1107_Buncombe_MSWLF_CDLF_Oct21GW_FID1655529_20220315

DEN
R USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR I IEnvironmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Bunnell-Lammons Engineering, Inc. (consultant)
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Andrew W. Alexander. PG RSM Phone: [phone]
E-mail: andy.alexander(cDblecorp.com
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
1107-MSWLF
Buncombe County Landfill 81 Panther Branch Road
-1996 .1600
Alexander, NC, 28701 1107-CDLF .0500 October 26-28, 2021
-1998 0
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data El
water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Andrew W. Alexander, PG RSM Consultant Hydrogeologist [phone]
Facility Representative Name (Print) Title (Area Code) Telephone Number
�� w a• �E,o•,....=a•d,a „®e,•o,owm, 3/15/2022
Signature Date
6004 Ponders Court, Greenville, SC, 29615
Facility Representative Address
C-284 & C-1538
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
Affix NC Licensed/ Professional Geologist Seal
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NS�c'titi9
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WATER QUALITY REPORT
2nd SEMI-ANNUAL
EVENT 2021
BUNCOMBE COUNTY LANDFILL
ALEXANDER, NORTH CAROLINA
Permit No. 1107-MSWLF-1996
Permit No. 1107-CDLF-1998
Prepared For:
Buncombe County
BLE Project Number J21-9378-26
March 7, 2022 ���"I 1CAR
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1nI#JIII% +'`
BLE North Carolina Business Licenses C-284 & C-1538
IM BUNNELL
LAMMONS
ENGINEERING
6G04 Ponders Court I Grppnville, SC 29515
`864.2OH.1265 e 864.28 AKA N_P. into @Nerorp.mm
BLECORRCOM

IM I BUNNELL
� LAMMONS
ENGINEERING
March 7, 2022
Buncombe County Solid Waste Department
81 Panther Branch Road
Alexander, North Carolina 28701
Attention: Ms. Kristy Smith
Subject: Water Quality Report
2°d Semi -Annual Event 2021
Buncombe County Landfill
Alexander, North Carolina
Permit Nos. 1107-MSWLF-1996 & 1107-CDLF-1998
BLE Project Number J21-9378-26
Dear Ms. Smith:
Pursuant to authorization of Bunnell-Lammons Engineering, Inc. (BLE) Proposal Number J21-9378-26, dated
June 22, 2021, BLE has prepared this water quality report for the 2t'd semi-annual sampling event of 2021 at
the Buncombe County Landfill. Consistent with the North Carolina Division of Waste Management (DWM)
— Solid Waste Section (SWS) approved monitoring program, sampling and analysis was conducted twice in
2021. This report contains the information required by the DWM to document the sampling and analysis
activities for the second event of 2021 in the State's permanent project record.
Sincerely,
BUNNELL LAMMONS ENGINEERING INC.
Ril . �Bla_is,
Staff Hydrogeologist
cc: Ms. Jaclynne Drummond — DWM-ARO
d4/
Andrew W. Ale der, P.G., RSM
Consultant Hydrogeologist
Registered, NC # 1475
Ilblegvlsvrllsolidwasteprojectslbuncombe county active d( nc19378-26a fy22 fall 2021 reportW5 reportlactive bclf 1107-mswlf--1996 2nd 2021
semi-annual 9378-26. docx
' 6004 Ponders Court, Greenville, SC 29615 '%864,28B,1255 6'�864,288,4430 info@bleEorp,LCm
BLECORP.COM

1s 1m 1i
Water Quality Report — 2nd Semi -Annual Event 2021 March 7, 2022
Buncombe County Landfill —Alexander, North Carolina BLE Project No. J21-9378-26
TABLE OF CONTENTS
1.0
PROJECT INFORMATION........................................................................................................1
2.0
FIELD ACTIVITIES, SAMPLING, AND ANALYSIS.............................................................1
3.0
GROUNDWATER FLOW........................................................................................................... 2
4.0
RESULTS....................................................................................................................................... 2
4.1
Groundwater.................................................................................................................................... 2
4.2
Surface Water.................................................................................................................................. 2
4.3
Leak Detectors and Leachate Samples............................................................................................. 2
5.0
CONCLUSIONS AND RECOMMENDATIONS.......................................................................3
6.0
QUALIFICATIONS OF REPORT.............................................................................................. 3
7.0
CLOSING.......................................................................................................................................3
Tables
Table 1
SWS Approved Sampling Matrix
Table 2
Well Construction and Monitoring Well Data
Table 3
Range of Groundwater Flow Velocities
Table 4
Groundwater VOCs
Table 5
Groundwater Field Parameters, Geochemical Parameters, and Total Metals
Table 6
Surface Water VOCs
Table 7 Surface Water Field Parameters and Total Metals
Table 8 Leak Detector and Leachate VOCs
Table 9 Leak Detector and Leachate Field Parameters and Total Metals
Figures
Figure 1 Site Location Map
Figure 2 Groundwater Elevation Contour Map — October 25 — 26, 2021
Appendices
Appendix A Field Sampling Logs — Pace Analytical Services, LLC.
Appendix B Laboratory Analytical Data — Pace Analytical Services, LLC.
iofi

1s 1m 1i
Water Quality Report — 2nd Semi -Annual Event 2021
Buncombe County Landfill —Alexander, North Carolina
1.0 PROJECT INFORMATION
March 7, 2022
BLE Project No. J21-9378-26
The subject 654-acre landfill site is located in Buncombe County, North Carolina, approximately nine miles
north of the city of Asheville with a physical address of 81 Panther Branch Road in Alexander, North Carolina.
Buncombe County owns and operates a Subtitle D MSWLF which includes Cell 1 through Cell 6 and a CDLF
consisting of Phase 1 through Phase 6. Currently Cell 6 of the MSWLF and Phase 6 of the CDLF are the
active waste units. MSWLF Cell 7 and CDLF Phase 7 have been permitted for construction and MSWLF
Cells 8 through 10 are planned (but not permitted) for future expansion.
A Water Quality Monitoring Plan (WQMP) was finalized by BLE and submitted to the North Carolina Solid
Waste Section (SWS). The WQMP was approved on April 16, 2021 (FID 1576846). The facility requires
semi-annual groundwater, surface water, and leachate monitoring and reporting in accordance with the
WQMP. Semi-annual sampling is typically conducted each April and October and those events are designated
"Spring" and "Fall," respectively. This report represents the 2nd semi-annual (Fall) sampling event of 2021.
The existing groundwater monitoring network for the Buncombe County Landfill consists of two (2)
upgradient (background) wells (MW-1 and MW-1D) and twenty-four (24) downgradient (compliance) wells
(MW-2, MW-213, MW-3R, MW-4, MW-413, MW-5, MW-513, MW-6, MW-7, MW-8, MW-81), MW-10,
MW-IOD, MW-11, MW-11D, MW-12, MW-121), MW-13, MW-13D, MW-14, MW-14D, MW-17R, MW-
17DR, and MW-18). Wells MW-17 and MW-17D were abandoned September 14, 2020 and replaced by
MW-17R and MW-17DR respectively. Wells MW-15 and MW-15D were removed as compliance points and
replaced by MW-18 as approved by the SWS on August 3, 2021 (FID 1595460). The MW-151MW-15D well
pair remains in place for the collection of water levels only. The current SWS approved sampling matrix is
included as Table 1.
In accordance with Rule .0602 and Rule .0544(c), eight (8) surface water monitoring locations have been
established for the facility to monitor surface water quality surrounding the existing waste footprint (Table
1). The existing surface water locations consist of one (1) upstream (background) point (SW-1) and seven (7)
downstream (compliance) points (SW-2 through SW-8).
In accordance with Rule .1626(12)(c), eight (8) active leachate sampling locations have been established for
the facility (Table 1). The locations include six (6) existing leak detection sampling locations associated with
each MSWLF cell (Cells 1 through 6) designated LD-1 through LD-6, one (1) leachate leak detection
sampling location near the leachate pond designated Leachate LD, and the Leachate Pond itself.
2.0 FIELD ACTIVITIES, SAMPLING, AND ANALYSIS
Groundwater, surface water, and leachate samples were collected for the 2nd semi-annual sampling event by
personnel from Pace Analytical Services, LLC. (Pace) of Asheville, North Carolina between October 26-28,
2021. Groundwater samples were collected from the groundwater monitoring well locations located on the
site as specified on Table 1. The seven (7) of the eight (8) surface water locations were sampled during the
event. Surface water location SW-7 was dry at the time of sampling; therefore, no sample was collected.
Additionally, the seven (7) leak detection and one (1) leachate pond locations were sampled.
The groundwater, surface water, and leachate samples were delivered and analyzed in Pace's Columbia, South
Carolina laboratory for the constituents in the approved matrix (Table 1). The field parameters of dissolved
oxygen, pH, redox potential, specific conductance, turbidity, and temperature were measured in the field by
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1s 1M 1i
Water Quality Report — 2nd Semi -Annual Event 2021
Buncombe County Landfill —Alexander, North Carolina
March 7, 2022
BLE Project No. J21-9378-26
Pace. A copy of the Pace field sampling logs is included in Appendix A. A copy of the laboratory analytical
data is included in Appendix B.
kxi=" .Z111 0 IWii/:r 104 451 y 1ClliiVA
The water level data collected during the groundwater sampling event on October 25-26, 2021 is presented
in Table 2. Groundwater flow velocity estimates are presented on Table 3. A groundwater elevation
contour map is presented as Figure 2 which includes generalized groundwater flow directions.
4.0 RESULTS
4.1 Groundwater
The results of the groundwater field and laboratory analyses are summarized on Tables 4 and 5 and the
laboratory analytical data is included in Appendix B.
Please refer to Tables 4 and 5 for a summary of which groundwater constituents exceeded North Carolina
Groundwater Quality Standards (NC2L) maximum contaminant levels' (MCLs).
Field parameters measured in the groundwater included pH, specific conductance, turbidity, and temperature.
The field parameter of pH was below its NC2L standard in thirteen (13) wells. However, previous semi-annual
reports for the subject site indicate that pH frequently varies between values both below and within the NC2L
standards in the majority of the wells on site. No other field parameters were outside their NC2L standard
limits for groundwater, if established.
4.2 Surface Water
The results of the surface water field and laboratory analyses are summarized on Tables 6 and 7 and the
laboratory analytical data is included in Appendix B.
Please refer to Table 6 and 7 for a summary of which surface water constituents exceeded their established
North Carolina Surface Water Quality Standards (NC2B)2 standard limits. Field parameters measured in the
surface water included dissolved oxygen, pH, redox potential, specific conductance, turbidity, and
temperature. The field parameter of turbidity was above its NC2B standards in three (3) locations. None of
the other sampled field parameters were outside their NC213 standard limits for surface water, if established.
4.3 Leak Detectors and Leachate Samples
The results of the leak detector field and laboratory analyses are summarized on Tables 8 and 9 and the
laboratory analytical data is included in Appendix B.
'North Carolina Department of Environmental Quality, Classifications of Water Quality Standards, Section 15A NCAC 2L.0202, April 1, 2013.
2 North Carolina Department of Environmental Quality, Surface Waters and Wetlands Standards, Section 15A NCAC 02B workbook dated June
10, 2019.
2 of 3

1s 1m 1i
Water Quality Report — 2nd Semi -Annual Event 2021
Buncombe County Landfill —Alexander, North Carolina
March 7, 2022
BLE Project No. J21-9378-26
Please note that the NC2L standards shown on Tables 8 and 9 are for reference only. There is no regulatory
standard for leak detectors or leachate.
Field parameters measured in the leak detectors and leachate samples included pH, specific conductance,
turbidity, and temperature.
5.0 CONCLUSIONS AND RECOMMENDATIONS
Semi-annual assessment monitoring was performed during the 2" d semi-annual event of 2021 in general
accordance with the approved WQMP and SWS approved sampling matrix (Table 1). Detected constituents
which exceed their respective groundwater and surface water standards are identified on the summary tables.
6.0 QUALIFICATIONS OF REPORT
The activities and evaluative approaches used in this assessment are consistent with those normally employed
in hydrogeological and environmental assessments of this type. Our evaluation of site conditions has been
based on our understanding of the site and project information and the data provided to BLE.
This report has been prepared on behalf of and exclusively for the use of Buncombe County, North Carolina.
This report and the findings contained herein shall not, in whole or in part, be used or relied upon by any other
party (excluding the DWM) without BLE's prior written consent.
7.0 CLOSING
We appreciate the opportunity to be of service to Buncombe County, North Carolina. Please contact us at
[phone] if you have any questions or comments.
3 of 3

TABLES

Table 1
SWS Approved Sampling Matrix
Buncombe County Landfill
Alexander, North Carolina
Permit No. 1107-CDLF-1998
Permit No. 1107-MSWLF-1996
BLE Project Number J21-9378-26
April
October
Station ID
*Analytical Suite*
1,4-Dioxane
*Analytical Suite*
1,4-Dioxane
a
MW-1
A-1 Plus
A-1 Plus
x �
u
Pa
MW-ID
A-1 Plus
A-1 Plus
MW-2
A-1
A-1
MW-21)
A-1
A-1
MW-3R
A-1
A-1
MW-4
A-1
yes
A-1
yes
MW-41)
A-1
yes
A-1
yes
MW-5
A-1
A-1
MW-5D
A-1
A-1
MW-6
A-1
A-1
MW-7
A-1
A-1
MW-8
A-1
A-1
MW-8D
A-1
A-1
MW-10
A-1
yes
A-1
yes
MW-lOD
A-1
yes
A-1
yes
MW-11
A-1
A-1
u
e
MW-11D
A-1
A-1
UMW-12
A-1 Plus
yes
A-1 Plus
yes
MW-12D
A-1 Plus
yes
A-1 Plus
yes
MW-13
A-1
A-1
MW-13D
A-1
A-1
MW-14
A-1 Plus
A-1 Plus
MW-14D
A-1 Plus
A-1 Plus
MW-15
W
W
MW-15D
W
W
MW-16
A-1
yes
A-1
yes
MW-16D
A-1
yes
A-1
yes
MW-17
Abandoned September 14, 2020
MW-17D
Abandoned September 14, 2020
MW-17R
A-1 Plus
yes
A-1 Plus
yes
MW-17DR
A-1 Plus
yes
A-1 Plus
yes
MW-18
A-1 Plus
yes
A-1 Plus
yes
SW-1
A-1
yes
A-1
yes
SW-2
A-1
yes
A-1
yes
SW-3
A-1
yes
A-1
yes
d
SW-4
A-1
yes
A-1
yes
o
SW-5
A-1T
yes
A -IT
yes
SW-6
A-1T
yes
A -IT
yes
SW-7
A-1
yes
A-1
yes
SW-8
A-1T
yes
A -IT
yes
LD-1
A-1
A-1
i,
LD-2
A-1
A-1
0
LD-3
A-1
A-1
Ca
R
LD-4
A-1
A-1
u
�?
LD-5
A-1
A-1
yes
d
R
LD-6
A-1
A-1
u
LD-7
A-1
A-1
.a
Leachate LD
A-1
A-1
Leachate Pond
LMP
LMP
Notes:
A-1 —Appendix I VOCs & Metals
A -IT = Appendix I VOCs plus Tetrahydrofuran & Metals
A-1 Plus = Appendix I VOCs plus Tetrahydrofuran,
& Metals plus Mercury, Manganese, Iron, Sulfate, Chloride,
Alkalinity, & Total Dissolved Solids
LMP (Leachate Monitoring Parameters) = Appendix I VOCs & Metals, pH,
specific conductance, BOD, COD, Nitrates, Sulfates, & Phosphates.
W = Water Level Only
LD = Leak Detector
Does Not Exist - Pennitted for Future MSWLF Cell 7
1,4-Dioxane removed for these points
Table revised July 16, 2019 (SW-8 and 1,4-doxane)
Table revised February 27, 2020 (BLE Project No. 9378-20 for Spring 2020)
Table revised June 19, 2020 (Change 1,4-Dioxane Matrix)
Table revised October 14, 2020 (Abandon MW-17/MW-17D)
Table revised July 20, 2021 (Remove MW-15/MW-15D & add MW-18)
Prepared by: AWA
Checked by: TJD
S:\Buncombe County Active LF, NC\9378-26A FY22 Fall 2021 Report\04 Tables\9378-26 SWS Approved Matrix

Table 2
Well Construction and Monitoring Well Data
Buncombe County Landfill
Alexander, North Carolina
Permit No. 1107-CDLF-1998
Permit No. 1107-MSWLF-1996
BLE Project Number J21-9378-26
Monitoring Point
MSW or
C&D
Latitude
Longitude
Northing'
Easting'
TOC
Elevation (ft)'
Ground Surface
Elevation (ft)'
Depth to GW (ft)
October 25-26, 2021
Groundwater
Elevation (ft)
Well Depth
(fit)'
Screen Depth
(below GS)'
Waste Unit
Monitored
Installation
Date'
Geology Monitored'
Well
Status/Purpose
Well
Diameter (in)'
MW-1
Facility
33.570245
-85.567196
737,383.3
923,481.5
2021.22
2019.28
64.70
1956.52
76
61.0 - 76.0
Facility
1990's
Saprolite/PWR
Background
2.0
MW-ID
Facility
33.570242
-85.567236
737,371.0
923,468.7
2021.57
2019.97
66.21
1955.36
200
85.0 - 95.0
Facility
1990's
Bedrock
Background
2.0
MW-2
MSW
33.570284
-85.566586
739,569.6
921,033.3
1920.86
1918.54
8.52
1912.34
20
5.0 20.0
Cell
1990's
Saprolite/PWR
Compliance
2.0
MW-2D
MSW
33.570283
-85.566599
739,565.7
921,027.7
1920.51
1918.63
8.73
1911.78
55
45.0 - 55.0
Cell
1990's
Bedrock
Compliance
2.0
MW-3R
MSW
33.570271
-85.566817
739,499.1
920,384.3
1973.18
1975.67
54.94
1918.24
55
45.0 - 55.0
Cell
7/28/2014
PWR
Compliance
2.0
MW-4
MSW
33.570228
-85.567590
739,263.0
920,192.1
1944.35
1942.48
12.95
1931.40
25
9.0 24.0
Cell
1011011996
Saprolite/PWR
Compliance
2.0
MW-4D
MSW
33.570228
-85.567597
739,261.0
920,177.3
1944.64
1942.79
14.27
1930.37
55
45.0 - 55.0
Cell
1011111996
Bedrock
Compliance
2.0
MW-5
MSW
33.570201
-85.568087
739,111.5
920,246.7
1977.12
1975.39
33.96
1943.16
50
35.0 - 50.0
Cell
101911996
Saprolite/PWR
Compliance
2.0
MW-5D
MSW
33.570199
-85.568112
739,103.6
920,242.3
1976.92
1975.31
35.86
1941.06
81
71.0 - 81.0
Cell
1011011996
Bedrock
Compliance
2.0
MW-6
MSW
33.570317
-85.565937
738,767.9
920,223.6
1987.34
1985.39
24.98
1962.36
50
35.0 - 50.0
Cell
101811996
Saprolite/PWR
Compliance
2.0
MW-7
MSW
33.570230
-85.567514
738,286.3
920,586.8
2022.83
2020.72
44.99
1977.84
61
42.0 - 61.0
Cell
101411996
Saprolite/PWR
Compliance
2.0
MW-8
MSW
33.570196
-85.568117
738,102.0
920,801.7
1962.06
1959.85
29.11
1932.95
70
55.0 - 70.0
Cell
1990's
Saprolite/PWR
Compliance
2.0
MW-8D
MSW
33.570199
-85.568069
738,116.7
920,812.0
1962.47
1960.57
27.86
1934.61
95
85.0 - 95.0
Cell
1990's
Bedrock
Compliance
2.0
MW-10
MSW
33.570239
-85.567391
739,324.0
921,597.0
2010.54
2007.50
68.44
1942.10
73
58.0 - 73.0
Cell
3/6/2002
Saprolite/PWR
Compliance
2.0
MW-10D
MSW
33.570239
-85.567391
739,324.0
921,590.8
2010.56
2007.50
69.03
1941.53
117
102.0 - 117.0
Cell
3/6/2002
Bedrock
Compliance
2.0
MW-11
MSW
33.570208
-85.567897
738,169.2
921,422.1
1966.71
1963.70
32.95
1933.76
50
35.0 - 50.0
Cell
3/6/2002
Bedrock
Compliance
2.0
MW-11D
MSW
33.570206
-85.567947
738,154.0
921,406.0
1966.15
1963.20
34.21
1931.94
70
60.0 - 70.0
Cell
3/6/2002
Bedrock
Compliance
2.0
MW-12
C&D
33.570306
-85.566147
738,703.7
919,192.4
1947.39
1944.70
12.20
1935.19
17
7.0 17.0
Phases 1 - 5
6/25/2002
Saprolite/PWR/Bedrock
Compliance
2.0
MW-12D
C&D
33.570269
-85.566849
739,489.5
921,966.6
1947.10
1944.30
10.91
1936.19
37
27.0 - 37.0
Phases 1 - 5
6/25/2002
Bedrock
Compliance
2.0
MW-13
MSW
33.570269
-85.566849
739,489.5
921,966.6
1953.92
1951.30
4.67
1949.25
16
6.0 16.0
Cell
612412005
Bedrock
Compliance
2.0
MW-13D
MSW
33.570316
-85.565957
738,761.6
919,055.7
1953.82
1951.40
7.36
1946.46
44
39.0 - 44.0
Cell
6/23/2005
Bedrock
Compliance
2.0
MW-14
C&D
33.570320
-85.565889
738,782.5
919,037.1
1952.77
1949.80
29.85
1922.92
49
39.0 - 49.0
Phases 1 -5
4/5/2006
Bedrock
Compliance
2.0
MW-14D
C&D
33.570306
-85.566147
738,703.7
919,192.4
1953.76
1950.70
30.28
1923.48
88
78.0 - 88.0
Phases 1 - 5
4/6/2006
Bedrock
Compliance
2.0
MW-15
C&D
33.570207
-85.567982
739,143.4
919,829.3
1973.29
1970.21
21.33
1951.96
26
16.0 - 26.0
Phases 1 - 5
6/7/2012
Saprolite/PWR
WL
2.0
MW-15D
C&D
33.570207
-85.567982
739,143.4
919,829.3
1973.51
1970.25
21.08
1952.43
43
33.0 - 43.0
Phases 1 - 5
6/7/2012
Bedrock
WL
2.0
MW-17
Abandoned - September 14, 2020
MW-17D
Abandoned - September 14, 2020
MW-17R
C&D
33.570283
-85.566553
738,579.7
918,662.0
1891.61
1888.96
15.82
1875.79
23.5
8.5 23.5
Phase 6
9/3/2020
Bedrock
Compliance
2.0
MW-17DR
C&D
33.570281
-85.566586
738,569.7
918,659.3
1891.70
1889.14
14.21
1877.49
39
34.0 - 39.0
Phase 6
9/2/2020
Bedrock
Compliance
2.0
MW-18
C&D
33.570214
-85.567851
739,183.2
919,705.2
1940.67
1937.97
44.75
1895.92
51.5
41.5 - 51.5
Phases 1 - 5
6/11/2008
Bedrock
Compliance
2.0
' - Data from Table 3, Well Construction, New Buncombe County Landfill, Buncombe County, North Carolina, provided by SCS Engineers.
Z - Based on visual observation of Sheet No I Groundwater and Methane Monitoring Well Locations by CDM Smith dated August 2014.
Some well installation dates appear inconsistent with water level records and may not be accurate. Changes to some dates (italics) made based on water level records and dates from SHR and DHR documents by CDM.
The top of casing and ground surface elevations for MW-3R are a probable error (reversed) based on April 2016 water levels in the SCS Engineers report.
The top of casing and ground surface elevations for MW-14 and MW-14D do not match those in the SHR and DHR documents by CDM.
The well construction and survey data for MW-17R and MW-17DR are from a report by SCS dated October 13, 2020
Location accuracy of the monitoing wells is limited by the references themselves
The well construction data for MW-18 are from the DHR table and boring log by CDM. Surveying was performed by Ed Holmes and Associates of Asheville, NC in September 2021.
TOC - Top of Casing.
GS - Ground Surface.
WL - Water Level only
All depth measurments in feet -- All elevations in feet above an arbitrary site datum
9378-26A GW Tables (Completion, water levels, detections) Prepared by: RLB
T2 (10-26-21) MW Points Checked by: TAO/ AWA

Table 3
Range of Groundwater Flow Velocities
Buncombe County Landfill
Alexander, North Carolina
Permit No. 1107-CDLF-1998
Permit No. 1107-MSWLF-1996
BLE Project Number J21-9378-26
Hydraulic Conductivity
K(ft/min)
K(cm/sec)
K(ft/day)
High Estimate
8.0E-03
4.1E-03
11.500
Low Estimate
9.7E-05
4.9E-05
0.140
Geometric Mean
8.8E-04
4.5E-04
1.269
Geometric Mean Hydraulic
Conductivity K(ft/day)
Hydraulic
Grad. (ft/ft)
Effective
Porosity
Flow
Vel. (ft/day)
Flow
Vel. (ft/year)
High Estimate
1.269
0.286
5%
7.25
2647
Low Estimate
1.269
0.025
28%
0.12
42
Notes
1. Hydraulic conductivity and effeictive porosity values obtainted from Tables 5 and 6 of the Design Hydrogeologic Report
- Phase 6 C&D prepared by BLE dated September 21, 2017.
3. The hydraulic gradients were measured from the October 25-26, 2021 groundwater elevation contour map (Figure 2).
The high hydraulic gradient was measured between the 1880-ft & 1900-ft groundwater contours near MW-17R and MW-19.
The low hydraulic gradient was measured between the 1950-ft & 1960-ft groundwater contours near MW-12.
4. Groundwater velocity derived from V = Ki/n, where:
K = geometric mean hydraulic conductivity, i = hydraulic gradient, and n, = effective porosity.
5. The high and low velocity estimates are calculated using the geometric mean K and the high and low range of site hydraulic data
obtained from BLE's 2017 DHR.
9378-26A GW Tables (Completion, water levels, detections) Prepared By: RLB
Table 3 GW Flow Vel. Checked By: TAO/ AWA

Table 4
Groundwater VOCs
Buncombe County Landfill
Alexander, North Carolina
Permit No. 1107-CDLF-1998
Permit No. 1107-MSWLF-1996
BLE Project Number J21-9378-26
Sampled by Pace Analytical Services, LLC. October 26-28, 2021
TEST
UNITS
LOQ
DL
MCL
MW-1
MW-11)
MW-2
MW-21)
MW-311
MW4
MW4D
KW-5
MW-513
KW-6
MW-7
KW-8
MW-81)
KW-10
MW-lOD
MW-11
MW-11D
MW-12
AM-12D
MW-13
MW-13D
MW-14
MW-14D
MW-15
MW-15D
MW-17R
MW-17DR
MW-18
EQUIP.
BLANK
Acetone
µg"
20
5.0
6,000
15.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
8.1 JL
<5.0
<5.0
<5.0
<5.0
<5.0
NS
NS
<5.0
<5.0
<5.0
<5.0
Acrylonitrile
99/1
20
0.80
NE
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
NS
NS
<0.8
<0.8
<0.8
<0.8
Benzene
µg"
1.0
0.40
1.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Bromochlommethane
99/1
1.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Bromodichlommethane
µg/1
1.0
0.40
0.6
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Bromoform
µg/1
1.0
0.40
4.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Carbon Disulfide
µg/1
1.0
0.40
700
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1 <0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
1 <0.4
<0.4
<0.4
Bromomethane (Methylbromide)
99/1
2.0
0.40
10.0 (i)
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Carbon tetrachloride
µg"
1.0
0.40
0.3
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1 <0.4
1 <0.4
<0.4
1 <0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Chlorobenzene (mono)
µg/l
1.0
0.40
50.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1 <0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Chloroethane
99/1
2.0
0.40
3,000
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Chloroform
µg/1
1.0
0.40
70.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Chloromethane (Methylchloride)
µg/1
1.0
0.50
3.0
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
NS
NS
<0.5
<0.5
<0.5
<0.5
Dibromochloromethane
µg/1
1.0
0.40
0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
1,2-Dibromo-3-chloropropane; DBCP
µg/1
1.0
0.40
0.04
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
1,2-Drbromoethane; Ethylene dibromide
µg"
1.0
0.40
0.02
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1 <0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
1 <0.4
<0.4
<0.4
Dibromomethane
µg/1
1.0
0.40
70.0 (i)
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
112-Dichlorobenzene
99/1
1.0
0.40
20.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
1,4-Dichlorobenzene
99/1
1.0
0.40
6.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1 <0.4
1 <0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
trans-1,4-Dichloro-2-butene
99/1
2.0
0.50
NE
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
NS
NS
<0.5
<0.5
<0.5
<0.5
1,1-Dichloroethane
99/1
1.0
0.40
6.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
0.84 J
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
1,2-Dichloroethane
µg/1
1.0
0.40
0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
10.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
1, 1-Dichloroethene (-ethylene)
µg/1
1.0
0.40
350.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
cis-1,2-DicNoroethene (-ethylene)
µg"
1.0
0.40
70.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
0.47 J
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
trans-1,2-Dichloroethene (-ylene)
µg"
1.0
0.40
100
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1 <0.4
<0.4
<0.4
<0.4
1 <0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1 <0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
1 <0.4
<0.4
<0.4
1,2-Dichloropropane
99/1
1.0
0.40
0.6
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1 <0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
cis-1,3-Dichlmopropene (-propylene)
99/1
1.0
0.40
0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
trans-1,3-Dichloropropene (-propylene)
99/1
1.0
0.40
0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Ethylbenzene
µg/1
1.0
0.40
600
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1 <0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
2-Hexanone
99/1
10
2.0
40.0 (1)
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
NS
NS
<2.0
<2.0
<2.0
<2.0
Iodomethane
99/1
5.0
0.40
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Dichloromethane (Methylene chloride)
µg"
1.0
0.40
5.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
2-Butanone (Methyl ethyl ketone)
µg"
10
2.0
4,000
<2.0
2.3 J
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
NS
NS
<2.0
<2.0
<2.0
<2.0
4-Methyl-2-Pentanone
µg/l
10
2.0
NE
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
NS
NS
<2.0
<2.0
<2.0
<2.0
Styrene
99/1
1.0
0.41
70.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
1, 1, 1,2-Tetrachloroethane
99/1
1.0
0.40
1.0(i)
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
1, 1,2,2-Tetrachloroethane
99/1
1.0
0.40
0.2
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Tetrachlomethene (-ethylene)
99/1
1.0
0.40
0.7
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Toluene
µg"
1.0
0.40
600
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1 <0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
1, 1, 1 -Trichloroethane
99/1
1.0
0.40
200
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
1,1,2-Trichloroethane
99/1
1.0
0.40
0.6(i)
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Trichloroethene (-ethylene)
99/1
1.0
0.40
3.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1 <0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Trichlorofluoromethane
µg/l
1.0
0.40
2,000
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
1,2,3-Trichloropropane
µg/1
1.0
0.40
0.005
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Vinyl acetate
99/1
5.0
1.2
88.0 (1)
<1.2
<12
<1.2
<12
<1.2
<1.2
<1.2
<12
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
NS
NS
<1.2
<1.2
<1.2
<1.2
Vinyl chloride
µg/1
1.0
0.40
0.03
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Total Xylenes
99/1
1.0
0.40
500
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
0.51 J
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
NS
NS
<0.4
<0.4
<0.4
<0.4
Tetrahydrofuran
µg/1
5.0
1.0
2,000 (1)
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
3.4 J
<1.0
<1.0
<1.0
<1.0
<1.0
NS
NS
<1.0
<1.0
<1.0
<1.0
1,4-Dioxane
µ 1
3.0
1.0
3.0
NT
NT
NT
NT
NT
<1.0
<1.0
NT
NT
NT
NT
NT
NT
<1.0
<1.0
NT
NT
2.8 J
1.9 J
NT
NT
NT
NT
NS
NS
<1.0
I <1.0
I <1.0
<1.0
Notes:
1. MCL = Maximum Contaminant Level, as established in the NCDENR, Classifications of Water Quality Standards Applicable
to Groundwaters of North Carolina, Section 15A NCAC 21, .0202. Amended Eff. April 1, 2013
2. (i) = Interim Maximum Allowable Concentrations (IMACs). Updated June 30, 2021
3. Shaded cells indicate exceedances of IMACs
4. Shaded cells indicated exceedances of MCLs
5. NE = Not Established; North Carolina has not established a MCL
6. LOQ = Limit of Quantitation
7. DL = method Detection Limit
8. NT = Not Tested
9. NS = Not Sampled
10. "J"-flagged data (i.e., values estimated between the DL and the LOQ) are presented on this spreadsheet.
11. "L" flagged data denote LCS/LCSD failure
9378-26A GW Tables (Completion, water levels, detections) Prepared by: RLB
T4 (10-28-21) VOC Checked by: TAO/ AWA

Table 5
Groundwater Field Parameters, Geochemical Parameters, and Total Metals
Buncombe County Landfill
Alexander, North Carolina
Permit No. 1107-CDLF-1998
Permit No. 1107-MSWLF-1996
BLE Project Number J21-9378-26
Sampled by Pace Analytical Services, LLC. October 26-28, 2021
TEST
UNITS
LOQ
DL
MCL
MW-1
MW-1D
MW-2
MW-2D
MW-3R
MW-4
MW-4D
MW-5
MW-5D
MW-6
MW-7
MW-8
MW-8D
MW-10
MW-10D
MW-11
MW-11D
MW-12
MW-12D
MW-13
MW-13D
MW-14
MW-14D
MW-15
MW-15D
MW-17R
MW-17DR
MW-18
EQUIP.
BLANK
pH
S.U.
<6.5; >8.5
6.4
7.5
6.3
6.6
6.1
6.3
6.7
6.3
6.3
6.1
6.4
6.5
6.3
6.1
6.5
6.6
6.7
6.3
6.8
6.5
6.3
6.2
7.3
NS
NS
6.5
7.2
6.7
NT
Specific Conductance
µmhos/cm
NE
180.1
280.1
449.8
262.1
96.7
237.7
306.9
224.1
216.7
144.5
694.0
388.2
440.7
333.8
361.2
458.4
444.0
965
470.7
469.3
423.7
179.1
332.1
NS
NS
215.9
276.7
214.2
NT
Temperature
°C
NE
12.9
10.5
14.2
13.8
17.3
15.4
14.7
17.9
16.1
13.8
16.2
13.8
14.1
13.2
15.7
13.0
14.8
19.0
17.1
15.8
14.9
14.2
13.5
NS
NS
10.8
10.5
15.7
NT
Turbidity
NTU
NE
9.7
9.8
7.3
3.1
6.9
1.0
1.3
8.3
3.2
3.2
9.0
5.4
2.4
3.7
4.2
8.6
5.4
1.7
3.4
3.2
2.2
8.4
2.4
NS
NS
5.2
0.5
9.2
NT
Alkalinity
mg/i
20
20
NE
59
83
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
240
170
NT
NT
65
140
NS
NS
79
120
79
NT
Total Dissolved Solids (TDS)
mg/l
25
25
500
140
180
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
680
290
NT
NT
140
210
NS
NS
150
190
150
NT
Iron H (Fe 2)
µ
50
13
300
190 B
160 B
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
130 B
290 B
NT
NT
150 B
240 B
NS
NS
290
200
300
NT
Sulfate
mg/l
1.0
0.25
250
20
41
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
290
66
NT
NT
21
31
NS
NS
33
25
30
NT
Chloride
mg/l
1.0
0.25
250
6.2
<0.3
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
38
12
NT
NT
2.5
4.1
NS
NS
3.2
3.9
1.7
NT
Total Antimony (Sb)
µg/I
2.0
0.5
1.0 (i)
<0.5
0.66 J
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
1.6 J
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
NS
NS
<0.5
<0.5
<0.5
<0.5
Total Arsenic (As)
µg/1
2.0
1.3
10.0
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
NS
NS
<1.3
<1.3
<1.3
<1.3
Total Barium (Ba)
µg/I
5.0
1.3
700
140
31
76
48
64
40
110
130
74
50
180
140
170
140
30
64
64
110
63
200
230
50
8.0
NS
NS
64
51
12
<1.3
Total Beryllium (Be)
µg/1
0.4
0.15
4.0 (i)
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
NS
NS
<0.2
<0.2
<0.2
<0.2
Total Cadmium (Cd)
µgfl
0.5
0.13
2.0
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
<0.1
0.40 J
<0.1
<0.1
<0.1
<0.1
<0.1
NS
NS
<0.1
<0.1
<0.1
<0.1
Total Chromium (Cr)
µg/1
5.0
1.3
10.0
2.3 J
<1.3
<1.3
<1.3
3.0 J
9.6
1.4 J
5.7
5.3
<1.3
2.7 J
2.7 J
1.4 J
3.9 J
3.8 J
<1.3
<1.3
1.5 J
<1.3
<1.3
<1.3
<1.3
<1.3
NS
NS
<1.3
<1.3
5.4
<1.3
Total Cobalt (Co)
µg/I
5.0
1.3
1.0 (i)
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
11
<1.3
<1.3
<1.3
1.8 J
<1.3
<1.3
3.3 J
<1.3
<1.3
<1.3
29
2.1 J
26
21
<1.3
<1.3
NS
NS
<1.3
<1.3
<1.3
<1.3
Total Copper (Cu)
µg/1
5.0
1.3
11000
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
3.2 J
<1.3
<1.3
<1.3
<1.3
1.7 J
<1.3
<1.3
<1.3
6.9
<1.3
19
<1.3
<1.3
<1.3
<1.3
<1.3
NS
NS
7.0
<1.3
1.4 J
<1.3
Total Lead (Ph)
µgfl
1.0
0.25
15.0
<0.3
0.37 J
<0.3
<0.3
<0.3
<0.3
0.46 J
0.33 J
<0.3
<0.3
<0.3
0.26 J
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
0.26 J
<0.3
<0.3
0.39 J
NS
NS
<0.3
<0.3
<0.3
<0.3
Total Manganese (Mn)
µg/1
5.0
1.3
50.0
7.5
14
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
2,500
470
NT
NT
4.0 J
31
NS
NS
8.8
24
NT
Total Mercury (Hg)
µg/I
0.20
0.091
1.0
<0.1
<0.1
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
0.23
<0.1
NT
NT
<0.1
<0.1
NS
NS
<0.1
<0.1
<0.1
NT
Total Nickel (Ni)
119/1
5.0
1.3
100
2.7 J
4.5 J
5.7
<1.3
3.1 J
7.8
34
8.7
5.5
<1.3
15
3.1 J
4.3 J
11
12
22
<1.3
34
3.6 J
6.3
9.6
2.8 J
<1.3
NS
NS
22
<1.3
3.7 J
<1.3
Total Selenium (Se)
µg/I
5.0
1.3
20.0
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
<1.3
NS
NS
<1.3
<1.3
<1.3
<1.3
Total Silver (Ag)
µg/1
1.0
0.25
20.0
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
<0.3
NS
NS
<0.3
<0.3
<0.3
<0.3
Total Thallium (TI)
µgfl
0.5
0.15
0.2 (i)
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
NS
NS
<0.2
<0.2
<0.2
<0.2
Total Vanadium (V)
µg/1
5.0
2.5
0.3 (1)
3.7 J
<2.5
2.8 J
3.2 J
4.3 J
<2.5
<2.5
2.8 J
<2.5
<2.5
<2.5
<2.5
<2.5
2.6 J
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
NS
NS
<2.5
<2.5
<2.5
<2.5
Total Zinc (Zn)
ggf,
10
2.5
1,000
7.5J
5.5J
<2.5
<2.5
5.9J
7.7J
14
5.1BJ
2.9J
3.0BJ
3.7J
16
4.7J
4.6J
<2.5
8.7J
<2.5
6.4J
<2.5
9.8J
<2.5
<2.5
8.8J
NS
NS
9.0J
<2.5
3.6J
<2.5
Notes:
1. MCL = Maximum Contaminant Level, as established in the NCDENR, Classifications of Water Quality Standards Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L .0202. Amended Eff. April 1, 2013
2. (i) = Interim Maximum Allowable Concentrations (IMACs). Updated July 30, 2021
3. Shaded cells indicate exceedances of IMACs
4. Shaded cells indicated exceedances of MCLs
5. NE = Not Established; North Carolina has not established a MCL
6. LOQ = Limit of Quanfitation
7. DL = method Detection Limit
8. NT = Not Tested
9. NS = Not Sampled
10. "J"-flagged data (i.e., values estimated between the DL and the LOQ) are presented on this spreadsheet.
11. 'B"-flagged data (i.e., constituents detected in the method blank) are presented on this spreadsheet.
9378-26A GW Tables (Completion, water levels, detections) Prepared by: RLB
T5 (10-28-21) Metals Checked by: TAO/ AWA

Table 6
Surface Water VOCs
Buncombe County Landfill
Alexander, North Carolina
Permit No. 1107-CDLF-1998
Permit No. 1107-MSWLF-1996
BLE Project Number J21-9378-26
Sampled by Pace Analytical Services, LLC. October 26-28, 2021
TEST
UNITS
LOQ
DL
NC2B
SW-1
SW-2
SW-3
SW4
SW-5
SW-6
SW-7
SW-8
Acetone
µg/l
20
5.0
2,000
<5.0
<5.0
9.7 JL
<5.0
<5.0
<5.0
Dry
<5.0
Acrylonitrile
AgIl
20
0.8
420
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
Dry
<0.8
Benzene
µg/l
1.0
0.4
51
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
Bromochloromethane
AgIl
1.0
0.4
NE
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
Bromodichloromethane
99/1
1.0
0.4
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
Bromoform
AgIl
1.0
0.4
120
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
Carbon Disulfide
µg/l
1.0
0.4
100
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
Bromomethane (Methylbromide)
µg/l
2.0
0.4
0.04
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
Carbontetrachlon
µg/l
1.0
0.4
1.6
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
Chlorobenzene (mono)
AgIl
1.0
0.4
800
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
Chloroethane
µg/l
2.0
0.4
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
Chloroform
µg/l
1.0
0.4
2,000
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
Chloromethane (Methylchloride)
µg/l
1.0
0.5
96
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
Dry
<0.5
Dibromochloromethane
AgIl
1.0
0.4
21
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
1,2-Dibromo-3-chloropropane; DBCP
µg/l
1.0
0.4
0.13
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
1,2-Dibromoethane; Ethylene dibromide
AgIl
1.0
0.4
0.1
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
Dibromomethane
µg/l
1.0
0.4
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
1,2-Dichlorobenzene
AgIl
1.0
0.4
3,000
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
1,4-Dichlorobenzene
µg/l
1.0
0.4
900
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
trans-1,4-Dichloro-2butene
µ
2.0
0.5
NE
<0,5
<0.5
<0,5
<0.5
<0.5
<0.5
Dry
<0.5
l,l-Dichloroethane
µg/l
1.0
0.4
100
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
1,2-Dichloroethane
AgIl
1.0
0.4
650
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
l,l-Dichloroethene(-ethylene)
99/1
1.0
0.4
20,000
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
cis-1,2-Dichloroethene (-ethylene)
AgIl
1.0
0.4
720
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
trans-1,2-Dichloroethene (-ylene)
µg/l
1.0
0.4
4,000
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
1,2-Dichloro ro ane
AgIl
1.0
0.4
31
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
cis-1,3-Dichloropropene (-propylene)
µg/l
1.0
0.4
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
trans-1,3-Dichloro roene (-propylene)
As/,
1.0
0.4
NE
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
Ethylbenzene
µg/l
1.0
0.4
97
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
2-Hexanone
AgIl
10
2.0
NE
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
Dry
<2.0
lodomethane
µg/l
5.0
0.4
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
Dichloromethane (Methylene chloride)
As/,
1.0
0.4
11000
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
2-Butanone (Methyl ethyl ketone)
µg/l
10
2.0
26,000
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
Dry
<2.0
4-Meth-2-Pentanone
AgIl
10
2.0
26000
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
Dry
<2.0
Styrene
µg/l
1.0
0.41
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
1, 1, 1,2-Tetrachloroedme
AgIl
1.0
0.4
NE
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
1, 1,2,2-Tetrachloroethane
µg/l
1.0
0.4
4.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
Tetrachloroethene (-ethylene)
µgFl
1.0
0.4
3.3
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
Toluene
µg/l
1.0
0.4
11
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
1,1,1-Trichloroethane
AgIl
1.0
0.4
200,000
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
1,1,2-Trichloroethane
µg/l
1.0
0.4
8.9
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
Trichlomethene (-ethylene)
AgIl
1.0
0.4
30
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
Trichlorofluoromethane
µg/l
1.0
0.4
67,000
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
1,2,3-Trichloro ro ane
AgIl
1.0
0.4
0.001
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
Vinyl acetate
µg/l
5.0
1.2
NE
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
Dry
<1.2
Vinyl chloride
µ911
1.0
0.4
2.4
<0,4
<0.4
<0,4
<0.4
<0.4
<0.4
Dry
<0.4
Total Xylenes
µg/l
1.0
0.4
670
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dry
<0.4
Tetrahydrofuran
AgIl
5.0
1.0
110,000
NT
NT
NT
NT
1.5 J
<1.0
NT
<1.0
1,4-Dioxane
AgIl
3.0
1.0
80
<1.0
<1.0
15
<1.0
8.0
<1.0
Dry
<1.0
Noter•
1. NC2B = North Carolina Surface Water Standards for Class C freshwater under Title 15A Subchapter 2B.
per NC DWR Surface Water Quality Standards, Criteria, & In -Stream Target Values (Workbook Dated 6-10-2019)
2. NE = Not Established; North Carolina has not established a MCL
3. "J"-flagged data (i.e., values estimated between the DL and the LOQ) are presented on this spreadsheet.
4. Shaded cells indicated exceedances ofMCLs
5. LOQ = Limit of Quantitation
6. DL = method Detection Limit
7. NT = Not Tested
8. DNA = Data Not Available
9. "L" flagged data denote LCS/LCSD failure
9378-26A SW Tables Prepared by: RLB
T6 SW VOC (10-28-21) Checked by: TAO/ AWA

