlorophenol BRL 0.33 mg/kg wet 2,4-Dimethylphenol BRL 0.33 mg/kg wet 2,4-Dinitrophenol BRL 0.33 mg/kg wet 2,4-Dinitrotoluene BRL 0.33 mg/kg wet 2,6-Dinitrotoluene BRL 0.33 mg/kg wet 2-Chloronaphthalene BRL 0.33 mg/kg wet 2-Chlorophenol BRL 0.33 mg/kg wet 2-Methyl naphthalene BRL 0.33 mg/kg wet 2-Methylphenol BRL 0.33 mg/kg wet 2-Nitrophenol BRL 0.33 mg/kg wet 3,3'-Dichlorobenzidine BRL 0.33 mg/kg wet 3/4-Methyl phenol BRL 0.33 mg/kg wet 4,6-Dinitro-2-methylphenol BRL 0.33 mg/kg wet 4-Bromophenyl phenyl ether BRL 0.33 mg/kg wet 4-Chloro-3-methylphenol BRL 0.33 mg/kg wet 4-Chloroaniline BRL 0.33 mg/kg wet 4-Chlorophenyl phenyl ether BRL 0.33 mg/kg wet 4-Nitrophenol BRL 0.33 mg/kg wet Acenaphthene BRL 0.33 mg/kg wet Acenaphthylene BRL 0.33 mg/kg wet Anthracene BRL 0.33 mg/kg wet Azobenzene BRL 0.33 mg/kg wet Benzo(a)anthracene BRL 0.33 mg/kg wet Benzo(a)pyrene BRL 0.33 mg/kg wet Benzo(b)fluoranthene BRL 0.33 mg/kg wet Benzo(g,h,i)perylene BRL 0.33 mg/kg wet Benzo(k)fluoranthene BRL 0.33 mg/kg wet Benzoic Acid BRL 0.33 mg/kg wet Benzyl alcohol BRL 0.33 mg/kg wet bis(2-Chloroethoxy)methane BRL 0.33 mg/kg wet Bis(2-Chloroethyl)ether BRL 0.33 mg/kg wet Bis(2-chloroisopropyl)ether BRL 0.33 mg/kg wet Bis(2-Ethylhexyl)phthalate BRL 0.33 mg/kg wet Butyl benzyl phthalate BRL 0.33 mg/kg wet Chrysene BRL 0.33 mg/kg wet Dibenzo(a,h)anthracene BRL 0.33 mg/kg wet Dibenzofuran BRL 0.33 mg/kg wet Diethyl phthalate BRL 0.33 mg/kg wet Dimethyl phthalate BRL 0.33 mg/kg wet Di-n-butyl phthalate BRL 0.33 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 35 Level II QC Report /P R I S M Environmental Full -Service Analytical & Environmental Solutions 2/18/14 �� ueoAAroAEs �� Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020008 Attn: Josh Dunbar Time Submitted: 1/31/2014 6:10:OOPM 1210 Trinity Road Raleigh, NC 27607 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0016 - 3550C MS Blank (P4B0016-BLK1) Prepared: 02/03/14 Analyzed: 02/04/14 Di-n-octyl phthalate BRL 0.33 mg/kg wet Fluoranthene BRL 0.33 mg/kg wet Fluorene BRL 0.33 mg/kg wet Hexachlorobenzene BRL 0.33 mg/kg wet Hexachlorobutadiene BRL 0.33 mg/kg wet Hexachlorocyclopentadiene BRL 0.33 mg/kg wet Hexachloroethane BRL 0.33 mg/kg wet Indeno(1,2,3-cd)pyrene BRL 0.33 mg/kg wet Isophorone BRL 0.33 mg/kg wet Naphthalene BRL 0.33 mg/kg wet Nitrobenzene BRL 0.33 mg/kg wet N-Nitroso-di-n-propylamine BRL 0.33 mg/kg wet N-Nitrosodiphenylamine BRL 0.33 mg/kg wet Pentachlorophenol BRL 0.33 mg/kg wet Phenanthrene BRL 0.33 mg/kg wet Phenol BRL 0.33 mg/kg wet Pyrene BRL 0.33 mg/kg wet Surrogate: 2,4,6-Tribromophenol 3.29 mg/kg wet 3.330 99 37-131 Surrogate: 2-Fluorobiphenyl 1.49 mg/kg wet 1.665 89 47-130 Surrogate: 2-Fluorophenol 2.82 mg/kg wet 3.330 85 44-117 Surrogate: Nitrobenzene-d5 1.45 mg/kg wet 1.665 87 45-121 Surrogate: Phenol-d5 2.81 mg/kg wet 3.330 84 37-127 Surrogate: Terphenyl-d14 1.65 mg/kg wet 1.665 99 38-135 LCS (P4B0016-BSI) Prepared: 02/03/14 Analyzed: 02/04/14 1,2,4-Trichlorobenzene 1.40 0.33 mg/kg wet 1.665 84 54-110 1,2-Dichlorobenzene 1.35 0.33 mg/kg wet 1.665 81 53-107 1,3-Dichlorobenzene 1.33 0.33 mg/kg wet 1.665 80 52-108 1,4-Dichlorobenzene 1.32 0.33 mg/kg wet 1.665 79 52-108 1-Methyl naphthalene 1.55 0.33 mg/kg wet 1.665 93 35-102 2,4,6-Trichlorophenol 1.65 0.33 mg/kg wet 1.665 99 62-120 2,4-Dichlorophenol 1.51 0.33 mg/kg wet 1.665 91 58-113 2,4-Dimethylphenol 1.55 0.33 mg/kg wet 1.665 93 59-110 2,4-Dinitrophenol 1.11 0.33 mg/kg wet 1.665 67 29-134 2,4-Dinitrotoluene 1.43 0.33 mg/kg wet 1.665 86 63-137 2,6-Dinitrotoluene 1.40 0.33 mg/kg wet 1.665 84 59-134 2-Chloronaphthalene 1.94 0.33 mg/kg wet 1.665 117 41-147 2-Chlorophenol 1.40 0.33 mg/kg wet 1.665 84 55-108 2-Methyl naphthalene 1.59 0.33 mg/kg wet 1.665 95 57-116 2-Methylphenol 1.46 0.33 mg/kg wet 1.665 88 56-111 2-Nitrophenol 1.39 0.33 mg/kg wet 1.665 84 58-112 3,3'-Dichlorobenzidine 1.65 0.33 mg/kg wet 1.665 99 51-161 3/4-Methyl phenol 1.49 0.33 mg/kg wet 1.665 89 56-111 4,6-Dinitro-2-methylphenol 1.38 0.33 mg/kg wet 1.665 83 46-148 4-Bromophenyl phenyl ether 1.77 0.33 mg/kg wet 1.665 107 58-137 4-Chloro-3-methylphenol 1.59 0.33 mg/kg wet 1.665 96 60-118 4-Chloroaniline 1.65 0.33 mg/kg wet 1.665 99 53-144 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 35 Level II QC Report /P R I S M Environmental Full -Service Analytical & Environmental Solutions 2/18/14 �� ueoAAroA�Es ��� Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P4B0016 - 3550C MS Prism Work Order: 4020008 Time Submitted: 1/31/2014 6:10:OOPM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS (P4B0016-BSI) Prepared: 02/03/14 Analyzed: 02/04/14 4-Chlorophenyl phenyl ether 1.72 0.33 mg/kg wet 1.665 103 59-131 4-Nitrophenol 1.58 0.33 mg/kg wet 1.665 95 48-148 Acenaphthene 1.69 0.33 mg/kg wet 1.665 102 62-118 Acenaphthylene 1.66 0.33 mg/kg wet 1.665 100 64-116 Anthracene 1.80 0.33 mg/kg wet 1.665 108 71-132 Azobenzene 1.71 0.33 mg/kg wet 1.665 103 56-125 Benzo(a)anthracene 1.76 0.33 mg/kg wet 1.665 106 71-129 Benzo(a)pyrene 1.78 0.33 mg/kg wet 1.665 107 74-129 Benzo(b)fluoranthene 1.78 0.33 mg/kg wet 1.665 107 63-138 Benzo(g,h,i)perylene 1.75 0.33 mg/kg wet 1.665 105 41-154 Benzo(k)fluoranthene 1.72 0.33 mg/kg wet 1.665 103 62-145 Benzoic Acid 0.428 0.33 mg/kg wet 1.665 26 10-83 Benzyl alcohol 1.56 0.33 mg/kg wet 1.665 93 55-112 bis(2-Chloroethoxy)methane 1.54 0.33 mg/kg wet 1.665 93 52-118 Bis(2-Chloroethyl)ether 1.36 0.33 mg/kg wet 1.665 82 50-116 Bis(2-chloroisopropyl)ether 1.47 0.33 mg/kg wet 1.665 88 48-119 Bis(2-Ethylhexyl)phthalate 1.76 0.33 mg/kg wet 1.665 106 62-135 Butyl benzyl phthalate 1.72 0.33 mg/kg wet 1.665 103 62-133 Chrysene 1.82 0.33 mg/kg wet 1.665 109 72-129 Dibenzo(a,h)anthracene 1.78 0.33 mg/kg wet 1.665 107 41-158 Dibenzofuran 1.62 0.33 mg/kg wet 1.665 97 64-115 Diethyl phthalate 1.68 0.33 mg/kg wet 1.665 101 73-120 Dimethyl phthalate 1.64 0.33 mg/kg wet 1.665 98 71-115 Di-n-butyl phthalate 1.73 0.33 mg/kg wet 1.665 104 68-127 Di-n-octyl phthalate 1.69 0.33 mg/kg wet 1.665 102 53-150 Fluoranthene 1.77 0.33 mg/kg wet 1.665 106 64-136 Fluorene 1.68 0.33 mg/kg wet 1.665 101 67-120 Hexachlorobenzene 1.67 0.33 mg/kg wet 1.665 100 63-134 Hexachlorobutadiene 1.41 0.33 mg/kg wet 1.665 85 55-112 Hexachlorocyclopentadiene 1.91 0.33 mg/kg wet 1.665 114 43-135 Hexachloroethane 1.31 0.33 mg/kg wet 1.665 79 49-113 Indeno(1,2,3-cd)pyrene 1.78 0.33 mg/kg wet 1.665 107 40-160 Isophorone 1.35 0.33 mg/kg wet 1.665 81 55-118 Naphthalene 1.49 0.33 mg/kg wet 1.665 90 62-111 Nitrobenzene 1.22 0.33 mg/kg wet 1.665 73 50-116 N-Nitroso-di-n-propylamine 1.56 0.33 mg/kg wet 1.665 94 53-113 N-Nitrosodiphenylamine 1.78 0.33 mg/kg wet 1.665 107 76-144 Pentachlorophenol 1.54 0.33 mg/kg wet 1.665 92 36-145 Phenanthrene 1.77 0.33 mg/kg wet 1.665 106 72-123 Phenol 1.44 0.33 mg/kg wet 1.665 87 56-108 Pyrene 1.82 0.33 mg/kg wet 1.665 109 51-141 Surrogate: 2,4,6-Tribromophenol 3.74 mg/kg wet 3.330 112 37-131 Surrogate: 2-Fluorobiphenyl 1.64 mg/kg wet 1,665 99 47-130 Surrogate: 2-Fluorophenol 3.02 mg/kg wet 3.330 91 44-117 Surrogate: Nitrobenzene-d5 1.45 mg/kg wet 1.665 87 45-121 Surrogate: Phenol-d5 2.97 mg/kg wet 3,330 89 37-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 35 Level II QC Report /P R I S M Environmental Full -Service Analytical & Environmental Solutions 2/18/14 �� ueoAAroA�Es ��� Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P4B0016 - 3550C MS Prism Work Order: 4020008 Time Submitted: 1/31/2014 6:10:OOPM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS (P4B0016-BS1) Prepared: 02/03/14 Analyzed: 02/04/14 Surrogate: Terphenyl-d14 1.75 mg/kg wet 1.665 105 38-135 LCS Dup (P4B0016-BSD1) Prepared: 02/03/14 Analyzed: 02/04/14 1,2,4-Trichlorobenzene 1.20 0.33 mg/kg wet 1.667 72 54-110 15 20 1,2-Dichlorobenzene 1.11 0.33 mg/kg wet 1.667 67 53-107 19 20 1,3-Dichlorobenzene 1.09 0.33 mg/kg wet 1.667 65 52-108 19 20 1,4-Dichlorobenzene 1.09 0.33 mg/kg wet 1.667 65 52-108 19 20 1-Methyl naphthalene 1.34 0.33 mg/kg wet 1.667 80 35-102 14 20 2,4,6-Trichlorophenol 1.47 0.33 mg/kg wet 1.667 88 62-120 12 20 2,4-Dichlorophenol 1.28 0.33 mg/kg wet 1.667 77 58-113 16 20 2,4-Dimethylphenol 1.31 0.33 mg/kg wet 1.667 79 59-110 16 20 2,4-Dinitrophenol 1.13 0.33 mg/kg wet 1.667 68 29-134 2 20 2,4-Dinitrotoluene 1.37 0.33 mg/kg wet 1.667 82 63-137 5 20 2,6-Dinitrotoluene 1.31 0.33 mg/kg wet 1.667 79 59-134 7 20 2-Chloronaphthalene 1.70 0.33 mg/kg wet 1.667 102 41-147 13 20 2-Chlorophenol 1.18 0.33 mg/kg wet 1.667 71 55-108 17 20 2-Methyl naphthalene 1.37 0.33 mg/kg wet 1.667 82 57-116 15 20 2-Methylphenol 1.23 0.33 mg/kg wet 1.667 74 56-111 17 20 2-Nitrophenol 1.21 0.33 mg/kg wet 1.667 73 58-112 14 20 3,3'-Dichlorobenzidine 1.50 0.33 mg/kg wet 1.667 90 51-161 9 20 3/4-Methyl phenol 1.25 0.33 mg/kg wet 1.667 75 56-111 17 20 4,6-Dinitro-2-methylphenol 1.39 0.33 mg/kg wet 1.667 83 46-148 0.6 20 4-Bromophenyl phenyl ether 1.65 0.33 mg/kg wet 1.667 99 58-137 7 20 4-Chloro-3-methylphenol 1.43 0.33 mg/kg wet 1.667 86 60-118 11 20 4-Chloroaniline 1.43 0.33 mg/kg wet 1.667 86 53-144 15 20 4-Chlorophenyl phenyl ether 1.57 0.33 mg/kg wet 1.667 94 59-131 9 20 4-Nitrophenol 1.54 0.33 mg/kg wet 1.667 93 48-148 2 20 Acenaphthene 1.50 0.33 mg/kg wet 1.667 90 62-118 12 20 Acenaphthylene 1.47 0.33 mg/kg wet 1.667 88 64-116 12 20 Anthracene 1.66 0.33 mg/kg wet 1.667 99 71-132 8 20 Azobenzene 1.57 0.33 mg/kg wet 1.667 94 56-125 8 20 Benzo(a)anthracene 1.64 0.33 mg/kg wet 1.667 98 71-129 7 20 Benzo(a)pyrene 1.62 0.33 mg/kg wet 1.667 97 74-129 9 20 Benzo(b)fluoranthene 1.61 0.33 mg/kg wet 1.667 96 63-138 10 20 Benzo(g,h,i)perylene 1.59 0.33 mg/kg wet 1.667 95 41-154 10 20 Benzo(k)fluoranthene 1.58 0.33 mg/kg wet 1.667 95 62-145 8 20 Benzoic Acid 0.372 0.33 mg/kg wet 1.667 22 10-83 14 20 Benzyl alcohol 1.31 0.33 mg/kg wet 1.667 79 55-112 17 20 bis(2-Chloroethoxy)methane 1.34 0.33 mg/kg wet 1.667 80 52-118 14 20 Bis(2-Chloroethyl)ether 1.10 0.33 mg/kg wet 1.667 66 50-116 21 20 D Bis(2-chloroisopropyl)ether 1.23 0.33 mg/kg wet 1.667 74 48-119 18 20 Bis(2-Ethylhexyl)phthalate 1.63 0.33 mg/kg wet 1.667 98 62-135 7 20 Butyl benzyl phthalate 1.59 0.33 mg/kg wet 1.667 96 62-133 7 20 Chrysene 1.69 0.33 mg/kg wet 1.667 101 72-129 7 20 Dibenzo(a,h)anthracene 1.62 0.33 mg/kg wet 1.667 97 41-158 9 20 Dibenzofuran 1.45 0.33 mg/kg wet 1.667 87 64-115 11 20 Diethyl phthalate 1.56 0.33 mg/kg wet 1.667 94 73-120 7 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 35 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/18/14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Analyte Result Limit Units Batch P4B0016 - 3550C MS Prism Work Order: 4020008 Time Submitted: 1/31/2014 6:10:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P4B0016-BSD1) Prepared: 02/03/14 Analyzed: 02/04/14 Dimethyl phthalate 1.53 0.33 mg/kg wet 1.667 92 71-115 7 20 Di-n-butyl phthalate 1.63 0.33 mg/kg wet 1.667 98 68-127 6 20 Di-n-octyl phthalate 1.54 0.33 mg/kg wet 1.667 92 53-150 9 20 Fluoranthene 1.65 0.33 mg/kg wet 1.667 99 64-136 7 20 Fluorene 1.54 0.33 mg/kg wet 1.667 92 67-120 9 20 Hexachlorobenzene 1.55 0.33 mg/kg wet 1.667 93 63-134 8 20 Hexachlorobutadiene 1.18 0.33 mg/kg wet 1.667 71 55-112 18 20 Hexachlorocyclopentadiene 1.64 0.33 mg/kg wet 1.667 98 43-135 15 20 Hexachloroethane 1.07 0.33 mg/kg wet 1.667 64 49-113 21 20 D Indeno(1,2,3-cd)pyrene 1.61 0.33 mg/kg wet 1.667 97 40-160 10 20 Isophorone 1.19 0.33 mg/kg wet 1.667 71 55-118 13 20 Naphthalene 1.28 0.33 mg/kg wet 1.667 77 62-111 15 20 Nitrobenzene 1.07 0.33 mg/kg wet 1.667 64 50-116 13 20 N-Nitroso-di-n-propylamine 1.29 0.33 mg/kg wet 1.667 78 53-113 19 20 N-Nitrosodiphenylamine 1.66 0.33 mg/kg wet 1.667 100 76-144 7 20 Pentachlorophenol 1.52 0.33 mg/kg wet 1.667 91 36-145 1 20 Phenanthrene 1.64 0.33 mg/kg wet 1.667 98 72-123 7 20 Phenol 1.24 0.33 mg/kg wet 1.667 74 56-108 15 20 Pyrene 1.68 0.33 mg/kg wet 1.667 101 51-141 8 20 Surrogate: 2,4,6-Tribromophenol 3.38 mg/kg wet 3.333 101 37-131 Surrogate: 2-Fluorobiphenyl 1.40 mg/kg wet 1.667 84 47-130 Surrogate: 2-Fluorophenol 2.48 mg/kg wet 3.333 75 44-117 Surrogate: Nitrobenzene-d5 1.23 mg/kg wet 1.667 74 45-121 Surrogate: Phenol-d5 2.51 mg/kg wet 3.333 75 37-127 Surrogate: Terphenyl-d14 1.59 mg/kg wet 1.667 96 38-135 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 35 Level II QC Report /P R I S M Environmental Full -Service Analytical & Environmental Solutions 2/18/14 �� ueoAAroAEs �� Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020008 Attn: Josh Dunbar Time Submitted: 1/31/2014 6:10:OOPM 1210 Trinity Road Raleigh, NC 27607 Organochlorine Pesticides by GC/ECD - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0032 - 3550C GC Blank (P4B0032-BLK1) Prepared: 02/04/14 Analyzed: 02/07/14 4,4'-DDD BRL 0.0020 mg/kg wet 4,4'-DDE BRL 0.0020 mg/kg wet 4,4'-DDT BRL 0.0030 mg/kg wet Aldrin BRL 0.0020 mg/kg wet alpha-BHC BRL 0.0020 mg/kg wet cis -Chlordane BRL 0.0020 mg/kg wet beta-BHC BRL 0.0020 mg/kg wet Chlordane BRL 0.050 mg/kg wet delta-BHC BRL 0.0020 mg/kg wet Dieldrin BRL 0.0020 mg/kg wet Endosulfan I BRL 0.0020 mg/kg wet Endosulfan II BRL 0.0020 mg/kg wet Endosulfan Sulfate BRL 0.0020 mg/kg wet Endrin BRL 0.0020 mg/kg wet Endrin Aldehyde BRL 0.0020 mg/kg wet Endrin Ketone BRL 0.0020 mg/kg wet gamma-BHC BRL 0.0020 mg/kg wet trans -Chlordane BRL 0.0020 mg/kg wet Heptachlor BRL 0.0020 mg/kg wet Heptachlor Epoxide BRL 0.0020 mg/kg wet Methoxychlor BRL 0.0020 mg/kg wet Toxaphene BRL 0.050 mg/kg wet Surrogate: Decachlorobiphenyl 0.0480 mg/kg wet 0.03331 144 26-204 Surrogate: Tetrachloro-m-xylene 0.0293 mg/kg wet 0.03331 88 40-162 LCS (P4B0032-BS1) Prepared: 02/04/14 Analyzed: 02/07/14 4,4'-DDD 0.0427 0.0020 mg/kg wet 0.03332 128 72-142 LH 4,4'-DDE 0.0377 0.0020 mg/kg wet 0.03332 113 74-129 4,4'-DDT 0.0490 0.0030 mg/kg wet 0.03332 147 75-141 LH Aldrin 0.0340 0.0020 mg/kg wet 0.03332 102 66-132 alpha-BHC 0.0327 0.0020 mg/kg wet 0.03332 98 72-126 cis -Chlordane 0.0327 0.0020 mg/kg wet 0.03332 98 71-132 beta-BHC 0.0347 0.0020 mg/kg wet 0.03332 104 79-134 delta-BHC 0.0310 0.0020 mg/kg wet 0.03332 93 74-132 Dieldrin 0.0343 0.0020 mg/kg wet 0.03332 103 72-136 Endosulfan 1 0.0323 0.0020 mg/kg wet 0.03332 97 74-134 Endosulfan II 0.0353 0.0020 mg/kg wet 0.03332 106 79-134 Endosulfan Sulfate 0.0390 0.0020 mg/kg wet 0.03332 117 73-147 Endrin 0.0450 0.0020 mg/kg wet 0.03332 135 74-147 Endrin Aldehyde 0.0343 0.0020 mg/kg wet 0.03332 103 73-138 Endrin Ketone 0.0370 0.0020 mg/kg wet 0.03332 ill 84-135 gamma-BHC 0.0340 0.0020 mg/kg wet 0.03332 102 71-129 trans -Chlordane 0.0327 0.0020 mg/kg wet 0.03332 98 71-132 Heptachlor 0.0403 0.0020 mg/kg wet 0.03332 121 72-134 Heptachlor Epoxide 0.0333 0.0020 mg/kg wet 0.03332 100 73-132 Methoxychlor 0.0613 0.0020 mg/kg wet 0.03332 184 91-138 LH This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 of 35 _�, P R 1 S M Full -Service Analytical Environmental Solutions -, uapAniONiES, �NF Level II QC Report 2/18/14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020008 Attn: Josh Dunbar Time Submitted: 1/31/2014 6:10:OOPM 1210 Trinity Road Raleigh, NC 27607 Organochlorine Pesticides by GC/ECD - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0032 - 3550C GC LCS (P4130032-13SI) Prepared: 02/04/14 Analyzed: 02/07/14 Surrogate: Decachlorobiphenyl 0.0523 mg/kg wet 0.03332 157 26-204 Surrogate: Tetrachloro-m-xylene 0.0283 mg/kg wet 0.03332 85 40-162 LCS (P41130032-113S2) Prepared: 02/04/14 Analyzed: 02/07/14 Chlordane 0.353 0.050 mg/kg wet 0.3328 106 50-150 Surrogate: Decachlorobiphenyl 0.0539 mg/kg wet 0.03328 162 26-204 Surrogate: Tetrachloro-m-xylene 0.0300 mg/kg wet 0.03328 90 40-162 LCS (P4130032-13S3) Prepared: 02/04/14 Analyzed: 02/07/14 Toxaphene 0.527 0.050 mg/kg wet 0.3328 158 50-150 LH Surrogate: Decachlorobiphenyl 0.0473 mg/kg wet 0.03328 142 26-204 Surrogate: Tetrachloro-m-xylene 0.0276 mg/kg wet 0.03328 83 40-162 LCS Dup (P41130032-113SD1) Prepared: 02/04/14 Analyzed: 02/07/14 4,4'-DDD 0.0420 0.0020 mg/kg wet 0.03332 126 72-142 2 20 LH 4,4'-DDE 0.0363 0.0020 mg/kg wet 0.03332 109 74-129 4 20 4,4'-DDT 0.0490 0.0030 mg/kg wet 0.03332 147 75-141 0 20 LH Aldrin 0.0317 0.0020 mg/kg wet 0.03332 95 66-132 7 20 alpha-BHC 0.0300 0.0020 mg/kg wet 0.03332 90 72-126 9 20 cis -Chlordane 0.0317 0.0020 mg/kg wet 0.03332 95 71-132 3 20 beta-BHC 0.0330 0.0020 mg/kg wet 0.03332 99 79-134 5 20 delta-BHC 0.0297 0.0020 mg/kg wet 0.03332 89 74-132 4 20 Dieldrin 0.0337 0.0020 mg/kg wet 0.03332 101 72-136 2 20 Endosulfan 1 0.0310 0.0020 mg/kg wet 0.03332 93 74-134 4 20 Endosulfan 11 0.0350 0.0020 mg/kg wet 0.03332 105 79-134 0.9 20 Endosulfan Sulfate 0.0390 0.0020 mg/kg wet 0.03332 117 73-147 0 20 Endrin 0.0440 0.0020 mg/kg wet 0.03332 132 74-147 2 20 Endrin Aldehyde 0.0340 0.0020 mg/kg wet 0.03332 102 73-138 1 20 Endrin Ketone 0.0370 0.0020 mg/kg wet 0.03332 ill 84-135 0 20 gamma-BHC 0.0320 0.0020 mg/kg wet 0.03332 96 71-129 6 20 trans -Chlordane 0.0313 0.0020 mg/kg wet 0.03332 94 71-132 4 20 Heptachlor 0.0383 0.0020 mg/kg wet 0.03332 115 72-134 5 20 Heptachlor Epoxide 0.0320 0.0020 mg/kg wet 0.03332 96 73-132 4 20 Methoxychlor 0.0620 0.0020 mg/kg wet 0.03332 186 91-138 1 20 LH Surrogate: Decachlorobiphenyl 0.0513 mg/kg wet 0.03332 154 26-204 Surrogate: Tetrachloro-m-xylene 0.0263 mg/kg wet 0.03332 79 40-162 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 30 of 35 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/18/14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control Reporting Analyte Result Limit Units Batch P4B0033 - 3550C GC Prism Work Order: 4020008 Time Submitted: 1/31/2014 6:10:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P41130033-131-11(1) Prepared & Analyzed: 02/04/14 Aroclor 1016 BRL 0.050 mg/kg wet Aroclor 1221 BRL 0.10 mg/kg wet Aroclor 1232 BRL 0.10 mg/kg wet Aroclor 1242 BRL 0.050 mg/kg wet Aroclor 1248 BRL 0.050 mg/kg wet Aroclor 1254 BRL 0.050 mg/kg wet Aroclor 1260 BRL 0.050 mg/kg wet Surrogate: Tetrachloro-m-xylene 0.0310 mg/kg wet 0.03331 93 36-182 Surrogate: Decachlorobiphenyl 0.0313 mg/kg wet 0.03331 94 34-182 LCS (P4B0033-BS1) Prepared & Analyzed: 02/04/14 Aroclor 1016 0.294 0.050 mg/kg wet 0.3333 88 64-151 Aroclor 1260 0.288 0.050 mg/kg wet 0.3333 87 45-166 Surrogate: Tetrachloro-m-xylene 0.0353 mg/kg wet 0.03333 106 36-182 Surrogate: Decachlorobiphenyl 0.0290 mg/kg wet 0.03333 87 34-182 LCS Dup (P4B0033-BSD1) Prepared & Analyzed: 02/04/14 Aroclor 1016 0.299 0.050 mg/kg wet 0.3323 90 64-151 2 50 Aroclor 1260 0.294 0.050 mg/kg wet 0.3323 88 45-166 2 50 Surrogate: Tetrachloro-m-xylene 0.0362 mg/kg wet 0.03323 109 36-182 Surrogate: Decachlorobiphenyl 0.0319 mg/kg wet 0.03323 96 34-182 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 31 of 35 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Total Metals - Quality Control Analyte Batch P4B0025 - 3050B Project: 828 Martin Luther King Jr Blvd. Level II QC Report 2/18/14 Prism Work Order: 4020008 Time Submitted: 1/31/2014 