Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
Home
My WebLink
About
23022_Chapel Hill Police Property_PIIR_20130718
LCON ENGINEERING PHASE I & LIMITED PHASE II ENVIRONMENTAL SITE ASSESSMENT Chapel Hill Police Department Property 828 Martin Luther King Jr. Boulevard Chapel Hill, Orange County, NC Phase I & Limited Phase II Environmental Site Assessment Chapel Hill Police Department Property 828 Martin Luther King Jr. Boulevard Chapel Hill, Orange County, NC Prepared for: Town of Chapel Hill Chapel Hill Town Hall 405 Martin Luther King, Jr. Blvd. Chapel Hill, NC 27514 Submitted by: Falcon Engineering, Inc. 1210 Trinity Road Suite 110 Raleigh, North Carolina 27607 (919) 871-0800 www.falconengineers.com Firm: C-3193 Falcon Project Number I El3026.00 July 18, 2013 TABLE OF CONTENTS Page Figures.................................................................................................................................................................. iii Preface............................................................................................................................................................... iv Section1 1 Introduction...................................................................................................................................1 1.1 Site Location and Description..........................................................................................1 1.2 Project Objective and Scope of Work...........................................................................3 Section2 1 Historic Land Use..........................................................................................................................4 2.1 Land Ownership History.....................................................................................................4 2.2 Maps and Aerial Photographs.........................................................................................4 Section 3 1 Current Land Use and Adjacent Property Information........................................................6 3.1 Current Land Use................................................................................................................6 3.2 Adjacent Property Information........................................................................................6 Section4 1 Regulatory Review.......................................................................................................................8 4.1 National Priorities List(NPL)................................................................................................8 4.2 CERCLIS Sites........................................................................................................................8 4.3 Resource Conservation and Recovery Information System (RCRIS) Treatment, Storage and Disposal (TSD) Facilities List........................................................................9 4.4 Resource Conservation and Recovery Act (RCRA) Generators List........................9 4.5 Emergency Response Notification System (ERNS) List...............................................10 4.6 State Lists of Hazardous Waste Sites..............................................................................10 4.7 State Leaking Underground Storage Tank (LUST) List.................................................1 1 4.8 State Landfill List(SWF/LF)................................................................................................12 4.9 State Registered Underground Storage Tank (UST) List.............................................12 4.10 PCB Activity Database (PADS).......................................................................................12 4.11 Federal Superfund Liens (NPL LIENS).............................................................................12 4.12 Public Water Supply (PWS) Systems..............................................................................13 4.13 Facility Permits...................................................................................................................13 4.14 Leaking Aboveground Storage Tank (LAST) Sites.......................................................13 Section 5 1 Site Reconnaissance and Characterization.........................................................................14 5.1 Hazardous Waste and Hazardous Substances...........................................................14 5.2 Onsite Storage Tanks........................................................................................................14 5.3 Air Emissions........................................................................................................................14 5.4 Water and Wastewater...................................................................................................15 5.5 Polychlorinated Biphenyls (PCBs)..................................................................................15 5.6 Geology and Hydrology.................................................................................................15 5.7 Spills, Leaks, and Stains....................................................................................................15 Section6 1 Phase II ESA.................................................................................................................................21 Section 7 1 Findings and Recommendations........................................................................16 Section8 1 Limitations....................................................................................................................................22 k JF TABLE OF CONTENTS (CONTINUED) Page Appendix A Historic Fire Insurance Maps..............................................................................................A-1 Appendix B Historic Topographic Maps.................................................................................................B-1 Appendix C Historic aerial photographs..............................................................................................C-1 Appendix Photographs........................................................................................................................D-2 Appendix E Regulatory Database Search............................................................................................E-8 Appendix F Well Record and Laboratory Data....................................................................................F-8 Appendix G Resumes of Environmental Professionals....................................................................... G-1 FIGURES Page Figure1 General Site Location....................................................................................................................2 Figure 1 General Site Location..........................................................................................17 k JF PREFACE This Phase I & Limited Phase II Environmental Site Assessment was conducted between March 12 and July 1, 2013, by Mr. Aric V. Geda, PE, with review performed by Mr. Joshua D. Dunbar, PE of Falcon Engineering, Inc. (Falcon). The opinions and observations rendered in this report are based solely on a site reconnaissance, review of historical land use, research and consultation with available State and local environmental databases and officials, a review of available maps and other records, and limited sampling of sediment, surface water, and groundwater. The Phase I portion of the Environmental Site Assessment was performed in accordance with generally accepted engineering practices and principles as outlined in ASTM E 1527-05, any deviations in fulfilling the requirements of ASTM E 1527-05 are duly noted within this report. Although Falcon believes that the information contained herein is reliable, a guarantee cannot be made as to the accuracy or completeness of the information provided to Falcon by others. FALCON ENGINEERING, INC. Report Prepared By: Aric V. Geda, PE Senior Engineer Report Reviewed By: Q� Joshua D. Dunbar, PE Director of Design Services SECTInN i INTRODUCTION Falcon Engineering, Inc. (Falcon) conducted a Phase I Environmental Site Assessment in general accordance with ASTM E 1527-05, Standard Practice for Environmental Site Assessments, on a property with the property identification number (PIN) 9789413949. Figure 1 is a general site location map of the subject property. 1.1 Site Location and Description The evaluated property is approximately a 10.24-acre property located along Martin Luther King Jr. Blvd. in Chapel Hill, North Carolina. The site is located to the east of Martin Luther King Jr. Blvd., with development primarily focused in the northwest corner. The property is located immediately north of Bolin Creek, beginning approximately 200 feet north of the centerline of Hillsborough Street. The property is currently developed with a 2 story structure approximately 35,000 square feet in size, parking lots, and a few cargo containers used for storage. The site is occupied by the Chapel Hill Police Department. The building is located in the northwest corner, with the majority of parking in the center of the site. The eastern and southern portions of the site are wooded. FIGURE 1 I GENERAL SITE LOCATION -72 1.2 Project Objective and Scope of Work The Town of Chapel Hill retained Falcon to conduct this Phase I & Limited Phase II Environmental Site Assessment. The purpose of the Phase I was to inspect the property for visible signs or indications of environmental conditions that present, or have presented an adverse impact on the site. In addition, historical records were obtained and reviewed to identify adverse conditions (past or present) that may have an environmental impact on the subject site or surrounding properties. The purpose of the limited Phase II was to confirm the absence or presence of environmental impact to site sediments and / or groundwater from potential adverse conditions. The project goals of the Phase I were accomplished through the completion of the following tasks: • Review of environmental databases and lists obtained from Federal, State, and local regulatory agencies including historic maps and directories of the site and the surrounding areas. • Visual inspection of the subject site, including photographic conditions and notation of adjacent property use and conditions. • Interviews with those knowledgeable of the site's history (as appropriate or required). The project goals of the Limited Phase II were accomplished through the completion of the following tasks: • Sediment and groundwater sampling to determine the existing conditions within identified areas on the subject property. Sampling included two sediment sample and 3 water samples. • Laboratory analyses of samples for chemicals of concern. 0 Comparison of analytical results to applicable criteria. HISTORIC LAND USE 2.1 Land Ownership History A formal deed search of the subject property was not performed by Falcon. Based upon Orange County Tax Records three owners have possessed deeds on this property as follows: Prior to 1980 S J HRS SPARROW 1980 - Present Town of Chapel Hill The prior owner was not available for interviews concerning historical uses of this property during the course of these Phase I ESA activities. 2.2 Maps and Aerial Photographs Sanborn Fire Insurance Maps were not available for this site. The Certified Sanborn Map Report can be seen in Appendix A. Historic United State Geological Survey (USGS) topographical maps (Appendix B) and historical aerial photographs (Appendix C) and were obtained and reviewed to determine historic developments at and adjacent to the subject property. The observations from these maps and photographs are as follows: 1946 USGS topographic map shows the subject property with no development. A single family residence is constructed across Martin Luther King Jr. Blvd. to the northwest. 1960 Aerial photograph shows excavation activity on the subject property along the west central portion of the site and across Martin Luther King Jr. Blvd. to the northwest. A dump truck can be seen on site, along with another on Martin Luther King Jr. Blvd. Residential development exists west of the site. The property to the south of the site appears to have been cleared for development. 1969 Aerial photograph shows significant dumping on site across the central portion. Significant piles of material can be seen in the photograph. Residential development exists to the east of the site, and the gas station has been constructed to the south. 1975 Aerial photograph shows a cleared and leveled area along the western border of the site. The remaining areas of filling have become overgrown with vegetation. There is development on the property to the northwest of the site. 1978 USGS topographic map shows the residential development to the east, but few of the other changes. 1981 USGS topographic map shows little change from the previous topographic map. 1993 USGS topographic map and aerial photograph both reflect the construction of the police station on the subject site, and additional commercial development to the south. 1998 Aerial photograph shows little change to the subject and surrounding properties. 2002 USGS topographic map and aerial photograph show little change to the subject and surrounding properties. 2004 Aerial photograph shows little change to the property. Cargo containers appear at the east end of the south parking lot. 2006 Aerial photograph shows little change to the property. It appears that a utility shed has been constructed at the east end of the north parking lot, and the area northeast of the building has been cleared for construction. 2008 Aerial photograph shows little change to the property. It appears that the emergency generator exists in the area northeast of the building. 2010 Aerial photograph shows little change to the property. The subject site and surrounding properties generally appear as they exist today. —75 SECTInN 1 CURRENT LAND USE AND ADJACENT PROPERTY INFORMATION Information was collected on potential sources of contamination from adjacent properties such as containers, drums, underground and aboveground storage tanks (USTs and ASTs), and drainage onto the site. To determine land use of the site and the surrounding properties, site reconnaissance of the area was conducted on April 26, 2013, as well as a review of available maps of the site and the surrounding area. Photographs were taken during the site reconnaissance to document environmental conditions, structures, and other key observations on the site. Some of the photographs taken are contained in Appendix D. 3.1 Current Land Use The subject property was generally undeveloped until the current police station was constructed after 1980. However, as discussed in the Historical Usage section, it appears the site was used as a borrow pit in the late 1950's through early 1960's then as fill site from the mid-1960's to mid- 1970's. The site has been the home of the Chapel Hill Police Station since the town acquired it in 1980. During the site reconnaissance, it became apparent that the site had significant amount of fill materials placed at one time. There is a steep slope along the southern portion of the property, where it was apparent that significant fly -ash and debris were placed on the site. A backup diesel generator exists northeast of the structure. The generator has a self-contained storage tank. No leaks or spills were observed in the area during the reconnaissance. 3.2 Adjacent Property Information Visual observations were made of the surrounding properties by vehicle and foot to identify any conditions that may present an adverse environmental impact to the subject property. The search was conducted from public right-of-way and did not include access to buildings or entry onto private properties. The following sections summarize land use on adjacent properties. Descriptions of adjacent properties are given in a clockwise order starting at the northern property boundary. No ASTs or indicators of USTs were observed on the surrounding properties. UF 3.2.1 Northern Property Boundary The subject property is bounded to the north by Bolinwood Drive, beyond which are single family homes. From the visual observations made and the review of available aerial photography and topographic maps, it is unlikely that any current activities carried out on these properties would have caused any environmental impacts to the subject property. 3.2.2 Eastern Property Boundary The subject property is bounded immediately to the east by single family homes to the north and multi -tenant apartments to the south. From the visual observations made and the review of available aerial photography and topographic maps, it is unlikely that any current activities carried out on these properties would have caused any environmental impacts to the subject property. 3.2.3 Southern Property Boundary The subject property is bounded to the south by a single family residence to the southeast, Lloyd's Tire and Alignment to the south central, and a Mobil fuel station to the southwest. Due to the existence of Bolin Creek between the commercial properties and the subject site, it is unlikely that any contaminants from these sites, were they to exist, would impact the subject site. 3.2.4 Western Property Boundary The subject property is bounded immediately to the west by Martin Luther King Jr. Blvd., beyond which is undeveloped, wooded land and a single family residences. Multi -family apartments exist to the northwest. From the visual observations made and the review of available aerial photography and topographic maps, it is unlikely that any current activities carried out on these properties would have caused any environmental impacts to the subject property. SECTION 4 Regulatory Review Falcon contracted with Environmental Data Resources Inc. (EDR) to search the Federal, State, and Tribal environmental databases for properties with the American Society for Testing and Materials (ASTM) specified standard radius of 1 /8 to 1 mile (depending upon the database) of the subject property. The EDR report contains all sites or occurrences identified by the database search. For more information regarding the list of databases and identified sites, please refer to Appendix E, which contains the complete EDR report. The findings of the search are summarized as follows: The subject property was not listed in any environmental databases searched. 4.1 National Priorities List (NPL) A subset of the Comprehensive Environmental Response, Compensation and Liability Information System (CERCLIS) database, the National Priorities List (NPL) is compiled by the U.S. Environmental Protection Agency (EPA) pursuant to Comprehensive Environmental Response, Compensation and Liability Act (CERCLA) and consists of properties with the highest priority for cleanup pursuant to EPA's Hazard Ranking System. • No NPL sites were identified within the 1-mile database search area. For further information, refer to Appendix E. 4.2 CERCLIS Sites The CERCLIS database contains information on potentially hazardous waste sites that have been reported to EPA by States, municipalities, private companies, and private individuals, pursuant to Section 103 of the CERCLA of 1980, as amended. The database contains information on the names, locations, and indicators for National Priority Status and Federal Facility. The EPA does not claim that CERCLIS contains all the potential hazardous waste sites that exist. • No CERCLIS sites were identified within the database search area. For further information, refer to Appendix E. I JF 4.3 Resource Conservation and Recovery Information System (RCRIS) Treatment, Storage and Disposal (TSD) Facilities List The RCRIS database contains information on hazardous waste handlers regulated by EPA under Resource Conservation and Recovery Act (RCRA). The regulated community and RCRA permitting and compliance program personnel supply the data. All hazardous waste handlers are required to notify EPA of their existence by submitting the Federal Notification of Regulated Waste Activity (EPA Form 8700-12) or a State equivalent. The Notification form provides basic identification information, specific hazardous waste activities, and wastes handled. TSD facilities are further required to submit Part A (EPA Form 8700-23) and Part B of their Hazardous Waste Permit Application. The Part A form provides more detailed information concerning wastes handled, plus SIC codes, and process data. Information from the Notification and Part A forms described above, permit issuance data supplied by RCRA permit writers, and nonsensitive compliance and enforcement data collected by compliance program personnel are included. • No RCRIS TSD facilities were found within the database search area. For further information, refer to Appendix E. 4.4 Resource Conservation and Recovery Act (RCRA) Generators List The RCRIS database contains information on hazardous waste generators regulated by EPA under RCRA. The regulated community and RCRA permitting and compliance program personnel supply the data. All hazardous waste handlers are required to notify EPA of their existence by submitting Federal and/or State forms, which provide basic identification information, specific hazardous waste activities, and wastes handled. A subset of this database is the RCRIS Violations/Corrective Actions (CORRACTS) database. This database is comprised of those facilities with past violations and/or corrective actions under RCRA. • No RCRIS - Large Quantity Generators (LQG) were found within the search area. For further information, refer to Appendix E. • Midtown Shops was identified on the Small Quantity Generators (SQG) list within the search area. Due to the existence of Bolin Creek between this site and the subject property, it is unlikely that this site would impact the subject property.For further information, refer to Appendix E. I JF • LLOYD TIRE & ALIGNMENT, a conditionally Exempt Small Quantity Generator (CESQG) was found with the search area. As indicated previously, due to the existence of Bolin Creek between this site and the subject property, it is unlikely that this site would impact the subject property. For further information, refer to Appendix E. • No CORRACTS sites were found within the search area. For further information, refer to Appendix E. 4.5 Emergency Response Notification System (ERNS) List The Emergency Response Notification System (ERNS) is a national computer database used to store information on releases of oil and hazardous substances. The ERNS program is a cooperative data sharing effort among the EPA Headquarters, the Department of Transportation (DOT), the ten (10) EPA Regions, and the National Response Center (NRC). The ERNS data are captured electronically when a release is reported to the NRC or EPA. When a release is submitted to Federal authorities, the individual reporting the release is asked a series of questions concerning the release and the information is immediately transferred to the appropriate Federal response authority. These initial notifications contain the preliminary release information available at the time of release. The information in ERNS is "unverified" because, at the time of the release, some of the important information may be added to ERNS later; often the only information found in ERNS is that derived from the initial notification. • No ERNS sites were found within the search area. For further information, refer to Appendix E. 4.6 State Lists of Hazardous Waste Sites The State of North Carolina publishes these data. • One State Hazardous Waste Site (SHWS) was identified within the database search area. The site is as follows: o UNC-PHILLIPS HALL located over 5000 feet south of the subject property. The SHWS facility ID is S101573932. Given the distance of this property to the subject property, no environmental impacts are expected. UF • Two Hazardous Substance Disposal Sites (HSDS) were identified within the database search area. The sites are as follows: o UNC-CHAPEL HILL located approximately 2500 feet northwest of the subject property. The HSDS facility ID is S102442306. Given the distance of this property to the subject property, no environmental impacts are expected. o UNIVERSITY OF NC/ARPT RD OLD SAN LDFL located over 4500 feet northwest of the subject property. The HSDS facility ID is S102442299. Given the distance of this property to the subject property, no environmental impacts are expected. 4.7 State Leaking Underground Storage Tank (LUST) List The State of North Carolina publishes these data. • Twenty Three (23) Leaking Underground Storage Tank (LUST) incident were found within a 1 mile search radius. The sites are as follows: o MINIS, LOIS RESIDENCE (Incident # 22668) is located adjacent and north of the site. An underground fuel oil tank leak in 1996 contaminated soil and the risk classification is listed as low. The site was closed later in 1996. Given the nature of this incident, no environmental impacts are expected. o WILLIAMS RES UST (Incident # 33891) is located adjacent and northeast of the site. An underground fuel oil tank leak in 1988 contaminated soil. Given the nature of this incident, no environmental impacts are expected o RUN-IN-JIMS (Incident # 22628) is located adjacent and south of the site. An underground kerosene tank leak in 1988 contaminated soil. Due to the existence of Bolin Creek between this site and the subject property, it is unlikely that this site would impact the subject property. o WESTERN RESIDENTIAL PROPERTIES Seven (7) residential leaking tank sites are located in the subdivision west of the subject property. Given the nature of these incidents, topography, and geological setting, no environmental impacts are expected from these incidents. UF o The remaining thirteen (13) leaking tank sites are located over '/4 mile from the subject property. Given the distances, topography, and/or geological setting, no environmental impacts are expected from these incidents. • For further information with respect to the incidents discussed above, refer to Appendix E. 4.8 State Landfill List (SWF/LF) The State of North Carolina publishes these data. • No State landfill was identified within the search area. For further information, refer to Appendix E. 4.9 State Registered Underground Storage Tank (UST) List The State of North Carolina publishes these data. • One State registered underground storage tanks (USTs) was identified within the search area. RUN-IN-JIMS is located adjacent and south of the site. An underground fuel oil tank leak in 1988 contaminated soil. Due to the existence of Bolin Creek between this site and the subject property, it is unlikely that this site would impact the subject property. For further information, refer to Appendix E. 4.10 PCB Activity Database (PADS) The EPA publishes these data. • The site was not listed within the PADS database search. For further information, refer to Appendix E. 4.11 Federal Superfund Liens (NPL LIENS) This list is compiled by the Office of Enforcement (OE), EPA, Washington, D.C., based on information submitted by EPA's 10 Regional Offices. • The site is not found within the Federal Superfund liens database search. For further information, refer to Appendix E. 12 4.12 Public Water Supply (PWS) Systems The EPA Office of Drinking Water publishes these data. • No PWS Systems were located within a mile of the subject site. 4.13 Facility Permits • From the Facility Index System (FINDS) no sites were identified. 4.14 Leaking Aboveground Storage Tank (LAST) Sites The State of North Carolina publishes this data. • One LAST site was located within the search area, over 2500 feet from the subject site. Given the distance, and/or geological setting, no environmental impact is expected from this incident. SECTInN r- SITE RECONNAISSANCE AND CHARACTERIZATION The purpose of the site reconnaissance was to inspect the property for visible signs or indications of environmental conditions that currently present, or have in the past presented an adverse impact to the site. Mr. Josh Dunbar, PE and Mr. Aric V. Geda, PE, with Falcon conducted site reconnaissance on various occasions during the duration of this project. 5.1 Hazardous Waste and Hazardous Substances Inspection was made of the subject property and as discussed earlier, fly ash was identified to exist on the subject property. While fly ash is currently not listed as a hazardous waste, this listing is currently being re-evaluated by the EPA. Fly ash is known to contain hazardous substances including heavy metals such as arsenic, lead, mercury, cadmium, chromium and selenium, as well as high concentrations of aluminum, antimony, barium, beryllium, boron, chlorine, cobalt, manganese, molybdenum, nickel, thallium, vanadium, and zinc. These contaminants can leach into the groundwater and impact streams and nearby wells. The existence of fly ash on the subject site is considered a Recognized Environmental Concern (REC) of the site. 5.2 Onsite Storage Tanks One AST was observed onsite at the time of the field reconnaissance. This is a diesel AST associated with the on -site generator. During site reconnaissance, there were no obvious observed indications (e.g., distressed vegetation, discolored soils, etc.) of leaks, spills, or potential contamination. 5.3 Air Emissions No visible emissions or unusual odors were observed on or generated from this site. The generator would pose a potential air emission source, however, given the nature and intent of its use at the property (i.e., back up) this source would not be considered an REC. 5.4 Water and Wastewater Potable water and domestic sewer connections are available for the site. 5.5 Polychlorinated Biphenyls (PCBs) No pad -mounted electrical transformers or other potential PCB containing devices were observed on the subject property. 5.6 Topography, Geology and Hydrology A review of the Chapel Hill, NC USGS 7.5-minute 2002 topographic map, which includes the project site, indicates that the site is located on varying elevations from 375 feet above mean sea level (msl) in the northwest corner of the site to 284 feet msl in the southeast corner where the site meets Bolin Creek. The 2010 Topographic Map from Orange County GIS indicates significantly different contours from the USGS maps. This data supports the filling and leveling of the site The US Natural Resource Conservation Service's Orange County Soil Survey maps Two (2) different soil types on the site: TaE - Tatum Silt Loam Complex (15 to 25 percent slopes) - well drained soil derived from red saprolite (50% of the overall subject site). • WmE - Wedowee Sandy Loam Complex (15 to 25 percent slopes) - well drained soil derived from red saprolite (50% of the overall subject site). The site is bounded on the north and west by paved streets, to the east by residential developed woodlands and to the south by Bolin Creek. The general site drainage is to the South via overland flow and along stormwater trenches aside Martin Luther King Jr. Blvd. All stormwater drains from this site into Bolin Creek. Very little, if any, surface water comes onto the site from offsite. 5.7 Spills, Leaks, and Stains No documentation was found that would indicate any spills have occurred on the property. No evidence was found on the property to indicate any type of reportable spill. SErTinti A LIMITED PHASE II ESA Falcon Engineering, Inc. completed a Limited Phase II Environmental Assessment (ESA) at the subject property. The purpose of the limited Phase II environmental assessment was to evaluate the on -site sediment and groundwater for potential contamination within the property boundaries. Based upon our findings from the Phase I ESA work performed, Falcon identified a Recognized Environmental Concern (REC) at the site which included: • The placement of "fly ash" as fill on the subject site. Fly ash is known to contain hazardous substances including heavy metals such as arsenic, lead, mercury, cadmium, chromium and selenium, as well as high concentrations of aluminum, antimony, barium, beryllium, boron, chlorine, cobalt, manganese, molybdenum, nickel, thallium, vanadium, and zinc. These contaminants can leach into the groundwater and impact streams and nearby wells. Our scope of services consisted of sediment and water sampling to determine the existing conditions within identified areas on the subject property. Sampling included the following: • Two sediment samples; One from monitoring well MW-1 location (labeled S-1); and one from a hand auger location in the area of known fly ash (S-4). • Three water samples, including samples from both MW-1 and MW-2, and a surface water sample from Bolin Creek. 6.1 Environmental Sampling Methods All environmental sampling methods followed NCDENR Division of Waste Management's (DWM) "Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST Releases" Sampling strategy was derived based upon the project scope and objectives. Based upon the collected historical data, Phase I information, site topography, storm water drainage, sewage drainage, and geologic survey data, an environmental sampling strategy UF and locations for samples were determined. Sampling locations were determined based upon the potential for contaminant. These locations are depicted in Figure 2 below. Sampling locations were established to identify any potential environmental concerns. FIGURE 2 1 SAMPLING LOCATION MAP 6.1.1 Sediment Samples S-1 was obtained using a geoprobe during the installation of MW-1 at a depth of 15 feet below existing ground surface. S-4 was obtained through Hand Auger techniques at a depth of approximately 1 foot below ground surface. To avoid cross contamination, an unused pair of non -powdered latex gloves was worn while extracting each sample. For the gas range organic (GRO) analysis, a new premeasured syringe was used for each soil sample collection of 5 grams and disposed of after a single use. For this analysis the 5 gram samples were placed into a methanol preserved VOA vial. Duplicate VOA vials were collected for each sampling location. For the diesel range organic (DRO) analysis an unpreserved soil sample was collected in a single 8-oz amber glass jar. Special care was taken during the DRO sample collection to pack the soil into the jar and eliminate unnecessary void space. The labels on each container were then completed so that each provided the date and time of sampling, method of analysis, sample collector, preservative used, and sampling location identification. EPA Method 8015C is used to determine the concentrations of various nonhalogenated volatile organic compounds and semi -volatile organic compounds by gas chromatography. This method is applicable to the analysis of petroleum hydrocarbons. The petroleum hydrocarbons include gasoline range organics (GRO) and diesel range organics (DRO). Additional sample collections were made for each sample collected to allow for a speciated analysis as desired for both volatile and semi -volatile organic compounds, and metals analyses. EPA Method 8260B, EPA Method 8270D, MADEP EPH, and MADEP VPH are the analytical methods for volatiles. EPA Method 8260B is a method used to determine volatile organic compounds via gas chromatography and mass spectrometry (GC/MS). EPA Method 8270D is a method used to determine semi -volatile organic compounds by GC/MS. MADEP EPH is used for determining extractable petroleum hydrocarbons (EPH) based on various extractions analyzed via GC. MADEP VPH is used to determine volatile petroleum hydrocarbons (VPH) based on a purge and trap with GC procedure using PID and FID in series. Method SW-846 6010C is the method used for all metal except Mercury, which is run by method SW-846 7471 B. These were collected to allow for a comparison with NCDENR's risk -based guidelines and were performed on sample S-4 only. All soil samples remained in an ice -filled cooler from the time they were sampled until they were picked up and transported to the lab. The lapse of time between sampling until arriving at the PJF lab was less than 48 hours. Chain of custody procedures, including the completion of necessary forms, was followed as per protocol. 6.1.2 Water Samples MW-1 was obtained using a geoprobe and the installation of a 2" casing with 10' screen to a depth of 40 feet below existing ground surface. The well record can be found in Appendix F. MW-2 was obtained through Hand Auger techniques and installation of a temporary casing to a depth of approximately 8 foot below ground surface. The Bolin Creek Sample was obtained utilizing standard surface water sampling techniques. The following methods were utilized for water analyses: • Volatiles- EPA Method 8260 • Semi-Volatiles- EPA Method 8270 • Metals- EPA Methods 6010C, 6020A, and 7470A All water samples remained in an ice -filled cooler from the time they were sampled until they were picked up and transported to the lab. The lapse of time between sampling until arriving at the lab was less than 48 hours. Chain of custody procedures, including the completion of necessary forms, was followed as per protocol. 6.2 Analytical Results Analytical results indicated the following detections that are above established criteria that could cause regulatory action: • Sediment sample S-4: Elevated levels of Arsenic, Cadmium, Chromium, Cobalt, Copper, Iron, Manganese and Diesel Range Organics. • Groundwater Sample MW-1: Elevated levels of Arsenic, Barium, Chromium, Cobalt, Iron, and Manganese. • Groundwater Sample MW-2: Elevated levels of Barium, Chromium, Cobalt, Copper, Iron, Manganese, Thallium, and Zinc 0 Surface water Sample from Bolin Creek: Elevated levels of Iron and Manganese. I JF The following is a summary of analytical result detections. Full analytical reports are included in Appendix F. TABLE 1 I SUMMARY OF SOIL AND GROUNDWATER SAMPLING SOIL Groundwater Compound S-1 S-4 Results Soil to GW MSCC GW protection RSLs Units MW-1 Results MW-2 Results Bolin Creek NC 2L DW MCL Aluminum RUnitsResults NT 23000 23000 u /I 5600 16000 290 16000Antimon NT <4.4 0.27 u /I 5.4 0.61 <2.0 6 6 Arsenic NT 14 - 0.0013 u /I 85 8.3 0.9 10 0.045 10 Barium NT 24 290 120 u /I 1100 1100 27 700 29000 2000 Beryllium mg/Kgmg/Kg NT <0.44 13 u /I 1.6 5.5 <0.80 - 16 4 Cadmium mg/Kgmg/Kg NT 1.5 0.52 u /I 0.17 0.93 <1.0 2 6.9 5 Calcium mg/Kgmg/Kg NT 9900 u /I 110000 260000 16000 Chromium mg/Kgmg/Kg NT 22 5.4* 0.00059* u /I 15 8.4 <2.0 10 0.031* Cobalt mg/Kgmg/Kg NT 30 0.21 u /I 15 23 0.37 4.7 Copper mg/Kgmg/Kg NT 65 22 u /I 25 1200 2.6 1000 620 1300 Iron mg/Kgmg/Kg NT 59000 2700 u /I 6500 13000 860 - 11000 300 Lead mci/Ka NT 20 270 140 u /I 5.8 27 0.5 15 - 150 Magnesium mg/Kgmg/Kg T 9000 u /I 25000 47000 5300 - - - Manganese m /K NT 1500 210 u /I 7600 1200 100 50 320 - Mercu m /K NT 0.011 0.033 u /I ND 0.18 <0.10 1 0.63 2 Nickel m /K NT 43 110 u /I 12 70 1.2 100 760 - Potassium m /K NT 680 u /I 7600 42,000 2300 - Selenium mg/Kq NT <8.8 0.4 u /I 2.5 18 <10 20 78 50 Silver ma/Kama/Ka NT <0.88 0.25 0.6 u /I ND 0.27 <1.0 20 71 Sodium mg/Kgmg/Kg NT 150 - - u /I 34000 52000 7800 - 60000** - Thallium mg/Kgmg/Kg NT <4.4 0.011 u /I 1 0.48 <0.40 0.16 2 Vanadium mg/Kgmg/Kg NT 21 78 u /I 38 71 <10 78 Zinc mg/Kgmg/Kg NT 120 290 u /I 52 2200 45 1000 4700 GRO mg/Kgmg/Kg ND ND 10 NT NT NT DRO m /K 8.0 27 10 NT NT NT Volatiles m /K NT ND u /I ND NT NT Semi-Volatiles mg/Kg NT ND ug/I ND NT NT ND= Not Detected NT= Not Tested Based on Chromium VI ** EPA Guidance -�720 FINDINGS AND RECOMMENDATIONS This Phase I Environmental Site Assessment of the property located at 828 Martin Luther King Jr. Blvd. in Chapel Hill, North Carolina, has been performed in conformance with the scope and limitations of ASTM Practice E1527-05. Based upon the investigations performed at this property no Recognized Environmental Concerns (RECs) were identified for the site except the following : 1. Fly ash was identified to exist on the subject property. Fly ash is known to contain hazardous substances including heavy metals such as arsenic, lead, mercury, cadmium, chromium and selenium, as well as high concentrations of aluminum, antimony, barium, beryllium, boron, chlorine, cobalt, manganese, molybdenum, nickel, thallium, vanadium, and zinc. These contaminants can leach into the groundwater and impact streams and nearby wells. The existence of fly ash on the subject site is considered a Recognized Environmental Concern (REC) of the site. A Limited Phase II Environmental Assessment was performed in an attempt to evaluate if the REC identified in the Phase I portion has adversely affected the environmental condition of the subject property. The results of the Limited Phase II Assessment indicate: 1. Sediment sampled confirmed the presence of fly ash which exhibited results indicative of environmental contamination above established action levels. 2. Groundwater sampled at the site has been impacted from leaching of the fly ash, exhibiting results indicative of environmental contamination above established action levels. 3. Groundwater appears to be impacting Bolin Creek. Surface water sampled from Bolin Creek exhibited results indicative of environmental contamination above established action levels. 4. A detailed sediment and groundwater investigation will be required to evaluate extent of impacts, potential remedial options, and potential remedial costs. SECTION 8 LIMITATIONS Falcon hereby gives notice that any statement or opinion contained in the Report prepared by Falcon shall not be construed to create any warranty or representation that the real property on which the investigation was conducted poses an environmental hazard, is free of pollution, or complies with any or all applicable or statutory requirements, or that the property is fit for any particular purpose. Unless otherwise indicated in the effort, no attempt was made to check on the compliance of present or past owners of the site with Federal, State, or local laws and regulations. The following responsibilities were distributed to the user or potential user of the subject property, as defined by ASTM 1527-05 and EPA's All Appropriate Inquiries (AAI) Rule: • Interviews with former property owners concerning historical usage that may have impacted the subject property. • Any potential environmental cleanup liens filed or recorded against the subject property. • Activity and use limitations in place at the subject property (i.e., environmental deed restrictions). • Specialized knowledge or experience related to the property or nearby property. • Relationship of the purchase price being paid for the property to its value if not contaminated. The conclusions presented in the Report are based on the services described, and not on scientific tasks or procedures beyond the scope of the described services, which were performed in accordance with the schedule and budget, set forth in the contract with The Town of Chapel Hill. Any person or entity considering use, acquisition, or other involvement or activity concerning the property shall be solely responsible for determining the adequacy of the property for any and all uses for which that person or entity shall use the property. Any person or entity considering use, acquisition, or other involvement or activity concerning the property which is subject of the Report should enter into any use, occupation, acquisition, or the like on sole reliance of its own judgment and on its own personal investigation of such property, and not in reliance on any —722 representation by Falcon regarding such property, character, quality, or its value. Falcon performed this assessment in a professional manner using that degree of skill and care exercised for similar projects under similar conditions by reputable and competent environmental consultants. Falcon shall not be responsible for conditions or consequences arising from relevant facts that were concealed, withheld, or not fully disclosed by others at the time the assessment was conducted. -�723 APPENDIX A HISTORIC FIRE INSURANCE MAPS Town of Chapel Hill 828 Martin Luther King Jr Blvd Chapel Hill, NC 27514 Inquiry Number: 3549422.3 March 20, 2013 440 Wheelers Farms Road Milford, CT 06461 (rEDR'1� Environmental Data Resources Inc 800.352.0050 www.edrnet.com Certified Sanborn® Map Report Site Name: Town of Chapel Hill 828 Martin Luther King Jr Blvd Chapel Hill, NC 27514 EDR Inquiry # 3549422.3 Client Name: Falcon Engineering, Inc. 1210 Trinity Road Raleigh, NC 27607-0000 Contact: Josh Dunbar 3/20/13 EDR Environmental Data Resources Inc The complete Sanborn Library collection has been searched by EDR, and fire insurance maps covering the target property location provided by Falcon Engineering, Inc. were identified for the years listed below. The certified Sanborn Library search results in this report can be authenticated by visiting www.edrnet.com/sanborn and entering the certification number. Only Environmental Data Resources Inc. (EDR) is authorized to grant rights for commercial reproduction of maps by Sanborn Library LLC, the copyright holder for the collection. Certified Sanborn Results: Site Name: Town of Chapel Hill Address: 828 Martin Luther King Jr Blvd City, State, Zip: Chapel Hill, NC 27514 Cross Street: P.O. # E 13026 Project: 828 Martin Luther King Blvd Certification # 48FC-4EOB-A598 UNMAPPED PROPERTY This report certifies that the complete holdings Library, LLC collection have been searched supplied target property information, and fire covering the target property were not found. Limited Permission To Make Copies Sanborn® Library search results Certification # 48FC-4EOB-A598 The Sanborn Library includes more than 1.2 million Sanborn fire insurance maps, which track historical of the Sanborn property usage in approximately 12,000 American cities and towns. Collections searched: based on client insurance maps ✓ Library of Congress ✓ University Publications of America ✓ EDR Private Collection The Sanborn Library LLC Since 1866TI Falcon Engineering, Inc. (the client) is permitted to make up to THREE photocopies of this Sanborn Map transmittal and each fire insurance map accompanying this report solely for the limited use of its customer. No one other than the client is authorized to make copies. Upon request made directly to an EDR Account Executive, the client may be permitted to make a limited number of additional photocopies. This permission is conditioned upon compliance by the client, its customer and their agents with EDR's copyright policy; a copy of which is available upon request. Disclaimer - Copyright and Trademark notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2013 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. 3549422 - 3 page 2 I»yk,llbl m:l HISTORIC TOPOGRAPHIC MAPS LF Town of Chapel Hill 828 Martin Luther King Jr Blvd Chapel Hill, NC 27514 Inquiry Number: 3549422.4 March 20, 2013 440 Wheelers Farms Road Milford, CT 06461 (CEDR'1� Environmental Data Resources Inc 800.352.0050 www.edrnet.com EDR Historical Topographic Map Report Environmental Data Resources, Inc.s (EDR) Historical Topographic Map Report is designed to assist professionals in evaluating potential liability on a target property resulting from past activities. EDRs Historical Topographic Map Report includes a search of a collection of public and private color historical topographic maps, dating back to the early 1900s. Thank you for your business. Please contact EDR at 1-800-352-0050 with any questions or comments. Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report AS IS. Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2013 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. Historical Topographic Map 0 ai5. Q74",ZeOtt_-r c '' PARIM In- SlTk • - - I� I� L 1 r 1. ,�•' y rHORA WIL LIAMS ?97 A i - * } Iron Mine �5 Hil z V. 8/ � •A 4 � J r ' I f y� • . qb . - • i f•� 1 `F. .•• 6• • 30 rasa b �►: * ' 54 _ 3�r •* .',• l°' C CHAPEL. ILL rig• • + _ (B M 487Y, �d .:. I - • i, 'ti,� \ ; � I _.�� :� .• ?►• '►•' • : .•'.: _ • . Meel Eli TARGET QUAD SITE NAME: Town of Chapel Hill CLIENT: Falcon Engineering, Inc. N NAME: CHAPEL HILL ADDRESS: 828 Martin Luther King Jr Blvd CONTACT: Josh Dunbar T MAP YEAR: 1946 Chapel Hill, NC 27514 INQUIRY#: 3549422.4 LAT/LONG: 35.9268 /-79.0529 RESEARCH DATE: 03/20/2013 SERIES: 7.5 SCALE: 1:24000 Historical Topographic Map Church - �- • r • Part ir)• 246 r . Hill' \\� • 7�Fp•• '�•' Uu� rch Iv \ 4 • A. 13 Well '11h AM( n Raidia Towers Fhilline FAtea Hills. • �■ ' �, _ - Horace Williams �dHiah't8ch Seh Airport j `•� 48B j64 r ♦.,, L 99 Cfi apel _: ` �• i f . �• t �a % • l� Iron Mine ---------- I �� : • �S Hillu 1 a +i El M r ' � Cit• ,Hail I 465 n Te % e• a Da ♦ .•• ' 11 i Lli�r• •'•�� Falroner hl !'• .••ti • �• 4 PQ CHA L HII L r r L .��rrrf G •... pL�•M� Mowe• 4Eid87�� i i 57 \•1 141TY OF NOR'1'3"*O INA V jr` lo• Wer r �• ..� rL Ken n , Golt Stadiums a. ladij% Course f St Thamxx Mora�+� Glen Sch TARGET QUAD SITE NAME: Town of Chapel Hill CLIENT: Falcon Engineering, Inc. N NAME: CHAPEL HILL ADDRESS: 828 Martin Luther King Jr Blvd CONTACT: Josh Dunbar T MAP YEAR: 1978 Chapel Hill, NC 27514 INQUIRY#: 3549422.4 LAT/LONG: 35.9268 /-79.0529 RESEARCH DATE: 03/20/2013 SERIES: 7.5 SCALE: 1:24000 Historical Topographic Map well yrh ` e� � f IF �'� U � � /,l% �� • • � _. � -VI OF {i IO{O=rorr= Ix KIP if (g43 ItJ Airport Illarrts— �g �� . /• 1 • chape 4 J 1 � rl -.� I 1 � • � -•fir L •' . • .J';. And i - • -� ��� • �•-�• t� HIII K- ir I � i v f • I 1 ,.r � . 1: _�1•, � �- •'�"' .,};•iv. �. i ` ��/Nr, L.i;le — r •ice •.• •. r q ( T le` �� 1 i i •L' Libry • 'wi. •� � � `�� I'ayh.nnyr' CHA.� T H R y •►�; } tA, — r//i k - 1 •• • .� Moore ,0 15h 0 •Q te 465 S. r c F 1. • Ro + 'I, [ N4 '��'f rt'iti rN "II:A1 OL NA ice, � f,r,ll O :;}• z� i-� � _,r a' :. gSla�rrjr_rr<<is.,• r' I• ' - q, /r �•a �kS -•'�'• .,� �}. _ hJ Si "]'IirrnUlsr Morn lib=tiu TARGET QUAD SITE NAME: Town of Chapel Hill CLIENT: Falcon Engineering, Inc. N CHAPEL HILL ADDRESS: 828 Martin Luther King Jr Blvd CONTACT: Josh Dunbar TNAME: MAP YEAR: 1981 Chapel Hill, NC 27514 INQUIRY#: 3549422.4 PHOTOREVISED FROM :1978 LAT/LONG: 35.9268 /-79.0529 RESEARCH DATE: 03/20/2013 SERIES: 7.5 SCALE: 1:24000 542 C— Uj 360 358 400 ge � pj 360 306 2010)Orangd APPENDIX C HISTORIC AERIAL PHOTOGRAPHS LF de Ad .4 4A.I* ht P, �'7.ejki r Job lw AA3 ®r j P.A E 7hk r'�• fQ. _ . .i: .f • R' 1, ' k • } e F a wr,,'-; - iy .. , ,f 0,1 a . IP � . *�.a� - ■ # At �' AL '�- - . - ,r MAO , __# - . !, .� %. - A` . A a • , ' �t ƒ # - . WOO � � ■ � � � '� � %- .� . | ■ ` � + � % IF ,- k� . � %-� ����■� � ' . - � �. ���� .� . • ���� - . `�� , -MCI, / �•� . . � , ■ . -140 , �b . . _ •� � - ,.� , , _ � - � • , � W �. � ,- . ' , . IPt - - r +P r Ap mom - , , L a f' Ar a lift ft .R J do April 1 19 � F +• r - - � � r f /+ F ' F. L i_ s + i r jbb r IN INE. PINWt Ap ■ -� ��i * IN +r NN r NNN jopL ++� 1 ko 9 Or f i {" � .+Ar a 1 ti NIL A, + - }, IF; IN Ir '.,�,+ r �, �'•� 'tip - y ' it0 -q vo ' As !!! ~ 96 p 4 t } fy dr Rh we r � � JL 41 '! —+ L - ' Nmb _ ID r FJ' L Paw , fy y,S .dI h R. ■ Aw , APPENDIX D PHOTOGRAPHS LF �a.; �,�R x •� ;t''L^i r�e� 7�� l �i���. � � i'i"::• �.�� -,may, 4 O- Photo 3: View of utility cleanout and building in background, looking northeast. Photo 4: View of retention area south of lower parking lot. LF •t . A .i H�4 a r' a� 41 kPPENDIX E REGULATORY DATABASE SEARCH LF Town of Chapel Hill 828 Martin Luther King Jr Blvd Chapel Hill, NC 27514 Inquiry Number: 3669805.1s July 18, 2013 440 Wheelers Farms Road www.edrnet.comt.com Milford, CT 06461 (rEDROEnvironmental Data Resources Inc Toll Free: FORM-NULL-CCA TABLE OF CONTENTS SECTION PAGE Executive Summary ES1 OverviewMap----------------------------------------------------------- 2 DetailMap-------------------------------------------------------------- 3 Map Findings Summary 4 MapFindings------------------------------------------------------------ 7 Orphan Summary--------------------------------------------------------- 93 Government Records Searched/Data Currency Tracking- - - - - - - - - - - - - - - - - - - - - - - - - - GRA GEOCHECK ADDENDUM Physical Setting Source Addendum A-1 Physical Setting Source Summary A-2 Physical Setting SSURGO Soil Map ------------------------------------------- A-5 Physical Setting Source Map------------------------------------------------ A-17 Physical Setting Source Map Findings A-19 Physical Setting Source Records Searched A-24 Thank you for your business. Please contact EDR at 1-800-352-0050 with any questions or comments. Disclaimer - Copyright and Trademark Notice This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF ERRORS OR OMISSIONS, NEGLIGENCE, ACCIDENT OR ANY OTHER CAUSE, FOR ANY LOSS OF DAMAGE, INCLUDING, WITHOUT LIMITATION, SPECIAL, INCIDENTAL, CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be construed as legal advice. Copyright 2013 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission. EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are the property of their respective owners. TC3669805.1s Page 1 EXECUTIVE SUMMARY A search of available environmental records was conducted by Environmental Data Resources, Inc (EDR). The report was designed to assist parties seeking to meet the search requirements of EPA's Standards and Practices for All Appropriate Inquiries (40 CFR Part 312), the ASTM Standard Practice for Environmental Site Assessments (E 1527-05) or custom requirements developed for the evaluation of environmental risk associated with a parcel of real estate. TARGET PROPERTY INFORMATION ADDRESS 828 MARTIN LUTHER KING JR BLVD CHAPEL HILL. NC 27514 COORDINATES Latitude (North): Longitude (West): Universal Tranverse Mercator: UTM X (Meters): UTM Y (Meters): Elevation: 35.9267000 - 35° 55' 36.12" 79.0534000 - 79' 3' 12.24" Zone 17 675619.4 3977369.0 327 ft. above sea level USGS TOPOGRAPHIC MAP ASSOCIATED WITH TARGET PROPERTY Target Property Map: 35079-Hl CHAPEL HILL, NC Most Recent Revision: 1993 AERIAL PHOTOGRAPHY IN THIS REPORT Photo Year: 2012 Source: USDA TARGET PROPERTY SEARCH RESULTS The target property was not listed in any of the databases searched by EDR DATABASES WITH NO MAPPED SITES No mapped sites were found in EDR's search of available ("reasonably ascertainable ") government records either on the target property or within the search radius around the target property for the following databases: STANDARD ENVIRONMENTAL RECORDS Federal NPL site list NPL National Priority List TC3669805.1s EXECUTIVE SUMMARY 1 EXECUTIVE SUMMARY Proposed NPL---------------- Proposed National Priority List Sites NPL LIENS Federal Superfund Liens Federal Delisted NPL site list Delisted NPL National Priority List Deletions Federal CERCLIS list CERCLIS--------------------. Comprehensive Environmental Response, Compensation, and Liability Information System FEDERAL FACILITY Federal Facility Site Information listing Federal CERCLIS NFRAP site List CERC-NFRAP CERCLIS No Further Remedial Action Planned Federal RCRA CORRACTS facilities list CORRACTS------------------ Corrective Action Report Federal RCRA non-CORRACTS TSD facilities list RCRA-TSDF----------------- RCRA - Treatment, Storage and Disposal Federal RCRA generators list RCRA-LQG------------------- RCRA- Large Quantity Generators Federal institutional controls / engineering controls registries US ENG CONTROLS--------. Engineering Controls Sites List US INST CONTROL Sites with Institutional Controls LUCIS Land Use Control Information System Federal ERNS list ERNS Emergency Response Notification System State and tribal landfill and/or solid waste disposal site lists SWF/LF List of Solid Waste Facilities OLI Old Landfill Inventory State and tribal leaking storage tank lists INDIAN LUST---------------- Leaking Underground Storage Tanks on Indian Land State and tribal registered storage tank lists AST AST Database INDIAN UST Underground Storage Tanks on Indian Land FEMA UST------------------- Underground Storage Tank Listing State and tribal institutional control / engineering control registries INST CONTROL No Further Action Sites With Land Use Restrictions Monitoring TC3669805.1s EXECUTIVE SUMMARY 2 EXECUTIVE SUMMARY State and tribal voluntary cleanup sites VCP-------------------------- Responsible Party Voluntary Action Sites INDIAN VCP Voluntary Cleanup Priority Listing State and tribal Brownfields sites BROWNFIELDS Brownfields Projects Inventory ADDITIONAL ENVIRONMENTAL RECORDS Local Brownfield lists US BROWNFIELDS---------- A Listing of Brownfields Sites Local Lists of Landfill / Solid Waste Disposal Sites DEBRIS REGION 9 Torres Martinez Reservation Illegal Dump Site Locations ODI Open Dump Inventory HIST LF---------------------- Solid Waste Facility Listing SWRCY Recycling Center Listing INDIAN ODI Report on the Status of Open Dumps on Indian Lands Local Lists of Hazardous waste / Contaminated Sites US CDL---------------------- Clandestine Drug Labs US HIST CDL National Clandestine Laboratory Register Local Land Records LIENS 2 CERCLA Lien Information Records of Emergency Release Reports HMIRS----------------------- Hazardous Materials Information Reporting System SPILLS 90 SPILLS 90 data from FirstSearch SPILLS 80-------------------- SPILLS 80 data from FirstSearch Other Ascertainable Records RCRA NonGen / NLR--------. RCRA - Non Generators DOT OPS Incident and Accident Data DOD Department of Defense Sites FUDS------------------------ Formerly Used Defense Sites CONSENT Superfund (CERCLA) Consent Decrees ROD Records Of Decision UMTRA---------------------- Uranium Mill Tailings Sites US MINES Mines Master Index File TRIS Toxic Chemical Release Inventory System TSC/------------------------ Toxic Substances Control Act FTTS FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act) HIST FTTS------------------- FIFRA/TSCA Tracking System Administrative Case Listing TC3669805.1s EXECUTIVE SUMMARY 3 EXECUTIVE SUMMARY SSTS------------------------. Section 7 Tracking Systems ICIS Integrated Compliance Information System PADS PCB Activity Database System MLTS------------------------ Material Licensing Tracking System RADINFO Radiation Information Database FINDS Facility Index System/Facility Registry System RAATS----------------------- RCRA Administrative Action Tracking System RMP Risk Management Plans UIC Underground Injection Wells Listing NPDES----------------------. NPDES Facility Location Listing INDIAN RESERV Indian Reservations SCRD DRYCLEANERS State Coalition for Remediation of Drycleaners Listing US AIRS--------------------- Aerometric Information Retrieval System Facility Subsystem PRP Potentially Responsible Parties 2020 COR ACTION 2020 Corrective Action Program List EPA WATCH LIST-----------. EPA WATCH LIST US FIN ASSUR Financial Assurance Information PCB TRANSFORMER PCB Transformer Registration Database COAL ASH------------------- Coal Ash Disposal Sites COAL ASH DOE Steam -Electric Plant Operation Data COAL ASH EPA Coal Combustion Residues Surface Impoundments List Financial Assurance---------- Financial Assurance Information Listing LEAD SMELTERS Lead Smelter Sites EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records EDR MGP EDR Proprietary Manufactured Gas Plants SURROUNDING SITES: SEARCH RESULTS Surrounding sites were identified in the following databases Elevations have been determined from the USGS Digital Elevation Model and should be evaluated on a relative (not an absolute) basis. Relative elevation information between sites of close proximity should be field verified. Sites with an elevation equal to or higher than the target property have been differentiated below from sites with an elevation lower than the target property. Page numbers and map identification numbers refer to the EDR Radius Map report where detailed data on individual sites can be reviewed. Sites listed in bold italics are in multiple databases. Unmappable (orphan) sites are not considered in the foregoing analysis. STANDARD ENVIRONMENTAL RECORDS Federal RCRA generators list RCRA-SQG: RCRAInfo is EPA's comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Small quantity generators (SQGs) generate between 100 kg and 1,000 kg of hazardous waste per month. A review of the RCRA-SQG list, as provided by EDR, and dated 02/12/2013 has revealed that there is 1 TC3669805.1s EXECUTIVE SUMMARY 4 EXECUTIVE SUMMARY RCRA-SQG site within approximately 0.25 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page NCDSCA 068-0005 (MIDTOWN SHOPS 750 MARTIN L KING JR BL SSW 1/8 - 1/4 (0.152 mi.) C14 34 RCRA-CESQG: RCRAInfo is EPA's comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Conditionally exempt small quantity generators (CESQGs) generate less than 100 kg of hazardous waste, or less than 1 kg of acutely hazardous waste per month. A review of the RCRA-CESQG list, as provided by EDR, and dated 02/12/2013 has revealed that there is 1 RCRA-CESQG site within approximately 0.25 miles of the target property. Lower Elevation Address Direction / Distance Map ID Page LLOYD TIRE & ALIGNMENT 730 HILLSBOROUGH ST SSE 0 - 118 (0.048 mi.) Al 7 State- and tribal - equivalent NPL NC HSDS: The Hazardous Substance Disposal Sites list contains locations of uncontrolled and unregulated hazardous waste sites. The file contains sites on the national priority list as well as the state priority list. The data source is the North Carolina Center for Geographic Information and Analysis. A review of the NC HSDS list, as provided by EDR, and dated 08/09/2011 has revealed that there are 2 NC HSDS sites within approximately 1 mile of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page UNC-CHAPEL HILL NNW 1/4 - 1/2 (0.471 mi.) 0 7 UNIVERSITY OF NC/ARPT RD OLD S NW 1/2 - 1 (0.862 mi.) 0 7 State- and tribal - equivalent CERCLIS SHWS: The State Hazardous Waste Sites records are the states' equivalent to CERCLIS. These sites may or may not already be listed on the federal