Table 7
Surface Water Field Parameters and Total Metals
Buncombe County Landfill
Alexander, North Carolina
Permit No. 1107-CDLF-1998
Permit No. 1107-MSWLF-1996
BLE Project Number J21-9378-26
Sampled by Pace Analytical Services, LLC. October 26-28, 2021
TEST
UNITS
LOQ
DL
NC2B
SW-1
NC2B
SW-2
NC2B
SW-3
NC2B
SW-4
NC2B
SW-5
NCHI
SW-6
NC2B
SW-7
NC2B
SW-8
PH
.u. (ao-site)
-
.
<6.0;>9.0
7
<6.0;>9.0
7.9
<6.0;>9.0
7.9
<6.0;>9.0
7.5
<6.0;>9.0
8.2
<6.0;>9.0
7.60
<6.0;>9.0
Dry
<6.0;>9.0
7.9
Specific Conductance
µ.hos/-(on-srte)
-
-
NE
136.7
NE
167.2
NE
1,220
NE
305.6
NE
1,449
NE
184.3
NE
Dry
NE
181.7
Temperature
-C (on-srte)
-
-
29.0
12.2
29.0
10A
29.0
14.8
29.0
10
29.0
10.8
29.0
14A
29.0
Dry
29.0
11.1
Turbidity
NTU (on-srte)
-
-
50.0
65.9
50.0
3.9
50.0
673
50.0
112.4
50.0
2.3
50.0
2.4
50.0
Dry
50.0
2.0
Hardness
-Ad
10
2.0
NE
NT
NE
NT
NE
NT
NE
NT
NE
NT
NE
NT
NE
Dry
NE
NT
Total Antimany(Sb)
Awl
2.0
0.5
5,300
<0.5
5,300
<0.5
5,300
<0.5
5,300
1.7J
5,300
<0.5
5,300
<0.5
5,300
Dry
5,300
<0.5
T-1 Arsenic (As)
Awl
2.0
L3
10
<1.3
10
<1.3
10
<1.3
10
<1.3
10
<1.3
10
<1.3
10
Dry
10
<1.3
Total Barium (Ba)
Awl
5.0
L3
21,000
130
21,000
53
21,000
190
21,000
130
21,000
190
21,000
100
21,000
Dry
21,000
52
T-1 Beryllium (Be)
Awl
0.4
0.15
65
<0.2
65
<0.2
65
<0.2
65
<0.2
65
<0.2
65
<0.2
65
Dry
65
<0.2
Total Cadmium (Cd)
Awl
0.5
0.13
0.79
<0.1
1.6
<0.1
3.67
<0.1
3.9
<0.1
16.86
<0.1
5.01
<0.1
52.31
Dry
4.57
<0.1
Total Chromtum(Cr)
Awl
5.0
L3
177
1.4J
343.97
<1.3
750.54
2.3J
794.17
7.0
3,160.41
<1.3
1,005.17
<1.3
9,235.43
Dry
922.07
<1.3
Total Cobalt(Cal
Awl
5.0
1.3
16
5.9
16
<1.3
16
7.7
16
5.4
16
12
16
<1.3
16
Dry
16
<1.3
Total Copper (Cu)
Awl
5.0
1.3
3.5
64
7.52
<1.3
18.45
4.1 J
19.69
5.8
96.46
<1.3
25.82
<1.3
331.22
Dry
23.38
<1.3
Total Lead (Pb)
µg/I
1.0
Q25
13.26
3.3
32.82
<0.3
92.97
0.90J
100.13
1.3
569A7
<0.3
136.14
<0.3
1,831.15
Dry
121.7
<0.3
Total alkkel(Ni)
Awl
5.0
L3
140
<1.3
27&02
<1.3
622.43
19
659.84
8.0
2,748.17
24
941.66
<1.3
8,319.73
Dry
769.88
<1.3
TAW Selenium (Se)
Awl
5.0
L3
5.0
<1.3
5.0
<1.3
5.0
<1.3
5.0
<1.3
5.0
<1.3
5.0
<1.3
5.0
Dry
5.0
<1.3
Total Sit-(Ag)
Awl
1.0
0.25
0.28
<0.3
1.11
<0.3
5.74
<0.3
6.46
<0.3
11T49
<0.3
10.6
<0.3
1,117.04
Dry
8.84
<0.3
Total Thallium (TI)
Awl
0.5
0.15
NE
<0.2
NE
<0.2
NE
<0.2
NE
<0.2
NE
<0.2
NE
<0.2
NE
Dry
NE
<0.2
Total Vanadium(M
Awl
5.0
2.5
NE
3.1J
NE
<2.5
NE
Q.5
NE
11
NE
Q.5
NE
<2.5
NE
Dry
NE
<2.5
Total Zinc (7.)
I
10
2.5
34.97
44
69.52
Q.5
155.84
13 B
165.22
19
689.63
8.6 J
210.82
Q.5
2,091.32
Dty
192.82
Q.5
Notes:
1. NC213 = NAdb Carolina Surface Water Standards for Class C t-h-ler under Title 15A Subchapter 2B.
per NC DWR Surface Water Quahty Standards, Criteria, & hr-Stream Target Values (Workbook Dated 6.10-2019)
Measured values of hardness were utilized to calculate an scnte standard a each surface water Imam for metals highlighted in green.
Hardness values were reposed in Report of Water Quality Sampfiug and Analysis Ist Semi-Aauual Evaa12020
Buncombe County Landf11 Alexander, North C-1- prepared by BLE, dated 7uly 13, 2020.
2. NE = N. Established; North Carolina has not established a standard
3. "1"-flagged data (Le., values estimated b-en the DL and the LOQ) are presented on this spreadsheet.
4. Shaded ceUs indicated exceedances ofMCLa
S. LOQ = Limit of Q-titalion
6. DL= method Detection L®it
7. NT =Nat Tested
8. DNA =Data Not Available
9. V' Bagged data denote LCS/LCSD failure
10. "B"-Bagged data (ie., constituents detected in the method blank) are presented en this spreadsheet.
9378-26A SW Tables Prepared by: RLB
T6 SW Metals (10-28-21) Checked by: TAO/ AWA

Table 8
Leak Detector and Leachate VOCs
Buncombe County Landfill
Alexander, North Carolina
Permit No. 1107-CDLF-1998
Permit No. 1107-MSWLF-1996
BLE Project Number J21-9378-26
Sampled by Pace Analytical Services, LLC. October 28, 2021
TEST
UNITS
LOQ
DL
MCL
LD-1
LD-2
LD-3
LD4
LD-5
LD-6
Leachate
LD
Leachate
Pond
Acetone
µg/l
20
5.0
6,000
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
80 JL
Acrylonitrile
µg/I
20
0.8
NE
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
<0.8
Benzene
µg/l
1.0
0.4
1.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Bromochlororrt
µg/I
1.0
0.4
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Bromodichloromethane
µg/l
1.0
0.4
0.6
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Bromoform
µg/I
1.0
0.4
4.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Carbon Disulfide
µg/l
1.0
0.4
700
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Bromomethane (Methylbromide)
µg/I
2.0
0.4
10.0 0)
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Carbon tetrachloride
µg/l
1.0
0.4
0.3
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Chlorobenzene (mono)
µg/I
1.0
0.4
50
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Chloroethane
µg/l
2.0
0.4
3,000
0.91 J
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Chloroform
µg/I
1.0
0.4
70.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Chloromethane (Methylchloride)
µg/l
1.0
0.5
3.0
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
Dibromochloromethane
µg/I
1.0
0.4
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dibromo-3-chlompropane; DBCP
µg/l
1.0
0.4
0.04
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dibromoethane; Ethylene dibromide
µg/I
1.0
0.4
0.02
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dibromomethame
µg/l
1.0
0.4
70.0 (i)
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dichlorobenzene
µg/I
1.0
0.4
20
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,4-Dichlorobenzene
µg/l
1.0
0.4
6.0
0.46 J
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
trans-1,4-Dichloro-2butene
µg/I
2.0
0.5
NE
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
1,1-Dichloroethane
µg/l
1.0
0.4
6.0
0.59 J
1.2
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dichloroethane
µg/I
1.0
0.4
0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,1-Dichloroetheme (-ethylene)
µg/l
1.0
0.4
7.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
cis-1,2-Dichloroethene (-ethylene)
µg/I
1.0
0.4
70
<0.4
0.45 J
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
trans-1,2-Dichloroetheme (-ylene)
µg/l
1.0
0.4
100
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,2-Dichloropropane
µg/I
1.0
0.4
0.6
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
cis-1,3-Dichloropropene (-propylene)
µg/l
1.0
0.4
0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
trans-1,3-Dichloropropene (-propylene)
µg/I
1.0
0.4
0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Ethylbenzene
µg/l
1.0
0.4
600
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
2-Hexanone
µg/I
10
2.0
40.0 (i) 1
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
Iodomethane
µg/l
5.0
0.4
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Dichloromethane (Methylene chloride)
µg/I
1.0
0.4
5.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
2-Butanone (Methyl ethyl ketone)
µg/l
10
2.0
4,000
28 H
<2.0
<2.0
<2.0
4.0 J
<2.0
<2.0
25 J
4-Methyl-2-Pentanone
µg/I
10
2.0
NE
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
Styrene
µg/l
1.0
0.41
70
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
<0.41
1,1,1,2-Tetrachloroethane
µg/I
1.0
0.4
1.0 (i)
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,1,2,2-Tetrachloroethane
µg/l
1.0
0.4
NE
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Tetrachloroethene (-ethylene)
µg/I
1.0
0.4
0.7
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Toluene
µg/l
1.0
0.4
600
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,1,1-Trichloroethane
µg/I
1.0
0.4
200
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,1,2-Trichloroethane
µg/l
1.0
0.4
0.6 (i) 1
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Trichloroethene (-ethylene)
µg/I
1.0
0.4
3.0
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Trichlorofluoromethane
µg/l
1.0
0.4
2,000
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,2,3-Trichloropropane
µg/I
1.0
0.4
0.005
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
Vinyl acetate
µg/l
5.0
1.2
88.0 (i)
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
<1.2
Vinyl chloride
µg/I
1.0
0.4
0.03
<0.4
<0.4
0.82 J
<0.4
<0.4
<0.4
<0.4
<0.4
Total Xylenes
µg/l
1.0
0.4
500
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
<0.4
1,4-Dioxane
I
3.0
1.0
3.0
NT
NT
NT
NT
1.6 J
NT
NT
NT
Notes;
1. MCL = Maximum Contaminant Level, as established in the NCDENR, Classifications of Water Quality Standards Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L .0202. Amended Eff. April 1, 2013
2. (i)=Interim Maximum Allowable Concentrations (IMACs). Updated June 30, 2021
3. Shaded cells indicate exceedances of IMACs
4. Shaded cells indicated exceedances of MCLs
5. NE = Not Established; North Carolina has not established a MCL
6. LOQ = Limit of Quantitation
7. DL = method Detection Limit
8. NT -Not Tested
9. "J"-flagged data (i.e., values estimated between the
DL and the LOQ) are presented on this spreadsheet.
10. "L" flagged data denote LCS/LCSD failure
11. "H" flagged data denote sample out of holding time
9378-26A Leachate Tables Prepared by: RLB
T8 LD VOC (10-28-21)Checked by TAO/ AWA

Table 9
Leak Detector and Leachate Field Parameters and Total Metals
Buncombe County Landfill
Alexander, North Carolina
Permit No. 1107-CDLF-1998
Permit No. 1107-MSWLF-1996
BLE Project Number J21-9378-26
Sampled by Pace Analytical Services, LLC. October 28, 2021
TEST
UNITS
LOQ
DL
MCL
LD-1
LD-2
LD-3
LD-4
LD-5
LD-6
Leachate
LD
Leachate
Pond
pH
s.u. units (on -site)
<6.5; >8.5
6.7
6.1
6.6
6.8
6.5
6.6
4.9
8.1
Specific Conductance
µmhos/cm (on -site)
NE
3,613
426.1
658
3,516
762
624
435.1
740.2
Temperature
°C (on -site)
NE
13.7
16.7
15.2
16.0
17.8
16.8
15.8
15.0
Turbidity
NTU (on -site)
NE
44.2
53.8
40.9
4.2
10.0
9.0
2.4
40
Biologic Oxygen Demand (BOD)
mg/1
2.0
-
NE
NT
NT
NT
NT
NT
NT
NT
49
Chemical Oxygen Demand (COD)
mg/1
80
80
NE
NT
NT
NT
NT
NT
NT
NT
1,100
Nitrates
mg/1
0.5
0.13
10
NT
NT
NT
NT
NT
NT
NT
<0.13
Sulfates
mg/1
10
2.5
250
NT
NT
NT
NT
NT
NT
NT
17
Phosphates
mg/1
0.05
0.02
NE
NT
NT
NT
NT
NT
NT
NT
2.9
Total Antimony (Sb)
µg/1
2.0
0.5
1.0 (i)
<0.5
<0.5
<0.5
0.96 J
<0.5
<0.5
<0.5
12
Total Arsenic (As)
µg/1
2.0
1.3
10
<1.3
<1.3
<1.3
4.1
<1.3
<1.3
<1.3
39
Total Barium (Ba)
µg/1
5.0
1.3
700
1,300
110
220
490
170
460
24
450
Total Beryllium (Be)
µg/1
0.4
0.15
4.0 (i)
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
0.15 J
<0.15
Total Cadmium (Cd)
µg/1
0.5
0.13
2.0
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
<0.13
Total Chromium (Cr)
µg/1
5.0
1.3
10
1.6 J
3.2 J
<1.3
290
<1.3
<1.3
<1.3
94
Total Cobalt (Co)
µg/1
5.0
1.3
1.0 (i)
270
23
5.2
11
78
98
24
22
Total Copper (Cu)
µg/1
5.0
1.3
1,000
<1.3
4.1 J
<1.3
12
<1.3
<1.3
7.9
1.8 J
Total Lead (Pb)
µg/1
1.0
0.25
15.0
<0.25
0.98 J
<0.25
<0.25
<0.25
<0.25
<0.25
0.54 J
Total Mercury (Hg)
µg/1
NT
NT
1.0
NT
NT
NT
NT
NT
NT
NT
NT
Total Nickel (Ni)
µg/1
5.0
1.3
100
60
25
2.4 J
89
21
4.4 J
210
89
Total Selenium (Se)
µg/1
5.0
1.3
20
1.8 J
<1.3
<1.3
1.6 J
<1.3
<1.3
1.4 J
1.8 J
Total Silver (Ag)
µg/1
1.0
0.25
20
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
Total Thallium (Tl)
µg/1
0.5
0.15
0.2 (i)
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
<0.15
Total Vanadium (V)
µg/1
5.0
2.5
0.3 (i)
<2.5
4.8 J
<2.5
17
<2.5
<2.5
<2.5
41
Total Zinc (Zn)
µ /1
10
2.5
1,000
5.5 BJ
18 B
<2.5
13 B
2.9 BJ
4.8 BJ
100 B
19 B
Notes:
1. MCL = Maximum Contaminant Level, as established in the NCDENR, Classifications of Water Quality Standards Applicable
to Groundwaters of North Carolina, Section 15A NCAC 2L .0202. Amended Eff. April 1, 2013
2. (i) = Interim Maximum Allowable Concentrations (IMACs). Updated June 30, 2021
3. Shaded cells indicate exceedances of IMACs
4. Shaded cells indicated exceedances of MCLs
5. NE = Not Established; North Carolina has not established a MCL
9378-26A Leachate Tables
T9 LD Metals (10-28-21)
6. LOQ = Limit of Quantitation
7. DL = method Detection Limit
8. NT = Not Tested
9. "J" -flagged data (i.e., values estimated between the
DL and the LOQ) are presented on this spreadsheet.
10. "B" -flagged data (constituent detected in the method blank)
are presented on this spreadsheet.
Prepared by: RLB
Checked by: TAO/AWA

FIGURES

J
o
M
�
\
1751
a
1745
�1
D
R1PRW0DD
�
\l l w; I,
$
N F
ti
,s�J
�1,
-
RTi
Af
�D
2\ 1
Alexander
2000 1000 0 2000 4000
APPROXIMATE SCALE IN FEET
DRAWN: KLW DATE: 1-6-22
' IM I BUNNELL
� LAMMONS
CHECKED: RLB CAD: BCLF26A-SLM ENGINEERING
6004 Ponders Court, Greenville, SC 29615
APPROVED: AWA JOB NO: J21-9378-26 Phone: [phone] Fax: (864] 288-4430
REFERENCE:
USGS TOPOGRAPHIC MAP, 7.5 MINUTE SERIES,
LEICESTER AND WEAVERVILLE, N.C. QUADRANGLES,
PHOTOREMSED 2017 AND PHOTOREMSED 2017.
SITE LOCATION MAP I
BUNCOMBE COUNTY LANDFILL
ALEXANDER, NORTH CAROLINA
FIGURE

N N � CONVE IE CE
CENTER
LANDFILL OFFICE �93
QP��0�� �� BUILDING
� F
OO
'007
it _.L �Sw 2 ,""_ WELL
` ` /
j � � � M_� 1912,34
HOUSE — Mw-2
SW-6,- �/ Qe SCALE HOUSE
MW-2D
Q1 18 24 1911,78
PANTHER BRANCH *111t\ _� -
( -FLOW) 0 1 , ,� 1942.10 MW-10D
MW-10
� /- LD 3 LU-4 1941,53
� MW-4 I
-- -- -- ----t
` � .ice/ Q`— — — — — /� T
�SW-8♦ MW-18 MW-4D21 /' V 1 i I
1895,92---1930,37 1 1941,06_
MW-SDI,.
1951.96
�MW-15 \SW_3 MW-5 1943.16 \ INACTIVE � = 1 INACTIVE _k"
CELL 3
MW-15D '���_- \ - s 11 CELL 4 '` I
19 5 2, 4 3 I ..INACTIVE ---------------
CELL 1
SW-5
� MW- 14
c o0
�� I I
IIj
cIII
MW-17R
a)1875,79T �
MW-17DR1,
1877.49 I MW-CD 17D
I04 MW-17 ® (AB)
(AB)
V
'1922,92-MW-14DIK
`®1923.48�
/ M
� 1 �
II �� M\
I � 19
1 �
PERMITTEDPHAE
�
C&DSAREA �
000,
L
SW_7
MW-13 MW-13D)K
1949.25 1946,46
D 6
— 7-7 7,f
I
/
/
oe
loe
loe
INACTIVE I
CELL 2 INACTIVE
CELL 5
�2•-r
E _
�ACHATE �
D
�MW-8
_1932,95
�D MW-11 ��193]
mw-
MW-8D)K 1933.76
1934.61
EMPLOYEE E
.EACHATE TRAILER E
'OND -� o
1000, 1 �,
1000,
SW -4
/ v
1
1 M-9
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Tom♦ � F'
FRENCH BROAD RIVER ♦n
V
MW-16MW-16D
NOT NOT PRESENT
PRESENT
-------��----------------------�`
� 1
PERMITTED
FUTURE
CELL 7
i
ACTIVE
CELL 6
/ 04/
N CAR,oy
NSF'�ti9
1 5
=> �;
w A�i,P,.
M-8
1956.52 1960
MW-1 S
MW-1D)K
1955,36
1950
REFERENCES:
1) SHEET NO. 1 GROUNDWATER AND METHANE MONITORING WELL
LOCATIONS, CDM SMITH, PROJECT NO. 6447-105257. FILE: SITEMAP
2014.DWG.
2) SURFACE WATER LOCATIONS FROM SHEET NO. 1 GROUNDWATER
AND METHANE MONITORING WELL LOCATION MAP, CDM SMITH,
NOVEMBER 2012 PROJECT NO. 6447-93318. FILE: SITEMAP. DWG.
3) PHASE 6 C&D BOUNDARY PROVIDED BY MCGILL.
4) SHEET NO. OP-1 EXISTING CONDITIONS, CDM SMITH, PROJECT NO.
6447-97693. FILE: OP-1.DWG.
5) FIGURE NO. 3-1 WATER QUALITY MONITORING PLAN CELL 6 AREA,
CDM, PROJECT NO. 6447, DATED NOVEMBER 2004.
6) SURVEY DATA FOR MW-17R, MW-17DR AND M-12R IN SCS
REPORT DATED OCTOBER 13, 2020
7) SURVEYING FOR MW-18 PERFORMED
BY ED HOLMES AND ASSOCIATES DATED
SEPTEMBER 24, 2021
,16111*�
LOCATION ACCURACY
OF THE FEATURES
SHOWN IS LIMITED BY
THE REFERENCES
THEMSELVES.
I0
i
1
go
I�
01
�M tD �
i
j
m
m
LEGEND
—1980 TOPOGRAPHIC CONTOUR
- - - - - WASTE UNIT BOUNDARY
FACILITY BOUNDARY
MW-10 EXISTING GROUNDWATER
MONITORING WELL
MW-16 PERMITTED FUTURE GROUNDWATER
MONITORING WELL
EXISTING SURFACE WATER
SW-2 MONITORING LOCATION
* LD-1 LEAK DETECTOR
* LD-7 PERMITTED FUTURE LEAK DETECTOR
0 M-3 EXISTING LANDFILL GAS MONITORING WELL
+M-5 PERMITTED FUTURE LANDFILL GAS MONITORING WE
m
EXISTING STRUCTURE MONITORED FOR
LANDFILL GAS
1950 POTENTIOMETRIC ELEVATION CONTOUR (FEET
MSL) CONTOUR INTERVAL = 10 FEET
GROUNDWATER FLOW DIRECTION
* DEEP WELL NOT USED FOR CONTOURING
PURPOSES
(AB) ABANDONED
STREAM
200 100 0 200 400
APPROXIMATE SCALE IN FEET
REVISIONS
No. DESCRIPTION BY
DRAWN: RLB
CHECKED: TAO
APPROVED: AWA
DATE: 1-28-22
CAD FILE:
BCLF 9378-26AWMT102621
JOB N0: J21-9378-26
IM BUNNELL
� LAMMONS
ENGINEERING
6004 Ponders Court, Greenville, SC 29615
Phone; [phone] Fax; [phone]
GROUNDWATER ELEVATION CONTOUR MAP-OCTOBER 25-26, 2021
BUNCOMBE COUNTY LANDFILL
ALEXANDER, NORTH CAROLINA
FIGURE NO.
2

APPENDIX A
FIELD SAMPLING LOGS
PACE ANALYTICAL SERVICES, LLC.

Dacun,nt Name: Field data Sheet
D7 ument Number. F-CAR_F1.D_00,_,,,.03
Lk
Name and Affiliation (Sampier(s): {� c, c e
Name and Affiliation (Inspector): a
Well Information
WeII ID: VA W - I
Well Diameter:
Total Well Depth: U 3 ft
Static Water Level•_ 7 U ft
Height of Water Column; (q3 3 ft
Well Locked:
Project #' Bwh
Id Data Sheet Review:
Date: Iofletf?'l
to ft o I, 1
construction: 40 /Steel/Stainless Steel)
Multi Factor*:0' It �31'(Radius/12)2x3,14x7,481
Casing Volume: a �? gallons
Cal. 3 Volumes;Z gallons
By: `a
view LF- Oct .Z(
Pump inhke:______ 6,_________-ft
Purge Information
Date Purged: 10 / Z (o / 2 l start: 0 9 SO
Plnish< 5 S Purge Rate: / 01
Purging
/ t
Method: Y`ti 5 v�5o sti\ (7 $0
Total Volume Purged: 0 (g�lons ny (L)
SamnlingInformation
Date Collected; I o jZb/ 2-(
Time Collected; // d ..r,�7/Pm)
Sampling Equipment Used: �'x%'"LSo ry___
x C�"-��'
Instrument ID: 3 TIOU 14. ,p 35S
Bottle Type _
las
I 25V K� OAS
3- Nu n,L via
Field Measurements/Observatieus
reservation
U n or�,s
1'�CL
y�Ana�lysis Required
S
vDC
Sample Temp (°C):
Diss Oxy
Time., // 7
me; __Turbitiity(ntu):
S 7
Time: U U
(mg/4%
----------.____
, p
Time; jj Do
Fe 2+ mg/ L:
D 0
Specific Cond. (uS):
1 5'0 )
.Time:. /% 1) D
--------------__
Res. Cl(mg/L)/(ltg/L):
T me: ___
"—'Inner
sample pH (s.u.): _
�. y
— _... _..._...
Time: / ° O
Odor: YW v�
________.__,
ReDox (mv):
t{�. U
_
Tune: ly U
--- �,
Appearagce; eqr
Time:
--
ReDox (EH value):YSi ProPlus +200mV y�) d
-----Time:�_
Other:
//OC
Genera 1/Weather Observations_
Time:
k,.uiy/t ouny •ain.) Temp.. SD (°F) Wind &
Sampler Signature;_ (mph)
Date:. / O Z (, - ? i
Time
Temp,
Diss Oxy.
Spec•
o ume
Purged
(aC)
(rngj1)
Cond.
pI-I(s.u.)
ReDox
Turbidity
remove,
Water
(u5)
(mV)
(ntu)
(gallons/ 1
level (ft) Other
0955
I I y
7. 2
I Q6,5,
(o, ro
o21, o
1,
k6
It Lf
. Z
/8L,8
(�. 6
z i. o
/, I
0
6t%95
i 1000
0.3'
1It.3
7.o
18Y.5
6.5
a.
/0.0
Gy9
6 y 96
I bl o
, _W
�,3
/frz.b
G.5
�z.6
6, e

Document Name: Document Issued: March g, 2019
any/ /a Field Data Sheet Pagel -of 1-
��' `l'a Document Number: Issueing Authority:
F-CAR-FLD-001.rev.03 Pace Hunte�aville Quality Office
I- E
nf� I tI
Location:.liS V'6�f A)
Project: N£w Lr-Or'f
Well ID: M W — (
Reviewed Date and By:_Is) ia.9 Iv (3n
Stabffization Test 16 f1f(fU GTq
dtrell.£?iaxss=ter
hYwltapliaal3axFact�zs
I 2:a�s
0-D'40B
2
tN.10
t1 �67'D
4
D ti530
1 <458D
2:�'i4iD
Time
Purged
TemZI
uCond.
(
Spec.
(u5)
pH(s.u. )(j
ReDox mV Turbidity
(ntu)
Volume Removed
(gallons/�ni /L)
circle one
Water level
Other
(ft)
(oZo
(uZ5
103D
1035•
t oLED
(01(5
1050
b
(o55
0.2
l�,o
Q,1
tz.0
!,Z-0
1z.z.
12—
/2.Z
1Z.6
G,`f
G.5
To
7.1
?,l
7.0
7.,
7.1
7,o
lgr.�
tftl.G
/Srl.z
179,G
r79,7
IW,t
[yo.z
17.7
179.7
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DOCument Name: BiLhl data Sheet.
Dmument Number: F-CA1?-Fl..l)-00r-re¢o3
Nance and Affiliation (Sarnpler(s): C C6- --P4 c z
Name and Affiliation (Inspector): Lk. 1
Well Information
Well ID: M W — I Well Locked:
Well Diameter: 1
'--------------_.. CollStruCEiOn?
Total Well Depth: �' s S ft
Static Water Level; �' G 2 1 {t
Height of Water Column: I •3Ift
Mc
U Data Sheet Review
Date:
10114 I t l
NO / Flushmmint l
/ Steel)
Multi Factor*: b - 16 3 1*(Radi1s/12)2.x 3:14 x Z481
Casing Volume; 5. 1 1 gallons
Cal.3 Volumes; / s• �3 .gallons
Pump Intake: i 5 . o
Co. IJcw Lr- Oct zl
—Iti
By;
c-xl3
Purge Information It
Date Purged w/ 1(0 / 2 1 Start; (2q 0O q /
Finish: � 1)-o PwrgeBate:
Purging Method: YVL 'vx:5 0 f
Total Volume Purged: Xy D (gaAons,�O/L)
Sampling Information Q Date Collected; I u / X6/ zl Time Collected: -
� / �5
(a/Pm)
Sampling Equipment Used: $out Instrument1D; 5'G'it 0"3 (PcJ 03SS
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Preservation Analysis Required
X50
4—AIL
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Sample Temp (°C): ) D , S Ttme; qq
Turbidity (ntu): (i 00 Time:
Diss Oxy (mg/L): % , z- Time: 0 `/ ZS
Fe 2+ mg/L; /� J Time:
Specific Cond. uS : a S D. 7 G 9L ( ) Time: Res. Cl (mglL)/(µg/L): '---Tune; ^
Sample pH(a,u): 7•-5 Time: Odor:
__ -_____Time: 9z 5
ReDox (in ---
( ) — 3---- 5'_ Time: � �1 ZS Appearance: �.(�e ReDox (EH value):YSI ProPlus +20o,11V �Z 3 S.
Other: Time: _
General/Weather Observations:
O — Z6- z/
Time
Pur urge,
g
Temp,
°
(C)
Diss Oxp.
(mg/I)
Spec
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Document Name: Field data Sheet gate
i Dmument Number: F-CAR-Fl..D_001-rev.03 Issuuig Autho:
Client;z�
Field Data Sheet
Location: L l
/� Project
Name and Affiliation (Sampler(s): ,,' _1(1e
' Field Data Sheet Review;
Name and Affiliation (Inspector):,//�j9 1 - z2. 2 i
Well Information !�/z le! Date: / J/� �U
4Ve11 ID: /Yf l l/ Zy( Well Locked: ( S NO n n,, i
Well Diameter: Z
Total Well Depth: 2g3a Z 6 It
Static Water Level• l� 15 S ft
Height of Water Column: t y- 6 L ft
Construction: Steel/Stainless steel)
Multi Factor*: Q= /a NRadius/ia)z x 3.14 x 7.481
Casing Volume: 2` 39 gallons
�I
Cal. 3 Volumes; / gallons
&L (L
By` Ohd-
Purge Information Pump Intake: 2�_ -- -ft
DatePurged:10 _/ 3- / Z( Start: % Z30 Finish: )30
I urge Rate: Z�10��/
Purging Method:_Total Volume Purged:-. � Z
-� �1 _ (gallons/[,)
Sampling Information
Date Collected: 11 t3 / 2a/ - I 'rime Collected; ).3 0 S
Sampling Equipment Used: Li r lilt Instrument ID a%S//,�`I� /L/ Td v .....
Bottle Type
Field Measurementalobservations
Preservation Analysis Required
Sample Temp (°C): ' I{ - l Time: 3 O S
_.-_....---Turbidity (ntu): �, 3 Time:
Diss Oxy (mg/L):_ 6,2 Time;
Fe 2+ mg/ L:_ I r S Time:
Specific Cond. (us): Time; Res. CI m L
( g/ )/(uB/L) Time:
Sample pE[ (s u,): _ 6 3__. -Time: _ - on e -. _Time:.--.
ReDox (mV): LiG 1 � Time: - —
Appearance: deg.- Time:
ReDox (EH value):YSI ProPlus +200mV i�_ timer: Ali/
General/Weather observations: Time
u /cloudy/rainy) Tem/pJ._(dF) Wind 0`S (mph)Sampler Signature: Date: lO���/ �f-
Stabilization Test
Time Temp. Diss Ox . Spec. Vo ume
Pur ed
0 1 y Cond. pH {s.u.) Ret?ox Turbidity removed Water
g ( C) (11g/[,) (us) (mV) (ntu) (gallons/ems leveI(ft)FOthei
za 71

Document Name: Fiehf data Shcet Date Issued: March 8; 2019
„r CCMkTIytiCaf Page:. 1 of
Document Number: F-CAR-FLD-001-rev.03 Issuing Authority: Pace Huatersville Qual [y
Office
Name and Affiliation (Sampler(s) 'I y�qq� /L T: I / Field Data Sheet Review:
Name and Affiliation (Inspector): Jf"1f m. (D Da . Z 2 _21 By: G L C
Well Information 1p / 2 t ( y �z r
Well ED: ! t / " o Well Lockett: ES5/ NO / Flushmaunt )
Well Diameter:_ Construction: (PVC Steel/Stainless Steel)
Total Well Depth: 3 �f ft Multi Factor*: ' ( ( (Radius/12)2 x 3.14 x 7.481
Static Water level: J fkFi �� Casing Volume: J gallons
Height of Water Column: g t"r�• �ft Cal.3 Volumes: _gallons
Pump Intake, S G+ . ft
Purge Information
It -
Date
Purged:/�/ II(I Start : Finish; Purge Rater i
Purging Method:_ �(� ri !< 7G( �J<, `C Total Volume Purged: t try/ o (gallons rails l,)
Sampling Information
Date Collected:f1l) /Z1/ r It Time Collected: �s (am
p q
Sampling Equipment Used! �Caf �>� C InstrumentID- 1,/S-� �� �%CyUrtp�
Bottle Type
Field Measurements/Obseryations
Sample Temp (°C): a 3 Time:.
Diss Oxy (mg/L): n Time:
a,
1
Preservation
Analysis Required
_Lk 47/Se S
��
Turbidity (ntu): _ 3• i Time:
Fe 2+ mg/L:%��i Time:
Specific Cond. (uS): ,r Time: Res. Cl (rng/L)/(pg/L): 'Time:
Sample pFl(s,u,): v . .... _ - .Time: Odor:_._ //t� ----------Ttme:._-i' SC!
/
ReDox (mV): S Time: :a Appearance Fpq( 'Trine:
ReDox (EH value):YSE ProPlus +200mV '7 Sr� Other: ,PVA Time:
General/Weather Observations:
(sou/cloudy/rainy) Temp. S `i (aF) Wind_(mph)
Sampler Signature
Stabilization Test
7
7PTimedTemp.
(°C)
Diss Oxy.
(mg/L)1t
Spec.
ond.
PH (s.u.)
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Document Name: Field data Sheet
Date
//' ,�,�aceAnntyiicat
r
DMURIent Number: F-CAR-FLD-001-rev.03
Name and Affiliation (Samolerfsi: `P / G.
3aare.,,b�, ev. Ncw c.F- Uei al -
Id Data. Sheet Review:
Name and Affiliation (Inspector): 1'vov
2 j0iz(f2i C rx3
Well Information
Date: By.
i�ylt9lxl BnY
WeII ID:
Well Locked; YE / NO J Flushmount)
Well Diameter: oZ y
Construction:.- Q!2�YSfeet/Stainless Steel)
Total Well Depth: $ � JQ� ft
Multi Factor*: 0 " 1 3 r(LRadius/ lz)2 x 3.14 x 7.a81
Static Water Level 53• !a ft
Casing Volume: 4 ' g 7 gallons
Height of Water Column: S ' 1 ft
Cal. 3 Volumes; °1' S Z gallons
Pump Intake: 57' D ft
Puree Information
Date Purged: ( , / 5 J Zi Start: �'-oS Finish: Z 5 Purge Rate: co tl`
Purging Method: Total Volume Purged: 3 0 0 D (gallons 16,
1 /L)
Sampling information
Date Collected: 1 D /A/ 7-( Time Collected;
Sampling Equipment Used: l t cr0r . InstrumentID:YST 'f Ow3 'I—PW F(D,sS
Bottle Type —
3 - 4 ttn,c.
Field Measurenxents/Observations
Preservation
_ JCL
Analysis Required
Vo C-
Sample Temp Cc):
3
Time:!
..
Turbidity (ntu): (o' 1 Time:
(Z'E O
Diss Oxy (mg/L),
�?` 0
Time:
12k�
Fe 2+ mg/L: ---Time:
/ 1Y
Specific Cond. (uS):
4 7
Time:
t Ltr O
Res. Cl (mg/L)/(µg/L): ` Time:
Sample pH (s.u.): _,
Ce' (_.-_-__....
Time:
- t Z� 0
Odor: Time:
z 4 U
ReDox (mV):
'3
Time;
f 2K D
— —
Appearance: CD'ea r r',im,
12k u
ReDox (EH value):YSI ProPlus +2OOmV 7H1 `+r • 3 Other:
General/Weather
Stabilization Test
Time: �
rainy) Temp. 7 -S (°'F)
(u-zg— zI
Time
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Document Name: Document issued: Much 8,2019
Field Data Sheet Pagel -of 7-
issueing Authority;
Document Number:
F-CAR-FLD-001.rev.03 Pace Huntersville Quality Office
AJ Location: (Z
Project: 15
Well ID:
Reviewed Date and BY: % '01 jIN pwo,
Stabilization Test 1()f?q(7J Cm
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1.625
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Ucxument Name: Field data Sheet
Date Issued: March 8, 2t119
deefbkllytiCal
Page: IOt
[7c�cument Numliee F CAR-F[.I3-00brev.0.3
IssuingAuthority: Pace Huutersville Quality
.._7
l
Office
Name and Affiliation (Sampler(s): C*'(-C' ` ha w
Name and Affiliation (Inspector):tiR,
Well Inforiation
Weil ID: h"`^)
Well Diameter: 2
Total Well Depth: a 5 • S'O ft
Static Water Level: 13 • ( 0
Height of Water Column:! Z- 2- ft
^)C Project#:$k"�f Co. JU-7LF- 0'1 2.t-
Sevv<,�
Field Data Sheet Review:
lw?z (211 CXi3
Date: By:
)oJa9lzi 13rws
Well Locked: 4IE3 / NO
Construction://Sheet/Stainless Steel)
Multi Factor*: 5 • (,63 ('(Radius/12)20.14 x.7,481
Casing Volume: . 9 9 gallons
CaL 3 Volumes: 5 • 94 gallons
Pump Intake: 23' C) ft
Purse Information
Date Purged: i 0 Start, (l y D Finish: � ( 5 5 Purge Rate: ) 6 D kvxL(t, _
Purging Method: S L 5'1 r. 1 [ r Total Volume Purged: 2-70 D (gallons/ ii /L)
Sampling Information
Date Collected: 1 0 / 7-1/ 'x I I I Time Collected; (tea o
Sampling Equipment Used: s Tc L� c instrument ID: Y 52-# 0 Z-0-S -rPw A o355
Bottle Type Preservation
0CI-
7j - 1-to n..L
Field Measurements/Observations
Analysis Required
- - - 5 ----- ---.............
Voc
Sample Temp (°C): 5 y Time: �_ ° Turbidity (ntu): / . 0 Time: J '2_0 0
Diss Oxy (mg/L): 1, D Time:
/ 2-Pa
Fe 2+ mg/ L: /J
Time: / ao 0
Specific Cond.(uS): a-3�•7 Time:
/2o0
Res. Cl(tiig/L)/(ltg/L):
� Time:
Sample pH (s.u.): . 3 .__._.__Time:
/ 2P a
Odor:_--. !A�.-._._-.._._
ReDox (mV): 3Y` (o Time:
/ z GD
-f
Appearance: t ter
Time: /Zo
ReDox (EH value):YSI ProPlus +20omV
Other: —
Time:
General/Weather Observations:
Sampler Signature
Stabilization Test
/rainy) Temp. S6 (°F)
l v- L7-
Spec.
o unle
Time
Temp.
Diss Oxy.
Cond.
pH (s.u.)
ReDox
Turbidity
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Water
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Document Name., Field data Sheet.
Date Issued: March 8, 2019
Page:.Iof-1
i
l�cicument Number: E-CAR-F[.D-007-rev.03
lssahig Authority: Pace Hunterwille Quality
Office
Name and Affiliation (Sampler(s): �'{ G " �q c e ,
Name and Affiliation (Inspector): L4ei
Well Information
Well ID: M -U- N
Well Diameter:
a tt
Total Well Depth: 5,7• 9 Z
Static Water Level: ) Li- 3 5 ft
Height of Water Column:�f 3• 57ft
Proje€t#:I�Iahconb� �.A)"i LF- 01'k 2J
- sutif
1d Data Sheet Review:
Date: 10 / 7,.^112a cz
10)79)21 By BNS
Well Locked: (C( S� NO / Flushmount ).
Construction: Q /,Steel/Stainless Steel)
Multi Factor;0,/L3 madius/12)20.14xa.I81
Casing Volume: _�• 1y gallons
CaL 3 Volumes: oZ I. 3 c' gallons
Pump Intake: 55. 0 it
PurgeInformation
Date Pur Purged: 10 �i Zt Start: 1110 Finish: Purge Rate:
g //L
Purging Method: Total Volume Purged: / i b (gallonsQ/L)
Sampling Information
Date Collected: n / ollf ZI f/ )) Time Collected: / 3 (0/pm)
Sampling Equipment Used:_fL41,sTc �T • C Instrument ]D: t 5`ZA,2 2.0 3 7 Pw #a3 sS
Bottle Type -
)
3- Yo &�L
Field Measurements/Observations
Preservation
ur_o,;
H cC
Analysis Required
i7'lY �4!'S
Vac
Sample Temp CC):
Time:
-'__Turbidity
(ntu): 3 Tillie:
1131,
Diss Oxy (mg/L):
O • 3
Time:
/) 3 0
Fe 2+ mg/ L: /)'b
Time:
// 3 0
Specific Cond. (uS):
30(` g
Time:
/) 30
Res.CI(mg/L)/(gg/L),
Time:
Sample pH. (s.u.):
to. -------
Time:
/) 3 o
Odor:_,_-. A
ReDox (mV);
3 5. 5
Time:
)/ 30
Appearance: /e5r
Iime:
1l36
ReDox (EH value):YSI ProPlus +200mV
= 3 5. 5
Other: -
Time:
—
General/Weather
Sampler Signature
Stabilization Test
Temp. 93 .("F)
0,7-7•z1
Time
Temp.
DissOxy'
Spec.
Coed.
pH(s.u.)
ReDox
Turbidity
o ume
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Document Name: Field data Sheet
Date Issued: March 8, 2019:
aEeNratyliCalx
Page: I of 1
Document Number F-CAR-FLD-001-rcv.03
IssuAuthority: Pace Htmtersvilte Quality
h,g y
Offi€e
Naive and Affiliation (Sam pler(s): /A -/A
Name and Affiliation (Inspector): 'zm
Well Information
Well ID: /Ij✓- 5
Well Diameter:
Total Well Depth: S ft
a
Static Water level: } ?l o "} ft
Height of Water Column: 1'.- _ft
Well Locked:
Construction:
C
ild Data Sheet Review:
Date:
Steel)
Multi Factor*: ["(Radius/12)2 x ,14 x 7.48]
Casing Volume: 3 7 gallons
Cal-3 Volumes; gallons
Pumphitake: 'r50, S 'f ft
Purge Information
Date Purged: L6 (� f�Start: i�« Finish: 3J Purge Rate:i�
Purging Method: A26 3ii l Total Volume Purged: 0 (gallons '/L,)
Sampling Information
Date Collected:— Time Collected:_. 5 !m
Sampling Equipment Used: Instrument ID:
Bottle Type
Field Measurements/Observations
Sample Temp (aC): _-1_7__q_Time:(
Diss Oxy (mg/L): 0 Time:
Specific Cond. (uS): 2 CI, Time:
Sample pH. (s.u.): _ -- Time:
ReDox (mV): L Tune:
ReDox (EH value);YSI ProPlus +200mV_
Generalf Weather Observations: &�
Sampler Signature
Stabilization Test
Preservation
Analysis 1Required
Turbidity (ntu): 9, 3 Tillie: ! D `�
Fe 2+ mg/L: &Z10 Time: i)
Res. Cl (mg/L)/(itg/L): — Time: �Y
Odor:__.. 0 Time: _, ` 5
Appearance i5k�qf Y Time:
Other: LA Timer
rainy)
Wind l'i-3� (mph)
Spec.
Volume
Time
Temp,
Diss Oxy.
Cond.
pH (s.u.)
ReDox
Turbidity
removed
Water
Other
Purged
(C)
(mg/L)
(US)
(mV)
(ntu)
(gallons/�lls
L
level (ft)
Jz
i
0,

.. c7G@MkT(yfiCa7 •
l
DocumentDate
Name: Field data Sheet
Issued: March 8, 2al
Page: 1 of
Document Number. fiCAR-FLI)-0Ol-rev.03
lssuuig Authority: Pace HimtersvilleQuality
Office
Name and Affiliation (Sampler(s): L' Wi e° c/(
Name and Affiliation (Inspector): '4(A
Well Information
Well ID: AV-fi 0
Well Diameter:
Total Well Depth: G� ft
Static Water Level: ft
Height of Water Column: et>. ,5 aft
Well Locked:
Construction:
Ad Data. Sheet Review:
Date:
NO / Flushmount )
eel/Stainless Steel)
l /{.
Multi Factor`: 5, la('(fRadius/12)2 x 3.14 x 7,481
Casing Volume: 7 s �l gallons
Cal.3 Volumes: gallons
Pump Intake: % 7,> D ft
BY:GcG-
Purge Information I
Date Purged:/ ( o= Start : I� Finish Y 5 1) Purge Rate: /,ice a fvf )
Purging Method:_ k� `i17o ra Total Volume Purged: l S o d (gallons/m--�f 1,)
Sampling Information -7
Date Collected:/ / — Time Collected; ' 0 ._ (am/ )
Sampling Equipment Used: mjmsa"' Instrument ID:
Bottle Type
Field Measurements/Observations
Sample Temp ('C): C& r t Time:.
Diss Oxy (mg/L): iJ > Time:
Specific Cond. (uS): ?—Time:
Sample pH (s.u): _y am..... ... ... . Time:
ReDox (mV): Time:
Preservation
Analysis Required
..�..-if<i
ej Turbidity (ntu): c d Time: G0
Fe 2+ mg/L: IVIa)Time:
Res. Cl (iitg/L)/(leg/L): —Time:
Odor._--4// /?- ._ Time: _.. 0
Appearance (7!e(.'. t_ rime:
ReDox (EH value):YSL I'roPlus+200iriV 'Z3 Z-/ Other: ✓V/ A Time.
GeneraVWeather Observations:
Temp. ( _(CF) Wind_I_5_(mph)
Sampler Signature
Stabilization Test
Spec.kV)(n
Volume
Time
Temp,
Diss Oxy.
pH (s.u.)(gallons
removed
Water
Purged
CC)
(mg/L)
(US)
(uS)�`I�>>
mis�Level
(ft)Other
i0Qv
1, C 0
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. ,. 8F2l171rTlyilCRl
Document Name: Field data Sheet
Date Issued: March 8, 2P19.
Page: lot
[Jucument Number F-CAR-Fl..p-001-rev.0.1
Issuial; Authority: Pace Huntersville Qua
Quality
Y
Office
/,i- ad ,_-G"2.i
Name and Affiliation (SampIer(s):...V44z664U,
Name and Affiliation (Inspector):
Well Information
Well ID: /� 6-V -6 ' Well Locked:
Well Diameter: �2 ,)'I Construction:
Total Well Depth: 5C 'a It
Static Water Level: �-5 r q £t
Height of Water Column: al,% ft
1d Data Sheet Review:
%o-Z2_zl
Date6/x�/ By%3.0 s
NO / Flushmount )
ael/Stainless Steel)
Multi Factor*; O�// 3 r(R'a,dlus/i2)2x3,I4x7.881
Casing Volume: v� L gallons
1(
Cal.3 Volumes: / .1 ( gallons
Pump lnfake: r/ ', s ft
Purge Information
Date Purged J Z / �/ Staft:.:1500 Finish: Purge Rate:
Purging Method;_ ���I I �j (� `` Total Volume Purged: " d (gallons] nlsIL)
SamolinElnformation
Date Collected: ) ti / 2tf 1-4 Time Colleeted:J 0- _ (am/ pi )
,
Sampling Equipment Used: �Q/5' .,/f,o Instrument:1 Yam# 151/7r1 Xk 6ylxly.ter-L)p,fl /1
Bottle Type N�C/4) Preservation Analysts Required
Field Measurements/Observations
Sample Temp CC): 0 i Time:_
Diss Oxy (mg/L): r4. a Time: _
��{ 5
Specific Cond. (uS): � Time: _
Sample pH (sm,);
ReDox (mV): l Time: _
ReDox (EH value):YST ProPlus +200mV 2
nramuzarion iesr
Turbidity (ntu): t, 1 Time:
Fe 2+ mg/L:/.,mod Time:
Res. CI (mg/L)/(µg/L): Tune:
Odor. _Time:._. I'
Appearance C •ea/ Time:
Other: ,41zli Time
Spec.
Vo ume
Time
Teemp,
Diss Ox
Cond.
pH (s.u.)6ReDoxTurbidity
removed
Water
r
Purged
(C)
(mg/I.)
(uS)
(ntu)
(gallons/m(s/LlJi
iip,
71
3
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Document Name: Field data Sheet
Date Issued: March 8, 2014:
Page:. I of 1
Document Number F-CAR-FI..I}-001-rev.03
Issuing Authority Pace Huntersville Quality
Office
Le
Name and Affiliation (Sampler(s): GLfr-�e
Name and Affiliation (Inspector):
Well Information
Well ID: rA\-J - 7
Well Diameter: 2_
Total Well Depth: 5 s' L 2_ It
Static Water Level: t( 31 A ft
Height of Water Column: (�• 0- ft
Sr Project#:&hc 'e Co. >JeW LF- bef,Z!-
Field Data Sheet Review:
Date: 1o12iru By: -
hI1s11.1 RhS
Well Locked: (YD/ NO / Flushmount )
Construction: &/Steel/Stainless Steel)
Multi Factor*: 0 " 3 ("(Radiu9/12)2 x 314 x 7.48j
Casing Volume: 5 5 gallons
Cal.3 Volumes: 1, � 5 gallons
Pump Intake. 66. s) ft
Purge Information /
Date Purged: 10 / Z r/ 2-1 Start; / 3 ZS Firtish: / 3115 Purge Rate: l o h/ �_
Purging Method: 1ti.8-h,So n y\ Total Volume Purged: °� ° , (gallons/ /71 /L)
Sampling information
Date Collected: 1 :7 / 2 k/ zl Time Collected: 3 S (am/j0m
SamplingEquipment Use& M,tShSv0r InstrumentlD:5 '4G263 TPW io�sS
Bottle Type
J z50 ryt_ \0(ap
3-Ku wL
Field Measurements/Observations
Preservation
WAfd3 -
k(c c.
Analysis Required
--------------
Sample Temp (eC):
�• Z-
Time
�3 5 D
Turbidity (nhr) :
ty
[ • 0
Time:
/ 3
Digs Oxy (mg/L):
00'
Time:
/ 3 5 U
Fe 2+ mg/L:
50
Time.
Specific Cond. (uS):
'5/
L F /
Time:
/ 3 5y
Res. Cl (mg/L)/(ltg/L): —
Time:
Sample pH. (s.u.):
._._.._-Time:
3 SO
Odor:—....
ReDox (mV):
a�' `i
Thne:
1 3 Se)
Appearance:
cl-e-tr
Time:
ReDox (EH value):YS1. ProPlus+2OOmV
)­Z7• `f
Other:
_
Time:
General/Weather
Sampler Signature
Stabilization Test
10-z?-Z1
Spec
volume
Time
Purged
Teemp,
(C)
Digs Oxy.
(mg/L)
Cond.
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
removed
(gallonso/
Water
level (ft)
Other
(US)
L
133
15•9
L93
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7
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t34,�
JT;�.5
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30, o
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Document Name: Field data Sheet
Date Issued: March 8, 2019
-
262A7k9/ytiCaf
Page:. t oft
Document Number. F-CAR-FL.17-001-rev.0:i
Issuing Authority: Pace HtuuersvilleQuality
'
t
Office
Name and Affiliation (Sampler(s) '-LQ -
Name and Affiliation (Inspector):
Well Inforinald
Well ID: iP1 Ll $ Well Locked:
Well Diameter: ,11 Construction:
Project #: LZ/ Zv2l
1d Data Sheet Review:
10-Zi.ZI Date: By:
By.�_
Steel)
Total Well Depth: o� r ft Muhl PacYor* Ur [*(Radius/I2)2 x 3:14 x 7.g81
Static Water Level: d (t J ft ( Casnig Volume: gallons
Height of Water Column: ��y.3 ft Cal, 3 volumes: gallons
Pump Intake: zj - 4`-- ft
Purge Inforniation
Date Purged:—[/ .2 /_ Start s.�-b Finish: ( Purge Rate: �dn
Purging Method:_ f %/ `l Total Volume Purged: 0 (gallonsJ nls 1.,)
Samplin¢Ltformation
Date Collected:-4C1_J�zJ-69�— - y_ Time Collected:_. 5 i y _ (amJ )y
Sampling Equipment Used: I C t �( �J fQ l'7�(��!E�Y(�I., '1�i
Instrument IA3
Bottle Type
Field Measurements/Observations
Preservation
Analysis Required
Sample Temp CC): _ � ^ 0 Time:-16_'!_'3 _Turbidity (ntu): s. ci Time: C_
Diss Oxy (mg/L): o Time: Fe 2+ mg/L: line:
Specific Cond. (uS): Time: Res. Ct (mg/L)/(Itg/L):'Time: {
Sant le H s.n. : c. 6 CI
P p ( ) �.� -..._._....._Time: Odor:—,_��if%._..........._— Time: _. --..._
ReDox (m.V): '71, 9- Tune: l/ Appearance:. Time:
ReDox (EH value):YSI ProPlus +200mV---a- , Other: s— Time:
General/Weather Observations:
Sampler Signature
Stabilization Test
Spec.
Volume
Time
Temp.
u
Diss Oxy.
Cond.
pH (s.u.)
ReDox
Turbidity
removed
Water
Other
Purged
(C)
(mg/
uS)
(mv)
(ntu)
(gallons mis
level (ft)
IMA
ro/2
L
y4
l
q
(o�1
330th
p�
31
00
oo
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Document Name: Field data Sheet
Date Issued: March 8, 2D19
Page: I of
nmument Number: F-CAR-FI S}-001-rev.03
Issuing Authority: Pace Huntersville Quality
Office
f/_„d'8C2Fh7f7/y(1CR(
r
Name and Affiliation (Sampler(s): lS/hj;ef7 —h
Name and Affiliation (Inspector): Z �
Well Information
WeII ID: Any — 'e/J
Well Diameter: Z�
Total Well Depth: 97.q it
Static Water Level; 2?. `3 ft
Height of Water Column: 69- SO ft
Well Locked:
_Project#46 c e �c Ac e Gh Uef,ze)z/
%r AMh4
Id Data Sheet Review;
Date: (Q-a'1-z1 By:
Construction: (steel/Stainless Steel)
Multi Factor: 0'163 [*(Radius/12)2 x 3.14 x 7.48]
Casing Volume: f /. 33 gallons
Cal. 3 Volumes: 33. 9 9 gallons
Pump Intake: %s ft
Pur a Information
DatePurged:/O—/ 26 /Z/ Start:/6 � Finish: 6SS Purge Rate:47a-,,4,
Purging Method/f Al G Total Volume Purged: � � O Z) (gallons/t�?L)
Samvline Information
Date Collected: /V _/ ZC/ el // / Time Colleetectj��t.__ (ant/ r�
Sampling Equipment Used: i7e// �C Instrument
Bottle Type Preservation nn pAnalysis Required
....\mt:.__..
4R
Field Measurements/Observatious
Sample Temp (aC): I H' I Time: __110n _Turbidity (ntu): Time: 11cjv
Diss Oxy (mg/L); ® , 5 Time: Fe 2+ mg/L; /Ue iJ , Time:
Specific Cond. (uS): `ff)")% Time: Res.0 (mg/L)/(gg/L): Thrtei
Sample pH(s.u,):_CJb__---- -Tine:_ Odor:_0one._.___„___�Tirne:._
ReDox(mV): 5"(J1 1 Tune: Appearance: Time:
ReDox(EHvalue):YSIProP1us+200mV 2S�' + Other: 1/�/� Time:
Generalf Weather
Wind D_S (mph)
Sampler Signature
Stabilization Test
Spec.ReDox
Volume
Time
Temp.
a
Diss Oxy.
Cond.
pH (s.u.)
Turbidity
removed
Water
Other
Purged
(C)
(mg/I,)
(US)
(mv)
(ntu)
(gallons/mQs/
level (ft)
-7-64o
L
10, 1
4u
6.3
5-o 3
Z_19
S
�It .6
63
66;1
4,
lcaqS
I4.
0.-+S
C,3
WI
1H
0
ZT
65o
i�
ftA3
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Sl,'3.Q
51J)tT
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S
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Document Name Field data Sheet
D,Xument Number: F-CAR-F1.D-001-Wv.03
rtela tiara
Client: o, E Locaticm:��
Name and Affiliation (Sampler(s):�r
Name and Affiliation (Inspector):
Well Information
Well ID: M W — i 0
Well Diameter: _
Total Well Depth: 6, L l ft
Static Water Level:__G_,£t
Height of Water Column. —I —.Aft
ft
Well Locked:
Construction:
!Id Data Sheet Review:
) o
Date: f,0 _ 2Q _ �I
vs+ l sw/ Nushmount)
(heel/Stainless Steel)
Multi Factor*: �6•� l*(Radius/ 12)2x 3: 14 x Z481
Casing Volume: t Z 7Z gallons
Cal.3 Volumes; / gallons
QVb
By: C,(. C.
Pump Intake:�_ft
Purge Information
Date Purged' /0 / 2$ Z /
/ Start:Finish:.l00s ' Purge
PurgungMeEhod:�?PrFy2DaJoo Total Volume Purged:_I660 allons L
Sampling Information
Date Collected:/ Z /
/ Time Collected:— 10 l .___ ant ptn)
Sampling Equipment Used: o va
InsrrumentID: f/q 7y��S
Bottle Type
Field Measurement;/Observations
Preservation /n1 PP-1
Required
._ APP-1 me -Jr i 110C__...__....._
Sample Temp (nC): 13.2 Time: 1010 _..__ Turbidi ntu : 3.
�' ( ) Time: I 0 l O
Diss Oxy (mg/L): 0 ,7 Time: Fe 2+ mg/L: So 5
Specific Cond. (uS): 333. d Time: Res.CI(pig/L)/(Rg/L): Time:
Time:
Sample pH {s.u.}: _ Fi• I ..____... Time:
Odor:�lc,� Tune:
--------_______ Tune: Appearance: clear Ti
mme:
ReDox (EH value):YSI ProPlus +200V 7-16.3 Other: yy
General/WeatherOhservar; ,.�. Time
Sampler
Time
Temp.
Diss Oxy.
Spec.
Purged
(uC)
(mg/L)
Cond.
pH ('s.u.)
(US)
O So
13,4
i i
3531 I
��
�-
}3,2
LQ4�
3,2
a,q
33�,3
6,
I
oos
_I�.2.
o.°l
2zz Cl
1
ri fey/iamy) lemp.'Z_.(ar) Wind tj- e�(mph)
ate:
Vo uume
ReDox
Turbidity
removed
Water
(mv)
(iitu)
(gaIlon ml
Level (ft) Other
}.6
s,L
L
s.g
3.6
60o
GR,}S

