24052 Dogget St Brownfields Assessment 20220114

P R O F E S S I O N A L | P R A C T I C A L | P R O V E N
417 Minuet Lane, Suite D, Charlotte, North Carolina 28217
NOVA North Carolina License No: C-2807
t. 980.321.4100 / usanova.com
January 14, 2022

COUSINS TREMONT DOGGETT LP
3344 Peachtree Road NE
Suite 1800
Atlanta, Georgia 30326

Attention: Mr. John McColl
Executive Vice President

Subject: Supplemental Subsurface Assessment
DOGGETT STREET/WEST TREMONT AVENUE SITE
Charlotte, North Carolina
NOVA Project Number 3021011

Dear Mr. McColl:

NOVA Engineering and Environmental, Inc. (NOVA) has completed the authorized Supplemental
Subsurface Assessment for the approximately 2.441-acres property located at 305 Doggett
Street and 242/306 West Tremont Avenue in Charlotte, Mecklenburg County, North Carolina.
The work was performed in general accordance with NOVA Proposal Number 005-30214502,
dated July 15, 2021.

The authorized Supplemental Subsurface Assessment work was performed in general
accordance with ASTM International (ASTM) Standard Practice for Environmental Site
Assessments: Phase II Environmental Site Assessment Process, Designation: E1903-19 and
the North Carolina Department of Environmental Quality (NC DEQ) Brownfields Program
requested additional assessment activities, unless otherwise stated herein. The attached
report presents our understanding of the project information, a description of the
environmental services provided by NOVA, and our findings and conclusions.

We appreciate your selection of NOVA and the opportunity to be of service on this project. If you
have any questions, or if we may be of further assistance, please do not hesitate to contact us.
Sincerely,
NOVA Engineering and Environmental, Inc.
Steven M. Aldis, PG, RSM Keith Rice
Project Manager Senior Geologist
Copies Submitted: Addressee (electronic)

TABLE OF CONTENTS

1.0 INTRODUCTION .............................................................................................................. 1
1.1 SITE AND PROJECT INFORMATION .............................................................................................. 1
1.2 LIMITATIONS ................................................................................................................................. 9
1.3 USER RELIANCE............................................................................................................................ 9
2.0 SUPPLEMENTAL SUBSURFACE ASSESSMENT ............................................................ 10
2.1 SOIL BORING INSTALLATION AND SOIL SAMPLING ................................................................. 10
2.2 GROUNDWATER SAMPLING ...................................................................................................... 11
2.3 SOIL GAS SAMPLING ................................................................................................................. 11
2.4 QUALITY CONTROL AND QUALITY ASSURANCE METHODS ...................................................... 11
3.0 RESULTS ...................................................................................................................... 13
3.1 SOIL LABORATORY RESULTS .................................................................................................... 13
3.2 GROUNDWATER LABORATORY RESULTS ................................................................................. 16
3.3 GROUNDWATER ELEVATIONS OR DEPTHS ............................................................................... 17
3.4 SOIL GAS LABORATORY RESULTS ............................................................................................ 18
4.0 CONCLUSIONS ............................................................................................................. 20
4.1 SOIL DETECTIONS ..................................................................................................................... 20
4.2 GROUNDWATER DETECTIONS .................................................................................................. 21
4.3 SOIL GAS DETECTIONS .............................................................................................................. 22

APPENDICES

Appendix A – Figures
Appendix B – Boring Logs and Well Logs
Appendix C – Soil and Groundwater Analytical
Appendix D – Soil Gas Analytical
Appendix E – Risk Calculator Results
Appendix F – Receptor Survey

Appendix G – Qualifications of Conclusions

Supplemental Subsurface Assessment January 14, 2022
Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

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1.0 INTRODUCTION

NOVA Engineering and Environmental, LLC (NOVA) was retained by Cousins Tremont Doggett
LP (Client) to complete a Supplemental Subsurface Assessment on the approximately 2.441-
acres property located at 305 Doggett Street and 242/306 West Tremont Avenue in Charlotte,
Mecklenburg County, North Carolina (Subject Property). A site location map is included as
Figure 1 in Appendix A.

1.1 SITE AND PROJECT INFORMATION

The Subject Property is located at 305 Doggett Street and 242/306 West Tremont
Avenue in Charlotte, Mecklenburg County, North Carolina. According to the
Mecklenburg County Geographic Information System (GIS) database, the Subject
Property measures approximately 2.441-acres and contains three (3) tax parcels
identified by Parcel Numbers 12103314 (305 Doggett Street), 12103307 (242 West
Tremont Avenue) and 12103306 (306 West Tremont Avenue). The Subject Property is
bordered by Doggett Street on the north, West Tremont Avenue on the south, an
unnamed alley on the west, and by other developed properties to the east. A Site Map
including an aerial photograph is included as Figures 2 in the Attachments.

The Subject Property is currently developed with following structures:

305 Doggett Street – This address contains three (3) buildings according to property
tax records.

• Building 1: 1-story warehouse building including 10,200 total square feet, built in
1954;
• Building 2: 2-story light-manufacturing building including 27,024 total square feet,
built in 1963; and,
• Building 3: 1-story warehouse building including 600 total square feet, built in
1981.

306 West Tremont Ave – This address contains one (1) 2-story warehouse building
including 11,644 total square feet, built in 1964. The structure is attached to a 2-story
office building with canopy structures located between and is referred to as the
“accounting” building.

242 West Tremont Ave – This address contains one (1) 1-story light manufacturing
building including 10,370 total square feet, built in 1950. This building is referred to
as the “Dilworth” building and is divided into the air heater production line with two
loading bays in the western portion with warehouse storage in the eastern portion.

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The Subject Property contains associated asphalt-paved parking to the north, east and
south of the office and manufacturing structures. The site also contains greenspace
including trees, grass, and low-growing vegetation.

A Phase I Limited Site Assessment Report, conducted by Altura Environmental, Inc.
(Altura), on Gas-Fired Products, Inc., at 306 West Tremont Avenue, Charlotte, North
Carolina was conducted on October 6, 2003. The document indicated that the Phase
I Limited Site Assessment (LSA) was performed in accordance with NCDENR (former
name for NCDEQ) guidance. Additional site history was provided in the LSA and stated
that “the subject property was formerly occupied by J.B. Thomas and Sons, a general
contracting firm, in the late 1940’s and early 1950’s. It is believed that the former UST
was installed by J.B. Thomas and Sons, and the last use of the UST was during that
time. There are no other USTs reported to be present on the subject site.” On August
22, 2003, Altura was onsite to drill one (1) soil boring, collect soil samples, install one
(1) groundwater monitoring well and collect a groundwater sample from said well. Soil
samples were collected at depths of -13’, -17’ and -22’ below ground surface (bgs)
from the soil boring drilled within the UST source area. Partially weathered rock was
encountered at -24’ below ground surface. The soil samples were analyzed for Volatile
Organic Constituents (VOCs), Methyl tert-Butyl Ether (MTBE), Isopropyl Ether (IPE),
Semi-VOCs (SVOCs), volatile petroleum hydrocarbons and extractable petroleum
hydrocarbons in accordance with NCDENR guidelines. The analytical results of soil
samples collected in the source area during the Phase I LSA indicated that no
petroleum constituents were detected at concentrations in excess of NCDENR soil to
groundwater maximum soil contaminant concentrations, which are the most stringent
limits established by NCDENR. A groundwater monitoring well was installed with
slotted screening from 19 to 24 feet bgs as groundwater was recorded at
approximately 18.5 feet. The groundwater sample was analyzed in accordance with
NCDENR guidelines for heating oil and included EPA Method 602 plus xylenes, EPA
Method 625, and volatile petroleum and extractable petroleum hydrocarbons by
MADEP VPH and EPH, respectively. The groundwater laboratory analysis indicated that
several petroleum constituents were detected in the groundwater at concentrations in
excess of the 2L or interim Standard and in excess of 10x the 2L or Interim standard.
However, none of the concentrations were detected in excess of the listed Gross
Contaminant Levels (GCLs).

Based on the findings of the LSA, Altura recommended that “based on the land use
information provided in this report for the subject site and surrounding properties, it is
the opinion of Altura that the property be designated an industrial/commercial property.
All petroleum constituents identified in the soil samples collected from the source area
boring were detected at concentrations below the NCDENR soil to groundwater
maximum soil concentrations values. In addition, the analytical results of the
groundwater sample collected from monitoring well MW-1 indicate that none of the
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required parameters were detected at concentrations in excess of the listed GCLs. As a
results, a Notice of Residual Petroleum (NRP) has been completed for the subject site
and recorded at the Mecklenburg County Register of Deeds Office…Altura requests that
the NCDENR issue a “No Further Action” letter for the subject site.”

A UST Closure and Assessment Report was conducted by Altura for Gas-Fired Products,
Inc., dated December 8, 2003. The UST closure report indicated that NCDENR provided
closure for UST release incident pending recordation of a Notice of Residual Petroleum
(NRP) at the Mecklenburg County Register of Deeds Office. The NRP placed a perpetual
land use restriction on the property. Due to the soil impact above the residential
MSCCs, the perpetual land use restriction states that, “the site shall be used for
industrial/commercial use only. The perpetual land use restriction, as it pertains to the
groundwater, states that, “groundwater from the site is prohibited from use as a water
supply. Water supply wells of any kind shall not be installed or operated on the site.”

Altura stated that, based on conversations with NCDENR, if impacted soils are removed
from the site such that confirmatory soil sampling indicated petroleum concentrations
are below the residential MSCCs, then the perpetual land use restriction pertaining to
the site soils can be removed from the deed restriction. In Altura’s opinion “if the site
building was razed providing easy access to subsurface soils, that the impacted soils
could be removed from the former UST area, confirmatory soil samples could be
collected (showing results that are below the residential MSCCs), and the soil restriction
could be removed from the property deed.

Hart & Hickman, PC (H&H) performed soil vapor assessment activities documented in
a Subslab Soil Vapor Sampling Report for Gas Fired Products Facility dated February
18, 2013. The subslab soil vapor sampling was conducted to evaluate the potential
for vapor intrusion into site buildings consistent with Brownfields program
requirements should the site enter the Brownfields program in the future. On
November 8, 2012, H&H conducted subslab soil vapor sampling from six (6) locations
within the manufacturing, office and warehouse areas of the Subject Property. H&H
utilized six-liter Summa canisters to collect the vapor samples as they were submitted
for laboratory analysis for volatile organic compounds (VOCs) by EPA Method TO-15
and for helium by EPA Method 3C.

H&H stated “Low concentrations of multiple VOCs were detected in the six samples
collected. The concentrations were compared to NCDENR Inactive Hazardous Sites
Branch (IHSB) Industrial/Commercial Soil Vapor Screening Levels. The ISHB screening
levels are based upon conservative assumptions. None of the detected compound
concentrations exceeded their IHSB Industrial/Commercial Soil Vapor Screening
Levels. In accordance with DENR Brownfields program guidance and H&H’s
professional experience with the Brownfields program, because the subslab soil vapor
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samples concentrations were less than the applicable screening levels, H&H does not
recommend further evaluation of the vapor intrusion pathway such as indoor air
sampling or indoor air mitigation.”

H&H performed a Phase I ESA Report for Dilworth Mattress Factory, 242 West Tremont
Avenue, Charlotte North Carolina, dated June 29, 2016. The Phase I ESA indicated that
the 0.43-acre land parcel was occupied by Dilworth Mattress Factory, a mattress
manufacturer, at the time of the Phase I ESA. The site was developed with the eastern
portion of the current site building in 1950 as the western portion of the site building
was developed in 1984. The site has reportedly operated as a mattress manufacturer
since it was constructed in 1950. H&H identified the following off-site issues resulting
in Recognized Environmental Conditions (RECs) in connection with the Subject
Property:

• “Virginia Carolina Chemical (VCC) Charlotte (249 Tremont Avenue) is located
adjacent to the south and southwest across Tremont Avenue and upgradient to
cross-gradient from the site. According to reports reviewed, this facility formerly
operated as a phosphate fertilizer plant from at least the 1890s until the 1930s.
An adjacent plant to the east also operated as a cottonseed oil plant. The facility
occupied the property until 1974 at which time the current commercial and light
industrial buildings were developed. Soil at the facility is impacted by arsenic and
lead as a result of the former activities and ExxonMobil is identified as the
responsible party for the cleanup. ExxonMobil has removed source area soil from
feasible locations at the facility and currently maintains a cap on the property.
Results of soil assessment indicated that metals were not detected above
screening levels in the samples located closest to the subject site and therefore
the potential for soil impact to the site from the VCC facility appears low. Recent
groundwater sampling events indicate the presence of low levels of lead, arsenic,
tetrachloroethene (PCE), and trichloroethene (TCE) in groundwater at this facility
above NC groundwater standards in monitoring wells located close to the site.
Concentrations of PCE (0.91 micrograms per liter (μg/l) versus standard of 0.7
μg/l) and TCE (4.2 μg/l versus standard of 3 μg/l) were detected in the wells closest
to the site.”

• “South Boulevard Properties, Inc./Atherton Mill Property/Flakt Inc. Bahnson/Parks-
Cramer Company (2000-2140 South Boulevard) is located approximately 1,200
feet to the east and topographically upgradient of the site. According to records
reviewed, in 1962, the Parks-Cramer facility began to operate a vapor degreasing
unit for cleaning and preparation of metal parts prior to paint application in the
main Parks-Cramer building north of the site. Initially trichloroethene (TCE) was
used as the solvent in the degreasing process, which was replaced with 1,1,1,-
trichloroethane (1,1,1-TCA) from 1976 to 1988. Releases of solvents occurred
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beneath the vapor degreaser and discharged through a stormwater system to the
adjacent Norfolk Southern railroad tracks west of the parent parcel. Releases of
volatile organic compounds also occurred through spraying of waste solvents for
weed control along an earthen embankment from 1962 to 1979. Results of
groundwater assessment indicate that groundwater impacts (TCE was detected as
high as 200,000 μg/l at this property) have migrated to the west-northwest toward
downgradient properties including the subject site. Results of analysis of
groundwater samples collected approximately 400 ft southeast and upgradient of
the site indicated the presence of TCE at greater than 5,000 μg/l. Interim soil
remediation was conducted in the late 1980s, and groundwater remediation using
a pump and treat system occurred from 1990 to 2001. The North Carolina
Department of Environmental Quality (DEQ) Hazardous Waste Section (HWS)
formerly regulated the Parks-Cramer release incident. On January 19, 2006, the
HWS ceased regulation pursuant to a risk assessment and technical
impracticability determination. The determination was primarily based on: 1) the
inability to continue groundwater extraction due to a county-wide moratorium on
discharge of treated groundwater to the sanitary system, 2) the inadequacy of
available technologies to address removal or in situ destruction of chlorinated
volatile organic compounds present as dense non-aqueous phase liquids in
bedrock, 3) the adoption of a county-wide well ordinance to ensure receptor
protection, 4) the lack of predicted impact to the ultimate surface water receptors,
and 5) the costs associated with continuation of remedial efforts. This facility is
cited as the source area for chlorinated solvent impacts to the groundwater in the
area near the site. In addition, according to groundwater model predictions of the
chlorinated solvent groundwater contamination plume, the subject site is predicted
to be impacted from the release at this facility.”

• “2000 Hawkins Street (2000 Hawkins Street) is located approximately 350 feet to
the east and topographically cross-gradient of the site. According to the reports
reviewed, the groundwater samples collected from the wells on the property
indicated the presence of chlorinated solvent compounds, phthalates, methyl-tert-
butyl ether (MTBE), and benzene in groundwater above North Carolina groundwater
standards. The highest compound concentrations were detected in the upgradient
sample in the eastern portion of the facility which had a concentration of the
chlorinated solvent TCE at 6,200 μg/l (versus the NC groundwater standard of 3
μg/l). The sample collected closest to the subject site contained TCE at a
concentration of 41 μg/l.”

H&H identified a potential environmental concern in connection with the Subject
Property as a heating oil AST was observed on the northern exterior wall of the western
portion of the site building. The AST is no longer utilized. No indications of releases were
observed in associate with the AST. H&H did not consider it to be evidence of a REC.
No recommendations were noted in the Phase I ESA.
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NOVA Engineering & Environmental, Inc. performed a Phase I ESA for the Doggett
Street & West Tremont Avenue Site dated September 17, 2020. NOVA identified the
following on-site issue resulting in Recognized Environmental Conditions (RECs) in
connection with the Subject Property:

• The impacts to soil and groundwater identified above applicable regulatory
thresholds during NOVA’s 2020 Limited Phase II ESA.

Additionally, NOVA identified the following on-site and off-site issues resulting in
Controlled Recognized Environmental Conditions (CRECs) in connection with the
Subject Property:

ON-SITE

• The former presence of a 300-gallon heating oil UST and associated residual
petroleum at the Subject Property.

OFF-SITE

• The Carolina Foundry facility located adjoining to the east and south of the Subject
Property.
• The Kale Bindex, Inc/2000 Hawkins Street facility located adjoining to the east of
the Subject Property.
• The Virginia Carolina Chemical (VCC)/ExxonMobil Oil Corp 99CLT facility located
adjoining to the south of the Subject Property.

NOVA Engineering & Environmental, Inc. performed a Limited Phase II ESA for the
Doggett Street & West Tremont Avenue Site dated September 17, 2020. The following
is a summary of the findings of NOVA’s Limited Phase II ESA:

VOC CONSTITUENTS IN SOIL

Bromomethane, Chloromethane, and Naphthalene were detected in a soil sample
collected on the northeastern portion of the Subject Property (S-2) at concentrations
above their NC DEQ Protection of Groundwater PSRGs. Naphthalene was detected in soil
sample S-2 at a concentration above its residential PSRG. The remaining VOC
constituents detected in soil were at concentrations below NC DEQ Preliminary Soil
Remediation Goals (PSRGs).

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SVOC CONSTITUENTS IN SOIL

1-Methylnaphthalene, 2-Methylnaphthalene, Benzo(a)anthracene, Benzo(a)pyrene,
Benzo(b)fluoranthene, Dibenzo(a,h)anthracene, Indeno(1,2,3-cd)pyrene, and
Naphthalene were detected in soil sample S-2 at concentrations above their NC DEQ
Protection of Groundwater PSRGs.

Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene,
Dibenzo(a,h)anthracene, Indeno(1,2,3-cd)pyrene, and Naphthalene were detected in
soil sample S-2 at concentrations above their residential PSRGs.

Benzo(a)pyrene was detected in soil sample S-2 at a concentration above its
industrial/commercial PSRG.

The remaining SVOC constituents detected in soil were at concentrations below NC DEQ
PSRGs.

METALS CONSTITUENTS IN SOIL

Arsenic was detected in the five (5) soil samples collected on the northeastern portion of
the Subject Property (S-1 through S-5) at concentrations above the NC DEQ residential
PSRG of 0.68 mg/kg and the NC DEQ industrial/commercial PSRG of 3.0 mg/kg.
However, the detected concentrations of Arsenic are below the mean concentration
reported to be naturally occurring in the eastern conterminous United States based on
the observed background concentrations in Element Concentrations in Soils and Other
Surface Materials of the Conterminous United States, Hansford T. Shacklette and
Josephine G. Boerngen, United States Geological Survey, 1984.

Total Chromium was detected in soil samples S-1 through S-5 at concentrations above
the most stringent NC DEQ PSRGs for Hexavalent Chromium. However, there have
been no known or suspected historical source of Hexavalent Chromium at the Subject
Property. Consequently, the less stringent Trivalent Chromium PSRGs have been used
for the purposes of this report.

The remaining detections of metals in soil were at concentrations below the NC DEQ
PRSGs.

VOC CONSTITUENTS IN GROUNDWATER

Naphthalene, Tetrachloroethylene (PCE) and Trichloroethylene (TCE) were detected in a
groundwater sample collected on the northeastern portion of the Subject Property (S-2)
above their NC DEQ 15A NCAC 02L .0202 Groundwater Standards.

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The remaining VOC constituents detected in groundwater were at concentrations below
NC DEQ 15A NCAC 02L .0202 Groundwater Standards.

SVOC CONSTITUENTS IN GROUNDWATER

The SVOC constituents detected in groundwater were at concentrations below NC DEQ
15A NCAC 02L .0202 Groundwater Standards.

METALS CONSTTIUENTS IN GROUNDWATER

The Chromium detected in groundwater sample collected on the southwestern portion
of the Subject Property (S-4) was at a concentration above its NC DEQ 15A NCAC 02L
.0202 Groundwater Standard.

The remaining metals constituents detected in groundwater were at concentrations
below NC DEQ 15A NCAC 02L .0202 Groundwater Standards.

Chromium occur naturally in Piedmont geology soils. Consequently, NOVA believes
that the concentrations of metals detected in the groundwater are likely associated
with excess sediment/background concentrations in the collected groundwater and
are not due to the historic operations on the Subject Property.

Based on the findings of the previous assessments and NOVA’s Phase I and Limited
Phase II ESAs, the Subject Property was entered into the NC DEQ Brownfields Programs
via a Brownfields Property Application dated September 17, 2020 and an amended
Brownfields Property Application dated January 18, 2021.

As part of the Brownfields Application process, Hart & Hickman, PC (H&H), on behalf
of the seller of the Subject Property, Gas-Fired Products, Inc., submitted a Site
Operations Plan (SOP)-Revision 1 dated December 10, 2020 to the NCDEQ
Brownfields Program. In the SOP, H&H provided details of the chemicals used at the
Subject Property. Gas Fired Products, Inc. is continuing operations at the Subject
Property after Cousins Tremont Doggett, LP take possession of the Subject Property.
As such, the NC DEQ Brownfield Program has indicated that chemical usage by Gas
Fired Products, Inc. will need to be discontinued and no storage of chemicals is to be
allowed at the Subject Property. The NC DEQ has requested that Compliance Audits
be completed on a quarterly basis to assess Gas Fired Products, Inc’s adherence to
the SOP.

NOVA prepared an Environmental Site Assessment Work Plan for supplemental
subsurface assessment of the Doggett Street & West Tremont Avenue Site dated June
11, 2021. This work plan was approved by the NC DEQ Brownfields Program on July 15,
2021.
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NOVA’s Supplemental Subsurface Assessment was conducted on the Subject Property
to further assess the potential impact of the identified RECs on soil, groundwater, and
soil gas at the Subject Property.

1.2 LIMITATIONS

NOVA has performed this assessment in general accordance with ASTM 1903-19 and
the North Carolina Department of Environmental Quality (NCDEQ) Brownfields
Program, which is a limited inquiry into a property's environmental status and is not
sufficient to discover every potential source of environmental liability or environmental
impact, if any, of the property to be evaluated. No assessment can wholly eliminate
uncertainty regarding the potential for Recognized Environmental Conditions (RECs) in
connection with a property. Performance of this assessment is intended to reduce,
but not eliminate, uncertainty regarding the potential for RECs in connection with a
property, and this practice recognizes reasonable limits of time and cost.

The level of inquiry is variable. Not every property will warrant the same level of
assessment. Consistent with good commercial or customary practices, the
appropriate level of assessment will be guided by the type of property subject to
assessment, the expertise and risk tolerance of Cousins Tremont Doggett LP (Client or
User), and the information developed in the course of the inquiry.

NOVA’s assessment represents our professional opinion, only. Therefore, NOVA
cannot, under any circumstances, make a statement of warranty or guarantee,
expressed or implied, that RECs, environmental impairment, or environmental impacts
are limited to those that are discovered while we are performing the Supplemental
Subsurface Assessment .

1.3 USER RELIANCE

NOVA’s Supplemental Subsurface Assessment report, along with the findings and
conclusions contained in the report, either in completed form, summary form, or by
extraction, is prepared, and intended, for the sole use of the Client and therefore may
not contain sufficient information for other purposes or parties. The Client is the only
intended beneficiary of this report. The contents of NOVA's report will continue to be
the property of NOVA. NOVA's report may not be disclosed to, used by, or relied upon
by, any person or entity other than the Client without the express written consent of
NOVA.

Authorization for disclosure to a third party or authorization for third-party reliance on
a final report of any report will be considered by NOVA upon the written request of the
Client. NOVA reserves the right to deny authorization to allow disclosure or reliance of
NOVA's report to third parties.
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2.0 SUPPLEMENTAL SUBSURFACE ASSESSMENT

Cousins Tremont Doggett, LP requested that NOVA conduct a Supplemental Subsurface
Assessment in general accordance with NOVA’s June 11, 2021, Environmental Site Assessment
Work Plan to further assess the potential impacts to soil, groundwater and soil gas on the Subject
Property from the above referenced RECs. Our investigation procedures, findings, conclusions,
and recommendations are presented in the following sections. A receptor survey was completed
and included in Appendix F.

2.1 SOIL BORING INSTALLATION AND SOIL SAMPLING

On August 30 & 31, 2021, NOVA provided oversight for the advancement of four (4) soil
borings (S-6 through S-9) on the Subject Property. Borings were advanced to termination
depths between 12 feet and 30 feet below ground surface (bgs), using direct push
technology (DPT). A Boring and Sampling Location Map is provided as Figure 4 in
Appendix A.

Soil boring samples were collected at two (2) feet bgs and then at every four to five (4-5)
feet bgs using a 1.5-inch dual tube sampling liner. The soil samples were field-screened
using a Photo-Ionization Detector (PID) for the presence of organic vapors. Field
screening and/or visual observations did not readily indicate impacted soil.
Consequently, one (1) soil sample from the deepest portion of the unsaturated zone of
each boring was submitted for laboratory analysis. Samples were collected from the
following depths:

Soil Boring Depth
(in feet below ground surface)
S-6 14-15
S-7 10-11
S-8 11-12
S-9 7-8

No elevated PID readings were identified in the soil collected from the four (4) soil borings
advanced on the Subject Property.

A total of four (4) soil samples were collected from soil borings S-6 through S-9 and were
submitted to Waypoint Analytical (Waypoint) of Charlotte, North Carolina for the following
analyses:

• Volatile Organic Compounds (VOCs) by United States Environmental Protection
Agency (US EPA) Solid Waste (SW)-846 Method 8260D,
• Semi-Volatile Organic Compounds (SVOCs) by USEPA SW-846 Method 8270E,
• Resource Conservation and Recovery Act (RCRA) Metals by USEPA SW-846 Method
6020B and 7471B, and
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• Hexavalent Chromium by USEPA SW-846 Method 7199.
2.2 GROUNDWATER SAMPLING

Four (4) temporary Monitoring Wells (MWs) were installed using direct push technology
to the desired depth. The MWs were constructed of two (2) inch PolyVinyl Chloride (PVC)
screen and riser by a North Carolina certified well driller. Between fifteen (15) and twenty
(20) feet of machine-slotted screen was installed. New polyethylene tubing was lowered
into the temporary monitoring wells and the boreholes were purged of three (3) to five (5)
volumes using a peristaltic pump. Once water was allowed to recharge, groundwater
samples were obtained for laboratory analysis. Four (4) groundwater samples (MW-1
through MW-4) were obtained for laboratory analysis. The collected groundwater
samples were then submitted to Waypoint for the following analyses:

• VOCs by USEPA SW-846 Method 8260D,
• SVOCs by USEPA SW-846 Method 8270E, and
• RCRA Metals by USEPA SW-846 Method 6020B and 7470A.

2.3 SOIL GAS SAMPLING

NOVA collected six (6) soil gas samples and one (1) sub-slab sample from the Subject
Property. The soil gas monitoring points were installed utilizing direct push technology
to a maximum depth of five (5) feet below ground surface (bgs). Following the
advancement of each soil gas sampling point, a length of 0.250-inch Interior Diameter
(ID) flexible nylon tubing equipped with a particulate filter was inserted into the
sampling point. The soil gas monitoring points were then filled with approximately four
(4) inches of industrial quartz sand. The remaining portion of the sampling points were
filled with granular bentonite in three (3) inch increments and hydrated with water to
create an airtight seal between the sampling point and the atmosphere. Collected soil
vapor samples were submitted to Waypoint for the following analysis:

• VOCs by US EPA Method TO-15.

2.4 QUALITY CONTROL AND QUALITY ASSURANCE METHODS

Field procedures and protocols used during the ESA were performed in general
accordance with those prescribed in ASTM International (ASTM) Standard Practice for
Environmental Site Assessments: Phase II Environmental Site Assessment Process,
Designation: E1903-19, USEPA Region IV Science and Ecosystem Support Division
(SESD) guideline document LSASDPROC-300-R4 dated June 11, 2020, for soil sampling,
and guideline document SESDPROC-301-R4 dated April 26, 2017, for groundwater
sampling.

Supplemental Subsurface Assessment January 14, 2022
Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

Page 12

Samples were labeled with a distinct sample identification number, the sampler’s initials,
and the date of collection. Each sample container was properly sealed, labeled, and
placed in an ice chest (with ice) and transport to an accredited laboratory (Waypoint)
which used USEPA SW-846 protocols. A properly completed chain-of-custody form was
initiated in the field and accompanied the samples when submitted to the laboratory for
analyses. Copies of the chain-of custody form(s) are shown in Appendix C and D.

Supplemental Subsurface Assessment January 14, 2022
Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

Page 13

3.0 RESULTS

3.1 SOIL LABORATORY RESULTS

The complete laboratory analytical reports for soil samples S-6(14-15), S-7(10-11),
S-8(11-12), S-9(7-8) and Dup-1 (a duplicate of soil sample S-6 (14-15’)) are included in
Appendix C.

3.1.1 VOC Constituents

The following VOC constituent was detected in soil at a concentration that exceeded the
laboratory reporting limit in soil samples S-6(14-15), S-7(10-11), S-8(11-12), S-9(7-8)
and Dup-1 (a duplicate of soil sample S-6 (14-15’)):

Residential
Health
Based
PSRG
Protection of
Groundwater
PSRG
S-6
(14-15’)
S-7
(10-11’)
S-8
(11-12’)
S-9
(7-8’) Dup-1
Acetone 12,000 25 0.006J 0.024 BRL 0.023J 0.014J
n-Butylbenzene 780 4.5 BRL BRL 1.45 BRL BRL
Sec-Butyl benzene 1,600 4.1 BRL BRL 0.656 BRL BRL
Tert-Butyl benzene 1,600 3.1 BRL BRL 0.113J BRL BRL
Carbon Disulfide 160 4.1 BRL BRL BRL 0.001J BRL
Ethylbenzene 6.1 13 BRL BRL 0.488 BRL BRL
Isopropylbenzene NE NE BRL BRL 0.370 0.001J BRL
Methyl Ethyl Ketone
(MEK) 5,500 17 BRL 0.002J BRL BRL 0.001J
Methylene Chloride 58 0.025 0.010J 0.009J BRL 0.002J 0.010J
Naphthalene 2.1 0.39 BRL BRL 11.2 BRL BRL
n-Propylbenzene NE NE BRL BRL 0.889 BRL BRL
Tetrachloroethene 17 0.0063 BRL BRL BRL 0.002J BRL
1,3,5-
Trimethylbenzene 56 11 BRL BRL 0.370 0.001J BRL

Based on North Carolina Department of Environmental Quality (NCDEQ) Preliminary Soil Remediation
Goals (PSRG)
Results in milligrams per kilograms (mg/kg)
BRL Below Laboratory Reporting Limits
NE no threshold established
J Laboratory Estimated Quantity
BOLD exceeds the Residential Health Based PSRG
Highlighted and Italic exceeds the Protection of Groundwater PSRG
Supplemental Subsurface Assessment January 14, 2022
Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

Page 14

The detected Acetone in the soil samples is believed to represent a laboratory relic
originating from the laboratory’s use of isopropyl alcohol or a product of the oxidation
of organics in the soil as a result of the sodium bisulfate sample preservation
technique.

Naphthalene was identified in soil sample S-8(11-12) above its Residential and
Protection of Groundwater North Carolina Department of Environmental Quality (NCDEQ)
Preliminary Soil Remediation Goals (PSRGs).