CERCLIS list. Priority sites planned for cleanup using state funds (state equivalent of Superfund) are identified along with sites where cleanup will be paid for by potentially responsible parties. The data come from the Department of Environment & Natural Resources' Inactive Hazardous Sites Program. A review of the SHWS list, as provided by EDR, and dated 05/24/2013 has revealed that there is 1 SHWS site within approximately 1 mile of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page UNC-PHILLIPS HALL 120 E CAMERON AVE S 112 - 1 (0.973 mi.) 35 89 TC3669805.1s EXECUTIVE SUMMARY 5 EXECUTIVE SUMMARY State and tribal leaking storage tank lists LUST: The Leaking Underground Storage Tank Incidents Management Database contains an inventory of reported leaking underground storage tank incidents. The data come from the Department of Environment, & Natural Resources' Incidents by Address. A review of the LUST list, as provided by EDR, and dated 05/10/2013 has revealed that there are 23 LUST sites within approximately 0.5 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page MINIS, LOIS RESIDENCE 6 MT BOLUS RD N 0 - 1/8 (0.119 mi.) 6 18 Incident Phase: Closed Out GALAS RESIDENCE (JOSEPH) 728 WILLIAMS CIRCLE W 1/8 - 1/4 (0.128 mL) B7 21 Incident Phase: Closed Out HUFFMAN PROPERTY 710 WILLIAMS CIRCLE W 1/8 - 1/4 (0.133 mL) B8 24 LANGDELL RESIDENCE 707 WILLIAMS CIRCLE W 1/8 - 1/4 (0.135 mi.) B9 27 Incident Phase: Closed Out WILSON RESIDENCE, TOM 700 WILLIAMS CIRCLE W 1/8 - 1/4 (0.135 mi.) B10 30 Incident Phase: Response WILLIAMS RES UST (ELIZ ET AL) 32 MT. BOLUS RD NE 1/8 - 1/4 (0.188 mi.) 15 36 Incident Phase: Closed Out BRITTON PROPERTY 726 BRADLEY ROAD W 1/8 - 1/4 (0.213 mi.) 16 38 Incident Phase: Closed Out RANCER PROPERTY 712 BRADLEY COURT W 1/8 - 1/4 (0.244 mi.) D17 41 Incident Phase: Closed Out BAXTER ESTATE PROPERTY 710 BRADLEY RD W 1/8 - 1/4 (0.248 mi.) D18 44 Incident Phase: Closed Out PAGE ESTATE (EDITH) 120 JUSTICE STREET NW 114 - 112 (0.253 mi.) 19 46 Incident Phase: Closed Out HUNT RESIDENCE (EMORY) 304 LONE PINE RD SE 1/4 - 1/2 (0.268 mi.) E21 50 Incident Phase: Closed Out LAWLER PROPERTY UST 421 HILLSBOROUGH ST SSE 114 - 112 (0.361 mL) 22 52 UNC-CH SERVICE STATION 109 AIRPORT DRIVE / CB NW 1/4 - 1/2 (0.417 mi.) F23 54 Incident Phase: Response UNC GILES F. HORNEY BUILDING 103 AIRPORT DRIVE NW 1/4 - 1/2 (0.427 mi.) F24 58 CHAPEL HILL TRANSIT MUNICIPAL DR. NNW 114 - 112 (0.463 mL) G25 60 Incident Phase: Closed Out HANSEN REVOCABLE TRUST PROPERT 357 TENNEY CIRCLE ESE 114 - 112 (0.467 mL) 26 63 Incident Phase: Closed Out TOWN OF CHAPEL HILL TRANSIT GA 1089 MARTIN LUTHER KING NNW 1/4 - 1/2 (0.473 mi.) G28 67 SPRUYT, JUNE S. - RESIDENCE 265 SEVER/N STREET W 1/4 - 1/2 (0.483 mi.) 30 71 Incident Phase: Closed Out FLEMING RESIDENTIAL UST 518 NORTH ST SSE 114 - 112 (0.485 mi.) 31 75 Incident Phase: Closed Out PUBLIC WORKS GARAGE 1099 AIRPORT RD NNW 114 - 112 (0.486 mi.) G33 79 Incident Phase: Closed Out Lower Elevation Address Direction / Distance Map ID Page RUN-IN-JIMS 800 AIRPORT ROAD SSW 0 - 118 (0.061 mi.) 3 10 Incident Phase: Closed Out TC3669805.1s EXECUTIVE SUMMARY 6 EXECUTIVE SUMMARY Lower Elevation Address Direction / Distance Map ID Page HOLTON RENTALS PROPERTY 607 HILLSBOROUGH ST SSE 0 - 118 (0.117 mi.) 5 16 BARAZANDEH PROPERTY (FARZIN) 311 BURLAGE CIRCLE ENE 114 - 112 (0.496 mi.) 34 87 LUST TRUST: This database contains information about claims against the State Trust Funds for reimbursements for expenses incurred while remediating Leaking USTs. A review of the LUST TRUST list, as provided by EDR, and dated 04/03/2013 has revealed that there are 17 LUST TRUST sites within approximately 0.5 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page GALAS RESIDENCE (JOSEPH) 728 WILLIAMS CIRCLE W 1/8 - 1/4 (0.128 mi.) B7 21 HUFFMAN PROPERTY 710 WILLIAMS CIRCLE W 1/8 - 1/4 (0.133 mi.) B8 24 LANGDELL RESIDENCE 707 WILLIAMS CIRCLE W 1/8 - 1/4 (0.135 mL) B9 27 WILLIAMS RES UST (ELIZ ET AL) 32 MT. BOLUS RD NE 1/8 - 1/4 (0.188 mi.) 15 36 BRITTON PROPERTY 726 BRADLEY ROAD W 1/8 - 1/4 (0.213 mi.) 16 38 RANCER PROPERTY 712 BRADLEY COURT W 1/8 - 1/4 (0.244 mi.) D17 41 BAXTER ESTATE PROPERTY 710 BRADLEY RD W 1/8 - 1/4 (0.248 mi.) D18 44 PAGE ESTATE (EDITH) 120 JUSTICE STREET NW 1/4 - 1/2 (0.253 mi.) 19 46 HUNT RESIDENCE (EMORY) 304 LONE PINE RD SE 1/4 - 1/2 (0.268 mL) E21 50 LAWLER PROPERTY UST 421 HILLSBOROUGH ST SSE 114 - 112 (0.361 mi.) 22 52 UNC-CH SERVICE STATION 109 AIRPORT DRIVE / CB NW 1/4 - 1/2 (0.417 mi.) F23 54 HANSEN REVOCABLE TRUST PROPERT 357 TENNEY CIRCLE ESE 114 - 112 (0.467 mL) 26 63 SPRUYT, JUNE S. - RESIDENCE 265 SEVER/N STREET W 1/4 - 1/2 (0.483 mi.) 30 71 FLEMING RESIDENTIAL UST 518 NORTH ST SSE 114 - 112 (0.485 mi.) 31 75 PUBLIC WORKS GARAGE 1099 AIRPORT RD NNW 114 - 112 (0.486 mL) G33 79 Lower Elevation Address Direction / Distance Map ID Page HOLTON RENTALS PROPERTY 607 HILLSBOROUGH ST SSE 0 - 118 (0.117 mi.) 5 16 BARAZANDEH PROPERTY (FARZIN) 311 BURLAGE CIRCLE ENE 1/4 - 1/2 (0.496 mL) 34 87 LAST: A listing of leaking aboveground storage tank site locations. A review of the LAST list, as provided by EDR, and dated 05/10/2013 has revealed that there is 1 LAST site within approximately 0.5 miles of the target property. Equal/Higher Elevation CHAPEL HILL TRANSIT GARAGE HYD Address Direction / Distance Map ID Page 1089 MARTIN LUTHER KING NNW 1/4 - 1/2 (0.473 mi.) G27 65 State and tribal registered storage tank lists UST: The Underground Storage Tank database contains registered USTs. USTs are regulated under Subtitle I of the Resource Conservation and Recovery Act (RCRA). The data come from the Department of Environment & Natural Resources' Petroleum Underground Storage Tank Database. A review of the UST list, as provided by EDR, and dated 05/10/2013 has revealed that there is 1 UST site within approximately 0.25 miles of the target property. TC3669805.1s EXECUTIVE SUMMARY 7 EXECUTIVE SUMMARY Lower Elevation Address Direction / Distance Map ID Page RUN-IN-JIMS 800 AIRPORT ROAD SSW 0 - 1/8 (0.061 mi.) 3 10 ADDITIONAL ENVIRONMENTAL RECORDS Records of Emergency Release Reports IMD: Incident Management Database. A review of the IMD list, as provided by EDR, and dated 07/21/2006 has revealed that there are 16 IMD sites within approximately 0.5 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page MINIS RESIDENCE (LOIS) 6 MT. BOLUS RD. NNW 0 - 1/8 (0.072 mi.) 4 15 MINIS, LOIS RESIDENCE 6 MT BOLUS RD N 0 - 1/8 (0.119 mi.) 6 18 GALAS RESIDENCE (JOSEPH) 728 WILLIAMS CIRCLE W 1/8 - 1/4 (0.128 mi.) B7 21 HUFFMAN PROPERTY 710 WILLIAMS CIRCLE W 1/8 - 1/4 (0.133 mi.) B8 24 LANGDELL RESIDENCE 707 WILLIAMS CIRCLE W 1/8 - 1/4 (0.135 mL) B9 27 WILSON RESIDENCE, TOM 700 WILLIAMS CIRCLE W 1/8 - 1/4 (0.135 mi.) B10 30 BRITTON PROPERTY 726 BRADLEY ROAD W 1/8 - 1/4 (0.213 mi.) 16 38 RANCER PROPERTY 712 BRADLEY COURT W 1/8 - 1/4 (0.244 mi.) D17 41 HUNT, EMORY RESIDENCE 304 LONE PINE ROAD SE 1/4 -1/2 (0.268 mi.) E20 49 UNC-CH SERVICE STATION 109 AIRPORT DRIVE / CB NW 1/4 - 1/2 (0.417 mi.) F23 54 CHAPEL HILL TRANSIT MUNICIPAL DR. NNW 114 - 112 (0.463 mL) G25 60 CHAPEL HILL,TOWN OF,TRANSPORTA 1089 AIRPORT ROAD NNW 1/4 - 1/2 (0.473 mi.) G29 70 SPRUYT, JUNE S. - RESIDENCE 265 SEVER/N STREET W 1/4 - 1/2 (0.483 mi.) 30 71 TOWN OF CHAPEL HILL PUBLIC WOR 1099 AIRPORT ROAD NNW 1/4 - 1/2 (0.486 mi.) G32 78 PUBLIC WORKS GARAGE 1099 AIRPORT RD NNW 114 - 112 (0.486 mi.) G33 79 Lower Elevation Address Direction / Distance Map ID Page RUN-IN-JIMS 800 AIRPORT ROAD SSW 0 - 1/8 (0.061 mi.) 3 10 Other Ascertainable Records DRYCLEANERS: Potential and known drycleaning sites, active and abandoned, that the Drycleaning Solvent Cleanup Program has knowledge of and entered into this database. A review of the DRYCLEANERS list, as provided by EDR, and dated 02/06/2013 has revealed that there is 1 DRYCLEANERS site within approximately 0.25 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page MIDTOWN SHOPS 750 MARTIN LUTHER KING SSW 1/8 - 1/4 (0.152 mi.) C12 33 TC3669805.1s EXECUTIVE SUMMARY 8 EXECUTIVE SUMMARY EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records EDR US Hist Auto Stat: EDR has searched selected national collections of business directories and has collected listings of potential gas station/filling station/service station sites that were available to EDR researchers. EDR's review was limited to those categories of sources that might, in EDR's opinion, include gas station/filling station/service station establishments. The categories reviewed included, but were not limited to gas, gas station, gasoline station, filling station, auto, automobile repair, auto service station, service station, etc. This database falls within a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR's HRHR effort presents unique and sometimes proprietary data about past sites and operations that typically create environmental concerns, but may not show up in current government records searches. A review of the EDR US Hist Auto Stat list, as provided by EDR, has revealed that there is 1 EDR US Hist Auto Stat site within approximately 0.25 miles of the target property. Lower Elevation Address Direction / Distance Map ID Page Not reported 730 HILLSBOROUGH ST SSE 0 - 1/8 (0.048 mi.) A2 10 EDR US Hist Cleaners: EDR has searched selected national collections of business directories and has collected listings of potential dry cleaner sites that were available to EDR researchers. EDR's review was limited to those categories of sources that might, in EDR's opinion, include dry cleaning establishments. The categories reviewed included, but were not limited to dry cleaners, cleaners, laundry, laundromat, cleaning/laundry, wash & dry etc. This database falls within a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR's HRHR effort presents unique and sometimes proprietary data about past sites and operations that typically create environmental concerns, but may not show up in current government records searches. A review of the EDR US Hist Cleaners list, as provided by EDR, has revealed that there are 2 EDR US Hist Cleaners sites within approximately 0.25 miles of the target property. Equal/Higher Elevation Address Direction / Distance Map ID Page Not reported 750 MARTIN LUTHER KING SSW 1/8 - 1/4 (0.152 mi.) C11 33 Not reported 750 AIRPORT RD SSW 1/8 - 1/4 (0.152 mi.) C13 34 TC3669805.1s EXECUTIVE SUMMARY 9 EXECUTIVE SUMMARY Due to poor or inadequate address information, the following sites were not mapped. Count: 20 records. Site Name AMERICAN STONE COMPANY - CHAPEL HI MIKE CORNER STORE BLUE CROSS BLUE SHIELD (DURHAM SER UNIVERSITY OF NC/ARPT RD OLD SAN L UNIVERSITY OF NC/ARPT WASTE DSPL A DOT-N-DASH KIRBY'S AMERICAN STATION PROPERTY ROCHELLE PROPERTY (CHARLES) BEAL-TILLMAN WAS KIRBY'S AMERICAN STATION GORDON'S GULF SERVICE GORDON'S BP SERVICE J LOUIS ALLEN TRIPP'S GROCERY STOP 'N SHOP JERRY'S STOP & SHOP CAROLINA CLEANERS CLEORA STERLING CORP NORTH CHAPEL BAPTIST CHURCH HILL TOP MHP Database(s) FINDS,RCRA-CESQG,AIRS (AFS) LAST LAST CERCLIS-NFRAP CERCLIS-NFRAP IMD,LUST LUST LUST TRUST,LUST UST UST UST UST UST UST UST UST FINDS,RCRA-CESQG FINDS,RCRA-CESQG FINDS FINDS TC3669805.1s EXECUTIVE SUMMARY 10 OVERVIEW MAP - 3669805.1 s Target Property Sites at elevations higher than or equal to the target property ♦ Sites at elevations lower than the target property 1 Manufactured Gas Plants National Priority List Sites Dept. Defense Sites 0 1/4 112 1 Mlles Indian Reservations BIA ° d h% Power transmission lines Oil & Gas pipelines from USGS 100-year flood zone 500-year flood zone National Wetland Inventory State Wetlands Hazardous Substance Disposal Sites This report includes Interactive Map Layers to display and/or hide map information. The legend includes only those icons for the default map view. SITE NAME: Town of Chapel Hill CLIENT: Falcon Engineering, Inc. ADDRESS: 828 Martin Luther King Jr Blvd CONTACT: Josh Dunbar Chapel Hill NC 27514 INQUIRY #: 3669805.1s LAT/LONG: 35.9267 / 79.0534 DATE: July 18, 2013 4:29 pm Copyright m 2013 EDR, Inc. (c) 2010 Tele Atlas Ref 0712009 DETAIL MAP - 3669805.1 s Target Property 0 1116 ire 1r4 Miles Sites at elevations higher than or equal to the target property Indian Reservations BIA Hazardous Substance ♦ Sites at elevations lower than °, a a a% Power transmission lines Disposal Sites the target property 1 Manufactured Gas Plants tF' Oil & Gas pipelines from USGS 100-year flood zone r Sensitive Receptors 500-year flood zone Li National Priority List Sites Dept. Defense Sites This report includes Interactive Map Layers to display and/or hide map information. The legend includes only those icons for the default map view. SITE NAME: Town of Chapel Hill CLIENT: Falcon Engineering, Inc. ADDRESS: 828 Martin Luther King Jr Blvd CONTACT: Josh Dunbar Chapel Hill NC 27514 INQUIRY #: 3669805.1s LAT/LONG: 35.9267 / 79.0534 DATE: July 18, 2013 4:35 pm Copyright m 2013 EDR, Inc. (c) 2010 Tele Atlas Rel 0712009 MAP FINDINGS SUMMARY Search Distance Target Total Database (Miles) Property < 1/8 1/8-1/4 1/4-1/2 1/2 - 1 > 1 Plotted STANDARD ENVIRONMENTAL RECORDS Federal NPL site list NPL 1.000 0 0 0 0 NR 0 Proposed NPL 1.000 0 0 0 0 NR 0 NPL LIENS TP NR NR NR NR NR 0 Federal Delisted NPL site list Delisted NPL 1.000 0 0 0 0 NR 0 Federal CERCLIS list CERCLIS 0.500 0 0 0 NR NR 0 FEDERAL FACILITY 0.500 0 0 0 NR NR 0 Federal CERCLIS NFRAP site List CERC-NFRAP 0.500 0 0 0 NR NR 0 Federal RCRA CORRACTS facilities list CORRACTS 1.000 0 0 0 0 NR 0 Federal RCRA non-CORRACTS TSD facilities list RCRA-TSDF 0.500 0 0 0 NR NR 0 Federal RCRA generators list RCRA-LQG 0.250 0 0 NR NR NR 0 RCRA-SQG 0.250 0 1 NR NR NR 1 RCRA-CESQG 0.250 1 0 NR NR NR 1 Federal institutional controls / engineering controls registries US ENG CONTROLS 0.500 0 0 0 NR NR 0 US INST CONTROL 0.500 0 0 0 NR NR 0 LUCIS 0.500 0 0 0 NR NR 0 Federal ERNS list ERNS TP NR NR NR NR NR 0 State- and tribal - equivalent NPL NC HSDS 1.000 0 0 1 1 NR 2 State- and tribal - equivalent CERCLIS SHWS 1.000 0 0 0 1 NR 1 State and tribal landfill and/or solid waste disposal site lists SWF/LF 0.500 0 0 0 NR NR 0 OLI 0.500 0 0 0 NR NR 0 State and tribal leaking storage tank lists LUST 0.500 3 8 12 NR NR 23 TC3669805.1s Page 4 Database MAP FINDINGS SUMMARY Search Distance Target Total (Miles) Property < 1/8 1/8-1/4 1/4-1/2 1/2 - 1 > 1 Plotted LUST TRUST 0.500 1 7 9 NR NR 17 LAST 0.500 0 0 1 NR NR 1 INDIAN LUST 0.500 0 0 0 NR NR 0 State and tribal registered storage tank lists UST 0.250 1 0 NR NR NR 1 AST 0.250 0 0 NR NR NR 0 INDIAN UST 0.250 0 0 NR NR NR 0 FEMA UST 0.250 0 0 NR NR NR 0 State and tribal institutional control / engineering control registries INST CONTROL 0.500 State and tribal voluntary cleanup sites VCP 0.500 INDIAN VCP 0.500 State and tribal Brownfields sites BROWNFIELDS 0.500 ADDITIONAL ENVIRONMENTAL RECORDS Local Brownfield lists US BROWNFIELDS 0.500 Local Lists of Landfill / Solid Waste Disposal Sites DEBRIS REGION 9 0.500 OD I 0.500 HIST LF 0.500 S W RCY 0.500 INDIAN ODI 0.500 Local Lists of Hazardous waste / Contaminated Sites US CDL TP US HIST CDL TP Local Land Records LIENS 2 TP Records of Emergency Release Reports HMIRS TP I M D 0.500 SPILLS 90 TP SPILLS 80 TP Other Ascertainable Records RCRA NonGen / NLR 0.250 0 0 0 NR NR 0 0 0 0 NR NR 0 0 0 0 NR NR 0 0 0 0 NR NR 0 0 0 0 NR NR 0 0 0 0 NR NR 0 0 0 0 NR NR 0 0 0 0 NR NR 0 0 0 0 NR NR 0 0 0 0 NR NR 0 NR NR NR NR NR 0 NR NR NR NR NR 0 NR NR NR NR NR 0 NR NR NR NR NR 0 3 6 7 NR NR 16 NR NR NR NR NR 0 NR NR NR NR NR 0 0 0 NR NR NR 0 TC3669805.1s Page 5 MAP FINDINGS SUMMARY Search Distance Target Database (Miles) Property < 1/8 1/8-1/4 1/4-1/2 1/2 - 1 > 1 DOT OPS TP NR NR NR NR NR DOD 1.000 0 0 0 0 NR FUDS 1.000 0 0 0 0 NR CONSENT 1.000 0 0 0 0 NR ROD 1.000 0 0 0 0 NR UMTRA 0.500 0 0 0 NR NR US MINES 0.250 0 0 NR NR NR TRIS TP NR NR NR NR NR TSCA TP NR NR NR NR NR FTTS TP NR NR NR NR NR HIST FTTS TP NR NR NR NR NR SSTS TP NR NR NR NR NR ICIS TP NR NR NR NR NR PADS TP NR NR NR NR NR MLTS TP NR NR NR NR NR RADINFO TP NR NR NR NR NR FINDS TP NR NR NR NR NR RAATS TP NR NR NR NR NR RMP TP NR NR NR NR NR UIC TP NR NR NR NR NR DRYCLEANERS 0.250 0 1 NR NR NR NPDES TP NR NR NR NR NR INDIAN RESERV 1.000 0 0 0 0 NR SCRD DRYCLEANERS 0.500 0 0 0 NR NR US AIRS TP NR NR NR NR NR PRP TP NR NR NR NR NR 2020 COR ACTION 0.250 0 0 NR NR NR EPA WATCH LIST TP NR NR NR NR NR US FIN ASSUR TP NR NR NR NR NR PCB TRANSFORMER TP NR NR NR NR NR COAL ASH 0.500 0 0 0 NR NR COAL ASH DOE TP NR NR NR NR NR COAL ASH EPA 0.500 0 0 0 NR NR Financial Assurance TP NR NR NR NR NR LEAD SMELTERS TP NR NR NR NR NR EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records EDR MGP 1.000 EDR US Hist Auto Stat 0.250 EDR US Hist Cleaners 0.250 NOTES: TP = Target Property NR = Not Requested at this Search Distance Sites may be listed in more than one database 0 0 0 0 NR 1 0 NR NR NR 0 2 NR NR NR Total 01-f+-.4 0 1 2 TC3669805.1s Page 6 Map ID Direction Distance Elevation Site HSDS UNC-CHAPEL HILL Region NNW NC 1/4-1/2 2485 ft. HSDS: Site Type: SuperfundID: Lat/Long: Total area in coverage units: Total perimeter in coverage units: X-value coordinate in feet: Y-value coordinate in feet: Sites designated as superfund cleanup sites Length of feature in internal units: Area of feature in internal units squared: HSDS UNIVERSITY OF NC/ARPT RD OLD SAN LDFL Region NW NC 1/2-1 4553 ft. HSDS: Site Type: Superfund ID: Lat/Long: Total area in coverage units: Total perimeter in coverage units: X-value coordinate in feet: Y-value coordinate in feet: Sites designated as superfund cleanup sites Length of feature in internal units: Area of feature in internal units squared: MAP FINDINGS Federal 982 093 783 35 56 2.588032 79 3 29.446862 9737.87109375 368.07861328 1982775.625 794875.4375 215 368.07855304 9737.86903121 Federal 980 557 615 35 56 23.497704 79 3 50.658644 237457.15625 1889.34265136 1981032.75 796990.6875 208 1889.34269263 237457.168419 Al LLOYD TIRE & ALIGNMENT SSE 730 HILLSBOROUGH ST < 1/8 CHAPEL HILL, NC 0.048 mi. 252 ft. Site 1 of 2 in cluster A Relative: RCRA-CESQG: Lower Date form received by agency:09/23/2003 Facility name: LLOYD TIRE & ALIGNMENT Actual: Facility address: 730 HILLSBOROUGH ST 314 ft. CHAPEL HILL, NC 27514 EPA ID: NCD986194959 Mailing address: HILLSBOROUGH ST CHAPEL HILL, NC 27514 Contact: DOUGLAS LLOYD Contact address: 730 HILLSBOROUGH ST CHAPEL HILL, NC 27514 Contact country: US Contact telephone: (919) 929-9444 Contact email: Not reported EPA Region: 04 Land type: Private EDR ID Number Database(s) EPA ID Number NC HSDS S102442306 N/A NC HSDS S102442299 N/A RCRA-CESQG 1000831587 FINDS NCD986194959 TC3669805.1s Page 7 Map ID Direction Distance Elevation MAP FINDINGS Site EDR ID Number Database(s) EPA ID Number LLOYD TIRE & ALIGNMENT (Continued) Classification: Conditionally Exempt Small Quantity Generator Description: Handler: generates 100 kg or less of hazardous waste per calendar month, and accumulates 1000 kg or less of hazardous waste at any time; or generates 1 kg or less of acutely hazardous waste per calendar month, and accumulates at any time: 1 kg or less of acutely hazardous waste; or 100 kg or less of any residue or contaminated soil, waste or other debris resulting from the cleanup of a spill, into or on any land or water, of acutely hazardous waste; or generates 100 kg or less of any residue or contaminated soil, waste or other debris resulting from the cleanup of a spill, into or on any land or water, of acutely hazardous waste during any calendar month, and accumulates at any time: 1 kg or less of acutely hazardous waste; or 100 kg or less of any residue or contaminated soil, waste or other debris resulting from the cleanup of a spill, into or on any land or water, of acutely hazardous waste Owner/Operator Summary Owner/operator name: DOUGLAS LLOYD Owner/operator address: Not reported NC Owner/operator country: US Owner/operator telephone: Not reported Legal status: Private Owner/Operator Type: Owner Owner/Op start date: 01/01/1996 Owner/Op end date: Not reported Owner/operator name: JOHN D LLOYD Owner/operator address: 6601 TEER RD. MEBANE, NC 27302 Owner/operator country: Not reported Owner/operator telephone: (919) 563-1874 Legal status: Private Owner/Operator Type: Owner Owner/Op start date: Not reported Owner/Op end date: Not reported Owner/operator name: DOUGLAS LLOYD Owner/operator address: Not reported NC Owner/operator country: US Owner/operator telephone: Not reported Legal status: Private Owner/Operator Type: Operator Owner/Op start date: 01/01/1996 Owner/Op end date: Not reported Handler Activities Summary: U.S. importer of hazardous waste: No Mixed waste (haz. and radioactive): No Recycler of hazardous waste: No Transporter of hazardous waste: No Treater, storer or disposer of HW: No Underground injection activity: No On -site burner exemption: No Furnace exemption: No 1000831587 TC3669805.1s Page 8 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number LLOYD TIRE & ALIGNMENT (Continued) 1000831587 Used oil fuel burner: No Used oil processor: No User oil refiner: No Used oil fuel marketer to burner: No Used oil Specification marketer: No Used oil transfer facility: No Used oil transporter: No Historical Generators: Date form received by agency:09/15/2003 Facility name: LLOYD TIRE & ALIGNMENT Classification: Conditionally Exempt Small Quantity Generator Date form received by agency:10/23/2000 Facility name: LLOYD TIRE & ALIGNMENT Classification: Small Quantity Generator Date form received by agency:09/11/1991 Facility name: LLOYD TIRE & ALIGNMENT Classification: Small Quantity Generator Hazardous Waste Summary: Waste code: D008 Waste name: LEAD Facility Has Received Notices of Violations: Regulation violated: SR - 262.41 Area of violation: Generators - General Date violation determined: 10/19/1995 Date achieved compliance: 11/08/1995 Violation lead agency: State Enforcement action: WRITTEN INFORMAL Enforcement action date: 10/19/1995 Enf. disposition status: Not reported Enf. disp. status date: Not reported Enforcement lead agency: State Proposed penalty amount: Not reported Final penalty amount: Not reported Paid penalty amount: Not reported Evaluation Action Summary Evaluation date: 11/08/1995 Evaluation: COMPLIANCE SCHEDULE EVALUATION Area of violation: Generators - General Date achieved compliance: 11/08/1995 Evaluation lead agency: State Evaluation date: 10/19/1995 Evaluation: FOCUSED COMPLIANCE INSPECTION Area of violation: Generators - General Date achieved compliance: 11/08/1995 Evaluation lead agency: State FINDS: Registry ID: 110004045989 TC3669805.1s Page 9 Map ID MAP FINDINGS Direction Distance Elevation Site EDR ID Number Database(s) EPA ID Number LLOYD TIRE & ALIGNMENT (Continued) Environmental Interest/Information System RCRAInfo is a national information system that supports the Resource Conservation and Recovery Act (RCRA) program through the tracking of events and activities related to facilities that generate, transport, and treat, store, or dispose of hazardous waste. RCRAInfo allows RCRA program staff to track the notification, permit, compliance, and corrective action activities required under RCRA. A2 SSE 730 HILLSBOROUGH ST < 1/8 CHAPEL HILL, NC 27514 0.048 mi. 252 ft. Site 2 of 2 in cluster A Relative: EDR Historical Auto Stations: Lower Name: LLOYD TIRE & ALIGNMENT Year: 2002 Actual: Address: 730 HILLSBOROUGH ST 314 ft. Name: LLOYD TIRE & ALIGNMENT CTR Year: 2003 Address: 730 HILLSBOROUGH ST Name: LLOYD TIRE & ALIGNMENT CENTER LLC Year: 2007 Address: 730 HILLSBOROUGH ST Name: LLOYD TIRE & ALIGNMENT CENTER LLC Year: 2009 Address: 730 HILLSBOROUGH ST Name: LLOYD TIRE & ALIGNMENT LLC Year: 2010 Address: 730 HILLSBOROUGH ST Name: LLOYD TIRE & ALIGNMENT LLC Year: 2011 Address: 730 HILLSBOROUGH ST 1000831587 EDR US Hist Auto Stat 1015618685 N/A 3 RUN-IN-JIMS SSW 800 AIRPORT ROAD < 118 CHAPEL HILL, NC 27514 0.061 mi. 321 ft. Relative: IMD: Lower Region: RAL Facility ID: 22628 Actual: Date Occurred: 3/31/1998 321 ft. Submit Date: 12/11/2000 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: SOIL CONTAMINATION DISCOVERED UPON UST REMOVAL Operator: Not reported Contact Phone: 9199421758 IMD 0003137604 LUST N/A UST TC3669805.1 s Page 10 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number RUN -IN -DIMS (Continued) 0003137604 Owner Company: JIMMY MORGAN Operator Address:800 AIRPORT RD. Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27514- Ownership: Private Operation: Commercial Material: Not reported Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Facility Setting: Urban Risk Site: Not reported Site Priority: U Priority Code: Not reported Priority Update: 12/12/2000 Dem Contact: MAF Wells Affected: No Num Affected: Not reported Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.92527777 Longitude:-79.05388888 Latitude Number: 355531 Longitude Number: 790314 Latitude Decimal: 35.9252777777778 Longitude Decimal: 79.0538888888889 GPS: NOD Agency: DWM Facility ID: 22628 Last Modified: 12/11/2000 Incident Phase: RE NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST: Facility ID: 00-0-000 UST Number: RA-3681 Incident Number: 22628 Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 06/01/1998 Date Occur: 03/31/1998 TC3669805.1 s Page 11 Map ID Direction Distance Elevation Site MAP FINDINGS EDR ID Number Database(s) EPA ID Number RUN -IN -DIMS (Continued) Cleanup: Not reported Closure Request: Not reported Close Out: 01/27/2012 Level Of Soil Cleanup Achieved: Residential Tank Regulated Status: Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: COMMERCIAL Risk Classification: I Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: 09/27/2001 Site Priority: Not reported Phase Of LSA Req: 1 Site Risk Reason: Surface water Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Cleanups to alternate standards PETOPT: 3 RPL: False CD Num: Not reported Reel Num: Not reported RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.5531-79.0314 Testlat: Not reported Regional Officer Project Mgr: DMD Region: Raleigh Company: JIMMY MORGAN Contact Person: Not reported Telephone: 9199421758 RP Address: 800 MARTIN LUTHER KING JR BLVD RP City,St,Zip: CHAPEL HILL, NC 27514- RP County: orange Comments: 550 gal kerosene UST and 38 tons of contam soil were removed in 1988. In 2001, a LSA was completed. In 2011, request was made to close site based on existing soil data and 2011 MW resampling data. Based on data, changed risk to Low. Sending soil and gw NRP request NORR. DMD, 10-25-11 ///nfa w gw only nrp. DMD, 1-27-12 5 Min Quad: Not reported PIRF: Facility Id: 22628 Date Occurred: 1998-03-31 00:00:00 Date Reported: 2000-12-11 00:00:00 Description Of Incident: SOIL CONTAMINATION DISCOVERED UPON UST REMOVAL Owner/Operator: JIMMY MORGAN Ownership: 4 Operation Type: 6 0003137604 TC3669805.1 s Page 12 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number RUN -IN -DIMS (Continued) 0003137604 Type: 3 Location: 1 Site Priority: U Priority Update: 2000-12-12 00:00:00 Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: Not reported 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: Not reported Source: C Ust Number: C Last Modified: 2000-12-11 00:00:00 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported UST: Facility Id: 00-0-0000022146 Contact: JIMMY. MORGAN Contact Address1: DBA RUN-IN-JIMS Contact Address2: 800 AIRPORT ROAD Contact City/State/Zip: CHAPEL HILL, NC 27514-2600 FIPS County Desc: Orange Latitude: 35.92519 Longitude: -79.05361 Tank Id: 1 Tank Status: Removed Installed Date: 05/08/1976 Perm Close Date: 12/31/1998 Product Key: 8 Product Name: Kerosene, Kero Mix Tank Capacity: 550 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: Not reported Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel Piping Construction: Other Piping System Key: Unknown Other CP Tank: Not reported TC3669805.1 s Page 13 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number RUN -IN -DIMS (Continued) 0003137604 Tank Id: 2 Tank Status: Current Installed Date: 05/08/1976 Perm Close Date: Not reported Product Key: 1 Product Name: Diesel Tank Capacity: 2000 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: 0 Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel Piping Construction: Double Wall FRP Piping System Key: Pressurized System Other CP Tank: Not reported Tank Id: 3 Tank Status: Current Installed Date: 05/08/1976 Perm Close Date: Not reported Product Key: 3 Product Name: Gasoline, Gas Mix Tank Capacity: 3000 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: 0 Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel Piping Construction: Double Wall FRP Piping System Key: Pressurized System Other CP Tank: Not reported Tank Id: 4 Tank Status: Current Installed Date: 05/08/1976 Perm Close Date: Not reported Product Key: 3 Product Name: Gasoline, Gas Mix Tank Capacity: 6000 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: 0 Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel Piping Construction: Double Wall FRP Piping System Key: Pressurized System Other CP Tank: Not reported TC3669805.1 s Page 14 Map ID MAP FINDINGS Direction Distance Elevation Site RUN -IN -DIMS (Continued) Tank Id: 5 Tank Status: Current Installed Date: 05/08/1976 Perm Close Date: Not reported Product Key: 3 Product Name: Gasoline, Gas Mix Tank Capacity: 6000 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: 0 Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel Piping Construction: Double Wall FRP Piping System Key: Pressurized System Other CP Tank: Not reported Tank Id: 6 Tank Status: Current Installed Date: 08/28/1991 Perm Close Date: Not reported Product Key: 3 Product Name: Gasoline, Gas Mix Tank Capacity: 8000 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: 0 Commercial: Yes Regulated: Yes Tank Construction: Single Wall FRP Piping Construction: Single Wall FRP Piping System Key: Unknown Other CP Tank: Not reported EDR ID Number Database(s) EPA ID Number 0003137604 4 MINIS RESIDENCE (LOIS) IMD S104914625 NNW 6 MT. BOLUS RD. N/A < 118 CHAPEL HILL, NC 0.072 mi. 379 ft. Relative: IMD Higher Region: RAL Facility ID: 22668 Actual: Date Occurred: 3/25/1996 394 ft. Submit Date: 1/4/2001 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: SOIL CONTAMINATION DISCOVERED DURING UST REMOVAL Operator: Not reported Contact Phone: Not reported Owner Company: DECEASED Operator Address:Not reported Operator City: Not reported Oper City,St,Zip: NC Ownership: Private TC3669805.1 s Page 15 Map ID MAP FINDINGS Direction Distance Elevation Site MINIS RESIDENCE (LOIS) (Continued) Operation: Residential Material: Not reported Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Residence Setting: Rural Risk Site: L Site Priority: Not reported Priority Code: Not reported Priority Update: 1/4/2001 Dem Contact: MRP Wells Affected: No Num Affected: Not reported Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.92722222 Longitude: -79.04611111 Latitude Number: 355538 Longitude Number: 790246 Latitude Decimal: 35.9272222222222 Longitude Decimal: 79.0461111111111 GPS: NOD Agency: DWM Facility ID: 22668 Last Modified: 6/7/2002 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: 4/16/1996 5 HOLTON RENTALS PROPERTY SSE 607 HILLSBOROUGH ST < 118 CHAPEL HILL, NC 27514 0.117 mi. 617 ft. Relative: LUST: Lower Facility ID: Not reported UST Number: RA-6024 Actual: Incident Number: 33564 303 ft. Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 07/25/2008 Date Occur: 07/24/2008 EDR ID Number Database(s) EPA ID Number S104914625 LUST S109164495 LUST TRUST N/A TC3669805.1 s Page 16 Map ID MAP FINDINGS Direction Distance Elevation Site HOLTON RENTALS PROPERTY (Continued) Cleanup: Not reported Closure Request: Not reported Close Out: Not reported Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: Not reported Risk Class Based On Review: U Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: 0 Reel Num: 0 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9245-79.0526 Testlat: Not reported EDR ID Number Database(s) EPA ID Number S109164495 Regional Officer Project Mgr: DMD Region: Raleigh Company: Holton Rentals, LLC Contact Person: Jerrel Kesling Telephone: 9196198607 RP Address: PO BOX 2686 RP City,St,Zip: CHAPEL HILL, NC 27515 RP County: Not reported Comments: 550 GAL RESIDENTIAL HEATING OIL UST RELEASE. 19,000/700 MG/KG TPH DRO/GRO IN SOIL AT 5.75'. TANK REMOVED. LIMITED EXCAVATION TO 14.5 FT DEEP BECAUSE OF FOUNDATION CONCERNS. - DMD,8/27/08.///Per IAA report, risk -based analysis confirmed exceedance of residential soil MSCCs in 3 of 5 samples, and stg MSCCS in the other two samples; groundwater reported at excavation base- DMD,9/23/08H// 5 Min Quad: Not reported PIRF: Facility Id: 33564 Date Occurred: 2008-07-24 00:00:00 Date Reported: 2008-07-25 00:00:00 Description Of Incident: 550 GAL RESIDENTIAL HEATING OIL UST RELEASE. 19,000/700 MG/KG TPH DRO/GRO IN SOIL AT 5.75'. DMD,8/27/08./// Owner/Operator: Not reported TC3669805.1 s Page 17 Map ID MAP FINDINGS Direction Distance Elevation Site HOLTON RENTALS PROPERTY (Continued) Ownership: 4 Operation Type: 3 Type: 4 Location: 7 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: Y 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: 3 Source: A Ust Number: P Last Modified: Not reported Incident Phase: Not reported NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: Facility ID: Not reported Site ID: 33564 Site Note: Noncommercial; 100% eligible; $0 deductible.[CGS 10/12/09] Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 Clink this by perlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. 6 MINIS, LOIS RESIDENCE North 6 MT BOLUS RD < 1/8 CHAPEL HILL, NC 0.119 mi. 629 ft. Relative: IMD: Higher Region: RAL Facility ID: 16285 Actual: Date Occurred: 4/11/1996 408 ft. Submit Date: 9/20/1996 GW Contam: No Groundwater Contamination detected EDR ID Number Database(s) EPA ID Number S109164495 IMD S106349118 LUST N/A TC3669805.1 s Page 18 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number MINIS, LOIS RESIDENCE (Continued) S106349118 Soil Contam: Yes Incident Desc: RELEASE CONFIRMED UPON TANK REMOVAL Operator: LOIS MINIS Contact Phone: 919 967-7513 Owner Company: Not reported Operator Address:6 MT BOLUS RD Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27514 Ownership: Private Operation: Residential Material: #2 FUEL OIL Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Residence Setting: Residential Risk Site: Not reported Site Priority: 10E Priority Code: E Priority Update: Not reported Dem Contact: MAF Wells Affected: Not reported Num Affected: 0 Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: Not reported Longitude: Not reported Latitude Number: Not reported Longitude Number: Not reported Latitude Decimal: Not reported Longitude Decimal: Not reported GPS: NOD Agency: Not reported Facility ID: 16285 Last Modified: 5/3/2001 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: 4/12/1996 LUST: Facility ID: Not reported UST Number: RA-3693 Incident Number: 22668 Contamination Type: Soil TC3669805.1 s Page 19 Map ID Direction Distance Elevation Site MAP FINDINGS EDR ID Number Database(s) EPA ID Number MINIS, LOIS RESIDENCE (Continued) Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 04/16/1996 Date Occur: 03/25/1996 Cleanup: Not reported Closure Request: Not reported Close Out: 04/16/1996 Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Not reported MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in Archives RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: 127 Reel Num: 24 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9272-79.6111 Testlat: Not reported Regional Officer Project Mgr: MRP Region: Raleigh Company: DECEASED Contact Person: Not reported Telephone: Not reported RP Address: Not reported RP City,St,Zip: NC RP County: Not reported Comments: Same as Incident #16285 which was closed out in 4/16/1996. 223 ppm TPH in soil, SSE was 240 ppm TPH so OK to close under rules in effect at that time. RKD. 5 Min Quad: Not reported PIRF: Facility Id: Date Occurred: Date Reported: Description Of Incident: Owner/Operator: S106349118 22668 1996-03-25 00:00:00 2001-01-04 00:00:00 SOIL CONTAMINATION DISCOVERED DURING UST REMOVAL DECEASED TC3669805.1 s Page 20 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number MINIS, LOIS RESIDENCE (Continued) S106349118 Ownership: 4 Operation Type: 3 Type: 4 Location: 7 Site Priority: Not reported Priority Update: 2001-01-04 00:00:00 Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: Not reported 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: Not reported Source: E Ust Number: E Last Modified: 2002-06-07 00:00:00 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: 1996-04-16 00:00:00 B7 GALAS RESIDENCE (JOSEPH) IMD S106196041 West 728 WILLIAMS CIRCLE LUST N/A 1/8-1/4 CHAPEL HILL, NC LUST TRUST 0.128 mi. 677 ft. Site 1 of 4 in cluster B Relative: IMD: Higher Region: RAL Facility ID: 26486 Actual: Date Occurred: 8/25/2003 425 ft. Submit Date: 12/17/2003 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: 270 GALLON HEATING OIL UST REMOVED; INITIAL SOIL SAMPLES INDICATED CONTAM, 6 TONS SOILS REMOVED, FOLLOWUP SOIL SAMPLES < SOIL TO GW MSCC; Operator: Not reported Contact Phone: Not reported Owner Company: JOSEPH GALAS Operator Add ress:1210 ALABAMA AVENUE Operator City: DURHAM Oper City,St,Zip: DURHAM, NC 27705- Ownership: Private Operation: Residential Material: Not reported Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground TC3669805.1 s Page 21 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number GALAS RESIDENCE (JOSEPH) (Continued) S106196041 Type: Gasoline/diesel Location: Residence Setting: Not reported Risk Site: L Site Priority: Not reported Priority Code: Not reported Priority Update: Not reported Dem Contact: MAF Wells Affected: Unknown Num Affected: Not reported Wells Contam: Not reported Sampled By: Y Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.8775 Longitude:-79.05611111 Latitude Number: 355239 Longitude Number: 790322 Latitude Decimal: 35.8775 Longitude Decimal: 79.0561111111111 GPS: 6 Agency: DWM Facility ID: 26486 Last Modified: 2/20/2004 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST: Facility ID: Not reported UST Number: RA-4948 Incident Number: 26486 Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 12/12/2003 Date Occur: 08/25/2003 Cleanup: Not reported Closure Request: Not reported Close Out: 02/20/2004 Level Of Soil Cleanup Achieved: Soil to Groundwater Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported TC3669805.1 s Page 22 Map ID MAP FINDINGS Direction Distance Elevation Site GALAS RESIDENCE (JOSEPH) (Continued) NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in Archives RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: 233 Reel Num: 116 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.8774-79.0561 Testlat: Not reported EDR ID Number Database(s) EPA ID Number S106196041 Regional Officer Project Mgr: MAF Region: Raleigh Company: JOSEPH GALAS Contact Person: Not reported Telephone: Not reported RP Address: 1210 ALABAMA AVENUE RP City,St,Zip: DURHAM, NC 27705- RP County: Not reported Comments: 12/17/2003 - 90 DAY REPORT SUBMITTED, 270 GALLON HEATING OIL UST REMOVED, 6 TONS CONTAMINATED SOILS EXCAVATED & DISPOSED OF, INITIAL SOIL SAMPLE AT 4'-5' FOUND 270 PPM (3550), AFTER SOILS WERE EXCAVATED FOLLOWUP SOIL SAMPLE TAKEN AT 6' FOUND < SOIL TO GW. 02/20/04 - NFA ISSUED. 5 Min Quad: Not reported PIRF: Facility Id: 26486 Date Occurred: 2003-08-25 00:00:00 Date Reported: 2003-12-17 00:00:00 Description Of Incident: 270 GALLON HEATING OIL UST REMOVED; INITIAL SOIL SAMPLES INDICATED CONTAM, 6 TONS SOILS REMOVED, FOLLOWUP SOIL SAMPLES < SOIL TO GW MSCC; Owner/Operator: Not reported Ownership: 4 Operation Type: 3 Type: 4 Location: 7 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: U Samples Include: Not reported 7#5 Minute Quad: Y 5 Minute Quad: Not reported Pirf/Min Soil: Not reported TC3669805.1 s Page 23 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number GALAS RESIDENCE (JOSEPH) (Continued) S106196041 Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: Not reported Source: C Ust Number: C Last Modified: 2004-02-20 00:00:00 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: Facility ID: Not reported Site ID: 26486 Site Note: Not reported Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 100000 Sum 3rd Party Amt Applied: 0 Clink this hgpprlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. B8 HUFFMAN PROPERTY IMD S104547347 West 710 WILLIAMS CIRCLE LUST N/A 1/8-1/4 CHAPEL HILL, NC LUST TRUST 0.133 mi. 701 ft. Site 2 of 4 in cluster B Relative: IMD: Higher Region: RAL Facility ID: 21888 Actual: Date Occurred: 1/14/2000 423 ft. Submit Date: 6/16/2000 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: (1) 550 GAL HEATING OIL UST LEAKS & IS STILL IN GROUND REMOVED SOON. SAMP FROM SITE DIESEL RANGE 1390.20 PPM: 3550. FURTHER INVEST REQUIRED Operator: CAMERON HUFFMAN Contact Phone: 9199683271 Owner Company: Not reported Operator Address:113 MILL RUN DRIVE Operator City: CHAPPEL HILL Oper City,St,Zip: CHAPPEL HILL, NC 27514- Ownership: Private Operation: Residential TC3669805.1 s Page 24 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number HUFFMAN PROPERTY (Continued) S104547347 Material: HEATING OIL Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Residence Setting: Residential Risk Site: L Site Priority: Not reported Priority Code: Not reported Priority Update: 7/20/2000 Dem Contact: MAF Wells Affected: Not reported Num Affected: Not reported Wells Contam: Not reported Sampled By: Responsible Parties Samples Include: Soil Samples 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.92555555 Longitude:-79.05888888 Latitude Number: 355532 Longitude Number: 790332 Latitude Decimal: 35.9255555555556 Longitude Decimal: 79.0588888888889 GPS: NOD Agency: DWM Facility ID: 21888 Last Modified: Not reported Incident Phase: Not reported NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST: Facility ID: Not reported UST Number: RA-3415 Incident Number: 21888 Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 02/24/2000 Date Occur: 01/14/2000 Cleanup: 01/14/2000 Closure Request: Not reported Close Out: Not reported Level Of Soil Cleanup Achieved: Residential Tank Regulated Status: Non Regulated # Of Supply Wells: 0 TC3669805.1 s Page 25 Map ID MAP FINDINGS Direction Distance Elevation Site HUFFMAN PROPERTY (Continued) Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: 11/21/2001 Site Priority: Not reported Phase Of LSA Req: 1 Site Risk Reason: Surface water Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: Not reported Reel Num: Not reported RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.5531-79.0331 Testlat: Not reported Regional Officer Project Mgr: CED Region: Raleigh Company: Not reported Contact Person: CAMERON HUFFMAN Telephone: 9199683271 RP Address: 113 MILL RUN DRIVE RP City,St,Zip: CHAPEL HILL, NC 27514- RP County: orange Comments: SAR (04/03/2001) approved. 11 /19/2001). 5 Min Quad: Not reported EDR ID Number Database(s) EPA ID Number S104547347 PIRF: Facility Id: 21888 Date Occurred: 2000-01-16 00:00:00 Date Reported: 2000-06-16 00:00:00 Description Of Incident: (1) 550 GAL HEATING OIL UST LEAKS & IS STILL IN GROUND REMOVED SOON. SAMP FROM SITE DIESEL RANGE 1390.20 PPM: 3550. FURTHER INVEST REQUIRED Owner/Operator: CAMERON & JENNIFER HUFFMAN Ownership: 4 Operation Type: 3 Type: 4 Location: 7 Site Priority: Not reported Priority Update: 2000-07-20 00:00:00 Wells Affected Y/N: Not reported Samples Include: Not reported 7#5 Minute Quad: 3 5 Minute Quad: 2 Pirf/Min Soil: Not reported TC3669805.1 s Page 26 Map ID Direction Distance Elevation Site HUFFMAN PROPERTY (Continued) MAP FINDINGS EDR ID Number Database(s) EPA ID Number Release Code: Not reported Source Code: PIRF Err Type: Not reported Cause: Not reported Source: Not reported Ust Number: Not reported Last Modified: Not reported Incident Phase: Not reported NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: Facility ID: Not reported Site ID: 21888 Site Note: Not reported Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 Clink this hgpprlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. B9 LANGDELL RESIDENCE IMD West 707 WILLIAMS CIRCLE LUST 1/8-1/4 CHAPEL HILL, NC LUST TRUST 0.135 mi. 713 ft. Site 3 of 4 in cluster B Relative: IMD: Higher Region: RAL Facility ID: 22719 Actual: Date Occurred: 9/11/2000 422 ft. Submit Date: 1/5/2000 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: SOIL CONTAMINATION DISCOVERED UPON UST REMOVAL Operator: ALICE LANGDELL Contact Phone: 9199295672 Owner Company: Not reported Operator Address:707 WILLIAMS CIRCLE Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27516- Ownership: Private Operation: Residential Material: Not reported S104547347 S105119909 N/A TC3669805.1 s Page 27 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number LANGDELL RESIDENCE (Continued) S105119909 Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Residence Setting: Residential Risk Site: L Site Priority: U Priority Code: Not reported Priority Update: 1/5/2001 Dem Contact: MRP Wells Affected: No Num Affected: Not reported Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.92666666 Longitude: -79.05666666 Latitude Number: 355536 Longitude Number: 790324 Latitude Decimal: 35.9266666666667 Longitude Decimal: 79.0566666666667 GPS: NOD Agency: DWM Facility ID: 22719 Last Modified: 2/28/2001 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: 1/17/2001 LUST: Facility ID: Not reported UST Number: RA-3732 Incident Number: 22719 Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 11/20/2000 Date Occur: 09/11/2000 Cleanup: Not reported Closure Request: 2000-11-20 00:00:00 Close Out: 01/17/2001 Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL TC3669805.1 s Page 28 Map ID MAP FINDINGS Direction Distance Elevation Site LANGDELL RESIDENCE (Continued) EDR ID Number Database(s) EPA ID Number S105119909 Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: 12/14/2000 Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Not reported MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in Archives RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: 127 Reel Num: 24 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9262-79.0571 Testlat: Not reported Regional Officer Project Mgr: MRP Region: Raleigh Company: Not reported Contact Person: ALICE LANGDELL Telephone: 9199295672 RP Address: 707 WILLIAMS CIRCLE RP City,St,Zip: CHAPEL HILL, NC 27516- RP County: Orange Comments: One (1) 550 gal heating oil ust was removed 10/5/00. 5 Min Quad: Not reported PIRF: Facility Id: Date Occurred: Date Reported: Description Of Incident: Owner/Operator: Ownership: Operation Type: Type: Location: Site Priority: Priority Update: Wells Affected Y/N: Samples Include: 7#5 Minute Quad: 5 Minute Quad: Pirf/Min Soil: Release Code: Source Code: 22719 2000-09-11 00:00:00 2000-01-05 00:00:00 SOIL CONTAMINATION DISCOVERED UPON UST REMOVAL ALICE LANGDELL 4 3 4 7 U 2001-01-05 00:00:00 N Not reported Not reported Not reported Not reported Not reported Not reported TC3669805.1 s Page 29 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number LANGDELL RESIDENCE (Continued) S105119909 Err Type: 2 Cause: Not reported Source: C Ust Number: C Last Modified: 2001-02-28 00:00:00 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: 2001-01-17 00:00:00 LUST TRUST: Facility ID: Not reported Site ID: 22719 Site Note: Not reported Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 Clink this h gnarlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. B10 WILSON RESIDENCE, TOM IMD S101573544 West 700 WILLIAMS CIRCLE LUST N/A 1/8-1/4 CHAPEL HILL, NC 0.135 mi. 715 ft. Site 4 of 4 in cluster B Relative: IMD: Higher Region: RAL Facility ID: 12051 Actual: Date Occurred: 3/29/1994 421 ft. Submit Date: 4/21/1994 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: TANK REMOVED; SOIL SAMPLE CONFIRMED SOIL CONTAMINATION. Operator: TOM WILSON Contact Phone: Not reported Owner Company: Not reported Operator Address:700 WILLIAMS CIRCLE Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27516- Ownership: Private Operation: Residential Material: #2 FUEL OIL Qty Lost 1: Not reported Qty Recovered 1: Not reported TC3669805.1 s Page 30 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number WILSON RESIDENCE, TOM (Continued) S101573544 Source: Leak -underground Type: Gasoline/diesel Location: Residence Setting: Residential Risk Site: L Site Priority: 10E Priority Code: E Priority Update: Not reported Dem Contact: CED Wells Affected: Not reported Num Affected: 0 Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.9284 Longitude:-79.0574 Latitude Number: Not reported Longitude Number: Not reported Latitude Decimal: Not reported Longitude Decimal: Not reported GPS: 4 Agency: DWM Facility ID: 12051 Last Modified: Not reported Incident Phase: RE NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST: Facility ID: Not reported UST Number: RA-1949 Incident Number: 12051 Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 04/21/1994 Date Occur: 03/29/1994 Cleanup: Not reported Closure Request: Not reported Close Out: Not reported Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L TC3669805.1 s Page 31 Map ID MAP FINDINGS Direction Distance Elevation Site WILSON RESIDENCE, TOM (Continued) Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: 10E Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Not reported MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: Not reported Reel Num: Not reported RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9258-79.0577 Testlat: Not reported EDR ID Number Database(s) EPA ID Number S101573544 Regional Officer Project Mgr: CED Region: Raleigh Company: Not reported Contact Person: TOM WILSON Telephone: Not reported RP Address: 700 WILLIAMS CIRCLE RP City,St,Zip: CHAPEL HILL, NC 27516- RP County: Not reported Comments: CONTAMINATION FOUND UPON REMOVAL OF 550-GAL HEATING OIL UST. UST ON BEDROCK. 04/94 - Soil sampling report submitted: Tank removed 03/14/94. Soils collected directly at UST base (each end of UST) > TPH. Additional sampling conducted at sidewall locations 5' from UST location. Soils < TPH. - CED 5 Min Quad: 144X PIRF: Facility Id: 12051 Date Occurred: 1994-03-29 00:00:00 Date Reported: 1994-04-21 00:00:00 Description Of Incident: TANK REMOVED; SOIL SAMPLE CONFIRMED SOIL CONTAMINATION. Owner/Operator: TOM WILSON Ownership: 4 Operation Type: 3 Type: 4 Location: 7 Site Priority: 10E Priority Update: Not reported Wells Affected Y/N: Not reported Samples Include: 0 7#5 Minute Quad: Not reported 5 Minute Quad: Not reported Pirf/Min Soil: Not reported TC3669805.1 s Page 32 Map ID MAP FINDINGS Direction Distance Elevation Site WILSON RESIDENCE, TOM (Continued) Release Code: Not reported Source Code: Min Soil Err Type: Not reported Cause: Not reported Source: Not reported Ust Number: Not reported Last Modified: Not reported Incident Phase: Response NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported C11 SSW 750 MARTIN LUTHER KING JR BLVD 1/8-1/4 CHAPEL HILL, NC 27514 0.152 mi. 803 ft. Site 1 of 4 in cluster C Relative: EDR Historical Cleaners: Higher Name: TOWN & COUNTRY LAUNDROMAT Year: 2009 Actual: Address: 750 MARTIN LUTHER KING JR BLVD 342 ft. Name: TOWN & COUNTRY LAUNDROMAT Year: 2010 Address: 750 MARTIN LUTHER KING JR BLVD C12 MIDTOWN SHOPS SSW 750 MARTIN LUTHER KING JR BLVD 1/8-1/4 CHAPEL HILL, NC 27514 0.152 mi. 803 ft. Site 2 of 4 in cluster C Relative: DRYCLEANERS: Higher Facility ID: 068-0005 Status: Interim Action Actual: Lat/Long: 35.923751831054-79.05439758300 342 ft. ID Number: 680005 Shopping Center: Midtown Shops Certified Date: 04/27/2005 PM: DT Project Manager: Diane Thomas Phone Number: (919)707-8362 Facility ID: 068-0005 Status: Not reported Lat/Long: 35.923751831054-79.05439758300 ID Number: 680005 EDR ID Number Database(s) EPA ID Number S101573544 EDR US Hist Cleaners 1015093467 N/A DRYCLEANERS S106916911 N/A TC3669805.1 s Page 33 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number MIDTOWN SHOPS (Continued) S106916911 Shopping Center: Midtown Shops Certified Date: Not reported PM: Not reported Project Manager: Not reported Phone Number: Not reported C13 EDR US Hist Cleaners 1015093445 SSW 750 AIRPORT RD N/A 1/8-1/4 CHAPEL HILL, NC 27514 0.152 mi. 803 ft. Site 3 of 4 in cluster C Relative: EDR Historical Cleaners: Higher Name: TOWN & COUNTRY LAUNDROMAT Year: 1999 Actual: Address: 750 AIRPORT RD 342 ft. Name: TOWN & COUNTRY LAUNDROMAT Year: 2000 Address: 750 AIRPORT RD Name: TOWN & COUNTRY LAUNDROMAT Year: 2001 Address: 750 AIRPORT RD Name: TOWN & COUNTRY LAUNDROMAT Year: 2003 Address: 750 AIRPORT RD Name: TOWN & COUNTRY LAUNDROMAT Year: 2004 Address: 750 AIRPORT RD Name: TOWN & COUNTRY LAUNDROMAT Year: 2005 Address: 750 AIRPORT RD C14 NCDSCA 068-0005 (MIDTOWN SHOPS) RCRA-SQG 1010323133 SSW 750 MARTIN L KING JR BLVD, STE NC0991302928 1/8-1/4 CHAPEL HILL, NC 27514 0.152 mi. 803 ft. Site 4 of 4 in cluster C Relative: RCRA-SQG: Higher Date form received by agency:09/10/2010 Facility name: NCDSCA 068-0005 (MIDTOWN SHOPS) Actual: Facility address: 750 MARTIN L KING JR BLVD, STE 342 ft. CHAPEL HILL, NC 27514 EPA ID: NC0991302928 Mailing address: MAIL SERVICE CTR RALEIGH, NC 27699 Contact: DIANNE B THOMAS Contact address: MAIL SERVICE CTR RALEIGH, NC 27699 Contact country: US Contact telephone: 919-508-8483 TC3669805.1 s Page 34 Map ID Direction Distance Elevation MAP FINDINGS Site EDR ID Number Database(s) EPA ID Number NCDSCA 068-0005 (MIDTOWN SHOPS) (Continued) Contact email: DIANNE.THOMAS@NCDENR.GOV EPA Region: 04 Classification: Small Small Quantity Generator Description: Handler: generates more than 100 and less than 1000 kg of hazardous waste during any calendar month and accumulates less than 6000 kg of hazardous waste at any time; or generates 100 kg or less of hazardous waste during any calendar month, and accumulates more than 1000 kg of hazardous waste at any time Owner/Operator Summary Owner/operator name: MIDTOWN SHOPS, LLC Owner/operator address: CLOISTER COURT, STE 114 CHAPEL HILL, NC 27514 Owner/operator country: US Owner/operator telephone: 919-508-8483 Legal status: Private Owner/Operator Type: Owner Owner/Op start date: 01/01/1988 Owner/Op end date: Not reported Owner/operator name: PETITIONER(S) FOR DSCA SITE ID 068-0005 Owner/operator address: MAIL SERVICE CTR RALEIGH, NC 27699 Owner/operator country: US Owner/operator telephone: 919-508-8483 Legal status: Private Owner/Operator Type: Operator Owner/Op start date: 04/27/2005 Owner/Op end date: Not reported Handler Activities Summary: U.S. importer of hazardous waste: No Mixed waste (haz. and radioactive): No Recycler of hazardous waste: No Transporter of hazardous waste: No Treater, storer or disposer of HW: No Underground injection activity: No On -site burner exemption: No Furnace exemption: No Used oil fuel burner: No Used oil processor: No User oil refiner: No Used oil fuel marketer to burner: No Used oil Specification marketer: No Used oil transfer facility: No Used oil transporter: No Historical Generators: Date form received by agency:03/01/2010 Facility name: NCDSCA 068-0005 (MIDTOWN SHOPS) Site name: NCDSCA 068-0005(MIDTOWN SHOPS) Classification: Large Quantity Generator Date form received by agency:02/22/2010 Facility name: NCDSCA 068-0005 (MIDTOWN SHOPS) Classification: Large Quantity Generator 1010323133 TC3669805.1 s Page 35 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number NCDSCA 068-0005 (MIDTOWN SHOPS) (Continued) 1010323133 Date form received by agency:07/05/2009 Facility name: NCDSCA 068-0005 (MIDTOWN SHOPS) Classification: Large Quantity Generator Date form received by agency:08/07/2006 Facility name: NCDSCA 068-0005 (MIDTOWN SHOPS) Classification: Small Quantity Generator Date form received by agency:11/10/2005 Facility name: NCDSCA 068-0005 (MIDTOWN SHOPS) Site name: NCDSCA SITE # 68-0005 (MIDTOWN SHOPS) Classification: Small Quantity Generator Hazardous Waste Summary Waste code: F002 Waste name: THE FOLLOWING SPENT HALOGENATED SOLVENTS: TETRACHLOROETHYLENE, METHYLENE CHLORIDE, TRICHLOROETHYLENE, 1,1,1-TRICHLOROETHANE, CHLOROBENZENE, 1,1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE, ORTHO-DICHLOROBENZENE, TRICHLOROFLUOROMETHANE, AND 1,1,2-TRICHLOROETHANE; ALL SPENT SOLVENT MIXTURES/BLENDS CONTAINING, BEFORE USE, A TOTAL OF TEN PERCENT OR MORE (BY VOLUME) OF ONE OR MORE OF THE ABOVE HALOGENATED SOLVENTS OR THOSE LISTED IN F001, F004, OR F005, AND STILL BOTTOMS FROM THE RECOVERY OF THESE SPENT SOLVENTS AND SPENT SOLVENT MIXTURES. Violation Status: No violations found 15 WILLIAMS RES UST (ELIZ ET AL) LUST S110629990 NE 32 MT. BOLUS RD LUST TRUST N/A 1/8-1/4 CHAPEL HILL, NC 27514 0.188 mi. 991 ft. Relative: LUST: Higher Facility ID: Not reported UST Number: RA-6737 Actual: Incident Number: 33891 435 ft. Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 08/27/2010 Date Occur: 07/06/2010 Cleanup: Not reported Closure Request: Not reported Close Out: 12/13/2010 Level Of Soil Cleanup Achieved: Soil to Groundwater Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: U Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Residential TC3669805.1 s Page 36 Map ID MAP FINDINGS Direction Distance Elevation Site WILLIAMS RES UST (ELIZ ET AL) (Continued) MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Cleanups to 2L.0202 standards PETOPT: 4 RPL: False CD Num: 0 Reel Num: 0 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9278-79.0461 Testlat: Not reported EDR ID Number Database(s) EPA ID Number S110629990 Regional Officer Project Mgr: DMD Region: Raleigh Company: Not reported Contact Person: ELIZABETH WILLIAMS ET AL Telephone: 9196010369 RP Address: 1321 FOUR WINDS DR RP City,St,Zip: RALEIGH, NC 27615 RP County: Not reported Comments: 550 GAL RES UST AND SOIL EXCAVATED 7/6/10. TPH DRO AT 4390 MG/KG AT 6.5 FT. MAX EXCAV DEPTH 13; RESULTS PENDING.////AFTER REMOVING 91 TONS, SOIL > RES MSCC////DRILLED TO 65' AND STOPPED PER INSTRUCTION FROM INCIDENT MGR. NO FP OR GW ENCOUNTERED. AS NO WELLS WITHIN 1000 RADIUS, NFA FOLLOWING PUB NOTICE FOR SOIL AND NRP GW.DMD,9.24.10////NRP for soil & GW. -MRP///PER TELECON WITH ELIZ WILLIAMS, 10-25-10, SHE AND HEIRS INTEND INSTEAD TO TRY DIGGING OUT SO THAT NRP WILL HOPEFULLY NOT BE NECESSARY. MEANWHILE, THEY HAVE INSTRUCTED TERRAQUEST NOT TO FILE THE APPROVED NRP - DMD, 10-25-10/// PN COMPLETED. DMD,10-26-10////FOLLOWING ADDITIONAL OVEREXCAVATION OF 60.35 TONSIN OCTOBER 2010, SAMPLES WERE COLLECTED AND ANALYZED BY 8260, 8270 AND VPH/EPH. RESULTS INDICATED NO CONTAMINATION ABOVE STG OR RES MSCCS; THEREFORE, NFA. DMD,12/13/10//// 5 Min Quad: Not reported PIRF: Facility Id: 33891 Date Occurred: 2010-07-06 00:00:00 Date Reported: 2010-08-27 00:00:00 Description Of Incident: 550 GAL RES UST AND SOIL EXCAVATED 7/6/10. TPH DRO AT 4390 MG/KG AT 6.5 FT. MAX EXCAV DEPTH 13; RESULTS PENDING. Owner/Operator: Not reported Ownership: 4 Operation Type: 3 Type: 4 Location: 7 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: Y TC3669805.1 s Page 37 Map ID Direction Distance Elevation Site WILLIAMS RES UST (ELIZ ET AL) (Continued) MAP FINDINGS EDR ID Number Database(s) EPA ID Number 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: 3 Source: A Ust Number: P Last Modified: 2010-12-13 00:00:00 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: Facility ID: Not reported Site ID: 33891 Site Note: RIF on file. Noncommercial; 100% eligible; $0 deductible.[CGS 3/3/11] Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 C;lirk this by perlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. 16 BRITTON PROPERTY IMD West 726 BRADLEY ROAD LUST 1/8-1/4 CHAPEL HILL, NC LUST TRUST 0.213 mi. 1125 ft. Relative: IMD: Higher Region: RAL Facility ID: 23669 Actual: Date Occurred: 6/12/2001 385 ft. Submit Date: 10/29/2001 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: SOIL CONTAMINATION DISCOVERED DURING UST REMOVAL Operator: Not reported Contact Phone: Not reported Owner Company: CHARLES V. BRITTON Operator Address:726 BRADLEY RD. Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27516- Ownership: Private S110629990 S105149944 N/A TC3669805.1 s Page 38 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number BRITTON PROPERTY (Continued) S105149944 Operation: Residential Material: Not reported Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Residence Setting: Residential Risk Site: L Site Priority: U Priority Code: Not reported Priority Update: 11/1/2001 Dem Contact: JFM Wells Affected: No Num Affected: Not reported Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.92833333 Longitude:-79.0575 Latitude Number: 355542 Longitude Number: 790327 Latitude Decimal: 35.9283333333333 Longitude Decimal: 79.0575 GPS: 7 Agency: DWM Facility ID: 23669 Last Modified: 10/29/2001 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST: Facility ID: Not reported UST Number: RA-3954 Incident Number: 23669 Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 08/06/2001 Date Occur: 06/12/2001 Cleanup: 06/12/2001 Closure Request: Not reported Close Out: 11/05/2002 Level Of Soil Cleanup Achieved: Residential Tank Regulated Status: Non Regulated TC3669805.1 s Page 39 Map ID MAP FINDINGS Direction Distance Elevation Site BRITTON PROPERTY (Continued) # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: 06/11/2002 Site Priority: Not reported Phase Of LSA Req: 1 Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in Archives RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: 233 Reel Num: 117 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9286-79.0577 Testlat: Not reported Regional Officer Project Mgr: JFM Region: Raleigh Company: CHARLES V. BRITTON Contact Person: Not reported Telephone: Not reported RP Address: 726 BRADLEY RD. RP City,St,Zip: CHAPEL HILL, NC 27516- RP County: orange Comments: One 280-gal heating oil UST removed on 6/12/01. Approx 225-gal product removed prior to UST closure. Following closure, 1 soil sample collected for analysis of TPH. Release identified, 20-Day report and 24 Hour notice filed. - CED 5 Min Quad: Not reported PIRF: Facility Id: Date Occurred: Date Reported: Description Of Incident: Owner/Operator: Ownership: Operation Type: Type: Location: Site Priority: Priority Update: Wells Affected Y/N: Samples Include: EDR ID Number Database(s) EPA ID Number S105149944 23669 2001-06-12 00:00:00 2001-10-29 00:00:00 SOIL CONTAMINATION DISCOVERED DURING UST REMOVAL CHARLES V. BRITTON 4 3 4 7 U 2001-11-01 00:00:00 N Not reported TC3669805.1 s Page 40 Map ID Direction Distance Elevation Site MAP FINDINGS EDR ID Number Database(s) EPA ID Number BRITTON PROPERTY (Continued) 7#5 Minute Quad: Not reported 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: Not reported Source: C Ust Number: C Last Modified: 2001-10-29 00:00:00 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: Facility ID: Not reported Site ID: 23669 Site Note: Not reported Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 Clink this hgpprlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. D17 RANCER PROPERTY IMD West 712 BRADLEY COURT LUST 1/8-1/4 CHAPEL HILL, NC LUST TRUST 0.244 mi. 1289 ft. Site 1 of 2 in cluster D Relative: IMD: Higher Region: RAL Facility ID: 23664 Actual: Date Occurred: 5/1/2001 371 ft. Submit Date: 10/29/2001 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: SOIL CONTAMINATION DISCOVERED DURING UST REMOVAL Operator: Not reported Contact Phone: Not reported Owner Company: VIOLA J. RANGER Operator Address:2453 WAYFARER COURT Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27514- S105149944 S105149939 N/A TC3669805.1 s Page 41 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number RANCER PROPERTY (Continued) S105149939 Ownership: Private Operation: Residential Material: Not reported Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Residence Setting: Residential Risk Site: L Site Priority: U Priority Code: Not reported Priority Update: 11/1/2001 Dem Contact: MAF Wells Affected: No Num Affected: Not reported Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.55583333 Longitude:-79.03444444 Latitude Number: 353321 Longitude Number: 790204 Latitude Decimal: 35.5558333333333 Longitude Decimal: 79.0344444444444 GPS: 7 Agency: DWM Facility ID: 23664 Last Modified: 10/29/2001 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST: Facility ID: Not reported UST Number: RA-3949 Incident Number: 23664 Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 08/15/2001 Date Occur: 05/01/2001 Cleanup: 05/01 /2001 Closure Request: Not reported Close Out: 08/22/2003 Level Of Soil Cleanup Achieved: Residential TC3669805.1 s Page 42 Map ID Direction Distance Elevation Site MAP FINDINGS EDR ID Number Database(s) EPA ID Number RANCER PROPERTY (Continued) Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: 09/24/2001 Site Priority: Not reported Phase Of LSA Req: 1 Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: No Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in Archives RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: 233 Reel Num: 116 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.5559-79.0345 Testlat: Not reported Regional Officer Project Mgr: MAF Region: Raleigh Company: VIOLA J. RANCER Contact Person: Not reported Telephone: Not reported RP Address: 2453 WAYFARER COURT RP City,St,Zip: CHAPEL HILL, NC 27514- RP County: Not reported Comments: 06/13/01 - 20-Day rpt submitted by Cohesion: 1 x 550-gal heating oil UST. 05/1/01 soil collected adj. to UST at a depth of 6' _ > TPH Action Level. On 05/10/01 UST was removed. Approx. 5.45 tons impacted soil removed. 5 soil samples collected following r 5 Min Quad: Not reported PIRF: Facility Id: Date Occurred: Date Reported: Description Of Incident: Owner/Operator: Ownership: Operation Type: Type: Location: Site Priority: Priority Update: Wells Affected Y/N: S105149939 23664 2001-05-07 00:00:00 2001-10-29 00:00:00 SOIL CONTAMINATION DISCOVERED DURING UST REMOVAL VIOLA J. RANCER 4 3 4 7 U 2001-11-01 00:00:00 N TC3669805.1 s Page 43 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number RANCER PROPERTY (Continued) S105149939 Samples Include: Not reported 7#5 Minute Quad: Not reported 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: Not reported Source: C Ust Number: C Last Modified: 2001-10-29 00:00:00 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: Facility ID: Not reported Site ID: 23664 Site Note: Not reported Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 Clink thic h gnarlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. D18 BAXTER ESTATE PROPERTY LUST S109367303 West 710 BRADLEY RD LUST TRUST N/A 1/8-1/4 CHAPEL HILL, NC 27516 0.248 mi. 1309 ft. Site 2 of 2 in cluster D Relative: LUST: Higher Facility ID: Not reported UST Number: RA-6032 Actual: Incident Number: 33569 366 ft. Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 08/21/2008 Date Occur: 08/21/2008 Cleanup: Not reported Closure Request: Not reported Close Out: 12/12/2008 Level Of Soil Cleanup Achieved: Residential TC3669805.1 s Page 44 Map ID MAP FINDINGS Direction Distance Elevation Site BAXTER ESTATE PROPERTY (Continued) Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: 02/20/2009 Release Detection: 0 Current Status: File Located in House RBCA GW: Cleanups to alternate standards PETOPT: 4 RPL: False CD Num: 0 Reel Num: 0 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9264-79.0576 Testlat: Not reported EDR ID Number Database(s) EPA ID Number S109367303 Regional Officer Project Mgr: DMD Region: Raleigh Company: Joan Baxter Estate Contact Person: James Baxter, Executor Telephone: 3155325061 RP Address: 7909 Kreeger Dr, #114 RP City,St,Zip: Adelphi, MD 20783 RP County: Not reported Comments: 550 GAL RESIDENTIAL HEATING OIL UST AND 50 TONS PETROL-CONTAM SOIL REMOVED BY CEDAR ROCK ENVIRONMENTAL PER UST-61 24-HR RELEASE NOTIF -DMD, 9/8/08////IAA report indicates bedrock encountered and residual soil contam exceeds residential MSCCs. Consultant recommends Low Risk NFA, aband of MW1, soil and gw NRP, and public notice -DMD, 12/12/08.////Public notice receipt copies received for closeout-dmd,3/13/09./// 5 Min Quad: Not reported PIRF: Facility Id: 33569 Date Occurred: 2008-08-21 00:00:00 Date Reported: 2008-08-21 00:00:00 Description Of Incident: 550 GAL RESIDENTIAL HEATING OIL UST AND 50 TONS PETROL-CONTAM SOIL REMOVED BY CEDAR ROCK ENVIRONMENTAL PER UST-61 24-HR RELEASE NOTIF -DMD, 9/8/08//// Owner/Operator: Not reported Ownership: 4 Operation Type: 3 TC3669805.1 s Page 45 Map ID MAP FINDINGS Direction Distance Elevation Site BAXTER ESTATE PROPERTY (Continued) Type: 4 Location: 7 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: N 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: 3 Source: A Ust Number: P Last Modified: Not reported Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: Facility ID: Not reported Site ID: 33569 Site Note: Noncommercial; 100% eligible; $0 deductible.[CGS 2/2/09] Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 Clink this hgpprlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. 19 PAGE ESTATE (EDITH) NW 120 JUSTICE STREET 1/4-1/2 CHAPEL HILL, NC 27516 0.253 mi. 1334 ft. Relative: LUST: Higher Facility ID: Not reported UST Number: RA-5830 Actual: Incident Number: 33386 469 ft. Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 10/03/2007 EDR ID Number Database(s) EPA ID Number S109367303 LUST S108852030 LUST TRUST N/A TC3669805.1 s Page 46 Map ID Direction Distance Elevation Site MAP FINDINGS EDR ID Number Database(s) EPA ID Number PAGE ESTATE (EDITH) (Continued) Date Occur: 09/25/2007 Cleanup: Not reported Closure Request: Not reported Close Out: 01/08/2008 Level Of Soil Cleanup Achieved: Industrial/Commercial Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: 1 Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: 02/01/2008 Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: 0 Reel Num: 0 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9300-79.0567 Testlat: Not reported Regional Officer Project Mgr: CED Region: Raleigh Company: Edith Page Estate Contact Person: James Page (Executor) Telephone: 9199421568 RP Address: 120 Justice Street RP City,St,Zip: Chapel Hill, NC 27516 RP County: Not reported Comments: 09/25/07 - 24-Hour Release Reporting form submitted. - CED //// 10/03/07 - 20-Day rpt submitted by Cedar Rock: Release discovered on 09/25/07 following removal of 550-gal heating oil UST. No Fp. Approx. 18.54 tons impacted soil removed. Soils pending lab data. - CED //// 10/15/07 - Initial Abatement rpt submitted by Cedar Rock: Soils > Res MSCCs and bedrock encountered. Recommends LSA. - CED //// Source is UST. 10/17/07 - LSA NORR issued. - CED //// 12/12/07 - LSA submitted: 1 inactive WSW within 1000'. No WHP. Bolin Creek -1250' NE. Low risk. Bedrock -9' bls. MW installed to 43' bls, DRY. Recommends NFA with PN???/ Soils > Res MSCCs so NRP Needed- CED /// 12/18/07 - NRP NORR Issued for soil only. - CED //// 01/08/08 - NRP for soil only received for signature. NFA Issued with PN. - CED //// 2/6/08 - Certified copy of NRP received. - CED //// 02/26/08 - PN received. - S108852030 TC3669805.1 s Page 47 Map ID Direction Distance Elevation Site MAP FINDINGS EDR ID Number Database(s) EPA ID Number PAGE ESTATE (EDITH) (Continued) S108852030 C E D //// 5 Min Quad: Not reported PIRF: Facility Id: 33386 Date Occurred: 2007-09-25 00:00:00 Date Reported: 2007-10-03 00:00:00 Description Of Incident: release discovered following removal of 550-al heating oil UST. Source is UST. Owner/Operator: Not reported Ownership: 4 Operation Type: 3 Type: 4 Location: 1 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: Y 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: Not reported Source: Not reported Ust Number: P Last Modified: Not reported Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: Facility ID: Not reported Site ID: 33386 Site Note: Noncommercial; 100% eligible; $0 deductible.[CGS 11/26/07] Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 Click this hyperlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. TC3669805.1 s Page 48 Map ID Direction Distance Elevation Site MAP FINDINGS EDR ID Number Database(s) EPA ID Number E20 HUNT, EMORY RESIDENCE IMD S106406522 SE 304 LONE PINE ROAD N/A 1/4-1/2 CHAPEL HILL, NC 0.268 mi. 1417 ft. Site 1 of 2 in cluster E Relative: IMD: Higher Region: Not reported Facility ID: 26598 Actual: Date Occurred: 3/18/2004 342 ft. Submit Date: 3/18/2004 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: HEATING OIL RELEASE Operator: C/O BETH HUNT Contact Phone: 5413427351 Owner Company: EMORY S. HUNT Operator Address:2650 CRESTA DE RUTA STREET Operator City: EUGENE Oper City,St,Zip: EUGENE, OR 97403- Ownership: Private Operation: Residential Material: Not reported Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Residence Setting: Not reported Risk Site: L Site Priority: Not reported Priority Code: Not reported Priority Update: Not reported Dem Contact: MAF Wells Affected: Not reported Num Affected: Not reported Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.55333333 Longitude:-79.0275 Latitude Number: 353312 Longitude Number: 790139 Latitude Decimal: 35.5533333333333 Longitude Decimal: 79.0275 GPS: 7 Agency: DWM Facility ID: 26598 Last Modified: 11/19/2004 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported TC3669805.1 s Page 49 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number HUNT, EMORY RESIDENCE (Continued) S106406522 IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported E21 HUNT RESIDENCE (EMORY) LUST S106495606 SE 304 LONE PINE RD LUST TRUST N/A 1/4-1/2 CHAPEL HILL, NC 0.268 mi. 1417 ft. Site 2 of 2 in cluster E Relative: LUST: Higher Facility ID: Not reported UST Number: RA-5046 Actual: Incident Number: 26598 342 ft. Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 03/18/2004 Date Occur: 03/18/2004 Cleanup: Not reported Closure Request: Not reported Close Out: 11/19/2004 Level Of Soil Cleanup Achieved: Soil to Groundwater Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: 1 Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: No Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in Archives RBCA GW: Cleanups to 2L.0202 standards PETOPT: 4 RPL: False CD Num: 264 Reel Num: 39 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.5534-79.0275 Testlat: Not reported Regional Officer Project Mgr: MAF Region: Raleigh Company: EMORY S. HUNT TC3669805.1 s Page 50 Map ID Direction Distance Elevation MAP FINDINGS Site EDR ID Number Database(s) EPA ID Number HUNT RESIDENCE (EMORY) (Continued) Contact Person: C/O BETH HUNT Telephone: 5413427351 RP Address: 2650 CRESTA DE RUTA STREET RP City,St,Zip: EUGENE, OR 97403- RP County: Not reported Comments: 03/18/04 - 24-Hour Reporting Release Reporting Form submitted. - CED //// 04/07/04 - 20-Day Rpt Submitted by Cedar Rock: Release discovered on 03/18/04 following removal of 550-gal heating oil UST. Approx. 26.21 tons impacted soil removed. Soils > Res MSCCs. - CED //// 05/27/04 - LSA submitted by Cedar Rock: Irrigation well within 300' upgradient. Bolin Creek —550'. No WHP. MW installed to 50' bls - dry. Recommends Low risk with SAR. - CED //// 09/10/04 - SAR submitted by Cedar Rock: Approx. 60 tons impacted soil > Res MSCCs. remains on -site. Recommends excavation for remediation. - CED 11/05/04 - SC Rpt submitted by Cedar Rock: Approx. 22.87 tons impacted soil removed. Soils <S-GW MSCCs. Recommends NFA. - CED //// 11/19/04 - NFA Issued. - CED 5 Min Quad: Not reported PIRF: Facility Id: 26598 Date Occurred: 2004-03-18 00:00:00 Date Reported: 2004-03-18 00:00:00 Description Of Incident: HEATING OIL RELEASE Owner/Operator: Not reported Ownership: 4 Operation Type: 3 Type: 4 Location: 7 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: Not reported Samples Include: Not reported 7#5 Minute Quad: Not reported 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: Not reported Source: C Ust Number: C Last Modified: 2004-11-19 00:00:00 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: S106495606 TC3669805.1 s Page 51 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number HUNT RESIDENCE (EMORY) (Continued) S106495606 Facility ID: Not reported Site ID: 26598 Site Note: Not reported Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 100000 Sum 3rd Party Amt Applied: 0 Click this hypprlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. 22 LAWLER PROPERTY UST LUST S110629988 SSE 421 HILLSBOROUGH ST LUST TRUST N/A 1/4-1/2 CHAPEL HILL, NC 27514 0.361 mi. 1906 ft. Relative: LUST Higher Facility ID: Not reported UST Number: RA-6735 Actual: Incident Number: 33889 381 ft. Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 08/27/2010 Date Occur: 05/27/2010 Cleanup: 05/27/2010 Closure Request: Not reported Close Out: Not reported Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: 0 Reel Num: 0 RPOW: False RPOP: False TC3669805.1 s Page 52 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number LAWLER PROPERTY UST (Continued) S110629988 Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9193-79.0518 Testlat: Not reported Regional Officer Project Mgr: WER Region: Raleigh Company: LAWLER DEVELOPMENTAL GRP LLC Contact Person: LESLIE LAWLER Telephone: 9194348498 RP Address: 420 WESTWOOD DR RP City,St,Zip: CHAPEL HILL, NC 27516 RP County: Not reported Comments: 550 GAL RES HEATING OIL UST AND CONTAMINATED SOIL REMOVED 5/27/10. TPH DRO AT 16,400 MG/KG DIRECTLY BENEATH TANK. EXCAVATED TO 12 MAX DEPTH. RESULTS PENDING. DMD,8/30/10 ////excav 33.8 tons soil along foundation; >stg; Isa reqd. dmd, 1-19-11 //// 5 Min Quad: Not reported PIRF: Facility Id: 33889 Date Occurred: 2010-05-27 00:00:00 Date Reported: 2010-08-27 00:00:00 Description Of Incident: 550 GAL RES HEATING OIL UST AND CONTAMINATED SOIL REMOVED 5/27/10. Owner/Operator: Not reported Ownership: 4 Operation Type: 3 Type: 4 Location: 7 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: Y 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: 3 Source: A Ust Number: P Last Modified: Not reported Incident Phase: Not reported NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: TC3669805.1 s Page 53 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number LAWLER PROPERTY UST (Continued) S110629988 Facility ID: Not reported Site ID: 33889 Site Note: Noncommercial; 100% eligible; $0 deductible.[CGS 6/22/11] Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 Click this hypprlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. F23 UNC-CH SERVICE STATION IMD 0003092093 NW 109 AIRPORT DRIVE / CB #1800 LUST N/A 1/4-1/2 CHAPEL HILL, NC 27599 LUST TRUST 0.417 mi. UST 2204 ft. Site 1 of 2 in cluster F Financial Assurance Relative: IMD: Higher Region: RAL Facility ID: 14054 Actual: Date Occurred: 11/21/1994 479 ft. Submit Date: 5/24/1995 GW Contam: Yes, Groundwater Contamination has been detected Soil Contam: No Incident Desc: UST FAILED TANK TIGHTNESS TEST. SOIL CONTAM. 751 PPM OF TPH. Operator: ROBERT WALTON Contact Phone: 919-962-6666 Owner Company: UNIVERSITY OF NORTH CAROLINA Operator Address:212 FINLEY GOLF COURSE RD Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27514- Ownership: State Operation: Educational/Religious Material: GASOLINE Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Facility Setting: Urban Risk Site: I Site Priority: 20E Priority Code: L Priority Update: 4/16/1998 Dem Contact: MAF Wells Affected: No Num Affected: 0 Wells Contam: Not reported Sampled By: Responsible Parties Samples Include: Soil Samples 7.5 Min Quad: Not reported 5 Min Quad: 144X Latitude: 35.9325 Longitude:-79.05861111 Latitude Number: 355557 Longitude Number: 790331 TC3669805.1 s Page 54 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number UNC-CH SERVICE STATION (Continued) 0003092093 Latitude Decimal: 35.9325 Longitude Decimal: 79.0586111111111 GPS: NOD Agency: DWM Facility ID: 14054 Last Modified: Not reported Incident Phase: RE NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST: Facility ID: 00-0-000 UST Number: RA-2216 Incident Number: 14054 Contamination Type: Groundwater/Both Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 11/21/1994 Date Occur: 11/21/1994 Cleanup: Not reported Closure Request: Not reported Close Out: Not reported Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: COMMERCIAL Risk Classification: I Risk Class Based On Review: I Corrective Action Plan Type: NT NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: 20E Phase Of LSA Req: Not reported Site Risk Reason: FG Land Use: Not reported MTBE: No MTBE1: Yes Flag: Yes Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 3 RPL: False CD Num: Not reported Reel Num: Not reported RPOW: False TC3669805.1 s Page 55 Map ID Direction Distance Elevation MAP FINDINGS Site UNC-CH SERVICE STATION (Continued) RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.5557-79.0331 Testlat: Not reported EDR ID Number Database(s) EPA ID Number 0003092093 Regional Officer Project Mgr: DMD Region: Raleigh Company: UNC ENVIRON, HEALTH & SAFETY Contact Person: LARRY DAW Telephone: 919-962-6666 RP Address: 1120 ESTES DRIVE EXTENSION RP City,St,Zip: CHAPEL HILL, NC 275991650 RP County: Not reported Comments: 05/13/2002 - review of most recent Monitoring Report, dated, 9/2001 indicates a CAP was submitted in 1996 and since then 5 Natural Attenuation Monitoring Reports have been submitted; In the most recent event (9/2001) 2L levels were exceeded in GW; TW1 & 2 exceeded GCL's; Trend thusfar is a decrease in overall contaminant levels, but, increase in benzene & MTBE levels; Also, MW7 is showing contam's and hasn't in the past; Plume extends 250' to NE; No Free Product; GW flow is to the NE; Consultant recommendations are to proceed with N.A. Monitoring and FP checks; No receptors; Contaminant type- Gas; -MAZ 8/5/2002 - MR review .... TW1 & 2 contained FP (5, 1.75'); MW2 & TW3 was > 2L; FP recovery socks were placed in TW1 & 2; Consultant suggests Mobile Multi -phase Extraction (MMPE) or AFVR to address FP; Once FP is eliminated site can be lowered to Low risk and possibly closed out; -MAZ 5/2003 - MR Review ..... (event 6/24/2003) - MW2-7 & TW1-3 were sampled; sample methods used- 602; No FP in any wells this event; MW2, 3, TW2, 3 > 2L; Only one constituent in 1 well is > GCL - - - TW2 benzene is 5700 ppb (2L - 5000 ppb); Continue with Natural Attenuation; -MAF 5/19/2005 - MW abandonment report rec'd for MW4; -MAF ////RE -SENDING FPR NORR TO LARRY DAW AT NEW ADDRESS (HB 2498)-DMD,12.1.09H//Sent Resume Funding NORR for Intermediate Risk Sites, DMD, 9.1.10//// 5 Min Quad: 144x PIRF: Facility Id: 14054 Date Occurred: 1994-11-21 00:00:00 Date Reported: 1995-05-24 00:00:00 Description Of Incident: UST FAILED TANK TIGHTNESS TEST. SOIL CONTAM. 751 PPM OF TPH. Owner/Operator: ROBERT WALTON Ownership: 7 Operation Type: 4 Type: 3 Location: 1 Site Priority: 20E Priority Update: 1998-04-16 00:00:00 Wells Affected Y/N: N Samples Include: 0 7#5 Minute Quad: 3 5 Minute Quad: 2 Pirf/Min Soil: Not reported Release Code: 144X Source Code: Pirf Err Type: Not reported Cause: Not reported TC3669805.1 s Page 56 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number UNC-CH SERVICE STATION (Continued) 0003092093 Source: Not reported Ust Number: Not reported Last Modified: Not reported Incident Phase: Response NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: Facility ID: 0-002149 Site ID: 14054 Site Note: Not reported Site Eligible?: True Commercial Find: 100% Commercial Priority Rank: Low Deductable Amount: 20000 3rd Party Deductable Amt: 100000 Sum 3rd Party Amt Applied: 0 C;lirk this by P'� rlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. UST: Facility Id: 00-0-0000034543 Contact: UNIVERSITY OF NC AT CHAPEL HILL Contact Address1: 1120 ESTES DR/EXTENSION CB 1650 Contact Address2: Not reported Contact City/State/Zip: CHAPEL HILL, NC 27599-1650 FIPS County Desc: Orange Latitude: 35.93238 Longitude: -79.05804 Tank Id: 1 Tank Status: Current Installed Date: 01/04/1996 Perm Close Date: Not reported Product Key: 3 Product Name: Gasoline, Gas Mix Tank Capacity: 10000 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: 0 Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel/FRP Piping Construction: Single Wall FRP Piping System Key: Unknown TC3669805.1 s Page 57 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number UNC-CH SERVICE STATION (Continued) 0003092093 Other CP Tank: Not reported Tank Id: 2 Tank Status: Current Installed Date: 01/02/1996 Perm Close Date: Not reported Product Key: 14 Product Name: Oil, New/Used/Mix Tank Capacity: 550 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: 0 Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel/FRP Piping Construction: SW Flexible Piping Piping System Key: Unknown Other CP Tank: Not reported NC Financial Assurance 1: Facility ID: 0-034543 Region: 1 Financial Responsibility Code: Not reported Financial Responsibility Desc: STATE FUND F24 UNC GILES F. HORNEY BUILDING LUST S108493142 NW 103 AIRPORT DRIVE N/A 1/4-1/2 CHAPEL HILL, NC 27516 0.427 mi. 2253 ft. Site 2 of 2 in cluster F Relative: LUST: Higher Facility ID: 00-0-000 UST Number: RA-5730 Actual: Incident Number: 33255 482 ft. Contamination Type: Groundwater/Both Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 09/27/2006 Date Occur: 09/26/2006 Cleanup: 09/26/2006 Closure Request: Not reported Close Out: Not reported Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: 1 Site Risk Reason: Not reported TC3669805.1 s Page 58 Map ID MAP FINDINGS Direction Distance Elevation Site UNC GILES F. HORNEY BUILDING (Continued) Land Use: Residential MTBE: No MTBE1: Yes Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 3 RPL: False CD Num: 0 Reel Num: 0 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9324-79.0582 Testlat: Not reported EDR ID Number Database(s) EPA ID Number S108493142 Regional Officer Project Mgr: CED Region: Raleigh Company: UNC Chapel Hill Contact Person: J. Laurence Daw Telephone: 9199626666 RP Address: 1120 Estes Drive Extension RP City,St,Zip: Chapel Hill, NC 275991650 RP County: Not reported Comments: 12/20/06 - UST Clo rpt submitted by Terraquest: Release discovered on 09/26/06 following removal of 10K heating oil UST. UST was replaced with 4K Heating oil AST. GW flow to N. Soils > TPH. Approx. 30.88 tons impacted soil. UST located on concrete slab. Soil samples on southern edge > S-GW MSCCs and MADEP > Res MSCCs. Recommends LSA. - CED //// 02/08/08 - LSA submitted by Terraquest: No WSW, no SWB, no WHP. Low risk classification. MW installed to 26' bls. No soil collected from boring. DTW=22.43' bls. GW > 2L (benz, PCE, Aromatics). MTBE detected < 2L. Benz and MTBE could be identified from gas release —150' SW from Inc #14054. Recommends reclassification from Res to Ind/Comm and NFA. - CED 5 Min Quad: Not reported PIRF: Facility Id: 33255 Date Occurred: 2006-09-26 00:00:00 Date Reported: 2006-12-20 00:00:00 Description Of Incident: Release discovered following removal of 10,000-gal heating oil UST on 09/26/06. Owner/Operator: Not reported Ownership: 4 Operation Type: 6 Type: 4 Location: 1 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: n Samples Include: Not reported 7#5 Minute Quad: y 5 Minute Quad: Not reported TC3669805.1 s Page 59 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number UNC GILES F. HORNEY BUILDING (Continued) S108493142 Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: Not reported Source: Not reported Ust Number: P Last Modified: Not reported Incident Phase: Not reported NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported G25 CHAPEL HILL TRANSIT IMD S106896240 NNW MUNICIPAL DR. LUST N/A 1/4-1/2 CHAPEL HILL, NC 0.463 mi. 2443 ft. Site 1 of 6 in cluster G Relative: IMD: Higher Region: RAL Facility ID: 4005 Actual: Date Occurred: 8/3/1992 458 ft. Submit Date: 2/8/1989 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: WASTE OIL TANK WAS TAKING ON WATER, AND DURING EXCAVATION TO PULL FILL PIPE CONTAM. SOIL WAS DISCOVERED. Operator: DONALD WELLS Contact Phone: Not reported Owner Company: CHAPEL HILL TRANSIT MAINT. FAC Operator Address:MUNICIPAL DR. Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27516- Ownership: Municipal Operation: Commercial Material: WASTE OIL Qty Lost 1: Not reported Qty Recovered 1: LINK Source: Leak -underground Type: Gasoline/diesel Location: Facility Setting: Urban Risk Site: L Site Priority: 50 Priority Code: Not reported Priority Update: Not reported Dem Contact: MAF Wells Affected: No Num Affected: 0 TC3669805.1 s Page 60 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number CHAPEL HILL TRANSIT (Continued) S106896240 Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.93805555 Longitude: -79.05666666 Latitude Number: 355617 Longitude Number: 790324 Latitude Decimal: 35.9380555555556 Longitude Decimal: 79.0566666666667 GPS: 7 Agency: DWM Facility ID: 4005 Last Modified: Not reported Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST: Facility ID: Not reported UST Number: RA-636 Incident Number: 4005 Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 11/12/1992 Date Occur: 08/03/1992 Cleanup: 01/20/1989 Closure Request: Not reported Close Out: 05/17/2005 Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: 50 Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Not reported MTBE: No MTBE1: Unknown Flag: No Flag1: No TC3669805.1 s Page 61 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number CHAPEL HILL TRANSIT (Continued) S106896240 LUR Filed: Not reported Release Detection: 0 Current Status: File Located in Archives RBCA GW: Not reported PETOPT: 5 RPL: False CD Num: 306 Reel Num: 198 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9380-79.0566 Testlat: Not reported Regional Officer Project Mgr: MAF Region: Raleigh Company: CHAPEL HILL TRANSIT MAINT. FAC Contact Person: DONALD WELLS Telephone: Not reported RP Address: MUNICIPAL DR. RP City,St,Zip: CHAPEL HILL, NC 27516- RP County: Not reported Comments: WASTE OIL TANK WAS TAKING ON WATER, AND DURING EXCAVATION TO PULL FILL PIPE CONTAM. SOIL WAS DISCOVE 5 Min Quad: Not reported PIRF: Facility Id: 4005 Date Occurred: 1989-01-20 00:00:00 Date Reported: 1989-02-08 00:00:00 Description Of Incident: WASTE OIL TANK WAS TAKING ON WATER, AND DURING EXCAVATION TO PULL FILL PIPE CONTAM. SOIL WAS DISCOVERED. Owner/Operator: CHAPEL HILL TRANSIT Ownership: 1 Operation Type: 6 Type: 5 Location: 1 Site Priority: 50 Priority Update: Not reported Wells Affected Y/N: N Samples Include: 0 7#5 Minute Quad: Not reported 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Pirf Err Type: Not reported Cause: Not reported Source: Not reported Ust Number: Not reported Last Modified: Not reported Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported TC3669805.1 s Page 62 Map ID Direction Distance Elevation Site MAP FINDINGS EDR ID Number Database(s) EPA ID Number CHAPEL HILL TRANSIT (Continued) S106896240 Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported 26 HANSEN REVOCABLE TRUST PROPERTY LUST S109836986 ESE 357 TENNEY CIRCLE LUST TRUST N/A 1/4-1/2 CHAPEL HILL, NC 0.467 mi. 2464 ft. Relative: LUST Higher Facility ID: Not reported UST Number: RA-6125 Actual: Incident Number: 33666 439 ft. Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 05/07/2009 Date Occur: 05/07/2009 Cleanup: Not reported Closure Request: Not reported Close Out: 06/23/2009 Level Of Soil Cleanup Achieved: Industrial/Commercial Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: H Risk Class Based On Review: H Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: 06/30/2009 Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: 0 Reel Num: 0 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9208-79.0430 Testlat: Not reported Regional Officer Project Mgr: DMD TC3669805.1 s Page 63 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number HANSEN REVOCABLE TRUST PROPERTY (Continued) S109836986 Region: Raleigh Company: NANCY HANSEN REVOCABLE TRUST Contact Person: NANCY HANSEN Telephone: 7043078102 RP Address: 2412 HOUSTON BRANCH RD RP City,St,Zip: CHARLOTTE, NC 28270 RP County: Not reported Comments: Removed 550 gal residential heating oil UST and 28.49 tons contaminated soil on 5/7/09. Observed physical evidence of oil release. Collected soil samples. Results pending--- DMD,6/3/09.//// IAR indicated samples collected following tank and contaminated soil removal exceeded S-T-G and residential MSCCs in two of five sample locations (pit center and east wall nearest house). Excavation reached a depth of 11.5 ft bls. No petroleum free product or groundwater was encountered. LSA is to be conducted as required due to contaminant levels--- DMD,6/3/09.////MW1 DRILLED TO 40' BLS: GW NOT ENCOUNTERED AND NO CONTAM IN 20' AND 30' SOIL SAMPLES; ALSO, NEAREST WELL IS 950' AWAY; THEREFORE, RECOMMENDING NFA-DMD,6/17/09 5 Min Quad: Not reported PIRF: Facility Id: 33666 Date Occurred: 2009-05-07 00:00:00 Date Reported: 2009-05-07 00:00:00 Description Of Incident: 550 GAL RESIDENTIAL HEATING OIL TANK RELEASE Owner/Operator: Not reported Ownership: 4 Operation Type: 3 Type: 4 Location: 7 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: Y 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: 3 Source: A Ust Number: P Last Modified: Not reported Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported TC3669805.1 s Page 64 Map ID Direction Distance Elevation MAP FINDINGS Site HANSEN REVOCABLE TRUST PROPERTY (Continued) EDR ID Number Database(s) EPA ID Number LUST TRUST: Facility ID: Not reported Site ID: 33666 Site Note: Noncommercial; $5,000 deductible; eligible for reimbursement of 90% of costs that exceed the $5,000 deductible.[CGS 8/31/09] Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 5000 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 Clink this h yperlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. G27 CHAPEL HILL TRANSIT GARAGE HYD NNW 1089 MARTIN LUTHER KING JR BL 1/4-1/2 CHAPEL HILL, NC 27514 0.473 mi. 2500 ft. Site 2 of 6 in cluster G Relative: LAST: Higher Facility ID: Not reported UST Number: RA-92020 Actual: Incident Number: 92020 458 ft. Contamination Type: Source Type: 14 Product Type: P Date Reported: 10/23/2007 Date Occur: 07/30/2007 Cleanup: Not reported Closure Request: Not reported Close Out: 10/24/2007 Level Of Soil Cleanup Achieved: Tank Regulated Status: # Of Supply Wells: 0 Commercial/NonCommercial UST Site: Risk Classification: Risk Class Based On Review: Corrective Action Plan Type: NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Not reported MTBE: No MTBE1: No Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: C RBCA GW: Not reported PETOPT: 3 RPL: False CD Num: 0 SL S3 R C L L Not reported S109836986 LAST S110629340 N/A TC3669805.1 s Page 65 Map ID MAP FINDINGS Direction Distance Elevation Site CHAPEL HILL TRANSIT GARAGE HYD (Continued) Reel Num: 0 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long: 35567933 Lat/Long Decimal: 35.93763 79.059533 Testlat: Not reported EDR ID Number Database(s) EPA ID Number S110629340 Regional Officer Project Mgr: JFM Region: RAIL Company: Town of Chapel Hill Contact Person: JOHN NEWARK Telephone: 9196129561 RP Address: 405 MARTIN LUTHER KING JR BLVD RP City,St,Zip: Chapel Hill, NC 27514 RP County: Not reported Comments: Hydraulic Lift removed, Post excavation samples < action levels. 10/24/2007, JFM/// 5 Min Quad: Not reported PIRF: Facility Id: 92020 Date Occurred: 7/30/2007 Date Reported: 10/24/2007 Description Of Incident: Hydraulic Lift removed, 10/24/2007, JFM/// Owner/Operator: Not reported Ownership: 1 Operation Type: 3 Type: 5 Location: 1 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: Y 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 9 Cause: Not reported Source: Not reported Ust Number: B Last Modified: Not reported Incident Phase: Not reported NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported Post excavation samples < action levels. TC3669805.1 s Page 66 Map ID Direction Distance Elevation Site MAP FINDINGS EDR ID Number Database(s) EPA ID Number G28 TOWN OF CHAPEL HILL TRANSIT GARAGE NNW 1089 MARTIN LUTHER KING BLVD 1/4-1/2 CHAPEL HILL, NC 27515 0.473 mi. 2500 ft. Site 3 of 6 in cluster G Relative: LUST: Higher Facility ID: 00-0-000 UST Number: RA-5834 Actual: Incident Number: 33389 458 ft. Contamination Type: Groundwater/Both Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 10/23/2007 Date Occur: 08/25/2007 Cleanup: 08/25/2007 Closure Request: Not reported Close Out: Not reported Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: 1 Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Yes Flag: Yes Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 3 RPL: False CD Num: 0 Reel Num: 0 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9376-79.0595 Testlat: Not reported Regional Officer Project Mgr: DMD Region: Raleigh Company: Town of Chapel Hill Contact Person: JOHN NEWARK Telephone: 9196129561 RP Address: 405 MLK Jr Blvd RP City,St,Zip: Chapel Hill, NC 27514 RP County: Not reported Comments: One (01) 20K-gallon diesel, one(01) 10K-gallon gasoline and one (01) LUST S110629979 N/A TC3669805.1 s Page 67 Map ID MAP FINDINGS Direction Distance Elevation Site TOWN OF CHAPEL HILL TRANSIT GARAGE (Continued) 5 Min Quad PIRF: Facility Id: Date Occurred: Date Reported: Description Of Incident: Owner/Operator: Ownership: Operation Type: Type: Location: Site Priority: Priority Update: Wells Affected Y/N: Samples Include: 7#5 Minute Quad: 5 Minute Quad: Pirf/Min Soil: Release Code: Source Code: Err Type: Cause: Source: Ust Number: EDR ID Number Database(s) EPA ID Number S110629979 1 K-gallon oil/water separator removed. 10/24/2007, JFMH/ Low risk site had FP in MW7, but none in nearby surrounding wells MW9,10,and 11. In response removed 169 tons soil to bedrock at and around location of MW7. One sidewall sample was contaminated at a level above the stg but below the res mscc. While there are other contamintated areas at this site under various different incident #s (former ust bas), in order to close the hydraulic lift area, gw analyses from MW9, 10, 11 must first be provided. DMD, 2-6-12 Not reported Last Modified: Incident Phase: NOV Issued: NORR Issued: 45 Day Report: Public Meeting Held: Corrective Action Planned SOC Signed: Reclassification Report: IRS Designation: Closure Request Date: Close-out Report: 33389 2007-08-25 00:00:00 2007-10-24 00:00:00 UST Initial Abatement Action Report. Not reported 6 1 3 1 Not reported Not reported N Not reported Y Not reported Not reported Not reported Not reported 2 3 A P Not reported Not reported Not reported Not reported Not reported Not reported Not reported Not reported Not reported Not reported Not reported Not reported Facility ID: Not reported UST Number: RA-6723 Incident Number: 33879 Contamination Type: Groundwater/Both Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 07/28/2010 Date Occur: 08/29/2009 Cleanup: Not reported Closure Request: Not reported Close Out: Not reported 10/24/2007, JFM/// TC3669805.1 s Page 68 Map ID MAP FINDINGS Direction Distance Elevation Site TOWN OF CHAPEL HILL TRANSIT GARAGE (Continued) Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: U Risk Class Based On Review: I Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Free product Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 5 RPL: False CD Num: 0 Reel Num: 0 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9376-79.0595 Testlat: Not reported EDR ID Number Database(s) EPA ID Number S110629979 Regional Officer Project Mgr: DMD Region: Raleigh Company: CHAPEL HILL PUBLIC WORKS Contact Person: FORREST HEATH Telephone: 9196146256 RP Address: 6850 MILLHOUSE RD RP City,St,Zip: CHAPEL HILL, NC 27515 RP County: Not reported Comments: ALTHOUGH 2O07 IAAR FOR FORMER HYDRAULIC LIFT SYSTEM INDICATES NO SOIL CONTAMINTION ABOVE STG MSCCS, >8000 PPM TPH DRO WAS REPORTED, AND SUBSEQUENT WELL INSTALLATION IN AUG 2009 CONFIRMED FP ACCORDING TO PROPERTY OWNER, UNC-CH.-DMD,8/2/10//// 5 Min Quad: Not reported PIRF: Facility Id: Date Occurred: Date Reported: Description Of Incident: Owner/Operator: Ownership: Operation Type: Type: Location: Site Priority: Priority Update: 33879 2009-08-29 00:00:00 2010-07-28 00:00:00 HYDRAULIC LIFT LEAK RESULTED IN FP Not reported 7 1 5 1 Not reported Not reported TC3669805.1 s Page 69 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number TOWN OF CHAPEL HILL TRANSIT GARAGE (Continued) S110629979 Wells Affected Y/N: Not reported Samples Include: Not reported 7#5 Minute Quad: Y 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: 1 Source: F Ust Number: P Last Modified: Not reported Incident Phase: Not reported NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported G29 CHAPEL HILL,TOWN OF,TRANSPORTA IMD S106195935 NNW 1089 AIRPORT ROAD N/A 1/4-1/2 CHAPEL HILL, NC 0.473 mi. 2500 ft. Site 4 of 6 in cluster G Relative: IMD: Higher Region: RAL Facility ID: 8228 Actual: Date Occurred: Not reported 458 ft. Submit Date: 6/16/1992 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: CONTAMINATION FOUND DURING UST REMOVAL Operator: Not reported Contact Phone: Not reported Owner Company: TOWN OF CHAPEL HILL Operator Address:306 N COLUMBIA ST Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27517- Ownership: Municipal Operation: Not reported Material: USED OIL Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Facility Setting: Urban Risk Site: L Site Priority: Not reported Priority Code: Not reported Priority Update: Not reported TC3669805.1 s Page 70 Map ID MAP FINDINGS Direction Distance Elevation Site CHAPEL HILL,TOWN OF,TRANSPORTA (Continued) Dem Contact: MAF Wells Affected: Not reported Num Affected: 0 Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: Not reported Longitude: Not reported Latitude Number: Not reported Longitude Number: Not reported Latitude Decimal: Not reported Longitude Decimal: Not reported GPS: NOD Agency: DWM Facility ID: 8228 Last Modified: 3/9/1999 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: 6/5/1992 30 SPRUYT, JUNE S. - RESIDENCE West 265 SEVERIN STREET 1/4-1/2 CHAPEL HILL, NC 27517 0.483 mi. 2549 ft. Relative: IMD EDR ID Number Database(s) EPA ID Number S106195935 IMD S105548354 LUST N/A LUST TRUST Higher Region: RAL Facility ID: 24475 Actual: Date Occurred: 3/25/2002 439 ft. Submit Date: 8/1/2002 GW Contam: Not reported Soil Contam: Yes Incident Desc: ONE 550 GALLON HEATING OIL UST REMOVED. SOIL CONTAMINATION DETECTED IN SAMPLES COLLECTED AT CLOSURE. 102 MG/KG C9-C22 AROMATICS IN SAMPLE "B1" Operator: JUNE S. & DIRK SPRUYT Contact Phone: 919-967-4746 Owner Company: Not reported Operator Address:98 MAXWELL RD. Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27517 Ownership: Private Operation: Residential Material: Not reported Qty Lost 1: Not reported Qty Recovered 1: Not reported TC3669805.1 s Page 71 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number SPRUYT, JUNE S. - RESIDENCE (Continued) S105548354 Source: Leak -underground Type: Heating Oil Location: Residence Setting: Residential Risk Site: Not reported Site Priority: U Priority Code: Not reported Priority Update: 8/1/2002 Dem Contact: Not reported Wells Affected: Not reported Num Affected: Not reported Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: Not reported Longitude: Not reported Latitude Number: Not reported Longitude Number: Not reported Latitude Decimal: Not reported Longitude Decimal: Not reported GPS: NOD Agency: DWM Facility ID: 24475 Last Modified: 8/1/2002 Incident Phase: RE NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported Region: RAL Facility ID: 26021 Date Occurred: 3/25/2002 Submit Date: 7/22/2002 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: Not reported Operator: Not reported Contact Phone: 919/967-4746 Owner Company: DIRK & JUNE S. SPRUYT Operator Address:98 MAXWELL RD. Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27517- Ownership: Private Operation: Residential Material: Not reported Qty Lost 1: Not reported Qty Recovered 1: Not reported TC3669805.1 s Page 72 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number SPRUYT, JUNE S. - RESIDENCE (Continued) S105548354 Source: Leak -underground Type: Gasoline/diesel Location: Residence Setting: Not reported Risk Site: L Site Priority: Not reported Priority Code: L Priority Update: Not reported Dem Contact: JFM Wells Affected: No Num Affected: Not reported Wells Contam: Not reported Sampled By: Dept. of Env. Management Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.92611111 Longitude:-79.06305555 Latitude Number: 355534 Longitude Number: 790347 Latitude Decimal: 35.9261111111111 Longitude Decimal: 79.0630555555556 GPS: 7 Agency: DWM Facility ID: 26021 Last Modified: 9/26/2002 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST: Facility ID: Not reported UST Number: RA-160 Incident Number: 26021 Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 07/22/2002 Date Occur: 03/25/2002 Cleanup: 03/25/2002 Closure Request: Not reported Close Out: 09/26/2002 Level Of Soil Cleanup Achieved: Residential Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L TC3669805.1 s Page 73 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number SPRUYT, JUNE S. - RESIDENCE (Continued) S105548354 Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: 07/30/2002 Site Priority: Not reported Phase Of LSA Req: 1 Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: No Flag: Yes Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in Archives RBCA GW: Cleanups to 2L.0202 standards PETOPT: 4 RPL: False CD Num: 233 Reel Num: 116 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9263-79.0633 Testlat: Not reported Regional Officer Project Mgr: JFM Region: Raleigh Company: DIRK & JUNE S. SPRUYT Contact Person: Not reported Telephone: 919/967-4746 RP Address: 98 MAXWELL RD. RP City,St,Zip: CHAPEL HILL, NC 27517- RP County: orange Comments: 07/18/02 - 20 Day rpt submitted by Terraquest: Release discovered following removal of a 550-gal heating oil UST on 03/25/02. UST was taken out of service in 1986 when 280-gal heating oil AST installed. AST removed in 1994. Approx. 103.03 tons impacted s 5 Min Quad: Not reported PIRF: Facility Id: 26021 Date Occurred: 2002-03-25 00:00:00 Date Reported: 2002-07-22 00:00:00 Description Of Incident: Not reported Owner/Operator: Not reported Ownership: 4 Operation Type: 3 Type: 4 Location: 7 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: 1 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported TC3669805.1 s Page 74 Map ID MAP FINDINGS Direction Distance Elevation Site SPRUYT, JUNE S. - RESIDENCE (Continued) Source Code: Not reported Err Type: 2 Cause: Not reported Source: C Ust Number: C Last Modified: 2002-09-26 00:00:00 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: Facility ID: Not reported Site ID: 26021 Site Note: Not reported Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 EDR ID Number Database(s) EPA ID Number S105548354 C;lirk this by perlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. 31 FLEMING RESIDENTIAL UST LUST S111161288 SSE 518 NORTH ST LUST TRUST N/A 1/4-1/2 CHAPEL HILL, NC 27514 0.485 mi. 2560 ft. Relative: LUST Higher Facility ID: Not reported UST Number: RA-6890 Actual: Incident Number: 39034 454 ft. Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 06/09/2011 Date Occur: 06/08/2011 Cleanup: Not reported Closure Request: Not reported Close Out: 09/28/2011 Level Of Soil Cleanup Achieved: Industrial/Commercial Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: U Risk Class Based On Review: L TC3669805.1 s Page 75 Map ID MAP FINDINGS Direction Distance Elevation Site FLEMING RESIDENTIAL UST (Continued) Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Unknown Flag: Yes Flag1: No LUR Filed: 10/04/2011 Release Detection: 0 Current Status: File Located in House RBCA GW: Cleanups to alternate standards PETOPT: 4 RPL: False CD Num: 0 Reel Num: 0 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9185-79.0475 Testlat: Not reported EDR ID Number Database(s) EPA ID Number S111161288 Regional Officer Project Mgr: DMD Region: Raleigh Company: Not reported Contact Person: CRESWELL FLEMING, JR REV TRUST Telephone: 9703752404 RP Address: PO BOX 2423 RP City,St,Zip: DURANGO, CO 81302 RP County: Not reported Comments: CONTAMINATION WAS DISCOVERED DURING REMOVAL OF A 550 GAL HEATING OIL UST AND APPROX 30 TONS SOIL ON 6/8/11. ///SOIL > RES MSCC; LSA REQUIRED.//H Soil > res mscc; gw >GCLs; therefore, intermediate risk. Although consultant suspects "another source," (not identified in report), welll log indicates "strong petroleum odor/soil discolored green" from base of excavation (16') to total well depth (30'). In addition, highest soil contam levels were at base of excavation. Combination of physical indicators and analyses supports that gw contam is not from an off site source. Contam levels are too high to close site. Sending stop -funding NORR. DMD, 8-15-11 1H DMD site visit today. DMD, 8.26.11 /// Re -sampled well and BTEX/other compounds were orders of magnitude lower than initial sample. Based on data and only slight 2L exceedances, consultant recommends reducing risk to Low and closing site with soil and gw NRP. Rescind stop -funding NORR. DMD, 9.16.11 1H Soil & GW NRP. -MRP//Prep NFA for MRP'S signature. DMD, 9-28-11 /// NRP filed 10/04/11 on pp 295-300 of Book RB5232. -MRP//recvd pn receipts.dmd.11.9.11 5 Min Quad: Not reported PIRF: Facility Id: 39034 Date Occurred: 2011-06-08 00:00:00 Date Reported: 2011-06-09 00:00:00 Description Of Incident: CONTAMINATION WAS DISCOVERED DURING REMOVAL OF A 550 GAL HEATING OIL TC3669805.1 s Page 76 Map ID Direction Distance Elevation Site FLEMING RESIDENTIAL UST (Continued) Owner/Operator: Ownership: Operation Type: Type: Location: Site Priority: Priority Update: Wells Affected Y/N: Samples Include: 7#5 Minute Quad: 5 Minute Quad: Pirf/Min Soil: Release Code: Source Code: Err Type: Cause: Source: Ust Number: Last Modified: Incident Phase: NOV Issued: NORR Issued: 45 Day Report: Public Meeting Held: Corrective Action Planned SOC Signed: Reclassification Report: IRS Designation: Closure Request Date: Close-out Report: MAP FINDINGS UST AND APPROX 30 TONS SOIL ON 6/8/11. Not reported 4 3 4 7 Not reported Not reported N Not reported Y Not reported Not reported Not reported Not reported 2 3 A P 2011-09-28 00:00:00 Closed Out Not reported Not reported Not reported Not reported Not reported Not reported Not reported Not reported Not reported Not reported EDR ID Number Database(s) EPA ID Number LUST TRUST: Facility ID: Not reported Site ID: 39034 Site Note: RIF on file. Noncommercial; 100% eligible; $0 deductible. Track this as a site that would have been 5K + 10% as this is receiving 100% because of Session Law 2010-154. [CGS 1/5/12] Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 Clink this hgpprlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. S111161288 TC3669805.1 s Page 77 Map ID Direction Distance Elevation Site MAP FINDINGS EDR ID Number Database(s) EPA ID Number G32 TOWN OF CHAPEL HILL PUBLIC WOR IMD S106074804 NNW 1099 AIRPORT ROAD N/A 1/4-1/2 CHAPEL HILL, NC 0.486 mi. 2564 ft. Site 5 of 6 in cluster G Relative: IMD: Higher Region: RAL Facility ID: 26371 Actual: Date Occurred: 6/2/2003 458 ft. Submit Date: 9/8/2003 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: One (1) 550-gallon Waste oil UST Operator: BRADY MOORE Contact Phone: 9199682800 Owner Company: TOWN OF CHAPEL HILL PUBLIC WOR Operator Address:1099 AIRPORT ROAD Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27516- Ownership: Municipal Operation: Public Service Material: Not reported Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Facility Setting: Not reported Risk Site: L Site Priority: Not reported Priority Code: Not reported Priority Update: Not reported Dem Contact: JFM Wells Affected: No Num Affected: Not reported Wells Contam: Not reported Sampled By: Dept. of Health Services Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.93861111 Longitude:-79.0575 Latitude Number: 355619 Longitude Number: 790327 Latitude Decimal: 35.9386111111111 Longitude Decimal: 79.0575 GPS: 7 Agency: DWM Facility ID: 26371 Last Modified: 9/15/2003 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported TC3669805.1 s Page 78 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number TOWN OF CHAPEL HILL PUBLIC WOR (Continued) S106074804 IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported G33 PUBLIC WORKS GARAGE IMD 0001438129 NNW 1099 AIRPORT RD LUST N/A 1/4-1/2 CHAPEL HILL, NC 27514 LUST TRUST 0.486 mi. UST 2564 ft. Site 6 of 6 in cluster G Relative: IMD: Higher Region: RAL Facility ID: 22669 Actual: Date Occurred: 3/24/1998 458 ft. Submit Date: 1/4/2001 GW Contam: Yes, Groundwater Contamination has been detected Soil Contam: No Incident Desc: SOIL CONTAMINATION DISCOVERED DURING UST REMOVAL Operator: BRADY MOORE Contact Phone: 9199682800 Owner Company: TOWN OF CHAPEL HILL Operator Address:306 N. COLOMBIA STREET Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27516- Ownership: Municipal Operation: Public Service Material: Not reported Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Facility Setting: Industrial Risk Site: L Site Priority: U Priority Code: Not reported Priority Update: 1/4/2001 Dem Contact: JFM Wells Affected: No Num Affected: Not reported Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: 35.93861111 Longitude:-79.05805555 Latitude Number: 355619 Longitude Number: 790329 Latitude Decimal: 35.9386111111111 Longitude Decimal: 79.0580555555556 GPS: 6 Agency: DWM Facility ID: 22669 Last Modified: 12/29/2000 Incident Phase: Closed Out NOV Issued: Not reported TC3669805.1 s Page 79 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number PUBLIC WORKS GARAGE (Continued) 0001438129 NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST: Facility ID: 00-0-000 UST Number: RA-3694 Incident Number: 22669 Contamination Type: Groundwater/Both Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 04/24/1998 Date Occur: 03/24/1998 Cleanup: 03/24/1998 Closure Request: Not reported Close Out: 08/26/2003 Level Of Soil Cleanup Achieved: Soil to Groundwater Tank Regulated Status: Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: 01/21/2001 Site Priority: Not reported Phase Of LSA Req: 1 Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Yes Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in Archives RBCA GW: Cleanups to 2L.0202 standards PETOPT: 3 RPL: False CD Num: 234 Reel Num: 118 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9388-79.0583 Testlat: Not reported Regional Officer Project Mgr: JFM Region: Raleigh TC3669805.1 s Page 80 Map ID Direction Distance Elevation MAP FINDINGS Site EDR ID Number Database(s) EPA ID Number PUBLIC WORKS GARAGE (Continued) 0001438129 Company: TOWN OF CHAPEL HILL Contact Person: BRADY MOORE Telephone: 9199682800 RP Address: 306 N. COLOMBIA STREET RP City,St,Zip: CHAPEL HILL, NC 27516- RP County: ORANGE Comments: 03/24/98 - Release discovered from closure of 1 x 8000-gal diesel UST, and 2 x 10000-gal gas USTs. Soil > SGW and Res. MSCCs. Approx 900 tons impacted soil removed from site - Recommend LSA. CED 01/21/01 - NORR requesting LSA following pull. 5 Min Quad: Not reported PIRF: Facility Id: 22669 Date Occurred: 1998-03-24 00:00:00 Date Reported: 2001-01-04 00:00:00 Description Of Incident: SOIL CONTAMINATION DISCOVERED DURING UST REMOVAL Owner/Operator: PAUL HARVEL Ownership: 1 Operation Type: 1 Type: 3 Location: 1 Site Priority: U Priority Update: 2001-01-04 00:00:00 Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: Y 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: 7 Source: G Ust Number: P Last Modified: 2000-12-29 00:00:00 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported Facility ID: UST Number: Incident Number: Contamination Type: Source Type: Product Type: Date Reported: Date Occur: Cleanup: 00-0-000 RA-4674 26371 Soil Leak -underground PETROLEUM 09/08/2003 06/02/2003 Not reported TC3669805.1 s Page 81 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number PUBLIC WORKS GARAGE (Continued) 0001438129 Closure Request: Not reported Close Out: 09/15/2003 Level Of Soil Cleanup Achieved: Residential Tank Regulated Status: Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in Archives RBCA GW: Not reported PETOPT: 5 RPL: False CD Num: 233 Reel Num: 116 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9388-79.0577 Testlat: Not reported Regional Officer Project Mgr: JFM Region: Raleigh Company: TOWN OF CHAPEL HILL PUBLIC WOR Contact Person: BRADY MOORE Telephone: 9199682800 RP Address: 1099 AIRPORT ROAD RP City,St,Zip: CHAPEL HILL, NC 27516- RP County: Not reported Comments: 09/03/03 - Tank Closure rpt submitted by Quantum: Release discovered following soil assessment surrounding a 550-gal waste oil UST which was installed on 03/15/79. Soil samples < Residential MSCCs. - Requested NFA - CED ///// 5 Min Quad: Not reported PIRF: Facility Id: 26371 Date Occurred: 2003-06-02 00:00:00 Date Reported: 2003-09-08 00:00:00 Description Of Incident: One (1) 550-gallon Waste oil UST Owner/Operator: Not reported Ownership: 1 Operation Type: 1 Type: 5 Location: 1 TC3669805.1 s Page 82 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number PUBLIC WORKS GARAGE (Continued) 0001438129 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: 2 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: Not reported Source: C Ust Number: C Last Modified: 2003-09-15 00:00:00 Incident Phase: Closed Out NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported Facility ID: Not reported UST Number: RA-5804 Incident Number: 33350 Contamination Type: Groundwater/Both Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 08/31/2007 Date Occur: 07/11/2007 Cleanup: 07/11 /2007 Closure Request: Not reported Close Out: Not reported Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: COMMERCIAL Risk Classification: Not reported Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: 1 Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 TC3669805.1 s Page 83 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number PUBLIC WORKS GARAGE (Continued) 0001438129 Current Status: File Located in House RBCA GW: Not reported PETOPT: 3 RPL: False CD Num: 0 Reel Num: 0 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9388-79.0583 Testlat: Not reported Regional Officer Project Mgr: JFM Region: Raleigh Company: Town of Chapel Hill Contact Person: Brady Moore Telephone: 9199695120 RP Address: 405 Martin Luther King RP City,St,Zip: Chapel Hill, NC 27514 RP County: Not reported Comments: One (01) 550-gallon waste oil UST, one (01) 1 K-gallon waste oil UST, one (01) 12K-gallon gasoline UST and one ()1) 12K-gallon diesel UST removed. 09/05/2007, JFM/H 12/19/07 - Updated receptor survey indicated no WSWs within 1500'. Low risk site. - CED 5 Min Quad: Not reported PIRF: Facility Id: 33350 Date Occurred: 2007-07-11 00:00:00 Date Reported: 2007-08-31 00:00:00 Description Of Incident: One (01) 550-gallon waste oil UST, one (01) 1 K-gallon waste oil UST, one (01) 12K-gallon gasoline UST and one ()1) 12K-gallon diesel UST removed. Owner/Operator: Not reported Ownership: 1 Operation Type: 1 Type: 3 Location: 1 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: Y 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: Not reported Source: Not reported Ust Number: P Last Modified: Not reported Incident Phase: Not reported NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported TC3669805.1 s Page 84 Map ID Direction Distance Elevation MAP FINDINGS Site EDR ID Number Database(s) EPA ID Number PUBLIC WORKS GARAGE (Continued) Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST TRUST: Facility ID: 0-035865 Site ID: 26371 Site Note: Commercial; first apply a 60% apportionment for ineligible tanks (which means 40% eligible), then apply a $20,000 deductible; then 100% eligible for costs that exceed the $20,000 deductible.[CGS 12/28/09] Site Eligible?: True Commercial Find: 100% Commercial Priority Rank: Not reported Deductable Amount: 20000 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 Clink this by P'� rlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. UST: Facility Id: 00-0-0000022269 Contact: TOWN OF CHAPEL HILL ATTN:TRANSIT Contact Address1: 306 N. COLUMBIA ST-MAINT SUPERIN Contact Address2: Not reported Contact City/State/Zip: CHAPEL HILL, NC 27516-2113 FIPS County Desc: Orange Latitude: 35.93907 Longitude: -79.05839 Tank Id: 1 Tank Status: Removed Installed Date: 03/15/1979 Perm Close Date: 03/24/1998 Product Key: 1 Product Name: Diesel Tank Capacity: 8000 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: Not reported Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel Piping Construction: Single Wall Steel Piping System Key: Unknown Other CP Tank: Not reported Tank Id: 2 Tank Status: Removed Installed Date: 03/15/1979 0001438129 TC3669805.1 s Page 85 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number PUBLIC WORKS GARAGE (Continued) 0001438129 Perm Close Date: 03/24/1998 Product Key: 3 Product Name: Gasoline, Gas Mix Tank Capacity: 10000 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: Not reported Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel Piping Construction: Single Wall Steel Piping System Key: Unknown Other CP Tank: Not reported Tank Id: 3 Tank Status: Removed Installed Date: 03/15/1979 Perm Close Date: 03/24/1998 Product Key: 3 Product Name: Gasoline, Gas Mix Tank Capacity: 10000 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: Not reported Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel Piping Construction: Single Wall Steel Piping System Key: Unknown Other CP Tank: Not reported Tank Id: 4 Tank Status: Removed Installed Date: 03/15/1979 Perm Close Date: 12/04/2001 Product Key: 14 Product Name: Oil, New/Used/Mix Tank Capacity: 550 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: Not reported Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel Piping Construction: Single Wall Steel Piping System Key: Unknown Other CP Tank: Not reported Tank Id: 5 Tank Status: Removed Installed Date: 03/15/1979 TC3669805.1 s Page 86 Map ID MAP FINDINGS Direction Distance Elevation Site PUBLIC WORKS GARAGE (Continued) Perm Close Date: 12/04/2001 Product Key: 14 Product Name: Oil, New/Used/Mix Tank Capacity: 1000 Root Tank Id: Not reported Main Tank: No Compartment Tank: No Manifold Tank: Not reported Commercial: Yes Regulated: Yes Tank Construction: Single Wall Steel Piping Construction: Single Wall Steel Piping System Key: Unknown Other CP Tank: Not reported EDR ID Number Database(s) EPA ID Number 0001438129 34 BARAZANDEH PROPERTY (FARZIN) LUST S109164494 ENE 311 BURLAGE CIRCLE LUST TRUST N/A 1/4-1/2 CHAPEL HILL, NC 27514 0.496 mi. 2617 ft. Relative: LUST Lower Facility ID: Not reported UST Number: RA-6023 Actual: Incident Number: 33563 310 ft. Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 07/24/2008 Date Occur: 07/16/2008 Cleanup: Not reported Closure Request: Not reported Close Out: Not reported Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: NON COMMERCIAL Risk Classification: Not reported Risk Class Based On Review: U Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: Not reported Phase Of LSA Req: Not reported Site Risk Reason: Not reported Land Use: Residential MTBE: No MTBE1: Unknown Flag: No Flag1: No LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: 0 Reel Num: 0 TC3669805.1 s Page 87 Map ID Direction Distance Elevation MAP FINDINGS Site EDR ID Number Database(s) EPA ID Number BARAZANDEH PROPERTY (FARZIN) (Continued) S109164494 RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: False Lat/Long Decimal: 35.9281-79.0411 Testlat: Not reported Regional Officer Project Mgr: DMD Region: Raleigh Company: BARAZANDEH PROPERTY (FARZIN) Contact Person: FARZIN BARAZANDEH Telephone: 9199686119 RP Address: 311 BURLAGE CIRCLE RP City,St,Zip: CHAPEL HILL, NC 27514 RP County: Not reported Comments: REMOVED 550 GAL RESIDENTIAL HEATING OIL UST AND SUSPECTED CONTAM SOIL ON 7/7/08. SOIL SAMPLE B1-5.5' CONFIRMED RELEASE OF 1100 DRO/60 GRO (MG/KG)-DMD,8/26/08.