7401_PittCounty_SouthernUnit_MSWLF_Jan22GW_FID1664420_20220413

ectronic Data - Email CD (data loaded: Yes / No ) Doc/Event #:
NC DENR I I Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
• Prepare one form for each individually monitored unit.
• Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
• Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 136 .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Groundwater Management Associates, Inc.
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Emma H. Shipley, P.G. Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Southern Unit of the Pitt County 3025 Landfill Road 74-01 .1600 January 25-26, 2022
Municipal Solid Waste Landfill Greenville, NC 27834
Environmental Status: (Check all that apply)
Initial/Background Monitoring Detection Monitoring ❑X Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑
Groundwater monitoring data from private water supply wells
Leachate monitoring data El
water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
)( Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Emma H. Shipley, P.G. Project Hydrogeologist 252-758-3310
Facility Representative Name (Print) Title (Area Code) Telephone Number
4/12/2022
Signature I k Date
4300 Sapphire Court, Suite 100, Greenville, NC 27834
Facility Representative Address
Affix NC Liceo0OWMI! p� 'Geologist Seal
p°tit •`'
�.'NSF©•.'
C-121 (PG Firm License Number)
NC PE Firm License Number (if applicable effective May 1, 2009)
o— A-4 ailnno

Compounds Detected At or Above Groundwater or Surface Water Standards during the January 2022 Sampling
Event (1/25-26/2022) - Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well ID
Date
Parameter
Results
(N9/L)
MDL
(N9/L)
NC 2L or
2B Std*
L
IMAC
(N9/L)
MCL
(N9/L)
Groundwater Samples
MW6R
1/25/2022
1,4-Dioxane
6.7
0.8
3
-
1/26/2022
Barium Total
1950
1.1
700
-
2000
1/26/2022
Cobalt Total
10.2
1.4
-
1
-
P11R
1/26/2022
Vanadium Total
3.381
1.4
-
0.3
-
1/25/2022
1,4-Dioxane
78
0.8
3
-
-
1/26/2022
Barium Total
1010
1.1
700
-
2000
P16R
1/25/2022
Benzene
2.4
0.15
1
-
5
1/26/2022
Cobalt Total
2.621
1.4
-
1
-
1/26/2022
1,4-Dioxane
4.8
0.8
3
-
-
P17
1/26/2022
Vanadium Total
3.613
1.4
-
0.3
-
1/25/2022
1,4-Dioxane
180 D
4.0
3
-
-
1/26/2022
Barium Total
1500
1.10
700
-
2000
P19
1/25/2022
Benzene
3.4
0.15
1
-
5
1/26/2022
Beryllium Total
12.5
0.16
-
4
4
1/26/2022
Cobalt Total
16.2
1.40
-
1
-
1/25/2022
1,4-Dioxane
62
0.8
3
-
-
P20R
1/25/2022
Benzene
1.3
0.15
1
-
5
1/26/2022
Barium Total
887
1.1
700
-
2000
1/26/2022
Cobalt Total
2.061
1.40
-
1
-
P20D
1/26/2022
Vanadium Total
3.663
1.4
-
0.3
-
1/26/2022
Cobalt Total
3.40 ]
1.40
-
1
P28
1/26/2022
Vanadium Total
4.611
1.4
-
0.3
-
1/25/2022
1,4-Dioxane
180 D
4.0
3
-
-
P29
1/25/2022
Benzene Total
2.0
0.15
1
-
5
1/26/2022
Vanadium Total
1 9.151
1 1.4
-
0.3
-
Surface Water Samp/es
SWi
1/26/2022
Cobalt Total
8.633
1.4
4
-
1/26/2022
Lead
3.533
3.1
0.54"
-
-
MDL = Method Detection Limit MCL = Federal Maximum Contaminant Level
IMAC = Interim Maximum Allowable Concentration
I = The analyte was positively identified, but the value is estimated below the reporting limit.
*15A NCAC 2L groundwater standards are listed for all groundwater sampling locations. 15A NCAC 2B standards are listed
for surface water sampling locations (SW1 and SW2).
Value represents an EPA action level.
#Value represents an EPA secondary Maximum Contaminant Level
+NC Protective Value for Surface Waters
Concentrations highlighted i yellow v were detected above the 2L (or 2B) standards.
Concentrations highlighted i orange a were detected above the IMAC.
Page 1 of 2

Compounds Detected At or Above Groundwater or Surface Water Standards during the January 2022 Sampling
Event (1/25-26/2022) - Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Preliminary analysis of cause and significance of concentrations detected at or above
groundwater or surface water standards:
1,4-Dioxane, barium, and benezene were detected at concentrations exceeding the 15A NCAC 02L
groundwater standards in monitoring wells for the Southern Unit. None of these constituents, however, were
detected at concentrations above state standards in groundwater samples collected from just below the
southern property ditch (which generally acts as a local groundwater discharge feature) or in the
downgradient surface -water sample. Pitt County is currently monitoring to assess the effectiveness of the
extensive cap and stormwater upgrades completed at the Southern Unit in June 2021. A reversal of
groundwater flow direction at well P16R during this monitoring event may represent the first indication of
hydraulic improvements resulting from the repairs. In accordance with the approved Pilot Study, the County
plans to monitoring until at least July 2022 before making a full assessment of improvements.
Page 2 of 2

PILOT STUDY UPDATE AND
JANUARY 2022 SEMI-ANNUAL WATER
QUALITY MONITORING EVENT
SOUTHERN PORTION OF THE
PITT COUNTY SOLID WASTE
MUNICIPAL LANDFILL
(FACILITY PERMIT # 74-01)
GREENVILLE, PITT COUNTY
PREPARED FOR
MR. TI M CORLEY, PE
ENGINEERING DEPARTMENT
PITT COUNTY
1717 WEST ST11 STREET
GREENVILLE, NC 27834
PREPARED BY
GROUNDWATER MANAGEMENT
ASSOCIATES, INC. (GMA)
4300 SAPPHIRE CT., SUITE 100
GREENVILLE, NORTH CAROLINA 27834
TELEPHONE: [phone]
APRIL 12, 2022
North Carolina Corporate Engineering License (GMA - Apex, NC) #: C-0854
North Carolina Corporate Geology Licen5e {GMA - Greenville & Apex, NC) 4: C-121

TABLE OF CONTENTS
1.0 INTRODUCTION..................................................................................... 1
1.1 Site Background.................................................................................. 2
1.2 Physical Setting and Hydrogeology..................................................... 2
1.3 Contaminants of Concern and Site Regulatory Status ........................ 3
2.0 1,4-DIOXANE ASSESSMENT AND PILOT STUDY UPDATEError! Bookmark not
defined.
3.0 JANUARY 2022 SEMI-ANNUAL MONITORING EVENT ............................ 7
3.1 Groundwater Hydrology.................................................................... 8
3.2 Sample Collection and Analyses........................................................ 9
3.3 Analytical Results and Discussion...................................................... 9
4.0 CONCLUSIONS AND FUTURE WORK .................................................... 11
5.0 REPORT CERTIFICATION..................................................................... 12
6.0 REFERENCES........................................................................................13
FIGURES
1. Site Layout and Existing Monitoring Network
2. Groundwater and Surface Water Sampling Locations - Southern Unit
3. Equipotential Map, January 25, 2022
TABLES
1. Monitoring Well Construction and Elevations
2. Monitoring Well Water Levels and Sample Purge Volumes
3. Staff Gauge Elevations and Water Levels
4. Calculations of Groundwater Velocity
5. Field -Water Quality Parameters
6. Appendix I Target Parameters
7. List of Compounds Detected during the January 2022 Sampling Event

APPENDICES
Correspondence from the NC Division of Waste Management
Sampling Records
Laboratory Report and Chain -of -Custody Forms for Water Samples

1.0 INTRODUCTION
The inactive Pitt County Solid Waste Municipal Landfill (Facility Permit #74-01, Figure 1) is
comprised of a Northern Unit that closed in 1990 and a Southern Unit that reached capacity and
closed in 1995. Based on its closure date, the Southern Unit is subject to the September 1993
rules for municipal solid waste landfills (15A NCAC 13B .1600). The Northern Unit, on the other
hand, is subject to the conditions of the solid waste permit and 15A NCAC 13B .0500.
Pitt County (the County) is currently working to address 1,4-dioxane and benzene groundwater
contamination at the Southern Unit of the inactive Pitt County Solid Waste Municipal Landfill
(Facility Permit #74-01, Figure 1). In 2017, the County confirmed slight exceedances of the NC
Groundwater Quality Standard (NCAC 02L) for benzene in two groundwater samples collected
from the landfill's monitoring well network. Exceedances of the NCAC 02L groundwater
standard for 1,4-dioxane were confirmed in January 2019. Testing for 1,4-dioxane began in
response to a May 2018 directive from the North Carolina Department of Environmental Quality
(NCDEQ), Division of Waste Management (DWM), Solid Waste Section (SWS) that required all
North Carolina landfills to begin testing for the constituent as part of their routine groundwater
monitoring (Appendix A).
Groundwater contamination at the facility is believed to be related to the degradation of the
low -permeability, clay caps that cover each unit. Over time, erosion of the caps, as well as
cracking due to heating/cooling, desiccation, and/or subsidence due to decomposition of fill
material, increases the permeability of these barriers and allows infiltration of water that can
leach contaminants downward into the underlying groundwater.
Following approval from the SWS, the County has collected groundwater samples from just
beneath the southern ditch to monitor the extent of 1,4-dioxane and benzene contamination at
the facility. This ditch serves as a groundwater discharge location for the Southern Unit. To
date, 1,4-dioxane and benzene have not been detected in exceedance of the NCAC 02L
standards in these samples, which suggests that 1,4-dioxane and benzene contamination above
the NCAC 02L groundwater standard does not extend off the facility property.
On November 4, 2020, the County began construction on an extensive cap and a stormwater
system repair and upgrade project at the Southern Unit as part of an approved pilot study for
corrective action (Appendix A). These improvements are designed to greatly reduce the
infiltration of water through the cap in order to protect the groundwater from further
contamination via leaching from landfill waste. The County completed construction on
this $1.065 million project in June of 2021. The County continues to monitor groundwater and
surface water at the Southern Unit on a semi-annual schedule. The remainder of this report
presents the results of the January 2022 semi-annual monitoring event and provides an update
of the ongoing pilot study at the Southern Unit of the Pitt County Landfill.

January 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
April 12, 2022
Page 2 of 13
1.1 Site Background
The Pitt County Landfill occupies approximately 156 acres along Allen Road west of the city of
Greenville, NC (Figure 1). The landfill is comprised of a Northern Unit that closed in 1990 and a
Southern Unit that reached capacity in 1995. An east -west trending railroad (Norfolk Southern
Railroad) separates the Northern and Southern Units. The Pitt County landfill is unlined, and
leachate is not collected. The Northern Unit received waste from 1974 until 1990, and the
Southern Unit received waste from 1991 until 1995. Due to the closure dates, only the
Southern Unit is subject to the September 1993 rules for municipal solid waste landfills (15A
NCAC 13B .1600). Pitt County monitors the Northern Unit in accordance with the conditions of
the solid waste permit and 15A NCAC 13B .0500.
1.2 Physical Setting and Hydrogeology
The Pitt County Landfill lies in the central portion of the Coastal Plain Physiographic Province of
North Carolina where Cretaceous to Recent age Coastal Plain sedimentary formations overlie
Mesozoic and older basement bedrock (Horton and Zullo, 1991). Coastal Plain sediments and
sedimentary rocks have significant variations in permeability and water -producing capabilities.
High -permeability strata that readily produce usable quantities of water are aquifers, and low -
permeability sediments that restrict the movement of groundwater, either into or out of
aquifers, are confining beds. Coastal Plain aquifers typically use the predominant geologic
formation name that is associated with the aquifer. The two uppermost aquifers at the Pitt
County Landfill are: the unconfined Surficial/Yorktown aquifer and the confined Peedee Aquifer.
The Surficial/Yorktown Aquifer is locally composed of fossiliferous clays and sands. The clays
within the unit tend to serve as confining layers and restrict recharge to underlying aquifers
(GMA and McGill, 2001). The Peedee Aquifer consists of unconsolidated sands and sandstones
of the of Late Cretaceous age Peedee Formation (Winner & Coble, 1996). In the western half
of Pitt County, the Peedee Aquifer lies directly beneath the Surficial/Yorktown Aquifer, and the
elevation of the top of the Peedee Aquifer is above sea level (GMA and McGill, 2001).
A detailed description of the local site hydrogeology is provided in the Water Quality Monitoring
Plan for the Southern Unit (GMA, 1994). In general, a sandy clay extends from the original land
surface beneath the landfill to varying depths of 6 to 13 feet. A portion of this clay may have
been excavated from adjacent to the Southern Unit mound and used as part of the clay cap for
the mound. Coarser, more permeable sediments (silty fine sand, clayey sand, and very clayey
sand) typically exist at depths of 10 to 16 feet. Underlying these more permeable sediments, at
a depth of approximately 16 feet below the original land surface, is a thin, discontinuous, dark
gray clay that ranges from 0.5 to 3.0 feet in thickness, with an average thickness of 1 foot.
This clay layer exists at an elevation of approximately 66 feet above mean sea level and has
previously been referred to as the "66-foot clay" (GMA, 1994). Below this clay layer lie silty,
fine sands. During the installation of deep monitoring well P20D, GMA observed a silty, clay
layer from approximately 45 to 48 feet below the land surface. Below this clay layer, GMA

January 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
April 12, 2022
Page 3 of 13
observed a fine, phosphatic sand. GMA believes the deepest on -site monitoring wells (e.g.
MW1R, MW3, and P20D) may penetrate the top of the Peedee Aquifer, which is estimated to be
about 25 feet thick at the location of the landfill (GMA and McGill, 2001). We provide a general
summary of the stratigraphy below.
Average depth of strata relative
to original land surface (feet)
Lithology
0 — 9.5
sandy clay
9.5 — 16
silty fine sand, clayey sand, and very clayey sand
16 — 17
dark gray clay
17 — 45
silty, fine sand
45 — 48
silty, clay
48 — 60+
fine, phosphatic sand
1.3 Contaminants of Concern and Site Regulatory Status
As described in the introduction, the Southern Unit of the Pitt County Landfill is currently under
assessment for low-level exceedances of the NC Groundwater Quality Standard (NCAC 02L) for
benzene. The County first confirmed a slight exceedance of the NCAC 02L groundwater
standard for benzene in 2017. Since that time and following approval from the NCDEQ, DWM,
SWS, the County has collected groundwater samples from just beneath the southern ditch to
monitor the extent of benzene contamination at the facility. This ditch serves as the
groundwater discharge location for the Surficial Aquifer at Southern Unit. To date, the County
has not detected benzene in exceedance of the NCAC 02L standard in these samples, which
suggests that benzene contamination above the NCAC 02L groundwater standard does not
extend off the facility property.
Pitt County is also currently assessing the Southern Landfill Unit for exceedances of the NCAC
02L standard for 1,4-dioxane. In May 2018, the NCDEQ DWM SWS directed all North Carolina
landfills to begin testing for 1,4-dioxane as part of their routine groundwater monitoring. 1,4-
Dioxane is used primarily as a chlorinated solvent stabilizer, but it can also be found in paint
strippers, varnishes, waxes, and a variety of consumer products (US EPA, 2014). 1,4-Dioxane is
fully miscible in water, and it migrates readily with groundwater. This compound is short-lived
in the atmosphere, but it does not volatilize rapidly from water.
1,4-Dioxane was detected at the landfill in July 2019, and the County immediately and
voluntarily chose to perform an updated potential receptor investigation to determine if any
water -supply wells might be at risk. Pitt County opted to conduct the potential receptor survey
as a proactive measure in the interest of public health. The updated potential receptor survey,
conducted by GMA in September 2018, did not identify any well being used as a drinking water
source within 2,000 feet of the facility (GMA, 2018).

January 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
April 12, 2022
Page 4 of 13
Exceedances of the NCAC 02L groundwater standard for 1,4-dioxane were confirmed at the
Southern Unit of the Pitt County Landfill in January 2019. GMA suspects that the detection of
1,4-dioxane in multiple monitoring wells adjacent to the Southern Landfill Unit relates to
degradation of the integrity of one or both landfill caps and the stormwater drainage systems
designed to quickly shunt surface water off the landfill mounds. Pitt County emplaced the clay
caps above the Landfill in the mid-1990s. Over time, erosion of the cap, as well as cracking due
to heating/cooling, desiccation, and/or subsidence due to decomposition of fill material, can
increase the permeability of this type of barrier. Cap degradation has likely allowed infiltration
of water that has leached contaminants downward into the underlying groundwater.
Eliminating infiltration of water through the cap, and ensuring that the stormwater conveyance
system operates as designed, are primary goals for reducing, or eliminating, the release of
additional contaminants into the groundwater.
GMA, on behalf of the County, submitted a proposal to the SWS on June 21, 2019 to further
assess and address 1,4-dioxane contamination at the landfill. Specifically, we proposed to:
1) Delineate the vertical and horizontal extents of 1,4-dioxane by installing two additional
groundwater monitoring wells (one Type II monitoring well located between the two landfill
units and one double -cased, deep Type III monitoring well south of the Southern Mound)
and six surface water staff gauges.
2) Conduct a pilot study to document and establish the effectiveness of cap upgrades and
repairs to limit the infiltration of rainwater through the soil cap, and to evaluate if the
repairs have reduced leachate volumes and contaminant concentrations. During the pilot
study, the County proposed to:
a) conduct geophysical testing of the Southern Unit to evaluate landfill cap integrity,
b) repair any areas of concern identified by the geophysical testing,
c) inspect surface water drainage structures on the mound to ensure that they are
operating as designed, and then
d) repeat geophysical testing after cap repairs are made to document the results of the
cap repairs.
3) Install two in -stream piezometers approximately 1.5 feet below the ditch bottom at the
locations of the currently collected porewater samples. The in -stream piezometers provide
repeatable locations to collect representative groundwater samples, measure groundwater
levels, and determine any discharge relationships just below the stream bed.
The NCDEQ-SWS approved the proposed activities on June 26, 2019 (Appendix A), and the
County immediately began to implement the pilot study. We provide an update regarding the
status of the approved activities in Section 2.0 below.

January 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
April 12, 2022
Page 5 of 13
2.0 1,4-DIOXANE ASSESSMENT AND PILOT STUDY UPDATE
North Carolina Administrative Code 15A NCAC 13B .1634 requires the County to characterize
the nature and extent of any release. The County began assessing the horizontal extent of 1,4-
dioxane during the January 2019 monitoring event by voluntarily sampling three additional wells
that were present at the facility, but no longer part of the required groundwater monitoring
program.
In June of 2019, the County installed the two monitoring wells and the six surface water staff
gauges described in GMA's Pilot Study proposal in June of 2019. A single -cased (Type -II)
monitoring well was installed between the Northern and Southern mounds, just north of well
P16R (Figure 1). This well, designated as well P29, is hydrologically separated from well P16R
by two drainage ditches along the railroad, and the well is screened from 7 to 12 feet below the
land surface. A 60-foot-deep, double -cased (telescoping, Type -III) groundwater monitoring
well was installed on the south side of the Southern Unit, just off the toe of the slope of the
Southern Mound (Figure 1). This well, designated as well P20D, allowed the County to further
assess the vertical extent of 1,4-dioxane at the Southern Unit. The outer casing of P20D
extends to 45 feet below land surface, and the well is screened from 50 to 60 feet below land
surface.
In accordance with the approved Pilot Plan, in August 2019, GMA also installed two shallow, in -
stream piezometers (PZ1 and PZ2) below the ditch bottom along the southern property
boundary near the locations of the historically collected porewater samples (Figure 1). Each
piezometer has a 9-inch-long screen, with the top of the screen set 1 foot below the ditch
bottom. The County uses the instream piezometers to collect representative groundwater
samples to monitor benzene migration and to evaluate groundwater discharge relationships to
the ditch.
To evaluate the integrity of the Southern Landfill Unit cap, and to provide a baseline from which
to evaluate hydrologic improvements following cap upgrades and repairs, Geo Solutions
Limited, Inc. completed electromagnetic (EM) and ground -penetrating radar (GPR) surveys of
the Southern Landfill Unit on June 26', July 15t and July 2nd 2019 (GMA, 2019). The EM survey
identified multiple areas of elevated apparent conductivity that may correspond to leachate
moving away from the landfill. Additionally, the EM survey indicated that solid waste appears to
extend beyond the toe of the slope to the edge of the gravel road in the proximity of monitoring
wells MW6R, P16R, and P20R. This finding was consistent with GMA's observations of trash
during the installation of well P20D. The GPR survey identified several areas that had only a
thin landfill cap that was completely eroded away in some locations. The identified areas
included the northwestern upper slope of the mound, the western narrow berm, and the

January 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
April 12, 2022
Page 6 of 13
southern toe north of monitoring wells P28 and P19. The GPR results indicated that the
impermeable cap thickness at the Southern Landfill was, on average, 10 inches and ranged
from 0 to 30 inches. Full details of the geophysical evaluation can be found in Geo Solutions'
report, which was provided as Appendix F of the July 2019 monitoring report from GMA (GMA,
2019). A revised version of that report is included as Appendix B in the July 2021 South
Monitoring Report and Pilot Study (GMA, 2021). The revised report includes a correction to the
estimates of the thickness of the impermeable cap layer based on a corrected understanding of
cap construction at the facility. This correction did not affect the implications or conclusions of
the original geophysical evaluation.
After completion of the geophysical survey, the County contracted with an engineering firm
(The Wooten Company) to design cap repairs and stormwater upgrades that will eliminate or
greatly reduce the infiltration of precipitation into the Southern Unit. The County provided the
geophysical report to Wooten to aid their design of cap repairs and stormwater upgrades for
the facility. The Wooten Company (Wooten) resurveyed the Southern Landfill Unit in early
2020, and in June 2020, Wooten submitted a final design to the County. This design included
repairing the cap on the western end of the Southern Landfill, regrading multiple areas to
eliminate ponding on the mound, restoring the stormwater conveyance system to operate as
originally designed, and adding new drainage pipes to the southwest corner of the mound. The
County chose to make these substantial upgrades to protect the groundwater from further
contamination via leaching from landfill waste.
Construction activities commenced at the site on November 4, 2020. The County's contractor
originally anticipated completing the work by March 2021, but the project experienced
significant weather -related delays due to long periods of high rainfall from December 2020
through February 2021 (NCSCO, 2021). Repairs at the Southern Unit were completed in June
of 2021. As -built drawings for the Southern Unit cap repair and stormwater upgrades are
provided in Appendix C in the July 2021 South Monitoring Report and Pilot Study (GMA, 2021).
Following completion of the cap repairs and stormwater system upgrades, GMA contacted Geo
Solutions Limited, Inc. to complete a post -repair geophysical evaluation of the Southern Unit.
The purpose of this evaluation was to document the remedial effort of the Pitt County Landfill
by comparing the pre -repair and post -repair geophysical data. Geo Solutions completed repeat
EM and GPR surveys of the Southern Landfill Unit on August 2"d thru August 4t", 2021 (GMA,
2021).
A comparison of the EM response before and after cap improvements showed a weaker EM
response in areas where new low permeability material was placed to repair eroded areas of
the cap, and in areas where regrading was performed to improve surface water drainage
toward the catch basins (Figure 2). The weaker EM response in these locations was due to the

January 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
April 12, 2022
Page 7 of 13
EM profiler being further above the waste following repairs. Based on GPR data, the most
apparent changes in landfill cap thickness from 2019 to 2021 are along the northern repaired
slope where the cap was significantly thickened (15 to 20 inches) during the recent repair
(GMA, 2021).
The areas of leachate seeps identified in 2019 appeared similar in EM response to the 2021
electromagnetic survey. It is likely too soon to see improvements at seep locations due to the
slow velocity of groundwater at this site. Future geophysical evaluations targeting only the
locations of previously identified seeps may provide a means to monitor the effectiveness of the
recently completed cap improvements. Regardless, geophysical results confirm improvements
to the landfill cap thickness and surface water drainage that should greatly reduce the
infiltration of precipitation into the Southern Landfill Unit.
The County is currently monitoring groundwater levels and contaminant concentrations to
assess the effectiveness of the cap and stormwater system upgrades, as approved by the
NCDEQ-SWS in their June 26, 2019 letter (Appendix A). The County will continue monitoring
until at least July 2022 to allow time for the existing groundwater to drain from the Southern
mound prior to making a full assessment of hydraulic improvements resulting from the repair of
the Southern cap. The County continues to monitor both the Northern and Southern Landfill
Units on their approved schedules (semi-annually for the Southern and annually for the
Northern).
3.0 JANUARY 2022 SEMI-ANNUAL MONITORING EVENT
GMA performed the semi-annual monitoring event at the Southern Unit on January 25 to 26,
2022. Historically, the County has monitored the Southern Landfill Unit for the parameters
identified in Appendix I of 40 CFR Part 258 plus 1,4-dioxane on a semi-annual basis and for the
parameters listed in 40 CFR Part 258 Appendix II on an annual basis. Based on the lack of
detections of Appendix II parameters over the last 20 years, GMA, on behalf of the County,
requested that the NCDEQ SWS allow a reduction in sampling frequency for Appendix II
constituents. Specifically, we requested that the NCDEQ SWS allow the County to sample for
Appendix II constituents on a biennial basis with the next scheduled Appendix II sampling event
occurring during July 2022. The NCDEQ SWS approved this request on July 2, 2020 (Appendix
A). Therefore, during the January 2022 monitoring event, the County analyzed all groundwater
and surface -water samples for Appendix I parameters and for 1,4-dioxane. Sampling
procedures and analytical methods complied with the approved Water Quality Monitoring Plan
dated September 8, 1994, and subsequent groundwater policy memos issued by the NCDEQ-
SWS (Appendix A).

January 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
April 12, 2022
Page 8 of 13
Twenty-eight groundwater -monitoring wells and two temporary groundwater piezometers
comprise the groundwater -monitoring network for the entire landfill facility (Figure 1, Table 1).
GMA also monitors surface water levels at thirteen staff gauges in the ditches surrounding the
site. The water -quality monitoring network used for the January 2022 semi-annual monitoring
of the Southern Unit consisted of two background monitoring wells (P4 and MW1R), seven
shallow' wells located around the Southern Mound (P11R, P12, P16R, P17, P19, P20R, P28, and
MW6R), a 'deep' well located south of the Southern mound (P20D), a well located between the
Northern and Southern Landfill Unit (P29), two temporary groundwater piezometers (PZ1 and
PZ2), a hydraulically-upgradient surface water sample location (SW1), and a hydraulically-
downgradient surface water sample location (SW2) (Figure 3).
3.1 Groundwater Hydrology
GMA measured static water levels in all monitoring wells and temporary piezometers (Table 2),
and at 12 of the 13 staff gauges (Table 3) on January 25, 2022. Staff gauge SG5 has been
damaged by mowing at the facility and has not been replaced to date. Depth to groundwater in
monitoring wells at the site ranged from approximately 0.80 to 13.35 feet below the land
surface. Estimates of groundwater velocity (Table 4) ranged from approximately 0.004 to 0.018
feet/day, or 1.46 to 8.09 feet/year. These represent relatively slow groundwater velocities.
An equipotential map prepared using these water -level measurements (Figure 3) shows that the
horizontal component of groundwater flow at the Southern Unit was generally directed to the
south and southeast. A portion of the Northern Landfill Unit lies hydraulically upgradient of the
Southern Unit, but the highest groundwater levels at the facility are located offsite, just
northwest of the landfill boundary near the Pitt County Solid Waste and Recycling site on
Stantonsburg Road. Groundwater samples collected and analyzed from wells in this
hydraulically-upgradient area represent background groundwater chemistry.
During the January 2022 monitoring event, the groundwater elevation measured in well P16R
was lower than the surface water elevation at the nearby staff gauge, SG3, indicating that
groundwater from the Southern mound was not discharging to the ditch at this location. Prior
to this monitoring event, the opposite relationship has been true. Since July 2019 when a staff
gauge was first installed at this location, the groundwater elevation in well P16R had
consistently been higher than the surface water elevation at SG3, which indicated that shallow
groundwater within the Southern Unit was discharging to the ditch in this area. GMA believes
that the change in the direction of shallow groundwater flow at this location may be the first
indication of hydraulic improvement resulting from the cap repairs and stormwater
improvements completed at the Southern Unit. Further monitoring and assessment is needed
to determine if this relationship continues in the future or whether this is due to seasonal
and/or annual variation in rainfall.

January 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
April 12, 2022
Page 9 of 13
The groundwater elevation at instream piezometer PZ1 was slightly higher than the surface
water elevation during the January 2022 monitoring event (Tables 2 and 3). There was no
difference between the groundwater and surface water elevations at instream piezometer PZ2..
The water level measurement collected at PZ1 indicates that groundwater was discharging to
the southern boundary ditch in this area during the January 2022 monitoring event.
3.2 Sample Collection and Analyses
For monitoring of the Southern Unit, GMA analyzed water samples collected from twelve
monitoring wells, two temporary piezometers, and two surface water sampling locations as
shown on Figure 2. During sampling, GMA collected field water -quality parameters to
document adequate purging prior to sample collection and to aid in evaluating groundwater
chemistry at the site (Table 5). We provide a copies of the well sampling records in Appendix
B. Sampling procedures and analytical methods complied with the approved Water Quality
Monitoring Plan dated September 8, 1994, and subsequent directives issued by the SWS
(Appendix A).
GMA transferred all samples to Environmental Conservation Laboratories, Inc. (ENCO) in ice -
filled coolers under chain -of -custody protocol for analysis of Appendix I parameters and 1,4-
dioxane (Table 6). Copies of the chain -of -custody forms and analytical reports are provided in
Appendix C. Consistent with the May 29, 2018 NCDEQ-SWS memo, ENCO analyzed the
samples using EPA -approved analytical methods sufficiently sensitive to detect the presence of
regulated constituents at or below the applicable standard (unless no such method currently
exists, e.g. for vinyl chloride analysis).
3.3 Analytical Results and Discussion
Twenty-two parameters (acetone, barium, benzene, beryllium, carbon disulfide, chlorobenzene,
chromium, cobalt, copper, 1,4-dichlorobenzene, 1,1-dichloroethane, 1,4-dioxane, ethylbenzene,
lead, m,p-xylenes, nickel, o-xylene, selenium, toluene, vanadium, xylene, and zinc) were
detected at concentrations above their method detection limits during the January 2022
sampling event (Table 7). Three of those constituents (barium, benzene, and 1,4-dioxane)
were detected at concentrations exceeding the NCAC 02L standard, and three parameters
(beryllium, cobalt, and vanadium) were detected at concentrations above their Interim
Maximum Allowable Concentration (IMAC) during this monitoring event (Table 7).
Zinc and carbon disulfide were detected in the equipment blank. GMA believes that zinc
concentrations are related to residual powder from the manufacturing process used to produce
the'powder-free' nitrile gloves that we used during sampling. Nitrile gloves are also the likely
source of the carbon disulfide detected in the equipment blank (USGS, 2012). 1,4-Dioxane was

January 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
April 12, 2022
Page 10 of 13
detected in the field blank, but GMA could not identify a known source. Detections may be
related to sampling techniques. GMA will review sampling procedures before the next
groundwater sampling event.
Samples from wells P16R, P19, P20R, and P29 contained benzene (2.4 µg/L, 3.4 µg/L, 1.3 µg/L,
and 2.0 µg/L, respectively) above the 1.0 µg/L NCAC 02L groundwater standard. Importantly,
benzene was not detected in either in -stream piezometer sample (PZ1 and PZ2). Therefore,
there continues to be no evidence that benzene is migrating off of the landfill property at this
time.
1,4-Dioxane was detected in wells MW6R, P16R, P17, P19, P20R, and P29 (6.7 µg/L, 78 µg/L,
4.8 µg/L, 180 µg/L, 62 µg/L, and 180 µg/L, respectively) at concentrations exceeding the NCAC
02L groundwater standard of 3 µg/L. The detection of 1,4-dioxane in well P29 located between
the two landfill units indicates that 1,4-dioxane may be leaching from both the Southern and
Northern mounds. 1,4-Dioxane was also detected in groundwater sample PZ1, in the southern
ditch, but the concentration was below the NCAC 02L standard. Importantly, the lab did not
detect 1,4-dioxane in the sample collected from the "deep" down -gradient monitoring well,
P20D, or in the downgradient surface water sample, SW2.
Samples from wells MW6R, P16R, P19, and P20R contained concentrations of barium (1950
µg/L, 1010 µg/L, 1500 µg/L, and 887 µg/L respectively) above the NCAC 02L standard of 700
µg/L. Barium occurs naturally in the native soils at the Pitt County Landfill as evidenced by the
ubiquitous occurrence of this alkaline metal in all samples collected at the site, including those
located in up -gradient off -site areas. GMA has previously demonstrated that barium is often a
constituent of the particulate matter in many of the groundwater samples collected at the Pitt
County Landfill and that dissolved barium concentrations do not exceed the NCAC 02L standard
in some locations (GMA, 2011 and 2015). Despite the apparent natural occurrence of barium at
this site, the concentrations of barium detected in wells MW6R and P19 are unlikely to be solely
attributable to natural sources.
Upgradient surface water sample SW1 contained concentrations of cobalt (8.63 J µg/L) and lead
(3.53 J µg/L) above the 15A NCAC 02B surface -water standards of 4 µg/L and 0.54 µg/L,
respectively. In recent years, multiple metals have exceeded the standards at this location (e.g.
7 parameters above the 2B standards in July 2019, GMA 2020). Metal exceedances at this
upgradient surface -water sample location corresponded with highway construction on the
adjoining parcel directly next to the SW1 sampling location. Per the NC DOT website,
construction on the bypass started in August 2016 and was completed in November of 2019
(NC DOT, 2019). The lab did not detect any of the target parameters above the 2B surface -
water standards in the down -gradient samples for the Southern Unit (SW2).