1,3,5-Trimethylbenzene, Tetrachloroethene, n-Propylbenzene, Isopropylbenzene,
Ethylbenzene, Carbon Disulfide, Sec-Butyl benzene, Tert-Butyl benzene, n-Butylbenzene
Methyl Ethyl Ketone (MEK), Methylene Chloride and n-Hexane were detected at
concentrations below NCDEQ PSRGs. No additional VOC constituents were detected in
the soil samples collected at concentrations that exceeded the laboratory reporting limits.

3.1.2 SVOC Constituents

The following SVOC constituents were detected in soil at concentrations that exceeded
the laboratory reporting limits in soil samples S-8(11-12) and S-9(7-8):

Residential
Health Based
PSRG
Protection of
Groundwater PSRG
S-8
(11-12’)
S-9
(7-8’)
Fluorene NE NE 0.737J BRL
1-Methylnaphthalene 18 0.11 6.17 0.224J
2-Methylnaphthalene 48 3.1 6.32 BRL
Naphthalene 2.1 0.39 2.02 BRL
Phenanthrene NE NE 1.69 1.69
Based on North Carolina Department of Environmental Quality (NCDEQ) Preliminary Soil Remediation
Goals (PSRG)
Results in milligrams per kilograms (mg/kg)
BRL Below Laboratory Reporting Limits
NE no threshold established
J Laboratory Estimated Quantity
BOLD exceeds the Residential Health Based PSRG
Italic exceeds the Protection of Groundwater PSRG

Fluorene and Phenanthrene were detected at concentrations below the NCDEQ PSRGs.
1-Methylnaphthalene, 2-Methylnaphthalene, and Naphthalene were detected at
concentrations below Residential PSRGs but above Protection of Groundwater PSRGs.
No additional SVOC constituents were detected in the soil samples collected at
concentrations that exceeded the laboratory reporting limits.
Supplemental Subsurface Assessment January 14, 2022
Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

Page 15

3.1.3 Metals Constituents

The following Metals constituents were detected in soil at concentrations that exceeded
the laboratory reporting limits in soil samples S-6(14-15), S-7(10-11), S-8(11-12),
S-9(7-8) and Dup-1 (a duplicate of soil sample S-6 (14-15’)):

Residential
Health Based
PSRG
Protection of
Groundwater
PSRG
S-6
(14-15’)
S-7
(10-11’)
S-8
(11-12’)
S-9
(7-8’) Dup-1
Arsenic 0.68 5.8 0.763J 2.80 2.65 2.09 1.04J
Barium 3,100 580 133 39.0 63.2 345 169
Cadmium 14.0 3.0 BRL BRL BRL BRL BRL
Chromium
(VI) 0.31 6.5 BRL 1.9 BRL BRL BRL
Chromium
(total) NE NE 76.6 74.9 47.2 53.1 88.7
Lead 400 270 2.64 17.4 17.3 4.20 2.94
Selenium 78 2.1 2.01J BRL 1.27J 5.76 2.96
Mercury 2.3 1.0 BRL 0.0921 0.0553 BRL BRL
Based on North Carolina Department of Environmental Quality (NCDEQ) Preliminary Soil Remediation
Goals (PSRG)
Results in milligrams per kilograms (mg/kg)
BRL Below Laboratory Reporting Limits
NE no threshold established
J Laboratory Estimated Quantity
BOLD exceeds the Residential Health Based PSRG
Italic exceeds the Protection of Groundwater PSRG

The detected concentrations of Barium, Lead and Mercury in the soil samples collected
are below their respective NC DEQ PSRGs. The detected concentrations of Arsenic in
soil samples S-6(14-15), S-7(10-11), S-8(11-12), S-9(7-8) and Dup-1 and Hexavalent
Chromium in S-7 (10-11’) are above their Residential NC DEQ PSRG. The detected
concentration of Selenium in soil samples S-9(7-8) and Dup-1 are above their Protection
of Groundwater NC DEQ PSRG.

The detected concentrations of Arsenic in soil samples S-6(14-15), S-7(10-11),
S-8(11-12), S-9(7-8) and Dup-1 are above the residential PSRGs; however, they are
below the mean concentration (11 mg/kg for Arsenic) reported to be naturally
occurring in Piedmont soils based on the observed background concentrations
reported in Elements in South Carolina Inferred Background Soil and Stream
Sediments Samples, Judy L. Canova, South Carolina Department of Health and
Environmental Control (SC DHEC), 1999, which can be a comparison for North
Carolina. Consequently, we believe the detected concentrations of Arsenic are
consistent with naturally occurring background concentrations.
Supplemental Subsurface Assessment January 14, 2022
Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

Page 16

The detected concentrations of Selenium in soil sample S-9 (7-8’) are above the naturally
occurring Selenium concentrations reported in Elements in South Carolina Inferred
Background Soil and Stream Sediments Samples, Judy L. Canova, South Carolina
Department of Health and Environmental Control (SC DHEC), 1999.

3.2 GROUNDWATER LABORATORY RESULTS

The complete laboratory analytical reports for groundwater samples MW-1, MW-2,
MW-3, MW-4 and Dup-1 (a duplicate of groundwater sample MW-4) are included in
Appendix D.

3.2.1 VOC Constituents

The following VOC constituents were detected at concentrations that exceeded the
laboratory reporting limits in groundwater samples MW-1, MW-2, MW-3, MW-4 and
Dup-1 (a duplicate of groundwater sample MW-4):

15A NCAC
02L .0202
Groundwater
Standards
MW-1 MW-2 MW-3 MW-4 Dup-1
Acetone 6,000 10.1 13.7 6.07 7.02 7.99
Carbon Disulfide 700 BRL BRL BRL 0.458 BRL
Methyl Ethyl Ketone
(MEK) 4,000 0.928J 1.16J BRL BRL BRL
Naphthalene 6 BRL BRL 0.828 BRL BRL
Trichloroethene
(TCE) 3 BRL BRL BRL 0.461 0.516
Results in micrograms per liter (ug/L)
NA not applicable
NE no threshold established
BRL Below Laboratory Reporting Limits

Acetone was identified in each of the groundwater samples collected. The solvent Methyl
Ethyl Ketone (MEK) was detected in groundwater samples MW-1 and MW-2, Carbon
Disulfide was identified in MW-4, Naphthalene was detected in MW-3, and the solvent
Trichloroethene (TCE) was detected in groundwater samples MW-4 and Dup-1. The
concentrations of each constituent identified were below their respective NCDEQ 15A
NCAC 02L.0202 Groundwater Standards (2L Standards).

Supplemental Subsurface Assessment January 14, 2022
Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

Page 17

3.2.2 SVOC Constituents

No SVOC constituents were detected at concentrations that exceeded the laboratory
reporting limits in groundwater samples MW-1, MW-2, MW-3, MW-4 and Dup-1.

3.2.3 Metals Constituents

The following metals constituent was detected at a concentration that exceeded the
laboratory reporting limits in groundwater sample MW-1, MW-2, MW-3, MW-4 and
Dup-1:

15A NCAC 02L
.0202
Groundwater
Standards
MW-1 MW-2 MW-3 MW-4 Dup-1
Arsenic 10 4.28J 1.42J 0.631J 0.538J 0.500J
Barium 700 388 111 101 141 139
Cadmium 2 BRL BRL 0.179J BRL BRL
Chromium 10 36 41.1 6.81 50.0 50.7
Lead 15 25.7 1.49 3.65 0.663J 0.676J
Selenium 20 BRL 2.73J 0.746J BRL BRL
Based on NCDEQ 15A NCAC 02l .0202 Groundwater Standards (2L Standards)
Results in micrograms per liter (µg/L)
BOLD exceeds the 2L Standards
NE no threshold established
BRL Below Laboratory Reporting Limits
J Laboratory Estimated Quantity

Chromium was detected in groundwater samples MW-1, MW-2 MW-4 and Dup-1 at
concentrations above its NC DEQ 2L Standard. Lead was detected in groundwater
sample MW-1 at a concentration above its NC DEQ 2L Standard. The remaining metals
concentrations detected were below their respective NC DEQ 2L Standards.

3.3 GROUNDWATER ELEVATIONS or DEPTHS

Following groundwater sampling activities on September 1, 2021, NOVA surveyed soil
borings MW-1 through MW-4. NOVA also allowed groundwater in the wells to equilibrate
overnight before collecting groundwater elevation data. The soil boring and groundwater
elevations are detailed in the table below:

Supplemental Subsurface Assessment January 14, 2022
Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

Page 18

Well Location Ground Surface Elevation* Groundwater Elevation*
MW-1 96.92 83.39
MW-2 104.64 95.16
MW-3 100.00 88.93
MW-4 98.47 87.99
* feet below arbitrary on-site benchmark of 100 feet

Based on the measured groundwater elevations, groundwater at the Subject Property
flows to the north-northwest, toward Irwin Creek. A Potentiometric Surface Map of the
Subject Property is included as Figure 5 in Appendix A.

3.4 SOIL GAS LABORATORY RESULTS

The complete laboratory analytical reports for soil gas samples SV-1, SV-2, SV-3, SV-4,
SV-5, SV-6, SV-7 and Dup-1 (a duplicate of soil gas sample SV-5) are included in
Appendix D.

3.4.1 VOC Constituents

The following VOC constituents were detected at concentrations that exceeded the
laboratory reporting limits in groundwater samples SV-1, SV-2, SV-3, SV-4, SV-5, SV-6, SV-
7 and Dup-1:

SGSL SV-1 SV-2 SV-3 SV-4 SV-5 SV-6 SV-7 Dup-1
Acetone 220,000 33.4 138 78.3 254 117 99.0 90.1J 119
Benzene 12 1.41J 66.5 29.1 34.3J 23.3J 34.6 10.4J 24.0J
Carbon disulfide 4,900 0.380J 70.1J 14.9 127J 16.7J 176 8.41J 17.9J
Carbon Tetrachloride 16 0.547J BRL 0.585J BRL BRL BRL BRL BRL
Chloroethane 70,000 BRL BRL 1.37 BRL BRL BRL BRL BRL
Chloroform 4.1 BRL BRL 1.87J BRL BRL 16.5J BRL BRL
Chloromethane 630 0.747J BRL 0.599J BRL BRL 9.37J BRL BRL
Cyclohexane 42,000 3.09J 50.2J 7.48 1,600 53.6J 164 32.1J 58.5J
1,4-Dichlorobenzene 8.5 BRL BRL 13.7 BRL BRL 12.0J BRL BRL
Dichlorodifluoromethane 700 3.10 BRL 2.78 BRL BRL BRL BRL BRL
trans-1,2-
Dichloroethene 280 BRL BRL 2.93 BRL BRL BRL BRL BRL
Ethylbenzene 37 0.560J 518 8.08 1,210 667 1,310 409 710
4-Ethyltoluene NE BRL 33.6J 0.796J BRL 35.9J 25.0J 34.1J 37.3J
1,1,2-Trichloro-1,2,2,-
trifluoroethane 35,000 0.613J BRL 5.60 BRL BRL BRL BRL BRL
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Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

Page 19

SGSL SV-1 SV-2 SV-3 SV-4 SV-5 SV-6 SV-7 Dup-1
Heptane 2,800 0.680J 112 13.7 3,800 128 561 67.0 165
n-Hexane 4,900 1.06J 46.7 13.5 115 12.3J 34.1J BRL 12.0J
Isopropyl Alcohol 1,400 4.88J 14.7J 9.25 82.1J 12.2J 11.7J 14.1J 11.5J
2-Butanone (MEK) 35,000 3.26 19.9J 12.8 55.6J BRL 13.5J 6.43J 12.5
Methyl tert-butyl ether
(MTBE) 360 1.12J BRL 1.20J BRL BRL BRL BRL BRL
4-Methyl-2-pentanone
(MIBK) 21,000 0.664J 13.4J 3.41 BRL BRL BRL BRL BRL
Methylene Chloride 3,400 1.01J BRL 0.973 BRL BRL 15.1J BRL BRL
Naphthalene 2.8 BRL 11.7J BRL BRL BRL BRL BRL BRL
Propene 21,000 2.58 298 75.8 360 BRL 179 BRL BRL
Styrene 7,000 13.1 BRL 3.48 BRL BRL BRL BRL BRL
Tetrachloroethene (PCE) 280 2.00J 4,330 1,650 1,400 3,020 2,470 2,210 3,070
Tetrahydrofuran NE BRL 11.0J BRL BRL BRL BRL BRL BRL
Toluene 35,000 1.79J 460 153 432 367 478 221 376
Trichloroethene (TCE) 14 BRL BRL 1.59J BRL BRL BRL BRL BRL
Trichlorofluoromethane NE 2.43J BRL 12.0 BRL 9.33J 9.21J BRL BRL
1,2,4-Trimethlbenzene 420 BRL 32.6J 1.95J BRL 29.1J 13.6J 35.6J 31.8J
1,3,5-Trimethlbenzene 420 BRL 115 0.826J BRL 117 72.8 116 125
Vinyl Chloride 5.6 BRL BRL 0.828J BRL BRL BRL BRL BRL
Xylene (Total) 700 1.79 1,320 26.9 1,650 1,650 2,700 1,090 1,770
Based on NCDEQ Division of Waste Management Residential Vapor Intrusion Screening Concentrations
for Sub-Slab and Exterior Soil Gas Screening Level (SGSL)
Results in micrograms per liter (ug/m3)
NA not applicable
NE no threshold established
BRL Below Laboratory Reporting Limits

Select concentrations of Benzene, Chloroform, 1,4-Dichlorobenzene, Ethylbenzene,
Heptane, Naphthalene, Tetrachloroethene (PCE), and Xylene (Total) in one (1) or more
soil gas samples were detected above the NC DEQ residential Soil Gas Screening Level
(SGSL). The remaining listed detections of VOCs were individually each below their
respective NC DEQ residential SGSL. NOVA then used the detected constituent
concentrations to complete the NC DEQ Risk Calculator for vapor intrusion for Residential
Soil Gas to Indoor Air. The Risk Calculator results for seven (7) of the eight (8) samples
indicate a Carcinogenic Risk (CR) and Non-Carcinogenic Hazard Quotient (HQ) equal to or
above the NC DEQ regulatory threshold for CR of 1.0E-06 and the NC DEQ regulatory
threshold Non-Carcinogenic HQ of 0.2. The results of the risk calculator are provided in
Appendix D.

Supplemental Subsurface Assessment January 14, 2022
Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

Page 20

4.0 CONCLUSIONS

NOVA performed a Limited Phase II ESA on the approximately 2.441-acres property located at
305 Doggett Street and 242/306 West Tremont Avenue in Charlotte, Mecklenburg County, North
Carolina (Subject Property). The study was performed in a manner generally consistent with the
requirements of the ASTM 1903-19 and generally accepted industry standards. A receptor
survey was completed and included in Appendix F.

4.1 SOIL DETECTIONS

4.1.1 VOCs

The detected Acetone in the soil samples is believed to represent a laboratory relic
originating from the laboratory’s use of isopropyl alcohol or a product of the oxidation
of organics in the soil as a result of the sodium bisulfate sample preservation
technique.

Naphthalene was identified in soil sample S-8(11-12) above its Residential and
Protection of Groundwater North Carolina Department of Environmental Quality (NCDEQ)
Preliminary Soil Remediation Goals (PSRGs).

1,3,5-Trimethylbenzene, Tetrachloroethene, n-Propylbenzene, Isopropylbenzene,
Ethylbenzene, Carbon Disulfide, Sec-Butyl benzene, Tert-Butyl benzene, n-Butylbenzene
Methyl Ethyl Ketone (MEK), Methylene Chloride and n-Hexane were detected at
concentrations below NCDEQ PSRGs. No additional VOC constituents were detected in
the soil samples collected at concentrations that exceeded the laboratory reporting limits.

4.1.2 SVOCs

Fluorene and Phenanthrene were detected at concentrations below the NCDEQ PSRGs.
1-Methylnaphthalene, 2-Methylnaphthalene, and Naphthalene were detected at
concentrations below Residential PSRGs but above Protection of Groundwater PSRGs.
No additional SVOC constituents were detected in the soil samples collected at
concentrations that exceeded the laboratory reporting limits.

4.1.3 Metals

The detected concentrations of Barium, Lead and Mercury in the soil samples collected
are below their respective NC DEQ PSRGs. The detected concentrations of Arsenic in
soil samples S-6(14-15), S-7(10-11), S-8(11-12), S-9(7-8) and Dup-1 and Hexavalent
Chromium in S-7 (10-11’) are above their Residential NC DEQ PSRG. The detected
Supplemental Subsurface Assessment January 14, 2022
Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

Page 21

concentration of Selenium in soil samples S-9(7-8) and Dup-1 are above their Protection
of Groundwater NC DEQ PSRG.
The detected concentrations of Arsenic in soil samples S-6(14-15), S-7(10-11),
S-8(11-12), S-9(7-8) and Dup-1 are above the residential PSRGs; however, they are
below the mean concentration (11 mg/kg for Arsenic) reported to be naturally
occurring in Piedmont soils based on the observed background concentrations
reported in Elements in South Carolina Inferred Background Soil and Stream
Sediments Samples, Judy L. Canova, South Carolina Department of Health and
Environmental Control (SC DHEC), 1999, which can be a comparison for North
Carolina. Consequently, we believe the detected concentrations of Arsenic are
consistent with naturally occurring background concentrations.

The detected concentrations of Selenium in soil sample S-9 (7-8’) are above the naturally
occurring Selenium concentrations reported in Elements in South Carolina Inferred
Background Soil and Stream Sediments Samples, Judy L. Canova, South Carolina
Department of Health and Environmental Control (SC DHEC), 1999.

4.2 GROUNDWATER DETECTIONS

4.2.1 VOCs

Acetone was identified in each of the groundwater samples collected. The solvent Methyl
Ethyl Ketone (MEK) was detected in groundwater samples MW-1 and MW-2, Carbon
Disulfide was identified in MW-4, Naphthalene was detected in MW-3, and the solvent
Trichloroethene (TCE) was detected in groundwater samples MW-4 and Dup-1. The
concentrations of each constituent identified were below their respective NCDEQ 15A
NCAC 02L.0202 Groundwater Standards (2L Standards).

4.2.2 SVOCs

No SVOC constituents were detected at concentrations that exceeded the laboratory
reporting limits in groundwater samples MW-1, MW-2, MW-3, MW-4 and Dup-1.

4.2.3 Metals

Chromium was detected in groundwater samples MW-1, MW-2 MW-4 and Dup-1 at
concentrations above its NC DEQ 2L Standard. Lead was detected in groundwater
sample MW-1 at a concentration above its NC DEQ 2L Standard. The remaining metals
concentrations detected were below their respective NC DEQ 2L Standards.

Supplemental Subsurface Assessment January 14, 2022
Doggett Street & West Tremont Avenue Site NOVA Project Number 3021011

Page 22

4.3 SOIL GAS DETECTIONS

4.3.1 VOCs

Select concentrations of Benzene, Chloroform, 1,4-Dichlorobenzene, Ethylbenzene,
Heptane, Naphthalene, Tetrachloroethene (PCE), and Xylene (Total) in one (1) or more
soil gas samples were detected above the NC DEQ residential Soil Gas Screening Level
(SGSL). The remaining listed detections of VOCs were individually each below their
respective NC DEQ residential SGSL. NOVA then used the detected constituent
concentrations to complete the NC DEQ Risk Calculator for vapor intrusion for
Residential Soil Gas to Indoor Air. The Risk Calculator results for seven (7) of the eight
(8) samples indicate a Carcinogenic Risk (CR) and Non-Carcinogenic Hazard Quotient
(HQ) equal to or above the NC DEQ regulatory threshold for CR of 1.0E-06 and the NC
DEQ regulatory threshold Non-Carcinogenic HQ of 0.2.

APPENDIX A

FIGURES

FIGURE 1
SITE LOCATION MAP

SOURCE: Google Maps
SCALE: As Shown
COUSINS TREMONT DOGGETT LP
Doggett Street/West Tremont Ave Site
Charlotte, North Carolina
NOVA Project Number 3021011

Approximate Subject
Property Boundary
Subject Property
Subject Property

FIGURE 2
SITE MAP

SOURCE: www.google.com
SCALE: As Shown
COUSINS TREMONT DOGGETT LP
Doggett Street/West Tremont Avenue
Charlotte, Mecklenburg County, North Carolina
NOVA Project Number 3021011

Approximate Subject
Property Boundary
Approximate Location of
Former Heating Oil UST

FIGURE 3
TOPOGRAPHIC MAP
SOURCE: EDR 7.5-Minute Series Topographic Quadrangles (2) 2013, Charlotte East and West, North Carolina SCALE: 1:24,000
COUSINS TREMONT DOGGETT LP
Doggett Street/West Tremont Ave Site
Charlotte, North Carolina
NOVA Project Number 3021011

Subject Property

FIGURE 4
BORING AND SAMPLING LOCATION MAP

SOURCE: www.google.com
SCALE: As Shown
COUSINS TREMONT DOGGETT. LP
Doggett Street/West Tremont Avenue
Charlotte, Mecklenburg County, North Carolina
NOVA Project Number 3021011

Approximate Subject
Property Boundary
Soil Boring and Sampling Location 8/30/21
Approximate Location of
Former Heating Oil UST
S-8
S-6 S-7
S-9
Soil Vapor Monitoring Point 8/30/21
SV-1
SV-2
SV-3 SV-4
SV-5
Groundwater Monitoring Point 8/31/21
MW-1
MW-2
MW-3
Soil Boring and Sampling Location 7/21/2020
S-1
S-2 S-3
S-4
S-5
Soil Vapor Monitoring Point 7/21/2020
VMP-2
VMP-1
VMP-3
VMP-4
VMP-5
VMP-6
MW-4
SubSlab Vapor Monitoring Point 8/30/21
SV-7
SV-6

FIGURE 5
GROUNDWATER POTENTIOMETRIC SURFACE MAP

SOURCE: www.google.com
SCALE: As Shown
COUSINS TREMONT DOGGETT. LP
Doggett Street/West Tremont Avenue
Charlotte, Mecklenburg County, North Carolina
NOVA Project Number 3021011

Approximate Subject
Property Boundary
Groundwater Monitoring Well 9/1/21
MW-1
MW-2
MW-3
MW-4
(73.33’) Groundwater Elevation
(95.16’)
(87.99’)
(88.93’)
(83.39’)
93.00’
91.00’
85.00’
83.00’
Groundwater
Elevation
Contours
87.00’
89.00’
95.00’

APPENDIX B

BORING LOGS AND WELL LOGS
TEMPORARY MONITORING WELL
CONSTRUCTION DIAGRAM

Logged By: S. Aldis Client: Cousins Tremont Doggett LP
Drilling Contractor: Geologic Exploration Project Name: Doggett St & West Tremont Ave
Well Number: MW-1 Project Number: 3021011
Date Installed: August 30, 2021
Comments: Refusal at 21’.

Depth in Reference to Ground Surface:

0’

5’

10’

15’

20’

25’

30’

35’

40’

Well Type: PVC
Well Diameter: 2”
Coupling Type: Threaded
Total Well Length: 21’
Screen Type: PVC
Screen Diameter: 2”
Screen Length: 10’
Screen Slot Size: 0.010”
Ground Surface 

Groundwater: 13.53’

 Top of Well Screen: 11’

 Bottom of Monitoring Well: 21’

TEMPORARY MONITORING WELL
CONSTRUCTION DIAGRAM

Logged By: S. Aldis Client: Cousins Tremont Doggett LP
Drilling Contractor: Geologic Exploration Project Name: Doggett St & West Tremont Ave
Well Number: MW-2 Project Number: 3021011
Date Installed: August 31, 2021
Comments: Refusal at 30’.

Depth in Reference to Ground Surface:

0’

5’

10’

15’

20’

25’

30’

35’

40’

Well Type: PVC
Well Diameter: 2”
Coupling Type: Threaded
Total Well Length: 30’
Screen Type: PVC
Screen Diameter: 2”
Screen Length: 20’
Screen Slot Size: 0.010”
Ground Surface 

Groundwater: 9.48’

 Bottom of Monitoring Well: 30’

 Top of Well Screen: 10’

TEMPORARY MONITORING WELL
CONSTRUCTION DIAGRAM

Logged By: S. Aldis Client: Cousins Tremont Doggett LP
Drilling Contractor: Geologic Exploration Project Name: Doggett St & West Tremont Ave
Well Number: MW-3 Project Number: 3021011
Date Installed: August 30, 2021
Comments: Terminated at 25’.

Depth in Reference to Ground Surface:

0’

5’

10’

15’

20’

25’

30’

35’

40’

Well Type: PVC
Well Diameter: 2”
Coupling Type: Threaded
Total Well Length: 25’
Screen Type: PVC
Screen Diameter: 2”
Screen Length: 20’
Screen Slot Size: 0.010”
Ground Surface 

Groundwater: 11.07’

 Bottom of Monitoring Well: 25’

 Top of Well Screen: 5’

TEMPORARY MONITORING WELL
CONSTRUCTION DIAGRAM

Logged By: S. Aldis Client: Cousins Tremont Doggett LP
Drilling Contractor: Geologic Exploration Project Name: Doggett St & West Tremont Ave
Well Number: MW-4 Project Number: 3021011
Date Installed: August 30, 2021
Comments: Refusal at 30’.

Depth in Reference to Ground Surface:

0’

5’

10’

15’

20’

25’

30’

35’

40’

Well Type: PVC
Well Diameter: 2”
Coupling Type: Threaded
Total Well Length: 30’
Screen Type: PVC
Screen Diameter: 2”
Screen Length: 20’
Screen Slot Size: 0.010”
Ground Surface 

Groundwater: 10.48’

 Bottom of Monitoring Well: 30’

 Top of Well Screen: 10’

SOIL TEST BORING RECORD
Project Information:
Boring Number: S-6 Boring Elevation: NA
Date Drilled: 8/31/2021 Groundwater TOB: NA
Project Number: 3021011 Groundwater 24-hour: NA
Project Name: Doggett St & West Tremont Ave Driller: Geologic Explorations
Client: Cousins Tremont Doggett LP Drilling Method: Direct Push
Client Location: Atlanta, GA Logged By: SMA
Project Location: Charlotte, NC

N-Value Description Depth (ft) PID
Reading
Concrete and Gravel 0
Clayey Silt, red brown, moist, semi-plastic semi-stiff _
_
_
_
_ 5
_
_
_
_
_ 10
_
Silt, tan brown, moist, non-plastic, semi-stiff _
_
_
_ 15
_
_
Silt with Clay and Fine Sand, mottled brown tan black white, wet, non-plastic, _
semi-stiff _
_ 20
_
_
_
_
_ 25
_
_
_
_
_ 30
Boring Refusal 30’ _
_
_
_
_ 35
_
_
_
_
_ 40
SOIL TEST BORING RECORD
Project Information:
Boring Number: S-7 Boring Elevation: NA
Date Drilled: 8/31/2021 Groundwater TOB: NA
Project Number: 3021011 Groundwater 24-hour: NA
Project Name: Doggett St & West Tremont Ave Driller: Geologic Explorations
Client: Cousins Tremont Doggett LP Drilling Method: Direct Push
Client Location: Atlanta, GA Logged By: SMA
Project Location: Charlotte, NC

N-Value Description Depth (ft) PID
Reading
Asphalt 0
Clayey Silt, red brown, moist, semi-plastic semi-stiff _
_
_
_
_ 5
_
_
_
_
_ 10
_
_
Silt, mottled tan red brown black, moist, non-plastic, semi-stiff _
Refusal at 12’ _
_ 15
_
_
_
_
_ 20
_
_
_
_
_ 25
_
_
_
_
_ 30
_
_
_
_
_ 35
_
_
_
_
_ 40
SOIL TEST BORING RECORD
Project Information:
Boring Number: S-8 Boring Elevation: NA
Date Drilled: 8/31/2021 Groundwater TOB: NA
Project Number: 3021011 Groundwater 24-hour: NA
Project Name: Doggett St & West Tremont Ave Driller: Geologic Explorations
Client: Cousins Tremont Doggett LP Drilling Method: Direct Push
Client Location: Atlanta, GA Logged By: SMA
Project Location: Charlotte, NC

N-Value Description Depth (ft) PID
Reading
Concrete 0
Clayey Silt, red brown, dry, semi-plastic semi-stiff _
_
_
_
_ 5
_
_
_
Clay and Silt, brown, moist, plastic semi-soft, petroleum odor _
_ 10
_
_
Silt, mottled brown black, moist, non-plastic, semi-stiff _
_
_ Refusal at 14’ 15
_
_
_
_
_ 20
_
_
_
_
_ 25
_
_
_
_
_ 30
_
_
_
_
_ 35
_
_
_
_
_ 40
SOIL TEST BORING RECORD
Project Information:
Boring Number: S-9 Boring Elevation: NA
Date Drilled: 8/30/2021 Groundwater TOB: NA
Project Number: 3021011 Groundwater 24-hour: NA
Project Name: Doggett St & West Tremont Ave Driller: Geologic Explorations
Client: Cousins Tremont Doggett LP Drilling Method: Direct Push
Client Location: Atlanta, GA Logged By: SMA
Project Location: Charlotte, NC

N-Value Description Depth (ft) PID
Reading
Top soil 0
Silt, tan gray, dry, non-plastic, brittle _
Clayey Silt, red brown, moist, semi-plastic, semi-stiff _
_
_
_ 5
_
_
_
_
_ Silt, gray, moist to wet, semi-plastic, semi-stiff 10
_
_
Silt with Clay and Fine Sand, mottled tan white black brown, wet, semi-soft, _
non-plastic, micaceous _
_ 15
_
_
_
_
_ 20
_
_
_
_
_ 25
Boring Terminated at 25’ _
_
_
_
_ 30
_
_
_
_
_ 35
_
_
_
_
_ 40