////ollowing removal of 26.96 tons contam soil, two resid sidewall soil samples > Comm/Ind MSCCs-DMD,12/12/08//// 5 Min Quad: Not reported PIRF: Facility Id: 33563 Date Occurred: 2008-07-16 00:00:00 Date Reported: 2008-07-24 00:00:00 Description Of Incident: REMOVED 550 GAL RESIDENTIAL HEATING OIL UST AND SUSPECTED CONTAM SOIL ON 7/7/08. SOIL SAMPLE 131-5.5' CONFIRMED RELEASE OF 1100 DRO/60 GRO (MG/KG). Owner/Operator: Not reported Ownership: 4 Operation Type: 3 Type: 4 Location: 7 Site Priority: Not reported Priority Update: Not reported Wells Affected Y/N: N Samples Include: Not reported 7#5 Minute Quad: Y 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Not reported Err Type: 2 Cause: 3 Source: A Ust Number: P Last Modified: Not reported Incident Phase: Not reported NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported TC3669805.1 s Page 88 Map ID MAP FINDINGS Direction Distance Elevation Site BARAZANDEH PROPERTY (FARZIN) (Continued) Close-out Report: Not reported LUST TRUST: Facility ID: Not reported Site ID: 33563 Site Note: Noncommercial; 100% eligible; $0 deductible.[CGS 1/12/09] Site Eligible?: True Commercial Find: 100% Non -Commercial Priority Rank: Not reported Deductable Amount: 0 3rd Party Deductable Amt: 0 Sum 3rd Party Amt Applied: 0 EDR ID Number Database(s) EPA ID Number Clink this hgpprlink while viewing on your computer to access additional NC LUST TRUST: detail in the EDR Site Report. 35 UNC-PHILLIPS HALL SHWS South 120 E CAMERON AVE IMD 1/2-1 CHAPEL HILL, NC LUST 0.973 mi. 5139 ft. Relative: SHWS: Higher Facility ID: NONCD0002408 Lat/Longitude: 35.91065 / -79.05263 Actual: Geolocation Method: On Screen Placement On Georeferenced Map 500 ft. IMD: Region: RAL Facility ID: 13251 Date Occurred: 10/5/1994 Submit Date: 1/26/1995 GW Contam: No Groundwater Contamination detected Soil Contam: Yes Incident Desc: SOIL SAMPLE AT 100000 GAL #2 UST FOR 5030 SHOWED 4000PPM TPH Operator: ROBERT WALTON Contact Phone: (919)966-6666 Owner Company: UNIVERSITY OF NORTH CAROLINA Operator Address:212 FINLEY GOLF COURSE RD Operator City: CHAPEL HILL Oper City,St,Zip: CHAPEL HILL, NC 27514- Ownership: State Operation: Educational/Religious Material: FUEL OIL Qty Lost 1: Not reported Qty Recovered 1: Not reported Source: Leak -underground Type: Gasoline/diesel Location: Facility Setting: Urban Risk Site: L Site Priority: 20E Priority Code: L Priority Update: 4/16/1998 Dem Contact: CED Wells Affected: Not reported Num Affected: 0 S109164494 S101573932 N/A TC3669805.1 s Page 89 Map ID MAP FINDINGS Direction Distance EDR ID Number Elevation Site Database(s) EPA ID Number UNC-PHILLIPS HALL (Continued) S101573932 Wells Contam: Not reported Sampled By: Not reported Samples Include: Not reported 7.5 Min Quad: Not reported 5 Min Quad: Not reported Latitude: Not reported Longitude: Not reported Latitude Number: Not reported Longitude Number: Not reported Latitude Decimal: Not reported Longitude Decimal: Not reported GPS: NOD Agency: DWM Facility ID: 13251 Last Modified: Not reported Incident Phase: RE NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Sighned: Not reported Reclassification Report: Not reported RS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported LUST: Facility ID: Not reported UST Number: RA-2176 Incident Number: 13251 Contamination Type: Soil Source Type: Leak -underground Product Type: PETROLEUM Date Reported: 10/05/1994 Date Occur: 09/19/1994 Cleanup: Not reported Closure Request: Not reported Close Out: Not reported Level Of Soil Cleanup Achieved: Not reported Tank Regulated Status: Non Regulated # Of Supply Wells: 0 Commercial/NonCommercial UST Site: COMMERCIAL Risk Classification: L Risk Class Based On Review: L Corrective Action Plan Type: Not reported NOV Issue Date: Not reported NORR Issue Date: Not reported Site Priority: 20E Phase Of LSA Req: 1 Site Risk Reason: Not reported Land Use: Not reported MTBE: No MTBE1: Unknown Flag: No Flag1: No TC3669805.1 s Page 90 Map ID Direction Distance Elevation Site UNC-PHILLIPS HALL (Continued) MAP FINDINGS LUR Filed: Not reported Release Detection: 0 Current Status: File Located in House RBCA GW: Not reported PETOPT: 4 RPL: False CD Num: Not reported Reel Num: Not reported RPOW: False RPOP: False Error Flag: 0 Error Code: N Valid: True Lat/Long Decimal: 35.9106-79.0528 Testlat: Not reported EDR ID Number Database(s) EPA ID Number S101573932 Regional Officer Project Mgr: DMD Region: Raleigh Company: UNIVERSITY OF NORTH CAROLINA Contact Person: Larry Daw Telephone: 9199626666 RP Address: 1120 Estes Drive Extension, RP City,St,Zip: CHAPEL HILL, NC 275991650 RP County: Not reported Comments: 03/06/95 - UST CLO rpt: 10K heating oil USTon-site. Soil contam. Identified @12-13' bls to N of UST, all other samples BDL. - CED //// 02/08/08 - UNC decided to remove the UST. On 08/06/07 UST removed from site. Closure samples collecetd from beneath UST > TPH (CS3=99 mg/kg). Resampled location for RBCA. Only dibenz (a.h)anthracene was > S-GW MSCCs. Approx. 19.53 tons impacted soil removed. SW sample > S-GW MSCCs. (SW-2 could not be excavated further due to building foundation)). GW not encountered. No FP. Irrigation WSW located adj to UST not in use, but not abandoned. Recommends LSA. - CED //// 02/19/08 - LSA NORR Issued. - CED ////Soil exceeds comm/indus MSCCs. GW exceeds 2L for PCE and is present above detection levels for trichlorofluoromethane and chloroform; however, no petroleum constituents were detected. Additional soils cannot be excavated due to presence of generator, etc. Site remains high risk due to irrigation well (still in use per Larry Daw, UNC). Site below TF funding bar; therefore, sending stop funding NORR.DMD, 10-21-10////MW Resampling.-MRPHnon-petroleum constituents only; data has been provided by UNC to Inactive Hazardous Sites Branch for review. DMD, 1-21-11 11H 5 Min Quad: Not reported PIRF: Facility Id: 13251 Date Occurred: 1994-10-05 00:00:00 Date Reported: 1995-01-26 00:00:00 Description Of Incident: SOIL SAMPLE AT 100000 GAL #2 UST FOR 5030 SHOWED 4000PPM TPH Owner/Operator: ROBERT WALTON Ownership: 7 Operation Type: 4 Type: 4 Location: 1 Site Priority: 20E Priority Update: 1998-04-16 00:00:00 Wells Affected Y/N: Not reported Samples Include: 0 TC3669805.1 s Page 91 Map ID MAP FINDINGS Direction Distance Elevation Site UNC-PHILLIPS HALL (Continued) 7#5 Minute Quad: Not reported 5 Minute Quad: Not reported Pirf/Min Soil: Not reported Release Code: Not reported Source Code: Min Soil Err Type: Not reported Cause: Not reported Source: Not reported Ust Number: Not reported Last Modified: Not reported Incident Phase: Response NOV Issued: Not reported NORR Issued: Not reported 45 Day Report: Not reported Public Meeting Held: Not reported Corrective Action Planned: Not reported SOC Signed: Not reported Reclassification Report: Not reported IRS Designation: Not reported Closure Request Date: Not reported Close-out Report: Not reported EDR ID Number Database(s) EPA ID Number S101573932 TC3669805.1 s Page 92 Count: 20 records. ORPHAN SUMMARY City EDR ID Site Name CHAPEL HILL 1001232809 CAROLINA CLEANERS CHAPEL HILL 1003868322 UNIVERSITY OF NC/ARPT RD OLD SAN L CHAPEL HILL 1003868323 UNIVERSITY OF NC/ARPT WASTE DSPL A CHAPEL HILL 1004745846 CLEORA STERLING CORP CHAPEL HILL 1004747005 AMERICAN STONE COMPANY - CHAPEL HI HILLSBOROUGH 1007713832 HILL TOP MHP CHAPEL HILL 1007714010 NORTH CHAPEL BAPTIST CHURCH CHAPEL HILL S106896242 DOT-N-DASH CHAPEL HILL S108664952 KIRBY'S AMERICAN STATION PROPERTY CHAPEL HILL S109164493 ROCHELLE PROPERTY (CHARLES) DURHAM S110628729 BLUE CROSS BLUE SHIELD (DURHAM SER CHAPEL HILL S110629421 MIKE CORNER STORE CARRBORO 0001438050 BEAL-TILLMAN CHAPEL HILL 0001438289 J LOUIS ALLEN CHAPEL HILL 0001438776 JERRY'S STOP & SHOP CHAPEL HILL 0001440050 GORDON'S GULF SERVICE CHAPEL HILL 0003134181 TRIPP'S GROCERY CHAPEL HILL 0003137316 STOP'N SHOP CHAPEL HILL 0003137754 GORDON'S BP SERVICE CHAPEL HILL 0003562969 WAS KIRBY'S AMERICAN STATION Site Address 2214 CHAPEL HILL/NELSON HWY AIRPORT RD AIRPORT RD 616HWY 54W 1807 US HIGHWAY 54 WEST 7105 HIGHWAY 86N 7707 HIGHWAY 86 NORTH HIGHWAY 54 / SMITH LEVEL ROAD 4721 HIGHWAY 54 WEST 6419 NC HWY 86 HIGHWAY 150-501 4908 HWY 54 WEST HIGHWAY 54 WEST HWY 54 RT 4, BOX 507-OLD GREENSBORO H ROUTE 3, HWY 15 ROUTE 6 ROUTE 9, BOX 370 RT. 3, HWY 15 RT 1 BOX 153 HWY 54 WEST Zip Database(s) FINDS,RCRA-CESQG 27514 CERCLIS-NFRAP 27514 CERCLIS-NFRAP 27516 FINDS,RCRA-CESQG 27516 FINDS,RCRA-CESQG,AIRS (AFS) FINDS FINDS IMD,LUST 27514 LUST 27514 LUST TRUST,LUST 27514 LAST 27516 LAST 27510 UST 27514 UST 27516 UST 27514 UST 27514 UST 27514 UST 27514 UST 27514 UST TC3669805.1 s Page 93 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING To maintain currency of the following federal and state databases, EDR contacts the appropriate governmental agency on a monthly or quarterly basis, as required. Number of Days to Update: Provides confirmation that EDR is reporting records that have been updated within 90 days from the date the government agency made the information available to the public. STANDARD ENVIRONMENTAL RECORDS Federal NPL site list NPL: National Priority List National Priorities List (Superfund). The NPL is a subset of CERCLIS and identifies over 1,200 sites for priority cleanup under the Superfund Program. NPL sites may encompass relatively large areas. As such, EDR provides polygon coverage for over 1,000 NPL site boundaries produced by EPA's Environmental Photographic Interpretation Center (EPIC) and regional EPA offices. Date of Government Version: 04/26/2013 Date Data Arrived at EDR: 05/09/2013 Date Made Active in Reports: 07/10/2013 Number of Days to Update: 62 NPL Site Boundaries Source: EPA Telephone: N/A Last EDR Contact: 05/09/2013 Next Scheduled EDR Contact: 07/22/2013 Data Release Frequency: Quarterly Sources: EPA's Environmental Photographic Interpretation Center (EPIC) Telephone:202-564-7333 EPA Region 1 Telephone 617-918-1143 EPA Region 3 Telephone 215-814-5418 EPA Region 4 Telephone 404-562-8033 EPA Region 5 Telephone 312-886-6686 EPA Region 10 Telephone 206-553-8665 EPA Region 6 Telephone: 214-6 55-6659 EPA Region 7 Telephone: 913-551-7247 EPA Region 8 Telephone: 303-312-6774 EPA Region 9 Telephone: 415-947-4246 Proposed NPL: Proposed National Priority List Sites A site that has been proposed for listing on the National Priorities List through the issuance of a proposed rule in the Federal Register. EPA then accepts public comments on the site, responds to the comments, and places on the NPL those sites that continue to meet the requirements for listing. Date of Government Version: 04/26/2013 Date Data Arrived at EDR: 05/09/2013 Date Made Active in Reports: 07/10/2013 Number of Days to Update: 62 Source: EPA Telephone: N/A Last EDR Contact: 05/09/2013 Next Scheduled EDR Contact: 07/22/2013 Data Release Frequency: Quarterly NPL LIENS: Federal Superfund Liens Federal Superfund Liens. Under the authority granted the USEPA by CERCLA of 1980, the USEPA has the authority to file liens against real property in order to recover remedial action expenditures or when the property owner received notification of potential liability. USEPA compiles a listing of filed notices of Superfund Liens. Date of Government Version: 10/15/1991 Date Data Arrived at EDR: 02/02/1994 Date Made Active in Reports: 03/30/1994 Number of Days to Update: 56 Source: EPA Telephone: 202-564-4267 Last EDR Contact: 08/15/2011 Next Scheduled EDR Contact: 11/28/2011 Data Release Frequency: No Update Planned TC3669805.1 s Page GR-1 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING Federal Delisted NPL site list DELISTED NPL: National Priority List Deletions The National Oil and Hazardous Substances Pollution Contingency Plan (NCP) establishes the criteria that the EPA uses to delete sites from the NPL. In accordance with 40 CFR 300.425.(e), sites may be deleted from the NPL where no further response is appropriate. Date of Government Version: 04/26/2013 Date Data Arrived at EDR: 05/09/2013 Date Made Active in Reports: 07/10/2013 Number of Days to Update: 62 Federal CERCLIS list Source: EPA Telephone: N/A Last EDR Contact: 05/09/2013 Next Scheduled EDR Contact: 07/22/2013 Data Release Frequency: Quarterly CERCLIS: Comprehensive Environmental Response, Compensation, and Liability Information System CERCLIS contains data on potentially hazardous waste sites that have been reported to the USEPA by states, municipalities, private companies and private persons, pursuant to Section 103 of the Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA). CERCLIS contains sites which are either proposed to or on the National Priorities List (NPL) and sites which are in the screening and assessment phase for possible inclusion on the NPL. Date of Government Version: 02/04/2013 Date Data Arrived at EDR: 03/01/2013 Date Made Active in Reports: 03/13/2013 Number of Days to Update: 12 Source: EPA Telephone: 703-412-9810 Last EDR Contact: 05/29/2013 Next Scheduled EDR Contact: 09/09/2013 Data Release Frequency: Quarterly FEDERAL FACILITY: Federal Facility Site Information listing A listing of National Priority List (NPL) and Base Realignment and Closure (BRAC) sites found in the Comprehensive Environmental Response, Compensation and Liability Information System (CERCLIS) Database where EPA Federal Facilities Restoration and Reuse Office is involved in cleanup activities. Date of Government Version: 07/31/2012 Date Data Arrived at EDR: 10/09/2012 Date Made Active in Reports: 12/20/2012 Number of Days to Update: 72 Federal CERCLIS NFRAP site List Source: Environmental Protection Agency Telephone: 703-603-8704 Last EDR Contact: 07/08/2013 Next Scheduled EDR Contact: 10/21/2013 Data Release Frequency: Varies CERCLIS-NFRAP: CERCLIS No Further Remedial Action Planned Archived sites are sites that have been removed and archived from the inventory of CERCLIS sites. Archived status indicates that, to the best of EPA's knowledge, assessment at a site has been completed and that EPA has determined no further steps will be taken to list this site on the National Priorities List (NPL), unless information indicates this decision was not appropriate or other considerations require a recommendation for listing at a later time. This decision does not necessarily mean that there is no hazard associated with a given site; it only means that, based upon available information, the location is not judged to be a potential NPL site. Date of Government Version: 02/05/2013 Date Data Arrived at EDR: 03/01/2013 Date Made Active in Reports: 03/13/2013 Number of Days to Update: 12 Federal RCRA CORRACTS facilities list Source: EPA Telephone: 703-412-9810 Last EDR Contact: 05/29/2013 Next Scheduled EDR Contact: 05/09/2013 Data Release Frequency: Quarterly CORRACTS: Corrective Action Report CORRACTS identifies hazardous waste handlers with RCRA corrective action activity. TC3669805.1 s Page GR-2 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING Date of Government Version: 02/12/2013 Date Data Arrived at EDR: 02/21/2013 Date Made Active in Reports: 02/27/2013 Number of Days to Update: 6 Federal RCRA non-CORRACTS TSD facilities list Source: EPA Telephone: 800-424-9346 Last EDR Contact: 07/01/2013 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Quarterly RCRA-TSDF: RCRA - Treatment, Storage and Disposal RCRAInfo is EPA's comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Transporters are individuals or entities that move hazardous waste from the generator offsite to a facility that can recycle, treat, store, or dispose of the waste. TSDFs treat, store, or dispose of the waste. Date of Government Version: 02/12/2013 Date Data Arrived at EDR: 02/15/2013 Date Made Active in Reports: 02/27/2013 Number of Days to Update: 12 Federal RCRA generators list Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 07/01/2013 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Quarterly RCRA-LQG: RCRA - Large Quantity Generators RCRAInfo is EPA's comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Large quantity generators (LQGs) generate over 1,000 kilograms (kg) of hazardous waste, or over 1 kg of acutely hazardous waste per month. Date of Government Version: 02/12/2013 Date Data Arrived at EDR: 02/15/2013 Date Made Active in Reports: 02/27/2013 Number of Days to Update: 12 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 07/01/2013 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Quarterly RCRA-SQG: RCRA - Small Quantity Generators RCRAInfo is EPA's comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Small quantity generators (SQGs) generate between 100 kg and 1,000 kg of hazardous waste per month. Date of Government Version: 02/12/2013 Date Data Arrived at EDR: 02/15/2013 Date Made Active in Reports: 02/27/2013 Number of Days to Update: 12 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 07/01/2013 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Quarterly RCRA-CESQG: RCRA - Conditionally Exempt Small Quantity Generators RCRAInfo is EPA's comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Conditionally exempt small quantity generators (CESQGs) generate less than 100 kg of hazardous waste, or less than 1 kg of acutely hazardous waste per month. Date of Government Version: 02/12/2013 Date Data Arrived at EDR: 02/15/2013 Date Made Active in Reports: 02/27/2013 Number of Days to Update: 12 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 07/01/2013 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Varies TC3669805.1 s Page GR-3 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING Federal institutional controls / engineering controls registries US ENG CONTROLS: Engineering Controls Sites List A listing of sites with engineering controls in place. Engineering controls include various forms of caps, building foundations, liners, and treatment methods to create pathway elimination for regulated substances to enter environmental media or effect human health. Date of Government Version: 03/14/2013 Date Data Arrived at EDR: 03/29/2013 Date Made Active in Reports: 05/10/2013 Number of Days to Update: 42 Source: Environmental Protection Agency Telephone: 703-603-0695 Last EDR Contact: 06/10/2013 Next Scheduled EDR Contact: 09/23/2013 Data Release Frequency: Varies US INST CONTROL: Sites with Institutional Controls A listing of sites with institutional controls in place. Institutional controls include administrative measures, such as groundwater use restrictions, construction restrictions, property use restrictions, and post remediation care requirements intended to prevent exposure to contaminants remaining on site. Deed restrictions are generally required as part of the institutional controls. Date of Government Version: 03/14/2013 Date Data Arrived at EDR: 03/29/2013 Date Made Active in Reports: 05/10/2013 Number of Days to Update: 42 Source: Environmental Protection Agency Telephone: 703-603-0695 Last EDR Contact: 06/10/2013 Next Scheduled EDR Contact: 09/23/2013 Data Release Frequency: Varies LUCIS: Land Use Control Information System LUCIS contains records of land use control information pertaining to the former Navy Base Realignment and Closure properties. Date of Government Version: 12/09/2005 Date Data Arrived at EDR: 12/11/2006 Date Made Active in Reports: 01/11/2007 Number of Days to Update: 31 Federal ERNS list Source: Department of the Navy Telephone: 843-820-7326 Last EDR Contact: 05/20/2013 Next Scheduled EDR Contact: 09/02/2013 Data Release Frequency: Varies ERNS: Emergency Response Notification System Emergency Response Notification System. ERNS records and stores information on reported releases of oil and hazardous substances. Date of Government Version: 12/31/2012 Source: National Response Center, United States Coast Guard Date Data Arrived at EDR: 01/17/2013 Telephone: 202-267-2180 Date Made Active in Reports: 02/15/2013 Last EDR Contact: 07/01/2013 Number of Days to Update: 29 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Annually State- and tribal - equivalent NPL HSDS: Hazardous Substance Disposal Site Locations of uncontrolled and unregulated hazardous waste sites. The file includes sites on the National Priority List as well as those on the state priority list. Date of Government Version: 08/09/2011 Date Data Arrived at EDR: 11/08/2011 Date Made Active in Reports: 12/05/2011 Number of Days to Update: 27 State- and tribal - equivalent CERCLIS Source: North Carolina Center for Geographic Information and Analysis Telephone: 919-754-6 580 Last EDR Contact: 05/03/2013 Next Scheduled EDR Contact: 08/19/2013 Data Release Frequency: Biennially TC3669805.1 s Page GR-4 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING SHWS: Inactive Hazardous Sites Inventory State Hazardous Waste Sites. State hazardous waste site records are the states' equivalent to CERCLIS. These sites may or may not already be listed on the federal CERCLIS list. Priority sites planned for cleanup using state funds (state equivalent of Superfund) are identified along with sites where cleanup will be paid for by potentially responsible parties. Available information varies by state. Date of Government Version: 05/24/2013 Source: Department of Environment, Health and Natural Resources Date Data Arrived at EDR: 06/20/2013 Telephone: 919-508-8400 Date Made Active in Reports: 07/05/2013 Last EDR Contact: 06/20/2013 Number of Days to Update: 15 Next Scheduled EDR Contact: 09/30/2013 Data Release Frequency: Quarterly State and tribal landfill and/or solid waste disposal site lists SWF/LF: List of Solid Waste Facilities Solid Waste Facilities/Landfill Sites. SWF/LF type records typically contain an inventory of solid waste disposal facilities or landfills in a particular state. Depending on the state, these may be active or inactive facilities or open dumps that failed to meet RCRA Subtitle D Section 4004 criteria for solid waste landfills or disposal sites. Date of Government Version: 04/01/2013 Source: Department of Environment and Natural Resources Date Data Arrived at EDR: 04/02/2013 Telephone: 919-733-0692 Date Made Active in Reports: 05/09/2013 Last EDR Contact: 07/03/2013 Number of Days to Update: 37 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Semi -Annually OLI: Old Landfill Inventory Old landfill inventory location information. (Does not include no further action sites and other agency lead sites). Date of Government Version: 04/05/2013 Source: Department of Environment & Natural Resources Date Data Arrived at EDR: 04/18/2013 Telephone: 919-733-4996 Date Made Active in Reports: 05/09/2013 Last EDR Contact: 04/16/2013 Number of Days to Update: 21 Next Scheduled EDR Contact: 07/29/2013 Data Release Frequency: Varies State and tribal leaking storage tank lists LUST: Regional UST Database This database contains information obtained from the Regional Offices. It provides a more detailed explanation of current and historic activity for individual sites, as well as what was previously found in the Incident Management Database. Sites in this database with Incident Numbers are considered LUSTS. Date of Government Version: 05/10/2013 Source: Department of Environment and Natural Resources Date Data Arrived at EDR: 05/16/2013 Telephone: 919-733-1308 Date Made Active in Reports: 07/05/2013 Last EDR Contact: 05/16/2013 Number of Days to Update: 50 Next Scheduled EDR Contact: 08/26/2013 Data Release Frequency: Quarterly LUST TRUST: State Trust Fund Database This database contains information about claims against the State Trust Funds for reimbursements for expenses incurred while remediating Leaking USTs. Date of Government Version: 04/03/2013 Source: Department of Environment and Natural Resources Date Data Arrived at EDR: 04/17/2013 Telephone: 919-733-1315 Date Made Active in Reports: 05/09/2013 Last EDR Contact: 10/17/2013 Number of Days to Update: 22 Next Scheduled EDR Contact: 10/28/2013 Data Release Frequency: Semi -Annually TC3669805.1 s Page GR-5 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING LAST: Leaking Aboveground Storage Tanks A listing of leaking aboveground storage tank site locations. Date of Government Version: 05/10/2013 Source: Department of Environment & Natural Resources Date Data Arrived at EDR: 05/16/2013 Telephone: 877-623-6748 Date Made Active in Reports: 07/05/2013 Last EDR Contact: 05/16/2013 Number of Days to Update: 50 Next Scheduled EDR Contact: 08/26/2013 Data Release Frequency: Quarterly INDIAN LUST R9: Leaking Underground Storage Tanks on Indian Land LUSTS on Indian land in Arizona, California, New Mexico and Nevada Date of Government Version: 03/01/2013 Date Data Arrived at EDR: 03/01/2013 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 42 Source: Environmental Protection Agency Telephone: 415-972-3 372 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Quarterly INDIAN LUST R8: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Colorado, Montana, North Dakota, South Dakota, Utah and Wyoming. Date of Government Version: 08/27/2012 Date Data Arrived at EDR: 08/28/2012 Date Made Active in Reports: 10/16/2012 Number of Days to Update: 49 Source: EPA Region 8 Telephone: 303-312-6271 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Quarterly INDIAN LUST R7: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Iowa, Kansas, and Nebraska Date of Government Version: 12/31/2012 Date Data Arrived at EDR: 02/28/2013 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 43 Source: EPA Region 7 Telephone: 913-551-7003 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Varies INDIAN LUST R6: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in New Mexico and Oklahoma. Date of Government Version: 09/12/2011 Date Data Arrived at EDR: 09/13/2011 Date Made Active in Reports: 11/11/2011 Number of Days to Update: 59 Source: EPA Region 6 Telephone: 214-665-6 597 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Varies INDIAN LUST R4: Leaking Underground Storage Tanks on Indian Land LUSTs on Indian land in Florida, Mississippi and North Carolina. Date of Government Version: 02/06/2013 Date Data Arrived at EDR: 02/08/2013 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 63 Source: EPA Region 4 Telephone: 404-562-8677 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Semi -Annually INDIAN LUST R1: Leaking Underground Storage Tanks on Indian Land A listing of leaking underground storage tank locations on Indian Land. Date of Government Version: 09/28/2012 Date Data Arrived at EDR: 11/01/2012 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 162 Source: EPA Region 1 Telephone: 617-918-1313 Last EDR Contact: 05/01/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Varies TC3669805.1 s Page GR-6 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING INDIAN LUST R10: Leaking Underground Storage Tanks on Indian Land LUSTS on Indian land in Alaska, Idaho, Oregon and Washington. Date of Government Version: 02/05/2013 Date Data Arrived at EDR: 02/06/2013 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 65 State and tribal registered storage tank lists Source: EPA Region 10 Telephone: 206-553-2857 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Quarterly UST: Petroleum Underground Storage Tank Database Registered Underground Storage Tanks. UST's are regulated under Subtitle I of the Resource Conservation and Recovery Act (RCRA) and must be registered with the state department responsible for administering the UST program. Available information varies by state program. Date of Government Version: 05/10/2013 Source: Department of Environment and Natural Resources Date Data Arrived at EDR: 05/16/2013 Telephone: 919-733-1308 Date Made Active in Reports: 07/03/2013 Last EDR Contact: 05/16/2013 Number of Days to Update: 48 Next Scheduled EDR Contact: 08/26/2013 Data Release Frequency: Quarterly AST: AST Database Facilities with aboveground storage tanks that have a capacity greater than 21,000 gallons. Date of Government Version: 03/25/2013 Source: Department of Environment and Natural Resources Date Data Arrived at EDR: 03/25/2013 Telephone: 919-715-6183 Date Made Active in Reports: 04/02/2013 Last EDR Contact: 06/20/2013 Number of Days to Update: 8 Next Scheduled EDR Contact: 10/07/2013 Data Release Frequency: Semi -Annually INDIAN UST R6: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 6 (Louisiana, Arkansas, Oklahoma, New Mexico, Texas and 65 Tribes). Date of Government Version: 05/10/2011 Date Data Arrived at EDR: 05/11/2011 Date Made Active in Reports: 06/14/2011 Number of Days to Update: 34 Source: EPA Region 6 Telephone: 214-665-7591 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Semi -Annually INDIAN UST R7: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 7 (Iowa, Kansas, Missouri, Nebraska, and 9 Tribal Nations). Date of Government Version: 12/31/2012 Date Data Arrived at EDR: 02/28/2013 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 43 Source: EPA Region 7 Telephone: 913-551-7003 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Varies INDIAN UST R8: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 8 (Colorado, Montana, North Dakota, South Dakota, Utah, Wyoming and 27 Tribal Nations). Date of Government Version: 08/27/2012 Date Data Arrived at EDR: 08/28/2012 Date Made Active in Reports: 10/16/2012 Number of Days to Update: 49 Source: EPA Region 8 Telephone: 303-312-6137 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Quarterly TC3669805.1 s Page GR-7 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING INDIAN UST R9: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 9 (Arizona, California, Hawaii, Nevada, the Pacific Islands, and Tribal Nations). Date of Government Version: 02/21/2013 Date Data Arrived at EDR: 02/26/2013 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 45 Source: EPA Region 9 Telephone: 415-972-3 368 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Quarterly INDIAN UST R1: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 1 (Connecticut, Maine, Massachusetts, New Hampshire, Rhode Island, Vermont and ten Tribal Nations). Date of Government Version: 09/28/2012 Date Data Arrived at EDR: 11/07/2012 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 156 Source: EPA, Region 1 Telephone: 617-918-1313 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Varies INDIAN UST R4: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 4 (Alabama, Florida, Georgia, Kentucky, Mississippi, North Carolina, South Carolina, Tennessee and Tribal Nations) Date of Government Version: 02/06/2013 Date Data Arrived at EDR: 02/08/2013 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 63 Source: EPA Region 4 Telephone: 404-562-9424 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Semi -Annually INDIAN UST R5: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 5 (Michigan, Minnesota and Wisconsin and Tribal Nations). Date of Government Version: 08/02/2012 Date Data Arrived at EDR: 08/03/2012 Date Made Active in Reports: 11/05/2012 Number of Days to Update: 94 Source: EPA Region 5 Telephone: 312-886-6136 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Varies INDIAN UST R10: Underground Storage Tanks on Indian Land The Indian Underground Storage Tank (UST) database provides information about underground storage tanks on Indian land in EPA Region 10 (Alaska, Idaho, Oregon, Washington, and Tribal Nations). Date of Government Version: 02/05/2013 Date Data Arrived at EDR: 02/06/2013 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 65 Source: EPA Region 10 Telephone: 206-553-2857 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Quarterly FEMA UST: Underground Storage Tank Listing A listing of all FEMA owned underground storage tanks. Date of Government Version: 01/01/2010 Date Data Arrived at EDR: 02/16/2010 Date Made Active in Reports: 04/12/2010 Number of Days to Update: 55 Source: FEMA Telephone: 202-646-5797 Last EDR Contact: 04/18/2013 Next Scheduled EDR Contact: 07/29/2013 Data Release Frequency: Varies TC3669805.1 s Page GR-8 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING State and tribal institutional control / engineering control registries INST CONTROL: No Further Action Sites With Land Use Restrictions Monitoring A land use restricted site is a property where there are limits or requirements on future use of the property due to varying levels of cleanup possible, practical, or necessary at the site. Date of Government Version: 05/24/2013 Source: Department of Environment, Health and Natural Resources Date Data Arrived at EDR: 06/20/2013 Telephone: 919-508-8400 Date Made Active in Reports: 07/05/2013 Last EDR Contact: 12/17/2110 Number of Days to Update: 15 Next Scheduled EDR Contact: 09/30/2013 Data Release Frequency: Quarterly State and tribal voluntary cleanup sites INDIAN VCP R1: Voluntary Cleanup Priority Listing A listing of voluntary cleanup priority sites located on Indian Land located in Region 1. Date of Government Version: 09/28/2012 Date Data Arrived at EDR: 10/02/2012 Date Made Active in Reports: 10/16/2012 Number of Days to Update: 14 Source: EPA, Region 1 Telephone: 617-918-1102 Last EDR Contact: 07/02/2013 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Varies INDIAN VCP R7: Voluntary Cleanup Priority Lisitng A listing of voluntary cleanup priority sites located on Indian Land located in Region 7. Date of Government Version: 03/20/2008 Date Data Arrived at EDR: 04/22/2008 Date Made Active in Reports: 05/19/2008 Number of Days to Update: 27 Source: EPA, Region 7 Telephone: 913-551-7365 Last EDR Contact: 04/20/2009 Next Scheduled EDR Contact: 07/20/2009 Data Release Frequency: Varies VCP: Responsible Party Voluntary Action Sites Responsible Party Voluntary Action site locations. Date of Government Version: 05/24/2013 Source: Department of Environment and Natural Resources Date Data Arrived at EDR: 06/20/2013 Telephone: 919-508-8400 Date Made Active in Reports: 07/05/2013 Last EDR Contact: 06/20/2013 Number of Days to Update: 15 Next Scheduled EDR Contact: 09/30/2013 Data Release Frequency: Semi -Annually State and tribal Brownfields sites BROWNFIELD& Brownfields Projects Inventory A brownfield site is an abandoned, idled, or underused property where the threat of environmental contamination has hindered its redevelopment. All of the sites in the inventory are working toward a brownfield agreement for cleanup and liabitliy control. Date of Government Version: 04/04/2013 Source: Department of Environment and Natural Resources Date Data Arrived at EDR: 04/10/2013 Telephone: 919-733-4996 Date Made Active in Reports: 05/23/2013 Last EDR Contact: 07/10/2013 Number of Days to Update: 43 Next Scheduled EDR Contact: 10/21/2013 Data Release Frequency: Varies ADDITIONAL ENVIRONMENTAL RECORDS Local Brownfield lists US BROWNFIELDS: A Listing of Brownfields Sites Brownfields are real property, the expansion, redevelopment, or reuse of which may be complicated by the presence or potential presence of a hazardous substance, pollutant, or contaminant. Cleaning up and reinvesting in these properties takes development pressures off of undeveloped, open land, and both improves and protects the environment. Assessment, Cleanup and Redevelopment Exchange System (ACRES) stores information reported by EPA Brownfields grant recipients on brownfields properties assessed or cleaned up with grant funding as well as information on Targeted Brownfields Assessments performed by EPA Regions. A listing of ACRES Brownfield sites is obtained from Cleanups in My Community. Cleanups in My Community provides information on Brownfields properties for which information is reported back to EPA, as well as areas served by Brownfields grant programs. TC3669805.1 s Page GR-9 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING Date of Government Version: 12/10/2012 Date Data Arrived at EDR: 12/11/2012 Date Made Active in Reports: 12/20/2012 Number of Days to Update: 9 Source: Environmental Protection Agency Telephone: 202-566-2777 Last EDR Contact: 06/25/2013 Next Scheduled EDR Contact: 10/07/2013 Data Release Frequency: Semi -Annually Local Lists of Landfill / Solid Waste Disposal Sites ODI: Open Dump Inventory An open dump is defined as a disposal facility that does not comply with one or more of the Part 257 or Part 258 Subtitle D Criteria. Date of Government Version: 06/30/1985 Date Data Arrived at EDR: 08/09/2004 Date Made Active in Reports: 09/17/2004 Number of Days to Update: 39 Source: Environmental Protection Agency Telephone: 800-424-9346 Last EDR Contact: 06/09/2004 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned DEBRIS REGION 9: Torres Martinez Reservation Illegal Dump Site Locations A listing of illegal dump sites location on the Torres Martinez Indian Reservation located in eastern Riverside County and northern Imperial County, California. Date of Government Version: 01/12/2009 Date Data Arrived at EDR: 05/07/2009 Date Made Active in Reports: 09/21/2009 Number of Days to Update: 137 HIST LF: Solid Waste Facility Listing A listing of solid waste facilities. Date of Government Version: 11/06/2006 Date Data Arrived at EDR: 02/13/2007 Date Made Active in Reports: 03/02/2007 Number of Days to Update: 17 SWRCY: Recycling Center Listing A listing of recycling center locations. Date of Government Version: 08/06/2012 Date Data Arrived at EDR: 08/08/2012 Date Made Active in Reports: 09/13/2012 Number of Days to Update: 36 Source: EPA, Region 9 Telephone: 415-947-4219 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: No Update Planned Source: Department of Environment & Natural Resources Telephone: 919-733-0692 Last EDR Contact: 01/19/2009 Next Scheduled EDR Contact: 04/19/2009 Data Release Frequency: Quarterly Source: Department of Environment & Natural Resources Telephone: 919-707-813 7 Last EDR Contact: 06/14/2013 Next Scheduled EDR Contact: 08/19/2013 Data Release Frequency: Varies INDIAN ODI: Report on the Status of Open Dumps on Indian Lands Location of open dumps on Indian land. Date of Government Version: 12/31/1998 Date Data Arrived at EDR: 12/03/2007 Date Made Active in Reports: 01/24/2008 Number of Days to Update: 52 Source: Environmental Protection Agency Telephone: 703-308-8245 Last EDR Contact: 05/03/2013 Next Scheduled EDR Contact: 08/19/2013 Data Release Frequency: Varies Local Lists of Hazardous waste / Contaminated Sites US CDL: Clandestine Drug Labs A listing of clandestine drug lab locations. The U.S. Department of Justice ("the Department') provides this web site as a public service. It contains addresses of some locations where law enforcement agencies reported they found chemicals or other items that indicated the presence of either clandestine drug laboratories or dumpsites. In most cases, the source of the entries is not the Department, and the Department has not verified the entry and does not guarantee its accuracy. Members of the public must verify the accuracy of all entries by, for example, contacting local law enforcement and local health departments. TC3669805.1 s Page GR-10 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING Date of Government Version: 03/04/2013 Date Data Arrived at EDR: 03/12/2013 Date Made Active in Reports: 05/10/2013 Number of Days to Update: 59 Source: Drug Enforcement Administration Telephone: 202-307-1000 Last EDR Contact: 06/03/2013 Next Scheduled EDR Contact: 09/16/2013 Data Release Frequency: Quarterly US HIST CDL: National Clandestine Laboratory Register A listing of clandestine drug lab locations. The U.S. Department of Justice ("the Department") provides this web site as a public service. It contains addresses of some locations where law enforcement agencies reported they found chemicals or other items that indicated the presence of either clandestine drug laboratories or dumpsites. In most cases, the source of the entries is not the Department, and the Department has not verified the entry and does not guarantee its accuracy. Members of the public must verify the accuracy of all entries by, for example, contacting local law enforcement and local health departments. Date of Government Version: 09/01/2007 Date Data Arrived at EDR: 11/19/2008 Date Made Active in Reports: 03/30/2009 Number of Days to Update: 131 Local Land Records Source: Drug Enforcement Administration Telephone: 202-307-1000 Last EDR Contact: 03/23/2009 Next Scheduled EDR Contact: 06/22/2009 Data Release Frequency: No Update Planned LIENS 2: CERCLA Lien Information A Federal CERCLA ('Superfund') lien can exist by operation of law at any site or property at which EPA has spent Superfund monies. These monies are spent to investigate and address releases and threatened releases of contamination. CERCLIS provides information as to the identity of these sites and properties. Date of Government Version: 02/06/2013 Date Data Arrived at EDR: 04/25/2013 Date Made Active in Reports: 05/10/2013 Number of Days to Update: 15 Records of Emergency Release Reports Source: Environmental Protection Agency Telephone: 202-564-602 3 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Varies HMIRS: Hazardous Materials Information Reporting System Hazardous Materials Incident Report System. HMIRS contains hazardous material spill incidents reported to DOT. Date of Government Version: 12/31/2012 Date Data Arrived at EDR: 01/03/2013 Date Made Active in Reports: 02/27/2013 Number of Days to Update: 55 Source: U.S. Department of Transportation Telephone: 202-366-4 555 Last EDR Contact: 07/01/2013 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Annually IMD: Incident Management Database Groundwater and/or soil contamination incidents Date of Government Version: 07/21/2006 Source: Department of Environment and Natural Resources Date Data Arrived at EDR: 08/01/2006 Telephone: 919-733-3221 Date Made Active in Reports: 08/23/2006 Last EDR Contact: 07/01/2011 Number of Days to Update: 22 Next Scheduled EDR Contact: 10/17/2011 Data Release Frequency: No Update Planned SPILLS 80: SPILLS80 data from FirstSearch Spills 80 includes those spill and release records available from FirstSearch databases prior to 1990. Typically, they may include chemical, oil and/or hazardous substance spills recorded before 1990. Duplicate records that are already included in EDR incident and release records are not included in Spills 80. Date of Government Version: 06/14/2001 Date Data Arrived at EDR: 01/03/2013 Date Made Active in Reports: 03/06/2013 Number of Days to Update: 62 Source: FirstSearch Telephone: N/A Last EDR Contact: 01/03/2013 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned TC3669805.1 s Page GR-11 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING SPILLS 90: SPILLS90 data from FirstSearch Spills 90 includes those spill and release records available exclusively from FirstSearch databases. Typically, they may include chemical, oil and/or hazardous substance spills recorded after 1990. Duplicate records that are already included in EDR incident and release records are not included in Spills 90. Date of Government Version: 09/27/2012 Date Data Arrived at EDR: 01/03/2013 Date Made Active in Reports: 03/06/2013 Number of Days to Update: 62 Other Ascertainable Records Source: FirstSearch Telephone: N/A Last EDR Contact: 01/03/2013 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned RCRA NonGen / NLR: RCRA - Non Generators RCRAInfo is EPA's comprehensive information system, providing access to data supporting the Resource Conservation and Recovery Act (RCRA) of 1976 and the Hazardous and Solid Waste Amendments (HSWA) of 1984. The database includes selective information on sites which generate, transport, store, treat and/or dispose of hazardous waste as defined by the Resource Conservation and Recovery Act (RCRA). Non -Generators do not presently generate hazardous waste. Date of Government Version: 02/12/2013 Date Data Arrived at EDR: 02/15/2013 Date Made Active in Reports: 02/27/2013 Number of Days to Update: 12 Source: Environmental Protection Agency Telephone: (404) 562-8651 Last EDR Contact: 07/01/2013 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Varies DOT OPS: Incident and Accident Data Department of Transporation, Office of Pipeline Safety Incident and Accident data. Date of Government Version: 07/31/2012 Source: Department of Transporation, Office of Pipeline Safety Date Data Arrived at EDR: 08/07/2012 Telephone: 202-366-4595 Date Made Active in Reports: 09/18/2012 Last EDR Contact: 05/07/2013 Number of Days to Update: 42 Next Scheduled EDR Contact: 08/19/2013 Data Release Frequency: Varies DOD: Department of Defense Sites This data set consists of federally owned or administered lands, administered by the Department of Defense, that have any area equal to or greater than 640 acres of the United States, Puerto Rico, and the U.S. Virgin Islands. Date of Government Version: 12/31/2005 Date Data Arrived at EDR: 11/10/2006 Date Made Active in Reports: 01/11/2007 Number of Days to Update: 62 Source: USGS Telephone: 888-275-8747 Last EDR Contact: 04/19/2013 Next Scheduled EDR Contact: 07/29/2013 Data Release Frequency: Semi -Annually FUDS: Formerly Used Defense Sites The listing includes locations of Formerly Used Defense Sites properties where the US Army Corps of Engineers is actively working or will take necessary cleanup actions. Date of Government Version: 12/31/2011 Date Data Arrived at EDR: 02/26/2013 Date Made Active in Reports: 03/13/2013 Number of Days to Update: 15 Source: U.S. Army Corps of Engineers Telephone: 202-528-4285 Last EDR Contact: 06/10/2013 Next Scheduled EDR Contact: 09/23/2013 Data Release Frequency: Varies CONSENT: Superfund (CERCLA) Consent Decrees Major legal settlements that establish responsibility and standards for cleanup at NPL (Superfund) sites. Released periodically by United States District Courts after settlement by parties to litigation matters. TC3669805.1 s Page GR-12 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING Date of Government Version: 12/31/2011 Source: Department of Justice, Consent Decree Library Date Data Arrived at EDR: 01/15/2013 Telephone: Varies Date Made Active in Reports: 03/13/2013 Last EDR Contact: 06/25/2013 Number of Days to Update: 57 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Varies ROD: Records Of Decision Record of Decision. ROD documents mandate a permanent remedy at an NPL (Superfund) site containing technical and health information to aid in the cleanup. Date of Government Version: 12/18/2012 Date Data Arrived at EDR: 03/13/2013 Date Made Active in Reports: 04/12/2013 Number of Days to Update: 30 Source: EPA Telephone: 703-416-022 3 Last EDR Contact: 06/11/2013 Next Scheduled EDR Contact: 09/23/2013 Data Release Frequency: Annually UMTRA: Uranium Mill Tailings Sites Uranium ore was mined by private companies for federal government use in national defense programs. When the mills shut down, large piles of the sand -like material (mill tailings) remain after uranium has been extracted from the ore. Levels of human exposure to radioactive materials from the piles are low; however, in some cases tailings were used as construction materials before the potential health hazards of the tailings were recognized. Date of Government Version: 09/14/2010 Date Data Arrived at EDR: 10/07/2011 Date Made Active in Reports: 03/01/2012 Number of Days to Update: 146 Source: Department of Energy Telephone: 505-845-0011 Last EDR Contact: 05/28/2013 Next Scheduled EDR Contact: 09/09/2013 Data Release Frequency: Varies US MINES: Mines Master Index File Contains all mine identification numbers issued for mines active or opened since 1971. The data also includes violation information. Date of Government Version: 02/05/2013 Source: Department of Labor, Mine Safety and Health Administration Date Data Arrived at EDR: 04/18/2013 Telephone: 303-231-5959 Date Made Active in Reports: 05/10/2013 Last EDR Contact: 06/04/2013 Number of Days to Update: 22 Next Scheduled EDR Contact: 09/16/2013 Data Release Frequency: Semi -Annually TRIS: Toxic Chemical Release Inventory System Toxic Release Inventory System. TRIS identifies facilities which release toxic chemicals to the air, water and land in reportable quantities under SARA Title III Section 313. Date of Government Version: 12/31/2009 Date Data Arrived at EDR: 09/01/2011 Date Made Active in Reports: 01/10/2012 Number of Days to Update: 131 Source: EPA Telephone: 202-566-0250 Last EDR Contact: 05/29/2013 Next Scheduled EDR Contact: 09/09/2013 Data Release Frequency: Annually TSCA: Toxic Substances Control Act Toxic Substances Control Act. TSCA identifies manufacturers and importers of chemical substances included on the TSCA Chemical Substance Inventory list. It includes data on the production volume of these substances by plant site. Date of Government Version: 12/31/2006 Date Data Arrived at EDR: 09/29/2010 Date Made Active in Reports: 12/02/2010 Number of Days to Update: 64 Source: EPA Telephone: 202-260-5521 Last EDR Contact: 06/25/2013 Next Scheduled EDR Contact: 10/07/2013 Data Release Frequency: Every 4 Years TC3669805.1 s Page GR-13 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING FTTS: FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act) FTTS tracks administrative cases and pesticide enforcement actions and compliance activities related to FIFRA, TSCA and EPCRA (Emergency Planning and Community Right -to -Know Act). To maintain currency, EDR contacts the Agency on a quarterly basis. Date of Government Version: 04/09/2009 Source: EPA/Office of Prevention, Pesticides and Toxic Substances Date Data Arrived at EDR: 04/16/2009 Telephone: 202-566-1667 Date Made Active in Reports: 05/11/2009 Last EDR Contact: 05/28/2013 Number of Days to Update: 25 Next Scheduled EDR Contact: 09/09/2013 Data Release Frequency: Quarterly FTTS INSP: FIFRA/ TSCA Tracking System - FIFRA (Federal Insecticide, Fungicide, & Rodenticide Act)/TSCA (Toxic Substances Control Act) A listing of FIFRA/TSCA Tracking System (FTTS) inspections and enforcements. Date of Government Version: 04/09/2009 Date Data Arrived at EDR: 04/16/2009 Date Made Active in Reports: 05/11/2009 Number of Days to Update: 25 Source: EPA Telephone: 202-566-1667 Last EDR Contact: 05/28/2013 Next Scheduled EDR Contact: 09/09/2013 Data Release Frequency: Quarterly HIST FTTS: FIFRA/TSCA Tracking System Administrative Case Listing A complete administrative case listing from the FIFRA/TSCA Tracking System (FTTS) for all ten EPA regions. The information was obtained from the National Compliance Database (NCDB). NCDB supports the implementation of FIFRA (Federal Insecticide, Fungicide, and Rodenticide Act) and TSCA (Toxic Substances Control Act). Some EPA regions are now closing out records. Because of that, and the fact that some EPA regions are not providing EPA Headquarters with updated records, it was decided to create a HIST FTTS database. It included records that may not be included in the newer FTTS database updates. This database is no longer updated. Date of Government Version: 10/19/2006 Date Data Arrived at EDR: 03/01/2007 Date Made Active in Reports: 04/10/2007 Number of Days to Update: 40 Source: Environmental Protection Agency Telephone: 202-564-2501 Last EDR Contact: 12/17/2007 Next Scheduled EDR Contact: 03/17/2008 Data Release Frequency: No Update Planned HIST FTTS INSP: FIFRA/TSCA Tracking System Inspection & Enforcement Case Listing A complete inspection and enforcement case listing from the FIFRA/TSCA Tracking System (FTTS) for all ten EPA regions. The information was obtained from the National Compliance Database (NCDB). NCDB supports the implementation of FIFRA (Federal Insecticide, Fungicide, and Rodenticide Act) and TSCA (Toxic Substances Control Act). Some EPA regions are now closing out records. Because of that, and the fact that some EPA regions are not providing EPA Headquarters with updated records, it was decided to create a HIST FTTS database. It included records that may not be included in the newer FTTS database updates. This database is no longer updated. Date of Government Version: 10/19/2006 Date Data Arrived at EDR: 03/01/2007 Date Made Active in Reports: 04/10/2007 Number of Days to Update: 40 Source: Environmental Protection Agency Telephone: 202-564-2501 Last EDR Contact: 12/17/2008 Next Scheduled EDR Contact: 03/17/2008 Data Release Frequency: No Update Planned SSTS: Section 7 Tracking Systems Section 7 of the Federal Insecticide, Fungicide and Rodenticide Act, as amended (92 Stat. 829) requires all registered pesticide -producing establishments to submit a report to the Environmental Protection Agency by March 1st each year. Each establishment must report the types and amounts of pesticides, active ingredients and devices being produced, and those having been produced and sold or distributed in the past year. Date of Government Version: 12/31/2009 Date Data Arrived at EDR: 12/10/2010 Date Made Active in Reports: 02/25/2011 Number of Days to Update: 77 Source: EPA Telephone: 202-564-420 3 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Annually TC3669805.1 s Page GR-14 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING ICIS: Integrated Compliance Information System The Integrated Compliance Information System (ICIS) supports the information needs of the national enforcement and compliance program as well as the unique needs of the National Pollutant Discharge Elimination System (NPDES) program. Date of Government Version: 07/20/2011 Date Data Arrived at EDR: 11/10/2011 Date Made Active in Reports: 01/10/2012 Number of Days to Update: 61 Source: Environmental Protection Agency Telephone: 202-564-5088 Last EDR Contact: 07/01/2013 Next Scheduled EDR Contact: 10/28/2013 Data Release Frequency: Quarterly PADS: PCB Activity Database System PCB Activity Database. PADS Identifies generators, transporters, commercial storers and/or brokers and disposers of PCB's who are required to notify the EPA of such activities. Date of Government Version: 11/01/2012 Date Data Arrived at EDR: 01/16/2013 Date Made Active in Reports: 05/10/2013 Number of Days to Update: 114 Source: EPA Telephone: 202-566-0 500 Last EDR Contact: 07/17/2013 Next Scheduled EDR Contact: 10/28/2013 Data Release Frequency: Annually MLTS: Material Licensing Tracking System MLTS is maintained by the Nuclear Regulatory Commission and contains a list of approximately 8,100 sites which possess or use radioactive materials and which are subject to NRC licensing requirements. To maintain currency, EDR contacts the Agency on a quarterly basis. Date of Government Version: 03/14/2013 Date Data Arrived at EDR: 03/20/2013 Date Made Active in Reports: 07/10/2013 Number of Days to Update: 112 Source: Nuclear Regulatory Commission Telephone: 301-415-7169 Last EDR Contact: 07/10/2013 Next Scheduled EDR Contact: 09/23/2013 Data Release Frequency: Quarterly RADINFO: Radiation Information Database The Radiation Information Database (RADINFO) contains information about facilities that are regulated by U.S. Environmental Protection Agency (EPA) regulations for radiation and radioactivity. Date of Government Version: 04/09/2013 Date Data Arrived at EDR: 04/11/2013 Date Made Active in Reports: 05/10/2013 Number of Days to Update: 29 Source: Environmental Protection Agency Telephone: 202-343-9775 Last EDR Contact: 07/12/2013 Next Scheduled EDR Contact: 10/21/2013 Data Release Frequency: Quarterly FINDS: Facility Index System/Facility Registry System Facility Index System. FINDS contains both facility information and 'pointers' to other sources that contain more detail. EDR includes the following FINDS databases in this report: PCS (Permit Compliance System), AIRS (Aerometric Information Retrieval System), DOCKET (Enforcement Docket used to manage and track information on civil judicial enforcement cases for all environmental statutes), FURS (Federal Underground Injection Control), C-DOCKET (Criminal Docket System used to track criminal enforcement actions for all environmental statutes), FFIS (Federal Facilities Information System), STATE (State Environmental Laws and Statutes), and PADS (PCB Activity Data System). Date of Government Version: 03/08/2013 Date Data Arrived at EDR: 03/21/2013 Date Made Active in Reports: 07/10/2013 Number of Days to Update: 111 Source: EPA Telephone: (404) 562-9900 Last EDR Contact: 06/13/2013 Next Scheduled EDR Contact: 09/23/2013 Data Release Frequency: Quarterly RAATS: RCRA Administrative Action Tracking System RCRA Administration Action Tracking System. RAATS contains records based on enforcement actions issued under RCRA pertaining to major violators and includes administrative and civil actions brought by the EPA. For administration actions after September 30, 1995, data entry in the RAATS database was discontinued. EPA will retain a copy of the database for historical records. It was necessary to terminate RAATS because a decrease in agency resources made it impossible to continue to update the information contained in the database. TC3669805.1 s Page GR-15 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING Date of Government Version: 04/17/1995 Date Data Arrived at EDR: 07/03/1995 Date Made Active in Reports: 08/07/1995 Number of Days to Update: 35 Source: EPA Telephone: 202-564-4104 Last EDR Contact: 06/02/2008 Next Scheduled EDR Contact: 09/01/2008 Data Release Frequency: No Update Planned RMP: Risk Management Plans When Congress passed the Clean Air Act Amendments of 1990, it required EPA to publish regulations and guidance for chemical accident prevention at facilities using extremely hazardous substances. The Risk Management Program Rule (RMP Rule) was written to implement Section 112(r) of these amendments. The rule, which built upon existing industry codes and standards, requires companies of all sizes that use certain flammable and toxic substances to develop a Risk Management Program, which includes a(n): Hazard assessment that details the potential effects of an accidental release, an accident history of the last five years, and an evaluation of worst -case and alternative accidental releases; Prevention program that includes safety precautions and maintenance, monitoring, and employee training measures; and Emergency response program that spells out emergency health care, employee training measures and procedures for informing the public and response agencies (e.g the fire department) should an accident occur. Date of Government Version: 05/08/2012 Date Data Arrived at EDR: 05/25/2012 Date Made Active in Reports: 07/10/2012 Number of Days to Update: 46 Source: Environmental Protection Agency Telephone: 202-564-8600 Last EDR Contact: 04/29/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Varies BRS: Biennial Reporting System The Biennial Reporting System is a national system administered by the EPA that collects data on the generation and management of hazardous waste. BRS captures detailed data from two groups: Large Quantity Generators (LQG) and Treatment, Storage, and Disposal Facilities. Date of Government Version: 12/31/2011 Date Data Arrived at EDR: 02/26/2013 Date Made Active in Reports: 04/19/2013 Number of Days to Update: 52 Source: EPA/NTIS Telephone: 800-424-9346 Last EDR Contact: 05/30/2013 Next Scheduled EDR Contact: 09/09/2013 Data Release Frequency: Biennially UIC: Underground Injection Wells Listing A listing of uncerground injection wells locations. Date of Government Version: 05/13/2013 Source: Department of Environment & Natural Resources Date Data Arrived at EDR: 05/16/2013 Telephone: 919-807-6412 Date Made Active in Reports: 07/05/2013 Last EDR Contact: 05/13/2013 Number of Days to Update: 50 Next Scheduled EDR Contact: 08/26/2013 Data Release Frequency: Varies DRYCLEANERS: Drycleaning Sites Potential and known drycleaning sites, active and abandoned, that the Drycleaning Solvent Cleanup Program has knowledge of and entered into this database. Date of Government Version: 02/06/2013 Source: Department of Environment & Natural Resources Date Data Arrived at EDR: 03/26/2013 Telephone: 919-508-8400 Date Made Active in Reports: 05/09/2013 Last EDR Contact: 06/25/2013 Number of Days to Update: 44 Next Scheduled EDR Contact: 10/07/2013 Data Release Frequency: Varies NPDES: NPDES Facility Location Listing General information regarding NPDES(National Pollutant Discharge Elimination System) permits. Date of Government Version: 05/01/2013 Source: Department of Environment & Natural Resources Date Data Arrived at EDR: 06/05/2013 Telephone: 919-733-7015 Date Made Active in Reports: 07/05/2013 Last EDR Contact: 05/28/2013 Number of Days to Update: 30 Next Scheduled EDR Contact: 08/19/2013 Data Release Frequency: Varies TC3669805.1 s Page GR-16 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING INDIAN RESERV: Indian Reservations This map layer portrays Indian administered lands of the United States that have any area equal to or greater than 640 acres. Date of Government Version: 12/31/2005 Date Data Arrived at EDR: 12/08/2006 Date Made Active in Reports: 01/11/2007 Number of Days to Update: 34 Source: USGS Telephone: 202-208-3710 Last EDR Contact: 04/19/2013 Next Scheduled EDR Contact: 07/29/2013 Data Release Frequency: Semi -Annually SCRD DRYCLEANERS: State Coalition for Remediation of Drycleaners Listing The State Coalition for Remediation of Drycleaners was established in 1998, with support from the U.S. EPA Office of Superfund Remediation and Technology Innovation. It is comprised of representatives of states with established drycleaner remediation programs. Currently the member states are Alabama, Connecticut, Florida, Illinois, Kansas, Minnesota, Missouri, North Carolina, Oregon, South Carolina, Tennessee, Texas, and Wisconsin. Date of Government Version: 03/07/2011 Date Data Arrived at EDR: 03/09/2011 Date Made Active in Reports: 05/02/2011 