B/afh9/}/i!C'il Document Name: Field data Sheet
J/
Document Number: F-CAR-171.D-001-rev.03
/YC
Name and Affiliation
J9/
ield Data Sheet Review:
Name and Affiliation (Inspector)-
Well Information Date:
Welt ID: ZI ✓-100 s, i
Well Lockett: NO / Ftushmount)
Well Diameter: )�_ Construction: teel/Stainless Steel)
Total Well Depth: J �j ft Multi Factor*; /
^, !' - G'�1J 1 f*(Radius/ 12)2x 3,1E x 7.481
Static Water LeveC C' I'' d
_.____ft Casing Volume: '—fEr 2_ gallons
Height of Water Column: S' 1a U 5 ft
Cal. 3 Vglumes; / /to ' gallons
Pure Information
Pump Intake: ii fr3 r=_ft
March
ma's-
G�C, o,
By:
Date Purged: c 1`
Start V� l ?Finistr Purge urge Rate: f0U rr, 11
Purging Method:_ i'rp6o Total Volume Purged: r) r; O (1
(gallons. uil LJ
SamD111, I Information
Date Collected:_//
Time Catlecteti:� r�tf an pin)
Sampling Equipment Used: AN5�4
Instrument ID
Battle Type Preservation
Analysis Required
Field Measurements/Observations
Sample Temp (°C); !'
Time::(%1:5.-__Turbidit nhz : e
Y ( gI ) I _ y ( ) Tinxe: t l Diss Ox m L : i1. Time:
Fe 2+ mg/L: () Time:
Specific Cond. (uSJ: � lv f . Tizrre: �-'`-----
y Res. Cl. (lrig/L)/(gg/L); 'Inner -
Sample pH (s.u.);
._-...Tine: Odor:_ _
ReDax (mV); _ / 12 Time
------ ,.� _Time: Appearance:
ReDox (EH value);YSI ProPlus +2p(rt7V I tme.,
Genera Other: /I✓ j Titne: t/4Veather Observatinns•
tsunny45toudy rainy) Temp. f (°P) Wind f
Sampler Signature: t�7.Gi./rG-' (mph)
_Date: ( f/���/ate`
Stabilz_______ anoTest n -
Time Temp. Diss Oxy. Spec. Vo wine
Purged (°C) (t11g/L) Cond. pH (s.u.) ReDox Turbidity removed Water
(US) (mV) ("to) (gallons _' Other
X nt) 6 �. h ��/ level (ft)

Document Name: Docanient Issued: Mardi s, 2015
Field Data Sheet Page --�tif t.
Document Number: Issuem Authority:
F-CAR-Ff.D-001.rev.03 Pace Huntemville Quality Office
/((�
Client: �J�L
(bell Diameter Multiplication Facto
—
1
0.Ws
�"
Location:Zilejl;lfy AlL
1.2
0.0418
((
ProjecY.1crvG1c1�ti�1P
if/
/',_ ���5,�
_
C,!-��i�� `�/„2/�.�,..(
1.625
0.1030
'
2
0.1630
WellID: AJI 1-4.)Q
_ 3
0.3670
Reviewed Date and By: %fin%%f
4
--
0.6530
Stabilization Test
!° 2Q.2j
CLCA
6
1.4680
3
2.6100
Time Temp,
u
Purged (C)
piss Oxy. Spec.
Cond.
(mg/L)
PH (s.u.)
ReDox (mV)
Turbidity
Volume Removed
(gallon
Water level
(u5)
(ntu)
ml /L)
Other
(ft)
circle. ne
3 /5,s
fW2
0, t • .,
0 11, �
C� s f Iva '
�' �
" � (� 3 s

_-. aCeArkttylical
r
i
Dmument Nnme: Field data Sheet
Dmument Number: F-CAR-Ft.p-0ol-rev.03
Name and Affiliation (Sampler(s)
Name and Affiliation (Inspector):.�i/ e
Well Information
atlon
Well ID:
Well Diameter:
Total Weil Depth:
Static Water Level: 3119 it
Height of Water Column:
ft
Well Locked:
ald Data Sheet Review:
to -yti-1t
Date:Io- zq_Zt
Construction: Steel/StaiialessSteel)
MultiFactor`:2� r(iiadius/12)2x3,14x7A8]
Casing Volume: 3— _ G(, —_ gallons
Cal, S Volumes
: Y gallons
By: G�
Pump Intake: sO -It Purge Information
Date Purged: a 0 / Z Z1 Start: I OY} 0
Finish: l 0 L] 0 PurgeRate:. Z©p , t„q„
Purging Method:_61 c r n n r,.,
Total Volume Purged: Ra oo (gallons.. xll /L)
Sampling information
Date Collected:to /�I/ Z
Time Collected;_ 0 pm)
Sampling Equipment Used:�ot nnn
Bottle Type Preservation
Analysis Required:
Field Measurements/Observations
Sample Temp (°C): 1 3, 0
__Time: l o l.s-_--_ Turbidity (ntu): _ ,',
Diss Oxy (m/L): O, N--� Time: t o
g y s
------ Time: Fe 2+ mg/L:
tj
Specific Cond. (uS): is �,cl Time: e: OdorRes.:
—Time:
P 1' (
Sam le H s•Lu): 6.6 Tim.' (ulg/L)/Time:
ReDox (mV); 36 b one une: _._-,-----.-___._--Time:...-
---- — __ T_..
RciDox (EH value):YSI ProPlus +20pmV Z36,o Appearance; cl e_ pime:
General/WeatherOoservations: Other: AzI4 Time: V
i
oudy/rainy Temp.
h5 (°P) Wnd— Q- ph)
StabiliSample.ati r, na. -c ���n �� Z /
Time
Purged
Temp.
{°C)
Diss Oxy,
(177g/t,)
Spec
Cond.
pH (s.u.)
ReDOX
Vo time
Turbidity removed Water
(US)
(mV)
(ntu) (gaBotas nl / level (it) Other
o00S
13.Q
©,'-
3<
�r
69.
L
UP
13,
4GZJ
6.E
c
lQv© 33,9V
ails
12,5
O,S
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r r_
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451S
1040 13.E N �VS9,Z 6.6 38,Z v, 1 0 0 0 3H,(; '6 o00

/...��'xCeftil.Tlytical
f
i
Document Name: Field data Sheet
Dmument Number: F-CAR-Ft.D-o01-rev.0.3
Name and Affiliation (Sampler(s):
Name and Affiliation (Inspector):
Well Information
Well ID: ill✓-d/ 1)
Well Diameter: 9 1) ,
Total Well Depth: % % , 0 ft
Static Water [.evel: 'q (3 ft
Height of Water Column:.; ,g !ft
Well Locked:
Construction:
1d Data Sheet Review:
Date:1 o z9 z,
to/-tVo
NO / Flushmount i
Steel)
Multi Factor*: ( iL (+{Radius/IF}2x3!Y4x7.A81
Casing Volume: G ,0.7 gallons
Cal, 3 Volumes:
gallons
Pump Intake: j 5 'V
March
By:
G'.Cc_
�M F
Puree Information = ft
Date Purged: f G ?
—/_ Start:100 S
Punish; I i, Purge Rake: f ��
Purging Method:_..1'1100S00 1
- Total Volume Purged: (gallons
Sampling infornlation
Date Collected: (G / ¢
/� Time Collected;
Sampling Equipment Used: Zo)9 S6'0o _14Z�L_ Op/pm)
Instrument fD: 1%
Bottle Type
Preservation Analysis Required
Field Measurement 'Observations
Sample Temp, CC): _ /I Tirne:iLY- 5
Diss Ox m L : ^
y ( g/) a•
_Turbidity (niu): v
— Time: i r
_ Time:
Specific Cond. (uS): clFi �� �1
Fe 2+ mg/L. ' 0
� --Time:
u
_ Time:
Sample pH (s tt ): �� r
Res. Cl (mg/L)/(Itg/L): '—
�Cuue:
_.__.-.. Time: _
ReDox (mV). 1J / \O
Time:
--;ySI
Odor:-✓�f� —
5 cir
„--.:'
ProPlus__.
ReDox (EH value):YS[ ProPlus +2p()mv �,y;
Appearance: ('%i<' ,
Time'.
Genera —Other:
1/Weather Observations:
( 6/
Time:
Sampler
Time Temp.
Purged (nC)
cloudy/rainy)
Wind I (lnph)
Diss Oxy. Spec o ume
m I Cond. pH (s.u.) ReDox Turbidity removed Water
( g/) (u5) (uiv) (ntu) (gallons/bra/ level (ft) Other
S
u

. 7cceAnalytical
f
Document Name:
Field Data Sheet
Dncutnen Issued: March 8, 2019
Page2of 2
Document Number:
F-CAR-FLD-001.rev.03
fssueing Authority:
Pace Huntersville Quality Office
Client: lt)L
Location: py; I f '�i I✓`✓
Project: bblA 61floe 1"'D• Afb4k. /_F od, 9,021
Well ID: /q\,/-1' 1
� o • 2sl -Zl 646-
Reviewed Date and By: Cale}ILI l��r
Stabilization Test
Well Diameter
Multiplication Factor*
1
0.0408
1.2
0.0918
1.623
0,1O30
2
0,1630
3
0.3670
4
0.6530
6
1.4680
S
2.6100
Time
Pur g
Purged
Temp,
u
(C)
DissOxy.
(mg/L)
Spec.
Cond.
(u5)
pH (s.u.)
ReDox (mV)
Turbidity
(ntu)
Volume Re ved
(gallons ml L)
circle one
Water level
(ft)
Other
w Ala
7
,2
2"1

Date Issued: Mareh 8, 2019
Document Name: Field data Sheet
Page: l of
eArW441Cal
19Subtg Authority: face tluntersville Quality
I
Document Number: F-CAR-FL.17-001-rev.03
-
Office
t
LG
Name and Affiliation (Sampler(s): L� - pac'_
Name and Affiliation (Inspector):. h-V-y�
Well Information
Well ID: V\k LV - 1 2—
Weil Diameter:
2"
Total Well Depth: °�' 9s ft
Static Water Level: / -Z • 1 " ft
Height of Water Column: & 16 It
IC.Project#:�ft cvw�iti Cv. /UewL ocT .2( —
Id Data Sheet Review: S'"t-
Date: 1CltDLiLt By c'X13
tolti9lu (3�„
Well Locked: C (XES:� NO / Flushmount)
Construction:. (& Steel/Stainless Steel)
Multi Factor*.. 0,143 r{Radius/12)2:13.140.481
Casing Volume: ) q3 gallons
Cal, 3 Volumes: / 2 gallons
Pump'lntake: �' A
Purge'In€ormation
Date Purged: L /�Z rr Start: l YOO Finish: l 15 Purge
)7
Purging Method_ 2-1 i s"l110. �p.c Total Volume Purged: 150 o (gallons /L)
Sam lin¢Information
Date Collected: / u / �/ 21 'rime Collected: / �7 0 _ (am/& Sampling Equipment Used: �l 5�4 c Instrument ID, �6 ;j D 20 3 -rp o 3SS
Bottle Type
25 O K..L a(as
(- zs v �l
K o h. _
3 4 0 V'L_
Preservation
Lkhprco .
Y{ C'
HcL
NCI.
Analysis Required
Vo c.
I q-b
Field Measurements/Observations
Sample Temp (aC): 1 Q, o Tinte:
_Turbidity (ntu):
1 ` 7
Time:
/
Diss Oxy (mg/L): o', 3Time:
/ Y•2-P
Fe 2+ mg/ L:
A)-b
Time:
/
Specific Cond. (uS): 1 5 Time:
/ VZ O
Res. Cl (mg/L)/(gg/L):
Pime:
Sample pH (s.u.): 3 ... Time:.
9 0Z
Odor: Lk47-rO-___
_Time:
T
_
C[Cat'
/ ��
ReDox (mV): Time:
Appearance
ReDox (EH value):YSI ProPlus+200mV
;j Z
Other:
Time:
_
General/Weather
Sampler Signature:-
0
,tablization Test
cloudy/rainy) Temp. 7('F) Wind__L_�_(mph)
(v -2.6-Z-(
Time
Purged
Temp.
(C)
DissOxy.
(mg/
Spec.
Cond.
(uS),
pH(s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/ n,/
L
Water
level (ft)
Omer
I 05
/7.3
O,
95/
(,•3
S/7,
/,la
Sav
/2.zc/
�wP
17.3
D.
95)
�.3
7,`/
!,!,
Iz. it
{ytv
/ ,v
O.tf
3
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1.
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1a-2.7
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a
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Document Name: Field data Sheet
Elate Issued: March 8, 2014
•
I of I
eAn,?1yl1W1 IPage.
bycument Number. F-CAR-FED-001-rev.03
Issubig Authority: Pare Htmtersville Quality
Office
ELF
Name and Affiliation (Samgler(s): `� G " �� r� r Field Data Sheet Review:
S
By:
CT
Purge Information
Date Purged: ! / LG /L 2I Start : / 3 2-0 Finish: 1335 Purge Rate:
Purging Method: t STD �' ( Total Volume Purged: 154,0 (gallons/(! /L)
Name and
s-
well ID: n ' % z Well
Affiliation (Inspector):
Date: jo(2�i(21
Well Information
It7(i it
Sampling Informiation
Date Collected: t ° / 2G/ z-( Time Collected:) 3 Z U _ (am
Sampling, Equipment Used: e t �V U' e _Instrument ID: (� b �3 TQW�S
Bottle Type
o L%,,L e l
mL
Field Measurements/Observations
Preservation
(r(GL
(JCL
Analysis Required
T(� 5
V6 C_
Sample Temp ('C):
/ 7 • )
Time:.
/ 3 `10
Turbidity (ntu):
3,q
Time: 3 y�
Diss Oxy (mg/L):
G ' 5
Time:
! 3 V O
Fe 2+ mg/ L:
N-
Time:
Specific Cond. (uS):
q7 7
Time:
/ 3 Y D
Res. Ct (mg/L)/(µg/L):
Time:
Sample pH (s.u.);
eb>'
✓� 2%_.._._Time:
/ 00
Odor:_.. Lw5)N-,—
._
Time: -- / 3 D
ReDox (mV):
S' o
Time:
3 V�
Appearance:
Cbec�
Time: / 3 Y0
ReDox (EH value):YS.I ProPlus +200mV
?'l 5 •
Other:
Time:
General/Weather
Wind -/ 3 (mph)
Sampler Signature
Stabilization Test
LF- Oci
Spec
Voume
Time
Temp.
Diss Oxy.
Cond.
pH (s.u.)
ReDox
Turbidity
removed
Water
Other
Purged
o
(C)
(mg/L)
(uS),
(mV)
(ntu)
(gallonsfrtt /
Ieve1(ft)
L
132.5
I
c.7
470.0
I
6,•2
500
it.Og
'D IF
15.7
cq .7
g70.0
Z
Sao
33a
/Z, t
D.Cv
41ei.(o
g
7 6- 5
`i.1
/ o00
!l•!�
t3a
t� g
o.L.
4iy.1
c�.sr
-Is.7
.3
, soo
11.,Y

Document Name: Field data Sheet
Date Issued: March 8, 2019.
Page: 1
r3GP.N7r71yliC8f
of
[7dcument Number F CAR-FI..13-001-rev.03
I:ssuuig Authority Pace Huntersville Quality
...
r�
Office
L
Name and Affiliation (Sampler(s): ' ' 74 ce _
Name and Affiliation (Inspector):. V VNA- --
Well Information
Well ID: M w - / 3
u
Well Diameter: 07
Total Well Depth: 15 3� ft
Static Water Level: �` �� ft
Height of Water Column:/0.7 2-- ft
A)
Data Sheet Review:
Date: 1Gl21 f zl
10(�q �L)
Well Locked: 4YE5 / NO / Flushmount )
Construction: (&/2Steel/Stainless Steel)
Multi Factor*: V `3 r(Radius/92)2x3.14x7.481
Casing Volume: / 5 gallons
Cal. 3 Volumes; S ' .)s gallons
Pump Intake: 13 • v It
1� LF-Off'z(—
By: a"'
131. I
Pure Information � kV_ / /
/it� Date Purged: I ° / Z� / c Z 11 Start : 3 7 Finish- / 51 5 Purge Rate: --
Purging Method_ D "L.Sr`x l Total Volume Purged; Zu o (gaitoiis(nlll� L)
Samplinglnformation ✓
Date Collected: tt q / 2-G/ 2-1 11 'rime Collected; ' S J .._ (am/Qi
Sampling Equipment Used: 5 It Instrument ID: r� 3 TPG J5s
Bottle Type
3 - Lf u .V, c
Preservation
d%oy_�', -
aCL
Analysis Required
__--_.i^�_lala�__.,w __......_....
Field Measurements/Observations
ISSv
Sample Temp (°C): _ 15 • S�) Time; _Turbidity (ntu): '3 • � Time: l 5 SD
Diss Oxy (mg/L):
0.3
Time: 15 Sb
Fe 2+ mg/L: Time:
/ 5 50
Specific Cond. uS :
p ( )(
4 � • 3
Time: 15,50
Res. Cl m L `
g/ )/(ttg/L}: 'Tune:
Sample pH (s.u.):
_L ``. 5 .._...
Time: / 5 S D
Odor: K _...__ Time:.....
I s U
ReDox (mV):
G I
Time: l S SD
Appearance: Gila rime:
/ 55D
ReDox (EH value):YSI ProPlus +200tuV • R
Other: -- Time:
—�
General/Weather Observations:
Sampler Signature
Stabilization Test
cloudy/rainy) Temp. SZ (°I) Wind 7 (mph)
/0- 2G' 2
Spec.
Volume
Time
Purged
Temp.
Diss Oxy.
Cond.
pH (s.u.)
ReDox
Turbidity
removed
(gallons
Water
level
Other
(C)
(mg/L)
(us)
(nv)
(ntu)
(ft)
L
( 35
iS,tf
o.y
`(G .3
(0.5
f5
�400
ID 1'VQ
15.`F
o,y
4`G •3
G.5
154,
9.4
—
i5b
t5.5
c, ,,3
art sf,6
G.5
9.1
a.
u
</
12_G6
�,

6aAntx"101
+r
Document Name: Field data Sheet.
Pate Issued: March &, 2019:page:. 1 of 1
Document Number F-CAR-Fi,D-001-rev.03
lsmiug Authority Pace Huntersvilte Quality
Office
--BL
Name and Affiliation (Sampler(s): C' 1�c c-c.
Name and Affiliation (Inspector): i`ly 1n.L.
Well Information
Well ID: r t W 1 3
Well Diameter:
as
Total Well Depth: q � ' 63 it
Static Water Level: —21 Y ft
Height of Water Column:3�, 13 ft
Well Locked:
) C Project #: Bkneoh1C �• �� I- - Oct ,7-\ —
.ld Data Sheet Review; U ti
Date: I of 4121 By: cv5
10113121 VAS
Construction: E5/Steel/Stainless Steel)
Multi Factor*:Ok/G3 r(Raadius/12)2x3,14x7.487.
Casing Volume: a gallons
Cal. 3 Volumes; 9, 11 gallons
Pump Intake: Lf �• d ft
Purge Information
Date Purged: l o / 'Zb / -7-11I j Start : 1 t l S� Finish: j s� s Purge Rate: l o o `-1 �
Purging Method: i 4 l 0. l� c Total Volume Purged: 2-0 . a (gallons g/L)
SamplinizInformation
Date Collected: lb / 2-G/ 21
Sampling Equipment Used:___1%e t
Time Collected: / s �_ (am/(@)
Instrument ID: y S1 * 0 2X3 TPw :4 d 3SS
Bottle Type Preservation
i - Z50 t,,,l pe s . /J0,3
a-gL? o.. Hct_
Field Measurements/Observations
Analysis Required
Uoc
Sample Temp CC): % y —/ Time*
5 ._Turbidity
(ntu): " Z Time:
/ s�
Diss Oxy (mg/L): 0.3 Time:
/S'Z6
L /2
Fe 2+ mg/L: Time:
/ 5
Specific Cond. (uS): �2'�.% Time:
/��o
Res. Cl (mg/L)/(ltg/L): — 'rime:
Sample pH (s.u.): —(e,3Time:
/ 5a
Odor:_ _
ReDox (mV): 5 2 •% Tune:
/ �oZ�
Appearance: Cl ear rime:
ReDox (EH value):YSI ProPlus +200niV
2-
Other: Time:
GeneraVWeather
Sampler Signature
Stabilization Test
y/rainy) Temp.
!o -ZG•z
Spec.
Volume
Time
Temp.
Diss Oxy.
Cond.
pI-f (s.u.)
ReDox
Turbidity
removed
Water
Other
Purged
(C)
(mg/I)
(US)
(MV)
(ntu)
(gallons/®/
level (ft)
L
1500
7.7
ya
•3
iS.
(9.
bD
I.Sz
'D e
l .�
a.�
N3.I
•3
(,a-.
.
7.52-
15v5
1 Lt,?
d. 5
yzl,,%
6.3
5'9• *,L
3.3
1 D00
�Y. o"l
115iv
11t,l,
1 o.y
y�71
L.3
s .v
lst,
g, ly
t515
1 iIf. g,
I o.3 I
g23.6
�•3
sy,
),3
9-00
za

Document Namc. Field data Sheet
Date &sued: March % 2019
r 0GCF11k71ytiCa!
Page:: I of J
C7gcument Number. FCAR-F•[ t)-0O7-rev.03
Issubig Authority: PaceHmitersville Quality
Office
Client: � L£
F...ge�I..d Data Sheet l 1
Location: L�5 V 1k AJQ- Project Ob av\cawtbT Co . NC Lr-oet 2 1^
Name and Affiliation (Sampler(s)c C' LG " � Field Data Sheet Review:
Name and Affiliation (Inspector):
Date: 10f7-41 l By .�
Well Information
1011.911) 13M1r
Well ID: VtiW - I �1
Well Locked: / NO / Flushmount )'
Well Diameter: 2"
Construction: �V °Steel/Stainless Steel)
Total Well Depth: 62- It
Multi Factor*:Ot 43 r(Radius/12)2x3.14x7.48l
Static Water Level: -2 9, 9 2- It
Casing Volume: -7 3 gallons
Height of Water Column: �Z• 11 it
CaL 3 Volumes: 1 1 ' 19 gallons
Pump Intake. 5b ° ft
Purge Information
Date Purged: 10 / 2_& 2_ I
Start. / 2ZO Finish: / a �S Purge Rate: (O p h, L- �=
(&/
Purging Method: o n So u Y.
Total Volume Purged 2 Sb ° (gallons/ L)
Sampling Information
Date Collected: 0.a / 74/ zl
Time Collected: L 7-5 0.,.._ (am/Q
Sampling Equipment Used: Y
$O" Instrument ID:7*r#o2'3 Tow o-;5✓r
Bottle Type
Preservation Analysis Required
2..5 n t, L, p�CtS
(�h r eS. Tb.5
l- -250 wt �lao.
o Mwf. /S
3 L(o AtyaA
HCL Vor—
Field Measurements/Observations
Sample Temp (eC): % t% z Time:. / � _Turbidity (ntu): 7 Time: / a5 v
Diss Oxy (mg/L): 5,1 Time:
I � S
Fe 2+ mg/L: N -D
Time: 2 5 0
Specific'Cond. (uS): f 7g & Time:
I �25 v
Res. Cl (mg/LV(ltg/L)i
—'rime: —�
Sample pH (s.u.): 4 " -2, -----Time:
/ -1- 5 b
Odor:_ _.- � _.-----
Time.......
ReDox (tnV): 7 V - `'' Time:
%,'-SP
Appearance: de4r'
Time:
ReDox (EH value):YSI ProPlus +200mV
270.0
Other:
Time:
General/Weather Observations:
Sampler Signature
Stabilization: Test
/rainy) Temp. S!, ff)
v • Z6- 2/
Spec.
Volume
Time
Temp.
Diss Oxy.
Cond.
pH (s.u.)
ReDox
Turbidity-
removed
Water
Other
Purged
(C)
(mg/I)
(us)
(mV)
(ntu)
(gallons/�/
level (ft)
L
z�5
13•�
g
/88.1
C.Z
5-S.1
27.2-
50c?
30.5
awpj
3.v
`F.
12%!.1
G•z-
'55,1
027.2
3a.5
lZ3o
3. Qi
q,7
ISy,�
L•z
Si I
o1 7
/tJao
30.G
Iz�Si
q(
55.0
ISlO.L
(a•2
`z•3 1
/ h
3o,7s�
1 L`do
1
q_5
ES.c,
/gD.N
&Y,0
1 13.7
'Aoo0
IZ'f5 ILf.4 5.1 119.9 (.•L (-5.2, ii.5 X500 30•77

Ark*tiCd1 ;E�xunientName., NnmFinld dataShec@. Date I
hl,
t Number: F-CAR-FLD-001-rev.o3 Lnuu,g Author
Field Dat Shee
Client; Locationn: 5 t'2, A' L Project#: 3k
Name and Affiliation (Sampler(s): �' L G _ t A c�J=niRun1tejvw'
Name and Affiliation (Inspector): VYry.
Well Information
Well ID: IvIW ` l t{ Well Locked: NO / Flusho
Well Diameter:
Total Well Depth: 9 1. 5y
Static Water Level: 3yft
/ • 3 I
Height of WaterColumtlel•l9 £t
Construction:
Steel)
Multi Factor*: ®' G3 (*(Radius/12)2x 3:14 x 2.481
Casing Volume; 017c� gallons
Cal. 3Volumes: a5, O gallons
/Vew LP- Oc� ,V -
c t1?>
By. 13, r
Pump Intake: n• o ft
Pure Information /
Date Purged: 10 / a � / Z1 Start- I ( I �{ S Finish: �j D Purge Rate: 1 0 D h- L / ( �'
Purging Method; KA_0 .5 C>UT Total Volume Purged: 1 S.- o anon m L (g / )
SamplingInformation
Date Collected: I u llc 1 I z U j
—�—/ Time Collected::
Sampling Equipment Used: �-�0 0 0- Instrument ID: y51 d 203 1-fCV 4 a 35S
Bottle Type _
--
z50 h,L- P'GS
/ z5u ry lC plus
Field Measurements/Observations
Preservation
I n+�s
t{lJO
_I_-26l"IGL
Analysis Required
� •IYTG(
yOC
Sample Temp (°C}:, / 3• S Time: �s _Turbid: ntu: a • 2 0-5
- — $' ( ) � Time: �
Diss Oxy (mg/L):
02 - 2- Time:
12-05
Fe 2+ mg/L; %✓ L
Time:
/ 0S
Specific Cond. (uS):
3 3 :L' Time:
1 2-0s
Res. Cl m)/(µg/) L L :
( g/
Time:
Sample pH(s.u.}:
. ___--_Time:.
/ZOS
Odor: - 0"'
-- —.
ReDox(mV):
5G• I Time:
/-'-O5
�/
Appearance: ` ,ecit'
Time:
/ay$
ReDox (EH value):YSI ProPtus +2oomV
zSG , 1
Other;
General/Weather
1-
Sampler Signature: ✓ n _ Date % v - Z-6 -
Time
Purged
Temp.
(°C)
Diss Oxy.
( m
Sec.
P
Con).
pH (s.u.)
ReDox
Turbidity
volume
removed
g/)I,
(US)
(tnV)
(ntu)
(gallons/ 11 /
13.1
z• Z
332-5
7. Z
G3.8
L
sc,
Dh�
131
z.Z
3325
7.z
!3�
�!
b�SS
I
2, Z
-43u.9
7.3
59.
I LOb
13.5
o2. 1
31. S'
7,3
57- 0
7.-A I
v sun
Wind /-5 (mph)
Water
level (ft) Other
30.8'
3 /z

aeeAnalyllcal
i
E
Dmunient Name: Fidd data Sheet
Document Number: F-CAR-FI,.D-001-rev.03
Name and Affiliation (Sampler(s): !' C- - e, c-e
Name and Affiliation (Inspector):
Well Information
Well ID: m lni- (% Z Well Locked:
Well Diameter: Z
Total Well Depth: oZ (o • q S ft
Static Water Level:1 6 1. lox-a?ft
Height of Water Column:( a 61 ft
C Project #; Sun�rrvt �p �Cp. nl LF- o�_f ,z(
Field Data Sheet Review: �t..i;
Date: po/Z9I7� B CZt3
Io�2Q �21 y BMS
Construction: NISI/Steel/Stainless Steel)'
[Multi Factor*; �'/�3 1+(Radius/12)2.x 3,14 x.7.481
Casing Volume: 1,73 gallons
CaL 3 Volumes: lJ, 19 gallons
Pump Intake:It
Purge Information
Date Purged: 1 0 / 17 / —A' Start- / v 05 / 0 " �i /
L 1 Finish: Purge Rate: � o(,V
Purging Method: Itwfe4 lc Total Volume Purged: y �0 allons
' (g Idg/L)
Samylin¢ Information
Date-Cdllected: 10 /d7/ rZ(
Sampling Equipment Used;
Time Collected; l? s
Bottle Type Preservation
/ • a 5o ML �GS ((y�pl'e$
- a5v na(- (as �A)0
3 - K 0 n,( C-L.,
--3 -`� a--"=L N c
Field Measurements/Observations
oxP3 Taw *-0355
Analysis Required
1u �fiG /s
V 1G e-
1, ` _
Sample Temp CC): / U • Time:
° ZS
_ Turbidityntu :
( )
5. 2
Time:
0
/ Zf
Diss Oxy (mg/L): 3, t Time:
/0 2 5
Fe 2+mg/L:
/
Time:
10 ZS
Specific Cond. (uS): 1 s • i Time:
/ U ZS
Res. Cl rn L g
( g/ )/(!t /L :
Time:
Sample pH (s.u.): 4' S __... Time:
U 2S
Odor:—__ Y\
`_¢__//
1J 2
f
ReDox (mV); 3.7• `/ Time,
!v ZS
Appearance:
__.._—_Time:
C� lzQ r-
__
•Time:
/ J 2S—
ReDox (EH value);YSI ProPlus +200n1V
23 7, °/
Other.
_
General/WeatherObservations:
Time:
Sampler
Time
Temp.41DissOxy
Spec.Purged
(°C)/L)
Cond.
pH (s,u.)
(uS)10
1 0
10 , 2-
z( 9,.Z)
ice. zD
�19. Ilull
/o.�
z1�
-G,5'
0 crouaYlramy) Temp. Y K CF) Wind 1 C2 (mph)
ate: /0- a7 2(
VoTite
ReDox Turbidity removed Wa/ 7rZ(mV) (ntu) (gallons level
0 v1 15,
77
0

_,,.+ry
taocument Name. Field data Sheet
pate Issued: March 8, 2014
j:
Alk?✓k 1/Ca1
f
Page: 1 of I
L'3ctcument Number F CAR-F•L.p-0Ql-rev.03
Issuing Authority: Pace Huntersville Quality
Office
j3 L jE
Name and Affiliation (Sampler(s):
Name and Affiliation (Inspector)-..
Well Information
WeII ID: M'j- I.
Well Diameter: 2"
b1K Well Locked;
Total Well Depth: H (' ' . ( ft
Static Water Level: , � 3 ft
Height of Water Column: ft
54
Data Sheet Review;
Date: lO fz91m
iult-1NI
�77 NO / Flushmount)
Construction (i'y�%Steel/Stainless Steel)
Multi Factor`; 0.163 ['(Radius/12)2:x 3.14 x 7,48]
Casing Volume: Lf` 61 gallons
Cal, 3 Volumes; 13 'S 3 gallons
Pump Intake: 3 R It
CTI3
By. ap-.
Purge Information
Date Purged: 1 0 / 1-7 / 21 II Start: 0 �
9 �5 Finish: g 5 ° Purge Rate:h
Purging Method: i ,1T , Total Volume Purged: 3 S a O (gallons nl L)
Sampling Information U g SS
Date Collecked: to /z7 / 2 I Tirane Collected; __0/pm)
Sampling Equipment Used: �i''S�aII!, Instrument1D:Tr'*0?-03-rpw-46,3SS
Bottle Type
I 2-5 o rr.c- p(is
f ' 2-5 ML P [[ S
3 _ 't V IL
3-'ion,(_
Preservation
Lkwp
N r-L
IJe
Field Measurements/Observations
Sample Temp (aC): 5 Time: 9-ss _Turbidity (ntu):
Analysis Required
'rJ).S
C.
Diss Oxy (mg/L): 0 ' Y Time: O 07 53 Fe 2+ mg/L: � - O Time: O 5 65
Specific Cond. (uS): 176' 7 Time: 015S Res. C1 (mg/L)/(ltg/L): 'rune: .--
Sample pH (s.u.): 7. 2— Tin -9 9 55 Odor:_-_ _.._____Time: ... U i SS_
ReDox (mV): d-5' 2' Time:.) 9 55 Appearance: d eon Time: 0155
ReDox (EH vatue):YSi ProPlus +200mV ;L'�O 2 Other: — Tune:
cloudy/rainy) Temp. 415 ff)
Sampler Signature
Stabilization Test
Spec.
Volume,_
Time
Purged
Temp.
u
(C)
Diss Oxy.
(mg/L)
Cond.
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
removed
(gallons/0/
Water
Ievel
Other
(us)
(ft)
L
093t
Io.3
0a8Q,3
(,•mod
57.5
`f
oo
I
e
/ 0.3
-0.7
;299.3
(.A
675
41.6
111,51
0135
1D.Z,
0.5
a•79,q
'7.
`f3.9
a.s-
/C&0
/y55
0 9t10
1/0
0.5
ja77.3
1 -2,
3 r. 9
(•Y
I zf na 1
/y.57
u 9`15
v.5
0.5
12,77,11
-7.t
57 6
cs.3
1 2$Vo I
/Y,//
0 950 10.4 D - Lf 277, y 7.7- z5.3 0.7 3500

ACCA/kTlyffCAl
Lkrcuo5ent Name: Field data Sheet
Date Issued: March 8, 2019'
Page: I ot7-
.,
'
[J�cument Number. F-CAR-Fl..p-0Ol-rcv.03
Issuing Authority: Pace Huntersville Quality
y
Office
Name and Affiliation
Name and Affiliation
Well Information
Well ID: All1✓-��
Well Diameter: r /? }�
Total Well Depth: 5 [.. U ft
Static Water Level It
Height of Water Column: ut 6-ft
1.
Well Locked:
Construction:
!Id Data Sheet Review:
Date.ie
Steel)
Multi Factor*: U l(a > i+(Radius/12)2x3.14x7,481
Casing Volume: gallons
i
Cal, 3 Volumes: '' a(o gallons
—� Sex,- Aq
By. C
!fir
Pum Intake: SO . C "' ft
Purge Information POA910
Date Purged, f Jam/ Start: Finish: Purge Rate:
Purging Method iylScc; /1 Total Volume Purged: i . S G (gallons/ 11s l,)
Sampling Information
Date Collected:_/1_1 / ( Time Collected:_ ` am m _-_( /P
Sampling Equipment Used: l nS('(4 Instrument ID: t 3` Ji1 f9;c Vd7 1�
Bottle Type
Preservation Analysis Required
"Vi -cry
Field Measurements/Observations
Sample Temp (eC): _ �/ Time: C660__Turbidity (nm)_ Time:
Diss Oxy (mg/L): ( G Time: Fe 2+ mg/L: Time.
bl�����u
Specific Cond. (uS): Time: Res. Cl (nig/L}/(hg�/L}: Time:
Sample pH (s.u.): _Time: Odor:__.-✓'�,'r__._-_ Time: 'Ile_
ReDox (mV): l U?a o Time: Appearance. 16-Timer
ReDox (EH value):YSI ProPlus +200mV 3 c'9, 2 Other: IV 6 Time:
General/Weather Observations: e�
. (funny)/cloudy/rainy) Temp..(°F) Wind (tr
Sampler Signature
Stabilization Test
Spec.
Vo urne
Time
Temp.
Diss Oxy.
Cond.
pH I (s.u.)
ReDox
Turbidity
removed
WT(ft)Other
Pwged
(C)
(111g/L)
(us)
(mV)
(ntu)
(gallons/�Iev
L
Al
lei,
"lo A
(,—�e l
67ay
1507
S.
a(?,�
(30,
� "�^
S� 2
�j�(J'
Z
i J
oa
d
=I s - - -6
!2 r;�r

Document Name:
Document Issued: March 8, 2019
.. �ceAr��ltylrc<�(
Field Data Sheet
Page?o£Z-
Document Number:
Issueing Authority:
P-CAR-Fi.D-001.rev.09
Pace Huntersville Quality Office
Client:
Location: / 5- ev' Ile
-
Project: 6 dI ocoU ok C,3- Ad;,IP� oct 2011 S Aqqe'
X""(
Well ID: /0 fin/ " ( tl
f*.Z0_ZI Gars
Reviewed Date and By: f o/2x /ti L��S
Stabilization Test
1\Tell Diameter
Multiplication Factor"
1
0.0408
1.2
0.0918
1.623
0.1030
2
0,1630
3
0.3670
4
0.6530
6
1.4680
3
2.6100
Time
Purged
g
Temp.
o
(C)
DissOxy.
(mg/L)
Spec.
Cond.
(us)
pH(s.u.).
ReDox(mV)
Turbidity
(ntu}
Volume Re ved
sJ
(gallons !s )
circle one
Water level
(ft)
Other
..3 S
V.5'
S, C
2 ILY
C- 7
105L
c1 U
750
c1 r, -7
Sc r
S,
�.15 S
- 7
Ow/',
G 0CIO
I C-leI r
Sa�
'11511.
6
( 0q, l'
a
.)So
oS�
1 6,7
t f 2
IL 1
O
c
(S.
5,.
0-1
111
sOcNI,0
? 11?0�
I '' -s
;. 5. 7
q,r
� I33
7
I11 �r
l'7�iCs "i
�+
�W S
7
214.

aceNtaq ffeaf' Document Name: Field data Sheet
i Document Number: F-CAR-FLD-oln-eev.o3
Name and Affiliation (Sampler(s):
Name and Affiliation (Inspector): . ,N j'A �—
Well Information
Well ID: r CY:vVt_ R n
Well Diameter: _
Total Well Depth: ft
Static Water Level: _ ft
Height of Water Column: _ ft
Purge Information
1d Data Sheet Review:
Date: Iu/2`I (z(
ioIAP,I
• t)
C
IL
Easee
Multi Factor": ['(Radius/12P x 3.14 x 7.48]
Casing Volume: — gallons,
Cal. 3 Volumes: — gallons
Pump Intake -
By:
Date Purged: _ /_/ Start:
Finish:— '— Purge Rate: --
Purging Method: Total Volume Purged: allons mis L
Sampling Information
Date Collecfed: f 0i . /*' Time Collected: I t 13 (ym (1
Sampling Equipment Used: v c b Instrument ID: YS� p roo � J-K- 3�r} MtLn� lY�� ra o
Bottle Type preservation A
I •_, 1 L nalysis Re d
AIG.sI-.L
tc
ryJ -t-I Q rwL 1/tq.Ci
Field Measurementons
al0 s
.1 re
Sat h\V-lu
Sulb�k IA1k I CI , tirYn
nnn 1a 1 S
C CIS
49T s V O C
Sample Temp (oq: K .Q Time: q _ Turbidity (ntu):
Dins Oxy ( m L : Time: t 3
g/) .`1 Time: 13� Fe 2+mg/L: Nl
Specific Cond. (uS): `I4=�Time:
me-'
— ._ TiTime: Res. Cl (mg/Ly(µg/L): Time:. —
Sample pH (s.u.): k Time: �l
/ Odor: L ,_g_ C."s.pn�Time:
ReDox (mV): )� Time: ) `1 0 pp
_ A earance: I� kacIC Time: .� k3 �
ReDox (EH value):YSI ProPlus +20llmV .M I
Genera Other' Time:
1/Weather Observatinnc 1 M O Y' I
]in4,es
- a rn --e7
I�.rtl.
JQ .I
NCI
tsurmy ouay/rainyF) Temp.�(OF) Wind I! (mph)
Sampler Signature• Date: Ia
Time Temp. Diss Oxy. Spec. o ume
Purged (eC) (mg/L) Con pH (s.u.) ReDox Turbidity removed Water
(US)
(mV) (nm) (gallons/mis/ level (ft) Other