6:10:OOPM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (P4130025-131-K1) Prepared & Analyzed: 02/04/14 Arsenic BRL 0.25 mg/kg wet Barium BRL 0.50 mg/kg wet Cadmium BRL 0.25 mg/kg wet Chromium BRL 0.25 mg/kg wet Lead BRL 0.25 mg/kg wet Selenium BRL 0.50 mg/kg wet Silver BRL 0.25 mg/kg wet LCS (P4B0025-BS1) Prepared & Analyzed: 02/04/14 Arsenic 22.4 0.25 mg/kg wet 24.51 91 80-120 Barium 23.1 0.49 mg/kg wet 24.51 94 80-120 Cadmium 21.8 0.25 mg/kg wet 24.51 89 80-120 Chromium 23.2 0.25 mg/kg wet 24.51 95 80-120 Lead 22.2 0.25 mg/kg wet 24.51 90 80-120 Selenium 21.1 0.49 mg/kg wet 24.51 86 80-120 Silver 22.9 0.25 mg/kg wet 24.51 93 80-120 Batch P4B0029 - 7471 B Blank (P4B0029-BLK1) Prepared: 02/03/14 Analyzed: 02/04/14 Mercury BRL 0.020 mg/kg wet LCS (P4B0029-13SI) Prepared: 02/03/14 Analyzed: 02/04/14 Mercury 0.448 0.021 mg/kg wet 0.4386 102 80-120 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 32 of 35 Level II QC Report /P R I S M Environmental Full -Service Analytical & Environmental Solutions 2/18/14 �� uaoanroAies iNa Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020008 Attn: Josh Dunbar Time Submitted: 1/31/2014 6:10:OOPM 1210 Trinity Road Raleigh, NC 27607 General Chemistry Parameters - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0021 - NO PREP Blank (P4B0021-BLK1) Prepared & Analyzed: 02/03/14 % Solids 100 0.100 % by Weight Duplicate (P4B0021-DUP2) Source: 4020008-03 Prepared & Analyzed: 02/03/14 % Solids 61.4 0.100 % by Weight 61.1 0.5 20 Batch P4B0057 - NO PREP Blank (P4B0057-BLK1) Prepared: 02/04/14 Analyzed: 02/05/14 Hexavalent Chromium BRL 0.40 mg/kg wet LCS (P41130057-13SI) Prepared: 02/04/14 Analyzed: 02/05/14 Hexavalent Chromium 15.5 0.40 mg/kg wet 16.00 97 90-110 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 of 35 Sample Extraction Data Prep Method: 3550C GC Lab Number Batch Initial Final Date/Time 4020008-01 134130032 30.01 g 10 mL 02/04/14 9:30 4020008-02 134130032 30.06 g 10 mL 02/04/14 9:30 4020008-03 P4130032 30.09 g 10 mL 02/04/14 9:30 Prep Method: 3550C GC Lab Number Batch Initial Final Date/Time 4020008-01 13460033 30.01 g 10 mL 02/04/14 9:30 4020008-02 134130033 30.06 g 10 mL 02/04/14 9:30 4020008-03 134130033 30.09 g 10 mL 02/04/14 9:30 Prep Method: 3550C MS Lab Number Batch Initial Final Date/Time 4020008-01 134130016 30.01 g 1 mL 02/04/14 9:05 4020008-02 13460016 30.02 g 1 mL 02/04/14 9:05 4020008-03 134130016 30.02 g 1 mL 02/04/14 9:05 Prep Method: 3050E Lab Number Batch Initial Final Date/Time 4020008-01 P4130025 1.98 g 50 mL 02/04/14 8:45 4020008-01 P460025 1.98 g 50 mL 02/04/14 8:45 4020008-02 P460025 1.97 g 50 mL 02/04/14 8:45 4020008-02 P4130025 1.97 g 50 mL 02/04/14 8:45 4020008-03 P4130025 1.97 g 50 mL 02/04/14 8:45 4020008-03 P4130025 1.97 g 50 mL 02/04/14 8:45 Prep Method: 7471E Lab Number Batch Initial Final Date/Time 4020008-01 13460029 0.6 g 50 mL 02/03/14 12:45 4020008-02 134130029 0.56 g 50 mL 02/03/14 12:45 4020008-03 134130029 0.58 g 50 mL 02/03/14 12:45 Prep Method: 5035 Lab Number Batch Initial Final Date/Time 4020008-01 P4130152 5.36 g 5 mL 02/11/14 14:39 4020008-02 P460223 4.83 g 5 mL 02/12/14 9:53 4020008-03 P4130223 5.07 g 5 mL 02/12/14 9:53 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 34 of 35 O K .._ A A A N C (n Pfi D 3 d 3 � G L a m m CD a a X O N u 3 ® r c $ m cn a U) g � m22 0-1 >m m m f m �.. c s ' O z a r D a (n < AD �= ` kA i O Om 3 0 i m ® b _n o C oi: m N 2i �rL _ _ n �m A cn D = 3 m z0 Ny O� Ogm['�m r D < DC rn mm n X03 m - ;im c ® w s oD cC) o S. m D N �_X 3 _ `® r�UB� c -Nip t� m N �" °z�z c) _ A A o� F s, ,>,o d o 3 m O X 2 L e m m C C Q I CD vi M w my in O p Z �? co 0< r>:: $ N r mCD m> m c c e� fp1 T c� ° d 3w -�. .v : m m -� o �°� m z -, �, z O O �1 ou 3 O w. A CD m A � ;o O D d m m = aG N O N N z CD w m O S N 0 D ID CDN � Cm m W CD pp �7 O CD o 'ty Bt O " < �!D C 7 p S k-A v� o to O z C Ln -:�' . C m X. CAIgI M C?Q m �} c� C y `7- 0 3 3 CD m fA ® cn C @ { 71 m ® ® r 22 Co CO) Co x, 0 ® 0 O K to 0 0 O rL 0 A 10 z m ,.( B Vu ID rL CD �® CD n ub m< �v �� 0 M, -Td �� CD x �g CD ea �a 'D F 3 CH 3 3 0 Q c m m�m o I m 1p N v ,0 n chi ® n ID CD d m m ID vN N QCL Co 22 A (D ❑ ❑ N -, n A o) s 3 A = O o O n. — `< fg N 5N z CD OIn ®p ° '< wmmm N O m N m m n z N D D ® ID0A X C - ' M E ID o 0 00Rex m n m � < r®co Q < m_ g n z0m LiA `NIm-OXp ACD n@N� (C-j n`GaS fn cn R p O o a�: � m m CD m f®b mo M f7 m CD 0 CD z I0 rl D("� _ z z m ® in- M ® D m cn M �1 z z D m 0 I� m � ® ® 0 ® Ge N (D �.21) Im N ® 7 D ® z N -i M d D 3 D $ 0 s 0 m m W v CD N i 3 zz� N r. 9 m ® ca m N f 0 m m N a ;D —1va l� 0 RIS Full -Service Analytical Environmental Solutions /PM 1W_Z1�, LABOFATOAIES.INC. Falcon Engineering Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 NC Certification No. 402 SC Certification No. 99012 NC Drinkinq Water Cent No. 37735 VA Certification No. 460211 DoD ELAP: L-A-B Accredited Certificate No. L2307 ISO/IEC 17025: L-A-B Accredited Certificate No. L2307 Project: 828 Martin Luther King Jr Blvd. Lab Submittal Date: 02/06/2014 Prism Work Order: 4020095 Case Narrative 02/21 /2014 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a ----I Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference: Reviewed By Angela D. Overcash VP Laboratory Services A Sample color required color blank. Aa Sample color required color blank. correction. CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. D RPD value outside of the control limits. ICV ICV result is above the control limits. Analyte not detected in the sample. No further action taken. P Recovery outside of the QC limits due to inconsistency during extraction and chromatographic performance of this compound. SE Surrogate recovery outside the QC limits due to emulsion. SR Surrogate recovery outside the QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 48 bnRISM Fullironm n Analyticals-' Environmental Solutions �Ili —a ATIEs,ING Sample Receipt Summary 02/21 /2014 Prism Work Order: 4020095 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received MW-4 4020095-01 Water 02/05/14 02/06/14 MW-3 4020095-02 Water 02/05/14 02/06/14 BC-2 4020095-03 Water 02/05/14 02/06/14 BC-1 4020095-04 Water 02/05/14 02/06/14 MW-3-A 4020095-05 Water 02/05/14 02/06/14 Samples were received in good condition at 3.2 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 48 Full -Service Analytical & 1°.P.RI S M Environmental Solutions �aao Tw IEs me Summary of Detections 02/21/2014 Prism Work Order: 4020095 Prism ID Client ID Parameter Method Result Units 4020095-01 MW-4 Mercury '7470A 0.0014 mg/L 4020095-01 MW-4 Arsenic '6010C 0.14 mg/L 4020095-01 MW-4 Barium '6010C 6.5 mg/L 4020095-01 MW-4 Cadmium `6010C 0.0017 mg/L 4020095-01 MW-4 Chromium '6010C 0.93 mg/L 4020095-01 MW-4 Lead "6010C 0.25 mg/L 4020095-01 MW-4 Selenium '6010C 0.099 mg/L 4020095-02 MW-3 Barium `6010C 0.16 mg/L 4020095-03 BC-2 Barium '6010C 0.024 mg/L 4020095-04 BC-1 Barium '6010C 0.024 mg/L 4020095-05 MW-3-A Barium `6010C 0.25 mg/L 4020095-05 MW-3-A Chromium '6010C 0.024 mg/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Sample Matrix: Water Client Sample ID: MW-4 Prism Sample ID: 4020095-01 Prism Work Order: 4020095 Time Collected: 02/05/14 14:30 Time Submitted: 02/06/14 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters Hexavalent Chromium BRL Aa mg/L 0.010 0.0026 1 *SM3500-Cr B 2/6/14 11:45 CDE P4130080 Organochlorine Pesticides by GC/ECD 4,4'-DDD BRL ug/L 0.050 0.0036 1 8081B 2/19/14 20:49 JMV P4130132 4,4'-DDE BRL ug/L 0.050 0.0038 1 8081B 2/19/14 20:49 JMV P4130132 4,4'-DDT BRL ug/L 0.050 0.021 1 8081B 2/19/14 20:49 JMV P4130132 Aldrin BRL ug/L 0.050 0.010 1 8081B 2/19/14 20:49 JMV P4130132 alpha-BHC BRLCCV ug/L 0.050 0.0044 1 8081B 2/19/14 20:49 JMV P4130132 cis -Chlordane BRLCCV ug/L 0.050 0.0070 1 8081B 2/19/14 20:49 JMV P4130132 beta-BHC BRL ug/L 0.050 0.0066 1 8081B 2/19/14 20:49 JMV P4130132 Chlordane BRL ug/L 0.50 0.14 1 8081B 2/19/14 20:49 JMV P4130132 delta-BHC BRL ug/L 0.050 0.0033 1 8081B 2/19/14 20:49 JMV P4130132 Dieldrin BRL ug/L 0.050 0.0046 1 8081B 2/19/14 20:49 JMV P4130132 EndosulfanI BRLCCV ug/L 0.050 0.0084 1 8081B 2/19/14 20:49 JMV P4130132 Endosulfan II BRL ug/L 0.050 0.0047 1 8081B 2/19/14 20:49 JMV P4130132 Endosulfan Sulfate BRLCCV ug/L 0.050 0.0047 1 8081B 2/19/14 20:49 JMV P4130132 Endrin BRL ug/L 0.050 0.0046 1 8081B 2/19/14 20:49 JMV P4130132 Endrin Aldehyde BRL ug/L 0.050 0.0053 1 8081B 2/19/14 20:49 JMV P4130132 Endrin Ketone BRLCCV ug/L 0.050 0.0043 1 8081B 2/19/14 20:49 JMV P4130132 gamma-BHC BRLCCV ug/L 0.050 0.0049 1 8081B 2/19/14 20:49 JMV P4130132 trans -Chlordane BRL ug/L 0.050 0.0060 1 8081B 2/19/14 20:49 JMV P4130132 Heptachlor BRL ug/L 0.050 0.0077 1 8081B 2/19/14 20:49 JMV P4130132 Heptachlor Epoxide BRL ug/L 0.050 0.0046 1 8081B 2/19/14 20:49 JMV P4130132 Methoxychlor BRL ug/L 0.050 0.0087 1 8081B 2/19/14 20:49 JMV P4130132 Toxaohene BRL ua/L 050 0.15 1 9081R 9119114 90-49 imv P4130132 Polychlorinated Biphenyls (PCBs) by GC/ECD Aroclor 1016 BRL ug/L Aroclor 1221 BRL ug/L Aroclor 1232 BRL ug/L Aroclor 1242 BRL ug/L Aroclor 1248 BRL ug/L Aroclor 1254 BRL ug/L Aroclor 1260 BRL ug/L Semivolatile Organic Compounds by GC/MS Surrogate Recovery Control Limits Decachlorobiphenyl 79 % 13-186 Tetrachloro-m-xylene 90 % 40-134 0.50 0.16 1 8082A 2/12/14 5:31 JMV P4130133 1.0 0.11 1 8082A 2/12/14 5:31 JMV P4130133 0.50 0.16 1 8082A 2/12/14 5:31 JMV P4130133 0.50 0.14 1 8082A 2/12/14 5:31 JMV P4130133 0.50 0.14 1 8082A 2/12/14 5:31 JMV P4130133 0.50 0.16 1 8082A 2/12/14 5:31 JMV P4130133 0.50 0.14 1 8082A 2/12/14 5:31 JMV P4130133 Surrogate Recovery Control Limits Tetrachloro-m-xylene 82 % 30-161 Decachlorobiphenyl 43 % 32-178 1,2,4-Trichlorobenzene BRL ug/L 10 2.2 1 8270D 2/11/14 19:44 KC P4130157 1,2-Dichlorobenzene BRL ug/L 10 1.8 1 8270D 2/11/14 19:44 KC P4130157 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-4 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-01 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 14:30 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,3-Dichlorobenzene BRL ug/L 10 1.8 1 8270D 2/11/14 19:44 KC P4130157 1,4-Dichlorobenzene BRL ug/L 10 2.0 1 8270D 2/11/14 19:44 KC P4130157 1-Methyl naphthalene BRL ug/L 10 2.5 1 8270D 2/11/14 19:44 KC P4130157 2,4,5-Trichlorophenol BRL ug/L 10 2.5 1 8270D 2/11/14 19:44 KC P4130157 2,4,6-Trichlorophenol BRL ug/L 10 2.3 1 8270D 2/11/14 19:44 KC P4130157 2,4-Dichlorophenol BRL ug/L 10 2.4 1 8270D 2/11/14 19:44 KC P4130157 2,4-Dimethyl phenol BRL ug/L 10 2.4 1 8270D 2/11/14 19:44 KC P4130157 2,4-Dinitrophenol BRL ug/L 10 2.4 1 8270D 2/11/14 19:44 KC P4130157 2,4-Dinitrotoluene BRL ug/L 10 0.95 1 8270D 2/11/14 19:44 KC P4130157 2,6-Dinitrotoluene BRL ug/L 10 1.6 1 8270D 2/11/14 19:44 KC P4130157 2-Chloronaphthalene BRL ug/L 10 2.3 1 8270D 2/11/14 19:44 KC P4130157 2-Chlorophenol BRL ug/L 10 2.1 1 8270D 2/11/14 19:44 KC P4130157 2-Methyl naphthalene BRL ug/L 10 2.6 1 8270D 2/11/14 19:44 KC P4130157 2-Methylphenol BRL ug/L 10 2.4 1 8270D 2/11/14 19:44 KC P4130157 2-Nitroaniline BRL ug/L 10 1.9 1 8270D 2/11/14 19:44 KC P4130157 2-Nitrophenol BRL ug/L 10 2.5 1 8270D 2/11/14 19:44 KC P4130157 3,3'-Dichlorobenzidine BRL ug/L 10 0.96 1 8270D 2/11/14 19:44 KC P4130157 3/4-Methyl phenol BRL ug/L 10 2.4 1 8270D 2/11/14 19:44 KC P4130157 3-Nitroaniline BRL ug/L 10 1.3 1 8270D 2/11/14 19:44 KC P4130157 4,6-Dinitro-2-methylphenol BRL CCV ug/L 10 2.7 1 8270D 2/11/14 19:44 KC P4130157 4-Bromophenyl phenyl ether BRL ug/L 10 1.8 1 8270D 2/11/14 19:44 KC P4130157 4-Chloro-3-methylphenol BRL ug/L 10 2.3 1 8270D 2/11/14 19:44 KC P4130157 4-Chloroaniline BRL CCV ug/L 10 2.5 1 8270D 2/11/14 19:44 KC P4130157 4-Chlorophenyl phenyl ether BRL ug/L 10 1.8 1 8270D 2/11/14 19:44 KC P4130157 4-Nitroaniline BRL ug/L 10 0.91 1 8270D 2/11/14 19:44 KC P4130157 4-Nitrophenol BRL ug/L 10 2.6 1 8270D 2/11/14 19:44 KC P4130157 Acenaphthene BRL ug/L 10 2.1 1 8270D 2/11/14 19:44 KC P4130157 Acenaphthylene BRL ug/L 10 2.2 1 8270D 2/11/14 19:44 KC P4130157 Aniline BRL ug/L 10 2.2 1 8270D 2/11/14 19:44 KC P4130157 Anthracene BRL ug/L 10 1.2 1 8270D 2/11/14 19:44 KC P4130157 Azobenzene BRL ug/L 10 1.8 1 8270D 2/11/14 19:44 KC P4130157 Benzo(a)anthracene BRL ug/L 10 0.95 1 8270D 2/11/14 19:44 KC P4130157 Benzo(a)pyrene BRL ug/L 10 1.1 1 8270D 2/11/14 19:44 KC P4130157 Benzo(b)fluoranthene BRL ug/L 10 1.4 1 8270D 2/11/14 19:44 KC P4130157 Benzo(g,h,i)perylene BRL ug/L 10 2.1 1 8270D 2/11/14 19:44 KC P4130157 Benzo(k)fluoranthene BRL ug/L 10 1.1 1 8270D 2/11/14 19:44 KC P4130157 Benzoic Acid BRL ug/L 100 50 1 8270D 2/11/14 19:44 KC P4130157 Benzyl alcohol BRL ug/L 10 2.1 1 8270D 2/11/14 19:44 KC P4130157 bis(2-Chloroethoxy)methane BRL ug/L 10 2.2 1 8270D 2/11/14 19:44 KC P4130157 Bis(2-Chloroethyl)ether BRL ug/L 10 1.9 1 8270D 2/11/14 19:44 KC P4130157 Bis(2-chloroisopropyl)ether BRL CCV ug/L 10 2.3 1 8270D 2/11/14 19:44 KC P4130157 Bis(2-Ethylhexyl)phthalate BRL ug/L 10 1.8 1 8270D 2/11/14 19:44 KC P4130157 Butyl benzyl phthalate BRL ug/L 10 1.5 1 8270D 2/11/14 19:44 KC P4130157 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-4 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-01 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 14:30 Time Submitted: 02/06/14 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Chrysene BRL ug/L 10 1.2 1 8270D 2/11/14 19:44 KC P4130157 Dibenzo(a,h)anth racene BRL ug/L 10 1.8 1 8270D 2/11/14 19:44 KC P4130157 Dibenzofuran BRL ug/L 10 2.2 1 8270D 2/11/14 19:44 KC P4130157 Diethyl phthalate BRL ug/L 10 1.4 1 8270D 2/11/14 19:44 KC P4130157 Dimethyl phthalate BRL ug/L 10 1.6 1 8270D 2/11/14 19:44 KC P4130157 Di-n-butyl phthalate BRL ug/L 10 1.8 1 8270D 2/11/14 19:44 KC P4130157 Di-n-octyl phthalate BRL ug/L 10 1.9 1 8270D 2/11/14 19:44 KC P4130157 Fluoranthene BRL ug/L 10 0.94 1 8270D 2/11/14 19:44 KC P4130157 Fluorene BRL ug/L 10 1.8 1 8270D 2/11/14 19:44 KC P4130157 Hexachlorobenzene BRL ug/L 10 1.4 1 8270D 2/11/14 19:44 KC P4130157 Hexachlorobutadiene BRL ug/L 10 2.3 1 8270D 2/11/14 19:44 KC P4130157 Hexachlorocyclopentadiene BRL CCV, ug/L 10 1.8 1 8270D 2/11/14 19:44 KC P4130157 ICV Hexachloroethane BRL ug/L 10 1.9 1 8270D 2/11/14 19:44 KC P4130157 Indeno(1,2,3-cd)pyrene BRL ug/L 10 1.6 1 8270D 2/11/14 19:44 KC P4130157 Isophorone BRL CCV ug/L 10 2.4 1 8270D 2/11/14 19:44 KC P4130157 Naphthalene BRL ug/L 10 2.3 1 8270D 2/11/14 19:44 KC P4130157 Nitrobenzene BRL ug/L 10 2.0 1 8270D 2/11/14 19:44 KC P4130157 N-Nitroso-di-n-propylamine BRL ug/L 10 2.3 1 8270D 2/11/14 19:44 KC P4130157 N-Nitrosodiphenylamine BRL ug/L 10 1.6 1 8270D 2/11/14 19:44 KC P4130157 Pentachlorophenol BRL ug/L 10 1.6 1 8270D 2/11/14 19:44 KC P4130157 Phenanthrene BRL ug/L 10 1.2 1 8270D 2/11/14 19:44 KC P4130157 Phenol BRL ug/L 10 2.2 1 8270D 2/11/14 19:44 KC P4130157 Pyrene BRL ug/L 10 1.4 1 8270D 2/11/14 19:44 KC P4130157 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 73 % 49-109 2-Fluorobiphenyl 58 % 55-96 2-Fluorophenol 35 % 27-74 Nitrobenzene-d5 65 % 53-99 Phenol-d5 24 % 11-52 Terphenyl-d14 70 % 42-133 Total Metals Mercury 0.0014 mg/L 0.00020 0.000012 1 *7470A 2/18/14 16:53 MEH P4130278 Arsenic 0.14 mg/L 0.010 0.0016 1 *6010C 2/7/14 17:01 BGM P4130106 Barium 6.5 mg/L 0.10 0.031 10 *6010C 2110/14 19:24 BGM P4130106 Cadmium 0.0017 mg/L 0.0010 0.000039 1 *6010C 2/7/14 17:01 BGM P4130106 Chromium 0.93 mg/L 0.0050 0.00036 1 *6010C 2/7/14 17:01 BGM P4130106 Lead 0.25 mg/L 0.0050 0.00039 1 *6010C 2/7/14 17:01 BGM P4130106 Selenium 0.099 mg/L 0.020 0.0037 1 *6010C 217/14 17:01 BGM P4130106 Silver BRL mg/L 0.0050 0.00012 1 *6010C 2/7/14 17:01 BGM P4130106 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.15 1 8260B 2/6/14 19:00 VHL P4130098 1,1,1-Trichloroethane BRL ug/L 0.50 0.063 1 8260B 2/6/14 19:00 VHL P4130098 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-4 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-01 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 14:30 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.071 1 8260B 2/6/14 19:00 VHL P4130098 1,1,2-Trichloroethane BRL ug/L 0.50 0.17 1 8260B 2/6/14 19:00 VHL P4130098 1,1-Dichloroethane BRL ug/L 0.50 0.096 1 8260B 2/6/14 19:00 VHL P4130098 1,1-Dichloroethylene BRL ug/L 0.50 0.078 1 8260B 2/6/14 19:00 VHL P4130098 1,1-Dichloropropylene BRL ug/L 0.50 0.061 1 8260B 2/6/14 19:00 VHL P4130098 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.20 1 8260B 2/6/14 19:00 VHL P4130098 1,2,3-Trichloropropane BRL ug/L 1.0 0.081 1 8260B 2/6/14 19:00 VHL P4130098 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.10 1 8260B 2/6/14 19:00 VHL P4130098 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.048 1 8260B 2/6/14 19:00 VHL P4130098 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.59 1 8260B 2/6/14 19:00 VHL P4130098 1,2-Dibromoethane BRL ug/L 0.50 0.14 1 8260B 2/6/14 19:00 VHL P4130098 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 2/6/14 19:00 VHL P4130098 1,2-Dichloroethane BRL ug/L 0.50 0.14 1 8260B 2/6/14 19:00 VHL P4130098 1,2-Dichloropropane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:00 VHL P4130098 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.057 1 8260B 2/6/14 19:00 VHL P4130098 1,3-Dichlorobenzene BRL ug/L 0.50 0.074 1 8260B 2/6/14 19:00 VHL P4130098 1,3-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 2/6/14 19:00 VHL P4130098 1,4-Dichlorobenzene BRL ug/L 0.50 0.068 1 8260B 2/6/14 19:00 VHL P4130098 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 2/6/14 19:00 VHL P4130098 2-Chloroethyl Vinyl Ether BRL ug/L 2.0 0.22 1 8260B 2/6/14 19:00 VHL P4130098 2-Chlorotoluene BRL ug/L 0.50 0.038 1 8260B 2/6/14 19:00 VHL P4130098 4-Chlorotoluene BRL ug/L 0.50 0.053 1 8260B 2/6/14 19:00 VHL P4130098 4-Isopropyltoluene BRL ug/L 0.50 0.065 1 8260B 2/6/14 19:00 VHL P4130098 Acetone BRL ug/L 5.0 0.62 1 8260B 2/6/14 19:00 VHL P4130098 Acrolein BRL ug/L 20 1.1 1 8260B 2/6/14 19:00 VHL P4130098 Acrylonitrile BRL ug/L 20 0.86 1 8260B 2/6/14 19:00 VHL P4130098 Benzene BRL ug/L 0.50 0.072 1 8260B 2/6/14 19:00 VHL P4130098 Bromobenzene BRL ug/L 0.50 0.064 1 8260B 2/6/14 19:00 VHL P4130098 Bromochloromethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:00 VHL P4130098 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 2/6/14 19:00 VHL P4130098 Bromoform BRL ug/L 1.0 0.27 1 8260B 2/6/14 19:00 VHL P4130098 Bromomethane BRL ug/L 1.0 0.47 1 8260B 2/6/14 19:00 VHL P4130098 Carbon disulfide BRL ug/L 5.0 1.4 1 8260B 2/6/14 19:00 VHL P4130098 Carbon Tetrachloride BRL ug/L 0.50 0.12 1 8260B 2/6/14 19:00 VHL P4130098 Chlorobenzene BRL ug/L 0.50 0.061 1 8260B 2/6/14 19:00 VHL P4130098 Chloroethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:00 VHL P4130098 Chloroform BRL ug/L 0.50 0.089 1 8260B 2/6/14 19:00 VHL P4130098 Chloromethane BRL ug/L 0.50 0.11 1 8260B 2/6/14 19:00 VHL P4130098 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.076 1 8260B 2/6/14 19:00 VHL P4130098 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.10 1 8260B 2/6/14 19:00 VHL P4130098 