APPENDIX C

SOIL AND GROUNDWATER ANALYTICAL

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/1/2021
NOVA Engineering & Environmental Steven Aldis
417 Minuet Lane Suite D Charlotte, NC, 28217
Ref: Analytical Testing
Revised Lab Report Number: 21-242-0018 Client Project Description: Doggette Site
Dear Steven Aldis:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/2/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 154
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-242-0018
Page 2 of 154
Report Number:
Sample Summary Table
Client Project Description:
21-242-0018
Doggette Site
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
08/31/2021 09:20Aqueous 94717 MW-1 09/02/2021 16:00
08/31/2021 16:47Aqueous 94718 MW-2 09/02/2021 16:00
08/31/2021 15:43Aqueous 94719 MW-3 09/02/2021 16:00
08/31/2021 13:37Aqueous 94720 MW-4 09/02/2021 16:00
08/31/2021Aqueous 94721 DUP-1 water 09/02/2021 16:00
08/30/2021 13:30Solids 94722 S-9(7-8)09/02/2021 16:00 7199
08/30/2021 13:30Solids 94722 S-9(7-8)09/02/2021 16:00
08/31/2021 10:45Solids 94723 S7(10-11)09/02/2021 16:00 7199
08/31/2021 10:45Solids 94723 S7(10-11)09/02/2021 16:00
08/31/2021 12:50Solids 94724 S6(14-15)09/02/2021 16:00 7199
08/31/2021 12:50Solids 94724 S6(14-15)09/02/2021 16:00
08/31/2021 09:30Solids 94725 S8(11-12)09/02/2021 16:00 7199
08/31/2021 09:30Solids 94725 S8(11-12)09/02/2021 16:00
08/31/2021Solids 94726 Dup-1 soil 09/02/2021 16:00 7199
08/31/2021Solids 94726 Dup-1 soil 09/02/2021 16:00
: Pace Analytical - Columbia, SC (Shealy), West Columbia, SC
Page 3 of 154
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-242-0018
Report Limit
Project:Doggette Site
V 94717MW-1
JB4.28 09/08/2021 18:596020BArsenicµg/L 0.850
388 09/07/2021 18:186020BBariumµg/L 4.05
36.0 09/07/2021 18:186020BChromiumµg/L 3.95
25.7 09/07/2021 18:186020BLeadµg/L 1.30
10.1 09/10/2021 08:488260DAcetoneµg/L 1.80
J0.928 09/10/2021 08:488260DMethyl Ethyl Ketone (MEK)µg/L 0.710
V 94718MW-2
B1.42 09/08/2021 18:336020BArsenicµg/L 0.170
111 09/07/2021 18:256020BBariumµg/L 0.810
41.1 09/07/2021 18:256020BChromiumµg/L 0.790
1.49 09/07/2021 18:256020BLeadµg/L 0.260
J2.73 09/08/2021 18:336020BSeleniumµg/L 0.740
13.7 09/10/2021 09:128260DAcetoneµg/L 1.80
J1.16 09/10/2021 09:128260DMethyl Ethyl Ketone (MEK)µg/L 0.710
V 94719MW-3
JB0.631 09/08/2021 18:406020BArsenicµg/L 0.170
101 09/07/2021 18:316020BBariumµg/L 0.810
J0.179 09/07/2021 18:316020BCadmiumµg/L 0.160
6.81 09/07/2021 18:316020BChromiumµg/L 0.790
3.65 09/07/2021 18:316020BLeadµg/L 0.260
J0.746 09/08/2021 18:406020BSeleniumµg/L 0.740
6.07 09/10/2021 09:378260DAcetoneµg/L 1.80
J0.828 09/10/2021 09:378260DNaphthaleneµg/L 0.470
V 94720MW-4
JB0.538 09/08/2021 18:466020BArsenicµg/L 0.170
141 09/07/2021 18:386020BBariumµg/L 0.810
50.0 09/07/2021 18:386020BChromiumµg/L 0.790
J0.663 09/07/2021 18:386020BLeadµg/L 0.260
7.02 09/10/2021 10:018260DAcetoneµg/L 1.80
J0.458 09/10/2021 10:018260DCarbon Disulfide µg/L 0.150
J0.461 09/10/2021 10:018260DTrichloroetheneµg/L 0.180
V 94721DUP-1 water
JB0.500 09/08/2021 18:536020BArsenicµg/L 0.170
139 09/07/2021 18:576020BBariumµg/L 0.810
Page 4 of 154
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-242-0018
Report Limit
Project:Doggette Site
V 94721DUP-1 water
50.7 09/07/2021 18:576020BChromiumµg/L 0.790
J0.676 09/07/2021 18:576020BLeadµg/L 0.260
7.99 09/10/2021 10:258260DAcetoneµg/L 1.80
0.516 09/10/2021 10:258260DTrichloroetheneµg/L 0.180
V 94722S-9(7-8)
2.09 09/07/2021 22:566020BArsenicmg/Kg - dry 0.126
345 09/07/2021 22:566020BBariummg/Kg - dry 1.87
53.1 09/07/2021 22:566020BChromiummg/Kg - dry 0.388
4.20 09/07/2021 22:566020BLeadmg/Kg - dry 0.187
5.76 09/08/2021 22:526020BSeleniummg/Kg - dry 1.20
J0.023 09/07/2021 11:078260DAcetonemg/Kg - dry 0.003
J0.001 09/07/2021 11:078260DCarbon Disulfide mg/Kg - dry 0.0009
J0.001 09/07/2021 11:078260DIsopropylbenzenemg/Kg - dry 0.0006
J0.002 09/07/2021 11:078260DMethylene Chloride mg/Kg - dry 0.001
J0.002 09/07/2021 11:078260DTetrachloroethenemg/Kg - dry 0.001
J0.001 09/07/2021 11:078260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.224 09/07/2021 17:218270E1-Methylnaphthalene mg/Kg - dry 0.141
25.3 09/08/2021 17:27SW-DRYWT Moisture %
V 94723S7(10-11)
2.80 09/07/2021 23:026020BArsenicmg/Kg - dry 0.114
39.0 09/07/2021 23:026020BBariummg/Kg - dry 1.71
74.9 09/07/2021 23:026020BChromiummg/Kg - dry 0.353
17.4 09/07/2021 23:026020BLeadmg/Kg - dry 0.171
0.0921 09/08/2021 14:287471BMercury (Total)mg/Kg - dry 0.0146
0.024 09/03/2021 14:148260DAcetonemg/Kg - dry 0.002
J0.002 09/03/2021 14:148260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.009 09/03/2021 14:148260DMethylene Chloride mg/Kg - dry 0.001
17.9 09/08/2021 17:27SW-DRYWT Moisture %
V 94724S6(14-15)
J0.763 09/07/2021 23:096020BArsenicmg/Kg - dry 0.119
133 09/07/2021 23:096020BBariummg/Kg - dry 1.77
76.6 09/07/2021 23:096020BChromiummg/Kg - dry 0.366
2.64 09/07/2021 23:096020BLeadmg/Kg - dry 0.177
J2.01 09/08/2021 23:056020BSeleniummg/Kg - dry 1.14
J0.006 09/03/2021 13:148260DAcetonemg/Kg - dry 0.003
Page 5 of 154
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-242-0018
Report Limit
Project:Doggette Site
V 94724S6(14-15)
J0.001 09/03/2021 13:148260Dn-Hexane mg/Kg - dry 0.0008
J0.010 09/03/2021 13:148260DMethylene Chloride mg/Kg - dry 0.001
20.8 09/08/2021 17:27SW-DRYWT Moisture %
V 94725S8(11-12)
2.65 09/07/2021 23:156020BArsenicmg/Kg - dry 0.124
63.2 09/07/2021 23:156020BBariummg/Kg - dry 1.85
47.2 09/07/2021 23:156020BChromiummg/Kg - dry 0.382
17.3 09/07/2021 23:156020BLeadmg/Kg - dry 0.185
J1.24 09/08/2021 23:126020BSeleniummg/Kg - dry 1.19
0.0553 09/08/2021 14:397471BMercury (Total)mg/Kg - dry 0.0158
1.45 09/07/2021 13:068260Dn-Butylbenzene mg/Kg - dry 0.016
0.656 09/07/2021 13:068260Dsec-Butyl benzene mg/Kg - dry 0.018
J0.113 09/07/2021 13:068260Dtert-Butyl benzene mg/Kg - dry 0.016
0.488 09/07/2021 13:068260DEthylbenzenemg/Kg - dry 0.019
0.370 09/07/2021 13:068260DIsopropylbenzenemg/Kg - dry 0.015
11.2 09/07/2021 13:068260DNaphthalenemg/Kg - dry 0.032
0.889 09/07/2021 13:068260Dn-Propylbenzene mg/Kg - dry 0.017
0.370 09/07/2021 13:068260D1,3,5-Trimethylbenzene mg/Kg - dry 0.017
J0.737 09/07/2021 18:508270EFluorenemg/Kg - dry 0.168
6.17 09/07/2021 18:508270E1-Methylnaphthalene mg/Kg - dry 0.139
6.32 09/07/2021 18:508270E2-Methylnaphthalene mg/Kg - dry 0.131
2.02 09/07/2021 18:508270ENaphthalenemg/Kg - dry 0.189
1.69 09/07/2021 18:508270EPhenanthrenemg/Kg - dry 0.274
24.2 09/08/2021 17:27SW-DRYWT Moisture %
V 94726Dup-1 soil
J1.04 09/07/2021 23:216020BArsenicmg/Kg - dry 0.121
169 09/07/2021 23:216020BBariummg/Kg - dry 1.80
88.7 09/07/2021 23:216020BChromiummg/Kg - dry 0.373
2.94 09/07/2021 23:216020BLeadmg/Kg - dry 0.180
2.96 09/08/2021 23:186020BSeleniummg/Kg - dry 1.16
J0.014 09/03/2021 14:448260DAcetonemg/Kg - dry 0.003
J0.001 09/03/2021 14:448260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.010 09/03/2021 14:448260DMethylene Chloride mg/Kg - dry 0.001
22.4 09/03/2021 17:05SW-DRYWT Moisture %
Page 6 of 154

Client: NOVA Engineering & Environmental CASE NARRATIVE
Project: Doggette Site Lab Report Number: 21-242-0018
Date: 10/1/2021
Metals Analyses Method 6020B Sample 94717 (MW-1) QC Batch No: V8497/V8436
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
QC Batch No: V8563/V8436 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Total Aqueous Mercury Analysis - CVAA Method 7470A Analyte: Mercury QC Batch No: V8479/V8451
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control acceptance ranges. Matrix interference is suspected
Solids Total Mercury Analysis - CVAA Method 7471B Sample 94722 (S-9(7-8)) Analyte: Mercury
QC Batch No: V8538/V8520 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Mercury QC Batch No: V8538/V8520 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: 4-Bromofluorobenzene QC Batch No: V8481/V8480 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all
showed surrogates within QC limits.
Analyte: Ethyl Tertiary Butyl Ether QC Batch No: V8448/V8613 Analyte flagged for 0% recovery in LCS and/or LCSD due to the results being below the MQL. The actual results were 91.755ug/L and 91.343ug/L which calculates to a recovery of 91.7% and 91.3% which is within the acceptable recovery range.
Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: 2,4-Dinitrophenol QC Batch No: V8596/V8443 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 1490 ug/kg which calculates to a recovery of 89.5% which is within the acceptable recovery range.
Page 7 of 154

Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V8596/V8443 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
1430 ug/kg which calculates to a recovery of 85.5% which is within the acceptable recovery range.
Analyte: Aniline QC Batch No: V8592/V8443
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 34 ug/L which calculates to a recovery of 68% which is within the acceptable recovery range.
Analyte: Benzoic Acid
QC Batch No: V8592/V8443 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
14.1 ug/L which calculates to a recovery of 28% which is within the acceptable recovery range.
Analyte: Benzoic Acid QC Batch No: V8596/V8443
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 1470 ug/kg which calculates to a recovery of 88% which is above the acceptable recovery range.
Analyte: Pentachlorophenol
QC Batch No: V8592/V8443 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 49 ug/L which calculates to a recovery of 97.8% which is within the acceptable recovery range.
Sample 94532 Analyte: 2,4-Dinitrophenol
QC Batch No: V8596/V8456 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1160 ug/kg which calculates to a recovery of 69.5% which is within the acceptable recovery range. Analyte: 2,4-Dinitrophenol QC Batch No: V8596/V8456
Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 1250 ug/kg which calculates to a recovery of 74.8% which is within the acceptable recovery range.
Analyte: 4,6-Dinitro-2-methylphenol QC Batch No: V8596/V8456 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1200 ug/kg which calculates to a recovery of 72% which is within the acceptable recovery range.
Analyte: 4,6-Dinitro-2-methylphenol QC Batch No: V8596/V8456 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 1260 ug/kg which calculates to a recovery of 75.6% which is within the acceptable recovery range. Analyte: Benzoic Acid QC Batch No: V8596/V8456 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1110 ug/kg which calculates to a recovery of 66% which is within the acceptable recovery range. Analyte: Benzoic Acid QC Batch No: V8596/V8456
Page 8 of 154

Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1240 ug/kg which calculates to a recovery of 74% which is within the acceptable recovery range.
Sample 94722 (S-9(7-8)) Analyte: Nitrobenzene-d5
QC Batch No: V8596/V8456 Surrogate recovery(s) was flagged as outside QC limits due to high levels of target and/or non-target analytes.
Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.