Document Name: Pielct duM Sheet Date Issued: Marc] 8, 2019
ase/limlyticat ` Pa e: t of l
Document Number. F-CAR-Ft,D-001-rev.03 Issuing Authority: Pace Himtersville Quality
Office
Field Data Shee
Client:iS L'+` Location; 1U-fC Project #: n C
Name and Affiliation (Sampier(s): = - a (-t �1na l�} Ce,) Field Data Sheet Review:
Name and Affiliation (Inspector): N 1 A IPifv) N-A
Date:
Well Information �` I A
Well ID' s-CI�-i�=i- tRe C�tGC W` .
Well Diameter: C an: ee : am ess tt -
—
TotalWellDepth: ft Multi Factor*: — [(RadiusJ12)2 xBYi4x7.t8]
Static Water Level: ft Casing Volume: gallons
Height of Water Column: — ft Cat 3 Volumes: gallons
Pump Intake: _ ft
Purge' Information
Date Purged: Start: Finish- Purge Rate:
By:
4 e 1-t= 0 l.�rnat .
Purging Method:_ Total Volume Purged: (gallons/uils/L)
Sampling Information
Date Collected: 1 0 j?_'L j - Thne Collected:- `' , Q ( p )
Sampling Equipment Used: 6'a6 Instrument ID: �/ ST ft (�L fk3_y�� (vls u oTG w * �o}q
Bottle Type
-'-lowl..rTGts
Field MeasurementslObservations
Preservation
,ja
Analysis Required
©T cl( S ._......__.
Alp�Z�Joc
Sample Temp (°C):j •B _Time:_�I QTurbidity(ntu): ;�` —Time; ]� 1 �
Diss Oxy (mg/L):­.... S } Thne:�_Pe2+mg/Lt t4) Time: I- i—D
Specific Cond. (uS): t I�iS • Time: ��AM ,Res. Cl (mg/L)/(µg/L): — `Dime= `—
SamplepH(s.u.): ��._... Time:-)� l� Odor:_--N_.... -- _�Tune:....t_`_'t1_—.
ReDox (mV): Time: Appearance: Gl e `Time:_
ReDox (EH value):YSI ProPlus +200mV -Tr . Cl Other: Time:
General/Weather
Wind t 1 (mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
CC)
Diss Oxy.
(mg/I,)
Spec
Cond.
(us)
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Vo ume
removed
(gallons/mis/
L
Water
level (ft)
Other
Q
B
S,�
S
lola�61

r'GkNylfea/' Document Name: Field data Sheet Date
B
t . Document Number. F-CAR-FLD-001-rev.03 Issuing Author
FieIdFieId Data Client:_ � lir
Location: �is�on.-I,la
Name and Affiliation (lei(
SamPs): Project #:]3�
.. �' dal ��(
Name and Affiliation (Inspector); l..r I f} Field Data Sheet Review:
Well In on,o ONI-b- 1 Date; Ycd�'i 17a
Well ID: L Y t n Mo/l 41
Well Diameter:
Total Well Depth:
Static Water Level:
Height of Water Column:
C
Multi Factor*: . _ [•(Radius/12)2 x 3.14 K 7.481.
Casing Volume: gallons
Cal, 3 Volumes: =� gallons
P —
By:
A-d, ,- LFock.D-)at�{j
Purge.Purge Information U'nP intake:�_�t
.Date Purged; Start
Fm'sh: Purge Rate:
Purging Method: Total Volume Purged:
(gallons/mis/L)
Sampling!ampling Information
Date Collected: l�-2-Z;/ a\
Time Collected: (a pm Sampling Equipment Used: G ` ,
Instrument ID(u y tk 3Y ? Bottle Type :_y Sr A- cn
I I (Y[vLcvTP a J
Preservation � 1 �
a ysis Required
Field Measurementa/Observations
Sample Temp (oq: -', Ttme: I
Turbidity (ntu): LA of Time:
Time: 1 � a Fe 2+ mg/L: �. (�
Specific Cond. (uS): 3 13 —?- Time:.
[ Time . ) Res. Cl (mg/L)/(µg/L): Time:.
Sample pH(s.u.): �i,� �-
Time: i S3 Odor:_, �2t� C�k Time: ReDox (mV): 36 4
Time: .i t $ Appearance: Uy��
ReDox (EH value):YSI ProPlus +200mV --Te S3
.._ ...._ -l-i Other•

Document Name: Field data Sheet
Date
saRnatylic 1
i
Document Number F-CAR-FIa)-00?-rev.03
Field D__ _ata Sheet
Name and Affiliation (Sampler(s): -Y-_ • �q(z awl +rc—
Name'and Affiliation (Inspector): N -_-_6-
We11 Information
Well ID: L> We i. n kF i r
Well Diameter:
Total Well Depth;
Static Water bevel: fk
Height of Water Column: ft
1'raject cJ, C- F 0c(Flo
�a(
Data Sheet Review: ,3
Date:14fICI
By: CM
(�
Cost . an Mess e@ )
Multi Factor*: r(Radio8/12)2 x3:1¢ x 7.Asj
Casing Volume: gallons
Cah 3`Volumes: — gallons
Pump Intake:�_ft
Purge Information
Date Purged: — f=/ — Start:
Futisit: —' Purge Rake: —
Purging Method:_ Total Volume Purged:
(gallons/cols/L)
Sarntsline In�Qn
Date Collected: 10 /fig / a�_ Time Collected;_.) �a
--
Sampling Equipment Used:
Instrument ID:/S_ (am/ cn
Bottle Type P
Field Measureme t Observations
re
servation
>-A-Cj _
Analysis Required
Sample Temp (°C}: (� Time:: 1 �Q
Turbidity (ntu): _S3-'7 Time:
Diss Oxy (mg/L):�"3_ Time: Q g/
-�_ Fe 2+ m I,; Aiy� Time:oV-
Specific Cond: (uS): Time: 1
_Res. CI (nig/L)/(ltg/L): Time: `—
Sample pH (s.u.): , (•ta+n
______ _.. Time; i Odor:_
. i S�Oc-
ReDox (mV): 81 �' — ---.-_ .—
_ Appearance: S) i 5A c iou Time: /�0 r
ReDox (EH value):YSi ProPlus +200mV t 7 r
General/Weather
.Lime.
1f Weather bbservaeinnx•
Temp, � (`F) Wind 1A (mph)
Time Temp. Diss Ox . Spec. o time
Purged ° y Cond. H' s u. ReDox Turbidity removed Water
g (�) (tng/I) (us) P ( ) (mV) (ntu) (gallons/mis/ level (ft) Other

Document Name: Field `data Shu,. Date
EBR171l1}/llEa7
fow
r
Document Number. @-CAR-PIA-001-mv:0.3 lasuing.Aathm
Field Data Sheet
Client,-_ �j (� _Location:
Prolect#: un,
Name and Affiliation(Sampler(s):�5�-i&ocn Ana(r cad Field Data Sheet Review:
Name and Affiliation (Inspector): `/
WellIn—nfOrMatiOn it/fL`t/2d
Well ID:
71 Date: �aida�dlwall T
Well Diameter:
Total Well Depth; _ ` _fit Multi Factor : }
[ (Radius/12)2 x 3,14 x7,481
Static Water Level:
ft Casing Volume: gallons
Height of Water Column:
ft Cal. 3 Volumes; gallons
Pump Intake —
Purge
_TInformlion•
DatePurged: � /_/ — Start: — �-
Finish. Purge Rate:
I of
4e+- ,e Lw oLt.D<)D_I M
By: 4
Purging Method:- Total Volume purged:
(gallons/mis/L )
Samnlin¢Info� r_ ttratiou
Date Collected: (O / ) B
—1 -Dtk- Time Collected:_ 1 S
_ (ant/ m)
Sampling Equipment Used: 6 mb
InatrumentID_YSr (.us -z�
Bottle Type--iCy1�UnYOwa 30
Preservation A l
4owl qAv:�'-
Field Measurements/Observations
na ysts Required
._---e4FG:(s _ -.._
,4 01)t � to C
Sample Temp (aC):_
Turbidity (ntu):% Q ` Time: l�
Diss Oxy (mg/L):_
Time: )( Fe 2+ mg/L: a O
SpecificCohd: (us): � Time: 1 —"�--Time:
Sample pH (s.u,): t can
� __Res. Cl (mg/L)/(pg/L)= Tbne:
(, , —
_.____,Tih1e: f� Odor: M
ReDox (mV); �6-1 _.. _P1}4.11_L__.._—Tirne:._
- �- Time: (_(��Appearance —
ReDox (EH value):YSI ProPlus +200mV4- -Time: r1
_

Dcxument"ame: Field data Sheet Date
GeArk7lyNcal
t Dmument Number: F-CAR-PIA-001=rev.03 l�uutg Autho:
Field Data Sheet
Client, -- Location; )byC
Name and Affiliation (ler Sam s : Project #:
P (� = e ( F` Co-k Field Data SheetReview:
Name and Affiliation (Inspector): A }(
Well I—of°nn— a _lion Date: L., I
Well ID:_ 1 D_ t 1
.Wells r a. �......;.,
Well Diameter:
Total Well Well Depth; — ?
"-'- —fit Multi Factpr*: ~ r(Radius/12)Zx 3.14 1.7.481
Static Water Level: —
--------ft Casing Volume: gallons
Height of Water Column;
ft Cal.3 Volumes; gallons
Ackt LP 00 ,DcY�,(
By:
NPA-
Purge Information Pump Intake:�_ft
Date Purged: f_
Start: _ Finish: — Purge urge Rate. -
Purging Method:_
Total Volume Purged: (glons/i1tlsjI,�
Sampling Infoematlon
Date Collected: 1 c) / O/
Time ColleetedcV) (,
Sampling Equipment Used: - Q -------- (am/0
Bottle Type --- InstrumentID_�/S�
Preservation Analysis Required
iClnt I .,J0\
ADD`(' �lclr
Field MeasurementslObservations
Sample Temp (°C): —A-6 ,
�Time:-A4 Turbidity
Diss Oxy (mg/L): P'-T (ntu): L ,a Time:
. Fe 2+ mg/ L; +--n--_._____-__Tmle.
--------_— Tune: b Q ' 6I �
Specific Cond. (uS): S (�
Time: _Res. Cl (nig/T)/(ug/q. "tune: '—
Sample plt(s.u.): Odor1�
Time:
1;eDox (mV): �� . ' I
--------- Time:
ReDox(EH value):YSIProPlus+200mV Appearance: �Zilow •(n�--•Time:___-______ Jb10
General/Weather Observations__
-v---------- —
Genera 0tiler: Time:
Sampler
Temp. S_(°F) Wind l a (mph)
Time Temp, Diss Oxy. Spec. Vo ume
Purged CC) (n1g/I) Cond. pH (s.u.) ReDox Turbidity removed
(us) (mV) (ntu) (gallons/mis/
10
Water level (ft) I Other

Document Name: Field data Sheet Date Issued: March S, 2019'
BGeNt,Tly(iCa! • page: I of „l
Document Number: F-CAR-Fl.D-0Ot-rev.03 Waing Authority::pace Huntersville Quality
Office
Field Data Sheet
Name and Affiliation (Sampler(s): �--P--Z---q�zc o 4Ac-� {t 1 field Data Sheet Review:
Name and Affiliation (Inspector):. nj + � i} ,U�i��
Well Information Date:
told�+ld f
Well ID: LD 1 u
Well Diameter: am ess
Total Well Depth: `� ft
Static Water Level; ft
Height of Water Column: — ft
Multi Factor*: — r(Radius(12)2x3ti4x7,481
Casing Volume: gallons
Cal. 3 Volumes; — gallons
By:
Pump intake: ft
Purge Information
Date Purged: / " / — Start: Finish: Purge Rate:
Purging Method: Total Volume Purged: (gallons/mis/1)
SamplinEInformation
Date Collected: f Cl / X13/,.a�_ Time Collected _ L'�1L\___ (anop
)
Sampling, Equipment Used: 6 c-c�` _ �
" 1— Instrument
Bottle Type Preservation Analysis Required
1��Cg tit uA t 0.Z ?
yJ�>71Cc3(�e-
Field Measurenrents/Observations
Sample Temp (eC): ` �. _Tine:, I ; 1Q.-._Turbidity (ntu): IQ • Time; 1 S-.No
Diss Oxy (mS/L): 3 t' Time: I Fe 2+mg/L Nl� Time: l''� O
Specific Cond. (uS): _ Time: j Res. Cl (nig/L)/(ltg/L): -- Time:
Sample pH (s,u.}:Odor:__.._ .__rvl .._.... Time: \ i aq_ _
ReDox (mV): ) Q l • i l Time: _� C f� _ Appearance: Sl �n1y l .• Lime: ) �s
ReDox (EH value);YSI ProPlus +200m V _ Other: Time:
General/Weather Observations:
Temp.'�(°F)
Sampler Signature
Stabilization Test
Ackt, l F x a,Do;)4�i
Time
Purged
Temp.
CC)
1
Diss Oxy.
(mg/L)
3,
Spec.
(us)
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
o ume
removed
(gallons/mis/
L
Water
level (ft)
Other

�' B.1nafyEFeat`
Document Name: Field data Sheet
Document Number: F-CAR-FLD-001-rev.03
Oct-'';) y 54
cc-D (-pcjid, 30�)
Name and Affiliation
Name and Affiliation (Inspector): tV
We11In— forte
Well ID: . U)
Well Diameter: -
Total Well Depth: _ft
Static Water Level!_�ft
Height of Water Column ft
Purge Inforaratin
L
!ld Data Sheet Review:
" i(j[?AfU
Date:
C e to ess
Multi Factor": l*(R3dius/l2)2 x 114 x 7.491.
Casing Volume: gallons
Cal. 3 Volumes: gallons
Pump Intake:_ ft
Office
By:. —
Date Purged: — Start:
Finish: Purge Rate: Purging Method:. � Total Volume Purged: allons mis (g / / L)
Sampling Information
Date Collected:
—LgL'/ / �( Time Collected: I �10
(am/ m)
Sampling Equipment Used: (;> M
Bottle Type �—Instrument ID. ySt
Preservati6n Analysis Required
Field Measurements/Observations
Sample Temp (aq; 1' \�
P —� Timer Turbidity (ntu): , Q
Diss Oxy (mg/L ` Time: b a C)
Time: is a Q Fe 2+ mg/L:�__ (,G
Specific Cond. uS : 4-e i Time:
( ) Time: )— 6 Res. Cl (mg/L)/(µg/L); Time:.
Sample pH (s.u.): �_ Time: 1 G'a >_
Odor: �ec,&to -e Time: �� ReDox (mV): �1.5
Time: 16 No Appearance: ife cvj General/Weather Observations: L1rktab� e:
ReDox (EH value):YSI PTOPlus +200mV S41 S
Genera Other: Time:
Temp.(-F)

Dxunient Name: Field data Sheet Date
aeesLt7tytioat
f �ocumeuC NumtmT. P-CAR_FhD-001,,0.3 Issuing. Autho
Field Data Sheet
Client: Location;_ Sh ¢ 11 e v o
Project #: l�
Nameand Affiliation (Sampler(s):�� -R(,,La
Name and Affiliation (Inspector): N(�` cell Pield Data Sheet Review:
l�rz, (Zt
Well Information Date:.i��I
Well ID:. a LU lVa l bAakr t as re .
Well Diameter: Co
Total Well Depth: — ft Multi Factor*:
Static Water Level:
( (Radius/12)2x314 x 7.A81
' it Casing Volume; — gallons
Height of Water Column: ft Cal. 3 Volumes
gallons
.S_Go. A-�i-�-eLt=oet.a0
c� S4
By:
Intake: __fk
Purrze Information1'ronp:
Date Purged: / - ! Start:
Finish: Purge Rate:
Purging Method: Total Volume Purged:
(gallonslullsl'L)
Sampling Information
Date Collected: tot /mil 1
Sampling Equipment Used:
Bottle Type
field Measureme ts/pbbservat;n ,_
Time Collected: 13�
---111._._ (am
Preservation Analysis Required
)`)A1
� 1 V
Sample Temp (eC): --A;!,Time; ! 7rL
—Turbidity (zltu): S Time;
Diss Oxy (mglL): l 1 • Time: Fe 2+ mg/l�
Specific Cond. (uS); y—Time:
Sample pH (s.u.):� Time:. Res. Cl
I � Odor._. _ iJ . ----Time: ..._ � �n..—
ReDox (mV): S�3. /I
-- e):ycTime: I t Q Appearance. Cla,,t w/ ���cul«} tme: I 1 Q
ReI7ox (EH vahta):YSI proPlus +20dmv G
Genera Other: Time:
t/tNeatherQbservations: �VS,to z%S' �,5�43-'AbCTN
Sampler
Time Temp, Diss Oxy, Spec. Vo nine
Purged CC) (mg/I) Cond. pH (s.u.) ReDox Turbidity removed Water
(US) (mv) (ntu) (gallons/cols/ 1:1 (ft) Other

Document Name: Field data Sheet. hate Issued: March 8, 2p1low z
aCeAna(ytisal' P: ge; 1 of
r Document Number. F-CAR-FLD-001-rev.03 Issuu,g Authority: Pace Huntersville Quality
Office
Field Data Sheet
Name and Affillation (Sampler(s): jU-?caCpAnatc,(sCv�l
Name and Affiliation (Inspector): hj\ A
Well Information
Well ID; 5In1 - D Well f arkscl•
Well Diameter:
Total Well Depth: — ft
Static Water 'Level: � ft
Height of Water Column: ft
Pic
ad Data Sheet Review:
Ivl2g1V
Date: 10/0i/�l
C au1 ess Steel)
Multi Factor*: [*(Radius/12)2 x 3,14 x.7,481
Casing Volume: gallons
Cal, 3 Volumes: gallons
Pump Intake. It
Purge Information
Date Purged: // — Starts Finish: Purge Rate:
CX3
By. Nk
Purging Method: Total Volume Purged; (gallons/m1s/1;)
Sampling information
Date Coilected:Aq._/�W_:)�k Time CollectedjQ (-�, am pm)
Sampling, Equipment Used: (2 rr % Instrument ID: iS�Gr S i.a_�.t (1CC�w r9W t� c�
Bottle Type Preservation Analysis Required
I -�'—C1rwL �
..Rg_(IS-........
C�n,L ..rc�f� I-I-C.(
Q-ul Ne( �i�Y C)tn�Cn v
Field Measurements/Observations
Sample Temp CC): ) �1 t _Time;�� !ICE _ Turbidity (ntu): •_ Time: I o 1 [\
DissOxy (mg/L):— Time: I 1�k(4n Fe2+mg/L; NZ Time: I Q)I I CI
Specific Cond. (uS): ) 6 ] ,-)- Time: J qy 1(Res- Cl (nig/L)/(µg/L): '— Ti1ue;
Sample pH(s.u.): g ___.... Time: I Q,An Odor:__-- _/Q)-�> ___—Time:..I
ReDox (mV): % Time:- I'"I I\ Appearance: C � Time: 1 Q�
ReDox (EH value):YSI ProPlus +200mV DLb(7 .a Other: Time:
General/WeatherObservations_ %.,pS rr, s 1N.-8L�3��at'�
Sampler Signature
Stabilization Test
Trine
Purged
Temp.
u
(C)
Diss Oxy:
(mg/L)
Spec.
Cond.
(us)
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/m1s/
Water
Level (ft)
Other
-Z,L

or z
Document Name Field data Sheet
Date Issued: March 8, 2019.
a�ieRttaij?�Lk71
Page: 1 of i
_
}
Document Number F CAR-FL.[i-p0l-rev.43
Issuing Authority: Pace Huntersville Quality
Office
Field Data Sheet
Client:_. L"ELocation:'P at -VC
Project#:5bnrornb�(a1w'
Name and Affiliation (Sampter(s): v nLkcrl Field Data Sheet Review:
Name and Affiliation (Inspector)i N 1R
f01 Ili
WellInfonnation
Date: jolt By:
Well ID: S IN
Well Diameter: �ctrt Af} (n�rr
Total Well Depth: ` It Multi Factor*:
((Radius/12)2 x31t4 x 7. ks)
Static Water Level: — £t Casing Volume: —
gallons
Height of Water Column: ft Cal.3 Volumes: —
gallons
Punip Intake:
`� ft
Purge Information
h
DatePuuged:'r —/ —Start:Finish: --
Purge Rate:
Purging Method:___________— Total Volume Purged: I(gallons/mis/I.)
Sampling Information
Date CaBected:_jq—f Time Collected;_, b )�_ (an pm
Q 0 . Z)oyt S�
Sampling Equipment Used: Vrrnl Instrument ID:_ y�C nnl�rr y_. �[vqt eL)Tt,,,#.3n
Bottle Type
Field Measurements/Observations
Preservation
14} j o?
`-1-c1
Analysis Required
A(in-r If x
[.tin:11'11AI
Sample Temp (aC): _� Cf •� _Time:�..�..a: _Turbidity (ntu): Time: i 6�
Diss Oxy (mg/L): C Time., D��_ Fe 2+ mg/ L: /yin Time: l b J-�_
Specific Cond. (uS): Time: l bat Res. CI (mg/L)/(itg/L): Time:
Sample pH (s,u); ` Ci_..._-. _. Time: Odor:----- 1`._'�2..-._ —Time:..._tr'--
ReDox (mV): Q) Time: t 6a Appearance: 1 I'ime: GaS
ReDox (EH value):YSI ProPlus +200mV 3Q (fib Other: Time:
General/WeatherObservations:
Temp _'�(°17)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
C)
Diss Oxy.
(ing/L)
Spec.
Cond.
(us)
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/mis/
L
Water
level (ft)
ether
)�
l0
1

.. r 06Analytica! �
i�
Document Name Field data Sheet
Date Issued: March S, 2019:
Pager I of
Document Number FChR-CAR
Issuing Authmity� Pace Huntersville Quality
Office
Field Data Sheet
Aske Ut Lin A-)C,
Name and Affiliation (Sampler(s): �Z- bate &nj9 Cab( Field Data Sheet Review;
Name and Affiliation (Inspector): 1 A ia(2y 12t
Date: Well Information I to/dtl! a1
Well ID: S w -
Well Diameter: ess eel)
Total Well Depth: it Multi Factor*; (+(Radius/12)2x3.14x7.18]
Static Water Level: ft Casing Volume: gallons
Height of Water Column: ft Cal. 3 Volumes: gal lorts
A, k-e LP OcOODl IS11
By: W ?4_
Pump Intake: ft
Purge Information
Date Purged: — // Start: Finish: _ Purge Rate: —
Purging Method:--- Total Volume Purged: — (gallons/cols/L)
Sampling Information (6Qq
Date Collected:10 / 'a i Time Collected: A (am pn )
vF �bcl,
Sampling Equipment Used:— 6),,�e)n Instrument ID:_ �/ S Q colt u sy}a�M c of v at3t ��
Bottle Type
�-a-SQML
"lQNL-act;
�-t-lQrvL vea�y
Preservation
HNb2
Analysis Required
An r. rnZ (f I ................... _
�d::1 V f)r
I K (J" 0Y&_R_
Field Measurements/Observations
Sample Temp CC): (3,�1 Tillie:�%Q
22 nn
Turbid! ty(ntu): Time: IGLZ)O
Diss Oxy (mg/L): FJ_ Time:
) 6 0 0
Fe 2+ mg/ Li /U1 Time: I.6 0 0
Specific Cond. (uS): I S h Tillie:
t b00
Res. Cl (Diig/Lu(µg/ L): _'Time:
Sample pH(s.u.): __...... ..Time:.
16Q0,
Odor :—._._--- --- ---Time:.__�0 ,.._.
ReDox (mV): 7 Time:
1 6 00
Appearance: GLer/ Time: ) 600
ReDox (EH value):YSIProPlus+200mV,
GeneraVWeather Observations:
L,dC4,100.4 q, j ""o
Sampler Signature
Stabilization Test
Tillie: --
F5M,^ C—D 1z JLL,J
Wind —(mph)
Time
Purged
Temp.
('C)
Diss Oxy.
(mg/L)
Spec..
Cond.
(u5)
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Vo ume
removed
(gallons/mis/
L
Water
level (ft)
Other
___--- ---------- ____-__.__

Document Name: Field data Sheet Hate Issued! March8; 2014
_,_ Z/Inalytical Page. 1 of t
Document Number: F-CAR-FLD-001-mv;03 Issuing. Authority: Pace Hmrtersville Quality
Office
Name and Affiliation(Sampler(s): ,ZTZ- } t x ,q L1,,{,c�.\
Name and Affiliation (Inspector): n t 11)
Well Information
Well ID: / kVan T acka .
t.1C
Well Diameter:
Total Well Depth:
Static Water Level: £t
Height of Water Column:—' ft
aid Data Sheet Review:
icfl n17I
Date: h(d`1IJI
el)
Multi Factor*: I" (Radiva/ lm2 x 3,14 x.7.481
Casing Volume: gallons
Cal. 3 Volumes: gallons
�]
C1�
By. N�
Pump Intake: ft
Puree Information
Date Purged: Start: — Finish: Purge Rate:
Purging Method:_ -- Total Volume Purged: (gallonsJmLsJh)
Sampling Information
Date Collected:/�/a Time 0/p Collected:_ )
1��i_.__ { n to
Sampling Equipment Used: 6 f,, 6 InstrumentID:
Bottle Type Preservation Anal sr 0 d
�Qr✓\-
`1 rJ.wL�n aRr,
Anal — is
Field Measurements/Observations
equxre
aPoT_ yo_c-
1, �tD-, pxr—
Sample Temp (°C): _ (Q Time_U30 _ Turbidity (ntu): _ Time: I 17) C)�
Diss Oxy (mg/L): Time: _ Fe 2+ mg/L: , D Time: 1 I (l
Specific Cond. (uS): ]C 7, �y —_ Time: Res. Cl (mg/L)/(ug/L): .line: "—
Sample f 130 Odor: _
ReDox (mV): 6 `i •6 Time: (I Zi 0 Appearance _( I o Finite:
ReDox (EH value):YSI ProPlus,+200mV-_aLT Other: Time:
General/Weather Observations: 1, O'�, rr, ,. -jr • �17
Temp.S�A__,f°ri
Sampler Signature
Stabilization Test
Time
Purged
Temp.
(eC)
Diss Oxy
(mg/I.)
Spec.
(us)Cond
PH (s.u.)
ReDox
(111V)
Turbidityremoved
(ntu)
Vo tune
(gallons/cols/
L
Water
level (ft)
Offler
IQ
1

Ihmmnent Name: Field data Sheet bate Issued: March 6, 2019
�eA+taly11sa1 Pa e: 1 of f
' Document Number: F-CAR-17I.1)-001-rev.03 Issuing. Authority: Pace Htmtersville Quality'
Office
1J C
Name and Affiliation (Sampler(s): �— {mac cn Aczj N(a\ Field Data Sheet Review:
Name and Affiliation (Inspector): _} J i0f2`lt?I
Well Information Date: lol zq jZ,]
Well ID: S(,J Well i nrt d( v's zo ,` Hubtu tuunt)
Well Diameter: C
Total Well Depth: ft Multi Factor*: ((Radius/12)4x 3i14x 7.481
Static Water Level £b
Height of Water Column: "— ft
Casing Volume: gallons
Cal.3 Volumes gallons
Pump Intake: ft
Purge Information
Date Purged: -- J= f — Start : Finish, Forge Rate:
Ac. &_ . L.r 0ck,3r.Dl S1
CTS
By: RM e
Purging Method:_ Total Volume Purged: {gallonsf a lsji:,}
Sampling Information
Date Collected:�(L/(_ Time Collected: `� am pm)
Sampling Equipment Used: instrument ID: j tV(rrrv'1 —", �(
Bottle Type Preservation Analysis Required
H'joz =rx��rlt
140 - d� _gym....._ _........_
ADp
3 �nC1M a a; I f( i, �t D Like z
Field Measuremen!g Observations
Sample Temp CC): j(13Time.,_ 0 _Turbidity (ntu): D.3 Time;L-
Diss Oxy (mg/L): b Time: 0'AW— Fe 2+mgJL: fJ' Time: 44(T
Specific Cond. (uS): ) e-14r'1 Time: n SC Res. Cl (nig/L)/(µg/L): — :Time:
Sample pH (s:u): 7• a __..., Time: O S {C Odor:;_..._ 711D...__--.___—Time:..._SL�V( ... _
ReDox (mV); Time: 0 A V$ Appearance: C 1Q.i?Y Time: Oa
ReDox (EH value):YSl ProPlus +2OOmV D � Other: Time:
General/Weather Observations: rnr,rrl 2 2
Sampler Signature
Stabilization Test
Purged
Temp.
(°C)
Diss Oxy:
(mgJL)
Spec,aReDoxTurbidity
(use.
PH (au.)(gal1onsjmisj
Vo Lime,
removed
Water
level (ff)L

Document Narne: Field data Sheet Date Issued March &, 2019
2CCflih2lytlCCt Page:. 1 of—)
Dmument Number F-CAR-FI:.D-001-rev.03 Issuing,Authority: Pace Htmtersville Quality
Office
Name and Affiliation (Sampler(s):. an_ P,, �nr c cif Field Data Sheet Review:
Name and Affiliation (Inspector): r`1 Date: iGJ2IR21
Well Information O 641
ja
Well ID: Cv1J
Well Diameter: ee aut e, - teel)
Total Well Depth; — It Multi Factor*: — r(Radiu5/12)2 x 114 x T481
Static Water Level: ft Casing Volume: gallons
Height of Water Column: ft CaL 3 Volumes; gallons
Pump Intake: — —it
Purge' Information
Date Purged: '--'" // "'—' Start : Finish: Purge Rate:
By: t'Tl3
Purging Method. Total Volume Purged: (gallons/nits/L)
Sampling Information
Date CoI1ected:_k_.yi_/X/ a-1 (- 'rime Collected: _Q� �.._ am/ptrl}
Sampling Equipment Used: V °� Instrument ID: YSr (A4j*
Bottle Type Preservation Analysis Required
6/N111 (S .........
Field MeasurenxentslObservations
Sample Temp ('C): 1 �Y. Timer( i_ Turbidity (ntu):
Diss Oxy (mg/L): �''�� Time: C1� a Cl Fe 2+ mg/ L: 1�%i Time:
Specific Cond. (uS); u��Time: OCl�C Res. Cl (nog/L)/(µg/L): 'rime: `—
Sample pH (s.u.): �,,. -__ - Time:. �- 0 F C1
pp
ReDox(mV): 'p�-jo Time: OS' 0 Appearance C Vca,a(' 'lime:. 0!x;'�Q
ReDox (EH value):YSI ProPlus #200mV 1 i� D • ( Other: Time: —
General/Weather
Sampler Signature
Stabilization Test
�tV
Temp.. L4\ (°F)
W
Purged
Pingeged
Temp.
CC)
Diss Oxy.
(mg/L)
Spec.
(US)
(s
ppH.u.)
ReDox
OTIV)
Turbidity
(ntu)
Vo me
removed
(gallons/mis/
Water
level (ft)
Other

., r1CeA/ts11yliCal
t
713 LE
Dcmurnant Name: Field data Sheet.
Document Number. F-CAR-FLD-001-rev.03
Name and Affiliation (Sampler(s): G'U'- -T0. C-e
Name and Affiliation (Inspector): V a- �
Weli Infuriation
Well TD: 5 L -- Locked:
We ameter: Z� e, Constr on:
Total Well D i If Multi Factor*;
Date Issued:
Page;
udhodty:.pai
of
3" K e014
Data Sheet Review:
Date: laf2L1l�
loM)'I
( YES / NO / Flushm
(PVC/Steel/Stainless Steel)
Static Water Level: If Casing Volume:
Height of Water Column: ft
Purge Information —�—
Date Purged:_//
Purging
1"(Radius/ 12)2:x 3,14 x 7,481
gallons
Pump Intake: If
Finish: Purge Rate:
of I
By: i3
(gallons/ailsIL)
Sampling Information
DateCollected: / a / 2 / 2/ Time Collected: =--- (am/pm)
Sampling Equipment Used: qL /o InstrumentID:7g'#yzo3 Tek463S5
Bottle Type Preservation Analysis Required
Sample Temp
.Turbidity (ntu):
Diss Oxy (mg/L), _ Fe 2+ mg/L:_
Specific Coud. (uS): Time: es (mg/L
Sample pH
ReDox (mV): Time: Appearance: _
ReDox (EH value):YSI ProPlus +200MV Other:
General/Weather Observations:____3
Sampler Signature
Stabilization Test
Time:
Time:
Time:
2- lLJ
Temp. So (°F)
l0-26-21
Time
Purged
Temp.
(aC)
Oxy.
(mg/L)
Spec.
Cond.
(uS
pH (s.u.)
ReDox
(mV)
Turbidity
(mu)
Volume
removed
(gallons/mis/
L
Water
level (ft)
Other
J`e n"C

O.c1-.3Q-I
5.4
. ua vapallClC1:
Total Well Depth:
Static Water Level:_______- ___ft
'-'eight of Water Column: ft
Multi Factor*: r(Radius/12)2 x 3,14 x7.as]
Casing Volume: gallons
Cal.3 Volumes; gallons
PurgePump Intake: _ft
Information , ��olyyyy�
Date PurgedS�--�-- .Start:
Finish; Purge Rate: `---
Purging Method:
Total Volume Purged: (gallons/ails/L)
Sainuline Information
Date Collected: iQ /—?I/ Time Collected:
Sampling Equipment Used: Cgv-r (n -AT!"/pm)
Instrument ID: `F— Serer,(.. *
Bottle Type �--�—i:-a'� C11S crb rpwrs
Preservation Analysis Re ' d
` Li
Field Measurements/Observations
1—I ✓v IJ
I�t1�
�C t
quire
At�nT V 3C
Sample Temp (°C): 1, Time: S
._Turbidity (ntu): c� ,(� Time:
Diss Oxy (mg/L): � ,
Time: I $ S Fe 2+ mg/ Li
1
Specific Cond. (uS); -- --------T e:
Time: 1 Res. Cl Sample pH (s.u.): `�f31 ._.._ _Timer I
—_Odor: ---- .._Nth Time:
Time: 1 Appearance: C"0.0
ReDox (EH value):Y(3l proptus +200mV �Sj V ---rime:
General/Weather Observations: Other:
(�C i J. ?
Sampler
/rainy) Temp(.
Time Temp. Diss Oxy. SpeC' me
Purged (°C) Cond. pH (s.u.) ReDox Turbidij7o
ved Water(US) (inV) (ntu)/mis/ level (ft) Other
1 .n

APPENDIX B
LABORATORY ANALYTICAL DATA -
PACE ANALYTICAL SERVICES, LLC.

0
aceAnalytical
Report of Analysis
Bunnell-Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Attention: Andy Alexander
Project Name: Active Buncombe County Landfill MW
Project Number: 9378-26A
Lot Number:WJ30017
Date Completed:12/07/2021
12/13/2021 10:58 AM
Approved and released by:
Project Manager II: Lucas Odom
pCCgF�
24r�A
SOA
ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 149

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Bunnell-Lammons Engineering, Inc.
Lot Number: WJ30017
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
VOCs by GUMS
The laboratory control sample (LCS) for analytical batch 21730 exceeded acceptance criteria for Acetone.
This analyte is biased high but not detected in the samples affected.
Due to the large number of spiked analytes, there is a high probability that one or more analytes will
recover outside acceptance limits. The laboratory's SOP allows for 10% of analytes to recover marginally
outside criteria. The following analytes recovered marginally outside LCS criteria: Acetone (141 %).
The laboratory control sample (LCS) for analytical batch 22207 exceeded acceptance criteria for 2-
Butanone. This analyte is biased high but not detected in the samples affected.
Reanalysis of the following samples was performed outside of the analytical holding time for Vinyl Acetate
with concurring results: WJ30017-001, WJ30017-002. The samples were not detected in the LOQ which
is required for these samples during initial analysis.
Reanalysis of the following samples was performed outside of the analytical holding time for 2-Butanone
and Vinyl Acetate with concurring results: WJ30017-004, WJ30017-005, WJ30017-006, WJ30017-007,
WJ30017-008, WJ30017-009, and WJ30017-010. The samples were not detected in the LOQ which is
required for these samples during initial analysis.
Metals by ICP
The method blank associated with batch 21233 yielded a "J" value detection for Iron and the MB
associated with batch 21241 yielded a "J" value detection for Zn. No corrective action is required as this is
an estimated value recovered below the LOQ.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] whw.pacelabs.com
Page 2 of 149

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: WJ30017
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
MW-17R
Aqueous
10/27/20211025
10/29/2021
002
MW-17DR
Aqueous
10/27/20210955
10/29/2021
003
MW-11
Aqueous
10/27/20211045
10/29/2021
004
MW-11D
Aqueous
10/27/20211045
10/29/2021
005
MW-4D
Aqueous
10/27/20211130
10/29/2021
006
MW-4
Aqueous
10/27/20211200
10/29/2021
007
MW-2D
Aqueous
10/27/20211250
10/29/2021
008
MW-2
Aqueous
10/27/20211305
10/29/2021
009
MW-18
Aqueous
10/27/20211640
10/29/2021
010
Trip Blank
Aqueous
10/27/2021
10/29/2021
011
MW-1D
Aqueous
10/26/20210925
10/28/2021
012
MW-1
Aqueous
10/26/20211100
10/28/2021
013
MW-14D
Aqueous
10/26/20211205
10/28/2021
014
MW-14
Aqueous
10/26/20211250
10/28/2021
015
MW-12D
Aqueous
10/26/20211340
10/28/2021
016
MW-12
Aqueous
10/26/20211420
10/28/2021
017
MW-13D
Aqueous
10/26/20211520
10/28/2021
018
MW-13
Aqueous
10/26/20211550
10/28/2021
019
MW-8
Aqueous
10/26/20211645
10/28/2021
020
MW-8D.
Aqueous
10/26/20211700
10/28/2021
021
MW-10
Aqueous
10/28/20211010
10/30/2021
022
MW-1OD
Aqueous
10/28/20211045
10/30/2021
023
MW-3R
Aqueous
10/28/20211240
10/30/2021
024
MW-7
Aqueous
10/28/20211350
10/30/2021
025
MW-5D
Aqueous
10/28/20211200
10/30/2021
026
MW-5
Aqueous
10/28/20211235
10/30/2021
027
MW-6
Aqueous
10/28/20211520
10/30/2021
(27 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 149

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: WJ30017
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
MW-17R
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
79
mg CaCO3/L
10
001
MW-17R
Aqueous
Chloride
9056A
3.2
mg/L
10
001
MW-17R
Aqueous
Sulfate
9056A
33
mg/L
10
001
MW-17R
Aqueous
TDS
SM 2540C-
150
mg/L
10
001
MW-17R
Aqueous
Barium
6020B
64
ug/L
12
001
MW-17R
Aqueous
Copper
6020B
7.0
ug/L
12
001
MW-17R
Aqueous
Iron
6020B
290
ug/L
12
001
MW-17R
Aqueous
Manganese
6020B
55
ug/L
12
001
MW-17R
Aqueous
Nickel
6020B
22
ug/L
12
001
MW-17R
Aqueous
Zinc
6020B
9.0
J
ug/L
12
002
MW-17DR
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
120
mg CaCO3/1-
13
002
MW-17DR
Aqueous
Chloride
9056A
3.9
mg/L
13
002
MW-17DR
Aqueous
Sulfate
9056A
25
mg/L
13
002
MW-17DR
Aqueous
TDS
SM 2540C-
190
mg/L
13
002
MW-17DR
Aqueous
Barium
6020B
51
ug/L
15
002
MW-17DR
Aqueous
Iron
6020B
200
ug/L
15
002
MW-17DR
Aqueous
Manganese
6020B
8.8
ug/L
15
003
MW-11
Aqueous
Barium
6020B
64
ug/L
17
003
MW-11
Aqueous
Copper
6020B
6.9
ug/L
17
003
MW-11
Aqueous
Nickel
6020B
22
ug/L
17
003
MW-11
Aqueous
Zinc
6020B
8.7
J
ug/L
17
004
MW-11D
Aqueous
Barium
6020B
64
ug/L
19
005
MW-41D
Aqueous
Barium
6020B
110
ug/L
21
005
MW-41D
Aqueous
Chromium
6020B
1.4
J
ug/L
21
005
MW-41D
Aqueous
Cobalt
6020B
11
ug/L
21
005
MW-41D
Aqueous
Copper
6020B
3.2
J
ug/L
21
005
MW-41D
Aqueous
Lead
6020B
0.46
J
ug/L
22
005
MW-41D
Aqueous
Nickel
6020B
34
ug/L
22
005
MW-41D
Aqueous
Zinc
6020B
14
ug/L
22
006
MW-4
Aqueous
Barium
6020B
40
ug/L
24
006
MW-4
Aqueous
Chromium
6020B
9.6
ug/L
24
006
MW-4
Aqueous
Nickel
6020B
7.8
ug/L
25
006
MW-4
Aqueous
Zinc
6020B
7.7
J
ug/L
25
007
MW-21D
Aqueous
Barium
6020B
48
ug/L
27
007
MW-21D
Aqueous
Vanadium
6020B
3.2
J
ug/L
27
008
MW-2
Aqueous
Barium
6020B
76
ug/L
29
008
MW-2
Aqueous
Nickel
6020B
5.7
ug/L
29
008
MW-2
Aqueous
Vanadium
6020B
2.8
J
ug/L
29
009
MW-18
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
79
mg CaCO3/1-
30
009
MW-18
Aqueous
Chloride
9056A
1.7
mg/L
30
009
MW-18
Aqueous
Sulfate
9056A
30
mg/L
30
009
MW-18
Aqueous
TDS
SM 2540C-
150
mg/L
30
009
MW-18
Aqueous
Barium
6020B
12
ug/L
32
009
MW-18
Aqueous
Chromium
6020B
5.4
ug/L
32
009
MW-18
Aqueous
Copper
6020B
1.4
J
ug/L
32
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 149

Detection Summary (Continued)
Lot Number: WJ30017
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
009
MW-18
Aqueous
Iron
6020B
300
ug/L
32
009
MW-18
Aqueous
Manganese
6020B
24
ug/L
32
009
MW-18
Aqueous
Nickel
6020B
3.7
J
ug/L
32
009
MW-18
Aqueous
Zinc
6020B
3.6
J
ug/L
32
011
MW-1 D
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
83
mg CaCO3/1-
35
011
MW-1D
Aqueous
Chloride
9056A
2.5
mg/L
35
011
MW-1D
Aqueous
Sulfate
9056A
41
mg/L
35
011
MW-1D
Aqueous
TDS
SM 2540C-
180
mg/L
35
011
MW-1D
Aqueous
2-Butanone (MEK)
8260D
2.3
J
ug/L
35
011
MW-1D
Aqueous
Antimony
6020B
0.66
J
ug/L
37
011
MW-1D
Aqueous
Barium
6020B
31
ug/L
37
011
MW-1D
Aqueous
Iron
6020B
160
B
ug/L
37
011
MW-1D
Aqueous
Lead
6020B
0.37
J
ug/L
37
011
MW-1D
Aqueous
Manganese
6020B
14
ug/L
37
011
MW-1D
Aqueous
Nickel
6020B
4.5
J
ug/L
37
011
MW-1D
Aqueous
Zinc
6020B
5.5
J
ug/L
37
012
MW-1
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
59
mg CaCO3/1-
38
012
MW-1
Aqueous
Chloride
9056A
6.2
mg/L
38
012
MW-1
Aqueous
Sulfate
9056A
20
mg/L
38
012
MW-1
Aqueous
TDS
SM 2540C-
140
mg/L
38
012
MW-1
Aqueous
Barium
6020B
140
ug/L
40
012
MW-1
Aqueous
Chromium
6020B
2.3
J
ug/L
40
012
MW-1
Aqueous
Iron
6020B
190
B
ug/L
40
012
MW-1
Aqueous
Manganese
6020B
7.5
ug/L
40
012
MW-1
Aqueous
Nickel
6020B
2.7
J
ug/L
40
012
MW-1
Aqueous
Vanadium
6020B
3.7
J
ug/L
40
012
MW-1
Aqueous
Zinc
6020B
7.5
J
ug/L
40
013
MW-14D
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
140
mg CaCO3/1-
41
013
MW-14D
Aqueous
Chloride
9056A
4.1
mg/L
41
013
MW-14D
Aqueous
Sulfate
9056A
31
mg/L
41
013
MW-14D
Aqueous
TDS
SM 2540C-
210
mg/L
41
013
MW-14D
Aqueous
Barium
6020B
8.0
ug/L
43
013
MW-14D
Aqueous
Iron
6020B
240
B
ug/L
43
013
MW-14D
Aqueous
Lead
6020B
0.39
J
ug/L
43
013
MW-14D
Aqueous
Manganese
6020B
31
ug/L
43
013
MW-14D
Aqueous
Zinc
6020B
8.8
J
ug/L
43
014
MW-14
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
65
mg CaCO3/1-
44
014
MW-14
Aqueous
Chloride
9056A
2.5
mg/L
44
014
MW-14
Aqueous
Sulfate
9056A
21
mg/L
44
014
MW-14
Aqueous
TDS
SM 2540C-
140
mg/L
44
014
MW-14
Aqueous
Barium
6020B
50
ug/L
46
014
MW-14
Aqueous
Iron
6020B
150
B
ug/L
46
014
MW-14
Aqueous
Manganese
6020B
4.0
J
ug/L
46
014
MW-14
Aqueous
Nickel
6020B
2.8
J
ug/L
46
015
MW-12D
Aqueous
Alkalinity @ pH 4.5 su
SM 232013-
170
mg CaCO3/1-
47
015
MW-12D
Aqueous
Chloride
9056A
12
mg/L
47
015
MW-12D
Aqueous
Sulfate
9056A
66
mg/L
47
015
MW-12D
Aqueous
TDS
SM 2540C-
290
mg/L
47
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 149

Detection Summary (Continued)
Lot Number: WJ30017
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
015
MW-12D
Aqueous
1,4-Dioxane
8260D (SIM)
1.9
J
ug/L
47
015
MW-12D
Aqueous
Barium
6020B
63
ug/L
49
015
MW-12D
Aqueous
Cobalt
6020B
2.1
J
ug/L
49
015
MW-12D
Aqueous
Iron
6020B
290
B
ug/L
49
015
MW-12D
Aqueous
Manganese
6020B
470
ug/L
49
015
MW-12D
Aqueous
Nickel
6020B
3.6
J
ug/L
49
016
MW-12
Aqueous
Alkalinity @ pH 4.5 su
SM 2320B-
240
mg CaCO3/1-
50
016
MW-12
Aqueous
Chloride
9056A
38
mg/L
50
016
MW-12
Aqueous
Sulfate
9056A
290
mg/L
50
016
MW-12
Aqueous
TDS
SM 2540C-
680
mg/L
50
016
MW-12
Aqueous
1,4-Dioxane
8260D (SIM)
2.8
J
ug/L
50
016
MW-12
Aqueous
Acetone
8260D
8.1
JL
ug/L
50
016
MW-12
Aqueous
Tetrahydrofuran
8260D
3.4
J
ug/L
51
016
MW-12
Aqueous
Mercury
7470A
0.00023
mg/L
52
016
MW-12
Aqueous
Barium
6020B
110
ug/L
52
016
MW-12
Aqueous
Cadmium
6020B
0.40
J
ug/L
52
016
MW-12
Aqueous
Chromium
6020B
1.5
J
ug/L
52
016
MW-12
Aqueous
Cobalt
6020B
29
ug/L
52
016
MW-12
Aqueous
Copper
6020B
19
ug/L
52
016
MW-12
Aqueous
Iron
6020B
130
B
ug/L
52
016
MW-12
Aqueous
Manganese
6020B
2500
ug/L
52
016
MW-12
Aqueous
Nickel
6020B
34
ug/L
52
016
MW-12
Aqueous
Zinc
6020B
6.4
J
ug/L
52
017
MW-13D
Aqueous
Barium
6020B
230
ug/L
54
017
MW-13D
Aqueous
Cobalt
6020B
21
ug/L
54
017
MW-13D
Aqueous
Nickel
6020B
9.6
ug/L
54
018
MW-13
Aqueous
Barium
6020B
200
ug/L
56
018
MW-13
Aqueous
Cobalt
6020B
26
ug/L
56
018
MW-13
Aqueous
Lead
6020B
0.26
J
ug/L
56
018
MW-13
Aqueous
Nickel
6020B
6.3
ug/L
56
018
MW-13
Aqueous
Zinc
6020B
9.8
J
ug/L
56
019
MW-8
Aqueous
Antimony
6020B
1.6
J
ug/L
58
019
MW-8
Aqueous
Barium
6020B
140
ug/L
58
019
MW-8
Aqueous
Chromium
6020B
2.7
J
ug/L
58
019
MW-8
Aqueous
Copper
6020B
1.7
J
ug/L
58
019
MW-8
Aqueous
Lead
6020B
0.26
J
ug/L
58
019
MW-8
Aqueous
Nickel
6020B
3.1
J
ug/L
58
019
MW-8
Aqueous
Zinc
6020B
16
ug/L
58
020
MW-81D.
Aqueous
Barium
6020B
170
ug/L
60
020
MW-81D.
Aqueous
Chromium
6020B
1.4
J
ug/L
60
020
MW-81D.
Aqueous
Nickel
6020B
4.3
J
ug/L
60
020
MW-81D.
Aqueous
Zinc
6020B
4.7
J
ug/L
60
021
MW-10
Aqueous
Xylenes (total)
8260D
0.51
J
ug/L
62
021
MW-10
Aqueous
Barium
6020B
140
ug/L
62
021
MW-10
Aqueous
Chromium
6020B
3.9
J
ug/L
62
021
MW-10
Aqueous
Cobalt
6020B
3.3
J
ug/L
62
021
MW-10
Aqueous
Nickel
6020B
11
ug/L
62
021
MW-10
Aqueous
Vanadium
6020B
2.6
J
ug/L
63
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 149