Number of Days to Update: 54 US AIRS MINOR: Air Facility System Data A listing of minor source facilities. Date of Government Version: 01/23/2013 Date Data Arrived at EDR: 01/30/2013 Date Made Active in Reports: 05/10/2013 Number of Days to Update: 100 Source: Environmental Protection Agency Telephone: 615-532-8 599 Last EDR Contact: 07/18/2013 Next Scheduled EDR Contact: 11/04/2013 Data Release Frequency: Varies Source: EPA Telephone: 202-564-5962 Last EDR Contact: 06/25/2013 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Annually US AIRS (AFS): Aerometric Information Retrieval System Facility Subsystem (AFS) The database is a sub -system of Aerometric Information Retrieval System (AIRS). AFS contains compliance data on air pollution point sources regulated by the U.S. EPA and/or state and local air regulatory agencies. This information comes from source reports by various stationary sources of air pollution, such as electric power plants, steel mills, factories, and universities, and provides information about the air pollutants they produce. Action, air program, air program pollutant, and general level plant data. It is used to track emissions and compliance data from industrial plants. Date of Government Version: 01/23/2013 Date Data Arrived at EDR: 01/30/2013 Date Made Active in Reports: 05/10/2013 Number of Days to Update: 100 Source: EPA Telephone: 202-564-5962 Last EDR Contact: 06/25/2013 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Annually COAL ASH: Coal Ash Disposal Sites A listing of coal combustion products distribution permits issued by the Division for the treatment, storage, transportation, use and disposal of coal combustion products. Date of Government Version: 12/31/2007 Source: Department of Environment & Natural Resources Date Data Arrived at EDR: 08/04/2009 Telephone: 919-807-6359 Date Made Active in Reports: 08/17/2009 Last EDR Contact: 05/06/2013 Number of Days to Update: 13 Next Scheduled EDR Contact: 08/19/2013 Data Release Frequency: Varies PRP: Potentially Responsible Parties A listing of verified Potentially Responsible Parties Date of Government Version: 12/18/2012 Date Data Arrived at EDR: 04/04/2013 Date Made Active in Reports: 07/10/2013 Number of Days to Update: 97 Source: EPA Telephone: 202-564-602 3 Last EDR Contact: 07/03/2013 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Quarterly TC3669805.1 s Page GR-17 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING 2020 COR ACTION: 2020 Corrective Action Program List The EPA has set ambitious goals for the RCRA Corrective Action program by creating the 2020 Corrective Action Universe. This RCRA cleanup baseline includes facilities expected to need corrective action. The 2020 universe contains a wide variety of sites. Some properties are heavily contaminated while others were contaminated but have since been cleaned up. Still others have not been fully investigated yet, and may require little or no remediation. Inclusion in the 2020 Universe does not necessarily imply failure on the part of a facility to meet its RCRA obligations. Date of Government Version: 11/11/2011 Date Data Arrived at EDR: 05/18/2012 Date Made Active in Reports: 05/25/2012 Number of Days to Update: 7 Source: Environmental Protection Agency Telephone: 703-308-4044 Last EDR Contact: 05/17/2013 Next Scheduled EDR Contact: 08/26/2013 Data Release Frequency: Varies LEAD SMELTER 2: Lead Smelter Sites A list of several hundred sites in the U.S. where secondary lead smelting was done from 1931and 1964. These sites may pose a threat to public health through ingestion or inhalation of contaminated soil or dust Date of Government Version: 04/05/2001 Date Data Arrived at EDR: 10/27/2010 Date Made Active in Reports: 12/02/2010 Number of Days to Update: 36 LEAD SMELTER 1: Lead Smelter Sites A listing of former lead smelter site locations. Date of Government Version: 01/29/2013 Date Data Arrived at EDR: 02/14/2013 Date Made Active in Reports: 02/27/2013 Number of Days to Update: 13 Source: American Journal of Public Health Telephone: 703-305-6451 Last EDR Contact: 12/02/2009 Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned Source: Environmental Protection Agency Telephone: 703-603-8787 Last EDR Contact: 07/03/2013 Next Scheduled EDR Contact: 10/21/2013 Data Release Frequency: Varies EPA WATCH LIST: EPA WATCH LIST EPA maintains a "Watch List' to facilitate dialogue between EPA, state and local environmental agencies on enforcement matters relating to facilities with alleged violations identified as either significant or high priority. Being on the Watch List does not mean that the facility has actually violated the law only that an investigation by EPA or a state or local environmental agency has led those organizations to allege that an unproven violation has in fact occurred. Being on the Watch List does not represent a higher level of concern regarding the alleged violations that were detected, but instead indicates cases requiring additional dialogue between EPA, state and local agencies - primarily because of the length of time the alleged violation has gone unaddressed or unresolved. Date of Government Version: 12/31/2012 Date Data Arrived at EDR: 02/18/2013 Date Made Active in Reports: 05/10/2013 Number of Days to Update: 81 Source: Environmental Protection Agency Telephone: 617-520-3000 Last EDR Contact: 05/10/2013 Next Scheduled EDR Contact: 08/26/2013 Data Release Frequency: Quarterly US FIN ASSUR: Financial Assurance Information All owners and operators of facilities that treat, store, or dispose of hazardous waste are required to provide proof that they will have sufficient funds to pay for the clean up, closure, and post -closure care of their facilities. Date of Government Version: 03/04/2013 Date Data Arrived at EDR: 03/15/2013 Date Made Active in Reports: 05/10/2013 Number of Days to Update: 56 Source: Environmental Protection Agency Telephone: 202-566-1917 Last EDR Contact: 05/20/2013 Next Scheduled EDR Contact: 09/02/2013 Data Release Frequency: Quarterly FEDLAND: Federal and Indian Lands Federally and Indian administrated lands of the United States. Lands included are administrated by: Army Corps of Engineers, Bureau of Reclamation, National Wild and Scenic River, National Wildlife Refuge, Public Domain Land, Wilderness, Wilderness Study Area, Wildlife Management Area, Bureau of Indian Affairs, Bureau of Land Management, Department of Justice, Forest Service, Fish and Wildlife Service, National Park Service. TC3669805.1 s Page GR-18 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING Date of Government Version: 12/31/2005 Date Data Arrived at EDR: 02/06/2006 Date Made Active in Reports: 01/11/2007 Number of Days to Update: 339 Source: U.S. Geological Survey Telephone: 888-275-874 7 Last EDR Contact: 04/19/2013 Next Scheduled EDR Contact: 07/29/2013 Data Release Frequency: N/A PCB TRANSFORMER: PCB Transformer Registration Database The database of PCB transformer registrations that includes all PCB registration submittals. Date of Government Version: 02/01/2011 Date Data Arrived at EDR: 10/19/2011 Date Made Active in Reports: 01/10/2012 Number of Days to Update: 83 Source: Environmental Protection Agency Telephone: 202-566-0 517 Last EDR Contact: 05/03/2013 Next Scheduled EDR Contact: 08/12/2013 Data Release Frequency: Varies COAL ASH DOE: Sleam-Electric Plan Operation Data A listing of power plants that store ash in surface ponds. Date of Government Version: 12/31/2005 Date Data Arrived at EDR: 08/07/2009 Date Made Active in Reports: 10/22/2009 Number of Days to Update: 76 Source: Department of Energy Telephone: 202-586-8719 Last EDR Contact: 04/18/2013 Next Scheduled EDR Contact: 07/29/2013 Data Release Frequency: Varies Financial Assurance 2: Financial Assurance Information Listing Information for solid waste facilities. Financial assurance is intended to ensure that resources are available to pay for the cost of closure, post -closure care, and corrective measures if the owner or operator of a regulated facility is unable or unwilling to pay. Date of Government Version: 10/02/2012 Source: Department of Environmental & Natural Resources Date Data Arrived at EDR: 10/03/2012 Telephone: 919-508-8496 Date Made Active in Reports: 10/26/2012 Last EDR Contact: 06/26/2013 Number of Days to Update: 23 Next Scheduled EDR Contact: 10/14/2013 Data Release Frequency: Varies COAL ASH EPA: Coal Combustion Residues Surface Impoundments List A listing of coal combustion residues surface impoundments with high hazard potential ratings. Date of Government Version: 08/17/2010 Date Data Arrived at EDR: 01/03/2011 Date Made Active in Reports: 03/21/2011 Number of Days to Update: 77 Source: Environmental Protection Agency Telephone: N/A Last EDR Contact: 06/14/2013 Next Scheduled EDR Contact: 09/23/2013 Data Release Frequency: Varies Financial Assurance 1: Financial Assurance Information Listing A listing of financial assurance information for underground storage tank facilities. Financial assurance is intended to ensure that resources are available to pay for the cost of closure, post -closure care, and corrective measures if the owner or operator of a regulated facility is unable or unwilling to pay. Date of Government Version: 09/23/2011 Source: Department of Environment & Natural Resources Date Data Arrived at EDR: 10/06/2011 Telephone: 919-733-1322 Date Made Active in Reports: 11/01/2011 Last EDR Contact: 05/16/2013 Number of Days to Update: 26 Next Scheduled EDR Contact: 08/26/2013 Data Release Frequency: Quarterly Financial Assurance 3: Financial Assurance Information Hazardous waste financial assurance information. Date of Government Version: 09/30/2012 Source: Department of Environment & Natural Resources Date Data Arrived at EDR: 10/19/2012 Telephone: 919-707-8222 Date Made Active in Reports: 11/29/2012 Last EDR Contact: 06/13/2013 Number of Days to Update: 41 Next Scheduled EDR Contact: 09/30/2013 Data Release Frequency: Varies TC3669805.1 s Page GR-19 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING EDR HIGH RISK HISTORICAL RECORDS EDR Exclusive Records EDR MGP: EDR Proprietary Manufactured Gas Plants The EDR Proprietary Manufactured Gas Plant Database includes records of coal gas plants (manufactured gas plants) compiled by EDR's researchers. Manufactured gas sites were used in the United States from the 1800's to 1950's to produce a gas that could be distributed and used as fuel. These plants used whale oil, rosin, coal, or a mixture of coal, oil, and water that also produced a significant amount of waste. Many of the byproducts of the gas production, such as coal tar (oily waste containing volatile and non-volatile chemicals), sludges, oils and other compounds are potentially hazardous to human health and the environment. The byproduct from this process was frequently disposed of directly at the plant site and can remain or spread slowly, serving as a continuous source of soil and groundwater contamination. Date of Government Version: N/A Source: EDR, Inc. Date Data Arrived at EDR: N/A Telephone: N/A Date Made Active in Reports: N/A Last EDR Contact: N/A Number of Days to Update: N/A Next Scheduled EDR Contact: N/A Data Release Frequency: No Update Planned EDR US Hist Auto Stat: EDR Exclusive Historic Gas Stations EDR has searched selected national collections of business directories and has collected listings of potential gas station/filling station/service station sites that were available to EDR researchers. EDR's review was limited to those categories of sources that might, in EDR's opinion, include gas station/filling station/service station establishments. The categories reviewed included, but were not limited to gas, gas station, gasoline station, filling station, auto, automobile repair, auto service station, service station, etc. This database falls within a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR's HRHR effort presents unique and sometimes proprietary data about past sites and operations that typically create environmental concerns, but may not show up in current government records searches. Date of Government Version: N/A Date Data Arrived at EDR: N/A Date Made Active in Reports: N/A Number of Days to Update: N/A Source: EDR, Inc. Telephone: N/A Last EDR Contact: N/A Next Scheduled EDR Contact: N/A Data Release Frequency: Varies EDR US Hist Cleaners: EDR Exclusive Historic Dry Cleaners EDR has searched selected national collections of business directories and has collected listings of potential dry cleaner sites that were available to EDR researchers. EDR's review was limited to those categories of sources that might, in EDR's opinion, include dry cleaning establishments. The categories reviewed included, but were not limited to dry cleaners, cleaners, laundry, laundromat, cleaning/laundry, wash & dry etc. This database falls within a category of information EDR classifies as "High Risk Historical Records", or HRHR. EDR's HRHR effort presents unique and sometimes proprietary data about past sites and operations that typically create environmental concerns, but may not show up in current government records searches. Date of Government Version: N/A Date Data Arrived at EDR: N/A Date Made Active in Reports: N/A Number of Days to Update: N/A Source: EDR, Inc. Telephone: N/A Last EDR Contact: N/A Next Scheduled EDR Contact: N/A Data Release Frequency: Varies EDR US Hist Auto Stat: EDR Proprietary Historic Gas Stations - Cole Date of Government Version: N/A Date Data Arrived at EDR: N/A Date Made Active in Reports: N/A Number of Days to Update: N/A Source: N/A Telephone: N/A Last EDR Contact: N/A Next Scheduled EDR Contact: N/A Data Release Frequency: Varies TC3669805.1 s Page GR-20 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING EDR US Hist Cleaners: EDR Proprietary Historic Dry Cleaners - Cole Date of Government Version: N/A Date Data Arrived at EDR: N/A Date Made Active in Reports: N/A Number of Days to Update: N/A OTHER DATABASE(S) Source: N/A Telephone: N/A Last EDR Contact: N/A Next Scheduled EDR Contact: N/A Data Release Frequency: Varies Depending on the geographic area covered by this report, the data provided in these specialty databases may or may not be complete. For example, the existence of wetlands information data in a specific report does not mean that all wetlands in the area covered by the report are included. Moreover, the absence of any reported wetlands information does not necessarily mean that wetlands do not exist in the area covered by the report. CT MANIFEST: Hazardous Waste Manifest Data Facility and manifest data. Manifest is a document that lists and tracks hazardous waste from the generator through transporters to a tsd facility. Date of Government Version: 05/20/2013 Source: Department of Energy & Environmental Protection Date Data Arrived at EDR: 05/21/2013 Telephone: 860-424-3375 Date Made Active in Reports: 06/27/2013 Last EDR Contact: 05/21/2013 Number of Days to Update: 37 Next Scheduled EDR Contact: 09/02/2013 Data Release Frequency: Annually NJ MANIFEST: Manifest Information Hazardous waste manifest information. Date of Government Version: 12/31/2011 Source: Department of Environmental Protection Date Data Arrived at EDR: 07/19/2012 Telephone: N/A Date Made Active in Reports: 08/28/2012 Last EDR Contact: 04/19/2013 Number of Days to Update: 40 Next Scheduled EDR Contact: 07/29/2013 Data Release Frequency: Annually NY MANIFEST: Facility and Manifest Data Manifest is a document that lists and tracks hazardous waste from the generator through transporters to a TSD facility. Date of Government Version: 05/01/2013 Source: Department of Environmental Conservation Date Data Arrived at EDR: 05/09/2013 Telephone: 518-402-8651 Date Made Active in Reports: 07/10/2013 Last EDR Contact: 05/09/2013 Number of Days to Update: 62 Next Scheduled EDR Contact: 08/19/2013 Data Release Frequency: Annually PA MANIFEST: Manifest Information Hazardous waste manifest information. Date of Government Version: 12/31/2011 Source: Department of Environmental Protection Date Data Arrived at EDR: 07/23/2012 Telephone: 717-783-8990 Date Made Active in Reports: 09/18/2012 Last EDR Contact: 07/18/2013 Number of Days to Update: 57 Next Scheduled EDR Contact: 11/04/2013 Data Release Frequency: Annually RI MANIFEST: Manifest information Hazardous waste manifest information Date of Government Version: 12/31/2011 Source: Department of Environmental Management Date Data Arrived at EDR: 06/22/2012 Telephone: 401-222-2797 Date Made Active in Reports: 07/31/2012 Last EDR Contact: 05/28/2013 Number of Days to Update: 39 Next Scheduled EDR Contact: 09/09/2013 Data Release Frequency: Annually TC3669805.1 s Page GR-21 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING WI MANIFEST: Manifest Information Hazardous waste manifest information. Date of Government Version: 12/31/2011 Date Data Arrived at EDR: 07/19/2012 Date Made Active in Reports: 09/27/2012 Number of Days to Update: 70 Source: Department of Natural Resources Telephone: N/A Last EDR Contact: 07/17/2013 Next Scheduled EDR Contact: 09/30/2013 Data Release Frequency: Annually Oil/Gas Pipelines: This data was obtained by EDR from the USGS in 1994. It is referred to by USGS as GeoData Digital Line Graphs from 1:100,000-Scale Maps. It was extracted from the transportation category including some oil, but primarily gas pipelines. Electric Power Transmission Line Data Source: Rextag Strategies Corp. Telephone: (281) 769-2247 U.S. Electric Transmission and Power Plants Systems Digital GIS Data Sensitive Receptors: There are individuals deemed sensitive receptors due to their fragile immune systems and special sensitivity to environmental discharges. These sensitive receptors typically include the elderly, the sick, and children. While the location of all sensitive receptors cannot be determined, EDR indicates those buildings and facilities - schools, daycares, hospitals, medical centers, and nursing homes - where individuals who are sensitive receptors are likely to be located. AHA Hospitals: Source: American Hospital Association, Inc. Telephone: 312-280-5991 The database includes a listing of hospitals based on the American Hospital Association's annual survey of hospitals. Medical Centers: Provider of Services Listing Source: Centers for Medicare & Medicaid Services Telephone:410-786-3000 A listing of hospitals with Medicare provider number, produced by Centers of Medicare & Medicaid Services, a federal agency within the U.S. Department of Health and Human Services. Nursing Homes Source: National Institutes of Health Telephone: 301-594-6248 Information on Medicare and Medicaid certified nursing homes in the United States. Public Schools Source: National Center for Education Statistics Telephone:202-502-7300 The National Center for Education Statistics' primary database on elementary and secondary public education in the United States. It is a comprehensive, annual, national statistical database of all public elementary and secondary schools and school districts, which contains data that are comparable across all states. Private Schools Source: National Center for Education Statistics Telephone: 202-502-7300 The National Center for Education Statistics' primary database on private school locations in the United States. Daycare Centers: Child Care Facility List Source: Department of Health & Human Services Telephone: 919-662-4499 Flood Zone Data: This data, available in select counties across the country, was obtained by EDR in 2003 & 2011 from the Federal Emergency Management Agency (FEMA). Data depicts 100-year and 500-year flood zones as defined by FEMA. NWI: National Wetlands Inventory. This data, available in select counties across the country, was obtained by EDR in 2002 and 2005 from the U.S. Fish and Wildlife Service. State Wetlands Data: Wetlands Inventory Source: Department of Environment & Natural Resources Telephone: 919-733-2090 TC3669805.1 s Page GR-22 GOVERNMENT RECORDS SEARCHED /DATA CURRENCY TRACKING Scanned Digital USGS 7.5' Topographic Map (DRG) Source: United States Geologic Survey A digital raster graphic (DRG) is a scanned image of a U.S. Geological Survey topographic map. The map images are made by scanning published paper maps on high -resolution scanners. The raster image is georeferenced and fit to the Universal Transverse Mercator (UTM) projection. STREET AND ADDRESS INFORMATION © 2010 Tele Atlas North America, Inc. All rights reserved. This material is proprietary and the subject of copyright protection and other intellectual property rights owned by or licensed to Tele Atlas North America, Inc. The use of this material is subject to the terms of a license agreement. You will be held liable for any unauthorized copying or disclosure of this material. TC3669805.1 s Page GR-23 GEOCHECK®- PHYSICAL SETTING SOURCE ADDENDUM TARGET PROPERTY ADDRESS TOWN OF CHAPEL HILL 828 MARTIN LUTHER KING JR BLVD CHAPEL HILL, NC 27514 TARGET PROPERTY COORDINATES Latitude (North): Longitude (West): Universal Tranverse Mercator: UTM X (Meters): UTM Y (Meters): Elevation: USGS TOPOGRAPHIC MAP Target Property Map: Most Recent Revision 35.9267 - 35' 55' 36.12" 79.0534 - 79' 3' 12.24" Zone 17 675619.4 3977369.0 327 ft. above sea level 35079-H1 CHAPEL HILL, NC 1993 EDR's GeoCheck Physical Setting Source Addendum is provided to assist the environmental professional in forming an opinion about the impact of potential contaminant migration. Assessment of the impact of contaminant migration generally has two principal investigative components: 1. Groundwater flow direction, and 2. Groundwater flow velocity. Groundwater flow direction may be impacted by surface topography, hydrology, hydrogeology, characteristics of the soil, and nearby wells. Groundwater flow velocity is generally impacted by the nature of the geologic strata. TC3669805.1 s Page A-1 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY GROUNDWATER FLOW DIRECTION INFORMATION Groundwater flow direction for a particular site is best determined by a qualified environmental professional using site -specific well data. If such data is not reasonably ascertainable, it may be necessary to rely on other sources of information, such as surface topographic information, hydrologic information, hydrogeologic data collected on nearby properties, and regional groundwater flow information (from deep aquifers). TOPOGRAPHIC INFORMATION Surface topography may be indicative of the direction of surficial groundwater flow. This information can be used to assist the environmental professional in forming an opinion about the impact of nearby contaminated properties or, should contamination exist on the target property, what downgradient sites might be impacted. TARGET PROPERTY TOPOGRAPHY General Topographic Gradient: General South SURROUNDING TOPOGRAPHY: ELEVATION PROFILES C W Of a W N W W A West Target Property Elevation: 327 ft. TIP TIP 0 East 1/2 1 Miles Source: Topography has been determined from the USGS 7.5' Digital Elevation Model and should be evaluated on a relative (not an absolute) basis. Relative elevation information between sites of close proximity should be field verified. TC3669805.1 s Page A-2 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY HYDROLOGIC INFORMATION Surface water can act as a hydrologic barrier to groundwater flow. Such hydrologic information can be used to assist the environmental professional in forming an opinion about the impact of nearby contaminated properties or, should contamination exist on the target property, what downgradient sites might be impacted. Refer to the Physical Setting Source Map following this summary for hydrologic information (major waterways and bodies of water). FEMA FLOOD ZONE Target Property County ORANGE,NC Flood Plain Panel at Target Property: Additional Panels in search area: NATIONAL WETLAND INVENTORY NWI Quad at Target Property CHAPEL HILL HYDROGEOLOGIC INFORMATION FEMA Flood Electronic Data YES - refer to the Overview Map and Detail Map 37135C - FEMA DFIRM Flood data Not Reported NWI Electronic Data Coverage YES - refer to the Overview Map and Detail Map Hydrogeologic information obtained by installation of wells on a specific site can often be an indicator of groundwater flow direction in the immediate area. Such hydrogeologic information can be used to assist the environmental professional in forming an opinion about the impact of nearby contaminated properties or, should contamination exist on the target property, what downgradient sites might be impacted. AQUIFLOW® Search Radius: 1.000 Mile. EDR has developed the AQUIFLOW Information System to provide data on the general direction of groundwater flow at specific points. EDR has reviewed reports submitted by environmental professionals to regulatory authorities at select sites and has extracted the date of the report, groundwater flow direction as determined hydrogeologically, and the depth to water table. LOCATION GENERAL DIRECTION MAP ID FROM TP GROUNDWATER FLOW Not Reported TC3669805.1 s Page A-3 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY GROUNDWATER FLOW VELOCITY INFORMATION Groundwater flow velocity information for a particular site is best determined by a qualified environmental professional using site specific geologic and soil strata data. If such data are not reasonably ascertainable, it may be necessary to rely on other sources of information, including geologic age identification, rock stratigraphic unit and soil characteristics data collected on nearby properties and regional soil information. In general, contaminant plumes move more quickly through sandy -gravelly types of soils than silty -clayey types of soils. GEOLOGIC INFORMATION IN GENERAL AREA OF TARGET PROPERTY Geologic information can be used by the environmental professional in forming an opinion about the relative speed at which contaminant migration may be occurring. :AZa :F� 1:L1111 0:L1011411 ki 1 I I GEOLOGIC AGE IDENTIFICATION Era: Mesozoic Category: Stratified Sequence System: Triassic Series: Triassic Code: Tr (decoded above as Era, System & Series) Geologic Age and Rock Stratigraphic Unit Source: P.G. Schruben, R.E. Arndt and W.J. Bawiec, Geology of the Conterminous U.S. at 1:2,500,000 Scale - a digital representation of the 1974 P.B. King and H.M. Beikman Map, USGS Digital Data Series DDS - 11 (1994). TC3669805.1 s Page A-4 SSURGO SOIL MAP - 3669805.1s Target Property SSURGO Soil Water 0 1116 118 14 Miles SITE NAME: Town of Chapel Hill CLIENT: Falcon Engineering, Inc. ADDRESS: 828 Martin Luther King Jr Blvd CONTACT: Josh Dunbar Chapel Hill NC 27514 INQUIRY #: 3669805.1s LAT/LONG: 35.9267 / 79.0534 DATE: July 18, 2013 4:35 pm Copyright cg 2013 EDR, Inc. cC, 2010 Te le Atlas Re 1. 07/2009. GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY DOMINANT SOIL COMPOSITION IN GENERAL AREA OF TARGET PROPERTY The U.S. Department of Agriculture's (USDA) Soil Conservation Service (SCS) leads the National Cooperative Soil Survey (NCSS) and is responsible for collecting, storing, maintaining and distributing soil survey information for privately owned lands in the United States. A soil map in a soil survey is a representation of soil patterns in a landscape. The following information is based on Soil Conservation Service SSURGO data. Soil Map ID: 1 Soil Component Name: Tatum Soil Surface Texture: silt loam Hydrologic Group: Class C - Slow infiltration rates. Soils with layers impeding downward movement of water, or soils with moderately fine or fine textures. Soil Drainage Class: Well drained Hydric Status: Not hydric Corrosion Potential - Uncoated Steel: High Depth to Bedrock Min: > 0 inches Depth to Watertable Min: > 0 inches Soil Layer Information Boundary Classification Saturated hydraulic conductivity Soil Reaction Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil micro m/sec (pH) 1 0 inches 7 inches silt loam Silt -Clay Not reported Max: 14 Max: Min: Materials (more Min: 0 than 35 pct. passing No. 200), Silty Soils. 2 7 inches 50 inches silty clay loam Silt -Clay Not reported Max: 14 Max: Min: Materials (more Min: 0 than 35 pct. passing No. 200), Silty Soils. 3 50 inches 59 inches weathered Silt -Clay Not reported Max: 14 Max: Min: bedrock Materials (more Min: 0 than 35 pct. passing No. 200), Silty Soils. TC3669805.1 s Page A-6 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY Soil Map ID: 2 Soil Component Name: Soil Surface Texture: Hydrologic Group: Urban land variable Class C - Slow infiltration rates. Soils with layers impeding downward movement of water, or soils with moderately fine or fine textures. Soil Drainage Class: Hydric Status: Not hydric Corrosion Potential - Uncoated Steel: Not Reported Depth to Bedrock Min: > 0 inches Depth to Watertable Min: > 0 inches Soil Layer Information Boundary Classification Saturated hydraulic conductivity Soil Reaction Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil micro m/sec (pH) 1 0 inches 5 inches variable Not reported Not reported Max: Max: Min: Min: Soil Map ID: 3 Soil Component Name: Wedowee Soil Surface Texture: sandy loam Hydrologic Group: Class B - Moderate infiltration rates. Deep and moderately deep, moderately well and well drained soils with moderately coarse textures. Soil Drainage Class: Well drained Hydric Status: Not hydric Corrosion Potential - Uncoated Steel: Moderate Depth to Bedrock Min: > 0 inches Depth to Watertable Min: > 0 inches TC3669805.1 s Page A-7 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY Soil Layer Information Boundary Classification Saturated hydraulic conductivity Soil Reaction Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil micro m/sec (pH) 1 0 inches 11 inches sandy loam Silt -Clay COARSE -GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Sands, Min: 4 Min: 3.6 than 35 pct. Sands with fines, passing No. Clayey sand. 200), Silty Soils. 2 11 inches 14 inches sandy clay loam Silt -Clay COARSE -GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Sands, Min: 4 Min: 3.6 than 35 pct. Sands with fines, passing No. Clayey sand. 200), Silty Soils. 3 14 inches 27 inches sandy clay Silt -Clay COARSE -GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Sands, Min: 4 Min: 3.6 than 35 pct. Sands with fines, passing No. Clayey sand. 200), Silty Soils. 4 27 inches 78 inches sandy loam Silt -Clay COARSE -GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Sands, Min: 4 Min: 3.6 than 35 pct. Sands with fines, passing No. Clayey sand. 200), Silty Soils. Soil Map ID: 4 Soil Component Name: Tatum Soil Surface Texture: silt loam Hydrologic Group: Class B - Moderate infiltration rates. Deep and moderately deep, moderately well and well drained soils with moderately coarse textures. Soil Drainage Class: Well drained Hydric Status: Not hydric Corrosion Potential - Uncoated Steel: High Depth to Bedrock Min: > 0 inches Depth to Watertable Min: > 0 inches TC3669805.1 s Page A-8 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY Soil Layer Information Boundary Classification Saturated hydraulic conductivity Soil Reaction Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil micro m/sec (pH) 1 0 inches 5 inches silt loam Silt -Clay Not reported Max: 0.42 Max: Min: Materials (more Min: 0 than 35 pct. passing No. 200), Silty Soils. 2 5 inches 53 inches silty clay Silt -Clay Not reported Max: 0.42 Max: Min: Materials (more Min: 0 than 35 pct. passing No. 200), Silty Soils. 3 53 inches 62 inches weathered Silt -Clay Not reported Max: 0.42 Max: Min: bedrock Materials (more Min: 0 than 35 pct. passing No. 200), Silty Soils. Soil Map ID: 5 Soil Component Name: Chewacla Soil Surface Texture: loam Hydrologic Group: Class C - Slow infiltration rates. Soils with layers impeding downward movement of water, or soils with moderately fine or fine textures. Soil Drainage Class: Somewhat poorly drained Hydric Status: Partially hydric Corrosion Potential - Uncoated Steel: High Depth to Bedrock Min: > 0 inches Depth to Watertable Min: > Winches TC3669805.1 s Page A-9 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY Soil Layer Information Boundary Classification Saturated hydraulic conductivity Soil Reaction Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil micro m/sec (pH) 1 0 inches 5 inches loam Silt -Clay COARSE -GRAINED Max: 141 Max: 6.5 Materials (more SOILS, Sands, Min: 14 Min: 3.6 than 35 pct. Sands with fines, passing No. Clayey sand. 200), Clayey COARSE -GRAINED Soils. SOILS, Sands, Sands with fines, Silty Sand. 2 5 inches 14 inches silty clay loam Silt -Clay COARSE -GRAINED Max: 141 Max: 6.5 Materials (more SOILS, Sands, Min: 14 Min: 3.6 than 35 pct. Sands with fines, passing No. Clayey sand. 200), Clayey COARSE -GRAINED Soils. SOILS, Sands, Sands with fines, Silty Sand. 3 14 inches 22 inches sandy clay loam Silt -Clay COARSE -GRAINED Max: 141 Max: 6.5 Materials (more SOILS, Sands, Min: 14 Min: 3.6 than 35 pct. Sands with fines, passing No. Clayey sand. 200), Clayey COARSE -GRAINED Soils. SOILS, Sands, Sands with fines, Silty Sand. 4 22 inches 50 inches clay loam Silt -Clay COARSE -GRAINED Max: 141 Max: 6.5 Materials (more SOILS, Sands, Min: 14 Min: 3.6 than 35 pct. Sands with fines, passing No. Clayey sand. 200), Clayey COARSE -GRAINED Soils. SOILS, Sands, Sands with fines, Silty Sand. 5 50 inches 59 inches loamy fine sand Silt -Clay COARSE -GRAINED Max: 141 Max: 6.5 Materials (more SOILS, Sands, Min: 14 Min: 3.6 than 35 pct. Sands with fines, passing No. Clayey sand. 200), Clayey COARSE -GRAINED Soils. SOILS, Sands, Sands with fines, Silty Sand. Soil Map ID: 6 Soil Component Name: Georgeville Soil Surface Texture: silt loam Hydrologic Group: Class B - Moderate infiltration rates. Deep and moderately deep, moderately well and well drained soils with moderately coarse textures. Soil Drainage Class: Well drained TC3669805.1 s Page A-10 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY Hydric Status: Not hydric Corrosion Potential - Uncoated Steel: High Depth to Bedrock Min: > 0 inches Depth to Watertable Min: > 0 inches Soil Layer Information Boundary Classification Saturated hydraulic conductivity Soil Reaction Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil micro m/sec (pH) 1 0 inches 7 inches silt loam Silt -Clay FINE-GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Silts and Min: 4 Min: 4.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), silt. Soils. 2 7 inches 14 inches clay loam Silt -Clay FINE-GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Silts and Min: 4 Min: 4.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), silt. Soils. 3 14 inches 44 inches clay Silt -Clay FINE-GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Silts and Min: 4 Min: 4.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), silt. Soils. 4 44 inches 78 inches loam Silt -Clay FINE-GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Silts and Min: 4 Min: 4.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), silt. Soils. Soil Map ID: 7 Soil Component Name: Georgeville Soil Surface Texture: silt loam Hydrologic Group: Class B - Moderate infiltration rates. Deep and moderately deep, moderately well and well drained soils with moderately coarse textures. Soil Drainage Class: Well drained TC3669805.1 s Page A-11 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY Hydric Status: Not hydric Corrosion Potential - Uncoated Steel: High Depth to Bedrock Min: > 0 inches Depth to Watertable Min: > 0 inches Soil Layer Information Boundary Classification Saturated hydraulic conductivity Soil Reaction Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil micro m/sec (pH) 1 0 inches 5 inches silt loam Silt -Clay FINE-GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Silts and Min: 4 Min: 4.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), silt. Soils. 2 5 inches 35 inches clay Silt -Clay FINE-GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Silts and Min: 4 Min: 4.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), silt. Soils. 3 35 inches 78 inches silt loam Silt -Clay FINE-GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Silts and Min: 4 Min: 4.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), silt. Soils. Soil Map ID: 8 Soil Component Name: Appling Soil Surface Texture: sandy loam Hydrologic Group: Class B - Moderate infiltration rates. Deep and moderately deep, moderately well and well drained soils with moderately coarse textures. Soil Drainage Class: Well drained Hydric Status: Not hydric Corrosion Potential - Uncoated Steel: Moderate Depth to Bedrock Min: > 0 inches Depth to Watertable Min: > 0 inches TC3669805.1 s Page A-12 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY Soil Layer Information Boundary Classification Saturated hydraulic conductivity Soil Reaction Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil micro m/sec (pH) 1 0 inches 7 inches sandy loam Granular COARSE -GRAINED Max: 42 Max: 5.5 materials (35 SOILS, Sands, Min: 14 Min: 4.5 pct. or less Sands with fines, passing No. Silty Sand. 200), Silty, or Clayey Gravel and Sand. 2 11 inches 48 inches sandy clay Granular COARSE -GRAINED Max: 42 Max: 5.5 materials (35 SOILS, Sands, Min: 14 Min: 4.5 pct. or less Sands with fines, passing No. Silty Sand. 200), Silty, or Clayey Gravel and Sand. 3 48 inches 55 inches clay loam Granular COARSE -GRAINED Max: 42 Max: 5.5 materials (35 SOILS, Sands, Min: 14 Min: 4.5 pct. or less Sands with fines, passing No. Silty Sand. 200), Silty, or Clayey Gravel and Sand. 4 55 inches 64 inches sandy loam Granular COARSE -GRAINED Max: 42 Max: 5.5 materials (35 SOILS, Sands, Min: 14 Min: 4.5 pct. or less Sands with fines, passing No. Silty Sand. 200), Silty, or Clayey Gravel and Sand. 5 7 inches 11 inches sandy loam Granular COARSE -GRAINED Max: 42 Max: 5.5 materials (35 SOILS, Sands, Min: 14 Min: 4.5 pct. or less Sands with fines, passing No. Silty Sand. 200), Silty, or Clayey Gravel and Sand. Soil Map ID: 9 Soil Component Name: Altavista Soil Surface Texture: fine sandy loam Hydrologic Group: Class C - Slow infiltration rates. Soils with layers impeding downward movement of water, or soils with moderately fine or fine textures. Soil Drainage Class: Moderately well drained TC3669805.1 s Page A-13 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY Hydric Status: Partially hydric Corrosion Potential - Uncoated Steel: Moderate Depth to Bedrock Min: > 0 inches Depth to Watertable Min: > 61 inches Soil Layer Information Boundary Classification Saturated hydraulic conductivity Soil Reaction Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil micro m/sec (pH) 1 0 inches 9 inches fine sandy loam Silt -Clay FINE-GRAINED Max: 14 Max: 6 Min: Materials (more SOILS, Silts and Min: 4 3.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), Lean Clay Soils. 2 9 inches 59 inches Silt -Clay FINE-GRAINED Max: 14 Max: 6 Min: Materials (more SOILS, Silts and Min: 4 3.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), Lean Clay Soils. Soil Map ID: 10 Soil Component Name: Iredell Soil Surface Texture: fine sandy loam Hydrologic Group: Class C/D - Drained/undrained hydrology class of soils that can be drained and classified. Soil Drainage Class: Moderately well drained Hydric Status: Not hydric Corrosion Potential - Uncoated Steel: High Depth to Bedrock Min: > 0 inches Depth to Watertable Min: > 46 inches TC3669805.1 s Page A-14 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY Soil Layer Information Boundary Classification Saturated hydraulic conductivity Soil Reaction Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil micro m/sec (pH) 1 0 inches 5 inches fine sandy loam Silt -Clay COARSE -GRAINED Max: 14 Max: 8.4 Materials (more SOILS, Sands, Min: 1.4 Min: 6.6 than 35 pct. Sands with fines, passing No. Silty Sand. 200), Silty Soils. 2 5 inches 24 inches clay Silt -Clay COARSE -GRAINED Max: 14 Max: 8.4 Materials (more SOILS, Sands, Min: 1.4 Min: 6.6 than 35 pct. Sands with fines, passing No. Silty Sand. 200), Silty Soils. 3 24 inches 27 inches clay loam Silt -Clay COARSE -GRAINED Max: 14 Max: 8.4 Materials (more SOILS, Sands, Min: 1.4 Min: 6.6 than 35 pct. Sands with fines, passing No. Silty Sand. 200), Silty Soils. 4 27 inches 64 inches loam Silt -Clay COARSE -GRAINED Max: 14 Max: 8.4 Materials (more SOILS, Sands, Min: 1.4 Min: 6.6 than 35 pct. Sands with fines, passing No. Silty Sand. 200), Silty Soils. Soil Map ID: 11 Soil Component Name: Georgeville Soil Surface Texture: silt loam Hydrologic Group: Class B - Moderate infiltration rates. Deep and moderately deep, moderately well and well drained soils with moderately coarse textures. Soil Drainage Class: Well drained Hydric Status: Not hydric Corrosion Potential - Uncoated Steel: High Depth to Bedrock Min: > 0 inches Depth to Watertable Min: > 0 inches TC3669805.1 s Page A-15 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY Soil Layer Information Boundary Classification Saturated hydraulic conductivity Soil Reaction Layer Upper Lower Soil Texture Class AASHTO Group Unified Soil micro m/sec (pH) 1 0 inches 7 inches silt loam Silt -Clay FINE-GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Silts and Min: 4 Min: 4.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), silt. Soils. 2 7 inches 61 inches clay Silt -Clay FINE-GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Silts and Min: 4 Min: 4.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), silt. Soils. 3 61 inches 78 inches silt loam Silt -Clay FINE-GRAINED Max: 14 Max: 5.5 Materials (more SOILS, Silts and Min: 4 Min: 4.5 than 35 pct. Clays (liquid passing No. limit less than 200), Silty 50%), silt. Soils. LOCAL / REGIONAL WATER AGENCY RECORDS EDR Local/Regional Water Agency records provide water well information to assist the environmental professional in assessing sources that may impact ground water flow direction, and in forming an opinion about the impact of contaminant migration on nearby drinking water wells. WELL SEARCH DISTANCE INFORMATION DATABASE SEARCH DISTANCE (miles) Federal USGS 1.000 Federal FRDS PWS Nearest PWS within 1 mile State Database 1.000 FEDERAL USGS WELL INFORMATION MAP ID WELL ID 1 USGS40000891849 2 USGS40000891888 3 USGS40000891737 LOCATION FROM TP 1/4 - 1/2 Mile WNW 1/4 - 1/2 Mile NNE 1/2 - 1 Mile SSE TC3669805.1 s Page A-16 GEOCHECK®- PHYSICAL SETTING SOURCE SUMMARY FEDERAL FRDS PUBLIC WATER SUPPLY SYSTEM INFORMATION LOCATION MAP ID WELL ID FROM TP No PWS System Found Note: PWS System location is not always the same as well location. STATE DATABASE WELL INFORMATION LOCATION MAP ID WELL ID FROM TP No Wells Found OTHER STATE DATABASE INFORMATION NORTH CAROLINA NATURAL HERITAGE ELEMENT OCCURRENCES ID Class NC50005306 Plants NC50005999 Plants NC50007525 Animal NC50009897 Plants NC50013273 Non Vascular NORTH CAROLINA SIGNIFICANT NATURAL HERITAGE AREAS DATABASE: ID Name NC10002135 BOLIN CREEK NC10002136 BATTLE PARK TC3669805.1 s Page A-17 PHYSICAL SETTING SOURCE MAP-3669805.1s NCounty Boundary N Major Roads N Contour Lines E Airports OO Earthquake epicenter, Richter 5 or greater ® Water Wells © Public Water Supply Wells ® Cluster of Multiple Icons 0 114 1/2 1 Miles Groundwater Flow Direction E2 Wildlife Areas c Indeterminate Groundwater Flow at Location 0 Natural Areas c v Groundwater Flow Varies at Location o Rare & Endangered Species SITE NAME: Town of Chapel Hill CLIENT: Falcon Engineering, Inc. ADDRESS: 828 Martin Luther King Jr Blvd CONTACT: Josh Dunbar Chapel Hill NC 27514 INQUIRY #: 3669805.1s LAT/LONG: 35.9267 / 79.0534 DATE: July 18, 2013 4:35 pm Copyright cg 2013 EDR, Inc. Is 2010 Tele Atlas Rel 07/2009. Map ID Direction Distance Elevation GEOCHECK®- PHYSICAL SETTING SOURCE MAP FINDINGS Database EDR ID Number 1 WNW FED USGS 1/4 - 1/2 Mile Higher Org.Identifier: USGS-NC Formal name: USGS North Carolina Water Science Center Monloc Identifier: USGS-355543079033001 Monloc name: OR-245 Monloc type: Well Monloc desc: Not Reported Huc code: 03030002 Drainagearea value: Not Reported Drainagearea Units: Not Reported Contrib drainagearea: Not Reported Contrib drainagearea units: Not Reported Latitude: 35.9287547 Longitude: -79.0580668 Sourcemap scale: 24000 Horiz Acc measure: 5 Horiz Acc measure units: seconds Horiz Collection method: Interpolated from map Horiz coord refsys: NAD83 Vert measure val: 420 Vert measure units: feet Vertacc measure val: 5 Vert accmeasure units: feet Vertcollection method: Interpolated from topographic map Vert coord refsys: NGVD29 Countrycode: US Aquifername: Piedmont and Blue Ridge crystalline -rock aquifers Formation type: Felsic Metaigneous Rock Aquifer type: Not Reported Construction date: 19770818 Welldepth: 220 Welldepth units: ft Wellholedepth: Not Reported Wellholedepth units: Not Reported Ground -water levels, Number of Measurements: 1 Feet below Feet to Date Surface Sealevel 1977-08-18 30.0 2 NNE 1/4 - 1/2 Mile Higher Org. Identifier: Formal name: Monloc Identifier: Monloc name: Monloc type: Monloc desc: Huc code: Drainagearea Units: Contrib drainagearea units Longitude: Horiz Acc measure: Horiz Collection method: Horiz coord refsys: Vert measure units: Vert accmeasure units: Vertcollection method: Vert coord refsys: Aquifername: Formation type: 94111bYcy USGS-NC USGS North Carolina Water Science Center U S G S-355559079025901 OR-246 Well Not Reported 03030002 Drainagearea value: Not Reported Not Reported Contrib drainagearea: Not Reported Not Reported Latitude: 35.9331991 -79.0494555 Sourcemap scale: 24000 5 Horiz Acc measure units: seconds Interpolated from map NAD83 Vert measure val: 395 feet Vertacc measure val: 5 feet Interpolated from topographic map NGVD29 Countrycode: US Piedmont and Blue Ridge crystalline -rock aquifers Felsic Metaigneous Rock USGS40000891849 USGS40000891888 TC3669805.1 s Page A-19 GEOCHECK®- PHYSICAL SETTING SOURCE MAP FINDINGS Aquifer type: Not Reported Construction date: 19810421 Welldepth: 420 Welldepth units: ft Wellholedepth: Not Reported Wellholedepth units: Not Reported Ground -water levels, Number of Measurements: 1 Feet below Feet to Date Surface Sealevel 1981-04-21 25.0 3 SSE FED USGS 1/2 - 1 Mile Higher Org.Identifier: USGS-NC Formal name: USGS North Carolina Water Science Center Monloc Identifier: USGS-355459079030201 Monloc name: OR-240 Monloc type: Well Monloc desc: Not Reported Huc code: 03030002 Drainagearea value: Not Reported Drainagearea Units: Not Reported Contrib drainagearea: Not Reported Contrib drainagearea units: Not Reported Latitude: 35.9165329 Longitude: -79.0502888 Sourcemap scale: 24000 Horiz Acc measure: 5 Horiz Acc measure units: seconds Horiz Collection method: Interpolated from map Horiz coord refsys: NAD83 Vert measure val: 450 Vert measure units: feet Vertacc measure val: 5 Vert accmeasure units: feet Vertcollection method: Interpolated from topographic map Vert coord refsys: NGVD29 Countrycode: US Aquifername: Piedmont and Blue Ridge crystalline -rock aquifers Formation type: Felsic Metaigneous Rock Aquifer type: Not Reported Construction date: 19770221 Welldepth: 200 Welldepth units: ft Wellholedepth: Not Reported Wellholedepth units: Not Reported Ground -water levels, Number of Measurements: 1 Feet below Feet to Date Surface Sealevel 1977-02-21 30.0 USGS40000891737 TC3669805.1 s Page A-20 GEOCHECK®- PHYSICAL SETTING SOURCE MAP FINDINGS Map ID Direction Distance Database EDR ID Number GIS ID: Classification by Type: Occurrence Status: GIS ID: Classification by Type: Occurrence Status: 52003 Plants Historic, no evidence of destruction 92665 Plants Historic, no evidence of destruction GISID: 442955 Classification by Type: Animal Occurrence Status: X GIS ID: 61771 Classification by Type: Plants Occurrence Status: Historic, no evidence of destruction GIS ID: Classification by Type: Occurrence Status: Site Name: Quality: Acres per Polygon: 42893 Non Vascular Extant BOLIN CREEK Not Reported 242.78 NC_NHEO NC50005306 NC_NHEO NC50005999 NC_NHEO NC50007525 NC_NHEO NC50009897 NC_NHEO NC50013273 NC_SNHA NC10002135 NC_SNHA NC10002136 TC3669805.1 s Page A-21 GEOCHECK®- PHYSICAL SETTING SOURCE MAP FINDINGS North Carolina - Significant Natural Heritage Areas: Site Name: Quality: Acres per Polygon: BATTLE PARK Not Reported 61.53 TC3669805.1 s Page A-22 GEOCHECK®- PHYSICAL SETTING SOURCE MAP FINDINGS RADON AREA RADON INFORMATION State Database: NC Radon Radon Test Results Num Results Avg pCi/L Min pCi/L Max pCi/L 10 6.18 0.3 4.5 7 0.74 0.3 2.2 Federal EPA Radon Zone for ORANGE County: 3 Note: Zone 1 indoor average level > 4 pCi/L. Zone 2 indoor average level — 2 pCi/L and — 4 pCi/L. Zone 3 indoor average level < 2 pCi/L. Federal Area Radon Information for Zip Code: 27514 Number of sites tested: 5 Area Average Activity % <4 pCi/L % 4-20 pCi/L Living Area - 1 st Floor 1.020 pCi/L 100% 0% Living Area - 2nd Floor Not Reported Not Reported Not Reported Basement 0.867 pCi/L 100% 0% % >20 eCi/L 0% Not Reported 0% TC3669805.1 s Page A-23 PHYSICAL SETTING SOURCE RECORDS SEARCHED TOPOGRAPHIC INFORMATION USGS 7.5' Digital Elevation Model (DEM) Source: United States Geologic Survey EDR acquired the USGS 7.5' Digital Elevation Model in 2002 and updated it in 2006. The 7.5 minute DEM corresponds to the USGS 1:24,000- and 1:25,000-scale topographic quadrangle maps. The DEM provides elevation data with consistent elevation units and projection. Scanned Digital USGS 7.5' Topographic Map (DRG) Source: United States Geologic Survey A digital raster graphic (DRG) is a scanned image of a U.S. Geological Survey topographic map. The map images are made by scanning published paper maps on high -resolution scanners. The raster image is georeferenced and fit to the Universal Transverse Mercator (UTM) projection. HYDROLOGIC INFORMATION Flood Zone Data: This data, available in select counties across the country, was obtained by EDR in 2003 & 2011 from the Federal Emergency Management Agency (FEMA). Data depicts 100-year and 500-year flood zones as defined by FEMA. NWI: National Wetlands Inventory. This data, available in select counties across the country, was obtained by EDR in 2002 and 2005 from the U.S. Fish and Wildlife Service. State Wetlands Data: Wetlands Inventory Source: Department of Environment & Natural Resources Telephone: 919-733-2090 HYDROGEOLOGIC INFORMATION AQUIFLOWR Information System Source: EDR proprietary database of groundwater flow information EDR has developed the AQUIFLOW Information System (AIS) to provide data on the general direction of groundwater flow at specific points. EDR has reviewed reports submitted to regulatory authorities at select sites and has extracted the date of the report, hydrogeologically determined groundwater flow direction and depth to water table information. GEOLOGIC INFORMATION Geologic Age and Rock Stratigraphic Unit Source: P.G. Schruben, R.E. Arndt and W.J. Bawiec, Geology of the Conterminous U.S. at 1:2,500,000 Scale - A digital representation of the 1974 P.B. King and H.M. Beikman Map, USGS Digital Data Series DDS - 11 (1994). STATSGO: State Soil Geographic Database Source: Department of Agriculture, Natural Resources Conservation Services The U.S. Department of Agriculture's (USDA) Natural Resources Conservation Service (NRCS) leads the national Conservation Soil Survey (NCSS) and is responsible for collecting, storing, maintaining and distributing soil survey information for privately owned lands in the United States. A soil map in a soil survey is a representation of soil patterns in a landscape. Soil maps for STATSGO are compiled by generalizing more detailed (SSURGO) soil survey maps. SSURGO: Soil Survey Geographic Database Source: Department of Agriculture, Natural Resources Conservation Services (NRCS) Telephone: 800-672-5559 SSURGO is the most detailed level of mapping done by the Natural Resources Conservation Services, mapping scales generally range from 1:12,000 to 1:63,360. Field mapping methods using national standards are used to construct the soil maps in the Soil Survey Geographic (SSURGO) database. SSURGO digitizing duplicates the original soil survey maps. This level of mapping is designed for use by landowners, townships and county natural resource planning and management. TC3669805.1 s Page A-24 PHYSICAL SETTING SOURCE RECORDS SEARCHED LOCAL / REGIONAL WATER AGENCY RECORDS FEDERAL WATER WELLS PWS: Public Water Systems Source: EPA/Office of Drinking Water Telephone: 202-564-3750 Public Water System data from the Federal Reporting Data System. A PWS is any water system which provides water to at least 25 people for at least 60 days annually. PWSs provide water from wells, rivers and other sources. PWS ENF: Public Water Systems Violation and Enforcement Data Source: EPA/Office of Drinking Water Telephone: 202-564-3750 Violation and Enforcement data for Public Water Systems from the Safe Drinking Water Information System (SDWIS) after August 1995. Prior to August 1995, the data came from the Federal Reporting Data System (FRDS). USGS Water Wells: USGS National Water Inventory System (NWIS) This database contains descriptive information on sites where the USGS collects or has collected data on surface water and/or groundwater. The groundwater data includes information on wells, springs, and other sources of groundwater. STATE RECORDS North Carolina Public Water Supply Wells Source: Department of Environmental Health Telephone: 919-715-324 3 OTHER STATE DATABASE INFORMATION NC Natural Areas: Significant Natural Heritage Areas Source: Center for Geographic Information and Analysis Telephone: 919-733-2090 A polygon converage identifying sites (terrestrial or aquatic that have particular biodiversity significance. A site's significance may be due to the presenceof rare species, rare or hight quality natural communities, or other important ecological features. NC Game Lands: Wildlife Resources Commission Game Lands Source: Center for Geographic Information and Analysis Telephone: 919-733-2090 All publicly owned game lands managed by the North Carolina Wildlife Resources Commission and as listed in Hunting and Fishing Maps. NC Natural Heritage Sites: Natural Heritage Element Occurrence Sites Source: Center for Geographic Information and Analysis Telephone: 919-733-2090 A point coverage identifying locations of rare and endangered species, occurrences of exemplary or unique natural ecosystems (terrestrial or aquatic), and special animal habitats (e.g., colonial waterbird nesting sites). RADON State Database: NC Radon Source: Department of Environment & Natural Resources Telephone: 919-733-4984 Radon Statistical and Non Statiscal Data Area Radon Information Source: USGS Telephone: 703-356-4020 The National Radon Database has been developed by the U.S. Environmental Protection Agency (USEPA) and is a compilation of the EPA/State Residential Radon Survey and the National Residential Radon Survey. The study covers the years 1986 - 1992. Where necessary data has been supplemented by information collected at private sources such as universities and research institutions. TC3669805.1 s Page A-25 PHYSICAL SETTING SOURCE RECORDS SEARCHED EPA Radon Zones Source: EPA Telephone: 703-356-4020 Sections 307 & 309 of IRAA directed EPA to list and identify areas of U.S. with the potential for elevated indoor radon levels. OTHER Airport Landing Facilities: Private and public use landing facilities Source: Federal Aviation Administration. 800-457-6656 Epicenters: World earthquake epicenters, Richter 5 or greater Source: Department of Commerce, National Oceanic and Atmospheric Administration STREET AND ADDRESS INFORMATION © 2010 Tele Atlas North America, Inc. All rights reserved. This material is proprietary and the subject of copyright protection and other intellectual property rights owned by or licensed to Tele Atlas North America, Inc. The use of this material is subject to the terms of a license agreement. You will be held liable for any unauthorized copying or disclosure of this material. TC3669805.1 s Page A-26 kPPENDIX F WELL RECORD & LABORATORY DATA LF ` NONRESIDENTIAL WELL CONSTRUCTION RECORD North Carolina Department of Environment and Natural Resources- Division of Water Quality Q"""'y9 WELL CONTRACTOR CERTIFICATION # 2986-A 1. WELL CONTRACTOR: Landa M. Shaver d. TOP OF CASING IS -.06 FT. Above Land Surface* *Top of casing terminated aVor below land surface may require Well Contractor (Individual) Name a variance in accordance with 15A NCAC 2C .0118. American Environmental Drilling, Inc. e. YIELD (gpm) N/A METHOD OF TEST N/A Well Contractor Company Name f. DISINFECTION: Type N/A Amount N/A 324 Fields Drive, Suite C g. WATER ZONES (depth): Street Address Top 30 Bottom 40 Top Bottom Aberdeen NC 28315 Top Bottom Top Bottom City or Town State Zip Code Top Bottom Top Bottom L910 )- 944-3140 Thickness/ Area code- Phone number 7. CASING: Depth Diameter Weight Material 2. WELL INFORMATION: Top -.06 Bottom 30' Ft.2" SCH40 PVC WELL CONSTRUCTION PERMIT # MW #1 Top Bottom —Ft.— Top Bottom OTHER ASSOCIATED PERMIT #(if applicable) —Ft.— SITE WELL ID #(if applicable) 8. GROUT: Depth Material Method 3. WELL USE (Check Applicable Box) Monitoring ® Municipal/Public ❑ Top 26' Bottom 28' Ft. Bentonite Tremie Top -.06 Bottom 26' Ft. Portland Tremie Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection ❑ Top Bottom Ft. Irrigation ❑ Other ❑ (list use) DATE DRILLED 4/29/2013 9. SCREEN: Depth Diameter Slot Size Material Top 30' Bottom 40' Ft.2" in..010 in. PVC 4. WELL LOCATION: Top Bottom Ft. in. in. 828 Martin Luther King Blvd. 27599 Top Bottom Ft. in. in. Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code) 10. SAND/GRAVEL PACK: CITY: Chapel Hill COUNTY Orange Depth Size Material TOPOGRAPHIC / LAND SETTING: (check appropriate box) Top 28' Bottom 40' Ft. #3 Sand ❑Slope ❑Valley ®Flat ❑Ridge ❑Other Top Bottom Ft. Top Bottom Ft. LATITUDE 35' 55' 602 " DMS OR 3X.XXXXXXXXX DID ; — , 11. DRILLING LOG: LONGITUDE 79' 03' 194 " DMS OR 7X.XXXXXXXXX DID: Top Bottom Formation Description Latitude/longitude source: ®GPS ❑ Topographic map (location of 0' / 5' Top Soil well must be shown on a USGS topo map and attached to this form 5' / 9' Fill if not using GPS) 91 / 40' Black Ash 5. FACILITY- is the name of the business where the well is located. / Chapel Hill Police Dept. / Facility Name Facility ID #(if applicable) / 828 Martin Luther King Blvd / Street Address / Chapel Hill NC 27599 / City or Town State Zip Code 12. REMARKS Contact Name Mailing Address City or Town State Zip Code ,I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH :15A NCAC 2C, WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS i ) RECORD HAS BEEN PROVIDED TO THE WELL OWNER. Area code - Phone number 6. WELL DETAILS: 4/30/2013 a. TOTAL DEPTH: 40 SIGNATURE tF CERTWKIED WELL CONTRACTOR DATE b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO ED c. WATER LEVEL Below Top of Casing: FT. Landa M. Shaver (Use "+" if Above Top of Casing) PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit within 30 days of completion to the Division of Water Quality - Information Processing, 1617 Mail Service Center- Raleigh, NC 27699-1617 Phone Form GW-1 b No. (919) 807-6300 Rev. 2/09 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 May 6, 2013 Josh Dunbar Falcon Engineering 1210 Trinity Road, Suite 110 Raleigh, NC 27607 Project Location: Chapel Hill Client Job Number: Project Number: [none] Laboratory Work Order Number: 13D 115 8 Enclosed are results of analyses for samples received by the laboratory on April 29, 2013. If you have any questions concerning this report, please feel free to contact me. Sincerely, �� �'V;��� Lisa A. Worthington Project Manager Page 1 of 14 13D1158 1 Contest Final 05 06 13 1310 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Falcon Engineering REPORT DATE: 5/6/2013 1210 Trinity Road, Suite 110 Raleigh, NC 27607 PURCHASE ORDER NUMBER: ATTN: Josh Dunbar PROJECT NUMBER: [none] ANALYTICAL SUMMARY WORK ORDER NUMBER: 13D1158 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Chapel Hill FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB S1 13131158-01 Soil SM 254OG SW-846 8015C S4 13131158-02 Soil SM 254OG SW-846 8015C Page 2 of 14 13D1158 1 Contest Final 05 06 13 1310 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Michael A. Erickson Laboratory Director Page 3 of 14 13D1158 1 Contest Final 05 06 13 1310 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13131158 Date Received: 4/29/2013 Field Sample #: S1 Samnle ID: 13131158-01 Start Date/Time: 4/29/2013 2:10:00PM Samnle Matrix: Soil Stop Date/Time: 4/29/2013 2:15:OOPM Petroleum Hydrocarbons Analyses Date Date/Time Analyte Results RL DL Units Dilution Flag Method Prepared Analyzed Analyst Gasoline Range Organics (GRO) ND 6.2 4.4 mg/Kg dry 1 SW-846 8015C 5/1/13 5/1/13 19:05 EEH Diesel Range Organics 8.0 14 3.2 mg/Kg dry 1 J SW-846 8015C 5/1/13 5/2/13 12:56 SCS Surrogates % Recovery Recovery Limits Flag 1-Chloro-3-fluorobenzene 93.6 70-130 5/1/13 19:05 o-Terphenyl 52.1 40-140 5/2/13 12:56 Page 4 of 14 13D1158 1 Contest Final 05 06 13 1310 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13131158 Date Received: 4/29/2013 Field Sample #: S1 Sample ID: 13131158-01 Start Date/Time: 4/29/2013 2:10:00PM Samnle Matrix: Soil Stop Date/Time: 4/29/2013 2:15:OOPM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag Method Prepared Analyzed Analyst % Solids 58.9 % Wt 1 SM 2540G 4/30/13 5/1/13 9:57 RH Page 5 of 14 13D1158 1 Contest Final 05 06 13 1310 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13131158 Date Received: 4/29/2013 Field Sample #: S4 Samnle ID: 13131158-02 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil Stop Date/Time: 4/29/2013 11:50:OOAM Petroleum Hydrocarbons Analyses Date Date/Time Analyte Results RL DL Units Dilution Flag Method Prepared Analyzed Analyst Gasoline Range Organics (GRO) ND 7.3 5.1 mg/Kg dry 1 SW-846 8015C 5/1/13 5/1/13 19:41 EEH Diesel Range Organics 27 15 3.4 mg/Kg dry 1 SW-846 8015C 5/1/13 5/2/13 13:14 SCS Surrogates % Recovery Recovery Limits Flag 1-Chloro-3-fluorobenzene 89.1 70-130 5/1/13 19:41 o-Terphenyl 70.8 40-140 5/2/13 13:14 Page 6 of 14 13D1158 1 Contest Final 05 06 13 1310 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13131158 Date Received: 4/29/2013 Field Sample #: S4 Sample ID: 13131158-02 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil Stop Date/Time: 4/29/2013 11:50:OOAM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag Method Prepared Analyzed Analyst % Solids 55.2 % Wt 1 SM 2540G 4/30/13 5/1/13 9:57 RH Page 7 of 14 13D1158 1 Contest Final 05 06 13 1310 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: % Solids-SM 2540G Lab Number [Field ID] Batch Date 13D1158-01 [S1] B072077 04/30/13 13D 115 8-02 [S4] B072077 04/30/13 Prep Method: SW-846 3546-SW-846 8015C Lab Number [Field ID] Batch Initial [g] Final [mL] Date 13D1158-01 [S1] B072120 30.0 1.00 05/01/13 13D1158-02 [S4] B072120 30.0 1.00 05/01/13 Prep Method: SW-846 5035/503OB-SW-846 8015C Lab Number [Field ID] Batch Initial [g] Final [mL] Date 13D1158-01[S1] B072173 4.60 16.9 05/01/13 13D1158-02[S4] B072173 4.20 16.9 05/01/13 Page 8 of 14 13D1158 1 Contest Final 05 06 13 1310 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072120 - SW-846 3546 Blank (B072120-BLK1) Prepared & Analyzed: 05/01/13 Diesel Range Organics ND 8.3 mg/Kg wet Surrogate:o-Terphenyl LCS (B072120-BS1) 2.91 mg/Kg wet 3.33 87.2 Prepared: 05/01/13 Analyzed: 05/02/13 40-140 Diesel Range Organics 32.3 8.3 mg/Kg wet 33.3 97.0 40-140 Surrogate: o-Terphenyl LCS Dup (B072120-BSD1) 3.16 mg/Kg wet 3.33 94.7 Prepared: 05/01/13 Analyzed: 05/02/13 40-140 Diesel Range Organics 29.9 8.3 mg/Kg wet 33.3 89.6 40-140 8.02 Surrogate:o-Terphenyl Batch B072173 - SW-846 5035/5030B 3.02 mg/Kg wet 3.33 90.6 40-140 Blank (B072173-BLK1) Prepared & Analyzed: 05/01/13 Gasoline Range Organics (GRO) ND 1.0 mg/Kg wet Surrogate:l-Chloro-3-fluorobenzene LCS (B072173-BSI) 0.0138 mg/Kg wet 0.0150 92.1 Prepared & Analyzed: 05/01/13 70-130 Gasoline Range Organics (GRO) 0.227 0.010 mg/Kg wet 0.250 90.9 80-120 Surrogate:l-Chloro-3-fluorobenzene LCS Dup (B072173-BSD1) 0.0146 mg/Kg wet 0.0150 97.6 Prepared & Analyzed: 05/01/13 70-130 Gasoline Range Organics (GRO) 0.240 0.010 mg/Kg wet 0.250 95.8 80-120 5.34 30 Surrogate: 1-Chloro-3-fluorobenzene 0.0155 mg/Kg wet 0.0150 104 70-130 Page 9 of 14 13D1158 1 Contest Final 05 06 13 1310 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). Page 10 of 14 13D 11581 Contest Final 05 06 13 1310 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8015C in Soil Gasoline Range Organics (GRO) NY,NY,VA,NH Diesel Range Organics NY,VA,NH The CON -TEST Environmental Laboratory operates under the following certifications and accreditation: Code Description Number Expires AIHA AIHA-LAP, LLC 100033 02/1/2014 MA Massachusetts DEP M-MA100 06/30/2013 CT Connecticut Department of Publilc Health PH-0567 09/30/2013 NY New York State Department of Health 10899 NELAP 04/1/2014 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2014 RI Rhode Island Department of Health LA000112 12/30/2013 NC North Carolina Div. of Water Quality 652 12/31/2013 NJ New Jersey DEP MA007 NELAP 06/30/2013 FL Florida Department of Health E871027 NELAP 06/30/2013 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2013 WA State of Washington Department of Ecology C2065 02/23/2014 ME State of Maine 2011028 06/9/2013 VA Commonwealth of Virginia 460217 12/14/2013 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2012 Page 11 of 14 13D 11581 Contest Final 05 06 13 1310 �3 3 �:I 00 006 § H I � lfl � lA 1--� i 00 A A < < a °<' o c. � x 0 0 0 0 c O GC) T m r a w � N 2 ,o CL , € '0 n , d qfo _ � 0 ; l 000 0 r O j ; D 7. r) 0 I �� O On t 00 0EE 0o ` i o F S Q v i C W O� m m m 3 W ll n � ti n N o w 3 7 3 n m O () \_ m 0 a O 3 b � � w m Qo - r) D O cn - y pC* 0C D o v+ o w n II u w 3 - � m a N l n d 0 x Q 0 c n o'a m a w (D I 0:? O 7 0 -0 0 v v 0 Q (D o_ 0 T m T 3 w R • r m 7 g 005. ® a " 3 C) o _ r O 2 //��. Ob n m 63 0 w n • n a a v m d v d a rr^^ * X � 0 O N n C, OII II XII II Kx— * V 7IIrII II II * 0 s s m fl ?