Page 9 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-1
94717 Matrix:
8/31/2021 9:20
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
4.28 JB µg/L 0.850 5.00Arsenic 5 09/08/21 18:59 6020BEDV
388 µg/L 4.05 50.0Barium 5 09/07/21 18:18 6020BEDV
<0.800 µg/L 0.800 5.00Cadmium 5 09/07/21 18:18 6020BEDV
36.0 µg/L 3.95 10.0Chromium 5 09/07/21 18:18 6020BEDV
25.7 µg/L 1.30 5.00Lead 5 09/07/21 18:18 6020BEDV
<0.00007 mg/L 0.00007 0.00020
Mercury (Total)1 09/07/21 16:33 7470AEDV
<3.70 µg/L 3.70 25.0Selenium 5 09/08/21 18:59 6020BEDV
<0.550 µg/L 0.550 5.00Silver 5 09/07/21 18:18 6020BEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 10 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-1
94717 Matrix:
8/31/2021 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
10.1 µg/L 1.80 5.00Acetone 1 09/10/21 08:48 V8614JLB
<2.00 µg/L 2.00 5.00Acrolein 1 09/10/21 08:48 V8614JLB
<0.230 µg/L 0.230 5.00Acrylonitrile 1 09/10/21 08:48 V8614JLB
<0.180 µg/L 0.180 0.500Benzene 1 09/10/21 08:48 V8614JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/10/21 08:48 V8614JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/10/21 08:48 V8614JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/10/21 08:48 V8614JLB
<1.50 µg/L 1.50 5.00Bromoform 1 09/10/21 08:48 V8614JLB
<0.280 µg/L 0.280 1.00
Bromomethane 1 09/10/21 08:48 V8614JLB
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 09/10/21 08:48 V8614JLB
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/10/21 08:48 V8614JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/10/21 08:48 V8614JLB
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 09/10/21 08:48 V8614JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/10/21 08:48 V8614JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/10/21 08:48 V8614JLB
<0.190 µg/L 0.190 0.500
Chlorodibromomethane 1 09/10/21 08:48 V8614JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 09/10/21 08:48 V8614JLB
<0.220 µg/L 0.220 0.500Chloroform 1 09/10/21 08:48 V8614JLB
<0.220 µg/L 0.220 0.500Chloromethane 1 09/10/21 08:48 V8614JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/10/21 08:48 V8614JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/10/21 08:48 V8614JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 09/10/21 08:48 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-1
94717 Matrix:
8/31/2021 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/10/21 08:48 V8614JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/10/21 08:48 V8614JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/10/21 08:48 V8614JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/10/21 08:48 V8614JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/10/21 08:48 V8614JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/10/21 08:48 V8614JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/10/21 08:48 V8614JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/10/21 08:48 V8614JLB
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 09/10/21 08:48 V8614JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/10/21 08:48 V8614JLB
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/10/21 08:48 V8614JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/10/21 08:48 V8614JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/10/21 08:48 V8614JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/10/21 08:48 V8614JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/10/21 08:48 V8614JLB
<0.200 µg/L 0.200 0.500
1,1-Dichloropropene 1 09/10/21 08:48 V8614JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/10/21 08:48 V8614JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/10/21 08:48 V8614JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/10/21 08:48 V8614JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 09/10/21 08:48 V8614JLB
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 09/10/21 08:48 V8614JLB
<1.30 µg/L 1.30 10.0n-Hexane 1 09/10/21 08:48 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-1
94717 Matrix:
8/31/2021 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<0.380 µg/L 0.380 5.002-Hexanone 1 09/10/21 08:48 V8614JLB
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 09/10/21 08:48 V8614JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/10/21 08:48 V8614JLB
0.928 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/10/21 08:48 V8614JLB
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 09/10/21 08:48 V8614JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 09/10/21 08:48 V8614JLB
<0.330 µg/L 0.330 1.00Methylene Chloride 1 09/10/21 08:48 V8614JLB
<0.470 µg/L 0.470 1.00Naphthalene 1 09/10/21 08:48 V8614JLB
<0.190 µg/L 0.190 0.500
n-Propylbenzene 1 09/10/21 08:48 V8614JLB
<0.220 µg/L 0.220 0.500Styrene 1 09/10/21 08:48 V8614JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/10/21 08:48 V8614JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/10/21 08:48 V8614JLB
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/10/21 08:48 V8614JLB
<0.220 µg/L 0.220 0.500Toluene 1 09/10/21 08:48 V8614JLB
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 09/10/21 08:48 V8614JLB
<0.310 µg/L 0.310 1.00
1,2,4-Trichlorobenzene 1 09/10/21 08:48 V8614JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/10/21 08:48 V8614JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/10/21 08:48 V8614JLB
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/10/21 08:48 V8614JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/10/21 08:48 V8614JLB
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 09/10/21 08:48 V8614JLB
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/10/21 08:48 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-1
94717 Matrix:
8/31/2021 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 09/10/21 08:48 V8614JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/10/21 08:48 V8614JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 09/10/21 08:48 V8614JLB
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/10/21 08:48 V8614JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/10/21 08:48 V8614
Surrogate: 4-Bromofluorobenzene 105 Limits: 80-124%09/10/21 08:481 JLB V8614
Surrogate: Dibromofluoromethane 105 Limits: 75-129%09/10/21 08:481 JLB V8614
Surrogate: 1,2-Dichloroethane - d4 96.8 Limits: 63-136%09/10/21 08:481 JLB V8614
Surrogate: Toluene-d8 99.2 Limits: 77-123%09/10/21 08:481 JLB V8614
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<8.47 µg/L 8.47 23.8
Acenaphthene 1 09/07/21 22:34 V8592JMV
<8.26 µg/L 8.26 23.8Acenaphthylene 1 09/07/21 22:34 V8592JMV
<8.48 µg/L 8.48 59.5Aniline 1 09/07/21 22:34 V8592JMV
<7.82 µg/L 7.82 11.9Anthracene 1 09/07/21 22:34 V8592JMV
<6.72 µg/L 6.72 11.9Benzo(a)anthracene 1 09/07/21 22:34 V8592JMV
<5.56 µg/L 5.56 11.9Benzo(a)pyrene 1 09/07/21 22:34 V8592JMV
<5.38 µg/L 5.38 11.9Benzo(b)fluoranthene 1 09/07/21 22:34 V8592JMV
<5.05 µg/L 5.05 11.9
Benzo(g,h,i)perylene 1 09/07/21 22:34 V8592JMV
<5.57 µg/L 5.57 11.9Benzo(k)fluoranthene 1 09/07/21 22:34 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-1
94717 Matrix:
8/31/2021 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<13.7 µg/L 13.7 119Benzoic Acid 1 09/07/21 22:34 V8592JMV
<10.2 µg/L 10.2 11.9Benzyl alcohol 1 09/07/21 22:34 V8592JMV
<6.75 µg/L 6.75 11.9Bis(2-Chloroethoxy)methane 1 09/07/21 22:34 V8592JMV
<8.69 µg/L 8.69 11.9Bis(2-Chloroethyl)ether 1 09/07/21 22:34 V8592JMV
<7.84 µg/L 7.84 11.9Bis(2-Chloroisopropyl)ether 1 09/07/21 22:34 V8592JMV
<10.5 µg/L 10.5 11.9Bis(2-ethylhexyl)phthalate 1 09/07/21 22:34 V8592JMV
<7.45 µg/L 7.45 23.84-Bromophenyl phenyl ether 1 09/07/21 22:34 V8592JMV
<3.50 µg/L 3.50 11.9Butyl benzyl phthalate 1 09/07/21 22:34 V8592JMV
<6.22 µg/L 6.22 11.9
4-Chloro-3-methylphenol 1 09/07/21 22:34 V8592JMV
<6.45 µg/L 6.45 11.94-Chloroaniline 1 09/07/21 22:34 V8592JMV
<8.78 µg/L 8.78 23.82-Chloronaphthalene 1 09/07/21 22:34 V8592JMV
<7.83 µg/L 7.83 11.92-Chlorophenol 1 09/07/21 22:34 V8592JMV
<8.32 µg/L 8.32 23.84-Chlorophenyl phenyl ether 1 09/07/21 22:34 V8592JMV
<6.40 µg/L 6.40 11.9Chrysene 1 09/07/21 22:34 V8592JMV
<7.15 µg/L 7.15 23.8Dibenz(a,h)anthracene 1 09/07/21 22:34 V8592JMV
<6.05 µg/L 6.05 23.8
Dibenzofuran 1 09/07/21 22:34 V8592JMV
<7.03 µg/L 7.03 11.91,2-Dichlorobenzene 1 09/07/21 22:34 V8592JMV
<6.94 µg/L 6.94 11.91,3-Dichlorobenzene 1 09/07/21 22:34 V8592JMV
<7.03 µg/L 7.03 11.91,4-Dichlorobenzene 1 09/07/21 22:34 V8592JMV
<7.85 µg/L 7.85 11.93,3'-Dichlorobenzidine 1 09/07/21 22:34 V8592JMV
<6.59 µg/L 6.59 11.92,4-Dichlorophenol 1 09/07/21 22:34 V8592JMV
<11.1 µg/L 11.1 23.8Diethyl phthalate 1 09/07/21 22:34 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-1
94717 Matrix:
8/31/2021 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<9.31 µg/L 9.31 11.9Dimethyl phthalate 1 09/07/21 22:34 V8592JMV
<13.0 µg/L 13.0 23.82,4-Dimethylphenol 1 09/07/21 22:34 V8592JMV
<8.75 µg/L 8.75 11.9Di-n-butyl phthalate 1 09/07/21 22:34 V8592JMV
<11.8 µg/L 11.8 35.74,6-Dinitro-2-methylphenol 1 09/07/21 22:34 V8592JMV
<12.6 µg/L 12.6 35.72,4-Dinitrophenol 1 09/07/21 22:34 V8592JMV
<6.19 µg/L 6.19 11.92,4-Dinitrotoluene 1 09/07/21 22:34 V8592JMV
<7.02 µg/L 7.02 23.82,6-Dinitrotoluene 1 09/07/21 22:34 V8592JMV
<5.96 µg/L 5.96 11.9Di-n-Octyl Phthalate 1 09/07/21 22:34 V8592JMV
<7.18 µg/L 7.18 11.9
Fluoranthene 1 09/07/21 22:34 V8592JMV
<8.65 µg/L 8.65 11.9Fluorene 1 09/07/21 22:34 V8592JMV
<6.84 µg/L 6.84 23.8Hexachlorobenzene 1 09/07/21 22:34 V8592JMV
<7.00 µg/L 7.00 23.8Hexachlorobutadiene 1 09/07/21 22:34 V8592JMV
<7.02 µg/L 7.02 23.8Hexachlorocyclopentadiene 1 09/07/21 22:34 V8592JMV
<6.21 µg/L 6.21 11.9Hexachloroethane 1 09/07/21 22:34 V8592JMV
<7.38 µg/L 7.38 11.9Indeno(1,2,3-cd)pyrene 1 09/07/21 22:34 V8592JMV
<7.98 µg/L 7.98 11.9
Isophorone 1 09/07/21 22:34 V8592JMV
<8.72 µg/L 8.72 11.91-Methylnaphthalene 1 09/07/21 22:34 V8592JMV
<8.23 µg/L 8.23 11.92-Methylnaphthalene 1 09/07/21 22:34 V8592JMV
<6.26 µg/L 6.26 11.92-Methylphenol 1 09/07/21 22:34 V8592JMV
<2.94 µg/L 2.94 11.93&4 Methylphenol 1 09/07/21 22:34 V8592JMV
<9.38 µg/L 9.38 11.9Naphthalene 1 09/07/21 22:34 V8592JMV
<5.85 µg/L 5.85 11.92-Nitroaniline 1 09/07/21 22:34 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-1
94717 Matrix:
8/31/2021 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<5.41 µg/L 5.41 11.93-Nitroaniline 1 09/07/21 22:34 V8592JMV
<6.07 µg/L 6.07 11.94-Nitroaniline 1 09/07/21 22:34 V8592JMV
<9.38 µg/L 9.38 11.9Nitrobenzene 1 09/07/21 22:34 V8592JMV
<6.53 µg/L 6.53 11.92-Nitrophenol 1 09/07/21 22:34 V8592JMV
<3.34 µg/L 3.34 11.94-Nitrophenol 1 09/07/21 22:34 V8592JMV
<7.72 µg/L 7.72 11.9N-Nitrosodimethylamine 1 09/07/21 22:34 V8592JMV
<13.0 µg/L 13.0 23.8N-Nitrosodiphenylamine 1 09/07/21 22:34 V8592JMV
<9.64 µg/L 9.64 23.8N-Nitroso-di-n-propylamine 1 09/07/21 22:34 V8592JMV
<11.6 µg/L 11.6 59.5
Pentachlorophenol 1 09/07/21 22:34 V8592JMV
<7.54 µg/L 7.54 11.9Phenanthrene 1 09/07/21 22:34 V8592JMV
<3.40 µg/L 3.40 11.9Phenol 1 09/07/21 22:34 V8592JMV
<6.45 µg/L 6.45 11.9Pyrene 1 09/07/21 22:34 V8592JMV
<6.33 µg/L 6.33 11.9Pyridine 1 09/07/21 22:34 V8592JMV
<7.44 µg/L 7.44 11.91,2,4-Trichlorobenzene 1 09/07/21 22:34 V8592JMV
<6.91 µg/L 6.91 23.82,4,5-Trichlorophenol 1 09/07/21 22:34 V8592JMV
<7.49 µg/L 7.49 23.8
2,4,6-Trichlorophenol 1 09/07/21 22:34 V8592JMV
Surrogate: Phenol-d5 27.1 Limits: 11-100%09/07/21 22:341 JMV V8592
Surrogate: 2-Fluorobiphenyl 68.7 Limits: 44-119%09/07/21 22:341 JMV V8592
Surrogate: 2-Fluorophenol 38.0 Limits: 19-119%09/07/21 22:341 JMV V8592
Surrogate: Nitrobenzene-d5 59.0 Limits: 44-120%09/07/21 22:341 JMV V8592
Surrogate: 4-Terphenyl-d14 93.4 Limits: 50-134%09/07/21 22:341 JMV V8592
Surrogate: 2,4,6-Tribromophenol 89.9 Limits: 43-140%09/07/21 22:341 JMV V8592
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-2
94718 Matrix:
8/31/2021 16:47
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
1.42 B µg/L 0.170 1.00Arsenic 1 09/08/21 18:33 6020BEDV
111 µg/L 0.810 10.0Barium 1 09/07/21 18:25 6020BEDV
<0.160 µg/L 0.160 1.00Cadmium 1 09/07/21 18:25 6020BEDV
41.1 µg/L 0.790 2.00Chromium 1 09/07/21 18:25 6020BEDV
1.49 µg/L 0.260 1.00Lead 1 09/07/21 18:25 6020BEDV
<0.00007 mg/L 0.00007 0.00020
Mercury (Total)1 09/07/21 17:03 7470AEDV
2.73 J µg/L 0.740 5.00Selenium 1 09/08/21 18:33 6020BEDV
<0.110 µg/L 0.110 1.00Silver 1 09/07/21 18:25 6020BEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 18 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-2
94718 Matrix:
8/31/2021 16:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
13.7 µg/L 1.80 5.00Acetone 1 09/10/21 09:12 V8614JLB
<2.00 µg/L 2.00 5.00Acrolein 1 09/10/21 09:12 V8614JLB
<0.230 µg/L 0.230 5.00Acrylonitrile 1 09/10/21 09:12 V8614JLB
<0.180 µg/L 0.180 0.500Benzene 1 09/10/21 09:12 V8614JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/10/21 09:12 V8614JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/10/21 09:12 V8614JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/10/21 09:12 V8614JLB
<1.50 µg/L 1.50 5.00Bromoform 1 09/10/21 09:12 V8614JLB
<0.280 µg/L 0.280 1.00
Bromomethane 1 09/10/21 09:12 V8614JLB
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 09/10/21 09:12 V8614JLB
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/10/21 09:12 V8614JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/10/21 09:12 V8614JLB
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 09/10/21 09:12 V8614JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/10/21 09:12 V8614JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/10/21 09:12 V8614JLB
<0.190 µg/L 0.190 0.500
Chlorodibromomethane 1 09/10/21 09:12 V8614JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 09/10/21 09:12 V8614JLB
<0.220 µg/L 0.220 0.500Chloroform 1 09/10/21 09:12 V8614JLB
<0.220 µg/L 0.220 0.500Chloromethane 1 09/10/21 09:12 V8614JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/10/21 09:12 V8614JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/10/21 09:12 V8614JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 09/10/21 09:12 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-2
94718 Matrix:
8/31/2021 16:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/10/21 09:12 V8614JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/10/21 09:12 V8614JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/10/21 09:12 V8614JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/10/21 09:12 V8614JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/10/21 09:12 V8614JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/10/21 09:12 V8614JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/10/21 09:12 V8614JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/10/21 09:12 V8614JLB
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 09/10/21 09:12 V8614JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/10/21 09:12 V8614JLB
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/10/21 09:12 V8614JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/10/21 09:12 V8614JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/10/21 09:12 V8614JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/10/21 09:12 V8614JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/10/21 09:12 V8614JLB
<0.200 µg/L 0.200 0.500
1,1-Dichloropropene 1 09/10/21 09:12 V8614JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/10/21 09:12 V8614JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/10/21 09:12 V8614JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/10/21 09:12 V8614JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 09/10/21 09:12 V8614JLB
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 09/10/21 09:12 V8614JLB
<1.30 µg/L 1.30 10.0n-Hexane 1 09/10/21 09:12 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-2
94718 Matrix:
8/31/2021 16:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<0.380 µg/L 0.380 5.002-Hexanone 1 09/10/21 09:12 V8614JLB
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 09/10/21 09:12 V8614JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/10/21 09:12 V8614JLB
1.16 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/10/21 09:12 V8614JLB
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 09/10/21 09:12 V8614JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 09/10/21 09:12 V8614JLB
<0.330 µg/L 0.330 1.00Methylene Chloride 1 09/10/21 09:12 V8614JLB
<0.470 µg/L 0.470 1.00Naphthalene 1 09/10/21 09:12 V8614JLB
<0.190 µg/L 0.190 0.500
n-Propylbenzene 1 09/10/21 09:12 V8614JLB
<0.220 µg/L 0.220 0.500Styrene 1 09/10/21 09:12 V8614JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/10/21 09:12 V8614JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/10/21 09:12 V8614JLB
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/10/21 09:12 V8614JLB
<0.220 µg/L 0.220 0.500Toluene 1 09/10/21 09:12 V8614JLB
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 09/10/21 09:12 V8614JLB
<0.310 µg/L 0.310 1.00
1,2,4-Trichlorobenzene 1 09/10/21 09:12 V8614JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/10/21 09:12 V8614JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/10/21 09:12 V8614JLB
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/10/21 09:12 V8614JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/10/21 09:12 V8614JLB
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 09/10/21 09:12 V8614JLB
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/10/21 09:12 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-2
94718 Matrix:
8/31/2021 16:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 09/10/21 09:12 V8614JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/10/21 09:12 V8614JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 09/10/21 09:12 V8614JLB
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/10/21 09:12 V8614JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/10/21 09:12 V8614
Surrogate: 4-Bromofluorobenzene 103 Limits: 80-124%09/10/21 09:121 JLB V8614
Surrogate: Dibromofluoromethane 104 Limits: 75-129%09/10/21 09:121 JLB V8614
Surrogate: 1,2-Dichloroethane - d4 96.8 Limits: 63-136%09/10/21 09:121 JLB V8614
Surrogate: Toluene-d8 99.8 Limits: 77-123%09/10/21 09:121 JLB V8614
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<7.73 µg/L 7.73 21.7
Acenaphthene 1 09/07/21 23:40 V8592JMV
<7.53 µg/L 7.53 21.7Acenaphthylene 1 09/07/21 23:40 V8592JMV
<7.74 µg/L 7.74 54.3Aniline 1 09/07/21 23:40 V8592JMV
<7.16 µg/L 7.16 10.9Anthracene 1 09/07/21 23:40 V8592JMV
<6.16 µg/L 6.16 10.9Benzo(a)anthracene 1 09/07/21 23:40 V8592JMV
<5.09 µg/L 5.09 10.9Benzo(a)pyrene 1 09/07/21 23:40 V8592JMV
<4.93 µg/L 4.93 10.9Benzo(b)fluoranthene 1 09/07/21 23:40 V8592JMV
<4.62 µg/L 4.62 10.9
Benzo(g,h,i)perylene 1 09/07/21 23:40 V8592JMV
<5.10 µg/L 5.10 10.9Benzo(k)fluoranthene 1 09/07/21 23:40 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-2
94718 Matrix:
8/31/2021 16:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<12.6 µg/L 12.6 109Benzoic Acid 1 09/07/21 23:40 V8592JMV
<9.37 µg/L 9.37 10.9Benzyl alcohol 1 09/07/21 23:40 V8592JMV
<6.18 µg/L 6.18 10.9Bis(2-Chloroethoxy)methane 1 09/07/21 23:40 V8592JMV
<7.96 µg/L 7.96 10.9Bis(2-Chloroethyl)ether 1 09/07/21 23:40 V8592JMV
<7.18 µg/L 7.18 10.9Bis(2-Chloroisopropyl)ether 1 09/07/21 23:40 V8592JMV
<9.59 µg/L 9.59 10.9Bis(2-ethylhexyl)phthalate 1 09/07/21 23:40 V8592JMV
<6.79 µg/L 6.79 21.74-Bromophenyl phenyl ether 1 09/07/21 23:40 V8592JMV
<3.20 µg/L 3.20 10.9Butyl benzyl phthalate 1 09/07/21 23:40 V8592JMV
<5.70 µg/L 5.70 10.9
4-Chloro-3-methylphenol 1 09/07/21 23:40 V8592JMV
<5.91 µg/L 5.91 10.94-Chloroaniline 1 09/07/21 23:40 V8592JMV
<8.01 µg/L 8.01 21.72-Chloronaphthalene 1 09/07/21 23:40 V8592JMV
<7.17 µg/L 7.17 10.92-Chlorophenol 1 09/07/21 23:40 V8592JMV
<7.58 µg/L 7.58 21.74-Chlorophenyl phenyl ether 1 09/07/21 23:40 V8592JMV
<5.86 µg/L 5.86 10.9Chrysene 1 09/07/21 23:40 V8592JMV
<6.52 µg/L 6.52 21.7Dibenz(a,h)anthracene 1 09/07/21 23:40 V8592JMV
<5.51 µg/L 5.51 21.7
Dibenzofuran 1 09/07/21 23:40 V8592JMV
<6.44 µg/L 6.44 10.91,2-Dichlorobenzene 1 09/07/21 23:40 V8592JMV
<6.35 µg/L 6.35 10.91,3-Dichlorobenzene 1 09/07/21 23:40 V8592JMV
<6.44 µg/L 6.44 10.91,4-Dichlorobenzene 1 09/07/21 23:40 V8592JMV
<7.19 µg/L 7.19 10.93,3'-Dichlorobenzidine 1 09/07/21 23:40 V8592JMV
<6.04 µg/L 6.04 10.92,4-Dichlorophenol 1 09/07/21 23:40 V8592JMV
<10.1 µg/L 10.1 21.7Diethyl phthalate 1 09/07/21 23:40 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-2
94718 Matrix:
8/31/2021 16:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<8.52 µg/L 8.52 10.9Dimethyl phthalate 1 09/07/21 23:40 V8592JMV
<11.8 µg/L 11.8 21.72,4-Dimethylphenol 1 09/07/21 23:40 V8592JMV
<8.01 µg/L 8.01 10.9Di-n-butyl phthalate 1 09/07/21 23:40 V8592JMV
<10.8 µg/L 10.8 32.64,6-Dinitro-2-methylphenol 1 09/07/21 23:40 V8592JMV
<11.5 µg/L 11.5 32.62,4-Dinitrophenol 1 09/07/21 23:40 V8592JMV
<5.67 µg/L 5.67 10.92,4-Dinitrotoluene 1 09/07/21 23:40 V8592JMV
<6.40 µg/L 6.40 21.72,6-Dinitrotoluene 1 09/07/21 23:40 V8592JMV
<5.46 µg/L 5.46 10.9Di-n-Octyl Phthalate 1 09/07/21 23:40 V8592JMV
<6.57 µg/L 6.57 10.9
Fluoranthene 1 09/07/21 23:40 V8592JMV
<7.92 µg/L 7.92 10.9Fluorene 1 09/07/21 23:40 V8592JMV
<6.24 µg/L 6.24 21.7Hexachlorobenzene 1 09/07/21 23:40 V8592JMV
<6.38 µg/L 6.38 21.7Hexachlorobutadiene 1 09/07/21 23:40 V8592JMV
<6.40 µg/L 6.40 21.7Hexachlorocyclopentadiene 1 09/07/21 23:40 V8592JMV
<5.69 µg/L 5.69 10.9Hexachloroethane 1 09/07/21 23:40 V8592JMV
<6.76 µg/L 6.76 10.9Indeno(1,2,3-cd)pyrene 1 09/07/21 23:40 V8592JMV
<7.31 µg/L 7.31 10.9
Isophorone 1 09/07/21 23:40 V8592JMV
<7.99 µg/L 7.99 10.91-Methylnaphthalene 1 09/07/21 23:40 V8592JMV
<7.54 µg/L 7.54 10.92-Methylnaphthalene 1 09/07/21 23:40 V8592JMV
<5.73 µg/L 5.73 10.92-Methylphenol 1 09/07/21 23:40 V8592JMV
<2.69 µg/L 2.69 10.93&4 Methylphenol 1 09/07/21 23:40 V8592JMV
<8.59 µg/L 8.59 10.9Naphthalene 1 09/07/21 23:40 V8592JMV
<5.36 µg/L 5.36 10.92-Nitroaniline 1 09/07/21 23:40 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-2
94718 Matrix:
8/31/2021 16:47
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<4.96 µg/L 4.96 10.93-Nitroaniline 1 09/07/21 23:40 V8592JMV
<5.56 µg/L 5.56 10.94-Nitroaniline 1 09/07/21 23:40 V8592JMV
<8.59 µg/L 8.59 10.9Nitrobenzene 1 09/07/21 23:40 V8592JMV
<5.98 µg/L 5.98 10.92-Nitrophenol 1 09/07/21 23:40 V8592JMV
<3.06 µg/L 3.06 10.94-Nitrophenol 1 09/07/21 23:40 V8592JMV
<7.07 µg/L 7.07 10.9N-Nitrosodimethylamine 1 09/07/21 23:40 V8592JMV
<11.9 µg/L 11.9 21.7N-Nitrosodiphenylamine 1 09/07/21 23:40 V8592JMV
<8.79 µg/L 8.79 21.7N-Nitroso-di-n-propylamine 1 09/07/21 23:40 V8592JMV
<10.6 µg/L 10.6 54.3
Pentachlorophenol 1 09/07/21 23:40 V8592JMV
<6.91 µg/L 6.91 10.9Phenanthrene 1 09/07/21 23:40 V8592JMV
<3.12 µg/L 3.12 10.9Phenol 1 09/07/21 23:40 V8592JMV
<5.91 µg/L 5.91 10.9Pyrene 1 09/07/21 23:40 V8592JMV
<5.80 µg/L 5.80 10.9Pyridine 1 09/07/21 23:40 V8592JMV
<6.81 µg/L 6.81 10.91,2,4-Trichlorobenzene 1 09/07/21 23:40 V8592JMV
<6.30 µg/L 6.30 21.72,4,5-Trichlorophenol 1 09/07/21 23:40 V8592JMV
<6.82 µg/L 6.82 21.7
2,4,6-Trichlorophenol 1 09/07/21 23:40 V8592JMV
Surrogate: Phenol-d5 22.3 Limits: 11-100%09/07/21 23:401 JMV V8592
Surrogate: 2-Fluorobiphenyl 60.8 Limits: 44-119%09/07/21 23:401 JMV V8592
Surrogate: 2-Fluorophenol 32.8 Limits: 19-119%09/07/21 23:401 JMV V8592
Surrogate: Nitrobenzene-d5 52.5 Limits: 44-120%09/07/21 23:401 JMV V8592
Surrogate: 4-Terphenyl-d14 92.6 Limits: 50-134%09/07/21 23:401 JMV V8592
Surrogate: 2,4,6-Tribromophenol 84.5 Limits: 43-140%09/07/21 23:401 JMV V8592
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-3
94719 Matrix:
8/31/2021 15:43
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
0.631 JB µg/L 0.170 1.00Arsenic 1 09/08/21 18:40 6020BEDV
101 µg/L 0.810 10.0Barium 1 09/07/21 18:31 6020BEDV
0.179 J µg/L 0.160 1.00Cadmium 1 09/07/21 18:31 6020BEDV
6.81 µg/L 0.790 2.00Chromium 1 09/07/21 18:31 6020BEDV
3.65 µg/L 0.260 1.00Lead 1 09/07/21 18:31 6020BEDV
<0.00007 mg/L 0.00007 0.00020
Mercury (Total)1 09/07/21 17:00 7470AEDV
0.746 J µg/L 0.740 5.00Selenium 1 09/08/21 18:40 6020BEDV
<0.110 µg/L 0.110 1.00Silver 1 09/07/21 18:31 6020BEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 26 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-3
94719 Matrix:
8/31/2021 15:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
6.07 µg/L 1.80 5.00Acetone 1 09/10/21 09:37 V8614JLB
<2.00 µg/L 2.00 5.00Acrolein 1 09/10/21 09:37 V8614JLB
<0.230 µg/L 0.230 5.00Acrylonitrile 1 09/10/21 09:37 V8614JLB
<0.180 µg/L 0.180 0.500Benzene 1 09/10/21 09:37 V8614JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/10/21 09:37 V8614JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/10/21 09:37 V8614JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/10/21 09:37 V8614JLB
<1.50 µg/L 1.50 5.00Bromoform 1 09/10/21 09:37 V8614JLB
<0.280 µg/L 0.280 1.00
Bromomethane 1 09/10/21 09:37 V8614JLB
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 09/10/21 09:37 V8614JLB
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/10/21 09:37 V8614JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/10/21 09:37 V8614JLB
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 09/10/21 09:37 V8614JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/10/21 09:37 V8614JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/10/21 09:37 V8614JLB
<0.190 µg/L 0.190 0.500
Chlorodibromomethane 1 09/10/21 09:37 V8614JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 09/10/21 09:37 V8614JLB
<0.220 µg/L 0.220 0.500Chloroform 1 09/10/21 09:37 V8614JLB
<0.220 µg/L 0.220 0.500Chloromethane 1 09/10/21 09:37 V8614JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/10/21 09:37 V8614JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/10/21 09:37 V8614JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 09/10/21 09:37 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-3
94719 Matrix:
8/31/2021 15:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/10/21 09:37 V8614JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/10/21 09:37 V8614JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/10/21 09:37 V8614JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/10/21 09:37 V8614JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/10/21 09:37 V8614JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/10/21 09:37 V8614JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/10/21 09:37 V8614JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/10/21 09:37 V8614JLB
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 09/10/21 09:37 V8614JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/10/21 09:37 V8614JLB
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/10/21 09:37 V8614JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/10/21 09:37 V8614JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/10/21 09:37 V8614JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/10/21 09:37 V8614JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/10/21 09:37 V8614JLB
<0.200 µg/L 0.200 0.500
1,1-Dichloropropene 1 09/10/21 09:37 V8614JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/10/21 09:37 V8614JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/10/21 09:37 V8614JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/10/21 09:37 V8614JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 09/10/21 09:37 V8614JLB
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 09/10/21 09:37 V8614JLB
<1.30 µg/L 1.30 10.0n-Hexane 1 09/10/21 09:37 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-3
94719 Matrix:
8/31/2021 15:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<0.380 µg/L 0.380 5.002-Hexanone 1 09/10/21 09:37 V8614JLB
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 09/10/21 09:37 V8614JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/10/21 09:37 V8614JLB
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/10/21 09:37 V8614JLB
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 09/10/21 09:37 V8614JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 09/10/21 09:37 V8614JLB
<0.330 µg/L 0.330 1.00Methylene Chloride 1 09/10/21 09:37 V8614JLB
0.828 J µg/L 0.470 1.00Naphthalene 1 09/10/21 09:37 V8614JLB
<0.190 µg/L 0.190 0.500
n-Propylbenzene 1 09/10/21 09:37 V8614JLB
<0.220 µg/L 0.220 0.500Styrene 1 09/10/21 09:37 V8614JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/10/21 09:37 V8614JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/10/21 09:37 V8614JLB
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/10/21 09:37 V8614JLB
<0.220 µg/L 0.220 0.500Toluene 1 09/10/21 09:37 V8614JLB
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 09/10/21 09:37 V8614JLB
<0.310 µg/L 0.310 1.00
1,2,4-Trichlorobenzene 1 09/10/21 09:37 V8614JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/10/21 09:37 V8614JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/10/21 09:37 V8614JLB
<0.180 µg/L 0.180 0.500Trichloroethene 1 09/10/21 09:37 V8614JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/10/21 09:37 V8614JLB
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 09/10/21 09:37 V8614JLB
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/10/21 09:37 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-3
94719 Matrix:
8/31/2021 15:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 09/10/21 09:37 V8614JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/10/21 09:37 V8614JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 09/10/21 09:37 V8614JLB