January 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
April 12, 2022
Page 11 of 13
4.0 CONCLUSIONS AND FUTURE WORK
1,4-Dioxane, barium, and benzene were detected at concentrations exceeding the NCAC 02L
groundwater standards at multiple locations during the January 2022 monitoring event.
However, these constituents were not detected at concentrations above state standards in
groundwater samples collected from just below the southern property ditch, which acts as a
local groundwater discharge feature, or in the downgradient surface -water sample. These
results suggest that these 1,4-dioxane, benzene, and concentrations in excess of naturally
occurring barium are not migrating off -site at this time. Further, neither 1,4-dioxane nor
benzene were detected in the sample collected from the deep monitoring well located down -
gradient of the Southern Landfill Unit (P20D). Barium was detected in this well, but the
concentration (49.0 ug/L) was well below the NCAC 02L standard and below concentrations
detected in upgradient, off -site monitoring wells. The absence of these target compounds
indicates that 1,4-dioxane, benzene, and non-native barium have not migrated out of the
Surficial/Yorktown Aquifer at the site.
In June 2021, the County completed the planned cap and stormwater system repairs and
upgrades at the Southern Unit (GMA, 2021). These upgrades were part of an approved pilot
study for corrective action following detections of 1,4-dioxane and benzene above the NCAC
02L groundwater standards. These improvements were designed to greatly reduce the
infiltration of water through the cap in order to protect the groundwater from further
contamination via leaching from landfill waste. The County is currently monitoring groundwater
levels and contaminant concentrations to assess the effectiveness of the cap and stormwater
system upgrades, as approved by the NCDEQ-SWS in their June 26, 2019 letter (Appendix A).
The reversal of shallow groundwater flow in the vicinity of well P16R measured during this
monitoring event may be the first indication of hydraulic improvement associated with the cap
repairs at the Southern Unit, but further assessment is needed. The County plans to continue
monitoring until at least July 2022 to allow time for the existing groundwater to drain from the
Southern mound and to better evaluate the effects of seasonal changes and varying amounts of
precipiation on groundwater levels prior to making a full assessment of hydraulic improvements
resulting from the cap repair. It is too soon to see reductions in contaminant levels associated
with the cap repairs.
The County continues to monitor groundwater at the Southern Unit on a semi-annual schedule.
The next semi-annual monitoring event at the Pitt County Solid Waste Municipal Landfill is
scheduled for July of 2022 and will include both Appendix I and Appendix II of 40 CFR Part 258
parameters plus 1,4-dioxane. The sampling network will continue to include wells P19, P20D,
and P29 and the two in -stream piezometers. GMA will also continue to document water levels
at all staff gauges that were installed during July of 2019.

January 2022 Semiannual Water Quality Nlonitorino Report
Southern Portion of the Pitt County Solid Waste Alunicipal Candfll
April 1Z 2022
Page 12 of 1.3
5.0 REPORT CERTIFICATION
This report was prepared by Groundwater Management Associates, Inc. (GMA), a professional
corporation licensed to practice geology (#C-121) and engineering (#C-0854) in North Carolina.
I, Emma H. Shipley, a North Carolina Licensed Geologist for GMA, do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
Emma H. Shipley, P.G.
Project Hydrogeologist
Cody J. Shell, P.G.
Project Hydrogeologist
6.0 REFERENCES
o..,cENsFa�f,�.
r'
SEAL _
23C ;i
Richard K. Spruill, Ph.D., P.G.
Principal Hydrogeologist
Groundwater Management Associates, Inc., 1994, Water Quality Monitoring Plan for the Active
Southern Unit of the Pitt County Landfill, 71 pages.
Groundwater Management Associates, Inc., 2011, Alternative Source Demonstration Report, Pitt
County Solid Waste Municipal Landfill, Greenville, Pitt County, 8 pages.
Groundwater Management Associates, Inc., 2015, January 2015 Semi-Annuaf Water Quality
Monitoring Event, Greenville, Pitt County, 147 pages.
Groundwater Management Associates, Inc., 2018, Potential Receptor Survey: Northern and
Southern Units of the Pitt County Landfill, Greenville, Pitt County, 14 pages.

January 2022 Semiannual Water Quality Monitoring Report
Southern Portion of the Pitt County Solid Waste Municipal Landfill
April 12, 2022
Page 13 of 13
Groundwater Management Associates, Inc., 2019, January 2019 Semi -Annual Water Quality
Monitoring Event and Pilot Study Update, Greenville, Pitt County, 201 pages.
Groundwater Management Associates, Inc., 2021, July 2021 Semi -Annual Water Quality
Monitoring Event and Pilot Study Update, Greenville, Pitt County, 216 pages.
Groundwater Management Associates, Inc. and McGill and Associates, 2001, Water Resources
Management Plan, Pitt County, North Carolina.
Horton, J.W. and V.A. Zullo, 1991, The Geology of the Carolinas: Carolina Geological Society
Fiftieth Anniversary Volume, 406 pp.
NC DOT, 2019, Southwest Bypass Opens to Traffic ahead of Schedule,
https://www.ncdot.gov/news/press-releases/Pages/2019/2019-11-21-pitt-count --
southwest-bypass-opens.aspx, accessed December 4, 2019.
NCSCO, 2021, North Carolina State Climate Office, Winter Recap 2020-21: La Nina Lays Low in
a Persistent Wet Winter, https://climate.ncsu.edu/blog/2021/03/winter-recap-2020-21-la-
nina-lays-low-in-a-persistent-wet-winter/, accessed July, 20, 2021.
USEPA, 2014, Technical Fact Sheet — 1,4-Dioxane, Office of Solid Waste and Emergency
Response, EPA 505-F-14-011, 8 pages.
USGS, 2012, Program Evaluation of Volatile Organic Compound (VOC) Blank Data and
Application of Study Reporting Levels to Groundwater Data Collected for the California
GAMA Priority Basin Project, May 2004 through September 2010. Scientific
Investigations Report 2012-5139, 106 pages.
Winner, M.D. and R.W. Coble, 1996, Hydrogeologic Framework of the North Carolina Coastal
Plain, USGS Professional Paper 1404-I, 119 pages.

FIGURES

,.
Al�~'
— 7 1
A?
Ar
=
+
t SW1
__ MW8
P26 SG96
r
P5
SG97
t,.
SG10 MW1 R
:-, •'
SW4
P15
SG4
sG111 SG12
" NORTHERN UNIT
i �• _
Y
P13
r_ .
MW4
on
- P29 SG1 _
- SG9
P2
-'
ll P23
P 16 R
P11R
SOUTHERN UNIT
_ .- ..
19 P
P1r7 P28
y
SG6
P20D
P12
9
SG8 P20R
PZ1
w
-
P8
SIG
PZ2
V
SW2
`'►�:''
- - -
THIS PRODUCT IS FORGE FRAL REFERENCE PURPOSES ONLY AND SHOULD NOT BE USED,
AND Is NOT INTENDED FOR, SURVEYOR ENGINEERING PURPOSES. LOCATIONS ARE APPROXIMATE.
SG2
-
.,�.
GIs SOURCE DATA:
` ORTHOIMAGERYOSTAINED FROM NO ONEMAP, IMAGE DATE: FEBRUARY 2020
PARCEL BOUNDARIES FROM PITTGOUNTY GIS, ttF,11",pittnc op-d.t, ,,gi,.w,
-LEGEND-
G SURFACE WATER SAMPLE
���
TEMPORARY PIEZOMETER DITCHES
SCALE IN FEET
STAFF GAUGE
)K ABANDONED / LOST WELL
0
MONITORING WELL
APPROXIMATE PARCEL BOUNDARIES
`00'
GROUNDWATER MANAGEMENT ASSO[1ATES,IN[-
File: DRAWINGS/25101
SITE LAYOUTAND EXISTING MONITORING NETWORK
DATE: 3/17/2021
FIG 1
PROJECT 25101
PITT COUNTY LANDFILL, GREENVILLE, PITT CO., NC
FIGURE 1

THIS PRODUCT IS FOR GENERAL REFERENCE PURPOSES ONLY AND SHOULD NOT BE USED,
AND IS NOT INTENDED FOR, SURVEY OR ENGINEERING PURPOSES. LOCATIONS ARE APPROXIMATE.
GIS SOURCE DATA:
TOPOGRAPHIC CONTOURS OBTAINED FROM NC ONEMAP,
PARCEL BOUNDARIES FROM PITT COUNTY GIS, https://map-pittnc.opendata.arcgis.com
�I Z' '
' 79
SGIO l 71
P05
79.in(76
_ W1R 79.55.17
79 ) /
I f�
V I,,— • I PO4
P_06_ �(77.03)I '
78
i77.89
MW,1
' SG11 SG12
.
I 77.86 77.85
f
��NOR�Ucn
_ 80
P11R=�
77 76.82
P17
76 1 75.16
1
r
Ez
P16R
76.97r
75'54
- '(73.'03) 75.77
77.33 _ - y-- - - 76 - OP 9 75
7 74.86 ��' ' 75.98 ;
l' LL —75
-77rr
r_ ;` l $ 74
1- ~ 76 N, ,,l '� o P23 80
rr - -��f j
CO 73.61 ,
r I/�J1� / 1� 80
MW6R MW5 73
72.59� SG6',
r-J
v
�P20D� 70 P24 P0�72
P12 �P, 28_—
�/ 73.39 �� - - (72.76)�69���0 a°
74.81 P_20R �: PZ1 P10
75 ��� _:1 ` 70.42 `� rx 71
74t/ � - - SG8 -� _ PM-
73 SG7 71:34�� PZ2 (surface water) �`0:67 00 r-
72 71.92 1 ; 71 70.71 N� 70
(surface water) CO SG2 69 J
' 68.53 N
GENERAL NOTES:
1. TOPOGRAPHIC CONTOUR INTERVAL = 2.0 FEET
2. GROUNDWATER CONTOUR INTERVAL = 1.0 FOOT
3. ARROW INDICATES DIRECTION OF GROUNDWATER FLOW
4. WATER LEVEL ELEVATIONS ARE POSTED BY EACH WELL
5.( ) INDICATES DATA NOT USED FOR CONTOURING
- LEGEND -
MONITORING WELL
UNMEASURED MONITORING WELL
ABANDONED MONITORING WELL
PROPERTY LINE
RAILROAD TRACKS
TOPOGRAPHIC CONTOUR
-
POND
GROUNDWATER ELEVATION
CONTOUR
INDICATES DIRECTION OF
GROUNDWATER FLOW
77.31
WATER LEVEL
(FEET ABOVE SEA LEVEL)
----
DITCH
IL
STAFF GAUGE
FIGURE 3
DATE 4/7/2022 PROJECT: 25101
DRW BY: CJS CHK BY: EHS
SCALE IN FEET
0 350 700'
1" = 350'
EQUIPOTENTIAL MAP
JAN UARY 25, 2022
A
IV,IA
GROUNDWATER MANAGEMENT ASSOCIATES, INC.

TABLES

Table 1. Monitoring Well Construction and Elevations
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Easting
(feet)*
Northing
(feet)*
S
(h * ^
M= J
U O V)
O R ++
a °
° W .`�°.
u
* ^
q= J
7 O V1
�+
_ °
M W .�°.
J d
- 01�
y= ^
3 3 3
as
° `_-, n
d d
i w
V
V)
+s+ O J
a a E
c ° o
V G7
w w
O
O J
a, E
c CO° o
w Gl
° i ^
= V J
O V1 V1
O
> a °
au ° °.
V
° w ^
= O J
O V)
O ,r
> + °
W m°
MW1R
2463487.26
676793.08
84.28
81.3
52.98
40.0
50.0
41.3
31.3
MW3
2467253.81
676198.15
81.77
79.3
47.47
35.0
45.0
44.3
34.3
MW4
2466875.66
676066.89
82.38
80.7
21.68
10.0
20.0
70.7
60.7
MW6R
2465083.71
675392.21
79.74
76.95
19.79
7.0
17.0
69.95
59.95
MW8
2464639.20
676915.58
83.21
80.42
16.79
4.0
14.0
76.42
66.42
MW8D
2464553.05
676827.15
83.08
80.17
30.91
18.0
28.0
62.17
52.17
P02
2467254.11
676191.82
83.45
79.4
19.05
11.0
15.0
68.4
64.4
PO4
2463438.60
676616.81
83.82
80.3
21.52
8.0
18.0
72.3
62.3
POs
2463490.61
676797.65
84.74
81.1
17.14
8.5
13.5
72.6
67.6
P06
2463171.35
676568.01
83.52
80.3
17.72
8.5
14.5
71.8
65.8
P07
2466875.67
676056.22
84.21
80.7
19.51
11.0
16.0
69.7
64.7
P08
2466074.39
674918.18
84.02
80.2
20.82
9.0
17.0
71.2
63.2
P09
2466189.91
675932.77
82.88
78.9
18.48
9.5
14.5
69.4
64.4
P11R
2463141.14
675651.83
84.84
81.1
19.74
13.0
16.0
68.1
65.1
P12
2463126.32
675048.53
78.21
75.1
20.61
10.5
17.5
64.6
57.6
P13
2466105.04
676161.21
83.79
80.8
18.99
11.0
16.0
69.8
64.8
P13D
2466119.99
676174.03
83.25
80.5
54.25
47.5
51.5
33
29
Pis
2465472.37
676703.00
86.7
83.05
20.65
4.0
17.0
79.05
66.05
P16R
2464194.10
675837.67
86.24
83.1
17.14
11.0
14.0
72.1
69.1
P17
2463319.94
675286.12
79.18
75.1
15.08
8.0
11.0
67.1
64.1
P19
2463898.87
675403.02
82.7
77.3
18.4
9.0
13.0
68.3
64.3
P20R
2464435.49
675068.13
84.01
80.5
33.51
10.0
30.0
70.5
50.5
P20D
2464583.16
675103.79
83.32
80.3
63.02
50.0
60.0
30.3
20.3
P21
2465286.45
675904.93
80.87
76.6
15.27
8.0
11.0
68.6
65.6
P23
2465657.48
675745.22
81.73
78.2
19.53
11.0
16.0
67.2
62.2
P26
2466246.80
676940.21
83.39
81
16.39
9.0
14.0
72
67
P28
2463542.16
675278.55
76.54
73.6
10.94
3.5
8.0
70.1
65.6
P29
2464558.30
676041.26
84.16
81.2
14.96
7.0
12.0
74.2
69.2
PZ1
2464848.16
675165.00
71.24
69.6
3.39
1.0
1.8
69.8
69.1
PZ2
2464485.95
675009.74
71.69
70
3.44
1.0
1.8
70.2
69.5
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid
(NCGS) control based on ties to NCGS Monument 'RUTH' and NCGS Monuments 'MARY'. Horizontal data referenced
to NAD 83(2011). Vertical data referenced to NAVD 88.
BLS = below land surface ASL = above sea level LS = land surface

Table 2. Monitoring Well Water Levels and Sample Purge Volumes
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Date
Elevation
of Top of
Casing
(feet ASL)
Land Surface
Elevation*
(feet ASL)
Total Well
Depth
below LS
(feet)
Depth to
Water
(feet)
Elevation
of Water
(feet ASL)
Height of
Water in
Well (feet)
Three Well
Volumes
(gallons)
Amount
Purged
(gallons
)
Number of
Well Volumes
Purged
Purged to
Dryness?
MW1R
1/25/22
84.28
81.30
50.0
8.11
76.17
44.9
21.8
21.8
3.0
no
MW3
1/25/22
81.77
79.30
45.0
8.99
72.78
38.5
18.7
18.7
3.0
1 no
MW4
1/25/22
82.38
80.70
20.0
6.57
75.81
not sampled
MW6R
1/25/22
79.74
76.95
17.0
7.15
72.59
12.6
6.1
6.1
3.0
no
MW8
1/25/22
83.21
80.42
14.0
7.19
76.02
9.6
4.7
4.7
3.0
no
MW8D
1/25/22
83.08
80.17
28.0
6.94
76.14
not sampled
P02
1/25/22
83.45
79.40
15.0
7.88
75.57
11.2
5.4
5.4
3.0
no
PO4
1/25/22
83.82
80.30
18.0
6.79
77.03
14.7
7.2
5.1
2.1
yes
P05
1/25/22
84.74
81.10
13.5
5.19
79.55
12.0
5.8
5.8
3.0
yes
P06
1/25/22
83.52
80.30
14.5
5.63
77.89
12.1
5.9
4.6
2.4
no
P07
1/25/22
84.21
80.70
16.0
8.44
75.77
11.1
5.4
1 4.0
1 2.2
yes
P08
1/25/22
84.02
80.20
17.0
13.35
70.67
not sampled
P09
1/25/22
82.88
78.90
14.5
6.90
75.98
11.6
5.6
5.6
3.0
no
P11R
1/25/22
84.84
81.10
16.0
8.02
76.82
11.7
5.7
2.9
1.5
yes
P12
1/25/22
78.21
75.10
17.5
3.40
74.81
17.2
8.4
3.3
1.2
yes
P13
1/25/22
83.79
80.80
16.0
8.69
75.10
10.3
5.0
3.9
2.3
yes
P13D
1/25/22
83.25
80.50
51.5
10.08
73.17
44.2
21.5
1 22.0
3.1
no
P15
1/25/22
86.70
83.05
17.0
7.05
79.65
not sampled
P16R
1/25/22
86.24
83.10
14.0
9.27
76.97
7.9
3.8
1.8
1.4
yes
P17
1/25/22
79.18
75.10
11.0
4.02
75.16
11.1
5.4
3.3
1.8
yes
P19
1/25/22
82.70
77.30
13.0
7.16
75.54
11.2
5.5
5.5
3.0
no
P20R
1/25/22
84.01
80.50
30.0
10.89
73.12
22.6
11.0
11.0
3.0
no
P20D
1/25/22
83.32
80.30
60.0
10.56
72.76
52.5
25.5
4.0
1 0.5
no
P21
1/25/22
80.87
76.60
11.0
6.01
74.86
9.3
4.5
3.3
2.2
yes
P23
1/25/22
81.73
78.20
16.0
8.12
73.61
11.4
5.5
2.9
1.5
yes
P26
1/25/22
83.39
81.00
14.0
8.31
75.08
not sampled
P28
1/25/22
76.54
73.60
8.0
3.15
73.39
7.8
3.8
2.6
2.1
yes
P29
1/25/22
84.16
81.20
12.0
7.15
77.01
7.8
3.8
3.8
3.0
no
PZ1
1 1/25/22
1 71.24
1 69.60
1 1.8
1 0.80
1 70.44
1 2.6
1.3
0.4
1.0
yes
PZ2
1 1/25/22
1 71.69
1 70.00
1 1.8
1 0.98
1 70.71
1 2.5
1.2
0.4
1.1
yes
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid (NCGS) control based on ties to NCGS
Monument'RUTH' and NCGS Monuments'MARY'. Horizontal data referenced to NAD 83(2011). Vertical data referenced to NAVD 88.
ASL = Above Sea Level LS = land surface

Table 3. Staff Gauge Elevations and Water Levels
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Staff
Gauge
Date
Easting
(feet)*
Northing
(feet)*
Reference
Point
Elevation of
Reference
Point
feet ASL
Staff Gauge
Reading or
Depth to Water
Measurement
ft
Elevation of
Water
feet ASL
SG1
1/25/22
2464589.3
676053.46
4-foot mark
79.86
1.12
76.98
SG2
1/25/22
2466082.36
674856.14
4-foot mark
70.48
2.05
68.53
SG3
1/25/22
2464175.98
675874.46
4-foot mark
79.40
1.93
77.33
SG4
1/25/22
2467192.35
676705.36
4-foot mark
75.18
1.48
72.66
SGS
1/25/22
2465262.23
675928.45
3-foot mark
75.68
-
-
SG6
1/25/22
2465175.63
675356.1
4-foot mark
72.98
0.79
69.77
SG7
1/25/22
2463215.14
675010.08
3-foot mark
73.93
0.99
71.92
SG8
1/25/22
2463932.14
675059.19
3-foot mark
72.71
1.63
71.34
SG9
1/25/22
2466110.5
676143.36
3-foot mark
75.76
0.27
73.03
SG10
1/25/22
2463086.65
676845.47
3-foot mark
80.82
1.38
79.20
SGI1
1/25/22
2463169.96
676528.73
3-foot mark
80.27
0.59
77.86
SG12
1/25/22
2463583.11
676511.02
3-foot mark
79.93
0.92
77.85
SG96
1/25/22
2466366.84
676889.34
3-foot mark
76.63
1.11
74.74
PZ1-SW+
1/25/22
2464848.16
675165.00
TOC
71.24
0.82
70.42
PZ2-SW+
1/25/22
2464485.95
675009.74
TOC
71.69
0.98
70.71
* Survey performed by Gary S. Miller & Associates, P.A. Land Surveyors (L-2562). North Carolina Geodetic Grid
(NCGS) control based on ties to NCGS Monument'RUTH' and NCGS Monuments'MARY. Horizontal data referenced
to NAD 83(2011). Vertical data referenced to NAVD 88.
+ Surface water elevations determined by measuring depth to surface water from top of casing
ASL = Above Sea Level
TOC = top of casing

Table 4. Calculations of Groundwater Velocity
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Date
Horizontal
Hydraulic
Gradient
(ft/ft)
Hydraulic
Conductivity
(ft/day)
Effective
Porosity
Horizontal
Groundwater
Velocity
(ft/day)
Horizontal
Groundwater
Velocity
(ft/year)
MW6R
1/25/22
0.013
0.50
0.29
0.022
8.09
PO4
1/25/22
0.006
0.50
0.19
0.015
5.49
P12
1/25/22
0.009
0.20
0.43
0.004
1.46
P20R
1/25/22
0.016
0.10
0.32
0.005
1.83
P28
1/25/22
0.010
0.30
0.17
0.018
6.44

Table 5. Field -Water Quality Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Well
Number
Sample
Date
pH
Temp-
erature
(degrees
Celsius)
Specific
Conductance
(µS)
Dissolved
oxygen
(mg/L)
Turbidity during
collection of
organic samples
(ntu)
Turbidity during
collection of
metals samples
(ntu)
MWiR
1/26/2022
5.15
15.9
65.4
5.29
8.37
8.37
MW3
1/26/2022
4.53
16.2
93.5
3.36
16.2
16.2
1/25/2022
6.75
16.6
2034
6.10
signal too low
--
MW6R
1/26/2022
--
--
--
--
--
15.0
MW8
1/26/2022
4.32
15.1
71.6
4.36
121
121
P02
1/26/2022
4.43
17.3
52
4.26
69
69
1/25/2022
4.77
15.9
62.7
5.99
8.5
--
PO4
1/26/2022
--
--
--
--
--
2.28
P05
1/26/2022
4.73
14.9
39.7
10.13
104
--
P06
1/26/2022
5.38
15.7
91.4
3.08
260
--
P07
1/26/2022
3.88
17.3
167.6
2.96
319
319
P09
1/26/2022
4.26
16.0
115.3
7.92
92.9
92.8
P11R
1/26/2022
4.67
15.8
88.7
9.83
227
227
1/25/2022
7.32
17.4
67.2
5.68
182
182
P12
1/26/2022
--
--
--
--
--
27.9
P13
1/26/2022
5.27
15.9
45.9
4.49
300
300
P13D
1/26/2022
5.66
17.2
69.1
4.97
58.9
58.9
P16R
1/25/2022
6.68
16.2
5713
3.37
out of range +1000
--
1/26/2022
--
--
--
--
--
26.8
P17
1/26/2022
5.35
15.0
192.7
5.42
183
183.00
1/25/2022
3.97
16.3
1312
5.06
278
--
P19
1/26/2022
--
--
--
--
--
5.75
1/25/2022
6.18
18.0
1939
3.87
881
--
P20R
1/26/2022
--
--
--
--
--
17.8
P20D
1/26/2022
5.59
16.7
55.7
1.20
19.4
19.4
P21
1/26/2022
4.79
14.8
65.6
7.54
64.8
64.8
1/25/2022
5.28
18.6
30.1
4.53
64.8
--
P23
1/26/2022
--
--
--
--
--
8.38
1/25/2022
5.26
13.8
66.6
5.60
out of range +1000
--
P28
1/26/2022
--
--
--
--
--
235
1/25/2022
4.96
14.7
2898
4.76
72.6
--
P29
1/26/2022
--
--
--
--
--
6.57
SW1
1/26/2022
5.43
8.70
178.9
12.17
6.20
6.20
SW2
1/26/2022
5.69
4.10
498.8
15.39
9.13
9.13
SW4
1/25/2022
5.93
6.90
119.7
6.59
7.80
7.80
PZ1
1/26/2022
3.50
6.20
1066
11.29
1.11
1.11
PZ2
1/26/2022
5.80
6.20
861
13.15
4.83
4.83

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
CAS
2L
IMAC
MCL
Calculated
Number
Name
Other Names
Std.
(Ng/L)
GWP Std
67-64-1
Acetone
2-Propanone
6000
--
--
--
107-13-1
Acrylonitrile
Acrylonitrile
--
--
--
--
7440-36-0
Antimony
Antimony
--
1
6
--
7440-38-2
Arsenic
Arsenic
10
--
10
--
7440-39-3
Barium
Barium
700
--
2000
--
71-43-2
Benzene
Benzene
1
--
5
--
7440-41-7
Beryllium
Beryllium
--
4
4
--
Bromochloromethane;
74-97-5
Chlorobromethane
Methane, bromochloro-
--
--
--
0.6
Bromodichloromethane;
Methane, bromodichloro
0.6
--
80
--
75-27-4
Dichlorobromomethane
Bromoform;
75-25-2
Tribromomethane
Methane, tribromo-
4
--
80
--
7440-43-9
Cadmium
Cadmium
2
--
5
--
75-15-0
Carbon disulfide
Carbon disulfide
700
--
--
--
56-23-5
Carbon tetrachloride
Methane, tetrachloro-
0.3
--
5
--
108-90-7
Chlorobenzene
Benzene, chloro-
50
--
100
--
Chloroethane; Ethyl
Ethane, chloro-
3000
--
--
--
75-00-3
chloride
Chloroform;
67-66-3
Trichloromethane
Methane, trichloro-
70
--
80
--
7440-47-3
Chromium
Chromium
10
--
100
--
7440-48-4
Cobalt
Cobalt
--
1
--
--
7440-50-8
Copper
Copper
1000
--
1300
--
Dibromochloromethane;
Methane, dibromochloro
0.4
--
80
--
124-48-1
Chlorodibromomethane
1,2-Dibromo-3-
Propane, 1,2-dibromo-3-
96-12-8
chloro ro ane; DBCP
chloro-
0.04
--
0.2
--
1,2-Dibromoethane;
Ethane, 1,2-dibromo-
0.02
--
0.05
--
106-93-4
Ethylene dibromide; EDB
o-Dichlorobenzene; 1,2-
Benzene, 1,2-dichloro-
20
--
600
--
95-50-1
Dichlorobenzene
p-Dichlorobenzene; 1,4-
106-46-7
Dichlorobenzene
Benzene, 1,4-dichloro-
6
--
75
--
trans-1,4-Dichloro-2-butene
2-Butene, E4-dichloro-,
110-57-6
1,1-Dichloroethane;
75-34-3
1 Eth Ididene chloride
Ethane, 1,1-dichloro-
6
--
--
--

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
IMAC
DEQ
CAS
2L
(Ng/L)
MCL
Calculated
Number
Name
Other Names
Std.
GWP Std
1,2-Dichloroethane;
Ethane, 1,2-dichloro-
0.4
--
5
--
107-06-2
Ethylene dichloride
1,1-Dichloroethylene; 111-
Ethene, 1,1-dichloro-
350
--
7
--
75-35-4
Dichloroethene•
cis-1,2-Dichloroethylene;
Ethene, 1,2-dichloro-,(Z)
70
--
70
--
156-59-2
cis-l2-Dichloroethene
trans-1,2-Dichloroethylene;
Ethene, 1,2-dichloro-,(E)
100
--
100
--
156-60-5
trans-l2-Dichloroethene
78-87-5
1,2-Dichloropropane
Propane, 1,2-dichloro-
0.6
--
5
--
cis-1 3-Dichloropropene
1-Propene, 1,3-dichloro-
0.4
--
--
--
10061-01-5
Z -
trans-1,3-Dichloropropene
1-Propene, 1,3-dichloro-
0.4
--
--
--
10061-02-6
E -
100-41-4
Ethylbenzene
Benzene, ethyl-
600
--
700
--
2-Hexanone; Methyl butyl
2-Hexanone
--
40
--
--
591-78-6
ketone
7439-92-1
Lead
Lead
15
--
15
--
Methyl bromide;
Methane, bromo-
--
10
--
--
74-83-9
Bromomethane
Methyl chloride;
Methane, chloro-
3
--
--
--
74-87-3
Chloromethane
Methylene bromide;
Methane, dibromo-
--
70
--
--
74-95-3
Dibromomethane
Methylene chloride;
Methane, dichloro-
5
--
5
--
75-09-2
Dichloromethane
Methyl ethyl ketone; MEK;
78-93-3
2-Butanone
2-Butanone
4000
--
--
--
Methyl iodide;
Methane, iodo-
--
--
--
--
74-88-4
Iodomethane
4-Methyl-2-pentanone;
2-pentanone, 4-methyl-
--
100
--
--
108-10-1
Methyl isobutyl ketone
7440-02-0
Nickel
Nickel
100
--
--
--
7782-49-2
Selenium
Selenium
20
--
50
--
7440-22-4
Silver
Silver
20
--
--
--
100-42-5
Styrene
Benzene, ethenyl-
70
--
100
--
1,1,1,2-Tetrachloroethane
Ethane 1112-
__
1
__
630-20-6
tetrachloro�
1,1,2,2-Tetrachloroethane
Ethane 1 1 2 2-
0.2
79-34-5
tetrachloro�

Table 6. Appendix I Target Parameters
Pitt County Municipal Solid Waste Landfill, Pitt County, NC (Permit # 74-01)
Groundwater Protection
Standards'
DEQ
CAS
2L
IMAC
MCL
Calculated
Number
Name
Other Names
Std.
(Ng/L)
GWP Std
Tetrachloroethylene;
Tetrachloroethene;
Ethene, tetrachloro-
0.7
--
5
--
127-18-4
Perch loroeth lene
7440-28-0
Thallium
Thallium
--
0.2
2
--
108-88-3
Toluene
Benzene, methyl-
600
--
1000
--
1,1,1-Trichloroethane;
71-55-6
Meth (chloroform
Ethane, 1,1,1-trichloro-
200
--
200
--
Trichloroethylene;
79-01-6
Trichloroethene
Ethene, trichloro-
3
--
5
--
79-00-5
1,1,2-Trichloroethane
Ethane, 1,1,2-trichloro-
--
0.6
5
--
Trichlorofluoromethane;
Methane,trichlorofluoro-
2000
--
--
--
75-69-4
CFC-11
96-18-4
1,2,3-Trichloropropane
Propane, 1,2,3-trichloro-
0.005
--
--
--
7440-62-2
Vanadium
Vanadium
--
0.3
--
--
108-05-4
Vinyl acetate
Acetic acid, ethenylester
--
88
--
--
75-01-4
VIIIYI uliviluc,Ethene,
chloro-
0.03
--
2
--
7440-66-6
Zinc
Zinc
1000
--
--
--
1330-20-7
Xylene (total)
Benzene, dimethyl-
500
--
10000
All units are in micrograms per liter (pg/L)
2L STD = 15A NCAC 2L groundwater standard
'Applicable Groundwater Protection Standard is the lower of the listed standards.