Dibromochloromethane BRL ug/L 0.50 0.30 1 8260B 2/6/14 19:00 VHL P4130098 Dibromomethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:00 VHL P4130098 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 8260B 2/6/14 19:00 VHL P4130098 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-4 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-01 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 14:30 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Ethylbenzene BRL ug/L 0.50 0.067 1 8260B 2/6/14 19:00 VHL P4130098 Hexachlorobutadiene BRL ug/L 2.0 0.36 1 8260B 2/6/14 19:00 VHL P4130098 Isopropyl Ether BRL ug/L 0.50 0.043 1 8260B 2/6/14 19:00 VHL P4130098 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.072 1 8260B 2/6/14 19:00 VHL P4130098 m,p-Xylenes BRL ug/L 1.0 0.081 1 8260B 2/6/14 19:00 VHL P4130098 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.19 1 8260B 2/6/14 19:00 VHL P4130098 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.90 1 8260B 2/6/14 19:00 VHL P4130098 Methyl Isobutyl Ketone BRL ug/L 5.0 0.12 1 8260B 2/6/14 19:00 VHL P4130098 Methylene Chloride BRL ug/L 1.0 0.44 1 8260B 2/6/14 19:00 VHL P4130098 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.070 1 8260B 2/6/14 19:00 VHL P4130098 Naphthalene BRL ug/L 1.0 0.098 1 8260B 2/6/14 19:00 VHL P4130098 n-Butylbenzene BRL ug/L 1.0 0.11 1 8260B 2/6/14 19:00 VHL P4130098 n-Propylbenzene BRL ug/L 0.50 0.060 1 8260B 2/6/14 19:00 VHL P4130098 o-Xylene BRL ug/L 0.50 0.046 1 8260B 2/6/14 19:00 VHL P4130098 sec-Butylbenzene BRL ug/L 0.50 0.087 1 8260B 2/6/14 19:00 VHL P4130098 Styrene BRL ug/L 0.50 0.047 1 8260B 2/6/14 19:00 VHL P4130098 tert-Butylbenzene BRL ug/L 0.50 0.080 1 8260B 2/6/14 19:00 VHL P4130098 Tetrachloroethylene BRL ug/L 0.50 0.069 1 8260B 2/6/14 19:00 VHL P4130098 Toluene BRL ug/L 0.50 0.042 1 8260B 2/6/14 19:00 VHL P4130098 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.12 1 8260B 2/6/14 19:00 VHL P4130098 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.043 1 8260B 2/6/14 19:00 VHL P4130098 Trichloroethylene BRL ug/L 0.50 0.054 1 8260B 2/6/14 19:00 VHL P4130098 Trichlorofluoromethane BRL ug/L 0.50 0.088 1 8260B 2/6/14 19:00 VHL P4130098 Vinyl acetate BRL ug/L 2.0 0.10 1 8260B 2/6/14 19:00 VHL P4130098 Vinyl chloride BRL ug/L 0.50 0.16 1 8260B 2/6/14 19:00 VHL P4130098 Xylenes, total BRL ug/L 3.0 0.13 1 8260B 2/6/14 19:00 VHL P4130098 Surrogate Recovery Control Limits 4-Bromofluorobenzene 111 % 80-124 Dibromofluoromethane 111 % 75-129 Toluene-d8 107 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Sample Matrix: Water Client Sample ID: MW-3 Prism Sample ID: 4020095-02 Prism Work Order: 4020095 Time Collected: 02/05/14 15:00 Time Submitted: 02/06/14 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters Hexavalent Chromium BRL mg/L 0.010 0.0026 1 *SM3500-Cr B 2/6/14 11:45 CDE P4130080 Organochlorine Pesticides by GC/ECD 4,4'-DDD BRL ug/L 0.050 0.0036 1 8081B 2/19/14 21:31 JMV P4130132 4,4'-DDE BRL ug/L 0.050 0.0038 1 8081B 2/19/14 21:31 JMV P4130132 4,4'-DDT BRL ug/L 0.050 0.021 1 8081B 2/19/14 21:31 JMV P4130132 Aldrin BRL ug/L 0.050 0.010 1 8081B 2/19/14 21:31 JMV P4130132 alpha-BHC BRLCCV ug/L 0.050 0.0044 1 8081B 2/19/14 21:31 JMV P4130132 cis -Chlordane BRLCCV ug/L 0.050 0.0070 1 8081B 2/19/14 21:31 JMV P4130132 beta-BHC BRL ug/L 0.050 0.0066 1 8081B 2/19/14 21:31 JMV P4130132 Chlordane BRL ug/L 0.50 0.14 1 8081B 2/19/14 21:31 JMV P4130132 delta-BHC BRL ug/L 0.050 0.0033 1 8081B 2/19/14 21:31 JMV P4130132 Dieldrin BRL ug/L 0.050 0.0046 1 8081B 2/19/14 21:31 JMV P4130132 EndosulfanI BRLCCV ug/L 0.050 0.0084 1 8081B 2/19/14 21:31 JMV P4130132 Endosulfan II BRL ug/L 0.050 0.0047 1 8081B 2/19/14 21:31 JMV P4130132 Endosulfan Sulfate BRLCCV ug/L 0.050 0.0047 1 8081B 2/19/14 21:31 JMV P4130132 Endrin BRL ug/L 0.050 0.0046 1 8081B 2/19/14 21:31 JMV P4130132 Endrin Aldehyde BRL ug/L 0.050 0.0053 1 8081B 2/19/14 21:31 JMV P4130132 Endrin Ketone BRLCCV ug/L 0.050 0.0043 1 8081B 2/19/14 21:31 JMV P4130132 gamma-BHC BRLCCV ug/L 0.050 0.0049 1 8081B 2/19/14 21:31 JMV P4130132 trans -Chlordane BRL ug/L 0.050 0.0060 1 8081B 2/19/14 21:31 JMV P4130132 Heptachlor BRL ug/L 0.050 0.0077 1 8081B 2/19/14 21:31 JMV P4130132 Heptachlor Epoxide BRL ug/L 0.050 0.0046 1 8081B 2/19/14 21:31 JMV P4130132 Methoxychlor BRL ug/L 0.050 0.0087 1 8081B 2/19/14 21:31 JMV P4130132 Toxaohene BRL ua/L 050 0.15 1 9081R 9119114 9131 IMV P4130132 Polychlorinated Biphenyls (PCBs) by GC/ECD Aroclor 1016 BRL ug/L Aroclor 1221 BRL ug/L Aroclor 1232 BRL ug/L Aroclor 1242 BRL ug/L Aroclor 1248 BRL ug/L Aroclor 1254 BRL ug/L Aroclor 1260 BRL ug/L Semivolatile Organic Compounds by GC/MS Surrogate Recovery Control Limits Decachlorobiphenyl 92 % 13-186 Tetrachloro-m-xylene 96 % 40-134 0.50 0.16 1 8082A 2/12/14 6:14 JMV P4130133 1.0 0.11 1 8082A 2/12/14 6:14 JMV P4130133 0.50 0.16 1 8082A 2/12/14 6:14 JMV P4130133 0.50 0.14 1 8082A 2/12/14 6:14 JMV P4130133 0.50 0.14 1 8082A 2/12/14 6:14 JMV P4130133 0.50 0.16 1 8082A 2/12/14 6:14 JMV P4130133 0.50 0.14 1 8082A 2/12/14 6:14 JMV P4130133 Surrogate Recovery Control Limits Tetrachloro-m-xylene 93 % 30-161 Decachlorobiphenyl 39 % 32-178 1,2,4-Trichlorobenzene BRL ug/L 10 2.2 1 8270D 2/14/14 18:26 KC P4130157 1,2-Dichlorobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 18:26 KC P4130157 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-3 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-02 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:00 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,3-Dichlorobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 18:26 KC P4130157 1,4-Dichlorobenzene BRL ug/L 10 2.0 1 8270D 2/14/14 18:26 KC P4130157 1-Methyl naphthalene BRL ug/L 10 2.5 1 8270D 2/14/14 18:26 KC P4130157 2,4,5-Trichlorophenol BRL ug/L 10 2.5 1 8270D 2/14/14 18:26 KC P4130157 2,4,6-Trichlorophenol BRL ug/L 10 2.3 1 8270D 2/14/14 18:26 KC P4130157 2,4-Dichlorophenol BRL ug/L 10 2.4 1 8270D 2/14/14 18:26 KC P4130157 2,4-Dimethyl phenol BRL ug/L 10 2.4 1 8270D 2/14/14 18:26 KC P4130157 2,4-Dinitrophenol BRL ug/L 10 2.4 1 8270D 2/14/14 18:26 KC P4130157 2,4-Dinitrotoluene BRL ug/L 10 0.95 1 8270D 2/14/14 18:26 KC P4130157 2,6-Dinitrotoluene BRL ug/L 10 1.6 1 8270D 2/14/14 18:26 KC P4130157 2-Chloronaphthalene BRL ug/L 10 2.3 1 8270D 2/14/14 18:26 KC P4130157 2-Chlorophenol BRL ug/L 10 2.1 1 8270D 2/14/14 18:26 KC P4130157 2-Methyl naphthalene BRL ug/L 10 2.6 1 8270D 2/14/14 18:26 KC P4130157 2-Methylphenol BRL ug/L 10 2.4 1 8270D 2/14/14 18:26 KC P4130157 2-Nitroaniline BRL ug/L 10 1.9 1 8270D 2/14/14 18:26 KC P4130157 2-Nitrophenol BRL ug/L 10 2.5 1 8270D 2/14/14 18:26 KC P4130157 3,3'-Dichlorobenzidine BRL ug/L 10 0.96 1 8270D 2/14/14 18:26 KC P4130157 3/4-Methyl phenol BRL ug/L 10 2.4 1 8270D 2/14/14 18:26 KC P4130157 3-Nitroaniline BRL ug/L 10 1.3 1 8270D 2/14/14 18:26 KC P4130157 4,6-Dinitro-2-methylphenol BRL ug/L 10 2.7 1 8270D 2/14/14 18:26 KC P4130157 4-Bromophenyl phenyl ether BRL ug/L 10 1.8 1 8270D 2/14/14 18:26 KC P4130157 4-Chloro-3-methylphenol BRL ug/L 10 2.3 1 8270D 2/14/14 18:26 KC P4130157 4-Chloroaniline BRL ug/L 10 2.5 1 8270D 2/14/14 18:26 KC P4130157 4-Chlorophenyl phenyl ether BRL ug/L 10 1.8 1 8270D 2/14/14 18:26 KC P4130157 4-Nitroaniline BRL ug/L 10 0.91 1 8270D 2/14/14 18:26 KC P4130157 4-Nitrophenol BRL ug/L 10 2.6 1 8270D 2/14/14 18:26 KC P4130157 Acenaphthene BRL ug/L 10 2.1 1 8270D 2/14/14 18:26 KC P4130157 Acenaphthylene BRL ug/L 10 2.2 1 8270D 2/14/14 18:26 KC P4130157 Aniline BRL ug/L 10 2.2 1 8270D 2/14/14 18:26 KC P4130157 Anthracene BRL ug/L 10 1.2 1 8270D 2/14/14 18:26 KC P4130157 Azobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 18:26 KC P4130157 Benzo(a)anthracene BRL ug/L 10 0.95 1 8270D 2/14/14 18:26 KC P4130157 Benzo(a)pyrene BRL ug/L 10 1.1 1 8270D 2/14/14 18:26 KC P4130157 Benzo(b)fluoranthene BRL ug/L 10 1.4 1 8270D 2/14/14 18:26 KC P4130157 Benzo(g,h,i)perylene BRL ug/L 10 2.1 1 8270D 2/14/14 18:26 KC P4130157 Benzo(k)fluoranthene BRL ug/L 10 1.1 1 8270D 2/14/14 18:26 KC P4130157 Benzoic Acid BRL ug/L 100 50 1 8270D 2/14/14 18:26 KC P4130157 Benzyl alcohol BRL ug/L 10 2.1 1 8270D 2/14/14 18:26 KC P4130157 bis(2-Chloroethoxy)methane BRL ug/L 10 2.2 1 8270D 2/14/14 18:26 KC P4130157 Bis(2-Chloroethyl)ether BRL ug/L 10 1.9 1 8270D 2/14/14 18:26 KC P4130157 Bis(2-chloroisopropyl)ether BRL ug/L 10 2.3 1 8270D 2/14/14 18:26 KC P4130157 Bis(2-Ethylhexyl)phthalate BRL ug/L 10 1.8 1 8270D 2/14/14 18:26 KC P4130157 Butyl benzyl phthalate BRL ug/L 10 1.5 1 8270D 2/14/14 18:26 KC P4130157 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-3 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-02 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:00 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Chrysene BRL ug/L 10 1.2 1 8270D 2/14/14 18:26 KC P4130157 Dibenzo(a,h)anth racene BRL ug/L 10 1.8 1 8270D 2/14/14 18:26 KC P4130157 Dibenzofuran BRL ug/L 10 2.2 1 8270D 2/14/14 18:26 KC P4130157 Diethyl phthalate BRL ug/L 10 1.4 1 8270D 2/14/14 18:26 KC P4130157 Dimethyl phthalate BRL ug/L 10 1.6 1 8270D 2/14/14 18:26 KC P4130157 Di-n-butyl phthalate BRL ug/L 10 1.8 1 8270D 2/14/14 18:26 KC P4130157 Di-n-octyl phthalate BRL ug/L 10 1.9 1 8270D 2/14/14 18:26 KC P4130157 Fluoranthene BRL ug/L 10 0.94 1 8270D 2/14/14 18:26 KC P4130157 Fluorene BRL ug/L 10 1.8 1 8270D 2/14/14 18:26 KC P4130157 Hexachlorobenzene BRL ug/L 10 1.4 1 8270D 2/14/14 18:26 KC P4130157 Hexachlorobutadiene BRL ug/L 10 2.3 1 8270D 2/14/14 18:26 KC P4130157 Hexachlorocyclopentadiene BRL ug/L 10 1.8 1 8270D 2/14/14 18:26 KC P4130157 Hexachloroethane BRL ug/L 10 1.9 1 8270D 2/14/14 18:26 KC P4130157 Indeno(1,2,3-cd)pyrene BRL ug/L 10 1.6 1 8270D 2/14/14 18:26 KC P4130157 Isophorone BRL ug/L 10 2.4 1 8270D 2/14/14 18:26 KC P4130157 Naphthalene BRL ug/L 10 2.3 1 8270D 2/14/14 18:26 KC P4130157 Nitrobenzene BRL ug/L 10 2.0 1 8270D 2/14/14 18:26 KC P4130157 N-Nitroso-di-n-propylamine BRL ug/L 10 2.3 1 8270D 2/14/14 18:26 KC P4130157 N-Nitrosodiphenylamine BRL ug/L 10 1.6 1 8270D 2/14/14 18:26 KC P4130157 Pentachlorophenol BRL ug/L 10 1.6 1 8270D 2/14/14 18:26 KC P4130157 Phenanthrene BRL ug/L 10 1.2 1 8270D 2/14/14 18:26 KC P4130157 Phenol BRL ug/L 10 2.2 1 8270D 2/14/14 18:26 KC P4130157 Pyrene BRL ug/L 10 1.4 1 8270D 2/14/14 18:26 KC P4130157 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 18 % 49-109 SE 2-Fluorobiphenyl 38 % 55-96 SE 2-Fluorophenol 12 % 27-74 SE Nitrobenzene-d5 42 % 53-99 SE Phenol-d5 8 % 11-52 SE Terphenyl-d14 43 % 42-133 Total Metals Mercury BRL mg/L 0.00020 0.000012 1 *7470A 2/18/14 16:56 MEH P4130278 Arsenic BRL mg/L 0.010 0.0016 1 *6010C 2/7/14 16:39 BGM P4130106 Barium 0.16 mg/L 0.010 0.0031 1 *6010C 2/7/14 16:39 BGM P4130106 Cadmium BRL mg/L 0.0010 0.000039 1 *6010C 2/7/14 16:39 BGM P4130106 Chromium BRL mg/L 0.0050 0.00036 1 *6010C 2/7/14 16:39 BGM P4130106 Lead BRL mg/L 0.0050 0.00039 1 *6010C 2/7/14 16:39 BGM P4130106 Selenium BRL mg/L 0.020 0.0037 1 *6010C 2/7/14 16:39 BGM P4130106 Silver BRL mg/L 0.0050 0.00012 1 *6010C 2/7/14 16:39 BGM P4130106 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.15 1 8260B 2/6/14 19:26 VHL P4130098 1,1,1-Trichloroethane BRL ug/L 0.50 0.063 1 8260B 2/6/14 19:26 VHL P4130098 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.071 1 8260B 2/6/14 19:26 VHL P4130098 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-3 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-02 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:00 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,2-Trichloroethane BRL ug/L 0.50 0.17 1 8260B 2/6/14 19:26 VHL P4130098 1,1-Dichloroethane BRL ug/L 0.50 0.096 1 8260B 2/6/14 19:26 VHL P4130098 1,1-Dichloroethylene BRL ug/L 0.50 0.078 1 8260B 2/6/14 19:26 VHL P4130098 1,1-Dichloropropylene BRL ug/L 0.50 0.061 1 8260B 2/6/14 19:26 VHL P4130098 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.20 1 8260B 2/6/14 19:26 VHL P4130098 1,2,3-Trichloropropane BRL ug/L 1.0 0.081 1 8260B 2/6/14 19:26 VHL P4130098 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.10 1 8260B 2/6/14 19:26 VHL P4130098 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.048 1 8260B 2/6/14 19:26 VHL P4130098 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.59 1 8260B 2/6/14 19:26 VHL P4130098 1,2-Dibromoethane BRL ug/L 0.50 0.14 1 8260B 2/6/14 19:26 VHL P4130098 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 2/6/14 19:26 VHL P4130098 1,2-Dichloroethane BRL ug/L 0.50 0.14 1 8260B 2/6/14 19:26 VHL P4130098 1,2-Dichloropropane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:26 VHL P4130098 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.057 1 8260B 2/6/14 19:26 VHL P4130098 1,3-Dichlorobenzene BRL ug/L 0.50 0.074 1 8260B 2/6/14 19:26 VHL P4130098 1,3-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 2/6/14 19:26 VHL P4130098 1,4-Dichlorobenzene BRL ug/L 0.50 0.068 1 8260B 2/6/14 19:26 VHL P4130098 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 2/6/14 19:26 VHL P4130098 2-Chloroethyl Vinyl Ether BRL ug/L 2.0 0.22 1 8260B 2/6/14 19:26 VHL P4130098 2-Chlorotoluene BRL ug/L 0.50 0.038 1 8260B 2/6/14 19:26 VHL P4130098 4-Chlorotoluene BRL ug/L 0.50 0.053 1 8260B 2/6/14 19:26 VHL P4130098 4-Isopropyltoluene BRL ug/L 0.50 0.065 1 8260B 2/6/14 19:26 VHL P4130098 Acetone BRL ug/L 5.0 0.62 1 8260B 2/6/14 19:26 VHL P4130098 Acrolein BRL ug/L 20 1.1 1 8260B 2/6/14 19:26 VHL P4130098 Acrylonitrile BRL ug/L 20 0.86 1 8260B 2/6/14 19:26 VHL P4130098 Benzene BRL ug/L 0.50 0.072 1 8260B 2/6/14 19:26 VHL P4130098 Bromobenzene BRL ug/L 0.50 0.064 1 8260B 2/6/14 19:26 VHL P4130098 Bromochloromethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:26 VHL P4130098 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 2/6/14 19:26 VHL P4130098 Bromoform BRL ug/L 1.0 0.27 1 8260B 2/6/14 19:26 VHL P4130098 Bromomethane BRL ug/L 1.0 0.47 1 8260B 2/6/14 19:26 VHL P4130098 Carbon disulfide BRL ug/L 5.0 1.4 1 8260B 2/6/14 19:26 VHL P4130098 Carbon Tetrachloride BRL ug/L 0.50 0.12 1 8260B 2/6/14 19:26 VHL P4130098 Chlorobenzene BRL ug/L 0.50 0.061 1 8260B 2/6/14 19:26 VHL P4130098 Chloroethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:26 VHL P4130098 Chloroform BRL ug/L 0.50 0.089 1 8260B 2/6/14 19:26 VHL P4130098 Chloromethane BRL ug/L 0.50 0.11 1 8260B 2/6/14 19:26 VHL P4130098 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.076 1 8260B 2/6/14 19:26 VHL P4130098 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.10 1 8260B 2/6/14 19:26 VHL P4130098 Dibromochloromethane BRL ug/L 0.50 0.30 1 8260B 2/6/14 19:26 VHL P4130098 Dibromomethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:26 VHL P4130098 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 8260B 2/6/14 19:26 VHL P4130098 Ethylbenzene BRL ug/L 0.50 0.067 1 8260B 2/6/14 19:26 VHL P4130098 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-3 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-02 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:00 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Hexachlorobutadiene BRL ug/L 2.0 0.36 1 8260B 2/6/14 19:26 VHL P4130098 Isopropyl Ether BRL ug/L 0.50 0.043 1 8260B 2/6/14 19:26 VHL P4130098 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.072 1 8260B 2/6/14 19:26 VHL P4130098 m,p-Xylenes BRL ug/L 1.0 0.081 1 8260B 2/6/14 19:26 VHL P4130098 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.19 1 8260B 2/6/14 19:26 VHL P4130098 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.90 1 8260B 2/6/14 19:26 VHL P4130098 Methyl Isobutyl Ketone BRL ug/L 5.0 0.12 1 8260B 2/6/14 19:26 VHL P4130098 Methylene Chloride BRL ug/L 1.0 0.44 1 8260B 2/6/14 19:26 VHL P4130098 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.070 1 8260B 2/6/14 19:26 VHL P4130098 Naphthalene BRL ug/L 1.0 0.098 1 8260B 2/6/14 19:26 VHL P4130098 n-Butylbenzene BRL ug/L 1.0 0.11 1 8260B 2/6/14 19:26 VHL P4130098 n-Propylbenzene BRL ug/L 0.50 0.060 1 8260B 2/6/14 19:26 VHL P4130098 o-Xylene BRL ug/L 0.50 0.046 1 8260B 2/6/14 19:26 VHL P4130098 sec-Butylbenzene BRL ug/L 0.50 0.087 1 8260B 2/6/14 19:26 VHL P4130098 Styrene BRL ug/L 0.50 0.047 1 8260B 2/6/14 19:26 VHL P4130098 tert-Butylbenzene BRL ug/L 0.50 0.080 1 8260B 2/6/14 19:26 VHL P4130098 Tetrachloroethylene BRL ug/L 0.50 0.069 1 8260B 2/6/14 19:26 VHL P4130098 Toluene BRL ug/L 0.50 0.042 1 8260B 2/6/14 19:26 VHL P4130098 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.12 1 8260B 2/6/14 19:26 VHL P4130098 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.043 1 8260B 2/6/14 19:26 VHL P4130098 Trichloroethylene BRL ug/L 0.50 0.054 1 8260B 2/6/14 19:26 VHL P4130098 Trichlorofluoromethane BRL ug/L 0.50 0.088 1 8260B 2/6/14 19:26 VHL P4130098 Vinyl acetate BRL ug/L 2.0 0.10 1 8260B 2/6/14 19:26 VHL P4130098 Vinyl chloride BRL ug/L 0.50 0.16 1 8260B 2/6/14 19:26 VHL P4130098 Xylenes, total BRL ug/L 3.0 0.13 1 8260B 2/6/14 19:26 VHL P4130098 Surrogate Recovery Control Limits 4-Bromofluorobenzene 109 % 80-124 Dibromofluoromethane 115 % 75-129 Toluene-d8 106 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Sample Matrix: Water Client Sample ID: BC-2 Prism Sample ID: 4020095-03 Prism Work Order: 4020095 Time Collected: 02/05/14 15:30 Time Submitted: 02/06/14 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters Hexavalent Chromium BRL mg/L 0.010 0.0026 1 *SM3500-Cr B 2/6/14 11:45 CDE P4130080 Organochlorine Pesticides by GC/ECD 4,4'-DDD BRL ug/L 0.050 0.0036 1 8081B 2/19/14 22:14 JMV P4130132 4,4'-DDE BRL ug/L 0.050 0.0038 1 8081B 2/19/14 22:14 JMV P4130132 4,4'-DDT BRL ug/L 0.050 0.021 1 8081B 2/19/14 22:14 JMV P4130132 Aldrin BRL ug/L 0.050 0.010 1 8081B 2/19/14 22:14 JMV P4130132 alpha-BHC BRLCCV ug/L 0.050 0.0044 1 8081B 2/19/14 22:14 JMV P4130132 cis -Chlordane BRLCCV ug/L 0.050 0.0070 1 8081B 2/19/14 22:14 JMV P4130132 beta-BHC BRL ug/L 0.050 0.0066 1 8081B 2/19/14 22:14 JMV P4130132 Chlordane BRL ug/L 0.50 0.14 1 8081B 2/19/14 22:14 JMV P4130132 delta-BHC BRL ug/L 0.050 0.0033 1 8081B 2/19/14 22:14 JMV P4130132 Dieldrin BRL ug/L 0.050 0.0046 1 8081B 2/19/14 22:14 JMV P4130132 EndosulfanI BRLCCV ug/L 0.050 0.0084 1 8081B 2/19/14 22:14 JMV P4130132 Endosulfan II BRL ug/L 0.050 0.0047 1 8081B 2/19/14 22:14 JMV P4130132 Endosulfan Sulfate BRLCCV ug/L 0.050 0.0047 1 8081B 2/19/14 22:14 JMV P4130132 Endrin BRL ug/L 0.050 0.0046 1 8081B 2/19/14 22:14 JMV P4130132 Endrin Aldehyde BRL ug/L 0.050 0.0053 1 8081B 2/19/14 22:14 JMV P4130132 Endrin Ketone BRLCCV ug/L 0.050 0.0043 1 8081B 2/19/14 22:14 JMV P4130132 gamma-BHC BRLCCV ug/L 0.050 0.0049 1 8081B 2/19/14 22:14 JMV P4130132 trans -Chlordane BRL ug/L 0.050 0.0060 1 8081B 2/19/14 22:14 JMV P4130132 Heptachlor BRL ug/L 0.050 0.0077 1 8081B 2/19/14 22:14 JMV P4130132 Heptachlor Epoxide BRL ug/L 0.050 0.0046 1 8081B 2/19/14 22:14 JMV P4130132 Methoxychlor BRL ug/L 0.050 0.0087 1 8081B 2/19/14 22:14 JMV P4130132 Toxaohene BRL ua/L 050 0.15 1 9081R 9119114 99-14 IMV