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/10/21 09:37 V8614JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/10/21 09:37 V8614
Surrogate: 4-Bromofluorobenzene 101 Limits: 80-124%09/10/21 09:371 JLB V8614
Surrogate: Dibromofluoromethane 102 Limits: 75-129%09/10/21 09:371 JLB V8614
Surrogate: 1,2-Dichloroethane - d4 95.8 Limits: 63-136%09/10/21 09:371 JLB V8614
Surrogate: Toluene-d8 101 Limits: 77-123%09/10/21 09:371 JLB V8614
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<7.90 µg/L 7.90 22.2
Acenaphthene 1 09/07/21 22:56 V8592JMV
<7.70 µg/L 7.70 22.2Acenaphthylene 1 09/07/21 22:56 V8592JMV
<7.93 µg/L 7.93 55.6Aniline 1 09/07/21 22:56 V8592JMV
<7.29 µg/L 7.29 11.1Anthracene 1 09/07/21 22:56 V8592JMV
<6.27 µg/L 6.27 11.1Benzo(a)anthracene 1 09/07/21 22:56 V8592JMV
<5.18 µg/L 5.18 11.1Benzo(a)pyrene 1 09/07/21 22:56 V8592JMV
<5.02 µg/L 5.02 11.1Benzo(b)fluoranthene 1 09/07/21 22:56 V8592JMV
<4.71 µg/L 4.71 11.1
Benzo(g,h,i)perylene 1 09/07/21 22:56 V8592JMV
<5.19 µg/L 5.19 11.1Benzo(k)fluoranthene 1 09/07/21 22:56 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-3
94719 Matrix:
8/31/2021 15:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<12.8 µg/L 12.8 111Benzoic Acid 1 09/07/21 22:56 V8592JMV
<9.55 µg/L 9.55 11.1Benzyl alcohol 1 09/07/21 22:56 V8592JMV
<6.29 µg/L 6.29 11.1Bis(2-Chloroethoxy)methane 1 09/07/21 22:56 V8592JMV
<8.10 µg/L 8.10 11.1Bis(2-Chloroethyl)ether 1 09/07/21 22:56 V8592JMV
<7.31 µg/L 7.31 11.1Bis(2-Chloroisopropyl)ether 1 09/07/21 22:56 V8592JMV
<9.77 µg/L 9.77 11.1Bis(2-ethylhexyl)phthalate 1 09/07/21 22:56 V8592JMV
<6.95 µg/L 6.95 22.24-Bromophenyl phenyl ether 1 09/07/21 22:56 V8592JMV
<3.26 µg/L 3.26 11.1Butyl benzyl phthalate 1 09/07/21 22:56 V8592JMV
<5.81 µg/L 5.81 11.1
4-Chloro-3-methylphenol 1 09/07/21 22:56 V8592JMV
<6.02 µg/L 6.02 11.14-Chloroaniline 1 09/07/21 22:56 V8592JMV
<8.19 µg/L 8.19 22.22-Chloronaphthalene 1 09/07/21 22:56 V8592JMV
<7.30 µg/L 7.30 11.12-Chlorophenol 1 09/07/21 22:56 V8592JMV
<7.76 µg/L 7.76 22.24-Chlorophenyl phenyl ether 1 09/07/21 22:56 V8592JMV
<5.97 µg/L 5.97 11.1Chrysene 1 09/07/21 22:56 V8592JMV
<6.67 µg/L 6.67 22.2Dibenz(a,h)anthracene 1 09/07/21 22:56 V8592JMV
<5.64 µg/L 5.64 22.2
Dibenzofuran 1 09/07/21 22:56 V8592JMV
<6.56 µg/L 6.56 11.11,2-Dichlorobenzene 1 09/07/21 22:56 V8592JMV
<6.47 µg/L 6.47 11.11,3-Dichlorobenzene 1 09/07/21 22:56 V8592JMV
<6.56 µg/L 6.56 11.11,4-Dichlorobenzene 1 09/07/21 22:56 V8592JMV
<7.33 µg/L 7.33 11.13,3'-Dichlorobenzidine 1 09/07/21 22:56 V8592JMV
<6.15 µg/L 6.15 11.12,4-Dichlorophenol 1 09/07/21 22:56 V8592JMV
<10.4 µg/L 10.4 22.2Diethyl phthalate 1 09/07/21 22:56 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-3
94719 Matrix:
8/31/2021 15:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<8.68 µg/L 8.68 11.1Dimethyl phthalate 1 09/07/21 22:56 V8592JMV
<12.1 µg/L 12.1 22.22,4-Dimethylphenol 1 09/07/21 22:56 V8592JMV
<8.16 µg/L 8.16 11.1Di-n-butyl phthalate 1 09/07/21 22:56 V8592JMV
<11.0 µg/L 11.0 33.34,6-Dinitro-2-methylphenol 1 09/07/21 22:56 V8592JMV
<11.8 µg/L 11.8 33.32,4-Dinitrophenol 1 09/07/21 22:56 V8592JMV
<5.77 µg/L 5.77 11.12,4-Dinitrotoluene 1 09/07/21 22:56 V8592JMV
<6.55 µg/L 6.55 22.22,6-Dinitrotoluene 1 09/07/21 22:56 V8592JMV
<5.56 µg/L 5.56 11.1Di-n-Octyl Phthalate 1 09/07/21 22:56 V8592JMV
<6.69 µg/L 6.69 11.1
Fluoranthene 1 09/07/21 22:56 V8592JMV
<8.07 µg/L 8.07 11.1Fluorene 1 09/07/21 22:56 V8592JMV
<6.38 µg/L 6.38 22.2Hexachlorobenzene 1 09/07/21 22:56 V8592JMV
<6.53 µg/L 6.53 22.2Hexachlorobutadiene 1 09/07/21 22:56 V8592JMV
<6.55 µg/L 6.55 22.2Hexachlorocyclopentadiene 1 09/07/21 22:56 V8592JMV
<5.79 µg/L 5.79 11.1Hexachloroethane 1 09/07/21 22:56 V8592JMV
<6.88 µg/L 6.88 11.1Indeno(1,2,3-cd)pyrene 1 09/07/21 22:56 V8592JMV
<7.45 µg/L 7.45 11.1
Isophorone 1 09/07/21 22:56 V8592JMV
<8.14 µg/L 8.14 11.11-Methylnaphthalene 1 09/07/21 22:56 V8592JMV
<7.68 µg/L 7.68 11.12-Methylnaphthalene 1 09/07/21 22:56 V8592JMV
<5.84 µg/L 5.84 11.12-Methylphenol 1 09/07/21 22:56 V8592JMV
<2.74 µg/L 2.74 11.13&4 Methylphenol 1 09/07/21 22:56 V8592JMV
<8.75 µg/L 8.75 11.1Naphthalene 1 09/07/21 22:56 V8592JMV
<5.46 µg/L 5.46 11.12-Nitroaniline 1 09/07/21 22:56 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-3
94719 Matrix:
8/31/2021 15:43
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<5.05 µg/L 5.05 11.13-Nitroaniline 1 09/07/21 22:56 V8592JMV
<5.66 µg/L 5.66 11.14-Nitroaniline 1 09/07/21 22:56 V8592JMV
<8.75 µg/L 8.75 11.1Nitrobenzene 1 09/07/21 22:56 V8592JMV
<6.09 µg/L 6.09 11.12-Nitrophenol 1 09/07/21 22:56 V8592JMV
<3.12 µg/L 3.12 11.14-Nitrophenol 1 09/07/21 22:56 V8592JMV
<7.20 µg/L 7.20 11.1N-Nitrosodimethylamine 1 09/07/21 22:56 V8592JMV
<12.1 µg/L 12.1 22.2N-Nitrosodiphenylamine 1 09/07/21 22:56 V8592JMV
<8.99 µg/L 8.99 22.2N-Nitroso-di-n-propylamine 1 09/07/21 22:56 V8592JMV
<10.8 µg/L 10.8 55.6
Pentachlorophenol 1 09/07/21 22:56 V8592JMV
<7.04 µg/L 7.04 11.1Phenanthrene 1 09/07/21 22:56 V8592JMV
<3.17 µg/L 3.17 11.1Phenol 1 09/07/21 22:56 V8592JMV
<6.02 µg/L 6.02 11.1Pyrene 1 09/07/21 22:56 V8592JMV
<5.91 µg/L 5.91 11.1Pyridine 1 09/07/21 22:56 V8592JMV
<6.94 µg/L 6.94 11.11,2,4-Trichlorobenzene 1 09/07/21 22:56 V8592JMV
<6.45 µg/L 6.45 22.22,4,5-Trichlorophenol 1 09/07/21 22:56 V8592JMV
<6.98 µg/L 6.98 22.2
2,4,6-Trichlorophenol 1 09/07/21 22:56 V8592JMV
Surrogate: Phenol-d5 23.0 Limits: 11-100%09/07/21 22:561 JMV V8592
Surrogate: 2-Fluorobiphenyl 64.4 Limits: 44-119%09/07/21 22:561 JMV V8592
Surrogate: 2-Fluorophenol 33.4 Limits: 19-119%09/07/21 22:561 JMV V8592
Surrogate: Nitrobenzene-d5 57.2 Limits: 44-120%09/07/21 22:561 JMV V8592
Surrogate: 4-Terphenyl-d14 97.8 Limits: 50-134%09/07/21 22:561 JMV V8592
Surrogate: 2,4,6-Tribromophenol 93.7 Limits: 43-140%09/07/21 22:561 JMV V8592
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-4
94720 Matrix:
8/31/2021 13:37
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
0.538 JB µg/L 0.170 1.00Arsenic 1 09/08/21 18:46 6020BEDV
141 µg/L 0.810 10.0Barium 1 09/07/21 18:38 6020BEDV
<0.160 µg/L 0.160 1.00Cadmium 1 09/07/21 18:38 6020BEDV
50.0 µg/L 0.790 2.00Chromium 1 09/07/21 18:38 6020BEDV
0.663 J µg/L 0.260 1.00Lead 1 09/07/21 18:38 6020BEDV
<0.00007 mg/L 0.00007 0.00020
Mercury (Total)1 09/07/21 17:06 7470AEDV
<0.740 µg/L 0.740 5.00Selenium 1 09/08/21 18:46 6020BEDV
<0.110 µg/L 0.110 1.00Silver 1 09/07/21 18:38 6020BEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 34 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-4
94720 Matrix:
8/31/2021 13:37
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
7.02 µg/L 1.80 5.00Acetone 1 09/10/21 10:01 V8614JLB
<2.00 µg/L 2.00 5.00Acrolein 1 09/10/21 10:01 V8614JLB
<0.230 µg/L 0.230 5.00Acrylonitrile 1 09/10/21 10:01 V8614JLB
<0.180 µg/L 0.180 0.500Benzene 1 09/10/21 10:01 V8614JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/10/21 10:01 V8614JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/10/21 10:01 V8614JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/10/21 10:01 V8614JLB
<1.50 µg/L 1.50 5.00Bromoform 1 09/10/21 10:01 V8614JLB
<0.280 µg/L 0.280 1.00
Bromomethane 1 09/10/21 10:01 V8614JLB
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 09/10/21 10:01 V8614JLB
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/10/21 10:01 V8614JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/10/21 10:01 V8614JLB
0.458 J µg/L 0.150 5.00Carbon Disulfide 1 09/10/21 10:01 V8614JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/10/21 10:01 V8614JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/10/21 10:01 V8614JLB
<0.190 µg/L 0.190 0.500
Chlorodibromomethane 1 09/10/21 10:01 V8614JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 09/10/21 10:01 V8614JLB
<0.220 µg/L 0.220 0.500Chloroform 1 09/10/21 10:01 V8614JLB
<0.220 µg/L 0.220 0.500Chloromethane 1 09/10/21 10:01 V8614JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/10/21 10:01 V8614JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/10/21 10:01 V8614JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 09/10/21 10:01 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-4
94720 Matrix:
8/31/2021 13:37
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/10/21 10:01 V8614JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/10/21 10:01 V8614JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/10/21 10:01 V8614JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/10/21 10:01 V8614JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/10/21 10:01 V8614JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/10/21 10:01 V8614JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/10/21 10:01 V8614JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/10/21 10:01 V8614JLB
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 09/10/21 10:01 V8614JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/10/21 10:01 V8614JLB
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/10/21 10:01 V8614JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/10/21 10:01 V8614JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/10/21 10:01 V8614JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/10/21 10:01 V8614JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/10/21 10:01 V8614JLB
<0.200 µg/L 0.200 0.500
1,1-Dichloropropene 1 09/10/21 10:01 V8614JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/10/21 10:01 V8614JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/10/21 10:01 V8614JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/10/21 10:01 V8614JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 09/10/21 10:01 V8614JLB
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 09/10/21 10:01 V8614JLB
<1.30 µg/L 1.30 10.0n-Hexane 1 09/10/21 10:01 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-4
94720 Matrix:
8/31/2021 13:37
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<0.380 µg/L 0.380 5.002-Hexanone 1 09/10/21 10:01 V8614JLB
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 09/10/21 10:01 V8614JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/10/21 10:01 V8614JLB
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/10/21 10:01 V8614JLB
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 09/10/21 10:01 V8614JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 09/10/21 10:01 V8614JLB
<0.330 µg/L 0.330 1.00Methylene Chloride 1 09/10/21 10:01 V8614JLB
<0.470 µg/L 0.470 1.00Naphthalene 1 09/10/21 10:01 V8614JLB
<0.190 µg/L 0.190 0.500
n-Propylbenzene 1 09/10/21 10:01 V8614JLB
<0.220 µg/L 0.220 0.500Styrene 1 09/10/21 10:01 V8614JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/10/21 10:01 V8614JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/10/21 10:01 V8614JLB
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/10/21 10:01 V8614JLB
<0.220 µg/L 0.220 0.500Toluene 1 09/10/21 10:01 V8614JLB
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 09/10/21 10:01 V8614JLB
<0.310 µg/L 0.310 1.00
1,2,4-Trichlorobenzene 1 09/10/21 10:01 V8614JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/10/21 10:01 V8614JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/10/21 10:01 V8614JLB
0.461 J µg/L 0.180 0.500Trichloroethene 1 09/10/21 10:01 V8614JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/10/21 10:01 V8614JLB
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 09/10/21 10:01 V8614JLB
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/10/21 10:01 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-4
94720 Matrix:
8/31/2021 13:37
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 09/10/21 10:01 V8614JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/10/21 10:01 V8614JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 09/10/21 10:01 V8614JLB
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/10/21 10:01 V8614JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/10/21 10:01 V8614
Surrogate: 4-Bromofluorobenzene 104 Limits: 80-124%09/10/21 10:011 JLB V8614
Surrogate: Dibromofluoromethane 105 Limits: 75-129%09/10/21 10:011 JLB V8614
Surrogate: 1,2-Dichloroethane - d4 96.4 Limits: 63-136%09/10/21 10:011 JLB V8614
Surrogate: Toluene-d8 99.4 Limits: 77-123%09/10/21 10:011 JLB V8614
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<8.08 µg/L 8.08 22.7
Acenaphthene 1 09/07/21 23:18 V8592JMV
<7.88 µg/L 7.88 22.7Acenaphthylene 1 09/07/21 23:18 V8592JMV
<8.10 µg/L 8.10 56.8Aniline 1 09/07/21 23:18 V8592JMV
<7.49 µg/L 7.49 11.4Anthracene 1 09/07/21 23:18 V8592JMV
<6.44 µg/L 6.44 11.4Benzo(a)anthracene 1 09/07/21 23:18 V8592JMV
<5.32 µg/L 5.32 11.4Benzo(a)pyrene 1 09/07/21 23:18 V8592JMV
<5.15 µg/L 5.15 11.4Benzo(b)fluoranthene 1 09/07/21 23:18 V8592JMV
<4.83 µg/L 4.83 11.4
Benzo(g,h,i)perylene 1 09/07/21 23:18 V8592JMV
<5.34 µg/L 5.34 11.4Benzo(k)fluoranthene 1 09/07/21 23:18 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-4
94720 Matrix:
8/31/2021 13:37
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<13.1 µg/L 13.1 114Benzoic Acid 1 09/07/21 23:18 V8592JMV
<9.80 µg/L 9.80 11.4Benzyl alcohol 1 09/07/21 23:18 V8592JMV
<6.46 µg/L 6.46 11.4Bis(2-Chloroethoxy)methane 1 09/07/21 23:18 V8592JMV
<8.32 µg/L 8.32 11.4Bis(2-Chloroethyl)ether 1 09/07/21 23:18 V8592JMV
<7.51 µg/L 7.51 11.4Bis(2-Chloroisopropyl)ether 1 09/07/21 23:18 V8592JMV
<10.0 µg/L 10.0 11.4Bis(2-ethylhexyl)phthalate 1 09/07/21 23:18 V8592JMV
<7.11 µg/L 7.11 22.74-Bromophenyl phenyl ether 1 09/07/21 23:18 V8592JMV
<3.35 µg/L 3.35 11.4Butyl benzyl phthalate 1 09/07/21 23:18 V8592JMV
<5.96 µg/L 5.96 11.4
4-Chloro-3-methylphenol 1 09/07/21 23:18 V8592JMV
<6.18 µg/L 6.18 11.44-Chloroaniline 1 09/07/21 23:18 V8592JMV
<8.38 µg/L 8.38 22.72-Chloronaphthalene 1 09/07/21 23:18 V8592JMV
<7.50 µg/L 7.50 11.42-Chlorophenol 1 09/07/21 23:18 V8592JMV
<7.93 µg/L 7.93 22.74-Chlorophenyl phenyl ether 1 09/07/21 23:18 V8592JMV
<6.13 µg/L 6.13 11.4Chrysene 1 09/07/21 23:18 V8592JMV
<6.82 µg/L 6.82 22.7Dibenz(a,h)anthracene 1 09/07/21 23:18 V8592JMV
<5.77 µg/L 5.77 22.7
Dibenzofuran 1 09/07/21 23:18 V8592JMV
<6.74 µg/L 6.74 11.41,2-Dichlorobenzene 1 09/07/21 23:18 V8592JMV
<6.65 µg/L 6.65 11.41,3-Dichlorobenzene 1 09/07/21 23:18 V8592JMV
<6.74 µg/L 6.74 11.41,4-Dichlorobenzene 1 09/07/21 23:18 V8592JMV
<7.52 µg/L 7.52 11.43,3'-Dichlorobenzidine 1 09/07/21 23:18 V8592JMV
<6.32 µg/L 6.32 11.42,4-Dichlorophenol 1 09/07/21 23:18 V8592JMV
<10.6 µg/L 10.6 22.7Diethyl phthalate 1 09/07/21 23:18 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-4
94720 Matrix:
8/31/2021 13:37
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<8.91 µg/L 8.91 11.4Dimethyl phthalate 1 09/07/21 23:18 V8592JMV
<12.4 µg/L 12.4 22.72,4-Dimethylphenol 1 09/07/21 23:18 V8592JMV
<8.38 µg/L 8.38 11.4Di-n-butyl phthalate 1 09/07/21 23:18 V8592JMV
<11.3 µg/L 11.3 34.14,6-Dinitro-2-methylphenol 1 09/07/21 23:18 V8592JMV
<12.0 µg/L 12.0 34.12,4-Dinitrophenol 1 09/07/21 23:18 V8592JMV
<5.93 µg/L 5.93 11.42,4-Dinitrotoluene 1 09/07/21 23:18 V8592JMV
<6.70 µg/L 6.70 22.72,6-Dinitrotoluene 1 09/07/21 23:18 V8592JMV
<5.71 µg/L 5.71 11.4Di-n-Octyl Phthalate 1 09/07/21 23:18 V8592JMV
<6.87 µg/L 6.87 11.4
Fluoranthene 1 09/07/21 23:18 V8592JMV
<8.29 µg/L 8.29 11.4Fluorene 1 09/07/21 23:18 V8592JMV
<6.53 µg/L 6.53 22.7Hexachlorobenzene 1 09/07/21 23:18 V8592JMV
<6.67 µg/L 6.67 22.7Hexachlorobutadiene 1 09/07/21 23:18 V8592JMV
<6.70 µg/L 6.70 22.7Hexachlorocyclopentadiene 1 09/07/21 23:18 V8592JMV
<5.95 µg/L 5.95 11.4Hexachloroethane 1 09/07/21 23:18 V8592JMV
<7.07 µg/L 7.07 11.4Indeno(1,2,3-cd)pyrene 1 09/07/21 23:18 V8592JMV
<7.65 µg/L 7.65 11.4
Isophorone 1 09/07/21 23:18 V8592JMV
<8.36 µg/L 8.36 11.41-Methylnaphthalene 1 09/07/21 23:18 V8592JMV
<7.89 µg/L 7.89 11.42-Methylnaphthalene 1 09/07/21 23:18 V8592JMV
<6.00 µg/L 6.00 11.42-Methylphenol 1 09/07/21 23:18 V8592JMV
<2.82 µg/L 2.82 11.43&4 Methylphenol 1 09/07/21 23:18 V8592JMV
<8.98 µg/L 8.98 11.4Naphthalene 1 09/07/21 23:18 V8592JMV
<5.61 µg/L 5.61 11.42-Nitroaniline 1 09/07/21 23:18 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:MW-4
94720 Matrix:
8/31/2021 13:37
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<5.19 µg/L 5.19 11.43-Nitroaniline 1 09/07/21 23:18 V8592JMV
<5.81 µg/L 5.81 11.44-Nitroaniline 1 09/07/21 23:18 V8592JMV
<8.98 µg/L 8.98 11.4Nitrobenzene 1 09/07/21 23:18 V8592JMV
<6.26 µg/L 6.26 11.42-Nitrophenol 1 09/07/21 23:18 V8592JMV
<3.20 µg/L 3.20 11.44-Nitrophenol 1 09/07/21 23:18 V8592JMV
<7.40 µg/L 7.40 11.4N-Nitrosodimethylamine 1 09/07/21 23:18 V8592JMV
<12.4 µg/L 12.4 22.7N-Nitrosodiphenylamine 1 09/07/21 23:18 V8592JMV
<9.19 µg/L 9.19 22.7N-Nitroso-di-n-propylamine 1 09/07/21 23:18 V8592JMV
<11.1 µg/L 11.1 56.8
Pentachlorophenol 1 09/07/21 23:18 V8592JMV
<7.23 µg/L 7.23 11.4Phenanthrene 1 09/07/21 23:18 V8592JMV
<3.26 µg/L 3.26 11.4Phenol 1 09/07/21 23:18 V8592JMV
<6.18 µg/L 6.18 11.4Pyrene 1 09/07/21 23:18 V8592JMV
<6.06 µg/L 6.06 11.4Pyridine 1 09/07/21 23:18 V8592JMV
<7.13 µg/L 7.13 11.41,2,4-Trichlorobenzene 1 09/07/21 23:18 V8592JMV
<6.59 µg/L 6.59 22.72,4,5-Trichlorophenol 1 09/07/21 23:18 V8592JMV
<7.14 µg/L 7.14 22.7
2,4,6-Trichlorophenol 1 09/07/21 23:18 V8592JMV
Surrogate: Phenol-d5 24.9 Limits: 11-100%09/07/21 23:181 JMV V8592
Surrogate: 2-Fluorobiphenyl 67.4 Limits: 44-119%09/07/21 23:181 JMV V8592
Surrogate: 2-Fluorophenol 36.1 Limits: 19-119%09/07/21 23:181 JMV V8592
Surrogate: Nitrobenzene-d5 58.5 Limits: 44-120%09/07/21 23:181 JMV V8592
Surrogate: 4-Terphenyl-d14 91.9 Limits: 50-134%09/07/21 23:181 JMV V8592
Surrogate: 2,4,6-Tribromophenol 82.2 Limits: 43-140%09/07/21 23:181 JMV V8592
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:DUP-1 water
94721 Matrix:
8/31/2021 0:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
0.500 JB µg/L 0.170 1.00Arsenic 1 09/08/21 18:53 6020BEDV
139 µg/L 0.810 10.0Barium 1 09/07/21 18:57 6020BEDV
<0.160 µg/L 0.160 1.00Cadmium 1 09/07/21 18:57 6020BEDV
50.7 µg/L 0.790 2.00Chromium 1 09/07/21 18:57 6020BEDV
0.676 J µg/L 0.260 1.00Lead 1 09/07/21 18:57 6020BEDV
<0.00007 mg/L 0.00007 0.00020
Mercury (Total)1 09/07/21 17:08 7470AEDV
<0.740 µg/L 0.740 5.00Selenium 1 09/08/21 18:53 6020BEDV
<0.110 µg/L 0.110 1.00Silver 1 09/07/21 18:57 6020BEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 42 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:DUP-1 water
94721 Matrix:
8/31/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
7.99 µg/L 1.80 5.00Acetone 1 09/10/21 10:25 V8614JLB
<2.00 µg/L 2.00 5.00Acrolein 1 09/10/21 10:25 V8614JLB
<0.230 µg/L 0.230 5.00Acrylonitrile 1 09/10/21 10:25 V8614JLB
<0.180 µg/L 0.180 0.500Benzene 1 09/10/21 10:25 V8614JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 09/10/21 10:25 V8614JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 09/10/21 10:25 V8614JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 09/10/21 10:25 V8614JLB
<1.50 µg/L 1.50 5.00Bromoform 1 09/10/21 10:25 V8614JLB
<0.280 µg/L 0.280 1.00
Bromomethane 1 09/10/21 10:25 V8614JLB
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 09/10/21 10:25 V8614JLB
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 09/10/21 10:25 V8614JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 09/10/21 10:25 V8614JLB
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 09/10/21 10:25 V8614JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 09/10/21 10:25 V8614JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 09/10/21 10:25 V8614JLB
<0.190 µg/L 0.190 0.500
Chlorodibromomethane 1 09/10/21 10:25 V8614JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 09/10/21 10:25 V8614JLB
<0.220 µg/L 0.220 0.500Chloroform 1 09/10/21 10:25 V8614JLB
<0.220 µg/L 0.220 0.500Chloromethane 1 09/10/21 10:25 V8614JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 09/10/21 10:25 V8614JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 09/10/21 10:25 V8614JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 09/10/21 10:25 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:DUP-1 water
94721 Matrix:
8/31/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 09/10/21 10:25 V8614JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 09/10/21 10:25 V8614JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 09/10/21 10:25 V8614JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 09/10/21 10:25 V8614JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 09/10/21 10:25 V8614JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 09/10/21 10:25 V8614JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 09/10/21 10:25 V8614JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 09/10/21 10:25 V8614JLB
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 09/10/21 10:25 V8614JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 09/10/21 10:25 V8614JLB
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 09/10/21 10:25 V8614JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 09/10/21 10:25 V8614JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 09/10/21 10:25 V8614JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 09/10/21 10:25 V8614JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 09/10/21 10:25 V8614JLB
<0.200 µg/L 0.200 0.500
1,1-Dichloropropene 1 09/10/21 10:25 V8614JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 09/10/21 10:25 V8614JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 09/10/21 10:25 V8614JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 09/10/21 10:25 V8614JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 09/10/21 10:25 V8614JLB
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 09/10/21 10:25 V8614JLB
<1.30 µg/L 1.30 10.0n-Hexane 1 09/10/21 10:25 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:DUP-1 water
94721 Matrix:
8/31/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<0.380 µg/L 0.380 5.002-Hexanone 1 09/10/21 10:25 V8614JLB
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 09/10/21 10:25 V8614JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 09/10/21 10:25 V8614JLB
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 09/10/21 10:25 V8614JLB
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 09/10/21 10:25 V8614JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 09/10/21 10:25 V8614JLB
<0.330 µg/L 0.330 1.00Methylene Chloride 1 09/10/21 10:25 V8614JLB
<0.470 µg/L 0.470 1.00Naphthalene 1 09/10/21 10:25 V8614JLB
<0.190 µg/L 0.190 0.500
n-Propylbenzene 1 09/10/21 10:25 V8614JLB
<0.220 µg/L 0.220 0.500Styrene 1 09/10/21 10:25 V8614JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 09/10/21 10:25 V8614JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 09/10/21 10:25 V8614JLB
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 09/10/21 10:25 V8614JLB
<0.220 µg/L 0.220 0.500Toluene 1 09/10/21 10:25 V8614JLB
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 09/10/21 10:25 V8614JLB
<0.310 µg/L 0.310 1.00
1,2,4-Trichlorobenzene 1 09/10/21 10:25 V8614JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 09/10/21 10:25 V8614JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 09/10/21 10:25 V8614JLB
0.516 µg/L 0.180 0.500Trichloroethene 1 09/10/21 10:25 V8614JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 09/10/21 10:25 V8614JLB
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 09/10/21 10:25 V8614JLB
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 09/10/21 10:25 V8614JLB
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:DUP-1 water
94721 Matrix:
8/31/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V8613 09/09/21 09:00
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 09/10/21 10:25 V8614JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 09/10/21 10:25 V8614JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 09/10/21 10:25 V8614JLB
<0.420 µg/L 0.420 1.00m,p-Xylene 1 09/10/21 10:25 V8614JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 09/10/21 10:25 V8614
Surrogate: 4-Bromofluorobenzene 101 Limits: 80-124%09/10/21 10:251 JLB V8614
Surrogate: Dibromofluoromethane 104 Limits: 75-129%09/10/21 10:251 JLB V8614
Surrogate: 1,2-Dichloroethane - d4 95.4 Limits: 63-136%09/10/21 10:251 JLB V8614
Surrogate: Toluene-d8 98.6 Limits: 77-123%09/10/21 10:251 JLB V8614
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<7.83 µg/L 7.83 22.0
Acenaphthene 1 09/07/21 22:11 V8592JMV
<7.63 µg/L 7.63 22.0Acenaphthylene 1 09/07/21 22:11 V8592JMV
<7.83 µg/L 7.83 54.9Aniline 1 09/07/21 22:11 V8592JMV
<7.23 µg/L 7.23 11.0Anthracene 1 09/07/21 22:11 V8592JMV
<6.22 µg/L 6.22 11.0Benzo(a)anthracene 1 09/07/21 22:11 V8592JMV
<5.14 µg/L 5.14 11.0Benzo(a)pyrene 1 09/07/21 22:11 V8592JMV
<4.97 µg/L 4.97 11.0Benzo(b)fluoranthene 1 09/07/21 22:11 V8592JMV
<4.66 µg/L 4.66 11.0
Benzo(g,h,i)perylene 1 09/07/21 22:11 V8592JMV
<5.15 µg/L 5.15 11.0Benzo(k)fluoranthene 1 09/07/21 22:11 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:DUP-1 water
94721 Matrix:
8/31/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<12.7 µg/L 12.7 110Benzoic Acid 1 09/07/21 22:11 V8592JMV
<9.46 µg/L 9.46 11.0Benzyl alcohol 1 09/07/21 22:11 V8592JMV
<6.24 µg/L 6.24 11.0Bis(2-Chloroethoxy)methane 1 09/07/21 22:11 V8592JMV
<8.03 µg/L 8.03 11.0Bis(2-Chloroethyl)ether 1 09/07/21 22:11 V8592JMV
<7.25 µg/L 7.25 11.0Bis(2-Chloroisopropyl)ether 1 09/07/21 22:11 V8592JMV
<9.68 µg/L 9.68 11.0Bis(2-ethylhexyl)phthalate 1 09/07/21 22:11 V8592JMV
<6.89 µg/L 6.89 22.04-Bromophenyl phenyl ether 1 09/07/21 22:11 V8592JMV
<3.23 µg/L 3.23 11.0Butyl benzyl phthalate 1 09/07/21 22:11 V8592JMV
<5.75 µg/L 5.75 11.0
4-Chloro-3-methylphenol 1 09/07/21 22:11 V8592JMV
<5.96 µg/L 5.96 11.04-Chloroaniline 1 09/07/21 22:11 V8592JMV
<8.12 µg/L 8.12 22.02-Chloronaphthalene 1 09/07/21 22:11 V8592JMV
<7.24 µg/L 7.24 11.02-Chlorophenol 1 09/07/21 22:11 V8592JMV
<7.69 µg/L 7.69 22.04-Chlorophenyl phenyl ether 1 09/07/21 22:11 V8592JMV
<5.92 µg/L 5.92 11.0Chrysene 1 09/07/21 22:11 V8592JMV
<6.61 µg/L 6.61 22.0Dibenz(a,h)anthracene 1 09/07/21 22:11 V8592JMV
<5.59 µg/L 5.59 22.0
Dibenzofuran 1 09/07/21 22:11 V8592JMV
<6.50 µg/L 6.50 11.01,2-Dichlorobenzene 1 09/07/21 22:11 V8592JMV
<6.41 µg/L 6.41 11.01,3-Dichlorobenzene 1 09/07/21 22:11 V8592JMV
<6.50 µg/L 6.50 11.01,4-Dichlorobenzene 1 09/07/21 22:11 V8592JMV
<7.26 µg/L 7.26 11.03,3'-Dichlorobenzidine 1 09/07/21 22:11 V8592JMV
<6.09 µg/L 6.09 11.02,4-Dichlorophenol 1 09/07/21 22:11 V8592JMV
<10.3 µg/L 10.3 22.0Diethyl phthalate 1 09/07/21 22:11 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:DUP-1 water
94721 Matrix:
8/31/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<8.60 µg/L 8.60 11.0Dimethyl phthalate 1 09/07/21 22:11 V8592JMV
<12.0 µg/L 12.0 22.02,4-Dimethylphenol 1 09/07/21 22:11 V8592JMV
<8.09 µg/L 8.09 11.0Di-n-butyl phthalate 1 09/07/21 22:11 V8592JMV
<10.9 µg/L 10.9 33.04,6-Dinitro-2-methylphenol 1 09/07/21 22:11 V8592JMV
<11.7 µg/L 11.7 33.02,4-Dinitrophenol 1 09/07/21 22:11 V8592JMV
<5.72 µg/L 5.72 11.02,4-Dinitrotoluene 1 09/07/21 22:11 V8592JMV
<6.49 µg/L 6.49 22.02,6-Dinitrotoluene 1 09/07/21 22:11 V8592JMV
<5.51 µg/L 5.51 11.0Di-n-Octyl Phthalate 1 09/07/21 22:11 V8592JMV
<6.63 µg/L 6.63 11.0
Fluoranthene 1 09/07/21 22:11 V8592JMV
<8.00 µg/L 8.00 11.0Fluorene 1 09/07/21 22:11 V8592JMV
<6.33 µg/L 6.33 22.0Hexachlorobenzene 1 09/07/21 22:11 V8592JMV
<6.47 µg/L 6.47 22.0Hexachlorobutadiene 1 09/07/21 22:11 V8592JMV
<6.49 µg/L 6.49 22.0Hexachlorocyclopentadiene 1 09/07/21 22:11 V8592JMV
<5.74 µg/L 5.74 11.0Hexachloroethane 1 09/07/21 22:11 V8592JMV
<6.82 µg/L 6.82 11.0Indeno(1,2,3-cd)pyrene 1 09/07/21 22:11 V8592JMV
<7.38 µg/L 7.38 11.0
Isophorone 1 09/07/21 22:11 V8592JMV
<8.06 µg/L 8.06 11.01-Methylnaphthalene 1 09/07/21 22:11 V8592JMV
<7.61 µg/L 7.61 11.02-Methylnaphthalene 1 09/07/21 22:11 V8592JMV
<5.79 µg/L 5.79 11.02-Methylphenol 1 09/07/21 22:11 V8592JMV
<2.72 µg/L 2.72 11.03&4 Methylphenol 1 09/07/21 22:11 V8592JMV
<8.67 µg/L 8.67 11.0Naphthalene 1 09/07/21 22:11 V8592JMV
<5.41 µg/L 5.41 11.02-Nitroaniline 1 09/07/21 22:11 V8592JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:DUP-1 water
94721 Matrix:
8/31/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V8443 09/07/21 10:20
<5.01 µg/L 5.01 11.03-Nitroaniline 1 09/07/21 22:11 V8592JMV
<5.61 µg/L 5.61 11.04-Nitroaniline 1 09/07/21 22:11 V8592JMV
<8.67 µg/L 8.67 11.0Nitrobenzene 1 09/07/21 22:11 V8592JMV
<6.04 µg/L 6.04 11.02-Nitrophenol 1 09/07/21 22:11 V8592JMV
<3.09 µg/L 3.09 11.04-Nitrophenol 1 09/07/21 22:11 V8592JMV
<7.14 µg/L 7.14 11.0N-Nitrosodimethylamine 1 09/07/21 22:11 V8592JMV
<12.0 µg/L 12.0 22.0N-Nitrosodiphenylamine 1 09/07/21 22:11 V8592JMV
<8.91 µg/L 8.91 22.0N-Nitroso-di-n-propylamine 1 09/07/21 22:11 V8592JMV
<10.7 µg/L 10.7 54.9
Pentachlorophenol 1 09/07/21 22:11 V8592JMV
<6.97 µg/L 6.97 11.0Phenanthrene 1 09/07/21 22:11 V8592JMV
<3.15 µg/L 3.15 11.0Phenol 1 09/07/21 22:11 V8592JMV
<5.96 µg/L 5.96 11.0Pyrene 1 09/07/21 22:11 V8592JMV
<5.85 µg/L 5.85 11.0Pyridine 1 09/07/21 22:11 V8592JMV
<6.88 µg/L 6.88 11.01,2,4-Trichlorobenzene 1 09/07/21 22:11 V8592JMV
<6.39 µg/L 6.39 22.02,4,5-Trichlorophenol 1 09/07/21 22:11 V8592JMV
<6.92 µg/L 6.92 22.0
2,4,6-Trichlorophenol 1 09/07/21 22:11 V8592JMV
Surrogate: Phenol-d5 23.0 Limits: 11-100%09/07/21 22:111 JMV V8592
Surrogate: 2-Fluorobiphenyl 66.1 Limits: 44-119%09/07/21 22:111 JMV V8592