Table 7. List of Compounds Detected during the January 2022 Sampling Event (1/25-26/2022)
Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well
ID
Date
Parameter
Results
(Ng/L)
MDL
(Ng/L)
NC 2L or 213
Std*(Ng/L)
IMAC
(Ng/L)
MCL
(Ng/L)
Groundwater Samp/es
EB
1/26/2022
Carbon Disulfide
6.00
1.5
700
-
1/26/2022
Zinc Total
81.50
4.4
1000
5000#
FB
1/26/2022
1,4-Dioxane
1.5 J
0.8
3
-
MW6R
1/25/2022
1,4-Dioxane
6.7
0.8
3
-
1/26/2022
Barium Total
1950
1.1
700
-
2000
1/25/2022
Barium Total
83.4
1.1
700
-
2000
PO4
1/25/2022
Beryllium Total
0.2053
0.16
-
4
4
1/25/2022
Zinc Total
8.961
4.4
1000
-
5000#
1/26/2022
Barium Total
116
1.1
700
-
2000
1/26/2022
Beryllium Total
2.67
0.16
-
4
4
1/26/2022
Cobalt Total
10.2
1.4
-
1
-
P11R
1/26/2022
Lead Total
4.08 J
3.10
15
-
15
1/26/2022
Nickel Total
6.86 J
2.2
100
-
-
1/26/2022
Vanadium Total
3.383
1.4
-
0.3
-
1/26/2022
Zinc Total
79.7
4.4
1000
-
5000#
1/25/2022
1,4-Dioxane
0.871
0.8
3
-
-
1/26/2022
Barium Total
25.3
1.1
700
-
2000
P12
1/26/2022
Beryllium Total
0.7783
0.16
-
4
4
1/26/2022
Lead Total
3.203
3.10
15
-
15
1/26/2022
Zinc Total
5.231
4.4
1000
-
5000#
1/25/2022
1,4-Dioxane
78
0.8
3
-
-
1/25/2022
Acetone
153
10
6000
-
-
1/26/2022
Barium Total
1010
1.1
700
-
2000
P16R
1/25/2022
Benzene
2.4
0.15
1
-
5
1/26/2022
Chromium Total
2.02 J
1.4
10
-
100
1/26/2022
Cobalt Total
2.623
1.4
-
1
-
1/26/2022
Nickel Total
9.87 J
2.2
100
-
-
1/25/2022
Toluene
0.441
0.14
600
-
1000
1/26/2022
1,4-Dioxane
4.8
0.8
3
-
-
1/26/2022
Barium Total
225
1.10
700
-
2000
1/26/2022
Beryllium Total
2.86
0.16
-
4
4
P17
1/26/2022
Chlorobenzene
2.2
0.17
50
-
100
1/26/2022
Lead Total
4.70 J
3.10
15
-
15
1/26/2022
Vanadium Total
3.613
1.4
-
0.3
-
1/26/2022
Zinc Total
10.8
4.4
1000
-
5000#
1/25/2022
1,1-Dichloroethane
3.2
0.13
6
-
7
1/25/2022
1,4-Dichlorobenzene
4.8
0.19
6
-
-
1/25/2022
1,4-Dioxane
180 D'S
4.0
3
-
-
1/26/2022
Barium Total
1500711.10
700
-
2000
1/25/2022
Benzene
3.4
0.15
1
-
5
1/26/2022
Beryllium Total
12.5
0.16
-
4
4
1/25/2022
Chlorobenzene
16
0.17
50
-
100
1/26/2022
Cobalt Total
1.40
-
1
-
P19
1/25/2022
Eth (benzene
1.4
0.13
600
-
700
1/26/2022
Lead
3.963
3.10
15
-
15
1/25/2022
m, -X lenes
0.543
0.17
500
-
-
1/26/2022
Nickel Total
22.4
2.2
100
-
-
1/25/2022
o-X lene
0.883
0.065
500
-
-
1/26/2022
Selenium Total
3.12
1.82
20
-
50
1/25/2022
Toluene
0.433
0.14
600
-
1000
1/25/2022
X lenes Total
1.4 J
0.45
500
-
-
1/26/2022
Zinc Total
98.7
4.4
1000
-
5000#
1/25/2022
1,4-Dichlorobenzene
3.0
0.19
6
-
-
1/25/2022
1,4-Dioxane
62
0.8
3
-
-
1/25/2022
Benzene
1.3
0.15
1
-
5
P20R
1/26/2022
Barium Total
887
1.1
700
-
2000
1/26/2022
Cobalt Total
2.061
1.40
-
1
-
1/26/2022
Lead Total
4.413
3.10
15
-
15
1/26/2022
Nickel Total
8.153
2.2
100
-
-

Table 7. List of Compounds Detected during the January 2022 Sampling Event (1/25-26/2022)
Southern Unit of the Pitt County Municipal Solid Waste Landfill (Permit #74-01)
Well
ID
Date
Parameter
Results
(Ng/L)
MDL
(Ng/L)
NC 2L or 213
Std*(Ng/L)
IMAC
(Ng/L)
MCL
(Ng/L)
1/26/2022
Barium Total
49.0
1.1
700
-
2000
1/26/2022
Beryllium Total
3.05
0.16
-
4
4
P20D
1/26/2022
Chromium Total
3.883
1.4
10
-
100
1/26/2022
Vanadium Total
3.663
1.4
-
0.3
-
1/26/2022
Zinc Total
16.6
4.4
1000
-
5000#
1/26/2022
Barium Total
52.4
1.1
700
-
2000
1/26/2022
Beryllium Total
0.9823
0.16
-
4
4
1/26/2022
Chromium Total
2.653
1.4
10
-
100
1/26/2022
Cobalt Total
3.403
1.40
-
1
-
P28
1/26/2022
Lead Total
5.173
3.10
15
-
15
1/26/2022
Nickel Total
2.863
2.2
100
-
-
1/26/2022
Vanadium Total
4.613
1.4
-
0.3
-
1/26/2022
Zinc Total
20.5
4.4
1000
-
5000#
1/25/2022
1,4-Dichlorobenzene
1.5
0.19
6
-
-
1/25/2022
1,4-Dioxane
180 D
4.0
3
-
-
P29
1/26/2022
Barium Total
602
1.1
700
-
2000
1/25/2022
Benzene Total
2.0
0.15
1
-
5
1/25/2022
Chlorobenzene
10
0.17
50
-
100
1/26/2022
Vanadium Total
9.153
1.4
-
0.3
-
PZi
1 1/26/2021
1,4-Dioxane
1.5 J
1 0.8
3
-
-
Surface Water Samples
1/26/2022
Barium Total
50.8
1.1
21,000+
-
2000
1/26/2022
Beryllium Total
0.2413
0.16
6.5
-
4
SWi
1/26/2022
Cobalt Total
8.633
1.4
4
-
-
1/26/2022
Lead
3.53 J
3.1
0.54"
-
-
1/26/2022
Nickel Total
2.883
2.2
16.10"
-
-
1/26/2022
Zinc Total
36.1
4.4
36.5-
-
5000#
1/26/2022
Barium Total
44.4
1.1
21,000+
-
2000
SW2
1/26/2022
Chromium Total
6.023
1.4
23.81"
-
-
1/26/2022
Copper Total
1.993
1.6
2.74-
-
1300
1/26/2022
Zinc Total
11.6
4.4
36.5"
-
5000#
MDL = Method Detection Limit MCL = Federal Maximum Contaminant Level
IMAC = Interim Maximum Allowable Concentration
J = The analyte was positively identified, but the value is estimated below the reporting limit.
*15A NCAC 2L groundwater standards are listed for all groundwater sampling locations. 15A NCAC 213 standards are listed for
surface water sampling locations (SW3 and SW2).
Value represents an EPA action level.
#Value represents an EPA secondary Maximum Contaminant Level
+NC In -Stream Target Value for Surface Waters
"Hardness -dependent metal standard calculated assuming an in -stream hardness of 25 mg/L of CaCO3
Concentrations highlighted in yellow were detected above the 2L (or 213) standards.
Concentrations highlighted in orange were detected above the IMAC.
Concentrations highlighted inblue were detected above the EPA MCL.

APPENDIX A
CORRESPONDENCE FROM THE
NC DIVISION OF WASTE MANAGEMENT

Waste Management
ENVIRONMENTAL QUALITY
March 16, 2017
Sent Via Email — iohn.demary@pittcountync.�ov
Mr. John Demary
Pitt County Director of Solid Waste & Recycling
3025 Landfill Road
Greenville, NC 27834
Re: Proposal for Assessment of Benzene Contamination Migration
Pitt County MSW Landfill (Northern and Southern)
Pitt County
Solid Waste Permit Number 74-01
DIN 27529
Dear Mr. Demary:
ROY COOPER
MICHAEL S. REGAN
Sec retao
MICHAEL SCOTT
Director
The NC Solid Waste Section has completed a review of the Proposal for Assessment of Benzene
Contamination Migration dated March 15, 2017 (DIN 27528) submitted on your behalf by Groundwater
Management Associates, Inc. (GMA) for the closed Pitt County MSW Landfill, NC Solid Waste Permit
Number 7401. During the January 2017 semiannual water quality monitoring event benzene was
detected at concentrations exceeding the NC 2L Groundwater Standards in two groundwater monitoring
wells.
Based upon the groundwater exceedances, Pitt County is requesting to collect two pore water samples
from the beneath the southern boundary ditch and analyze for Appendix I constituents. The proposed
sampling locations are located downgradient of groundwater monitoring well P20R and will be sampled
during the July 2017 semiannual water quality monitoring event.
As a result, the Proposal for Assessment of Benzene Contamination Migration is approved as described. If
you have any questions, please feel free to contact me by email at [e-mail] or
by phone at 828.296.4706. Thank you for your continued cooperation with this matter.
Sincerely,
L)4—
Jaclynne Drummond
Compliance Hydrogeologist
Solid Waste Section, Division of Waste Management
NCDEQ
State of North Carolina I Environmental Quality I Waste Management
Asheville Regional Office 1 2090 U.S. Highway 70 1 Swannanoa, NC 28778
828 296 4500

cc sent via email: Tim Corley, Pitt County Engineer
Jason Watkins, Field Operations Branch Head
Drew Hammonds, Eastern District Supervisor
Ray Williams, Environmental Senior Specialist
Elizabeth Werner, Permitting Hydrogeologist
Emma Shipley, GMA
Steve Campbell, GMA
tit�dcr71 Nnrdt['au'ullns I lawlt'ruur►rntnlQuellty i Wastrti4annyrurrut
n.+i*Y111e Rcwrw,at 0fhrr 1 AMI U% 1liglmay I0 I Swannwiai► NC AM
eta 1W, asw

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCOTT
Director
NORTH CAROLINA
Environmental Quality
June 26, 2019
Sent Via Email - [e-mail]
Mr. John Demary
Pitt County Director of Solid Waste & Recycling
3025 Landfill Road
Greenville, NC 27834
Re: Proposal for 1,4-Dioxane Assessment and Pilot Study at the Pitt County Municipal Solid
Waste Landfill
Closed and Unlined Pitt County MSW Landfill Northern and Southern Units
Pitt County
Solid Waste Permit Numbers 7401-MSWLF- and 7401-MSWLF-1974
FID 1323161
Dear Mr. Demary,
The Solid Waste Section (Section) has completed a review of the Proposal for 1,4-Dioxane Assessment
and Pilot Study at the Pitt County Municipal Solid Waste Landfill dated June 21, 2019 (FID 1323159)
and submitted on your behalf by Groundwater Management Associates, Inc. for the closed and unlined
Pitt County Landfill, Solid Waste Permit Numbers 7401-MSWLF- and 7401-MSWLF-1974.
To address the 1,4-Dioxane being detected within the groundwater at the landfill, Pitt County is
proposing to:
1) Delineate the vertical and horizontal extent of 1,4-Dioxane by installing two additional groundwater
monitoring wells (Type II and Type III) and six surface water gauges;
2) Initiate a one-year pilot study to determine the effectiveness of cap upgrades and repairs to see if
they have limited the infiltration of rainwater into the soil cap, and if they have reduced leachate
volumes and concentrations. Geophysical testing of the Southern Unit only will also be conducted to
evaluate landfill cap integrity. The County will repair any areas identified by the geophysical testing
and will inspect surface water drainage structures on the mound to ensure that they are operating as
designed. Once repairs are made, geophysical testing will be repeated to document hydrologic
benefits from cap repairs and to determine if the repairs have significantly reduced rainfall infiltration;
and
3) Install two instream piezometers approximately 1.5 feet below the ditch bottom at the locations of
the currently collected porewater samples. The instream piezometers will be used to collect
representative groundwater samples, measure groundwater levels, and determine any discharge
relationships at repeatable locations just below the stream bed.
Based upon a review of the Proposal for 1,4-Dioxane Assessment and Pilot Study at the Pitt County
Municipal Solid Waste Landfill, the Section approves the activities as described. If you have any
questions or concerns regarding this letter, please feel free to contact me by phone at 828.296.4706
or by email at [e-mail]. Thank you for your continued cooperation with this
matter.
G+p�wal ! FMen�Yl � W q�
North Carolina Department ofEnvlronmental Quality 1 Division of Waste Management
Asheville Regional Office 1 2090 U.S. Highway 70 1 Swannanoa: North Carolina 28778
828.296.4500

Sincerely,
L;�4' rc�—�
Jaclynne Drummond
Hyd rogeologist
Solid Waste Section, Division of Waste Management
NCDEQ
cc sent via email: Tim Corley, Pitt County Engineer
Ed Mussler, SWS Chief
Adam Ulishney, SWS Environmental Compliance Branch Head
Jason Watkins, SWS Field Operations Branch Head
Drew Hammonds, SWS Eastern District Supervisor
Ray Williams, SWS Environmental Senior Specialist
Sherri Stanley, SWS Permitting Branch Head
Ethan Caldwell, SWS Permitting Engineer
Emma Shipley, GMA
Dr. Richard Spruill, GMA
Jay Holley, GMA
Epp
North Camllna Gcpartmrm of Envlramrwdal Quality I N+ Won of Wastc Managrrnent
Asheville Reglvna[ Mce 12090 U.5. Hlghway 70 I Swannanoa, North Carolina 28778
82&2q&4500

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
MICHAEL SCOTT
Director
NORTH CAROLINA
Environmental Quality
July 2, 2020
Sent Via Email - [e-mail]
Mr. John Demary
Pitt County Director of Solid Waste & Recycling
3025 Landfill Road
Greenville, NC 27834
Re: Request for Reduced Sampling Frequency of Appendix 11 Constituents
Closed and Unlined Pitt County MSW Landfill Southern Unit
Pitt County
Solid Waste Permit Number 7401-MSWLF-1974
FID 1417776
Dear Mr. Demary,
The Solid Waste Section (Section) has completed a review of the Request for Reduced Sampling
Frequency of Appendix II Constituents dated July 1, 2020 (FID 1417773) and submitted on your behalf
by Groundwater Management Associates, Inc. for the closed and unlined Pitt County Landfill Southern
Unit, Solid Waste Permit Number 7401-MSWLF-1974.
In accordance with 15A NCAC 13B .1634 a request was provided to the Section to modify the
groundwater monitoring frequency for the full set of Appendix II constituents because no Appendix II
constituents have been detected since 2014. Pitt County is requesting to sample for Appendix II
constituents on a biennial basis with the next scheduled Appendix II sampling event occurring during
July 2022. The County will continue to sample for Appendix I parameters and for 1,4-dioxane on a
semi-annual basis.
Based upon a review of the Request for Reduced Sampling Frequency of Appendix 11 Constituents, the
Section approves the request as written at this time. If you have any questions or concerns regarding
this response letter, please feel free to contact me by phone at 828.296.4706 or by email at
[e-mail].
Sincerely,
1
Jaclynne Drummond
Hyd rogeologist
Solid Waste Section, Division of Waste Management
NCDEQ
cc sent via email: Tim Corley, Pitt County
G+p�wal ! FMen�Yl � W q�
North Carolina Department ofEnvlronmental Quality 1 Division of Waste Management
Asheville Regional Office 1 2090 U.S. Highway 70 1 Swannanoa: North Carolina 28778
828.296.4500

Adam Ulishney, SWS Environmental Compliance Branch Head
Jason Watkins, SWS Field Operations Branch Head
Drew Hammonds, SWS Eastern District Supervisor
Ray Williams, SWS Environmental Senior Specialist
Ethan Caldwell, SWS Permitting Engineer
Emma Shipley, GMA
North Carull na Oepan menl of Erntronmental Quality I DWsion of Waste Ktamgeme nl
Asheville Reylunal DMre 1 2090 US. Righwiv 70 1 Sw mmnua, North Ca llmk 28778
829-296g5pP

APPENDIX B
SAMPLING RECORDS

GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet
Sample ID: MW1R Field Team Members:
Date: J -Z(G - 2 -,L
Llama- C,--s5
Rel tall Initials Duties (check all that apply)
Notes 67,Water Level 4Yfield Parameters EXample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: ci�, Appendix I ❑ Appendix II ❑ Delayed Metals?
Sample Type: zK Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: &N PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 52.98 ft Diameter: 2 in Screen interval: 40.0 - 50.0 ft BLS
QQ Water Level
Water Level: 2) ft Water Level Date: I - Z5 -Z-L time: l' 2 ,Z0.
-
Water Column yy.e-- ft 3 Well Volume
I .cal gal
Puma Parameters continue on rid below, if necessary)
Bails
pH
(S.U.$)
Sp. Cond.
(µS/cm)
ORP
(mvolts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTLI)
?
Dry'
Comments- Purge Volume
(gal)
1st Bail
5r -,-7
5'2 ,`7
1?:5'
Well
Volume
Volume
5 . t
VAC"CA
1 • � U
and Well
Volume
S^ '
.�
7
?s
J. N
« c r.3
7
Sample Collection bate/Time;
1- 2(o -ZZ. E,
Delayed Metals Collection Date/Time:
L horatory Analysis & Containers:
All samples preserved
GAII samples placed on ice/cooler
Notes/Maps etc.:
NC T
a. Irl
Turbidity during Metals Collection:
Lab Analysis
Container T e
No. of Containers
Preservation
8260Q A I
VOAS
3
HCl
,r
$260Q SIM IQ
1 4-dioxane
VQAS
3
HCl
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
IL Amber
2
n/a
3 Vols (in gallons) = 70.5 rzh = 0.4856745 * h *Use Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
Z:\GMAVSD0(-RrrT COU"75101 - LANDHLL�METHDDS & BLANK WELL SAMPLING FORMS�WELL SAMPLING FORM -BAILING 20220124.0000

GMA #25101 - Pitt County Landfill - Sample Collection Field Sheet
Date: I ` 2 I-P -2 7—
q8
-Z
Sample ID: MW3
Field Team Members:
LI+9,� C75
F"el toff Initials Duties (check all that apply)
Mates <<,�- •Water Level cE�,,Field Parameters OSample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: LI, Appendix I ❑ Appendix II ❑ Delayed Metals?
Sample Type: d0—Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: �4- PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well info:
Total Depth + Well
Stickup (ft): 47.47 ft Diameter: 2 in Screen interval: 35.0 - 45.0 ft BLS
Water Level
Water Level: ft Water Level Date: f - ZS -2Z time: E; -. a I
Water Column 38,4125 ft 3 Well Volume I F3 , �i gal
Purge Parameters continue on 90d
below, if necessary)
Bails
pH
(5.U.$)
Sp. Cond.
(gSJcm)
ORP
(m►►olts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTU)
Dry"
Comments- Purge Volume
(gal)
1st Bai I
�'
C
�►+ l
I�
�r� . I �G'
2nd Well
Volume
�� c�
rq, L
171.5
? ,�'5
1 S ' 3
4
Sample Collection Date/Time: L &---22 ``' 8,r l
Delayed Metals Collection Date/Time: Turbidity during Metals Collection:
L!�oratory Analysis & Containers:
Z11 samples preserved
ll samples placed on ice/cooler
Notes/Maps etc.:
Lab Analysis
Container Type
No. of Containers
preservation
8260D App I
VOAs
3
HCI
8260D SIM ID
1 4-dioxane
VOAS
3
HCl
Er
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
n/a
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h *Use Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
Z;\GMAj251*(-Prrr COLIMY7 25101 - LAN OFILLNMErHOD5 &BLANK WELL SAMPLING FORM%WELL SAMPLING F0RM_6AILING_20220124.004f

GMA #25101 - Pitt County Landfill - Sample Collection Field Sheet
Sample ID: MW6R
Date: 1- ZS - 4 z
Field Team Members: ! its -.�-G
Field -staff Initials Duties (check all that apply)
Ei Notes D ' ater Level &Tffeld Parameters i9-Sampie Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
I �
Sampling For: Fs Appendix I �r�' Appencfi 3T E�` Delayed Metals?
Sample Type: CF Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: ❑ PVC Bailer Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 19.79 ft Diameter: 2
Water Level: ft Water Level Date: 1-2-5-2 Z
Water Column Z .Irs-� ft 3 Well Volume • 1
in Screen interval: 7.0 - 17.0 ft 81-5
Water Level
time: 1
gal
Purge Parameters continue on grid below, if necessary)
Bails
pH
(S.U.$)
Sp. Cond.
(AS/cm)
ORP
(mvolts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTU)
Dry"
Comments- Purge Volume
(gal)
1st Bail
Z"d Well
Volume
•
26 I�
4
D
`
r��
S iG
�icy
3'd Well
Volume
(v
�C���f
�i�a�
�v • ��
�G- i
5 i n'L I
i-aca.�
Sample Collection Date/Time: � - 2 S 2Z Qom'_j(o: ZC
Delayed Metals Collection Date/Time: - 1g1gTurbidity during Metals Collection: V 7 c:
Laboratory Analysis & Containers:
A I samples preserved
f3 All samples placed on ice/cooler
Notes/Maps etc.:
'-Mewcq P.C'1UVeD
Lab Analysis
Container Type
No. of Containers
Preservation
CY
8260D App I
VOAs
3
HCI
8260D SIM ID
1 4-dioxane
VOAs
3
HCl
App I Metals
250 mL Plastic
i
HNO3
❑
App II Pesticides
IL Amber
2
n/a
3 Vols (in gallons) = 70.5 r2h - 0.4856745 * h *Use Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App I1 collected every other July starting in 2022.
Z:�GMA�251XX-Prrr COUNTA2S101 - LAN DFILL�METHG DS & BLANK WELL SAMPLING FORMS�WELLSAMPLING FORM BAILTNG_20Z2U12gmCX

1 z
M
GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet
Sample ID: MW8
Field Team Members:
Date: t —Z(AO —ZZ
L1 DJ- C-73
F'el tall Initials Duties (check all that apply)
.PNotes `Water Level -O!f-Field Parameters cigample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For. d&_ Appendix I ❑ Appendix II ❑ Delayed Metals?
Sample Type: Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: &'- PVC Bailer ❑ Teflon Bailer ❑ Submersible pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 16.79 ft Diameter: 2 in Screen interval: 4.0 -14.0 ftBLS
Water Level
Water Level: . 19 ft water Level Date: I - 2S --2 Z time: 30
water Column 9 •(12 0 ft 3 Well Volume Lj .--q` gal
Purge
Parameters continue on grid below, if
necessary)
Bails
pH
(S.U.$)
Sp. Cond.
(VS/cm)
ORP
(mvolts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTU)
Dry'
Comments- Purge Volume
(gal)
1st Bail
�51 ,�
,
t �.�
f. �'
nd
Volume)
Ll, J
7 I r
�r7(' .
t`)
t'
!*�(:
Volume)3rd We]
�y W.
!�
I
c
Sample Collection Date/Time: 1—ZL=- Zl-- ('' f4 •
Delayed Metals Collection Date/Time:
La oratory Analysis & Containers:
3ll samples preserved
-El All samples placed on ice cooler
Notes/Maps etc.:
Turbidity during Metals Collection:
Lab Analysis
Container Type
No. of Containers
Preservation
EY
8260D App I
VOAs
3
HCI
8260D 5IM ID
1 4-dioxane
VOAs
3
HCI
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
IL Amber
2
n/a
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h *Use Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
Z:1GMA\251XX-PITT COUNTYX251M-1ANDFILL\ME7NODS & BLANK WELL SAMPLING FORMS�WELL SAMPLING F0RM_8AILING_W220124.O0CY

V
GMA #25101 - Pitt County Landfill - Sample Collection Field Sheet
Sample ID: R2
Field Team Members:
Date: 1 —2G —7—Z
U 0 4- C3 S
Reld,,Staff initials Duties (check all that apply)
dotes -E�,1later Level Field Parameters C 2tampfe Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: P",- Appendix I ❑ Appendix II ❑ Delayed Metals?
Sample Type: CtY-, Monitoring Well ❑ Surface Water ❑ Temporary Piexometer
Collection Method: iW,, PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 19.05 ft Diameter: 2 in Screen interval: 11.0 - 15.0 ft BLS
Water Level
Water Level: ft Water Level Date: r - 2$ -22- time: OC]
Water Column + ft 3 Well Volume 5A gal
Purge Parameters continue on grid below, if
necessary)
Bails
pH
(S.U.S)
Sp. Cond.
(µS/cm)
ORP
(mvolts)
DO
(mg/l)
Temp
VC)
Turgidity
(NTU)
?
Dry'
Comments- Purge Volume
(gal)
1 Bail
y.
3 Z
iS y77
2"d Well
Volume
�'L
S?
3'd Wei I
Volume
�` 3
�:
Otis `�1
C� 2
I❑ _�
{��1.c.
Sample Collection Date/Time: I " &'"2 Z `j t ''S
Delayed Metals Collection Date/Time:
tioratory Analysis & Containers:
All samples preserved
,�/
L"J All samples placed on ice/cooler
Notes/ Maps etc.:
Turbidity during Metals Collection:
Lab Analysis
Container Type
No. of Containers
Preservation
8260D App I
VOAs
3
HCl
8260D SIM ID
14-dioxane
VOAs
3
HCl
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
I Amber
2
n/a
3 Vols (in gallons) = 70.5 r2h = 0,4856745 * h *Use Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
Z:NGMA\251XX-PrTTCOUNTYX25101-LANOFILLIMETHODS&BLAN KWELL SAMPUNGrORMSIWELLSAMPLING FORM MLING_20220124.D0CX

e;
GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet Date:
Sample ID: P4 Field Team Members: L n ' _5
Fie Staff Initials Duties (check,all that apply)
� D/Notes &6ater Level VField Parameters ❑ Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: E**' Appendix I ❑ Appendix 11 M amDelayed Metals?
Sample Type: I Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: ❑ PVC Bailer VTeflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 21.52 ft Diameter: 2 in Screen interval: 8.0 -18.0 ft BLS
Water Level
Water Level: _p. ft Water Level Date: 2 time: 1 ,
Water Column j ` ,*3 5 ft 3 Well Volume '-f . I j gal
Purge Parameters continue on grid
below, if necessa
Bails
pH
Sp. Cond.
DRP
DO
Temp
Turbidity
Dry?
ry
Comments- Purge Volume
(S.IJ.$)
(µS/cm)
(mvolts)
(mg/1)
(°C)
(NTLI)
(gal)
1st Bail
j, J �
ca
I
29=
I & tc
6. %
2"d Well
t
"l�.`4
.yeS.
'
ts
-7ryZVolume
3rdwell
Volume
y
�i Z,�-
-�
, 7
5•9C`3 l
�j
qq
men -weed 6
Z3; � ba61
Sample Collection Date/Time: /'-25 - 47 "' 9 3+
Delayed Metals Collection Date/Time: �2z_6_j.1u+13 Turbidity during Metals Collection: = - • - �
�jboratory Analysis & Containers:
f�l All samples preserved
BfAll samples placed on ice/cooler
Notes/Maps etc.:
fen ed-kii7',I►
Lab Analysis
Container Type
No. of Containers
Preservation
8260D App I
VOAs
3
HCl
8260D 5IM I❑
1 4-dioxane
VOAs
3
HCI
ETr
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
n/a
3 Vols (in gallons) = 70.5 rah = 0,4856745 * h
All wells 2" in diameter. Use r = 0.083 feet
*Use Teflon bailers for delayed metals
App II collected every other July starting in 2022.
Z:NGMA%25=-PrrT COUNTY625101 - LANRFILL%METHOD5 & BLANK WELL SAMPLING FORMS�WELL SAMPLING FCRM_BAILING_20220124.DOC7C

/s
23
GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet
Sample ID: P5 Field Team Members:
Date:
Fi d- aff Initials Duties (check all that apply)
GZ�,Notes eRr%ater Level zO�Eield Parameters Sample Collection ❑ Other
❑ Notes ❑ Water level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: cL-?e, Appendix I ❑ Appendix II ❑ Delayed Metals?
Sample Type: d2L Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: &?'- PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth +
Stickup (ft):
Well
17.14 ft Diameter:
Water Level: D - / cI ft Water Level Date:
Water Column //• qS ft 3 Well Volume
2 in Screen interval: 8.5 - 13.5 ft BLS
Water Level
ZZ time:
—gal
Pur a Parameters continue on rid below, if
necessary)
Bails
pH
(S.U.$)
Sp. Cond.
(,IS/cm)
ORP
(mvolts)
DO
(mg/0(°C)
Temp
Turbidity
(NTU)
Dry?
Comments- Purge Volume
(gal)
1-%T Bail
c
y2.
-7,
S Q
2nd Well
Volume
�' L�
C �.�
i .�
�,13
I .c
y2
Yoluvmeel l
Lt.�.
J9.4
jC��.2_
)C i
1q.9
/LPL!
Sample Collection Date/Time: L"' 17 1 rI
Delayed Metals Collection Date/Time:
Laboratory Analysis & Containers:
Vit samples preserved
ll samples placed on ice/cooler
Notes/ Maps etc.:
Turbidity during Metals Collection:
Lab Analysis
Container Type
No. of Containers
Preservation
ET
8260D App I
VQAs
3
HCl
Eye
8260D SIM ID
14-dioxane
VOAs
3
HCI
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
11-Arnber
2
n/a
3 Vols (in gallons) = 70.5 r 2 h = 0.4856745 * h *Use Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
Z.1GMA1 SIXX-P117 COUNTYj25101 - YANDFILL�METHODS & BLANK WELL SAMPLING FORMSjWELL SAMPLING FORM_BAILING_202241Z4.DQa

19
M
i
GMA #25101 - Pitt County Landfill - Sample Collection Field Sheet
Sample ID: P6
Date: I -Z 6 _2- Z
(Field Team Members: L 10 .4- C35
Field
_Staff Initials Duties (check all that apply)
dates ct�i4ater Level KField Parameters ::,f�ample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: c21— Appendix I ❑ Appendix II ❑ Delayed Metals?
Sample Type: eE3'-- Monitoring Well ❑ Surface Water ❑ Temporary Piezorneter
Collection Method: cR, PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Weil Info:
Total Depth + Well
Stickup (ft): 17.72 ft Diameter: 2 in Screen interval: 8.5 -14.5 ft BLS
Water Level
Water Level: g , 31 ft Water Level Date. - ZS -2 Z time, L4
Water Column , Ll ft 3 Well Volume y , (D gal
Purge Parameters continue on grid below, if necessa
Bails
pH
(S.U.$)
Sp. Cond.
(JASjcm)
ORP
(mvolts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTII)
a
Dry'
Comments- Purge Volume
(gal)
1st Bail
�.�Z
`lt c�
1?z-�
I'j.4"Z
1�_Z
2"d well
Volume
"i �
►z��.[�
�
15 , -.
'--ty �'�
3'd Well
Volume
S.
C��.y
24�C
Sample Collection Date/Time: i -eta Z-Z-
Delayed Metals Collection Date/Time:
Laboratory Analysis & Containers:
ll/ Il samples preserved
0' All samples placed an ice/cooler
Notes/Maps etc.:
Turbidity during Metals Collection:
Lab Analysis
Container Type
No. of Containers
Preservation
8260D App I
VOAs
3
HCl
8260D 5IM ID
1 4-dioxane
VOAs
3
HCl
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
nla
3 Vols (in gallons) = 70.5 r1h = 0.4856745 * h
All wells 2" in diameter. Use r = 0.083 feet
*Use Teflon bailers for delayed metals
App II collected every other July starting in 2022.
Z:\GMA\251xX-PITT COUMM25101- LANDFILL\METHODS & BLANK WELL SAMPLING FORMSIWELL SAMPLING FORM_BAILING 20220124.000(

GMA *2S101 - Pitt County Landfill - Sample Collection Field Sheet
Date: 1-Z(o -2-2-
Izk
Sample ID: P7
Field Team Members: L. j 0 a- CUS
Fi I taff Initials Duties (check all that apply)
;�-Notes &'Water Level .6�-Field Parameters -Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: ❑ Appendix I ❑ Appendix II ❑ Delayed Metals?
Sample Type: 60"-Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: eEY- PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 19.51 ft Diameter: 2 in Screen interval: 11.0 - 16.0 ft 6L5
Water Level: S .
Water Level
y- ft Water Level Date: - 25 Z time: S Li
Water Column i • C,P' ft 3 Well Volumerj . gal
Purge Parameters continue on grid below, if necessary)
Bails
pH
(S.U.$)
Sp. Cond.
(PS/CM)
ORP
(molts)
DO
(mg/0
Temp
(OC)
Turbidity
(NTU)
Dry'
Comments- Purge Volume
(gal)
ist Bail
.I 5
nS77
Vv'L.-L�-
2"d Well
Volumed
1- %,
t� 11
31d Well
Volume-
ll�;'t�
slit/
►� 31��5
ti� �7��V�
Sample Collection Date/Time: 21 ` Su
Delayed Metals Collection Date/Time; - Turbidity during Metals Collection:
Laboratory Analysis & Containers:
2t samples preserved
samples placed on ice/cooler
Notes/Maps etc.:
Lab Analysis
Container Type
No. of Containers
Preservation
8260D App I
VOAs
3
HCi
1(
8260D SIM ID
1 4-dioxa ne
VOAs
3
HCI
App I Metals
250 mL Plastic
1
HNO3
❑
App 1I Pesticides
ILAmber
2
n/a
3 Vols (in gallons) = 70.5 rzh = 0.4856745 * h
All wells 2" in diameter. Use r = 0.083 feet
*Use Teflon bailers for delayed metals
App II collected every other July starting in 2022.
Z:�GMAVSIX (-P TT COUNlYX25101 - LANOFILL\MET-HODS & BLANK WELL SAMPLING FORMSjWELL SAMPLING FORM_BAIUNG_AZ201Z4.000X