P4130132 Polychlorinated Biphenyls (PCBs) by GC/ECD Aroclor 1016 BRL ug/L Aroclor 1221 BRL ug/L Aroclor 1232 BRL ug/L Aroclor 1242 BRL ug/L Aroclor 1248 BRL ug/L Aroclor 1254 BRL ug/L Aroclor 1260 BRL ug/L Semivolatile Organic Compounds by GC/MS Surrogate Recovery Control Limits Decachlorobiphenyl 125 % 13-186 Tetrachloro-m-xylene 95 % 40-134 0.50 0.16 1 8082A 2/12/14 6:57 JMV P4130133 1.0 0.11 1 8082A 2/12/14 6:57 JMV P4130133 0.50 0.16 1 8082A 2/12/14 6:57 JMV P4130133 0.50 0.14 1 8082A 2/12/14 6:57 JMV P4130133 0.50 0.14 1 8082A 2/12/14 6:57 JMV P4130133 0.50 0.16 1 8082A 2/12/14 6:57 JMV P4130133 0.50 0.14 1 8082A 2/12/14 6:57 JMV P4130133 Surrogate Recovery Control Limits Tetrachloro-m-xylene 88 % 30-161 Decachlorobiphenyl 66 % 32-178 1,2,4-Trichlorobenzene BRL ug/L 10 2.2 1 8270D 2/14/14 18:48 KC P4130157 1,2-Dichlorobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 18:48 KC P4130157 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: BC-2 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-03 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:30 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID 1,3-Dichlorobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 18:48 KC P4130157 1,4-Dichlorobenzene BRL ug/L 10 2.0 1 8270D 2/14/14 18:48 KC P4130157 1-Methyl naphthalene BRL ug/L 10 2.5 1 8270D 2/14/14 18:48 KC P4130157 2,4,5-Trichlorophenol BRL ug/L 10 2.5 1 8270D 2/14/14 18:48 KC P4130157 2,4,6-Trichlorophenol BRL ug/L 10 2.3 1 8270D 2/14/14 18:48 KC P4130157 2,4-Dichlorophenol BRL ug/L 10 2.4 1 8270D 2/14/14 18:48 KC P4130157 2,4-Dimethyl phenol BRL ug/L 10 2.4 1 8270D 2/14/14 18:48 KC P4130157 2,4-Dinitrophenol BRL ug/L 10 2.4 1 8270D 2/14/14 18:48 KC P4130157 2,4-Dinitrotoluene BRL ug/L 10 0.95 1 8270D 2/14/14 18:48 KC P4130157 2,6-Dinitrotoluene BRL ug/L 10 1.6 1 8270D 2/14/14 18:48 KC P4130157 2-Chloronaphthalene BRL ug/L 10 2.3 1 8270D 2/14/14 18:48 KC P4130157 2-Chlorophenol BRL ug/L 10 2.1 1 8270D 2/14/14 18:48 KC P4130157 2-Methyl naphthalene BRL ug/L 10 2.6 1 8270D 2/14/14 18:48 KC P4130157 2-Methylphenol BRL ug/L 10 2.4 1 8270D 2/14/14 18:48 KC P4130157 2-Nitroaniline BRL ug/L 10 1.9 1 8270D 2/14/14 18:48 KC P4130157 2-Nitrophenol BRL ug/L 10 2.5 1 8270D 2/14/14 18:48 KC P4130157 3,3'-Dichlorobenzidine BRL ug/L 10 0.96 1 8270D 2/14/14 18:48 KC P4130157 3/4-Methyl phenol BRL ug/L 10 2.4 1 8270D 2/14/14 18:48 KC P4130157 3-Nitroaniline BRL ug/L 10 1.3 1 8270D 2/14/14 18:48 KC P4130157 4,6-Dinitro-2-methylphenol BRL ug/L 10 2.7 1 8270D 2/14/14 18:48 KC P4130157 4-Bromophenyl phenyl ether BRL ug/L 10 1.8 1 8270D 2/14/14 18:48 KC P4130157 4-Chloro-3-methylphenol BRL ug/L 10 2.3 1 8270D 2/14/14 18:48 KC P4130157 4-Chloroaniline BRL ug/L 10 2.5 1 8270D 2/14/14 18:48 KC P4130157 4-Chlorophenyl phenyl ether BRL ug/L 10 1.8 1 8270D 2/14/14 18:48 KC P4130157 4-Nitroaniline BRL ug/L 10 0.91 1 8270D 2/14/14 18:48 KC P4130157 4-Nitrophenol BRL ug/L 10 2.6 1 8270D 2/14/14 18:48 KC P4130157 Acenaphthene BRL ug/L 10 2.1 1 8270D 2/14/14 18:48 KC P4130157 Acenaphthylene BRL ug/L 10 2.2 1 8270D 2/14/14 18:48 KC P4130157 Aniline BRL ug/L 10 2.2 1 8270D 2/14/14 18:48 KC P4130157 Anthracene BRL ug/L 10 1.2 1 8270D 2/14/14 18:48 KC P4130157 Azobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 18:48 KC P4130157 Benzo(a)anthracene BRL ug/L 10 0.95 1 8270D 2/14/14 18:48 KC P4130157 Benzo(a)pyrene BRL ug/L 10 1.1 1 8270D 2/14/14 18:48 KC P4130157 Benzo(b)fluoranthene BRL ug/L 10 1.4 1 8270D 2/14/14 18:48 KC P4130157 Benzo(g,h,i)perylene BRL ug/L 10 2.1 1 8270D 2/14/14 18:48 KC P4130157 Benzo(k)fluoranthene BRL ug/L 10 1.1 1 8270D 2/14/14 18:48 KC P4130157 Benzoic Acid BRL ug/L 100 50 1 8270D 2/14/14 18:48 KC P4130157 Benzyl alcohol BRL ug/L 10 2.1 1 8270D 2/14/14 18:48 KC P4130157 bis(2-Chloroethoxy)methane BRL ug/L 10 2.2 1 8270D 2/14/14 18:48 KC P4130157 Bis(2-Chloroethyl)ether BRL ug/L 10 1.9 1 8270D 2/14/14 18:48 KC P4130157 Bis(2-chloroisopropyl)ether BRL ug/L 10 2.3 1 8270D 2/14/14 18:48 KC P4130157 Bis(2-Ethylhexyl)phthalate BRL ug/L 10 1.8 1 8270D 2/14/14 18:48 KC P4130157 Butyl benzyl phthalate BRL ug/L 10 1.5 1 8270D 2/14/14 18:48 KC P4130157 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: BC-2 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-03 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:30 Time Submitted: 02/06/14 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Chrysene BRL ug/L 10 1.2 1 8270D 2/14/14 18:48 KC P4130157 Dibenzo(a,h)anth racene BRL ug/L 10 1.8 1 8270D 2/14/14 18:48 KC P4130157 Dibenzofuran BRL ug/L 10 2.2 1 8270D 2/14/14 18:48 KC P4130157 Diethyl phthalate BRL ug/L 10 1.4 1 8270D 2/14/14 18:48 KC P4130157 Dimethyl phthalate BRL ug/L 10 1.6 1 8270D 2/14/14 18:48 KC P4130157 Di-n-butyl phthalate BRL ug/L 10 1.8 1 8270D 2/14/14 18:48 KC P4130157 Di-n-octyl phthalate BRL ug/L 10 1.9 1 8270D 2/14/14 18:48 KC P4130157 Fluoranthene BRL ug/L 10 0.94 1 8270D 2/14/14 18:48 KC P4130157 Fluorene BRL ug/L 10 1.8 1 8270D 2/14/14 18:48 KC P4130157 Hexachlorobenzene BRL ug/L 10 1.4 1 8270D 2/14/14 18:48 KC P4130157 Hexachlorobutadiene BRL ug/L 10 2.3 1 8270D 2/14/14 18:48 KC P4130157 Hexachlorocyclopentadiene BRL ug/L 10 1.8 1 8270D 2/14/14 18:48 KC P4130157 Hexachloroethane BRL ug/L 10 1.9 1 8270D 2/14/14 18:48 KC P4130157 Indeno(1,2,3-cd)pyrene BRL ug/L 10 1.6 1 8270D 2/14/14 18:48 KC P4130157 Isophorone BRL ug/L 10 2.4 1 8270D 2/14/14 18:48 KC P4130157 Naphthalene BRL ug/L 10 2.3 1 8270D 2/14/14 18:48 KC P4130157 Nitrobenzene BRL ug/L 10 2.0 1 8270D 2/14/14 18:48 KC P4130157 N-Nitroso-di-n-propylamine BRL ug/L 10 2.3 1 8270D 2/14/14 18:48 KC P4130157 N-Nitrosodiphenylamine BRL ug/L 10 1.6 1 8270D 2/14/14 18:48 KC P4130157 Pentachlorophenol BRL ug/L 10 1.6 1 8270D 2/14/14 18:48 KC P4130157 Phenanthrene BRL ug/L 10 1.2 1 8270D 2/14/14 18:48 KC P4130157 Phenol BRL ug/L 10 2.2 1 8270D 2/14/14 18:48 KC P4130157 Pyrene BRL ug/L 10 1.4 1 8270D 2/14/14 18:48 KC P4130157 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 105 % 49-109 2-Fluorobiphenyl 89 % 55-96 2-Fluorophenol 53 % 27-74 Nitrobenzene-d5 100 % 53-99 SR Phenol-d5 31 % 11-52 Terphenyl-d14 103 % 42-133 Total Metals Mercury BRL mg/L 0.00020 0.000012 1 *7470A 2/18/14 17:00 MEH P4130278 Arsenic BRL mg/L 0.010 0.0016 1 *6010C 2/7/14 17:08 BGM P4130106 Barium 0.024 mg/L 0.010 0.0031 1 *6010C 2/7/14 17:08 BGM P4130106 Cadmium BRL mg/L 0.0010 0.000039 1 *6010C 2/7/14 17:08 BGM P4130106 Chromium BRL mg/L 0.0050 0.00036 1 *6010C 2/7/14 17:08 BGM P4130106 Lead BRL mg/L 0.0050 0.00039 1 *6010C 2/7/14 17:08 BGM P4130106 Selenium BRL mg/L 0.020 0.0037 1 *6010C 2/7/14 17:08 BGM P4130106 Silver BRL mg/L 0.0050 0.00012 1 *6010C 2/7/14 17:08 BGM P4130106 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.15 1 8260B 2/6/14 19:52 VHL P4130098 1,1,1-Trichloroethane BRL ug/L 0.50 0.063 1 8260B 2/6/14 19:52 VHL P4130098 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.071 1 8260B 2/6/14 19:52 VHL P4130098 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: BC-2 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-03 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:30 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,2-Trichloroethane BRL ug/L 0.50 0.17 1 8260B 2/6/14 19:52 VHL P4130098 1,1-Dichloroethane BRL ug/L 0.50 0.096 1 8260B 2/6/14 19:52 VHL P4130098 1,1-Dichloroethylene BRL ug/L 0.50 0.078 1 8260B 2/6/14 19:52 VHL P4130098 1,1-Dichloropropylene BRL ug/L 0.50 0.061 1 8260B 2/6/14 19:52 VHL P4130098 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.20 1 8260B 2/6/14 19:52 VHL P4130098 1,2,3-Trichloropropane BRL ug/L 1.0 0.081 1 8260B 2/6/14 19:52 VHL P4130098 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.10 1 8260B 2/6/14 19:52 VHL P4130098 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.048 1 8260B 2/6/14 19:52 VHL P4130098 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.59 1 8260B 2/6/14 19:52 VHL P4130098 1,2-Dibromoethane BRL ug/L 0.50 0.14 1 8260B 2/6/14 19:52 VHL P4130098 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 2/6/14 19:52 VHL P4130098 1,2-Dichloroethane BRL ug/L 0.50 0.14 1 8260B 2/6/14 19:52 VHL P4130098 1,2-Dichloropropane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:52 VHL P4130098 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.057 1 8260B 2/6/14 19:52 VHL P4130098 1,3-Dichlorobenzene BRL ug/L 0.50 0.074 1 8260B 2/6/14 19:52 VHL P4130098 1,3-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 2/6/14 19:52 VHL P4130098 1,4-Dichlorobenzene BRL ug/L 0.50 0.068 1 8260B 2/6/14 19:52 VHL P4130098 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 2/6/14 19:52 VHL P4130098 2-Chloroethyl Vinyl Ether BRL ug/L 2.0 0.22 1 8260B 2/6/14 19:52 VHL P4130098 2-Chlorotoluene BRL ug/L 0.50 0.038 1 8260B 2/6/14 19:52 VHL P4130098 4-Chlorotoluene BRL ug/L 0.50 0.053 1 8260B 2/6/14 19:52 VHL P4130098 4-Isopropyltoluene BRL ug/L 0.50 0.065 1 8260B 2/6/14 19:52 VHL P4130098 Acetone BRL ug/L 5.0 0.62 1 8260B 2/6/14 19:52 VHL P4130098 Acrolein BRL ug/L 20 1.1 1 8260B 2/6/14 19:52 VHL P4130098 Acrylonitrile BRL ug/L 20 0.86 1 8260B 2/6/14 19:52 VHL P4130098 Benzene BRL ug/L 0.50 0.072 1 8260B 2/6/14 19:52 VHL P4130098 Bromobenzene BRL ug/L 0.50 0.064 1 8260B 2/6/14 19:52 VHL P4130098 Bromochloromethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:52 VHL P4130098 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 2/6/14 19:52 VHL P4130098 Bromoform BRL ug/L 1.0 0.27 1 8260B 2/6/14 19:52 VHL P4130098 Bromomethane BRL ug/L 1.0 0.47 1 8260B 2/6/14 19:52 VHL P4130098 Carbon disulfide BRL ug/L 5.0 1.4 1 8260B 2/6/14 19:52 VHL P4130098 Carbon Tetrachloride BRL ug/L 0.50 0.12 1 8260B 2/6/14 19:52 VHL P4130098 Chlorobenzene BRL ug/L 0.50 0.061 1 8260B 2/6/14 19:52 VHL P4130098 Chloroethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:52 VHL P4130098 Chloroform BRL ug/L 0.50 0.089 1 8260B 2/6/14 19:52 VHL P4130098 Chloromethane BRL ug/L 0.50 0.11 1 8260B 2/6/14 19:52 VHL P4130098 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.076 1 8260B 2/6/14 19:52 VHL P4130098 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.10 1 8260B 2/6/14 19:52 VHL P4130098 Dibromochloromethane BRL ug/L 0.50 0.30 1 8260B 2/6/14 19:52 VHL P4130098 Dibromomethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 19:52 VHL P4130098 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 8260B 2/6/14 19:52 VHL P4130098 Ethylbenzene BRL ug/L 0.50 0.067 1 8260B 2/6/14 19:52 VHL P4130098 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: BC-2 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-03 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:30 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Hexachlorobutadiene BRL ug/L 2.0 0.36 1 8260B 2/6/14 19:52 VHL P4130098 Isopropyl Ether BRL ug/L 0.50 0.043 1 8260B 2/6/14 19:52 VHL P4130098 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.072 1 8260B 2/6/14 19:52 VHL P4130098 m,p-Xylenes BRL ug/L 1.0 0.081 1 8260B 2/6/14 19:52 VHL P4130098 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.19 1 8260B 2/6/14 19:52 VHL P4130098 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.90 1 8260B 2/6/14 19:52 VHL P4130098 Methyl Isobutyl Ketone BRL ug/L 5.0 0.12 1 8260B 2/6/14 19:52 VHL P4130098 Methylene Chloride BRL ug/L 1.0 0.44 1 8260B 2/6/14 19:52 VHL P4130098 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.070 1 8260B 2/6/14 19:52 VHL P4130098 Naphthalene BRL ug/L 1.0 0.098 1 8260B 2/6/14 19:52 VHL P4130098 n-Butylbenzene BRL ug/L 1.0 0.11 1 8260B 2/6/14 19:52 VHL P4130098 n-Propylbenzene BRL ug/L 0.50 0.060 1 8260B 2/6/14 19:52 VHL P4130098 o-Xylene BRL ug/L 0.50 0.046 1 8260B 2/6/14 19:52 VHL P4130098 sec-Butylbenzene BRL ug/L 0.50 0.087 1 8260B 2/6/14 19:52 VHL P4130098 Styrene BRL ug/L 0.50 0.047 1 8260B 2/6/14 19:52 VHL P4130098 tert-Butylbenzene BRL ug/L 0.50 0.080 1 8260B 2/6/14 19:52 VHL P4130098 Tetrachloroethylene BRL ug/L 0.50 0.069 1 8260B 2/6/14 19:52 VHL P4130098 Toluene BRL ug/L 0.50 0.042 1 8260B 2/6/14 19:52 VHL P4130098 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.12 1 8260B 2/6/14 19:52 VHL P4130098 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.043 1 8260B 2/6/14 19:52 VHL P4130098 Trichloroethylene BRL ug/L 0.50 0.054 1 8260B 2/6/14 19:52 VHL P4130098 Trichlorofluoromethane BRL ug/L 0.50 0.088 1 8260B 2/6/14 19:52 VHL P4130098 Vinyl acetate BRL ug/L 2.0 0.10 1 8260B 2/6/14 19:52 VHL P4130098 Vinyl chloride BRL ug/L 0.50 0.16 1 8260B 2/6/14 19:52 VHL P4130098 Xylenes, total BRL ug/L 3.0 0.13 1 8260B 2/6/14 19:52 VHL P4130098 Surrogate Recovery Control Limits 4-Bromofluorobenzene 112 % 80-124 Dibromofluoromethane 113 % 75-129 Toluene-d8 108 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Sample Matrix: Water Client Sample ID: BC-1 Prism Sample ID: 4020095-04 Prism Work Order: 4020095 Time Collected: 02/05/14 15:45 Time Submitted: 02/06/14 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters Hexavalent Chromium BRL mg/L 0.010 0.0026 1 *SM3500-Cr B 2/6/14 11:45 CDE P4130080 Organochlorine Pesticides by GC/ECD 4,4'-DDD BRL ug/L 0.050 0.0036 1 8081B 2/19/14 22:57 JMV P4130132 4,4'-DDE BRL ug/L 0.050 0.0038 1 8081B 2/19/14 22:57 JMV P4130132 4,4'-DDT BRL ug/L 0.050 0.021 1 8081B 2/19/14 22:57 JMV P4130132 Aldrin BRL ug/L 0.050 0.010 1 8081B 2/19/14 22:57 JMV P4130132 alpha-BHC BRLCCV ug/L 0.050 0.0044 1 8081B 2/19/14 22:57 JMV P4130132 cis -Chlordane BRLCCV ug/L 0.050 0.0070 1 8081B 2/19/14 22:57 JMV P4130132 beta-BHC BRL ug/L 0.050 0.0066 1 8081B 2/19/14 22:57 JMV P4130132 Chlordane BRL ug/L 0.50 0.14 1 8081B 2/19/14 22:57 JMV P4130132 delta-BHC BRL ug/L 0.050 0.0033 1 8081B 2/19/14 22:57 JMV P4130132 Dieldrin BRL ug/L 0.050 0.0046 1 8081B 2/19/14 22:57 JMV P4130132 EndosulfanI BRLCCV ug/L 0.050 0.0084 1 8081B 2/19/14 22:57 JMV P4130132 Endosulfan II BRL ug/L 0.050 0.0047 1 8081B 2/19/14 22:57 JMV P4130132 Endosulfan Sulfate BRLCCV ug/L 0.050 0.0047 1 8081B 2/19/14 22:57 JMV P4130132 Endrin BRL ug/L 0.050 0.0046 1 8081B 2/19/14 22:57 JMV P4130132 Endrin Aldehyde BRL ug/L 0.050 0.0053 1 8081B 2/19/14 22:57 JMV P4130132 Endrin Ketone BRLCCV ug/L 0.050 0.0043 1 8081B 2/19/14 22:57 JMV P4130132 gamma-BHC BRLCCV ug/L 0.050 0.0049 1 8081B 2/19/14 22:57 JMV P4130132 trans -Chlordane BRL ug/L 0.050 0.0060 1 8081B 2/19/14 22:57 JMV P4130132 Heptachlor BRL ug/L 0.050 0.0077 1 8081B 2/19/14 22:57 JMV P4130132 Heptachlor Epoxide BRL ug/L 0.050 0.0046 1 8081B 2/19/14 22:57 JMV P4130132 Methoxychlor BRL ug/L 0.050 0.0087 1 8081B 2/19/14 22:57 JMV P4130132 Toxaohene BRL ua/L 050 0.15 1 9081R 9119114 99-57 IMV P4130132 Polychlorinated Biphenyls (PCBs) by GC/ECD Surrogate Recovery Control Limits Decachlorobiphenyl 110 % 13-186 Tetrachloro-m-xylene 95 % 40-134 Aroclor 1016 BRL ug/L 0.50 0.16 1 8082A 2/12/14 11:50 JMV P4130133 Aroclor 1221 BRL ug/L 1.0 0.11 1 8082A 2/12/14 11:50 JMV P4130133 Aroclor 1232 BRL ug/L 0.50 0.16 1 8082A 2/12/14 11:50 JMV P4130133 Aroclor 1242 BRL ug/L 0.50 0.14 1 8082A 2/12/14 11:50 JMV P4130133 Aroclor 1248 BRL ug/L 0.50 0.14 1 8082A 2/12/14 11:50 JMV P4130133 Aroclor 1254 BRL ug/L 0.50 0.16 1 8082A 2/12/14 11:50 JMV P4130133 Aroclor 1260 BRL ug/L 0.50 0.14 1 8082A 2/12/14 11:50 JMV P4130133 Surrogate Recovery Control Limits Tetrachloro-m-xylene 84 % 30-161 Decachlorobiphenyl 50 % 32-178 Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 10 2.2 1 8270D 2/14/14 19:09 KC P4130157 1,2-Dichlorobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 19:09 KC P4130157 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: BC-1 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-04 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:45 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID 1,3-Dichlorobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 19:09 KC P4130157 1,4-Dichlorobenzene BRL ug/L 10 2.0 1 8270D 2/14/14 19:09 KC P4130157 1-Methyl naphthalene BRL ug/L 10 2.5 1 8270D 2/14/14 19:09 KC P4130157 2,4,5-Trichlorophenol BRL ug/L 10 2.5 1 8270D 2/14/14 19:09 KC P4130157 2,4,6-Trichlorophenol BRL ug/L 10 2.3 1 8270D 2/14/14 19:09 KC P4130157 2,4-Dichlorophenol BRL ug/L 10 2.4 1 8270D 2/14/14 19:09 KC P4130157 2,4-Dimethyl phenol BRL ug/L 10 2.4 1 8270D 2/14/14 19:09 KC P4130157 2,4-Dinitrophenol BRL ug/L 10 2.4 1 8270D 2/14/14 19:09 KC P4130157 2,4-Dinitrotoluene BRL ug/L 10 0.95 1 8270D 2/14/14 19:09 KC P4130157 2,6-Dinitrotoluene BRL ug/L 10 1.6 1 8270D 2/14/14 19:09 KC P4130157 2-Chloronaphthalene BRL ug/L 10 2.3 1 8270D 2/14/14 19:09 KC P4130157 2-Chlorophenol BRL ug/L 10 2.1 1 8270D 2/14/14 19:09 KC P4130157 2-Methyl naphthalene BRL ug/L 10 2.6 1 8270D 2/14/14 19:09 KC P4130157 2-Methylphenol BRL ug/L 10 2.4 1 8270D 2/14/14 19:09 KC P4130157 2-Nitroaniline BRL ug/L 10 1.9 1 8270D 2/14/14 19:09 KC P4130157 2-Nitrophenol BRL ug/L 10 2.5 1 8270D 2/14/14 19:09 KC P4130157 3,3'-Dichlorobenzidine BRL ug/L 10 0.96 1 8270D 2/14/14 19:09 KC P4130157 3/4-Methyl phenol BRL ug/L 10 2.4 1 8270D 2/14/14 19:09 KC P4130157 3-Nitroaniline BRL ug/L 10 1.3 1 8270D 2/14/14 19:09 KC P4130157 4,6-Dinitro-2-methylphenol BRL ug/L 10 2.7 1 8270D 2/14/14 19:09 KC P4130157 4-Bromophenyl phenyl ether BRL ug/L 10 1.8 1 8270D 2/14/14 19:09 KC P4130157 4-Chloro-3-methylphenol BRL ug/L 10 2.3 1 8270D 2/14/14 19:09 KC P4130157 4-Chloroaniline BRL ug/L 10 2.5 1 8270D 2/14/14 19:09 KC P4130157 4-Chlorophenyl phenyl ether BRL ug/L 10 1.8 1 8270D 2/14/14 19:09 KC P4130157 4-Nitroaniline BRL ug/L 10 0.91 1 8270D 2/14/14 19:09 KC P4130157 4-Nitrophenol BRL ug/L 10 2.6 1 8270D 2/14/14 19:09 KC P4130157 Acenaphthene BRL ug/L 10 2.1 1 8270D 2/14/14 19:09 KC P4130157 Acenaphthylene BRL ug/L 10 2.2 1 8270D 2/14/14 19:09 KC P4130157 Aniline BRL ug/L 10 2.2 1 8270D 2/14/14 19:09 KC P4130157 Anthracene BRL ug/L 10 1.2 1 8270D 2/14/14 19:09 KC P4130157 Azobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 19:09 KC P4130157 Benzo(a)anthracene BRL ug/L 10 0.95 1 8270D 2/14/14 19:09 KC P4130157 Benzo(a)pyrene BRL ug/L 10 1.1 1 8270D 2/14/14 19:09 KC P4130157 Benzo(b)fluoranthene BRL ug/L 10 1.4 1 8270D 2/14/14 19:09 KC P4130157 Benzo(g,h,i)perylene BRL ug/L 10 2.1 1 8270D 2/14/14 19:09 KC P4130157 Benzo(k)fluoranthene BRL ug/L 10 1.1 1 8270D 2/14/14 19:09 KC P4130157 Benzoic Acid BRL ug/L 100 50 1 8270D 2/14/14 19:09 KC P4130157 Benzyl alcohol BRL ug/L 10 2.1 1 8270D 2/14/14 19:09 KC P4130157 bis(2-Chloroethoxy)methane BRL ug/L 10 2.2 1 8270D 2/14/14 19:09 KC P4130157 Bis(2-Chloroethyl)ether BRL ug/L 10 1.9 1 8270D 2/14/14 19:09 KC P4130157 Bis(2-chloroisopropyl)ether BRL ug/L 10 2.3 1 8270D 2/14/14 19:09 KC P4130157 Bis(2-Ethylhexyl)phthalate BRL ug/L 10 1.8 1 8270D 2/14/14 19:09 KC P4130157 Butyl benzyl phthalate BRL ug/L 10 1.5 1 8270D 2/14/14 19:09 KC P4130157 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: BC-1 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-04 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:45 Time Submitted: 02/06/14 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Chrysene