Surrogate: 2-Fluorophenol 33.1 Limits: 19-119%09/07/21 22:111 JMV V8592
Surrogate: Nitrobenzene-d5 58.1 Limits: 44-120%09/07/21 22:111 JMV V8592
Surrogate: 4-Terphenyl-d14 92.7 Limits: 50-134%09/07/21 22:111 JMV V8592
Surrogate: 2,4,6-Tribromophenol 83.8 Limits: 43-140%09/07/21 22:111 JMV V8592
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S-9(7-8)
94722 Matrix:
8/30/2021 13:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.3 %Moisture 1 09/08/21 17:27 SW-DRYWTBAM
2.09 mg/Kg - dry 0.126 1.34Arsenic 10 09/07/21 22:56 6020BEDV
345 mg/Kg - dry 1.87 13.4Barium 10 09/07/21 22:56 6020BEDV
<0.0736 mg/Kg - dry 0.0736 0.669Cadmium 10 09/07/21 22:56 6020BEDV
53.1 mg/Kg - dry 0.388 1.34Chromium 10 09/07/21 22:56 6020BEDV
4.20 mg/Kg - dry 0.187 1.34
Lead 10 09/07/21 22:56 6020BEDV
<0.0161 mg/Kg - dry 0.0161 0.0402Mercury (Total)1 09/08/21 14:12 7471BEDV
5.76 mg/Kg - dry 1.20 2.68Selenium 10 09/08/21 22:52 6020BEDV
<0.0548 mg/Kg - dry 0.0548 0.669Silver 10 09/07/21 22:56 6020BEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 50 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S-9(7-8)
94722 Matrix:
8/30/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8480 09/07/21 08:00
0.023 J mg/Kg - dry 0.003 0.026Acetone 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 09/07/21 11:07 V8481TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/07/21 11:07 V8481TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 09/07/21 11:07 V8481TBL
0.001 J mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 09/07/21 11:07 V8481TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/07/21 11:07 V8481TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/07/21 11:07 V8481TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 09/07/21 11:07 V8481TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/07/21 11:07 V8481TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 09/07/21 11:07 V8481TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S-9(7-8)
94722 Matrix:
8/30/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8480 09/07/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 09/07/21 11:07 V8481TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/07/21 11:07 V8481TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/07/21 11:07 V8481TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/07/21 11:07 V8481TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/07/21 11:07 V8481TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/07/21 11:07 V8481TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/07/21 11:07 V8481TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.066Ethyl Tertiary Butyl Ether (ETBE)1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 09/07/21 11:07 V8481TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 09/07/21 11:07 V8481TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S-9(7-8)
94722 Matrix:
8/30/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8480 09/07/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 09/07/21 11:07 V8481TBL
0.001 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/07/21 11:07 V8481TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 09/07/21 11:07 V8481TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/07/21 11:07 V8481TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 09/07/21 11:07 V8481TBL
0.002 J mg/Kg - dry 0.001 0.013Methylene Chloride 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/07/21 11:07 V8481TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/07/21 11:07 V8481TBL
0.002 J mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/07/21 11:07 V8481TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 09/07/21 11:07 V8481TBL
<0.0009 mg/Kg - dry 0.0009 0.013
1,2,4-Trichlorobenzene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/07/21 11:07 V8481TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/07/21 11:07 V8481TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 09/07/21 11:07 V8481TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 09/07/21 11:07 V8481TBL
0.001 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/07/21 11:07 V8481TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S-9(7-8)
94722 Matrix:
8/30/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8480 09/07/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 09/07/21 11:07 V8481TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 09/07/21 11:07 V8481TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 09/07/21 11:07 V8481TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 09/07/21 11:07 V8481
Surrogate: 4-Bromofluorobenzene 139 *Limits: 70-130%09/07/21 11:071 TBL V8481
Surrogate: Dibromofluoromethane 105 Limits: 84-123%09/07/21 11:071 TBL V8481
Surrogate: Toluene-d8 108 Limits: 76-129%09/07/21 11:071 TBL V8481
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.155 mg/Kg - dry 0.155 0.883Acenaphthene 1 09/07/21 17:21 V8596JMV
<0.140 mg/Kg - dry 0.140 0.883Acenaphthylene 1 09/07/21 17:21 V8596JMV
<0.203 mg/Kg - dry 0.203 0.883Aniline 1 09/07/21 17:21 V8596JMV
<0.191 mg/Kg - dry 0.191 0.883Anthracene 1 09/07/21 17:21 V8596JMV
<0.186 mg/Kg - dry 0.186 0.883Benzo(a)anthracene 1 09/07/21 17:21 V8596JMV
<0.196 mg/Kg - dry 0.196 0.883Benzo(a)pyrene 1 09/07/21 17:21 V8596JMV
<0.195 mg/Kg - dry 0.195 0.883
Benzo(b)fluoranthene 1 09/07/21 17:21 V8596JMV
<0.182 mg/Kg - dry 0.182 0.883Benzo(g,h,i)perylene 1 09/07/21 17:21 V8596JMV
<0.183 mg/Kg - dry 0.183 0.883Benzo(k)fluoranthene 1 09/07/21 17:21 V8596JMV
<0.776 mg/Kg - dry 0.776 2.68Benzoic Acid 1 09/07/21 17:21 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S-9(7-8)
94722 Matrix:
8/30/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.140 mg/Kg - dry 0.140 0.883Benzyl alcohol 1 09/07/21 17:21 V8596JMV
<0.157 mg/Kg - dry 0.157 0.883Bis(2-Chloroethoxy)methane 1 09/07/21 17:21 V8596JMV
<0.143 mg/Kg - dry 0.143 0.883Bis(2-Chloroethyl)ether 1 09/07/21 17:21 V8596JMV
<0.182 mg/Kg - dry 0.182 0.441Bis(2-Chloroisopropyl)ether 1 09/07/21 17:21 V8596JMV
<0.160 mg/Kg - dry 0.160 0.883Bis(2-ethylhexyl)phthalate 1 09/07/21 17:21 V8596JMV
<0.145 mg/Kg - dry 0.145 0.8834-Bromophenyl phenyl ether 1 09/07/21 17:21 V8596JMV
<0.151 mg/Kg - dry 0.151 0.441Butyl benzyl phthalate 1 09/07/21 17:21 V8596JMV
<0.123 mg/Kg - dry 0.123 0.8834-Chloro-3-methylphenol 1 09/07/21 17:21 V8596JMV
<0.149 mg/Kg - dry 0.149 0.441
4-Chloroaniline 1 09/07/21 17:21 V8596JMV
<0.155 mg/Kg - dry 0.155 0.8832-Chloronaphthalene 1 09/07/21 17:21 V8596JMV
<0.131 mg/Kg - dry 0.131 0.8832-Chlorophenol 1 09/07/21 17:21 V8596JMV
<0.168 mg/Kg - dry 0.168 1.344-Chlorophenyl phenyl ether 1 09/07/21 17:21 V8596JMV
<0.190 mg/Kg - dry 0.190 0.883Chrysene 1 09/07/21 17:21 V8596JMV
<0.307 mg/Kg - dry 0.307 0.883Dibenz(a,h)anthracene 1 09/07/21 17:21 V8596JMV
<0.159 mg/Kg - dry 0.159 0.883Dibenzofuran 1 09/07/21 17:21 V8596JMV
<0.126 mg/Kg - dry 0.126 0.883
1,2-Dichlorobenzene 1 09/07/21 17:21 V8596JMV
<0.130 mg/Kg - dry 0.130 0.8831,3-Dichlorobenzene 1 09/07/21 17:21 V8596JMV
<0.130 mg/Kg - dry 0.130 0.4411,4-Dichlorobenzene 1 09/07/21 17:21 V8596JMV
<0.196 mg/Kg - dry 0.196 0.8833,3'-Dichlorobenzidine 1 09/07/21 17:21 V8596JMV
<0.128 mg/Kg - dry 0.128 0.8832,4-Dichlorophenol 1 09/07/21 17:21 V8596JMV
<0.240 mg/Kg - dry 0.240 0.883Diethyl phthalate 1 09/07/21 17:21 V8596JMV
<0.232 mg/Kg - dry 0.232 0.883Dimethyl phthalate 1 09/07/21 17:21 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S-9(7-8)
94722 Matrix:
8/30/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.144 mg/Kg - dry 0.144 0.4412,4-Dimethylphenol 1 09/07/21 17:21 V8596JMV
<0.143 mg/Kg - dry 0.143 0.883Di-n-butyl phthalate 1 09/07/21 17:21 V8596JMV
<0.321 mg/Kg - dry 0.321 2.014,6-Dinitro-2-methylphenol 1 09/07/21 17:21 V8596JMV
<0.696 mg/Kg - dry 0.696 2.012,4-Dinitrophenol 1 09/07/21 17:21 V8596JMV
<0.129 mg/Kg - dry 0.129 0.8832,4-Dinitrotoluene 1 09/07/21 17:21 V8596JMV
<0.144 mg/Kg - dry 0.144 0.8832,6-Dinitrotoluene 1 09/07/21 17:21 V8596JMV
<0.191 mg/Kg - dry 0.191 0.441Di-n-Octyl Phthalate 1 09/07/21 17:21 V8596JMV
<0.164 mg/Kg - dry 0.164 0.883Fluoranthene 1 09/07/21 17:21 V8596JMV
<0.171 mg/Kg - dry 0.171 0.883
Fluorene 1 09/07/21 17:21 V8596JMV
<0.141 mg/Kg - dry 0.141 0.883Hexachlorobenzene 1 09/07/21 17:21 V8596JMV
<0.130 mg/Kg - dry 0.130 0.883Hexachlorobutadiene 1 09/07/21 17:21 V8596JMV
<0.210 mg/Kg - dry 0.210 0.883Hexachlorocyclopentadiene 1 09/07/21 17:21 V8596JMV
<0.106 mg/Kg - dry 0.106 0.883Hexachloroethane 1 09/07/21 17:21 V8596JMV
<0.239 mg/Kg - dry 0.239 0.883Indeno(1,2,3-cd)pyrene 1 09/07/21 17:21 V8596JMV
<0.255 mg/Kg - dry 0.255 0.883Isophorone 1 09/07/21 17:21 V8596JMV
0.224 J
mg/Kg - dry 0.141 0.883
1-Methylnaphthalene 1 09/07/21 17:21 V8596JMV
<0.133 mg/Kg - dry 0.133 0.8832-Methylnaphthalene 1 09/07/21 17:21 V8596JMV
<0.129 mg/Kg - dry 0.129 0.8832-Methylphenol 1 09/07/21 17:21 V8596JMV
<0.113 mg/Kg - dry 0.113 0.8833&4 Methylphenol 1 09/07/21 17:21 V8596JMV
<0.192 mg/Kg - dry 0.192 0.883Naphthalene 1 09/07/21 17:21 V8596JMV
<0.129 mg/Kg - dry 0.129 0.8832-Nitroaniline 1 09/07/21 17:21 V8596JMV
<0.160 mg/Kg - dry 0.160 0.8833-Nitroaniline 1 09/07/21 17:21 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S-9(7-8)
94722 Matrix:
8/30/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.124 mg/Kg - dry 0.124 0.4414-Nitroaniline 1 09/07/21 17:21 V8596JMV
<0.155 mg/Kg - dry 0.155 0.441Nitrobenzene 1 09/07/21 17:21 V8596JMV
<0.118 mg/Kg - dry 0.118 0.8832-Nitrophenol 1 09/07/21 17:21 V8596JMV
<0.156 mg/Kg - dry 0.156 0.8834-Nitrophenol 1 09/07/21 17:21 V8596JMV
<0.352 mg/Kg - dry 0.352 0.883N-Nitrosodimethylamine 1 09/07/21 17:21 V8596JMV
<0.242 mg/Kg - dry 0.242 0.883N-Nitrosodiphenylamine 1 09/07/21 17:21 V8596JMV
<0.157 mg/Kg - dry 0.157 0.883N-Nitroso-di-n-propylamine 1 09/07/21 17:21 V8596JMV
<0.464 mg/Kg - dry 0.464 1.34Pentachlorophenol 1 09/07/21 17:21 V8596JMV
<0.278 mg/Kg - dry 0.278 0.883
Phenanthrene 1 09/07/21 17:21 V8596JMV
<0.149 mg/Kg - dry 0.149 0.883Phenol 1 09/07/21 17:21 V8596JMV
<0.179 mg/Kg - dry 0.179 0.883Pyrene 1 09/07/21 17:21 V8596JMV
<0.106 mg/Kg - dry 0.106 0.441Pyridine 1 09/07/21 17:21 V8596JMV
<0.143 mg/Kg - dry 0.143 0.8831,2,4-Trichlorobenzene 1 09/07/21 17:21 V8596JMV
<0.128 mg/Kg - dry 0.128 0.8832,4,5-Trichlorophenol 1 09/07/21 17:21 V8596JMV
<0.129 mg/Kg - dry 0.129 0.8832,4,6-Trichlorophenol 1 09/07/21 17:21 V8596JMV
Surrogate: Phenol-d5 102 Limits: 34-121%09/07/21 17:211 JMV V8596
Surrogate: 2-Fluorobiphenyl 74.9 Limits: 44-115%09/07/21 17:211 JMV V8596
Surrogate: 2-Fluorophenol 90.7 Limits: 35-115%09/07/21 17:211 JMV V8596
Surrogate: Nitrobenzene-d5 8.50 *Limits: 37-122%09/07/21 17:211 JMV V8596
Surrogate: 4-Terphenyl-d14 81.4 Limits: 54-127%09/07/21 17:211 JMV V8596
Surrogate: 2,4,6-Tribromophenol 83.5 Limits: 39-132%09/07/21 17:211 JMV V8596
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S7(10-11)
94723 Matrix:
8/31/2021 10:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.9 %Moisture 1 09/08/21 17:27 SW-DRYWTBAM
2.80 mg/Kg - dry 0.114 1.22Arsenic 10 09/07/21 23:02 6020BEDV
39.0 mg/Kg - dry 1.71 12.2Barium 10 09/07/21 23:02 6020BEDV
<0.0669 mg/Kg - dry 0.0669 0.609Cadmium 10 09/07/21 23:02 6020BEDV
74.9 mg/Kg - dry 0.353 1.22Chromium 10 09/07/21 23:02 6020BEDV
17.4 mg/Kg - dry 0.171 1.22
Lead 10 09/07/21 23:02 6020BEDV
0.0921 mg/Kg - dry 0.0146 0.0365Mercury (Total)1 09/08/21 14:28 7471BEDV
<1.10 mg/Kg - dry 1.10 2.44Selenium 10 09/08/21 22:59 6020BEDV
<0.0499 mg/Kg - dry 0.0499 0.609Silver 10 09/07/21 23:02 6020BEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 58 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S7(10-11)
94723 Matrix:
8/31/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
0.024 mg/Kg - dry 0.002 0.024Acetone 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 09/03/21 14:14 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 09/03/21 14:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/03/21 14:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/03/21 14:14 V8431TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/03/21 14:14 V8431TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/03/21 14:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/03/21 14:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/03/21 14:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/03/21 14:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 09/03/21 14:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/03/21 14:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/03/21 14:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/03/21 14:14 V8431TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/03/21 14:14 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/03/21 14:14 V8431TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S7(10-11)
94723 Matrix:
8/31/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 09/03/21 14:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 09/03/21 14:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/03/21 14:14 V8431TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/03/21 14:14 V8431TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/03/21 14:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/03/21 14:14 V8431TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/03/21 14:14 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/03/21 14:14 V8431TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/03/21 14:14 V8431TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 09/03/21 14:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/03/21 14:14 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 09/03/21 14:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/03/21 14:14 V8431TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 09/03/21 14:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 09/03/21 14:14 V8431TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 09/03/21 14:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/03/21 14:14 V8431TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S7(10-11)
94723 Matrix:
8/31/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 09/03/21 14:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/03/21 14:14 V8431TBL
0.002 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 09/03/21 14:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/03/21 14:14 V8431TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 09/03/21 14:14 V8431TBL
0.009 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 09/03/21 14:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/03/21 14:14 V8431TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/03/21 14:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/03/21 14:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/03/21 14:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/03/21 14:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/03/21 14:14 V8431TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/03/21 14:14 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/03/21 14:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/03/21 14:14 V8431TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S7(10-11)
94723 Matrix:
8/31/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/03/21 14:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/03/21 14:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/03/21 14:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/03/21 14:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/03/21 14:14 V8431
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%09/03/21 14:141 TBL V8431
Surrogate: Dibromofluoromethane 105 Limits: 84-123%09/03/21 14:141 TBL V8431
Surrogate: Toluene-d8 108 Limits: 76-129%09/03/21 14:141 TBL V8431
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.141 mg/Kg - dry 0.141 0.803Acenaphthene 1 09/07/21 18:05 V8596JMV
<0.127 mg/Kg - dry 0.127 0.803Acenaphthylene 1 09/07/21 18:05 V8596JMV
<0.185 mg/Kg - dry 0.185 0.803Aniline 1 09/07/21 18:05 V8596JMV
<0.174 mg/Kg - dry 0.174 0.803Anthracene 1 09/07/21 18:05 V8596JMV
<0.169 mg/Kg - dry 0.169 0.803Benzo(a)anthracene 1 09/07/21 18:05 V8596JMV
<0.179 mg/Kg - dry 0.179 0.803Benzo(a)pyrene 1 09/07/21 18:05 V8596JMV
<0.177 mg/Kg - dry 0.177 0.803
Benzo(b)fluoranthene 1 09/07/21 18:05 V8596JMV
<0.165 mg/Kg - dry 0.165 0.803Benzo(g,h,i)perylene 1 09/07/21 18:05 V8596JMV
<0.166 mg/Kg - dry 0.166 0.803Benzo(k)fluoranthene 1 09/07/21 18:05 V8596JMV
<0.706 mg/Kg - dry 0.706 2.44Benzoic Acid 1 09/07/21 18:05 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S7(10-11)
94723 Matrix:
8/31/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.127 mg/Kg - dry 0.127 0.803Benzyl alcohol 1 09/07/21 18:05 V8596JMV
<0.143 mg/Kg - dry 0.143 0.803Bis(2-Chloroethoxy)methane 1 09/07/21 18:05 V8596JMV
<0.130 mg/Kg - dry 0.130 0.803Bis(2-Chloroethyl)ether 1 09/07/21 18:05 V8596JMV
<0.165 mg/Kg - dry 0.165 0.401Bis(2-Chloroisopropyl)ether 1 09/07/21 18:05 V8596JMV
<0.146 mg/Kg - dry 0.146 0.803Bis(2-ethylhexyl)phthalate 1 09/07/21 18:05 V8596JMV
<0.132 mg/Kg - dry 0.132 0.8034-Bromophenyl phenyl ether 1 09/07/21 18:05 V8596JMV
<0.137 mg/Kg - dry 0.137 0.401Butyl benzyl phthalate 1 09/07/21 18:05 V8596JMV
<0.112 mg/Kg - dry 0.112 0.8034-Chloro-3-methylphenol 1 09/07/21 18:05 V8596JMV
<0.136 mg/Kg - dry 0.136 0.401
4-Chloroaniline 1 09/07/21 18:05 V8596JMV
<0.141 mg/Kg - dry 0.141 0.8032-Chloronaphthalene 1 09/07/21 18:05 V8596JMV
<0.119 mg/Kg - dry 0.119 0.8032-Chlorophenol 1 09/07/21 18:05 V8596JMV
<0.153 mg/Kg - dry 0.153 1.224-Chlorophenyl phenyl ether 1 09/07/21 18:05 V8596JMV
<0.172 mg/Kg - dry 0.172 0.803Chrysene 1 09/07/21 18:05 V8596JMV
<0.280 mg/Kg - dry 0.280 0.803Dibenz(a,h)anthracene 1 09/07/21 18:05 V8596JMV
<0.144 mg/Kg - dry 0.144 0.803Dibenzofuran 1 09/07/21 18:05 V8596JMV
<0.114 mg/Kg - dry 0.114 0.803
1,2-Dichlorobenzene 1 09/07/21 18:05 V8596JMV
<0.118 mg/Kg - dry 0.118 0.8031,3-Dichlorobenzene 1 09/07/21 18:05 V8596JMV
<0.118 mg/Kg - dry 0.118 0.4011,4-Dichlorobenzene 1 09/07/21 18:05 V8596JMV
<0.179 mg/Kg - dry 0.179 0.8033,3'-Dichlorobenzidine 1 09/07/21 18:05 V8596JMV
<0.116 mg/Kg - dry 0.116 0.8032,4-Dichlorophenol 1 09/07/21 18:05 V8596JMV
<0.219 mg/Kg - dry 0.219 0.803Diethyl phthalate 1 09/07/21 18:05 V8596JMV
<0.211 mg/Kg - dry 0.211 0.803Dimethyl phthalate 1 09/07/21 18:05 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S7(10-11)
94723 Matrix:
8/31/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.131 mg/Kg - dry 0.131 0.4012,4-Dimethylphenol 1 09/07/21 18:05 V8596JMV
<0.130 mg/Kg - dry 0.130 0.803Di-n-butyl phthalate 1 09/07/21 18:05 V8596JMV
<0.292 mg/Kg - dry 0.292 1.834,6-Dinitro-2-methylphenol 1 09/07/21 18:05 V8596JMV
<0.633 mg/Kg - dry 0.633 1.832,4-Dinitrophenol 1 09/07/21 18:05 V8596JMV
<0.117 mg/Kg - dry 0.117 0.8032,4-Dinitrotoluene 1 09/07/21 18:05 V8596JMV
<0.131 mg/Kg - dry 0.131 0.8032,6-Dinitrotoluene 1 09/07/21 18:05 V8596JMV
<0.174 mg/Kg - dry 0.174 0.401Di-n-Octyl Phthalate 1 09/07/21 18:05 V8596JMV
<0.149 mg/Kg - dry 0.149 0.803Fluoranthene 1 09/07/21 18:05 V8596JMV
<0.155 mg/Kg - dry 0.155 0.803
Fluorene 1 09/07/21 18:05 V8596JMV
<0.129 mg/Kg - dry 0.129 0.803Hexachlorobenzene 1 09/07/21 18:05 V8596JMV
<0.118 mg/Kg - dry 0.118 0.803Hexachlorobutadiene 1 09/07/21 18:05 V8596JMV
<0.191 mg/Kg - dry 0.191 0.803Hexachlorocyclopentadiene 1 09/07/21 18:05 V8596JMV
<0.096 mg/Kg - dry 0.096 0.803Hexachloroethane 1 09/07/21 18:05 V8596JMV
<0.218 mg/Kg - dry 0.218 0.803Indeno(1,2,3-cd)pyrene 1 09/07/21 18:05 V8596JMV
<0.232 mg/Kg - dry 0.232 0.803Isophorone 1 09/07/21 18:05 V8596JMV
<0.129 mg/Kg - dry 0.129 0.803
1-Methylnaphthalene 1 09/07/21 18:05 V8596JMV
<0.121 mg/Kg - dry 0.121 0.8032-Methylnaphthalene 1 09/07/21 18:05 V8596JMV
<0.118 mg/Kg - dry 0.118 0.8032-Methylphenol 1 09/07/21 18:05 V8596JMV
<0.103 mg/Kg - dry 0.103 0.8033&4 Methylphenol 1 09/07/21 18:05 V8596JMV
<0.175 mg/Kg - dry 0.175 0.803Naphthalene 1 09/07/21 18:05 V8596JMV
<0.117 mg/Kg - dry 0.117 0.8032-Nitroaniline 1 09/07/21 18:05 V8596JMV
<0.146 mg/Kg - dry 0.146 0.8033-Nitroaniline 1 09/07/21 18:05 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S7(10-11)
94723 Matrix:
8/31/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.113 mg/Kg - dry 0.113 0.4014-Nitroaniline 1 09/07/21 18:05 V8596JMV
<0.141 mg/Kg - dry 0.141 0.401Nitrobenzene 1 09/07/21 18:05 V8596JMV
<0.108 mg/Kg - dry 0.108 0.8032-Nitrophenol 1 09/07/21 18:05 V8596JMV
<0.142 mg/Kg - dry 0.142 0.8034-Nitrophenol 1 09/07/21 18:05 V8596JMV
<0.320 mg/Kg - dry 0.320 0.803N-Nitrosodimethylamine 1 09/07/21 18:05 V8596JMV
<0.220 mg/Kg - dry 0.220 0.803N-Nitrosodiphenylamine 1 09/07/21 18:05 V8596JMV
<0.143 mg/Kg - dry 0.143 0.803N-Nitroso-di-n-propylamine 1 09/07/21 18:05 V8596JMV
<0.422 mg/Kg - dry 0.422 1.22Pentachlorophenol 1 09/07/21 18:05 V8596JMV
<0.253 mg/Kg - dry 0.253 0.803
Phenanthrene 1 09/07/21 18:05 V8596JMV
<0.136 mg/Kg - dry 0.136 0.803Phenol 1 09/07/21 18:05 V8596JMV
<0.163 mg/Kg - dry 0.163 0.803Pyrene 1 09/07/21 18:05 V8596JMV
<0.096 mg/Kg - dry 0.096 0.401Pyridine 1 09/07/21 18:05 V8596JMV
<0.130 mg/Kg - dry 0.130 0.8031,2,4-Trichlorobenzene 1 09/07/21 18:05 V8596JMV
<0.117 mg/Kg - dry 0.117 0.8032,4,5-Trichlorophenol 1 09/07/21 18:05 V8596JMV
<0.117 mg/Kg - dry 0.117 0.8032,4,6-Trichlorophenol 1 09/07/21 18:05 V8596JMV
Surrogate: Phenol-d5 67.6 Limits: 34-121%09/07/21 18:051 JMV V8596
Surrogate: 2-Fluorobiphenyl 75.4 Limits: 44-115%09/07/21 18:051 JMV V8596
Surrogate: 2-Fluorophenol 66.7 Limits: 35-115%09/07/21 18:051 JMV V8596
Surrogate: Nitrobenzene-d5 67.7 Limits: 37-122%09/07/21 18:051 JMV V8596
Surrogate: 4-Terphenyl-d14 88.0 Limits: 54-127%09/07/21 18:051 JMV V8596
Surrogate: 2,4,6-Tribromophenol 78.1 Limits: 39-132%09/07/21 18:051 JMV V8596
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S6(14-15)
94724 Matrix:
8/31/2021 12:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.8 %Moisture 1 09/08/21 17:27 SW-DRYWTBAM
0.763 J mg/Kg - dry 0.119 1.26Arsenic 10 09/07/21 23:09 6020BEDV
133 mg/Kg - dry 1.77 12.6Barium 10 09/07/21 23:09 6020BEDV
<0.0694 mg/Kg - dry 0.0694 0.631Cadmium 10 09/07/21 23:09 6020BEDV
76.6 mg/Kg - dry 0.366 1.26Chromium 10 09/07/21 23:09 6020BEDV
2.64 mg/Kg - dry 0.177 1.26
Lead 10 09/07/21 23:09 6020BEDV
<0.0152 mg/Kg - dry 0.0152 0.0379Mercury (Total)1 09/08/21 14:30 7471BEDV
2.01 J mg/Kg - dry 1.14 2.53Selenium 10 09/08/21 23:05 6020BEDV
<0.0517 mg/Kg - dry 0.0517 0.631Silver 10 09/07/21 23:09 6020BEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 66 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S6(14-15)
94724 Matrix:
8/31/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
0.006 J mg/Kg - dry 0.003 0.025Acetone 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 09/03/21 13:14 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 09/03/21 13:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/03/21 13:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/03/21 13:14 V8431TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/03/21 13:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/03/21 13:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/03/21 13:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/03/21 13:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 09/03/21 13:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/03/21 13:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/03/21 13:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/03/21 13:14 V8431TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/03/21 13:14 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/03/21 13:14 V8431TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 67 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S6(14-15)
94724 Matrix:
8/31/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/03/21 13:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 09/03/21 13:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/03/21 13:14 V8431TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/03/21 13:14 V8431TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/03/21 13:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/03/21 13:14 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/03/21 13:14 V8431TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/03/21 13:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/03/21 13:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/03/21 13:14 V8431TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 09/03/21 13:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/03/21 13:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 09/03/21 13:14 V8431TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 09/03/21 13:14 V8431TBL
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 09/03/21 13:14 V8431TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 68 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S6(14-15)
94724 Matrix:
8/31/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/03/21 13:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/03/21 13:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/03/21 13:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/03/21 13:14 V8431TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 09/03/21 13:14 V8431TBL
0.010 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 09/03/21 13:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/03/21 13:14 V8431TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/03/21 13:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/03/21 13:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/03/21 13:14 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/03/21 13:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/03/21 13:14 V8431TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/03/21 13:14 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/03/21 13:14 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/03/21 13:14 V8431TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 69 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S6(14-15)
94724 Matrix:
8/31/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/03/21 13:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/03/21 13:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/03/21 13:14 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/03/21 13:14 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/03/21 13:14 V8431
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%09/03/21 13:141 TBL V8431
Surrogate: Dibromofluoromethane 105 Limits: 84-123%09/03/21 13:141 TBL V8431
Surrogate: Toluene-d8 108 Limits: 76-129%09/03/21 13:141 TBL V8431
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.146 mg/Kg - dry 0.146 0.833Acenaphthene 1 09/07/21 18:28 V8596JMV
<0.132 mg/Kg - dry 0.132 0.833Acenaphthylene 1 09/07/21 18:28 V8596JMV
<0.191 mg/Kg - dry 0.191 0.833Aniline 1 09/07/21 18:28 V8596JMV
<0.180 mg/Kg - dry 0.180 0.833Anthracene 1 09/07/21 18:28 V8596JMV
<0.175 mg/Kg - dry 0.175 0.833Benzo(a)anthracene 1 09/07/21 18:28 V8596JMV
<0.185 mg/Kg - dry 0.185 0.833Benzo(a)pyrene 1 09/07/21 18:28 V8596JMV
<0.184 mg/Kg - dry 0.184 0.833
Benzo(b)fluoranthene 1 09/07/21 18:28 V8596JMV
<0.171 mg/Kg - dry 0.171 0.833Benzo(g,h,i)perylene 1 09/07/21 18:28 V8596JMV
<0.172 mg/Kg - dry 0.172 0.833Benzo(k)fluoranthene 1 09/07/21 18:28 V8596JMV
<0.732 mg/Kg - dry 0.732 2.53Benzoic Acid 1 09/07/21 18:28 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 70 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S6(14-15)
94724 Matrix:
8/31/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.132 mg/Kg - dry 0.132 0.833Benzyl alcohol 1 09/07/21 18:28 V8596JMV
<0.148 mg/Kg - dry 0.148 0.833Bis(2-Chloroethoxy)methane 1 09/07/21 18:28 V8596JMV
<0.135 mg/Kg - dry 0.135 0.833Bis(2-Chloroethyl)ether 1 09/07/21 18:28 V8596JMV
<0.171 mg/Kg - dry 0.171 0.416Bis(2-Chloroisopropyl)ether 1 09/07/21 18:28 V8596JMV
<0.151 mg/Kg - dry 0.151 0.833Bis(2-ethylhexyl)phthalate 1 09/07/21 18:28 V8596JMV
<0.137 mg/Kg - dry 0.137 0.8334-Bromophenyl phenyl ether 1 09/07/21 18:28 V8596JMV
<0.142 mg/Kg - dry 0.142 0.416Butyl benzyl phthalate 1 09/07/21 18:28 V8596JMV
<0.116 mg/Kg - dry 0.116 0.8334-Chloro-3-methylphenol 1 09/07/21 18:28 V8596JMV
<0.141 mg/Kg - dry 0.141 0.416
4-Chloroaniline 1 09/07/21 18:28 V8596JMV
<0.146 mg/Kg - dry 0.146 0.8332-Chloronaphthalene 1 09/07/21 18:28 V8596JMV
<0.123 mg/Kg - dry 0.123 0.8332-Chlorophenol 1 09/07/21 18:28 V8596JMV
<0.159 mg/Kg - dry 0.159 1.264-Chlorophenyl phenyl ether 1 09/07/21 18:28 V8596JMV
<0.179 mg/Kg - dry 0.179 0.833Chrysene 1 09/07/21 18:28 V8596JMV
<0.290 mg/Kg - dry 0.290 0.833Dibenz(a,h)anthracene 1 09/07/21 18:28 V8596JMV
<0.150 mg/Kg - dry 0.150 0.833Dibenzofuran 1 09/07/21 18:28 V8596JMV
<0.119 mg/Kg - dry 0.119 0.833
1,2-Dichlorobenzene 1 09/07/21 18:28 V8596JMV
<0.122 mg/Kg - dry 0.122 0.8331,3-Dichlorobenzene 1 09/07/21 18:28 V8596JMV
<0.123 mg/Kg - dry 0.123 0.4161,4-Dichlorobenzene 1 09/07/21 18:28 V8596JMV
<0.185 mg/Kg - dry 0.185 0.8333,3'-Dichlorobenzidine 1 09/07/21 18:28 V8596JMV
<0.120 mg/Kg - dry 0.120 0.8332,4-Dichlorophenol 1 09/07/21 18:28 V8596JMV
<0.227 mg/Kg - dry 0.227 0.833Diethyl phthalate 1 09/07/21 18:28 V8596JMV
<0.219 mg/Kg - dry 0.219 0.833Dimethyl phthalate 1 09/07/21 18:28 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 71 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S6(14-15)