15
2-Z
GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet
Sample ID: P9 Field Team Members:
Date: / - 2 �, -2 z
F'el, taff Initials
Duties (check all that apply)
dotes
'ET4Vater Level
Field Parameters
sample Collection ❑ Other
❑ Notes
❑ Water Level
❑ Field Parameters
❑ Sample Collection ❑ Other
Sampling For: 1E
' Appendix I
❑ Appendix II
❑ Delayed Metals?
Sample Type: a
Monitoring Well
❑ Surface Water ❑ Temporary Piezometer
Collection Method:
0, PVC Bailer
❑ Teflon Bailer
❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 1.8.48 ft Diameter: 2 in
Water Level: ,qQ ft Water level Date: 1-25—,?z
Water Column 11-*58 ft 3 Well Volume 5. (o gal
Screen interval: 9.5 - 14.5 ft BLS
Water Level
time: /0 : 3 7-
Purge Parameters continue on qrid below, if
necessary)
Bails
pH
(S.U.$)
Sp. Cond.
(µS/cm)
DRP
(mvolts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTU)
D ry'a
Comments- Purge Volume
(gal)
15t Bail
q. YS-
1 i5--2
I (Arr-�v
to, 4
f -2 •`_i
l 2
2"a Well
Volume
9..5
1��,.�
��••'
5-��
r��
i W Cr
3rdWel
Volume e
Sample Collection Date/Time: / -2C-' -Z Z r ' o`-'
Delayed Metals Collection Date/Time: Turbidity during Metals Collection:
La oratory Analysis & Containers:
Ail samples preserved
0 All samples placed on icelcooler
Notes/Maps etc.:
Lab Analysis
Container Type
No. of Containers
Preservation
8260DAW I
VOAs
3
HG
8260D SIGN ID
14-dioxane
VOAs
3
HCI
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
n/a
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h
All wells 2" in diameter. Use r = 0.083 feet
*Use Teflon bailers for delayed metals
App II collected every other July starting in 2022.
Z:�GMA�25=-PrrTCOUNTY125101- LAN DFILL�ME7HODS & BLANK WELL SAMPLING FORMSIWELL SAMPLING FORM_9AIUNG_20220124-DOCY

15
2�
GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet
Sample ID: P11R
Field Team Members:
Date: / —2(_Z Z
4-1 U a GSA
Feld- aff Initials Duties (check all that apply)
dotes �Ifater Level wield Parameters 4TSample Collection ❑ Other
❑ Notes El Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
F
Sampling For: ' 9 Appendix I ❑ Delayed Metals?
Sample Type: d2�- Monitoring Well ❑ Surface Water ❑ Temporary Piexometer
Collection Method: A�— PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 19.74 ft Diameter: 2
Water level: , Q Z It Water Level Date: _a s-
Water Column r) • -qz ft 3 Well Volume 3-
in Screen interval: 13.0 -16.0 ft BLS
Water Level
time: /0 -'55L
gal
Purge Parameters continue on grid below, if necessary)
Bails
pH
(S.U.$)
Sp. Cond,
(µS/cm)
ORP
(mvolts)
Do
(mg/I]
Temp
(°C]
Turbidity
(NTU)
,
Dry'
Comments- Purge Volume
(gal)
is, Bail
�119
j(=; ��
1 ` CI. �'
I �, 5�'
I z - C�
•13
i i I C_S
Vnlumel
L4
C)l.
�G'
�� 3
51
3rd Well
Volume
Sample Collection Date/Time: J 24c' ­ 2.? 1 Ty ZG
Delayed Metals Collection Date/Time:
La oratory Analysis & Containers:
[XIt samples preserved
II samples placed on ice/cooler
Notes/Maps etc.:
I
Turbidity during Metals Collection:
Lab Analysis
Container Type
No. of Containers
Preservation
8260D App I
VOAs
3
HCl
8260D SIM ID
14-dioxane
VOAs
3
HCl
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
nla
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h
All wells 2" in diameter. Use r = 0.083 feet
*Use Teflon bailers for delayed metals
App II collected every other July starting in 2022.
Z:\GMA�251%X-PLTT CDUNTY125101 - LANDFILL�MMODS & BLANK WELL SAMPLING FORMS�WELL SAMPLING FORM_ MUNG_20220124-DOO

r� a
GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet Date:
Sample ID: P12 Field Team Members: L I L-) d LS.1
Fief Staff Initials Duties (check all that apply)
Cg'1Votes O'Water Level a Field Parameters ER Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
f
Sampling For: ®r Appendix I �Appd"i�e - Delayed Metals?
Sample Type: ,per Monitoring Wed ❑ Surface Water ❑ Temporary Piexometer
Collection Method: ❑ PVC Bailer g�i, Teflon Bailer ❑ Submersible Pump ❑ Gram
Well Info:
Total Depth + Well
Stickup (ft): 20.91 ft Diameter: 2 in
Water Level: ft Water Level Date: 1= j 2 Z
Water Column 171 • �ji ft 3 Well Volume ,_� gal
Screen interval. 10.5 -17.5 ft BLS
Water Level
time: /
Purge Parameters continue on grid below, if necessary)
Bails
pH
(S.U.$)
Sp. Cond.
(µ5/cm)
ORP
(molts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTLI)
Dry?
Comments- Purge Volume
(gal)
15t Bail
+
1`73..4
I;p _ Iv
3. S
12.�
`"I 3 9
YES
`- I S 8r4rCS
Volume)
i , L
{�7.
CGS` y
51
4�j
3rd Weil
Volume
Sample Collection Date/Time: I ZS -22 " 1 3(n
Delayed Metals Collection Date/Time: i-2� "L2 � _i4-10 Turbidity during Metals Collection:
a
Laboratory Analysis & Containers:
I]/All samples preserved
©All samples placed on ice/cooler
Notes/Maps etc.:
/VO 1ut3'NC�
Lab Analysis
Container Type
No. of Containers
Preservation
8260DAppI
VOAs
3
HCI
®/
8260D SIM I❑
1 4-dioxane
VCAs
3
HCI
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
n/a
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h
All wells 2" in diameter. Use r = 0.083 feet
*Use Teflon bailers for delayed metals
App II collected every other July starting in 2022.
Z.�GMA\251XX-PrrT COUNTYN25101 - LANDFILLLMFTMODS & BLANK WELL SAMPLING FORMSIWELL SAMPLING T-ORM_BAILING 20220124MCX

21
GMA #25101- Pitt County Landfill — Sample Collection Field Sheet
Sample ID: P13
Field Team Members:
Date: 1-26 —,? z
L 10 A C3S
Fiel taff Initials Duties (check all that apply)
(K�4otes d� YNater Level Field Parameters •`ample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: eg- Appendix I ❑ Appendix II ❑ Delayed Metals?
Sample Type: Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: .0— PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 19.8 ft Diameter: 2 in
Water Level: ft Water Level Date:
Water Column f ft 3 Well Volume
�-z5-2Z
gal
Screen interval: 11.0 - 16.0 ft BLS
Water Level
time: 0 " 7-:7-
Purge Parameters continue on grid below, if
necessa
Bails
PH
(S.U.$)
Sp. Cond.
(PS/cm)
ORP
(mvolts)
DO
(mg/1)
Temp
VQ
Turbidity
(NTU)
Dry?
Comments- Purge Volume
(gal)
1n Bail
y . c1a�
43.L
I42 `\
`1.4:'-�
1�.�
► vy
2"d Well
Volume
_
'i`is
3"d Well
Volume
t3
j
Sample Collection DatelTime: 1-ZL"- ZL rJ
Delayed Metals Collection Date/Time:
Lapnratory Analysis & Containers:
pg ll samples preserved
All samples placed on ice/cooler
Notes/Maps etc.:
Turbidity during Metals Collection;
Lab Ana! sis
Container Type
No. of Containers
Preservation
8250D A I
VOAs
3
HCl
8260D 5IM ID
1 4-dioxane
VOAs
3
HCI
App I Metals
250 mL Plastic
1 1
HNO3
❑
App II Pesticides
1L Amber
1 2
n/a
3 Vol$ (in gallons) = 70.5 r 2 h = 0.4856745 * h *Use Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
Z:�GMAV51XX-PITTCOUNTYX25101 - LANDFILLIMETHODS & BLANK WELL SAMPLING FORMSLWEL.LSAMPLING F0RM_AMUNG_20220124.D0CX

I
5(o
8�
GMA #25101- Pitt County Landfill - Sample Collection Field Sheet
Sample ID: P13D
Date: 1-26 !Z Z
Field Team Members: L 1 Q a>- CJS
el afi Initials Duties (check all that apply)
&rWbtes 04iVater Level wield Parameters -!!�5ample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: dt- Appendix I ❑ Appendix II ❑ Delayed Metals?
Sample Type: �*- Monitoring Well ❑ Surface Water ❑ Temporary Piexometer
Collection Method: 0-- PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well unknown -
Stickup (ft): 54.97 ft Diameter: 2 in Screen interval: 51.5 ft BLS
Water Level
Water Level: �ft Water Levei Date: �- 2� —Z 2 time: 10ZS
Water Column AL4.89 ft 3 Well Volume 22-. P gal
Purge Parameters continue on grid below, if necessary)
Bails
pH
(S.U.S)
Sp. Cond.
(PS/cm)
ORP
(molts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTU)
Dry?
D
Comments- Purge Volume
(gal)
1st Bail
5 .S-1k
:L-. Lk
i ku,
-v7
15 .1
l 1-oL
nd
20lume umel
Vo
"-
-Z
(olC i
tw.S'
3LS
Volume
UI •
i 2u1. Z�
b .
Sample Collection Date/Time: 7 r
Delayed Metals Collection Date/Time:
Laboratory Analysis & Containers:
Y11 11 samples preserved
® All samples placed on ice/cooler
Notes/Maps etc.:
Turbidity during Metals Collection:
Lab Analysis
Container T e
No. of Containers
Preservation
$2fi0Q A I
VOAs
3
HCI
8250D SIM ID
14-dioxane
V OAs
3
HCl
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
n/a
3 Vois (in gallons) = 70.5 r2h = 0.4856745 * h *Use Teflon hailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other ]uly starting in 2022.
Z:�GMAN25M-PiTT COLJNTYN25101 - LANDFILL\MErHODS & BLANK WELL SAMPLING FORMS\WELL SAMPLING FORM _BAILING_207.2.0124MOCK

GMA #25101- Pitt County Landfill — Sample Collection Field Sheet
Sample ID: P15R
Date: I —e5 —ZL
Field Team Members: L 10 � C JS
Fi Staff Initials Duties (check all that apply)
M-Notes "ater Level 19'rield Parameters El"Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: ❑ Appendix I 2'- Appendix II O—Delayed Metals?
Sample Type: JEK, Monitoring Well ❑ Surface Water ❑ Temporary Piexometer
Collection Method: ❑ PVC Bailer J& Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 17.14 f: Diameter: 2 in Screen internal: 11.0 -14.0 ft BL5
Water Level
Water Level: ,Z ft Water Level Date: f ZS-22. time:
Water Column ft 3 Well Volume _,�,9 gal
Purge Parameters continue on grid below, if necessary)
Bails
pH
Sp. Cond.
ORP
DO
Temp
Turbidity
a
Dry'
Comments- Purge Volume
(S.LI.$)
(µS/Cm)
(mVolts)
(Mg/1)
(OC)
(NTU)
(gal)
1st Ball
.57
3SL.
12y.,�f
� `l ►
2"d Well
Volume
L t,-�►�
i� 3.3�
jb
-�
3rd Well
Volume
I
Sample Collection Date/Time:
t @ AV is
Delayed Metals Collection Date/Time: !-21.-22 H Turbidity during Metals Collection:
oratory Analysis & Containers:
II samples preserved
IAAll
�J samples placed on ice/cooler
Loh Analysis
Container Type
Na, of Containers
Preservation
8250❑ A I
VOAs
3
HCI
8260p SIM I❑
1 4-diioxane
VDAS
3
HCI
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
n/a
Notes/Maps etc.:
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h *Use Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
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GMA #25101 - Pitt County Landfill - Sample Collection Field Sheet
Sample ID: P17
Field Team Members
Date: 1
L10aC5s
F'ff Initials Duties (check all that apply)
Notes-04ater Level 42�Field Parameters 'Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: B Appendix I _Appendix -lam ❑ Delayer! Metals?
Sample Type: 41- Monitoring Well ❑ Surface Water ❑ Temporary Piexometer
Collection Method: c�-2K PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 15.08 ft Diameter: 2 in Screen interval: 8.0 - 11.0 ft BL5
! r Water Level
`-1
Water Level: . 62 ft Water Level Date: "�5�Zz time:
Water Column / /. 0 6 ft 3 Well Volume Jam. gal
Purge Parameters continue on grid below, if necessa
Bails
pH
(S.11.$)
Sp. Cond.
(µslcm)
❑RP
(mvolts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTU)
?
Dry-
Comments- Purge Volume
(gal)
11Bail
5.3u
I :s.a
i-Zz-1
��
iZ
'}L.C.
2"a Well
Volume
S •�3
ic'��. y
��I.1
`�5
15 _(a
' 3Z
`1
'c5
�i^ 44 X5
-�
3'd Well
Volume
1�iZ
Sample Collection Date/Time: 1--2 L: -- ,? Z `'�
Delayed Metals Collection Date/Time:
La oratory Analysis & Containers:
AllEr samples preserved
0 Alf samples placed on iceJmoler
Notes/Maps etc.:
r q."I,-)
Turbidity during Metals Collection:
Lab Analysis
Container Type
No. of Containers
Preservation
—197
$260D App I
VOAs
3
HCI
Or
8260D SIM ID
14-dioxane
VOAs
3
HO
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
ILAmber
2
n/a
3 Vols (in gallons) = 70.5 r 2 h = 0.4856745 * h *Use Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
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GMA #25101 - Pitt County Landfill - Sample Collection Field Sheet
Sample ID: P19
Date:
Field Team Members: LIf) 7- C_3�
Fi taff Initials Duties (check all that apply)
,( Notes G�*ater Level 0-Held Parameters ;!`Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
r
Sampling For: l Appendix I -�---AppendlA4t -Or, Delayed Metals?
Sample Type: Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: ❑ PVC Bailer A Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 18.4 ft Diameter: 2 in
Water Level: -t. 1�0 ft Water Level Date:
Water Column I L. Z4 ft 3 Well Volume j, j gal
Screen interval: 9.0 - 13.0 ft BLS
Water Level
time: 11 1 3
Pure Parameters continue on grid below, if
necessary)
Bails
pH
(S,U.$)
Sp. Cond.
(µS/cm}
ORP
(molts}
DO
(mg/1)
Temp
(°C}
Turbidity
(NTU}
Dry'
Comments- Purge Volume
(gal)
1n Bail
3.:7 -
l q lu
j qG— 9
2.10
13 S.
S .
2"d Well
Volume
,�
3.
Z
f 22. i0
9.90
l � • �
1 � �
and Well
Volume
3 9--l-
13
1 21-5
5. o(o
• 7
Sample Collection Date/Time: l - 25 --_ZZ /5 *2 W
Delayed Metals Collection Date/Time: I-N, -Zl Ej .� � Turbidity during Metals Collection: �'�~
Laboratory Analysis & Containers:
v2l1 samples preserved
ll samples placed on ice/cooler
Notes/Maps etc.:
Lab Analysis
Container lype
No. of Containers
Preservation
8260D Appj
VOAs
3
HCl
8260D SIM ID
1 4-dioxane
VOAs
3
HCl
App I Metals
250 mL Plastic
1 IHNO3
©
App II Pesticides
I Amber
2
n/a
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h
All wells 2" in diameter. Use r = 0.083 feet
*Use Teflon bailers for delayed metals
App II collected every other July starting in 2022.
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GMA #25101 - Pitt County Landfill -- Sample Collection Field Sheet
Sample ID: P20R Field Team Members:
Date: / _Z 5 -
bD - CIS
Field -staff Ijrjitials Duties (chec II that apply) �
Q Notes E(Water Level field Parameters C3'Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: ISY Appendix I - AppeMAIXO't Delayed Metals?
Sample Type: Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: ❑ PVC Bailer 10�eflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 33.51 ft Diameter: 2
Water Level: jCJ,, CI ft Water Level Date:
Water Column 2 `. UL ft 3 Well Volume
in Screen interval: 10.0 - 30.0 ft BLS
Water Level
time: f 2
gal
Purge Parameters continue on grid below, if necessary)
Bails
pH
Sp. Cond.
ORP
DO
Temp
Turbidity
Dry?
i'Y
Comments- Purge Volume
(S.U.$)
(PS/CM)
(m olts)
(mg/0(CC)
(HTLI)
(gal)
1A Bail
ILL- -2,
-7'l _ 3
2'2. IZ
16
2nd Well
L- ��
221 6
`1
�: a,_
Volume
3'd Well
Volume
Sample Collection Date/Time: e� 1k-Ot'
Delayed Metals Collection Date/Time:1-' • -Z � 4 Turbidity during Metals Collection: / 7
Laporatory Analysis & Containers:
CVAll samples preserved
C5"AII samples placed on ice/cooler
Notes/Maps etc.:
Tuo, NC3 REMC v E-0
Lab Anal sis
Container Type
No. of Containers
Preservation
8260D App I
VOAs
3
HCl
8260D SIM ID
1 4-dioxa ne
VOAs
3
HCl
App I Metals
250 mL Plastic
1
HNO3
❑
App H Pesticides
11-Amber
2
n/a
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h
All wells 2" in diameter. Use r = 0.083 feet
*Use Teflon bailers for delayed metals
App II collected every other July starting in 2022.
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GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet
Sample ID: P20D
Field Team Members:
Date:
CSC 01;1t- Cz-5
Sampling For: Appendix I ❑ Appendix II ❑ 1,4-Dioxane ❑ Delayed Metals?
Sample Type: Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: Cj�,PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Gram
Well Info: Depth: 60 ft BLS Total Well Length: 63.02 ft Screen interval: 50.0 - 60.0 ft BL5
Well Diameter: 2 in Water Level: ft Water Level Date/Time:
Water Column: J ft 3 well Volume: Z5 S, gal
Purge
Parameters continue on grid below if necessa
Time
pH
{S.U.s}
Sp.
(µSS m).
ORP
{m o ts)
DO
(mg/1))
Temp
(°C)
Turbidity
(NTU)
Depth to
Water {ft
below TOC
Flow
uand
Purge Volume {gal}
1610
)�9
4IF1.0
131.1
1,(,5,
1 L�.L'
Pump On
41'50r) f"l
11e:IQ
5.LL
13
133.E
0-LID
IG- . 1k,
.3C'1�
3y .9
C' .
I ic.r�
-7 `FG�
i 3 • I
�Cic.�rnG m 1
1(0 2
15.,5pl
S5..3-
13L, . +
C , s 3
v-, +
31. 1
1 3. 19
` Ce-) ,-n L ' h2La
i�
Sample Collection Time
Sample Collection Date/Time: 1 `2 fo 22 1 G - .' 0
Delayed Metals Collection Date/Time:
La oratory, Analysis & Containers:
All samples preserved
All samples placed on icelcooler
Lab Anal sis
Container Type
No. of Containers
Preservation
❑
8260D App I
VOAs
3
HCI
❑
8260D SIM ID
14-dioxane
VOAs
3
HCI
❑
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
n/a
Notes/Maps etc.:
Lep-r rk1-q1pVy IN vJtLI
V (in gallons) = 70.5 rxh = 0.4856745 * h
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
INDICATOR PARAMETERS HAVE STABILIZED WHEN 3 CONSECUTIVE READINGS ARE WITHIN: Less than 10% variance for Specific
Conductance. leas than 30/6 varianrp fnr Ta.nnArnt.ira + 1_ n Y ..nit for nu i,r- i n ..,., f— non

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GMA #25101 - Pitt County Landfill -- Sample Collection Field Sheet
Sample ID: P21 Field Team Members:
Date: 1 -2 {e - Z Z
L!0� C3I
Fi Id- off Initials Duties (check all that apply)
—€dotes &later Level .2%Neld Parameters &'Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: Q' Appendix I O—Appendb Il- ❑ Delayed Metals?
Sample Type: eg Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: &?�- PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 15.27 ft Diameter: 2
Water Level: Io . a ( ft Water Level Date:
Water Column q• Z& ft 3 Well Volume y. S
in Screen interval: 8.0 - 11.0 ft BLS
Water Level
time: lC] L,IS
gal
Purge Parameters continue on grid below, if
necessa
Bails
PH
Sp. Cond.
ORP
DO
TempDry?
Turbidity
?
Comments- Purge Volume
(S.U.$)
(µS/cm)
(mvolts)
(mg/1)
VQ
(NTU)
(gal)
1st Bail
4:- L\
I S�:'
11.1c--"
12. u
k -tc\
2"d Well
Volume
�G
5
3rd Well
Volume
c.i:ic\
a . i✓
, j
�L\
111
Sample Collection Date/Time: ZZ L tL-oo
Delayed Metals Collection Date/Time:
Laboratory Analysis & Containers:
6 All samples preserved
[All samples placed on ice/coo[er
Notes/Maps etc.:
Turbidity during Metals Collection:
Lab Analysis
Container Type
No. of Containers
Preservation
8260D App I
VQAs
3
HCI
©r
8250D 5IM ID
1 4-dioxane
VDAs
3
HCl
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
11-Amher
2
n/a
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h *Use Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
Z:�GMAN25IXX-Prrr0D INFM25I01 - LANUFILL�MErHODS & BLANK WELL SAMPLING FORMSMFLL SAMPLING FORNI_BAILING_20220124.000C

2l
GMA #25101 - Pitt County landfill — Sample Collection Field Sheet
Sample ID: P23
Date: I -Z5 -22-
Field Team Members: L i P -t- C5 j
Ftaff Initials Duties (check all that apply)
,E Notes eEFAWter Level Cf� Field Parameters 44Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: Appendix I :== 1 Delayed Metals?
Sample Type: Monitoring Well ❑ Surface Water El Temporary Piexometer
Collection Method: El Bailer Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth +
Stickup (ft):
Water Level: a. 1 2-
Well
19.53 ft Diameter: 2
ft Water Level Date:
1-25 22-
in Screen interval: 11.0 -16.0 ft 6L5
Water Level
time: 1 G '1,3
Water Column l I '[ I ft 3 Well Volume 5. 5 gal
Purge Parameters continue on rid below, if necessary)
Balls
pH
(S.11.$)
Sp. Cond.
(µS/cm)
OPP
(molts)
DO
(mg/1)
Temp
(°C)
Turbidity
(NTLI)
Dry?
D
Comments- Purge Volume
(gal)
1st Bail
S, ZU
3-41. 4
10 � - l
Zsq
1 io. 9
o- 75
Lies
&--y C-) i3 bads
Z"d Well
Volume
S- Z
.�C- I
lovs
�,�7�
and Well
Volume
Sample Collection Date/Time: 1 -25--2- z
Delayed Metals Collection Date/Time: f -lL
--
16313-3
1 Turbidity during Metals Collection:
Laporatory Analysis & Containers:
VAEr samples preserved
ll samples placed on ice/cooler
Notes/Maps etc.:
—n6 4LAI-31 IX
Lab Analysis
Container Type
No. of Containers
Preservation
82600 App I
VOAs
3
HCl
8260❑ 5IM IQ
14-dioxane
VOAs
3
HCl
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
I Amber
2
n/a
3 Vols (in gallons) = 70.5 rzh = 0.4856745 * h
All wells 2" in diameter. Use r = 0.083 feet
*Use Teflon bailers for delayed metals
App II collected every other July starting in 2022.
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L)It
1'5
GMA #25101 - Pitt County Landfill - Sample Collection Field Sheet
Sample ID: P28
Date: 1-2-5
Field Team Members: /_ i n 7 c_% f
Fie taff Initials Duties (check all that apply)
' E?'Notes 2rWater Level 0-Field Parameters ©'Sample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: 11i, Appendix I Appendix-n- J2�—Delayed Metals?
Sample Type: _rB-- Monitoring Well ❑ Surface Water ❑ Temporary Piezometer
Collection Method: ❑ PVC Bailer Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 10.94 ft Diameter: 2 in Screen interval: 3.5 - 8.0 ft BLS
Water Level
Water Level: ft Water Level Date: 1 -25 -,77-- time:
Water Column r4,rlg ft 3 Well Volume 3, gal
Purge Parameters continue on grid below, if necessa
Bails
pH
Sp. Cond.
ORP
DO
Temp
Turbidity
7
Dry'
Comments- Purge Volume
(S.U.$)
(its/cm)
(mvolts)
(mg/0VC)
(NTU)
(gal)
1st sail
6, 3
r1 j, i
6 ntiC\
Znd Well
Volume
�� `'�
�i.�3
13 y
`tci�
3'd Well
t' G
°lfv.`1
13
t
Volume
�(,V t
Sample Collection Date/Time:
-,
Delayed Metals Collection Date/Time: )-Zt. 2L�� Turbidity during Metals Collection: G •_ �-�
Laboratory Analysis & Containers:
0 All samples preserved
All samples placed on ice/cooler
Notes/Maps etc.:
1 Ll�rrV�7 �Ernc✓�27
Lab Analysis
Container Type
No. of Containers
Preservation
8260D App I
VOAs
3
HC1
8260D SIM ID
1 4-dioxane
VOAs
3
HCI
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
1L Amber
2
n/a
3 Vols (in gallons) = 70.5 r1h = 0.4856745 * h *Else Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App IT collected every other July starting in 2022.
Z:\GMA\251M-PrrrCOUNMZ5101 - LANOFILLjMETHODS &WNK WELL SAMPLING FORMSjWELLSAMPLING FORM_SAILING-2A2201Z9.00Cx

15
GMA #25101 - Pitt County Landfill — Sample Collection Field Sheet
Sample ID: P29
Date:-Z5--2-7—
Field Team Members: L i o� Lis
Figig Staff Ijitials Duties (check all that apply)
P Notes C�Water Level R Field Parameters 015ample Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: R""'Appendix I ❑ Appendix II Y' Delayed Metals?
Sample Type: 2"" Monitoring Well / ❑ Surface Water El Temporary Piezometer
Collection Method: ❑ PVC Bailer Rr Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 14.96 ft Diameter: 2 in Screen interval; 7.0 -12.0 ft BLS
Water Level
Water Level: ft Water Level Date: —'c = time:
Water Column t`fy 3 ft 3 Well Volume gal
Purge Parameters continue on grid below, if
necessa
Bails
pH
(S.U.$)
Sp. Cond.
(PS/CM)
ORP
(molts)
DO
(mg1l)
Temp
(°C)
Turbidity
(NTU)
D �'?
Comments- Purge Volume
(gal)
1st Bail
4 96
23Z
03- Z
_2 . I S
1 3 • -
17-Cl
2^d Well
Volume
'-�, '�`�
1 Ll g'�
1 / 1. 5
2.2-9
1 y y
�
3rd Well
Volume
(G
22T16
1 U3.
G
q . --
-7 2.(0
Sample Collection Date/Time: i•-as zZ 6 /0-yo
Delayed Metals Collection Date/Time: j lc, Turbidity during Metals Collection: 5
0AL 6oratory Analysis & Containers:
ll samples preserved
All samples placed on ice/cooler
Notes/Maps etc.:
Lab Analysis
Container Type
No. of Containers
Preservation
f'
8260D App I
VOAs
3
HCl
8260D SIM ID
14-dioxane
VOAs
3
HCI
EC
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
I Amber
2
n/a
3 Vols (in gallons) = 70.5 rzh = 0.4856745 * h
All wells 2" in diameter. Use r = 0.083 feet
*Use Teflon bailers for delayed metals
App II collected every other July starting in 2022.
I:�GMA�MXX-Plrr COUNTYi25101 - LANDFILL%MMODS & BLANK WELL SAMPLING F6RM51WELL5AMPLING FORM SA1LiNG_2022A124.00KX

GMA #25101 - Pitt County Landfill - Sample Collection Field Sheet
Sample ID: P21
Field Team Members:
Date: I- 2 (a-2 2
L 1 0 0- CT.S
F' I aff Initials Duties (check all that apply)
&"otes Water Level �F1eld Parameters .&�Sample Collection ❑ Other
❑ Notes 0 Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: ®� Appendix I ppendix-- ❑ Delayed Metals?
Sample Type: ❑ Monitoring Well ❑ Surface Water :;8Temporary Piezometer
Collection Method: &Y- PVC Bailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 3,39 ft Diameter: 2 in
Water Level: 0,W ft Water Level Date:
Water Column 2-- &59 ft 3 Well Volume gal
Screen interval: n J a ft BLS
Water Level
time:
Purge Parameters continue on grid below, if
necessary)
Bails
pH
Sp. Cond.
DRP
DU
Temp
Turbidity
Dry?
Comments- Purge Volume
(S.U.$)
(VS/cm)
(mvolts)
(mg/1)
(OC)
(NTU)
(gal)
ist Bail
J j�zLi
1.z cl
.1
rd Well
Volume
3rd Well
Volume
Sample Collection Date/Time; i --Z?v- 'L ci 1,5.. I --
Delayed Metals Collection Date/Time: Turbidity during Metals Collection:
Laboratory Analysis & Containers:
lE( Il samples preserved
All samples placed on ice/cooler
Notes/Maps etc.:
Lab Analysis
Container Type
No. of Containers
Preservation
8260D App I
VOAs
3
HCl
Q,,-
8260D 5IM ID
i 4-dioxane
VOAs
3
HCl
❑
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
ILAmber
2
n/a
3 Vols (in gallons) = 70.5 rzh = 0.4856745 * h *Use Teflon hailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
2:jGMQ!i1XX-Pr1T COUNM25101 - LANOFILL�MEMODS & BLANK WELL SAMPLING FORMS�WELL SAMPLING FORM-3ATUNG_20220124.DDOC

GMA #25101- Pitt County Landfill — Sample Collection Field Sheet
Sample ID: PZ2
Field Team Members:
Date: 1--2G -Zz
L n -� CTS
Fi W- taff Initials Duties (check all that apply)
ceAotes Later Level -vE�+leld Parameters EAemple Collection ❑ Other
❑ Notes ❑ Water Level ❑ Field Parameters ❑ Sample Collection ❑ Other
Sampling For: M� Appendix I 6j"pp`enatx-4F` ❑ Delayed Metals?
Sample Type: ❑ Monitoring Well ❑ Surface Water cam Temporary Piezometer
Collection Method: 4�-?e PVC Sailer ❑ Teflon Bailer ❑ Submersible Pump ❑ Grab
Well Info:
Total Depth + Well
Stickup (ft): 3.44 ft Diameter: 2
Water Level: (),9S ft Water Level Date: 25-22
Water Column 7— .44 6 ft 3 Well Volume
in Screen interval: N/02- ft BLS
Water Level
time: / ):3 44
gal
Purge Parameters continue on arid below, if
necessary)
Bails
pH
(S.U.$)
Sp. Cond.
(PS/cm)
DRP
(molts]
DO
(mg/0
Temp
(°C)
Turbidity
(NTU)
Dry?
Comments- Purge Volume
(gal)
1"t Bail
2ne Well
Volume
3'a Well
Volume
Sample Collection Dateinme: 1 22 15: 09
Delayed Metals Collection Date/Time:
La oratory Analysis & Containers:
Er All samples preserved
W� ll samples placed on ice/cooler
Notes/Maps etc.:
Turbidity during Metals Collection:
Lab Analysis
Container T e
No. of Containers
Preservation
8260D App I
VOAs
3
HCI
EV,-
8260D SIM ID
1 4-dioxane
VOAs
3
HCi
❑
App I Metals
250 mL Plastic
1
HNO3
❑
App II Pesticides
IL Amber
2
nja
3 Vols (in gallons) = 70.5 r2h = 0.4856745 * h *Use Teflon bailers for delayed metals
All wells 2" in diameter. Use r = 0.083 feet App II collected every other July starting in 2022.
Z:LGMA�251KX-PITT COLINM2S101 - LANDFILL�MF DDS &BLANK WELL SAMPLING FORMS�WELL SAMPLING FORM_SMLING_20220124.ORCX