� 0 T 2 0 0 3 ri D w w x iT D Q O O. O N Q c Q m � v m s 3 ° m °N o 3 -' i-i N 3• cr w ro w n 0g n 00 a)0 N m e 12 of 14 13D1158 1 Con ami w N N r � 0 7 n QO rp r w w 0_ 0 D O t-� O C. * * O 0 O * w 0 �� N 0 N 0 T T ?. w I m =• yf o � CrD 0 a 0- st Final 05 06 13 1310 4/30/13 Track your package or shipment with FedExTracldng 5h;p (P1U) date: Mon 4/29/2013 6:33 pm RAI" LIS Travel History +Daterime Activity - 4/30/2013 - Tuesday 9:58 am Delivered 8:26 ant On FedExvehicle for delivery 7:32 am At local FedExfacility 6:32 am At destination sort facility 4:52 am Departed FedEx location 12:01 am Arrived at FedEx location - 4/29/2013 - Monday 8:35 pm Left FedEx origin facility 6:33 pnr Picked up Tendercid al FedExOnice Shipment Facts Deliverer! Sgn,d f ., b,, a caU VqS Actual delivery; Tues 4130/2013 9:58 am MA US Location MA WINDSOR LOCKS, CT WINDSOR LOCKS, CT EAST GRANBY, CT iNU':ANApOLlS. IN lNDiANAPiiLiS, IN RALEIGH, NC RALEIGN, NC Local Scan Time Tracking number 802631889500 Service FedEx Priority Overnight Dimensions 180105 in. DeOveredTo Shipping/ReceMng Total pieces 1 Packaging Your Packaging Special handling DeliverWeekday section Page 13 of 14 13D 11581 Contest —Final 05 06 13 1310 https:/Am&w.fedex com/fedekrackrindex html?traclmumbers= 802631889500&cntry_code— 39 Spruce St. East Longmeadow, MA. 01028 P:413-525-2332 F: 413-525-6405 www.contestiabs.com 10 con -test."' ANALYTICAL LABORATORY Sample Recei CLIENT NAME+Aj('e/) RECEIVED BY: C, L f�- DATE: e1j3 1) Was the chain(s) of custody relinquished and signed? es No No CDC Included 2) Does the chain agree with the samples? Yes No If not, explain: 3) Are all the samples in good condition? Ye No If not, explain: 4) How e the samples received: w On Ice Direct from Sampling ❑ Ambient ❑ In Cooler(s) Were the samples received in Temperature Compliance of (2-60C)? e No N/A Temperature °C by Temp blank Temperature °C by Temp gun K- 5) Are there Dissolved samples for the lab to filter? Yes N Who was notified Date Time 6) Are there any RUSH or SHORT HOLDING TIME samples? Yes 1 No► Who was notified Date Time ll 7) Location where samples are stored: 8) Do all samples have the proper Acid pH: 9) Do all samples have the proper Base pH: Yes No Yes No Permission to subcontract samples? Yes No (Walk-in clients only) if not already approved Client Signature: 10) Was the PC notified of any discrepancies with the CoC W the samples: Yes No Containers received at Con -Test # of containers 1 Liter Amber 500 mL Amber 250 mL Amber (8oz amber) 1 Liter Plastic 500 mL Plastic 250 mL plastic 40 mL Vial - type listed below Colisure / bacteria bottle Dissolved Oxygen bottle Encore Flashpoint bottle Perchlorate Kit Other Laboratory Comments: 40 mL vials: # HCI # Methanol # Bisulfate # DI Water Rev 3m.ay 2 .12 # Thiosulfate UnpreservE # of containers 8 oz[ambe clear jar 4 oz amber/clear jar 2 oz amber/clear jar Air Cassette Hg/Hopcalite Tube Plastic Bag / Ziploc PM2.5/PM10 PUF Cartridge SOC Kit TO-17 Tubes Non-ConTest Container Other glass jar Other Time and Date Frozen: e 14 of 14 13D1158 1 Contest Final 05 06 13 1310 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 May 29, 2013 Josh Dunbar Falcon Engineering 1210 Trinity Road, Suite 110 Raleigh, NC 27607 Project Location: Chapel Hill Client Job Number: Project Number: [none] Laboratory Work Order Number: 13EO754 Enclosed are results of analyses for samples received by the laboratory on May 22, 2013. If you have any questions concerning this report, please feel free to contact me. Sincerely, �� �'V;��� Lisa A. Worthington Project Manager Page 1 of 13 13EO754 1 Contest Final 05 29 13 2026 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Falcon Engineering REPORT DATE: 5/29/2013 1210 Trinity Road, Suite 110 Raleigh, NC 27607 PURCHASE ORDER NUMBER: ATTN: Josh Dunbar PROJECT NUMBER: [none] ANALYTICAL SUMMARY WORK ORDER NUMBER: 13EO754 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Chapel Hill FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB S4 13EO754-01 Soil SM 254OG SW-846 6010C SW-846 7471B Page 2 of 13 13EO754 1 Contest Final 05 29 13 2026 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. SW-846 6010C Qualifications Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the high side. Analyte & Samples(s) Qualified: Sodium 13E0754-01[S4], B073667-BSI, B073667-BSDI The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Daren J. Damboragian Laboratory Manager Page 3 of 13 13EO754 1 Contest Final 05 29 13 2026 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13EO754 Date Received: 5/22/2013 Field Sample #: S4 Samnle ID: 13EO754-01 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil Stun Date/Time: 4/29/2013 11:50:OOAM Metals Analyses (Total) Analyte Results RL DL Units Dilution Flag Method Date Prepared Date/Time Analyzed Analyst Aluminum 23000 4.4 1.9 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Antimony ND 4.4 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Arsenic 14 4.4 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Barium 24 4.4 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Beryllium ND 0.44 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Cadmium 1.5 0.44 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Calcium 9900 13 mg/Kg dry I SW-846 601OC 5/23/13 5/29/13 0:44 OP Chromium 22 0.88 mg/Kg dry I SW-846 6010C 5/23/13 5/24/13 18:56 OP Cobalt 30 4.4 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Copper 65 0.88 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Iron 59000 440 mg/Kg dry 100 SW-846 6010C 5/23/13 5/29/13 14:12 OP Lead 20 1.3 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Magnesium 9000 13 1.4 mg/Kg dry 1 SW-846 6010C 5/23/13 5/29/13 0:44 OP Manganese 1500 0.88 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Mercury 0.011 0.044 0.0028 mg/Kg dry 1 J SW-846 7471B 5/23/13 5/24/13 12:10 SAJ Nickel 43 0.88 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Potassium 680 180 30 mg/Kg dry 1 SW-846 6010C 5/23/13 5/29/13 0:44 OP Selenium ND 8.8 mg/Kg dry I SW-846 6010C 5/23/13 5/24/13 18:56 OP Silver ND 0.88 mg/Kg dry I SW-846 6010C 5/23/13 5/24/13 18:56 OP Sodium 150 180 86 mg/Kg dry 1 L-06, J SW-846 6010C 5/23/13 5/29/13 0:44 OP Thallium ND 4.4 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Vanadium 21 1.8 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Zinc 120 1.8 mg/Kg dry 1 SW-846 6010C 5/23/13 5/24/13 18:56 OP Page 4 of 13 13EO754 1 Contest Final 05 29 13 2026 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13EO754 Date Received: 5/22/2013 Field Sample #: S4 Sample ID: 13EO754-01 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil Stop Date/Time: 4/29/2013 11:50:OOAM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag Method Prepared Analyzed Analyst % Solids 55.2 % Wt 1 SM 2540G 5/22/13 5/22/13 16:36 EW Page 5 of 13 13EO754 1 Contest Final 05 29 13 2026 ,con -testy ANALYTICAL LABORATORY Prep Method: % Solids-SM 2540G Lab Number [Field ID] 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Batch Date 13EO754-01 [S4] B073559 05/22/13 Prep Method: SW-846 305OB-SW-846 6010C Lab Number [Field ID] Batch Initial [g] Final [mL] Date 13EO754-01 [S4] B073667 1.03 50.0 05/23/13 Prep Method: SW-846 7471-SW-846 7471 B Lab Number [Field ID] Batch Initial [g] Final [mL] Date 13EO754-01 [S4] B073644 0.614 50.0 05/23/13 Page 6 of 13 13EO754 1 Contest Final 05 29 13 2026 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Metals Analyses (Total) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B073644 - SW-846 7471 Blank (B073644-BLK1) Prepared: 05/23/13 Analyzed: 05/24/13 Mercury ND 0.025 mg/Kg wet LCS (B073644-BS1) Prepared: 05/23/13 Analyzed: 05/24/13 Mercury 4.77 0.33 mg/Kgwet 4.05 118 71.6-128.1 LCS Dup (B073644-BSDI) Prepared: 05/23/13 Analyzed: 05/24/13 Mercury 4.09 0.33 mg/Kg wet 4.05 101 71.6-128.1 15.4 30 Batch B073667 - SW-846 3050B Blank (B073667-BLK1) Prepared: 05/23/13 Analyzed: 05/24/13 Aluminum 1.9 2.5 mg/Kg wet J Antimony ND 2.5 mg/Kg wet Arsenic ND 2.5 mg/Kg wet Barium ND 2.5 mg/Kg wet Beryllium ND 0.25 mg/Kg wet Cadmium ND 0.25 mg/Kg wet Calcium ND 7.5 mg/Kg wet Chromium ND 0.50 mg/Kg wet Cobalt ND 2.5 mg/Kg wet Copper ND 0.50 mg/Kg wet Iron ND 2.5 mg/Kg wet Lead ND 0.75 mg/Kg wet Magnesium 0.83 7.5 mg/Kg wet J Manganese ND 0.50 mg/Kg wet Nickel ND 0.50 mg/Kg wet Potassium ND 100 mg/Kg wet Selenium ND 5.0 mg/Kg wet Silver ND 0.50 mg/Kg wet Sodium 64 100 mg/Kg wet J Thallium ND 2.5 mg/Kg wet Vanadium ND 1.0 mg/Kg wet Zinc ND 1.0 mg/Kg wet LCS (B073667-BS1) Prepared: 05/23/13 Analyzed: 05/24/13 Aluminum 8550 5.0 mg/Kg wet 9060 94.4 46.1-153.4 Antimony 105 5.0 mg/Kg wet 106 99.2 8.2-218.9 Arsenic 189 5.0 mg/Kg wet 182 104 83-117.6 Barium 146 5.0 mg/Kg wet 143 102 83.2-117.5 Beryllium 106 0.50 mg/Kg wet 98.3 107 83.9-116 Cadmium 65.6 0.50 mg/Kg wet 60.4 109 83.1-116.9 Calcium 6320 15 mg/Kg wet 6040 105 83.1-116.7 Chromium 132 0.99 mg/Kg wet 125 105 81.6-117.6 Cobalt 171 5.0 mg/Kg wet 163 105 84.7-115.3 Copper 86.8 0.99 mg/Kg wet 80.1 108 83.8-116.1 Iron 12400 5.0 mg/Kg wet 12900 96.2 50.8-149.6 Lead 129 1.5 mg/Kg wet 136 94.5 82.4-117.8 Magnesium 2710 15 mg/Kg wet 2640 102 75.4-124.2 Manganese 286 0.99 mg/Kg wet 279 103 82.8-117.5 Nickel 134 0.99 mg/Kg wet 128 104 84.4-115.6 Potassium 2880 200 mg/Kg wet 2820 102 72.7-127.3 Selenium 89.6 9.9 mg/Kg wet 85.9 104 80-120 Silver 59.8 0.99 mg/Kg wet 61.3 97.5 66.2-133.8 Sodium 620 200 mg/Kg wet 439 141 • 73.8-126.2 L-06 Page 7 of 13 13EO754 1 Contest Final 05 29 13 2026 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Metals Analyses (Total) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B073667 - SW-846 3050B LCS (B073667-BSI) Prepared: 05/23/13 Analyzed: 05/24/13 Thallium 148 5.0 mg/Kg wet 144 103 81.2-118.8 Vanadium 112 2.0 mg/Kg wet 104 108 75.5-124 Zinc 210 2.0 mg/Kg wet 204 103 81.9-117.6 LCS Dup (B073667-BSDl) Prepared: 05/23/13 Analyzed: 05/24/13 Aluminum 8300 5.0 mg/Kg wet 9060 91.7 46.1-153.4 2.94 30 Antimony 105 5.0 mg/Kg wet 106 99.0 8.2-218.9 0.283 30 Arsenic 190 5.0 mg/Kg wet 182 104 83-117.6 0.174 30 Barium 146 5.0 mg/Kg wet 143 102 83.2-117.5 0.208 30 Beryllium 105 0.50 mg/Kg wet 98.3 107 83.9-116 0.746 30 Cadmium 70.3 0.50 mg/Kg wet 60.4 116 83.1-116.9 7.00 30 Calcium 6360 15 mg/Kg wet 6040 105 83.1-116.7 0.551 30 Chromium 131 1.0 mg/Kg wet 125 104 81.6-117.6 0.988 30 Cobalt 168 5.0 mg/Kg wet 163 103 84.7-115.3 1.86 30 Copper 86.0 1.0 mg/Kg wet 80.1 107 83.8-116.1 0.925 30 Iron 12400 5.0 mg/Kg wet 12900 95.7 50.8-149.6 0.466 30 Lead 128 1.5 mg/Kg wet 136 94.1 82.4-117.8 0.481 30 Magnesium 2670 15 mg/Kg wet 2640 101 75.4-124.2 1.26 30 Manganese 291 1.0 mg/Kg wet 279 104 82.8-117.5 1.51 30 Nickel 131 1.0 mg/Kg wet 128 102 84.4-115.6 1.92 30 Potassium 2810 200 mg/Kg wet 2820 99.6 72.7-127.3 2.46 30 Selenium 96.7 10 mg/Kg wet 85.9 113 80-120 7.68 30 Silver 59.7 1.0 mg/Kg wet 61.3 97.3 66.2-133.8 0.238 30 Sodium 979 200 mg/Kg wet 439 132 * 73.8-126.2 6.84 30 L-06 Thallium 147 5.0 mg/Kg wet 144 102 81.2-118.8 0.598 30 Vanadium 110 2.0 mg/Kg wet 104 106 75.5-124 1.22 30 Zinc 204 2.0 mg/Kg wet 204 100 81.9-117.6 2.80 30 MRL Check (B073667-MRL1) Prepared: 05/23/13 Analyzed: 05/24/13 Lead 0.745 0.69 mg/Kg wet 0.691 108 80-120 Page 8 of 13 13EO754 1 Contest Final 05 29 13 2026 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). L-06 Laboratory fortified blankilaboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the high side. MS-19 Sample to spike ratio is greater than or equal to 4:1. Spiked amount is not representative of the native amount in the sample. Appropriate or meaningful recoveries cannot be calculated. Page 9 of 13 13EO754 1 Contest Final 05 29 13 2026 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 6010C in Soil Aluminum CT,NH,NY,ME,VA Antimony CT,NH,NY,NC,ME,VA Arsenic CT,NH,NY,ME,NC,VA Barium CT,NH,NY,ME,NC,VA Beryllium CT,NH,NY,ME,NC,VA Cadmium CT,NH,NY,ME,NC,VA Calcium CT,NH,NY,ME,NC,VA Chromium CT,NH,NY,ME,NC,VA Cobalt CT,NH,NY,ME,NC,VA Copper CT,NH,NY,ME,NC,VA Iron CT,NH,NY,ME,NC,VA Lead CT,NH,NY,AIHA,ME,NC,VA Magnesium CT,NH,NY,ME,NC,VA Manganese CT,NH,NY,ME,NC,VA Nickel CT,NH,NY,ME,NC,VA Potassium CT,NH,NY,ME,NC,VA Selenium CT,NH,NY,ME,NC,VA Silver CT,NH,NY,ME,NC,VA Sodium CT,NH,NY,ME,NC,VA Thallium CT,NH,NY,ME,NC,VA Vanadium CT,NH,NY,ME,NC,VA Zinc CT,NH,NY,ME,NC,VA SW-846 7470A in Water Mercury CT,NH,NY,NC,ME,VA SW-846 7471B in Soil Mercury CT,NH,NY,NC,ME,VA The CON -TEST Environmental Laboratory operates under the following certifications and accreditation: Code Description Number Expires AIHA AIHA-LAP, LLC 100033 02/1/2014 MA Massachusetts DEP M-MA100 06/30/2013 CT Connecticut Department of Publilc Health PH-0567 09/30/2013 NY New York State Department of Health 10899 NELAP 04/1/2014 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2014 RI Rhode Island Department of Health LA000112 12/30/2013 NC North Carolina Div. of Water Quality 652 12/31/2013 NJ New Jersey DEP MA007 NELAP 06/30/2013 FL Florida Department of Health E871027 NELAP 06/30/2013 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2013 WA State of Washington Department of Ecology C2065 02/23/2014 ME State of Maine 2011028 06/9/2015 VA Commonwealth of Virginia 460217 12/14/2013 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2012 Page 10 of 13 13EO754 1 Contest Final 05 29 13 2026 m k � yn � c. xc ro 5 � C4 � $ f 1 =L ro :« o... q P7, III rb _ v m p' a I { v--�-444-H � a i w m rc n t i � y�i ��! l�✓n In P x H S.VM 0. •„9 ° T 00 c U < ( i T f x Y,7 >•T 1 J S O A M us �0 m Q E [Y � ,l m RO C) y,v�vF�Ctci-a?�ww=g-r^^�a �^8Tsn�G17a m f1 II II z2 @ W 4 ryry V r e [Y} ry C G p f: CL c- r v�Ca ae. m re ro n ii C a c w .-• ri D g, a' fro a !a, n w w a ®. m. m C'k. bti" Of W C d 7 f p r(w y, fu ; N ro Page 11 of 13 13EO754 1 Contest Final 05 29 13 2026 4130113 Trackyrlur package or shiptnentvAth Fed&Trad6ng EN. Travel History b'd7-o W> W. GCOLO," &MeMme Acemty Location - 4f3012013 - Tuesday 9:53 �sm Deliver-6 u 8:26 am Ou Fe rKwhi(la fw deivrr}r W1N0,9,�A tOx9,5. r.r 7:32 am At local FedEx fs.{Cl!!fy N/tNO1 OR iticm, CT 6:32 am Atdo54tnafion sortfadlily [ASr GRANBY, CT 4:.52 am Departed Fedlnx lc)rallco M)IANA OL{5. Iry 12:01 sm Arnwd st FodCx lucaflon EN - 4/29/2013 - Monday 8.35 prtI Left F rP IIF.x ori5in far iliiy R,, ES H. M; 6:33 pal Pi(ked up RAiF.f Gli nrr, l'ar5de�rarl C+f F't?d F�x C)1R'[!;tl Local Scan Time Shipment Facts 'rraeklreg number 802631669506 Servire FedEx PnrjrjSy Ov&rnighz i' Dimensions lax1tx15in. Oellvered to ShlppIngIRecei4ng %talPiaces i Puakaeing YourPackagirg 5pectla3harsd€Irrc DeliverWeek ay sectlon https.Ilv*w.#IwdexconVfcdextracWInde)r htm71raclmumbers=802631889500Uniry rude=us ill Page 12 of 13 13EO754 1 Contest Final 05 29 13 2026 3S 5presce 5t. I .7aC co East Longmeadow, AAA, 01028 -Nsto n P: 413-525-2332 ANALYTiCAL LA8Q�_AT_(TA__y F; 413-525-6405 www.contesdabs.corri SaMpL�_ftqjmlt haChecklist K6 ��� 4 CLIENT NAE. CEIVED BY: LI _C_ DATE 1) Was the chain(s) of custody relinquished and stgned? No No CoC Included 2) Does the charagree with the samples? No If not, explain: @ 3) Are all the samples in good condition? No If not, explain: 4) How e the samples received.: y Direct from Sampling Ej Ambient in Cooler(s) Le" Were the samples received in Temperature Compfience, of (2-6°C)7 & No N/A Temperature oC by Tomp blank Temperature '1C icy Temp gun 5) Are there Dissolved samples for the lab to filter? Yes Who was notified Date Time 6) Are there any RUSH or SHORT HOLDING TIME samples? Yes Who was notified Date Time Permission to subcontract samples? Yes No 7) Location where samples are rtoreda (Walk-in clients only) if not already approved Client Signature: 8) Do all samples have the proper Acid pH: Yes No 9) DO all samples have the proper Base pH- Yes No 10) Was the PC notified of any discrepancies with the GoC the samples: yes Containers received at C'ton-Test # of containers I Liter Amber 500 ML Amber 250 mL Am 1 Liter Plastic 500 rnL Plastic 250 TL_e1astjc 40 ML Vial - tY�e listed below Colisure / bacteria hnffifl 0 UXyQtn bottle Encore 'i2oint bottle -hlorate Kit Other Laboratory Comments-. 40roLvials: #HCI # Methanol fate # DI Water .. ... ... # Thiosultale Unproserved 211 4 0z aEn �/Oea�rar 2 oz amber/clear jar —Air Cassette Hq/1-lopeahle Tube Plastic Ba 1 Zi lac PM 2.5 / PM 10 PUF Cartridge SOC Kit TO- 17 Tubes �n-ConTest Container GWier alass iar I nn of containers Tirne and Date Frozen; I Page 13 of 13 13EO7541 ContestFinal05 29 13 2026 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 May 20, 2013 Josh Dunbar Falcon Engineering 1210 Trinity Road, Suite 110 Raleigh, NC 27607 Project Location: Chapel Hill Client Job Number: Project Number: [none] Laboratory Work Order Number: 13EO396 Enclosed are results of analyses for samples received by the laboratory on May 13, 2013. If you have any questions concerning this report, please feel free to contact me. Sincerely, �� �'V;��� Lisa A. Worthington Project Manager Page 1 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Falcon Engineering REPORT DATE: 5/20/2013 1210 Trinity Road, Suite 110 Raleigh, NC 27607 PURCHASE ORDER NUMBER: ATTN: Josh Dunbar PROJECT NUMBER: [none] ANALYTICAL SUMMARY WORK ORDER NUMBER: 13EO396 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Chapel Hill FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB S4 13EO396-01 Soil MADEP-EPH-04-1.1 MADEP-VPH-04-1.1 SM 254OG SW-846 8260B SW-846 8270D Page 2 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. Page 3 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028' FAX 413/525-6405 ` TEL. 413/525-2332 MADEP-VPH-04-1.1 Qualifications: Soil/methanol ratio does not meet method specifications. Insufficient amount of soil. Data validation is not affected since a sufficient amount of preservative is present. Detection limits may be above useful levels. Analyte & Samples(s) Qualified: 13EO396-01[S4] SW-846 8260B Qualifications Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is on the high side. Analyte & Samples(s) Qualified: Acetone B072887-BSI,B072887-BSDI Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the low side. Analyte & Samples(s) Qualified: Bromoform 13EO396-01[S4], 13EO396-01RE1[S4], B072887-BLKI, B072887-BSI, B072887-BSD1 Surrogate recovery outside of control limits due to suspected sample matrix interference. Analyte & Samples(s) Qualified: 1,2-Dichloroethane-d4,4-Bromofluorobenzene 13EO396-01[S4],13EO396-01RE1[S4] Continuing calibration did not meet method specifications and was biased on the low side for this compound. Increased uncertainty is associated with the reported value which is likely to be biased on the low side. Analyte & Samples(s) Qualified: 1,2,4-Trichlorobenzene, Bromoform, Naphthalene 13EO396-01[S4], 13EO396-OIRE1[S4], B072887-BLKI, B072887-BS1, B072887-BSD1 Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported result. Analyte & Samples(s) Qualified: 1,4-Dioxane, tert-Butyl Alcohol (TBA) 13EO396-01[S4], 13EO396-OIRE1[S4], B072887-BLKI, B072887-BS1, B072887-BSD1 Internal standard area <50% of associated calibration standard internal standard area. Analyte & Samples(s) Qualified: 1,2,3-Trichlorobenzene, 1,2,4-Trichlorobenzene, 1,2,4-Trimethylbenzene, 1,2-Dibromo-3-chloropropane (DBCP), 1,2-Dichlorobenzene, 1,3,5-Trichlorobenzene, 1,3-Dichlorobenzene, 1,4-Dichlorobenzene, 1,4-Dichlorobenzene-d4, Hexachlorobutadiene, Naphthalene, n-Butylbenzene, p-Isopropyltoluene (p-Cymene), sec-Butylbenzene, tert-Butylbenzene 13EO396-01[S4],13EO396-01RE1[S4] Page 4 of 38 13EO396 1 Contest Final 05 20 13 1552 ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: Acetone B072887-BS1, B072887-BSD1 SW-846 8270D Qualifications: Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for this compound. Analyte & Samples(s) Qualified: Benzoic Acid B072855-BSDI Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. Analyte & Samples(s) Qualified: Benzoic Acid, Di-n-octylphthalate, Fluoranthene,Indeno(1,2,3-cd)pyrene 13EO396-01[S4], B072855-BLKI, B072855-BS1, B072855-BSDI Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method specified criteria. Analyte & Samples(s) Qualified: Benzidine 13EO396-01[S4], B072855-BLKI, B072855-BS1, B072855-BSDI Continuing calibration did not meet method specifications and was biased on the low side for this compound. Increased uncertainty is associated with the reported value which is likely to be biased on the low side. Analyte & Samples(s) Qualified: 2,4-Dinitrophenol, 4-Nitroaniline, 4-Nitrophenol B072855-BLKI, B072855-BSI Continuing calibration did not meet method specifications and was biased on the high side for this compound. Increased uncertainty is associated with the reported value which is likely to be biased on the high side. Analyte & Samples(s) Qualified: Benzidine B072855-BSDI Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported result. Analyte & Samples(s) Qualified: Pentachloronitrobenzene 13EO396-01[S4], B072855-BLKI, B072855-BS1, B072855-BSDI Initial calibration did not meet method specifications. Compound was calibrated using linear regression with correlation coefficient <0.99. Analyte & Samples(s) Qualified: Benzoic Acid 13EO396-01[S4], B072855-BLKI, B072855-BSI, B072855-BSDI Page 5 of 38 13EO396 1 Contest Final 05 20 13 1552 icon-testo ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: Benzidine 13E0396-01[S4] MADEP-EPH-04-1.1 SPE cartridge contamination with non -petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C 11-C22 aromatic range fraction in all samples in the batch. No significant modifications were made to the method. MADEP-VPH-04-1.1 No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely covered by methanol in the proper containers specified on the chain -of -custody form unless specified in this narrative. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Daren J. Damboragian Laboratory Manager Page 6 of 38 13EO396 1 Contest Final 05 20 13 1552 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13E0396 Date Received: 5/13/2013 Field Sample #: S4 Sample ID: 13E0396-01 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil StoD Date/Time: 4/29/2013 11:50:OOAM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.25 0.059 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Acetone ND 0.25 0.057 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Acrylonitrile ND 0.015 0.0063 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Acrylonitrile ND 0.015 0.0061 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF tert-Amyl Methyl Ether (TAME) ND 0.0025 0.0018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF tert-Amyl Methyl Ether (TAME) ND 0.0025 0.0017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Benzene ND 0.0050 0.0018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Benzene ND 0.0049 0.0017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Bromobenzene ND 0.0050 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Bromobenzene ND 0.0049 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Bromochloromethane ND 0.0050 0.0035 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Bromochloromethane ND 0.0049 0.0034 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Bromodichloromethane ND 0.0050 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Bromodichloromethane ND 0.0049 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Bromoform ND 0.0050 0.0035 mg/Kg dry 1 L-04, V-05 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Bromoform ND 0.0049 0.0034 mg/Kg dry 1 L-04, V-05 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Bromomethane ND 0.025 0.0043 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Bromomethane ND 0.025 0.0042 mg/Kg dry I SW-846 8260B 5/13/13 5/13/13 14:53 MFF 2-Butanone (MEK) ND 0.10 0.044 mg/Kg dry I SW-846 8260B 5/13/13 5/13/13 13:05 MFF 2-Butanone (MEK) ND 0.098 0.043 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF tert-Butyl Alcohol (TBA) ND 0.10 0.052 mg/Kg dry 1 V-16 SW-846 8260B 5/13/13 5/13/13 13:05 MFF tert-Butyl Alcohol (TBA) ND 0.098 0.051 mg/Kg dry 1 V-16 SW-846 8260B 5/13/13 5/13/13 14:53 MFF n-Butylbenzene ND 0.0050 0.0018 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF n-Butylbenzene ND 0.0049 0.0017 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF sec-Butylbenzene ND 0.0050 0.0025 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF sec-Butylbenzene ND 0.0049 0.0025 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF tert-Butylbenzene ND 0.0050 0.0023 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF tert-Butylbenzene ND 0.0049 0.0022 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0025 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0025 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Carbon Disulfide ND 0.015 0.0083 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Carbon Disulfide ND 0.015 0.0081 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Carbon Tetrachloride ND 0.0050 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Carbon Tetrachloride ND 0.0049 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Chlorobenzene ND 0.0050 0.0018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Chlorobenzene ND 0.0049 0.0017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Chlorodibromomethane ND 0.0025 0.0018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Chlorodibromomethane ND 0.0025 0.0017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Chloroethane ND 0.050 0.0038 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Chloroethane ND 0.049 0.0037 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Chloroform ND 0.010 0.0018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Chloroform ND 0.0098 0.0017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Chloromethane ND 0.025 0.0023 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Chloromethane ND 0.025 0.0022 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Page 7 of 38 13EO396 1 Contest Final 05 20 13 1552 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13E0396 Date Received: 5/13/2013 Field Sample #: S4 Sample ID: 13E0396-01 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil StoD Date/Time: 4/29/2013 11:50:OOAM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag Method Date Prepared Date/Time Analyzed Analyst 2-Chlorotoluene ND 0.0050 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 2-Chlorotoluene ND 0.0049 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 4-Chlorotoluene ND 0.0050 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 4-Chlorotoluene ND 0.0049 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0050 0.0028 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0049 0.0027 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,2-Dibromoethane (EDB) ND 0.0025 0.0025 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,2-Dibromoethane (EDB) ND 0.0025 0.0025 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Dibromomethane ND 0.0050 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Dibromomethane ND 0.0049 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,2-Dichlorobenzene ND 0.0050 0.0018 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,2-Dichlorobenzene ND 0.0049 0.0017 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,3-Dichlorobenzene ND 0.0050 0.0018 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,3-Dichlorobenzene ND 0.0049 0.0017 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,4-Dichlorobenzene ND 0.0050 0.0020 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,4-Dichlorobenzene ND 0.0049 0.0020 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF trans-1,4-Dichloro-2-butene ND 0.010 0.0030 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF trans-1,4-Dichloro-2-butene ND 0.0098 0.0029 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Dichlorodifluoromethane (Freon 12) ND 0.050 0.0033 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Dichlorodifluoromethane (Freon 12) ND 0.049 0.0032 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,1-Dichloroethane ND 0.0050 0.0018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,1-Dichloroethane ND 0.0049 0.0017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,2-Dichloroethane ND 0.0050 0.0033 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,2-Dichloroethane ND 0.0049 0.0032 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,1-Dichloroethylene ND 0.010 0.0028 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,1-Dichloroethylene ND 0.0098 0.0027 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF cis-1,2-Dichloroethylene ND 0.0050 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF cis-1,2-Dichloroethylene ND 0.0049 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF trans-1,2-Dichloroethylene ND 0.0050 0.0023 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF trans-1,2-Dichloroethylene ND 0.0049 0.0022 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,2-Dichloropropane ND 0.0050 0.0033 mg/Kg dry I SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,2-Dichloropropane ND 0.0049 0.0032 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,3-Dichloropropane ND 0.0025 0.0018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,3-Dichloropropane ND 0.0025 0.0017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 2,2-Dichloropropane ND 0.0050 0.0023 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 2,2-Dichloropropane ND 0.0049 0.0022 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,1-Dichloropropene ND 0.0050 0.0023 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,1-Dichloropropene ND 0.0049 0.0022 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF cis-1,3-Dichloropropene ND 0.0025 0.0018 mg/Kg dry I SW-846 8260B 5/13/13 5/13/13 13:05 MFF cis-1,3-Dichloropropene ND 0.0025 0.0017 mg/Kg dry I SW-846 8260B 5/13/13 5/13/13 14:53 MFF trans-1,3-Dichloropropene ND 0.0025 0.0018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF trans-1,3-Dichloropropene ND 0.0025 0.0017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Diethyl Ether ND 0.050 0.0045 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Diethyl Ether ND 0.049 0.0044 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Page 8 of 38 13EO396 1 Contest Final 05 20 13 1552 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13E0396 Date Received: 5/13/2013 Field Sample #: S4 Sample ID: 13E0396-01 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil StoD Date/Time: 4/29/2013 11:50:OOAM Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag Method Date Prepared Date/Time Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0025 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Diisopropyl Ether (DIPE) ND 0.0025 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,4-Dioxane ND 0.25 0.14 mg/Kg dry 1 V-16 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,4-Dioxane ND 0.25 0.14 mg/Kg dry 1 V-16 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Ethylbenzene ND 0.0050 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Ethylbenzene ND 0.0049 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Hexachlorobutadiene ND 0.0050 0.0025 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Hexachlorobutadiene ND 0.0049 0.0025 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 2-Hexanone (MBK) ND 0.050 0.027 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 2-Hexanone (MBK) ND 0.049 0.027 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Isopropylbenzene (Cumene) ND 0.0050 0.0018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Isopropylbenzene (Cumene) ND 0.0049 0.0017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF p-Isopropyltoluene (p-Cymene) ND 0.0050 0.0020 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF p-Isopropyltoluene (p-Cymene) ND 0.0049 0.0020 mg/Kg dry I V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Methyl tert-Butyl Ether (MTBE) ND 0.010 0.0023 mg/Kg dry I SW-846 8260B 5/13/13 5/13/13 13:05 MFF Methyl tert-Butyl Ether (MT 3E) ND 0.0098 0.0022 mg/Kg dry I SW-846 8260B 5/13/13 5/13/13 14:53 MFF Methylene Chloride ND 0.050 0.018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Methylene Chloride ND 0.049 0.017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 4-Methyl-2-pentanone (MIBK) ND 0.050 0.019 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 4-Methyl-2-pentanone (MIBK) ND 0.049 0.019 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Naphthalene ND 0.010 0.0018 mg/Kg dry 1 V-05, V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Naphthalene ND 0.0098 0.0017 mg/Kg dry 1 V-05, V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF n-Propylbenzene ND 0.0050 0.0018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF n-Propylbenzene ND 0.0049 0.0017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Styrene ND 0.0050 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Styrene ND 0.0049 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0050 0.0023 mg/Kg dry 1 SW-8468260B 5/13/13 5/13/13 13:05 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0049 0.0022 mg/Kg dry 1 SW-8468260B 5/13/13 5/13/13 14:53 MFF 1,1,2,2-Tetrachloroethane ND 0.0025 0.0023 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,1,2,2-Tetrachloroethane ND 0.0025 0.0022 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Tetrachloroethylene ND 0.0050 0.0033 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Tetrachloroethylene ND 0.0049 0.0032 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Tetrahydrofuran ND 0.025 0.0055 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Tetrahydrofuran ND 0.025 0.0054 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Toluene ND 0.0050 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Toluene ND 0.0049 0.0020 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,2,3-Trichlorobenzene ND 0.0050 0.0015 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,2,3-Trichlorobenzene ND 0.0049 0.0015 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,2,4-Trichlorobenzene ND 0.0050 0.0020 mg/Kg dry 1 V-05, V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,2,4-Trichlorobenzene ND 0.0049 0.0020 mg/Kg dry 1 V-05, V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,3,5-Trichlorobenzene ND 0.0050 0.0018 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,3,5-Trichlorobenzene ND 0.0049 0.0017 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1, 1, 1 -Trichloroethane ND 0.0050 0.0025 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Page 9 of 38 13EO396 1 Contest Final 05 20 13 1552 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13E0396 Date Received: 5/13/2013 Field Sample #: S4 Sample ID: 13E0396-01 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil StoD Date/Time: 4/29/2013 11:50:OOAM Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag Method Prepared Analyzed Analyst 1, 1, 1 -Trichloroethane ND 0.0049 0.0025 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,1,2-Trichloroethane ND 0.0050 0.0030 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,1,2-Trichloroethane ND 0.0049 0.0029 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Trichloroethylene ND 0.0050 0.0023 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Trichloroethylene ND 0.0049 0.0022 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Trichlorofluoromethane (Freon 11) ND 0.025 0.0028 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Trichlorofluoromethane (Freon 11) ND 0.025 0.0027 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,2,3-Trichloropropane ND 0.0050 0.0028 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,2,3-Trichloropropane ND 0.0049 0.0027 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.025 0.0023 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF (Freon 113) 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 0.025 0.0022 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0050 0.0020 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,2,4-Trimethylbenzene ND 0.0049 0.0020 mg/Kg dry 1 V-17 SW-846 8260B 5/13/13 5/13/13 14:53 MFF 1,3,5-Trimethylbenzene ND 0.0050 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF 1,3,5-Trimethylbenzene ND 0.0049 0.0015 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Vinyl Chloride ND 0.025 0.0028 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF Vinyl Chloride ND 0.025 0.0027 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF m+p Xylene ND 0.010 0.0043 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF m+p Xylene ND 0.0098 0.0042 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF o-Xylene ND 0.0050 0.0018 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 13:05 MFF o-Xylene ND 0.0049 0.0017 mg/Kg dry 1 SW-846 8260B 5/13/13 5/13/13 14:53 MFF Surrogates % Recovery Recovery Limits Flag 1,2-Dichloroethane-d4 132 * 70-130 5-03 5/13/13 13:05 1,2-Dichloroethane-d4 121 70-130 5/13/13 14:53 Toluene-d8 96.0 70-130 5/13/13 13:05 Toluene-d8 94.8 70-130 5/13/13 14:53 4-Bromofluorobenzene 51.6 * 70-130 5-03 5/13/13 13:05 4-Bromofluorobenzene 47.0 * 70-130 5-03 5/13/13 14:53 Page 10 of 38 13EO396 1 Contest Final 05 20 13 1552 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13EO396 Date Received: 5/13/2013 Field Sample #: S4 Samnle ID: 13EO396-01 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil StoD Date/Time: 4/29/2013 11:50:OOAM Semivolatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.31 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Acenaphthylene ND 0.31 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Acetophenone ND 0.62 0.22 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Aniline ND 0.62 0.20 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Anthracene ND 0.31 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Benzidine ND 0.62 0.14 mg/Kg dry 1 V-04, V-20 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Benzo(a)anthracene ND 0.31 0.14 mg/Kg dry I SW-846 8270D 5/13/13 5/14/13 17:18 CMR Benzo(a)pyrene ND 0.31 0.16 mg/Kg dry I SW-846 8270D 5/13/13 5/14/13 17:18 CMR Benzo(b)fluoranthene ND 0.31 0.16 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Benzo(g,h,i)perylene ND 0.31 0.13 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Benzo(k)fluoranthene ND 0.31 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Benzoic Acid 0.39 1.8 0.27 mg/Kg dry 1 R-05, V-19, J SW-846 8270D 5/13/13 5/14/13 17:18 CMR Bis(2-chloroethoxy)methane ND 0.62 0.16 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Bis(2-chloroethyl)ether ND 0.62 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Bis(2-chloroisopropyl)ether ND 0.62 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Bis(2-Ethylhexyl)phthalate ND 0.62 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 4-Bromophenylphenylether ND 0.62 0.13 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Butylbenzylphthalate ND 1.2 0.20 mg/Kg dry I SW-846 8270D 5/13/13 5/14/13 17:18 CMR Carbazole ND 0.31 0.14 mg/Kg dry I SW-846 8270D 5/13/13 5/14/13 17:18 CMR 4-Chloroaniline ND 1.2 0.16 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 4-Chloro-3-methylphenol ND 1.2 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2-Chloronaphthalene ND 0.62 0.13 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2-Chlorophenol ND 0.62 0.16 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 4-Chlorophenylphenylether ND 0.62 0.22 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Chrysene ND 0.31 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Dibenz(a,h)anthracene ND 0.31 0.13 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Dibenzofuran ND 0.62 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Di-n-butylphthalate ND 0.62 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 1,2-Dichlorobenzene ND 0.62 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 1,3-Dichlorobenzene ND 0.62 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 1,4-Dichlorobenzene ND 0.62 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 3,3-Dichlorobenzidine ND 0.31 0.11 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2,4-Dichlorophenol ND 0.62 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Diethylphthalate ND 0.62 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2,4-Dimethylphenol ND 0.62 0.13 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Dimethylphthalate ND 1.2 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 4,6-Dinitro-2-methylphenol ND 0.62 0.072 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2,4-Dinitrophenol ND 1.2 0.072 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2,4-Dinitrotoluene ND 0.62 0.20 mg/Kg dry I SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2,6-Dinitrotoluene ND 0.62 0.20 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Di-n-octylphthalate ND 1.2 0.24 mg/Kg dry 1 R-05 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 1,2-Diphenylhydrazine (as Azobenzene) ND 0.62 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Fluoranthene ND 0.31 0.13 mg/Kg dry 1 R-05 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Flumene ND 0.31 0.16 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Page 11 of 38 13EO396 1 Contest Final 05 20 13 1552 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13E0396 Date Received: 5/13/2013 Field Sample #: S4 Samnle ID: 13E0396-01 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil StoD Date/Time: 4/29/2013 11:50:OOAM Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.62 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Hexachlorobutadiene ND 0.62 0.11 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Hexachlorocyclopentadiene ND 1.2 0.11 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Hexachloroethane ND 0.62 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Indeno(1,2,3-cd)pyrene ND 0.31 0.13 mg/Kg dry 1 R-05 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Isophorone ND 0.62 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 1-Methylnaphthalene ND 0.31 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2-Methylnaphthalene ND 0.31 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2-Methylphenol ND 0.62 0.24 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 3/4-Methylphenol ND 0.62 0.29 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Naphthalene ND 0.31 0.13 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2-Nitroaniline ND 0.62 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 3-Nitroaniline ND 0.62 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 4-Nitroaniline ND 0.62 0.22 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Nitrobenzene ND 0.62 0.13 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2-Nitrophenol ND 0.62 0.091 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 4-Nitrophenol ND 1.2 0.072 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR N-Nitrosodimethylamine ND 0.62 0.11 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR N-Nitrosodiphenylamine ND 0.62 0.20 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR N-Nitrosodi-n-propylamine ND 0.62 0.24 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Pentachloronitrobenzene ND 0.62 0.20 mg/Kg dry 1 V-16 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Pentachlorophenol ND 0.62 0.11 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Phenanthrene ND 0.31 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Phenol ND 0.62 0.16 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Pyrene ND 0.31 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Pyridine ND 0.62 0.14 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 1,2,4,5-Tetrachlorobenzene ND 0.62 0.13 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 1,2,4-Trichlorobenzene ND 0.62 0.11 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2,4,5-Trichlorophenol ND 0.62 0.18 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR 2,4,6-Trichlorophenol ND 0.62 0.13 mg/Kg dry 1 SW-846 8270D 5/13/13 5/14/13 17:18 CMR Surrogates % Recovery Recovery Limits Flag 2-Fluorophenol 42.0 30-130 5/14/13 17:18 Phenol-d6 48.4 30-130 5/14/13 17:18 Nitrobenzene-d5 66.4 30-130 5/14/13 17:18 2-Fluorobiphenyl 83.4 30-130 5/14/13 17:18 2,4,6-Tribromophenol 30.8 30-130 5/14/13 17:18 p-Terphenyl-dl4 63.1 30-130 5/14/13 17:18 Page 12 of 38 13EO396 1 Contest Final 05 20 13 1552 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13EO396 Date Received: 5/13/2013 Field Sample #: S4 Samnle ID: 13EO396-01 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil Stun Date/Time: 4/29/2013 11:50:OOAM Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL Units Dilution Flag Method Prepared Analyzed Analyst C9-C18 Aliphatics ND 18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS C19-C36 Aliphatics ND 18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Unadjusted C11-C22 Aromatics ND 18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS C11-C22 Aromatics ND 18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Acenaphthene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Acenaphthylene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Anthracene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Benzo(a)anthracene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Benzo(a)pyrene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Benzo(b)fluoranthene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Benzo(g,h,i)perylene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Benzo(k)fluoranthene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Chrysene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Dibenz(a,h)anthracene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Fluoranthene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Fluorene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Indeno(1,2,3-cd)pyrene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS 2-Methylnaphthalene ND 0.18 mg/Kg dry I MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Naphthalene ND 0.18 mg/Kg dry I MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Phenanthrene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Pyrene ND 0.18 mg/Kg dry 1 MADEP-EPH-04-1.1 5/13/13 5/13/13 17:14 SCS Surrogates % Recovery Recovery Limits Flag Chlorooctadecane (COD) 57.0 40-140 5/13/13 17:14 o-Terphenyl (OTP) 49.1 40-140 5/13/13 17:14 2-Bromonaphthalene 81.1 40-140 5/13/13 17:14 2-Fluorobiphenyl 84.3 40-140 5/13/13 17:14 Page 13 of 38 13EO396 1 Contest Final 05 20 13 1552 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13EO396 Date Received: 5/13/2013 Field Sample #: S4 Sample ID: 13EO396-01 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil Stop Date/Time: 4/29/2013 11:50:OOAM Sample Flags: 0-02 Petroleum Hydrocarbons Analyses - VPH Soil/Methanol Preservation Ratio: 0.28 Date Date/Time Analyte Results RL Units Dilution Flag Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics ND 73 mg/Kg dry 1 MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH C5-C8 Aliphatics ND 73 mg/Kg dry 1 MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH Unadjusted C9-C12 Aliphatics ND 73 mg/Kg dry 1 MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH C9-C12 Aliphatics ND 73 mg/Kg dry 1 MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH C9-C10 Aromatics ND 73 mg/Kg dry 1 MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH Benzene ND 0.36 mg/Kg dry 1 MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH Ethylbenzene ND 0.36 mg/Kg dry 1 MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH Methyl tert-Butyl Ether (MTBE) ND 0.36 mg/Kg dry 1 MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH Naphthalene ND 1.8 mg/Kg dry 1 MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH Toluene ND 0.36 mg/Kg dry 1 MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH m+p Xylene ND 0.73 mg/Kg dry 1 MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH o-Xylene ND 0.36 mg/Kg dry I MADEP-VPH-04-1.1 5/13/13 5/13/13 13:59 EEH Surrogates % Recovery Recovery Limits Flag 2,5-Dibromotoluene (FID) 110 70-130 5/13/13 13:59 2,5-Dibromotoluene (PID) 97.4 70-130 5/13/13 13:59 Page 14 of 38 13EO396 1 Contest Final 05 20 13 1552 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: Chapel Hill Sample Description: Work Order: 13EO396 Date Received: 5/13/2013 Field Sample #: S4 Sample ID: 13EO396-01 Start Date/Time: 4/29/2013 11:45:OOAM Samnle Matrix: Soil Stop Date/Time: 4/29/2013 11:50:OOAM Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag Method Prepared Analyzed Analyst % Solids 55.2 % Wt 1 SM 2540G 5/14/13 5/14/13 13:40 EW Page 15 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: SW-846 3546-MADEP-EPH-04-1.1 Lab Number [Field ID] Batch Initial [g] Final [mL] Date 13EO396-01 [S4] B072854 20.0 2.00 05/13/13 Prep Method: MA VPH-MADEP-VPH-04-1.1 Lab Number [Field ID] Batch Initial [g] Final [mL] Date 13EO396-01[S4] B072883 4.20 16.9 05/13/13 Prep Method: % Solids-SM 2540G Lab Number [Field ID] Batch Date 13EO396-01[S4] B072992 05/14/13 Prep Method: SW-846 5035-SW-846 8260B Lab Number [Field ID] Batch Initial [g] Final [mL] Date 13EO396-01 [S4] B072887 3.62 10.0 05/13/13 13EO396-OIRE1 [S4] B072887 3.69 10.0 05/13/13 Prep Method: SW-846 3546-SW-846 8270D Lab Number [Field ID] Batch Initial [g] Final [mL] Date 13EO396-01 [S4] B072855 30.0 1.00 05/13/13 Page 16 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072887 - SW-846 5035 Blank (B072887-BLK1) Prepared & Analyzed: 05/13/13 Acetone ND 0.10 mg/Kg wet Acrylonitrile ND 0.0060 mg/Kg wet tert-Amyl Methyl Ether (TAME) ND 0.0010 mg/Kg wet Benzene ND 0.0020 mg/Kg wet Bromobenzene ND 0.0020 mg/Kg wet Bromochloromethane ND 0.0020 mg/Kg wet Bromodichloromethane ND 0.0020 mg/Kg wet Bromoform ND 0.0020 mg/Kg wet L-04, V-05 Bromomethane ND 0.010 mg/Kg wet 2-Butanone (MEK) ND 0.040 mg/Kg wet tert-Butyl Alcohol (TBA) ND 0.040 mg/Kg wet V-16 n-Butylbenzene ND 0.0020 mg/Kg wet sec-Butylbenzene ND 0.0020 mg/Kg wet tert-Butylbenzene ND 0.0020 mg/Kg wet tert-Butyl Ethyl Ether (TBEE) ND 0.0010 mg/Kg wet Carbon Disulfide ND 0.0060 mg/Kg wet Carbon Tetrachloride ND 0.0020 mg/Kg wet Chlorobenzene ND 0.0020 mg/Kg wet Chlorodibromomethane ND 0.0010 mg/Kg wet Chloroethane ND 0.020 mg/Kg wet Chloroform ND 0.0040 mg/Kg wet Chloromethane ND 0.010 mg/Kg wet 2-Chlorotoluene ND 0.0020 mg/Kg wet 4-Chlorotoluene ND 0.0020 mg/Kg wet 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0020 mg/Kg wet 1,2-Dibromoethane (EDB) ND 0.0010 mg/Kg wet Dibromomethane ND 0.0020 mg/Kg wet 1,2-Dichlorobenzene ND 0.0020 mg/Kg wet 1,3-Dichlorobenzene ND 0.0020 mg/Kg wet 1,4-Dichlorobenzene ND 0.0020 mg/Kg wet trans-1,4-Dichloro-2-butene ND 0.0040 mg/Kg wet Dichlorodifluoromethane (Freon 12) ND 0.020 mg/Kg wet 1,1-Dichloroethane ND 0.0020 mg/Kg wet 1,2-Dichloroethane ND 0.0020 mg/Kg wet 1,1-Dichloroethylene ND 0.0040 mg/Kg wet cis-1,2-Dichloroethylene ND 0.0020 mg/Kg wet trans-1,2-Dichloroethylene ND 0.0020 mg/Kg wet 1,2-Dichloropropane ND 0.0020 mg/Kg wet 1,3-Dichloropropane ND 0.0010 mg/Kg wet 2,2-Dichloropropane ND 0.0020 mg/Kg wet 1,1-Dichloropropene ND 0.0020 mg/Kg wet cis-1,3-Dichloropropene ND 0.0010 mg/Kg wet trans-1,3-Dichloropropene ND 0.0010 mg/Kg wet Diethyl Ether ND 0.020 mg/Kg wet Diisopropyl Ether (RIPE) ND 0.0010 mg/Kg wet 1,4-Dioxane ND 0.10 mg/Kg wet V-16 Ethylbenzene ND 0.0020 mg/Kg wet Hexachlorobutadiene ND 0.0020 mg/Kg wet 2-Hexanone (MBK) ND 0.020 mg/Kg wet Isopropylbenzene (Cumene) ND 0.0020 mg/Kg wet p-Isopropyltoluene (p-Cymene) ND 0.0020 mg/Kg wet Methyl tert-Butyl Ether (MTBE) ND 0.0040 mg/Kg wet Page 17 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD 4nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072887 - SW-846 5035 Blank (B072887-BLK1) Prepared & Analyzed: 05/13/13 Methylene Chloride ND 0.020 mg/Kg wet 4-Methyl-2-pentanone (MIBK) ND 0.020 mg/Kg wet Naphthalene ND 0.0040 mg/Kg wet V-05 n-Propylbenzene ND 0.0020 mg/Kg wet Styrene ND 0.0020 mg/Kg wet 1, 1, 1,2-Tetrachloroethane ND 0.0020 mg/Kg wet 1,1,2,2-Tetrachloroethane ND 0.0010 mg/Kg wet Tetrachloroethylene ND 0.0020 mg/Kg wet Tetrahydrofuran ND 0.010 mg/Kg wet Toluene ND 0.0020 mg/Kg wet 1,2,3-Trichlorobenzene ND 0.0020 mg/Kg wet 1,2,4-Trichlorobenzene ND 0.0020 mg/Kg wet V-05 1,3,5-Trichlorobenzene ND 0.0020 mg/Kg wet 1, 1, 1 -Trichloroethane ND 0.0020 mg/Kg wet 1,1,2-Trichloroethane ND 0.0020 mg/Kg wet Trichloroethylene ND 0.0020 mg/Kg wet Trichlorofluoromethane (Freon 11) ND 0.010 mg/Kg wet 1,2,3-Trichloropropane ND 0.0020 mg/Kg wet 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.010 mg/Kg wet 113) 1,2,4-Trimethylbenzene ND 0.0020 mg/Kg wet 1,3,5-Trimethylbenzene ND 0.0020 mg/Kg wet Vinyl Chloride ND 0.010 mg/Kg wet m+p Xylene ND 0.0040 mg/Kg wet o-Xylene ND 0.0020 mg/Kg wet Surrogate: 1,2-Dichloroethane-d4 0.0582 mg/Kg wet 0.0500 116 70-130 Surrogate: Toluene-d8 0.0512 mg/Kg wet 0.0500 102 70-130 Surrogate:4-Bromofluorobenzene 0.0450 mg/Kg wet 0.0500 90.0 70-130 LCS (B072887-BS1) Prepared & Analyzed: 05/13/13 Acetone 0.377 0.10 Acrylonitrile 0.0212 0.0060 tert-Amyl Methyl Ether (TAME) 0.0212 0.0010 Benzene 0.0221 0.0020 Bromobenzene 0.0194 0.0020 Bromochloromethane 0.0238 0.0020 Bromodichloromethane 0.0189 0.0020 Bromoform 0.0126 0.0020 Bromomethane 0.0115 0.010 2-Butanone (MEK) 0.272 0.040 tert-Butyl Alcohol (TBA) 0.165 0.040 n-Butylbenzene 0.0208 0.0020 sec-Butylbenzene 0.0225 0.0020 tert-Butylbenzene 0.0211 0.0020 tert-Butyl Ethyl Ether (TBEE) 0.0214 0.0010 Carbon Disulfide 0.0225 0.0060 Carbon Tetrachloride 0.0174 0.0020 Chlorobenzene 0.0201 0.0020 Chlorodibromomethane 0.0167 0.0010 Chloroethane 0.0217 0.020 Chloroform 0.0220 0.0040 Chloromethane 0.0189 0.010 2-Chlorotoluene 0.0210 0.0020 mg/Kg wet 0.200 188 * 70-160 L-02, V-20 t mg/Kgwet 0.0200 106 70-130 mg/Kg wet 0.0200 106 70-130 mg/Kg wet 0.0200 110 70-130 mg/Kgwet 0.0200 96.8 70-130 mg/Kg wet 0.0200 119 70-130 mg/Kg wet 0.0200 94.6 70-130 mg/Kgwet 0.0200 63.2 * 70-130 V-05,L-04 mg/Kg wet 0.0200 57.3 40-130 t mg/Kg wet 0.200 136 70-160 t mg/Kgwet 0.200 82.7 40-130 V-16 f mg/Kg wet 0.0200 104 70-130 mg/Kg wet 0.0200 112 70-130 mg/Kgwet 0.0200 106 70-160 f mg/Kg wet 0.0200 107 70-130 mg/Kg wet 0.0200 112 70-130 mg/Kgwet 0.0200 86.9 70-130 mg/Kg wet 0.0200 100 70-130 mg/Kg wet 0.0200 83.4 70-130 mg/Kgwet 0.0200 108 70-130 mg/Kg wet 0.0200 110 70-130 mg/Kg wet 0.0200 94.3 70-130 mg/Kg wet 0.0200 105 70-130 Page 18 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD knalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072887 - SW-846 5035 LCS (B072887-BSI) Prepared & Analyzed: 05/13/13 4-Chlorotoluene 0.0214 0.0020 mg/Kg wet 0.0200 107 70-130 1,2-Dibromo-3-chloropropane (DBCP) 0.0164 0.0020 mg/Kg wet 0.0200 82.0 70-130 1,2-Dibromoethane (EDB) 0.0206 0.0010 mg/Kg wet 0.0200 103 70-130 Dibromomethane 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 1,2-Dichlorobenzene 0.0203 0.0020 mg/Kg wet 0.0200 102 70-130 1,3-Dichlorobenzene 0.0210 0.0020 mg/Kg wet 0.0200 105 70-130 1,4-Dichlorobenzene 0.0195 0.0020 mg/Kg wet 0.0200 97.4 70-130 trans-1,4-Dichloro-2-butene 0.0152 0.0040 mg/Kg wet 0.0200 75.9 70-130 Dichlorodifluoromethane(Freon 12) 0.0156 0.020 mg/Kg wet 0.0200 78.1 40-160 1,1-Dichloroethane 0.0213 0.0020 mg/Kg wet 0.0200 106 70-130 1,2-Dichloroethane 0.0199 0.0020 mg/Kg wet 0.0200 99.7 70-130 1,1-Dichloroethylene 0.0221 0.0040 mg/Kg wet 0.0200 110 70-130 cis-1,2-Dichloroethylene 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 trans-1,2-Dichloroethylene 0.0220 0.0020 mg/Kg wet 0.0200 110 70-130 1,2-Dichloropropane 0.0210 0.0020 mg/Kg wet 0.0200 105 70-130 1,3-Dichloropropane 0.0216 0.0010 mg/Kg wet 0.0200 108 70-130 2,2-Dichloropropane 0.0178 0.0020 mg/Kg wet 0.0200 89.0 70-130 1,1-Dichloropropene 0.0220 0.0020 mg/Kg wet 0.0200 110 70-130 cis-1,3-Dichloropropene 0.0181 0.0010 mg/Kg wet 0.0200 90.5 70-130 trans-1,3-Dichloropropene 0.0187 0.0010 mg/Kg wet 0.0200 93.6 70-130 Diethyl Ether 0.0206 0.020 mg/Kg wet 0.0200 103 70-130 Diisopropyl Ether (DIPE) 0.0237 0.0010 mg/Kg wet 0.0200 118 70-130 1,4-Dioxane 0.219 0.10 mg/Kg wet 0.200 110 40-160 Ethylbenzene 0.0199 0.0020 mg/Kg wet 0.0200 99.7 70-130 Hexachlorobutadiene 0.0170 0.0020 mg/Kg wet 0.0200 85.2 70-160 2-Hexanone (MBK) 0.226 0.020 mg/Kg wet 0.200 113 70-160 Isopropylbenzene (Cumene) 0.0207 0.0020 mg/Kg wet 0.0200 104 70-130 p-Isopropyltoluene (p-Cymene) 0.0211 0.0020 mg/Kg wet 0.0200 106 70-130 Methyl tert-Butyl Ether (MTBE) 0.0226 0.0040 mg/Kg wet 0.0200 113 70-130 Methylene Chloride 0.0225 0.020 mg/Kg wet 0.0200 113 40-160 4-Methyl-2-pentanone (MIBK) 0.210 0.020 mg/Kg wet 0.200 105 70-160 Naphthalene 0.0140 0.0040 mg/Kg wet 0.0200 70.0 40-130 n-Propylbenzene 0.0214 0.0020 mg/Kg wet 0.0200 107 70-130 Styrene 0.0194 0.0020 mg/Kg wet 0.0200 96.9 70-130 1, 1, 1,2-Tetrachloroethane 0.0163 0.0020 mg/Kg wet 0.0200 81.7 70-130 1,1,2,2-Tetrachloroethane 0.0191 0.0010 mg/Kg wet 0.0200 95.4 70-130 Tetrachloroethylene 0.0193 0.0020 mg/Kg wet 0.0200 96.6 70-130 Tetrahydrofuran 0.0235 0.010 mg/Kg wet 0.0200 117 70-130 Toluene 0.0211 0.0020 mg/Kg wet 0.0200 105 70-130 1,2,3-Trichlorobenzene 0.0154 0.0020 mg/Kg wet 0.0200 76.9 70-130 1,2,4-Trichlorobenzene 0.0149 0.0020 mg/Kg wet 0.0200 74.5 70-130 1,3,5-Trichlorobenzene 0.0178 0.0020 mg/Kg wet 0.0200 88.9 70-130 1, 1, 1 -Trichloroethane 0.0198 0.0020 mg/Kg wet 0.0200 99.1 70-130 1,1,2-Trichloroethane 0.0194 0.0020 mg/Kg wet 0.0200 96.8 70-130 Trichloroethylene 0.0197 0.0020 mg/Kg wet 0.0200 98.6 70-130 Trichlorofluoromethane (Freon 11) 0.0229 0.010 mg/Kg wet 0.0200 114 70-130 1,2,3-Trichloropropane 0.0197 0.0020 mg/Kg wet 0.0200 98.7 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.0247 0.010 mg/Kg wet 0.0200 124 70-130 113) 1,2,4-Trimethylbenzene 0.0207 0.0020 mg/Kg wet 0.0200 104 70-130 1,3,5-Trimethylbenzene 0.0188 0.0020 mg/Kg wet 0.0200 93.9 70-130 Vinyl Chloride 0.0192 0.010 mg/Kg wet 0.0200 96.0 40-130 J f V-16 t t t t V-05 t V-05 Page 19 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD .nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072887 - SW-846 5035 LCS (B072887-BSI) Prepared & Analyzed: 05/13/13 m+p Xylene 0.0406 0.0040 mg/Kg wet 0.0400 101 70-130 o-Xylene 0.0203 0.0020 mg/Kg wet 0.0200 102 70-130 Surrogate:l,2-Dichloroethane-d4 0.0578 mg/Kg wet 0.0500 116 70-130 Surrogate: Toluene-d8 0.0516 mg/Kg wet 0.0500 103 