94724 Matrix:
8/31/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.136 mg/Kg - dry 0.136 0.4162,4-Dimethylphenol 1 09/07/21 18:28 V8596JMV
<0.135 mg/Kg - dry 0.135 0.833Di-n-butyl phthalate 1 09/07/21 18:28 V8596JMV
<0.303 mg/Kg - dry 0.303 1.894,6-Dinitro-2-methylphenol 1 09/07/21 18:28 V8596JMV
<0.656 mg/Kg - dry 0.656 1.892,4-Dinitrophenol 1 09/07/21 18:28 V8596JMV
<0.121 mg/Kg - dry 0.121 0.8332,4-Dinitrotoluene 1 09/07/21 18:28 V8596JMV
<0.136 mg/Kg - dry 0.136 0.8332,6-Dinitrotoluene 1 09/07/21 18:28 V8596JMV
<0.180 mg/Kg - dry 0.180 0.416Di-n-Octyl Phthalate 1 09/07/21 18:28 V8596JMV
<0.155 mg/Kg - dry 0.155 0.833Fluoranthene 1 09/07/21 18:28 V8596JMV
<0.161 mg/Kg - dry 0.161 0.833
Fluorene 1 09/07/21 18:28 V8596JMV
<0.133 mg/Kg - dry 0.133 0.833Hexachlorobenzene 1 09/07/21 18:28 V8596JMV
<0.123 mg/Kg - dry 0.123 0.833Hexachlorobutadiene 1 09/07/21 18:28 V8596JMV
<0.198 mg/Kg - dry 0.198 0.833Hexachlorocyclopentadiene 1 09/07/21 18:28 V8596JMV
<0.100 mg/Kg - dry 0.100 0.833Hexachloroethane 1 09/07/21 18:28 V8596JMV
<0.226 mg/Kg - dry 0.226 0.833Indeno(1,2,3-cd)pyrene 1 09/07/21 18:28 V8596JMV
<0.241 mg/Kg - dry 0.241 0.833Isophorone 1 09/07/21 18:28 V8596JMV
<0.133 mg/Kg - dry 0.133 0.833
1-Methylnaphthalene 1 09/07/21 18:28 V8596JMV
<0.126 mg/Kg - dry 0.126 0.8332-Methylnaphthalene 1 09/07/21 18:28 V8596JMV
<0.122 mg/Kg - dry 0.122 0.8332-Methylphenol 1 09/07/21 18:28 V8596JMV
<0.107 mg/Kg - dry 0.107 0.8333&4 Methylphenol 1 09/07/21 18:28 V8596JMV
<0.181 mg/Kg - dry 0.181 0.833Naphthalene 1 09/07/21 18:28 V8596JMV
<0.122 mg/Kg - dry 0.122 0.8332-Nitroaniline 1 09/07/21 18:28 V8596JMV
<0.151 mg/Kg - dry 0.151 0.8333-Nitroaniline 1 09/07/21 18:28 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 72 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S6(14-15)
94724 Matrix:
8/31/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.117 mg/Kg - dry 0.117 0.4164-Nitroaniline 1 09/07/21 18:28 V8596JMV
<0.146 mg/Kg - dry 0.146 0.416Nitrobenzene 1 09/07/21 18:28 V8596JMV
<0.112 mg/Kg - dry 0.112 0.8332-Nitrophenol 1 09/07/21 18:28 V8596JMV
<0.147 mg/Kg - dry 0.147 0.8334-Nitrophenol 1 09/07/21 18:28 V8596JMV
<0.332 mg/Kg - dry 0.332 0.833N-Nitrosodimethylamine 1 09/07/21 18:28 V8596JMV
<0.228 mg/Kg - dry 0.228 0.833N-Nitrosodiphenylamine 1 09/07/21 18:28 V8596JMV
<0.148 mg/Kg - dry 0.148 0.833N-Nitroso-di-n-propylamine 1 09/07/21 18:28 V8596JMV
<0.438 mg/Kg - dry 0.438 1.26Pentachlorophenol 1 09/07/21 18:28 V8596JMV
<0.262 mg/Kg - dry 0.262 0.833
Phenanthrene 1 09/07/21 18:28 V8596JMV
<0.141 mg/Kg - dry 0.141 0.833Phenol 1 09/07/21 18:28 V8596JMV
<0.169 mg/Kg - dry 0.169 0.833Pyrene 1 09/07/21 18:28 V8596JMV
<0.100 mg/Kg - dry 0.100 0.416Pyridine 1 09/07/21 18:28 V8596JMV
<0.135 mg/Kg - dry 0.135 0.8331,2,4-Trichlorobenzene 1 09/07/21 18:28 V8596JMV
<0.121 mg/Kg - dry 0.121 0.8332,4,5-Trichlorophenol 1 09/07/21 18:28 V8596JMV
<0.121 mg/Kg - dry 0.121 0.8332,4,6-Trichlorophenol 1 09/07/21 18:28 V8596JMV
Surrogate: Phenol-d5 77.5 Limits: 34-121%09/07/21 18:281 JMV V8596
Surrogate: 2-Fluorobiphenyl 76.6 Limits: 44-115%09/07/21 18:281 JMV V8596
Surrogate: 2-Fluorophenol 79.6 Limits: 35-115%09/07/21 18:281 JMV V8596
Surrogate: Nitrobenzene-d5 71.3 Limits: 37-122%09/07/21 18:281 JMV V8596
Surrogate: 4-Terphenyl-d14 86.8 Limits: 54-127%09/07/21 18:281 JMV V8596
Surrogate: 2,4,6-Tribromophenol 85.3 Limits: 39-132%09/07/21 18:281 JMV V8596
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 73 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S8(11-12)
94725 Matrix:
8/31/2021 9:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
24.2 %Moisture 1 09/08/21 17:27 SW-DRYWTBAM
2.65 mg/Kg - dry 0.124 1.32Arsenic 10 09/07/21 23:15 6020BEDV
63.2 mg/Kg - dry 1.85 13.2Barium 10 09/07/21 23:15 6020BEDV
<0.0725 mg/Kg - dry 0.0725 0.660Cadmium 10 09/07/21 23:15 6020BEDV
47.2 mg/Kg - dry 0.382 1.32Chromium 10 09/07/21 23:15 6020BEDV
17.3 mg/Kg - dry 0.185 1.32
Lead 10 09/07/21 23:15 6020BEDV
0.0553 mg/Kg - dry 0.0158 0.0396Mercury (Total)1 09/08/21 14:39 7471BEDV
1.24 J mg/Kg - dry 1.19 2.64Selenium 10 09/08/21 23:12 6020BEDV
<0.0540 mg/Kg - dry 0.0540 0.660Silver 10 09/07/21 23:15 6020BEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 74 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S8(11-12)
94725 Matrix:
8/31/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V8447 09/07/21 08:00
<0.079 mg/Kg - dry 0.079 0.659Acetone 50 09/07/21 13:06 V8448TBL
<0.039 mg/Kg - dry 0.039 0.659Acrolein 50 09/07/21 13:06 V8448TBL
<0.024 mg/Kg - dry 0.024 0.659Acrylonitrile 50 09/07/21 13:06 V8448TBL
<0.019 mg/Kg - dry 0.019 0.164Benzene 50 09/07/21 13:06 V8448TBL
<0.016 mg/Kg - dry 0.016 0.164Bromobenzene 50 09/07/21 13:06 V8448TBL
<0.026 mg/Kg - dry 0.026 0.164Bromochloromethane 50 09/07/21 13:06 V8448TBL
<0.039 mg/Kg - dry 0.039 0.164Bromodichloromethane 50 09/07/21 13:06 V8448TBL
<0.033 mg/Kg - dry 0.033 0.164Bromoform 50 09/07/21 13:06 V8448TBL
<0.060 mg/Kg - dry 0.060 0.329
Bromomethane 50 09/07/21 13:06 V8448TBL
1.45 mg/Kg - dry 0.016 0.164n-Butylbenzene 50 09/07/21 13:06 V8448TBL
0.656 mg/Kg - dry 0.018 0.164sec-Butyl benzene 50 09/07/21 13:06 V8448TBL
0.113 J mg/Kg - dry 0.016 0.164tert-Butyl benzene 50 09/07/21 13:06 V8448TBL
<0.021 mg/Kg - dry 0.021 0.164Carbon Disulfide 50 09/07/21 13:06 V8448TBL
<0.052 mg/Kg - dry 0.052 0.164Carbon Tetrachloride 50 09/07/21 13:06 V8448TBL
<0.022 mg/Kg - dry 0.022 0.164Chlorobenzene 50 09/07/21 13:06 V8448TBL
<0.029 mg/Kg - dry 0.029 0.164
Chlorodibromomethane 50 09/07/21 13:06 V8448TBL
<0.029 mg/Kg - dry 0.029 0.329Chloroethane 50 09/07/21 13:06 V8448TBL
<0.034 mg/Kg - dry 0.034 0.164Chloroform 50 09/07/21 13:06 V8448TBL
<0.020 mg/Kg - dry 0.020 0.329Chloromethane 50 09/07/21 13:06 V8448TBL
<0.016 mg/Kg - dry 0.016 0.1642-Chlorotoluene 50 09/07/21 13:06 V8448TBL
<0.012 mg/Kg - dry 0.012 0.1644-Chlorotoluene 50 09/07/21 13:06 V8448TBL
<0.024 mg/Kg - dry 0.024 0.164Di-Isopropyl Ether (DIPE)50 09/07/21 13:06 V8448TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 75 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S8(11-12)
94725 Matrix:
8/31/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V8447 09/07/21 08:00
<0.014 mg/Kg - dry 0.014 0.3291,2-Dibromo-3-Chloropropane 50 09/07/21 13:06 V8448TBL
<0.019 mg/Kg - dry 0.019 0.1641,2-Dibromoethane 50 09/07/21 13:06 V8448TBL
<0.032 mg/Kg - dry 0.032 0.164Dibromomethane 50 09/07/21 13:06 V8448TBL
<0.010 mg/Kg - dry 0.010 0.1641,2-Dichlorobenzene 50 09/07/21 13:06 V8448TBL
<0.012 mg/Kg - dry 0.012 0.1641,3-Dichlorobenzene 50 09/07/21 13:06 V8448TBL
<0.019 mg/Kg - dry 0.019 0.1641,4-Dichlorobenzene 50 09/07/21 13:06 V8448TBL
<0.043 mg/Kg - dry 0.043 0.329Dichlorodifluoromethane 50 09/07/21 13:06 V8448TBL
<0.027 mg/Kg - dry 0.027 0.1641,1-Dichloroethane 50 09/07/21 13:06 V8448TBL
<0.045 mg/Kg - dry 0.045 0.164
1,2-Dichloroethane 50 09/07/21 13:06 V8448TBL
<0.024 mg/Kg - dry 0.024 0.1641,1-Dichloroethene 50 09/07/21 13:06 V8448TBL
<0.026 mg/Kg - dry 0.026 0.164cis-1,2-Dichloroethene 50 09/07/21 13:06 V8448TBL
<0.034 mg/Kg - dry 0.034 0.164trans-1,2-Dichloroethene 50 09/07/21 13:06 V8448TBL
<0.014 mg/Kg - dry 0.014 0.1641,2-Dichloropropane 50 09/07/21 13:06 V8448TBL
<0.018 mg/Kg - dry 0.018 0.1641,3-Dichloropropane 50 09/07/21 13:06 V8448TBL
<0.041 mg/Kg - dry 0.041 0.1642,2-Dichloropropane 50 09/07/21 13:06 V8448TBL
<0.025 mg/Kg - dry 0.025 0.164
1,1-Dichloropropene 50 09/07/21 13:06 V8448TBL
<0.017 mg/Kg - dry 0.017 0.164cis-1,3-Dichloropropene 50 09/07/21 13:06 V8448TBL
<0.026 mg/Kg - dry 0.026 0.164trans-1,3-Dichloropropene 50 09/07/21 13:06 V8448TBL
0.488 mg/Kg - dry 0.019 0.164Ethylbenzene 50 09/07/21 13:06 V8448TBL
<0.027 mg/Kg - dry 0.027 3.30Ethyl Tertiary Butyl Ether (ETBE)50 09/07/21 13:06 V8448TBL
<0.026 mg/Kg - dry 0.026 0.329Hexachlorobutadiene 50 09/07/21 13:06 V8448TBL
<0.021 mg/Kg - dry 0.021 0.329n-Hexane 50 09/07/21 13:06 V8448TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 76 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S8(11-12)
94725 Matrix:
8/31/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V8447 09/07/21 08:00
<0.020 mg/Kg - dry 0.020 0.6592-Hexanone 50 09/07/21 13:06 V8448TBL
0.370 mg/Kg - dry 0.015 0.164Isopropylbenzene 50 09/07/21 13:06 V8448TBL
<0.042 mg/Kg - dry 0.042 0.1644-Isopropyl toluene 50 09/07/21 13:06 V8448TBL
<0.021 mg/Kg - dry 0.021 0.659Methyl Ethyl Ketone (MEK)50 09/07/21 13:06 V8448TBL
<0.020 mg/Kg - dry 0.020 0.164Methyl tert-butyl ether (MTBE)50 09/07/21 13:06 V8448TBL
<0.494 mg/Kg - dry 0.494 0.6594-Methyl-2-Pentanone 50 09/07/21 13:06 V8448TBL
<0.048 mg/Kg - dry 0.048 0.164Methylene Chloride 50 09/07/21 13:06 V8448TBL
11.2 mg/Kg - dry 0.032 0.329Naphthalene 50 09/07/21 13:06 V8448TBL
0.889 mg/Kg - dry 0.017 0.164
n-Propylbenzene 50 09/07/21 13:06 V8448TBL
<0.046 mg/Kg - dry 0.046 0.164Styrene 50 09/07/21 13:06 V8448TBL
<0.034 mg/Kg - dry 0.034 0.1641,1,1,2-Tetrachloroethane 50 09/07/21 13:06 V8448TBL
<0.010 mg/Kg - dry 0.010 0.1641,1,2,2-Tetrachloroethane 50 09/07/21 13:06 V8448TBL
<0.029 mg/Kg - dry 0.029 0.164Tetrachloroethene 50 09/07/21 13:06 V8448TBL
<0.021 mg/Kg - dry 0.021 0.164Toluene 50 09/07/21 13:06 V8448TBL
<0.017 mg/Kg - dry 0.017 0.3291,2,3-Trichlorobenzene 50 09/07/21 13:06 V8448TBL
<0.021 mg/Kg - dry 0.021 0.329
1,2,4-Trichlorobenzene 50 09/07/21 13:06 V8448TBL
<0.047 mg/Kg - dry 0.047 0.1641,1,1-Trichloroethane 50 09/07/21 13:06 V8448TBL
<0.015 mg/Kg - dry 0.015 0.1641,1,2-Trichloroethane 50 09/07/21 13:06 V8448TBL
<0.030 mg/Kg - dry 0.030 0.164Trichloroethene 50 09/07/21 13:06 V8448TBL
<0.068 mg/Kg - dry 0.068 0.329Trichlorofluoromethane 50 09/07/21 13:06 V8448TBL
<0.023 mg/Kg - dry 0.023 0.1641,2,3-Trichloropropane 50 09/07/21 13:06 V8448TBL
0.370 mg/Kg - dry 0.017 0.1641,3,5-Trimethylbenzene 50 09/07/21 13:06 V8448TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 77 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S8(11-12)
94725 Matrix:
8/31/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V8447 09/07/21 08:00
<0.015 mg/Kg - dry 0.015 0.329Vinyl Acetate 50 09/07/21 13:06 V8448TBL
<0.015 mg/Kg - dry 0.015 0.329Vinyl Chloride 50 09/07/21 13:06 V8448TBL
<0.016 mg/Kg - dry 0.016 0.164o-Xylene 50 09/07/21 13:06 V8448TBL
<0.041 mg/Kg - dry 0.041 0.329m,p-Xylene 50 09/07/21 13:06 V8448TBL
<0.016 mg/Kg - dry 0.016 0.164Xylene (Total)50 09/07/21 13:06 V8448
Surrogate: 4-Bromofluorobenzene 98.5 Limits: 70-130%09/07/21 13:0650 TBL V8448
Surrogate: Dibromofluoromethane 102 Limits: 70-130%09/07/21 13:0650 TBL V8448
Surrogate: Toluene-d8 109 Limits: 76-129%09/07/21 13:0650 TBL V8448
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.153 mg/Kg - dry 0.153 0.870Acenaphthene 1 09/07/21 18:50 V8596JMV
<0.138 mg/Kg - dry 0.138 0.870Acenaphthylene 1 09/07/21 18:50 V8596JMV
<0.200 mg/Kg - dry 0.200 0.870Aniline 1 09/07/21 18:50 V8596JMV
<0.188 mg/Kg - dry 0.188 0.870Anthracene 1 09/07/21 18:50 V8596JMV
<0.183 mg/Kg - dry 0.183 0.870Benzo(a)anthracene 1 09/07/21 18:50 V8596JMV
<0.193 mg/Kg - dry 0.193 0.870Benzo(a)pyrene 1 09/07/21 18:50 V8596JMV
<0.192 mg/Kg - dry 0.192 0.870
Benzo(b)fluoranthene 1 09/07/21 18:50 V8596JMV
<0.179 mg/Kg - dry 0.179 0.870Benzo(g,h,i)perylene 1 09/07/21 18:50 V8596JMV
<0.180 mg/Kg - dry 0.180 0.870Benzo(k)fluoranthene 1 09/07/21 18:50 V8596JMV
<0.765 mg/Kg - dry 0.765 2.64Benzoic Acid 1 09/07/21 18:50 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 78 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S8(11-12)
94725 Matrix:
8/31/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.138 mg/Kg - dry 0.138 0.870Benzyl alcohol 1 09/07/21 18:50 V8596JMV
<0.155 mg/Kg - dry 0.155 0.870Bis(2-Chloroethoxy)methane 1 09/07/21 18:50 V8596JMV
<0.141 mg/Kg - dry 0.141 0.870Bis(2-Chloroethyl)ether 1 09/07/21 18:50 V8596JMV
<0.179 mg/Kg - dry 0.179 0.435Bis(2-Chloroisopropyl)ether 1 09/07/21 18:50 V8596JMV
<0.158 mg/Kg - dry 0.158 0.870Bis(2-ethylhexyl)phthalate 1 09/07/21 18:50 V8596JMV
<0.143 mg/Kg - dry 0.143 0.8704-Bromophenyl phenyl ether 1 09/07/21 18:50 V8596JMV
<0.149 mg/Kg - dry 0.149 0.435Butyl benzyl phthalate 1 09/07/21 18:50 V8596JMV
<0.121 mg/Kg - dry 0.121 0.8704-Chloro-3-methylphenol 1 09/07/21 18:50 V8596JMV
<0.147 mg/Kg - dry 0.147 0.435
4-Chloroaniline 1 09/07/21 18:50 V8596JMV
<0.153 mg/Kg - dry 0.153 0.8702-Chloronaphthalene 1 09/07/21 18:50 V8596JMV
<0.129 mg/Kg - dry 0.129 0.8702-Chlorophenol 1 09/07/21 18:50 V8596JMV
<0.166 mg/Kg - dry 0.166 1.324-Chlorophenyl phenyl ether 1 09/07/21 18:50 V8596JMV
<0.187 mg/Kg - dry 0.187 0.870Chrysene 1 09/07/21 18:50 V8596JMV
<0.303 mg/Kg - dry 0.303 0.870Dibenz(a,h)anthracene 1 09/07/21 18:50 V8596JMV
<0.156 mg/Kg - dry 0.156 0.870Dibenzofuran 1 09/07/21 18:50 V8596JMV
<0.124 mg/Kg - dry 0.124 0.870
1,2-Dichlorobenzene 1 09/07/21 18:50 V8596JMV
<0.128 mg/Kg - dry 0.128 0.8701,3-Dichlorobenzene 1 09/07/21 18:50 V8596JMV
<0.128 mg/Kg - dry 0.128 0.4351,4-Dichlorobenzene 1 09/07/21 18:50 V8596JMV
<0.193 mg/Kg - dry 0.193 0.8703,3'-Dichlorobenzidine 1 09/07/21 18:50 V8596JMV
<0.126 mg/Kg - dry 0.126 0.8702,4-Dichlorophenol 1 09/07/21 18:50 V8596JMV
<0.237 mg/Kg - dry 0.237 0.870Diethyl phthalate 1 09/07/21 18:50 V8596JMV
<0.229 mg/Kg - dry 0.229 0.870Dimethyl phthalate 1 09/07/21 18:50 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 79 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S8(11-12)
94725 Matrix:
8/31/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.142 mg/Kg - dry 0.142 0.4352,4-Dimethylphenol 1 09/07/21 18:50 V8596JMV
<0.141 mg/Kg - dry 0.141 0.870Di-n-butyl phthalate 1 09/07/21 18:50 V8596JMV
<0.316 mg/Kg - dry 0.316 1.984,6-Dinitro-2-methylphenol 1 09/07/21 18:50 V8596JMV
<0.686 mg/Kg - dry 0.686 1.982,4-Dinitrophenol 1 09/07/21 18:50 V8596JMV
<0.127 mg/Kg - dry 0.127 0.8702,4-Dinitrotoluene 1 09/07/21 18:50 V8596JMV
<0.142 mg/Kg - dry 0.142 0.8702,6-Dinitrotoluene 1 09/07/21 18:50 V8596JMV
<0.188 mg/Kg - dry 0.188 0.435Di-n-Octyl Phthalate 1 09/07/21 18:50 V8596JMV
<0.162 mg/Kg - dry 0.162 0.870Fluoranthene 1 09/07/21 18:50 V8596JMV
0.737 J
mg/Kg - dry 0.168 0.870
Fluorene 1 09/07/21 18:50 V8596JMV
<0.139 mg/Kg - dry 0.139 0.870Hexachlorobenzene 1 09/07/21 18:50 V8596JMV
<0.128 mg/Kg - dry 0.128 0.870Hexachlorobutadiene 1 09/07/21 18:50 V8596JMV
<0.207 mg/Kg - dry 0.207 0.870Hexachlorocyclopentadiene 1 09/07/21 18:50 V8596JMV
<0.104 mg/Kg - dry 0.104 0.870Hexachloroethane 1 09/07/21 18:50 V8596JMV
<0.236 mg/Kg - dry 0.236 0.870Indeno(1,2,3-cd)pyrene 1 09/07/21 18:50 V8596JMV
<0.251 mg/Kg - dry 0.251 0.870Isophorone 1 09/07/21 18:50 V8596JMV
6.17 mg/Kg - dry 0.139 0.870
1-Methylnaphthalene 1 09/07/21 18:50 V8596JMV
6.32 mg/Kg - dry 0.131 0.8702-Methylnaphthalene 1 09/07/21 18:50 V8596JMV
<0.127 mg/Kg - dry 0.127 0.8702-Methylphenol 1 09/07/21 18:50 V8596JMV
<0.112 mg/Kg - dry 0.112 0.8703&4 Methylphenol 1 09/07/21 18:50 V8596JMV
2.02 mg/Kg - dry 0.189 0.870Naphthalene 1 09/07/21 18:50 V8596JMV
<0.127 mg/Kg - dry 0.127 0.8702-Nitroaniline 1 09/07/21 18:50 V8596JMV
<0.158 mg/Kg - dry 0.158 0.8703-Nitroaniline 1 09/07/21 18:50 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 80 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:S8(11-12)
94725 Matrix:
8/31/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.123 mg/Kg - dry 0.123 0.4354-Nitroaniline 1 09/07/21 18:50 V8596JMV
<0.153 mg/Kg - dry 0.153 0.435Nitrobenzene 1 09/07/21 18:50 V8596JMV
<0.117 mg/Kg - dry 0.117 0.8702-Nitrophenol 1 09/07/21 18:50 V8596JMV
<0.154 mg/Kg - dry 0.154 0.8704-Nitrophenol 1 09/07/21 18:50 V8596JMV
<0.346 mg/Kg - dry 0.346 0.870N-Nitrosodimethylamine 1 09/07/21 18:50 V8596JMV
<0.238 mg/Kg - dry 0.238 0.870N-Nitrosodiphenylamine 1 09/07/21 18:50 V8596JMV
<0.155 mg/Kg - dry 0.155 0.870N-Nitroso-di-n-propylamine 1 09/07/21 18:50 V8596JMV
<0.457 mg/Kg - dry 0.457 1.32Pentachlorophenol 1 09/07/21 18:50 V8596JMV
1.69 mg/Kg - dry 0.274 0.870
Phenanthrene 1 09/07/21 18:50 V8596JMV
<0.147 mg/Kg - dry 0.147 0.870Phenol 1 09/07/21 18:50 V8596JMV
<0.176 mg/Kg - dry 0.176 0.870Pyrene 1 09/07/21 18:50 V8596JMV
<0.104 mg/Kg - dry 0.104 0.435Pyridine 1 09/07/21 18:50 V8596JMV
<0.141 mg/Kg - dry 0.141 0.8701,2,4-Trichlorobenzene 1 09/07/21 18:50 V8596JMV
<0.126 mg/Kg - dry 0.126 0.8702,4,5-Trichlorophenol 1 09/07/21 18:50 V8596JMV
<0.127 mg/Kg - dry 0.127 0.8702,4,6-Trichlorophenol 1 09/07/21 18:50 V8596JMV
Surrogate: Phenol-d5 73.6 Limits: 34-121%09/07/21 18:501 JMV V8596
Surrogate: 2-Fluorobiphenyl 79.0 Limits: 44-115%09/07/21 18:501 JMV V8596
Surrogate: 2-Fluorophenol 73.9 Limits: 35-115%09/07/21 18:501 JMV V8596
Surrogate: Nitrobenzene-d5 71.3 Limits: 37-122%09/07/21 18:501 JMV V8596
Surrogate: 4-Terphenyl-d14 88.0 Limits: 54-127%09/07/21 18:501 JMV V8596
Surrogate: 2,4,6-Tribromophenol 92.5 Limits: 39-132%09/07/21 18:501 JMV V8596
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 81 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:Dup-1 soil
94726 Matrix:
8/31/2021 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.4 %Moisture 1 09/03/21 17:05 SW-DRYWTBAM
1.04 J mg/Kg - dry 0.121 1.29Arsenic 10 09/07/21 23:21 6020BEDV
169 mg/Kg - dry 1.80 12.9Barium 10 09/07/21 23:21 6020BEDV
<0.0708 mg/Kg - dry 0.0708 0.644Cadmium 10 09/07/21 23:21 6020BEDV
88.7 mg/Kg - dry 0.373 1.29Chromium 10 09/07/21 23:21 6020BEDV
2.94 mg/Kg - dry 0.180 1.29
Lead 10 09/07/21 23:21 6020BEDV
<0.0155 mg/Kg - dry 0.0155 0.0387Mercury (Total)1 09/08/21 14:41 7471BEDV
2.96 mg/Kg - dry 1.16 2.58Selenium 10 09/08/21 23:18 6020BEDV
<0.0528 mg/Kg - dry 0.0528 0.644Silver 10 09/07/21 23:21 6020BEDV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 82 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:Dup-1 soil
94726 Matrix:
8/31/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
0.014 J mg/Kg - dry 0.003 0.025Acetone 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 09/03/21 14:44 V8431TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 09/03/21 14:44 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/03/21 14:44 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/03/21 14:44 V8431TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/03/21 14:44 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/03/21 14:44 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/03/21 14:44 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/03/21 14:44 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/03/21 14:44 V8431TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/03/21 14:44 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/03/21 14:44 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/03/21 14:44 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 09/03/21 14:44 V8431TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/03/21 14:44 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/03/21 14:44 V8431TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 83 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:Dup-1 soil
94726 Matrix:
8/31/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/03/21 14:44 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/03/21 14:44 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/03/21 14:44 V8431TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/03/21 14:44 V8431TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/03/21 14:44 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/03/21 14:44 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/03/21 14:44 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/03/21 14:44 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/03/21 14:44 V8431TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 09/03/21 14:44 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/03/21 14:44 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 09/03/21 14:44 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 09/03/21 14:44 V8431TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 84 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:Dup-1 soil
94726 Matrix:
8/31/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/03/21 14:44 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/03/21 14:44 V8431TBL
0.001 J mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/03/21 14:44 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/03/21 14:44 V8431TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 09/03/21 14:44 V8431TBL
0.010 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 09/03/21 14:44 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/03/21 14:44 V8431TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/03/21 14:44 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 09/03/21 14:44 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 09/03/21 14:44 V8431TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/03/21 14:44 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/03/21 14:44 V8431TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/03/21 14:44 V8431TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/03/21 14:44 V8431TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/03/21 14:44 V8431TBL
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 85 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:Dup-1 soil
94726 Matrix:
8/31/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8429 09/03/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/03/21 14:44 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/03/21 14:44 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/03/21 14:44 V8431TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/03/21 14:44 V8431TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/03/21 14:44 V8431
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/03/21 14:441 TBL V8431
Surrogate: Dibromofluoromethane 103 Limits: 84-123%09/03/21 14:441 TBL V8431
Surrogate: Toluene-d8 107 Limits: 76-129%09/03/21 14:441 TBL V8431
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.149 mg/Kg - dry 0.149 0.850Acenaphthene 1 09/07/21 19:12 V8596JMV
<0.135 mg/Kg - dry 0.135 0.850Acenaphthylene 1 09/07/21 19:12 V8596JMV
<0.195 mg/Kg - dry 0.195 0.850Aniline 1 09/07/21 19:12 V8596JMV
<0.184 mg/Kg - dry 0.184 0.850Anthracene 1 09/07/21 19:12 V8596JMV
<0.179 mg/Kg - dry 0.179 0.850Benzo(a)anthracene 1 09/07/21 19:12 V8596JMV
<0.189 mg/Kg - dry 0.189 0.850Benzo(a)pyrene 1 09/07/21 19:12 V8596JMV
<0.188 mg/Kg - dry 0.188 0.850
Benzo(b)fluoranthene 1 09/07/21 19:12 V8596JMV
<0.175 mg/Kg - dry 0.175 0.850Benzo(g,h,i)perylene 1 09/07/21 19:12 V8596JMV
<0.176 mg/Kg - dry 0.176 0.850Benzo(k)fluoranthene 1 09/07/21 19:12 V8596JMV
<0.747 mg/Kg - dry 0.747 2.58Benzoic Acid 1 09/07/21 19:12 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 86 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:Dup-1 soil
94726 Matrix:
8/31/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.135 mg/Kg - dry 0.135 0.850Benzyl alcohol 1 09/07/21 19:12 V8596JMV
<0.152 mg/Kg - dry 0.152 0.850Bis(2-Chloroethoxy)methane 1 09/07/21 19:12 V8596JMV
<0.137 mg/Kg - dry 0.137 0.850Bis(2-Chloroethyl)ether 1 09/07/21 19:12 V8596JMV
<0.175 mg/Kg - dry 0.175 0.425Bis(2-Chloroisopropyl)ether 1 09/07/21 19:12 V8596JMV
<0.154 mg/Kg - dry 0.154 0.850Bis(2-ethylhexyl)phthalate 1 09/07/21 19:12 V8596JMV
<0.140 mg/Kg - dry 0.140 0.8504-Bromophenyl phenyl ether 1 09/07/21 19:12 V8596JMV
<0.145 mg/Kg - dry 0.145 0.425Butyl benzyl phthalate 1 09/07/21 19:12 V8596JMV
<0.119 mg/Kg - dry 0.119 0.8504-Chloro-3-methylphenol 1 09/07/21 19:12 V8596JMV
<0.144 mg/Kg - dry 0.144 0.425
4-Chloroaniline 1 09/07/21 19:12 V8596JMV
<0.149 mg/Kg - dry 0.149 0.8502-Chloronaphthalene 1 09/07/21 19:12 V8596JMV
<0.126 mg/Kg - dry 0.126 0.8502-Chlorophenol 1 09/07/21 19:12 V8596JMV
<0.162 mg/Kg - dry 0.162 1.294-Chlorophenyl phenyl ether 1 09/07/21 19:12 V8596JMV
<0.182 mg/Kg - dry 0.182 0.850Chrysene 1 09/07/21 19:12 V8596JMV
<0.296 mg/Kg - dry 0.296 0.850Dibenz(a,h)anthracene 1 09/07/21 19:12 V8596JMV
<0.153 mg/Kg - dry 0.153 0.850Dibenzofuran 1 09/07/21 19:12 V8596JMV
<0.121 mg/Kg - dry 0.121 0.850
1,2-Dichlorobenzene 1 09/07/21 19:12 V8596JMV
<0.125 mg/Kg - dry 0.125 0.8501,3-Dichlorobenzene 1 09/07/21 19:12 V8596JMV
<0.125 mg/Kg - dry 0.125 0.4251,4-Dichlorobenzene 1 09/07/21 19:12 V8596JMV
<0.189 mg/Kg - dry 0.189 0.8503,3'-Dichlorobenzidine 1 09/07/21 19:12 V8596JMV
<0.123 mg/Kg - dry 0.123 0.8502,4-Dichlorophenol 1 09/07/21 19:12 V8596JMV
<0.231 mg/Kg - dry 0.231 0.850Diethyl phthalate 1 09/07/21 19:12 V8596JMV
<0.224 mg/Kg - dry 0.224 0.850Dimethyl phthalate 1 09/07/21 19:12 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 87 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:Dup-1 soil
94726 Matrix:
8/31/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.139 mg/Kg - dry 0.139 0.4252,4-Dimethylphenol 1 09/07/21 19:12 V8596JMV
<0.137 mg/Kg - dry 0.137 0.850Di-n-butyl phthalate 1 09/07/21 19:12 V8596JMV
<0.309 mg/Kg - dry 0.309 1.934,6-Dinitro-2-methylphenol 1 09/07/21 19:12 V8596JMV
<0.670 mg/Kg - dry 0.670 1.932,4-Dinitrophenol 1 09/07/21 19:12 V8596JMV
<0.124 mg/Kg - dry 0.124 0.8502,4-Dinitrotoluene 1 09/07/21 19:12 V8596JMV
<0.139 mg/Kg - dry 0.139 0.8502,6-Dinitrotoluene 1 09/07/21 19:12 V8596JMV
<0.184 mg/Kg - dry 0.184 0.425Di-n-Octyl Phthalate 1 09/07/21 19:12 V8596JMV
<0.158 mg/Kg - dry 0.158 0.850Fluoranthene 1 09/07/21 19:12 V8596JMV
<0.164 mg/Kg - dry 0.164 0.850
Fluorene 1 09/07/21 19:12 V8596JMV
<0.136 mg/Kg - dry 0.136 0.850Hexachlorobenzene 1 09/07/21 19:12 V8596JMV
<0.125 mg/Kg - dry 0.125 0.850Hexachlorobutadiene 1 09/07/21 19:12 V8596JMV
<0.202 mg/Kg - dry 0.202 0.850Hexachlorocyclopentadiene 1 09/07/21 19:12 V8596JMV
<0.102 mg/Kg - dry 0.102 0.850Hexachloroethane 1 09/07/21 19:12 V8596JMV
<0.230 mg/Kg - dry 0.230 0.850Indeno(1,2,3-cd)pyrene 1 09/07/21 19:12 V8596JMV
<0.246 mg/Kg - dry 0.246 0.850Isophorone 1 09/07/21 19:12 V8596JMV
<0.136 mg/Kg - dry 0.136 0.850
1-Methylnaphthalene 1 09/07/21 19:12 V8596JMV
<0.128 mg/Kg - dry 0.128 0.8502-Methylnaphthalene 1 09/07/21 19:12 V8596JMV
<0.125 mg/Kg - dry 0.125 0.8502-Methylphenol 1 09/07/21 19:12 V8596JMV
<0.109 mg/Kg - dry 0.109 0.8503&4 Methylphenol 1 09/07/21 19:12 V8596JMV
<0.185 mg/Kg - dry 0.185 0.850Naphthalene 1 09/07/21 19:12 V8596JMV
<0.124 mg/Kg - dry 0.124 0.8502-Nitroaniline 1 09/07/21 19:12 V8596JMV
<0.154 mg/Kg - dry 0.154 0.8503-Nitroaniline 1 09/07/21 19:12 V8596JMV
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 88 of 154
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0018
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Revised Report Date: 10/01/2021
Original Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:Dup-1 soil
94726 Matrix:
8/31/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8456 09/07/21 10:35
<0.120 mg/Kg - dry 0.120 0.4254-Nitroaniline 1 09/07/21 19:12 V8596JMV
<0.149 mg/Kg - dry 0.149 0.425Nitrobenzene 1 09/07/21 19:12 V8596JMV
<0.114 mg/Kg - dry 0.114 0.8502-Nitrophenol 1 09/07/21 19:12 V8596JMV
<0.150 mg/Kg - dry 0.150 0.8504-Nitrophenol 1 09/07/21 19:12 V8596JMV
<0.338 mg/Kg - dry 0.338 0.850N-Nitrosodimethylamine 1 09/07/21 19:12 V8596JMV
<0.233 mg/Kg - dry 0.233 0.850N-Nitrosodiphenylamine 1 09/07/21 19:12 V8596JMV
<0.152 mg/Kg - dry 0.152 0.850N-Nitroso-di-n-propylamine 1 09/07/21 19:12 V8596JMV
<0.447 mg/Kg - dry 0.447 1.29Pentachlorophenol 1 09/07/21 19:12 V8596JMV
<0.268 mg/Kg - dry 0.268 0.850
Phenanthrene 1 09/07/21 19:12 V8596JMV
<0.144 mg/Kg - dry 0.144 0.850Phenol 1 09/07/21 19:12 V8596JMV
<0.172 mg/Kg - dry 0.172 0.850Pyrene 1 09/07/21 19:12 V8596JMV
<0.102 mg/Kg - dry 0.102 0.425Pyridine 1 09/07/21 19:12 V8596JMV
<0.137 mg/Kg - dry 0.137 0.8501,2,4-Trichlorobenzene 1 09/07/21 19:12 V8596JMV
<0.123 mg/Kg - dry 0.123 0.8502,4,5-Trichlorophenol 1 09/07/21 19:12 V8596JMV
<0.124 mg/Kg - dry 0.124 0.8502,4,6-Trichlorophenol 1 09/07/21 19:12 V8596JMV
Surrogate: Phenol-d5 74.8 Limits: 34-121%09/07/21 19:121 JMV V8596
Surrogate: 2-Fluorobiphenyl 74.1 Limits: 44-115%09/07/21 19:121 JMV V8596
Surrogate: 2-Fluorophenol 76.0 Limits: 35-115%09/07/21 19:121 JMV V8596
Surrogate: Nitrobenzene-d5 67.5 Limits: 37-122%09/07/21 19:121 JMV V8596
Surrogate: 4-Terphenyl-d14 86.1 Limits: 54-127%09/07/21 19:121 JMV V8596
Surrogate: 2,4,6-Tribromophenol 84.1 Limits: 39-132%09/07/21 19:121 JMV V8596
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 89 of 154
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172Tel: [phone] Fax: [phone] www.pacelabs.com
Report of Analysis
Waypoint Analytical
PO Box 240543Charlotte, NC 28224Attention: Angela Overcash
Project Name: 21-242-0018
Lot Number:WI27071
Date Completed:09/30/2021
10/01/2021 11:59 AMApproved and released by:
Project Manager II:Lucas Odom
Page 1 of 16
Page 90 of 154
PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Waypoint Analytical
Lot Number: WI27071
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header informationassociated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page ordiscussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non-Potable Water: SGT-HEM EPA 1664B,Silica EPA 200.7, Boron, Calcium,Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weightunless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Page 2 of 16
Page 91 of 154
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: WI27071