Pitt County Landfill January Monitoring Event Field Sheet Year- Collected By: Zl D o- [,_
`i
Total Well
Depth
Depth
Height of
Field Parameters
Date/Time
Specific
_
E
(including
to
Water
3 Well
Well
Water Purging
a
stickup) (ft
water
Column
Volumes
Gallons Bailed
Temp
Conductance
DO
Turbidity
level completion/ Metals
Well
,`£�°
BLS)
(ft}
{h} (ft]
{gallons]
extracted Dry?
Baits
PH
{°C}
{µS}
(mg/
(ntu]
collected Volatilleesr'Sampling sampling
Notes
SW1
App 1 8260D,
dimxane.
NIA
NIA 7]
n
ij
i
�y
L 7
�.1
�' �
y
1 . U
` 1 ZJ4. Z_ Z.
l`
��
�(:
/ Q + 'r
V F'F ! "7 y 9
App I metals
Ap
r
-'.
� l� • ��
SWZ
App182600,
1,4-dimxane,
N/A
NIA
�'
�' +
(�� r
j ry
�i
C�
�% �yG
q
r Z �
('�
yL.J
r
L, 16 ,
App I metals
ItJi�
L .tiV}
r �F"
App 1 8260D,
I
l
�
SW4
1,4-dloxane,
NIA
NIA
pp��
Ll/ 9
r
! -1 [�
.�
�.�9
� •
y
1
OLP l3j l . V1
App I metals
, ?j,Gj
1st Ball:
2nd Vol:
PI1
App18260D,
1,4-dloxane
3.4
NIA
3rd Vol:
15t Hall:
Pit
App 182bDD,
1,4-dioxane
3.4
N/A
I
Znd Vol:
3rd Vol:
l -Z LPL L
FB
App i 8260D,
NIA
N/A
NIA
1,4-dloxane,
_
IT
App I metals
E8
App I82SOD,
1,4-dimxane,
NIA
NIA
N/A
�� U
App I metals
Collect surface water samples facing upstream. Collect from point of confluence For SW2,
FB: Pour tab DI water into bailer and over gloves and rope into ss pitcher then into sample containers. Collect before sampling well P4 and use equip blank bailer For P4.
FB: Use lab DI water to fill sample containers directly. Collect on -site preferably near the dirt road within the landfill to evaluate for possible field contaminants from road dust.
3 We11 Volumes (in gaIIon s) = 70.5 rzh = 0.4856745 • h All wells 2 inch diameter. use r = 0.083 feet One 3-foot bailer = 0.27 gal r.7M"""'
Page 1 of 1

APPENDIX C
LABORATORY REPORT AND CHAIN -OF -CUSTODY
FORMS FOR WATER SAMPLES

ENCO Laboratones
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, February 11, 2022
Groundwater Management Associates, Inc. (GR022)
Attn: Emma Shipley
4300 Sapphire Court, Suite 100
Greenville, NC 27834
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Pitt County Landfill - App I
ENCO Workorder(s): CF00921
Dear Emma Shipley,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, January 27, 2022.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
;,� ✓mac T�y�
Shahla Vakili
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 96

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-MW1R
Lab ID: CF00921-01
Sampled: 01/26/22 17:45
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/27/22 06:58
02/03/22 14:10
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 12:11
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 16:04
EPA 8260D
EPA 503013_MS
02/09/22
02/03/22 16:15
02/03/22 23:09
Client ID: 7401-MW3
Lab ID: CF00921-02
Sampled: 01/26/22 09:18
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/27/22 06:58
02/03/22 14:12
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 12:56
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 16:30
EPA 8260D
EPA 503013_MS
02/09/22
02/03/22 16:15
02/03/22 23:37
Client ID: 7401-MW6R
Lab ID: CF00921-04
Sampled: 01/25/22 16:20
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/08/22
02/01/22 19:27
02/02/22 10:30
Client ID: 7401-MW6R
Lab ID: CF00921-04RE1
Sampled: 01/25/22 16:20
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/08/22
02/02/22 10:21
02/03/22 09:18
Client ID: 7401-MW8
Lab ID: CF00921-05
Sampled: 01/26/22 10:00
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 10:42
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:00
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 17:21
EPA 8260D
EPA 503013_MS
02/09/22
02/03/22 16:15
02/04/22 00:05
Client ID: 7401-122
Lab ID: CF00921-06
Sampled: 01/26/22 09:35
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 10:45
EPA 6020B
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:04
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 17:47
EPA 8260D
EPA 5030B_MS
02/09/22
02/03/22 16:15
02/04/22 00:33
Client ID: 7401-P4
Lab ID: CF00921-07
Sampled: 01/25/22 09:37
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(sl
EPA 8260D
EPA 5030B_MIS
02/08/22
02/01/22 19:27
02/02/22 10:58
Client ID: 7401-P4
Lab ID: CF00921-07RE1
Sampled: 01/25/22 09:37
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(sl
EPA 8260D
EPA 503013_MS
02/08/22
02/02/22 10:21
02/03/22 09:43
Client ID: 7401-135
Lab ID: CF00921-08
Sampled: 01/26/22 17:19
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 10:47
EPA 6020B
EPA 200.8
07/25/22
01/28/22 04:36
02/11/22 10:50
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 18:38
EPA 8260D
EPA 5030B_MS
02/09/22
02/03/22 16:15
02/04/22 01:01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 96

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-136
Lab ID: CF00921-09
Sampled: 01/26/22 10:30
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 10:10
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:08
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 19:04
EPA 8260D
EPA 503013_MS
02/09/22
02/03/22 16:15
02/04/22 01:29
Client ID: 7401-137
Lab ID: CF00921-10
Sampled: 01/26/22 08:50
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 10:50
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:13
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 19:29
EPA 8260D
EPA 503013_MS
02/09/22
02/03/22 16:15
02/04/22 01:57
Client ID: 7401-129
Lab ID: CF00921-11
Sampled: 01/26/22 12:06
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 10:52
EPA 6020B
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:17
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 19:55
EPA 8260D
EPA 5030B_MS
02/09/22
02/03/22 16:15
02/04/22 02:25
Client ID: 7401-P11R
Lab ID: CF00921-12
Sampled: 01/26/22 14:20
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(
Analysis Date/Time(sj
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 10:55
EPA 6020B
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:21
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 20:21
EPA 8260D
EPA 503013_MS
02/09/22
02/03/22 15:38
02/04/22 22:49
Client ID: 7401-P12
Lab ID: CF00921-13
Sampled: 01/25/22 14:36
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/08/22
02/01/22 14:12
02/01/22 20:47
EPA 8260D
EPA 503013_MS
02/08/22
02/01/22 19:27
02/02/22 11:26
Client ID: 7401-1313
Lab ID: CF00921-14
Sampled: 01/26/22 11:17
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 10:58
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:35
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 21:12
EPA 8260D
EPA 503013_MS
02/09/22
02/03/22 15:38
02/04/22 23:16
Client ID: 7401-13131)
Lab ID: CF00921-15
Sampled: 01/26/22 11:37
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 11:00
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:39
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 21:38
EPA 8260D
EPA 503013_MS
02/09/22
02/03/22 15:38
02/04/22 23:44
Client ID: 7401-121611
Lab ID: CF00921-16
Sampled: 01/25/22 14:15
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/08/22
02/01/22 14:12
02/01/22 22:04
EPA 8260D
EPA 503013_MS
02/08/22
02/01/22 19:27
02/02/22 11:54
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 96

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-1337
Lab ID: CF00921-17
Sampled: 01/26/22 14:45
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 11:14
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:44
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 14:12
02/01/22 22:29
EPA 8260D
EPA 503013_MS
02/09/22
02/03/22 15:38
02/05/22 00:12
Client ID: 7401-1319
Lab ID: CF00921-18
Sampled: 01/25/22 15:24
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/08/22
02/01/22 19:27
02/02/22 12:22
Client ID: 7401-1319
Lab ID: CF00921-18RE1
Sampled: 01/25/22 15:24
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/08/22
02/02/22 10:21
02/03/22 10:09
EPA 8260D
EPA 5030B_MIS
02/08/22
02/03/22 16:15
02/03/22 21:18
Client ID: 7401-P20R
Lab ID: CF00921-19
Sampled: 01/25/22 16:00
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/08/22
02/01/22 19:27
02/02/22 12:50
EPA 8260D
EPA 503013_MS
02/08/22
02/02/22 10:21
02/03/22 10:35
Client ID: 7401-P20D
Lab ID: CF00921-20
Sampled: 01/26/22 16:30
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 11:16
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:48
EPA 8260D
EPA 5030B_MS
02/09/22
02/02/22 10:21
02/03/22 11:00
EPA 8260D
EPA 503013_MS
02/09/22
02/03/22 15:38
02/05/22 00:40
Client ID: 7401-1321
Lab ID: CF00921-21
Sampled: 01/26/22 14:00
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 11:19
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:52
EPA 8260D
EPA 503013_MS
02/09/22
02/02/22 10:21
02/03/22 11:26
EPA 8260D
EPA 503013_MS
02/09/22
02/08/22 14:31
02/08/22 22:34
Client ID: 7401-1323
Lab ID: CF00921-22
Sampled: 01/25/22 13:55
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/08/22
02/01/22 19:27
02/02/22 13:17
EPA 8260D
EPA 5030B_MS
02/08/22
02/02/22 10:21
02/03/22 11:52
Client ID: 7401-P28
Lab ID: CF00921-23
Sampled: 01/25/22 15:00
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/08/22
02/01/22 19:27
02/02/22 13:45
EPA 8260D
EPA 503013_MS
02/08/22
02/02/22 10:21
02/03/22 12:17
Client ID: 7401-P29
Lab ID: CF00921-24
Sampled: 01/25/22 10:06
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/08/22
02/01/22 19:27
02/02/22 14:13
Client ID: 7401-P29
Lab ID: CF00921-24RE1
Sampled: 01/25/22 10:06
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/08/22
02/04/22 10:41
02/04/22 13:50
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 96

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-SW3
Lab ID: CF00921-25
Sampled: 01/26/22 16:53
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 11:21
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 13:57
EPA 8260D
EPA 503013_MS
02/09/22
02/08/22 14:31
02/08/22 23:02
Client ID: 7401-SW1
Lab ID: CF00921-25RE1
Sampled: 01/26/22 16:53
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/09/22
02/04/22 10:41
02/04/22 14:16
Client ID: 7401-SW2
Lab ID: CF00921-26
Sampled: 01/26/22 15:32
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 11:24
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 14:01
EPA 8260D
EPA 5030B_MS
02/09/22
02/02/22 10:21
02/03/22 13:34
EPA 8260D
EPA 503013_MS
02/09/22
02/08/22 14:31
02/08/22 23:30
Client ID: 7401-SW4
Lab ID: CF00921-27
Sampled: 01/25/22 12:35
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/24/22
01/28/22 04:30
02/10/22 11:26
EPA 6020E
EPA 200.8
07/24/22
01/27/22 11:09
02/08/22 14:05
EPA 8260D
EPA 503013_MS
02/08/22
02/01/22 19:27
02/02/22 14:41
EPA 8260D
EPA 503013_MS
02/08/22
02/02/22 10:21
02/03/22 14:00
Client ID: 7401-PZ1
Lab ID: CF00921-28
Sampled: 01/26/22 15:17
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/09/22
02/02/22 10:21
02/03/22 14:26
EPA 8260D
EPA 503013_MS
02/09/22
02/08/22 14:31
02/08/22 23:58
Client ID: 7401-PZ2
Lab ID: CF00921-29
Sampled: 01/26/22 15:09
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 19:27
02/02/22 15:09
EPA 8260D
EPA 503013_MS
02/09/22
02/02/22 10:21
02/03/22 14:51
Client ID: 7401-EB
Lab ID: CF00921-30
Sampled: 01/26/22 17:00
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 11:29
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 14:14
EPA 8260D
EPA 5030B_MIS
02/09/22
02/01/22 19:27
02/02/22 09:06
EPA 8260D
EPA 503013_MS
02/09/22
02/02/22 10:21
02/03/22 15:17
Client ID: 7401-FB
Lab ID: CF00921-31
Sampled: 01/26/22 17:05
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 11:31
EPA 6020E
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 14:18
EPA 8260D
EPA 503013_MS
02/09/22
02/01/22 19:27
02/02/22 09:34
EPA 8260D
EPA 503013_MS
02/09/22
02/02/22 10:21
02/03/22 15:43
Client ID: 7401-TripBlank
Lab ID: CF00921-32
Sampled: 01/25/22 09:37
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 5030B_MS
02/08/22
02/01/22 19:27
02/02/22 08:38
Client ID: 7401-MW6R-M
Lab ID: CF00921-33
Sampled: 01/26/22 15:24
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 11:34
EPA 6020B
EPA 200.8
07/25/22
01/27/22 11:09
02/08/22 14:31
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 96

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 7401-134-M
Lab ID: CF00921-34
Sampled: 01/26/22 10:13
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(sl
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 11:37
EPA 6020E
EPA 200.8
07/25/22
01/28/22 04:36
02/11/22 10:55
Client ID: 7401-1212-M
Lab ID: CF00921-35
Sampled: 01/26/22 14:30
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:30
02/10/22 11:45
EPA 6020B
EPA 200.8
07/25/22
01/28/22 04:36
02/11/22 11:08
Client ID: 7401-P16R-M
Lab ID: CF00921-36
Sampled: 01/26/22 14:03
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:34
02/04/22 13:08
EPA 6020E
EPA 200.8
07/25/22
01/28/22 04:36
02/11/22 10:25
Client ID: 7401-1319-M
Lab ID: CF00921-37
Sampled: 01/26/22 14:58
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:34
02/04/22 13:34
EPA 6020E
EPA 200.8
07/25/22
01/28/22 04:36
02/11/22 11:12
Client ID: 7401-P20R-M
Lab ID: CF00921-38
Sampled: 01/26/22 15:04
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:34
02/04/22 13:36
EPA 6020B
EPA 200.8
07/25/22
01/28/22 04:36
02/11/22 11:17
Client ID: 7401-P23-M
Lab ID: CF00921-39
Sampled: 01/26/22 13:39
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:34
02/04/22 13:39
EPA 6020E
EPA 200.8
07/25/22
01/28/22 04:36
02/11/22 11:21
Client ID: 7401-1328-M
Lab ID: CF00921-40
Sampled: 01/26/22 14:50
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:34
02/04/22 13:42
EPA 6020E
EPA 200.8
07/25/22
01/28/22 04:36
02/11/22 11:25
Client ID: 7401-1329-M
Lab ID: CF00921-41
Sampled: 01/26/22 10:45
Received: 01/27/22 10:15
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
07/25/22
01/28/22 04:34
02/04/22 13:44
EPA 6020E
EPA 200.8
07/25/22
01/28/22 04:36
02/11/22 11:29
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 96

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SAMPLE DETECTION SUMMARY
Client ID: 7401-MWlR
Lab ID:
CF00921-01
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Barium - Total
54.0
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.460
J
0.160
1.00
ug/L
EPA 6010D
Client ID: 7401-MW3
Lab ID:
CF00921-02
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
179
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.319
J
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
6.72
J
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
5.09
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
5.29
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
32.6
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-MW6R
Lab ID:
CF00921-04RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
6.7
0.80
2.0
ug/L
EPA 8260D
Client ID: 7401-MW8
Lab ID:
CF00921-05
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
42.0
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.413
J
0.160
1.00
ug/L
EPA 6010D
Client ID: 7401-132
Lab ID:
CF00921-06
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
0.91
J
0.80
2.0
ug/L
EPA 8260D
Barium - Total
8.87
J
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.164
J
0.160
1.00
ug/L
EPA 6010D
Client ID: 7401-PS
Lab ID:
CF00921-08
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
0.92
J
0.80
2.0
ug/L
EPA 8260D
Barium - Total
38.0
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.179
J
0.160
1.00
ug/L
EPA 6010D
Chromium - Total
2.55
J
1.40
10.0
ug/L
EPA 6010D
Vanadium - Total
2.56
J
1.40
10.0
ug/L
EPA 6010D
Client ID: 7401-136
Lab ID:
CF00921-09
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
48.8
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.336
J
0.160
1.00
ug/L
EPA 6010D
Zinc - Total
4.45
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P7
Lab ID:
CF00921-10
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
189
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.542
J
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
2.24
J
1.40
10.0
ug/L
EPA 6010D
Lead - Total
4.39
J
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
2.43
J
2.20
10.0
ug/L
EPA 6010D
Selenium - Total
2.49
1.82
2.00
ug/L
EPA 6020E
Vanadium - Total
3.38
J
1.40
10.0
ug/L
EPA 6010D
Client ID: 7401-139
Lab ID:
CF00921-11
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
130
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.799
1
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
2.54
1
1.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 96

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SAMPLE DETECTION SUMMARY
Client ID: 7401-P11R
Lab ID:
CF00921-12
Analvte
Results
Flag
MDL
Q
Units
Method Notes
Barium - Total
116
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
2.67
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
10.2
1.40
10.0
ug/L
EPA 6010D
Lead - Total
4.08
J
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
6.86
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
3.38
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
79.7
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1312
Lab ID:
CF00921-13
Analvte
Results
Flag
MDL
Q
Units
Method Notes
1,4-Dioxane
0.87
J
0.80
2.0
uq/L
EPA 8260D
Client ID: 7401-1313
Lab ID:
CF00921-14
Analvte
Results
Flag
MDL
Q
Units
Method Notes
Barium - Total
101
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
1.01
0.160
1.00
ug/L
EPA 6010D
Chromium - Total
1.90
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
1.53
J
1.40
10.0
ug/L
EPA 6010D
Lead - Total
3.42
J
3.10
10.0
ug/L
EPA 6010D
Vanadium - Total
2.70
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
7.86
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-131311)
Lab ID:
CF00921-15
Analvte
Results
Flag
MDL
Q
Units
Method Notes
1,4-Dioxane
0.96
J
0.80
2.0
ug/L
EPA 8260D
Barium - Total
82.8
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.163
J
0.160
1.00
ug/L
EPA 6010D
Chromium - Total
2.31
J
1.40
10.0
ug/L
EPA 6010D
Vanadium - Total
2.20
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
4.98
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-11316R
Lab ID:
CF00921-16
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
1,4-Dioxane
78
0.80
2.0
ug/L
EPA 8260D
Acetone
15
J
10
20
ug/L
EPA 8260D 0-01
Benzene
2.4
0.15
1.0
ug/L
EPA 8260D
Toluene
0.44
J
0.14
1.0
uq/L
EPA 8260D
Client ID: 7401-1317
Lab ID:
CF00921-17
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
1,4-Dioxane
4.8
0.80
2.0
ug/L
EPA 8260D
Barium - Total
225
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
2.86
0.160
1.00
ug/L
EPA 6010D
Chlorobenzene
2.2
0.17
1.0
ug/L
EPA 8260D
Lead - Total
4.70
J
3.10
10.0
ug/L
EPA 6010D
Vanadium - Total
3.61
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
10.8
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1319
Lab ID:
CF00921-18
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
1,4-Dichlorobenzene
4.8
0.19
1.0
ug/L
EPA 8260D
Benzene
3.4
0.15
1.0
ug/L
EPA 8260D
Chlorobenzene
16
0.17
1.0
ug/L
EPA 8260D
Ethylbenzene
1.4
0.13
1.0
ug/L
EPA 8260D
m,p-Xylenes
0.54
J
0.17
2.0
ug/L
EPA 8260D
o-Xylene
0.88
J
0.065
1.0
ug/L
EPA 8260D
Toluene
0.43
J
0.14
1.0
ug/L
EPA 8260D
Xylenes (Total)
1.4
J
0.45
3.0
ug/L
EPA 8260D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 96

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SAMPLE DETECTION SUMMARY
Client ID: 7401-1319
Lab ID:
CF00921-18RE1
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
1,1-Dichloroethane
3.2
0.13
1.0
ug/L
EPA 8260D
1,4-Dioxane
180
D
4.0
10
ug/L
EPA 8260D
Vinyl chloride
0.49
J
0.32
1.0
ug/L
EPA 8260D
Client ID: 7401-132011
Lab ID:
CF00921-19
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
1,4-Dichlorobenzene
3.0
0.19
1.0
ug/L
EPA 8260D
1,4-Dioxane
62
0.80
2.0
ug/L
EPA 8260D
Benzene
1.3
0.15
1.0
ug/L
EPA 8260D
Client ID: 7401-132011)
Lab ID:
CF00921-20
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
49.0
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
3.05
0.160
1.00
ug/L
EPA 6010D
Chromium - Total
3.88
J
1.40
10.0
ug/L
EPA 6010D
Vanadium - Total
3.66
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
16.6
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1321
Lab ID:
CF00921-21
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
59.4
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
2.14
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
1.74
J
1.40
10.0
ug/L
EPA 6010D
Lead - Total
3.81
J
3.10
10.0
ug/L
EPA 6010D
Vanadium - Total
1.97
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
6.80
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1329
Lab ID:
CF00921-24
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dichlorobenzene
1.5
0.19
1.0
ug/L
EPA 8260D
Benzene
2.0
0.15
1.0
ug/L
EPA 8260D
Chlorobenzene
10
0.17
1.0
ug/L
EPA 8260D
Client ID: 7401-1329
Lab ID:
CF00921-24RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
180
D
4.0
10
ug/L
EPA 8260D
Client ID: 7401-SW3
Lab ID:
CF00921-25
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
50.8
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.241
J
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
8.63
J
1.40
10.0
ug/L
EPA 6010D
Lead - Total
3.53
J
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
2.88
J
2.20
10.0
ug/L
EPA 6010D
Zinc - Total
36.1
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-SW2
Lab ID:
CF00921-26
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
44.4
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
6.02
J
1.40
10.0
ug/L
EPA 6010D
Copper - Total
1.99
J
1.60
10.0
ug/L
EPA 6010D
Zinc - Total
11.6
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-SW4
Lab ID:
CF00921-27
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
2.0
0.80
2.0
ug/L
EPA 8260D
Barium - Total
17.3
1.10
10.0
ug/L
EPA 6010D
Zinc - Total
9.99
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-PZ3
Lab ID:
CF00921-28
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
1.5
1
0.80
2.0
ug/L
EPA 8260D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 96

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SAMPLE DETECTION SUMMARY
Client ID: 7401-EB
Lab ID:
CF00921-30
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Carbon disulfide
6.0
1.5
5.0
ug/L
EPA 8260D
Zinc - Total
81.5
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-FB
Lab ID:
CF00921-31
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
1,4-Dioxane
1.5
J
0.80
2.0
ug/L
EPA 8260D
Client ID: 7401-MW6R-M
Lab ID:
CF00921-33
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
1950
1.10
10.0
ug/L
EPA 6010D
Client ID: 7401-P4-M
Lab ID:
CF00921-34
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
83.4
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.205
J
0.160
1.00
ug/L
EPA 6010D
Zinc - Total
8.96
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P12-M
Lab ID:
CF00921-35
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
25.3
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.778
J
0.160
1.00
ug/L
EPA 6010D
Lead - Total
3.20
J
3.10
10.0
ug/L
EPA 6010D
Zinc - Total
5.23
J
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P36R-M
Lab ID:
CF00921-36
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
1010
1.10
10.0
ug/L
EPA 6010D
Chromium - Total
2.02
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
2.62
J
1.40
10.0
ug/L
EPA 6010D
Nickel - Total
9.84
J
2.20
10.0
ug/L
EPA 6010D
Client ID: 7401-P19-M
Lab ID:
CF00921-37
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
1500
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
12.5
0.160
1.00
ug/L
EPA 6010D
Cobalt - Total
16.2
1.40
10.0
ug/L
EPA 6010D
Lead - Total
3.96
J
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
22.4
2.20
10.0
ug/L
EPA 6010D
Selenium - Total
3.12
1.82
2.00
ug/L
EPA 6020E
Zinc - Total
98.7
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-P20R-M
Lab ID:
CF00921-38
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Barium - Total
887
1.10
10.0
ug/L
EPA 6010D
Cobalt - Total
2.06
J
1.40
10.0
ug/L
EPA 6010D
Lead - Total
4.41
J
3.10
10.0
ug/L
EPA 6010D
Nickel- Total
8.15
J
2.20
10.0
ug/L
EPA 6010D
Client ID: 7401-P23-M
Lab ID:
CF00921-39
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
15.3
1.10
10.0
ug/L
EPA 6010D
Cobalt - Total
1.88
J
1.40
10.0
ug/L
EPA 6010D
Lead - Total
3.23
J
3.10
10.0
ug/L
EPA 6010D
Zinc - Total
7.84
J
4.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 96

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SAMPLE DETECTION SUMMARY
Client ID: 7401-1328-M
Lab ID:
CF00921-40
Analvte
Results
Flag
MDL
Q
Units
Method Notes
Barium - Total
52.4
1.10
10.0
ug/L
EPA 6010D
Beryllium - Total
0.982
J
0.160
1.00
ug/L
EPA 6010D
Chromium - Total
2.65
J
1.40
10.0
ug/L
EPA 6010D
Cobalt - Total
3.40
J
1.40
10.0
ug/L
EPA 6010D
Lead - Total
5.17
J
3.10
10.0
ug/L
EPA 6010D
Nickel - Total
2.86
J
2.20
10.0
ug/L
EPA 6010D
Vanadium - Total
4.61
J
1.40
10.0
ug/L
EPA 6010D
Zinc - Total
20.5
4.40
10.0
ug/L
EPA 6010D
Client ID: 7401-1329-M
Lab ID:
CF00921-41
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Barium - Total
602
1.10
10.0
ug/L
EPA 6010D
Vanadium - Total
9.15
J
1.40
10.0
ug/L
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 96

00�
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ANALYTICAL RESULTS
Description: 7401-MWlR Lab Sample ID:CF00921-01 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 17:45 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3042
EPA 8260D
02/03/22
23:09
RKY
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 12 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MWlR Lab Sample ID:CF00921-01 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 17:45 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3042 EPA 8260D 02/03/22 23:09 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3042 EPA 8260D 02/03/22 23:09 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
54
1
50.0
109 %
53-136
2BO3042
EPA 8260D
02103122 23:09
RKY
Dibromofluoromethane
43
1
50.0
86 %
67-129
2BO3042
EPA 8260D
02103122 23:09
RKY
Toluene-d8
50
1
50.0
100 %
59-134
2BO3042
EPA 8260D
02103122 23:09
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 12:11
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A27005
EPA 6010D
02/03/22 14:10
JDH
Barium [7440-39-3]^
54.0
ug/L
1
1.10
10.0
2A27005
EPA 6010D
02/03/22 14:10
JDH
Beryllium [7440-41-7]^
0.460
J
ug/L
1
0.160
1.00
2A27005
EPA 6010D
02/03/22 14:10
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A27005
EPA 6010D
02/03/22 14:10
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A27005
EPA 6010D
02/03/22 14:10
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A27005
EPA 6010D
02/03/22 14:10
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A27005
EPA 6010D
02/03/22 14:10
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A27005
EPA 6010D
02/03/22 14:10
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A27005
EPA 6010D
02/03/22 14:10
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 12:11
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A27005
EPA 6010D
02/03/22 14:10
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 12:11
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A27005
EPA 6010D
02/03/22 14:10
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2A27005
EPA 6010D
02/03/22 14:10
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 16:04
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.2
1
5.00
103 %
75-125
2BO1026
EPA 8260D
02101122 16:04
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 96

00�
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ANALYTICAL RESULTS
Description: 7401-MW3 Lab Sample ID:CF00921-02 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 09:18 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3042
EPA 8260D
02/03/22
23:37
RKY
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 14 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW3 Lab Sample ID:CF00921-02 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 09:18 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3042 EPA 8260D 02/03/22 23:37 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3042 EPA 8260D 02/03/22 23:37 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
55
1
50.0
110 %
53-136
2BO3042
EPA 8260D
02103122 23:37
RKY
Dibromofluoromethane
43
1
50.0
85 %
67-129
2BO3042
EPA 8260D
02103122 23:37
RKY
Toluene-d8
50
1
50.0
100 %
59-134
2BO3042
EPA 8260D
02103122 2337
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 12:56
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A27005
EPA 6010D
02/03/22 14:12
JDH
Barium [7440-39-3]^
179
ug/L
1
1.10
10.0
2A27005
EPA 6010D
02/03/22 14:12
JDH
Beryllium [7440-41-7]^
0.319
J
ug/L
1
0.160
1.00
2A27005
EPA 6010D
02/03/22 14:12
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A27005
EPA 6010D
02/03/22 14:12
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A27005
EPA 6010D
02/03/22 14:12
JDH
Cobalt[7440-48-4]^
6.72
J
ug/L
1
1.40
10.0
2A27005
EPA 6010D
02/03/22 14:12
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A27005
EPA 6010D
02/03/22 14:12
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A27005
EPA 6010D
02/03/22 14:12
JDH
Nickel[7440-02-O]^
5.09
J
ug/L
1
2.20
10.0
2A27005
EPA 6010D
02/03/22 14:12
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 12:56
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A27005
EPA 6010D
02/03/22 14:12
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 12:56
JDH
Vanadium [7440-62-2]^
5.29
J
ug/L
1
1.40
10.0
2A27005
EPA 6010D
02/03/22 14:12
JDH
Zinc[7440-66-6]^
32.6
ug/L
1
4.40
10.0
2A27005
EPA 6010D
02/03/22 14:12
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 16:30
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.9
1
5.00
98 %
75-125
2BO1026
EPA 8260D
021011221620
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 96

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ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CF00921-04 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 16:20 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY A-07
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 10:30
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 16 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW6R Lab Sample ID:CF00921-04 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 16:20 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 10:30 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 10:30 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
53
1
50.0
107 %
53-136
2BO1032
EPA 8260D
02102122 10:30
RKY
Dibromofluoromethane
45
1
50.0
90 %
67-129
2BO1032
EPA 8260D
0210212210:30
RKY
Toluene-d8
48
1
50.0
96 %
59-134
2BO1032
EPA 8260D
021021221030
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
6.7
ug/L
1
0.80 2.0
2BO2026
EPA 8260D
02/03/22 09:18
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
Toluene-d8
5.5
1
5.00
110 %
75-125
2BO2026
EPA 8260D
02103122 09:18
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW8 Lab Sample ID:CF00921-05 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 10:00 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3042
EPA 8260D
02/04/22 00:05
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 18 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-MW8 Lab Sample ID:CF00921-05 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 10:00 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3042 EPA 8260D 02/04/22 00:05 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3042 EPA 8260D 02/04/22 00:05 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
55
1
50.0
110 %
53-136
2BO3042
EPA 8260D
02104122 00:05
RKY
Dibromofluoromethane
45
1
50.0
89 %
67-129
2BO3042
EPA 8260D
02104122 00:05
RKY
Toluene-d8
49
1
50.0
98 %
59-134
2BO3042
EPA 8260D
02104122 00:05
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:00
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 10:42
JDH
Barium [7440-39-3]^
42.0
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 10:42
JDH
Beryllium [7440-41-7]^
0.413
J
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 10:42
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 10:42
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:42
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:42
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 10:42
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 10:42
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 10:42
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:00
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 10:42
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:00
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:42
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 10:42
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 17:21
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.2
1
5.00
105 %
75-125
2BO1026
EPA 8260D
0210112217:21
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P2 Lab Sample ID:CF00921-06 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 09:35 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3042
EPA 8260D
02/04/22 00:33
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 20 of 96

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ANALYTICAL RESULTS
Description: 7401-P2 Lab Sample ID:CF00921-06 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 09:35 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3042 EPA 8260D 02/04/22 00:33 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3042 EPA 8260D 02/04/22 00:33 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
54
1
50.0
108 %
53-136
2BO3042
EPA 8260D
02104122 00:33
RKY
Dibromofluoromethane
44
1
50.0
87 %
67-129
2BO3042
EPA 8260D
02104122 00:33
RKY
Toluene-d8
48
1
50.0
97 %
59-134
2BO3042
EPA 8260D
02104122 0033
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:04
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 10:45
JDH
Barium [7440-39-3]^
8.87
J
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 10:45
JDH
Beryllium [7440-41-7]^
0.164
J
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 10:45
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 10:45
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:45
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:45
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 10:45
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 10:45
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 10:45
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:04
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 10:45
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:04
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:45
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 10:45
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.91
J
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 17:47
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.4
1
5.00
108 %
75-125
2BO1026
EPA 8260D
0210112217:47
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 96

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ANALYTICAL RESULTS
Description: 7401-P4 Lab Sample ID:CF00921-07 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 09:37 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY A-07
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 10:58
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 22 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P4 Lab Sample ID:CF00921-07 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 09:37 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 10:58 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 10:58 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
51
1
50.0
103 %
53-136
2BO1032
EPA 8260D
0210212210:58
RKY
Dibromofluoromethane
44
1
50.0
88 %
67-129
2BO1032
EPA 8260D
0210212210:58
RKY
Toluene-d8
49
1
50.0
98 %
59-134
2BO1032
EPA 8260D
0210212210:58
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
2BO2026
EPA 8260D
02/03/22 09:43
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
Toluene-d8
5.2
1
5.00
105 %
75-125
2BO2026
EPA 8260D
02103122 09:43
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 96