BRL ug/L 10 1.2 1 8270D 2/14/14 19:09 KC P4130157 Dibenzo(a,h)anth racene BRL ug/L 10 1.8 1 8270D 2/14/14 19:09 KC P4130157 Dibenzofuran BRL ug/L 10 2.2 1 8270D 2/14/14 19:09 KC P4130157 Diethyl phthalate BRL ug/L 10 1.4 1 8270D 2/14/14 19:09 KC P4130157 Dimethyl phthalate BRL ug/L 10 1.6 1 8270D 2/14/14 19:09 KC P4130157 Di-n-butyl phthalate BRL ug/L 10 1.8 1 8270D 2/14/14 19:09 KC P4130157 Di-n-octyl phthalate BRL ug/L 10 1.9 1 8270D 2/14/14 19:09 KC P4130157 Fluoranthene BRL ug/L 10 0.94 1 8270D 2/14/14 19:09 KC P4130157 Fluorene BRL ug/L 10 1.8 1 8270D 2/14/14 19:09 KC P4130157 Hexachlorobenzene BRL ug/L 10 1.4 1 8270D 2/14/14 19:09 KC P4130157 Hexachlorobutadiene BRL ug/L 10 2.3 1 8270D 2/14/14 19:09 KC P4130157 Hexachlorocyclopentadiene BRL ug/L 10 1.8 1 8270D 2/14/14 19:09 KC P4130157 Hexachloroethane BRL ug/L 10 1.9 1 8270D 2/14/14 19:09 KC P4130157 Indeno(1,2,3-cd)pyrene BRL ug/L 10 1.6 1 8270D 2/14/14 19:09 KC P4130157 Isophorone BRL ug/L 10 2.4 1 8270D 2/14/14 19:09 KC P4130157 Naphthalene BRL ug/L 10 2.3 1 8270D 2/14/14 19:09 KC P4130157 Nitrobenzene BRL ug/L 10 2.0 1 8270D 2/14/14 19:09 KC P4130157 N-Nitroso-di-n-propylamine BRL ug/L 10 2.3 1 8270D 2/14/14 19:09 KC P4130157 N-Nitrosodiphenylamine BRL ug/L 10 1.6 1 8270D 2/14/14 19:09 KC P4130157 Pentachlorophenol BRL ug/L 10 1.6 1 8270D 2/14/14 19:09 KC P4130157 Phenanthrene BRL ug/L 10 1.2 1 8270D 2/14/14 19:09 KC P4130157 Phenol BRL ug/L 10 2.2 1 8270D 2/14/14 19:09 KC P4130157 Pyrene BRL ug/L 10 1.4 1 8270D 2/14/14 19:09 KC P4130157 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 98 % 49-109 2-Fluorobiphenyl 73 % 55-96 2-Fluorophenol 44 % 27-74 Nitrobenzene-d5 82 % 53-99 Phenol-d5 26 % 11-52 Terphenyl-d14 102 % 42-133 Total Metals Mercury BRL mg/L 0.00020 0.000012 1 *7470A 2/18/14 17:04 MEH P4130278 Arsenic BRL mg/L 0.010 0.0016 1 *6010C 2/7/14 17:15 BGM P4130106 Barium 0.024 mg/L 0.010 0.0031 1 *6010C 2/7/14 17:15 BGM P4130106 Cadmium BRL mg/L 0.0010 0.000039 1 *6010C 2/7/14 17:15 BGM P4130106 Chromium BRL mg/L 0.0050 0.00036 1 *6010C 2/7/14 17:15 BGM P4130106 Lead BRL mg/L 0.0050 0.00039 1 *6010C 2/7/14 17:15 BGM P4130106 Selenium BRL mg/L 0.020 0.0037 1 *6010C 2/7/14 17:15 BGM P4130106 Silver BRL mg/L 0.0050 0.00012 1 *6010C 2/7/14 17:15 BGM P4130106 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.15 1 8260B 2/6/14 20:17 VHL P4130098 1,1,1-Trichloroethane BRL ug/L 0.50 0.063 1 8260B 2/6/14 20:17 VHL P4130098 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.071 1 8260B 2/6/14 20:17 VHL P4130098 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: BC-1 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-04 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:45 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,2-Trichloroethane BRL ug/L 0.50 0.17 1 8260B 2/6/14 20:17 VHL P4130098 1,1-Dichloroethane BRL ug/L 0.50 0.096 1 8260B 2/6/14 20:17 VHL P4130098 1,1-Dichloroethylene BRL ug/L 0.50 0.078 1 8260B 2/6/14 20:17 VHL P4130098 1,1-Dichloropropylene BRL ug/L 0.50 0.061 1 8260B 2/6/14 20:17 VHL P4130098 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.20 1 8260B 2/6/14 20:17 VHL P4130098 1,2,3-Trichloropropane BRL ug/L 1.0 0.081 1 8260B 2/6/14 20:17 VHL P4130098 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.10 1 8260B 2/6/14 20:17 VHL P4130098 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.048 1 8260B 2/6/14 20:17 VHL P4130098 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.59 1 8260B 2/6/14 20:17 VHL P4130098 1,2-Dibromoethane BRL ug/L 0.50 0.14 1 8260B 2/6/14 20:17 VHL P4130098 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 2/6/14 20:17 VHL P4130098 1,2-Dichloroethane BRL ug/L 0.50 0.14 1 8260B 2/6/14 20:17 VHL P4130098 1,2-Dichloropropane BRL ug/L 0.50 0.13 1 8260B 2/6/14 20:17 VHL P4130098 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.057 1 8260B 2/6/14 20:17 VHL P4130098 1,3-Dichlorobenzene BRL ug/L 0.50 0.074 1 8260B 2/6/14 20:17 VHL P4130098 1,3-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 2/6/14 20:17 VHL P4130098 1,4-Dichlorobenzene BRL ug/L 0.50 0.068 1 8260B 2/6/14 20:17 VHL P4130098 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 2/6/14 20:17 VHL P4130098 2-Chloroethyl Vinyl Ether BRL ug/L 2.0 0.22 1 8260B 2/6/14 20:17 VHL P4130098 2-Chlorotoluene BRL ug/L 0.50 0.038 1 8260B 2/6/14 20:17 VHL P4130098 4-Chlorotoluene BRL ug/L 0.50 0.053 1 8260B 2/6/14 20:17 VHL P4130098 4-Isopropyltoluene BRL ug/L 0.50 0.065 1 8260B 2/6/14 20:17 VHL P4130098 Acetone BRL ug/L 5.0 0.62 1 8260B 2/6/14 20:17 VHL P4130098 Acrolein BRL ug/L 20 1.1 1 8260B 2/6/14 20:17 VHL P4130098 Acrylonitrile BRL ug/L 20 0.86 1 8260B 2/6/14 20:17 VHL P4130098 Benzene BRL ug/L 0.50 0.072 1 8260B 2/6/14 20:17 VHL P4130098 Bromobenzene BRL ug/L 0.50 0.064 1 8260B 2/6/14 20:17 VHL P4130098 Bromochloromethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 20:17 VHL P4130098 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 2/6/14 20:17 VHL P4130098 Bromoform BRL ug/L 1.0 0.27 1 8260B 2/6/14 20:17 VHL P4130098 Bromomethane BRL ug/L 1.0 0.47 1 8260B 2/6/14 20:17 VHL P4130098 Carbon disulfide BRL ug/L 5.0 1.4 1 8260B 2/6/14 20:17 VHL P4130098 Carbon Tetrachloride BRL ug/L 0.50 0.12 1 8260B 2/6/14 20:17 VHL P4130098 Chlorobenzene BRL ug/L 0.50 0.061 1 8260B 2/6/14 20:17 VHL P4130098 Chloroethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 20:17 VHL P4130098 Chloroform BRL ug/L 0.50 0.089 1 8260B 2/6/14 20:17 VHL P4130098 Chloromethane BRL ug/L 0.50 0.11 1 8260B 2/6/14 20:17 VHL P4130098 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.076 1 8260B 2/6/14 20:17 VHL P4130098 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.10 1 8260B 2/6/14 20:17 VHL P4130098 Dibromochloromethane BRL ug/L 0.50 0.30 1 8260B 2/6/14 20:17 VHL P4130098 Dibromomethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 20:17 VHL P4130098 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 8260B 2/6/14 20:17 VHL P4130098 Ethylbenzene BRL ug/L 0.50 0.067 1 8260B 2/6/14 20:17 VHL P4130098 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: BC-1 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-04 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 15:45 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Hexachlorobutadiene BRL ug/L 2.0 0.36 1 8260B 2/6/14 20:17 VHL P4130098 Isopropyl Ether BRL ug/L 0.50 0.043 1 8260B 2/6/14 20:17 VHL P4130098 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.072 1 8260B 2/6/14 20:17 VHL P4130098 m,p-Xylenes BRL ug/L 1.0 0.081 1 8260B 2/6/14 20:17 VHL P4130098 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.19 1 8260B 2/6/14 20:17 VHL P4130098 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.90 1 8260B 2/6/14 20:17 VHL P4130098 Methyl Isobutyl Ketone BRL ug/L 5.0 0.12 1 8260B 2/6/14 20:17 VHL P4130098 Methylene Chloride BRL ug/L 1.0 0.44 1 8260B 2/6/14 20:17 VHL P4130098 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.070 1 8260B 2/6/14 20:17 VHL P4130098 Naphthalene BRL ug/L 1.0 0.098 1 8260B 2/6/14 20:17 VHL P4130098 n-Butylbenzene BRL ug/L 1.0 0.11 1 8260B 2/6/14 20:17 VHL P4130098 n-Propylbenzene BRL ug/L 0.50 0.060 1 8260B 2/6/14 20:17 VHL P4130098 o-Xylene BRL ug/L 0.50 0.046 1 8260B 2/6/14 20:17 VHL P4130098 sec-Butylbenzene BRL ug/L 0.50 0.087 1 8260B 2/6/14 20:17 VHL P4130098 Styrene BRL ug/L 0.50 0.047 1 8260B 2/6/14 20:17 VHL P4130098 tert-Butylbenzene BRL ug/L 0.50 0.080 1 8260B 2/6/14 20:17 VHL P4130098 Tetrachloroethylene BRL ug/L 0.50 0.069 1 8260B 2/6/14 20:17 VHL P4130098 Toluene BRL ug/L 0.50 0.042 1 8260B 2/6/14 20:17 VHL P4130098 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.12 1 8260B 2/6/14 20:17 VHL P4130098 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.043 1 8260B 2/6/14 20:17 VHL P4130098 Trichloroethylene BRL ug/L 0.50 0.054 1 8260B 2/6/14 20:17 VHL P4130098 Trichlorofluoromethane BRL ug/L 0.50 0.088 1 8260B 2/6/14 20:17 VHL P4130098 Vinyl acetate BRL ug/L 2.0 0.10 1 8260B 2/6/14 20:17 VHL P4130098 Vinyl chloride BRL ug/L 0.50 0.16 1 8260B 2/6/14 20:17 VHL P4130098 Xylenes, total BRL ug/L 3.0 0.13 1 8260B 2/6/14 20:17 VHL P4130098 Surrogate Recovery Control Limits 4-Bromofluorobenzene 110 % 80-124 Dibromofluoromethane 111 % 75-129 Toluene-d8 107 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Sample Matrix: Water Client Sample ID: MW-3-A Prism Sample ID: 4020095-05 Prism Work Order: 4020095 Time Collected: 02/05/14 16:00 Time Submitted: 02/06/14 09:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters Hexavalent Chromium BRL A mg/L 0.010 0.0026 1 *SM3500-Cr B 2/6/14 11:45 CDE P4130080 Organochlorine Pesticides by GC/ECD 4,4'-DDD BRL ug/L 0.050 0.0036 1 8081B 2/19/14 20:06 JMV P4130132 4,4'-DDE BRL ug/L 0.050 0.0038 1 8081B 2/19/14 20:06 JMV P4130132 4,4'-DDT BRL ug/L 0.050 0.021 1 8081B 2/19/14 20:06 JMV P4130132 Aldrin BRL ug/L 0.050 0.010 1 8081B 2/19/14 20:06 JMV P4130132 alpha-BHC BRLCCV ug/L 0.050 0.0044 1 8081B 2/19/14 20:06 JMV P4130132 cis -Chlordane BRLCCV ug/L 0.050 0.0070 1 8081B 2/19/14 20:06 JMV P4130132 beta-BHC BRL ug/L 0.050 0.0066 1 8081B 2/19/14 20:06 JMV P4130132 Chlordane BRL ug/L 0.50 0.14 1 8081B 2/19/14 20:06 JMV P4130132 delta-BHC BRL ug/L 0.050 0.0033 1 8081B 2/19/14 20:06 JMV P4130132 Dieldrin BRL ug/L 0.050 0.0046 1 8081B 2/19/14 20:06 JMV P4130132 EndosulfanI BRLCCV ug/L 0.050 0.0084 1 8081B 2/19/14 20:06 JMV P4130132 Endosulfan II BRL ug/L 0.050 0.0047 1 8081B 2/19/14 20:06 JMV P4130132 Endosulfan Sulfate BRLCCV ug/L 0.050 0.0047 1 8081B 2/19/14 20:06 JMV P4130132 Endrin BRL ug/L 0.050 0.0046 1 8081B 2/19/14 20:06 JMV P4130132 Endrin Aldehyde BRL ug/L 0.050 0.0053 1 8081B 2/19/14 20:06 JMV P4130132 Endrin Ketone BRLCCV ug/L 0.050 0.0043 1 8081B 2/19/14 20:06 JMV P4130132 gamma-BHC BRLCCV ug/L 0.050 0.0049 1 8081B 2/19/14 20:06 JMV P4130132 trans -Chlordane BRL ug/L 0.050 0.0060 1 8081B 2/19/14 20:06 JMV P4130132 Heptachlor BRL ug/L 0.050 0.0077 1 8081B 2/19/14 20:06 JMV P4130132 Heptachlor Epoxide BRL ug/L 0.050 0.0046 1 8081B 2/19/14 20:06 JMV P4130132 Methoxychlor BRL ug/L 0.050 0.0087 1 8081B 2/19/14 20:06 JMV P4130132 Toxaohene BRL ua/L 050 0.15 1 9081R 9119114 9o-or, imv P4130132 Polychlorinated Biphenyls (PCBs) by GC/ECD Aroclor 1016 BRL ug/L Aroclor 1221 BRL ug/L Aroclor 1232 BRL ug/L Aroclor 1242 BRL ug/L Aroclor 1248 BRL ug/L Aroclor 1254 BRL ug/L Aroclor 1260 BRL ug/L Semivolatile Organic Compounds by GC/MS Surrogate Recovery Control Limits Decachlorobiphenyl 73 % 13-186 Tetrachloro-m-xylene 89 % 40-134 0.50 0.16 1 8082A 2/12/14 4:49 JMV P4130133 1.0 0.11 1 8082A 2/12/14 4:49 JMV P4130133 0.50 0.16 1 8082A 2/12/14 4:49 JMV P4130133 0.50 0.14 1 8082A 2/12/14 4:49 JMV P4130133 0.50 0.14 1 8082A 2/12/14 4:49 JMV P4130133 0.50 0.16 1 8082A 2/12/14 4:49 JMV P4130133 0.50 0.14 1 8082A 2/12/14 4:49 JMV P4130133 Surrogate Recovery Control Limits Tetrachloro-m-xylene 78 % 30-161 Decachlorobiphenyl 42 % 32-178 1,2,4-Trichlorobenzene BRL ug/L 10 2.2 1 8270D 2/14/14 19:30 KC P4130157 1,2-Dichlorobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 19:30 KC P4130157 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-3-A Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-05 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 16:00 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,3-Dichlorobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 19:30 KC P4130157 1,4-Dichlorobenzene BRL ug/L 10 2.0 1 8270D 2/14/14 19:30 KC P4130157 1-Methyl naphthalene BRL ug/L 10 2.5 1 8270D 2/14/14 19:30 KC P4130157 2,4,5-Trichlorophenol BRL ug/L 10 2.5 1 8270D 2/14/14 19:30 KC P4130157 2,4,6-Trichlorophenol BRL ug/L 10 2.3 1 8270D 2/14/14 19:30 KC P4130157 2,4-Dichlorophenol BRL ug/L 10 2.4 1 8270D 2/14/14 19:30 KC P4130157 2,4-Dimethyl phenol BRL ug/L 10 2.4 1 8270D 2/14/14 19:30 KC P4130157 2,4-Dinitrophenol BRL ug/L 10 2.4 1 8270D 2/14/14 19:30 KC P4130157 2,4-Dinitrotoluene BRL ug/L 10 0.95 1 8270D 2/14/14 19:30 KC P4130157 2,6-Dinitrotoluene BRL ug/L 10 1.6 1 8270D 2/14/14 19:30 KC P4130157 2-Chloronaphthalene BRL ug/L 10 2.3 1 8270D 2/14/14 19:30 KC P4130157 2-Chlorophenol BRL ug/L 10 2.1 1 8270D 2/14/14 19:30 KC P4130157 2-Methyl naphthalene BRL ug/L 10 2.6 1 8270D 2/14/14 19:30 KC P4130157 2-Methylphenol BRL ug/L 10 2.4 1 8270D 2/14/14 19:30 KC P4130157 2-Nitroaniline BRL ug/L 10 1.9 1 8270D 2/14/14 19:30 KC P4130157 2-Nitrophenol BRL ug/L 10 2.5 1 8270D 2/14/14 19:30 KC P4130157 3,3'-Dichlorobenzidine BRL ug/L 10 0.96 1 8270D 2/14/14 19:30 KC P4130157 3/4-Methyl phenol BRL ug/L 10 2.4 1 8270D 2/14/14 19:30 KC P4130157 3-Nitroaniline BRL ug/L 10 1.3 1 8270D 2/14/14 19:30 KC P4130157 4,6-Dinitro-2-methylphenol BRL ug/L 10 2.7 1 8270D 2/14/14 19:30 KC P4130157 4-Bromophenyl phenyl ether BRL ug/L 10 1.8 1 8270D 2/14/14 19:30 KC P4130157 4-Chloro-3-methylphenol BRL ug/L 10 2.3 1 8270D 2/14/14 19:30 KC P4130157 4-Chloroaniline BRL ug/L 10 2.5 1 8270D 2/14/14 19:30 KC P4130157 4-Chlorophenyl phenyl ether BRL ug/L 10 1.8 1 8270D 2/14/14 19:30 KC P4130157 4-Nitroaniline BRL ug/L 10 0.91 1 8270D 2/14/14 19:30 KC P4130157 4-Nitrophenol BRL ug/L 10 2.6 1 8270D 2/14/14 19:30 KC P4130157 Acenaphthene BRL ug/L 10 2.1 1 8270D 2/14/14 19:30 KC P4130157 Acenaphthylene BRL ug/L 10 2.2 1 8270D 2/14/14 19:30 KC P4130157 Aniline BRL ug/L 10 2.2 1 8270D 2/14/14 19:30 KC P4130157 Anthracene BRL ug/L 10 1.2 1 8270D 2/14/14 19:30 KC P4130157 Azobenzene BRL ug/L 10 1.8 1 8270D 2/14/14 19:30 KC P4130157 Benzo(a)anthracene BRL ug/L 10 0.95 1 8270D 2/14/14 19:30 KC P4130157 Benzo(a)pyrene BRL ug/L 10 1.1 1 8270D 2/14/14 19:30 KC P4130157 Benzo(b)fluoranthene BRL ug/L 10 1.4 1 8270D 2/14/14 19:30 KC P4130157 Benzo(g,h,i)perylene BRL ug/L 10 2.1 1 8270D 2/14/14 19:30 KC P4130157 Benzo(k)fluoranthene BRL ug/L 10 1.1 1 8270D 2/14/14 19:30 KC P4130157 Benzoic Acid BRL ug/L 100 50 1 8270D 2/14/14 19:30 KC P4130157 Benzyl alcohol BRL ug/L 10 2.1 1 8270D 2/14/14 19:30 KC P4130157 bis(2-Chloroethoxy)methane BRL ug/L 10 2.2 1 8270D 2/14/14 19:30 KC P4130157 Bis(2-Chloroethyl)ether BRL ug/L 10 1.9 1 8270D 2/14/14 19:30 KC P4130157 Bis(2-chloroisopropyl)ether BRL ug/L 10 2.3 1 8270D 2/14/14 19:30 KC P4130157 Bis(2-Ethylhexyl)phthalate BRL ug/L 10 1.8 1 8270D 2/14/14 19:30 KC P4130157 Butyl benzyl phthalate BRL ug/L 10 1.5 1 8270D 2/14/14 19:30 KC P4130157 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-3-A Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-05 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 16:00 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Chrysene BRL ug/L 10 1.2 1 8270D 2/14/14 19:30 KC P4130157 Dibenzo(a,h)anth racene BRL ug/L 10 1.8 1 8270D 2/14/14 19:30 KC P4130157 Dibenzofuran BRL ug/L 10 2.2 1 8270D 2/14/14 19:30 KC P4130157 Diethyl phthalate BRL ug/L 10 1.4 1 8270D 2/14/14 19:30 KC P4130157 Dimethyl phthalate BRL ug/L 10 1.6 1 8270D 2/14/14 19:30 KC P4130157 Di-n-butyl phthalate BRL ug/L 10 1.8 1 8270D 2/14/14 19:30 KC P4130157 Di-n-octyl phthalate BRL ug/L 10 1.9 1 8270D 2/14/14 19:30 KC P4130157 Fluoranthene BRL ug/L 10 0.94 1 8270D 2/14/14 19:30 KC P4130157 Fluorene BRL ug/L 10 1.8 1 8270D 2/14/14 19:30 KC P4130157 Hexachlorobenzene BRL ug/L 10 1.4 1 8270D 2/14/14 19:30 KC P4130157 Hexachlorobutadiene BRL ug/L 10 2.3 1 8270D 2/14/14 19:30 KC P4130157 Hexachlorocyclopentadiene BRL ug/L 10 1.8 1 8270D 2/14/14 19:30 KC P4130157 Hexachloroethane BRL ug/L 10 1.9 1 8270D 2/14/14 19:30 KC P4130157 Indeno(1,2,3-cd)pyrene BRL ug/L 10 1.6 1 8270D 2/14/14 19:30 KC P4130157 Isophorone BRL ug/L 10 2.4 1 8270D 2/14/14 19:30 KC P4130157 Naphthalene BRL ug/L 10 2.3 1 8270D 2/14/14 19:30 KC P4130157 Nitrobenzene BRL ug/L 10 2.0 1 8270D 2/14/14 19:30 KC P4130157 N-Nitroso-di-n-propylamine BRL ug/L 10 2.3 1 8270D 2/14/14 19:30 KC P4130157 N-Nitrosodiphenylamine BRL ug/L 10 1.6 1 8270D 2/14/14 19:30 KC P4130157 Pentachlorophenol BRL ug/L 10 1.6 1 8270D 2/14/14 19:30 KC P4130157 Phenanthrene BRL ug/L 10 1.2 1 8270D 2/14/14 19:30 KC P4130157 Phenol BRL ug/L 10 2.2 1 8270D 2/14/14 19:30 KC P4130157 Pyrene BRL ug/L 10 1.4 1 8270D 2/14/14 19:30 KC P4130157 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 31 % 49-109 SE 2-Fluorobiphenyl 83 % 55-96 2-Fluorophenol 32 % 27-74 Nitrobenzene-d5 91 % 53-99 Phenol-d5 22 % 11-52 Terphenyl-d14 95 % 42-133 Total Metals Mercury BRL mg/L 0.00020 0.000012 1 *7470A 2/18/14 17:08 MEH P4130278 Arsenic BRL mg/L 0.010 0.0016 1 *6010C 2/7/14 17:22 BGM P4130106 Barium 0.25 mg/L 0.010 0.0031 1 *6010C 2/7/14 17:22 BGM P4130106 Cadmium BRL mg/L 0.0010 0.000039 1 *6010C 2/7/14 17:22 BGM P4130106 Chromium 0.024 mg/L 0.0050 0.00036 1 *6010C 2/7/14 17:22 BGM P4130106 Lead BRL mg/L 0.0050 0.00039 1 *6010C 2/7/14 17:22 BGM P4130106 Selenium BRL mg/L 0.020 0.0037 1 *6010C 2/7/14 17:22 BGM P4130106 Silver BRL mg/L 0.0050 0.00012 1 *6010C 2/7/14 17:22 BGM P4130106 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.15 1 8260B 2/6/14 20:43 VHL P4130098 1,1,1-Trichloroethane BRL ug/L 0.50 0.063 1 8260B 2/6/14 20:43 VHL P4130098 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.071 1 8260B 2/6/14 20:43 VHL P4130098 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-3-A Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-05 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 16:00 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,2-Trichloroethane BRL ug/L 0.50 0.17 1 8260B 2/6/14 20:43 VHL P4130098 1,1-Dichloroethane BRL ug/L 0.50 0.096 1 8260B 2/6/14 20:43 VHL P4130098 1,1-Dichloroethylene BRL ug/L 0.50 0.078 1 8260B 2/6/14 20:43 VHL P4130098 1,1-Dichloropropylene BRL ug/L 0.50 0.061 1 8260B 2/6/14 20:43 VHL P4130098 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.20 1 8260B 2/6/14 20:43 VHL P4130098 1,2,3-Trichloropropane BRL ug/L 1.0 0.081 1 8260B 2/6/14 20:43 VHL P4130098 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.10 1 8260B 2/6/14 20:43 VHL P4130098 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.048 1 8260B 2/6/14 20:43 VHL P4130098 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.59 1 8260B 2/6/14 20:43 VHL P4130098 1,2-Dibromoethane BRL ug/L 0.50 0.14 1 8260B 2/6/14 20:43 VHL P4130098 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 2/6/14 20:43 VHL P4130098 1,2-Dichloroethane BRL ug/L 0.50 0.14 1 8260B 2/6/14 20:43 VHL P4130098 1,2-Dichloropropane BRL ug/L 0.50 0.13 1 8260B 2/6/14 20:43 VHL P4130098 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.057 1 8260B 2/6/14 20:43 VHL P4130098 1,3-Dichlorobenzene BRL ug/L 0.50 0.074 1 8260B 2/6/14 20:43 VHL P4130098 1,3-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 2/6/14 20:43 VHL P4130098 1,4-Dichlorobenzene BRL ug/L 0.50 0.068 1 8260B 2/6/14 20:43 VHL P4130098 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 2/6/14 20:43 VHL P4130098 2-Chloroethyl Vinyl Ether BRL ug/L 2.0 0.22 1 8260B 2/6/14 20:43 VHL P4130098 2-Chlorotoluene BRL ug/L 0.50 0.038 1 8260B 2/6/14 20:43 VHL P4130098 4-Chlorotoluene BRL ug/L 0.50 0.053 1 8260B 2/6/14 