Detection Summary (Continued)
Lot Number: WJ30017
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
021
MW-10
Aqueous
Zinc
6020B
4.6
J
ug/L
63
022
MW-1OD
Aqueous
1, 1 -Dichloroethane
8260D
0.84
J
ug/L
64
022
MW-10D
Aqueous
cis- 1,2-Dichloroethene
8260D
0.47
J
ug/L
64
022
MW-1OD
Aqueous
Barium
6020B
30
ug/L
65
022
MW-1OD
Aqueous
Chromium
6020B
3.8
J
ug/L
65
022
MW-1OD
Aqueous
Nickel
6020B
12
ug/L
65
023
MW-3R
Aqueous
Barium
6020B
64
ug/L
68
023
MW-3R
Aqueous
Chromium
6020B
3.0
J
ug/L
68
023
MW-3R
Aqueous
Nickel
6020B
3.1
J
ug/L
68
023
MW-3R
Aqueous
Vanadium
6020B
4.3
J
ug/L
68
023
MW-3R
Aqueous
Zinc
6020B
5.9
J
ug/L
68
024
MW-7
Aqueous
Barium
6020B
180
ug/L
70
024
MW-7
Aqueous
Chromium
6020B
2.7
J
ug/L
70
024
MW-7
Aqueous
Cobalt
6020B
1.8
J
ug/L
70
024
MW-7
Aqueous
Nickel
6020B
15
ug/L
70
024
MW-7
Aqueous
Zinc
6020B
3.7
J
ug/L
70
025
MW-51D
Aqueous
Barium
6020B
74
ug/L
72
025
MW-51D
Aqueous
Chromium
6020B
5.3
ug/L
72
025
MW-51D
Aqueous
Nickel
6020B
5.5
ug/L
72
025
MW-51D
Aqueous
Zinc
6020B
2.9
J
ug/L
72
026
MW-5
Aqueous
Barium
6020B
130
ug/L
74
026
MW-5
Aqueous
Chromium
6020B
5.7
ug/L
74
026
MW-5
Aqueous
Lead
6020B
0.33
J
ug/L
74
026
MW-5
Aqueous
Nickel
6020B
8.7
ug/L
74
026
MW-5
Aqueous
Vanadium
6020B
2.8
J
ug/L
74
026
MW-5
Aqueous
Zinc
6020B
5.1
BJ
ug/L
74
027
MW-6
Aqueous
Barium
6020B
50
ug/L
76
027
MW-6
Aqueous
Zinc
6020B
3.0
BJ
ug/L
76
(169 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-001
Description: MW-17R Matrix: Aqueous
Date Sampled:10/27/2021 1025
Date Received:10/29/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 11/07/2021 0421 AAB
21752
1
(Chloride) 9056A
1 11/02/2021 1640 AMR
21118
1
(Sulfate) 9056A
1 11/02/2021 1640 AMR
21115
1
(TDS) SM 2540C-2011
1 11/02/2021 1916 MOM
21024
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
79
20
20
mg CaCO3/L
1
Chloride
9056A
3.2
1.0
0.25
mg/L
1
Sulfate
9056A
33
1.0
0.25
mg/L
1
TDS
SM 254OC-2011
150
25
25
mg/L
1
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM)
1 11/03/2021 0245 JWO
21040
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
81 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
1 11/09/20211809 CAW
21793
2 5030B
8260D
1 11/12/20211224 CAW
22328
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl
bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl
chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-001
Description: MW-17R Matrix: Aqueous
Date Sampled:10/27/2021 1025
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/20211809 CAW 21793
2 5030B 8260D 1 11/12/20211224 CAW 22328
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Tetrahydrofuran
109-99-9
8260D
ND
5.0
1.0
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND H
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-001
Description: MW-17R Matrix: Aqueous
Date Sampled:10/27/2021 1025
Date Received:10/29/2021
Run 1 Acceptance Run 2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery
Limits
Bromofluorobenzene
93 70-130 H 101
70-130
1,2-Dichloroethane-d4
114 70-130 H 106 70-130
Toluene-d8
104 70-130 H 98
70-130
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/09/2021 1550 CMS2
11/08/2021 1655
21630
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7470A
ND 0.00020
0.000091
mg/L
1
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/04/2021 1023 BNW
11/02/2021 0357
20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
64
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
7.0
5.0
1.3
ug/L
1
Iron
7439-89-6 6020B
290
50
13
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Manganese
7439-96-5 6020B
55
5.0
1.3
ug/L
1
Nickel
7440-02-0 6020B
22
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
9.0 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-002
Description: MW-17DR Matrix: Aqueous
Date Sampled:10/27/2021 0955
Date Received:10/29/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 11/07/2021 0427 AAB
21752
1
(Chloride) 9056A
1 11/02/2021 1659 AMR
21118
1
(Sulfate) 9056A
1 11/02/2021 1659 AMR
21115
1
(TDS) SM 2540C-2011
1 11/02/2021 1916 MOM
21024
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
120
20
20
mg CaCO3/L
1
Chloride
9056A
3.9
1.0
0.25
mg/L
1
Sulfate
9056A
25
1.0
0.25
mg/L
1
TDS
SM 254OC-2011
190
25
25
mg/L
1
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM)
1 11/03/2021 0309 JWO
21040
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
81 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
1 11/09/20211833 CAW
21793
2 5030B
8260D
1 11/12/20211247 CAW
22328
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl
bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl
chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-002
Description: MW-17DR Matrix: Aqueous
Date Sampled:10/27/2021 0955
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/20211833 CAW 21793
2 5030B 8260D 1 11/12/20211247 CAW 22328
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Tetrahydrofuran
109-99-9
8260D
ND
5.0
1.0
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND H
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-002
Description: MW-17DR Matrix: Aqueous
Date Sampled:10/27/2021 0955
Date Received:10/29/2021
Run 1 Acceptance Run 2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery
Limits
Bromofluorobenzene
92 70-130 H 102 70-130
1,2-Dichloroethane-d4
115 70-130 H 107 70-130
Toluene-d8
105 70-130 H 99
70-130
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/09/2021 1558 CMS2
11/08/2021 1655
21630
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7470A
ND 0.00020
0.000091
mg/L
1
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/02/2021 1847 BNW
11/02/2021 0357
20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
51
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Iron
7439-89-6 6020B
200
50
13
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Manganese
7439-96-5 6020B
8.8
5.0
1.3
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-003
Description: MW-11 Matrix: Aqueous
Date Sampled:10/27/2021 1045
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/20210038 BBW 21870
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-003
Description: MW-11 Matrix: Aqueous
Date Sampled:10/27/2021 1045
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/20210038 BBW
21870
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
92 70-130
1,2-Dichloroethane-d4
114 70-130
Toluene-d8
104 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2021 1822 BNW
11/02/2021 0357 20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
64
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
6.9
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
22
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
8.7 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-004
Description: MW-11D Matrix: Aqueous
Date Sampled:10/27/2021 1045
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/20210304 JWO 21878
2 5030B 8260D 1 11/12/20211310 CAW 22328
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND H
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-004
Description: MW-11D Matrix: Aqueous
Date Sampled:10/27/2021 1045
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/20210304 JWO
21878
2 5030B
8260D 1 11/12/20211310 CAW
22328
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
1,1,1-Trichloroethane
71-55-6 8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance Run 2
Acceptance
Surrogate
Q % Recovery Limits Q % Recovery Limits
Bromofluorobenzene
89 70-130 H 94
70-130
1,2-Dichloroethane-d4
98 70-130 H 104
70-130
Toluene-d8
97 70-130 H 98
70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2021 1829 BNW 11/02/2021 0357
20754
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
64
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-005
Description: MW-4D Matrix: Aqueous
Date Sampled:10/27/2021 1130
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2021 0334 JWO
21040
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
82 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/2021 0329 JWO
21878
2 5030B
8260D 1 11/12/20211334 CAW
22328
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND H
10
2.0
ug/L
2
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-005
Description: MW-4D Matrix: Aqueous
Date Sampled:10/27/2021 1130
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/20210329 JWO 21878
2 5030B 8260D 1 11/12/20211334 CAW 22328
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery Limits
Q % Recovery
Limits
Bromofluorobenzene
92 70-130
H 97
70-130
1,2-Dichloroethane-d4
98 70-130
H 103
70-130
Toluene-d8
99 70-130
H 97
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/02/2021 1831 BNW
11/02/2021 0357 20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
110
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
1.4 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
11
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
3.2 J
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-005
Description: MW-4D Matrix: Aqueous
Date Sampled:10/27/2021 1130
Date Received:10/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2021 1831 BNW
11/02/2021 0357
20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Lead
7439-92-1 6020B
0.46 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
34
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
14
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-006
Description: MW-4 Matrix: Aqueous
Date Sampled:10/27/2021 1200
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2021 0358 JWO
21040
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
81 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/2021 0354 JWO
21878
2 5030B
8260D 1 11/12/20211357 CAW
22328
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND H
10
2.0
ug/L
2
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-006
Description: MW-4 Matrix: Aqueous
Date Sampled:10/27/2021 1200
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/20210354 JWO 21878
2 5030B 8260D 1 11/12/20211357 CAW 22328
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery Limits
Q % Recovery
Limits
Bromofluorobenzene
93 70-130
H 99
70-130
1,2-Dichloroethane-d4
101 70-130
H 104
70-130
Toluene-d8
102 70-130
H 99
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/02/2021 1833 BNW
11/02/2021 0357 20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
40
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
9.6
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-006
Description: MW-4 Matrix: Aqueous
Date Sampled:10/27/2021 1200
Date Received:10/29/2021
ICP-MS Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 11/02/2021 1833 BNW 11/02/2021 0357 20754
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Lead
7439-92-1
Nickel
7440-02-0
Selenium
7782-49-2
Silver
7440-22-4
Thallium
7440-28-0
Vanadium
7440-62-2
Zinc
7440-66-6
6020B
ND
1.0
0.25
ug/L 1
6020B
7.8
5.0
1.3
ug/L 1
6020B
ND
5.0
1.3
ug/L 1
6020B
ND
1.0
0.25
ug/L 1
6020B
ND
0.50
0.15
ug/L 1
6020B
ND
5.0
2.5
ug/L 1
6020B
7.7 J
10
2.5
ug/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 23 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-007
Description: MW-2D Matrix: Aqueous
Date Sampled:10/27/2021 1250
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/20210419 JWO 21878
2 5030B 8260D 1 11/12/20211420 CAW 22328
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND H
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 24 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-007
Description: MW-2D Matrix: Aqueous
Date Sampled:10/27/2021 1250
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/20210419 JWO
21878
2 5030B
8260D 1 11/12/20211420 CAW
22328
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
1,1,1-Trichloroethane
71-55-6 8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance Run 2
Acceptance
Surrogate
Q % Recovery Limits Q % Recovery Limits
Bromofluorobenzene
88 70-130 H 100
70-130
1,2-Dichloroethane-d4
95 70-130 H 106
70-130
Toluene-d8
96 70-130 H 99
70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2021 1835 BNW 11/02/2021 0357
20754
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
48
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
3.2 J
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 25 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-008
Description: MW-2 Matrix: Aqueous
Date Sampled:10/27/2021 1305
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/2021 0443 JWO 21878
2 5030B 8260D 1 12/03/20211125 BWS 24540
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND H
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-008
Description: MW-2 Matrix: Aqueous
Date Sampled:10/27/2021 1305
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/2021 0443 JWO
21878
2 5030B
8260D 1 12/03/20211125 BWS
24540
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
1,1,1-Trichloroethane
71-55-6 8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance Run 2
Acceptance
Surrogate
Q % Recovery Limits Q % Recovery Limits
Bromofluorobenzene
89 70-130 H 94
70-130
1,2-Dichloroethane-d4
99 70-130 H 126
70-130
Toluene-d8
100 70-130 H 106
70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2021 1837 BNW 11/02/2021 0357
20754
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
76
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
5.7
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
2.8 J
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 27 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-009
Description: MW-18 Matrix: Aqueous
Date Sampled:10/27/2021 1640
Date Received:10/29/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 11/07/2021 0433 AAB
21752
1
(Chloride) 9056A
1 11/02/2021 1718 AMR
21118
1
(Sulfate) 9056A
1 11/02/2021 1718 AMR
21115
1
(TDS) SM 2540C-2011
1 11/02/2021 1916 MOM
21024
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
79
20
20
mg CaCO3/L
1
Chloride
9056A
1.7
1.0
0.25
mg/L
1
Sulfate
9056A
30
1.0
0.25
mg/L
1
TDS
SM 254OC-2011
150
25
25
mg/L
1
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM)
1 11/03/2021 0422 JWO
21040
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
81 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
1 11/10/20210508 JWO
21878
2 5030B
8260D
1 12/03/20211150 BWS
24540
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl
bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND H
10
2.0
ug/L
2
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl
chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 28 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-009
Description: MW-18 Matrix: Aqueous
Date Sampled:10/27/2021 1640
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/2021 0508 JWO 21878
2 5030B 8260D 1 12/03/20211150 BWS 24540
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Tetrahydrofuran
109-99-9
8260D
ND
5.0
1.0
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
Vinyl acetate
108-05-4
8260D
ND H
5.0
1.2
ug/L
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-009
Description: MW-18 Matrix: Aqueous
Date Sampled:10/27/2021 1640
Date Received:10/29/2021
Run 1 Acceptance Run 2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery
Limits
Bromofluorobenzene
92 70-130 H 87
70-130
1,2-Dichloroethane-d4
100 70-130 H 123 70-130
Toluene-d8
100 70-130 H 105 70-130
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/09/2021 1601 CMS2
11/08/2021 1655
21630
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7470A
ND 0.00020
0.000091
mg/L
1
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/02/2021 1853 BNW
11/02/2021 0357
20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
12
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
5.4
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
1.4 J
5.0
1.3
ug/L
1
Iron
7439-89-6 6020B
300
50
13
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Manganese
7439-96-5 6020B
24
5.0
1.3
ug/L
1
Nickel
7440-02-0 6020B
3.7 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
3.6 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 30 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-010
Description: Trip Blank Matrix: Aqueous
Date Sampled:10/27/2021
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/2021 0533 JWO 21878
2 5030B 8260D 1 12/03/20211216 BWS 24540
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND H
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Tetrahydrofuran
109-99-9
8260D
ND
5.0
1.0
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 31 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-010
Description: Trip Blank Matrix: Aqueous
Date Sampled:10/27/2021
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/2021 0533 JWO
21878
2 5030B
8260D 1 12/03/20211216 BWS
24540
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Toluene
108-88-3 8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6 8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance Run 2
Acceptance
Surrogate
Q % Recovery Limits Q % Recovery Limits
Bromofluorobenzene
92 70-130 H 91
70-130
1,2-Dichloroethane-d4
101 70-130 H 125
70-130
Toluene-d8
101 70-130 H 108
70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 32 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-011
Description: MW-1D Matrix: Aqueous
Date Sampled:10/26/2021 0925
)ate Received:10/28/2021
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (Alkalinity @) SM 2320B-2011
1 11/07/2021 0439 AAB
21752
1 (Chloride) 9056A
1 11/02/2021 1737 AMR
21118
1 (Sulfate) 9056A
1 11/02/2021 1737 AMR
21115
1 (TDS) SM 2540C-2011
1 11/02/2021 1916 MOM
21024
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
83
20
20
mg CaCO3/L
1
Chloride
9056A
2.5
1.0
0.25
mg/L
1
Sulfate
9056A
41
1.0
0.25
mg/L
1
TDS
SM 254OC-2011
180
25
25
mg/L
1
Volatile Organic Compounds by
GC/MS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 11/09/2021 0245 JWO
21730
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
2.3 J
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of compound exceeded the calibration
range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds
40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 33 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-011
Description: MW-1D Matrix: Aqueous
Date Sampled:10/26/2021 0925
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/2021 0245 JWO 21730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
ND
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
93 70-130
1,2-Dichloroethane-d4
115 70-130
Toluene-d8
104 70-130
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/09/2021 1604 CMS2
11/08/2021 1655 21630
CAS Analytical
Parameter
Number Method
Result Q
LOQ DL
Units Run
Mercury
7439-97-6 7470A
ND
0.00020 0.000091
mg/L 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 34 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-011
Description: MW-1D Matrix: Aqueous
Date Sampled:10/26/2021 0925
Date Received:10/28/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep
Date
Batch
1 3005A
6020B 1 11/05/2021 1302 BNW
11/04/2021
0914
21233
CAS Analytical
Parameter
Number Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
0.66
J
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
31
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Iron
7439-89-6 6020B
160
B
50
13
ug/L
1
Lead
7439-92-1 6020B
0.37
J
1.0
0.25
ug/L
1
Manganese
7439-96-5 6020B
14
5.0
1.3
ug/L
1
Nickel
7440-02-0 6020B
4.5
J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
5.5
J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 35 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-012
Description: MW-1 Matrix: Aqueous
Date Sampled:10/26/2021 1100
)ate Received:10/28/2021
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (Alkalinity @) SM 2320B-2011
1 11/07/2021 0444 AAB
21752
1 (Chloride) 9056A
1 11/02/2021 1834 AMR
21118
1 (Sulfate) 9056A
1 11/02/2021 1834 AMR
21115
1 (TDS) SM 2540C-2011
1 11/02/2021 1916 MOM
21024
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
59
20
20
mg CaCO3/L
1
Chloride
9056A
6.2
1.0
0.25
mg/L
1
Sulfate
9056A
20
1.0
0.25
mg/L
1
TDS
SM 254OC-2011
140
25
25
mg/L
1
Volatile Organic Compounds by
GC/MS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 11/09/2021 0309 JWO
21730
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of compound exceeded the calibration
range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds
40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 36 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-012
Description: MW-1 Matrix: Aqueous
Date Sampled:10/26/2021 1100
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/2021 0309 JWO 21730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
ND
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
91 70-130
1,2-Dichloroethane-d4
114 70-130
Toluene-d8
102 70-130
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/09/2021 1606 CMS2
11/08/2021 1655 21630
CAS Analytical
Parameter
Number Method
Result Q
LOQ DL
Units Run
Mercury
7439-97-6 7470A
ND
0.00020 0.000091
mg/L 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 37 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-012
Description: MW-1 Matrix: Aqueous
Date Sampled:10/26/2021 1100
Date Received:10/28/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep
Date
Batch
1 3005A
6020B 1 11/05/2021 1304 BNW
11/04/2021
0914
21233
CAS Analytical
Parameter
Number Method
Result
Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
140
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
2.3
J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Iron
7439-89-6 6020B
190
B
50
13
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Manganese
7439-96-5 6020B
7.5
5.0
1.3
ug/L
1
Nickel
7440-02-0 6020B
2.7
J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
3.7
J
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
7.5
J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 38 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-013
Description: MW-14D Matrix: Aqueous
Date Sampled:10/26/2021 1205
)ate Received:10/28/2021
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (Alkalinity @) SM 2320B-2011
1 11/07/2021 0450 AAB
21752
1 (Chloride) 9056A
1 11/02/2021 1853 AMR
21118
1 (Sulfate) 9056A
1 11/02/2021 1853 AMR
21115
1 (TDS) SM 2540C-2011
1 11/02/2021 1916 MOM
21024
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
140
20
20
mg CaCO3/L
1
Chloride
9056A
4.1
1.0
0.25
mg/L
1
Sulfate
9056A
31
1.0
0.25
mg/L
1
TDS
SM 254OC-2011
210
25
25
mg/L
1
Volatile Organic Compounds by
GC/MS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 11/09/2021 0333 JWO
21730
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of compound exceeded the calibration
range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds
40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 39 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-013
Description: MW-14D Matrix: Aqueous
Date Sampled:10/26/2021 1205
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/2021 0333 JWO 21730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
ND
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
90 70-130
1,2-Dichloroethane-d4
112 70-130
Toluene-d8
101 70-130
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/09/2021 1609 CMS2
11/08/2021 1655 21630
CAS Analytical
Parameter
Number Method
Result Q
LOQ DL
Units Run
Mercury
7439-97-6 7470A
ND
0.00020 0.000091
mg/L 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 40 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-013
Description: MW-14D Matrix: Aqueous
Date Sampled:10/26/2021 1205
Date Received:10/28/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/05/2021 1306 BNW
11/04/2021 0914
21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
8.0
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Iron
7439-89-6 6020B
240 B
50
13
ug/L
1
Lead
7439-92-1 6020B
0.39 J
1.0
0.25
ug/L
1
Manganese
7439-96-5 6020B
31
5.0
1.3
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
8.8 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 41 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-014
Description: MW-14 Matrix: Aqueous
Date Sampled:10/26/2021 1250
)ate Received:10/28/2021
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (Alkalinity @) SM 2320B-2011
1 11/07/2021 0456 AAB
21752
1 (Chloride) 9056A
1 11/02/2021 1949 AMR
21118
1 (Sulfate) 9056A
1 11/02/2021 1949 AMR
21115
1 (TDS) SM 2540C-2011
1 11/02/2021 1916 MOM
21024
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
65
20
20
mg CaCO3/L
1
Chloride
9056A
2.5
1.0
0.25
mg/L
1
Sulfate
9056A
21
1.0
0.25
mg/L
1
TDS
SM 254OC-2011
140
25
25
mg/L
1
Volatile Organic Compounds by
GC/MS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 11/09/2021 0357 JWO
21730
CAS Analytical
Parameter
Number Method Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of compound exceeded the calibration
range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds
40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 42 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-014
Description: MW-14 Matrix: Aqueous
Date Sampled:10/26/2021 1250
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/2021 0357 JWO 21730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
ND
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
92 70-130
1,2-Dichloroethane-d4
115 70-130
Toluene-d8
105 70-130
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/09/2021 1612 CMS2
11/08/2021 1655 21630
CAS Analytical
Parameter
Number Method
Result Q
LOQ DL
Units Run
Mercury
7439-97-6 7470A
ND
0.00020 0.000091
mg/L 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 43 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-014
Description: MW-14 Matrix: Aqueous
Date Sampled:10/26/2021 1250
Date Received:10/28/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/05/2021 1308 BNW
11/04/2021 0914
21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
50
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Iron
7439-89-6 6020B
150 B
50
13
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Manganese
7439-96-5 6020B
4.0 J
5.0
1.3
ug/L
1
Nickel
7440-02-0 6020B
2.8 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 44 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-015
Description: MW-12D Matrix: Aqueous
Date Sampled:10/26/2021 1340
Date Received:10/28/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 11/07/2021 0502 AAB
21752
1
(Chloride) 9056A
1 11/02/2021 2008 AMR
21118
1
(Sulfate) 9056A
1 11/02/2021 2008 AMR
21115
1
(TDS) SM 2540C-2011
1 11/02/2021 1916 MOM
21024
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
170
20
20
mg CaCO3/L
1
Chloride
9056A
12
1.0
0.25
mg/L
1
Sulfate
9056A
66
1.0
0.25
mg/L
1
TDS
SM 254OC-2011
290
25
25
mg/L
1
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM)
1 11/08/2021 1312 CAW
21673
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
1.9 J
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
85 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
1 11/09/20210421 JWO
21730
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl
bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl
chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 45 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-015
Description: MW-12D Matrix: Aqueous
Date Sampled:10/26/2021 1340
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/20210421 JWO 21730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
ND
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 114 70-130
Toluene-d8 104 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 46 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-015
Description: MW-12D Matrix: Aqueous
Date Sampled:10/26/2021 1340
Date Received:10/28/2021
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/09/2021 1614 CMS2
11/08/2021 1655
21630
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7470A
ND
0.00020
0.000091
mg/L
1
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/05/2021 1310 BNW
11/04/2021 0914 21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
63
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
2.1 J
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Iron
7439-89-6 6020B
290 B
50
13
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Manganese
7439-96-5 6020B
470
5.0
1.3
ug/L
1
Nickel
7440-02-0 6020B
3.6 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 47 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-016
Description: MW-12 Matrix: Aqueous
Date Sampled:10/26/2021 1420
Date Received:10/28/2021
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(Alkalinity @) SM 2320B-2011
1 11/07/2021 0510 AAB
21752
1
(Chloride) 9056A
1 11/02/2021 2027 AMR
21118
2
(Sulfate) 9056A
5 11/03/2021 1855 AMR
21362
1
(TDS) SM 2540C-2011
1 11/02/2021 1916 MOM
21024
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Alkalinity @ pH 4.5 su
SM 2320B-2011
240
20
20
mg CaCO3/L
1
Chloride
9056A
38
1.0
0.25
mg/L
1
Sulfate
9056A
290
5.0
1.3
mg/L
2
TDS
SM 2540C-2011
680
25
25
mg/L
1
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM)
1 11/08/2021 1336 CAW
21673
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
2.8 J
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
85 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
1 11/09/20210445 JWO
21730
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
8.1 JL
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl
bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl
chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 48 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-016
Description: MW-12 Matrix: Aqueous
Date Sampled:10/26/2021 1420
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/2021 0445 JWO 21730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
3.4 J
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene 91 70-130
1,2-Dichloroethane-d4 114 70-130
Toluene-d8 104 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 49 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-016
Description: MW-12 Matrix: Aqueous
Date Sampled:10/26/2021 1420
Date Received:10/28/2021
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
7470A
1 11/09/2021 1622 CMS2
11/08/2021 1655
21630
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7470A 0.00023
0.00020
0.000091
mg/L
1
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/05/2021 1312 BNW
11/04/2021 0914 21233
2 3005A
6020B
5 11/10/2021 1200 BNW
11/04/2021 0914 21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
110
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
0.40 J
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
1.5 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
29
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
19
5.0
1.3
ug/L
1
Iron
7439-89-6 6020B
130 B
50
13
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Manganese
7439-96-5 6020B
2500
25
6.3
ug/L
2
Nickel
7440-02-0 6020B
34
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
6.4 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 50 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-017
Description: MW-13D Matrix: Aqueous
Date Sampled:10/26/2021 1520
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/2021 0509 JWO 21730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 51 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-017
Description: MW-13D Matrix: Aqueous
Date Sampled:10/26/2021 1520
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/09/2021 0509 JWO
21730
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
92 70-130
1,2-Dichloroethane-d4
113 70-130
Toluene-d8
104 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/05/2021 1314 BNW
11/04/2021 0914 21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
230
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
21
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
9.6
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 52 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-018
Description: MW-13 Matrix: Aqueous
Date Sampled:10/26/2021 1550
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/2021 0533 JWO 21730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 53 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-018
Description: MW-13 Matrix: Aqueous
Date Sampled:10/26/2021 1550
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/09/2021 0533 JWO
21730
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
91 70-130
1,2-Dichloroethane-d4
112 70-130
Toluene-d8
104 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/05/2021 1316 BNW
11/04/2021 0914 21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
200
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
26
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.26 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
6.3
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
9.8 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 54 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-019
Description: MW-8 Matrix: Aqueous
Date Sampled:10/26/2021 1645
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/2021 0557 JWO 21730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 55 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-019
Description: MW-8 Matrix: Aqueous
Date Sampled:10/26/2021 1645
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/09/2021 0557 JWO
21730
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
92 70-130
1,2-Dichloroethane-d4
115 70-130
Toluene-d8
103 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/05/2021 1323 BNW
11/04/2021 0914 21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
1.6 J
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
140
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
2.7 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
1.7 J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.26 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
3.1 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
16
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 56 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-020
Description: MW-8D. Matrix: Aqueous
Date Sampled:10/26/2021 1700
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/20210621 JWO 21730
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 57 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-020
Description: MW-8D. Matrix: Aqueous
Date Sampled:10/26/2021 1700
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/09/20210621 JWO
21730
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
92 70-130
1,2-Dichloroethane-d4
114 70-130
Toluene-d8
103 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/05/2021 1325 BNW
11/04/2021 0914 21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
170
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
1.4 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
4.3 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
4.7 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 58 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-021
Description: MW-10 Matrix: Aqueous
Date Sampled:10/28/2021 1010
Date Received:10/30/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/08/2021 1401 CAW
21673
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
88 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/11/20211309 BWS
22207
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND L
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 59 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-021
Description: MW-10 Matrix: Aqueous
Date Sampled:10/28/2021 1010
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211309 BWS 22207
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
0.51 J
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
86 70-130
1,2-Dichloroethane-d4
108 70-130
Toluene-d8
99 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/05/2021 1327 BNW
11/04/2021 0914 21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
140
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
3.9 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
3.3 J
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
11
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 60 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-021
Description: MW-10 Matrix: Aqueous
Date Sampled:10/28/2021 1010
Date Received:10/30/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/05/2021 1327 BNW
11/04/2021 0914
21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
2.6 J
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
4.6 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 61 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-022
Description: MW-10D Matrix: Aqueous
Date Sampled:10/28/2021 1045
Date Received:10/30/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/08/2021 1425 CAW
21673
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
86 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/11/20211335 BWS
22207
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND L
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
0.84 J
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2 8260D
0.47 J
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 62 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-022
Description: MW-10D Matrix: Aqueous
Date Sampled:10/28/2021 1045
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211335 BWS 22207
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
81 70-130
1,2-Dichloroethane-d4
104 70-130
Toluene-d8
112 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/05/2021 1329 BNW
11/04/2021 0914 21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
30
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
3.8 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
12
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 63 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-022
Description: MW-10D Matrix: Aqueous
Date Sampled:10/28/2021 1045
Date Received:10/30/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/05/2021 1329 BNW
11/04/2021 0914
21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 64 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-023
Description: MW-3R Matrix: Aqueous
Date Sampled:10/28/2021 1240
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211400 BWS 22207
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND L
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 65 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-023
Description: MW-3R Matrix: Aqueous
Date Sampled:10/28/2021 1240
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/11/20211400 BWS
22207
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
82 70-130
1,2-Dichloroethane-d4
106 70-130
Toluene-d8
97 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/05/2021 1331 BNW
11/04/2021 0914 21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
64
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
3.0 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
3.1 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
4.3 J
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
5.9 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 66 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-024
Description: MW-7 Matrix: Aqueous
Date Sampled:10/28/2021 1350
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211425 BWS 22207
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND L
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 67 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-024
Description: MW-7 Matrix: Aqueous
Date Sampled:10/28/2021 1350
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/11/20211425 BWS
22207
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
83 70-130
1,2-Dichloroethane-d4
107 70-130
Toluene-d8
98 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/05/2021 1333 BNW
11/04/2021 0914 21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
180
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
2.7 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
1.8 J
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
15
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
3.7 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 68 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-025
Description: MW-5D Matrix: Aqueous
Date Sampled:10/28/2021 1200
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211451 BWS 22207
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND L
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 69 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-025
Description: MW-5D Matrix: Aqueous
Date Sampled:10/28/2021 1200
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/11/20211451 BWS
22207
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
70 70-130
1,2-Dichloroethane-d4
104 70-130
Toluene-d8
96 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/05/2021 1335 BNW
11/04/2021 0914 21233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
74
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
5.3
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
5.5
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
2.9 J
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 70 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-026
Description: MW-5 Matrix: Aqueous
Date Sampled:10/28/2021 1235
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211516 BWS 22207
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND L
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 71 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-026
Description: MW-5 Matrix: Aqueous
Date Sampled:10/28/2021 1235
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/11/20211516 BWS
22207
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
83 70-130
1,2-Dichloroethane-d4
105 70-130
Toluene-d8
96 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/08/2021 1703 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
130
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
5.7
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.33 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
8.7
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
2.8 J
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
5.1 BJ
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 72 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-027
Description: MW-6 Matrix: Aqueous
Date Sampled:10/28/2021 1520
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211541 BWS 22207
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND L
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
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Page 73 of 149

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID: WJ30017-027
Description: MW-6 Matrix: Aqueous
Date Sampled:10/28/2021 1520
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/11/20211541 BWS
22207
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
83 70-130
1,2-Dichloroethane-d4
105 70-130
Toluene-d8
98 70-130
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/08/2021 1705 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
50
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
3.0 BJ
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 74 of 149

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 75 of 149

Inorganic non-metals - MB
Sample ID: WQ21024-001 Matrix: Aqueous
Batch: 21024
Analytical Method: SM 2540C-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
TDS ND 1 25 25 mg/L 11/02/2021 1719
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 76 of 149

Inorganic non-metals - LCS
Sample ID: WQ21024-002 Matrix: Aqueous
Batch: 21024
Analytical Method: SM 2540C-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
TDS 1500 1500 1 101 90-110 11/02/2021 1719
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 77 of 149

Inorganic non-metals - Duplicate
Sample ID: WJ30017-015DU Matrix: Aqueous
Batch: 21024
Analytical Method: SM 2540C-2011
Sample
Amount Result %RPD
Parameter (mg/L) (mg/L) Q Dil % RPD Limit Analysis Date
TDS 290 300 1 3.7 20 11/02/2021 1719
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 78 of 149

Inorganic non-metals - Duplicate
Sample ID: WJ30017-016DU Matrix: Aqueous
Batch: 21024
Analytical Method: SM 2540C-2011
Sample
Amount Result %RPD
Parameter (mg/L) (mg/L) Q Dil % RPD Limit Analysis Date
TDS 680 700 1 2.8 20 11/02/2021 1719
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 79 of 149

Inorganic non-metals - MB
Sample ID: WQ21115-001 Matrix: Aqueous
Batch: 21115
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfate ND 1 1.0 0.25 mg/L 11/02/2021 1544
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 80 of 149

Inorganic non-metals - LCS
Sample ID: WQ21115-002 Matrix: Aqueous
Batch: 21115
Analytical Method: 9056A
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 20 1 102 80-120 11/02/2021 1621
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 81 of 149

Inorganic non-metals - MS
Sample ID: WJ30017-01 1 MS Matrix: Aqueous
Batch: 21115
Analytical Method: 9056A
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 41 10 51 1 95 80-120 11/02/2021 1756
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 82 of 149

Inorganic non-metals - MSD
Sample ID: WJ30017-011MID Matrix: Aqueous
Batch: 21115
Analytical Method: 9056A
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Sulfate 41 10 51 1 98 0.48 80-120 20 11/02/2021 1815
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 83 of 149

Inorganic non-metals - MB
Sample ID: WQ21118-001 Matrix: Aqueous
Batch: 21118
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Chloride ND 1 1.0 0.25 mg/L 11/02/2021 1544
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 84 of 149

Inorganic non-metals - LCS
Sample ID: WQ21118-002 Matrix: Aqueous
Batch: 21118
Analytical Method: 9056A
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 20 21 1 104 80-120 11/02/2021 1621
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 85 of 149

Inorganic non-metals - MS
Sample ID: WJ30017-01 1 MS Matrix: Aqueous
Batch: 21118
Analytical Method: 9056A
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Chloride 2.5 10 13 1 103 80-120 11/02/2021 1756
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 86 of 149

Inorganic non-metals - MSD
Sample ID: WJ30017-011MID Matrix: Aqueous
Batch: 21118
Analytical Method: 9056A
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Chloride 2.5 10 13 1 102 0.29 80-120 20 11/02/2021 1815
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 87 of 149

Inorganic non-metals - MB
Sample ID: WQ21362-001 Matrix: Aqueous
Batch: 21362
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfate ND 1 1.0 0.25 mg/L 11/03/2021 1605
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 88 of 149

Inorganic non-metals - LCS
Sample ID: WQ21362-002 Matrix: Aqueous
Batch: 21362
Analytical Method: 9056A
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 20 1 101 80-120 11 /03/2021 1643
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 89 of 149

Inorganic non-metals - LCS
Sample ID: WQ21752-002 Matrix: Aqueous
Batch: 21752
Analytical Method: SM 2320B-2011
Spike
Amount Result %Rec
Parameter (mg CaCO3/L) (mg CaCO3/L) Q Dil % Rec Limit Analysis Date
Alkalinity @ pH 4.5 su 100 99 1 99 90-110 11/07/2021 0313
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 90 of 149

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: WQ21040-001 Matrix: Aqueous
Batch:21040 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 11/02/2021 1938
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
83 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 91 of 149

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: WQ21040-002 Matrix: Aqueous
Batch:21040 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 49 1 98 70-130 11/02/2021 1831
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
101 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 92 of 149

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: WQ21673-001 Matrix: Aqueous
Batch:21673 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 11/08/2021 1012
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
85 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 93 of 149