00�
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ANALYTICAL RESULTS
Description: 7401-P5 Lab Sample ID:CF00921-08 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 17:19 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3042
EPA 8260D
02/04/22 01:01
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 24 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P5 Lab Sample ID:CF00921-08 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 17:19 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3042 EPA 8260D 02/04/22 01:01 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3042 EPA 8260D 02/04/22 01:01 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
54
1
50.0
108 %
53-136
2BO3042
EPA 8260D
02104122 01:01
RKY
Dibromofluoromethane
44
1
50.0
88 %
67-129
2BO3042
EPA 8260D
02104122 01:01
RKY
Toluene-d8
49
1
50.0
98 %
59-134
2BO3042
EPA 8260D
02104122 01:01
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A28003
EPA 6020B
02/11/22 10:50
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 10:47
JDH
Barium [7440-39-3]^
38.0
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 10:47
JDH
Beryllium [7440-41-7]^
0.179
J
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 10:47
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 10:47
JDH
Chromium [7440-47-3]^
2.55
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:47
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:47
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 10:47
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 10:47
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 10:47
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A28003
EPA 6020B
02/11/22 10:50
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 10:47
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A28003
EPA 6020B
02/11/22 10:50
JDH
Vanadium [7440-62-2]^
2.56
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:47
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 10:47
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.92
J
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 18:38
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.3
1
5.00
105 %
75-125
2BO1026
EPA 8260D
02101122 1828
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P6 Lab Sample ID:CF00921-09 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 10:30 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3042
EPA 8260D
02/04/22 01:29
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 26 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P6 Lab Sample ID:CF00921-09 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 10:30 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3042 EPA 8260D 02/04/22 01:29 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3042 EPA 8260D 02/04/22 01:29 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
55
1
50.0
111 %
53-136
2BO3042
EPA 8260D
02104122 01:29
RKY
Dibromofluoromethane
45
1
50.0
90 %
67-129
2BO3042
EPA 8260D
02104122 01:29
RKY
Toluene-d8
50
1
50.0
99 %
59-134
2BO3042
EPA 8260D
02104122 01:29
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:08
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 10:10
JDH
Barium [7440-39-3]^
48.8
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 10:10
JDH
Beryllium [7440-41-7]^
0.336
J
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 10:10
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 10:10
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:10
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:10
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 10:10
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 10:10
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 10:10
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:08
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 10:10
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:08
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:10
JDH
Zinc[7440-66-6]^
4.45
J
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 10:10
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 19:04
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.0
1
5.00
101 %
75-125
2BO1026
EPA 8260D
02101122 19:04
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P7 Lab Sample ID:CF00921-10 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 08:50 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3042
EPA 8260D
02/04/22 01:57
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 28 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P7 Lab Sample ID:CF00921-10 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 08:50 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3042 EPA 8260D 02/04/22 01:57 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3042 EPA 8260D 02/04/22 01:57 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
55
1
50.0
111 %
53-136
2BO3042
EPA 8260D
02104122 01:57
RKY
Dibromofluoromethane
45
1
50.0
90 %
67-129
2BO3042
EPA 8260D
02104122 01:57
RKY
Toluene-d8
50
1
50.0
100 %
59-134
2BO3042
EPA 8260D
02104122 01:57
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:13
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 10:50
JDH
Barium [7440-39-3]^
189
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 10:50
JDH
Beryllium [7440-41-7]^
0.542
J
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 10:50
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 10:50
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:50
JDH
Cobalt[7440-48-4]^
2.24
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:50
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 10:50
JDH
Lead [7439-92-1]^
4.39
J
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 10:50
JDH
Nickel[7440-02-O]^
2.43
J
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 10:50
JDH
Selenium [7782-49-2]^
2.49
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:13
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 10:50
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:13
JDH
Vanadium [7440-62-2]^
3.38
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:50
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 10:50
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 19:29
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.2
1
5.00
105 %
75-125
2BO1026
EPA 8260D
0210112219:29
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 29 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P9 Lab Sample ID:CF00921-11 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 12:06 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3042
EPA 8260D
02/04/22 02:25
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 30 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P9 Lab Sample ID:CF00921-11 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 12:06 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3042 EPA 8260D 02/04/22 02:25 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3042 EPA 8260D 02/04/22 02:25 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
53
1
50.0
106 %
53-136
2BO3042
EPA 8260D
02104122 02:25
RKY
Dibromofluoromethane
45
1
50.0
91 %
67-129
2BO3042
EPA 8260D
02104122 02:25
RKY
Toluene-d8
49
1
50.0
98 %
59-134
2BO3042
EPA 8260D
02104122 02:25
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:17
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 10:52
JDH
Barium [7440-39-3]^
130
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 10:52
JDH
Beryllium [7440-41-7]^
0.799
J
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 10:52
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 10:52
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:52
JDH
Cobalt[7440-48-4]^
2.54
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:52
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 10:52
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 10:52
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 10:52
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:17
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 10:52
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:17
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:52
JDH
Zinc[7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 10:52
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 19:55
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.0
1
5.00
100 %
75-125
2BO1026
EPA 8260D
0210112219:55
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 31 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P11R Lab Sample ID:CF00921-12 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 14:20 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3039
EPA 8260D
02/04/22 22:49
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 32 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PllR Lab Sample ID:CF00921-12 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 14:20 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3039 EPA 8260D 02/04/22 22:49 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3039 EPA 8260D 02/04/22 22:49 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
57
1
50.0
113 %
53-136
2BO3039
EPA 8260D
02104122 22:49
RKY
Dibromofluoromethane
45
1
50.0
90 %
67-129
2BO3039
EPA 8260D
02104122 22:49
RKY
Toluene-d8
51
1
50.0
102 %
59-134
2BO3039
EPA 8260D
02104122 22:49
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:21
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 10:55
JDH
Barium [7440-39-3]^
116
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 10:55
JDH
Beryllium [7440-41-7]^
2.67
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 10:55
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 10:55
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:55
JDH
Cobalt[7440-48-4]^
10.2
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:55
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 10:55
JDH
Lead [7439-92-1]^
4.08
J
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 10:55
JDH
Nickel[7440-02-O]^
6.86
J
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 10:55
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:21
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 10:55
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:21
JDH
Vanadium [7440-62-2]^
3.38
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:55
JDH
Zinc[7440-66-6]^
79.7
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 10:55
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 20:21
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
14
1
5.00
277 %
75-125
2BO1026
EPA 8260D
02101122 20:21
KKW
QS-03
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 33 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P12 Lab Sample ID:CF00921-13 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 14:36 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY A-07
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 11:26
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 34 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P12 Lab Sample ID:CF00921-13 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 14:36 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 11:26 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 11:26 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
54
1
50.0
107 %
53-136
2BO1032
EPA 8260D
02102122 11:26
RKY
Dibromofluoromethane
45
1
50.0
90 %
67-129
2BO1032
EPA 8260D
0210212211:26
RKY
Toluene-d8
49
1
50.0
98 %
59-134
2BO1032
EPA 8260D
0210212211:26
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.87
3
ug/L
1
0.80 2.0
2BO1026
EPA 8260D
02/01/22 20:47
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
Toluene-d8
4.8
1
5.00
95 %
75-125
2BO1026
EPA 8260D
02101122 20:47
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 35 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P13 Lab Sample ID:CF00921-14 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 11:17 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3039
EPA 8260D
02/04/22
23:16
RKY
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 36 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P13 Lab Sample ID:CF00921-14 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 11:17 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3039 EPA 8260D 02/04/22 23:16 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3039 EPA 8260D 02/04/22 23:16 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
57
1
50.0
113 %
53-136
2BO3039
EPA 8260D
02104122 23:16
RKY
Dibromofluoromethane
45
1
50.0
89 %
67-129
2BO3039
EPA 8260D
02104122 23:16
RKY
Toluene-d8
50
1
50.0
100 %
59-134
2BO3039
EPA 8260D
02104122 23:16
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:35
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 10:58
JDH
Barium [7440-39-3]^
101
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 10:58
JDH
Beryllium [7440-41-7]^
1.01
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 10:58
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 10:58
JDH
Chromium [7440-47-3]^
1.90
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:58
JDH
Cobalt[7440-48-4]^
1.53
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:58
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 10:58
JDH
Lead [7439-92-1]^
3.42
J
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 10:58
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 10:58
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:35
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 10:58
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:35
JDH
Vanadium [7440-62-2]^
2.70
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 10:58
JDH
Zinc[7440-66-6]^
7.86
J
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 10:58
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 21:12
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
7.4
1
5.00
149 %
75-125
2BO1026
EPA 8260D
02101122 21:12
KKW
Q5-03
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 37 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P131) Lab Sample ID:CF00921-15 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 11:37 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3039
EPA 8260D
02/04/22 23:44
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 38 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P13D Lab Sample ID:CF00921-15 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 11:37 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3039 EPA 8260D 02/04/22 23:44 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3039 EPA 8260D 02/04/22 23:44 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
58
1
50.0
116 %
53-136
2BO3039
EPA 8260D
02104122 23:44
RKY
Dibromofluoromethane
45
1
50.0
90 %
67-129
2BO3039
EPA 8260D
02104122 23:44
RKY
Toluene-d8
49
1
50.0
98 %
59-134
2BO3039
EPA 8260D
02104122 23:44
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:39
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 11:00
JDH
Barium [7440-39-3]^
82.8
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 11:00
JDH
Beryllium [7440-41-7]^
0.163
J
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 11:00
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 11:00
JDH
Chromium [7440-47-3]^
2.31
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:00
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:00
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 11:00
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 11:00
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 11:00
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:39
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 11:00
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:39
JDH
Vanadium [7440-62-2]^
2.20
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:00
JDH
Zinc[7440-66-6]^
4.98
J
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 11:00
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.96
J
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 21:38
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.4
1
5.00
108 %
75-125
2BO1026
EPA 8260D
02101122 21:38
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 39 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P1611 Lab Sample ID:CF00921-16 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 14:15 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY A-07
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Acetone [67-64-1]A
15
J
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 11:54
RKY 0-01
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Benzene [71-43-2]A
2.4
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Styrene[100-42-5]A
0.11
U
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Toluene [108-88-3]A
0.44
J
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 11:54
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 40 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P16R Lab Sample ID:CF00921-16 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 14:15 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 11:54 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 11:54 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
57
1
50.0
114 %
53-136
2BO1032
EPA 8260D
02102122 11:54
RKY
Dibromofluoromethane
44
1
50.0
88 %
67-129
2BO1032
EPA 8260D
0210212211:54
RKY
Toluene-d8
49
1
50.0
98 %
59-134
2BO1032
EPA 8260D
0210212211:54
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
78
ug/L
1
0.80 2.0
2BO1026
EPA 8260D
02/01/22 22:04
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
Toluene-d8
5.0
1
5.00
99 %
75-125
2BO1026
EPA 8260D
02101122 22:04
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 41 of 96

00�
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ANALYTICAL RESULTS
Description: 7401-P17 Lab Sample ID:CF00921-17 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 14:45 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Chlorobenzene [108-90-7]A
2.2
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3039
EPA 8260D
02/05/22
00:12
RKY
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 42 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P17 Lab Sample ID:CF00921-17 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 14:45 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3039 EPA 8260D 02/05/22 00:12 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3039 EPA 8260D 02/05/22 00:12 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
56
1
50.0
112 %
53-136
2BO3039
EPA 8260D
02105122 00:12
RKY
Dibromofluoromethane
45
1
50.0
90 %
67-129
2BO3039
EPA 8260D
02105122 00:12
RKY
Toluene-d8
50
1
50.0
99 %
59-134
2BO3039
EPA 8260D
02105122 00:12
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:44
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 11:14
JDH
Barium [7440-39-3]^
225
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 11:14
JDH
Beryllium [7440-41-7]^
2.86
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 11:14
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 11:14
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:14
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:14
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 11:14
JDH
Lead [7439-92-1]^
4.70
J
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 11:14
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 11:14
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:44
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 11:14
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:44
JDH
Vanadium [7440-62-2]^
3.61
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:14
JDH
Zinc[7440-66-6]^
10.8
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 11:14
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
4.8
ug/L
1
0.80
2.0
2BO1026
EPA 8260D
02/01/22 22:29
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
4.9
1
5.00
98 %
75-125
2BO1026
EPA 8260D
02101122 22:29
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 43 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P19 Lab Sample ID:CF00921-18 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 15:24 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
1,1,1-Trichloroethane [71-55-6]^
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
1,1,2-Trichloroethane [79-00-5]^
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
1,1-Dichloroethane [75-34-3]A
3.2
ug/L
1
0.13
1.0
2BO3042
EPA 8260D
02/03/22 21:18
RKY
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
1,4-Dichlorobenzene [306-46-7]^
4.8
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
2-Butanone [78-93-3]^
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
2-Hexanone [591-78-6]^
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Acetone [67-64-1]^
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Benzene [71-43-2]A
3.4
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Bromochloromethane [74-97-5]^
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Bromomethane [74-83-9]^
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Carbon disulfide [75-15-0]^
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Carbon tetrachloride [56-23-5]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Chlorobenzene [108-90-7]A
16
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Chloroethane [75-00-3]^
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Chloromethane [74-87-3]^
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
cis-1,3-Dichloropropene [10061-01-5]^
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Dibromochloromethane [124-48-1]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Dibromomethane [74-95-3]^
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Ethylbenzene [100-41-4]A
1.4
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
m,p-Xylenes[108-38-3/306-42-3]A
0.54
J
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
o-Xylene [95-47-6]A
0.88
J
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Toluene [108-88-3]A
0.43
J
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 12:22
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 44 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P19 Lab Sample ID:CF00921-18 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 15:24 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.49 1 ug/L 1 0.32 1.0 2BO3042 EPA 8260D 02/03/22 21:18 RKY
Xylenes(Total)[1330-20-7]^ 1.4 1 ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 12:22 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
51
1
50.0
102 %
53-136
2BO1032
EPA 8260D
02102122 12:22
RKY
4-Bromofluorobenzene
54
1
50.0
108 %
53-136
2BO3042
EPA 8260D
02103122 21:16
RKY
Dibromofluoromethane
43
1
50.0
85 %
67-129
2BO1032
EPA 8260D
0210212212:22
RKY
Dibromofluoromethane
42
1
50.0
85 %
67-129
2BO3042
EPA 6260D
02103122 21:16
RKY
Toluene-d8
46
1
50.0
92 %
59-134
2BO1032
EPA 6260D
0210212212:22
RKY
Toluene-d8
49
1
50.0
98 %
59-134
2BO3042
EPA 6260D
02103122 21:16
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
gy Notes
1,4-Dioxane [123-91-1]^
160
D
ug/L
5
4.0 10
2BO2026
EPA 8260D
02/03/22 10:09
KKW
Surrogates
Results
DF
Syike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-d8
5.4
1
5.00
109 %
75-125
2BO2026
EPA 8260D
0210312210:09
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 45 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CF00921-19 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 16:00 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
1,1,1-Trichloroethane [71-55-6]^
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
1,1,2-Trichloroethane [79-00-5]^
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY A-07
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
1,4-Dichlorobenzene [306-46-7]^
3.0
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
2-Butanone [78-93-3]^
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
2-Hexanone [591-78-6]^
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Acetone [67-64-1]^
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Benzene [71-43-2]A
1.3
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Bromochloromethane [74-97-5]^
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Bromomethane [74-83-9]^
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Carbon disulfide [75-15-0]^
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Carbon tetrachloride [56-23-5]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Chlorobenzene[108-90-7]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Chloroethane [75-00-3]^
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Chloromethane [74-87-3]^
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
cis-1,3-Dichloropropene [10061-01-5]^
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Dibromochloromethane [124-48-1]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Dibromomethane [74-95-3]^
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Ethylbenzene[100-41-4]^
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 12:50
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 46 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R Lab Sample ID:CF00921-19 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 16:00 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 12:50 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 12:50 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
54
1
50.0
108 %
53-136
2BO1032
EPA 8260D
02102122 12:50
RKY
Dibromofluoromethane
43
1
50.0
86 %
67-129
2BO1032
EPA 8260D
0210212212:50
RKY
Toluene-d8
47
1
50.0
95 %
59-134
2BO1032
EPA 8260D
0210212212:50
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
62
ug/L
1
0.80 2.0
2BO2026
EPA 8260D
02/03/22 10:35
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
Toluene-d8
5.4
1
5.00
107 %
75-125
2BO2026
EPA 8260D
021031221025
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 47 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P201) Lab Sample ID:CF00921-20 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 16:30 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO3039
EPA 8260D
02/05/22 00:40
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 48 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20D Lab Sample ID:CF00921-20 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 16:30 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO3039 EPA 8260D 02/05/22 00:40 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO3039 EPA 8260D 02/05/22 00:40 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
54
1
50.0
109 %
53-136
2BO3039
EPA 8260D
02105122 00:40
RKY
Dibromofluoromethane
44
1
50.0
89 %
67-129
2BO3039
EPA 8260D
02105122 00:40
RKY
Toluene-d8
50
1
50.0
100 %
59-134
2BO3039
EPA 8260D
02105122 00:40
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:48
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 11:16
JDH
Barium [7440-39-3]^
49.0
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 11:16
JDH
Beryllium [7440-41-7]^
3.05
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 11:16
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 11:16
JDH
Chromium [7440-47-3]^
3.88
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:16
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:16
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 11:16
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 11:16
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 11:16
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:48
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 11:16
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:48
JDH
Vanadium [7440-62-2]^
3.66
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:16
JDH
Zinc[7440-66-6]^
16.6
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 11:16
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO2026
EPA 8260D
02/03/22 11:00
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.5
1
5.00
110 %
75-125
2BO2026
EPA 8260D
0210312211:00
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 49 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P21 Lab Sample ID:CF00921-21 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 14:00 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,2-Dichloroethane [507-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Ethylbenzene[500-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO8021
EPA 8260D
02/08/22 22:34
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 50 of 96

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www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P21 Lab Sample ID:CF00921-21 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 14:00 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO8021 EPA 8260D 02/08/22 22:34 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO8021 EPA 8260D 02/08/22 22:34 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
57
1
50.0
113 %
53-136
2BO8021
EPA 8260D
02106122 22:34
RKY
Dibromofluoromethane
45
1
50.0
90 %
67-129
2BO8021
EPA 8260D
02106122 22:34
RKY
Toluene-d8
50
1
50.0
100 %
59-134
2BO8021
EPA 8260D
02108122 22:34
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:52
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 11:19
JDH
Barium [7440-39-3]^
59.4
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 11:19
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 11:19
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 11:19
JDH
Chromium [7440-47-3]^
2.14
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:19
JDH
Cobalt[7440-48-4]^
1.74
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:19
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 11:19
JDH
Lead [7439-92-1]^
3.81
J
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 11:19
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 11:19
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:52
JDH
Silver[7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 11:19
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:52
JDH
Vanadium [7440-62-2]^
1.97
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:19
JDH
Zinc[7440-66-6]^
6.80
J
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 11:19
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO2026
EPA 8260D
02/03/22 11:26
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.2
1
5.00
105 %
75-125
2BO2026
EPA 8260D
0210312211:26
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 51 of 96

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ANALYTICAL RESULTS
Description: 7401-P23 Lab Sample ID:CF00921-22 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 13:55 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY A-07
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Chlorobenzene [108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Ethylbenzene [500-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22
13:17
RKY
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 52 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P23 Lab Sample ID:CF00921-22 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 13:55 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 13:17 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 13:17 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
54
1
50.0
108 %
53-136
2BO1032
EPA 8260D
02102122 13:17
RKY
Dibromofluoromethane
44
1
50.0
89 %
67-129
2BO1032
EPA 8260D
0210212213:17
RKY
Toluene-d8
48
1
50.0
95 %
59-134
2BO1032
EPA 8260D
0210212213:17
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
2BO2026
EPA 8260D
02/03/22 11:52
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
Toluene-d8
5.3
1
5.00
106 %
75-125
2BO2026
EPA 8260D
0210312211:52
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 53 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P28 Lab Sample ID:CF00921-23 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 15:00 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY A-07
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Ethylbenzene [500-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 13:45
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 54 of 96

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ANALYTICAL RESULTS
Description: 7401-P28 Lab Sample ID:CF00921-23 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 15:00 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 13:45 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 13:45 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
53
1
50.0
107 %
53-136
2BO1032
EPA 8260D
02102122 13:45
RKY
Dibromofluoromethane
43
1
50.0
86 %
67-129
2BO1032
EPA 8260D
0210212213:45
RKY
Toluene-d8
48
1
50.0
95 %
59-134
2BO1032
EPA 8260D
0210212213:45
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
2BO2026
EPA 8260D
02/03/22 12:17
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
Toluene-d8
5.2
1
5.00
105 %
75-125
2BO2026
EPA 8260D
0210312212:17
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 55 of 96

00�
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ANALYTICAL RESULTS
Description: 7401-P29 Lab Sample ID:CF00921-24 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 10:06 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
1,1,1-Trichloroethane [71-55-6]^
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
1,1,2-Trichloroethane [79-00-5]^
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY A-07
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
1,4-Dichlorobenzene [306-46-7]^
1.5
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
2-Butanone [78-93-3]^
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
2-Hexanone [591-78-6]^
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Acetone [67-64-1]^
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Acrylonitrile [107-13-1]^
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Benzene [71-43-2]A
2.0
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Bromochloromethane [74-97-5]^
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Bromomethane [74-83-9]^
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Carbon disulfide [75-15-0]^
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Carbon tetrachloride [56-23-5]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Chlorobenzene [108-90-7]A
10
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Chloroethane [75-00-3]^
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Chloromethane [74-87-3]^
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
cis-1,3-Dichloropropene [10061-01-5]^
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Dibromochloromethane [124-48-1]^
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Dibromomethane [74-95-3]^
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Ethylbenzene [500-41-4]^
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Iodomethane [74-88-4]^
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
m,p-Xylenes[108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Styrene [100-42-5]^
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22
14:13
RKY
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 56 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P29 Lab Sample ID:CF00921-24 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/25/22 10:06 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 14:13 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 14:13 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
54
1
50.0
108 %
53-136
2BO1032
EPA 8260D
02102122 14:13
RKY
Dibromofluoromethane
43
1
50.0
85 %
67-129
2BO1032
EPA 8260D
0210212214:13
RKY
Toluene-d8
47
1
50.0
95 %
59-134
2BO1032
EPA 8260D
0210212214:13
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
180
D
ug/L
5
4.0 10
2BO4023
EPA 8260D
02/04/22 13:50
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
Toluene-d8
5.3
1
5.00
106 %
75-125
2BO4023
EPA 8260D
0210412213:50
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 57 of 96

0Nk"q09
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ANALYTICAL RESULTS
Description: 7401-SW1 Lab Sample ID:CF00921-25 Received: 01/27/22 10:15
Matrix: Surface Water Sampled:01/26/22 16:53 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,2-Dichloroethane [507-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Ethylbenzene[500-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO8021
EPA 8260D
02/08/22 23:02
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 58 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW1 Lab Sample ID:CF00921-25 Received: 01/27/22 10:15
Matrix: Surface Water Sampled:01/26/22 16:53 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO8021 EPA 8260D 02/08/22 23:02 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO8021 EPA 8260D 02/08/22 23:02 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
55
1
50.0
110 %
53-136
2BO8021
EPA 8260D
02106122 23:02
RKY
Dibromofluoromethane
46
1
50.0
91 %
67-129
2BO8021
EPA 8260D
02106122 23:02
RKY
Toluene-c48
50
1
50.0
99 %
59-134
2BO8021
EPA 8260D
02106122 23:02
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 13:57
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 11:21
JDH
Barium [7440-39-3]^
50.8
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 11:21
JDH
Beryllium [7440-41-7]^
0.241
J
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 11:21
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 11:21
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:21
JDH
Cobalt[7440-48-4]^
8.63
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:21
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 11:21
JDH
Lead [7439-92-1]^
3.53
J
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 11:21
JDH
Nickel[7440-02-O]^
2.88
J
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 11:21
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 13:57
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 11:21
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 13:57
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:21
JDH
Zinc[7440-66-6]^
36.1
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 11:21
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO4023
EPA 8260D
02/04/22 14:16
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.3
1
5.00
105 %
75-125
2BO4023
EPA 8260D
0210412214:16
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 59 of 96

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CF00921-26 Received: 01/27/22 10:15
Matrix: Surface Water Sampled:01/26/22 15:32 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO8021
EPA 8260D
02/08/22 23:30
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 60 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW2 Lab Sample ID:CF00921-26 Received: 01/27/22 10:15
Matrix: Surface Water Sampled:01/26/22 15:32 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO8021 EPA 8260D 02/08/22 23:30 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO8021 EPA 8260D 02/08/22 23:30 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
57
1
50.0
114 %
53-136
2BO8021
EPA 8260D
02106122 23:30
RKY
Dibromofluoromethane
46
1
50.0
91 %
67-129
2BO8021
EPA 8260D
02106122 23:30
RKY
Toluene-c48
50
1
50.0
101 %
59-134
2BO8021
EPA 8260D
02108122 2330
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 14:01
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 11:24
JDH
Barium [7440-39-3]^
44.4
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 11:24
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 11:24
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 11:24
JDH
Chromium [7440-47-3]^
6.02
J
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:24
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:24
JDH
Copper[7440-50-8]^
1.99
J
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 11:24
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 11:24
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 11:24
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 14:01
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 11:24
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 14:01
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:24
JDH
Zinc[7440-66-6]^
11.6
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 11:24
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO2026
EPA 8260D
02/03/22 13:34
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.2
1
5.00
105 %
75-125
2BO2026
EPA 8260D
021031221324
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 61 of 96

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW4 Lab Sample ID:CF00921-27 Received: 01/27/22 10:15
Matrix: Surface Water Sampled:01/25/22 12:35 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY A-07
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 14:41
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 62 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-SW4 Lab Sample ID:CF00921-27 Received: 01/27/22 10:15
Matrix: Surface Water Sampled:01/25/22 12:35 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 14:41 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 14:41 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
51
1
50.0
102 %
53-136
2BO1032
EPA 8260D
02102122 14:41
RKY
Dibromofluoromethane
41
1
50.0
83 %
67-129
2BO1032
EPA 8260D
0210212214:41
RKY
Toluene-c48
45
1
50.0
91 %
59-134
2BO1032
EPA 8260D
0210212214:41
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 14:05
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 11:26
JDH
Barium [7440-39-3]^
17.3
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 11:26
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 11:26
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 11:26
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:26
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:26
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 11:26
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 11:26
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 11:26
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 14:05
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 11:26
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 14:05
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:26
JDH
Zinc[7440-66-6]^
9.99
J
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 11:26
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]A
2.0
ug/L
1
0.80
2.0
2BO2026
EPA 8260D
02/03/22 14:00
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.3
1
5.00
106 %
75-125
2BO2026
EPA 8260D
0210312214:00
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 63 of 96

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ1 Lab Sample ID:CF00921-28 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 15:17 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO8021
EPA 8260D
02/08/22 23:58
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 64 of 96

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ANALYTICAL RESULTS
Description: 7401-PZ1 Lab Sample ID:CF00921-28 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 15:17 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO8021 EPA 8260D 02/08/22 23:58 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO8021 EPA 8260D 02/08/22 23:58 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
56
1
50.0
112 %
53-136
2BO8021
EPA 8260D
02106122 23:58
RKY
Dibromofluoromethane
45
1
50.0
91 %
67-129
2BO8021
EPA 8260D
02106122 23:58
RKY
Toluene-d8
50
1
50.0
99 %
59-134
2BO8021
EPA 8260D
02106122 23:58
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
1.5
1
ug/L
1
0.80 2.0
2BO2026
EPA 8260D
02/03/22 14:26
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
Toluene-d8
5.2
1
5.00
105 %
75-125
2BO2026
EPA 8260D
0210312214:26
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 65 of 96

00�
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ANALYTICAL RESULTS
Description: 7401-PZ2 Lab Sample ID:CF00921-29 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 15:09 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY A-07
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Styrene [100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 15:09
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 66 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-PZ2 Lab Sample ID:CF00921-29 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 15:09 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 15:09 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 15:09 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
52
1
50.0
104 %
53-136
2BO1032
EPA 8260D
02102122 15:09
RKY
Dibromofluoromethane
43
1
50.0
86 %
67-129
2BO1032
EPA 8260D
0210212215:09
RKY
Toluene-d8
48
1
50.0
95 %
59-134
2BO1032
EPA 8260D
0210212215:09
RKY
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80 2.0
2BO2026
EPA 8260D
02/03/22 14:51
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/yzed
By Notes
Toluene-d8
5.2
1
5.00
104 %
75-125
2BO2026
EPA 8260D
0210312214:51
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 67 of 96

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CF00921-30 Received: 01/27/22 10:15
Matrix: Water Sampled:01/26/22 17:00 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY A-07
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Carbon disulfide [75-15-0]A
6.0
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 09:06
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 68 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-EB Lab Sample ID:CF00921-30 Received: 01/27/22 10:15
Matrix: Water Sampled:01/26/22 17:00 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 09:06 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 09:06 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
54
1
50.0
107 %
53-136
2BO1032
EPA 8260D
02102122 09:06
RKY
Dibromofluoromethane
45
1
50.0
91 %
67-129
2BO1032
EPA 8260D
02102122 09:06
RKY
Toluene-d8
48
1
50.0
95 %
59-134
2BO1032
EPA 8260D
02102122 09:06
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 14:14
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 11:29
JDH
Barium [7440-39-3]^
1.10
U
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 11:29
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 11:29
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 11:29
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:29
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:29
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 11:29
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 11:29
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 11:29
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 14:14
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 11:29
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 14:14
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:29
JDH
Zinc[7440-66-6]^
81.5
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 11:29
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
0.80
U
ug/L
1
0.80
2.0
2BO2026
EPA 8260D
02/03/22 15:17
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.2
1
5.00
105 %
75-125
2BO2026
EPA 8260D
0210312215:17
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 69 of 96

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CF00921-31 Received: 01/27/22 10:15
Matrix: Water Sampled:01/26/22 17:05 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY A-07
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 09:34
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 70 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-FB Lab Sample ID:CF00921-31 Received: 01/27/22 10:15
Matrix: Water Sampled:01/26/22 17:05 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 09:34 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 09:34 RKY
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
53
1
50.0
106 %
53-136
2BO1032
EPA 8260D
02102122 09:34
RKY
Dibromofluoromethane
45
1
50.0
90 %
67-129
2BO1032
EPA 8260D
02102122 09:34
RKY
Toluene-d8
48
1
50.0
96 %
59-134
2BO1032
EPA 8260D
02102122 0934
RKY
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
Antimony [7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 14:18
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 11:31
JDH
Barium [7440-39-3]^
1.10
U
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 11:31
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 11:31
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 11:31
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:31
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:31
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 11:31
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 11:31
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 11:31
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 14:18
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 11:31
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 14:18
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:31
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 11:31
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.5
J
ug/L
1
0.80
2.0
2BO2026
EPA 8260D
02/03/22 15:43
KKW
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Analyzed
ffy
Notes
Toluene-d8
5.3
1
5.00
105 %
75-125
2BO2026
EPA 8260D
0210312215:43
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 71 of 96