20:43 VHL P4130098 4-Isopropyltoluene BRL ug/L 0.50 0.065 1 8260B 2/6/14 20:43 VHL P4130098 Acetone BRL ug/L 5.0 0.62 1 8260B 2/6/14 20:43 VHL P4130098 Acrolein BRL ug/L 20 1.1 1 8260B 2/6/14 20:43 VHL P4130098 Acrylonitrile BRL ug/L 20 0.86 1 8260B 2/6/14 20:43 VHL P4130098 Benzene BRL ug/L 0.50 0.072 1 8260B 2/6/14 20:43 VHL P4130098 Bromobenzene BRL ug/L 0.50 0.064 1 8260B 2/6/14 20:43 VHL P4130098 Bromochloromethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 20:43 VHL P4130098 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 2/6/14 20:43 VHL P4130098 Bromoform BRL ug/L 1.0 0.27 1 8260B 2/6/14 20:43 VHL P4130098 Bromomethane BRL ug/L 1.0 0.47 1 8260B 2/6/14 20:43 VHL P4130098 Carbon disulfide BRL ug/L 5.0 1.4 1 8260B 2/6/14 20:43 VHL P4130098 Carbon Tetrachloride BRL ug/L 0.50 0.12 1 8260B 2/6/14 20:43 VHL P4130098 Chlorobenzene BRL ug/L 0.50 0.061 1 8260B 2/6/14 20:43 VHL P4130098 Chloroethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 20:43 VHL P4130098 Chloroform BRL ug/L 0.50 0.089 1 8260B 2/6/14 20:43 VHL P4130098 Chloromethane BRL ug/L 0.50 0.11 1 8260B 2/6/14 20:43 VHL P4130098 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.076 1 8260B 2/6/14 20:43 VHL P4130098 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.10 1 8260B 2/6/14 20:43 VHL P4130098 Dibromochloromethane BRL ug/L 0.50 0.30 1 8260B 2/6/14 20:43 VHL P4130098 Dibromomethane BRL ug/L 0.50 0.13 1 8260B 2/6/14 20:43 VHL P4130098 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 8260B 2/6/14 20:43 VHL P4130098 Ethylbenzene BRL ug/L 0.50 0.067 1 8260B 2/6/14 20:43 VHL P4130098 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 48 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 02/21/2014 LA6pAATOA Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: MW-3-A Attn: Josh Dunbar Blvd. Prism Sample ID: 4020095-05 1210 Trinity Road Prism Work Order: 4020095 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 02/05/14 16:00 Time Submitted: 02/06/14 09:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Hexachlorobutadiene BRL ug/L 2.0 0.36 1 8260B 2/6/14 20:43 VHL P4130098 Isopropyl Ether BRL ug/L 0.50 0.043 1 8260B 2/6/14 20:43 VHL P4130098 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.072 1 8260B 2/6/14 20:43 VHL P4130098 m,p-Xylenes BRL ug/L 1.0 0.081 1 8260B 2/6/14 20:43 VHL P4130098 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.19 1 8260B 2/6/14 20:43 VHL P4130098 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.90 1 8260B 2/6/14 20:43 VHL P4130098 Methyl Isobutyl Ketone BRL ug/L 5.0 0.12 1 8260B 2/6/14 20:43 VHL P4130098 Methylene Chloride BRL ug/L 1.0 0.44 1 8260B 2/6/14 20:43 VHL P4130098 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.070 1 8260B 2/6/14 20:43 VHL P4130098 Naphthalene BRL ug/L 1.0 0.098 1 8260B 2/6/14 20:43 VHL P4130098 n-Butylbenzene BRL ug/L 1.0 0.11 1 8260B 2/6/14 20:43 VHL P4130098 n-Propylbenzene BRL ug/L 0.50 0.060 1 8260B 2/6/14 20:43 VHL P4130098 o-Xylene BRL ug/L 0.50 0.046 1 8260B 2/6/14 20:43 VHL P4130098 sec-Butylbenzene BRL ug/L 0.50 0.087 1 8260B 2/6/14 20:43 VHL P4130098 Styrene BRL ug/L 0.50 0.047 1 8260B 2/6/14 20:43 VHL P4130098 tert-Butylbenzene BRL ug/L 0.50 0.080 1 8260B 2/6/14 20:43 VHL P4130098 Tetrachloroethylene BRL ug/L 0.50 0.069 1 8260B 2/6/14 20:43 VHL P4130098 Toluene BRL ug/L 0.50 0.042 1 8260B 2/6/14 20:43 VHL P4130098 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.12 1 8260B 2/6/14 20:43 VHL P4130098 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.043 1 8260B 2/6/14 20:43 VHL P4130098 Trichloroethylene BRL ug/L 0.50 0.054 1 8260B 2/6/14 20:43 VHL P4130098 Trichlorofluoromethane BRL ug/L 0.50 0.088 1 8260B 2/6/14 20:43 VHL P4130098 Vinyl acetate BRL ug/L 2.0 0.10 1 8260B 2/6/14 20:43 VHL P4130098 Vinyl chloride BRL ug/L 0.50 0.16 1 8260B 2/6/14 20:43 VHL P4130098 Xylenes, total BRL ug/L 3.0 0.13 1 8260B 2/6/14 20:43 VHL P4130098 Surrogate Recovery Control Limits 4-Bromofluorobenzene 110 % 80-124 Dibromofluoromethane 116 % 75-129 Toluene-d8 106 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 48 P R I S M FullAnalytical Environmental tal Solutions LA6-QRIES INC. Level II QC Report 2/21/14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0098 - 5030B Blank (P460098-131-K1) Prepared & Analyzed: 02/06/14 1,1,1,2-Tetrachloroethane BRL 0.50 ug/L 1,1,1-Trichloroethane BRL 0.50 ug/L 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 1,1,2-Trichloroethane BRL 0.50 ug/L 1,1-Dichloroethane BRL 0.50 ug/L 1,1-Dichloroethylene BRL 0.50 ug/L 1,1-Dichloropropylene BRL 0.50 ug/L 1,2,3-Trichlorobenzene BRL 2.0 ug/L 1,2,3-Trichloropropane BRL 1.0 ug/L 1,2,4-Trichlorobenzene BRL 1.0 ug/L 1,2,4-Trimethyl benzene BRL 0.50 ug/L 1,2-Dibromo-3-chloropropane BRL 2.0 ug/L 1,2-Dibromoethane BRL 0.50 ug/L 1,2-Dichlorobenzene BRL 0.50 ug/L 1,2-Dichloroethane BRL 0.50 ug/L 1,2-Dichloropropane BRL 0.50 ug/L 1,3,5-Trimethyl benzene BRL 0.50 ug/L 1,3-Dichlorobenzene BRL 0.50 ug/L 1,3-Dichloropropane BRL 0.50 ug/L 1,4-Dichlorobenzene BRL 0.50 ug/L 2,2-Dichloropropane BRL 2.0 ug/L 2-Chloroethyl Vinyl Ether BRL 2.0 ug/L 2-Chlorotoluene BRL 0.50 ug/L 4-Chlorotoluene BRL 0.50 ug/L 4-Isopropyltoluene BRL 0.50 ug/L Acetone BRL 5.0 ug/L Acrolein BRL 20 ug/L Acrylonitrile BRL 20 ug/L Benzene BRL 0.50 ug/L Bromobenzene BRL 0.50 ug/L Bromochloromethane BRL 0.50 ug/L Bromodichloromethane BRL 0.50 ug/L Bromoform BRL 1.0 ug/L Bromomethane BRL 1.0 ug/L Carbon disulfide BRL 5.0 ug/L Carbon Tetrachloride BRL 0.50 ug/L Chlorobenzene BRL 0.50 ug/L Chloroethane BRL 0.50 ug/L Chloroform BRL 0.50 ug/L Chloromethane BRL 0.50 ug/L cis-1,2-Dichloroethylene BRL 0.50 ug/L cis-1,3-Dichloropropylene BRL 0.50 ug/L Dibromochloromethane BRL 0.50 ug/L Dibromomethane BRL 0.50 ug/L Dichlorodifluoromethane BRL 1.0 ug/L Ethylbenzene BRL 0.50 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 2/21 /14 Prism Work Order: 4020095 Time Submitted: 2/6/2014 9:55:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0098 - 5030B Blank (P4B0098-BLK1) Prepared & Analyzed: 02/06/14 Hexachlorobutadiene BRL 2.0 ug/L Isopropyl Ether BRL 0.50 ug/L Isopropylbenzene (Cumene) BRL 0.50 ug/L m,p-Xylenes BRL 1.0 ug/L Methyl Butyl Ketone (2-Hexanone) BRL 5.0 ug/L Methyl Ethyl Ketone (2-Butanone) BRL 5.0 ug/L Methyl Isobutyl Ketone BRL 5.0 ug/L Methylene Chloride BRL 1.0 ug/L Methyl-tert-Butyl Ether BRL 0.50 ug/L Naphthalene BRL 1.0 ug/L n-Butylbenzene BRL 1.0 ug/L n-Propylbenzene BRL 0.50 ug/L o-Xylene BRL 0.50 ug/L sec-Butylbenzene BRL 0.50 ug/L Styrene BRL 0.50 ug/L tert-Butylbenzene BRL 0.50 ug/L Tetrachloroethylene BRL 0.50 ug/L Toluene BRL 0.50 ug/L trans-1,2-Dichloroethylene BRL 0.50 ug/L trans-1,3-Dichloropropylene BRL 0.50 ug/L Trichloroethylene BRL 0.50 ug/L Trichlorofluoromethane BRL 0.50 ug/L Vinyl acetate BRL 2.0 ug/L Vinyl chloride BRL 0.50 ug/L Xylenes, total BRL 3.0 ug/L Surrogate:4-Bromofluorobenzene 55.0 ug/L 50.00 110 80-124 Surrogate: Dibromofluoromethane 56.1 ug/L 50.00 112 75-129 Surrogate: Toluene-d8 53.8 ug/L 50.00 108 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 30 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/21 /14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0098 - 5030B LCS (P4B0098-BS1) Prepared & Analyzed: 02/06/14 1,1-Dichloroethylene 22.0 0.50 ug/L 20.00 110 70-154 Methyl Butyl Ketone (2-Hexanone) 18.2 5.0 ug/L 20.00 91 64-137 Tetrachloroethylene 22.1 0.50 ug/L 20.00 ill 80-129 Vinyl chloride 25.1 0.50 ug/L 20.00 126 57-141 Xylenes, total 64.5 3.0 ug/L 60.00 108 77-133 Surrogate:4-Bromofluorobenzene 54.6 ug/L 50.00 109 80-124 Surrogate: Dibromofluoromethane 55.7 ug/L 50.00 111 75-129 Surrogate: Toluene-d8 52.4 ug/L 50.00 105 77-123 LCS Dup (P41130098-13SD1) Prepared & Analyzed: 02/06/14 Methyl Butyl Ketone (2-Hexanone) 18.6 5.0 ug/L 20.00 93 64-137 2 20 Methyl Ethyl Ketone (2-Butanone) 19.9 5.0 ug/L 20.00 100 71-134 5 20 Trichloroethylene 21.8 0.50 ug/L 20.00 109 77-133 2 20 Vinyl chloride 23.7 0.50 ug/L 20.00 118 57-141 6 20 Xylenes, total 64.4 3.0 ug/L 60.00 107 77-133 0.3 20 Surrogate:4-Bromofluorobenzene 54.5 ug/L 50.00 109 80-124 Surrogate: Dibromofluoromethane 54.7 ug/L 50.00 109 75-129 Surrogate: Toluene-d8 53.3 ug/L 50.00 107 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 31 of 48 Level II QC Report /P R I S M Environmental Full -Service Analytical & Environmental Solutions 2/21/14 �� ueoAAroAEs �� Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0157 - 351 OC MS Blank (P4B0157-BLK1) Prepared & Analyzed: 02/11/14 1,2,4-Trichlorobenzene BRL 10 ug/L 1,2-Dichlorobenzene BRL 10 ug/L 1,3-Dichlorobenzene BRL 10 ug/L 1,4-Dichlorobenzene BRL 10 ug/L 1-Methyl naphthalene BRL 10 ug/L 2,4,5-Trichlorophenol BRL 10 ug/L 2,4,6-Trichlorophenol BRL 10 ug/L 2,4-Dichlorophenol BRL 10 ug/L 2,4-Dimethylphenol BRL 10 ug/L 2,4-Dinitrophenol BRL 10 ug/L 2,4-Dinitrotoluene BRL 10 ug/L 2,6-Dinitrotoluene BRL 10 ug/L 2-Chloronaphthalene BRL 10 ug/L 2-Chlorophenol BRL 10 ug/L 2-Methyl naphthalene BRL 10 ug/L 2-Methylphenol BRL 10 ug/L 2-Nitroaniline BRL 10 ug/L 2-Nitrophenol BRL 10 ug/L 3,3'-Dichlorobenzidine BRL 10 ug/L 3/4-Methyl phenol BRL 10 ug/L 3-Nitroaniline BRL 10 ug/L 4,6-Dinitro-2-methylphenol BRL 10 ug/L 4-Bromophenyl phenyl ether BRL 10 ug/L 4-Chloro-3-methylphenol BRL 10 ug/L 4-Chloroaniline BRL 10 ug/L 4-Chlorophenyl phenyl ether BRL 10 ug/L 4-Nitroaniline BRL 10 ug/L 4-Nitrophenol BRL 10 ug/L Acenaphthene BRL 10 ug/L Acenaphthylene BRL 10 ug/L Aniline BRL 10 ug/L Anthracene BRL 10 ug/L Azobenzene BRL 10 ug/L Benzo(a)anthracene BRL 10 ug/L Benzo(a)pyrene BRL 10 ug/L Benzo(b)fluoranthene BRL 10 ug/L Benzo(g,h,i)perylene BRL 10 ug/L Benzo(k)fluoranthene BRL 10 ug/L Benzoic Acid BRL 100 ug/L Benzyl alcohol BRL 10 ug/L bis(2-Chloroethoxy)methane BRL 10 ug/L Bis(2-Chloroethyl)ether BRL 10 ug/L Bis(2-chloroisopropyl)ether BRL 10 ug/L Bis(2-Ethylhexyl)phthalate BRL 10 ug/L Butyl benzyl phthalate BRL 10 ug/L Chrysene BRL 10 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 32 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/21 /14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0157 - 351 OC MS Blank (P4B0157-BLK1) Prepared & Analyzed: 02/11/14 Dibenzo(a,h)anthracene BRL 10 ug/L Dibenzofuran BRL 10 ug/L Diethyl phthalate BRL 10 ug/L Dimethyl phthalate BRL 10 ug/L Di-n-butyl phthalate BRL 10 ug/L Di-n-octyl phthalate BRL 10 ug/L Fluoranthene BRL 10 ug/L Fluorene BRL 10 ug/L Hexachlorobenzene BRL 10 ug/L Hexachlorobutadiene BRL 10 ug/L Hexachlorocyclopentadiene BRL 10 ug/L Hexachloroethane BRL 10 ug/L Indeno(1,2,3-cd)pyrene BRL 10 ug/L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug/L Nitrobenzene BRL 10 ug/L N-Nitroso-di-n-propylamine BRL 10 ug/L N-Nitrosodiphenylamine BRL 10 ug/L Pentachlorophenol BRL 10 ug/L Phenanthrene BRL 10 ug/L Phenol BRL 10 ug/L Pyrene BRL 10 ug/L Surrogate: 2,4,6-Tribromophenol 81.5 ug/L 100.0 82 49-109 Surrogate:2-Fluorobiphenyl 38.0 ug/L 50.00 76 55-96 Surrogate:2-Fluorophenol 45.5 ug/L 100.0 46 27-74 Surrogate: Nitrobenzene-d5 44.7 ug/L 50.00 89 53-99 Surrogate: Phenol-d5 25.6 ug/L 100.0 26 11-52 Surrogate: Terphenyl-d14 40.8 ug/L 50.00 82 42-133 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� ueoAAroAiEs iN� Level II QC Report 2/21 /14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0157 - 351 OC MS LCS (P4B0157-BS1) Prepared & Analyzed: 02/11/14 1,2,4-Trichlorobenzene 32.5 10 ug/L 50.00 65 45-103 1,2-Dichlorobenzene 30.5 10 ug/L 50.00 61 43-100 1,3-Dichlorobenzene 29.6 10 ug/L 50.00 59 42-98 1,4-Dichlorobenzene 29.1 10 ug/L 50.00 58 42-100 1-Methyl naphthalene 38.2 10 ug/L 50.00 76 45-135 2,4,5-Trichlorophenol 37.0 10 ug/L 50.00 74 66-120 2,4,6-Trichlorophenol 36.6 10 ug/L 50.00 73 62-121 2,4-Dichlorophenol 34.7 10 ug/L 50.00 69 58-113 2,4-Dimethylphenol 34.6 10 ug/L 50.00 69 42-120 2,4-Dinitrophenol 24.6 10 ug/L 50.00 49 27-129 2,4-Dinitrotoluene 35.6 10 ug/L 50.00 71 62-136 2,6-Dinitrotoluene 35.4 10 ug/L 50.00 71 64-129 2-Chloronaphthalene 41.7 10 ug/L 50.00 83 38-141 2-Chlorophenol 30.7 10 ug/L 50.00 61 49-107 2-Methyl naphthalene 38.2 10 ug/L 50.00 76 55-112 2-Methylphenol 27.5 10 ug/L 50.00 55 40-106 2-Nitroaniline 41.6 10 ug/L 50.00 83 65-122 2-Nitrophenol 35.4 10 ug/L 50.00 71 57-115 3,3'-Dichlorobenzidine 40.8 10 ug/L 50.00 82 58-139 3/4-Methyl phenol 25.9 10 ug/L 50.00 52 34-101 3-Nitroaniline 42.1 10 ug/L 50.00 84 52-155 4,6-Dinitro-2-methylphenol 37.9 10 ug/L 50.00 76 49-138 4-Bromophenyl phenyl ether 41.2 10 ug/L 50.00 82 63-135 4-Chloro-3-methylphenol 38.3 10 ug/L 50.00 77 33-149 4-Chloroaniline 39.5 10 ug/L 50.00 79 44-163 4-Chlorophenyl phenyl ether 39.5 10 ug/L 50.00 79 63-129 4-Nitroaniline 39.4 10 ug/L 50.00 79 63-147 4-Nitrophenol 12.5 10 ug/L 50.00 25 10-77 Acenaphthene 37.3 10 ug/L 50.00 75 64-118 Acenaphthylene 38.2 10 ug/L 50.00 76 65-119 Aniline 34.0 10 ug/L 50.00 68 12-197 Anthracene 44.0 10 ug/L 50.00 88 69-134 Azobenzene 43.2 10 ug/L 50.00 86 56-129 Benzo(a)anthracene 42.2 10 ug/L 50.00 84 71-125 Benzo(a)pyrene 36.8 10 ug/L 50.00 74 67-135 Benzo(b)fluoranthene 35.3 10 ug/L 50.00 71 56-145 Benzo(g,h,i)perylene 35.5 10 ug/L 50.00 71 44-149 Benzo(k)fluoranthene 35.6 10 ug/L 50.00 71 65-138 Benzoic Acid BRL 100 ug/L 50.00 10-125 P Benzyl alcohol 30.6 10 ug/L 50.00 61 35-111 bis(2-Chloroethoxy)methane 39.6 10 ug/L 50.00 79 49-126 Bis(2-Chloroethyl)ether 35.9 10 ug/L 50.00 72 47-124 Bis(2-chloroisopropyl)ether 37.2 10 ug/L 50.00 74 42-126 Bis(2-Ethylhexyl)phthalate 43.5 10 ug/L 50.00 87 59-139 Butyl benzyl phthalate 43.0 10 ug/L 50.00 86 67-133 Chrysene 42.2 10 ug/L 50.00 84 64-124 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 34 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/21 /14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0157 - 351 OC MS LCS (P4B0157-BSI) Prepared & Analyzed: 02/11/14 Dibenzo(a,h)anthracene 36.1 10 ug/L 50.00 72 49-144 Dibenzofuran 37.6 10 ug/L 50.00 75 68-113 Diethyl phthalate 41.2 10 ug/L 50.00 82 70-124 Dimethyl phthalate 40.1 10 ug/L 50.00 80 71-117 Di-n-butyl phthalate 43.1 10 ug/L 50.00 86 69-128 Di-n-octyl phthalate 37.2 10 ug/L 50.00 74 52-150 Fluoranthene 42.8 10 ug/L 50.00 86 66-135 Fluorene 39.9 10 ug/L 50.00 80 67-124 Hexachlorobenzene 38.9 10 ug/L 50.00 78 62-124 Hexachlorobutadiene 30.3 10 ug/L 50.00 61 42-105 Hexachlorocyclopentadiene 41.8 10 ug/L 50.00 84 32-117 Hexachloroethane 29.3 10 ug/L 50.00 59 40-99 Indeno(1,2,3-cd)pyrene 35.3 10 ug/L 50.00 71 40-150 Isophorone 34.3 10 ug/L 50.00 69 54-125 Naphthalene 35.6 10 ug/L 50.00 71 54-111 Nitrobenzene 31.0 10 ug/L 50.00 62 51-117 N-Nitroso-di-n-propylamine 37.8 10 ug/L 50.00 76 55-115 N-Nitrosodiphenylamine 42.4 10 ug/L 50.00 85 70-152 Pentachlorophenol 35.0 10 ug/L 50.00 70 23-139 Phenanthrene 42.8 10 ug/L 50.00 86 68-128 Phenol 11.4 10 ug/L 50.00 23 12-58 Pyrene 43.0 10 ug/L 50.00 86 62-139 Surrogate: 2,4,6-Tribromophenol 87.2 ug/L 100.0 87 49-109 Surrogate:2-Fluorobiphenyl 35.8 ug/L 50.00 72 55-96 Surrogate:2-Fluorophenol 38.6 ug/L 100.0 39 27-74 Surrogate: Nitrobenzene-d5 37.0 ug/L 50.00 74 53-99 Surrogate: Phenol-d5 22.6 ug/L 100.0 23 11-52 Surrogate: Terphenyl-d14 40.5 ug/L 50.00 81 42-133 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 35 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� ueoAAroAiEs iN� Level II QC Report 2/21 /14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0157 - 351 OC MS LCS Dup (P4B0157-BSD1) Prepared & Analyzed: 02/11/14 1,2,4-Trichlorobenzene 35.6 10 ug/L 50.00 71 45-103 9 20 1,2-Dichlorobenzene 34.2 10 ug/L 50.00 68 43-100 11 20 1,3-Dichlorobenzene 33.3 10 ug/L 50.00 67 42-98 12 20 1,4-Dichlorobenzene 33.0 10 ug/L 50.00 66 42-100 12 20 1-Methyl naphthalene 40.6 10 ug/L 50.00 81 45-135 6 20 2,4,5-Trichlorophenol 39.4 10 ug/L 50.00 79 66-120 7 20 2,4,6-Trichlorophenol 39.6 10 ug/L 50.00 79 62-121 8 20 2,4-Dichlorophenol 38.8 10 ug/L 50.00 78 58-113 11 20 2,4-Dimethylphenol 38.4 10 ug/L 50.00 77 42-120 11 20 2,4-Dinitrophenol 30.9 10 ug/L 50.00 62 27-129 23 20 D 2,4-Dinitrotoluene 35.7 10 ug/L 50.00 71 62-136 0.4 20 2,6-Dinitrotoluene 35.2 10 ug/L 50.00 70 64-129 0.5 20 2-Chloronaphthalene 44.7 10 ug/L 50.00 89 38-141 7 20 2-Chlorophenol 34.9 10 ug/L 50.00 70 49-107 13 20 2-Methyl naphthalene 40.7 10 ug/L 50.00 81 55-112 6 20 2-Methylphenol 31.8 10 ug/L 50.00 64 40-106 15 20 2-Nitroaniline 41.6 10 ug/L 50.00 83 65-122 0.07 20 2-Nitrophenol 39.5 10 ug/L 50.00 79 57-115 11 20 3,3'-Dichlorobenzidine 41.3 10 ug/L 50.00 83 58-139 1 20 3/4-Methyl phenol 30.2 10 ug/L 50.00 60 34-101 16 20 3-Nitroaniline 42.1 10 ug/L 50.00 84 52-155 0.1 20 4,6-Dinitro-2-methylphenol 42.8 10 ug/L 50.00 86 49-138 12 20 4-Bromophenyl phenyl ether 42.1 10 ug/L 50.00 84 63-135 2 20 4-Chloro-3-methylphenol 40.2 10 ug/L 50.00 80 33-149 5 20 4-Chloroaniline 43.3 10 ug/L 50.00 87 44-163 9 20 4-Chlorophenyl phenyl ether 40.6 10 ug/L 50.00 81 63-129 3 20 4-Nitroaniline 40.8 10 ug/L 50.00 82 63-147 3 20 4-Nitrophenol 13.7 10 ug/L 50.00 27 10-77 9 20 Acenaphthene 38.8 10 ug/L 50.00 78 64-118 4 20 Acenaphthylene 40.5 10 ug/L 50.00 81 65-119 6 20 Aniline 38.4 10 ug/L 50.00 77 12-197 12 20 Anthracene 44.1 10 ug/L 50.00 88 69-134 0.3 20 Azobenzene 43.0 10 ug/L 50.00 86 56-129 0.4 20 Benzo(a)anthracene 42.6 10 ug/L 50.00 85 71-125 0.9 20 Benzo(a)pyrene 36.7 10 ug/L 50.00 73 67-135 0.4 20 Benzo(b)fluoranthene 35.2 10 ug/L 50.00 70 56-145 0.2 20 Benzo(g,h,i)perylene 35.6 10 ug/L 50.00 71 44-149 0.5 20 Benzo(k)fluoranthene 35.7 10 ug/L 50.00 71 65-138 0.2 20 Benzoic Acid BRL 100 ug/L 50.00 10-125 20 P Benzyl alcohol 34.0 10 ug/L 50.00 68 35-111 11 20 bis(2-Chloroethoxy)methane 42.5 10 ug/L 50.00 85 49-126 7 20 Bis(2-Chloroethyl)ether 41.1 10 ug/L 50.00 82 47-124 13 20 Bis(2-chloroisopropyl)ether 43.1 10 ug/L 50.00 86 42-126 15 20 Bis(2-Ethylhexyl)phthalate 44.2 10 ug/L 50.00 88 59-139 2 20 Butyl benzyl phthalate 43.0 10 ug/L 50.00 86 67-133 0.07 20 Chrysene 42.8 10 ug/L 50.00 86 64-124 1 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 36 of 48 Level II QC Report /P R I S M Environmental Full -Service Analytical & Environmental Solutions 2/21/14 �� uaoanroAies iNa Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0157 - 351 OC MS LCS Dup (P4B0157-BSD1) Prepared & Analyzed: 02/11/14 Dibenzo(a,h)anthracene 36.2 10 ug/L 50.00 72 49-144 0.2 20 Dibenzofuran 38.6 10 ug/L 50.00 77 68-113 3 20 Diethyl phthalate 40.9 10 ug/L 50.00 82 70-124 0.5 20 Dimethyl phthalate 40.2 10 ug/L 50.00 80 71-117 0.4 20 Di-n-butyl phthalate 42.5 10 ug/L 50.00 85 69-128 1 20 Di-n-octyl phthalate 37.1 10 ug/L 50.00 74 52-150 0.3 20 Fluoranthene 42.6 10 ug/L 50.00 85 66-135 0.4 20 Fluorene 40.4 10 ug/L 50.00 81 67-124 1 20 Hexachlorobenzene 39.3 10 ug/L 50.00 79 62-124 0.9 20 Hexachlorobutadiene 34.8 10 ug/L 50.00 70 42-105 14 20 Hexachlorocyclopentadiene 46.3 10 ug/L 50.00 93 32-117 10 20 Hexachloroethane 33.3 10 ug/L 50.00 67 40-99 13 20 Indeno(1,2,3-cd)pyrene 36.2 10 ug/L 50.00 72 40-150 2 20 Isophorone 37.2 10 ug/L 50.00 74 54-125 8 20 Naphthalene 38.7 10 ug/L 50.00 77 54-111 8 20 