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: WQ21673-002 Matrix: Aqueous
Batch:21673 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 53 1 106 70-130 11/08/2021 0907
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
92 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 94 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21730-001 Matrix: Aqueous
Batch: 21730 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/09/2021 0001
Acrylonitrile
ND
1
20
0.80
ug/L
11/09/2021 0001
Benzene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Bromoform
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/09/2021 0001
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/09/2021 0001
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Chloroethane
ND
1
2.0
0.40
ug/L
11/09/2021 0001
Chloroform
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/09/2021 0001
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/09/2021 0001
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/09/2021 0001
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
2-Hexanone
ND
1
10
2.0
ug/L
11/09/2021 0001
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/09/2021 0001
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/09/2021 0001
Methylene chloride
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Styrene
ND
1
1.0
0.41
ug/L
11/09/2021 0001
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Toluene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Trichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 95 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21730-001 Matrix: Aqueous
Batch:21730 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/09/2021 0001
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 93 70-130
1,2-Dichloroethane-d4 113 70-130
Toluene-d8 103 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 96 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21730-002 Matrix: Aqueous
Batch: 21730 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
150
N 1
148
60-140
11/08/2021 1938
Acrylonitrile
100
120
1
121
70-130
11/08/2021 1938
Benzene
50
56
1
111
70-130
11/08/2021 1938
Bromochloromethane
50
53
1
107
70-130
11/08/2021 1938
Bromodichloromethane
50
54
1
109
70-130
11/08/2021 1938
Bromoform
50
52
1
105
70-130
11/08/2021 1938
Bromomethane (Methyl bromide)
50
49
1
98
70-130
11/08/2021 1938
2-Butanone (MEK)
100
120
1
118
70-130
11/08/2021 1938
Carbon disulfide
50
63
1
126
70-130
11/08/2021 1938
Carbon tetrachloride
50
56
1
112
70-130
11/08/2021 1938
Chlorobenzene
50
52
1
104
70-130
11/08/2021 1938
Chloroethane
50
57
1
115
70-130
11/08/2021 1938
Chloroform
50
53
1
107
70-130
11/08/2021 1938
Chloromethane (Methyl chloride)
50
57
1
113
60-140
11/08/2021 1938
1,2-Dibromo-3-chloropropane (DBCP)
50
57
1
114
70-130
11/08/2021 1938
Dibromochloromethane
50
54
1
107
70-130
11/08/2021 1938
1,2-Dibromoethane (EDB)
50
52
1
103
70-130
11/08/2021 1938
Dibromomethane (Methylene bromide)
50
55
1
109
70-130
11/08/2021 1938
trans- 1,4-Dichloro-2-butene
50
56
1
112
70-130
11/08/2021 1938
1,2-Dichlorobenzene
50
52
1
104
70-130
11/08/2021 1938
1,4-Dichlorobenzene
50
50
1
99
70-130
11/08/2021 1938
1,1-Dichloroethane
50
55
1
110
70-130
11/08/2021 1938
1,2-Dichloroethane
50
54
1
109
70-130
11/08/2021 1938
1,1-Dichloroethene
50
61
1
122
70-130
11/08/2021 1938
cis- 1,2-Dichloroethene
50
55
1
111
70-130
11/08/2021 1938
trans- 1,2-Dichloroethene
50
57
1
115
70-130
11/08/2021 1938
1,2-Dichloropropane
50
55
1
109
70-130
11/08/2021 1938
cis- 1,3-Dichloropropene
50
54
1
109
70-130
11/08/2021 1938
trans- 1,3-Dichloropropene
50
55
1
110
70-130
11/08/2021 1938
Ethylbenzene
50
54
1
109
70-130
11/08/2021 1938
2-Hexanone
100
120
1
121
70-130
11/08/2021 1938
Methyl iodide (lodomethane)
50
56
1
112
70-130
11/08/2021 1938
4-Methyl-2-pentanone
100
120
1
119
70-130
11/08/2021 1938
Methylene chloride
50
56
1
112
70-130
11/08/2021 1938
Styrene
50
57
1
113
70-130
11/08/2021 1938
1,1,1,2-Tetrachloroethane
50
54
1
108
70-130
11/08/2021 1938
1,1,2,2-Tetrachloroethane
50
54
1
109
70-130
11/08/2021 1938
Tetrachloroethene
50
52
1
105
70-130
11/08/2021 1938
Toluene
50
55
1
110
70-130
11/08/2021 1938
1,1,1-Trichloroethane
50
55
1
110
70-130
11/08/2021 1938
1,1,2-Trichloroethane
50
52
1
105
70-130
11/08/2021 1938
Trichloroethene
50
50
1
100
70-130
11/08/2021 1938
Trichlorofluoromethane
50
58
1
115
70-130
11/08/2021 1938
1,2,3-Trichloropropane
50
53
1
106
70-130
11/08/2021 1938
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 97 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21730-002
Matrix: Aqueous
Batch:21730
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Vinyl acetate
50
52
1 103
60-140
11/08/2021 1938
Vinyl chloride
50
55
1 110
70-130
11/08/2021 1938
Xylenes (total)
100
110
1 112
70-130
11/08/2021 1938
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 108 70-130
Toluene-d8 105 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 98 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21730-001 Matrix: Aqueous
Batch: 21730 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/09/2021 0001
Acrylonitrile
ND
1
20
0.80
ug/L
11/09/2021 0001
Benzene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Bromoform
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/09/2021 0001
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/09/2021 0001
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Chloroethane
ND
1
2.0
0.40
ug/L
11/09/2021 0001
Chloroform
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/09/2021 0001
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/09/2021 0001
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/09/2021 0001
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
2-Hexanone
ND
1
10
2.0
ug/L
11/09/2021 0001
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/09/2021 0001
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/09/2021 0001
Methylene chloride
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Styrene
ND
1
1.0
0.41
ug/L
11/09/2021 0001
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Tetrahydrofuran
ND
1
5.0
1.0
ug/L
11/09/2021 0001
Toluene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Trichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 99 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21730-001 Matrix: Aqueous
Batch:21730 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/09/2021 0001
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/09/2021 0001
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 93 70-130
1,2-Dichloroethane-d4 113 70-130
Toluene-d8 103 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 100 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21730-002 Matrix: Aqueous
Batch: 21730 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
150
N 1
148
60-140
11/08/2021 1938
Acrylonitrile
100
120
1
121
70-130
11/08/2021 1938
Benzene
50
56
1
111
70-130
11/08/2021 1938
Bromochloromethane
50
53
1
107
70-130
11/08/2021 1938
Bromodichloromethane
50
54
1
109
70-130
11/08/2021 1938
Bromoform
50
52
1
105
70-130
11/08/2021 1938
Bromomethane (Methyl bromide)
50
49
1
98
70-130
11/08/2021 1938
2-Butanone (MEK)
100
120
1
118
70-130
11/08/2021 1938
Carbon disulfide
50
63
1
126
70-130
11/08/2021 1938
Carbon tetrachloride
50
56
1
112
70-130
11/08/2021 1938
Chlorobenzene
50
52
1
104
70-130
11/08/2021 1938
Chloroethane
50
57
1
115
70-130
11/08/2021 1938
Chloroform
50
53
1
107
70-130
11/08/2021 1938
Chloromethane (Methyl chloride)
50
57
1
113
60-140
11/08/2021 1938
1,2-Dibromo-3-chloropropane (DBCP)
50
57
1
114
70-130
11/08/2021 1938
Dibromochloromethane
50
54
1
107
70-130
11/08/2021 1938
1,2-Dibromoethane (EDB)
50
52
1
103
70-130
11/08/2021 1938
Dibromomethane (Methylene bromide)
50
55
1
109
70-130
11/08/2021 1938
trans- 1,4-Dichloro-2-butene
50
56
1
112
70-130
11/08/2021 1938
1,2-Dichlorobenzene
50
52
1
104
70-130
11/08/2021 1938
1,4-Dichlorobenzene
50
50
1
99
70-130
11/08/2021 1938
1,1-Dichloroethane
50
55
1
110
70-130
11/08/2021 1938
1,2-Dichloroethane
50
54
1
109
70-130
11/08/2021 1938
1,1-Dichloroethene
50
61
1
122
70-130
11/08/2021 1938
cis- 1,2-Dichloroethene
50
55
1
111
70-130
11/08/2021 1938
trans- 1,2-Dichloroethene
50
57
1
115
70-130
11/08/2021 1938
1,2-Dichloropropane
50
55
1
109
70-130
11/08/2021 1938
cis- 1,3-Dichloropropene
50
54
1
109
70-130
11/08/2021 1938
trans- 1,3-Dichloropropene
50
55
1
110
70-130
11/08/2021 1938
Ethylbenzene
50
54
1
109
70-130
11/08/2021 1938
2-Hexanone
100
120
1
121
70-130
11/08/2021 1938
Methyl iodide (lodomethane)
50
56
1
112
70-130
11/08/2021 1938
4-Methyl-2-pentanone
100
120
1
119
70-130
11/08/2021 1938
Methylene chloride
50
56
1
112
70-130
11/08/2021 1938
Styrene
50
57
1
113
70-130
11/08/2021 1938
1,1,1,2-Tetrachloroethane
50
54
1
108
70-130
11/08/2021 1938
1,1,2,2-Tetrachloroethane
50
54
1
109
70-130
11/08/2021 1938
Tetrachloroethene
50
52
1
105
70-130
11/08/2021 1938
Tetrahydrofuran
50
61
1
121
70-130
11/08/2021 1938
Toluene
50
55
1
110
70-130
11/08/2021 1938
1,1,1-Trichloroethane
50
55
1
110
70-130
11/08/2021 1938
1,1,2-Trichloroethane
50
52
1
105
70-130
11/08/2021 1938
Trichloroethene
50
50
1
100
70-130
11/08/2021 1938
Trichlorofluoromethane
50
58
1
115
70-130
11/08/2021 1938
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 101 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21730-002
Matrix: Aqueous
Batch:21730
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
1,2,3-Trichloropropane
50
53
1
106
70-130
11/08/2021 1938
Vinyl acetate
50
52
1
103
60-140
11/08/2021 1938
Vinyl chloride
50
55
1
110
70-130
11/08/2021 1938
Xylenes (total)
100
110
1
112
70-130
11/08/2021 1938
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 108 70-130
Toluene-d8 105 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 102 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21793-001 Matrix: Aqueous
Batch: 21793 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/09/2021 1038
Acrylonitrile
ND
1
20
0.80
ug/L
11/09/2021 1038
Benzene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Bromoform
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/09/2021 1038
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/09/2021 1038
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Chloroethane
ND
1
2.0
0.40
ug/L
11/09/2021 1038
Chloroform
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/09/2021 1038
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/09/2021 1038
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/09/2021 1038
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
2-Hexanone
ND
1
10
2.0
ug/L
11/09/2021 1038
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/09/2021 1038
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/09/2021 1038
Methylene chloride
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Styrene
ND
1
1.0
0.41
ug/L
11/09/2021 1038
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Tetrahydrofuran
ND
1
5.0
1.0
ug/L
11/09/2021 1038
Toluene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Trichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 103 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21793-001 Matrix: Aqueous
Batch: 21793 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 112 70-130
Toluene-d8 102 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 104 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21793-002 Matrix: Aqueous
Batch: 21793 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
140
N 1
141
60-140
11/09/2021 0935
Acrylonitrile
100
120
1
119
70-130
11/09/2021 0935
Benzene
50
55
1
110
70-130
11/09/2021 0935
Bromochloromethane
50
53
1
107
70-130
11/09/2021 0935
Bromodichloromethane
50
55
1
109
70-130
11/09/2021 0935
Bromoform
50
53
1
107
70-130
11/09/2021 0935
Bromomethane (Methyl bromide)
50
49
1
98
70-130
11/09/2021 0935
2-Butanone (MEK)
100
120
1
116
70-130
11/09/2021 0935
Carbon disulfide
50
58
1
115
70-130
11/09/2021 0935
Carbon tetrachloride
50
53
1
106
70-130
11/09/2021 0935
Chlorobenzene
50
52
1
104
70-130
11/09/2021 0935
Chloroethane
50
57
1
114
70-130
11/09/2021 0935
Chloroform
50
53
1
106
70-130
11/09/2021 0935
Chloromethane (Methyl chloride)
50
57
1
113
60-140
11/09/2021 0935
1,2-Dibromo-3-chloropropane (DBCP)
50
56
1
111
70-130
11/09/2021 0935
Dibromochloromethane
50
53
1
107
70-130
11/09/2021 0935
1,2-Dibromoethane (EDB)
50
52
1
104
70-130
11/09/2021 0935
Dibromomethane (Methylene bromide)
50
56
1
112
70-130
11/09/2021 0935
trans- 1,4-Dichloro-2-butene
50
56
1
112
70-130
11/09/2021 0935
1,2-Dichlorobenzene
50
52
1
104
70-130
11/09/2021 0935
1,4-Dichlorobenzene
50
50
1
99
70-130
11/09/2021 0935
1,1-Dichloroethane
50
54
1
109
70-130
11/09/2021 0935
1,2-Dichloroethane
50
55
1
110
70-130
11/09/2021 0935
1,1-Dichloroethene
50
56
1
112
70-130
11/09/2021 0935
cis- 1,2-Dichloroethene
50
53
1
107
70-130
11/09/2021 0935
trans- 1,2-Dichloroethene
50
56
1
111
70-130
11/09/2021 0935
1,2-Dichloropropane
50
55
1
109
70-130
11/09/2021 0935
cis- 1,3-Dichloropropene
50
54
1
107
70-130
11/09/2021 0935
trans- 1,3-Dichloropropene
50
54
1
109
70-130
11/09/2021 0935
Ethylbenzene
50
54
1
108
70-130
11/09/2021 0935
2-Hexanone
100
120
1
125
70-130
11/09/2021 0935
Methyl iodide (lodomethane)
50
53
1
106
70-130
11/09/2021 0935
4-Methyl-2-pentanone
100
120
1
119
70-130
11/09/2021 0935
Methylene chloride
50
54
1
108
70-130
11/09/2021 0935
Styrene
50
58
1
115
70-130
11/09/2021 0935
1,1,1,2-Tetrachloroethane
50
55
1
109
70-130
11/09/2021 0935
1,1,2,2-Tetrachloroethane
50
55
1
109
70-130
11/09/2021 0935
Tetrachloroethene
50
51
1
102
70-130
11/09/2021 0935
Tetrahydrofuran
50
61
1
122
70-130
11/09/2021 0935
Toluene
50
55
1
110
70-130
11/09/2021 0935
1,1,1-Trichloroethane
50
53
1
106
70-130
11/09/2021 0935
1,1,2-Trichloroethane
50
53
1
106
70-130
11/09/2021 0935
Trichloroethene
50
49
1
98
70-130
11/09/2021 0935
Trichlorofluoromethane
50
53
1
105
70-130
11/09/2021 0935
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 105 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21793-002
Matrix: Aqueous
Batch: 21793
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
1,2,3-Trichloropropane
50
53
1 106
70-130
11/09/2021 0935
Vinyl chloride
50
52
1 103
70-130
11/09/2021 0935
Xylenes (total)
100
110
1 111
70-130
11/09/2021 0935
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 109 70-130
Toluene-d8 103 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 106 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21870-001 Matrix: Aqueous
Batch: 21870 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/09/2021 2311
Acrylonitrile
ND
1
20
0.80
ug/L
11/09/2021 2311
Benzene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Bromoform
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/09/2021 2311
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/09/2021 2311
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Chloroethane
ND
1
2.0
0.40
ug/L
11/09/2021 2311
Chloroform
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/09/2021 2311
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/09/2021 2311
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/09/2021 2311
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
2-Hexanone
ND
1
10
2.0
ug/L
11/09/2021 2311
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/09/2021 2311
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/09/2021 2311
Methylene chloride
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Styrene
ND
1
1.0
0.41
ug/L
11/09/2021 2311
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Toluene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Trichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 2311
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 107 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21870-001 Matrix: Aqueous
Batch:21870 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/09/2021 2311
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/09/2021 2311
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 111 70-130
Toluene-d8 102 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 108 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21870-002 Matrix: Aqueous
Batch: 21870 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
130
1
132
60-140
11/09/2021 2205
Acrylonitrile
100
120
1
122
70-130
11/09/2021 2205
Benzene
50
54
1
107
70-130
11/09/2021 2205
Bromochloromethane
50
53
1
106
70-130
11/09/2021 2205
Bromodichloromethane
50
54
1
107
70-130
11/09/2021 2205
Bromoform
50
51
1
101
70-130
11/09/2021 2205
Bromomethane (Methyl bromide)
50
47
1
93
70-130
11/09/2021 2205
2-Butanone (MEK)
100
110
1
114
70-130
11/09/2021 2205
Carbon disulfide
50
60
1
120
70-130
11/09/2021 2205
Carbon tetrachloride
50
53
1
105
70-130
11/09/2021 2205
Chlorobenzene
50
50
1
101
70-130
11/09/2021 2205
Chloroethane
50
56
1
113
70-130
11/09/2021 2205
Chloroform
50
53
1
106
70-130
11/09/2021 2205
Chloromethane (Methyl chloride)
50
55
1
111
60-140
11/09/2021 2205
1,2-Dibromo-3-chloropropane (DBCP)
50
55
1
110
70-130
11/09/2021 2205
Dibromochloromethane
50
52
1
104
70-130
11/09/2021 2205
1,2-Dibromoethane (EDB)
50
52
1
103
70-130
11/09/2021 2205
Dibromomethane (Methylene bromide)
50
54
1
109
70-130
11/09/2021 2205
trans- 1,4-Dichloro-2-butene
50
54
1
109
70-130
11/09/2021 2205
1,2-Dichlorobenzene
50
50
1
101
70-130
11/09/2021 2205
1,4-Dichlorobenzene
50
48
1
97
70-130
11/09/2021 2205
1,1-Dichloroethane
50
53
1
107
70-130
11/09/2021 2205
1,2-Dichloroethane
50
54
1
107
70-130
11/09/2021 2205
1,1-Dichloroethene
50
59
1
118
70-130
11/09/2021 2205
cis- 1,2-Dichloroethene
50
54
1
108
70-130
11/09/2021 2205
trans- 1,2-Dichloroethene
50
56
1
111
70-130
11/09/2021 2205
1,2-Dichloropropane
50
53
1
107
70-130
11/09/2021 2205
cis- 1,3-Dichloropropene
50
53
1
106
70-130
11/09/2021 2205
trans- 1,3-Dichloropropene
50
54
1
107
70-130
11/09/2021 2205
Ethylbenzene
50
52
1
104
70-130
11/09/2021 2205
2-Hexanone
100
120
1
116
70-130
11/09/2021 2205
Methyl iodide (lodomethane)
50
54
1
108
70-130
11/09/2021 2205
4-Methyl-2-pentanone
100
120
1
116
70-130
11/09/2021 2205
Methylene chloride
50
56
1
112
70-130
11/09/2021 2205
Styrene
50
55
1
111
70-130
11/09/2021 2205
1,1,1,2-Tetrachloroethane
50
53
1
105
70-130
11/09/2021 2205
1,1,2,2-Tetrachloroethane
50
52
1
104
70-130
11/09/2021 2205
Tetrachloroethene
50
50
1
99
70-130
11/09/2021 2205
Toluene
50
53
1
107
70-130
11/09/2021 2205
1,1,1-Trichloroethane
50
53
1
107
70-130
11/09/2021 2205
1,1,2-Trichloroethane
50
52
1
105
70-130
11/09/2021 2205
Trichloroethene
50
48
1
96
70-130
11/09/2021 2205
Trichlorofluoromethane
50
50
1
100
70-130
11/09/2021 2205
1,2,3-Trichloropropane
50
52
1
104
70-130
11/09/2021 2205
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 109 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21870-002
Matrix: Aqueous
Batch:21870
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Vinyl acetate
50
51
1 102
60-140
11/09/2021 2205
Vinyl chloride
50
51
1 102
70-130
11/09/2021 2205
Xylenes (total)
100
110
1 107
70-130
11/09/2021 2205
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 98 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 100 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 110 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21878-001 Matrix: Aqueous
Batch: 21878 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/09/2021 2245
Acrylonitrile
ND
1
20
0.80
ug/L
11/09/2021 2245
Benzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromoform
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/09/2021 2245
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chloroethane
ND
1
2.0
0.40
ug/L
11/09/2021 2245
Chloroform
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/09/2021 2245
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/09/2021 2245
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
2-Hexanone
ND
1
10
2.0
ug/L
11/09/2021 2245
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/09/2021 2245
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/09/2021 2245
Methylene chloride
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Styrene
ND
1
1.0
0.41
ug/L
11/09/2021 2245
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Toluene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Trichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/09/2021 2245
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 111 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21878-001 Matrix: Aqueous
Batch:21878 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
Xylenes (total) ND 1 1.0 0.40 ug/L 11/09/2021 2245
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 90 70-130
1,2-Dichloroethane-d4 97 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 112 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21878-002 Matrix: Aqueous
Batch: 21878 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
78
1
78
60-140
11/09/2021 2141
Acrylonitrile
100
86
1
86
70-130
11/09/2021 2141
Benzene
50
46
1
93
70-130
11/09/2021 2141
Bromochloromethane
50
45
1
90
70-130
11/09/2021 2141
Bromodichloromethane
50
49
1
97
70-130
11/09/2021 2141
Bromoform
50
54
1
109
70-130
11/09/2021 2141
Bromomethane (Methyl bromide)
50
43
1
87
70-130
11/09/2021 2141
Carbon disulfide
50
50
1
99
70-130
11/09/2021 2141
Carbon tetrachloride
50
47
1
95
70-130
11/09/2021 2141
Chlorobenzene
50
48
1
97
70-130
11/09/2021 2141
Chloroethane
50
42
1
84
70-130
11/09/2021 2141
Chloroform
50
43
1
86
70-130
11/09/2021 2141
Chloromethane (Methyl chloride)
50
38
1
76
60-140
11/09/2021 2141
1,2-Dibromo-3-chloropropane (DBCP)
50
47
1
94
70-130
11/09/2021 2141
Dibromochloromethane
50
51
1
102
70-130
11/09/2021 2141
1,2-Dibromoethane (EDB)
50
50
1
100
70-130
11/09/2021 2141
Dibromomethane (Methylene bromide)
50
46
1
93
70-130
11/09/2021 2141
trans- 1,4-Dichloro-2-butene
50
46
1
91
70-130
11/09/2021 2141
1,2-Dichlorobenzene
50
48
1
96
70-130
11/09/2021 2141
1,4-Dichlorobenzene
50
45
1
90
70-130
11/09/2021 2141
1,1-Dichloroethane
50
43
1
86
70-130
11/09/2021 2141
1,2-Dichloroethane
50
45
1
90
70-130
11/09/2021 2141
1,1-Dichloroethene
50
47
1
93
70-130
11/09/2021 2141
cis- 1,2-Dichloroethene
50
43
1
87
70-130
11/09/2021 2141
trans- 1,2-Dichloroethene
50
43
1
87
70-130
11/09/2021 2141
1,2-Dichloropropane
50
49
1
98
70-130
11/09/2021 2141
cis- 1,3-Dichloropropene
50
54
1
108
70-130
11/09/2021 2141
trans- 1,3-Dichloropropene
50
48
1
96
70-130
11/09/2021 2141
Ethylbenzene
50
49
1
98
70-130
11/09/2021 2141
2-Hexanone
100
100
1
103
70-130
11/09/2021 2141
Methyl iodide (lodomethane)
50
50
1
100
70-130
11/09/2021 2141
4-Methyl-2-pentanone
100
110
1
106
70-130
11/09/2021 2141
Methylene chloride
50
49
1
98
70-130
11/09/2021 2141
Styrene
50
53
1
107
70-130
11/09/2021 2141
1,1,1,2-Tetrachloroethane
50
50
1
99
70-130
11/09/2021 2141
1,1,2,2-Tetrachloroethane
50
45
1
90
70-130
11/09/2021 2141
Tetrachloroethene
50
48
1
96
70-130
11/09/2021 2141
Toluene
50
48
1
96
70-130
11/09/2021 2141
1,1,1-Trichloroethane
50
47
1
95
70-130
11/09/2021 2141
1,1,2-Trichloroethane
50
48
1
95
70-130
11/09/2021 2141
Trichloroethene
50
46
1
91
70-130
11/09/2021 2141
Trichlorofluoromethane
50
49
1
97
70-130
11/09/2021 2141
1,2,3-Trichloropropane
50
46
1
93
70-130
11/09/2021 2141
Vinyl chloride
50
40
1
80
70-130
11/09/2021 2141
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 113 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21878-002
Matrix: Aqueous
Batch:21878
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
Xylenes (total)
100
100
1 102 70-130 11/09/2021 2141
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 91 70-130
1,2-Dichloroethane-d4 86 70-130
Toluene-d8 91 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 114 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21878-001 Matrix: Aqueous
Batch: 21878 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/09/2021 2245
Acrylonitrile
ND
1
20
0.80
ug/L
11/09/2021 2245
Benzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromoform
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/09/2021 2245
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chloroethane
ND
1
2.0
0.40
ug/L
11/09/2021 2245
Chloroform
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/09/2021 2245
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/09/2021 2245
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
2-Hexanone
ND
1
10
2.0
ug/L
11/09/2021 2245
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/09/2021 2245
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/09/2021 2245
Methylene chloride
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Styrene
ND
1
1.0
0.41
ug/L
11/09/2021 2245
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Tetrahydrofuran
ND
1
5.0
1.0
ug/L
11/09/2021 2245
Toluene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Trichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 115 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21878-001 Matrix: Aqueous
Batch:21878 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
Vinyl chloride ND 1 1.0 0.40 ug/L 11/09/2021 2245
Xylenes (total) ND 1 1.0 0.40 ug/L 11/09/2021 2245
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 90 70-130
1,2-Dichloroethane-d4 97 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 116 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21878-002 Matrix: Aqueous
Batch: 21878 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
78
1
78
60-140
11/09/2021 2141
Acrylonitrile
100
86
1
86
70-130
11/09/2021 2141
Benzene
50
46
1
93
70-130
11/09/2021 2141
Bromochloromethane
50
45
1
90
70-130
11/09/2021 2141
Bromodichloromethane
50
49
1
97
70-130
11/09/2021 2141
Bromoform
50
54
1
109
70-130
11/09/2021 2141
Bromomethane (Methyl bromide)
50
43
1
87
70-130
11/09/2021 2141
Carbon disulfide
50
50
1
99
70-130
11/09/2021 2141
Carbon tetrachloride
50
47
1
95
70-130
11/09/2021 2141
Chlorobenzene
50
48
1
97
70-130
11/09/2021 2141
Chloroethane
50
42
1
84
70-130
11/09/2021 2141
Chloroform
50
43
1
86
70-130
11/09/2021 2141
Chloromethane (Methyl chloride)
50
38
1
76
60-140
11/09/2021 2141
1,2-Dibromo-3-chloropropane (DBCP)
50
47
1
94
70-130
11/09/2021 2141
Dibromochloromethane
50
51
1
102
70-130
11/09/2021 2141
1,2-Dibromoethane (EDB)
50
50
1
100
70-130
11/09/2021 2141
Dibromomethane (Methylene bromide)
50
46
1
93
70-130
11/09/2021 2141
trans- 1,4-Dichloro-2-butene
50
46
1
91
70-130
11/09/2021 2141
1,2-Dichlorobenzene
50
48
1
96
70-130
11/09/2021 2141
1,4-Dichlorobenzene
50
45
1
90
70-130
11/09/2021 2141
1,1-Dichloroethane
50
43
1
86
70-130
11/09/2021 2141
1,2-Dichloroethane
50
45
1
90
70-130
11/09/2021 2141
1,1-Dichloroethene
50
47
1
93
70-130
11/09/2021 2141
cis- 1,2-Dichloroethene
50
43
1
87
70-130
11/09/2021 2141
trans- 1,2-Dichloroethene
50
43
1
87
70-130
11/09/2021 2141
1,2-Dichloropropane
50
49
1
98
70-130
11/09/2021 2141
cis- 1,3-Dichloropropene
50
54
1
108
70-130
11/09/2021 2141
trans- 1,3-Dichloropropene
50
48
1
96
70-130
11/09/2021 2141
Ethylbenzene
50
49
1
98
70-130
11/09/2021 2141
2-Hexanone
100
100
1
103
70-130
11/09/2021 2141
Methyl iodide (lodomethane)
50
50
1
100
70-130
11/09/2021 2141
4-Methyl-2-pentanone
100
110
1
106
70-130
11/09/2021 2141
Methylene chloride
50
49
1
98
70-130
11/09/2021 2141
Styrene
50
53
1
107
70-130
11/09/2021 2141
1,1,1,2-Tetrachloroethane
50
50
1
99
70-130
11/09/2021 2141
1,1,2,2-Tetrachloroethane
50
45
1
90
70-130
11/09/2021 2141
Tetrachloroethene
50
48
1
96
70-130
11/09/2021 2141
Tetrahydrofuran
50
44
1
88
70-130
11/09/2021 2141
Toluene
50
48
1
96
70-130
11/09/2021 2141
1,1,1-Trichloroethane
50
47
1
95
70-130
11/09/2021 2141
1,1,2-Trichloroethane
50
48
1
95
70-130
11/09/2021 2141
Trichloroethene
50
46
1
91
70-130
11/09/2021 2141
Trichlorofluoromethane
50
49
1
97
70-130
11/09/2021 2141
1,2,3-Trichloropropane
50
46
1
93
70-130
11/09/2021 2141
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 117 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21878-002
Matrix: Aqueous
Batch:21878
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit Analysis Date
Vinyl chloride
50
40
1 80
70-130 11/09/2021 2141
Xylenes (total)
100
100
1 102
70-130 11/09/2021 2141
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 91 70-130
1,2-Dichloroethane-d4 86 70-130
Toluene-d8 91 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 118 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ22207-001 Matrix: Aqueous
Batch: 22207 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/11/2021 1006
Acrylonitrile
ND
1
20
0.80
ug/L
11/11/2021 1006
Benzene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Bromoform
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/11/2021 1006
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/11/2021 1006
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Chloroethane
ND
1
2.0
0.40
ug/L
11/11/2021 1006
Chloroform
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/11/2021 1006
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/11/2021 1006
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/11/2021 1006
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
2-Hexanone
ND
1
10
2.0
ug/L
11/11/2021 1006
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/11/2021 1006
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/11/2021 1006
Methylene chloride
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Styrene
ND
1
1.0
0.41
ug/L
11/11/2021 1006
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Toluene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Trichloroethene
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/11/2021 1006
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 119 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ22207-001 Matrix: Aqueous
Batch:22207 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/11/2021 1006
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/11/2021 1006
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 87 70-130
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 91 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 120 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ22207-002 Matrix: Aqueous
Batch: 22207 Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
140
1
136
60-140
11/11/2021 0902
Acrylonitrile
100
93
1
93
70-130
11/11/2021 0902
Benzene
50
49
1
99
70-130
11/11/2021 0902
Bromochloromethane
50
46
1
93
70-130
11/11/2021 0902
Bromodichloromethane
50
44
1
89
70-130
11/11/2021 0902
Bromoform
50
50
1
99
70-130
11/11/2021 0902
Bromomethane (Methyl bromide)
50
48
1
96
70-130
11/11/2021 0902
2-Butanone (MEK)
100
140
N 1
136
70-130
11/11/2021 0902
Carbon disulfide
50
46
1
93
70-130
11/11/2021 0902
Carbon tetrachloride
50
45
1
90
70-130
11/11/2021 0902
Chlorobenzene
50
48
1
97
70-130
11/11/2021 0902
Chloroethane
50
50
1
101
70-130
11/11/2021 0902
Chloroform
50
52
1
104
70-130
11/11/2021 0902
Chloromethane (Methyl chloride)
50
49
1
99
60-140
11/11/2021 0902
1,2-Dibromo-3-chloropropane (DBCP)
50
44
1
87
70-130
11/11/2021 0902
Dibromochloromethane
50
49
1
97
70-130
11/11/2021 0902
1,2-Dibromoethane (EDB)
50
50
1
100
70-130
11/11/2021 0902
Dibromomethane (Methylene bromide)
50
45
1
91
70-130
11/11/2021 0902
trans- 1,4-Dichloro-2-butene
50
48
1
96
70-130
11/11/2021 0902
1,2-Dichlorobenzene
50
47
1
94
70-130
11/11/2021 0902
1,4-Dichlorobenzene
50
46
1
92
70-130
11/11/2021 0902
1,1-Dichloroethane
50
45
1
89
70-130
11/11/2021 0902
1,2-Dichloroethane
50
46
1
92
70-130
11/11/2021 0902
1,1-Dichloroethene
50
49
1
97
70-130
11/11/2021 0902
cis- 1,2-Dichloroethene
50
49
1
97
70-130
11/11/2021 0902
trans- 1,2-Dichloroethene
50
46
1
93
70-130
11/11/2021 0902
1,2-Dichloropropane
50
44
1
89
70-130
11/11/2021 0902
cis- 1,3-Dichloropropene
50
50
1
101
70-130
11/11/2021 0902
trans- 1,3-Dichloropropene
50
50
1
100
70-130
11/11/2021 0902
Ethylbenzene
50
53
1
105
70-130
11/11/2021 0902
2-Hexanone
100
95
1
95
70-130
11/11/2021 0902
Methyl iodide (lodomethane)
50
51
1
102
70-130
11/11/2021 0902
4-Methyl-2-pentanone
100
93
1
93
70-130
11/11/2021 0902
Methylene chloride
50
47
1
93
70-130
11/11/2021 0902
Styrene
50
49
1
98
70-130
11/11/2021 0902
1,1,1,2-Tetrachloroethane
50
48
1
96
70-130
11/11/2021 0902
1,1,2,2-Tetrachloroethane
50
50
1
100
70-130
11/11/2021 0902
Tetrachloroethene
50
50
1
100
70-130
11/11/2021 0902
Toluene
50
53
1
106
70-130
11/11/2021 0902
1,1,1-Trichloroethane
50
47
1
93
70-130
11/11/2021 0902
1,1,2-Trichloroethane
50
47
1
94
70-130
11/11/2021 0902
Trichloroethene
50
46
1
93
70-130
11/11/2021 0902
Trichlorofluoromethane
50
45
1
89
70-130
11/11/2021 0902
1,2,3-Trichloropropane
50
47
1
93
70-130
11/11/2021 0902
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 121 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ22207-002
Matrix: Aqueous
Batch:22207
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Vinyl acetate
50
48
1 96
60-140
11/11/2021 0902
Vinyl chloride
50
47
1 94
70-130
11/11/2021 0902
Xylenes (total)
100
94
1 94
70-130
11/11/2021 0902
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 92 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 122 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ22328-001 Matrix: Aqueous
Batch:22328 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
2-Butanone (MEK) ND 1 10 2.0 ug/L 11/12/2021 1055
Vinyl acetate ND 1 5.0 1.2 ug/L 11/12/2021 1055
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 98 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 123 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ22328-002
Matrix: Aqueous
Batch:22328
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit Analysis Date
2-Butanone (MEK)
100
110
1 109
70-130 11/12/2021 0953
Vinyl acetate
50
46
1 92
60-140 11/12/2021 0953
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 95 70-130
Toluene-d8 88 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 124 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ22328-001 Matrix: Aqueous
Batch:22328 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
Vinyl acetate ND 1 5.0 1.2 ug/L 11/12/2021 1055
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 98 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 125 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ22328-002
Matrix: Aqueous
Batch:22328
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
Vinyl acetate
50
46
1 92 60-140 11/12/2021 0953
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 95 70-130
Toluene-d8 88 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 126 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ24540-001 Matrix: Aqueous
Batch:24540 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
2-Butanone (MEK) ND 1 10 2.0 ug/L 12/03/2021 1027
Vinyl acetate ND 1 5.0 1.2 ug/L 12/03/2021 1027
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 123 70-130
Toluene-d8 107 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 127 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ24540-002
Matrix: Aqueous
Batch:24540
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit Analysis Date
2-Butanone (MEK)
100
120
1 119
70-130 12/03/2021 0923
Vinyl acetate
50
53
1 105
60-140 12/03/2021 0923
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 128 of 149

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ24540-001 Matrix: Aqueous
Batch:24540 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
2-Butanone (MEK) ND 1 10 2.0 ug/L 12/03/2021 1027
Vinyl acetate ND 1 5.0 1.2 ug/L 12/03/2021 1027
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 123 70-130
Toluene-d8 107 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 129 of 149

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ24540-002
Matrix: Aqueous
Batch:24540
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit Analysis Date
2-Butanone (MEK)
100
120
1 119
70-130 12/03/2021 0923
Vinyl acetate
50
53
1 105
60-140 12/03/2021 0923
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 130 of 149

ICP-MS Metals - MB
Sample ID: WQ20754-001 Matrix: Aqueous
Batch: 20754 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/02/2021 0357
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
11/02/2021 1749
Arsenic
ND
1
2.0
1.3
ug/L
11/02/2021 1749
Barium
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Beryllium
ND
1
0.40
0.15
ug/L
11/02/2021 1749
Cadmium
ND
1
0.50
0.13
ug/L
11/02/2021 1749
Chromium
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Cobalt
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Copper
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Iron
ND
1
50
13
ug/L
11/02/2021 1749
Lead
ND
1
1.0
0.25
ug/L
11/02/2021 1749
Manganese
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Nickel
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Selenium
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Silver
ND
1
1.0
0.25
ug/L
11/02/2021 1749
Thallium
ND
1
0.50
0.15
ug/L
11/02/2021 1749
Vanadium
ND
1
5.0
2.5
ug/L
11/02/2021 1749
Zinc
ND
1
10
2.5
ug/L
11/02/2021 1749
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 131 of 149

ICP-MS Metals - LCS
Sample ID: WQ20754-002 Matrix: Aqueous
Batch: 20754 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/02/2021 0357
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
100
98
1
98
80-120
11/02/2021 1751
Arsenic
100
100
1
102
80-120
11/02/2021 1751
Barium
100
97
1
97
80-120
11/02/2021 1751
Beryllium
100
99
1
99
80-120
11/02/2021 1751
Cadmium
100
100
1
101
80-120
11/02/2021 1751
Chromium
100
100
1
104
80-120
11/02/2021 1751
Cobalt
100
100
1
101
80-120
11/02/2021 1751
Copper
100
110
1
107
80-120
11/02/2021 1751
Iron
1000
980
1
98
80-120
11/02/2021 1751
Lead
100
100
1
101
80-120
11/02/2021 1751
Manganese
100
100
1
102
80-120
11/02/2021 1751
Nickel
100
110
1
105
80-120
11/02/2021 1751
Selenium
100
100
1
104
80-120
11/02/2021 1751
Silver
100
96
1
96
80-120
11/02/2021 1751
Thallium
100
96
1
96
80-120
11/02/2021 1751
Vanadium
100
100
1
102
80-120
11/02/2021 1751
Zinc
100
100
1
103
80-120
11/02/2021 1751
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 132 of 149

ICP-MS Metals - MB
Sample ID: WQ21233-001 Matrix: Aqueous
Batch: 21233 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/04/2021 0914
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
11/05/2021 1235
Arsenic
ND
1
2.0
1.3
ug/L
11/05/2021 1235
Barium
ND
1
5.0
1.3
ug/L
11/05/2021 1235
Beryllium
ND
1
0.40
0.15
ug/L
11/05/2021 1235
Cadmium
ND
1
0.50
0.13
ug/L
11/05/2021 1235
Chromium
ND
1
5.0
1.3
ug/L
11/05/2021 1235
Cobalt
ND
1
5.0
1.3
ug/L
11/05/2021 1235
Copper
ND
1
5.0
1.3
ug/L
11/05/2021 1235
Iron
15 J
1
50
13
ug/L
11105/20211235
Lead
ND
1
1.0
0.25
ug/L
11/05/2021 1235
Manganese
ND
1
5.0
1.3
ug/L
11/05/2021 1235
Nickel
ND
1
5.0
1.3
ug/L
11/05/2021 1235
Selenium
ND
1
5.0
1.3
ug/L
11/05/2021 1235
Silver
ND
1
1.0
0.25
ug/L
11/05/2021 1235
Thallium
ND
1
0.50
0.15
ug/L
11/05/2021 1235
Vanadium
ND
1
5.0
2.5
ug/L
11/05/2021 1235
Zinc
ND
1
10
2.5
ug/L
11/05/2021 1235
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 133 of 149

ICP-MS Metals - LCS
Sample ID: WQ21233-002 Matrix: Aqueous
Batch: 21233 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/04/2021 0914
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
100
98
1
98
80-120
11/05/2021 1237
Arsenic
100
100
1
103
80-120
11/05/2021 1237
Barium
100
96
1
96
80-120
11/05/2021 1237
Beryllium
100
110
1
113
80-120
11/05/2021 1237
Cadmium
100
100
1
102
80-120
11/05/2021 1237
Chromium
100
100
1
104
80-120
11/05/2021 1237
Cobalt
100
100
1
102
80-120
11/05/2021 1237
Copper
100
110
1
108
80-120
11/05/2021 1237
Iron
1000
1000
1
101
80-120
11/05/2021 1237
Lead
100
99
1
99
80-120
11/05/2021 1237
Manganese
100
100
1
105
80-120
11/05/2021 1237
Nickel
100
110
1
107
80-120
11/05/2021 1237
Selenium
100
94
1
94
80-120
11/05/2021 1237
Silver
100
98
1
98
80-120
11/05/2021 1237
Thallium
100
97
1
97
80-120
11/05/2021 1237
Vanadium
100
100
1
104
80-120
11/05/2021 1237
Zinc
100
100
1
103
80-120
11/05/2021 1237
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 134 of 149

ICP-MS Metals - MB
Sample ID: WQ21241-001 Matrix: Aqueous
Batch: 21241 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/07/2021 0954
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
11/08/2021 1659
Arsenic
ND
1
2.0
1.3
ug/L
11/08/2021 1659
Barium
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Beryllium
ND
1
0.40
0.15
ug/L
11/08/2021 1659
Cadmium
ND
1
0.50
0.13
ug/L
11/08/2021 1659
Chromium
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Cobalt
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Copper
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Lead
ND
1
1.0
0.25
ug/L
11/08/2021 1659
Nickel
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Selenium
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Silver
ND
1
1.0
0.25
ug/L
11/08/2021 1659
Thallium
ND
1
0.50
0.15
ug/L
11/08/2021 1659
Vanadium
ND
1
5.0
2.5
ug/L
11/08/2021 1659
Zinc
3.2 J
1
10
2.5
ug/L
11/08/2021 1659
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 135 of 149

ICP-MS Metals - LCS
Sample ID: WQ21241-002 Matrix: Aqueous
Batch: 21241 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/07/2021 0954
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
100
97
1
97
80-120
11/08/2021 1701
Arsenic
100
99
1
99
80-120
11/08/2021 1701
Barium
100
93
1
93
80-120
11/08/2021 1701
Beryllium
100
110
1
105
80-120
11/08/2021 1701
Cadmium
100
100
1
100
80-120
11/08/2021 1701
Chromium
100
100
1
101
80-120
11/08/2021 1701
Cobalt
100
99
1
99
80-120
11/08/2021 1701
Copper
100
110
1
106
80-120
11/08/2021 1701
Lead
100
95
1
95
80-120
11/08/2021 1701
Nickel
100
100
1
103
80-120
11/08/2021 1701
Selenium
100
97
1
97
80-120
11/08/2021 1701
Silver
100
97
1
97
80-120
11/08/2021 1701
Thallium
100
93
1
93
80-120
11/08/2021 1701
Vanadium
100
100
1
101
80-120
11/08/2021 1701
Zinc
100
100
1
102
80-120
11/08/2021 1701
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 136 of 149

CVAA -MB
Sample ID: WQ21630-001 Matrix: Aqueous
Batch: 21630 Prep Method:
Analytical Method: 7470A Prep Date: 11/08/2021 1655
Parameter Result Q Dil LOQ DL Units Analysis Date
Mercury ND 1 0.00020 0.000091 mg/L 11/09/2021 1526
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 137 of 149

CVAA - LCS
Sample ID: WQ21630-002 Matrix: Aqueous
Batch: 21630 Prep Method:
Analytical Method: 7470A Prep Date: 11/08/2021 1655
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury 0.0020 0.0020 1 100 80-120 11/09/2021 1529
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 138 of 149

CVAA - MS
Sample ID: WJ30017-001MS Matrix: Aqueous
Batch: 21630 Prep Method:
Analytical Method: 7470A Prep Date: 11/08/2021 1655
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Mercury ND 0.0020 0.0020 1 98 80-120 11/09/2021 1553
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 139 of 149

CVAA - MSD
Sample ID: WJ30017-001MD Matrix: Aqueous
Batch: 21630 Prep Method:
Analytical Method: 7470A Prep Date: 11/08/2021 1655
Sample Spike
Amount Amount Result %Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Mercury ND 0.0020 0.0020 1 101 3.1 80-120 20 11/09/2021 1556
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 140 of 149

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 141 of 149

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Sant/ $ Receipt Checklist (SBc) (ME0131ac-15) ltevised=9 29f FOCI]
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LdNA 1 If tC1KPL;uL.Ire. a11,V C:LPQJ4% c)ceed01 4.0°C, vas P jert Manager ? jt=fled? —
PM yrt'sls Tlntif b.-! OW i ME! iI { fh4A-tc4'pCfl (ciirle un,).
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✓ Yes
i Nv
10, Did all corttaLmf
label irL implion P. date, dmt) ftgree wilh the {;f1o?
Yes
NQ
11, Were tells to be
[performed Iistc+d on the MC"
17.DYes a
arriv-e in the prop --Fr aMMLIcrw for each test andlor in good core tiai
(unbr4ca, lids on,
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wr Yes
lva
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vol wme zi-y0Ible?
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No
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received wirhin %s t[1Ghold ingtine or49lion rs, whicktcrt`rflames first
Yns I I
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contabters missin 'excess (cimic one) Samples 1hlk t Jis!ed on COC•?
Yes
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-175 mnplaq, were ba:ita[e,s presant?"pr�size" (Velar 5mT1 it dialtt4
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s
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Sant Des. umcive 1 at a H > 12 and suiflde ��mplcs reorived 8L a pH ;;� 9
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s � Jff,�l !{N c}+a��it6a'phennll�i�5_]t502G.3 (< 0 #m 1 s�rm les Fr -
residual altlnr 110
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cdrracrl}r trar.srt;ribed rrum the COC into t'he r�1.wrjerrt. sectinr in LAMS?
� Yrs No 21. Was the taflty -rL ber [[Bred on the cor lairler l I't IY w:s, Quolc 4S�lnnple Prt:aervatEon I�[41i]Mt },� completed any satnp[t{s} i,scon"octJy Jx��'nw�ed nr +�•itlti tteltdspace-)
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in sample »wing wish mL o circle oil = H2SC14. 111403, HC-`I, Na01{ usit],g SR
17mc of psl crvat[an `� tf morn t]tia1 ne a preservative is nm&d, please note in the connrt ri.fi below,
MA
. anpJ°(s) _were retxi wed with k$tPTcs :-6 mrtl it dia3rIL'twr.
Sumples(s;) were rect[ved with TRC > 0.5 _ngA, (If i+19 is Ouy jjr�d j je1e
.lusted aGOordh1gly in sample receivi:tg a ith S iulr'hioa:rlfmo (NF1,5zt"1a) witil Shealy ID: NA
SR hxrocde rijbe[s apprir~d bu 1r4t;2 fate: IDi30"� I
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 144 of 149

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Samples F1QCQipk Checklist IS111C] (MC0018C.15) RevlsEd:9f29/202.0
aAnaii4 al Is5uiug.Au.ncriLy: Pace ENV -1L"CO'_ Page 1 of 1
Sample RcceiPt Checklist (SRC)
Client: xr.F
C'+xFler 1rL n Lud byldatt: .l r; I tlC21242L Le- ; , WJ"'J7 t1Ulli K
lrTeansofroceipl:
Waco Client UPS Fedf Oil -
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I 1. W= clrAodty seals yFJr-scnt on 1:1r, cooler?
ti eaF1No
NA
2. If cusLvdy —15 were. r-�C[, wM ifley intnCt and hlWb. kCI] -
p11 Strip ID: 21452 _ 011u6110 SUip 1D, NA TesCW : JRI-I
original tern Nrrl,rrz upon rcceipt P' Deriver (Corrcmrtcd) teinperaturc upon receipt °lo5rrli { Snap-cilp ID: h:h
3.4 0-4 oC, NA fN.' c+ M1A INA uC NA. iN.A cC —
M.--shod: [ZltcmperatcreBlank 17Ctigabur Bottles 11Z C3un:i3= IR GTI CIOLTectiQ11 fMAM °C
Methtxl of r.(iolant: E Wet ]::u ❑ Ice Packs ❑ D 'cp 0 tdoue —
❑ Ycs C] No ONA 1. Iftempt:lature ofany c fllerexct~ 1t 6 C`ti was Projac: Manage Vot;iied?
- PM was Notified by; phbmc 1 emfil I face-tt�-Facc (Circle Ixne).
d Yw No NA 4. Is the canuucrc W oacricr's paakjrk slip a l.adma Lo this form?
Yca
No
5, Wern P=ustod}• FnK eJu rs {J+�3inquistedlrccaivadj fo[iowccl
Yes
AIo!
6. Wcrc sample 1Ds Iis�ed oti tFie CL)C7
Yes
'O
17. Werc sample IDS Iisuxl ain rril mniple C000-ncrg?
0.7 YC5
fir"
$. Wits WI'Wipll dater & tirno listed an the WU;
© yes
KU
9. Was ceflcctior. date & IilnO IISted Lark rtll-%Lmple mitainem? —
, 'es
Nr
M. T)id,911 conraiiler labrt.] ui€orJrtation (ID, r=atle, Imp) ag= with tt,c C;OU7
J 'es
No
1 ] . 1Y+xc tests to be wrka:m ad listed on the CDC?
J 2. VJ d aA samples arrive in the proNer cxm Wnm fbr ean-h refit and/or ill good Lundi t iep
(urLb-m-im, [ids on. ctc,)',
❑ Yes
❑ Nor
17 Yes
Yes!
Yes
1Na
No
Vj No
II Was ad&LllLxL sample voierne aysilablel
14- Were AJ[ samples deceived w[tiJn V. the Iioldirig Limrt or 4F) ],ours, wbi!c;lever conlex rrst?
15. Were any samplcs containerfi Mi!94ingJ-excess circle Inc) samples NrA listed oil ('0C.?
C Yes
71 No
CKA
16. i'or VDA and tL K-175 sautples, 3vcru buWe3 PfUErli "pea-s;za" ('/�"ur brorn in diameter)
in anv of the VOA 113.157
Yes
No
NA
17. Were al' DROlrnetatsluutri-2nI milples recei tit Fit a pK of <2? -
yea
No
e NA
I& Vk ffe aft cyanido samp: es rmx:ived a` a I > 12 and sl;lfide sample roocivod at a ]-r = 9?
❑-,es
❑No
L,(jVA 1
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❑ Yes ❑Nor ❑ N'20 em cliAlt CL 1 LSl1GR rregUeSt$ (1,ia. regl]estk dd d 1]Iltt4n36 h190,M > 4esi guarloiLs, rtc, , ,)
eorrcri�tlytJrameribed frorn dte COC ijl;u lla: t:umment sectinrt in L[1vf57
Lj Yes J - N rk 21, kVas the Note num b l fisted ar, tlac contsi- label? if -ably g R
Sarrlp1e PLWeJTaliolt i~?v:usc be corrpleted for oily sample(s) [nvwnctly preF;arvcd Or with 'MaEs u,)
3alnp]e(�j) NA — u^ra receiveLi in4UrrECtlj�praser,er[ar,r? were a[li�sicdaccorcirgJy
n �auiple rceaiving with a1L of circle one: 1 l2SCkt, HNO3, H-C.I,' ;j0H using SR ri
L Imc of l]reOCrylltl on NA If mom Than rsne pre.-,e.rvetive iS 1100dvd, pkcx:e n ote i n to comments be!OW
1�'A
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Cominews:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 147 of 149

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CO.Qlcr Jji&pected 13Addle: KDIt A' j I lmno2l Lot g; W11017
M ai uCrc:cipt�
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4, Js the oamn,erc[at cvuricr's pa:kin� �Iip Mas:Jsed 1p this farm?
PYcs
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6, Werr €arrpla: iDs 11s17Ndim 1k- COC?
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Yes Ala
10, Did all Cantrncr label irnt:6rmat[olt CID, dHir., tone) agm with rlre COC',
Yes No
I I . W era tests to be peu'iirnuu;d hstmd on thr. CC}C7
Yes No
12. DU all sainplen arrivc in the �ygper cantaircrs for cash test andfar in gaud rat riditio�
{unh,'olteu, lt{15 on, i:'C.)?
lJ Ye5 LI � Jo 13- W8s adqullt� sari le vr~lume avziiabir?
Ycs No 14. Were a:] samples received within'/ �tC huldi¢L time ar 48 holes, whichever oNyles firat'�
Lj Yes ! Na I5, Were &nysamplescontainers rrii ;:nglexocss �irrleone' Saiapics Not lister on C )C%
Q ve No DNA 16, For VCA and KB&-175 3arrlplca, Were hlrbbles present>"pea„iF "( �"ar Groin In diameter)
in any of the VOA vials?
1`es N❑ l+IA1 17-1�e�e a]I M.Wrre#aJskiwrieat Samples reccivM at a pIt 0r<
Yea R'u J NA I 18. Were all cy.M,ide sarnpJesnCeCivcd at a U'� i and u,]Iida sElnplts reeei�ed at apH 97
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uorrectily, w msoribed from the WC Jnpo the cam niart>arMon in LI`viS?
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were re"NQy Wilt ']'RC > 0.5 m[�L (lf 419 Min) an[f were
ester accordingly in sample r3eivi»1 with sodium #h:osailfale ll 2%) wish Shealy ID: NA
R bwcolie labels applied by: KUK►V
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 149 of 149

0
aceAnalytical
Report of Analysis
Bunnell-Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Attention: Andy Alexander
Project Name: Active Buncombe County Landfill SW
Project Number: 9378-26A
Lot Number:WJ30018
Date Completed:12/07/2021
12/13/2021 11:15 AM
Approved and released by:
Project Manager II: Lucas Odom
pCC/►F�
24r�A
SOA
ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 58

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Bunnell-Lammons Engineering, Inc.
Lot Number: WJ30018
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
VOCs by GUMS
Due to the large number of spiked analytes, there is a high probability that one or more analytes will
recover outside acceptance limits. The laboratory's SOP allows for 10% of analytes to recover marginally
outside criteria. The following analytes recovered marginally outside LCS criteria: Acetone (141 %).
Reanalysis of the following samples was performed outside of the analytical holding time for 2-Butanone
and Vinyl Acetate due to not being detected in the LOQ: WJ30018-001, WJ30018-002, WJ30018-003,
WJ30018-004, WJ30018-005, WJ30018-006.
Metals by ICP-MS
The method blank associated with batch 21241 yielded a "J" value detection for Zinc. No corrective action
is required as this is an estimated value recovered below the LOQ.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] whw.pacelabs.com
Page 2 of 58

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: WJ30018
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
SW-6
Aqueous
10/27/20210920
10/29/2021
002
SW-5
Aqueous
10/27/20210955
10/29/2021
003
SW-2
Aqueous
10/27/20211040
10/29/2021
004
SW-8
Aqueous
10/27/20211155
10/29/2021
005
SW-1
Aqueous
10/27/20211210
10/29/2021
006
SW-4
Aqueous
10/27/20211130
10/29/2021
007
SW-4
Aqueous
10/26/20211600
10/28/2021
008
SW-3
Aqueous
10/26/20211625
10/28/2021
(8 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 58

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: WJ30018
Sample
Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
SW-6
Aqueous
Barium
6020B
100
ug/L
7
002
SW-5
Aqueous
1,4-Dioxane
8260D (SIM)
8.0
ug/L
9
002
SW-5
Aqueous
Tetrahydrofuran
8260D
1.5
J
ug/L
10
002
SW-5
Aqueous
Barium
6020B
190
ug/L
10
002
SW-5
Aqueous
Cobalt
6020B
12
ug/L
10
002
SW-5
Aqueous
Nickel
6020B
24
ug/L
11
002
SW-5
Aqueous
Zinc
6020B
8.6
J
ug/L
11
003
SW-2
Aqueous
Barium
6020B
53
ug/L
13
004
SW-8
Aqueous
Barium
6020B
52
ug/L
16
005
SW-1
Aqueous
Barium
6020B
130
ug/L
19
005
SW-1
Aqueous
Chromium
6020B
1.4
J
ug/L
19
005
SW-1
Aqueous
Cobalt
6020B
5.9
ug/L
19
005
SW-1
Aqueous
Copper
6020B
64
ug/L
19
005
SW-1
Aqueous
Lead
6020B
3.3
ug/L
20
005
SW-1
Aqueous
Vanadium
6020B
3.1
J
ug/L
20
005
SW-1
Aqueous
Zinc
6020B
44
ug/L
20
006
SW-4
Aqueous
Antimony
6020B
1.7
J
ug/L
22
006
SW-4
Aqueous
Barium
6020B
130
ug/L
22
006
SW-4
Aqueous
Chromium
6020B
7.0
ug/L
22
006
SW-4
Aqueous
Cobalt
6020B
5.4
ug/L
22
006
SW-4
Aqueous
Copper
6020B
5.8
ug/L
22
006
SW-4
Aqueous
Lead
6020B
1.3
ug/L
23
006
SW-4
Aqueous
Nickel
6020B
8.0
ug/L
23
006
SW-4
Aqueous
Vanadium
6020B
11
ug/L
23
006
SW-4
Aqueous
Zinc
6020B
19
ug/L
23
008
SW-3
Aqueous
1,4-Dioxane
8260D (SIM)
15
ug/L
24
008
SW-3
Aqueous
Acetone
8260D
9.7
JL
ug/L
24
008
SW-3
Aqueous
Barium
6020B
190
ug/L
25
008
SW-3
Aqueous
Chromium
6020B
2.3
J
ug/L
25
008
SW-3
Aqueous
Cobalt
6020B
7.7
ug/L
25
008
SW-3
Aqueous
Copper
6020B
4.1
J
ug/L
25
008
SW-3
Aqueous
Lead
6020B
0.90
J
ug/L
26
008
SW-3
Aqueous
Nickel
6020B
19
ug/L
26
008
SW-3
Aqueous
Zinc
6020B
13
B
ug/L
26
(34 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-001
Description: SW-6 Matrix: Aqueous
Date Sampled:10/27/2021 0920
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2021 2018 JWO
21225
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
82 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/2021 0557 JWO
21878
2 5030B
8260D 1 12/03/20211241 BWS
24540
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND H
10
2.0
ug/L
2
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-001
Description: SW-6 Matrix: Aqueous
Date Sampled:10/27/2021 0920
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/2021 0557 JWO 21878
2 5030B 8260D 1 12/03/20211241 BWS 24540
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
ND
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery Limits
Q % Recovery
Limits
Bromofluorobenzene
92 70-130
H 89
70-130
1,2-Dichloroethane-d4
103 70-130
H 124
70-130
Toluene-d8
101 70-130
H 107
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11 /02/2021 1839 BN W
11 /02/2021 0357 20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
100
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-001
Description: SW-6 Matrix: Aqueous
Date Sampled:10/27/2021 0920
Date Received:10/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2021 1839 BNW
11/02/2021 0357
20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-002
Description: SW-5 Matrix: Aqueous
Date Sampled:10/27/2021 0955
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2021 2043 JWO
21225
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
8.0
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
82 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/2021 0622 JWO
21878
2 5030B
8260D 1 12/03/20211306 BWS
24540
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND H
10
2.0
ug/L
2
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-002
Description: SW-5 Matrix: Aqueous
Date Sampled:10/27/2021 0955
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/2021 0622 JWO 21878
2 5030B 8260D 1 12/03/20211306 BWS 24540
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
1.5
J
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery Limits
Q % Recovery
Limits
Bromofluorobenzene
90 70-130
H 84
70-130
1,2-Dichloroethane-d4
100 70-130
H 124
70-130
Toluene-d8
99 70-130
H 106
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11 /02/2021 1841 BN W
11 /02/2021 0357 20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
190
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
12
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-002
Description: SW-5 Matrix: Aqueous
Date Sampled:10/27/2021 0955
Date Received:10/29/2021
ICP-MS Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6020B 1 11/02/2021 1841 BNW 11/02/2021 0357 20754
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Copper
7440-50-8
Lead
7439-92-1
Nickel
7440-02-0
Selenium
7782-49-2
Silver
7440-22-4
Thallium
7440-28-0
Vanadium
7440-62-2
Zinc
7440-66-6
6020B
ND
5.0
1.3
ug/L 1
6020B
ND
1.0
0.25
ug/L 1
6020B
24
5.0
1.3
ug/L 1
6020B
ND
5.0
1.3
ug/L 1
6020B
ND
1.0
0.25
ug/L 1
6020B
ND
0.50
0.15
ug/L 1
6020B
ND
5.0
2.5
ug/L 1
6020B
8.6 J
10
2.5
ug/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-003
Description: SW-2 Matrix: Aqueous
Date Sampled:10/27/2021 1040
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2021 2107 JWO
21225
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
83 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/2021 0647 JWO
21878
2 5030B
8260D 1 12/03/20211332 BWS
24540
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND H
10
2.0
ug/L
2
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-003
Description: SW-2 Matrix: Aqueous
Date Sampled:10/27/2021 1040
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/2021 0647 JWO 21878
2 5030B 8260D 1 12/03/20211332 BWS 24540
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery Limits
Q % Recovery
Limits
Bromofluorobenzene
91 70-130
H 85
70-130
1,2-Dichloroethane-d4
105 70-130
H 126
70-130
Toluene-d8
101 70-130
H 106
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/02/2021 1843 BNW
11/02/2021 0357 20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
53
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 58

Client: Bun nell-Lammons Engineering, Inc. Laboratory ID: WJ30018-003
Description: SW-2 Matrix: Aqueous
Date Sampled:10/27/2021 1040
Date Received:10/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/02/2021 1843 BNW
11/02/2021 0357 20754
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOCI = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-004
Description: SW-8 Matrix: Aqueous
Date Sampled:10/27/2021 1155
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2021 2132 JWO
21225
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
85 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/2021 0712 JWO
21878
2 5030B
8260D 1 12/03/20211358 BWS
24540
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND H
10
2.0
ug/L
2
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-004
Description: SW-8 Matrix: Aqueous
Date Sampled:10/27/2021 1155
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/2021 0712 JWO 21878
2 5030B 8260D 1 12/03/20211358 BWS 24540
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Tetrahydrofuran
109-99-9
8260D
ND
5.0
1.0
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery Limits
Q % Recovery
Limits
Bromofluorobenzene
88 70-130
H 87
70-130
1,2-Dichloroethane-d4
99 70-130
H 129
70-130
Toluene-d8
99 70-130
H 105
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11 /03/2021 1806 BN W
11 /02/2021 1210 20753
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
52
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
ND
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-004
Description: SW-8 Matrix: Aqueous
Date Sampled:10/27/2021 1155
Date Received:10/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/03/2021 1806 BNW
11/02/2021 1210
20753
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-005
Description: SW-1 Matrix: Aqueous
Date Sampled:10/27/2021 1210
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2021 2156 JWO
21225
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
84 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/2021 0736 JWO
21878
2 5030B
8260D 1 12/03/20211423 BWS
24540
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND H
10
2.0
ug/L
2
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-005
Description: SW-1 Matrix: Aqueous
Date Sampled:10/27/2021 1210
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/2021 0736 JWO 21878
2 5030B 8260D 1 12/03/20211423 BWS 24540
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery Limits
Q % Recovery
Limits
Bromofluorobenzene
91 70-130
H 89
70-130
1,2-Dichloroethane-d4
100 70-130
H 126
70-130
Toluene-d8
99 70-130
H 107
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/03/2021 1808 BNW
11/02/2021 1210 20753
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
130
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
1.4 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
5.9
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
64
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 58