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-TripBlank Lab Sample ID:CF00921-32 Received: 01/27/22 10:15
Matrix: Water Sampled:01/25/22 09:37 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
1,1-Dichloroethane [75-34-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY A-07
1,1-Dichloroethene [75-35-4]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
1,2,3-Trichloropropane [96-18-4]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
1,2-Dibromo-3-chloropropane [96-12-8]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
1,2-Dibromoethane [106-93-4]A
0.66
U
ug/L
1
0.66
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
1,2-Dichlorobenzene [95-50-1]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
1,2-Dichloroethane [107-06-2]A
0.21
U
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
1,2-Dichloropropane [78-87-5]A
0.10
U
ug/L
1
0.10
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
1,4-Dichlorobenzene [106-46-7]A
0.19
U
ug/L
1
0.19
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
4-Methyl-2-pentanone [108-10-1]A
1.1
U
ug/L
1
1.1
5.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Acetone [67-64-1]A
10
U
ug/L
1
10
20
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Acrylonitrile [107-13-1]A
3.5
U
ug/L
1
3.5
10
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Bromodichloromethane [75-27-4]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Bromoform [75-25-2]A
0.22
U
ug/L
1
0.22
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Bromomethane [74-83-9]A
0.14
U
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Carbon disulfide [75-15-0]A
1.5
U
ug/L
1
1.5
5.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Carbon tetrachloride [56-23-5]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Chlorobenzene[108-90-7]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Chloroethane [75-00-3]A
0.23
U
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Chloroform [67-66-3]A
0.18
U
ug/L
1
0.18
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Chloromethane [74-87-3]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
cis-1,2-Dichloroethene [156-59-2]A
0.15
U
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
cis-1,3-Dichloropropene [10061-01-5]A
0.20
U
ug/L
1
0.20
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Dibromochloromethane [124-48-1]A
0.17
U
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Dibromomethane [74-95-3]A
0.27
U
ug/L
1
0.27
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Ethylbenzene[100-41-4]A
0.13
U
ug/L
1
0.13
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Iodomethane [74-88-4]A
1.7
U
ug/L
1
1.7
5.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Methylene chloride [75-09-2]A
0.23
u
ug/L
1
0.23
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
o-Xylene [95-47-6]A
0.065
u
ug/L
1
0.065
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Styrene[100-42-5]A
0.11
u
ug/L
1
0.11
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Tetrachloroethene [127-18-4]A
0.17
u
ug/L
1
0.17
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Toluene [108-88-3]A
0.14
u
ug/L
1
0.14
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
trans-1,2-Dichloroethene [156-60-5]A
0.21
u
ug/L
1
0.21
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
trans-1,3-Dichloropropene [10061-02-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
trans-1,4-Dichloro-2-butene [110-57-6]A
0.70
u
ug/L
1
0.70
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Trichloroethene [79-01-6]A
0.15
u
ug/L
1
0.15
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Trichlorofluoromethane [75-69-4]A
0.24
u
ug/L
1
0.24
1.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
Vinyl acetate [108-05-4]A
0.95
u
ug/L
1
0.95
5.0
2BO1032
EPA 8260D
02/02/22 08:38
RKY
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 72 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-TripBlank Lab Sample ID:CF00921-32 Received: 01/27/22 10:15
Matrix: Water Sampled:01/25/22 09:37 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 2BO1032 EPA 8260D 02/02/22 08:38 RKY
Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 2BO1032 EPA 8260D 02/02/22 08:38 RKY
Surrogates Results DF
4-Bromofluorobenzene 52 1
Dibromofluoromethane 45 1
Toluene-d8 48 1
Spike L N % Rec % Rec Limits Batch Method
50.0 104 % 53-136 2BO1032 EPA 8260D
50.0 90 % 67-129 2BO1032 EPA 8260D
50.0 96 % 59-134 2BO1032 EPA 8260D
Ana/vzed By Notes
02102122 08:38 RKY
02102122 08:38 RKY
02102122 08:38 RKY
Description: 7401-MW6R-M Lab Sample ID:CF00921-33 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 15:24 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Metals (total recoverable) by
EPA 6000/7000
Series Methods
^ - ENCO Cary certified analyte [NC 5911
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A27015
EPA 6020B
02/08/22 14:31
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 11:34
JDH
Barium [7440-39-3]^
1950
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 11:34
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 11:34
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 11:34
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:34
JDH
Cobalt [7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:34
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 11:34
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 11:34
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 11:34
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A27015
EPA 6020B
02/08/22 14:31
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 11:34
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A27015
EPA 6020B
02/08/22 14:31
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:34
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 11:34
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 73 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P4-M Lab Sample ID:CF00921-34 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 10:13 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Metals (total recoverable)
by EPA 6000/7000
Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A28003
EPA 6020B
02/11/22 10:55
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22 11:37
JDH
Barium [7440-39-3]^
83.4
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22 11:37
JDH
Beryllium [7440-41-7]^
0.205
J
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22 11:37
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22 11:37
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:37
JDH
Cobalt [7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:37
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22 11:37
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22 11:37
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22 11:37
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A28003
EPA 6020B
02/11/22 10:55
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22 11:37
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A28003
EPA 6020B
02/11/22 10:55
JDH
Vanadium [7440-62-2]1
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22 11:37
JDH
Zinc[7440-66-6]^
8.96
J
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22 11:37
JDH
Description: 7401-P12-M Lab Sample ID:CF00921-35 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 14:30 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Metals (total recoverable) by
EPA 6000/7000
Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
E-Q L
Batch
Method
Analyzed
By Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A28003
EPA 6020E
02/11/22
11:08
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28001
EPA 6010D
02/10/22
11:45
JDH
Barium [7440-39-3]^
25.3
ug/L
1
1.10
10.0
2A28001
EPA 6010D
02/10/22
11:45
JDH
Beryllium [7440-41-7]^
0.778
J
ug/L
1
0.160
1.00
2A28001
EPA 6010D
02/10/22
11:45
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28001
EPA 6010D
02/10/22
11:45
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22
11:45
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22
11:45
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28001
EPA 6010D
02/10/22
11:45
JDH
Lead [7439-92-1]^
3.20
J
ug/L
1
3.10
10.0
2A28001
EPA 6010D
02/10/22
11:45
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28001
EPA 6010D
02/10/22
11:45
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A28003
EPA 6020E
02/11/22
11:08
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28001
EPA 6010D
02/10/22
11:45
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A28003
EPA 6020E
02/11/22
11:08
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28001
EPA 6010D
02/10/22
11:45
JDH
Zinc[7440-66-6]^
5.23
J
ug/L
1
4.40
10.0
2A28001
EPA 6010D
02/10/22
11:45
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 74 of 96

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P16R-M Lab Sample ID:CF00921-36 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 14:03 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Metals (total recoverable)
by EPA 6000/7000
Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A28003
EPA 6020B
02/11/22
10:25
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28002
EPA 6010D
02/04/22
13:08
JDH
Barium [7440-39-3]^
1010
ug/L
1
1.10
10.0
2A28002
EPA 6010D
02/04/22
13:08
JDH
Beryllium [7440-41-7]1
0.160
U
ug/L
1
0.160
1.00
2A28002
EPA 6010D
02/04/22
13:08
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28002
EPA 6010D
02/04/22
13:08
JDH
Chromium [7440-47-3]^
2.02
J
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22
13:08
JDH
Cobalt[7440-48-4]^
2.62
J
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22
13:08
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28002
EPA 6010D
02/04/22
13:08
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28002
EPA 6010D
02/04/22
13:08
JDH
Nickel[7440-02-O]^
9.84
J
ug/L
1
2.20
10.0
2A28002
EPA 6010D
02/04/22
13:08
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A28003
EPA 6020B
02/11/22
10:25
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28002
EPA 6010D
02/04/22
13:08
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A28003
EPA 6020B
02/11/22
10:25
JDH
Vanadium [7440-62-2]1
1.40
U
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22
13:08
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2A28002
EPA 6010D
02/04/22
13:08
JDH
Description: 7401-P19-M Lab Sample ID:CF00921-37 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 14:58 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
E-Q L
Batch
Method
Analyzed
By Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A28003
EPA 6020E
02/11/22 11:12
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28002
EPA 6010D
02/04/22 13:34
JDH
Barium [7440-39-3]^
1500
ug/L
1
1.10
10.0
2A28002
EPA 6010D
02/04/22 13:34
JDH
Beryllium [7440-41-7]^
12.5
ug/L
1
0.160
1.00
2A28002
EPA 6010D
02/04/22 13:34
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28002
EPA 6010D
02/04/22 13:34
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22 13:34
JDH
Cobalt[7440-48-4]^
16.2
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22 13:34
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28002
EPA 6010D
02/04/22 13:34
JDH
Lead [7439-92-1]^
3.96
J
ug/L
1
3.10
10.0
2A28002
EPA 6010D
02/04/22 13:34
JDH
Nickel[7440-02-O]^
22.4
ug/L
1
2.20
10.0
2A28002
EPA 6010D
02/04/22 13:34
JDH
Selenium [7782-49-2]^
3.12
ug/L
2
1.82
2.00
2A28003
EPA 6020E
02/11/22 11:12
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28002
EPA 6010D
02/04/22 13:34
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A28003
EPA 6020E
02/11/22 11:12
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22 13:34
JDH
Zinc[7440-66-6]^
98.7
ug/L
1
4.40
10.0
2A28002
EPA 6010D
02/04/22 13:34
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 75 of 96

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www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P20R-M Lab Sample ID:CF00921-38 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 15:04 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Metals (total recoverable)
by EPA 6000/7000
Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A28003
EPA 6020B
02/11/22
11:17
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28002
EPA 6010D
02/04/22
13:36
JDH
Barium [7440-39-3]^
887
ug/L
1
1.10
10.0
2A28002
EPA 6010D
02/04/22
13:36
JDH
Beryllium [7440-41-7]1
0.160
U
ug/L
1
0.160
1.00
2A28002
EPA 6010D
02/04/22
13:36
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28002
EPA 6010D
02/04/22
13:36
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22
13:36
JDH
Cobalt[7440-48-4]^
2.06
J
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22
13:36
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28002
EPA 6010D
02/04/22
13:36
JDH
Lead [7439-92-1]^
4.41
J
ug/L
1
3.10
10.0
2A28002
EPA 6010D
02/04/22
13:36
JDH
Nickel[7440-02-O]^
8.15
J
ug/L
1
2.20
10.0
2A28002
EPA 6010D
02/04/22
13:36
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A28003
EPA 6020B
02/11/22
11:17
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28002
EPA 6010D
02/04/22
13:36
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A28003
EPA 6020B
02/11/22
11:17
JDH
Vanadium [7440-62-2]1
1.40
U
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22
13:36
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2A28002
EPA 6010D
02/04/22
13:36
JDH
Description: 7401-P23-M Lab Sample ID:CF00921-39 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 13:39 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
E-Q L
Batch
Method
Analyzed
By Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A28003
EPA 6020E
02/11/22 11:21
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28002
EPA 6010D
02/04/22 13:39
JDH
Barium [7440-39-3]^
15.3
ug/L
1
1.10
10.0
2A28002
EPA 6010D
02/04/22 13:39
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
2A28002
EPA 6010D
02/04/22 13:39
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28002
EPA 6010D
02/04/22 13:39
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22 13:39
JDH
Cobalt[7440-48-4]^
1.88
J
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22 13:39
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28002
EPA 6010D
02/04/22 13:39
JDH
Lead [7439-92-1]^
3.23
J
ug/L
1
3.10
10.0
2A28002
EPA 6010D
02/04/22 13:39
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28002
EPA 6010D
02/04/22 13:39
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A28003
EPA 6020E
02/11/22 11:21
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28002
EPA 6010D
02/04/22 13:39
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A28003
EPA 6020E
02/11/22 11:21
JDH
Vanadium [7440-62-2]^
1.40
U
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22 13:39
JDH
Zinc[7440-66-6]^
7.84
J
ug/L
1
4.40
10.0
2A28002
EPA 6010D
02/04/22 13:39
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 76 of 96

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www.encolabs.com
ANALYTICAL RESULTS
Description: 7401-P28-M Lab Sample ID:CF00921-40 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 14:50 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Metals (total recoverable)
by EPA 6000/7000
Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PDL
Batch
Method
Analyzed
By Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A28003
EPA 6020B
02/11/22
11:25
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28002
EPA 6010D
02/04/22
13:42
JDH
Barium [7440-39-3]^
52.4
ug/L
1
1.10
10.0
2A28002
EPA 6010D
02/04/22
13:42
JDH
Beryllium [7440-41-7]^
0.982
J
ug/L
1
0.160
1.00
2A28002
EPA 6010D
02/04/22
13:42
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28002
EPA 6010D
02/04/22
13:42
JDH
Chromium [7440-47-3]^
2.65
J
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22
13:42
JDH
Cobalt[7440-48-4]^
3.40
J
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22
13:42
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28002
EPA 6010D
02/04/22
13:42
JDH
Lead [7439-92-1]^
5.17
J
ug/L
1
3.10
10.0
2A28002
EPA 6010D
02/04/22
13:42
JDH
Nickel[7440-02-O]^
2.86
J
ug/L
1
2.20
10.0
2A28002
EPA 6010D
02/04/22
13:42
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A28003
EPA 6020B
02/11/22
11:25
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28002
EPA 6010D
02/04/22
13:42
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A28003
EPA 6020B
02/11/22
11:25
JDH
Vanadium [7440-62-2]^
4.61
J
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22
13:42
JDH
Zinc[7440-66-6]^
20.5
ug/L
1
4.40
10.0
2A28002
EPA 6010D
02/04/22
13:42
JDH
Description: 7401-P29-M Lab Sample ID:CF00921-41 Received: 01/27/22 10:15
Matrix: Ground Water Sampled:01/26/22 10:45 Work Order: CF00921
Project: Pitt County Landfill - App I Sampled By: Laura De Sousa
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
E-Q L
Batch
Method
Analyzed
By Notes
Antimony[7440-36-0]^
0.740
U
ug/L
2
0.740
2.00
2A28003
EPA 6020E
02/11/22 11:29
JDH
Arsenic[7440-38-2]^
7.60
U
ug/L
1
7.60
10.0
2A28002
EPA 6010D
02/04/22 13:44
JDH
Barium [7440-39-3]^
602
ug/L
1
1.10
10.0
2A28002
EPA 6010D
02/04/22 13:44
JDH
Beryllium [7440-41-7]^
0.160
U
ug/L
1
0.160
1.00
2A28002
EPA 6010D
02/04/22 13:44
JDH
Cadmium [7440-43-9]^
0.360
U
ug/L
1
0.360
1.00
2A28002
EPA 6010D
02/04/22 13:44
JDH
Chromium [7440-47-3]^
1.40
U
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22 13:44
JDH
Cobalt[7440-48-4]^
1.40
U
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22 13:44
JDH
Copper[7440-50-8]^
1.60
U
ug/L
1
1.60
10.0
2A28002
EPA 6010D
02/04/22 13:44
JDH
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10
10.0
2A28002
EPA 6010D
02/04/22 13:44
JDH
Nickel[7440-02-0]^
2.20
U
ug/L
1
2.20
10.0
2A28002
EPA 6010D
02/04/22 13:44
JDH
Selenium [7782-49-2]^
1.82
U
ug/L
2
1.82
2.00
2A28003
EPA 6020E
02/11/22 11:29
JDH
Silver [7440-22-4]^
1.90
U
ug/L
1
1.90
10.0
2A28002
EPA 6010D
02/04/22 13:44
JDH
Thallium [7440-28-0]^
0.220
U
ug/L
2
0.220
2.00
2A28003
EPA 6020E
02/11/22 11:29
JDH
Vanadium [7440-62-2]^
9.15
J
ug/L
1
1.40
10.0
2A28002
EPA 6010D
02/04/22 13:44
JDH
Zinc [7440-66-6]^
4.40
U
ug/L
1
4.40
10.0
2A28002
EPA 6010D
02/04/22 13:44
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 77 of 96

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www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2BO1032 - EPA 5030E MS
Blank (2B01032-BLK1) Prepared: 02/01/2022 19:27 Analyzed: 02/02/2022 08:09
Analvte
Result
Flaq
POL
Units
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 78 of 96

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2BO1032 - EPA 5030E MS - Continued
Blank (2B01032-BLK1) Continued Prepared: 02/01/2022 19:27 Analyzed: 02/02/2022 08:09
Spike Source %REC RPD
Analvte
Result Flaq POL
Units
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene
53
u91L
50.0 106 53-136
Dibromofluoromethane
43
u91L
50.0 86 67-129
Toluene-d8
48
u91L
50.0 95 59-134
LCS (2B01032-BSI)
Prepared: 02/01/2022 19:27 Analyzed: 02/02/2022 06:17
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
17
1.0
ug/L
20.0
85
75-133
Benzene
18
1.0
ug/L
20.0
88
80-134
Chlorobenzene
17
1.0
ug/L
20.0
87
80-120
Toluene
18
1.0
ug/L
20.0
91
71-120
Trichloroethene
19
1.0
ug/L
20.0
93
74-120
4-Bromofluorobenzene
53
u91L
50.0
106
53-136
Dibromofluoromethane
43
u91L
50.0
86
67-129
Toluene-d8
48
u91L
50.0
96
59-134
Matrix Spike (2B03032-MS1)
Prepared: 02/01/2022 19:27 Analyzed: 02/02/2022 06:45
Source: CF01262-07
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
0.21 U
88
75-133
Benzene
18
1.0
ug/L
20.0
0.15 U
91
80-134
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
92
80-120
Toluene
19
1.0
ug/L
20.0
0.14 U
97
71-120
Trichloroethene
21
1.0
ug/L
20.0
0.15 U
103
74-120
4-Bromofluorobenzene
52
u91L
50.0
103
53-136
Dibromofluoromethane
42
u91L
50.0
84
67-129
Toluene-d8
47
u91L
50.0
95
59-134
Matrix Spike Dup (2B03032-MSD1)
Prepared: 02/01/2022 19:27 Analyzed: 02/02/2022 07:13
Source: CF01262-07
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
17
1.0
ug/L
20.0
0.21 U
86
75-133
3
20
Benzene
18
1.0
ug/L
20.0
0.15 U
89
80-134
3
17
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
91
80-120
0.8
16
Toluene
19
1.0
ug/L
20.0
0.14 U
94
71-120
4
17
Trichloroethene
20
1.0
ug/L
20.0
0.15 U
100
74-120
3
22
4-Bromofluorobenzene 53 u91L 50.0 105 53-136
Dibromofluoromethane 43 u91L 50.0 86 67-129
Toluene-d8 48 u91L 50.0 96 59-134
Batch 2803039 - EPA 50308 MS
Blank (2B03039-BLK3) Prepared: 02/03/2022 15:38 Analyzed: 02/04/2022 18:09
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L
1,1,1-Trichloroethane 0.12 U 1.0 ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 79 of 96

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2BO3039 - EPA 5030E MS - Continued
Blank (2B03039-BLK1) Continued Prepared: 02/03/2022 15:38 Analyzed: 02/04/2022 18:09
Analvte
Result
Flaq
POL
Units
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 55 u9/L 50.0 109 53-136
Dibromofluoromethane 43 u9/L 50.0 86 67-129
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 80 of 96

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2BO3039 - EPA 5030E MS - Continued
Blank (2B03039-BLK1) Continued Prepared: 02/03/2022 15:38 Analyzed: 02/04/2022 18:09
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Toluene-d8 49 u9/L 50.0 96 59-134
LCS (2B03039-BS1) Prepared: 02/03/2022 15:38 Analyzed: 02/04/2022 16:16
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
94
75-133
Benzene
18
1.0
ug/L
20.0
90
80-134
Chlorobenzene
19
1.0
ug/L
20.0
93
80-120
Toluene
19
1.0
ug/L
20.0
96
71-120
Trichloroethene
19
1.0
ug/L
20.0
96
74-120
4-Bromofluorobenzene
55
ug/L
50.0
110
53-136
Dibromofluoromethane
43
ug/L
50.0
67
67-129
Toluene-d8
50
ug/L
50.0
100
59-134
Matrix Spike (2B03039-MS1)
Prepared: 02/03/2022 15:38 Analyzed: 02/04/2022 16:45
Source: CF01262-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
0.21 U
99
75-133
Benzene
19
1.0
ug/L
20.0
0.15 U
93
80-134
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
97
80-120
Toluene
20
1.0
ug/L
20.0
0.14 U
102
71-120
Trichloroethene
20
1.0
ug/L
20.0
0.15 U
98
74-120
4-Bromofluorobenzene
55
ug/L
50.0
110
53-136
Dibromofluoromethane
43
ug/L
50.0
86
67-129
Toluene-d8
49
u9/L
50.0
97
59-134
Matrix Spike Dup (2B03039-MSD1)
Prepared: 02/03/2022 15:38 Analyzed: 02/04/2022 17:13
Source: CF01262-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
17
1.0
ug/L
20.0
0.21 U
85
75-133
15
20
Benzene
17
1.0
ug/L
20.0
0.15 U
85
80-134
9
17
Chlorobenzene
17
1.0
ug/L
20.0
0.17 U
85
80-120
13
16
Toluene
18
1.0
ug/L
20.0
0.14 U
90
71-120
12
17
Trichloroethene
17
1.0
ug/L
20.0
0.15 U
87
74-120
12
22
4-Bromofluorobenzene 55 u9/L 50.0 111 53-136
Dibromofluoromethane 43 u9/L 50.0 66 67-129
Toluene-& 50 u9/L 50.0 100 59-134
Batch 2BO3042 - EPA 5030E MS
Blank (2B03042-BLK3) Prepared: 02/03/2022 16:15 Analyzed: 02/03/2022 19:55
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
FINAL
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full. Page 81 of 96

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2BO3042 - EPA 5030E MS - Continued
Blank (2B03042-BLK1) Continued Prepared: 02/03/2022 16:15 Analyzed: 02/03/2022 19:55
Analvte
Result
Flaq
POL
Units
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 54 u9/L 50.0 107 53-136
Dibromofluoromethane 43 u9/L 50.0 66 67-129
Toluene-d8 50 u9/L 50.0 101 59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 82 of 96

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2BO3042 - EPA 5030E MS - Continued
LCS (2B03042-BSI) Prepared: 02/03/2022 16:15 Analyzed: 02/03/2022 18:04
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
95
75-133
Benzene
18
1.0
ug/L
20.0
92
80-134
Chlorobenzene
20
1.0
ug/L
20.0
98
80-120
Toluene
20
1.0
ug/L
20.0
101
71-120
Trichloroethene
19
1.0
ug/L
20.0
96
74-120
4-Bromofluorobenzene
56
ug/L
50.0
111
53-136
Dibromofluoromethane
43
u91L
50.0
86
67-129
Toluene-d8
50
u91L
50.0
101
59-134
Matrix Spike (2B03042-MS1)
Prepared: 02/03/2022 16:15 Analyzed: 02/03/2022 18:31
Source: CF01262-12
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
96
75-133
Benzene
19
1.0
ug/L
20.0
0.15 U
94
80-134
Chlorobenzene
20
1.0
ug/L
20.0
0.17 U
100
80-120
Toluene
20
1.0
ug/L
20.0
0.14 U
102
71-120
Trichloroethene
20
1.0
ug/L
20.0
0.15 U
98
74-120
4-Bromofluorobenzene
53
ug/L
50.0
107
53-136
Dibromofluoromethane
43
u91L
50.0
85
67-129
Toluene-d8
50
ug/L
50.0
100
59-134
Matrix Spike Dup (2B03042-MSD1)
Prepared: 02/03/2022 16:15 Analyzed: 02/03/2022 18:59
Source: CF01262-12
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
0.21 U
91
75-133
6
20
Benzene
19
1.0
ug/L
20.0
0.15 U
93
80-134
0.6
17
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
97
80-120
3
16
Toluene
20
1.0
ug/L
20.0
0.14 U
100
71-120
1
17
Trichloroethene
20
1.0
ug/L
20.0
0.15 U
98
74-120
0.2
22
4-Bromofluorobenzene 55 u91L 50.0 109 53-136
Dibromofluoromethane 42 u91L 50.0 64 67-129
Toluene-d8 51 u91L 50.0 102 59-134
Batch 2BO8021 - EPA 50308 MS
Blank (2B08021-BLK3) Prepared: 02/08/2022 14:31 Analyzed: 02/08/2022 18:22
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
FINAL
This report relates only to
the sample as received by the laboratory, and may only be reproduced in full. Page 83 of 96

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2BOS021 - EPA 5030E MS - Continued
Blank (2B08021-BLK1) Continued Prepared: 02/08/2022 14:31 Analyzed: 02/08/2022 18:22
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit Notes
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
4-Bromofluorobenzene
57
u91L
50.0
114
53-136
Dibromofluoromethane
44
u91L
50.0
69
67-129
Toluene-d8
51
u91L
50.0
102
59-134
LCS (2B08021-BSI)
Prepared: 02/08/2022 14:31 Analyzed: 02/08/2022 16:30
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result %REC
Limits RPD
Limit Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
101
75-133
Benzene
19
1.0
ug/L
20.0
95
80-134
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be reproduced in
full.
Page 84 of 96

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 2BOB021 - EPA 5030E MS - Continued
LCS (2B08021-BSI) Continued Prepared: 02/08/2022 14:31 Analyzed: 02/08/2022 16:30
Spike Source %REC RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Chlorobenzene
19
1.0
ug/L
20.0 95 80-120
Toluene
20
1.0
ug/L
20.0 99 71-120
Trichloroethene
20
1.0
ug/L
20.0 98 74-120
4-Bromofluorobenzene
56
u91L
50.0 112 53-136
Dibromofluoromethane
45
u91L
50.0 90 67-129
Toluene-d8
50
u91L
50.0 99 59-134
Matrix Spike (2B08021-MS1)
Prepared: 02/08/2022 14:31 Analyzed: 02/08/2022 16:58
Source: CF01262-13
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,1-Dichloroethene
23
1.0
ug/L
20.0
0.21 U
117
75-133
Benzene
21
1.0
ug/L
20.0
0.15 U
103
80-134
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
104
80-120
Toluene
22
1.0
ug/L
20.0
0.14 U
108
71-120
Trichloroethene
22
1.0
ug/L
20.0
0.15 U
110
74-120
4-Bromofluorobenzene
55
u91L
50.0
111
53-136
Dibromofluoromethane
45
u91L
50.0
90
67-129
Toluene-d8
50
u91L
50.0
101
59-134
Matrix Spike Dup (2B08021-MSD1)
Prepared: 02/08/2022 14:31 Analyzed: 02/08/2022 17:26
Source: CF01262-13
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
0.21 U
100
75-133
16
20
Benzene
19
1.0
ug/L
20.0
0.15 U
94
80-134
9
17
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
92
80-120
12
16
Toluene
19
1.0
ug/L
20.0
0.14 U
94
71-120
15
17
Trichloroethene
19
1.0
ug/L
20.0
0.15 U
97
74-120
13
22
4-Bromofluorobenzene 56 u91L 50.0 112 53-136
Dibromofluoromethane 45 u91L 50.0 91 67-129
Toluene-d8 51 u91L 50.0 101 59-134
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2A27005 - EPA 3005A
Blank (2A27005-BLK3) Prepared: 01/27/2022 06:58 Analyzed: 02/03/2022 12:54
Analvte
Result
Flaq
POL
Units
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 85 of 96

0Nk"q09
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2A27005 - EPA 3005A - Continued
Blank (2A27005-BLKI) Continued Prepared: 01/27/2022 06:58 Analyzed: 02/03/2022 12:54
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Vanadium 1.40 U 10.0 ug/L
Zinc 4.40 U 10.0 ug/L
Blank (2A27005-BLK2) Prepared: 01/27/2022 06:58 Analyzed: 02/03/2022 12:57
Spike Source %REC RPD
Analvte
Result
Flaa
POL
Units
Level Res I %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
LCS (2A27005-BS1)
Prepared: 01/27/2022 06:58 Analyzed: 02/03/2022 13:08
Spike
Source
%REC
RPD
Analvte
Result Flaa
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Arsenic
209
10.0
ug/L
200
104
80-120
Barium
213
10.0
ug/L
200
106
80-120
Beryllium
21.1
1.00
ug/L
20.0
105
80-120
Cadmium
21.0
1.00
ug/L
20.0
105
80-120
Chromium
210
10.0
ug/L
200
105
80-120
Cobalt
215
10.0
ug/L
200
108
80-120
Copper
209
10.0
ug/L
200
105
80-120
Lead
212
10.0
ug/L
200
106
80-120
Nickel
211
10.0
ug/L
200
106
80-120
Silver
211
10.0
ug/L
200
106
80-120
Vanadium
207
10.0
ug/L
200
104
80-120
Zinc
217
10.0
ug/L
200
109
80-120
Matrix Spike (2A27005-MS3)
Prepared: 01/27/2022
06:58 Analyzed: 02/03/2022 13:10
Source: CE19340-01
Spike
Source
%REC
RPD
Awe
Result Flaa
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Arsenic
198
10.0
ug/L
200
7.60 U
99
75-125
Barium
593
10.0
ug/L
200
370
112
75-125
Beryllium
21.0
1.00
ug/L
20.0
0.160 U
105
75-125
Cadmium
18.6
1.00
ug/L
20.0
0.360 U
93
75-125
Chromium
212
10.0
ug/L
200
4.80
104
75-125
Cobalt
215
10.0
ug/L
200
9.71
103
75-125
Copper
205
10.0
ug/L
200
1.60 U
102
75-125
Lead
202
10.0
ug/L
200
3.10 U
101
75-125
Nickel
236
10.0
ug/L
200
29.3
103
75-125
Silver
213
10.0
ug/L
200
1.90 U
107
75-125
Vanadium
205
10.0
ug/L
200
1.40 U
103
75-125
Zinc
226
10.0
ug/L
200
16.9
105
75-125
Matrix Spike Dup (2A27005-MSD1)
Prepared: 01/27/2022
06:58 Analyzed: 02/03/2022 13:13
Source: CE19340-01
Spike
Source
%REC
RPD
Analvte
Result Flaa
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Arsenic
193
10.0
ug/L
200
7.60 U
96
75-125
3
20
Barium
568
10.0
ug/L
200
370
99
75-125
4
20
Beryllium
20.2
1.00
ug/L
20.0
0.160 U
101
75-125
4
20
FINAL
This report relates only to the sample as received by the laboratory, and
may only be
reproduced in
full.
Page 86 of 96

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2A27005 - EPA 3005A - Continued
Matrix Spike Dup (2A27005-MSDS)
Continued
Prepared:
01/27/2022
06:58 Analyzed: 02/03/2022 13:13
Source: CE19340-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Cadmium
18.0
1.00
ug/L
20.0
0.360 U
90 75-125 3
20
Chromium
203
10.0
ug/L
200
4.80
99 75-125 4
20
Cobalt
205
10.0
ug/L
200
9.71
98 75-125 5
20
Copper
195
10.0
ug/L
200
1.60 U
98 75-125 5
20
Lead
192
10.0
ug/L
200
3.10 U
96 75-125 5
20
Nickel
225
10.0
ug/L
200
29.3
98 75-125 5
20
Silver
207
10.0
ug/L
200
1.90 U
104 75-125 3
20
Vanadium
196
10.0
ug/L
200
1.40 U
98 75-125 4
20
Zinc
216
10.0
ug/L
200
16.9
99 75-125 5
20
Post Spike (2A27005-PS1)
Prepared:
01/27/2022
06:58 Analyzed: 02/03/2022 13:16
Source: CE19340-01
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
0.199
0.0100
mg/L
0.200
-0.0125
100
80-120
Barium
0.594
0.0100
mg/L
0.200
0.370
112
80-120
Beryllium
0.0212
0.00100
mg/L
0.0200
-7.37E-5
106
80-120
Cadmium
0.0188
0.00100
mg/L
0.0200
-0.00138
94
80-120
Chromium
0.214
0.0100
mg/L
0.200
0.00480
105
80-120
Cobalt
0.216
0.0100
mg/L
0.200
0.00971
103
80-120
Copper
0.206
0.0100
mg/L
0.200
-0.00407
103
80-120
Lead
0.201
0.0100
mg/L
0.200
-0.00274
101
80-120
Nickel
0.237
0.0100
mg/L
0.200
0.0293
104
80-120
Silver
0.208
0.0100
mg/L
0.200
0.000814
103
80-120
Vanadium
0.206
0.0100
mg/L
0.200
-0.00405
103
80-120
Zinc
0.228
0.0100
mg/L
0.200
0.0169
105
80-120
Batch 1A27015 - EPA 200.8
Blank (2A27015-BLK1)
Prepared:
01/27/2022
11:09 Analyzed: 02/08/2022 12:02
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
0.370
U
1.00
ug/L
Selenium
0.910
U
1.00
ug/L
Thallium
0.110
U
1.00
ug/L
LCS (2A27015-BSI)
Prepared: 01/27/2022 11:09 Analyzed: 02/08/2022 12:06
Spike Source %REC RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
22.1
1.00
ug/L
20.0 111 80-120
Selenium
21.6
1.00
ug/L
20.0 108 80-120
Thallium
22.4
1.00
ug/L
20.0 112 80-120
Matrix Spike (2A27015-MS3)
Prepared: 01/27/2022 11:09 Analyzed: 02/08/2022 12:15
Source: CF00921-01
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Antimony
44.8
2.00
ug/L
40.0
0.740 U
112
75-125
Selenium
43.1
2.00
ug/L
40.0
1.82 U
108
75-125
Thallium
45.1
2.00
ug/L
40.0
0.220 U
113
75-125
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be
reproduced in
full. Page 87 of 96

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2A27015 - EPA 200.8 - Continued
Matrix Spike Dup (2A27015-MSDS)
Prepared: 01/27/2022 11:09 Analyzed: 02/08/2022 12:43
Source: CF00921-01
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
45.4
2.00
ug/L
40.0 0.740 U 113 75-125 1
20
Selenium
42.8
2.00
ug/L
40.0 1.82 U 107 75-125 0.7
20
Thallium
44.6
2.00
ug/L
40.0 0.220 U 111 75-125 1
20
Post Spike (2A27015-PS1)
Prepared: 01/27/2022 11:09 Analyzed: 02/08/2022 12:47
Source: CF00921-01
Spike Source %REC RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
21.8
1.00
ug/L
20.0-0.0298 109 75-125
Selenium
21.4
1.00
ug/L
20.0-0.0710 107 75-125
Thallium
21.8
1.00
ug/L
20.0 0.0143 109 75-125
Batch 2A28001 - EPA 3005A
Blank (2A28001-BLK1)
Prepared: 01/28/2022 04:30 Analyzed: 02/10/2022 09:58
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
LCS (2A28001-BSI)
Prepared: 01/28/2022 04:30 Analyzed: 02/10/2022 10:13
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Arsenic
222
10.0
ug/L
200
111
80-120
Barium
223
10.0
ug/L
200
112
80-120
Beryllium
22.0
1.00
ug/L
20.0
110
80-120
Cadmium
22.7
1.00
ug/L
20.0
113
80-120
Chromium
220
10.0
ug/L
200
110
80-120
Cobalt
224
10.0
ug/L
200
112
80-120
Copper
201
10.0
ug/L
200
101
80-120
Lead
227
10.0
ug/L
200
113
80-120
Nickel
225
10.0
ug/L
200
112
80-120
Silver
219
10.0
ug/L
200
110
80-120
Vanadium
216
10.0
ug/L
200
108
80-120
Zinc
233
10.0
ug/L
200
116
80-120
Matrix Spike (2A28001-MS3)
Prepared:
01/28/2022
04:30 Analyzed: 02/10/2022 10:16
Source: CF00921-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 88 of 96