70-130 Surrogate:4-Bromofluorobenzene 0.0475 mg/Kg wet 0.0500 95.0 70-130 LCS Dup (B072887-BSDI) Prepared & Analyzed: 05/13/13 Acetone 0.383 0.10 mg/Kg wet 0.200 192 • 70-160 1.74 25 L-02, V-20 t Acrylonitrile 0.0215 0.0060 mg/Kg wet 0.0200 108 70-130 1.50 25 tert-Amyl Methyl Ether (TAME) 0.0217 0.0010 mg/Kg wet 0.0200 109 70-130 2.42 25 Benzene 0.0231 0.0020 mg/Kg wet 0.0200 115 70-130 4.43 25 Bromobenzene 0.0198 0.0020 mg/Kg wet 0.0200 99.2 70-130 2.45 25 Bromochloromethane 0.0245 0.0020 mg/Kg wet 0.0200 122 70-130 2.81 25 Bromodichloromethane 0.0190 0.0020 mg/Kg wet 0.0200 94.9 70-130 0.317 25 Bromoform 0.0127 0.0020 mg/Kg wet 0.0200 63.5 * 70-130 0.474 25 L-04, V-05 Bromomethane 0.0144 0.010 mg/Kg wet 0.0200 72.0 40-130 22.7 25 f 2-Butanone (MEK) 0.271 0.040 mg/Kg wet 0.200 136 70-160 0.346 25 t tert-Butyl Alcohol (TBA) 0.168 0.040 mg/Kg wet 0.200 84.0 40-130 1.60 25 V-16 t n-Butylbenzene 0.0211 0.0020 mg/Kg wet 0.0200 105 70-130 1.43 25 sec-Butylbenzene 0.0229 0.0020 mg/Kg wet 0.0200 115 70-130 1.85 25 tert-Butylbenzene 0.0215 0.0020 mg/Kg wet 0.0200 108 70-160 1.87 25 t tert-Butyl Ethyl Ether (TBEE) 0.0221 0.0010 mg/Kg wet 0.0200 111 70-130 3.59 25 Carbon Disulfide 0.0241 0.0060 mg/Kg wet 0.0200 121 70-130 7.04 25 Carbon Tetrachloride 0.0181 0.0020 mg/Kg wet 0.0200 90.6 70-130 4.17 25 Chlorobenzene 0.0203 0.0020 mg/Kg wet 0.0200 102 70-130 1.29 25 Chlorodibromomethane 0.0171 0.0010 mg/Kg wet 0.0200 85.6 70-130 2.60 25 Chloroethane 0.0227 0.020 mg/Kg wet 0.0200 114 70-130 4.77 25 Chloroform 0.0227 0.0040 mg/Kg wet 0.0200 114 70-130 3.40 25 Chloromethane 0.0203 0.010 mg/Kg wet 0.0200 101 70-130 7.16 25 2-Chlorotoluene 0.0215 0.0020 mg/Kg wet 0.0200 108 70-130 2.54 25 4-Chlorotoluene 0.0220 0.0020 mg/Kg wet 0.0200 110 70-130 2.76 25 1,2-Dibromo-3-chloropropane (DBCP) 0.0167 0.0020 mg/Kg wet 0.0200 83.3 70-130 1.57 25 1,2-Dibromoethane (EDB) 0.0204 0.0010 mg/Kg wet 0.0200 102 70-130 0.976 25 Dibromomethane 0.0211 0.0020 mg/Kg wet 0.0200 106 70-130 2.68 25 1,2-Dichlorobenzene 0.0210 0.0020 mg/Kg wet 0.0200 105 70-130 3.00 25 1,3-Dichlorobenzene 0.0215 0.0020 mg/Kg wet 0.0200 108 70-130 2.54 25 1,4-Dichlorobenzene 0.0198 0.0020 mg/Kg wet 0.0200 98.8 70-130 1.43 25 trans-1,4-Dichloro-2-butene 0.0156 0.0040 mg/Kg wet 0.0200 78.1 70-130 2.86 25 Dichlorodifluoromethane(Freon 12) 0.0164 0.020 mg/Kg wet 0.0200 82.1 40-160 4.99 25 J t 1, 1 -Dichloroethane 0.0223 0.0020 mg/Kg wet 0.0200 112 70-130 4.86 25 1,2-Dichloroethane 0.0201 0.0020 mg/Kg wet 0.0200 101 70-130 0.998 25 1,1-Dichloroethylene 0.0234 0.0040 mg/Kg wet 0.0200 117 70-130 5.80 25 cis-1,2-Dichloroethylene 0.0215 0.0020 mg/Kg wet 0.0200 107 70-130 3.90 25 trans-1,2-Dichloroethylene 0.0238 0.0020 mg/Kg wet 0.0200 119 70-130 8.13 25 1,2-Dichloropropane 0.0213 0.0020 mg/Kg wet 0.0200 106 70-130 1.52 25 1,3-Dichloropropane 0.0218 0.0010 mg/Kg wet 0.0200 109 70-130 1.11 25 2,2-Dichloropropane 0.0185 0.0020 mg/Kg wet 0.0200 92.4 70-130 3.75 25 1,1-Dichloropropene 0.0229 0.0020 mg/Kg wet 0.0200 114 70-130 3.92 25 cis-1,3-Dichloropropene 0.0183 0.0010 mg/Kg wet 0.0200 91.5 70-130 1.10 25 trans-1,3-Dichloropropene 0.0191 0.0010 mg/Kg wet 0.0200 95.6 70-130 2.11 25 Diethyl Ether 0.0223 0.020 mg/Kg wet 0.0200 111 70-130 7.55 25 Diisopropyl Ether (DIPE) 0.0247 0.0010 mg/Kg wet 0.0200 124 70-130 4.13 25 Page 20 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072887 - SW-846 5035 LCS Dup (B072887-BSD1) Prepared & Analyzed: 05/13/13 1,4-Dioxane 0.212 0.10 mg/Kgwet 0.200 106 40-160 3.44 50 V-16 f $ Ethylbenzene 0.0201 0.0020 mg/Kg wet 0.0200 101 70-130 0.998 25 Hexachlorobutadiene 0.0173 0.0020 mg/Kg wet 0.0200 86.6 70-160 1.63 25 2-Hexanone (MBK) 0.228 0.020 mg/Kg wet 0.200 114 70-160 0.617 25 f Isopropylbenzene (Cumene) 0.0211 0.0020 mg/Kg wet 0.0200 105 70-130 1.53 25 p-Isopropyltoluene (p-Cymene) 0.0216 0.0020 mg/Kg wet 0.0200 108 70-130 1.97 25 Methyl tert-Butyl Ether (MTBE) 0.0237 0.0040 mg/Kg wet 0.0200 119 70-130 4.74 25 Methylene Chloride 0.0236 0.020 mg/Kg wet 0.0200 118 40-160 4.77 25 f 4-Methyl-2-pentanone (MIBK) 0.215 0.020 mg/Kg wet 0.200 108 70-160 2.65 25 t Naphthalene 0.0142 0.0040 mg/Kg wet 0.0200 71.2 40-130 1.70 25 V-05 f n-Propylbenzene 0.0219 0.0020 mg/Kg wet 0.0200 110 70-130 2.40 25 Styrene 0.0197 0.0020 mg/Kg wet 0.0200 98.3 70-130 1.43 25 1, 1, 1,2-Tetrachloroethane 0.0166 0.0020 mg/Kg wet 0.0200 83.1 70-130 1.70 25 1,1,2,2-Tetrachloroethane 0.0194 0.0010 mg/Kg wet 0.0200 97.1 70-130 1.77 25 Tetrachloroethylene 0.0197 0.0020 mg/Kg wet 0.0200 98.3 70-130 1.74 25 Tetrahydrofuran 0.0259 0.010 mg/Kg wet 0.0200 130 70-130 9.96 25 Toluene 0.0214 0.0020 mg/Kg wet 0.0200 107 70-130 1.60 25 1,2,3-Trichlorobenzene 0.0155 0.0020 mg/Kg wet 0.0200 77.3 70-130 0.519 25 1,2,4-Trichlorobenzene 0.0150 0.0020 mg/Kg wet 0.0200 75.1 70-130 0.802 25 V-05 1,3,5-Trichlorobenzene 0.0179 0.0020 mg/Kg wet 0.0200 89.6 70-130 0.784 25 1, 1, 1 -Trichloroethane 0.0202 0.0020 mg/Kg wet 0.0200 101 70-130 2.10 25 1,1,2-Trichloroethane 0.0200 0.0020 mg/Kg wet 0.0200 100 70-130 3.35 25 Trichloroethylene 0.0204 0.0020 mg/Kg wet 0.0200 102 70-130 3.49 25 Trichlorofluoromethane (Freon 11) 0.0243 0.010 mg/Kg wet 0.0200 121 70-130 6.02 25 1,2,3-Trichloropropane 0.0201 0.0020 mg/Kg wet 0.0200 100 70-130 1.71 25 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.0257 0.010 mg/Kg wet 0.0200 129 70-130 4.04 25 113) 1,2,4-Trimethylbenzene 0.0209 0.0020 mg/Kg wet 0.0200 105 70-130 0.960 25 1,3,5-Trimethylbenzene 0.0191 0.0020 mg/Kg wet 0.0200 95.7 70-130 1.90 25 Vinyl Chloride 0.0203 0.010 mg/Kg wet 0.0200 101 40-130 5.47 25 t m+p Xylene 0.0409 0.0040 mg/Kg wet 0.0400 102 70-130 0.884 25 o-Xylene 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 1.47 25 Surrogate: 1,2-Dichloroethane-d4 0.0573 mg/Kg wet 0.0500 115 70-130 Surrogate: Toluene-d8 0.0520 mg/Kg wet 0.0500 104 70-130 Surrogate:4-Bromofluorobenzene 0.0479 mg/Kg wet 0.0500 95.9 70-130 Page 21 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072855 - SW-846 3546 Blank (B072855-BLK1) Prepared & Analyzed: 05/13/13 Acenaphthene ND 0.17 mg/Kg wet Acenaphthylene ND 0.17 mg/Kg wet Acetophenone ND 0.34 mg/Kg wet Aniline ND 0.34 mg/Kg wet Anthracene ND 0.17 mg/Kg wet Benzidine ND 0.34 mg/Kg wet V-04 Benzo(a)anthracene ND 0.17 mg/Kg wet Benzo(a)pyrene ND 0.17 mg/Kg wet Benzo(b)fluoranthene ND 0.17 mg/Kg wet Benzo(g,h,i)perylene ND 0.17 mg/Kg wet Benzo(b)fluoranthene ND 0.17 mg/Kg wet Benzoic Acid ND 1.0 mg/Kg wet R-05, V-19 Bis(2-chloroethoxy)methane ND 0.34 mg/Kg wet Bis(2-chloroethyl)ether ND 0.34 mg/Kg wet Bis(2-chloroisopropyl)ether ND 0.34 mg/Kg wet Bis(2-Ethylhexyl)phthalate ND 0.34 mg/Kg wet 4-Bromophenylphenylether ND 0.34 mg/Kg wet Butylbenzylphthalate ND 0.66 mg/Kg wet Carbazole ND 0.17 mg/Kg wet 4-Chloroaniline ND 0.66 mg/Kg wet 4-Chloro-3-methylphenol ND 0.66 mg/Kg wet 2-Chloronaphthalene ND 0.34 mg/Kg wet 2-Chlorophenol ND 0.34 mg/Kg wet 4-Chlorophenylphenylether ND 0.34 mg/Kg wet Chrysene ND 0.17 mg/Kg wet Dibenz(a,h)anthracene ND 0.17 mg/Kg wet Dibenzofuran ND 0.34 mg/Kg wet Di-n-butylphthalate ND 0.34 mg/Kg wet 1,2-Dichlorobenzene ND 0.34 mg/Kg wet 1,3-Dichlorobenzene ND 0.34 mg/Kg wet 1,4-Dichlorobenzene ND 0.34 mg/Kg wet 3,3-Dichlorobenzidine ND 0.17 mg/Kg wet 2,4-Dichlorophenol ND 0.34 mg/Kg wet Diethylphthalate ND 0.34 mg/Kg wet 2,4-Dimethylphenol ND 0.34 mg/Kg wet Dimethylphthalate ND 0.66 mg/Kg wet 4,6-Dinitro-2-methylphenol ND 0.34 mg/Kg wet 2,4-Dinitrophenol ND 0.66 mg/Kg wet V-05 2,4-Dinitrotoluene ND 0.34 mg/Kg wet 2,6-Dinitrotoluene ND 0.34 mg/Kg wet Di-n-octylphthalate ND 0.66 mg/Kg wet R-05 1,2-Diphenylhydrazine (as Azobenzene) ND 0.34 mg/Kg wet Fluoranthene ND 0.17 mg/Kg wet R-05 Fluorene ND 0.17 mg/Kg wet Hexachlorobenzene ND 0.34 mg/Kg wet Hexachlorobutadiene ND 0.34 mg/Kg wet Hexachlorocyclopentadiene ND 0.66 mg/Kg wet Hexachloroethane ND 0.34 mg/Kg wet Indeno(1,2,3-cd)pyrene ND 0.17 mg/Kg wet R-05 Isophorone ND 0.34 mg/Kg wet 1-Methylnaphthalene ND 0.17 mg/Kg wet 2-Methylnaphthalene ND 0.17 mg/Kg wet Page 22 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD .nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072855 - SW-846 3546 Blank (B072855-BLK1) Prepared & Analyzed: 05/13/13 2-Methylphenol ND 0.34 mg/Kg wet 3/4-Methylphenol ND 0.34 mg/Kg wet Naphthalene ND 0.17 mg/Kg wet 2-Nitroaniline ND 0.34 mg/Kg wet 3-Nitroaniline ND 0.34 mg/Kg wet 4-Nitroaniline ND 0.34 mg/Kg wet V-05 Nitrobenzene ND 0.34 mg/Kg wet 2-Nitrophenol ND 0.34 mg/Kg wet 4-Nitrophenol ND 0.66 mg/Kg wet V-05 N-Nitrosodimethylamine ND 0.34 mg/Kg wet N-Nitrosodiphenylamine ND 0.34 mg/Kg wet N-Nitrosodi-n-propylamine ND 0.34 mg/Kg wet Pentachloronitrobenzene ND 0.34 mg/Kg wet V-16 Pentachlorophenol ND 0.34 mg/Kg wet Phenanthrene ND 0.17 mg/Kg wet Phenol ND 0.34 mg/Kg wet Pyrene ND 0.17 mg/Kg wet Pyridine ND 0.34 mg/Kg wet 1,2,4,5-Tetrachlorobenzene ND 0.34 mg/Kg wet 1,2,4-Trichlorobenzene ND 0.34 mg/Kg wet 2,4,5-Trichlorophenol ND 0.34 mg/Kg wet 2,4,6-Trichlorophenol ND 0.34 mg/Kg wet Surrogate:2-Fluorophenol 6.81 mg/Kg wet 6.67 102 30-130 Surrogate: Phenol-d6 6.82 mg/Kg wet 6.67 102 30-130 Surrogate: Nitrobenzene-d5 3.20 mg/Kg wet 3.33 95.9 30-130 Surrogate:2-Fluorobiphenyl 3.17 mg/Kg wet 3.33 95.0 30-130 Surrogate: 2,4,6-Tribromophenol 7.21 mg/Kg wet 6.67 108 30-130 Surrogate: p-Terphenyl-dl4 3.21 mg/Kg wet 3.33 96.2 30-130 LCS (B072855-BS1) Prepared & Analyzed: 05/13/13 Acenaphthene 1.71 0.17 mg/Kg wet 1.67 103 40-140 Acenaphthylene 1.73 0.17 mg/Kg wet 1.67 104 40-140 Acetophenone 1.64 0.34 mg/Kg wet 1.67 98.5 40-140 Aniline 1.52 0.34 mg/Kg wet 1.67 91.5 10-140 t Anthracene 1.87 0.17 mg/Kg wet 1.67 112 40-140 Benzidine 1.44 0.34 mg/Kg wet 1.67 86.5 40-140 V-04 Benzo(a)anthracene 1.86 0.17 mg/Kg wet 1.67 112 40-140 Benzo(a)pyrene 1.85 0.17 mg/Kg wet 1.67 ill 40-140 Benzo(b)fluoranthene 1.86 0.17 mg/Kg wet 1.67 ill 40-140 Benzo(g,h,i)perylene 1.98 0.17 mg/Kg wet 1.67 94.5 40-140 Benzo(k)fluoranthene 1.84 0.17 mg/Kg wet 1.67 110 40-140 Benzoic Acid 0.733 1.0 mg/Kg wet 1.67 44.0 30-130 J, R-05, V-19 Bis(2-chloroethoxy)methane 1.72 0.34 mg/Kg wet 1.67 103 40-140 Bis(2-chloroethyl)ether 1.48 0.34 mg/Kg wet 1.67 94.6 40-140 Bis(2-chloroisopropyl)ether 1.56 0.34 mg/Kg wet 1.67 93.6 40-140 Bis(2-Ethylhexyl)phthalate 1.87 0.34 mg/Kg wet 1.67 112 40-140 4-Bromophenylphenylether 1.80 0.34 mg/Kg wet 1.67 108 40-140 Butylbenzylphthalate 1.83 0.66 mg/Kg wet 1.67 110 40-140 Carbazole 1.96 0.17 mg/Kg wet 1.67 118 40-140 4-Chloroaniline 1.59 0.66 mg/Kg wet 1.67 95.2 10-140 4-Chloro-3-methylphenol 1.77 0.66 mg/Kg wet 1.67 106 30-130 2-Chloronaphthalene 1.51 0.34 mg/Kg wet 1.67 90.6 40-140 Page 23 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072855 - SW-846 3546 LCS (B072855-BSI) 2-Chlorophenol 1.77 0.34 mg/Kg wet 4-Chlorophenylphenylether 1.72 0.34 mg/Kg wet Chrysene 1.80 0.17 mg/Kg wet Dibenz(a,h)anthracene 1.61 0.17 mg/Kg wet Dibenzofuran 1.73 0.34 mg/Kg wet Di-n-butylphthalate 1.87 0.34 mg/Kg wet 1,2-Dichlorobenzene 1.54 0.34 mg/Kg wet 1,3-Dichlorobenzene 1.92 0.34 mg/Kg wet 1,4-Dichlorobenzene 1.48 0.34 mg/Kg wet 3,3-Dichlorobenzidine 1.45 0.17 mg/Kg wet 2,4-Dichlorophenol 1.78 0.34 mg/Kg wet Diethylphthalate 1.74 0.34 mg/Kg wet 2,4-Dimethylphenol 1.78 0.34 mg/Kg wet Dimethylphthalate 1.72 0.66 mg/Kg wet 4,6-Dinitro-2-methylphenol 1.66 0.34 mg/Kg wet 2,4-Dinitrophenol 1.25 0.66 mg/Kg wet 2,4-Dinitrotoluene 1.90 0.34 mg/Kg wet 2,6-Dinitrotoluene 1.88 0.34 mg/Kg wet Di-n-octylphthalate 1.97 0.66 mg/Kg wet 1,2-Diphenylhydrazine (as Azobenzene) 1.86 0.34 mg/Kg wet Fluoranthene 2.02 0.17 mg/Kg wet Fluorene 1.75 0.17 mg/Kg wet Hexachlorobenzene 1.72 0.34 mg/Kg wet Hexachlorobutadiene 1.55 0.34 mg/Kg wet Hexachlorocyclopentadiene 1.55 0.66 mg/Kg wet Hexachloroethane 1.56 0.34 mg/Kg wet Indeno(1,2,3-cd)pyrene 1.59 0.17 mg/Kg wet Isophorone 1.59 0.34 mg/Kg wet 1-Methylnaphthalene 1.98 0.17 mg/Kg wet 2-Methylnaphthalene 1.42 0.17 mg/Kg wet 2-Methylphenol 1.70 0.34 mg/Kg wet 3/4-Methylphenol 1.97 0.34 mg/Kg wet Naphthalene 1.54 0.17 mg/Kg wet 2-Nitroaniline 1.80 0.34 mg/Kg wet 3-Nitroaniline 1.86 0.34 mg/Kg wet 4-Nitroaniline 1.74 0.34 mg/Kg wet Nitrobenzene 1.47 0.34 mg/Kg wet 2-Nitrophenol 1.66 0.34 mg/Kg wet 4-Nitrophenol 1.76 0.66 mg/Kg wet N-Nitrosodimethylamine 1.65 0.34 mg/Kg wet N-Nitrosodiphenylamine 2.13 0.34 mg/Kg wet N-Nitrosodi-n-propylamine 1.60 0.34 mg/Kg wet Pentachloronitrobenzene 1.85 0.34 mg/Kg wet Pentachlorophenol 1.84 0.34 mg/Kg wet Phenanthrene 1.82 0.17 mg/Kg wet Phenol 1.64 0.34 mg/Kg wet Pyrene 1.39 0.17 mg/Kg wet Pyridine 1.27 0.34 mg/Kg wet 1,2,4,5-Tetrachlorobenzene 1.67 0.34 mg/Kg wet 1,2,4-Trichlorobenzene 1.56 0.34 mg/Kg wet 2,4,5-Trichlorophenol 1.87 0.34 mg/Kg wet 2,4,6-Trichlorophenol 1.86 0.34 mg/Kg wet Prepared & Analyzed: 05/13/13 1.67 106 30-130 1.67 103 40-140 1.67 108 40-140 1.67 96.8 40-140 1.67 104 40-140 1.67 112 40-140 1.67 92.5 40-140 1.67 91.0 40-140 1.67 88.6 40-140 1.67 87.1 20-140 t 1.67 107 30-130 1.67 104 40-140 1.67 107 30-130 1.67 103 40-140 1.67 99.6 30-130 1.67 75.0 30-130 V-05 1.67 114 40-140 1.67 113 40-140 1.67 118 40-140 R-05 1.67 112 40-140 1.67 121 40-140 R-05 1.67 105 40-140 1.67 103 40-140 1.67 93.3 40-140 1.67 93.2 40-140 1.67 93.5 40-140 1.67 95.6 40-140 R-05 1.67 95.5 40-140 1.67 94.7 40-140 1.67 91.1 40-140 1.67 102 30-130 1.67 93.9 30-130 1.67 92.7 40-140 1.67 108 40-140 1.67 112 30-140 t 1.67 104 40-140 V-05 1.67 94.1 40-140 1.67 99.4 30-130 1.67 105 30-130 V-05 1.67 98.9 40-140 1.67 128 40-140 1.67 95.7 40-140 1.67 111 40-140 V-16 1.67 110 30-130 1.67 109 40-140 1.67 98.3 30-130 1.67 83.7 40-140 1.67 76.2 30-140 1.67 100 40-140 1.67 93.3 40-140 1.67 112 30-130 1.67 112 30-130 Page 24 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD malyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072855 - SW-846 3546 LCS (B072855-BSI) Prepared & Analyzed: 05/13/13 Surrogate:2-Fluorophenol 7.09 mg/Kg wet 6.67 106 30-130 Surrogate: Phenol-d6 7.10 mg/Kg wet 6.67 107 30-130 Surrogate: Nitrobenzene-d5 3.29 mg/Kg wet 3.33 98.6 30-130 Surrogate:2-Fluorobiphenyl 3.41 mg/Kg wet 3.33 102 30-130 Surrogate: 2,4,6-Tribromophenol 7.65 mg/Kg wet 6.67 115 30-130 Surrogate:p-Terphenyl-dl4 3.10 mg/Kg wet 3.33 93.0 30-130 LCS Dup (B072855-BSD1) Prepared: 05/13/13 Analyzed: 05/14/13 Acenaphthene 1.59 0.17 mg/Kg wet Acenaphthylene 1.60 0.17 mg/Kg wet Acetophenone 1.36 0.34 mg/Kg wet Aniline 1.33 0.34 mg/Kg wet Anthracene 1.70 0.17 mg/Kg wet Benzidine 1.46 0.34 mg/Kg wet Benzo(a)anthracene 1.76 0.17 mg/Kg wet Benzo(a)pyrene 1.67 0.17 mg/Kg wet Benzo(b)fluoranthene 1.60 0.17 mg/Kg wet Benzo(g,h,i)perylene 2.04 0.17 mg/Kg wet Benzo(b)fluoranthene 1.49 0.17 mg/Kg wet Benzoic Acid 0.270 1.0 mg/Kg wet Bis(2-chloroethoxy)methane 1.45 0.34 mg/Kg wet Bis(2-chloroethyl)ether 1.35 0.34 mg/Kg wet Bis(2-chloroisopropyl)ether 1.32 0.34 mg/Kg wet Bis(2-Ethylhexyl)phthalate 1.70 0.34 mg/Kg wet 4-Bromophenylphenylether 1.69 0.34 mg/Kg wet Butylbenzylphthalate 1.64 0.66 mg/Kg wet Carbazole 1.64 0.17 mg/Kg wet 4-Chloroaniline 1.98 0.66 mg/Kg wet 4-Chloro-3-methylphenol 1.87 0.66 mg/Kg wet 2-Chloronaphthalene 1.26 0.34 mg/Kg wet 2-Chorophenol 1.47 0.34 mg/Kg wet 4-Chlorophenylphenylether 1.80 0.34 mg/Kg wet Chrysene 1.67 0.17 mg/Kg wet Dibenz(a,h)anthracene 2.11 0.17 mg/Kg wet Dibenzofuran 1.70 0.34 mg/Kg wet Di-n-butylphthalate 1.50 0.34 mg/Kg wet 1,2-Dichlorobenzene 1.43 0.34 mg/Kg wet 1,3-Dichlorobenzene 1.44 0.34 mg/Kg wet 1,4-Dichlorobenzene 1.42 0.34 mg/Kg wet 3,3-Dichlorobenzidine 1.46 0.17 mg/Kg wet 2,4-Dichlorophenol 1.37 0.34 mg/Kg wet Diethylphthalate 1.95 0.34 mg/Kg wet 2,4-Dimethylphenol 1.54 0.34 mg/Kg wet Dimethylphthalate 1.85 0.66 mg/Kg wet 4,6-Dinitro-2-methylphenol 1.52 0.34 mg/Kg wet 2,4-Dinitrophenol 1.46 0.66 mg/Kg wet 2,4-Dinitrotoluene 2.21 0.34 mg/Kg wet 2,6-Dinitrotoluene 2.10 0.34 mg/Kg wet Di-n-octylphthalate 1.43 0.66 mg/Kg wet 1,2-Diphenylhydrazine (as Azobenzene) 1.63 0.34 mg/Kg wet Fluoranthene 1.48 0.17 mg/Kg wet Fluorene 1.84 0.17 mg/Kg wet 1.67 95.3 40-140 7.45 30 1.67 95.8 40-140 8.21 30 1.67 81.7 40-140 18.7 30 1.67 79.6 10-140 13.9 50 t 1 1.67 102 40-140 9.39 30 1.67 87.4 40-140 0.989 30 V-04, V-06 1.67 106 40-140 5.40 30 1.67 100 40-140 10.1 30 1.67 96.3 40-140 14.6 30 1.67 122 40-140 25.6 30 1.67 89.3 40-140 21.0 30 1.67 16.2 * 30-130 92.3 * 50 J,L-07A,V-19 $ 1.67 87.2 40-140 16.8 30 1.67 81.0 40-140 15.5 30 1.67 79.3 40-140 16.5 30 1.67 102 40-140 9.83 30 1.67 101 40-140 6.28 30 1.67 98.1 40-140 11.0 30 1.67 98.1 40-140 18.2 30 1.67 94.8 10-140 0.421 30 t 1.67 112 30-130 5.35 30 1.67 75.9 40-140 17.6 30 1.67 88.2 30-130 18.3 30 1.67 108 40-140 4.17 30 1.67 100 40-140 7.45 30 1.67 127 40-140 26.7 30 1.67 102 40-140 2.14 30 1.67 90.0 40-140 22.1 30 1.67 85.7 40-140 7.63 30 1.67 86.6 40-140 4.96 30 1.67 85.2 40-140 3.87 30 1.67 87.4 20-140 0.275 50 t 1 1.67 94.2 30-130 12.4 30 1.67 117 40-140 11.2 30 1.67 92.3 30-130 14.3 30 1.67 ill 40-140 7.60 30 1.67 91.1 30-130 8.92 30 1.67 87.8 30-130 15.7 30 1.67 132 40-140 15.0 30 1.67 126 40-140 11.1 30 1.67 85.9 40-140 31.8 * 30 R-05 1.67 98.0 40-140 13.1 30 1.67 89.0 40-140 30.8 * 30 R-05 1.67 ill 40-140 5.35 30 Page 25 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072855 - SW-846 3546 LCS Dup (B072855-BSD1) Prepared: 05/13/13 Analyzed: 05/14/13 Hexachlorobenzene 1.64 0.34 mg/Kg wet 1.67 98.4 40-140 4.57 30 Hexachlorobutadiene 1.92 0.34 mg/Kg wet 1.67 91.0 40-140 2.45 30 Hexachlorocyclopentadiene 1.17 0.66 mg/Kg wet 1.67 69.9 40-140 28.5 30 Hexachloroethane 1.44 0.34 mg/Kg wet 1.67 86.4 40-140 7.80 30 Indeno(1,2,3-cd)pyrene 2.20 0.17 mg/Kg wet 1.67 132 40-140 31.9 * 30 R-05 Isophorone 1.40 0.34 mg/Kg wet 1.67 84.1 40-140 12.7 30 1-Methylnaphthalene 1.45 0.17 mg/Kg wet 1.67 86.9 40-140 8.59 30 2-Methylnaphthalene 1.39 0.17 mg/Kg wet 1.67 83.4 40-140 8.78 30 2-Methylphenol 1.35 0.34 mg/Kg wet 1.67 80.8 30-130 23.2 30 3/4-Methylphenol 1.31 0.34 mg/Kg wet 1.67 78.8 30-130 17.5 30 Naphthalene 1.43 0.17 mg/Kg wet 1.67 85.6 40-140 7.92 30 2-Nitroanihne 1.90 0.34 mg/Kg wet 1.67 114 40-140 5.50 30 3-Nitroaniline 2.21 0.34 mg/Kg wet 1.67 132 30-140 17.0 30 f 4-Nitroaniline 1.95 0.34 mg/Kg wet 1.67 117 40-140 12.0 30 Nitrobenzene 1.44 0.34 mg/Kg wet 1.67 86.4 40-140 8.49 30 2-Nitrophenol 1.54 0.34 mg/Kg wet 1.67 92.7 30-130 6.98 30 4-Nitrophenol 1.96 0.66 mg/Kg wet 1.67 117 30-130 10.7 50 $ N-Nitrosodimethylamine 1.55 0.34 mg/Kg wet 1.67 92.9 40-140 6.30 30 N-Nitrosodiphenylamine 1.96 0.34 mg/Kg wet 1.67 118 40-140 8.07 30 N-Nitrosodi-n-propylamine 1.26 0.34 mg/Kg wet 1.67 75.6 40-140 23.5 30 Pentachloronitrobenzene 1.73 0.34 mg/Kg wet 1.67 104 40-140 6.94 30 V-16 Pentachlorophenol 1.72 0.34 mg/Kg wet 1.67 103 30-130 6.53 30 Phenanthrene 1.66 0.17 mg/Kg wet 1.67 99.5 40-140 9.37 30 Phenol 1.36 0.34 mg/Kg wet 1.67 81.3 30-130 18.9 30 Pyrene 1.48 0.17 mg/Kg wet 1.67 95.0 40-140 12.7 30 Pyridine 1.31 0.34 mg/Kg wet 1.67 78.8 30-140 3.35 30 t 1,2,4,5-Tetrachlorobenzene 1.31 0.34 mg/Kg wet 1.67 78.4 40-140 24.5 30 1,2,4-Trichlorobenzene 1.47 0.34 mg/Kg wet 1.67 87.9 40-140 5.91 30 2,4,5-Trichlorophenol 1.84 0.34 mg/Kg wet 1.67 110 30-130 1.57 30 2,4,6-Trichlorophenol 1.68 0.34 mg/Kg wet 1.67 101 30-130 10.2 30 Surrogate:2-Fluorophenol 5.98 mg/Kg wet 6.67 89.7 30-130 Surrogate: Phenol-d6 5.65 mg/Kg wet 6.67 84.7 30-130 Surrogate: Nitrobenzene-d5 2.93 mg/Kg wet 3.33 87.9 30-130 Surrogate: 2-Fluorobiphenyl 2.56 mg/Kg wet 3.33 77.0 30-130 Surrogate: 2,4,6-Tribromophenol 8.65 mg/Kg wet 6.67 130 30-130 Surrogate: p-Terphenyl-dl4 3.29 mg/Kg wet 3.33 98.7 30-130 Page 26 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - EPH - Quality Control Reporting Spike Source %REC RPD \nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072854 - SW-846 3546 Blank (B072854-BLK1) Prepared & Analyzed: 05/13/13 C9-C 18 Aliphatics ND 10 mg/Kg wet C19-C36 Aliphatics ND 10 mg/Kg wet Unadjusted CI I-C22 Aromatics ND 10 mg/Kg wet Cl 1-C22 Aromatics ND 10 mg/Kg wet Acenaphthene ND 0.10 mg/Kg wet Acenaphthylene ND 0.10 mg/Kg wet Anthracene ND 0.10 mg/Kg wet Benzo(a)anthracene ND 0.10 mg/Kg wet Benzo(a)pyrene ND 0.10 mg/Kg wet Benzo(b)fluoranthene ND 0.10 mg/Kg wet Benzo(g,h,i)perylene ND 0.10 mg/Kg wet Benzo(k)fluoranthene ND 0.10 mg/Kg wet Chrysene ND 0.10 mg/Kg wet Dibenz(a,h)anthracene ND 0.10 mg/Kg wet Fluoranthene ND 0.10 mg/Kg wet Fluorene ND 0.10 mg/Kg wet Indeno(1,2,3-cd)pyrene ND 0.10 mg/Kg wet 2-Methylnaphthalene ND 0.10 mg/Kg wet Naphthalene ND 0.10 mg/Kg wet Phenanthrene ND 0.10 mg/Kg wet Pyrene ND 0.10 mg/Kg wet Surrogate: Chlorooctadecane (COD) 3.44 mg/Kg wet 4.99 69.0 40-140 Surrogate: o-Terphenyl (OTP) 3.05 mg/Kg wet 5.00 61.1 40-140 Surrogate:2-Bromonaphthalene 4.30 mg/Kg wet 5.00 86.0 40-140 Surrogate: 2-Fluorobiphenyl 4.46 mg/Kg wet 5.00 89.2 40-140 LCS (B072854-BS1) Prepared & Analyzed: 05/13/13 Acenaphthene 3.31 0.10 mg/Kg wet Acenaphthylene 3.19 0.10 mg/Kg wet Anthracene 3.61 0.10 mg/Kg wet Benzo(a)anthracene 3.63 0.10 mg/Kg wet Benzo(a)pyrene 3.36 0.10 mg/Kg wet Benzo(b)fluoranthene 3.68 0.10 mg/Kg wet Benzo(g,h,i)perylene 3.91 0.10 mg/Kg wet Benzo(k)fluoranthene 3.64 0.10 mg/Kg wet Chrysene 3.44 0.10 mg/Kg wet Dibenz(a,h)anthracene 3.90 0.10 mg/Kg wet Fluoranthene 3.37 0.10 mg/Kg wet Fluorene 3.45 0.10 mg/Kg wet Indeno(1,2,3-cd)pyrene 3.93 0.10 mg/Kg wet 2-Methylnaphthalene 3.11 0.10 mg/Kg wet Naphthalene 2.81 0.10 mg/Kg wet Phenanthrene 3.53 0.10 mg/Kg wet Pyrene 3.48 0.10 mg/Kg wet n-Decane 2.55 0.10 mg/Kg wet n-Docosane 4.20 0.10 mg/Kg wet n-Dodecane 3.35 0.10 mg/Kg wet n-Eicosane 4.23 0.10 mg/Kg wet n-Hexacosane 4.03 0.10 mg/Kg wet n-Hexadecane 4.26 0.10 mg/Kg wet n-Hexatriacontane 4.30 0.10 mg/Kg wet n-Nonadecane 4.28 0.10 mg/Kg wet 5.00 66.2 40-140 5.00 63.8 40-140 5.00 72.2 40-140 5.00 72.7 40-140 5.00 71.2 40-140 5.00 73.6 40-140 5.00 78.2 40-140 5.00 72.8 40-140 5.00 68.8 40-140 5.00 78.0 40-140 5.00 71.4 40-140 5.00 68.9 40-140 5.00 78.6 40-140 5.00 62.3 40-140 5.00 56.2 40-140 5.00 70.5 40-140 5.00 69.6 40-140 5.00 51.0 40-140 5.00 84.0 40-140 5.00 67.0 40-140 5.00 84.6 40-140 5.00 80.7 40-140 5.00 85.2 40-140 5.00 86.0 40-140 5.00 85.6 40-140 Page 27 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - EPH - Quality Control Reporting Spike Source %REC RPD knalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072854 - SW-846 3546 LCS (B072854-BSI) Prepared & Analyzed: 05/13/13 n-Nonane 1.73 0.10 mg/Kg wet 5.00 34.6 30-140 n-Octacosane 3.96 0.10 mg/Kg wet 5.00 79.2 40-140 n-Octadecane 4.26 0.10 mg/Kg wet 5.00 85.2 40-140 n-Tetracosane 4.11 0.10 mg/Kg wet 5.00 82.1 40-140 n-Tetradecane 3.92 0.10 mg/Kg wet 5.00 78.4 40-140 n-Triacontane 4.06 0.10 mg/Kg wet 5.00 81.3 40-140 Naphthalene -aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 2-Methylnaphthalene-aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 Surrogate: Chlorooctadecane (COD) 4.17 mg/Kg wet 4.99 83.6 40-140 Surrogate: o-Terphenyl (OTP) 3.33 mg/Kg wet 5.00 66.6 40-140 Surrogate:2-Bromonaphthalene 3.98 mg/Kg wet 5.00 79.6 40-140 Surrogate:2-Fluorobiphenyl 4.24 mg/Kg wet 5.00 84.7 40-140 LCS Dup (11072854-11SD1) Prepared & Analyzed: 05/13/13 Acenaphthene 3.47 0.10 mg/Kg wet 5.00 69.4 40-140 4.66 25 Acenaphthylene 3.32 0.10 mg/Kg wet 5.00 66.4 40-140 4.03 25 Anthracene 3.88 0.10 mg/Kg wet 5.00 77.7 40-140 7.39 25 Benzo(a)anthracene 4.01 0.10 mg/Kg wet 5.00 80.1 40-140 9.73 25 Benzo(a)pyrene 3.93 0.10 mg/Kg wet 5.00 78.6 40-140 9.82 25 Benzo(b)fluoranthene 4.06 0.10 mg/Kg wet 5.00 81.1 40-140 9.77 25 Benzo(g,h,i)perylene 4.34 0.10 mg/Kg wet 5.00 86.8 40-140 10.5 25 Benzo(k)fluoranthene 4.01 0.10 mg/Kg wet 5.00 80.1 40-140 9.60 25 Chrysene 3.78 0.10 mg/Kg wet 5.00 75.7 40-140 9.45 25 Dibenz(a,h)anthracene 4.29 0.10 mg/Kg wet 5.00 85.8 40-140 9.53 25 Fluoranthene 3.90 0.10 mg/Kg wet 5.00 78.1 40-140 8.84 25 Fluorene 3.63 0.10 mg/Kg wet 5.00 72.7 40-140 5.28 25 Indeno(1,2,3-cd)pyrene 4.34 0.10 mg/Kg wet 5.00 86.7 40-140 9.79 25 2-Methylnaphthalene 3.22 0.10 mg/Kg wet 5.00 64.4 40-140 3.30 25 Naphthalene 2.93 0.10 mg/Kg wet 5.00 58.6 40-140 4.15 25 Phenanthrene 3.79 0.10 mg/Kg wet 5.00 75.7 40-140 7.12 25 Pyrene 3.82 0.10 mg/Kg wet 5.00 76.4 40-140 9.35 25 n-Decane 2.36 0.10 mg/Kg wet 5.00 47.2 40-140 7.82 25 n-Docosane 4.18 0.10 mg/Kg wet 5.00 83.7 40-140 0.379 25 n-Dodecane 3.04 0.10 mg/Kg wet 5.00 60.9 40-140 9.60 25 n-Eicosane 4.16 0.10 mg/Kg wet 5.00 83.1 40-140 1.77 25 n-Hexacosane 4.04 0.10 mg/Kg wet 5.00 80.7 40-140 0.0867 25 n-Hexadecane 4.03 0.10 mg/Kg wet 5.00 80.7 40-140 5.48 25 n-Hexatriacontane 4.33 0.10 mg/Kg wet 5.00 86.5 40-140 0.582 25 n-Nonadecane 4.16 0.10 mg/Kg wet 5.00 83.2 40-140 2.80 25 n-Nonane 1.61 0.10 mg/Kg wet 5.00 32.2 30-140 7.27 25 n-Octacosane 3.97 0.10 mg/Kg wet 5.00 79.5 40-140 0.406 25 n-Octadecane 4.10 0.10 mg/Kg wet 5.00 81.9 40-140 3.88 25 n-Tetracosane 4.09 0.10 mg/Kg wet 5.00 81.9 40-140 0.324 25 n-Tetradecane 3.36 0.10 mg/Kg wet 5.00 71.2 40-140 9.67 25 n-Triacontane 4.07 0.10 mg/Kg wet 5.00 81.3 40-140 0.0615 25 Naphthalene -aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 2-Methylnaphthalene-aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 Surrogate: Chlorooctadecane (COD) 4.07 mg/Kg wet 4.99 81.6 40-140 Surrogate: o-Terphenyl (OTP) 3.49 mg/Kg wet 5.00 69.9 40-140 Surrogate:2-Bromonaphthalene 4.04 mg/Kg wet 5.00 80.7 40-140 Surrogate:2-Fluorobiphenyl 4.39 mg/Kg wet 5.00 87.9 40-140 Page 28 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - VPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072883 - MA VPH Blank (B072883-BLK1) Prepared & Analyzed: 05/13/13 Unadjusted C5-C8 Aliphatics ND 10 mg/Kg wet C5-C8 Aliphatics ND 10 mg/Kg wet Unadjusted C9-C 12 Aliphatics ND 10 mg/Kg wet C9-C12 Aliphatics ND 10 mg/Kg wet C9-C10 Aromatics ND 10 mg/Kg wet Benzene ND 0.050 mg/Kg wet Ethylbenzene ND 0.050 mg/Kg wet Methyl tert-Butyl Ether (MTBE) ND 0.050 mg/Kg wet Naphthalene ND 0.25 mg/Kg wet Toluene ND 0.050 mg/Kg wet m+p Xylene ND 0.10 mg/Kg wet o-Xylene ND 0.050 mg/Kg wet Surrogate: 2,5-Dibromotoluene (FID) 0.0423 mg/Kg wet 0.0400 106 70-130 Surrogate: 2,5-Dibromotoluene (PID) 0.0372 mg/Kg wet 0.0400 93.1 70-130 LCS (B072883-BS1) Prepared & Analyzed: 05/13/13 Benzene 0.0973 0.0010 mg/Kg wet 0.100 97.3 70-130 Butylcyclohexane 0.0885 0.0010 mg/Kg wet 0.100 88.5 70-130 Decane 0.0958 0.0010 mg/Kg wet 0.100 95.8 70-130 Ethylbenzene 0.0993 0.0010 mg/Kg wet 0.100 99.3 70-130 Methyl tert-Butyl Ether (MTBE) 0.0987 0.0010 mg/Kg wet 0.100 98.7 70-130 2-Methylpentane 0.101 0.0010 mg/Kg wet 0.100 101 70-130 Naphthalene 0.101 0.0050 mg/Kg wet 0.100 101 70-130 Nonane 0.0897 0.0010 mg/Kg wet 0.100 89.7 30-130 Pentane 0.104 0.0010 mg/Kg wet 0.100 104 70-130 Toluene 0.0996 0.0010 mg/Kg wet 0.100 99.6 70-130 1,2,4-Trimethylbenzene 0.0995 0.0010 mg/Kg wet 0.100 99.5 70-130 2,2,4-Trimethylpentane 0.0936 0.0010 mg/Kgwet 0.100 93.6 70-130 m+p Xylene 0.202 0.0020 mg/Kg wet 0.200 101 70-130 o-Xylene 0.0993 0.0010 mg/Kg wet 0.100 99.3 70-130 Surrogate:2,5-Dibromotoluene (FID) 0.0318 mg/Kg wet 0.0400 79.4 70-130 Surrogate: 2,5-Dibromotoluene (PID) 0.0316 mg/Kg wet 0.0400 79.0 70-130 LCS Dup (B072883-BSD1) Prepared & Analyzed: 05/13/13 Benzene 0.103 0.0010 mg/Kg wet 0.100 103 70-130 5.82 25 Butylcyclohexane 0.0926 0.0010 mg/Kg wet 0.100 92.6 70-130 4.56 25 Decane 0.102 0.0010 mg/Kg wet 0.100 102 70-130 5.82 25 Ethylbenzene 0.105 0.0010 mg/Kg wet 0.100 105 70-130 5.70 25 Methyl tert-Butyl Ether (MTBE) 0.0991 0.0010 mg/Kg wet 0.100 99.1 70-130 0.379 25 2-Methylpentane 0.106 0.0010 mg/Kg wet 0.100 106 70-130 4.56 25 Naphthalene 0.101 0.0050 mg/Kg wet 0.100 101 70-130 0.250 25 Nonane 0.0928 0.0010 mg/Kg wet 0.100 92.8 30-130 3.45 25 Pentane 0.110 0.0010 mg/Kg wet 0.100 110 70-130 5.28 25 Toluene 0.105 0.0010 mg/Kg wet 0.100 105 70-130 5.68 25 1,2,4-Trimethylbenzene 0.106 0.0010 mg/Kg wet 0.100 106 70-130 5.88 25 2,2,4-Trimethylpentane 0.101 0.0010 mg/Kg wet 0.100 101 70-130 7.29 25 m+p Xylene 0.214 0.0020 mg/Kg wet 0.200 107 70-130 5.62 25 o-Xylene 0.105 0.0010 mg/Kg wet 0.100 105 70-130 5.55 25 Surrogate: 2,5-Dibromotoluene (FID) 0.0401 mg/Kg wet 0.0400 100 70-130 Surrogate: 2,5-Dibromotoluene (PID) 0.0400 mg/Kg wet 0.0400 99.9 70-130 Page 29 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). L-02 Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is on the high side. L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the low side. L-07A Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for this compound. 0-02 Soil/methanol ratio does not meet method specifications. Insufficient amount of soil. Data validation is not affected since a sufficient amount of preservative is present. Detection limits may be above useful levels. R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. S-03 Surrogate recovery outside of control limits due to suspected sample matrix interference. V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method specified criteria. V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound. Increased uncertainty is associated with the reported value which is likely to be biased on the low side. V-06 Continuing calibration did not meet method specifications and was biased on the high side for this compound. Increased uncertainty is associated with the reported value which is likely to be biased on the high side. V-16 Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported result. V-17 Internal standard area <50% of associated calibration standard internal standard area. V-19 Initial calibration did not meet method specifications. Compound was calibrated using linear regression with correlation coefficient <0.99. V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Page 30 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications MADEP-EPH-04-1.1 in Soil C9-C18 Aliphatics CT,NC,WA,ME,ME,NH-P C19-06 Aliphatics CT,NC,WA,ME,ME,NH-P Unadjusted Cl1-C22 Aromatics CT,NC,WA,ME,ME,NH-P C11-C22 Aromatics CT,NC,WA,ME,ME,NH-P Acenaphthene CT,NC,WA,ME,ME,NH-P Acenaphthylene CT,NC,WA,ME,ME,NH-P Anthracene CT,NC,WA,ME,ME,NH-P Benzo(a)anthracene CT,NC,WA,ME,ME,NH-P Benzo(a)pyrene CT,NC,WA,ME,ME,NH-P Benzo(b)fluoranthene CT,NC,WA,ME,ME,NH-P Benzo(g,h,i)perylene CT,NC,WA,ME,ME,NH-P Benzo(k)fluoranthene CT,NC,WA,ME,ME,NH-P Chrysene CT,NC,WA,ME,ME,NH-P Dibenz(a,h)anthracene CT,NC,WA,ME,ME,NH-P Fluoranthene CT,NC,WA,ME,ME,NH-P Fluorene CT,NC,WA,ME,ME Indeno(1,2,3-cd)pyrene CT,NC,WA,ME,ME,NH-P 2-Methylnaphthalene CT,NC,WA,ME,ME Naphthalene CT,NC,WA,ME,ME,NH-P Phenanthrene CT,NC,WA,ME,ME,NH-P Pyrene CT,NC,WA,ME,ME,NH-P MADEP-VPH-04-1.1 in Soil Unadjusted C5-C8 Aliphatics CT,NC,WA,ME,NH-P C5-C8 Aliphatics CT,NC,WA,ME,NH-P Unadjusted C9-C12 Aliphatics CT,NC,WA,ME,NH-P C9-C12 Aliphatics CT,NC,WA,ME,NH-P C9-C10 Aromatics CT,NC,WA,ME,NH-P Benzene CT,NC,WA,ME,NH-P Ethylbenzene CT,NC,WA,ME,NH-P Methyl tert-Butyl Ether (MTBE) CT,NC,WA,ME,NH-P Naphthalene CT,NC,WA,ME,NH-P Toluene CT,NC,WA,ME,NH-P m+p Xylene CT,NC,WA,ME,NH-P o-Xylene CT,NC,WA,ME,NH-P SW-846 8260B in Soil Acetone CT,NH,NY,NC,ME Acrylonitrile CT,NH,NY,NC,ME tert-Amyl Methyl Ether (TAME) NC Benzene CT,NH,NY,NC,ME Bromobenzene NH,NY,NC,ME Bromochloromethane NH,NY,NC,ME Bromodichloromethane CT,NH,NY,NC,ME Bromoform CT,NH,NY,NC,ME Bromomethane CT,NH,NY,NC,ME 2-Butanone (MEK) CT,NH,NY,NC,ME tert-Butyl Alcohol (TBA) NC Page 31 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8260B in Soil n-Butylbenzene CT,NH,NY,NC,ME sec-Butylbenzene CT,NH,NY,NC,ME tert-Butylbenzene CT,NH,NY,NC,ME tert-Butyl Ethyl Ether (TBEE) NC Carbon Disulfide CT,NH,NY,NC,ME Carbon Tetrachloride CT,NH,NY,NC,ME Chlorobenzene CT,NH,NY,NC,ME Chlorodibromomethane CT,NH,NY,NC,ME Chloroethane CT,NH,NY,NC,ME Chloroform CT,NH,NY,NC,ME Chloromethane CT,NH,NY,NC,ME 2-Chlorotoluene CT,NH,NY,NC,ME 4-Chlorotoluene CT,NH,NY,NC,ME 1,2-Dibromo-3-chloropropane (DBCP) NC 1,2-Dibromoethane (EDB) NC Dibromomethane NH,NY,NC,ME 1,2-Dichlorobenzene CT,NH,NY,NC,ME 1,3-Dichlorobenzene CT,NH,NY,NC,ME 1,4-Dichlorobenzene CT,NH,NY,NC,ME trans-1,4-Dichloro-2-butene NC Dichlorodifluoromethane (Freon 12) NY,NC,ME 1,1-Dichloroethane CT,NH,NY,NC,ME 1,2-Dichloroethane CT,NH,NY,NC,ME 1,1-Dichloroethylene CT,NH,NY,NC,ME cis-1,2-Dichloroethylene CT,NH,NY,NC,ME trans-1,2-Dichloroethylene CT,NH,NY,NC,ME 1,2-Dichloropropane CT,NH,NY,NC,ME 1,3-Dichloropropane NH,NY,NC,ME 2,2-Dichloropropane NH,NY,NC,ME 1,1-Dichloropropene NH,NY,NC,ME cis- 1,3 -Dichloropropene CT,NH,NY,NC,ME trans- l,3-Dichloropropene CT,NH,NY,NC,ME Diethyl Ether NC Diisopropyl Ether (DIPE) NC 1,4-Dioxane NC Ethylbenzene CT,NH,NY,NC,ME Hexachlorobutadiene NH,NY,NC,ME 2-Hexanone (MBK) CT,NH,NY,NC,ME Isopropylbenzene (Cumene) CT,NH,NY,NC,ME p-Isopropyltoluene (p-Cymene) NH,NY,NC Methyl tert-Butyl Ether (MTBE) NY,NC Methylene Chloride CT,NH,NY,NC,ME 4-Methyl-2-pentanone (MIBK) CT,NH,NY,NC Naphthalene NH,NY,NC,ME n-Propylbenzene NH,NY,NC Styrene CT,NH,NY,NC,ME 1, 1, 1,2-Tetrachloroethane CT,NH,NY,NC,ME Page 32 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte SW-846 8260B in Soil 1,1,2,2-Tetrachloroethane Tetrachloroethylene Tetrahydrofuran Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trichlorobenzene 1, 1, 1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethylene Trichlorofluoromethane (Freon 11) 1,2,3-Trichloropropane 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 113) 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Chloride m+p Xylene o-Xylene SW-846 8270D in Soil Acenaphthene Acenaphthylene Acetophenone Aniline Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyzene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Bis(2-chloroethoxy)methane Bis(2-chloroethyl)ether Bis(2-chloroisopropyl)ether Bis(2-Ethylhexyl)phthalate 4-Bromophenylphenylether Butylbenzylphthalate Carbazole 4-Chloroaniline 4-Chloro-3-methylphenol 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenylether Chrysene Dibenz(a,h)anthracene Dibenzofiiran Certifications CT,NH,NY,NC,ME CT,NH,NY,NC,ME NC CT,NH,NY,NC,ME NC,ME NH,NY,NC,ME NC,ME CT,NH,NY,NC,ME CT,NH,NY,NC,ME CT,NH,NY,NC,ME CT,NH,NY,NC,ME NH,NY,NC,ME NC CT,NH,NY,NC,ME CT,NH,NY,NC,ME CT,NH,NY,NC,ME CT,NH,NY,NC,ME CT,NH,NY,NC,ME CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA NY,NH,ME,NC,VA NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA NC CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA Page 33 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8270D in Soil Di-n-butylphthalate CT,NY,NH,ME,NC,VA 1,2-Dichlorobenzene NY,NH,ME,NC,VA 1,3-Dichlorobenzene NY,NH,ME,NC,VA 1,4-Dichlorobenzene NY,NH,ME,NC,VA 3,3-Dichlorobenzidine CT,NY,NH,ME,NC,VA 2,4-Dichlorophenol CT,NY,NH,ME,NC,VA Diethylphthalate CT,NY,NH,ME,NC,VA 2,4-Dimethylphenol CT,NY,NH,ME,NC,VA Dimethylphthalate CT,NY,NH,ME,NC,VA 4,6-Dinitro-2-methylphenol CT,NY,NH,ME,NC,VA 2,4-Dinitrophenol CT,NY,NH,ME,NC,VA 2,4-Dinitrotoluene CT,NY,NH,ME,NC,VA 2,6-Dinitrotoluene CT,NY,NH,ME,NC,VA Di-n-octylphthalate CT,NY,NH,ME,NC,VA 1,2-Diphenylhydrazine (as Azobenzene) NY,NH,ME,NC,VA Fluoranthene CT,NY,NH,ME,NC,VA Fluorene NY,NH,ME,NC,VA Hexachlorobenzene CT,NY,NH,ME,NC,VA Hexachlorobutadiene CT,NY,NH,ME,NC,VA Hexachlorocyclopentadiene CT,NY,NH,ME,NC,VA Hexachloroethane CT,NY,NH,ME,NC,VA Indeno(1,2,3-cd)pyrene CT,NY,NH,ME,NC,VA Isophorone CT,NY,NH,ME,NC,VA I -Methylnaphthalene NC 2-Methylnaphthalene CT,NY,NH,ME,NC,VA 2-Methylphenol CT,NY,NH,ME,NC,VA 3/4-Methylphenol CT,NY,NH,ME,NC,VA Naphthalene CT,NY,NH,ME,NC,VA 2-Nitroaniline CT,NY,NH,ME,NC,VA 3-Nitroaniline CT,NY,NH,ME,NC,VA 4-Nitroaniline CT,NY,NH,ME,NC,VA Nitrobenzene CT,NY,NH,ME,NC,VA 2-Nitrophenol CT,NY,NH,ME,NC,VA 4-Nitrophenol CT,NY,NH,ME,NC,VA N-Nitrosodimethylamine CT,NY,NH,ME,NC,VA N-Nitrosodiphenylamine CT,NY,NH,ME,NC,VA N-Nitrosodi-n-propylamine CT,NY,NH,ME,NC,VA Pentachloronitrobenzene NC Pentachlorophenol CT,NY,NH,ME,NC,VA Phenanthrene CT,NY,NH,ME,NC,VA Phenol CT,NY,NH,ME,NC,VA Pyrene CT,NY,NH,ME,NC,VA Pyridine CT,NY,NH,ME,NC,VA 1,2,4,5-Tetrachlorobenzene NC 1,2,4-Trichlorobenzene CT,NY,NH,ME,NC,VA 2,4,5-Trichlorophenol CT,NY,NH,ME,NC,VA 2,4,6-Trichlorophenol CT,NY,NH,ME,NC,VA Page 34 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8270D in Soil 2-Fluorophenol NC The CON -TEST Environmental Laboratory operates under the following certifications and accreditation: Code Description Number Expires AIHA AIHA-LAP, LLC 100033 02/1/2014 MA Massachusetts DEP M-MA100 06/30/2013 CT Connecticut Department of Publilc Health PH-0567 09/30/2013 NY New York State Department of Health 10899 NELAP 04/1/2014 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2014 RI Rhode Island Department of Health LA000112 12/30/2013 NC North Carolina Div. of Water Quality 652 12/31/2013 NJ New Jersey DEP MA007 NELAP 06/30/2013 FL Florida Department of Health E871027 NELAP 06/30/2013 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2013 WA State of Washington Department of Ecology C2065 02/23/2014 ME State of Maine 2011028 06/9/2015 VA Commonwealth of Virginia 460217 12/14/2013 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2012 Page 35 of 38 13EO396 1 Contest Final 05 20 13 1552 1 8i ra ro m � rD I � a rb 0 6 fU %�A Kz:jl w, 0000 0`s m Y' 9 N VI -0 D O aln a 2• � m � 73 `p (D c� 'a (p L Co Q 4 C @ V '" p� y q 0. :h lD a rt O 4YY � o O � n » r� r rL .� ® m o N C3 " CD n ' a a � TI izi "Pi gy � '1 rt C7 � ID y OOP n i 8 ro i� Om Q 0, G1 n V ! O a cm X � Q Q d n e6 n d _ik/ii—i m E.4 e ; m n li II II — FI 11 li II If E1 31 g, -� yr �+ 6y 11 II II mi fl « # 00 a w p o w II iE - O o c 2 v"n c �' p Q n A Iv w p- Cq +-r m °} G N� d CL 00 sw C 0 u A n m ea ^ 4. O QQ v G r�^o b N O o`{s rt ps v' a. vi G. n m ,y j�z m Page 36 of 38 13E0396 1 Contest Final 05 20 13 1552 4/30/13 TrackWur package or shipmentwith FedExTracWng Shop (NU) date: Aortal dr,-hX fir: Mon 412912013 6:33 prn Tues 413612o13 9m am RAL US Delivered MA us -j—y Ft r o,: C. rur.G+vs Travel History DateP9 me Activity - 4/30/2013 - Tuesday q:58 ant delivered 8:26 ant On FedExvehicle for de#ivary 7:32 am At Ineol FOdEx faoilily 6:32 tam Atdeslinathn sorzfacikiy 4:52 am Departed Fed Exloratlen 12:01 am Arrived at FedEx location - 4129/2013 - Monday 8.35 pm left Fwffx origin f (Jifly 6:33 pri ricked up Tn, rld v I'rA a r F't c Ei'-x Q f i Dn Shipment Facts Location M VVINDrOR tQCKS, 0 WINDSOR {OCKS_ CT EAST GRANUY, CT IWDIANAFCX-iS_ !N INDIAN,4P')�Mr IN RAL EW-N N(; NM DGi NC Local Scan Time Tracking number 802631BB9500 Service Fe.di=xPr6rilyOverniglit �F Dimensions 18x11x15in, WiveredTo Shipping/RecehAnt; Total Pieces 1 Packaging Your Packaging Spenlal handling Denver Wee Way section https:/AvA rv.tedexcomltede)dracWindexhtml?tracknumbers=802631889500&Cntry_code=us 1/1 Page 37 of 38 13EO396 1 Contest Final 05 20 13 1552 39 Spruce St, R East Lnragr¢aeadavr, FAA. 01028 — - P: 413-525-2332 A74ALYTICA L LABORATORvF; 413-525-6405 Ob con -test �. K uvww.contesifabs.corn SB Die Rem t Checklist <,a-_...:,.e. ;w :.3 .:.+5•::.m...,zF.. .,�-��: as ::"., a�,�.,. .' _:_--:-: - -.-°�',.,. ..>,.'.YF_ ....'.� ., ., ...--:: CLIENT NAME: m (, RECEIVE Y: D E. by 1) Was the chain(s) of custody relinquished and signed? e No No CoC Included 2) Does the chain agree with the samples? Ye No If not, explain: 3) Are all the samples in good condition? No If not, explain: ) How w e the samples received, On Ice Direct from Sampling ❑ Ambient ❑ In Cooler(s) Were the samples received in Temperature Compliance of (2-60C)? e No N/A 1 Temperature °C by Temp blank Temperature °C by Temp gun { 5) Are there Dissolved samples for the lab to filter? Yes Who was notified Date _ Time 6) Are there any RUSH or SHORT HOLDING TIME samples? Yes Who was notified Date Time Permission to subcontract samples? Yes No 7) Location where samples are stored- (Walk-in clients only) if not already approved Client Signature: # of containers 1 Liter Amber 500 mL Amber 250 mL Amber f 8oz amber 1 Liter Plastic 500 mL Plastic 250 mL plastic 40 mL Vial - type listed below Colisure / bacteria bottle Dissolved Oxygen bottle Encore Flashpoint bottle Perchlorate Kit Other Laboratory Comments: 40 mL vials: # HCl # Methanol rso 27 # Bisulfate # DI Water F6ev s Ni y 2C1T # Thiosulfate Unpreserved 8 o4ambej�clear jar 4 oz amber/clear jar 2 oz amber/clear jar Air Cassette Hg/Hopcallte Tube Plastic Bag / Zi loo PM2.5/PM10 PUF Cartridge SOC Kit TO- 17 Tubes Non-ConTest Container Other glass iar Other # of containers Time and Bate Frozen. - Page 38 of 38 13EO396 1 Contest Final 05 20 13 1552 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 May 14, 2013 Josh Dunbar Falcon Engineering 1210 Trinity Road, Suite 110 Raleigh, NC 27607 Project Location: 828 MLK-Ch.Hill Client Job Number: Project Number: [none] Laboratory Work Order Number: 13EO159 Enclosed are results of analyses for samples received by the laboratory on May 3, 2013. If you have any questions concerning this report, please feel free to contact me. Sincerely, �� �'V;��� Lisa A. Worthington Project Manager Page 1 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Falcon Engineering REPORT DATE: 5/14/2013 1210 Trinity Road, Suite 110 Raleigh, NC 27607 PURCHASE ORDER NUMBER: ATTN: Josh Dunbar PROJECT NUMBER: [none] ANALYTICAL SUMMARY WORK ORDER NUMBER: 13EO 159 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: 828 MLK-Ch.Hill FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB MW-1 13EO159-01 Water SW-846 6010C SW-846 6020A SW-846 7470A SW-846 8260B SW-846 8270D Page 2 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. Page 3 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028' FAX 413/525-6405 ` TEL. 413/525-2332 SW-846 6010C Qualifications: Sample to spike ratio is greater than or equal to 4:1. Spiked amount is not representative of the native amount in the sample. Appropriate or meaningful recoveries cannot be calculated. Analyte & Samples(s) Qualified: Sodium 13EO159-01[MW-1], B072721-MS1 SW-846 8260B Qualifications: Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. Analyte & Samples(s) Qualified: Dichloroditluoromethane (Freon 12) B072403-BSDI Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. Analyte & Samples(s) Qualified: Bromomethane 13EO159-OI[MW-1], B072403-BLKI, B072403-BSI, B072403-BSDI Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported result. Analyte & Samples(s) Qualified: 1,4-Dioxane, tert-Butyl Alcohol (TBA) 13EO159-OI[MW-1], B072403-BLKI, B072403-BSI, B072403-BSDI Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: Bromomethane B072403-BS1, B072403-BSD1 SW-846 8270D Qualifications: Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. Analyte & Samples(s) Qualified: Benzo(g,h,i)perylene B072641-BSDI Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. Analyte & Samples(s) Qualified: 2-Chloronaphthalene, Benzidine 13EO159-01[MW-1], B072641-BLKI, B072641-BSI, B072641-BSDI Page 4 of 33 13E0159 1 Contest Final 05 14 13 1358 icon-testo ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Continuing calibration did not meet method specifications and was biased on the low side for this compound. Increased uncertainty is associated with the reported value which is likely to be biased on the low side. Analyte & Samples(s) Qualified: Anthracene, Di-n-butylphthalate 13E0159-01[MW-1], B072641-BLKI, B072641-BSI, B072641-BSDI Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported result. Analyte & Samples(s) Qualified: Pentachloronitrobenzene 13E0159-01[MW-1], B072641-BLKI, B072641-BSI, B072641-BSDI The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Daren J. Damboragian Laboratory Manager Page 5 of 33 13EO159 1 Contest Final 05 14 13 1358 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 828 MLK-Ch.Hill Sample Description: Work Order: 13EO159 Date Received: 5/3/2013 Field Sample #: MW-1 Sampled: 5/3/2013 12:00 Sample ID: 13EO159-01 Samnle Matrix: Water Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 4.7 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Acrylonitrile ND 5.0 0.58 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD tert-Amyl Methyl Ether (TAME) ND 0.50 0.091 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Benzene ND 1.0 0.079 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Bromobenzene ND 1.0 0.044 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Bromochloromethane ND 1.0 0.22 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Bromodichloromethane ND 1.0 0.088 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Bromoform ND 1.0 0.21 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Bromomethane ND 2.0 0.94 µg/L 1 R-05 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 2-Butanone (MEK) ND 20 2.4 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD tert-Butyl Alcohol (TBA) ND 20 2.2 µg/L 1 V-16 SW-846 8260B 5/6/13 5/6/13 13:24 LBD n-Butylbenzene ND 1.0 0.054 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD sec-Butylbenzene ND 1.0 0.084 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD tert-Butylbenzene ND 1.0 0.096 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD tert-Butyl Ethyl Ether (TBEE) ND 0.50 0.075 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Carbon Disulfide ND 10 1.0 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Carbon Tetrachloride ND 5.0 0.10 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Chlorobenzene ND 1.0 0.12 µg/L I SW-846 8260B 5/6/13 5/6/13 13:24 LBD Chlorodibromomethane ND 0.50 0.054 µg/L I SW-846 8260B 5/6/13 5/6/13 13:24 LBD Chloroethane ND 2.0 0.16 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Chloroform ND 2.0 0.14 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Chloromethane ND 2.0 0.32 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 2-Chlorotoluene ND 1.0 0.070 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 4-Chlorotoluene ND 1.0 0.074 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 0.34 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,2-Dibromoethane (EDB) ND 0.50 0.089 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Dibromomethane ND 1.0 0.070 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,2-Dichlorobenzene ND 1.0 0.076 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,3-Dichlorobenzene ND 1.0 0.079 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,4-Dichlorobenzene ND 1.0 0.046 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD trans-1,4-Dichloro-2-butene ND 2.0 0.12 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Dichlorodifluoromethane (Freon 12) ND 2.0 0.12 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,1-Dichloroethane ND 1.0 0.16 µg/L 1 SW-8468260B 5/6/13 5/6/13 13:24 LBD 1,2-Dichloroethane ND 1.0 0.19 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1, 1 -Dichloroethylene ND 1.0 0.21 µg/L 1 SW-8468260B 5/6/13 5/6/13 13:24 LBD cis-1,2-Dichloroethylene ND 1.0 0.15 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD trans-1,2-Dichloroethylene ND 1.0 0.15 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,2-Dichloropropane ND 1.0 0.11 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,3-Dichloropropane ND 0.50 0.099 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 2,2-Dichloropropane ND 1.0 0.072 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1, 1 -Dichloropropene ND 2.0 0.13 µg/L 1 SW-8468260B 5/6/13 5/6/13 13:24 LBD cis-1,3-Dichloropropene ND 2.0 0.062 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD trans-1,3-Dichloropropene ND 0.50 0.056 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Diethyl Ether ND 2.0 0.22 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Page 6 of 33 13EO159 1 Contest Final 05 14 13 1358 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 828 MLK-Ch.Hill Sample Description: Work Order: 13EO159 Date Received: 5/3/2013 Field Sample #: MW-1 Sampled: 5/3/2013 12:00 Samnle ID: 13EO159-01 Samnle Matrix: Water Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.50 0.18 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,4-Dioxane ND 50 26 µg/L 1 V-16 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Ethylbenzene ND 1.0 0.092 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Hexachlorobutadiene ND 1.0 0.17 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 2-Hexanone (MBK) ND 10 1.5 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Isopropylbenzene (Cumene) ND 1.0 0.11 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD p-Isopropyltoluene (p-Cymene) ND 1.0 0.12 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Methyl tert-Butyl Ether (MTBE) ND 1.0 0.090 µg/L I SW-846 8260B 5/6/13 5/6/13 13:24 LBD Methylene Chloride ND 5.0 3.2 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 4-Methyl-2-pentanone (MIBK) ND 10 1.5 µg/L I SW-846 8260B 5/6/13 5/6/13 13:24 LBD Naphthalene ND 2.0 0.12 µg/L I SW-846 8260B 5/6/13 5/6/13 13:24 LBD n-Propylbenzene ND 1.0 0.094 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Styrene ND 1.0 0.12 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1, 1, 1,2-Tetrachloroethane ND 1.0 0.12 µg/L 1 SW-8468260B 5/6/13 5/6/13 13:24 LBD 1,1,2,2-Tetrachloroethane ND 0.50 0.12 µg/L 1 SW-8468260B 5/6/13 5/6/13 13:24 LBD Tetrachloroethylene ND 1.0 0.080 µg/L I SW-846 8260B 5/6/13 5/6/13 13:24 LBD Tetrahydrofman ND 10 1.1 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Toluene ND 1.0 0.090 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,2,3-Trichlorobenzene ND 5.0 0.14 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,2,4-Trichlorobenzene ND 1.0 0.12 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,3,5-Trichlorobenzene ND 2.0 0.14 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1, 1, 1 -Trichloroethane ND 1.0 0.094 µg/L 1 SW-8468260B 5/6/13 5/6/13 13:24 LBD 1,1,2-Trichloroethane ND 1.0 0.12 µg/L 1 SW-8468260B 5/6/13 5/6/13 13:24 LBD Trichloroethylene ND 1.0 0.077 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Trichlorofluoromethane (Freon 11) ND 2.0 0.15 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,2,3-Trichloropropane ND 2.0 0.12 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1, 1,2-Trichloro- 1,2,2-trifluoroethane ND 1.0 0.092 µg/L 1 SW-8468260B 5/6/13 5/6/13 13:24 LBD (Freon 113) 1,2,4-Trimethylbenzene ND 1.0 0.18 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD 1,3,5-Trimethylbenzene ND 1.0 0.10 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Vinyl Chloride ND 2.0 0.13 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD m+p Xylene ND 2.0 0.18 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD o-Xylene ND 1.0 0.11 µg/L 1 SW-846 8260B 5/6/13 5/6/13 13:24 LBD Surrogates % Recovery Recovery Limits Flag 1,2-Dichloroethane-d4 96.0 70-130 5/6/13 13:24 Toluene-d8 93.6 70-130 5/6/13 13:24 4-Bromofluorobenzene 93.3 70-130 5/6/13 13:24 Page 7 of 33 13EO159 1 Contest Final 05 14 13 1358 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 828 MLK-Ch.Hill Sample Description: Work Order: 13EO159 Date Received: 5/3/2013 Field Sample #: MW-1 Sampled: 5/3/2013 12:00 Samnle ID: 13EO159-01 Samnle Matrix: Water Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag Method Prepared Analyzed Analyst Acenaphthene ND 5.0 2.7 µg/L Acenaphthylene ND 5.0 2.7 µg/L Acetophenone ND 10 3.4 µg/L Aniline ND 5.0 2.3 µg/L Anthracene ND 5.0 2.4 µg/L Benzidine ND 10 6.3 µg/L Benzo(a)anthracene ND 5.0 2.3 µg/L Benzo(a)pyrene ND 5.0 2.9 µg/L Benzo(b)fluoranthene ND 5.0 2.1 µg/L Benzo(g,h,i)perylene ND 5.0 5.0 µg/L Benzo(k)fluoranthene ND 5.0 3.1 µg/L Benzoic Acid ND 10 2.8 µg/L Bis(2-chloroethoxy)methane ND 10 3.1 µg/L Bis(2-chloroethyl)ether ND 10 4.5 µg/L Bis(2-chloroisopropyl)ether ND 10 4.1 µg/L Bis(2-Ethylhexyl)phthalate ND 10 7.1 µg/L 4-Bromophenylphenylether ND 10 3.8 µg/L Butylbenzylphthalate ND 10 2.6 µg/L Carbazole ND 10 1.7 µg/L 4-Chloroaniline ND 10 2.9 µg/L 4-Chloro-3-methylphenol ND 10 2.9 µg/L 2-Chloronaphthalene ND 10 4.0 µg/L 2-Chlorophenol ND 10 3.6 µg/L 4-Chlorophenylphenylether ND 10 2.9 µg/L Chrysene ND 5.0 2.7 µg/L Dibenz(a,h)anthracene ND 5.0 5.0 µg/L Dibenzofman ND 5.0 2.8 µg/L Di-n-butylphthalate ND 10 2.2 µg/L 1,2-Dichlorobenzene ND 5.0 3.5 µg/L 1,3-Dichlorobenzene ND 5.0 3.9 µg/L 1,4-Dichlorobenzene ND 5.0 3.7 µg/L 3,3-Dichlorobenzidine ND 10 5.5 µg/L 2,4-Dichlorophenol ND 10 3.4 µg/L Diethylphthalate ND 10 2.8 µg/L 2,4-Dimethylphenol ND 10 7.2 µg/L Dimethylphthalate ND 10 2.6 µg/L 4,6-Dinitro-2-methylphenol ND 10 4.7 µg/L 2,4-Dinitrophenol ND 10 3.2 µg/L 2,4-Dinitrotoluene ND 10 3.0 µg/L 2,6-Dinitrotoluene ND 10 2.7 µg/L Di-n-octylphthalate ND 10 6.8 µg/L 1,2-Diphenylhydrazine (as Azobenzene) ND 10 4.8 µg/L Fluoranthene ND 5.0 2.0 µg/L Flumene ND 5.0 2.4 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 V-05 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 R-05 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5111113 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR I SW-846 8270D 5/9/13 5/11/13 18:36 CMR I SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 R-05 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5111113 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 V-05 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5111113 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Page 8 of 33 13EO159 1 Contest Final 05 14 13 1358 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 828 MLK-Ch.Hill Sample Description: Work Order: 13EO159 Date Received: 5/3/2013 Field Sample #: MW-1 Sampled: 5/3/2013 12:00 Samnle ID: 13EO159-01 Samnle Matrix: Water Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag Method Prepared Analyzed Analyst Hexachlorobenzene ND 10 3.5 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Hexachlorobutadiene ND 10 5.6 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Hexachlorocyclopentadiene ND 10 7.9 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Hexachloroethane ND 10 4.5 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Indeno(1,2,3-cd)pyrene ND 5.0 4.6 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Isophorone ND 10 3.2 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1-Methylnaphthalene ND 5.0 3.1 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 2-Methylnaphthalene ND 5.0 3.5 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 2-Methylphenol ND 10 3.1 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 3/4-Methylphenol ND 10 3.2 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Naphthalene ND 5.0 3.0 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 2-Nitroaniline ND 10 2.9 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 3-Nitroaniline ND 10 3.5 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 4-Nitroaniline ND 10 3.9 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Nitrobenzene ND 10 3.5 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 2-Nitrophenol ND 10 3.3 µg/L I SW-846 8270D 5/9/13 5/11/13 18:36 CMR 4-Nitrophenol ND 10 3.8 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR N-Nitrosodimethylamine ND 5.0 3.2 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR N-Nitrosodiphenylamine ND 10 3.9 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR N-Nitrosodi-n-propylamine ND 10 5.5 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Pentachloronitrobenzene ND 10 2.3 µg/L 1 V-16 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Pentachlorophenol ND 10 3.7 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Phenanthrene ND 5.0 2.6 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Phenol ND 10 1.5 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Pyrene ND 5.0 2.6 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Pyridine ND 5.0 3.0 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1,2,4,5-Tetrachlorobenzene ND 10 5.4 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 1,2,4-Trichlorobenzene ND 5.0 4.8 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 2,4,5-Trichlorophenol ND 10 2.7 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR 2,4,6-Trichlorophenol ND 10 3.6 µg/L 1 SW-846 8270D 5/9/13 5/11/13 18:36 CMR Surrogates % Recovery Recovery Limits Flag 2-Fluorophenol 52.1 15-110 5/11/13 18:36 Phenol-d6 36.3 15-110 5/11/13 18:36 Nitrobenzene-d5 68.3 30-130 5/11/13 18:36 2-Fluorobiphenyl 61.7 30-130 5/11/13 18:36 2,4,6-Tribromophenol 73.1 15-110 5/11/13 18:36 p-Terphenyl-dl4 64.9 30-130 5/11/13 18:36 Page 9 of 33 13EO159 1 Contest Final 05 14 13 1358 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 828 MLK-Ch.Hill Sample Description: Work Order: 13EO159 Date Received: 5/3/2013 Field Sample #: MW-1 Sampled: 5/3/2013 12:00 Samnle ID: 13EO159-01 Samnle Matrix: Water Analyte Results RL DL Metals Analyses (Total) Units Dilution Flag Method Date Prepared Date/Time Analyzed Analyst Aluminum 5.6 0.050 0.026 mg/L 1 SW-846 6010C 5/9/13 5/10/13 19:00 OP Antimony 5.4 2.0 0.30 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Arsenic 85 0.80 0.70 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Barium 1100 20 2.4 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Beryllium 1.6 2.0 0.36 µg/L 5 J SW-846 6020A 5/9/13 5/10/13 15:58 KSH Cadmium 0.17 1.0 0.059 µg/L 2 J SW-846 6020A 5/9/13 5/10/13 16:22 KSH Calcium 110 0.15 mg/L 1 SW-846 6010C 5/9/13 5/10/13 19:00 OP Chromium 15 2.0 1.3 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Cobalt 15 2.0 0.067 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Copper 25 10 0.16 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Iron 6.5 0.050 mg/L 1 SW-846 6010C 5/9/13 5/10/13 19:00 OP Lead 5.8 2.0 0.12 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Magnesium 25 0.15 0.037 mg/L 1 SW-846 6010C 5/9/13 5/10/13 19:00 OP Manganese 7600 100 9.9 µg/L 100 SW-846 6020A 5/9/13 5/10/13 16:51 KSH Mercury ND 0.00010 0.000047 mg/L 1 SW-846 7470A 5/8/13 5/8/13 15:19 SAJ Nickel 12 10 0.13 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Potassium 7.6 2.0 0.46 mg/L 1 SW-846 6010C 5/9/13 5/10/13 19:00 OP Selenium 2.5 10 1.5 µg/L 2 J SW-846 6020A 5/9/13 5/10/13 16:22 KSH Silver ND LO 0.13 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Sodium 34 2.0 1.9 mg/L 1 MS-19 SW-846 6010C 5/9/13 5/13/13 16:57 OP Thallium 1.0 0.40 0.073 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Vanadium 38 10 1.1 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Zinc 52 20 3.9 µg/L 2 SW-846 6020A 5/9/13 5/10/13 16:22 KSH Page 10 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: SM 303OC-SW-846 6010C Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 13EO159-01 [MW-1] B072721 50.0 50.0 05/09/13 Prep Method: SM 303OC-SW-846 6020A Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 13EO159-01 [MW-1] B072722 50.0 50.0 05/09/13 Prep Method: SW-846 7470A Prep-SW-846 7470A Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 13EO159-01 [MW-1] B072571 6.00 6.00 05/08/13 Prep Method: SW-846 5035-SW-846 8260B Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 13EO159-01 [MW-1] B072403 5 5.00 05/06/13 Prep Method: SW-846 351OC-SW-846 8270D Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 13EO159-01 [MW-1] B072641 1000 1.00 05/09/13 Page 11 of 33 13E0159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072403 - SW-846 5035 Blank (B072403-BLK1) Prepared & Analyzed: 05/06/13 Acetone ND 50 µg/L Acrylonitrile ND 5.0 µg/L tert-Amyl Methyl Ether (TAME) ND 0.50 µg/L Benzene ND 1.0 µg/L Bromobenzene ND 1.0 µg/L Bromochloromethane ND 1.0 µg/L Bromodichloromethane ND 0.50 µg/L Bromoform ND 1.0 µg/L Bromomethane ND 2.0 µg/L 2-Butanone (MEK) ND 20 µg/L tert-Butyl Alcohol (TBA) ND 20 µg/L n-Butylbenzene ND 1.0 µg/L sec-Butylbenzene ND 1.0 µg/L tert-Butylbenzene ND 1.0 µg/L tert-Butyl Ethyl Ether (TBEE) ND 0.50 µg/L Carbon Disulfide ND 2.0 µg/L Carbon Tetrachloride ND 5.0 µg/L Chlorobenzene ND 1.0 µg/L Chlorodibromomethane ND 0.50 µg/L Chloroethane ND 2.0 µg/L Chloroform ND 2.0 µg/L Chloromethane ND 2.0 µg/L 2-Chlorotoluene ND 1.0 µg/L 4-Chlorotoluene ND 1.0 µg/L 1,2-Dibromo-3-chloropropane (DBCP) ND 5.0 µg/L 1,2-Dibromoethane (EDB) ND 0.50 µg/L Dibromomethane ND 1.0 µg/L 1,2-Dichlorobenzene ND 1.0 µg/L 1,3-Dichlorobenzene ND 1.0 µg/L 1,4-Dichlorobenzene ND 1.0 µg/L trans-1,4-Dichloro-2-butene ND 2.0 µg/L Dichlorodifluoromethane (Freon 12) ND 2.0 µg/L 1,1-Dichloroethane ND 1.0 µg/L 1,2-Dichloroethane ND 1.0 µg/L 1,1-Dichloroethylene ND 1.0 µg/L cis-1,2-Dichloroethylene ND 1.0 µg/L trans-1,2-Dichloroethylene ND 1.0 µg/L 1,2-Dichloropropane ND 1.0 µg/L 1,3-Dichloropropane ND 0.50 µg/L 2,2-Dichloropropane ND 1.0 µg/L 1,1-Dichloropropene ND 2.0 µg/L cis-1,3-Dichloropropene ND 0.50 µg/L trans- 1, 3 -Dichloropropene ND 0.50 µg/L Diethyl Ether ND 2.0 µg/L Diisopropyl Ether (RIPE) ND 0.50 µg/L 1,4-Dioxane ND 50 µg/L Ethylbenzene ND 1.0 µg/L Hexachlorobutadiene ND 0.50 µg/L 2-Hexanone (MBK) ND 10 µg/L Isopropylbenzene (Cumene) ND 1.0 µg/L p-Isopropyltoluene (p-Cymene) ND 1.0 µg/L Methyl tert-Butyl Ether (MTBE) ND 1.0 µg/L R-05 V-16 V-16 Page 12 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072403 - SW-846 5035 Blank (B072403-BLK1) Prepared & Analyzed: 05/06/13 Methylene Chloride ND 5.0 µg/L 4-Methyl-2-pentanone (MIBK) ND 10 µg/L Naphthalene ND 2.0 µg/L n-Propylbenzene ND 1.0 µg/L Styrene ND 1.0 µg/L 1, 1, 1,2-Tetrachloroethane ND 1.0 µg/L 1,1,2,2-Tetrachloroethane ND 0.50 µg/L Tetrachloroethylene ND 1.0 µg/L Tetrahydrofuran ND 10 µg/L Toluene ND 1.0 µg/L 1,2,3-Trichlorobenzene ND 5.0 µg/L 1,2,4-Trichlorobenzene ND 1.0 µg/L 1,3,5-Trichlorobenzene ND 1.0 µg/L 1, 1, 1 -Trichloroethane ND 1.0 µg/L 1,1,2-Trichloroethane ND 1.0 µg/L Trichloroethylene ND 1.0 µg/L Trichlorofluoromethane (Freon 11) ND 2.0 µg/L 1,2,3-Trichloropropane ND 2.0 µg/L 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 1.0 µg/L 113) 1,2,4-Trimethylbenzene ND 1.0 µg/L 1,3,5-Trimethylbenzene ND 1.0 µg/L Vinyl Chloride ND 2.0 µg/L m+p Xylene ND 2.0 µg/L o-Xylene ND 1.0 µg/L Surrogate:l,2-Dichloroethane-d4 22.8 µg/L 25.0 91.2 70-130 Surrogate: Toluene-d8 23.6 µg/L 25.0 94.5 70-130 Surrogate:4-Bromofluorobenzene 23.8 µg/L 25.0 95.1 70-130 LCS (B072403-BSI) Prepared & Analyzed: 05/06/13 Acetone 126 50 Acrylonitrile 10.9 5.0 tert-Amyl Methyl Ether (TAME) 10.6 0.50 Benzene 10.1 1.0 Bromobenzene 10.6 1.0 Bromochloromethane 11.5 1.0 Bromodichloromethane 10.1 0.50 Bromoform 10.4 1.0 Bromomethane 4.31 2.0 2-Butanone (MEK) 102 20 tert-Butyl Alcohol (TBA) 104 20 n-Butylbenzene 8.70 1.0 sec-Butylbenzene 9.64 1.0 tert-Butylbenzene 9.90 1.0 tert-Butyl Ethyl Ether (TBEE) 10.4 0.50 Carbon Disulfide 9.30 2.0 Carbon Tetrachloride 9.60 5.0 Chlorobenzene 12.1 1.0 Chlorodibromomethane 9.31 0.50 Chloroethane 10.1 2.0 Chloroform 10.4 2.0 Chloromethane 6.35 2.0 