Client: Bun nell-Lammons Engineering, Inc. Laboratory ID: WJ30018-005
Description: SW-1 Matrix: Aqueous
Date Sampled:10/27/2021 1210
Date Received:10/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/03/2021 1808 BNW
11/02/2021 1210
20753
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Lead
7439-92-1 6020B
3.3
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
ND
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
3.1 J
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
44
10
2.5
ug/L
1
LOCI = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-006
Description: SW-4 Matrix: Aqueous
Date Sampled:10/27/2021 1130
Date Received:10/29/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/03/2021 2221 JWO
21225
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
ND
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
89 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/10/2021 0802 JWO
21878
2 5030B
8260D 1 12/03/20211448 BWS
24540
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND H
10
2.0
ug/L
2
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-006
Description: SW-4 Matrix: Aqueous
Date Sampled:10/27/2021 1130
Date Received:10/29/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/10/2021 0802 JWO 21878
2 5030B 8260D 1 12/03/20211448 BWS 24540
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery Limits
Q % Recovery
Limits
Bromofluorobenzene
93 70-130
H 87
70-130
1,2-Dichloroethane-d4
102 70-130
H 126
70-130
Toluene-d8
104 70-130
H 105
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/03/2021 1814 BNW
11/02/2021 1210 20753
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
1.7 J
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
130
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
7.0
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
5.4
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
5.8
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 58

Client: Bun nell-Lammons Engineering, Inc. Laboratory ID: WJ30018-006
Description: SW-4 Matrix: Aqueous
Date Sampled:10/27/2021 1130
Date Received:10/29/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/03/2021 1814 BNW
11/02/2021 1210
20753
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Lead
7439-92-1 6020B
1.3
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
8.0
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
11
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
19
10
2.5
ug/L
1
LOCI = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-008
Description: SW-3 Matrix: Aqueous
Date Sampled:10/26/2021 1625
Date Received:10/28/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/08/2021 1247 CAW
21673
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
15
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
81 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/09/20211922 CAW
21793
2 5030B
8260D 1 12/03/20211514 BWS
24540
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
9.7 JL
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 23 of 58

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WJ30018-008
Description: SW-3 Matrix: Aqueous
Date Sampled:10/26/2021 1625
Date Received:10/28/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/09/20211922 CAW 21793
2 5030B 8260D 1 12/03/20211514 BWS 24540
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
H
5.0
1.2
ug/L
2
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery Limits
Q % Recovery
Limits
Bromofluorobenzene
91 70-130
H 87
70-130
1,2-Dichloroethane-d4
113 70-130
H 124
70-130
Toluene-d8
104 70-130
H 105
70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/08/2021 1707 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
190
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
1
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
2.3 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
7.7
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
4.1 J
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 24 of 58

Client: Bun nell-Lammons Engineering, Inc. Laboratory ID: WJ30018-008
Description: SW-3 Matrix: Aqueous
Date Sampled:10/26/2021 1625
Date Received:10/28/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B 1 11/08/2021 1707 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Lead
7439-92-1 6020B
0.90 J
1.0
0.25
ug/L
1
Nickel
7440-02-0 6020B
19
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
1
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
13 B
10
2.5
ug/L
1
LOCI = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 25 of 58

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 58

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: WQ21225-001 Matrix: Aqueous
Batch: 21225 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 11/04/2021 0907
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
92 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 27 of 58

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: WQ21225-002 Matrix: Aqueous
Batch: 21225 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 48 1 97 70-130 11/03/2021 1758
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
102 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 28 of 58

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: WQ21673-001 Matrix: Aqueous
Batch: 21673 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 11/08/2021 1012
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
85 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 58

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: WQ21673-002 Matrix: Aqueous
Batch: 21673 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 53 1 106 70-130 11/08/2021 0907
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
92 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 30 of 58

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21793-001 Matrix: Aqueous
Batch: 21793 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/09/2021 1038
Acrylonitrile
ND
1
20
0.80
ug/L
11/09/2021 1038
Benzene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Bromoform
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/09/2021 1038
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/09/2021 1038
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Chloroethane
ND
1
2.0
0.40
ug/L
11/09/2021 1038
Chloroform
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/09/2021 1038
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/09/2021 1038
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/09/2021 1038
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
2-Hexanone
ND
1
10
2.0
ug/L
11/09/2021 1038
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/09/2021 1038
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/09/2021 1038
Methylene chloride
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Styrene
ND
1
1.0
0.41
ug/L
11/09/2021 1038
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Toluene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Trichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 1038
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 1038
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 31 of 58

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21793-001 Matrix: Aqueous
Batch: 21793 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
Vinyl chloride ND 1 1.0 0.40 ug/L 11/09/2021 1038
Xylenes (total) ND 1 1.0 0.40 ug/L 11/09/2021 1038
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 112 70-130
Toluene-d8 102 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 32 of 58

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21793-002
Matrix:
Aqueous
Batch: 21793
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
140
N 1
141
60-140
11/09/2021 0935
Acrylonitrile
100
120
1
119
70-130
11/09/2021 0935
Benzene
50
55
1
110
70-130
11/09/2021 0935
Bromochloromethane
50
53
1
107
70-130
11/09/2021 0935
Bromodichloromethane
50
55
1
109
70-130
11/09/2021 0935
Bromoform
50
53
1
107
70-130
11/09/2021 0935
Bromomethane (Methyl bromide)
50
49
1
98
70-130
11/09/2021 0935
2-Butanone (MEK)
100
120
1
116
70-130
11/09/2021 0935
Carbon disulfide
50
58
1
115
70-130
11/09/2021 0935
Carbon tetrachloride
50
53
1
106
70-130
11/09/2021 0935
Chlorobenzene
50
52
1
104
70-130
11/09/2021 0935
Chloroethane
50
57
1
114
70-130
11/09/2021 0935
Chloroform
50
53
1
106
70-130
11/09/2021 0935
Chloromethane (Methyl chloride)
50
57
1
113
60-140
11/09/2021 0935
1,2-Dibromo-3-chloropropane (DBCP)
50
56
1
111
70-130
11/09/2021 0935
Dibromochloromethane
50
53
1
107
70-130
11/09/2021 0935
1,2-Dibromoethane (EDB)
50
52
1
104
70-130
11/09/2021 0935
Dibromomethane (Methylene bromide)
50
56
1
112
70-130
11/09/2021 0935
trans- 1,4-Dichloro-2-butene
50
56
1
112
70-130
11/09/2021 0935
1,2-Dichlorobenzene
50
52
1
104
70-130
11/09/2021 0935
1,4-Dichlorobenzene
50
50
1
99
70-130
11/09/2021 0935
1,1-Dichloroethane
50
54
1
109
70-130
11/09/2021 0935
1,2-Dichloroethane
50
55
1
110
70-130
11/09/2021 0935
1,1-Dichloroethene
50
56
1
112
70-130
11/09/2021 0935
cis- 1,2-Dichloroethene
50
53
1
107
70-130
11/09/2021 0935
trans- 1,2-Dichloroethene
50
56
1
111
70-130
11/09/2021 0935
1,2-Dichloropropane
50
55
1
109
70-130
11/09/2021 0935
cis- 1,3-Dichloropropene
50
54
1
107
70-130
11/09/2021 0935
trans- 1,3-Dichloropropene
50
54
1
109
70-130
11/09/2021 0935
Ethylbenzene
50
54
1
108
70-130
11/09/2021 0935
2-Hexanone
100
120
1
125
70-130
11/09/2021 0935
Methyl iodide (lodomethane)
50
53
1
106
70-130
11/09/2021 0935
4-Methyl-2-pentanone
100
120
1
119
70-130
11/09/2021 0935
Methylene chloride
50
54
1
108
70-130
11/09/2021 0935
Styrene
50
58
1
115
70-130
11/09/2021 0935
1,1,1,2-Tetrachloroethane
50
55
1
109
70-130
11/09/2021 0935
1,1,2,2-Tetrachloroethane
50
55
1
109
70-130
11/09/2021 0935
Tetrachloroethene
50
51
1
102
70-130
11/09/2021 0935
Toluene
50
55
1
110
70-130
11/09/2021 0935
1,1,1-Trichloroethane
50
53
1
106
70-130
11/09/2021 0935
1,1,2-Trichloroethane
50
53
1
106
70-130
11/09/2021 0935
Trichloroethene
50
49
1
98
70-130
11/09/2021 0935
Trichlorofluoromethane
50
53
1
105
70-130
11/09/2021 0935
1,2,3-Trichloropropane
50
53
1
106
70-130
11/09/2021 0935
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 33 of 58

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21793-002
Matrix:
Aqueous
Batch: 21793
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q Dil
% Rec
Limit Analysis Date
Vinyl chloride
50
52 1
103
70-130 11/09/2021 0935
Xylenes (total)
100
110 1
111
70-130 11/09/2021 0935
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 109 70-130
Toluene-d8 103 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 34 of 58

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21878-001 Matrix: Aqueous
Batch: 21878 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/09/2021 2245
Acrylonitrile
ND
1
20
0.80
ug/L
11/09/2021 2245
Benzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromoform
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/09/2021 2245
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chloroethane
ND
1
2.0
0.40
ug/L
11/09/2021 2245
Chloroform
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/09/2021 2245
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/09/2021 2245
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
2-Hexanone
ND
1
10
2.0
ug/L
11/09/2021 2245
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/09/2021 2245
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/09/2021 2245
Methylene chloride
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Styrene
ND
1
1.0
0.41
ug/L
11/09/2021 2245
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Toluene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Trichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/09/2021 2245
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 35 of 58

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21878-001 Matrix: Aqueous
Batch: 21878 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
Xylenes (total) ND 1 1.0 0.40 ug/L 11/09/2021 2245
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 90 70-130
1,2-Dichloroethane-d4 97 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 36 of 58

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21878-002
Matrix:
Aqueous
Batch: 21878
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
78
1
78
60-140
11/09/2021 2141
Acrylonitrile
100
86
1
86
70-130
11/09/2021 2141
Benzene
50
46
1
93
70-130
11/09/2021 2141
Bromochloromethane
50
45
1
90
70-130
11/09/2021 2141
Bromodichloromethane
50
49
1
97
70-130
11/09/2021 2141
Bromoform
50
54
1
109
70-130
11/09/2021 2141
Bromomethane (Methyl bromide)
50
43
1
87
70-130
11/09/2021 2141
Carbon disulfide
50
50
1
99
70-130
11/09/2021 2141
Carbon tetrachloride
50
47
1
95
70-130
11/09/2021 2141
Chlorobenzene
50
48
1
97
70-130
11/09/2021 2141
Chloroethane
50
42
1
84
70-130
11/09/2021 2141
Chloroform
50
43
1
86
70-130
11/09/2021 2141
Chloromethane (Methyl chloride)
50
38
1
76
60-140
11/09/2021 2141
1,2-Dibromo-3-chloropropane (DBCP)
50
47
1
94
70-130
11/09/2021 2141
Dibromochloromethane
50
51
1
102
70-130
11/09/2021 2141
1,2-Dibromoethane (EDB)
50
50
1
100
70-130
11/09/2021 2141
Dibromomethane (Methylene bromide)
50
46
1
93
70-130
11/09/2021 2141
trans- 1,4-Dichloro-2-butene
50
46
1
91
70-130
11/09/2021 2141
1,2-Dichlorobenzene
50
48
1
96
70-130
11/09/2021 2141
1,4-Dichlorobenzene
50
45
1
90
70-130
11/09/2021 2141
1,1-Dichloroethane
50
43
1
86
70-130
11/09/2021 2141
1,2-Dichloroethane
50
45
1
90
70-130
11/09/2021 2141
1,1-Dichloroethene
50
47
1
93
70-130
11/09/2021 2141
cis- 1,2-Dichloroethene
50
43
1
87
70-130
11/09/2021 2141
trans- 1,2-Dichloroethene
50
43
1
87
70-130
11/09/2021 2141
1,2-Dichloropropane
50
49
1
98
70-130
11/09/2021 2141
cis- 1,3-Dichloropropene
50
54
1
108
70-130
11/09/2021 2141
trans- 1,3-Dichloropropene
50
48
1
96
70-130
11/09/2021 2141
Ethylbenzene
50
49
1
98
70-130
11/09/2021 2141
2-Hexanone
100
100
1
103
70-130
11/09/2021 2141
Methyl iodide (lodomethane)
50
50
1
100
70-130
11/09/2021 2141
4-Methyl-2-pentanone
100
110
1
106
70-130
11/09/2021 2141
Methylene chloride
50
49
1
98
70-130
11/09/2021 2141
Styrene
50
53
1
107
70-130
11/09/2021 2141
1,1,1,2-Tetrachloroethane
50
50
1
99
70-130
11/09/2021 2141
1,1,2,2-Tetrachloroethane
50
45
1
90
70-130
11/09/2021 2141
Tetrachloroethene
50
48
1
96
70-130
11/09/2021 2141
Toluene
50
48
1
96
70-130
11/09/2021 2141
1,1,1-Trichloroethane
50
47
1
95
70-130
11/09/2021 2141
1,1,2-Trichloroethane
50
48
1
95
70-130
11/09/2021 2141
Trichloroethene
50
46
1
91
70-130
11/09/2021 2141
Trichlorofluoromethane
50
49
1
97
70-130
11/09/2021 2141
1,2,3-Trichloropropane
50
46
1
93
70-130
11/09/2021 2141
Vinyl chloride
50
40
1
80
70-130
11/09/2021 2141
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 37 of 58

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21878-002
Matrix:
Aqueous
Batch: 21878
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q Dil
% Rec Limit Analysis Date
Xylenes (total)
100
100 1
102 70-130 11/09/2021 2141
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 91 70-130
1,2-Dichloroethane-d4 86 70-130
Toluene-d8 91 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 38 of 58

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21878-001 Matrix: Aqueous
Batch: 21878 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/09/2021 2245
Acrylonitrile
ND
1
20
0.80
ug/L
11/09/2021 2245
Benzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromoform
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/09/2021 2245
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chloroethane
ND
1
2.0
0.40
ug/L
11/09/2021 2245
Chloroform
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/09/2021 2245
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/09/2021 2245
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
2-Hexanone
ND
1
10
2.0
ug/L
11/09/2021 2245
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/09/2021 2245
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/09/2021 2245
Methylene chloride
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Styrene
ND
1
1.0
0.41
ug/L
11/09/2021 2245
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Tetrahydrofuran
ND
1
5.0
1.0
ug/L
11/09/2021 2245
Toluene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Trichloroethene
ND
1
1.0
0.40
ug/L
11/09/2021 2245
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/09/2021 2245
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 39 of 58

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ21878-001 Matrix: Aqueous
Batch: 21878 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
Vinyl chloride ND 1 1.0 0.40 ug/L 11/09/2021 2245
Xylenes (total) ND 1 1.0 0.40 ug/L 11/09/2021 2245
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 90 70-130
1,2-Dichloroethane-d4 97 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 40 of 58

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21878-002
Matrix:
Aqueous
Batch: 21878
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
78
1
78
60-140
11/09/2021 2141
Acrylonitrile
100
86
1
86
70-130
11/09/2021 2141
Benzene
50
46
1
93
70-130
11/09/2021 2141
Bromochloromethane
50
45
1
90
70-130
11/09/2021 2141
Bromodichloromethane
50
49
1
97
70-130
11/09/2021 2141
Bromoform
50
54
1
109
70-130
11/09/2021 2141
Bromomethane (Methyl bromide)
50
43
1
87
70-130
11/09/2021 2141
Carbon disulfide
50
50
1
99
70-130
11/09/2021 2141
Carbon tetrachloride
50
47
1
95
70-130
11/09/2021 2141
Chlorobenzene
50
48
1
97
70-130
11/09/2021 2141
Chloroethane
50
42
1
84
70-130
11/09/2021 2141
Chloroform
50
43
1
86
70-130
11/09/2021 2141
Chloromethane (Methyl chloride)
50
38
1
76
60-140
11/09/2021 2141
1,2-Dibromo-3-chloropropane (DBCP)
50
47
1
94
70-130
11/09/2021 2141
Dibromochloromethane
50
51
1
102
70-130
11/09/2021 2141
1,2-Dibromoethane (EDB)
50
50
1
100
70-130
11/09/2021 2141
Dibromomethane (Methylene bromide)
50
46
1
93
70-130
11/09/2021 2141
trans- 1,4-Dichloro-2-butene
50
46
1
91
70-130
11/09/2021 2141
1,2-Dichlorobenzene
50
48
1
96
70-130
11/09/2021 2141
1,4-Dichlorobenzene
50
45
1
90
70-130
11/09/2021 2141
1,1-Dichloroethane
50
43
1
86
70-130
11/09/2021 2141
1,2-Dichloroethane
50
45
1
90
70-130
11/09/2021 2141
1,1-Dichloroethene
50
47
1
93
70-130
11/09/2021 2141
cis- 1,2-Dichloroethene
50
43
1
87
70-130
11/09/2021 2141
trans- 1,2-Dichloroethene
50
43
1
87
70-130
11/09/2021 2141
1,2-Dichloropropane
50
49
1
98
70-130
11/09/2021 2141
cis- 1,3-Dichloropropene
50
54
1
108
70-130
11/09/2021 2141
trans- 1,3-Dichloropropene
50
48
1
96
70-130
11/09/2021 2141
Ethylbenzene
50
49
1
98
70-130
11/09/2021 2141
2-Hexanone
100
100
1
103
70-130
11/09/2021 2141
Methyl iodide (lodomethane)
50
50
1
100
70-130
11/09/2021 2141
4-Methyl-2-pentanone
100
110
1
106
70-130
11/09/2021 2141
Methylene chloride
50
49
1
98
70-130
11/09/2021 2141
Styrene
50
53
1
107
70-130
11/09/2021 2141
1,1,1,2-Tetrachloroethane
50
50
1
99
70-130
11/09/2021 2141
1,1,2,2-Tetrachloroethane
50
45
1
90
70-130
11/09/2021 2141
Tetrachloroethene
50
48
1
96
70-130
11/09/2021 2141
Tetrahydrofuran
50
44
1
88
70-130
11/09/2021 2141
Toluene
50
48
1
96
70-130
11/09/2021 2141
1,1,1-Trichloroethane
50
47
1
95
70-130
11/09/2021 2141
1,1,2-Trichloroethane
50
48
1
95
70-130
11/09/2021 2141
Trichloroethene
50
46
1
91
70-130
11/09/2021 2141
Trichlorofluoromethane
50
49
1
97
70-130
11/09/2021 2141
1,2,3-Trichloropropane
50
46
1
93
70-130
11/09/2021 2141
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 41 of 58

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ21878-002
Matrix:
Aqueous
Batch: 21878
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q Dil
% Rec
Limit Analysis Date
Vinyl chloride
50
40 1
80
70-130 11/09/2021 2141
Xylenes (total)
100
100 1
102
70-130 11/09/2021 2141
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 91 70-130
1,2-Dichloroethane-d4 86 70-130
Toluene-d8 91 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 42 of 58

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ24540-001 Matrix: Aqueous
Batch: 24540 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
2-Butanone (MEK) ND 1 10 2.0 ug/L 12/03/2021 1027
Vinyl acetate ND 1 5.0 1.2 ug/L 12/03/2021 1027
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 123 70-130
Toluene-d8 107 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 43 of 58

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ24540-002
Matrix:
Aqueous
Batch: 24540
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q Dil
% Rec
Limit Analysis Date
2-Butanone (MEK)
100
120 1
119
70-130 12/03/2021 0923
Vinyl acetate
50
53 1
105
60-140 12/03/2021 0923
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 44 of 58

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ24540-001 Matrix: Aqueous
Batch: 24540 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
2-Butanone (MEK) ND 1 10 2.0 ug/L 12/03/2021 1027
Vinyl acetate ND 1 5.0 1.2 ug/L 12/03/2021 1027
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 123 70-130
Toluene-d8 107 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 45 of 58

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ24540-002
Matrix:
Aqueous
Batch: 24540
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q Dil
% Rec
Limit Analysis Date
2-Butanone (MEK)
100
120 1
119
70-130 12/03/2021 0923
Vinyl acetate
50
53 1
105
60-140 12/03/2021 0923
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 46 of 58

ICP-MS Metals - MB
Sample ID: WQ20753-001 Matrix: Aqueous
Batch: 20753 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/02/2021 1210
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
11/03/2021 1721
Arsenic
ND
1
2.0
1.3
ug/L
11/03/2021 1721
Barium
ND
1
5.0
1.3
ug/L
11/03/2021 1721
Beryllium
ND
1
0.40
0.15
ug/L
11/03/2021 1721
Cadmium
ND
1
0.50
0.13
ug/L
11/03/2021 1721
Chromium
ND
1
5.0
1.3
ug/L
11/03/2021 1721
Cobalt
ND
1
5.0
1.3
ug/L
11/03/2021 1721
Copper
ND
1
5.0
1.3
ug/L
11/03/2021 1721
Lead
ND
1
1.0
0.25
ug/L
11/03/2021 1721
Nickel
ND
1
5.0
1.3
ug/L
11/03/2021 1721
Selenium
ND
1
5.0
1.3
ug/L
11/03/2021 1721
Silver
ND
1
1.0
0.25
ug/L
11/03/2021 1721
Thallium
ND
1
0.50
0.15
ug/L
11/03/2021 1721
Vanadium
ND
1
5.0
2.5
ug/L
11/03/2021 1721
Zinc
ND
1
10
2.5
ug/L
11/03/2021 1721
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 47 of 58

ICP-MS Metals - LCS
Sample ID: WQ20753-002
Matrix:
Aqueous
Batch: 20753
Prep Method:
3OO5A
Analytical Method: 6020B
Prep Date:
11/02/2021 1210
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
100
92
1
92
80-120
11/03/2021 1723
Arsenic
100
99
1
99
80-120
11/03/2021 1723
Barium
100
94
1
94
80-120
11/03/2021 1723
Beryllium
100
97
1
97
80-120
11/03/2021 1723
Cadmium
100
95
1
95
80-120
11/03/2021 1723
Chromium
100
99
1
99
80-120
11/03/2021 1723
Cobalt
100
98
1
98
80-120
11/03/2021 1723
Copper
100
100
1
105
80-120
11/03/2021 1723
Lead
100
94
1
94
80-120
11/03/2021 1723
Nickel
100
100
1
101
80-120
11/03/2021 1723
Selenium
100
96
1
96
80-120
11/03/2021 1723
Silver
100
90
1
90
80-120
11/03/2021 1723
Thallium
100
91
1
91
80-120
11/03/2021 1723
Vanadium
100
96
1
96
80-120
11/03/2021 1723
Zinc
100
98
1
98
80-120
11/03/2021 1723
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 48 of 58

ICP-MS Metals - MB
Sample ID: WQ20754-001 Matrix: Aqueous
Batch: 20754 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/02/2021 0357
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
11/02/2021 1749
Arsenic
ND
1
2.0
1.3
ug/L
11/02/2021 1749
Barium
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Beryllium
ND
1
0.40
0.15
ug/L
11/02/2021 1749
Cadmium
ND
1
0.50
0.13
ug/L
11/02/2021 1749
Chromium
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Cobalt
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Copper
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Lead
ND
1
1.0
0.25
ug/L
11/02/2021 1749
Nickel
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Selenium
ND
1
5.0
1.3
ug/L
11/02/2021 1749
Silver
ND
1
1.0
0.25
ug/L
11/02/2021 1749
Thallium
ND
1
0.50
0.15
ug/L
11/02/2021 1749
Vanadium
ND
1
5.0
2.5
ug/L
11/02/2021 1749
Zinc
ND
1
10
2.5
ug/L
11/02/2021 1749
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 49 of 58

ICP-MS Metals - LCS
Sample ID: WQ20754-002
Matrix:
Aqueous
Batch: 20754
Prep Method:
3005A
Analytical Method: 6020B
Prep Date:
11/02/2021 0357
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
100
98
1
98
80-120
11/02/2021 1751
Arsenic
100
100
1
102
80-120
11/02/2021 1751
Barium
100
97
1
97
80-120
11/02/2021 1751
Beryllium
100
99
1
99
80-120
11/02/2021 1751
Cadmium
100
100
1
101
80-120
11/02/2021 1751
Chromium
100
100
1
104
80-120
11/02/2021 1751
Cobalt
100
100
1
101
80-120
11/02/2021 1751
Copper
100
110
1
107
80-120
11/02/2021 1751
Lead
100
100
1
101
80-120
11/02/2021 1751
Nickel
100
110
1
105
80-120
11/02/2021 1751
Selenium
100
100
1
104
80-120
11/02/2021 1751
Silver
100
96
1
96
80-120
11/02/2021 1751
Thallium
100
96
1
96
80-120
11/02/2021 1751
Vanadium
100
100
1
102
80-120
11/02/2021 1751
Zinc
100
100
1
103
80-120
11/02/2021 1751
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 50 of 58

ICP-MS Metals - MB
Sample ID: WQ21241-001 Matrix: Aqueous
Batch: 21241 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/07/2021 0954
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
11/08/2021 1659
Arsenic
ND
1
2.0
1.3
ug/L
11/08/2021 1659
Barium
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Beryllium
ND
1
0.40
0.15
ug/L
11/08/2021 1659
Cadmium
ND
1
0.50
0.13
ug/L
11/08/2021 1659
Chromium
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Cobalt
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Copper
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Lead
ND
1
1.0
0.25
ug/L
11/08/2021 1659
Nickel
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Selenium
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Silver
ND
1
1.0
0.25
ug/L
11/08/2021 1659
Thallium
ND
1
0.50
0.15
ug/L
11/08/2021 1659
Vanadium
ND
1
5.0
2.5
ug/L
11/08/2021 1659
Zinc
3.2 J
1
10
2.5
ug/L
11/08/2021 1659
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 51 of 58

ICP-MS Metals - LCS
Sample ID: WQ21241-002
Matrix:
Aqueous
Batch: 21241
Prep Method:
3005A
Analytical Method: 6020B
Prep Date:
11/07/2021 0954
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
100
97
1
97
80-120
11/08/2021 1701
Arsenic
100
99
1
99
80-120
11/08/2021 1701
Barium
100
93
1
93
80-120
11/08/2021 1701
Beryllium
100
110
1
105
80-120
11/08/2021 1701
Cadmium
100
100
1
100
80-120
11/08/2021 1701
Chromium
100
100
1
101
80-120
11/08/2021 1701
Cobalt
100
99
1
99
80-120
11/08/2021 1701
Copper
100
110
1
106
80-120
11/08/2021 1701
Lead
100
95
1
95
80-120
11/08/2021 1701
Nickel
100
100
1
103
80-120
11/08/2021 1701
Selenium
100
97
1
97
80-120
11/08/2021 1701
Silver
100
97
1
97
80-120
11/08/2021 1701
Thallium
100
93
1
93
80-120
11/08/2021 1701
Vanadium
100
100
1
101
80-120
11/08/2021 1701
Zinc
100
100
1
102
80-120
11/08/2021 1701
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 52 of 58

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 53 of 58

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amrnants;
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 56 of 58

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PACE ANALYTICAL SERVICES, LLC
Sam plea RaCeipt Chaddist (SReI I l MUj.Br_j S) Revlsed;912912U21)
ce4rta{y P r al
Issu lnfl Authority. Pare ENV - WCOL Page 1 of I
Sample Receipt Checklist (SRc)
Clieu., 3LG
_ C.OLACT 13)5PCCXd [p,104cc. J$I1 1 '.L.+CZ203t Lo. .: W_U00J71JMD[S
14lcans oJ' 1-t!"ipt;
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rl' Strip I I]; 21.02
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terrlperatuve upotr rcoeipt I Derived (Corrected) I=peraturo upon receipt %uS olid Snap -Cup TT): NA
Iorigins!
3.4 13.4 eC KA f NA a(; IxA 1NA ac NA MA oc — —
MCthod; 71-1—tai urjoima3lank EJA48 )81 t3 #bm IRCii.-I ID; 1RG11.41.0urrerriaat ['actor. 4 Ge
Meluxi Ofeaaiant_
0 wet Zee Q Ice Pecs n TEO
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.3. if telrtl] raLur a` any cOnlrr weeded (i.0"[ , vas Project L+ianaPur N[�ifiad?
PM was 1'U[i�ed by phone 1 err.aiI / faOitiLp-face (ci-4 r one).
V Yes
LLJJ N-D 11
NA
4. is Lhacoutke-vial co ulm-'s packiTlpslip idia;;hud to 9)is ra,rm?
Yes
LJ,.\el
5. Wee; praper c�stnr�w pra0edares (relinquisisal,'reci ivetl) falJawed7
d yihs
Tr o
G, VJe�e .pan) !e Ills li stud an ciao COC?
,f Yes
N42
7_ Wlm, sample IDr, II&W art al] gArn [e co-LLaine:s?
lr-es
No
8- 'N45 SallecLiQn data & ttaw listcd are the CO "?
[�Yes
l �10
_
9_ 'A'as coJlectign dwk& timelistCc onLI[so-uup[e cai:iairvss? -
,f Yes
No
10. Did all conrainnr label irrrunnatiae (11], (f;'[e, time) agrec wsth the Coe?
J Yes
Nol
P'_ Were ; Is t,tr lkr perfarrnl[stud oul rho CUC° I
2:1 If 12 Did all s,uF pics a.: [ve inN�� piuJ,er curLtai a yr fax oa rh test J oF&ar in
Q-Noll (unbroken, I[da on, etc.)? bond ovndiliai
❑d yr,s L—I Na 13, Was adngtra a sample volumt< available?LZI -
Yee QjqG 14. Were all tsmples rec-civcd within ;i Thelro]clij,g;rite or48 h9urs. tivhiohcvercomc5 fuse?
Yes—ONa 15. Weia any sarin Je,t eoa;,tittet-s Iruasinj�'excess (circl,: Ogle) $:Rmpies Not Iisttid on C'[?C?
E]Yes M Nu C]NA 16, Por VDA and RSK-17� sampJa; wurc bubbler pFOSpnE>"1rua�ixe" ('/."or 6min U: diamctar)
a ire any afore VOA via[g"'
ye� Flo AIA 17. Were all 1}RO;nietalslnutrien.somplez necaives l at a pH of < 2?
' s No ! NA ] $_ VdetC Ail cyanide .srlrnpks t euei v�vt xt a H 12 and s�u l edp sa7� [t 9 rCc� i Ye[1 ai: a pri .' C
), Mn .QN.A J J, %;'ere all �p icable NM,r T-'�Nlc� side e„ull 5, ]r60$ = 0,51rg,L} sa n}�1e3 fr4t
residwd r'l,lrTine?
Elyed ONO PINA 4_ Kira; rlirncieinurk3VrcqLws (iix. requeged d-Autiorv, M.1.fW3ll4asignaIicns,
correctly transcribed from the CIX inm
to the o ment sm. ion in LIMS?
Yes V No ? 1. Vr'as the use n rnn bee li9cd 001 the rantaioer IabW1 If yQ, QLH)t�k #
ample i'rct rrutiau [Must ba cam lcfcd fnr am' sttt>7ple(s} [np�et ctly pL+eI N'ed ar %vUj ccadspaoc_.) —
aLuplaf } M ltere rocaived i1K4_M;aetJy Irresprved and were adjusted deco„ irlgly
s Iuls]G n uoivin With NA_ _rtil, cf circle once. H2SO4, IN03, MC1, Nuo ij usiyc SR if NA
' W" 4� j}rC9RrV8ti�il NA - If mate t13a,I sine prZ-9- vMlivu is tmikd, please note in Commeris hr.luw_
>Irt plo(s ua _ war a teceikEd t}irh bubbJec >6 mm indirricter.
rmpirs(s) 146 were rcocived wi!h '1'RC > 0.3 mgrL (Tf P 19 k itv) an d ivem
[jimtcd accord in91Y ill suRlpie receiving wide sodiu.-n thiasulfRlc (Nacr2C)c) it[ti Slre0ly !J?- NA
8R harcade labe& applied lyy;
{ orrrntents:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 58 of 58

0
aceAnalytical
Report of Analysis
Bunnell-Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Attention: Andy Alexander
Project Name: Active Buncombe County Landfill LD
Project Number: 9378-26A
Lot Number:WK02030
Date Completed:12/07/2021
N
N
NO � � J
12/13/2021 11:51 AM
Approved and released by:
Project Manager II: Lucas Odom
pCC/►F�
24r�A
lkiA
ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 65

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Bunnell-Lammons Engineering, Inc.
Lot Number: WK02030
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
VOCs by GC/MS
The following samples were diluted due to the nature of the sample matrix: WK02030-001, WK02030-
007. The LOQ has been elevated to reflect the dilution.
The laboratory control sample (LCS) for analytical batch 22172 exceeded acceptance criteria for
Acetone. This analyte is biased high but not detected in the samples affected.
Sample -001 was received with a pH above 2.0. The pH was found to be 3.0.
Reanalysis of the following sample was performed outside of the analytical holding time for 2-Butanone
due to exceeding upper control limit: WK02030-005.
Inorganic Non -Metals
An additional dilution was needed for sample -010 Nitrate analysis. This dilution was performed outside of
the 48 hour hold time.
Subcontracted Analysis
The analysis for BOD has been performed by Pace Asheville. This data has been ammended to this lot.
Metals by ICP-MS
The method blank associated with batch 21241 yielded a "J" value detection for Zinc. No corrective action
is required as this is an estimated value recovered below the LOQ.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] whw.pacelabs.com
Page 2 of 65

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: WK02030
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
Leachate Pond
Aqueous
10/28/2021 1435
10/30/2021
002
Leachate LID
Aqueous
10/28/2021 1450
10/30/2021
003
LD-2
Aqueous
10/28/20211505
10/30/2021
004
LD-5
Aqueous
10/28/20211520
10/30/2021
005
LD-1
Aqueous
10/28/20211535
10/30/2021
006
LD-3
Aqueous
10/28/20211550
10/30/2021
007
LD-4
Aqueous
10/28/20211610
10/30/2021
008
LD-6
Aqueous
10/28/20211620
10/30/2021
009
TB
Aqueous
10/28/2021
10/30/2021
010
Leachate Pond
Aqueous
11/03/2021 1255
11/04/2021
(10 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 65

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Bunnell-Lammons Engineering, Inc.
Lot Number: WK02030
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
Leachate Pond
Aqueous
COD
SM 5220D-
1100
mg/L
7
001
Leachate Pond
Aqueous
Phosphorus
365.1
2.9
mg/L
7
001
Leachate Pond
Aqueous
Sulfate
9056A
17
mg/L
7
001
Leachate Pond
Aqueous
Acetone
8260D
80
JL
ug/L
7
001
Leachate Pond
Aqueous
2-Butanone (MEK)
8260D
25
J
ug/L
7
001
Leachate Pond
Aqueous
Antimony
6020B
12
ug/L
8
001
Leachate Pond
Aqueous
Arsenic
6020B
39
ug/L
8
001
Leachate Pond
Aqueous
Barium
6020B
450
ug/L
8
001
Leachate Pond
Aqueous
Chromium
6020B
94
ug/L
8
001
Leachate Pond
Aqueous
Cobalt
6020B
22
ug/L
8
001
Leachate Pond
Aqueous
Copper
6020B
1.8
J
ug/L
8
001
Leachate Pond
Aqueous
Lead
6020B
0.54
J
ug/L
9
001
Leachate Pond
Aqueous
Nickel
6020B
89
ug/L
9
001
Leachate Pond
Aqueous
Selenium
6020B
1.8
J
ug/L
9
001
Leachate Pond
Aqueous
Vanadium
6020B
41
ug/L
9
001
Leachate Pond
Aqueous
Zinc
6020B
19
B
ug/L
9
002
Leachate LID
Aqueous
Barium
6020B
24
ug/L
11
002
Leachate LID
Aqueous
Beryllium
6020B
0.15
J
ug/L
11
002
Leachate LID
Aqueous
Cobalt
6020B
24
ug/L
11
002
Leachate LID
Aqueous
Copper
6020B
7.9
ug/L
11
002
Leachate LID
Aqueous
Nickel
6020B
210
ug/L
11
002
Leachate LID
Aqueous
Selenium
6020B
1.4
J
ug/L
11
002
Leachate LID
Aqueous
Zinc
6020B
100
B
ug/L
11
003
LD-2
Aqueous
1,1-Dichloroethane
8260D
1.2
ug/L
12
003
LD-2
Aqueous
cis- 1,2-Dichloroethene
8260D
0.45
J
ug/L
12
003
LD-2
Aqueous
Barium
6020B
110
ug/L
13
003
LD-2
Aqueous
Chromium
6020B
3.2
J
ug/L
13
003
LD-2
Aqueous
Cobalt
6020B
23
ug/L
13
003
LD-2
Aqueous
Copper
6020B
4.1
J
ug/L
13
003
LD-2
Aqueous
Lead
6020B
0.98
J
ug/L
13
003
LD-2
Aqueous
Nickel
6020B
25
ug/L
13
003
LD-2
Aqueous
Vanadium
6020B
4.8
J
ug/L
13
003
LD-2
Aqueous
Zinc
6020B
18
B
ug/L
13
004
LD-5
Aqueous
1,4-Dioxane
8260D (SIM)
1.6
J
ug/L
14
004
LD-5
Aqueous
2-Butanone (MEK)
8260D
4.0
J
ug/L
14
004
LD-5
Aqueous
Barium
6020B
170
ug/L
15
004
LD-5
Aqueous
Cobalt
6020B
78
ug/L
15
004
LD-5
Aqueous
Nickel
6020B
21
ug/L
16
004
LD-5
Aqueous
Zinc
6020B
2.9
BJ
ug/L
16
005
LD-1
Aqueous
Benzene
8260D
1.9
ug/L
17
005
LD-1
Aqueous
2-Butanone (MEK)
8260D
28
H
ug/L
17
005
LD-1
Aqueous
Chloroethane
8260D
0.91
J
ug/L
17
005
LD-1
Aqueous
1,4-Dichlorobenzene
8260D
0.46
J
ug/L
17
005
LD-1
Aqueous
1,1-Dichloroethane
8260D
0.59
J
ug/L
17
005
LD-1
Aqueous
Barium
6020B
1300
ug/L
18
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 65

Detection Summary (Continued)
Lot Number: WK02030
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
005
LID-1
Aqueous
Chromium
6020B
1.6
J
ug/L
18
005
LD-1
Aqueous
Cobalt
6020B
270
ug/L
18
005
LID-1
Aqueous
Nickel
6020B
60
ug/L
18
005
LID-1
Aqueous
Selenium
6020B
1.8
J
ug/L
18
005
LD-1
Aqueous
Zinc
6020B
5.5
BJ
ug/L
18
006
LD-3
Aqueous
Vinyl chloride
8260D
0.82
J
ug/L
20
006
LD-3
Aqueous
Barium
6020B
220
ug/L
20
006
LD-3
Aqueous
Cobalt
6020B
5.2
ug/L
20
006
LD-3
Aqueous
Nickel
6020B
2.4
J
ug/L
20
007
LD-4
Aqueous
Antimony
6020B
0.96
J
ug/L
22
007
LD-4
Aqueous
Arsenic
6020B
4.1
ug/L
22
007
LD-4
Aqueous
Barium
6020B
490
ug/L
22
007
LD-4
Aqueous
Chromium
6020B
290
ug/L
22
007
LD-4
Aqueous
Cobalt
6020B
11
ug/L
22
007
LD-4
Aqueous
Copper
6020B
12
ug/L
22
007
LD-4
Aqueous
Nickel
6020B
89
ug/L
22
007
LD-4
Aqueous
Selenium
6020B
1.6
J
ug/L
22
007
LD-4
Aqueous
Vanadium
6020B
17
ug/L
22
007
LD-4
Aqueous
Zinc
6020B
13
B
ug/L
22
008
LD-6
Aqueous
Barium
6020B
460
ug/L
24
008
LD-6
Aqueous
Cobalt
6020B
98
ug/L
24
008
LD-6
Aqueous
Nickel
6020B
4.4
J
ug/L
24
008
LD-6
Aqueous
Zinc
6020B
4.8
BJ
ug/L
24
(68 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-001
Description: Leachate Pond Matrix: Aqueous
Date Sampled:10/28/2021 1435
Date Received:10/30/2021
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
2 (COD) SM 5220D-2011
2 11/13/2021 1532 DAK
22412
1 (Phosphorus) 365.1
5 11/03/2021 1909 DMA
21192
1 (Sulfate) 9056A
10 11/03/2021 1650 AMR
21322
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
COD
SM 5220D-2011
1100
40
40
mg/L
2
Phosphorus
7723-14-0 365.1
2.9
0.25
0.10
mg/L
1
Sulfate
9056A
17
10
2.5
mg/L
1
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
10 11/11/20211941 TML
22172
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
80 JL
200
50
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
200
8.0
ug/L
1
Benzene
71-43-2 8260D
ND
10
4.0
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
10
4.0
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
10
4.0
ug/L
1
Bromoform
75-25-2 8260D
ND
10
4.0
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
20
4.0
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
25 J
100
20
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
10
4.0
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
10
4.0
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
10
4.0
ug/L
1
Chloroethane
75-00-3 8260D
ND
20
4.0
ug/L
1
Chloroform
67-66-3 8260D
ND
10
4.0
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
10
5.0
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8 8260D
ND
10
4.0
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
10
4.0
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
10
4.0
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3 8260D
ND
10
4.0
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
20
5.0
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
10
4.0
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
10
4.0
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
10
4.0
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
10
4.0
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
10
4.0
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
10
4.0
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
10
4.0
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
10
4.0
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
10
4.0
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-001
Description: Leachate Pond Matrix: Aqueous
Date Sampled:10/28/2021 1435
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 10 11/11/20211941 TML 22172
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
10
4.0
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
10
4.0
ug/L
1
2-Hexanone
591-78-6
8260D
ND
100
20
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
50
4.0
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
100
20
ug/L
1
Methylene chloride
75-09-2
8260D
ND
10
4.0
ug/L
1
Styrene
100-42-5
8260D
ND
10
4.1
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
10
4.0
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
10
4.0
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
10
4.0
ug/L
1
Toluene
108-88-3
8260D
ND
10
4.0
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
10
4.0
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
10
4.0
ug/L
1
Trichloroethene
79-01-6
8260D
ND
10
4.0
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
10
4.0
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
10
4.0
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
50
12
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
10
4.0
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
10
4.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
96 70-130
1,2-Dichloroethane-d4
114 70-130
Toluene-d8
103 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/08/2021 1728 BNW
11/07/2021 0954 21241
2 3005A
6020B
1 11/09/2021 1855 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
12
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
39
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
450
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
2
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
94
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
22
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
1.8 J
5.0
1.3
ug/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-001
Description: Leachate Pond Matrix: Aqueous
Date Sampled:10/28/2021 1435
Date Received:10/30/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date Batch
1 3005A
6020B 1 11/08/2021 1728 BNW
11/07/2021 0954 21241
2 3005A
6020B 1 11/09/2021 1855 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Lead
7439-92-1 6020B
0.54 J 1.0
0.25
ug/L
2
Nickel
7440-02-0 6020B
89 5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
1.8 J 5.0
1.3
ug/L
2
Silver
7440-22-4 6020B
ND 1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND 0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
41 5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
19 B 10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-002
Description: Leachate LD Matrix: Aqueous
Date Sampled:10/28/2021 1450
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211542 TML 22172
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-002
Description: Leachate LD Matrix: Aqueous
Date Sampled:10/28/2021 1450
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
1 11/11/20211542 TML
22172
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
100 70-130
1,2-Dichloroethane-d4
107 70-130
Toluene-d8
104 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/08/2021 1730 BNW
11/07/2021 0954 21241
2 3005A
6020B
1 11/09/2021 1242 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
24
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
0.15 J
0.40
0.15
ug/L
2
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
24
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
7.9
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
2
Nickel
7440-02-0 6020B
210
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
1.4 J
5.0
1.3
ug/L
2
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
100 B
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-003
Description: LD-2 Matrix: Aqueous
Date Sampled:10/28/2021 1505
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211606 TML 22172
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
1.2
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis-1,2-Dichloroethene
156-59-2
8260D
0.45 J
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-003
Description: LD-2 Matrix: Aqueous
Date Sampled:10/28/2021 1505
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
1 11/11/20211606 TML
22172
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
95 70-130
1,2-Dichloroethane-d4
105 70-130
Toluene-d8
103 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/08/2021 1732 BNW
11/07/2021 0954 21241
2 3005A
6020B
1 11/09/2021 1245 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
110
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
2
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
3.2 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
23
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
4.1 J
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
0.98 J
1.0
0.25
ug/L
2
Nickel
7440-02-0 6020B
25
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
2
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
4.8 J
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
18 B
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-004
Description: LD-5 Matrix: Aqueous
Date Sampled:10/28/2021 1520
Date Received:10/30/2021
Volatile Organic Compounds by
GC/MS (SIM)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D (SIM) 1 11/05/2021 2008 CAW
21469
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,4-Dioxane
123-91-1 8260D (SIM)
1.6 J
3.0
1.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
87 40-170
Volatile Organic Compounds
by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D 1 11/11/20211630 TML
22172
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1 8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1 8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2 8260D
ND
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5 8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4 8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2 8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3 8260D
4.0 J
10
2.0
ug/L
1
Carbon disulfide
75-15-0 8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5 8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7 8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3 8260D
ND
2.0
0.40
ug/L
1
Chloroform
67-66-3 8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1 8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4 8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide) 74-95-3 8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6 8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1 8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2 8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5 8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5 8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5 8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6 8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W
= Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-004
Description: LD-5 Matrix: Aqueous
Date Sampled:10/28/2021 1520
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211630 TML 22172
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
95 70-130
1,2-Dichloroethane-d4
105 70-130
Toluene-d8
102 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/08/2021 1734 BNW
11/07/2021 0954 21241
2 3005A
6020B
1 11/09/2021 1251 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
170
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
2
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
78
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
2
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-004
Description: LD-5 Matrix: Aqueous
Date Sampled:10/28/2021 1520
Date Received:10/30/2021
ICP-MS Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date Batch
1 3005A
6020B 1 11/08/2021 1734 BNW
11/07/2021 0954 21241
2 3005A
6020B 1 11/09/2021 1251 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Nickel
7440-02-0 6020B
21 5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND 5.0
1.3
ug/L
2
Silver
7440-22-4 6020B
ND 1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND 0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND 5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
2.9 BJ 10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-005
Description: LD-1 Matrix: Aqueous
Date Sampled:10/28/2021 1535
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 11/11/20211654
TML
22172
2 5030B 8260D
1 12/03/20211539 BWS
24540
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
1
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
1
Benzene
71-43-2
8260D
1.9
1.0
0.40
ug/L
1
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
28 H
10
2.0
ug/L
2
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3
8260D
0.91 J
2.0
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
1
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
0.46 J
1.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
0.59 J
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range DL =
Detection Limit
Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 % J = Estimated result <
LOQ and > DL
L = LCS/LCSD
failure
H = Out of holding time W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-005
Description: LD-1 Matrix: Aqueous
Date Sampled:10/28/2021 1535
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
1 11/11/20211654 TML
22172
2 5030B
8260D
1 12/03/20211539 BWS
24540
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,1-Trichloroethane
71-55-6 8260D
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance Run
2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery
Limits
Bromofluorobenzene
98 70-130 H 92
70-130
1,2-Dichloroethane-d4
105 70-130 H 124 70-130
Toluene-d8
107 70-130 H 108 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/08/2021 1736 BNW
11/07/2021 0954
21241
2 3005A
6020B
1 11/09/2021 1253 BNW
11/07/2021 0954
21241
3 3005A
6020B
5 11/09/2021 1255 BNW
11/07/2021 0954
21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
1300
25
6.3
ug/L
3
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
2
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
1.6 J
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
270
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
2
Nickel
7440-02-0 6020B
60
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
1.8 J
5.0
1.3
ug/L
2
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
5.5 BJ
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-006
Description: LD-3 Matrix: Aqueous
Date Sampled:10/28/2021 1550
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211718 TML 22172
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-006
Description: LD-3 Matrix: Aqueous
Date Sampled:10/28/2021 1550
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
1 11/11/20211718 TML
22172
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
0.82 J
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
97 70-130
1,2-Dichloroethane-d4
112 70-130
Toluene-d8
106 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/08/2021 1738 BNW
11/07/2021 0954 21241
2 3005A
6020B
1 11/09/2021 1257 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
220
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
2
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
5.2
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
2
Nickel
7440-02-0 6020B
2.4 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
2
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
ND
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-007
Description: LD-4 Matrix: Aqueous
Date Sampled:10/28/2021 1610
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 10 11/11/20212004 TML 22172
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
200
50
ug/L
Acrylonitrile
107-13-1
8260D
ND
200
8.0
ug/L
Benzene
71-43-2
8260D
ND
10
4.0
ug/L
Bromochloromethane
74-97-5
8260D
ND
10
4.0
ug/L
Bromodichloromethane
75-27-4
8260D
ND
10
4.0
ug/L
Bromoform
75-25-2
8260D
ND
10
4.0
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
20
4.0
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
100
20
ug/L
Carbon disulfide
75-15-0
8260D
ND
10
4.0
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
10
4.0
ug/L
Chlorobenzene
108-90-7
8260D
ND
10
4.0
ug/L
Chloroethane
75-00-3
8260D
ND
20
4.0
ug/L
Chloroform
67-66-3
8260D
ND
10
4.0
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
10
5.0
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
10
4.0
ug/L
Dibromochloromethane
124-48-1
8260D
ND
10
4.0
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
10
4.0
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
10
4.0
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
20
5.0
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
10
4.0
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
10
4.0
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
10
4.0
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
10
4.0
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
10
4.0
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
10
4.0
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
10
4.0
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
10
4.0
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
10
4.0
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
10
4.0
ug/L
Ethylbenzene
100-41-4
8260D
ND
10
4.0
ug/L
2-Hexanone
591-78-6
8260D
ND
100
20
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
50
4.0
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
100
20
ug/L
Methylene chloride
75-09-2
8260D
ND
10
4.0
ug/L
Styrene
100-42-5
8260D
ND
10
4.1
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
10
4.0
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
10
4.0
ug/L
Tetrachloroethene
127-18-4
8260D
ND
10
4.0
ug/L
Toluene
108-88-3
8260D
ND
10
4.0
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
10
4.0
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-007
Description: LD-4 Matrix: Aqueous
Date Sampled:10/28/2021 1610
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
10 11/11/20212004 TML
22172
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
10
4.0
ug/L
1
Trichloroethene
79-01-6 8260D
ND
10
4.0
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND S
10
4.0
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
10
4.0
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
50
12
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
10
4.0
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
10
4.0
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
95 70-130
1,2-Dichloroethane-d4
113 70-130
Toluene-d8
105 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/08/2021 1741 BNW
11/07/2021 0954 21241
2 3005A
6020B
1 11/09/2021 1259 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
0.96 J
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
4.1
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
490
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
2
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
290
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
11
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
12
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
2
Nickel
7440-02-0 6020B
89
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
1.6 J
5.0
1.3
ug/L
2
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
17
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
13 B
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-008
Description: LD-6 Matrix: Aqueous
Date Sampled:10/28/2021 1620
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211742 TML 22172
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-008
Description: LD-6 Matrix: Aqueous
Date Sampled:10/28/2021 1620
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
8260D
1 11/11/20211742 TML
22172
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
1,1,2-Trichloroethane
79-00-5 8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4 8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4 8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4 8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4 8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7 8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
96 70-130
1,2-Dichloroethane-d4
108 70-130
Toluene-d8
105 70-130
ICP-MS Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3005A
6020B
1 11/08/2021 1743 BNW
11/07/2021 0954 21241
2 3005A
6020B
1 11/09/2021 1301 BNW
11/07/2021 0954 21241
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Antimony
7440-36-0 6020B
ND
2.0
0.50
ug/L
1
Arsenic
7440-38-2 6020B
ND
2.0
1.3
ug/L
1
Barium
7440-39-3 6020B
460
5.0
1.3
ug/L
1
Beryllium
7440-41-7 6020B
ND
0.40
0.15
ug/L
2
Cadmium
7440-43-9 6020B
ND
0.50
0.13
ug/L
1
Chromium
7440-47-3 6020B
ND
5.0
1.3
ug/L
1
Cobalt
7440-48-4 6020B
98
5.0
1.3
ug/L
1
Copper
7440-50-8 6020B
ND
5.0
1.3
ug/L
1
Lead
7439-92-1 6020B
ND
1.0
0.25
ug/L
2
Nickel
7440-02-0 6020B
4.4 J
5.0
1.3
ug/L
1
Selenium
7782-49-2 6020B
ND
5.0
1.3
ug/L
2
Silver
7440-22-4 6020B
ND
1.0
0.25
ug/L
1
Thallium
7440-28-0 6020B
ND
0.50
0.15
ug/L
1
Vanadium
7440-62-2 6020B
ND
5.0
2.5
ug/L
1
Zinc
7440-66-6 6020B
4.8 BJ
10
2.5
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
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Page 23 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-009
Description: TB Matrix: Aqueous
Date Sampled:10/28/2021
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211343 TML 22172
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Acetone
67-64-1
8260D
ND L
20
5.0
ug/L
Acrylonitrile
107-13-1
8260D
ND
20
0.80
ug/L
Benzene
71-43-2
8260D
ND
1.0
0.40
ug/L
Bromochloromethane
74-97-5
8260D
ND
1.0
0.40
ug/L
Bromodichloromethane
75-27-4
8260D
ND
1.0
0.40
ug/L
Bromoform
75-25-2
8260D
ND
1.0
0.40
ug/L
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
2.0
0.40
ug/L
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
Carbon disulfide
75-15-0
8260D
ND
1.0
0.40
ug/L
Carbon tetrachloride
56-23-5
8260D
ND
1.0
0.40
ug/L
Chlorobenzene
108-90-7
8260D
ND
1.0
0.40
ug/L
Chloroethane
75-00-3
8260D
ND
2.0
0.40
ug/L
Chloroform
67-66-3
8260D
ND
1.0
0.40
ug/L
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1.0
0.50
ug/L
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1.0
0.40
ug/L
Dibromochloromethane
124-48-1
8260D
ND
1.0
0.40
ug/L
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1.0
0.40
ug/L
Dibromomethane (Methylene bromide)
74-95-3
8260D
ND
1.0
0.40
ug/L
trans- 1,4-Dichloro-2-butene
110-57-6
8260D
ND
2.0
0.50
ug/L
1,2-Dichlorobenzene
95-50-1
8260D
ND
1.0
0.40
ug/L
1,4-Dichlorobenzene
106-46-7
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethane
75-34-3
8260D
ND
1.0
0.40
ug/L
1,2-Dichloroethane
107-06-2
8260D
ND
1.0
0.40
ug/L
1,1-Dichloroethene
75-35-4
8260D
ND
1.0
0.40
ug/L
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1.0
0.40
ug/L
trans- 1,2-Dichloroethene
156-60-5
8260D
ND
1.0
0.40
ug/L
1,2-Dichloropropane
78-87-5
8260D
ND
1.0
0.40
ug/L
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1.0
0.40
ug/L
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1.0
0.40
ug/L
Ethylbenzene
100-41-4
8260D
ND
1.0
0.40
ug/L
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
Methyl iodide (lodomethane)
74-88-4
8260D
ND
5.0
0.40
ug/L
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
Methylene chloride
75-09-2
8260D
ND
1.0
0.40
ug/L
Styrene
100-42-5
8260D
ND
1.0
0.41
ug/L
1,1,1,2-Tetrachloroethane
630-20-6
8260D
ND
1.0
0.40
ug/L
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1.0
0.40
ug/L
Tetrachloroethene
127-18-4
8260D
ND
1.0
0.40
ug/L
Toluene
108-88-3
8260D
ND
1.0
0.40
ug/L
1,1,1-Trichloroethane
71-55-6
8260D
ND
1.0
0.40
ug/L
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 24 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory I D: WK02030-009
Description: TB Matrix: Aqueous
Date Sampled:10/28/2021
Date Received:10/30/2021
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 11/11/20211343 TML 22172
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,1,2-Trichloroethane
79-00-5
8260D
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6
8260D
ND
1.0
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
1.0
0.40
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260D
ND
1.0
0.40
ug/L
1
Vinyl acetate
108-05-4
8260D
ND
5.0
1.2
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
1.0
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
95 70-130
112 70-130
106 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
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Page 25 of 65