Nitrobenzene 34.6 10 ug/L 50.00 69 51-117 11 20 N-Nitroso-di-n-propylamine 41.5 10 ug/L 50.00 83 55-115 9 20 N-Nitrosodiphenylamine 42.9 10 ug/L 50.00 86 70-152 1 20 Pentachlorophenol 38.7 10 ug/L 50.00 77 23-139 10 20 Phenanthrene 42.8 10 ug/L 50.00 86 68-128 0.1 20 Phenol 13.5 10 ug/L 50.00 27 12-58 17 20 Pyrene 43.1 10 ug/L 50.00 86 62-139 0.3 20 Surrogate: 2,4,6-Tribromophenol 83.0 ug/L 100.0 83 49-109 Surrogate:2-Fluorobiphenyl 37.4 ug/L 50.00 75 55-96 Surrogate:2-Fluorophenol 44.4 ug/L 100.0 44 27-74 Surrogate: Nitrobenzene-d5 39.3 ug/L 50.00 79 53-99 Surrogate: Phenol-d5 26.1 ug/L 100.0 26 11-52 Surrogate: Terphenyl-d14 39.2 ug/L 50.00 78 42-133 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 37 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� ueoAAroAiEs iN� Level II QC Report 2/21 /14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Organochlorine Pesticides by GC/ECD - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4BO132 - 3510C GC Blank (P4B0132-BLK1) Prepared: 02/10/14 Analyzed: 02/19/14 4,4'-DDD BRL 0.050 ug/L 4,4'-DDE BRL 0.050 ug/L 4,4'-DDT BRL 0.050 ug/L Aldrin BRL 0.050 ug/L alpha-BHC BRL 0.050 ug/L cis -Chlordane BRL 0.050 ug/L beta-BHC BRL 0.050 ug/L Chlordane BRL 0.50 ug/L delta-BHC BRL 0.050 ug/L Dieldrin BRL 0.050 ug/L Endosulfan I BRL 0.050 ug/L Endosulfan II BRL 0.050 ug/L Endosulfan Sulfate BRL 0.050 ug/L Endrin BRL 0.050 ug/L Endrin Aldehyde BRL 0.050 ug/L Endrin Ketone BRL 0.050 ug/L gamma-BHC BRL 0.050 ug/L trans -Chlordane BRL 0.050 ug/L Heptachlor BRL 0.050 ug/L Heptachlor Epoxide BRL 0.050 ug/L Methoxychlor BRL 0.050 ug/L Toxaphene BRL 0.50 ug/L Surrogate: Decachlorobiphenyl 1.15 ug/L 1.000 115 13-186 Surrogate: Tetrachloro-m-xylene 0.940 ug/L 1.000 94 40-134 LCS (P4B0132-BSI) Prepared: 02/10/14 Analyzed: 02/19/14 4,4'-DDD 0.940 0.050 ug/L 1.000 94 66-138 4,4'-DDE 1.02 0.050 ug/L 1.000 102 67-127 4,4'-DDT 1.03 0.050 ug/L 1.000 103 66-142 Aldrin 1.03 0.050 ug/L 1.000 103 62-124 alpha-BHC 1.00 0.050 ug/L 1.000 100 63-125 cis -Chlordane 1.05 0.050 ug/L 1.000 105 68-126 beta-BHC 1.03 0.050 ug/L 1.000 103 65-137 Chlordane BRL 0.50 ug/L 50-150 delta-BHC 1.02 0.050 ug/L 1.000 102 65-132 Dieldrin 1.00 0.050 ug/L 1.000 100 69-130 Endosulfan 1 1.01 0.050 ug/L 1.000 101 71-129 Endosulfan II 0.990 0.050 ug/L 1.000 99 73-135 Endosulfan Sulfate 1.00 0.050 ug/L 1.000 100 72-137 Endrin 0.970 0.050 ug/L 1.000 97 69-144 Endrin Aldehyde 0.870 0.050 ug/L 1.000 87 68-139 Endrin Ketone 0.980 0.050 ug/L 1.000 98 68-150 gamma-BHC 1.05 0.050 ug/L 1.000 105 66-129 trans -Chlordane 1.03 0.050 ug/L 1.000 103 66-126 Heptachlor 0.910 0.050 ug/L 1.000 91 61-136 Heptachlor Epoxide 1.00 0.050 ug/L 1.000 100 69-131 Methoxychlor 1.00 0.050 ug/L 1.000 100 70-157 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 38 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/21 /14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Organochlorine Pesticides by GC/ECD - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4BO132 - 3510C GC LCS (P4B0132-BSI) Prepared: 02/10/14 Analyzed: 02/19/14 Toxaphene BRL 0.50 ug/L 50-150 Surrogate: Decachlorobiphenyl 1.06 ug/L 1.000 106 13-186 Surrogate: Tetrachloro-m-xylene 0.920 ug/L 1.000 92 40-134 LCS (P4B0132-BS2) Prepared: 02/10/14 Analyzed: 02/19/14 4,4'-DDD BRL 0.050 ug/L 66-138 4,4'-DDE BRL 0.050 ug/L 67-127 4,4'-DDT BRL 0.050 ug/L 66-142 Aldrin BRL 0.050 ug/L 62-124 alpha-BHC BRL 0.050 ug/L 63-125 cis -Chlordane BRL 0.050 ug/L 68-126 beta-BHC BRL 0.050 ug/L 65-137 Chlordane 10.3 0.50 ug/L 10.00 103 50-150 delta-BHC BRL 0.050 ug/L 65-132 Dieldrin BRL 0.050 ug/L 69-130 Endosulfan I BRL 0.050 ug/L 71-129 Endosulfan II BRL 0.050 ug/L 73-135 Endosulfan Sulfate BRL 0.050 ug/L 72-137 Endrin BRL 0.050 ug/L 69-144 Endrin Aldehyde BRL 0.050 ug/L 68-139 Endrin Ketone BRL 0.050 ug/L 68-150 gamma-BHC BRL 0.050 ug/L 66-129 trans -Chlordane BRL 0.050 ug/L 66-126 Heptachlor BRL 0.050 ug/L 61-136 Heptachlor Epoxide BRL 0.050 ug/L 69-131 Methoxychlor BRL 0.050 ug/L 70-157 Toxaphene BRL 0.50 ug/L 50-150 Surrogate: Decachlorobiphenyl 1.60 ug/L 1.000 160 13-186 Surrogate: Tetrachloro-m-xylene 0.950 ug/L 1.000 95 40-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 39 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� ueoAAroAiEs iN� Level II QC Report 2/21 /14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Organochlorine Pesticides by GC/ECD - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4BO132 - 3510C GC LCS (P4B0132-BS3) Prepared: 02/10/14 Analyzed: 02/19/14 4,4'-DDD BRL 0.050 ug/L 66-138 4,4'-DDE BRL 0.050 ug/L 67-127 4,4'-DDT BRL 0.050 ug/L 66-142 Aldrin BRL 0.050 ug/L 62-124 alpha-BHC BRL 0.050 ug/L 63-125 cis -Chlordane BRL 0.050 ug/L 68-126 beta-BHC BRL 0.050 ug/L 65-137 Chlordane BRL 0.50 ug/L 50-150 delta-BHC BRL 0.050 ug/L 65-132 Dieldrin BRL 0.050 ug/L 69-130 Endosulfan I BRL 0.050 ug/L 71-129 Endosulfan II BRL 0.050 ug/L 73-135 Endosulfan Sulfate BRL 0.050 ug/L 72-137 Endrin BRL 0.050 ug/L 69-144 Endrin Aldehyde BRL 0.050 ug/L 68-139 Endrin Ketone BRL 0.050 ug/L 68-150 gamma-BHC BRL 0.050 ug/L 66-129 trans -Chlordane BRL 0.050 ug/L 66-126 Heptachlor BRL 0.050 ug/L 61-136 Heptachlor Epoxide BRL 0.050 ug/L 69-131 Methoxychlor BRL 0.050 ug/L 70-157 Toxaphene 10.5 0.50 ug/L 10.00 105 50-150 Surrogate: Decachlorobiphenyl 1.24 ug/L 1.000 124 13-186 Surrogate: Tetrachloro-m-xylene 0.910 ug/L 1.000 91 40-134 LCS Dup (P4BO132-BSD1) Prepared: 02/10/14 Analyzed: 02/19/14 4,4'-DDD 0.850 0.050 ug/L 1.000 85 66-138 10 20 4,4'-DDE 0.930 0.050 ug/L 1.000 93 67-127 9 20 4,4'-DDT 0.930 0.050 ug/L 1.000 93 66-142 10 20 Aldrin 0.960 0.050 ug/L 1.000 96 62-124 7 20 alpha-BHC 0.940 0.050 ug/L 1.000 94 63-125 6 20 cis -Chlordane 0.970 0.050 ug/L 1.000 97 68-126 8 20 beta-BHC 0.980 0.050 ug/L 1.000 98 65-137 5 20 Chlordane BRL 0.50 ug/L 50-150 20 delta-BHC 0.960 0.050 ug/L 1.000 96 65-132 6 20 Dieldrin 0.930 0.050 ug/L 1.000 93 69-130 7 20 Endosulfan 1 0.930 0.050 ug/L 1.000 93 71-129 8 20 Endosulfan II 0.930 0.050 ug/L 1.000 93 73-135 6 20 Endosulfan Sulfate 0.950 0.050 ug/L 1.000 95 72-137 5 20 Endrin 0.900 0.050 ug/L 1.000 90 69-144 7 20 Endrin Aldehyde 0.820 0.050 ug/L 1.000 82 68-139 6 20 Endrin Ketone 0.920 0.050 ug/L 1.000 92 68-150 6 20 gamma-BHC 0.990 0.050 ug/L 1.000 99 66-129 6 20 trans -Chlordane 0.960 0.050 ug/L 1.000 96 66-126 7 20 Heptachlor 0.850 0.050 ug/L 1.000 85 61-136 7 20 Heptachlor Epoxide 0.930 0.050 ug/L 1.000 93 69-131 7 20 Methoxychlor 0.900 0.050 ug/L 1.000 90 70-157 11 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 40 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/21 /14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Organochlorine Pesticides by GC/ECD - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4BO132 - 3510C GC LCS Dup (P4B0132-BSD1) Prepared: 02/10/14 Analyzed: 02/19/14 Toxaphene BRL 0.50 ug/L 50-150 20 Surrogate: Decachlorobiphenyl 0.980 ug/L 1.000 98 13-186 Surrogate: Tetrachloro-m-xylene 0.870 ug/L 1.000 87 40-134 Matrix Spike (P4B0132-MS1) Source: 4020095-04 Prepared: 02/10/14 Analyzed: 02/19/14 4,4'-DDD 2.00 0.10 ug/L 2.000 BRL 100 17-160 4,4'-DDE 2.06 0.10 ug/L 2.000 BRL 103 10-158 4,4'-DDT 2.24 0.10 ug/L 2.000 BRL 112 15-171 Aldrin 2.02 0.10 ug/L 2.000 BRL 101 24-142 alpha-BHC 1.88 0.10 ug/L 2.000 BRL 94 52-130 cis -Chlordane 2.10 0.10 ug/L 2.000 BRL 105 18-147 beta-BHC 2.12 0.10 ug/L 2.000 BRL 106 31-166 Chlordane BRL 1.0 ug/L BRL 50-150 delta-BHC 2.14 0.10 ug/L 2.000 BRL 107 20-171 Dieldrin 2.08 0.10 ug/L 2.000 BRL 104 27-148 Endosulfan 1 2.02 0.10 ug/L 2.000 BRL 101 40-141 Endosulfan 11 2.08 0.10 ug/L 2.000 BRL 104 43-146 Endosulfan Sulfate 2.16 0.10 ug/L 2.000 BRL 108 37-153 Endrin 2.06 0.10 ug/L 2.000 BRL 103 35-165 Endrin Aldehyde 1.82 0.10 ug/L 2.000 BRL 91 15-165 Endrin Ketone 2.04 0.10 ug/L 2.000 BRL 102 36-172 gamma-BHC 2.04 0.10 ug/L 2.000 BRL 102 45-150 trans -Chlordane 2.08 0.10 ug/L 2.000 BRL 104 35-136 Heptachlor 1.80 0.10 ug/L 2.000 BRL 90 38-150 Heptachlor Epoxide 1.98 0.10 ug/L 2.000 BRL 99 40-141 Methoxychlor 2.30 0.10 ug/L 2.000 BRL 115 37-187 Toxaphene BRL 1.0 ug/L BRL 50-150 Surrogate: Decachlorobiphenyl 2.46 ug/L 2.000 123 13-186 Surrogate: Tetrachloro-m-xylene 1.76 ug/L 2.000 88 40-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 41 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/21 /14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Organochlorine Pesticides by GC/ECD - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4BO132 - 3510C GC Matrix Spike Dup (P4B0132-MSD1) Source: 4020095-04 Prepared: 02/10/14 Analyzed: 02/19/14 4,4'-DDD 2.12 0.10 ug/L 2.000 BRL 106 17-160 6 29 4,4'-DDE 2.26 0.10 ug/L 2.000 BRL 113 10-158 9 38 4,4'-DDT 2.32 0.10 ug/L 2.000 BRL 116 15-171 4 30 Aldrin 2.18 0.10 ug/L 2.000 BRL 109 24-142 8 35 alpha-BHC 2.10 0.10 ug/L 2.000 BRL 105 52-130 11 31 cis -Chlordane 2.22 0.10 ug/L 2.000 BRL ill 18-147 6 40 beta-BHC 2.22 0.10 ug/L 2.000 BRL ill 31-166 5 29 Chlordane BRL 1.0 ug/L BRL 50-150 50 delta-BHC 2.24 0.10 ug/L 2.000 BRL 112 20-171 5 27 Dieldrin 2.22 0.10 ug/L 2.000 BRL ill 27-148 7 28 Endosulfan 1 2.14 0.10 ug/L 2.000 BRL 107 40-141 6 40 Endosulfan II 2.20 0.10 ug/L 2.000 BRL 110 43-146 6 32 Endosulfan Sulfate 2.28 0.10 ug/L 2.000 BRL 114 37-153 5 36 Endrin 2.18 0.10 ug/L 2.000 BRL 109 35-165 6 27 Endrin Aldehyde 2.00 0.10 ug/L 2.000 BRL 100 15-165 9 33 Endrin Ketone 2.16 0.10 ug/L 2.000 BRL 108 36-172 6 29 gamma-BHC 2.24 0.10 ug/L 2.000 BRL 112 45-150 9 32 trans -Chlordane 2.20 0.10 ug/L 2.000 BRL 110 35-136 6 34 Heptachlor 1.98 0.10 ug/L 2.000 BRL 99 38-150 10 36 Heptachlor Epoxide 2.10 0.10 ug/L 2.000 BRL 105 40-141 6 36 Methoxychlor 2.40 0.10 ug/L 2.000 BRL 120 37-187 4 34 Toxaphene BRL 1.0 ug/L BRL 50-150 50 Surrogate: Decachlorobiphenyl 2.54 ug/L 2.000 127 13-186 Surrogate: Tetrachloro-m-xylene 1.92 ug/L 2.000 96 40-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 42 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Level II QC Report 2/21 /14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Polychlorinated Biphenyls (PCBs) by GC/ECD - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0133 - 3510C GC Blank (P41130133-131-11(1) Prepared & Analyzed: 02/10/14 Aroclor 1016 BRL 0.50 ug/L Aroclor 1221 BRL 1.0 ug/L Aroclor 1232 BRL 0.50 ug/L Aroclor 1242 BRL 0.50 ug/L Aroclor 1248 BRL 0.50 ug/L Aroclor 1254 BRL 0.50 ug/L Aroclor 1260 BRL 0.50 ug/L Surrogate: Tetrachloro-m-xylene 1.01 ug/L 1.000 101 30-161 Surrogate: Decachlorobiphenyl 0.720 ug/L 1.000 72 32-178 LCS (P4B0133-BSI) Prepared & Analyzed: 02/10/14 Aroclor 1016 8.98 0.50 ug/L 10.00 90 50-114 Aroclor 1260 8.58 0.50 ug/L 10.00 86 10-127 Surrogate: Tetrachloro-m-xylene 0.970 ug/L 1.000 97 30-161 Surrogate: Decachlorobiphenyl 0.600 ug/L 1.000 60 32-178 LCS Dup (P4B0133-BSD1) Prepared & Analyzed: 02/10/14 Aroclor 1016 8.48 0.50 ug/L 10.00 85 50-114 6 50 Aroclor 1260 7.89 0.50 ug/L 10.00 79 10-127 8 50 Surrogate: Tetrachloro-m-xylene 0.980 ug/L 1.000 98 30-161 Surrogate: Decachlorobiphenyl 0.560 ug/L 1.000 56 32-178 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 43 of 48 _�, P R 1 S M Full -Service Analytical Environmental Solutions -, uaP�.�0NiE5, �NF Level II QC Report 2/21/14 Falcon Engineering Project: 828 Martin Luther King Jr Blvd. Prism Work Order: 4020095 Attn: Josh Dunbar Time Submitted: 2/6/2014 9:55:OOAM 1210 Trinity Road Raleigh, NC 27607 Total Metals - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P4B0106 - 3010A Blank (P4B0106-BLK1) Prepared & Analyzed: 02/07/14 Arsenic BRL 0.010 mg/L Barium BRL 0.010 mg/L Cadmium BRL 0.0010 mg/L Chromium BRL 0.0050 mg/L Lead BRL 0.0050 mg/L Selenium BRL 0.020 mg/L Silver BRL 0.0050 mg/L LCS (P4B0106-BS1) Prepared & Analyzed: 02/07/14 Arsenic 0.254 0.010 mg/L 0.2500 102 80-120 Barium 0.252 0.010 mg/L 0.2500 101 80-120 Cadmium 0.249 0.0010 mg/L 0.2500 100 80-120 Chromium 0.254 0.0050 mg/L 0.2500 102 80-120 Lead 0.251 0.0050 mg/L 0.2500 100 80-120 Selenium 0.251 0.020 mg/L 0.2500 100 80-120 Silver 0.250 0.0050 mg/L 0.2500 100 80-120 Matrix Spike (P4B0106-MS1) Source: 4020095-02 Prepared & Analyzed: 02/07/14 Arsenic 0.249 0.010 mg/L 0.2500 0.00326 98 75-125 Barium 0.386 0.010 mg/L 0.2500 0.158 91 75-125 Cadmium 0.224 0.0010 mg/L 0.2500 BRL 89 75-125 Chromium 0.234 0.0050 mg/L 0.2500 BRL 93 75-125 Lead 0.230 0.0050 mg/L 0.2500 0.00111 91 75-125 Selenium 0.254 0.020 mg/L 0.2500 0.0168 95 75-125 Silver 0.237 0.0050 mg/L 0.2500 BRL 95 75-125 Matrix Spike Dup (P460106-MSD1) Source: 4020095-02 Prepared & Analyzed: 02/07/14 Arsenic 0.245 0.010 mg/L 0.2500 0.00326 97 75-125 2 20 Barium 0.382 0.010 mg/L 0.2500 0.158 89 75-125 1 20 Cadmium 0.221 0.0010 mg/L 0.2500 BRL 88 75-125 1 20 Chromium 0.231 0.0050 mg/L 0.2500 BRL 93 75-125 1 20 Lead 0.227 0.0050 mg/L 0.2500 0.00111 91 75-125 1 20 Selenium 0.250 0.020 mg/L 0.2500 0.0168 93 75-125 2 20 Silver 0.234 0.0050 mg/L 0.2500 BRL 94 75-125 1 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 44 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Total Metals - Quality Control Analyte Batch P4BO163 - 7470A Project: 828 Martin Luther King Jr Blvd. Level II QC Report 2/21 /14 Prism Work Order: 4020095 Time Submitted: 2/6/2014 9:55:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (P4B0163-BLK1) Prepared & Analyzed: 02/11/14 Mercury BRL 0.00020 mg/L Matrix Spike (P4B0163-MS1) Source: 4020095-03 Prepared & Analyzed: 02/11/14 Mercury 0.00993 0.00020 mg/L 0.009375 BRL 106 80-120 Batch P4BO278 - 7470A Blank (P4B0278-BLK1) Prepared & Analyzed: 02/18/14 Mercury BRL 0.00020 mg/L LCS (P4B0278-BS1) Prepared & Analyzed: 02/18/14 Mercury 0.00990 0.00020 mg/L 0.009375 106 80-120 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 45 of 48 /P R I S M Environmental Full -Service Analytical Environmental Solutions �� uaoanroAies iNa Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 General Chemistry Parameters - Quality Control Analyte Batch P4B0080 - NO PREP Project: 828 Martin Luther King Jr Blvd. Level II QC Report 2/21 /14 Prism Work Order: 4020095 Time Submitted: 2/6/2014 9:55:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (P4B0080-BLK1) Prepared & Analyzed: 02/06/14 Hexavalent Chromium BRL 0.010 mg/L LCS (P4B0080-BS1) Prepared & Analyzed: 02/06/14 Hexavalent Chromium 0.381 0.010 mg/L 0.4000 95 90-110 Matrix Spike (P4130080-MS7) Source: 4020095-02 Prepared & Analyzed: 02/06/14 Hexavalent Chromium 0.374 0.010 mg/L 0.4000 BRL 93 85-115 Matrix Spike Dup (P4130080-1VISD1) Source: 4020095-02 Prepared & Analyzed: 02/06/14 Hexavalent Chromium 0.375 0.010 mg/L 0.4000 BRL 94 85-115 0.3 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 46 of 48 Sample Extraction Data Prep Method: 3510C GC Lab Number Batch Initial Final Date/Time 4020095-01 134130132 1000 mL 10 mL 02/10/14 9:20 4020095-02 P4130132 1000 mL 10 mL 02/10/14 9:20 4020095-03 P4130132 1000 mL 10 mL 02/10/14 9:20 4020095-04 P4130132 1000 mL 10 mL 02/10/14 9:20 4020095-05 P4130132 1000 mL 10 mL 02/10/14 9:20 Prep Method: 3510C GC Lab Number Batch Initial Final Date/Time 4020095-01 P4130133 1000 mL 10 mL 02/10/14 9:20 4020095-02 P4130133 1000 mL 10 mL 02/10/14 9:20 4020095-03 P4130133 1000 mL 10 mL 02/10/14 9:20 4020095-04 P4130133 1000 mL 10 mL 02/10/14 9:20 4020095-05 134130133 1000 mL 10 mL 02/10/14 9:20 Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 4020095-01 P4130157 1000 mL 1 mL 02/11/14 9:00 4020095-02 P4130157 1000 mL 1 mL 02/11/14 13:00 4020095-03 P4130157 1000 mL 1 mL 02/11/14 13:00 4020095-04 134130157 1000 mL 1 mL 02/11/14 13:00 4020095-05 13460157 1000 mL 1 mL 02/11/14 13:00 Prep Method: 3010A Lab Number Batch Initial Final DatelTime 4020095-01 P4130106 50 mL 50 mL 02/07/14 8:50 4020095-01 P4130106 50 mL 50 mL 02/07/14 8:50 4020095-02 134130106 50 mL 50 mL 02/07/14 8:50 4020095-03 13460106 50 mL 50 mL 02/07/14 8:50 4020095-04 134130106 50 mL 50 mL 02/07/14 8:50 4020095-05 134130106 50 mL 50 mL 02/07/14 8:50 Prep Method: 7470A Lab Number Batch Initial Final Date/Time 4020095-01 134130278 20 mL 30 mL 02/18/14 11:10 4020095-02 13460278 20 mL 30 mL 02/18/14 11:10 4020095-03 13460278 20 mL 30 mL 02/18/14 11:10 4020095-04 134130278 20 mL 30 mL 02/18/14 11:10 4020095-05 P4130278 20 mL 30 mL 02/18/14 11:10 Prep Method: 5030E Lab Number Batch Initial Final Date/Time 4020095-01 134130098 10 mL 10 mL 02/06/14 14:00 4020095-02 13460098 10 mL 10 mL 02/06/14 14:00 4020095-03 134130098 10 mL 10 mL 02/06/14 14:00 4020095-04 P4130098 10 mL 10 mL 02/06/14 14:00 4020095-05 P4130098 10 mL 10 mL 02/06/14 14:00 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 47 of 48 cn cn rn M -u L) Z c E x x c U) T . , - 0 -0 M z F, . 5' 0 a M 0 - r C) U) L S. 0 r M 03 -J3 a r M m0 (D z -C� :r a cn ;z z cn Z 0 > 0 CD u K --I — (D z , M U) L m r (D D x > 0 CD U) 1 > M t-, 0 r- — t -n 3 [i L) Z -0 CD 4 r- )_, rh 0 r 3 0 c) 0 0 > 0 -00 E 0 rn C: 0 00 C z 1. 1 . 00 .2 u) L) 0 3 ma r ID E; -2 —C —k x ID m r U) :E 21 -4 ;a ---- L M cn >to cn > 3: 3�0 0 Orr r M Z 0 a a 0 < CCD r- — m o M Mm ;o 03 LJ ii m -1 rn CD z 1 0 a L >m•co V% GN C. 0 a N L, cn 9t 3•rn z -2. 0 Z M —a' U) C, U = CD G) X F x o ;c ID 2p - M C) 0 ol Z! X 0 r z fn -U Cn n U * CD m 3 3 o CD U) F,lt Mcn M w _0 ;o 0 'A 0 co rri "a Mz M. =s I., cn m a L) Cn �,- Z"� 0 , El r, rn > a ;a CL C�D CD O M M = CD o 0 cn z < m 0 CD A T 0 r ICDL Yuri 0 (D cn (D -n Ll M ICDL Ulm w 0 CD >* 0 CD U) z oQV)- ;32 z 30, M -j :r C), cA0 iii >E z D CD o cn r> M 0CD 0 — - 0 m 0 cn cn N 0 =D 0 >Ct 0 COD Lj IQ ID m C-q 0 0 W z 0 (A CD z CO 0 E 2, 00 z (D Li " --1 0 0 :r ID (Mn - ID =1 0 .0 I co 0 Z (n CD CD X (D CL x Cl) m (D 1 0 CD -1 m 0 cn -1 0 M E cD CL 0 G) 9� M > X or M im z M (0, 2 X 0 • CL 0 rn * Gz -Z) L) , 0 > o (n -u;o Mx "<D N !D U) CD< COL p- > m m 79 li L) l< 0 0 z =r (n 0 CD ;� 0 CLC D) 0 U) p CD Z> 0 'arc > r C Li 0 cr z cn o 0 M M 10 M -h ,4. S0 'D U) x x cm,) (D 0 o M Q -1. = M » C:L CL 0 rp Z 0 :3• gp 0 > 0 rr, 0 0 iom cn E: 0 M 3 (D L K, z 0 M X z 0 m 0 cn cn r CA z co 0 0 Z > cn rn p Co r M ;u 0 CD CD (D 0 0 0 % 0 > 0, 0 M M :5 0) 0 (p e M M L ZAP 2L > SIL > B- EL < 3 — (D 0 CL 0 C. CD U) (D N.I'D X 0 > 2. z -U) CL > 0 'sN o L %..M CD (D W 'COD z Cf 0 cn (D "a 0 02 2 0.2. , (D P M rt M 'D< PRISM Full -Service Analytical & Environmental Solutions �ii. LABOAATOAIFS ING Falcon Engineering Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 NC Certification No. 402 SC Certification No. 99012 NC Drinkinq Water Cert No. 37735 VA Certification No. 460211 DoD ELAP: L-A-B Accredited Certificate No. L2307 ISO/IEC 17025: L-A-B Accredited Certificate No. L2307 Project: 828 Martin Luther King Jr Blvd. Lab Submittal Date: 02/07/2014 Prism Work Order: 4020127 Case Narrative 02/24/2014 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a ----I Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference: Reviewed By Angela D. Overcash VP Laboratory Services MI Matrix spike outside of the control limits. Matrix interference suspected. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 18 LRR I S M Full -Service Analytical Environmental Solutions -WATOHIES INC. Sample Receipt Summary 02/24/2014 Prism Work Order: 4020127 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received GP-1 4020127-01 Solid 02/03/14 02/07/14 GP-2 4020127-02 Solid 02/03/14 02/07/14 GP-3 4020127-03 Solid 02/03/14 02/07/14 GP-4 4020127-04 Solid 02/04/14 02/07/14 GP-5 4020127-05 Solid 02/04/14 02/07/14 GP-6 4020127-06 Solid 02/04/14 02/07/14 GP-7 4020127-07 Solid 02/04/14 02/07/14 GP-8 4020127-08 Solid 02/04/14 02/07/14 GP-11 4020127-09 Solid 02/04/14 02/07/14 GP-12 4020127-10 Solid 02/04/14 02/07/14 Samples were received in good condition at 4.6 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 18 P R I S M Full -Service Analytical Environmental Solutions uiaoanroai E� — Laboratory Report 02/24/2014 Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Project: 828 Martin Luther King Jr Blvd. Sample Matrix: Solid Client Sample ID: GP-1 Prism Sample ID: 4020127-01 Prism Work Order: 4020127 Time Collected: 02/03/14 10:00 Time Submitted: 02/07/14 08:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 79.2 % by 0.100 0.100 1 *SM2540 G 2/10/14 16:00 JAB P4130148 Weight Hexavalent Chromium BRL mg/kg dry 0.50 0.19 1 *7196A 2/21/14 10:45 CDE P4130315 Total Metals Mercury 0.083 mg/kg dry 0.024 0.0082 1 *7471B 2/17/14 14:38 MEH P4130244 Arsenic 3.5 mg/kg dry 0.32 0.047 1 *6010C 2/11/14 20:44 BGM P4130126 Barium 86 mg/kg dry 0.64 0.032 1 *6010C 2111/14 20:44 BGM P4B0126 Cadmium BRL mg/kg dry 0.32 0.0031 1 *6010C 2/11/14 20:44 BGM P4130126 Chromium 8.8 mg/kg dry 0.32 0.10 1 *6010C 2/11/14 20:44 BGM P4130126 Lead 26 mg/kg dry 0.32 0.038 1 *6010C 2/11/14 20:44 BGM P4130126 Selenium BRL mg/kg dry 0.64 0.078 1 *6010C 2/11/14 20:44 BGM P4130126 Silver BRL mg/kg dry 0.32 0.0052 1 *6010C 2/11/14 20:44 BGM P4130126 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 18 Laboratory Report P R I S M Full -Service Analytical & L0.6O ORIE$ Environmental Solutions 02/24/2014 Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: GP-2 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020127-02 1210 Trinity Road Prism Work Order: 4020127 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 02/03/14 10:30 Time Submitted: 02/07/14 08:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 48.1 % by 0.100 0.100 1 *SM2540 G 2/10/14 16:00 JAB P4B0148 Weight Hexavalent Chromium BRL mg/kg dry 0.83 0.32 1 *7196A 2/21/14 10:45 CDE P4130315 Total Metals Mercury 0.24 mg/kg dry 0.039 0.013 1 *7471B 2/17/14 14:51 MEH P4130244 Arsenic 41 mg/kg dry 0.51 0.075 1 *6010C 2/11/14 21:06 BGM P4130126 Barium 1100 mg/kg dry 20 1.0 20 *6010C 2/12/14 14:11 BGM P460126 Cadmium BRL mg/kg dry 0.51 0.0049 1 *6010C 2/11/14 21:06 BGM P4130126 Chromium 19 mg/kg dry 0.51 0.17 1 *6010C 2/11/14 21:06 BGM P4130126 Lead 11 mg/kg dry 0.51 0.060 1 *6010C 2/11/14 21:06 BGM P4130126 Selenium 4.0 mg/kg dry 1.0 0.12 1 *6010C 2/11/14 21:06 BGM P460126 Silver BRL mg/kg dry 0.51 0.0082 1 *6010C 2/11/14 21:06 BGM P4130126 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 18 Laboratory Report P R I S M Full -Service Analytical & L0.6O ORIE$ Environmental Solutions 02/24/2014 Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: GP-3 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020127-03 1210 Trinity Road Prism Work Order: 4020127 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 02/03/14 11:00 Time Submitted: 02/07/14 08:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 79.7 % by 0.100 0.100 1 *SM2540 G 2/10/14 16:00 JAB P4B0148 Weight Hexavalent Chromium 0.53 mg/kg dry 0.50 0.19 1 *7196A 2121/14 10:45 CDE P4130315 Total Metals Mercury 0.42 mg/kg dry 0.025 0.0083 1 *7471B 2/17/14 14:56 MEH P4130244 Arsenic 48 mg/kg dry 0.32 0.046 1 *6010C 2/11/14 21:13 BGM 134130126 Barium 1200 mg/kg dry 32 1.6 50 *6010C 2/12/14 14:18 BGM P460126 Cadmium BRL mg/kg dry 0.32 0.0030 1 *6010C 2/11/14 21:13 BGM P4130126 Chromium 23 mg/kg dry 0.32 0.10 1 *6010C 2/11/14 21:13 BGM P4130126 Lead 39 mg/kg dry 0.32 0.037 1 *6010C 2/11/14 21:13 BGM P4130126 Selenium BRL mg/kg dry 0.63 0.076 1 *6010C 2/11/14 21:13 BGM P4130126 Silver BRL mg/kg dry 0.32 0.0051 1 *6010C 2/11/14 21:13 BGM P4130126 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 18 Laboratory Report P R I S M Full -Service Analytical & L0.6O ORIE$ Environmental Solutions 02/24/2014 Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: GP-4 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020127-04 1210 Trinity Road Prism Work Order: 4020127 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 02/04/14 10:30 Time Submitted: 02/07/14 08:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 53.3 % by 0.100 0.100 1 *SM2540 G 2/10/14 16:00 JAB P4B0148 Weight Hexavalent Chromium BRL mg/kg dry 0.75 0.29 1 *7196A 2/21/14 10:45 CDE P4130315 Total Metals Mercury 0.51 mg/kg dry 0.039 0.013 1 *7471B 2/17/14 15:00 MEH P4130244 Arsenic 59 mg/kg dry 0.48 0.070 1 *6010C 2/11/14 21:20 BGM P4130126 Barium 2900 mg/kg dry 95 4.8 100 *6010C 2/12/14 14:25 BGM P460126 Cadmium BRL mg/kg dry 0.48 0.0046 1 *6010C 2/11/14 21:20 BGM P4130126 Chromium 20 mg/kg dry 0.48 0.15 1 *6010C 2/11/14 21:20 BGM P4130126 Lead 11 mg/kg dry 0.48 0.056 1 *6010C 2/11/14 21:20 BGM P4130126 Selenium 5.8 mg/kg dry 0.95 0.12 1 *6010C 2/11/14 21:20 BGM P460126 Silver BRL mg/kg dry 0.48 0.0077 1 *6010C 2/11/14 21:20 BGM P4130126 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 18 Laboratory Report P R I S M Full -Service Analytical & L0.6O ORIE$ Environmental Solutions 02/24/2014 Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: GP-5 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020127-05 1210 Trinity Road Prism Work Order: 4020127 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 02/04/14 11:00 Time Submitted: 02/07/14 08:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 88.5 % by 0.100 0.100 1 *SM2540 G 2/10/14 16:00 JAB P4B0148 Weight Hexavalent Chromium BRL mg/kg dry 0.45 0.17 1 *7196A 2/21/14 10:45 CDE P4130315 Total Metals Mercury 0.33 mg/kg dry 0.024 0.0080 1 *7471B 2/17/14 15:14 MEH P4130244 Arsenic 72 mg/kg dry 0.29 0.042 1 *6010C 2/11/14 21:29 BGM P4130126 Barium 2800 mg/kg dry 57 2.9 100 *6010C 2/12/14 14:30 BGM P460126 Cadmium BRL mg/kg dry 0.29 0.0027 1 *6010C 2/11/14 21:29 BGM P4130126 Chromium 19 mg/kg dry 0.29 0.092 1 *6010C 2/11/14 21:29 BGM P4130126 Lead 9.5 mg/kg dry 0.29 0.033 1 *6010C 2/11/14 21:29 BGM P4130126 Selenium 2.6 mg/kg dry 0.57 0.069 1 *6010C 2/11/14 21:29 BGM P460126 Silver BRL mg/kg dry 0.29 0.0046 1 *6010C 2/11/14 21:29 BGM P4130126 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 18 Laboratory Report P R I S M Full -Service Analytical & L0.6O ORIE$ Environmental Solutions 02/24/2014 Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: GP-6 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020127-06 1210 Trinity Road Prism Work Order: 4020127 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 02/04/14 11:30 Time Submitted: 02/07/14 08:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 78.9 % by 0.100 0.100 1 *SM2540 G 2/10/14 16:00 JAB P4B0148 Weight Hexavalent Chromium BRL mg/kg dry 0.51 0.20 1 *7196A 2/21/14 10:45 CDE P4130315 Total Metals Mercury 11 mg/kg dry 1.4 0.48 60 *7471B 2/20/14 17:47 MEH P4130339 Arsenic 65 mg/kg dry 0.31 0.045 1 *6010C 2/11/14 21:36 BGM P4130126 Barium 850 mg/kg dry 31 1.6 50 *6010C 2/12/14 14:37 BGM P460126 Cadmium BRL mg/kg dry 0.31 0.0030 1 *6010C 2/11/14 21:36 BGM P4130126 Chromium 19 mg/kg dry 0.31 0.10 1 *6010C 2/11/14 21:36 BGM P4130126 Lead 27 mg/kg dry 0.31 0.036 1 *6010C 2/11/14 21:36 BGM P4130126 Selenium 4.1 mg/kg dry 0.62 0.075 1 *6010C 2/11/14 21:36 BGM P460126 Silver BRL mg/kg dry 0.31 0.0050 1 *6010C 2/11/14 21:36 BGM P4130126 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 18 Laboratory Report P R I S M Full -Service Analytical & L0.6O ORIE$ Environmental Solutions 02/24/2014 Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: GP-7 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020127-07 1210 Trinity Road Prism Work Order: 4020127 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 02/04/14 12:00 Time Submitted: 02/07/14 08:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 71.3 % by 0.100 0.100 1 *SM2540 G 2/10/14 16:00 JAB P4B0148 Weight Hexavalent Chromium BRL mg/kg dry 0.56 0.22 1 *7196A 2/21/14 10:45 CDE P4130315 Total Metals Mercury 0.26 mg/kg dry 0.028 0.0093 1 *7471B 2/17/14 15:24 MEH P4130244 Arsenic 55 mg/kg dry 0.36 0.052 1 *6010C 2/11/14 21:43 BGM P4130126 Barium 1700 mg/kg dry 36 1.8 50 *6010C 2/12/14 14:44 BGM P460126 Cadmium BRL mg/kg dry 0.36 0.0034 1 *6010C 2/11/14 21:43 BGM P4130126 Chromium 19 mg/kg dry 0.36 0.12 1 *6010C 2/11/14 21:43 BGM P4130126 Lead 11 mg/kg dry 0.36 0.042 1 *6010C 2/11/14 21:43 BGM P4130126 Selenium 4.3 mg/kg dry 0.72 0.087 1 *6010C 2/11/14 21:43 BGM P460126 Silver BRL mg/kg dry 0.36 0.0058 1 *6010C 2/11/14 21:43 BGM P4130126 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 18 Laboratory Report P R I S M Full -Service Analytical & L0.6O ORIE$ Environmental Solutions 02/24/2014 Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: GP-8 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020127-08 1210 Trinity Road Prism Work Order: 4020127 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 02/04/14 12:30 Time Submitted: 02/07/14 08:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 51.8 % by 0.100 0.100 1 *SM2540 G 2/10/14 16:00 JAB P4B0148 Weight Hexavalent Chromium BRL mg/kg dry 0.76 0.29 1 *7196A 2/21/14 10:45 CDE P4130315 Total Metals Mercury 0.29 mg/kg dry 0.038 0.013 1 *7471B 2/17/14 15:29 MEH P4130244 Arsenic 54 mg/kg dry 0.48 0.070 1 *6010C 2/11/14 21:51 BGM P4130126 Barium 4100 mg/kg dry 95 4.8 100 *6010C 2/12/14 14:52 BGM P460126 Cadmium BRL mg/kg dry 0.48 0.0045 1 *6010C 2/11/14 21:51 BGM P4130126 Chromium 20 mg/kg dry 0.48 0.15 1 *6010C 2/11/14 21:51 BGM P4130126 Lead 9.2 mg/kg dry 0.48 0.056 1 *6010C 2/11/14 21:51 BGM P4130126 Selenium 4.5 mg/kg dry 0.95 0.12 1 *6010C 2/11/14 21:51 BGM P460126 Silver BRL mg/kg dry 0.48 0.0076 1 *6010C 2/11/14 21:51 BGM P4130126 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 18 Laboratory Report P R I S M Full -Service Analytical & L0.6O ORIE$ Environmental Solutions 02/24/2014 Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: GP-11 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020127-09 1210 Trinity Road Prism Work Order: 4020127 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 02/04/14 13:00 Time Submitted: 02/07/14 08:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 79.8 % by 0.100 0.100 1 *SM2540 G 2/10/14 16:00 JAB P4B0148 Weight Hexavalent Chromium BRL mg/kg dry 0.50 0.19 1 *7196A 2/21/14 10:45 CDE P4130315 Total Metals Mercury 0.35 mg/kg dry 0.024 0.0082 1 *7471B 2/17/14 15:33 MEH P4130244 Arsenic 16 mg/kg dry 0.31 0.046 1 *6010C 2/11/14 21:59 BGM P4130126 Barium 450 mg/kg dry 13 0.63 20 *6010C 2/12/14 14:57 BGM P460126 Cadmium BRL mg/kg dry 0.31 0.0030 1 *6010C 2/11/14 21:59 BGM P4130126 Chromium 16 mg/kg dry 0.31 0.10 1 *6010C 2/11/14 21:59 BGM P4130126 Lead 23 mg/kg dry 0.31 0.037 1 *6010C 2/11/14 21:59 BGM P4130126 Selenium BRL mg/kg dry 0.63 0.076 1 *6010C 2/11/14 21:59 BGM P4130126 Silver BRL mg/kg dry 0.31 0.0050 1 *6010C 2/11/14 21:59 BGM P4130126 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 18 Laboratory Report P R I S M Full -Service Analytical & L0.6O ORIE$ Environmental Solutions 02/24/2014 Falcon Engineering Project: 828 Martin Luther King Jr Client Sample ID: GP-12 Attn: Josh Dunbar Blvd. Prism Sample ID: 4020127-10 1210 Trinity Road Prism Work Order: 4020127 Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 02/04/14 13:30 Time Submitted: 02/07/14 08:35 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 59.9 % by 0.100 0.100 1 *SM2540 G 2/10/14 16:00 JAB P4B0148 Weight Hexavalent Chromium BRL mg/kg dry 0.67 0.26 1 *7196A 2/21/14 10:45 CDE P4130315 Total Metals Mercury 0.28 mg/kg dry 0.033 0.011 1 *7471B 2/17/14 15:38 MEH P4130244 Arsenic 52 mg/kg dry 0.42 0.062 1 *6010C 2/11/14 22:05 BGM 134130126 Barium 2000 mg/kg dry 42 2.1 50 *6010C 2/12/14 15:04 BGM P460126 Cadmium BRL mg/kg dry 0.42 0.0041 1 *6010C 2/11/14 22:05 BGM P4130126 Chromium 19 mg/kg dry 0.42 0.14 1 *6010C 2/11/14 22:05 BGM P4130126 Lead 14 mg/kg dry 0.42 0.050 1 *6010C 2/11/14 22:05 BGM P4130126 Selenium 2.1 mg/kg dry 0.85 0.10 1 *6010C 2/11/14 22:05 BGM P460126 Silver BRL mg/kg dry 0.42 0.0068 1 *6010C 2/11/14 22:05 BGM P4130126 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 18 Full -Service Analytical P R I S M Environmental Solutions -D-QR1- ING Level II QC Report 2/24/14 Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Total Metals - Quality Control Analyte Batch P4B0126 - 3050B Project: 828 Martin Luther King Jr Blvd Prism Work Order: 4020127 Time Submitted: 2/7/2014 8:35:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (P4130126-BLK1) Prepared: 02/10/14 Analyzed: 02/11/14 Arsenic BRL 0.25 mg/kg wet Barium BRL 0.50 mg/kg wet Cadmium BRL 0.25 mg/kg wet Chromium BRL 0.25 mg/kg wet Lead BRL 0.25 mg/kg wet Selenium BRL 0.50 mg/kg wet Silver BRL 0.25 mg/kg wet LCS (P41130126-13S1) Prepared: 02/10/14 Analyzed: 02/11/14 Arsenic 21.5 0.24 mg/kg wet 24.39 88 80-120 Barium 22.6 0.49 mg/kg wet 24.39 93 80-120 Cadmium 21.0 0.24 mg/kg wet 24.39 86 80-120 Chromium 22.9 0.24 mg/kg wet 24.39 94 80-120 Lead 21.3 0.24 mg/kg wet 24.39 87 80-120 Selenium 20.9 0.49 mg/kg wet 24.39 86 80-120 Silver 22.4 0.24 mg/kg wet 24.39 92 80-120 Matrix Spike (P4B0126-MS1) Source: 4020127-01 Prepared: 02/10/14 Analyzed: 02/11/14 Arsenic 26.4 0.32 mg/kg dry 32.38 3.50 71 75-125 MI Barium 99.0 0.65 mg/kg dry 32.38 86.4 39 75-125 MI Cadmium 23.5 0.32 mg/kg dry 32.38 0.0590 72 75-125 MI Chromium 36.7 0.32 mg/kg dry 32.38 8.75 86 75-125 Lead 35.9 0.32 mg/kg dry 32.38 26.3 30 75-125 MI Selenium 23.2 0.65 mg/kg dry 32.38 BRL 72 75-125 MI Silver 28.1 0.32 mg/kg dry 32.38 BRL 87 75-125 Matrix Spike Dup (112460126-MSD1) Source: 4020127-01 Prepared: 02/10/14 Analyzed: 02/11/14 Arsenic 26.8 0.31 mg/kg dry 31.25 3.50 74 75-125 1 20 MI Barium 119 0.63 mg/kg dry 31.25 86.4 105 75-125 19 20 Cadmium 21.1 0.31 mg/kg dry 31.25 0.0590 67 75-125 11 20 MI Chromium 41.5 0.31 mg/kg dry 31.25 8.75 105 75-125 12 20 Lead 38.0 0.31 mg/kg dry 31.25 26.3 37 75-125 6 20 MI Selenium 20.0 0.63 mg/kg dry 31.25 BRL 64 75-125 15 20 MI Silver 25.3 0.31 mg/kg dry 31.25 BRL 81 75-125 10 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 18 P R I S M Environmental Full -Service Analytical Environmental Solutions ueoanroAies iNa Level II QC Report 2/24/14 Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Total Metals - Quality Control Analyte Batch P4BO126 - 3050B Project: 828 Martin Luther King Jr Blvd Prism Work Order: 4020127 Time Submitted: 2/7/2014 8:35:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Post Spike (P4B0126-PS1) Source: 4020127-01 Prepared: 02/10/14 Analyzed: 02/11/14 Arsenic 0.907 mg/L 1.000 0.109 80 80-120 Barium 3.36 mg/L 1.000 2.70 67 80-120 MI Cadmium 0.734 mg/L 1.000 0.00184 73 80-120 MI Chromium 1.06 mg/L 1.000 0.273 79 80-120 MI Lead 1.52 mg/L 1.000 0.820 69 80-120 MI Selenium 0.745 mg/L 1.000-0.0472 79 80-120 MI Silver 0.859 mg/L 1.000-0.00195 86 80-120 Batch P460244 - 7471 B Blank (P4B0244-BLK1) Prepared & Analyzed: 02/17/14 Mercury BRL 0.018 mg/kg wet LCS (P4B0244-BS1) Prepared & Analyzed: 02/17/14 Mercury 0.422 0.019 mg/kg wet 0.3968 106 80-120 Matrix Spike (P4B0244-MS1) Source: 4020127-01 Prepared & Analyzed: 02/17/14 Mercury 0.634 0.024 mg/kg dry 0.5010 0.0833 110 80-120 Matrix Spike Dup (P4B0244-MSD1) Source: 4020127-01 Prepared & Analyzed: 02/17/14 Mercury 0.762 0.028 mg/kg dry 0.5739 0.0833 118 80-120 18 20 Batch P41130339 - 7471 B Blank (P4130339-BLK1) Prepared & Analyzed: 02/20/14 Mercury BRL 0.020 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 18 P R I S M Environmental Full -Service Analytical Environmental Solutions uiaoanroAies, iNa Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 Total Metals - Quality Control Analyte Batch P4B0339 - 7471 B Project: 828 Martin Luther King Jr Blvd Level II QC Report 2/24/14 Prism Work Order: 4020127 Time Submitted: 2/7/2014 8:35:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS (P4B0339-BSI) Prepared & Analyzed: 02/20/14 Mercury 0.458 0.020 mg/kg wet 0.4237 108 80-120 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 18 P R I S M Environmental Full -Service Analytical Environmental Solutions ueoanroAies iNa Falcon Engineering Attn: Josh Dunbar 1210 Trinity Road Raleigh, NC 27607 General Chemistry Parameters - Quality Control Analyte Batch P4BO148 - NO PREP Project: 828 Martin Luther King Jr Blvd Level II QC Report 2/24/14 Prism Work Order: 4020127 Time Submitted: 2/7/2014 8:35:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (P4B0148-BLK1) Prepared & Analyzed: 02/10/14 % Solids 100 0.100 % by Weight Duplicate (P4B0148-DUP5) Source: 4020127-05 Prepared & Analyzed: 02/10/14 % Solids 88.9 0.100 % by Weight 88.5 0.5 20 Batch P4BO315 - NO PREP Blank (P4B0315-BLK1) Prepared: 02/19/14 Analyzed: 02/21/14 Hexavalent Chromium BRL 0.40 mg/kg wet LCS (P4B0315-BS1) Prepared: 02/19/14 Analyzed: 02/21/14 Hexavalent Chromium 15.3 0.40 mg/kg wet 16.00 96 90-110 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 18 Sample Extraction Data Prep Method: 3050E Lab Number Batch Initial Final Date/Time 4020127-01 P4130126 1.97 g 50 mL 02/10/14 9:50 4020127-02 P4130126 2.03 g 50 mL 02/10/14 9:50 4020127-02 P4130126 2.03 g 50 mL 02/10/14 9:50 4020127-03 P4130126 1.99 g 50 mL 02/10/14 9:50 4020127-03 P4130126 1.99 g 50 mL 02/10/14 9:50 4020127-04 P4130126 1.97 g 50 mL 02/10/14 9:50 4020127-04 P460126 1.97 g 50 mL 02/10/14 9:50 4020127-05 P4130126 1.98 g 50 mL 02/10/14 9:50 4020127-05 P4130126 1.98 g 50 mL 02/10/14 9:50 4020127-06 P4130126 2.04 g 50 mL 02/10/14 9:50 4020127-06 P4130126 2.04 g 50 mL 02/10/14 9:50 4020127-07 P4130126 1.96 g 50 mL 02/10/14 9:50 4020127-07 P4130126 1.96 g 50 mL 02/10/14 9:50 4020127-08 P4130126 2.03 g 50 mL 02/10/14 9:50 4020127-08 P4130126 2.03 g 50 mL 02/10/14 9:50 4020127-09 P460126 2 g 50 mL 02/10/14 9:50 4020127-09 P4130126 2 g 50 mL 02/10/14 9:50 4020127-10 P4130126 1.97 g 50 mL 02/10/14 9:50 4020127-10 P4130126 1.97 g 50 mL 02/10/14 9:50 Prep Method: 7471E Lab Number Batch Initial Final Date/Time 4020127-01 P460244 0.62 g 50 mL 02/17/14 9:30 4020127-02 P4130244 0.64 g 50 mL 02/17/14 9:30 4020127-03 P4130244 0.61 g 50 mL 02/17/14 9:30 4020127-04 P4130244 0.58 g 50 mL 02/17/14 9:30 4020127-05 P4130244 0.57 g 50 mL 02/17/14 9:30 4020127-06 P4130339 0.64 g 50 mL 02/20/14 10:40 4020127-07 P4130244 0.61 g 50 mL 02/17/14 9:30 4020127-08 P460244 0.61 g 50 mL 02/17/14 9:30 4020127-09 P4130244 0.62 g 50 mL 02/17/14 9:30 4020127-10 P4130244 0.61 g 50 mL 02/17/14 9:30 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. 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