2-Chlorotoluene 11.5 1.0 µg/L 100 126 70-160 t µg/L 10.0 105 70-130 µg/L 10.0 106 70-130 µg/L 10.0 101 70-130 µg/L 10.0 106 70-130 µg/L 10.0 115 70-130 µg/L 10.0 101 70-130 µg/L 10.0 104 70-130 µg/L 10.0 43.1 40-160 R-05, V-20 t µg/L 100 102 40-160 t µg/L 100 104 40-160 V-16 t µg/L 10.0 87.0 70-130 µg/L 10.0 96.4 70-130 µg/L 10.0 99.0 70-130 µg/L 10.0 103 70-130 µg/L 10.0 93.0 70-130 µg/L 10.0 96.0 70-130 µg/L 10.0 121 70-130 µg/L 10.0 93.1 70-130 µg/L 10.0 101 70-130 µg/L 10.0 104 70-130 µg/L 10.0 63.5 40-160 t µg/L 10.0 115 70-130 Page 13 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD .nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072403 - SW-846 5035 LCS (B072403-BSI) Prepared & Analyzed: 05/06/13 4-Chlorotoluene 11.9 1.0 µg/L 1,2-Dibromo-3-chloropropane (DBCP) 8.76 5.0 µg/L 1,2-Dibromoethane (EDB) 10.9 0.50 µg/L Dibromomethane 10.8 1.0 µg/L 1,2-Dichlorobenzene 112 1.0 µg/L 1,3-Dichlorobenzene 11.2 1.0 µg/L 1,4-Dichlorobenzene 10.3 1.0 µg/L trans-1,4-Dichloro-2-butene 9.95 2.0 µg/L Dichlorodifluoromethane (Freon 12) 4.19 2.0 µg/L 1,1-Dichloroethane 9.84 1.0 µg/L 1,2-Dichloroethane 10.1 1.0 µg/L 1,1-Dichloroethylene 10.2 1.0 µg/L cis-1,2-Dichloroethylene 9.56 1.0 µg/L trans-1,2-Dichloroethylene 10.1 1.0 µg/L 1,2-Dichloropropane 10.2 1.0 µg/L 1,3-Dichloropropane 9.94 0.50 µg/L 2,2-Dichloropropane 10.8 1.0 µg/L 1,1-Dichloropropene 9.90 2.0 µg/L cis- 1,3 -Dichloropropene 9.10 0.50 µg/L trans- 1, 3 -Dichloropropene 9.47 0.50 µg/L Diethyl Ether 11.3 2.0 µg/L Diisopropyl Ether(DIPE) 11.1 0.50 µg/L 1,4-Dioxane 123 50 µg/L Ethylbenzene 11.1 1.0 µg/L Hexachlorobutadiene 9.37 0.50 µg/L 2-Hexanone (MBK) 111 10 µg/L Isopropylbenzene (Cumene) 11.5 1.0 µg/L p-Isopropyltoluene (p-Cymene) 9.85 1.0 µg/L Methyl tert-Butyl Ether (MTBE) 10.4 1.0 µg/L Methylene Chloride 8.78 5.0 µg/L 4-Methyl-2-pentanone (MIBK) 108 10 µg/L Naphthalene 8.25 2.0 µg/L n-Propylbenzene 11.4 1.0 µg/L Styrene 12.0 1.0 µg/L 1, 1, 1,2-Tetrachloroethane 11.4 1.0 µg/L 1,1,2,2-Tetrachloroethane 10.8 0.50 µg/L Tetrachloroethylene 11.0 1.0 µg/L Tetrahydrofuran 11.5 10 µg/L Toluene 10.4 1.0 µg/L 1,2,3-Trichlorobenzene 8.49 5.0 µg/L 1,2,4-Trichlorobenzene 9.37 1.0 µg/L 1,3,5-Trichlorobenzene 9.41 1.0 µg/L 1, 1, 1 -Trichloroethane 10.3 1.0 µg/L 1,1,2-Trichloroethane 10.3 1.0 µg/L Trichloroethylene 10.2 1.0 µg/L Trichlorofluoromethane (Freon 11) 9.84 2.0 µg/L 1,2,3-Trichloropropane 11.3 2.0 µg/L 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 11.5 1.0 µg/L 113) 1,2,4-Trimethylbenzene 9.84 1.0 µg/L 1,3,5-Trimethylbenzene 10.8 1.0 µg/L Vinyl Chloride 7.18 2.0 µg/L 10.0 119 70-130 10.0 87.6 70-130 10.0 109 70-130 10.0 108 70-130 10.0 112 70-130 10.0 112 70-130 10.0 103 70-130 10.0 99.5 70-130 10.0 41.9 40-160 f 10.0 98.4 70-130 10.0 101 70-130 10.0 102 70-130 10.0 95.6 70-130 10.0 101 70-130 10.0 102 70-130 10.0 99.4 70-130 10.0 108 40-130 t 10.0 99.0 70-130 10.0 91.0 70-130 10.0 94.7 70-130 10.0 113 70-130 10.0 111 70-130 100 123 40-130 V-16 t 10.0 ill 70-130 10.0 93.7 70-130 100 ill 70-160 t 10.0 115 70-130 10.0 98.5 70-130 10.0 104 70-130 10.0 87.8 70-130 100 108 70-160 f 10.0 82.5 40-130 t 10.0 114 70-130 10.0 120 70-130 10.0 114 70-130 10.0 108 70-130 10.0 110 70-130 10.0 115 70-130 10.0 104 70-130 10.0 85.9 70-130 10.0 93.7 70-130 10.0 94.1 70-130 10.0 103 70-130 10.0 103 70-130 10.0 102 70-130 10.0 98.4 70-130 10.0 113 70-130 10.0 115 70-130 10.0 98.4 70-130 10.0 108 70-130 10.0 71.8 40-160 Page 14 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072403 - SW-846 5035 LCS (B072403-BSI) Prepared & Analyzed: 05/06/13 m+p Xylene 23.6 2.0 µg/L 20.0 118 70-130 o-Xylene 11.9 1.0 µg/L 10.0 119 70-130 Surrogate:l,2-Dichloroethane-d4 22.1 µg/L 25.0 88.6 70-130 Surrogate: Toluene-d8 24.0 µg/L 25.0 96.2 70-130 Surrogate:4-Bromofluorobenzene 25.2 µg/L 25.0 101 70-130 LCS Dup (B072403-BSDI) Prepared & Analyzed: 05/06/13 Acetone 110 50 µg/L 100 110 70-160 13.9 25 t Acrylonitrile 9.71 5.0 µg/L 10.0 97.1 70-130 7.53 25 tert-Amyl Methyl Ether (TAME) 10.4 0.50 µg/L 10.0 104 70-130 1.82 25 Benzene 9.77 1.0 µg/L 10.0 97.7 70-130 3.12 25 Bromobenzene 10.4 1.0 µg/L 10.0 104 70-130 2.09 25 Bromochloromethane 11.5 1.0 µg/L 10.0 115 70-130 0.261 25 Bromodichloromethane 10.1 0.50 µg/L 10.0 101 70-130 0.0988 25 Bromoform 9.89 1.0 µg/L 10.0 98.9 70-130 4.55 25 Bromomethane 6.89 2.0 µg/L 10.0 68.9 40-160 46.1 * 25 R-05, V-20 f 2-Butanone (MEK) 90.4 20 µg/L 100 90.4 40-160 12.3 25 t tert-Butyl Alcohol(TBA) 85.5 20 µg/L 100 85.5 40-160 19.4 25 V-16 t n-Butylbenzene 8.58 1.0 µg/L 10.0 85.8 70-130 1.39 25 sec-Butylbenzene 9.47 1.0 µg/L 10.0 94.7 70-130 1.78 25 tert-Butylbenzene 9.58 1.0 µg/L 10.0 95.8 70-130 3.29 25 tert-Butyl Ethyl Ether (TBEE) 9.97 0.50 µg/L 10.0 99.7 70-130 2.96 25 Carbon Disulfide 8.35 2.0 µg/L 10.0 83.5 70-130 10.8 25 Carbon Tetrachloride 9.14 5.0 µg/L 10.0 91.4 70-130 4.91 25 Chlorobenzene 11.8 1.0 µg/L 10.0 118 70-130 2.84 25 Chlorodibromomethane 9.20 0.50 µg/L 10.0 92.0 70-130 1.19 25 Chloroethane 9.52 2.0 µg/L 10.0 95.2 70-130 6.11 25 Chloroform 10.1 2.0 µg/L 10.0 101 70-130 2.92 25 Chloromethane 5.95 2.0 µg/L 10.0 59.5 40-160 6.50 25 t 2-Chlorotoluene 11.1 1.0 µg/L 10.0 111 70-130 3.72 25 4-Chlorotoluene 11.6 1.0 µg/L 10.0 116 70-130 2.81 25 1,2-Dibromo-3-chloropropane (DBCP) 7.54 5.0 µg/L 10.0 75.4 70-130 15.0 25 1,2-Dibromoethane (EDB) 10.6 0.50 µg/L 10.0 106 70-130 2.60 25 Dibromomethane 10.5 1.0 µg/L 10.0 105 70-130 3.00 25 1,2-Dichlorobenzene 10.7 1.0 µg/L 10.0 107 70-130 4.31 25 1,3-Dichlorobenzene 10.9 1.0 µg/L 10.0 109 70-130 3.08 25 1,4-Dichlorobenzene 9.87 1.0 µg/L 10.0 98.7 70-130 3.87 25 trans-1,4-Dichloro-2-butene 9.52 2.0 µg/L 10.0 95.2 70-130 4.42 25 Dichlorodifluoromethane (Freon 12) 3.90 2.0 µg/L 10.0 39.0 * 40-160 7.17 25 L-07 t 1, 1 -Dichloroethane 10.7 1.0 µg/L 10.0 107 70-130 8.65 25 1,2-Dichloroethane 9.65 1.0 µg/L 10.0 96.5 70-130 4.26 25 1,1-Dichloroethylene 9.59 1.0 µg/L 10.0 95.9 70-130 5.97 25 cis-1,2-Dichloroethylene 9.38 1.0 µg/L 10.0 93.8 70-130 1.90 25 trans-1,2-Dichloroethylene 9.46 1.0 µg/L 10.0 94.6 70-130 6.74 25 1,2-Dichloropropane 9.70 1.0 µg/L 10.0 97.0 70-130 4.93 25 1,3-Dichloropropane 9.95 0.50 µg/L 10.0 99.5 70-130 0.101 25 2,2-Dichloropropane 10.1 1.0 µg/L 10.0 101 40-130 6.40 25 t 1,1-Dichloropropene 9.54 2.0 µg/L 10.0 95.4 70-130 3.70 25 cis- 1,3 -Dichloropropene 8.84 0.50 µg/L 10.0 88.4 70-130 2.90 25 trans- l,3-Dichloropropene 9.18 0.50 µg/L 10.0 91.8 70-130 3.11 25 Diethyl Ether 10.8 2.0 µg/L 10.0 108 70-130 4.60 25 Diisopropyl Ether(DIPE) 13.0 0.50 µg/L 10.0 130 70-130 16.0 25 Page 15 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072403 - SW-846 5035 LCS Dup (B072403-BSD1) Prepared & Analyzed: 05/06/13 1,4-Dioxane 95.9 50 µg/L 100 95.9 40-130 24.7 50 V-16 f $ Ethylbenzene 10.7 1.0 µg/L 10.0 107 70-130 4.04 25 Hexachlorobutadiene 9.29 0.50 µg/L 10.0 92.9 70-130 0.857 25 2-Hexanone (MBK) 99.7 10 µg/L 100 99.7 70-160 11.1 25 f Isopropylbenzene(Cumene) 11.3 1.0 µg/L 10.0 113 70-130 1.67 25 p-Isopropyltoluene (p-Cymene) 9.51 1.0 µg/L 10.0 95.1 70-130 3.51 25 Methyl tert-Butyl Ether (MTBE) 9.71 1.0 µg/L 10.0 97.1 70-130 6.86 25 Methylene Chloride 8.29 5.0 µg/L 10.0 82.9 70-130 5.74 25 4-Methyl-2-pentanone (MIBK) 98.8 10 µg/L 100 98.8 70-160 8.94 25 t Naphthalene 7.21 2.0 µg/L 10.0 72.1 40-130 13.5 25 f n-Propylbenzene 11.0 1.0 µg/L 10.0 110 70-130 2.95 25 Styrene 11.7 1.0 µg/L 10.0 117 70-130 2.61 25 1, 1, 1,2-Tetrachloroethane 10.8 1.0 µg/L 10.0 108 70-130 5.13 25 1,1,2,2-Tetrachloroethane 10.1 0.50 µg/L 10.0 101 70-130 6.80 25 Tetrachloroethylene 10.7 1.0 µg/L 10.0 107 70-130 2.68 25 Tetrahydrofuran 9.74 10 µg/L 10.0 97.4 70-130 16.9 25 J Toluene 10.1 1.0 µg/L 10.0 101 70-130 2.53 25 1,2,3-Trichlorobenzene 7.37 5.0 µg/L 10.0 73.7 70-130 15.3 25 1,2,4-Trichlorobenzene 8.90 1.0 µg/L 10.0 89.0 70-130 5.15 25 1,3,5-Trichlorobenzene 8.97 1.0 µg/L 10.0 89.7 70-130 4.79 25 1, 1, 1 -Trichloroethane 9.93 1.0 µg/L 10.0 99.3 70-130 3.37 25 1,1,2-Trichloroethane 10.3 1.0 µg/L 10.0 103 70-130 0.291 25 Trichloroethylene 9.61 1.0 µg/L 10.0 96.1 70-130 5.56 25 Trichlorofluoromethane (Freon 11) 9.14 2.0 µg/L 10.0 91.4 70-130 7.38 25 1,2,3-Trichloropropane 10.6 2.0 µg/L 10.0 106 70-130 6.40 25 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 10.7 1.0 µg/L 10.0 107 70-130 7.29 25 113) 1,2,4-Trimethylbenzene 9.66 1.0 µg/L 10.0 96.6 70-130 1.85 25 1,3,5-Trimethylbenzene 10.5 1.0 µg/L 10.0 105 70-130 2.63 25 Vinyl Chloride 7.05 2.0 µg/L 10.0 70.5 40-160 1.83 25 t m+p Xylene 22.6 2.0 µg/L 20.0 113 70-130 4.46 25 o-Xylene 11.5 1.0 µg/L 10.0 115 70-130 2.82 25 Surrogate:l,2-Dichloroethane-d4 21.8 µg/L 25.0 87.4 70-130 Surrogate: Toluene-d8 24.3 µg/L 25.0 97.1 70-130 Surrogate:4-Bromofluorobenzene 25.3 µg/L 25.0 101 70-130 Page 16 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072641 - SW-846 3510C Blank (B072641-BLK1) Prepared & Analyzed: 05/09/13 Acenaphthene ND 5.0 µg/L Acenaphthylene ND 5.0 µg/L Acetophenone ND 10 µg/L Aniline ND 5.0 µg/L Anthracene ND 5.0 µg/L Benzidine ND 10 µg/L Benzo(a)anthracene ND 5.0 µg/L Benzo(a)pyrene ND 5.0 µg/L Benzo(b)fluoranthene ND 5.0 µg/L Benzo(g,h,i)perylene ND 5.0 µg/L Benzo(b)fluoranthene ND 5.0 µg/L Benzoic Acid ND 10 µg/L Bis(2-chloroethoxy)methane ND 10 µg/L Bis(2-chloroethyl)ether ND 10 µg/L Bis(2-chloroisopropyl)ether ND 10 µg/L Bis(2-Ethylhexyl)phthalate ND 10 µg/L 4-Bromophenylphenylether ND 10 µg/L Butylbenzylphthalate ND 10 µg/L Carbazole ND 10 µg/L 4-Chloroaniline ND 10 µg/L 4-Chloro-3-methylphenol ND 10 µg/L 2-Chloronaphthalene ND 10 µg/L 2-Chlorophenol ND 10 µg/L 4-Chlorophenylphenylether ND 10 µg/L Chrysene ND 5.0 µg/L Dibenz(a,h)anthracene ND 5.0 µg/L Dibenzofuran ND 5.0 µg/L Di-n-butylphthalate ND 10 µg/L 1,2-Dichlorobenzene ND 5.0 µg/L 1,3-Dichlorobenzene ND 5.0 µg/L 1,4-Dichlorobenzene ND 5.0 µg/L 3,3-Dichlorobenzidine ND 10 µg/L 2,4-Dichlorophenol ND 10 µg/L Diethylphthalate ND 10 µg/L 2,4-Dimethylphenol ND 10 µg/L Dimethylphthalate ND 10 µg/L 4,6-Dinitro-2-methylphenol ND 10 µg/L 2,4-Dinitrophenol ND 10 µg/L 2,4-Dinitrotoluene ND 10 µg/L 2,6-Dinitrotoluene ND 10 µg/L Di-n-octylphthalate ND 10 µg/L 1,2-Diphenylhydrazine (as Azobenzene) ND 10 µg/L Fluoranthene ND 5.0 µg/L Fluorene ND 5.0 µg/L Hexachlorobenzene ND 10 µg/L Hexachlorobutadiene ND 10 µg/L Hexachlorocyclopentadiene ND 10 µg/L Hexachloroethane ND 10 µg/L Indeno(1,2,3-cd)pyrene ND 5.0 µg/L Isophorone ND 10 µg/L 1-Methylnaphthalene ND 5.0 µg/L 2-Methylnaphthalene ND 5.0 µg/L R-05 R-05 V-05 Page 17 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072641 - SW-846 3510C Blank (B072641-BLK1) Prepared & Analyzed: 05/09/13 2-Methylphenol ND 10 µg/L 3/4-Methylphenol ND 10 µg/L Naphthalene ND 5.0 µg/L 2-Nitroaniline ND 10 µg/L 3-Nitroaniline ND 10 µg/L 4-Nitroaniline ND 10 µg/L Nitrobenzene ND 10 µg/L 2-Nitrophenol ND 10 µg/L 4-Nitrophenol ND 10 µg/L N-Nitrosodimethylamine ND 5.0 µg/L N-Nitrosodiphenylamine ND 10 µg/L N-Nitrosodi-n-propylamine ND 10 µg/L Pentachloronitrobenzene ND 10 µg/L V-16 Pentachlorophenol ND 10 µg/L Phenanthrene ND 5.0 µg/L Phenol ND 10 µg/L Pyrene ND 5.0 µg/L Pyridine ND 5.0 µg/L 1,2,4,5-Tetrachlorobenzene ND 10 µg/L 1,2,4-Trichlorobenzene ND 5.0 µg/L 2,4,5-Trichlorophenol ND 10 µg/L 2,4,6-Trichlorophenol ND 10 µg/L Surrogate:2-Fluorophenol 95.2 µg/L 200 47.6 15-110 Surrogate: Phenol-d6 84.4 µg/L 200 42.2 15-110 Surrogate: Nitrobenzene-d5 77.9 µg/L 100 77.9 30-130 Surrogate:2-Fluorobiphenyl 70.1 µg/L 100 70.1 30-130 Surrogate: 2,4,6-Tribromophenol 146 µg/L 200 72.9 15-110 Surrogate:p-Terphenyl-dl4 77.8 µg/L 100 77.8 30-130 LCS (B072641-BSI) Prepared & Analyzed: 05/09/13 Acenaphthene 69.9 5.0 µg/L Acenaphthylene 69.4 5.0 µg/L Acetophenone 86.0 10 µg/L Aniline 71.3 5.0 µg/L Anthracene 65.2 5.0 µg/L Benzidine 49.0 10 µg/L Benzo(a)anthracene 109 5.0 µg/L Benzo(a)pyrene 89.7 5.0 µg/L Benzo(b)fluoranthene 110 5.0 µg/L Benzo(g,h,i)perylene 43.6 5.0 µg/L Benzo(k)fluoranthene 66.9 5.0 µg/L Benzoic Acid 24.0 10 µg/L Bis(2-chloroethoxy)methane 94.6 10 µg/L Bis(2-chloroethyl)ether 89.8 10 µg/L Bis(2-chloroisopropyl)ether 80.9 10 µg/L Bis(2-Ethylhexyl)phthalate 88.2 10 µg/L 4-Bromophenylphenylether 76.7 10 µg/L Butylbenzylphthalate 93.8 10 µg/L Carbazole 81.9 10 µg/L 4-Chloroaniline 71.6 10 µg/L 4-Chloro-3-methylphenol 76.5 10 µg/L 2-Chloronaphthalene 45.0 10 µg/L 100 69.9 40-140 100 69.4 40-140 100 86.0 40-140 100 71.3 40-140 100 65.2 40-140 100 49.0 40-140 R-05 100 109 40-140 100 89.7 40-140 100 110 40-140 100 43.6 40-140 100 66.9 40-140 100 24.0 10-130 t 100 94.6 40-140 100 89.8 40-140 100 80.9 40-140 100 88.2 40-140 100 76.7 40-140 100 93.8 40-140 100 81.9 40-140 100 71.6 40-140 100 76.5 30-130 100 45.0 40-140 R-05 Page 18 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD .nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072641 - SW-846 3510C LCS (B072641-BSI) Prepared & Analyzed: 05/09/13 2-Chlorophenol 84.2 10 µg/L 4-Chlorophenylphenylether 65.1 10 µg/L Chrysene 84.0 5.0 µg/L Dibenz(a,h)anthracene 57.8 5.0 µg/L Dibenzofuran 75.3 5.0 µg/L Di-n-butylphthalate 72.9 10 µg/L 1,2-Dichlorobenzene 74.5 5.0 µg/L 1,3-Dichlorobenzene 71.4 5.0 µg/L 1,4-Dichlorobenzene 72.1 5.0 µg/L 3,3-Dichlorobenzidine 65.3 10 µg/L 2,4-Dichlorophenol 82.2 10 µg/L Diethylphthalate 75.9 10 µg/L 2,4-Dimethylphenol 83.1 10 µg/L Dimethylphthalate 80.3 10 µg/L 4,6-Dinitro-2-methylphenol 102 10 µg/L 2,4-Dinitrophenol 97.0 10 µg/L 2,4-Dinitrotoluene 74.7 10 µg/L 2,6-Dinitrotoluene 39.2 10 µg/L Di-n-octylphthalate 91.6 10 µg/L 1,2-Diphenylhydrazine (as Azobenzene) 79.7 10 µg/L Fluoranthene 84.0 5.0 µg/L Fluorene 69.8 5.0 µg/L Hexachlorobenzene 74.3 10 µg/L Hexachlorobutadiene 69.4 10 µg/L Hexachlorocyclopentadiene 71.1 10 µg/L Hexachloroethane 60.9 10 µg/L Indeno(1,2,3-cd)pyrene 61.8 5.0 µg/L Isophorone 83.2 10 µg/L 1-Methylnaphthalene 73.2 5.0 µg/L 2-Methylnaphthalene 73.2 5.0 µg/L 2-Methylphenol 91.4 10 µg/L 3/4-Methylphenol 89.5 10 µg/L Naphthalene 68.3 5.0 µg/L 2-Nitroaniline 70.0 10 µg/L 3-Nitroaniline 85.0 10 µg/L 4-Nitroaniline 66.3 10 µg/L Nitrobenzene 77.9 10 µg/L 2-Nitrophenol 82.6 10 µg/L 4-Nitrophenol 77.8 10 µg/L N-Nitrosodimethylamine 43.7 5.0 µg/L N-Nitrosodiphenylamine 91.3 10 µg/L N-Nitrosodi-n-propylamine 75.2 10 µg/L Pentachloronitrobenzene 84.4 10 µg/L Pentachlorophenol 101 10 µg/L Phenanthrene 69.8 5.0 µg/L Phenol 44.6 10 µg/L Pyrene 93.4 5.0 µg/L Pyridine 44.8 5.0 µg/L 1,2,4,5-Tetrachlorobenzene 69.8 10 µg/L 1,2,4-Trichlorobenzene 73.0 5.0 µg/L 2,4,5-Trichlorophenol 72.8 10 µg/L 2,4,6-Trichlorophenol 91.1 10 µg/L 100 84.2 30-130 100 65.1 40-140 100 84.0 40-140 100 57.8 40-140 100 75.3 40-140 100 72.9 40-140 V-05 100 74.5 40-140 100 71.4 40-140 100 72.1 40-140 100 65.3 40-140 100 82.2 30-130 100 75.9 40-140 100 83.1 30-130 100 80.3 40-140 100 102 30-130 100 97.0 30-130 100 74.7 40-140 100 59.2 40-140 100 91.6 40-140 100 79.7 40-140 100 84.0 40-140 100 69.8 40-140 100 74.3 40-140 100 69.4 40-140 100 71.1 30-140 t 100 60.9 40-140 100 61.8 40-140 100 83.2 40-140 100 73.2 40-140 100 73.2 40-140 100 91.4 30-130 100 89.5 30-130 100 68.3 40-140 100 70.0 40-140 100 85.0 40-140 100 66.3 40-140 100 77.9 40-140 100 82.6 30-130 100 77.8 10-130 f 100 53.7 40-140 100 91.3 40-140 100 75.2 40-140 100 84.4 40-140 V-16 100 101 30-130 100 69.8 40-140 100 44.6 20-130 T 100 93.4 40-140 100 44.8 10-140 100 69.8 40-140 100 73.0 40-140 100 72.8 30-130 100 91.1 30-130 Page 19 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072641 - SW-846 3510C LCS (B072641-BSI) Prepared & Analyzed: 05/09/13 Surrogate:2-Fluorophenol 132 µg/L 200 65.8 15-110 Surrogate: Phenol-d6 90.0 µg/L 200 45.0 15-110 Surrogate: Nitrobenzene-d5 78.6 µg/L 100 78.6 30-130 Surrogate:2-Fluorobiphenyl 72.9 µg/L 100 72.9 30-130 Surrogate: 2,4,6-Tribromophenol 167 µg/L 200 83.5 15-110 Surrogate:p-Terphenyl-dl4 92.8 µg/L 100 92.8 30-130 LCS Dup (B072641-BSD1) Prepared & Analyzed: 05/09/13 Acenaphthene 71.5 5.0 µg/L Acenaphthylene 70.3 5.0 µg/L Acetophenone 86.5 10 µg/L Aniline 72.1 5.0 µg/L Anthracene 64.2 5.0 µg/L Benzidine 62.6 10 µg/L Benzo(a)anthracene 90.1 5.0 µg/L Benzo(a)pyrene 87.9 5.0 µg/L Benzo(b)fluoranthene 96.9 5.0 µg/L Benzo(g,h,i)perylene 39.5 5.0 µg/L Benzo(b)fluoranthene 75.3 5.0 µg/L Benzoic Acid 22.6 10 µg/L Bis(2-chloroethoxy)methane 93.0 10 µg/L Bis(2-chloroethyl)ether 86.0 10 µg/L Bis(2-chloroisopropyl)ether 80.8 10 µg/L Bis(2-Ethylhexyl)phthalate 80.4 10 µg/L 4-Bromophenylphenylether 72.8 10 µg/L Butylbenzylphthalate 81.1 10 µg/L Carbazole 73.4 10 µg/L 4-Chloroaniline 64.4 10 µg/L 4-Chloro-3-methylphenol 69.5 10 µg/L 2-Chloronaphthalene 58.1 10 µg/L 2-Chorophenol 84.5 10 µg/L 4-Chlorophenylphenylether 65.2 10 µg/L Chrysene 79.8 5.0 µg/L Dibenz(a,h)anthracene 55.5 5.0 µg/L Dibenzofuran 71.3 5.0 µg/L Di-n-butylphthalate 68.4 10 µg/L 1,2-Dichlorobenzene 73.6 5.0 µg/L 1,3-Dichlorobenzene 70.1 5.0 µg/L 1,4-Dichlorobenzene 71.9 5.0 µg/L 3,3-Dichlorobenzidine 58.1 10 µg/L 2,4-Dichlorophenol 80.2 10 µg/L Diethylphthalate 71.0 10 µg/L 2,4-Dimethylphenol 81.6 10 µg/L Dimethylphthalate 76.7 10 µg/L 4,6-Dinitro-2-methylphenol 85.6 10 µg/L 2,4-Dinitrophenol 77.9 10 µg/L 2,4-Dinitrotoluene 71.0 10 µg/L 2,6-Dinitrotoluene 61.4 10 µg/L Di-n-octylphthalate 89.5 10 µg/L 1,2-Diphenylhydrazine (as Azobenzene) 76.1 10 µg/L Fluoranthene 74.0 5.0 µg/L Fluorene 68.4 5.0 µg/L 100 71.5 40-140 2.18 20 100 70.3 40-140 1.36 20 100 86.5 40-140 0.475 20 100 72.1 40-140 1.14 50 $ 100 64.2 40-140 1.64 20 100 62.6 40-140 24.3 * 20 R-05 100 90.1 40-140 19.2 20 100 87.9 40-140 2.08 20 100 96.9 40-140 12.2 20 100 39.5 * 40-140 9.84 20 L-07 100 75.3 40-140 11.8 20 100 22.6 10-130 5.71 50 f $ 100 93.0 40-140 1.74 20 100 86.0 40-140 4.28 20 100 80.8 40-140 0.0124 20 100 80.4 40-140 9.27 20 100 72.8 40-140 5.19 20 100 81.1 40-140 14.6 20 100 73.4 40-140 11.0 20 100 64.4 40-140 10.6 20 100 69.5 30-130 9.62 20 100 58.1 40-140 25.3 * 20 R-05 100 84.5 30-130 0.379 20 100 65.2 40-140 0.200 20 100 79.8 40-140 5.10 20 100 55.5 40-140 4.08 20 100 71.3 40-140 5.43 20 100 68.4 40-140 6.33 20 V-05 100 73.6 40-140 1.24 20 100 70.1 40-140 1.78 20 100 71.9 40-140 0.194 20 100 58.1 40-140 11.7 20 100 80.2 30-130 2.41 20 100 71.0 40-140 6.75 20 100 81.6 30-130 1.85 20 100 76.7 40-140 4.56 50 $ 100 85.6 30-130 17.3 50 $ 100 77.9 30-130 21.9 50 $ 100 71.0 40-140 5.13 20 100 61.4 40-140 3.63 20 100 89.5 40-140 2.24 20 100 76.1 40-140 4.58 20 100 74.0 40-140 12.6 20 100 68.4 40-140 2.04 20 Page 20 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072641 - SW-846 3510C LCS Dup (B072641-BSD1) Prepared & Analyzed: 05/09/13 Hexachlorobenzene 78.2 10 µg/L 100 78.2 40-140 5.06 20 Hexachlorobutadiene 66.4 10 µg/L 100 66.4 40-140 4.42 20 Hexachlorocyclopentadiene 68.4 10 µg/L 100 68.4 30-140 3.89 50 f $ Hexachloroethane 60.0 10 µg/L 100 60.0 40-140 1.54 50 $ Indeno(1,2,3-cd)pyrene 55.2 5.0 µg/L 100 55.2 40-140 11.3 50 $ Isophorone 80.2 10 µg/L 100 80.2 40-140 3.72 20 1-Methylnaphthalene 70.7 5.0 µg/L 100 70.7 40-140 3.39 20 2-Methylnaphthalene 68.3 5.0 µg/L 100 68.3 40-140 6.95 20 2-Methylphenol 91.7 10 µg/L 100 91.7 30-130 0.382 20 3/4-Methylphenol 88.0 10 µg/L 100 88.0 30-130 1.65 20 Naphthalene 65.8 5.0 µg/L 100 65.8 40-140 3.71 20 2-Nitroanihne 68.0 10 µg/L 100 68.0 40-140 2.97 20 3-Nitroaniline 78.4 10 µg/L 100 78.4 40-140 8.19 20 4-Nitroaniline 65.7 10 µg/L 100 65.7 40-140 0.879 20 Nitrobenzene 74.7 10 µg/L 100 74.7 40-140 4.19 20 2-Nitrophenol 78.8 10 µg/L 100 78.8 30-130 4.78 20 4-Nitrophenol 672 10 µg/L 100 67.2 10-130 14.6 50 t # N-Nitrosodimethylamine 32.5 5.0 µg/L 100 52.5 40-140 2.22 20 N-Nitrosodiphenylamine 91.2 10 µg/L 100 91.2 40-140 0.142 20 N-Nitrosodi-n-propylamine 73.9 10 µg/L 100 73.9 40-140 1.74 20 Pentachloronitrobenzene 81.0 10 µg/L 100 81.0 40-140 4.15 20 V-16 Pentachlorophenol 84.8 10 µg/L 100 84.8 30-130 17.4 50 $ Phenanthrene 67.8 5.0 µg/L 100 67.8 40-140 2.98 20 Phenol 44.5 10 µg/L 100 44.5 20-130 0.0449 20 f Pyrene 79.6 5.0 µg/L 100 79.6 40-140 16.0 20 Pyridine 44.8 5.0 µg/L 100 44.8 10-140 0.112 50 t # 1,2,4,5-Tetrachlorobenzene 71.3 10 µg/L 100 71.3 40-140 2.04 20 1,2,4-Trichlorobenzene 70.5 5.0 µg/L 100 70.5 40-140 3.55 20 2,4,5-Trichlorophenol 74.0 10 µg/L 100 74.0 30-130 1.72 20 2,4,6-Trichlorophenol 85.3 10 µg/L 100 85.3 30-130 6.61 50 $ Surrogate:2-Fluorophenol 128 µg/L 200 64.0 15-110 Surrogate: Phenol-d6 87.0 µg/L 200 43.5 15-110 Surrogate: Nitrobenzene-d5 74.8 µg/L 100 74.8 30-130 Surrogate:2-Fluorobiphenyl 73.0 µg/L 100 73.0 30-130 Surrogate: 2,4,6-Tribromophenol 150 µg/L 200 75.0 15-110 Surrogate:p-Terphenyl-dl4 77.1 µg/L 100 77.1 30-130 Page 21 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Metals Analyses (Total) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072571 - SW-846 7470A Prep Blank (B072571-BLK1) Prepared & Analyzed: 05/08/13 Mercury ND 0.00010 mg/L LCS (B072571-BS1) Prepared & Analyzed: 05/08/13 Mercury 0.00188 0.00010 mg/L 0.00200 93.8 80-120 LCS Dup (B072571-BSD1) Prepared & Analyzed: 05/08/13 Mercury 0.00185 0.00010 mg/L 0.00200 92.4 80-120 1.46 20 Duplicate (B072571-DUPl) Source: 13EO159-01 Prepared & Analyzed: 05/08/13 Mercury ND 0.00010 mg/L ND NC 20 Matrix Spike (B072571-MS1) Source: 13EO159-01 Prepared & Analyzed: 05/08/13 Mercury 0.00181 0.00010 mg/L 0.00200 ND 90.3 75-125 Batch B072721 - SM 3030C Blank (B072721-BLK1) Prepared: 05/09/13 Analyzed: 05/10/13 Aluminum ND 0.050 mg/L Calcium ND 0.15 mg/L Iron ND 0.050 mg/L Magnesium ND 0.15 mg/L Potassium ND 2.0 mg/L Sodium ND 2.0 mg/L LCS (B072721-BSI) Prepared: 05/09/13 Analyzed: 05/10/13 Aluminum 2.00 0.050 mg/L 2.00 99.8 80-120 Calcium 2.09 0.15 mg/L 2.00 104 80-120 Iron 1.97 0.050 mg/L 2.00 98.3 80-120 Magnesium 2.10 0.15 mg/L 2.00 105 80-120 Potassium 20.4 2.0 mg/L 20.0 102 80-120 Sodium 2.01 2.0 mg/L 2.00 100 80-120 LCS Dup (B072721-BSD1) Prepared: 05/09/13 Analyzed: 05/10/13 Aluminum 2.00 0.050 mg/L 2.00 100 80-120 0.162 20 Calcium 2.10 0.15 mg/L 2.00 105 80-120 0.419 20 Iron 1.96 0.050 mg/L 2.00 98.2 80-120 0.0863 20 Magnesium 2.11 0.15 mg/L 2.00 105 80-120 0.102 20 Potassium 20.4 2.0 mg/L 20.0 102 80-120 0.229 20 Sodium 2.00 2.0 mg/L 2.00 99.9 80-120 0.396 20 J Duplicate (B072721-DUPI) Source: 13EO159-01 Prepared: 05/09/13 Analyzed: 05/10/13 Aluminum 5.57 0.050 mg/L 5.61 0.830 20 Calcium 107 0.15 mg/L 108 0.680 20 Iron 6.48 0.050 mg/L 6.52 0.691 20 Magnesium 25.1 0.15 mg/L 25.3 0.929 20 Potassium 7.54 2.0 mg/L 7.59 0.645 20 Sodium 34.1 2.0 mg/L 34.4 0.849 20 Page 22 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Metals Analyses (Total) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072721 - SM 3030C Matrix Spike (B072721-MS1) Source: 13EO159-01 Prepared: 05/09/13 Analyzed: 05/10/13 Aluminum 7.71 0.050 mg/L 2.00 5.61 105 75-125 Calcium 110 0.15 mg/L 2.00 108 110 75-125 Iron 8.47 0.050 mg/L 2.00 6.52 97.4 75-125 Magnesium 27.5 0.15 mg/L 2.00 25.3 107 75-125 Potassium 28.4 2.0 mg/L 20.0 7.59 104 75-125 Sodium 35.3 2.0 mg/L 2.00 34.4 42.8 * 75-125 MS-19 Batch B072722 - SM 3030C Blank (B072722-BLKI) Prepared: 05/09/13 Analyzed: 05/10/13 Antimony ND 2.0 µg/L Arsenic ND 0.80 µg/L Barium ND 20 µg/L Beryllium ND 2.0 µg/L Cadmium ND 1.0 µg/L Chromium 1.5 2.0 µg/L J Cobalt ND 2.0 µg/L Copper ND 10 µg/L Lead ND 2.0 µg/L Manganese ND 2.0 µg/L Nickel 1.1 10 µg/L J Selenium ND 10 µg/L Silver ND 1.0 µg/L Thallium ND 0.40 µg/L Vanadium ND 10 µg/L Zinc ND 20 µg/L LCS (B072722-BSI) Prepared: 05/09/13 Analyzed: 05/10/13 Antimony 503 10 µg/L 500 101 80-120 Arsenic 490 4.0 µg/L 500 98.1 80-120 Barium 484 100 µg/L 500 96.8 80-120 Beryllium 499 4.0 µg/L 500 99.9 80-120 Cadmium 499 5.0 µg/L 500 99.7 80-120 Chromium 494 10 µg/L 500 98.8 80-120 Cobalt 471 10 µg/L 500 94.1 80-120 Copper 511 50 µg/L 500 102 80-120 Lead 485 10 µg/L 500 97.1 80-120 Manganese 478 10 µg/L 500 95.7 80-120 Nickel 495 50 µg/L 500 99.0 80-120 Selenium 496 50 µg/L 500 99.2 80-120 Silver 514 5.0 µg/L 500 103 80-120 Thallium 466 2.0 µg/L 500 93.3 80-120 Vanadium 494 50 µg/L 500 98.7 80-120 Zinc 523 100 µg/L 500 105 80-120 Page 23 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Metals Analyses (Total) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B072722 - SM 3030C LCS Dup (B072722-BSD1) Prepared: 05/09/13 Analyzed: 05/10/13 Antimony 509 10 µg/L 500 102 80-120 1.26 20 Arsenic 489 4.0 µg/L 500 97.7 80-120 0.388 20 Barium 482 100 µg/L 500 96.3 80-120 0.494 20 Beryllium 505 4.0 µg/L 500 101 80-120 1.08 20 Cadmium 499 5.0 µg/L 500 99.8 80-120 0.0865 20 Chromium 493 10 µg/L 500 98.5 80-120 0.327 20 Cobalt 464 10 µg/L 500 92.8 80-120 1.45 20 Copper 507 50 µg/L 500 101 80-120 0.759 20 Lead 486 10 µg/L 500 97.1 80-120 0.0329 20 Manganese 480 10 µg/L 500 95.9 80-120 0.221 20 Nickel 482 50 µg/L 500 96.4 80-120 2.67 20 Selenium 493 50 µg/L 500 98.6 80-120 0.579 20 Silver 513 5.0 µg/L 500 103 80-120 0.105 20 Thallium 474 2.0 µg/L 500 94.8 80-120 1.62 20 Vanadium 492 50 µg/L 500 98.3 80-120 0.367 20 Zinc 526 100 µg/L 500 105 80-120 0.469 20 Duplicate (B072722-DUPl) Source: 13EO159-01 Prepared: 05/09/13 Analyzed: 05/10/13 Antimony 5.36 2.0 µg/L 5.42 1.10 20 Arsenic 84.2 0.80 µg/L 85.0 0.954 20 Barium 1080 20 µg/L 1100 1.82 20 Beryllium 1.51 2.0 µg/L 1.56 2.80 20 1 Cadmium 0.153 1.0 µg/L 0.166 8.12 20 1 Chromium 14.3 2.0 µg/L 14.6 2.16 20 Cobalt 14.4 2.0 µg/L 14.7 1.85 20 Copper 23.9 10 µg/L 24.6 3.02 20 Lead 5.81 2.0 µg/L 5.84 0.473 20 Manganese 7840 100 µg/L 7600 3.07 20 Nickel 12.1 10 µg/L 12.1 0.264 20 Selenium 2.26 10 µg/L 2.46 8.46 20 J Silver ND 1.0 µg/L ND NC 20 Thallium 1.03 0.40 µg/L 1.04 1.27 20 Vanadium 38.3 10 µg/L 37.8 1.47 20 Zinc 49.6 20 µg/L 52.2 5.21 20 Matrix Spike (B072722-MS1) Source: 13EO159-01 Prepared: 05/09/13 Analyzed: 05/10/13 Antimony 525 10 µg/L Arsenic 587 4.0 µg/L Barium 1500 100 µg/L Beryllium 505 4.0 µg/L Cadmium 501 5.0 µg/L Chromium 511 10 µg/L Cobalt 485 10 µg/L Copper 527 50 µg/L Lead 500 10 µg/L Manganese 8020 100 µg/L Nickel 504 50 µg/L Selenium 494 50 µg/L Silver 517 5.0 µg/L Thallium 477 2.0 µg/L Vanadium 563 50 µg/L Zinc 565 100 µg/L 500 5.42 104 75-125 500 85.0 100 75-125 500 1100 78.5 75-125 500 1.56 101 75-125 500 0.166 100 75-125 500 14.6 99.3 75-125 500 14.7 94.0 75-125 500 24.6 101 75-125 500 5.84 98.9 75-125 500 7600 84.5 75-125 500 12.1 98.3 75-125 500 2.46 98.4 75-125 500 ND 103 75-125 500 1.04 95.2 75-125 500 37.8 105 75-125 500 52.2 103 75-125 Page 24 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. MS-19 Sample to spike ratio is greater than or equal to 4:1. Spiked amount is not representative of the native amount in the sample. Appropriate or meaningful recoveries cannot be calculated. R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound. Increased uncertainty is associated with the reported value which is likely to be biased on the low side. V-16 Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported result. V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Page 25 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 6010C in Water Aluminum CT,NH,NY,ME,VA Calcium CT,NH,NY,ME,NC,VA Iron CT,NH,NY,ME,NC,VA Magnesium CT,NH,NY,ME,NC,VA Potassium CT,NH,NY,ME,NC,VA Sodium CT,NH,NY,ME,NC,VA SW-846 6020A in Water Antimony CT,NH,NY,NC,ME,VA Arsenic CT,NH,NY,NC,ME,VA Barium CT,NH,NY,NC,ME,VA Beryllium CT,NH,NY,NC,ME,VA Cadmium CT,NH,NY,RI,NC,ME,VA Chromium CT,NH,NY,NC,ME,VA Cobalt CT,NH,NY,NC,ME,VA Copper CT,NH,NY,NC,ME,VA Lead CT,NH,NY,NC,ME,VA Manganese CT,NH,NY,NC,ME,VA Nickel CT,NH,NY,NC,ME,VA Selenium CT,NH,NY,NC,ME,VA Silver CT,NH,NY,NC,ME,VA Thallium CT,NH,NY,NC,ME,VA Vanadium CT,NC,NH,NY,ME,VA Zinc CT,NH,NY,NC,ME,VA SW-846 7470A in Water Mercury CT,NH,NY,NC,ME,VA SW-846 8260B in Water Acetone CT,NH,NY,NC,ME Acrylonitrile CT,NY,NC,ME tert-Amyl Methyl Ether (TAME) NH,NY,NC,ME Benzene CT,NH,NY,NC,ME Bromobenzene NC Bromochloromethane NH,NY,NC,ME Bromodichloromethane CT,NH,NY,NC,ME Bromoform CT,NH,NY,NC,ME Bromomethane CT,NH,NY,NC,ME 2-Butanone (MEK) CT,NH,NY,NC,ME tert-Butyl Alcohol (TBA) NH,NY,NC,ME n-Butylbenzene NY,NC,ME sec-Butylbenzene NY,NC,ME tert-Butylbenzene NY,NC,ME tert-Butyl Ethyl Ether (TBEE) NH,NY,NC,ME Carbon Disulfide CT,NH,NY,NC,ME Carbon Tetrachloride CT,NH,NY,NC,ME Chlorobenzene CT,NH,NY,NC,ME Chlorodibromomethane CT,NH,NY,NC,ME Chloroethane CT,NH,NY,NC,ME Page 26 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8260B in Water Chloroform CT,NH,NY,NC,ME Chloromethane CT,NH,NY,NC,ME 2-Chlorotoluene NY,NC,ME 4-Chlorotoluene NY,NC,ME 1,2-Dibromo-3-chloropropane (DBCP) NC 1,2-Dibromoethane (EDB) NC Dibromomethane NH,NY,NC,ME 1,2-Dichlorobenzene CT,NY,NC,ME 1,3-Dichlorobenzene CT,NH,NY,NC,ME 1,4-Dichlorobenzene CT,NH,NY,NC,ME trans-1,4-Dichloro-2-butene NH,NY,NC,ME Dichlorodifluoromethane (Freon 12) NH,NY,NC,ME I,I-Dichloroethane CT,NH,NY,NC,ME 1,2-Dichloroethane CT,NH,NY,NC,ME 1, 1 -Dichloroethylene CT,NH,NY,NC,ME cis-1,2-Dichloroethylene NY,NC,ME trans-1,2-Dichloroethylene CT,NH,NY,NC,ME 1,2-Dichloropropane CT,NH,NY,NC,ME 1,3-Dichloropropane NY,NC,ME 2,2-Dichloropropane NH,NY,NC,ME I,I-Dichloropropene NH,NY,NC,ME cis- 1,3 -Dichloropropene CT,NH,NY,NC,ME trans- l,3-Dichloropropene CT,NH,NY,NC,ME Diethyl Ether NC Diisopropyl Ether (DIPE) NH,NY,NC,ME 1,4-Dioxane NC Ethylbenzene CT,NH,NY,NC,ME Hexachlorobutadiene CT,NH,NY,NC,ME 2-Hexanone (MBK) CT,NH,NY,NC,ME Isopropylbenzene (Cumene) NY,NC,ME p-Isopropyltoluene (p-Cymene) CT,NH,NY,NC,ME Methyl tert-Butyl Ether (MTBE) CT,NH,NY,NC,ME Methylene Chloride CT,NH,NY,NC,ME 4-Methyl-2-pentanone (MIBK) CT,NH,NY,NC,ME Naphthalene NH,NY,NC,ME n-Propylbenzene CT,NH,NY,NC,ME Styrene CT,NH,NY,NC,ME 1, 1, 1,2-Tetrachloroethane CT,NH,NY,NC,ME 1,1,2,2-Tetrachloroethane CT,NH,NY,NC,ME Tetrachloroethylene CT,NH,NY,NC,ME Tetrahydrofuran NC Toluene CT,NH,NY,NC,ME 1,2,3-Trichlorobenzene NH,NY,NC,ME 1,2,4-Trichlorobenzene CT,NH,NY,NC,ME 1,3,5-Trichlorobenzene NC,ME 1, 1, 1 -Trichloroethane CT,NH,NY,NC,ME 1,1,2-Trichloroethane CT,NH,NY,NC,ME Page 27 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte SW-846 8260B in Water Trichloroethylene Trichlorofluoromethane (Freon 11) 1,2,3-Trichloropropane 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 1,2,4-Trimethylb enzene 1,3,5-Trimethylbenzene Vinyl Chloride m+p Xylene o-Xylene SW-846 8270D in Water Acenaphthene Acenaphthylene Acetophenone Aniline Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid B is(2-chloroethoxy)methane Bis(2-chloroethyl)ether Bis(2-chloroisopropyl)ether Bis(2-Ethylhexyl)phthalate 4-Bromophenylphenylether Butylbenzylphthalate Carbazole 4-Chloroaniline 4-Chloro-3-methylphenol 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenylether Chrysene Dibenz(a,h)anthracene Dibenzofuran Di-n-butylphthalate 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 3,3-Dichlorobenzidine 2,4-Dichlorophenol Diethylphthalate 2,4-Dimethylphenol Dimethylphthalate Certifications CT,NH,NY,NC,ME CT,NH,NY,NC,ME NH,NY,NC,ME NC NY,NC,ME NY,NC,ME CT,NH,NY,NC,ME CT,NH,NY,NC,ME CT,NH,NY,NC,ME CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA NC CT,NY,NC,ME,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA NC CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA Page 28 of 33 13EO159 1 Contest Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY Certified Analyses included in this Report Analyte SW-846 8270D in Water 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate 1,2-Diphenylhydrazine (as Azobenzene) Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone 1-Methylnaphthalene 2-Methylnaphthalene 2-Methylphenol 3/4-Methylphenol Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitrosodimethylamine N-Nitrosodiphenylamine N-Nitrosodi-n-propylamine Pentachloronitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine 1,2,4,5-Tetrachlorobenzene 1,2,4-Trichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2-Fluorophenol 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certifications CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA NC CT,NY,NC,ME,NH,VA NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA NC CT,NY,NC,ME,NH,VA CT,NY,NC,NH,VA CT,NY,NC,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA NC CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA NC CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA CT,NY,NC,ME,NH,VA NC Page 29 of 33 13EO159 1 Contest Final 05 14 13 1358 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 The CON -TEST Environmental Laboratory operates under the following certifications and accreditation: Code Description Number Expires AIHA AIHA-LAP, LLC 100033 02/1/2014 MA Massachusetts DEP M-MA100 06/30/2013 CT Connecticut Department of Publilc Health PH-0567 09/30/2013 NY New York State Department of Health 10899 NELAP 04/1/2014 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2014 RI Rhode Island Department of Health LA000112 12/30/2013 NC North Carolina Div. of Water Quality 652 12/31/2013 NJ New Jersey DEP MA007 NELAP 06/30/2013 FL Florida Department of Health E871027 NELAP 06/30/2013 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2013 WA State of Washington Department of Ecology C2065 02/23/2014 ME State of Maine 2011028 06/9/2013 VA Commonwealth of Virginia 460217 12/14/2013 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2012 Page 30 of 33 13EO159 1 Contest Final 05 14 13 1358 n O s rD rt CD A �E d....,w. 0.9: 00 0 0 0 N W � ILA � O n o nID n Y. o M . n ,. 000 n _ o 00 q tiiYr C � 2 � X � v m w €� m O r-• W n Q a. C @ X rD CL n C n e � G "G n O -o O > G [ -ray g e � N ro I'I -n rn -rs O rli� O It a O U M i 000 s G o O 0 m � Gl cL n M 0 0 r(G n 0 ®% ur < D u fdS cv r?i o; 31 of 33 13E0159 1 Con m w r � a � n on (D Ln rD n) 0 D a CD 0 00 � n Q r�• q f0 n PJ s m VY ro Est Final05 1358 14 13 39 spruce st Eo st ?.ongmeadow, MA 01028 P: 413-525-2332 F:413-525-6405 www.contestlabs.enrn con _testIII ANALYTICAL LABORATORY F 1) Was the chain(s) of custody relinquished and signed? 2) Does the chain agree with the samples? If not, explain: 8) Are all the samples in good condition? If not, explain: 4) How were'ihe samples received- m..._ Oo Ice Direct from Sampling Ambient i !1n Ier(s) Were the samples received in Temperature Cor pliance of (2-60C)? s :,- o N/A Temperature °C by Temp blank Temperature °C by Temp gunk 5) Are there 3issoived samples for the lab to filter? Yes o i Who was notified [late Time 6) Are there any RUSH or SHORT HOLDING T'E E samples? Yes Who was notified Date Time 7) Location where samples are stored: Permission to subcontract samples? Yes No (Walk-in clients only) if not already approved Client Signature: 8) Do all samples have the proper Acid ply: No N/A11, 9) Lice all samples have the proper Base pH. Yes.._., o N/A,/ 10) Was the PC notified of any discrepancies with the CoC vs the samples: Yes No N/A # of containers 1 Liter Amber �500 mL Amber 250 mL Amber (8oz amber) 1 Liter Plastic 500 mL Plastic 260 mL lastic 40 mL Vial - tVpe listed below Colisure / bacteria bottle Dissolved Oxygen bottle: Encore Flashpoint bottle Perchlorate Kit Other Laboratory Comments: 40 mL vials: # NCIMethanol flo6 277 # Bisulfate # DI Water Rev:::3 May 20t2 # Thiosuifate Unpreserve # of containers 8 oz amber/clear jar _4 oz amber/clear jar 2 oz amber/clear jar Air Cassette Hq/Hopcalite Tube Plastic Bag 1.Ziploc PM 2.5 / PM 10 PUF Cartrid e SOC Kit TO-17 Tubes ikon-ConTest Container Other glass jar Other Time and Date Frozen: Pape 32 of 33 13EO159 1 Contest Final 05 14 13 1358 1 Track your package or ghipmont with FedEx Tracking Page I of I M= 1 0025396971Fri 88 p 5/0312013 6:21 Pm . . .............. .................................. Travel History 5j0,V20i3 - satuTday .0. JI � Fed;:.vo �.x nide, rid fiver am At, klcal V, fmn�Iy Fm. :)a"'ed , ,')[..x ja"20(,n SiO3),2013 Friday 10 47 pri, Nr:1vid ai FedEx Soar k.,n S 41,i Pm elt IlaoEx �2! -m up CTmtored a3'. �',odi:mx Off:,!,' Shipment Facts Tmg;Rimj number 20 flbs LMIverO To Sl �ippnq-Remivmq 'M t x", 9.1 kgs Gpec�a� handling f ) 11! iVCJL I C�l �11 SLrVice Dlmen�Mans Tota; piect,3 pockagi g Sat 5/04/2013 iOM am Locitim Locai Scan Time.j- iraff-.x P`OIy Overmcflh! hitps://www.fedex.coiii/fedextr�ick/index.liti-n.]?trackni Page 33 of 33 13EO1591 Contest —Final 05 14 13 1358 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 June 24, 2013 Josh Dunbar Falcon Engineering 1210 Trinity Road, Suite 110 Raleigh, NC 27607 Project Location: 828 MLK, Chapel Hill Client Job Number: Project Number: El3026 Laboratory Work Order Number: 13FO722 Enclosed are results of analyses for samples received by the laboratory on June 21, 2013. If you have any questions concerning this report, please feel free to contact me. Sincerely, �� �'V;��� Lisa A. Worthington Project Manager Page 1 of 15 13FO722 1 Contest Final 06 24 13 1659 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Falcon Engineering REPORT DATE: 6/24/2013 1210 Trinity Road, Suite 110 Raleigh, NC 27607 PURCHASE ORDER NUMBER: ATTN: Josh Dunbar PROJECT NUMBER: E13026 ANALYTICAL SUMMARY WORK ORDER NUMBER: 13FO722 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: 828 MLK, Chapel Hill FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB Well #1 13FO722-01 Ground Water Bolin Creek 13FO722-02 Ground Water SW-846 6010C SW-846 6020A SW-846 7470A SW-846 6010C SW-846 6020A SW-846 7470A Page 2 of 15 13FO722 1 Contest Final 06 24 13 1659 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. SW-846 6020A Qualifications Duplicate relative percent difference (RPD) is a less useful indicator of sample precision for sample results that are <5 times the reporting limit (RL). Analyte & Samples(s) Qualified: Zinc B075429-DUP1 The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. ,in 6"4�� Michael A. Erickson Laboratory Director Page 3 of 15 13FO722 1 Contest Final 06 24 13 1659 icon-te w ANALYTICAL LABORATORY Project Location: 828 MILK, Chapel Hill Date Received: 6/21/2013 Field Sample #: Well #1 Samnle ID: 13FO722-01 Samnle Matrix: Ground Water 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Sample Description: Start Date/Time: 6/20/2013 11:15:OOAM Stop Date/Time: 6/20/2013 11:25:OOAM Work Order: 13FO722 Metals Analyses (Total) Date Date/Time Analyte Results RL DL Units Dilution Flag Method Prepared Analyzed Analyst Aluminum 16 0.050 0.026 mg/L 1 SW-846 6010C 6/21/13 6/24/13 10:45 OP Antimony 0.61 2.0 0.30 µg/L 2 J SW-846 6020A 6/21/13 6/24/13 12:15 KSH Arsenic 8.3 0.80 0.70 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:15 KSH Barium 1100 200 24 µg/L 20 SW-846 6020A 6/21/13 6/24/13 12:24 KSH Beryllium 5.5 0.80 0.15 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:15 KSH Cadmium 0.93 1.0 0.059 µg/L 2 J SW-846 6020A 6/21/13 6/24/13 12:15 KSH Calcium 260 0.15 0.088 mg/L 1 SW-846 6010C 6/21/13 6/24/13 10:45 OP Chromium 8.4 2.0 1.3 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:15 KSH Cobalt 23 2.0 0.067 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:15 KSH Copper 1200 100 1.6 µg/L 20 SW-846 6020A 6/21/13 6/24/13 12:24 KSH Iron 13 0.050 0.026 mg/L 1 SW-846 6010C 6/21/13 6/24/13 10:45 OP Lead 27 2.0 0.12 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:15 KSH Magnesium 47 0.15 0.037 mg/L 1 SW-846 6010C 6/21/13 6/24/13 10:45 OP Manganese 1200 20 2.0 µg/L 20 SW-846 6020A 6/21/13 6/24/13 12:24 KSH Mercury 0.00018 0.00010 0.000048 m9/1- 1 SW-846 7470A 6/21/13 6/24/13 12:19 SAJ Nickel 70 10 0.13 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:15 KSH Potassium 42 2.0 0.46 mg/L 1 SW-846 6010C 6/21/13 6/24/13 10:45 OP Selenium 18 10 1.5 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:15 KSH Silver 0.27 LO 0.13 µg/L 2 J SW-846 6020A 6/21/13 6/24/13 12:15 KSH Sodium 52 2.0 1.9 mg/L 1 SW-846 6010C 6/21/13 6/24/13 10:45 OP Thallium 0.48 0.40 0.073 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:15 KSH Vanadium 71 10 1.1 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:15 KSH Zinc 2200 200 39 µg/L 20 SW-846 6020A 6/21/13 6/24/13 12:24 KSH Page 4 of 15 13FO722 1 Contest Final 06 24 13 1659 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 828 MILK, Chapel Hill Sample Description: Work Order: 13FO722 Date Received: 6/21/2013 Field Sample #: Bolin Creek Sampled: 6/20/2013 11:50 Samnle ID: 13FO722-02 Samnle Matrix: Ground Water Analyte Results RL DL Metals Analyses (Total) Units Dilution Flag Method Date Prepared Date/Time Analyzed Analyst Aluminum 0.29 0.050 0.026 mg/L 1 SW-846 6010C 6/21/13 6/24/13 11:02 OP Antimony ND 2.0 0.30 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Arsenic 0.90 0.80 0.70 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Barium 27 20 2.4 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Beryllium ND 0.80 0.15 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Cadmium ND 1.0 0.059 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Calcium 16 0.15 0.088 mg/L 1 SW-846 6010C 6/21/13 6/24/13 11:02 OP Chromium ND 2.0 1.3 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Cobalt 0.37 2.0 0.067 µg/L 2 J SW-846 6020A 6/21/13 6/24/13 12:09 KSH Copper 2.6 10 0.16 µg/L 2 J SW-846 6020A 6/21/13 6/24/13 12:09 KSH Iron 0.86 0.050 0.026 mg/L 1 SW-846 6010C 6/21/13 6/24/13 11:02 OP Lead 0.50 2.0 0.12 µg/L 2 J SW-846 6020A 6/21/13 6/24/13 12:09 KSH Magnesium 5.3 0.15 0.037 mg/L 1 SW-846 6010C 6/21/13 6/24/13 11:02 OP Manganese 100 2.0 0.20 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Mercury ND 0.00010 0.000048 mg/L 1 SW-846 7470A 6/21/13 6/24/13 12:20 SAJ Nickel 1.2 10 0.13 µg/L 2 J SW-846 6020A 6/21/13 6/24/13 12:09 KSH Potassium 2.3 2.0 0.46 mg/L 1 SW-846 6010C 6/21/13 6/24/13 11:02 OP Selenium ND 10 1.5 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Silver ND LO 0.13 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Sodium 7.8 2.0 1.9 mg/L 1 SW-846 6010C 6/21/13 6/24/13 11:02 OP Thallium ND 0.40 0.073 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Vanadium ND 10 1.1 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Zinc 45 20 3.9 µg/L 2 SW-846 6020A 6/21/13 6/24/13 12:09 KSH Page 5 of 15 13FO722 1 Contest Final 06 24 13 1659 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: SW-846 3005A-SW-846 6010C Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 13FO722-01 [Well #1] B075426 50.0 50.0 06/21/13 13FO722-02 [Bolin Creek] B075426 50.0 50.0 06/21/13 Prep Method: SW-846 3005A-SW-846 6020A Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 13FO722-01 [Well #1] B075429 50.0 50.0 06/21/13 13FO722-02 [Bolin Creek] B075429 50.0 50.0 06/21/13 Prep Method: SW-846 7470A Prep-SW-846 7470A Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 13FO722-01 [Well #1] B075437 6.00 6.00 06/21/13 13FO722-02 [Bolin Creek] B075437 6.00 6.00 06/21/13 Page 6 of 15 13FO722 1 Contest Final 06 24 13 1659 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Metals Analyses (Total) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B075426 - SW-846 3005A Blank (B075426-BLK1) Prepared: 06/21/13 Analyzed: 06/24/13 Aluminum ND 0.050 mg/L Calcium ND 0.15 mg/L Iron ND 0.050 mg/L Magnesium ND 0.15 mg/L Potassium ND 2.0 mg/L Sodium ND 2.0 mg/L LCS (B075426-BS2) Prepared: 06/21/13 Analyzed: 06/24/13 Aluminum 2.08 0.050 mg/L 2.00 104 80-120 Calcium 2.11 0.15 mg/L 2.00 106 80-120 Iron 2.05 0.050 mg/L 2.00 102 80-120 Magnesium 2.12 0.15 mg/L 2.00 106 80-120 Potassium 20.2 2.0 mg/L 20.0 101 80-120 Sodium 2.05 2.0 mg/L 2.00 103 80-120 LCS Dup (B075426-BSD2) Prepared: 06/21/13 Analyzed: 06/24/13 Aluminum 2.03 0.050 mg/L 2.00 101 80-120 2.54 20 Calcium 2.06 0.15 mg/L 2.00 103 80-120 2.58 20 Iron 2.01 0.050 mg/L 2.00 101 80-120 1.72 20 Magnesium 2.07 0.15 mg/L 2.00 104 80-120 2.16 20 Potassium 19.7 2.0 mg/L 20.0 98.6 80-120 2.22 20 Sodium 2.01 2.0 mg/L 2.00 101 80-120 2.16 20 Batch B075429 - SW-846 3005A Blank (B075429-BLK1) Prepared: 06/21/13 Analyzed: 06/24/13 Antimony ND 2.0 µg/L Arsenic ND 0.80 µg/L Barium ND 20 µg/L Beryllium ND 0.80 µg/L Cadmium ND 1.0 µg/L Chromium ND 2.0 µg/L Cobalt ND 2.0 µg/L Copper ND 10 µg/L Lead ND 2.0 µg/L Manganese ND 2.0 µg/L Nickel ND 10 µg/L Selenium ND 10 µg/L Silver ND 1.0 µg/L Thallium ND 0.40 µg/L Vanadium ND 10 µg/L Zinc ND 20 µg/L Page 7 of 15 13FO722 1 Contest Final 06 24 13 1659 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Metals Analyses (Total) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B075429 - SW-846 3005A LCS (B075429-BSI) Prepared: 06/21/13 Analyzed: 06/24/13 Antimony 279 5.0 µg/L 250 112 80-120 Arsenic 270 2.0 µg/L 250 108 80-120 Barium 269 50 µg/L 250 108 80-120 Beryllium 270 2.0 µg/L 250 108 80-120 Cadmium 279 2.5 µg/L 250 112 80-120 Chromium 267 5.0 µg/L 250 107 80-120 Cobalt 262 5.0 µg/L 250 105 80-120 Copper 269 25 µg/L 250 108 80-120 Lead 278 5.0 µg/L 250 ill 80-120 Manganese 260 5.0 µg/L 250 104 80-120 Nickel 264 25 µg/L 250 105 80-120 Selenium 272 25 µg/L 250 109 80-120 Silver 284 2.5 µg/L 250 114 80-120 Thallium 258 1.0 µg/L 250 103 80-120 Vanadium 264 25 µg/L 250 106 80-120 Zinc 279 50 µg/L 250 112 80-120 LCS Dup (B075429-BSD1) Prepared: 06/21/13 Analyzed: 06/24/13 Antimony 232 5.0 µg/L 250 101 80-120 10.0 20 Arsenic 245 2.0 µg/L 250 98.2 80-120 9.57 20 Barium 245 50 µg/L 250 98.0 80-120 9.21 20 Beryllium 244 2.0 µg/L 250 97.8 80-120 9.87 20 Cadmium 252 2.5 µg/L 250 101 80-120 10.2 20 Chromium 247 5.0 µg/L 250 98.7 80-120 7.98 20 Cobalt 244 5.0 µg/L 250 97.5 80-120 7.06 20 Copper 252 25 µg/L 250 101 80-120 6.57 20 Lead 251 5.0 µg/L 250 100 80-120 10.1 20 Manganese 243 5.0 µg/L 250 97.2 80-120 6.78 20 Nickel 247 25 µg/L 250 99.0 80-120 6.37 20 Selenium 251 25 µg/L 250 100 80-120 8.23 20 Silver 234 2.5 µg/L 250 102 80-120 11.0 20 Thallium 233 1.0 µg/L 250 93.2 80-120 10.3 20 Vanadium 240 25 µg/L 250 96.1 80-120 9.53 20 Zinc 237 50 µg/L 250 103 80-120 8.13 20 Duplicate (B075429-DUPl) Source: 13FO722-02 Prepared: 06/21/13 Analyzed: 06/24/13 Antimony ND 2.0 µg/L Arsenic 0.827 0.80 µg/L Barium 27.9 20 µg/L Beryllium ND 0.80 µg/L Cadmium ND 1.0 µg/L Chromium ND 2.0 µg/L Cobalt 0.359 2.0 µg/L Copper 2.57 10 µg/L Lead 0.483 2.0 µg/L Manganese 99.9 2.0 µg/L Nickel 1.03 10 µg/L Selenium ND 10 µg/L Silver ND 1.0 µg/L Thallium ND 0.40 µg/L Vanadium ND 10 µg/L Zinc 7.86 20 µg/L ND NC 20 0.904 8.94 20 26.9 3.61 20 ND NC 20 ND NC 20 ND NC 20 0.367 2.22 20 J 2.59 0.793 20 1 0.501 3.55 20 J 102 1.74 20 1.18 14.0 20 1 ND NC 20 ND NC 20 ND NC 20 ND NC 20 45.3 141 * 20 R-04,1 Page 8 of 15 13FO722 1 Contest Final 06 24 13 1659 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Metals Analyses (Total) - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B075429 - SW-846 3005A Matrix Spike (B075429-MS1) Source: 13FO722-02 Prepared: 06/21/13 Analyzed: 06/24/13 Antimony 247 5.0 µg/L 250 ND 103 75-125 Arsenic 293 2.0 µg/L 250 0.904 101 75-125 Barium 272 50 µg/L 250 26.9 97.9 75-125 Beryllium 248 2.0 µg/L 250 ND 99.1 75-125 Cadmium 252 2.5 µg/L 250 ND 101 75-125 Chromium 246 5.0 µg/L 250 ND 98.2 75-125 Cobalt 243 5.0 µg/L 250 0.367 96.9 75-125 Copper 248 25 µg/L 250 2.59 98.0 75-125 Lead 255 5.0 µg/L 250 0.501 102 75-125 Manganese 359 5.0 µg/L 250 102 103 75-125 Nickel 242 25 µg/L 250 1.18 96.4 75-125 Selenium 233 25 µg/L 250 ND 101 75-125 Silver 240 2.5 µg/L 250 ND 99.9 75-125 Thallium 234 1.0 µg/L 250 ND 93.7 75-125 Vanadium 245 25 µg/L 250 ND 98.1 75-125 Zinc 261 50 µg/L 250 45.3 86.4 75-125 Batch B075437 - SW-846 7470A Prep Blank (B075437-BLKI) Prepared: 06/21/13 Analyzed: 06/24/13 Mercury ND 0.00010 mg/L LCS (B075437-BSI) Prepared: 06/21/13 Analyzed: 06/24/13 Mercury 0.00198 0.00010 mg/L 0.00200 99.2 80-120 LCS Dup (B075437-BSD1) Prepared: 06/21/13 Analyzed: 06/24/13 Mercury 0.00201 0.00010 mg/L 0.00200 100 80-120 1.15 20 Page 9 of 15 13FO722 1 Contest Final 06 24 13 1659 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). R-04 Duplicate relative percent difference (RPD) is a less useful indicator of sample precision for sample results that are <5 times the reporting limit (RL). Page 10 of 15 13FO722 1 Contest Final 06 24 13 1659 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 6010C in Water Aluminum CT,NH,NY,ME,VA Calcium CT,NH,NY,ME,NC,VA Iron CT,NH,NY,ME,NC,VA Magnesium CT,NH,NY,ME,NC,VA Potassium CT,NH,NY,ME,NC,VA Sodium CT,NH,NY,ME,NC,VA SW-846 6020A in Water Antimony CT,NH,NY,NC,ME,VA Arsenic CT,NH,NY,NC,ME,VA Barium CT,NH,NY,NC,ME,VA Beryllium CT,NH,NY,NC,ME,VA Cadmium CT,NH,NY,RI,NC,ME,VA Chromium CT,NH,NY,NC,ME,VA Cobalt CT,NH,NY,NC,ME,VA Copper CT,NH,NY,NC,ME,VA Lead CT,NH,NY,NC,ME,VA Manganese CT,NH,NY,NC,ME,VA Nickel CT,NH,NY,NC,ME,VA Selenium CT,NH,NY,NC,ME,VA Silver CT,NH,NY,NC,ME,VA Thallium CT,NH,NY,NC,ME,VA Vanadium CT,NC,NH,NY,ME,VA Zinc CT,NH,NY,NC,ME,VA SW-846 7470A in Water Mercury CT,NH,NY,NC,ME,VA The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC 100033 02/1/2014 MA Massachusetts DEP M-MA100 06/30/2013 CT Connecticut Department of Publilc Health PH-0567 09/30/2013 NY New York State Department of Health 10899 NELAP 04/1/2014 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2014 RI Rhode Island Department of Health LA000112 12/30/2013 NC North Carolina Div. of Water Quality 652 12/31/2013 NJ New Jersey DEP MA007 NELAP 06/30/2013 FL Florida Department of Health E871027 NELAP 06/30/2014 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2013 WA State of Washington Department of Ecology C2065 02/23/2014 ME State of Maine 2011028 06/9/2015 VA Commonwealth of Virginia 460217 12/14/2013 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2012 Page 11 of 15 13FO722 1 Contest Final 06 24 13 1659 c z z a O c z v K a F. I 0 000 'S N I S � N A � I C F.a N l.n v j ' v v C O A A < 2 I m _ � 0 0 0-0 o O N G) S Ev z 'o : fD = €0 ID CL ACC, 10 OOO 0 r 0 0 rD o � .�i O 00 qr AaN WO O i = 7 R T Q O1 W m r n w m F" M = S n D fD = = D (D Q Q (D (' IZ D m o� 7 01 w ID ID _. 1 7 0 fD � � o o m rD n 7 1 m a o n 3 N � z a) 3 � D z >0 °1Ion !' r L D �� W r O t � n IA OW 1 O v S m 3 v 1 = x 0 50~ p {Y A 0O 0 N W p (!( yl ry A A {n O 01 01 N N N n � � 3 3 M o m 0 0 'a K n S O u 7 U (D "7 a 00 O D O c r (dry _0 m T R9 Q _ _ s m n - WQ v i d Q of a. m -p 'o ` O n ID X � (� n 0 c n � rD � O-Ix wv,Z=— II II II II II 11 II II if S a M r N (D S .0 C n S o n 3 C) D d d M0 cr D 0. a o C 0 (D rD m i W y 0 D O (D cc: < (D oa n °° m °N pa N ry Paqe 12 of 15 13FO722 1 Con 00 ° ci aD tr D ^ 0 ° o rD T3 rD j m N o n ,y 0 a � ;t Final 06 24 13 1659 6/21113 Sh:p (P IU) data Thur 6/20/2013 4:29 pm RAL US Travel History ADaterrime Activity - 6/21/2013 - Friday 9:14 am Delivered 8:08 am On FerlExvehicle for delivery 7:34 am Al local FedExfacilily 6:15 am At destination sort facility 4:39 am Departed FedExIoGation 12:20 am Arrived at FedEx location - 6/20/2013 - Thursday 8:50 pm Left FedExorigin facility 4:29 pm Picked up Tendered at FedEx0f ice Shipment Facts Tracking number Weight Delivered To Total shipment Weight Packaging 803285755115 32lbs Receptionist/Front Desk 32 Ibs 114.5 kgs Your Packaging Location AAA WINDSOR LOCKS, CT WINDSOR LUCKS, CT EAST GRANBY, CT INDIANAPOLIS, IN INDIANAPOLIS, IN RALFIGH. NC RALEIGH, NC Local Scan Time Service FedEx Priority Overnight Dimensions 23xl3x16 in: Total pieces 1 Shipper reference 80 Special handling Deliver Weekday. Additional section Handlino Surrharoe Page 13 of 15 13FO722 1 Contest —Final 06 24 13 1659 https:/A vw.fedexcom/fedextrack/iridexhtml?tracknumbers=803285755115&cntry_Poae=us Chris Collins From: Lisa Worthington[lisa.worthington@contestlabs.com] Sent: Thursday, June 20, 2013 3:37 PM To: Login@ContestLabs.com'; 'Chris Collins'; 'Andrea Palpini' Subject: FW: Falcon 24hr TAT COC Attachments: photo.JPG; ATT00295.txt This is arriving tomorrow. Please use 6J21 as the receipt date and log in for a 1 day TAT. The metals list he needs is the TAL 23 list. Thanks -----Original Message ----- From: Tiffany Butz[mailto:tiffany.butz(@contestlabs.com] Sent: Thursday, June 20, 2013 3:31 PM To: Lisa Worthington Subject: Falcon 24hr TAT COC 1 Page 14 of 15 13FO722 1 Contest Final 06 24 13 1659 39 Spruce St. East Longmeadow, MA. 01028 P: 413-525-2332 F:413-525-6405 www.contestiabs.com CLIENT NAME: C -tE to ANALYTICAL LABORATORY Sample Receipt Checkli RECEIVED BY: 1) Was the chain(s) of custody relinquished and signed? 2) Does the chain agree with the samples? If not, explain: 3) Are all the samples in good condition? If not, explain: 4) How were the samples received: On Ice ;E35 Direct from Sampling ❑ Ambient ❑ Were the samples received in Temperature Compliance of (2-60C)? Temperature °C by Temp blank 13 DATE:ko . p1.1 Ye No No CoC Included Ye No In Cooler(s) Ye No N/A Temperature °C by Temp gun Y• / 5) Are there Dissolved samples for the lab to filter? Yes NN Who was notified Date Time 6) Are there any RUSH or SHORT HOLDING TIME samples? Yes I Who was notified Date Time Permission to subcontract samples? Yes No 7) Location where samples are stored: (Walk-in clients only) if not already approved Client Signature: 8) Do all samples have the proper Acid pH: Y No N/A 9) Do all samples have the proper Base pH: Yes No I/ 10) Was the PC notified of any discrepancies with the CoC vs the samples: Yes No N�/ Containers received at Con -Test # of containers # of containers 1 Liter Amber 8 oz amber/clear jar 500 mL Amber 4 oz amber/clear jar 250 mL Amber 8oz amber 2 oz amber/clear 'ar 1 Liter Plastic Air Cassette 500 mL Plastic H /Ho calite Tube 250 mL plastic Plastic Bag / Zi loc 40 mL Vial - type listed below PM 2.5 / PM 10 Colisure / bacteria bottle Yam" PUF Cartridge Dissolved Oxygen bottle SOC Kit Encore TO-17 Tubes Flashpoint bottle Non-ConTest Container Perchlorate Kit ="' Other glass jar Other F, , Other Laboratory Commentsf Re�Q;y¢ l '14S p� Well $ eA eX W 'RO�a ; S -1S 'r) I 40 mL vials: # HCI Doe# 2�7 : >: # Bisulfate kev::3aViay:20t :::::::::::::> # Thlosulfate # Methanol # DI Water Time and Date Frozen: Unpresery Page 15 of 15 13FO722 1 Contest Final 06 24 13 1659 kPPENDIX F RESUMES OF ENVIRONMENTAL PROFESSIONALS JOSHUA D. DUNBAR, PE Josh is a registered Professional Engineer (PE) in the State of North Carolina who has over 14 years experience in a variety of consulting and engineering applications. This includes project management and technical experience in environmental due diligence, indoor air quality investigations, multi -media environmental assessments, air quality permitting and dispersion modeling, emission inventories, regulatory compliance support, hazardous waste management, pollution control/prevention projects, preliminary engineering design specifications, and evaluation of various control technologies. Josh has conducted a variety of environmental due diligence assessments, which have included Phase I and Phase II ESAs, UST Closure Assessments, Limited Site Assessments, and Environmental compliance audits. He has also assisted clients in obtaining permits to construct and operate air emission sources at major (Title V/PSD) and minor industrial facilities. He has managed and performed air dispersion modeling efforts for air toxics impact and risk assessment purposes. Through these efforts he has successfully assisted numerous clients in complying with complex environmental regulations. In the area of waste management, Josh has managed efforts in assessment and remediation projects involving leaking underground petroleum storage tanks and above ground chemical storage tanks. He has also managed and assisted in efforts to remove Underground Storage Tanks (UST) and perform integrity testing of Aboveground Storage Tank (AST) as part of the Resource Conservation and Recovery Act (RCRA) requirements. Josh has performed Phase I and Phase II environmental site assessments of commercial, residential, and industrial properties in accordance with various ASTM standards, as well as US EPA's All Appropriate Inquiries (AAI) Rule. Facility compliance audits have included a review of multi -media environmental programs, an evaluation of exceptions found, and development of recommendations for achieving compliance. In the area of compliance assistance, Josh has satisfied the various recordkeeping and reporting requirements associated with Federal and State regulatory programs including SARA Title III/EPCRA, NSPS, NESHAP/MACT, and State VOC and air toxics rules. He has assisted clients in documentation and preparing Title V compliance certifications. As part of these efforts, Josh has been responsible for the development and design of several emission/permit environmental tracking systems that have been used to comply with extensive recordkeeping and reporting requirements. Josh has prepared test plans and managed stack testing efforts in conjunction with NESHAP and NSPS applicability assessment for various industries. Josh has prepared applications and obtained construction and operating permits for various industries including cement, chemical, personal hygiene products, wood products, construction products (i.e., aggregates, ready mix concrete, and asphalt), and waste management facilities. He has participated in several successful Prevention of Significant Deterioration (PSD) and PSD avoidance projects. He has conducted permitting projects for major industrial facility modifications and prepared Title V and synthetic minor permit applications in various States. In association with permitting efforts, he has conducted dispersion modeling projects for 1 F-2 JOSHUA D. DUNBAR, PE (CONTINUED) demonstration of compliance with National Ambient Air Quality Standards (NAAQS), PSD increments, and State air toxics standards. In the area of water pollution prevention and control, Josh has conducted wastewater discharge compliance investigations and storm water evaluations at multiple industrial facilities. These efforts have included managing and assisting in the site design and layout to comply with National Pollution Discharge Elimination Systems (NPDES) permitting requirements for numerous sites. He has assisted in preparing spill prevention, control, and countermeasure (SPCC) plans and oil discharge contingency plans under Federal and State requirements for oil and chemical storage facilities. He has also prepared storm water pollution prevention plans (SWP3) for a number of facilities. Josh is also experienced in the field of Indoor Air Quality Assessments. He has conducted numerous microbial assessments that involved the identification and recommendations regarding the presence of such molds as Stachybotrys, Apergillius and Penicillium. These assessments were used to improve and identify concerned areas with regard to the Indoor Air Quality within occupied buildings. Assessments have included both commercial and residential properties. Josh has also assisted in the performance assessment of HVAC systems with regard to adequate Indoor Air Quality as described in ASHRAE Standards 62 and overall occupant thermal comfort as outlined in ASHRAE Standard 55. In addition to microbial and HVAC assessments, Josh has assisted in the sampling efforts for the identification of Asbestos containing material used in indoor environments. Josh is an Accredited Asbestos Inspector and Management Planner. He has also been trained in the use and implementation of lead inspections within buildings using portable XRF instrumentation. EDUCATION B.S. I Mechanical Engineering I North Carolina State University 1 1999 Graphic Communications I North Carolina State University 1 1999 REGISTRATION AND CERTIFICATIONS Professional Engineer (PE), North Carolina Board of Examiners (036969) OSHA 40-hour HAZWOPER Training Hazardous Waste Site Supervisor Training Permit -Required Confined Space Training AHERA Building Inspector (Accreditation # 12060) AHERA Management Planner (Accreditation # 20900) Certified Environmental Inspector, Environmental Assessment Association F-3 ARIC GEDA, PE Aric is not only a professional engineer, but also a licensed builder with over 26 years of experience. His extensive breadth of experience includes the fields of Special Inspections, materials testing, environmental, geotechnical, and facilities engineering. With this broad based knowledge, Aric is an ideal point of contact for projects requiring several consulting service lines. As Construction Services Manager, Aric's primary responsibilities include the growth and management of the overall construction materials testing and inspections program, which includes supervising a staff consisting of expert project managers, technicians, inspectors, and laboratory technicians. Aric enjoys a special involvement in the Economic Development of North Carolina. Aric is an active member and participant in numerous Economic Development Groups including NCEDA, Research Triangle Partnership, Pitt County Committee of 100, North Carolina's Northeast Commission, the Kerr Tar Regional Council of Governments, the Upper Coastal Plain Regional Council of Governments, along with the Raleigh and Durham Chambers. Aric has established numerous relationships with private Economic Development consulitng firms and County Economic Developers across the region providing consulting services in support of Economic Development. EDUCATION B.S., Geological Engineering I Michigan Technological University 1 1987 Professional Engineer North Carolina 1 035138 Professional Engineer Michigan 1 39843 Licensed Builder I Michigan ASTM Technical and Professional Risk -Based Corrective Action Certification SPECIAL TALENTS Aric has become heavily involved in the NC Department of Commerce Certified Sites Program. Aric has been involved with Environmental, Wetland, NEPA, and Geotechnical consulting and engineering on 18 Site Certifications across the region. Due to his extensive experience with the program, Aric was appointed as a technical advisor to the Certified Sites Steering Committee by Secretary Crisco and is currently serving a minimum two year term that started in September 2010. SPOTLIGHT PROJECT Selma Crossings Certified Rail Site I Selma, NC Selma Crossings is a 163 acre site that has successfully gone through the 32 step process of the Department of Commerce's Certified Sites Program. The Site is the only "Dual Rail" Certified Site, having a Rail Crossing bounding the Northern and Western Boundaries in addition to extensive 1-95 frontage along the southern boundary. Aric teamed with representatives of Sanford Holshouser, CSX, and Norfolk Southern, providing Environmental, Wetland, NEPA, Geotechnical, and Planning services for the proposed project. This challenging project took over 2 years to complete, with Secretary Crisco presenting Site Certification to Selma Town Council in March of 2012. 1 F-4