Client: Bunnell-Lammons Engineering, Inc. Laboratory ID:WK02030-010
Description: Leachate Pond Matrix: Aqueous
Date Sampled:11/03/2021 1255
Date Received: 11 /04/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 (Nitrate - N) 9056A 25 11/05/2021 1252 AMR 21837
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Nitrate - N
9056A ND H 0.50 0.13 mg/L 2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 65

QC Summary
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Page 27 of 65

Inorganic non-metals - MB
Sample ID: WQ21192-001 Matrix: Aqueous
Batch: 21192
Analytical Method: 365.1
Parameter Result Q Dil LOQ DL Units Analysis Date
Phosphorus ND 1 0.050 0.020 mg/L 11/03/2021 1820
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 28 of 65

Inorganic non-metals - LCS
Sample ID: WQ21192-002 Matrix: Aqueous
Batch: 21192
Analytical Method: 365.1
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Phosphorus 1.0 0.99 1 99 90-110 11/03/2021 1824
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 65

Inorganic non-metals - MB
Sample ID: WQ21322-001 Matrix: Aqueous
Batch: 21322
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Sulfate ND 1 1.0 0.25 mg/L 11/03/2021 1310
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 30 of 65

Inorganic non-metals - LCS
Sample ID: WQ21322-002 Matrix: Aqueous
Batch: 21322
Analytical Method: 9056A
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Sulfate 20 20 1 102 80-120 11/03/2021 1440
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 31 of 65

Inorganic non-metals - MB
Sample ID: WQ21837-001 Matrix: Aqueous
Batch: 21837
Analytical Method: 9056A
Parameter Result Q Dil LOQ DL Units Analysis Date
Nitrate - N ND 1 0.020 0.0050 mg/L 11/05/2021 1214
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 32 of 65

Inorganic non-metals - LCS
Sample ID: WQ21837-002 Matrix: Aqueous
Batch: 21837
Analytical Method: 9056A
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Nitrate - N 0.80 0.82 1 102 80-120 11/05/2021 1233
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 33 of 65

Inorganic non-metals - MB
Sample ID: WQ22412-001 Matrix: Aqueous
Batch: 22412
Analytical Method: SM 5220D-2011
Parameter Result Q Dil LOQ DL Units Analysis Date
COD ND 1 20 20 mg/L 11/13/2021 1531
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 34 of 65

Inorganic non-metals - LCS
Sample ID: WQ22412-002 Matrix: Aqueous
Batch: 22412
Analytical Method: SM 5220D-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
COD 400 390 1 98 95-105 11/13/2021 1531
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 35 of 65

Volatile Organic Compounds by GC/MS (SIM) - MB
Sample ID: WQ21469-001 Matrix: Aqueous
Batch: 21469 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Parameter Result Q Dil LOQ DL Units Analysis Date
1,4-Dioxane ND 1 3.0 1.0 ug/L 11/05/2021 1102
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
93 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 36 of 65

Volatile Organic Compounds by GC/MS (SIM) - LCS
Sample ID: WQ21469-002 Matrix: Aqueous
Batch: 21469 Prep Method: 5030E
Analytical Method: 8260D (SIM)
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
1,4-Dioxane 50 56 1 112 70-130 11/05/2021 1003
Surrogate
1,2-Dichloroethane-d4
LOQ = Limit of Quantitation
DL = Detection Limit
Acceptance
Q % Rec Limit
113 40-170
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Page 37 of 65

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ22172-001 Matrix: Aqueous
Batch: 22172 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
20
5.0
ug/L
11/11/2021 1254
Acrylonitrile
ND
1
20
0.80
ug/L
11/11/2021 1254
Benzene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Bromochloromethane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Bromodichloromethane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Bromoform
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Bromomethane (Methyl bromide)
ND
1
2.0
0.40
ug/L
11/11/2021 1254
2-Butanone (MEK)
ND
1
10
2.0
ug/L
11/11/2021 1254
Carbon disulfide
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Carbon tetrachloride
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Chlorobenzene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Chloroethane
ND
1
2.0
0.40
ug/L
11/11/2021 1254
Chloroform
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Chloromethane (Methyl chloride)
ND
1
1.0
0.50
ug/L
11/11/2021 1254
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Dibromochloromethane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
1,2-Dibromoethane (EDB)
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Dibromomethane (Methylene bromide)
ND
1
1.0
0.40
ug/L
11/11/2021 1254
trans- 1,4-Dichloro-2-butene
ND
1
2.0
0.50
ug/L
11/11/2021 1254
1,2-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
1,4-Dichlorobenzene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
1,1-Dichloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
1,2-Dichloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
1,1-Dichloroethene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
cis- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
trans- 1,2-Dichloroethene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
1,2-Dichloropropane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
cis- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
trans- 1,3-Dichloropropene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Ethylbenzene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
2-Hexanone
ND
1
10
2.0
ug/L
11/11/2021 1254
Methyl iodide (lodomethane)
ND
1
5.0
0.40
ug/L
11/11/2021 1254
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
11/11/2021 1254
Methylene chloride
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Styrene
ND
1
1.0
0.41
ug/L
11/11/2021 1254
1,1,1,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
1,1,2,2-Tetrachloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Tetrachloroethene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Toluene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
1,1,1-Trichloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
1,1,2-Trichloroethane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Trichloroethene
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Trichlorofluoromethane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
1,2,3-Trichloropropane
ND
1
1.0
0.40
ug/L
11/11/2021 1254
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 38 of 65

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ22172-001 Matrix: Aqueous
Batch: 22172 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
DL
Units
Analysis Date
Vinyl acetate
ND
1
5.0
1.2
ug/L
11/11/2021 1254
Vinyl chloride
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Xylenes (total)
ND
1
1.0
0.40
ug/L
11/11/2021 1254
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 95 70-130
1,2-Dichloroethane-d4 110 70-130
Toluene-d8 103 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 39 of 65

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ22172-002
Matrix:
Aqueous
Batch: 22172
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
160
N 1
163
60-140
11/11/2021 1143
Acrylonitrile
100
110
1
115
70-130
11/11/2021 1143
Benzene
50
51
1
102
70-130
11/11/2021 1143
Bromochloromethane
50
50
1
101
70-130
11/11/2021 1143
Bromodichloromethane
50
51
1
102
70-130
11/11/2021 1143
Bromoform
50
49
1
98
70-130
11/11/2021 1143
Bromomethane (Methyl bromide)
50
47
1
95
70-130
11/11/2021 1143
2-Butanone (MEK)
100
120
1
124
70-130
11/11/2021 1143
Carbon disulfide
50
55
1
111
70-130
11/11/2021 1143
Carbon tetrachloride
50
52
1
105
70-130
11/11/2021 1143
Chlorobenzene
50
49
1
98
70-130
11/11/2021 1143
Chloroethane
50
56
1
111
70-130
11/11/2021 1143
Chloroform
50
51
1
102
70-130
11/11/2021 1143
Chloromethane (Methyl chloride)
50
58
1
116
60-140
11/11/2021 1143
1,2-Dibromo-3-chloropropane (DBCP)
50
55
1
111
70-130
11/11/2021 1143
Dibromochloromethane
50
50
1
101
70-130
11/11/2021 1143
1,2-Dibromoethane (EDB)
50
50
1
100
70-130
11/11/2021 1143
Dibromomethane (Methylene bromide)
50
51
1
103
70-130
11/11/2021 1143
trans- 1,4-Dichloro-2-butene
50
55
1
109
70-130
11/11/2021 1143
1,2-Dichlorobenzene
50
48
1
96
70-130
11/11/2021 1143
1,4-Dichlorobenzene
50
46
1
93
70-130
11/11/2021 1143
1,1-Dichloroethane
50
52
1
103
70-130
11/11/2021 1143
1,2-Dichloroethane
50
52
1
105
70-130
11/11/2021 1143
1,1-Dichloroethene
50
55
1
110
70-130
11/11/2021 1143
cis- 1,2-Dichloroethene
50
52
1
105
70-130
11/11/2021 1143
trans- 1,2-Dichloroethene
50
53
1
107
70-130
11/11/2021 1143
1,2-Dichloropropane
50
51
1
101
70-130
11/11/2021 1143
cis- 1,3-Dichloropropene
50
52
1
103
70-130
11/11/2021 1143
trans- 1,3-Dichloropropene
50
54
1
108
70-130
11/11/2021 1143
Ethylbenzene
50
51
1
101
70-130
11/11/2021 1143
2-Hexanone
100
120
1
116
70-130
11/11/2021 1143
Methyl iodide (lodomethane)
50
53
1
106
70-130
11/11/2021 1143
4-Methyl-2-pentanone
100
110
1
111
70-130
11/11/2021 1143
Methylene chloride
50
51
1
102
70-130
11/11/2021 1143
Styrene
50
53
1
106
70-130
11/11/2021 1143
1,1,1,2-Tetrachloroethane
50
49
1
99
70-130
11/11/2021 1143
1,1,2,2-Tetrachloroethane
50
49
1
98
70-130
11/11/2021 1143
Tetrachloroethene
50
48
1
96
70-130
11/11/2021 1143
Toluene
50
52
1
104
70-130
11/11/2021 1143
1,1,1-Trichloroethane
50
53
1
106
70-130
11/11/2021 1143
1,1,2-Trichloroethane
50
49
1
98
70-130
11/11/2021 1143
Trichloroethene
50
48
1
96
70-130
11/11/2021 1143
Trichlorofluoromethane
50
55
1
111
70-130
11/11/2021 1143
1,2,3-Trichloropropane
50
52
1
104
70-130
11/11/2021 1143
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 40 of 65

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ22172-002
Matrix:
Aqueous
Batch: 22172
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Vinyl acetate
50
45
1
91
60-140
11/11/2021 1143
Vinyl chloride
50
56
1
113
70-130
11/11/2021 1143
Xylenes (total)
100
110
1
105
70-130
11/11/2021 1143
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 96 70-130
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 98 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 41 of 65

Volatile Organic Compounds by GC/MS - MS
Sample ID: WK02030-007MS
Matrix:
Aqueous
Batch: 22172
Prep Method:
5030E
Analytical Method: 8260D
Sample
Spike
Amount
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Acetone
ND
1000
1100
10
111
60-140
11/11/2021 2028
Acrylonitrile
ND
1000
1200
10
116
70-122
11/11/2021 2028
Benzene
ND
500
580
10
115
70-130
11/11/2021 2028
Bromochloromethane
ND
500
550
10
111
70-130
11/11/2021 2028
Bromodichloromethane
ND
500
570
10
114
70-130
11/11/2021 2028
Bromoform
ND
500
520
10
104
70-130
11/11/2021 2028
Bromomethane (Methyl bromide)
ND
500
520
10
104
70-130
11/11/2021 2028
2-Butanone (MEK)
ND
1000
1100
10
114
70-130
11/11/2021 2028
Carbon disulfide
ND
500
640
10
128
70-130
11/11/2021 2028
Carbon tetrachloride
ND
500
620
10
123
70-130
11/11/2021 2028
Chlorobenzene
ND
500
540
10
107
70-130
11/11/2021 2028
Chloroethane
ND
500
640
10
127
70-130
11/11/2021 2028
Chloroform
ND
500
570
10
114
70-130
11/11/2021 2028
Chloromethane (Methyl chloride)
ND
500
660
10
131
60-140
11/11/2021 2028
1,2-Dibromo-3-chloropropane (DBCP)
ND
500
550
10
110
70-130
11/11/2021 2028
Dibromochloromethane
ND
500
550
10
110
70-130
11/11/2021 2028
1,2-Dibromoethane (EDB)
ND
500
530
10
106
70-130
11/11/2021 2028
Dibromomethane (Methylene bromide)
ND
500
560
10
113
70-130
11/11/2021 2028
trans- 1,4-Dichloro-2-butene
ND
500
510
10
103
70-130
11/11/2021 2028
1,2-Dichlorobenzene
ND
500
510
10
103
70-130
11/11/2021 2028
1,4-Dichlorobenzene
ND
500
490
10
98
70-130
11/11/2021 2028
1,1-Dichloroethane
ND
500
580
10
116
70-130
11/11/2021 2028
1,2-Dichloroethane
ND
500
580
10
115
70-130
11/11/2021 2028
1,1-Dichloroethene
ND
500
650
10
129
70-130
11/11/2021 2028
cis- 1,2-Dichloroethene
ND
500
580
10
115
70-130
11/11/2021 2028
trans- 1,2-Dichloroethene
ND
500
600
10
119
70-130
11/11/2021 2028
1,2-Dichloropropane
ND
500
560
10
112
70-130
11/11/2021 2028
cis- 1,3-Dichloropropene
ND
500
550
10
109
70-130
11/11/2021 2028
trans- 1,3-Dichloropropene
ND
500
570
10
114
70-130
11/11/2021 2028
Ethylbenzene
ND
500
570
10
113
70-130
11/11/2021 2028
2-Hexanone
ND
1000
1100
10
113
70-130
11/11/2021 2028
Methyl iodide (lodomethane)
ND
500
590
10
119
70-130
11/11/2021 2028
4-Methyl-2-pentanone
ND
1000
1100
10
115
70-130
11/11/2021 2028
Methylene chloride
ND
500
570
10
114
70-130
11/11/2021 2028
Styrene
ND
500
580
10
115
70-130
11/11/2021 2028
1,1,1,2-Tetrachloroethane
ND
500
550
10
110
70-130
11/11/2021 2028
1,1,2,2-Tetrachloroethane
ND
500
510
10
103
70-130
11/11/2021 2028
Tetrachloroethene
ND
500
550
10
109
70-130
11/11/2021 2028
Toluene
ND
500
570
10
115
70-130
11/11/2021 2028
1,1,1-Trichloroethane
ND
500
610
10
122
70-130
11/11/2021 2028
1,1,2-Trichloroethane
ND
500
520
10
105
70-130
11/11/2021 2028
Trichloroethene
ND
500
540
10
108
70-130
11/11/2021 2028
Trichlorofluoromethane
ND
500
660 N
10
131
70-130
11/11/2021 2028
1,2,3-Trichloropropane
ND
500
520
10
104
70-130
11/11/2021 2028
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 42 of 65

Volatile Organic Compounds by GC/MS - MS
Sample ID: WK02030-007MS
Matrix:
Aqueous
Batch: 22172
Prep Method:
5030E
Analytical Method: 8260D
Sample
Spike
Amount
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Vinyl acetate
ND
500
530
10
105
60-140
11/11/2021 2028
Vinyl chloride
ND
500
650
10
130
70-130
11/11/2021 2028
Xylenes (total)
ND
1000
1200
10
116
70-130
11/11/2021 2028
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 111 70-130
Toluene-d8 108 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 43 of 65

Volatile Organic Compounds by GC/MS - MSD
Sample ID: WK02030-007MD
Matrix:
Aqueous
Batch: 22172
Prep Method:
5030E
Analytical Method: 8260D
Sample
Spike
Amount
Amount
Result
%Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec % RPD
Limit
Limit
Analysis Date
Acetone
ND
1000
1100
10
108
2.5
60-140
20
11/11/2021 2052
Acrylonitrile
ND
1000
1200
10
116
0.045
70-122
20
11/11/2021 2052
Benzene
ND
500
560
10
113
2.1
70-130
20
11/11/2021 2052
Bromochloromethane
ND
500
540
10
108
2.2
70-130
20
11/11/2021 2052
Bromodichloromethane
ND
500
560
10
113
0.74
70-130
20
11/11/2021 2052
Bromoform
ND
500
520
10
104
0.17
70-130
20
11/11/2021 2052
Bromomethane (Methyl bromide)
ND
500
500
10
100
3.9
70-130
20
11/11/2021 2052
2-Butanone (MEK)
ND
1000
1100
10
112
2.3
70-130
20
11/11/2021 2052
Carbon disulfide
ND
500
620
10
123
4.0
70-130
20
11/11/2021 2052
Carbon tetrachloride
ND
500
610
10
122
0.87
70-130
20
11/11/2021 2052
Chlorobenzene
ND
500
530
10
107
0.32
70-130
20
11/11/2021 2052
Chloroethane
ND
500
620
10
123
3.3
70-130
20
11/11/2021 2052
Chloroform
ND
500
570
10
113
1.2
70-130
20
11/11/2021 2052
Chloromethane (Methyl chloride)
ND
500
640
10
127
3.1
60-140
20
11/11/2021 2052
1,2-Dibromo-3-chloropropane (DBCP)
ND
500
570
10
113
3.1
70-130
20
11/11/2021 2052
Dibromochloromethane
ND
500
550
10
110
0.42
70-130
20
11/11/2021 2052
1,2-Dibromoethane (EDB)
ND
500
530
10
106
0.59
70-130
20
11/11/2021 2052
Dibromomethane (Methylene bromide)
ND
500
550
10
110
2.3
70-130
20
11/11/2021 2052
trans- 1,4-Dichloro-2-butene
ND
500
520
10
104
1.7
70-130
20
11/11/2021 2052
1,2-Dichlorobenzene
ND
500
510
10
102
0.74
70-130
20
11/11/2021 2052
1,4-Dichlorobenzene
ND
500
490
10
98
0.17
70-130
20
11/11/2021 2052
1,1-Dichloroethane
ND
500
580
10
115
0.64
70-130
20
11/11/2021 2052
1,2-Dichloroethane
ND
500
570
10
114
0.65
70-130
20
11/11/2021 2052
1,1-Dichloroethene
ND
500
620
10
124
3.9
70-130
20
11/11/2021 2052
cis- 1,2-Dichloroethene
ND
500
570
10
114
1.1
70-130
20
11/11/2021 2052
trans- 1,2-Dichloroethene
ND
500
600
10
119
0.038
70-130
20
11/11/2021 2052
1,2-Dichloropropane
ND
500
550
10
110
2.1
70-130
20
11/11/2021 2052
cis- 1,3-Dichloropropene
ND
500
550
10
109
0.25
70-130
20
11/11/2021 2052
trans- 1,3-Dichloropropene
ND
500
570
10
113
1.0
70-130
20
11/11/2021 2052
Ethylbenzene
ND
500
570
10
113
0.16
70-130
20
11/11/2021 2052
2-Hexanone
ND
1000
1100
10
115
1.0
70-130
20
11/11/2021 2052
Methyl iodide (lodomethane)
ND
500
570
10
115
3.3
70-130
20
11/11/2021 2052
4-Methyl-2-pentanone
ND
1000
1100
10
113
1.0
70-130
20
11/11/2021 2052
Methylene chloride
ND
500
550
10
110
3.6
70-130
20
11/11/2021 2052
Styrene
ND
500
570
10
114
1.0
70-130
20
11/11/2021 2052
1,1,1,2-Tetrachloroethane
ND
500
540
10
108
2.0
70-130
20
11/11/2021 2052
1,1,2,2-Tetrachloroethane
ND
500
530
10
105
2.1
70-130
20
11/11/2021 2052
Tetrachloroethene
ND
500
540
10
107
2.1
70-130
20
11/11/2021 2052
Toluene
ND
500
570
10
114
0.68
70-130
20
11/11/2021 2052
1,1,1-Trichloroethane
ND
500
600
10
120
1.7
70-130
20
11/11/2021 2052
1,1,2-Trichloroethane
ND
500
520
10
104
0.29
70-130
20
11/11/2021 2052
Trichloroethene
ND
500
530
10
107
1.2
70-130
20
11/11/2021 2052
Trichlorofluoromethane
ND
500
620
10
124
5.6
70-130
20
11/11/2021 2052
1,2,3-Trichloropropane
ND
500
530
10
105
0.93
70-130
20
11/11/2021 2052
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 44 of 65

Volatile Organic Compounds by GC/MS - MSD
Sample ID: WK02030-007MD
Matrix:
Aqueous
Batch: 22172
Prep Method:
5030E
Analytical Method: 8260D
Sample
Spike
Amount
Amount
Result
%Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec % RPD
Limit
Limit
Analysis Date
Vinyl acetate
ND
500
510
10
102 2.7
60-140
20
11/11/2021 2052
Vinyl chloride
ND
500
630
10
126 2.6
70-130
20
11/11/2021 2052
Xylenes (total)
ND
1000
1200
10
116 0.25
70-130
20
11/11/2021 2052
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 110 70-130
Toluene-d8 108 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 45 of 65

Volatile Organic Compounds by GC/MS - MB
Sample ID: WQ24540-001 Matrix: Aqueous
Batch: 24540 Prep Method: 5030E
Analytical Method: 8260D
Parameter Result Q Dil LOQ DL Units Analysis Date
2-Butanone (MEK) ND 1 10 2.0 ug/L 12/03/2021 1027
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 92 70-130
1,2-Dichloroethane-d4 123 70-130
Toluene-d8 107 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 46 of 65

Volatile Organic Compounds by GC/MS - LCS
Sample ID: WQ24540-002
Matrix:
Aqueous
Batch: 24540
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L) Q Dil
% Rec Limit Analysis Date
2-Butanone (MEK)
100
120 1
119 70-130 12/03/2021 0923
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 70-130
1,2-Dichloroethane-d4 102 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 47 of 65

ICP-MS Metals - MB
Sample ID: WQ21241-001 Matrix: Aqueous
Batch: 21241 Prep Method: 3005A
Analytical Method: 6020B Prep Date: 11/07/2021 0954
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Antimony
ND
1
2.0
0.50
ug/L
11/08/2021 1659
Arsenic
ND
1
2.0
1.3
ug/L
11/08/2021 1659
Barium
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Beryllium
ND
1
0.40
0.15
ug/L
11/08/2021 1659
Cadmium
ND
1
0.50
0.13
ug/L
11/08/2021 1659
Chromium
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Cobalt
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Copper
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Lead
ND
1
1.0
0.25
ug/L
11/08/2021 1659
Nickel
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Selenium
ND
1
5.0
1.3
ug/L
11/08/2021 1659
Silver
ND
1
1.0
0.25
ug/L
11/08/2021 1659
Thallium
ND
1
0.50
0.15
ug/L
11/08/2021 1659
Vanadium
ND
1
5.0
2.5
ug/L
11/08/2021 1659
Zinc
3.2 J
1
10
2.5
ug/L
11/08/2021 1659
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 48 of 65

ICP-MS Metals - LCS
Sample ID: WQ21241-002
Matrix:
Aqueous
Batch: 21241
Prep Method:
3005A
Analytical Method: 6020B
Prep Date:
11/07/2021 0954
Spike
Amount
Result
%Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Antimony
100
97
1
97
80-120
11/08/2021 1701
Arsenic
100
99
1
99
80-120
11/08/2021 1701
Barium
100
93
1
93
80-120
11/08/2021 1701
Beryllium
100
110
1
105
80-120
11/08/2021 1701
Cadmium
100
100
1
100
80-120
11/08/2021 1701
Chromium
100
100
1
101
80-120
11/08/2021 1701
Cobalt
100
99
1
99
80-120
11/08/2021 1701
Copper
100
110
1
106
80-120
11/08/2021 1701
Lead
100
95
1
95
80-120
11/08/2021 1701
Nickel
100
100
1
103
80-120
11/08/2021 1701
Selenium
100
97
1
97
80-120
11/08/2021 1701
Silver
100
97
1
97
80-120
11/08/2021 1701
Thallium
100
93
1
93
80-120
11/08/2021 1701
Vanadium
100
100
1
101
80-120
11/08/2021 1701
Zinc
100
100
1
102
80-120
11/08/2021 1701
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 49 of 65

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 50 of 65

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S:'MPl105 Reeeipt ChCddist (SRO �MEU018[-1$l Iwevised;W29j2020
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J Yea NO �J?1, if Cusu�rl 9rls 1ver resent, werelev intact taad tttlbrx7kun?
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PM was Notified by- phone r ern ail 1 fac.34r-rice (circle orrC)_
d `deal Na NA 4. Is the colnmrmial courier's packing slip aftacloerl to tVis forth?
V YCE Nn Wpm P`nWcLL'cw WY Procedures (relingtlishcdrreteivcd) foliowetl2
{ Yes No 6. W.,ro mmple Ids listed on the COC7
`has ❑ No !. Wffe Miple IDs listed on al ;ample ugrr obi ;?
At ye -a No $. Wam collection dnto & time li6#ed on tlt4 WC? —
❑ Ve`' No y, Wa$ o0IJecdOn date & tirrfe listed cn all epinple coi:L tuirlcrsl
a Los ❑ o rU_ UiG ill contairr<r Jabel in�prnmtion (iD, date, time) dgree wittt 03P, COC?
71 Yes No l J . Wert 1-051s to bo perfor mud listed on the CC+C?
Yes ❑ 12, Did all sarnlrlcs jrr:ve in Iheptroper c:,,ntainen for each test andlor h good onndi:'on
(nntrcokari, lids om, etc,)? _
+r cs IJ No 13.1Nas adequate. sample vcalume avalltabf$'�
Yea + N 14. WBre all 5amglcs rece3x'ed wJJrirr I� the �Jclrng tirne or 48 hours, whjaCMr cause first'
Yes +� yo 15_ LVtrc ten s rtrples cba7tairru" missittg'exccss {cite Ie one) &=g1cs Not liatrxl ell COC?
❑ ' s ❑ 12a ❑NA lii_ Par 1�OA a�ld UKJ73 s,]ntplas, yrere hobbles Jr, s:�l pea- i e+" ('r:,'or 4mun in Siam err}
r all n[',Jrc VOA via!s't
5'4s Nn NA 17. Were all DR0jnteoalsfnuttjent samples received a# a R of < 27
Yes No J NA M Wm all rY&k iclta samples received at a pH > 12 and sllifirdc sa hplrs received :4l- a u FI � 9? —
❑ YcR El No ❑,t NA 19' Were AIT aplalicabl& N11je A'l;.yfni erpborte625_ Ii802i.3 [< 0._5M_ rL sanipies fee Uf
residuid chlarine?
❑Yes �Nlo ��l:l0. Werc olien'renlark f:ayuets(i.e. r-gjmted dilutiorys, M2'MSD deftnaticrns,ctc..eorrectl}• {xanscrihed from ihm C oe into tits wilimellt seetion in UNIS?
Yesf of a 9.1. Vk'as tFtc rluore nUmbar JLStec on the oomtaiycr labL-J? Tr'ves_ O:rore g
S�tnp�e !*res�rvatian (�r±us. Ix aompl�red l47 #tn}sartp[C(s} ircnrrpr.tl}preserved or u�rlJt ileadspacc_1 .
Sair331c(s) "A _ wale rumdved ?reor„cxtJy re3ervcd and uerc ad use J ttt caordinpry
hi sartrtflc roceivin witty VA mL of elmle one- T12,904, HN00, HCJ, NaOH using SR # NA
Titne efrtraseTvacion tom` lfrucrcthan onePreservttliyc is noedad,Plca,enoU; i:r ihvcnmmants belcrw.
5: tttp]c(sj tea — _ wetm received with IHaaSles ?
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�dj�s'ed aCCarCir!O}+ in sample rescivrnig wide sodigtn Momlfalt~ {Naas:R j rrith Skiealy ID. NA
5R harcade labels applied b3+:
Ccunmrals',
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 52 of 65

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PACE ANALYTICAL SERVICES, LLC
Samplcs Receipt Checklist (SRC (r01ILDD18G1S) Revised-9,f�/2020
c � Y!�+ Essuir1jjAtcharity, Paoe ENV -W-COL Page 1 01
anl;p]e keceh)( Chtekiist (SRC)
Client; rdr,t` Gaoler Jm acred b '1441C; JR❑3 e I Il9+?11C1 l.nt ir' WNW(130
Meam.uFL- ipl: Paco Client I., PS V red EX Otlyer.
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Y
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12. ki eustody s--Is iverelnreseq were ;hav it]MO and Ulllj- IkCJ37
p H Strip ]D: I" _ C;h lorine Strip 1D: JqA Tested by "A
Original =peratum upon reccipt O' Darived (Carnacted) tempmalprc upon rcc2ipr YQSolld Saap Cup ID: NA
1-3 ae NA INA oC NA /NA cC NA j34A aC -
Mel=i4d; Z omperatum BlaiA [3k�irkq l3attl, s IR Gull ID: $ 1R Gun Comaction Factor- 0
M21hnd nrr.colant 0 WetTce d lct,F'acks 0 Uly kcR .Q plane
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PM wm Kotifted by: :ions ? em4i1 / face-to-face Ccirulo imc).
Ycs3 No
NA
4_ Is t_e ,euurrnemial caurier's paCMHg sl ip HLt:+chM tr, tt}is farm?
5. Were proper custody procedures (retinqu:sltcXm-.t::vcd) fol lojved2
6. Weve samplo IDs listed on the G' c?
l
Ycsf
Lj No
,l
Yes
NO
d
Yea
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'7_ Were Lample JIM listed on at: �HFUPlc cantain4rs;"
771
Yes
LJ
No
8_ Was Col laotion care & ti me I Is xd on. tho CUC 2
9. Wus calbm ion date& time Ikfiledan Hll sample comajoem?
l tt_ Did all wontainer 'abel information (1D, d+rtc, time) a e with the COG?
d
Yes
77 Nu
❑ No.
Yes
my—
Flo
. 1. Wurc t: a� to be perfntrn&J F VLP j on tlra COC7
12. Did a:1 sam;sles arrive in the prop-. conta;nem for each test �xndJor in good condikipn
_
rJ
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13. Was adequato sn nt k volume ava:lilb'47
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14. Wtru Hll ss,mp;ng received wtihin � the Folding tune or 4,8 Ilou-B, whirl-mrrcomes first?
ym
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J 5, Alem any sam plc& cer.m4icrs Iniss UI. *iexc-6 (6mlc one) camp les Not 1JSk4'tl +x] CO ?
❑ Y
❑ No
❑,
16. For VUA and RSK-17S szrnplets, wom bubbles pien;c,iL>" pea-siZc' f'!,"or 51nm in diam�tr )
:tr.
pry uf;hc VOA vials'
17. Were all DROinieE^als,+uutrient recci vcd at a o k-1 af< 2?
IS, Were all cyanide sarnplw rmcivrd at.9 pi i } 12 2md sulfide sar:taleg received a:_ a pr15 W
1 U
7qa
LJJNAJ
❑ Yes
Nu
d
NA
❑ Ycs
❑ He,
❑NA
19_ Vdnrc T,Ik a „sa e iwl!! �T +7�l cyarit coo i633, I ItiGS.3 (t. F.79g(L) samPIts free o'
rsid; ai c--Ilzrin_?
❑ Ycs
❑ No
Lvj A
0. Wcrc cltcnt rcn1arkcVregne.ls {i. , rar.0ested dilutao=rs, WMSD dcsi+gnadons, em... j
r orrc rely trFnscr:hed fmin the f'.GC into die comment stmticn in LIMS?
ycs
No
21. I�+as rho acre n6w—bor I-stcd on 11% CCmlutiiar IHhal4 1Fye.5, Quote P
�ample Fr�crti+utaon �lMlnst be completed ftir�rY sample{sj J1YcorrecJq 1;rrscr�'+J rsr €t�itl� kreadspare.j
%jrnple(e) 14* wen twHivmd :ncarre-- ly preserved and wcrc adjusted accordin.*
in .sa-npie roceivbtg WAIL ran mL of c hie one: k-13904. l NO3, HCJ, NaOH using SR 4 ""
_
Tune cf pr,eservalion NA if more than one pr'eszm, Hve is neeced, plu sc nut.- in the ewrimena 3alnw.
mple(a) rdA were recei;red ,;v itkr mm in diam eter_
Salnpics(S) NA wow received with TRC > 0.5 mp'L (iiI1� Is he) anti Vier_
adjusted accntrliingly in sample receiv-no wick sodium thiosujfaU (Ka,S,Or) witlt Sheay ID- MA
4R herc,otie labels a-3plied by: JR93 l a0c: Ill 4P202r
Comments:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 54 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
November 04, 2021
Lucas Odom
Shealy Environmental Services, Inc.
106 Vantage Point Drive
West Columbia, SC 29172
RE: Project: WK02030 BLE
Pace Project No.: 92570350
Dear Lucas Odom:
Enclosed are the analytical results for sample(s) received by the laboratory on November 03, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sara Poulson
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 55 of 65
Page 1 of 11

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WK02030 BLE
Pace Project No.: 92570350
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 56 of 65
Page 2 of 11

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: WK02030 BLE
Pace Project No.: 92570350
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92570350001 LEACHATE POND SM 521OB-2016 NFW 1 PASI-A
PASI-A = Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 11
Page 57 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WK02030 BLE
Pace Project No.: 92570350
Sample: LEACHATE POND Lab ID: 92570350001 Collected: 10/28/21 14:35 Received: 11/03/21 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210B BOD, 5 day Analytical Method: SM 521OB-2016
Pace Analytical Services -Asheville
BOD, 5 day 49.0 mg/L 2.0 1 10/30/21 05:48 11/04/21 03:50 B2,H3
Date: 11/04/2021 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 58 of 65
Page 4 of 11

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WK02030 BLE
Pace Project No.: 92570350
QC Batch: 657279 Analysis Method: SM 521 OB-2016
QC Batch Method: SM 521OB-2016 Analysis Description: 5210E BOD, 5 day
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92570350001
METHOD BLANK: 3445474
Associated Lab Samples: 92570350001
Parameter Units
BOD, 5 day mg/L
LABORATORY CONTROL SAMPLE: 3445476
Parameter Units
BOD, 5 day mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 11 /04/21 03:23
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
198 212 107 84.6-115
SAMPLE DUPLICATE: 3445477
92569626004 Dup
Parameter Units Result Result
BOD, 5 day mg/L 12000 ug/L 13.8
RPD Qualifiers
14 B2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /04/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 59 of 65
Page 5 of 11

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: WK02030 BLE
Pace Project No.: 92570350
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /04/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 60 of 65
Page 6 of 11

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: WK02030 BLE
Pace Project No.: 92570350
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92570350001 LEACHATE POND SM 521OB-2016 657279 SM 521OB-2016 657295
Date: 11/04/2021 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 61 of 65
Page 7 of 11

acaAnalyfbl'
r
Document N a me:
Sam le Candttlon Upon Recelpl(SCUR)
oocument Revised: October 28, 2020
Page 1 of 2
Document No,:
F•CAR-0-033•Rev,07
Issuing Authority:
Pace Carolin9sQu0litY0ffTCe
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑
Huntersville ❑
Raleigh[)
Mechanicsville❑ Atlanta❑ Kernersville❑
Saws • Condition Client Name:
. 92570350
r, 7
Project
g:WO#
Courier: ❑Fed Etc ❑UPS
❑USPS
❑Client
�1
11�
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���
1 l
❑Commercial ❑Pace
[]other:—L82570350
I 1
i11 1
Custody Seal Present? []Yes ❑No Seals Intact? ❑Yes
❑No
Date/Iniliafs Person ExantiningCantents: / 11`9
Packing Material: ❑Bubble Wrap ❑Oubble
Bags []hone
❑ Other
Biological Tissue Frozen?
QN/A
❑Yes ❑No
Thermometer:
❑Wet
❑lllue
❑NoAe
( IFt Gun ID: e;f r +
Type of Ice:
Correction Factor:
Cooler Temp: Add/5ubtract (T)
t '
Temp should be above freezing to VC
❑Samples oui of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected ('0:
basbegun
USDA Regulated SOIL ( [} NIA, ,Aaler samples
Did samples originate in'a quarantine zone within the United
rr..
States: CA, NY, or 5C (check
maps)?
Did samples originate from a foreign source [internationally,
lnrli,arnnA.... Ii aad 17ijrrm Wca17l`IYes nNo
Co mments/Discrepancy:
Chi In of Custody Present?
}Yes
[]Ito
❑NJA
].
Samples Arrived wl thin [told Time?
i
❑Yes
❑No
❑N!A
2.
Sho rt Hold Time Analysis 102 hf,)?
Ycs
❑No
❑N/A
3.
Rus h Turn Around Time Requested?
OYes
ON.__
❑N/A
4.
StIfflcient VOtame?
0yes
❑No
❑N1A
5.
Correct Containers Used?
-Pace Containers Used?
}Yes
©Yas
❑No
[]No
❑H/A
NIA
6.
Containers Intact?
Qyes
❑Na
©N/A
7,
Dissolved analysis: Samples Field Flitered?
Dyes
❑Na
' N/A
8•
Sample Labels Match COO
•lRcludesDate/Tine/lD/Aiialpsls Matrix:__
14eadspace In VOA Vials (>5-6ntnt)?
❑Yes
j
❑Yes
ONO
[:]No
❑NIA
©NIA.
9.
I
10.
Trip BiankPresent?
Trip Blank Custody Seals Present?
❑Yes
[]Yes
ONO
ONO
[(tt/A
rVA
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time,
Lot ID of split containers:
Date;
Date:
Field Data Required? ❑Ycs [IN*
Page 62 of 65
Page 8 of 11

.,. aceAnalytica!'
r
Document {Name:
Conditfan Upon Rece€
Document No.:
F-CAR•CS-033-Rev.07
*Check mark top Ralf of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples,
Exceptforts: VOA, Collfurm,TOC, Oil and Grease, DRO/8015 {viater) DOC, Mig
tweattom half of box Is to list number of battles
Document Revisgcl: October 28, 2020
CUR) Page 2 of 2
fssu€ngAuthority:
Project lWOff : 92570350
PM: SG Due Date: 11/10/21
CLIENT: 92-Pa,;e5hea1
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pH Adjustment Log for Preserved Samples
Sample to Type of Presefvat€ve pH upon receipt oats preseruJtlon adjusted Time preservation Amount or Preservative lot U
adjusted added
Nate: wflenever Share Is a discfepar}Sy alfecllnl; ilort€7 Carol}na compliance samples, a copy of this lorm win ce sent CO [I a @ortn CarOnna ptrlfVSS C@rniiWUOn Uln[e p.e.
Out of hold, mwrrect preservative, out of temp, incorrect containers.
Page 9 of
Page 63 of 65

Chain of Custody
Workorder: WK02030 Workorder Name: Active Buncombe Leachate Owner Received Date:
Report To: Subcontract To:
Lucas J. Odom Project # 9378-26A
Pace Analytical
106 Vantage Point Drive Pace Asheville
Columbia SC, 29223
803-206-9537
iucas.odomCu7pacelabs_com ;Preserved containers
Sample Collect z m
Item Sample ID- Type Date/Time ' Lab ID " Matrix
1 Leachate Pond grab 10/29/2021 @ 1435 WK02030-001 Aqueous x X
2
3
4
5
6
;7
18
9
10
Transfers Released By Date/Time Reveived By' Date/Time
1
2
aceAnalv6cal'
r
Results Requested By: 11/10/2C
Requested Analysis
Comments
IL
1
Z.5 733,5C3
!AS USE ONLY
Cooler Temperature on Receipt �CI Custody Seal Y or N Received on Ice Y or N I sample Intact Y or N
***In order to maintain client confidentiality, location/name of the sampling site, sampler's name and signature may not be provided on this COC
This chain of custody is considered complete as is since this information is available in the owner laboratory.
Friday, June 17, 2016 11:01:34 AM FMT-ALL-C-002rev_00 24March2009 Page 1 of 1

1.10 1.1• 96ed
593° S9 aged
Ship to :
aceAi2alytical
f Pace Asheville
Phone
INTER LABORATORY WORK ORDER q W K02030
(To be complete by sending tab)
Sending Project No:
WK02030
Receiving Project No:
Check Box for Consolidated Invoice:
x
Date Prepared:
3-Nov
REQUESTED COMPLETION DATE:
11-Nov
Sending Region IR77-SC Sending Project Mgr. LJO
Receiving Region Asheville External Client BLE
State of Sample origin NC Q L2
All questions should be addressed to sending project manager.
Requested Reportable Units mg/L Report Wet or Dry Weight? Cert Needed:
WORK.REQUESTED :..
uan y o Quantity o .
Method Description Container Type containers ' Preservattva . samples.::; Unit Price 'Amount
BOD plastic 1 none 1 25 25
TOTAL 25
Speclal RequlremenW
Acctg,Code. Totals from above Revenue Allocation
Receiving Reglon Department Receiving Region Client Services Dept.
(80%) Sending Region (20%)
25 20 5
"Custom Revenue AllDcatlon TOTAL 20 5
FOR ANALYTICAL WORK COMPLETED THIS SECTION ALSO
Chain of Custody Included: x Yes =No Return Samples to Sending Regulon: Yes x No
Matrix: ❑ 50H water F]Air Other (identity)
CaNFIRMATION;OF WORK.COMPLETED '
Date Completed: Receiving Project Manager:
Original sent to the receiving lab - Copy kept at the sending lab.
when work completed: Original sent to the ABM at the receiving laboratory. Copies are made to corporate as needed.
Friday, )une 17, 2016 11:01:35 AM FMT-ALL-C-001 fev.00 24March2009 Page 1 of 1