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2A28001 - EPA 3005A - Continued
Matrix Spike (2A28001-MS3) Continued
Prepared:
01/28/2022
04:30 Analyzed: 02/10/2022 10:16
Source: CF00921-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
234
10.0
ug/L
200
7.60 U
117 75-125
Barium
288
10.0
ug/L
200
48.8
120 75-125
Beryllium
23.4
1.00
ug/L
20.0
0.336
115 75-125
Cadmium
23.8
1.00
ug/L
20.0
0.360 U
119 75-125
Chromium
228
10.0
ug/L
200
1.40 U
114 75-125
Cobalt
240
10.0
ug/L
200
1.40 U
120 75-125
Copper
202
10.0
ug/L
200
1.60 U
101 75-125
Lead
240
10.0
ug/L
200
3.10 U
120 75-125
Nickel
239
10.0
ug/L
200
2.20 U
120 75-125
Silver
224
10.0
ug/L
200
1.90 U
112 75-125
Vanadium
223
10.0
ug/L
200
1.40 U
111 75-125
Zinc
251
10.0
ug/L
200
4.45
123 75-125
Matrix Spike Dup (2A28001-MSD1)
Prepared:
01/28/2022
04:30 Analyzed: 02/10/2022 10:19
Source: CF00921-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
234
10.0
ug/L
200
7.60 U
117 75-125 0.2
20
Barium
291
10.0
ug/L
200
48.8
121 75-125 1
20
Beryllium
23.5
1.00
ug/L
20.0
0.336
116 75-125 0.2
20
Cadmium
24.1
1.00
ug/L
20.0
0.360 U
121 75-125 1
20
Chromium
230
10.0
ug/L
200
1.40 U
115 75-125 0.8
20
Cobalt
243
10.0
ug/L
200
1.40 U
121 75-125 1
20
Copper
201
10.0
ug/L
200
1.60 U
100 75-125 0.5
20
Lead
241
10.0
ug/L
200
3.10 U
120 75-125 0.6
20
Nickel
241
10.0
ug/L
200
2.20 U
120 75-125 0.7
20
Silver
222
10.0
ug/L
200
1.90 U
111 75-125 0.5
20
Vanadium
224
10.0
ug/L
200
1.40 U
112 75-125 0.4
20
Zinc
253
10.0
ug/L
200
4.45
124 75-125 1
20
Post Spike (2A28001-PS1)
Prepared:
01/28/2022
04:30 Analyzed: 02/10/2022 10:37
Source: CF00921-09
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit
Notes
Arsenic
0.243
0.0100
mg/L
0.200
0.000218
121
80-120
QM-08
Barium
0.295
0.0100
mg/L
0.200
0.0488
123
80-120
QM-08
Beryllium
0.0241
0.00100
mg/L
0.0200
0.000336
119
80-120
Cadmium
0.0245
0.00100
mg/L
0.0200
-0.000162
122
80-120
QM-08
Chromium
0.236
0.0100
mg/L
0.200
0.000349
118
80-120
Cobalt
0.248
0.0100
mg/L
0.200
0.000559
124
80-120
QM-08
Copper
0.205
0.0100
mg/L
0.200
-0.0181
103
80-120
Lead
0.246
0.0100
mg/L
0.200
0.00279
122
80-120
QM-08
Nickel
0.247
0.0100
mg/L
0.200
-0.00128
123
80-120
QM-08
Silver
0.223
0.0100
mg/L
0.200
0.000144
112
80-120
Vanadium
0.230
0.0100
mg/L
0.200
0.00114
114
80-120
Zinc
0.260
0.0100
mg/L
0.200
0.00445
128
80-120
QM-08
Batch 1A28001- EPA 3005A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 89 of 96

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2A28001- EPA 3005A - Continued
Blank (2A28002-BLK3) Prepared: 01/28/2022 04:34 Analyzed: 02/04/2022 13:05
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Beryllium
0.160
U
1.00
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Cobalt
1.40
U
10.0
ug/L
Copper
1.60
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Nickel
2.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Vanadium
1.40
U
10.0
ug/L
Zinc
4.40
U
10.0
ug/L
LCS (2A28002-BSI)
Prepared: 01/28/2022 04:34 Analyzed: 02/04/2022 13:12
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit
Notes
Arsenic
206
10.0
ug/L
200
103 80-120
Barium
213
10.0
ug/L
200
107 80-120
Beryllium
21.0
1.00
ug/L
20.0
105 80-120
Cadmium
21.0
1.00
ug/L
20.0
105 80-120
Chromium
209
10.0
ug/L
200
105 80-120
Cobalt
210
10.0
ug/L
200
105 80-120
Copper
208
10.0
ug/L
200
104 80-120
Lead
210
10.0
ug/L
200
105 80-120
Nickel
213
10.0
ug/L
200
107 80-120
Silver
208
10.0
ug/L
200
104 80-120
Vanadium
206
10.0
ug/L
200
103 80-120
Zinc
219
10.0
ug/L
200
110 80-120
Matrix Spike (2A28002-MS3)
Prepared:
01/28/2022
04:34 Analyzed: 02/04/2022 13:15
Source: CF00921-36
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit
Notes
Arsenic
181
10.0
ug/L
200
7.60 U
90 75-125
Barium
1280
10.0
ug/L
200
1010
135 75-125
QM-07
Beryllium
19.6
1.00
ug/L
20.0
0.160 U
98 75-125
Cadmium
16.4
1.00
ug/L
20.0
0.360 U
82 75-125
Chromium
196
10.0
ug/L
200
2.02
97 75-125
Cobalt
190
10.0
ug/L
200
2.62
93 75-125
Copper
175
10.0
ug/L
200
1.60 U
88 75-125
Lead
191
10.0
ug/L
200
3.10 U
96 75-125
Nickel
199
10.0
ug/L
200
9.84
95 75-125
Silver
205
10.0
ug/L
200
1.90 U
103 75-125
Vanadium
199
10.0
ug/L
200
1.40 U
100 75-125
Zinc
201
10.0
ug/L
200
4.40 U
100 75-125
Matrix Spike Dup (2A28002-MSDS)
Prepared:
01/28/2022
04:34 Analyzed: 02/04/2022 13:18
Source: CF00921-36
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit
Notes
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be reproduced in full.
Page 90 of 96

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QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2A28001- EPA 3005A - Continued
Matrix Spike Dup (2A28002-MSDS)
Continued
Prepared:
01/28/2022
04:34 Analyzed: 02/04/2022 13:18
Source: CF00921-36
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
173
10.0
ug/L
200
7.60 U
87 75-125 4
20
Barium
1210
10.0
ug/L
200
1010
99 75-125 6
20
Beryllium
18.4
1.00
ug/L
20.0
0.160 U
92 75-125 6
20
Cadmium
15.5
1.00
ug/L
20.0
0.360 U
78 75-125 6
20
Chromium
184
10.0
ug/L
200
2.02
91 75-125 6
20
Cobalt
177
10.0
ug/L
200
2.62
87 75-125 7
20
Copper
165
10.0
ug/L
200
1.60 U
83 75-125 6
20
Lead
183
10.0
ug/L
200
3.10 U
91 75-125 4
20
Nickel
186
10.0
ug/L
200
9.84
88 75-125 7
20
Silver
196
10.0
ug/L
200
1.90 U
98 75-125 5
20
Vanadium
188
10.0
ug/L
200
1.40 U
94 75-125 6
20
Zinc
188
10.0
ug/L
200
4.40 U
94 75-125 7
20
Post Spike (2A28002-PS1)
Prepared:
01/28/2022
04:34 Analyzed: 02/04/2022 13:20
Source: CF00921-36
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
0.178
0.0100
mg/L
0.200
-0.0199
89
80-120
Barium
1.25
0.0100
mg/L
0.200
1.01
124
80-120 QM-08
Beryllium
0.0190
0.00100
mg/L
0.0200
-0.000265
95
80-120
Cadmium
0.0162
0.00100
mg/L
0.0200
-0.00213
81
80-120
Chromium
0.191
0.0100
mg/L
0.200
0.00202
94
80-120
Cobalt
0.185
0.0100
mg/L
0.200
0.00262
91
80-120
Copper
0.171
0.0100
mg/L
0.200
-0.0253
85
80-120
Lead
0.189
0.0100
mg/L
0.200
0.000504
94
80-120
Nickel
0.195
0.0100
mg/L
0.200
0.00984
92
80-120
Silver
0.198
0.0100
mg/L
0.200
-0.000740
99
80-120
Vanadium
0.194
0.0100
mg/L
0.200
0.000844
97
80-120
Zinc
0.196
0.0100
mg/L
0.200
0.00254
97
80-120
Batch 2A28003 - EPA 200.8
Blank (2A28003-BLK1)
Prepared:
01/28/2022
04:36 Analyzed: 02/11/2022 10:11
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Antimony
0.370
U
1.00
ug/L
Selenium
0.910
U
1.00
ug/L
Thallium
0.110
U
1.00
ug/L
LCS (2A28003-BSI)
Prepared: 01/28/2022 04:36 Analyzed: 02/11/2022 10:15
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Antimony
23.8
1.00
ug/L
20.0 119 80-120
Selenium
24.1
1.00
ug/L
20.0 120 80-120
Thallium
23.4
1.00
ug/L
20.0 117 80-120
Matrix Spike (2A28003-MS3)
Prepared: 01/28/2022 04:36 Analyzed: 02/11/2022 10:29
Source: CF00921-36
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
FINAL
This report relates only to
the sample as received by the
laboratory, and may only be reproduced in full.
Page 91 of 96

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www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 2A28003 - EPA 200.8 - Continued
Matrix Spike (2A28003-MS3) Continued
Prepared: 01/28/2022 04:36 Analyzed: 02/11/2022 10:29
Source: CF00921-36
Spike
Source
O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Antimony
48.3
2.00
ug/L
40.0
0.740 U
121
75-125
Selenium
45.0
2.00
ug/L
40.0
1.82 U
112
75-125
Thallium
44.7
2.00
ug/L
40.0
0.220 U
112
75-125
Matrix Spike Dup (2A28003-MSDS)
Prepared: 01/28/2022 04:36 Analyzed: 02/11/2022 10:33
Source: CF00921-36
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
O/oREC
Limits RPD
Limit Notes
Antimony
49.6
2.00
ug/L
40.0
0.740 U
124
75-125 3
20
Selenium
49.0
2.00
ug/L
40.0
1.82 U
123
75-125 9
20
Thallium
45.9
2.00
ug/L
40.0
0.220 U
115
75-125 3
20
Post Spike (2A28003-PS3)
Prepared: 01/28/2022 04:36 Analyzed: 02/11/2022 10:38
Source: CF00921-36
Spike
Source
O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
O/oREC
Limits RPD
Limit Notes
Antimony
25.1
1.00
ug/L
20.0
0.197
125
75-125
Selenium
24.5
1.00
ug/L
20.0
0.700
119
75-125
Thallium
23.2
1.00
ug/L
20.0
0.0642
115
75-125
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch 2BO1026 - EPA 5030B MS
Blank (2B03026-BLK3)
Prepared: 02/01/2022 00:00 Analyzed: 02/01/2022 14:17
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
1,4-Dioxane
0.80
U
2.0
ug/L
Toluene-&
5.4
u91L
5.00 108 75-125
LCS (2B01026-BSI)
Prepared: 02/01/2022 00:00 Analyzed: 02/01/2022 13:51
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
1,4-Dioxane
26
2.0
ug/L
25.0 104 80-133
Toluene-&
5.3
u9/L
5.00 106 75-125
Matrix Spike (2B03026-MS1)
Prepared: 02/01/2022 00:00 Analyzed: 02/01/2022 23:20
Source: CF00921-01
Spike Source O/oREC
RPD
Analvte
Result
Flaa
Q
Units
Level Result O/oREC Limits RPD
Limit
Notes
1,4-Dioxane
24
2.0
ug/L
25.0 0.80 U 98 80-133
Toluene-&
4.7
u91L
5.00 93 75-125
Matrix Spike Dup (2B01026-MSDI)
Prepared: 02/01/2022 00:00 Analyzed: 02/01/2022 23:46
Source: CF00921-01
Spike Source O/oREC
RPD
Analvte
Result
Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit
Notes
1,4-Dioxane
25
2.0
ug/L
25.0 0.80 U 100 80-133 2
19
Toluene-&
4.3
u9/L
5.00 87 75-125
Batch 2BO2026 - EPA 5030E MS
FINAL This
report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 92 of 96

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www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch 2BO2026 - EPA 5030E MS - Continued
Blank (2B02026-BLK1)
Prepared: 02/02/2022 00:00 Analyzed: 02/03/2022 08:49
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
0.80
U
2.0
ug/L
Toluene-d8
5.3
u9/L
5.00 106 75-125
LCS (2B02026-BSI)
Prepared: 02/02/2022 00:00 Analyzed: 02/03/2022 08:24
Spike Source %REC
RPD
Analvte
Result
Flao
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
25
2.0
ug/L
25.0 101 80-133
Toluene-d8
4.9
u9/L
5.00 99 75-125
Matrix Spike (2B02026-MS1)
Prepared: 02/02/2022 00:00 Analyzed: 02/03/2022 17:51
Source: CF00921-19
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
87
2.0
ug/L
25.0 62 98 80-133
Toluene-d8
5.5
u9/L
5.00 110 75-125
Matrix Spike Dup (2B02026-MSD1)
Prepared: 02/02/2022 00:00 Analyzed: 02/03/2022 18:16
Source: CF00921-19
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
86
2.0
ug/L
25.0 62 94 80-133 1
19
Toluene-d8
5.3
u9/L
5.00 106 75-125
Batch 2BO4023 - EPA 5030E MS
Blank (2B04023-BLKI)
Prepared: 02/04/2022 00:00 Analyzed: 02/04/2022 10:40
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
0.80
U
2.0
ug/L
Toluene-d8
5.2
u9/L
5.00 104 75-125
LCS (2B04023-BS1)
Prepared: 02/04/2022 00:00 Analyzed: 02/04/2022 10:15
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
24
2.0
ug/L
25.0 97 80-133
Toluene-d8
5.4
u9/L
5.00 107 75-125
Matrix Spike (2B04023-MS1)
Prepared: 02/04/2022 00:00 Analyzed: 02/04/2022 19:49
Source: AF00794-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
40
2.0
ug/L
25.0 17 93 80-133
Toluene-d8
5.4
u9/L
5.00 108 75-125
Matrix Spike Dup (2B04023-MSD1)
Prepared: 02/04/2022 00:00 Analyzed: 02/04/2022 20:15
Source: AF00794-03
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
1,4-Dioxane
40
2.0
ug/L
25.0 17 93 80-133 0.2
19
FINAL This report relates only to
the sample as received by the laboratory, and may only be reproduced in full.
Page 93 of 96

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch 2BO4023 - EPA 5030E MS - Continued
Matrix Spike Dup (2B04023-MSDS) Continued Prepared: 02/04/2022 00:00 Analyzed: 02/04/2022 20:15
Source: AF00794-03
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Toluene-d8 5.3 ug/L 5.00 106 75-125
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 94 of 96

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www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
A-07 Analyte biased low in LCS but detected in the reporting limit standard. Since the analyte in the associated
sample was not detected, there is no impact on data quality.
0-01 This compound is a common laboratory contaminant.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QS-03 Surrogate recovery outside acceptance limits
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 95 of 96

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
10775 C
� Orlando. Central
3N24 Or. Jacksonv10 ille. FL 32216-6069 tive Park Count, une 111 CDarya Woodwinds Industrial Cl.
CS NS [phone] Fax [phone] [phone] Fax [phone] [phone] Fax [phone] Page 1 of
Client Name Project Number Requested Analyses Requested Turnaround
Groundwaw mainagerrhom Associates, Inc. (GRM) [none] Q Times
Address Project NamerDesc W
Note: Rush requests subject to
4300 Sapphire Court, Slbte 100 Pitt County Lerldfill - App I _ ❑ � acceptance by the raciI4
CIty1STIZp PO 01 Billing Info ir: tD
Greenville, NC 27834 =p o
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Tel Fax Reporting Contact & x Q
[phone] Emma Shipley a C] _ Expedited
Sampler(s) Name. Affixation (Pant) Billie Contact Q m
�1U2h1 DE SWSA - C Mf91mma Shipley o o M Due
Se piers} S ure Site Location me Time Zone C3 Lab Workorder
f2eeNV)4Lf NC/EASTERN C00 ` $'
Preservation (See Codes) (Combine as necessary) C F 00921
C-01 lion Matrix Total 4 of
item fl Sampte ID (Field Identification) Collection Date Time Comp, Grab (see codes) Containers Sample Comments
7401-Mw1 R 1- 2. 17 4W 6WAD GW 7 _ -
7401-11 !-2(o-2Z 9 A GaAe GW 7 X X
740141M R I --Z5 -ZZ 1(0; zo (qF-A Q GW =F 40 X
7401.4MB r 10 Q Gw 1 7 X X
7401-P'2 1- Z4-2 Z cif: 35 G ?- to GW 7 X X
7401-P'4 1-25 2 Z 9 : 3 } (UiPi (N Gw :z- (a x
7401-Pr5 IT (6f VtB GW 7 X X
74014P'6 1 fX 30 C e-0`9 GW 7 X X
7401-P'7 1-2(. --22 ..5o GO a GW 7 X X
7401-P'9 / a&-2 /Z:06 tea" GW 7 X X
7401-P'11R it -20 -Z,?/q:'20C7 AB GW 7 X X
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f—sample Kit Prepared By
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Date +me
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ID N
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Received By
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Relinquished By
DateMme
Received By 1 0
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Cooler n's & Temps on Receipt
I I
�� ✓ f IJ�JR
Cowan upon Receipt
Acceptable Unacceptable
Matrix' GWGroundwaler SO -Sod OW -Drinking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O.Other (detail In cammeks) Preservation: Flos H•H I N-HNO3 S-142SO4 NO-Na0H Other (cletal In comments)
Note: All samples submitted to ENCO Labs are in accordance with the terms and conditions fisted on the reverse of this form, unless prior written agreements exist

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
10775 Central Port or 4810 Executive Park Court, Suite 111 102-A Woodwinds Industrial C1.
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[phone] Fax (407) 85"945 [phone] Fau [phone] (919) 46T-3090 Fax [phone] Page Z of
Client Name Project Number Requested Analyses Requested Turnaround
GroutidwaW Management Associates, Ina- (GRM) [none] 0 Times
Address Project Name/Desc Nate RU5h requeSts subjact to
43DO Sapphire Court, Suite 100 Pitt County Landfill - App �"
Q � acceptance by the facility
r _
CitylST/Ztp PO A / Billing Info X z
pp
C�'eenv lle, NC 27834 =v at; c's Standard
Tel Fax Reporting Contact C V
[phone] Emma Shipley FL Expedited
Sampler(s) Name, Atfillation (Pnni) 9dtin Cn I C1 O
LAtvzA L1ESUu5 � - tri1Pr I mma Shiley Q m9 Due /
Sa pler(s) lure Site Locaflon I Time Zone fl � 4 Lab Workorder
�QEENY,u-E Nc Efyf7-6-Z V co ZF CF00921
Preservation (See Codes) (Combine as necessary]
Collection Matrix Tot.3i -t of
Item q Sample ID (Field Identification) Collection Date Time Comp / Grab (see codes) Conlamers Sample Comments
7401-P12 _ow to
7401-P13 I+ Uepqa GW 7 X X
7401-P13D 1 Z& ZZ 11:3q GP_48 w 7 X X --
7401-P16R I-ZS-22 14:15 (a2R13 GW -'r (o X
7401-PIT ! Z(o ZZ jq .`q!S Gef e GW 7 X X `
74101-P19 1-75-22 (27eAa GW X Ar
7401-P2DR r-zs za IL: ov GaAO GW X
741011-17201) 1-26--ZZ 1(C ) 006 GW 7 X X
7401-P21 1-Z(P-Z7- 1f : Ub A13 Gull 7 X X
T4401-P23 1-Z5-Z2 13•'55 CW8 GW all {a X
744D1-P26 1-25-2Z /S: DO C=Wf ? GW X
74101-P29 I 1- Z5 -2z 110 : O G C12A 13 GW if 0 X i ;
—4=f- <-- Total N of Containers
Sample Kit Prepared By
Datelrime
Ralirsquish y
DalelRme
Roc d By
(�
Da
effim
(1
�f
Comments/Special Reponing Requirements
Tielinquished By
Datw7ime
Received By
Daler rime
Relinquished By
Date/Time
Received By
Date/Tme
Cooler 115 & Temps on Receipt
1
Condbon Upon Receipl
Y Acceptable Unacceptable
Matrix GW-Groundwater SO -Soil DW-Drink(ng Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-other (debit in comments) Preservation: I -Ice H-HCI N-HNO3 S-H2SO4 NO-NaOH O-Other (detel In comments)
Note. Ail samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form. unless prior written agreements exist

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
PECP 10775 Central 48t 0 Executive Park f Quit, Suite t 11 102-A Woodwinds Industrial Ct
Orlando, FL 32824 Jacksonville, FL 3221 B-6069 Cary, NC 27511
[phone] Fax (407) M-6945 [phone] Fax (904) 296-&210 (9191 467-3090 Fax [phone]
www.encolabs.com
Page 3 of
Client Name
GrourKKvatrMBrtagelneint Assodtaes, kv- (GM22)
Project Number
[nor*]
Proileed NeernelDesc
PM WUrdy L.8�11 - App I
Requested
Analyses
Requested Turnaround
Times
NWe Rushte by ssuhjty to
acceptance she facility
Standard
_ Expedited
Due l�l_
C
FL
CL
Q
p
m
fl
?
N
aOORL
tO
t�R//
ri
�
0
L
gF
AddrelsrsV� SapphireCourt, i.. 4�/�
43DO Sapp ire Cou `r Sul tO !V0
City/STOp
Greenville, NC 27W
PO It / Billing info
Tel Fax
(252) 75S.3310
Reporting Contact
Emma Shipley
Sampler(s) Name, Affiliation (Print)
L�ur2p 6,5oud'R —C�. mlq-
BIIIing Contact
Emma Shipley
Sampler(s) S1 lure
Glvc
Site Location / nme Zone
G2EE/Jl/1L1-E /UC E►�ST�ieiAJ
Lab WOrkorder
CFO g21
Preservation
{Sae
Codes)
(Combine
as necessary)
lem #
Sample ID (Field IdenfiTicalion)
Collection Date
Collection
Time
Comp i G+ab
Matrix
(see codes)
-total # of
Containers
Sample Comments
7401-SW1
l-zt,"
14:):S3
G42AO
f ftO
7401-SW2
f-Zf�;-2.2
15 3Z
SW
7
X
X
7401-SW4
1-25 2Z
12: 3.5
SW
7
X
X
7401-PZ3
I -Ze ZZ
l 5. I�t-
fl a
GW
X fo
X
v,
f
7401-Pz2
172AP 2P.
15. C9
E,24a
GW
Mo "
7401-EB
I -Z fp-ZZ
1 W
CRIP?
WA
7
X
X
7401-FB
l -Z(o-
I
WA
7
X
X
7401-Tri Blanc
C';R-P'3
WA
2
X
<- Total # of Containers
Sample Kit Prepared By
DatwTime
Re inquss By
l
Dame
i a& --z z Ins
R By
ice---
D te/f i
2�I
717 10% l�
CommentslSpacial Reporting Requirements
eltnquished By
Dalalt'ime
Received By
ernrne
Relinquished By
Datemme
Received By
DalerRme
ooler Its & Temps on Receipt
r
Condtinn Upon Receipt
Acceptable Unacceptable
Matrix: GWGroundwatar SOSoll DW-Ddnking Water SE -Sediment SW -Surface Water WW-Wastewater A -Air O-Other (detail in comments) Preservation: I -Ice H.HCI N-HNO3 S-H2SO4 NO-NaOli D-Other (detail in comments)
Note: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse at this (arm, unless prior written agreements exist

ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com
10775 Central Part of. 4810 Execubve Park Court, Suite 111 102-A Woodwinds Industrial CL
CIS Nkk G 0 Orlando, FL 32824 Jacksonville, FL 32216.6069 Cary, NC 27511
[phone] Fax [phone] T04) 296-3407 Fax [phone] [phone] Fax [phone] Page _q_ of
Client Name
CJ-;
Projecl Number
Requested
Analyses
I Requested Tumaround
Times
Nate :Rush requests subject to
acceptance by the lath ty
Standard
_ Expedited
Due
k
V
°
><
a �
Address
C A��� f Co
y J
Project NamelDest
T�
L/ Y— _
[ Aepr
CitylSTOP
C 2EEN vl t.L� ►J C Z�3
PO 4 1 Billing Into
Tat
Z54- 58-3310
Fax
Reporting Contact
CMMO SH I PL Ey
Sampler(s) Name, Atfirratron (Print)
LauQill+ Dc SUuxt4 A
- ��
Billing Contact
�Mm19 SN�Pr_Ey
S pler(s) S lure /
site Location i Time Zone
GO BEN VI LLE N G /C49S7-E0e,
Lab Workorder
Preservation
)Sea
Codes)
(Combine
as necessary)
Hem 4
Sample ID (Field Identification)
Collection Date
Colleciton
Time
Camp / Grab
Matrix
(see codes)
Total 4 of
Containers
Sample Comments
_7401-mw(oR-M
1-2e-Z7-
15'.Z4
C-7eA9
GW
I
X
_7901- Py-M
1-2e zz
1u:13
CeAG
Caw
I
-71-4 o 1- P/2 - M
I--7]6-Zz
l L; 3L-)
C Vr3
ICJ
1
?-101-- PI&Q-M
1-2_r, zZ
r-q.03
K-XA(3
w
I
x
'Nw - P 11-M
27
tyt'Sg
alQa3
7 y 0 1 - PZOQ -M
i5.,og
CRAB
W
l
X
7 b1-P13-M
I -2-(v 7t
1339
G*19S
7y01- P -/W
1-2.,--2-z
1y:5)
EiRf\3
' L-Z
1
X
7y01- P29 -M
j-%0-o--2Z
ID;`ISGgAB
�(
q
< Total # of containers
Sample Kit Prepared By
Date/Time
Re' quished B
Datorrme
R - By
0 lelil
e
�---
Camments/Speciat Reporting Requirements
Aelinquishe'd By
Date7rime
Received By
Da eiTime
Relsnquished By
DateiTime
Received By `
4�
DaleMme
Cooler k's 8 Temps on Receipt
Corwtion Upon Receipt
2
1�- d i I C) - Z C�la3 � — CC
_�t Acceptable Unacceptable
Matrllr : GW-Gmundwaier So -Soil OW-Onriking Water SE-Sedimenl SW-Surtace Water WW-Waslewaler A - Alt O-Ocher (derail In camrnenls) Presemat)on: 1-Ice H-HCi N•HNO3 S-H2SO4 NO-NaOH O-Outer (petal in commonlsl
Nate : Ali samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist

Sample Preservation Verification
ENCO Cary
Work Order CF00921 ProjecL Pitt County Landfill - App I
Client Groundwater Management Associates, Inc (GR022; Project#: [none]
Logged In: 27-Jan-22 10:21 Logged By Rachel Ann` ronis
Preservation Check Performed By -4) DatelTime:
CF00921-01
Cunt
Type
Pres (pH)
Requirement
pH Checked 1
In Control
pH Adjusted Datemme
Adjusted
Reagent Used/Comments
A
2.50ml-P+ HNO3
<2
Y , N 1 NA
YIN NA
CF00921-02
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y I N i NA
Y! N i NA
CF00921-05
Cont
Type
Pres (pH)
Requirement
pH Checked I
In Control
pl-! Adjusted DatefTime
Adjusted
Reagent Used/Comments
A
250mLPi-1-11\103
�2
Y N I NA
Y N NA
C F00921-06
Cont
Type
Pres (pH)
Requirement
pH Checked 1
In Control
pH Adjusted DateMme
Adjusted
Reagent Used/Comments
A
250mLf' 1 HNO3
<2
Y I N I NA
Y I N NA
C F 009 21-08
Cont
Type
Pres (pH)
Requiiernent
pH Checked /
In Control
pH Adjusted DatelTime
Adjusted
Reagent UsedlComments
G
250mt-P+HNO3
<2
Y '1 N i NA
Y I N I NA
C F00921-09
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DateMme
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y N/ NA
Y)
Y (N NA
C F00921-10
Cant
Type
Pres (pH)
pH Checked /
pH Adjusted DatelTime
Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
Y I N I NA
Y I N NA
C F00921 -11
Cont
Type
Pres (PH)
Requirement
pH Checked I
In Control
pH Adjusted DatelTime
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
YIN / NA
+ / N NA
CF00921-12
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DateMme
Adjusted
Reagent Used/Comments
A
250rnLP+HNO3
2
Y N/ NA
Y{ N/ NA
C1e:lmnt%Printlwko_Preservation Check rpt Page I of 4

Sample Preservation Verification
ENCO Cary
Work Order CF00921 Project Pitt County Landfill - App I
Client: Groundwater Management Associates. Inc (GRO22; Project #: [none]
Logged In: 27-Jan-22 10:21 Logged By: Rachel An Yonsh ` 1,
Preservation Check Performed By: S i
ZI ZL 4 i
CF00921-14
Cont
Type
Pres (pH}
pH Checked 1
pH Adjusted DatelTime
Reagent UsedlComments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
Y N 1 NA
Y/ N NA
CF00921-15
Cont
Type
Pres (pH) pH Checked I
pH Adjusted DatelTime
Reagent Used/Comments
Requirement In Control
Adjusted
A
250mLP+HNO3
Y N NA
CF00921-17
Cant
Type
Pres (pH) J
Requirement
pH Checked !
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y N / NAJ
Y 1&/ NA
CF00921-20
Cant
Type
Pres (pH)
pH Checked /
pH Adjusted Date/Time
Reagent UsedlComments
Requirement
in Control
Adjusted
A
250ml P+HNO3
=2
Y )1 N / NA
Y / N NA
CF00921-21
Cont
Type
Pres (pH)
Requirement
pH Checked /
in Control
pH Adjusted DatelTime
Adjusted
Reagent UsedlComments
A
250mLP+HNO3
<2
Y N 1 NA
Y N NA
CF00921-25
Cont
Type
Pres (pH)
pH Checked I
pH Adjusted DatelTime
Reagent UsedlComments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
Yj / N I NA
Y l; N 1) NA
CF00921-26
Cant
Type
Pres (pH)
pH Checked /
pH Adjusted DatelTime
I
Reagent Used/Comments
Requirement
I In Control
Adjusted
A
250mLPi HNO3
<2
Y/ N I NA
Y 1 N NA
CF00921-27
Gont
Type
Pres (pH) pH Checked /
pH AUjusted DateMme
Reagent UsedlComments
Requirement In Control
Adjusted
A
250mLP+HNO3
<2 Y N/ NA
Y N NA
CF00921-30
Cant
Type
Pres (pH) pH Checked /
Requirement In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2 Y t N I NA
Y 1 NA
CIelmntlPrintlwko_Preservation Check. rpt Page 2 of d

Sample Preservation Verification
ENCO Cary OD
9 CE
Work Order: CF00921 Project: Pitt County Landfill - App I
Client. Groundwater Management Associates, Inc (GR022; Project #: [none]
Logged In 27-Jan-22 10:21 Logged By: Rachel Ann Yonih
Preservation Check Performed By A Date/Time: 21 ILL 1 '4 0-->
CF00921-31
Cont
Type
Pres (PH)
Requirement
pH Checked 1
in Control
PH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250ml-P+HNO3
<2 f
Y N/ NA
Y N' NA
C F00921-33
Cont
Type
Pres (pH)
Requirement
pH Checked 1
In Control
pH Adjusted DatelTme
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
- 2
Y N I NA
Y Ly NA
CF00921-34
Cant
Type Pres (pH)
pH Checked /
pH Adjusted DateJTirne
Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLPA-HNO3 <2
Y/ N/ NA
Y kNJ NA
C F00921-35
Cant
Type
Pres (pH)
PH Checked /
Date/Time
pH .Adjusted
Reagent Used/Comments
Requirement
in Control
Adjusted
A
250mLP+HNO3
Y, N! NA
Y I N I NA
CF00921-36
Cont
Type
Pres (pl-1)
Requirement
pH Checked 1
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y 'I! N / NA
b1 N / NA 4
Z14 [ qW
C F00921-37
Cont
Type Pres (PH)
Requirement
pH C ecked 1
In Control
pH Adjusted DatelTime
Adjusted
Reagent Used/Comments
A
2.50mLP+HNO3 <2 1
Y N / NA
Y -N / NA
CF00921-38
Cont
Type
Pies (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y N/ NA
Y N NA
CF00921-39
Gont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adtusted DateTme
Adjusted
Reagent Used/Curnments
A
250mLP+HNO3
'2
Y N/ NA
Y/ N NA.
C F00921-40
Cont
Type
Pres (pH)
Requirement
pH Checked /
n Control
pH Adjusted Dateffime
Adjusted
Reagent Used/Comments
A
250mt_P+HNO3
-2
! N/ NA
Y N I NA
C'leimntlPrintlwko_PreservationCheck .rpt Page 3 of 4

Sample Preservation Verification
ENGO Gary
co
Work Order. CF00921 Project: Pitt County Landfill - App I
Client. Groundwater Management Associates, Inc. (GR022) Project #: [none]
Logged In: 27-Jan-22 10:21 Logged By: Rachel Ann Yon�ii `
Preservation Check Performed By: _ DaterFime: Z f u_ ! U
CF00921-41
Cant
Type Pres (pH)
Requirement
pH Checked !
In Control
pH Adjusted Daterrime
Adiusted
Reagent Used/Comments
r;OmLP+HNO3 <2
Y N / NA
Y !
N NA
Reacient Name ID
1
2
pH Strip ID:
PH Strips C0F0555
Rea ent Name ID
3
4
Rea ent Name ID
5
6
C-Ielmnt\Prit _ .�.,.,,.,�r.,�wrTecx.rpt Pat -IL, a :