Sample Number Sample ID Matrix Date Sampled Date Received
001 08/30/2021 1330S-9 (7-8)Solid 09/27/2021
002 08/31/2021 1045S7 (10-11)Solid 09/27/2021
003 08/31/2021 1250S6 (14-15)Solid 09/27/2021
004 08/31/2021 0930S8 (11-12)Solid 09/27/2021
005 08/31/2021Dup-1 Soil Solid 09/27/2021
(5 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 16
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Waypoint Analytical
Lot Number: WI27071

Sample Sample ID Matrix Parameter Method Result Q Units Page
002 S7 (10-11) Solid Hexavalent Chromium 7199 1.9 mg/kg 6
(1 detection)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 16
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S-9 (7-8)
WI27071-001
08/30/2021 1330
09/27/2021
Solid
% Solids:75.4 09/27/2021 2236
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 09/29/2021 1638 AMR 09/29/2021 1152 16787
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.271.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 16
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S7 (10-11)
WI27071-002
08/31/2021 1045
09/27/2021
Solid
% Solids:82.5 09/27/2021 2236
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 09/29/2021 1651 AMR 09/29/2021 1152 16787
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 1.9 1mg/kg0.241.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 16
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S6 (14-15)
WI27071-003
08/31/2021 1250
09/27/2021
Solid
% Solids:80.0 09/27/2021 2236
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 09/29/2021 1704 AMR 09/29/2021 1152 16787
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.251.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 16
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S8 (11-12)
WI27071-004
08/31/2021 0930
09/27/2021
Solid
% Solids:72.3 09/27/2021 2236
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 09/29/2021 1730 AMR 09/29/2021 1152 16787
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.281.4
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 16
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
Dup-1 Soil
WI27071-005
08/31/2021
09/27/2021
Solid
% Solids:78.5 09/27/2021 2236
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 09/29/2021 1743 AMR 09/29/2021 1152 16787
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.251.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 16
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 16
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ16787-001
16787 3060A
09/29/2021 1152Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 09/29/2021 15591.0 0.20 mg/kg1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 16
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ16787-002
16787 3060A
09/29/2021 1152Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg) (mg/kg)
Hexavalent Chromium 9.0 09/29/2021 1625901080-1201
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 12 of 16
Inorganic non-metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:WI27071-003MS
16787 3060A
09/29/2021 1152Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
Limit
Sample
Amount
Dil(mg/kg) (mg/kg) (mg/kg)
Hexavalent Chromium 1400 09/29/2021 1717107130075-125ND50
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 13 of 16
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 14 of 16
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 15 of 16
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 16 of 16
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Metals Analyses
6020B
V8496,V8545QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V8434
Associated Lab Samples: 94722, 94723, 94724, 94725, 94726
LRB-V8434 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/07/21 21:581.000.0940<0.0940mg/KgArsenic
09/07/21 21:5810.01.40<1.40mg/KgBarium
09/07/21 21:580.5000.0550<0.0550mg/KgCadmium
09/07/21 21:581.000.290<0.290mg/KgChromium
09/07/21 21:581.000.140<0.140mg/KgLead
09/08/21 16:102.000.900<0.900mg/KgSelenium
09/07/21 21:580.5000.0410<0.0410mg/KgSilver
LCS-V8434Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10212.812.5mg/KgArsenic 80-120
10813.512.5mg/KgBarium 80-120
10613.212.5mg/KgCadmium 80-120
10713.412.5mg/KgChromium 80-120
10312.912.5mg/KgLead 80-120
99.012.412.5mg/KgSelenium 80-120
1035.155.00mg/KgSilver 80-120
Page 1 of 46Date:10/01/2021 12:25 PM
Page 106 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Metals Analyses
6020B
V8470,V8497,V8563QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V8436
Associated Lab Samples: 94717, 94718, 94719, 94720, 94721
LRB-V8436 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/08/21 18:271.000.1700.447µg/LArsenic
09/07/21 17:4010.00.810<0.810µg/LBarium
09/07/21 17:401.000.160<0.160µg/LCadmium
09/07/21 17:402.000.790<0.790µg/LChromium
09/07/21 17:401.000.260<0.260µg/LLead
09/08/21 18:275.000.740<0.740µg/LSelenium
09/07/21 17:401.000.110<0.110µg/LSilver
LCS-V8436Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.095.8100µg/LArsenic 80-120
96.096.3100µg/LBarium 80-120
100100100µg/LCadmium 80-120
93.092.9100µg/LChromium 80-120
99.099.0100µg/LLead 80-120
96.095.9100µg/LSelenium 80-120
98.098.3100µg/LSilver 80-120
V 94792-MS-V8436 V 94792-MSD-V8436Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
95.9 96.095.01001000.948µg/LArsenic 95.0 75-125 0.9 20.0
107 93.010910010014.2µg/LBarium 95.0 75-125 1.8 20.0
97.7 98.098.3100100< 0.160µg/LCadmium 98.0 75-125 0.6 20.0
102 1021051001001.92µg/LChromium 105 75-125 2.8 20.0
Page 2 of 46Date:10/01/2021 12:25 PM
Page 107 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Metals Analyses
6020B
V8470,V8497,V8563QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V8436
V 94792-MS-V8436 V 94792-MSD-V8436Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
99.6 98.099.31001001.11µg/LLead 98.0 75-125 0.3 20.0
98.3 98.0101100100< 0.740µg/LSelenium 101 75-125 2.7 20.0
99.8 10099.0100100< 0.110µg/LSilver 99.0 75-125 0.8 20.0
V 94792-PDS-V8436Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/08/21 19:2599.049.5µg/LArsenic
09/07/21 18:0599.056.6µg/LBarium
09/07/21 18:0510351.5µg/LCadmium
09/07/21 18:0510853.8µg/LChromium
09/07/21 18:0510151.2µg/LLead
09/08/21 19:2594.047.1µg/LSelenium
09/07/21 18:0510251.1µg/LSilver
Page 3 of 46Date:10/01/2021 12:25 PM
Page 108 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Total Aqueous Mercury Analysis - CVAA
7470A
V8475,V8479QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7470A
QC Prep:V8451
Associated Lab Samples: 94717, 94718, 94719, 94720, 94721
LRB-V8451 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/07/21 16:240.000200.00007<0.00007mg/LMercury (Total)
LCS-V8451Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
92.00.008590.00937mg/LMercury (Total)80-120
V 94717-MS-V8451 V 94717-MSD-V8451Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.00622 66.0*0.006120.009370.00937< 0.00007mg/LMercury (Total)65.0*80-120 1.6 20.0
V 94717-PDS-V8451Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/07/21 17:1780.0*0.00373mg/LMercury (Total)
Page 4 of 46* QC Fail Date:10/01/2021 12:25 PM
Page 109 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V8538QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V8520
Associated Lab Samples: 94722, 94723, 94724, 94725, 94726
LRB-V8520 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/08/21 14:060.03000.0120<0.0120mg/KgMercury (Total)
LCS-V8520Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.00.4010.417mg/KgMercury (Total)80-120
V 94722-MS-V8520 V 94722-MSD-V8520Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.313 75.0*0.2150.4170.417<0.0120mg/KgMercury (Total)52.0*80-120 37.1*20
V 94722-PDS-V8520Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/08/21 14:201030.214mg/KgMercury (Total)
Page 5 of 46* QC Fail Date:10/01/2021 12:25 PM
Page 110 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8431QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8429
Associated Lab Samples: 94723, 94724, 94726
LRB-V8429 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/03/21 10:150.0200.002<0.002mg/KgAcetone
09/03/21 10:150.0200.001<0.001mg/KgAcrolein
09/03/21 10:150.0200.0008<0.0008mg/KgAcrylonitrile
09/03/21 10:150.0050.0006<0.0006mg/KgBenzene
09/03/21 10:150.0050.0005<0.0005mg/KgBromobenzene
09/03/21 10:150.0050.0008<0.0008mg/KgBromochloromethane
09/03/21 10:150.0050.001<0.001mg/KgBromodichloromethane
09/03/21 10:150.0050.001<0.001mg/KgBromoform
09/03/21 10:150.0100.001<0.001mg/KgBromomethane
09/03/21 10:150.0050.0005<0.0005mg/Kgn-Butylbenzene
09/03/21 10:150.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/03/21 10:150.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/03/21 10:150.0050.0006<0.0006mg/KgCarbon Disulfide
09/03/21 10:150.0050.001<0.001mg/KgCarbon Tetrachloride
09/03/21 10:150.0050.0007<0.0007mg/KgChlorobenzene
09/03/21 10:150.0050.0009<0.0009mg/KgChlorodibromomethane
09/03/21 10:150.0100.0009<0.0009mg/KgChloroethane
09/03/21 10:150.0050.001<0.001mg/KgChloroform
09/03/21 10:150.0100.0006<0.0006mg/KgChloromethane
09/03/21 10:150.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/03/21 10:150.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/03/21 10:150.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/03/21 10:150.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/03/21 10:150.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/03/21 10:150.0050.0006<0.0006mg/KgDibromomethane
09/03/21 10:150.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/03/21 10:150.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 6 of 46Date:10/01/2021 12:25 PM
Page 111 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8431QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8429
Associated Lab Samples: 94723, 94724, 94726
LRB-V8429 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/03/21 10:150.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/03/21 10:150.0100.001<0.001mg/KgDichlorodifluoromethane
09/03/21 10:150.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/03/21 10:150.0050.001<0.001mg/Kg1,2-Dichloroethane
09/03/21 10:150.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/03/21 10:150.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/03/21 10:150.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/03/21 10:150.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/03/21 10:150.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/03/21 10:150.0050.001<0.001mg/Kg2,2-Dichloropropane
09/03/21 10:150.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/03/21 10:150.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/03/21 10:150.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/03/21 10:150.0050.0006<0.0006mg/KgEthylbenzene
09/03/21 10:150.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/03/21 10:150.0100.0008<0.0008mg/KgHexachlorobutadiene
09/03/21 10:150.0100.0007<0.0007mg/Kgn-Hexane
09/03/21 10:150.0200.0006<0.0006mg/Kg2-Hexanone
09/03/21 10:150.0050.0005<0.0005mg/KgIsopropylbenzene
09/03/21 10:150.0050.001<0.001mg/Kg4-Isopropyl toluene
09/03/21 10:150.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/03/21 10:150.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/03/21 10:150.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/03/21 10:150.0100.001<0.001mg/KgMethylene Chloride
09/03/21 10:150.0100.0010<0.0010mg/KgNaphthalene
09/03/21 10:150.0050.0005<0.0005mg/Kgn-Propylbenzene
09/03/21 10:150.0050.001<0.001mg/KgStyrene
Page 7 of 46Date:10/01/2021 12:25 PM
Page 112 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8431QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8429
Associated Lab Samples: 94723, 94724, 94726
LRB-V8429 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/03/21 10:150.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/03/21 10:150.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/03/21 10:150.0050.0009<0.0009mg/KgTetrachloroethene
09/03/21 10:150.0050.0007<0.0007mg/KgToluene
09/03/21 10:150.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/03/21 10:150.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/03/21 10:150.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/03/21 10:150.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/03/21 10:150.0050.0009<0.0009mg/KgTrichloroethene
09/03/21 10:150.0100.002<0.002mg/KgTrichlorofluoromethane
09/03/21 10:150.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/03/21 10:150.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/03/21 10:150.0100.0005<0.0005mg/KgVinyl Acetate
09/03/21 10:150.0100.0005<0.0005mg/KgVinyl Chloride
09/03/21 10:150.0050.0005<0.0005mg/Kgo-Xylene
09/03/21 10:150.0100.001<0.001mg/Kgm,p-Xylene
09/03/21 10:154-Bromofluorobenzene (S)105 70-130
09/03/21 10:15Dibromofluoromethane (S)103 84-123
09/03/21 10:15Toluene-d8 (S)108 76-129
LCS-V8429 LCSD-V8429Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.086 86.688.80.0880.100mg/KgAcetone 29-198 2.5 20
0.099 99.21010.1010.100mg/KgAcrolein 70-130 1.7 20
0.095 95.496.60.0960.100mg/KgAcrylonitrile 65-134 1.2 20
Page 8 of 46Date:10/01/2021 12:25 PM
Page 113 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8431QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8429
LCS-V8429 LCSD-V8429Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 84.888.00.0440.050mg/KgBenzene 74-127 3.7 20
0.049 99.61040.0510.050mg/KgBromobenzene 73-125 3.9 20
0.044 88.490.20.0450.050mg/KgBromochloromethane 72-134 2.0 20
0.043 87.087.80.0430.050mg/KgBromodichloromethane 75-122 0.9 20
0.049 98.299.00.0490.050mg/KgBromoform 66-135 0.8 20
0.040 81.891.60.0450.050mg/KgBromomethane 20-180 11.3 20
0.050 1001080.0530.050mg/Kgn-Butylbenzene 65-135 7.1 20
0.049 99.01050.0520.050mg/Kgsec-Butyl benzene 66-131 5.8 20
0.049 99.21040.0520.050mg/Kgtert-Butyl benzene 67-132 5.1 20
0.042 84.888.80.0440.050mg/KgCarbon Disulfide 61-129 4.6 20
0.040 81.888.00.0440.050mg/KgCarbon Tetrachloride 64-143 7.3 20
0.045 91.494.60.0470.050mg/KgChlorobenzene 74-118 3.4 20
0.047 95.498.00.0490.050mg/KgChlorodibromomethane 73-122 2.6 20
0.038 76.282.40.0410.050mg/KgChloroethane 33-149 7.8 20
0.041 83.685.40.0420.050mg/KgChloroform 73-127 2.1 20
0.043 86.291.00.0450.050mg/KgChloromethane 45-143 5.4 20
0.050 1001040.0510.050mg/Kg2-Chlorotoluene 67-124 3.5 20
0.049 99.41030.0510.050mg/Kg4-Chlorotoluene 71-126 3.5 20
0.043 87.889.40.0440.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.8 20
0.057 1141100.0550.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.3 20
0.048 96.097.40.0480.050mg/Kg1,2-Dibromoethane 70-132 1.4 20
0.044 89.090.00.0450.050mg/KgDibromomethane 74-133 1.1 20
0.049 99.41030.0510.050mg/Kg1,2-Dichlorobenzene 72-123 3.3 20
0.049 99.41030.0510.050mg/Kg1,3-Dichlorobenzene 71-120 3.7 20
0.050 1001020.0500.050mg/Kg1,4-Dichlorobenzene 71-123 1.5 20
0.044 89.694.00.0470.050mg/KgDichlorodifluoromethane 26-146 4.7 20
Page 9 of 46Date:10/01/2021 12:25 PM
Page 114 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8431QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8429
LCS-V8429 LCSD-V8429Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 84.888.00.0440.050mg/Kg1,1-Dichloroethane 74-127 3.7 20
0.043 86.487.00.0430.050mg/Kg1,2-Dichloroethane 68-128 0.6 20
0.042 84.289.40.0440.050mg/Kg1,1-Dichloroethene 67-149 5.9 20
0.042 85.288.40.0440.050mg/Kgcis-1,2-Dichloroethene 76-134 3.6 20
0.042 85.288.20.0440.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.4 20
0.042 85.487.80.0430.050mg/Kg1,2-Dichloropropane 73-130 2.7 20
0.047 95.295.60.0470.050mg/Kg1,3-Dichloropropane 75-124 0.4 20
0.041 83.691.00.0450.050mg/Kg2,2-Dichloropropane 50-142 8.4 20
0.042 84.488.40.0440.050mg/Kg1,1-Dichloropropene 71-130 4.6 20
0.043 87.290.00.0450.050mg/Kgcis-1,3-Dichloropropene 71-125 3.1 20
0.044 89.690.20.0450.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.6 20
0.045 90.895.40.0470.050mg/KgEthylbenzene 74-128 4.9 20
0.091 91.191.40.0910.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.3 20
0.049 98.21030.0510.050mg/KgHexachlorobutadiene 64-125 4.7 20
0.044 88.297.60.0480.050mg/Kgn-Hexane 70-130 10.1 20
0.051 1031030.0510.050mg/Kg2-Hexanone 61-157 0.1 20
0.049 98.61040.0510.050mg/KgIsopropylbenzene 68-126 5.1 20
0.050 1011060.0520.050mg/Kg4-Isopropyl toluene 68-129 4.8 20
0.045 91.893.20.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.5 20
0.044 89.890.40.0450.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.6 20
0.047 94.294.80.0470.050mg/Kg4-Methyl-2-Pentanone 57-162 0.6 20
0.040 80.082.60.0410.050mg/KgMethylene Chloride 74-129 3.1 20
0.053 1071090.0540.050mg/KgNaphthalene 57-157 1.4 20
0.049 99.21050.0520.050mg/Kgn-Propylbenzene 67-130 6.0 20
0.047 95.298.40.0490.050mg/KgStyrene 77-121 3.3 20
0.046 92.695.00.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 2.5 20
Page 10 of 46Date:10/01/2021 12:25 PM
Page 115 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8431QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8429
LCS-V8429 LCSD-V8429Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.052 1061080.0540.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.2 20
0.041 82.488.20.0440.050mg/KgTetrachloroethene 68-130 6.7 20
0.042 84.887.40.0430.050mg/KgToluene 71-129 3.0 20
0.051 1031040.0520.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.5 20
0.051 1031040.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.1 20
0.041 82.286.80.0430.050mg/Kg1,1,1-Trichloroethane 67-131 5.4 20
0.047 95.697.80.0480.050mg/Kg1,1,2-Trichloroethane 70-133 2.2 20
0.042 84.488.40.0440.050mg/KgTrichloroethene 75-133 4.6 20
0.044 89.095.20.0470.050mg/KgTrichlorofluoromethane 44-146 6.7 20
0.053 1081070.0530.050mg/Kg1,2,3-Trichloropropane 60-137 1.1 20
0.049 98.61040.0510.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.1 20
0.052 1041000.0500.050mg/KgVinyl Acetate 85-161 3.9 20
0.043 86.091.40.0450.050mg/KgVinyl Chloride 48-147 6.0 20
0.046 92.495.60.0470.050mg/Kgo-Xylene 74-126 3.4 20
0.093 93.598.60.0980.100mg/Kgm,p-Xylene 75-124 5.3 20
1011024-Bromofluorobenzene (S)70-130
102102Dibromofluoromethane (S)84-123
108108Toluene-d8 (S)76-129
Page 11 of 46Date:10/01/2021 12:25 PM
Page 116 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8448QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V8447
Associated Lab Samples: 94725
LRB-V8447 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 10:370.0200.002<0.002mg/KgAcetone
09/07/21 10:370.0200.001<0.001mg/KgAcrolein
09/07/21 10:370.0200.0008<0.0008mg/KgAcrylonitrile
09/07/21 10:370.0050.0006<0.0006mg/KgBenzene
09/07/21 10:370.0050.0005<0.0005mg/KgBromobenzene
09/07/21 10:370.0050.0008<0.0008mg/KgBromochloromethane
09/07/21 10:370.0050.001<0.001mg/KgBromodichloromethane
09/07/21 10:370.0050.001<0.001mg/KgBromoform
09/07/21 10:370.0100.001<0.001mg/KgBromomethane
09/07/21 10:370.0050.0005<0.0005mg/Kgn-Butylbenzene
09/07/21 10:370.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/07/21 10:370.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/07/21 10:370.0050.0006<0.0006mg/KgCarbon Disulfide
09/07/21 10:370.0050.001<0.001mg/KgCarbon Tetrachloride
09/07/21 10:370.0050.0007<0.0007mg/KgChlorobenzene
09/07/21 10:370.0050.0009<0.0009mg/KgChlorodibromomethane
09/07/21 10:370.0100.0009<0.0009mg/KgChloroethane
09/07/21 10:370.0050.001<0.001mg/KgChloroform
09/07/21 10:370.0100.0006<0.0006mg/KgChloromethane
09/07/21 10:370.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/07/21 10:370.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/07/21 10:370.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/07/21 10:370.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/07/21 10:370.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/07/21 10:370.0050.0010<0.0010mg/KgDibromomethane
09/07/21 10:370.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/07/21 10:370.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 12 of 46Date:10/01/2021 12:25 PM
Page 117 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8448QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V8447
Associated Lab Samples: 94725
LRB-V8447 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 10:370.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/07/21 10:370.0100.001<0.001mg/KgDichlorodifluoromethane
09/07/21 10:370.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/07/21 10:370.0050.001<0.001mg/Kg1,2-Dichloroethane
09/07/21 10:370.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/07/21 10:370.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/07/21 10:370.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/07/21 10:370.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/07/21 10:370.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/07/21 10:370.0050.001<0.001mg/Kg2,2-Dichloropropane
09/07/21 10:370.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/07/21 10:370.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/07/21 10:370.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/07/21 10:370.0050.0006<0.0006mg/KgEthylbenzene
09/07/21 10:370.1000.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/07/21 10:370.0100.0008<0.0008mg/KgHexachlorobutadiene
09/07/21 10:370.0100.0007<0.0007mg/Kgn-Hexane
09/07/21 10:370.0200.0006<0.0006mg/Kg2-Hexanone
09/07/21 10:370.0050.0005<0.0005mg/KgIsopropylbenzene
09/07/21 10:370.0050.001<0.001mg/Kg4-Isopropyl toluene
09/07/21 10:370.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/07/21 10:370.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/07/21 10:370.0050.001<0.001mg/KgMethylene Chloride
09/07/21 10:370.0100.0010<0.0010mg/KgNaphthalene
09/07/21 10:370.0050.0005<0.0005mg/Kgn-Propylbenzene
09/07/21 10:370.0050.001<0.001mg/KgStyrene
09/07/21 10:370.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
Page 13 of 46Date:10/01/2021 12:25 PM
Page 118 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8448QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V8447
Associated Lab Samples: 94725
LRB-V8447 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 10:370.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/07/21 10:370.0050.0009<0.0009mg/KgTetrachloroethene
09/07/21 10:370.0050.0007<0.0007mg/KgToluene
09/07/21 10:370.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/07/21 10:370.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/07/21 10:370.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/07/21 10:370.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/07/21 10:370.0050.0009<0.0009mg/KgTrichloroethene
09/07/21 10:370.0100.002<0.002mg/KgTrichlorofluoromethane
09/07/21 10:370.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/07/21 10:370.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/07/21 10:370.0100.0005<0.0005mg/KgVinyl Acetate
09/07/21 10:370.0100.0005<0.0005mg/KgVinyl Chloride
09/07/21 10:370.0050.0005<0.0005mg/Kgo-Xylene
09/07/21 10:370.0100.001<0.001mg/Kgm,p-Xylene
09/07/21 10:374-Bromofluorobenzene (S)101 70-130
09/07/21 10:37Dibromofluoromethane (S)103 70-130
09/07/21 10:37Toluene-d8 (S)108 76-129
LCS-V8447 LCSD-V8447Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.117 1171140.1140.100mg/KgAcetone 29-198 2.5 20
0.092 92.191.30.0910.100mg/KgAcrolein 70-130 0.8 20
0.097 97.097.10.0970.100mg/KgAcrylonitrile 65-134 0.1 20
0.043 86.689.00.0440.050mg/KgBenzene 74-127 2.7 20
Page 14 of 46Date:10/01/2021 12:25 PM
Page 119 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8448QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V8447
LCS-V8447 LCSD-V8447Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1011020.0510.050mg/KgBromobenzene 73-125 1.3 20
0.045 91.089.20.0440.050mg/KgBromochloromethane 72-134 1.9 20
0.043 87.689.20.0440.050mg/KgBromodichloromethane 75-122 1.8 20
0.052 1041030.0510.050mg/KgBromoform 66-135 1.7 20
0.041 83.489.60.0440.050mg/KgBromomethane 20-180 7.1 20
0.051 1021050.0520.050mg/Kgn-Butylbenzene 65-135 2.8 20
0.050 1001020.0510.050mg/Kgsec-Butyl benzene 66-131 2.3 20
0.050 1001030.0510.050mg/Kgtert-Butyl benzene 67-132 2.7 20
0.042 85.088.40.0440.050mg/KgCarbon Disulfide 61-129 3.9 20
0.042 84.088.20.0440.050mg/KgCarbon Tetrachloride 64-143 4.8 20
0.046 93.093.20.0460.050mg/KgChlorobenzene 74-118 0.2 20
0.049 99.098.40.0490.050mg/KgChlorodibromomethane 73-122 0.6 20
0.044 89.891.60.0450.050mg/KgChloroethane 33-149 1.9 20
0.041 83.286.00.0430.050mg/KgChloroform 73-127 3.3 20
0.046 92.496.20.0480.050mg/KgChloromethane 45-143 4.0 20
0.049 99.61020.0510.050mg/Kg2-Chlorotoluene 67-124 2.5 20
0.050 1001020.0500.050mg/Kg4-Chlorotoluene 71-126 1.5 20
0.046 92.893.60.0460.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.8 20
0.058 1161160.0570.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 0.3 20
0.049 99.099.00.0490.050mg/Kg1,2-Dibromoethane 70-132 0.0 20
0.044 89.889.80.0440.050mg/KgDibromomethane 74-133 0.0 20
0.050 1011010.0500.050mg/Kg1,2-Dichlorobenzene 72-123 0.0 20
0.050 1011010.0500.050mg/Kg1,3-Dichlorobenzene 71-120 0.3 20
0.050 1021020.0500.050mg/Kg1,4-Dichlorobenzene 71-123 0.1 20
0.049 99.41030.0510.050mg/KgDichlorodifluoromethane 26-146 3.9 20
0.043 87.090.00.0450.050mg/Kg1,1-Dichloroethane 74-127 3.3 20
Page 15 of 46Date:10/01/2021 12:25 PM
Page 120 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8448QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V8447
LCS-V8447 LCSD-V8447Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.043 87.488.80.0440.050mg/Kg1,2-Dichloroethane 68-128 1.5 20
0.045 91.494.00.0470.050mg/Kg1,1-Dichloroethene 67-149 2.8 20
0.043 86.888.80.0440.050mg/Kgcis-1,2-Dichloroethene 76-134 2.2 20
0.044 88.290.60.0450.050mg/Kgtrans-1,2-Dichloroethene 73-132 2.6 20
0.044 88.689.60.0440.050mg/Kg1,2-Dichloropropane 73-130 1.1 20
0.048 97.896.80.0480.050mg/Kg1,3-Dichloropropane 75-124 1.0 20
0.042 84.086.80.0430.050mg/Kg2,2-Dichloropropane 50-142 3.2 20
0.042 85.287.80.0430.050mg/Kg1,1-Dichloropropene 71-130 3.0 20
0.043 87.889.20.0440.050mg/Kgcis-1,3-Dichloropropene 71-125 1.5 20
0.044 89.690.60.0450.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.1 20
0.046 92.494.80.0470.050mg/KgEthylbenzene 74-128 2.5 20
0.091 0.0*0.0*0.0910.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.0 20
0.048 97.81000.0500.050mg/KgHexachlorobutadiene 64-125 2.6 20
0.044 88.093.00.0460.050mg/Kgn-Hexane 70-130 5.5 20
0.050 1011110.0550.050mg/Kg2-Hexanone 61-157 8.8 20
0.050 1001030.0510.050mg/KgIsopropylbenzene 68-126 2.5 20
0.050 1011030.0510.050mg/Kg4-Isopropyl toluene 68-129 2.1 20
0.050 1021160.0580.050mg/KgMethyl Ethyl Ketone (MEK)63-149 13.2 20
0.045 90.691.00.0450.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.4 20
0.043 86.887.40.0430.050mg/KgMethylene Chloride 74-129 0.6 20
0.057 1151120.0560.050mg/KgNaphthalene 57-157 2.2 20
0.050 1011040.0510.050mg/Kgn-Propylbenzene 67-130 2.3 20
0.048 96.697.60.0480.050mg/KgStyrene 77-121 1.0 20
0.047 95.096.40.0480.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.4 20
0.055 1101080.0530.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.2 20
0.041 83.886.80.0430.050mg/KgTetrachloroethene 68-130 3.5 20
Page 16 of 46* QC Fail Date:10/01/2021 12:25 PM
Page 121 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8448QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V8447
LCS-V8447 LCSD-V8447Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 85.086.80.0430.050mg/KgToluene 71-129 2.0 20
0.052 1051040.0520.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.9 20
0.052 1051040.0510.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.9 20
0.041 83.887.40.0430.050mg/Kg1,1,1-Trichloroethane 67-131 4.2 20
0.049 98.297.40.0480.050mg/Kg1,1,2-Trichloroethane 70-133 0.8 20
0.042 85.086.80.0430.050mg/KgTrichloroethene 75-133 2.0 20
0.046 92.897.40.0480.050mg/KgTrichlorofluoromethane 44-146 4.8 20
0.054 1081090.0540.050mg/Kg1,2,3-Trichloropropane 60-137 1.1 20
0.050 1001030.0510.050mg/Kg1,3,5-Trimethylbenzene 69-128 2.5 20
0.040 80.477.20.0380.050mg/KgVinyl Acetate 60-140 4.0 20
0.046 92.296.80.0480.050mg/KgVinyl Chloride 48-147 4.8 20
0.047 94.695.40.0470.050mg/Kgo-Xylene 74-126 0.8 20
0.094 94.897.40.0970.100mg/Kgm,p-Xylene 75-124 2.7 20
1031024-Bromofluorobenzene (S)70-130
102102Dibromofluoromethane (S)70-130
109108Toluene-d8 (S)76-129
Page 17 of 46Date:10/01/2021 12:25 PM
Page 122 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8480
Associated Lab Samples: 94722
LRB-V8480 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 10:370.0200.002<0.002mg/KgAcetone
09/07/21 10:370.0200.001<0.001mg/KgAcrolein
09/07/21 10:370.0200.0008<0.0008mg/KgAcrylonitrile
09/07/21 10:370.0050.0006<0.0006mg/KgBenzene
09/07/21 10:370.0050.0005<0.0005mg/KgBromobenzene
09/07/21 10:370.0050.0008<0.0008mg/KgBromochloromethane
09/07/21 10:370.0050.001<0.001mg/KgBromodichloromethane
09/07/21 10:370.0050.001<0.001mg/KgBromoform
09/07/21 10:370.0100.001<0.001mg/KgBromomethane
09/07/21 10:370.0050.0005<0.0005mg/Kgn-Butylbenzene
09/07/21 10:370.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/07/21 10:370.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/07/21 10:370.0050.0006<0.0006mg/KgCarbon Disulfide
09/07/21 10:370.0050.001<0.001mg/KgCarbon Tetrachloride
09/07/21 10:370.0050.0007<0.0007mg/KgChlorobenzene
09/07/21 10:370.0050.0009<0.0009mg/KgChlorodibromomethane
09/07/21 10:370.0100.0009<0.0009mg/KgChloroethane
09/07/21 10:370.0050.001<0.001mg/KgChloroform
09/07/21 10:370.0100.0006<0.0006mg/KgChloromethane
09/07/21 10:370.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/07/21 10:370.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/07/21 10:370.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/07/21 10:370.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/07/21 10:370.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/07/21 10:370.0050.0006<0.0006mg/KgDibromomethane
09/07/21 10:370.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/07/21 10:370.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 18 of 46Date:10/01/2021 12:25 PM
Page 123 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8480
Associated Lab Samples: 94722
LRB-V8480 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 10:370.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/07/21 10:370.0100.001<0.001mg/KgDichlorodifluoromethane
09/07/21 10:370.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/07/21 10:370.0050.001<0.001mg/Kg1,2-Dichloroethane
09/07/21 10:370.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/07/21 10:370.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/07/21 10:370.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/07/21 10:370.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/07/21 10:370.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/07/21 10:370.0050.001<0.001mg/Kg2,2-Dichloropropane
09/07/21 10:370.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/07/21 10:370.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/07/21 10:370.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/07/21 10:370.0050.0006<0.0006mg/KgEthylbenzene
09/07/21 10:370.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/07/21 10:370.0100.0008<0.0008mg/KgHexachlorobutadiene
09/07/21 10:370.0100.0007<0.0007mg/Kgn-Hexane
09/07/21 10:370.0200.0006<0.0006mg/Kg2-Hexanone
09/07/21 10:370.0050.0005<0.0005mg/KgIsopropylbenzene
09/07/21 10:370.0050.001<0.001mg/Kg4-Isopropyl toluene
09/07/21 10:370.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/07/21 10:370.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/07/21 10:370.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/07/21 10:370.0100.001<0.001mg/KgMethylene Chloride
09/07/21 10:370.0100.0010<0.0010mg/KgNaphthalene
09/07/21 10:370.0050.0005<0.0005mg/Kgn-Propylbenzene
09/07/21 10:370.0050.001<0.001mg/KgStyrene
Page 19 of 46Date:10/01/2021 12:25 PM
Page 124 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8480
Associated Lab Samples: 94722
LRB-V8480 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 10:370.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/07/21 10:370.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/07/21 10:370.0050.0009<0.0009mg/KgTetrachloroethene
09/07/21 10:370.0050.0007<0.0007mg/KgToluene
09/07/21 10:370.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/07/21 10:370.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/07/21 10:370.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/07/21 10:370.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/07/21 10:370.0050.0009<0.0009mg/KgTrichloroethene
09/07/21 10:370.0100.002<0.002mg/KgTrichlorofluoromethane
09/07/21 10:370.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/07/21 10:370.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/07/21 10:370.0100.0005<0.0005mg/KgVinyl Acetate
09/07/21 10:370.0100.0005<0.0005mg/KgVinyl Chloride
09/07/21 10:370.0050.0005<0.0005mg/Kgo-Xylene
09/07/21 10:370.0100.001<0.001mg/Kgm,p-Xylene
09/07/21 10:374-Bromofluorobenzene (S)101 70-130
09/07/21 10:37Dibromofluoromethane (S)103 84-123
09/07/21 10:37Toluene-d8 (S)108 76-129
LCS-V8480 LCSD-V8480Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.117 1171140.1140.100mg/KgAcetone 29-198 2.5 20
0.092 92.191.30.0910.100mg/KgAcrolein 70-130 0.8 20
0.097 97.097.10.0970.100mg/KgAcrylonitrile 65-134 0.1 20
Page 20 of 46Date:10/01/2021 12:25 PM
Page 125 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8480
LCS-V8480 LCSD-V8480Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.043 86.689.00.0440.050mg/KgBenzene 74-127 2.7 20
0.050 1011020.0510.050mg/KgBromobenzene 73-125 1.3 20
0.045 91.089.20.0440.050mg/KgBromochloromethane 72-134 1.9 20
0.043 87.689.20.0440.050mg/KgBromodichloromethane 75-122 1.8 20
0.052 1041030.0510.050mg/KgBromoform 66-135 1.7 20
0.041 83.489.60.0440.050mg/KgBromomethane 20-180 7.1 20
0.051 1021050.0520.050mg/Kgn-Butylbenzene 65-135 2.8 20
0.050 1001020.0510.050mg/Kgsec-Butyl benzene 66-131 2.3 20
0.050 1001030.0510.050mg/Kgtert-Butyl benzene 67-132 2.7 20
0.042 85.088.40.0440.050mg/KgCarbon Disulfide 61-129 3.9 20
0.042 84.088.20.0440.050mg/KgCarbon Tetrachloride 64-143 4.8 20
0.046 93.093.20.0460.050mg/KgChlorobenzene 74-118 0.2 20
0.049 99.098.40.0490.050mg/KgChlorodibromomethane 73-122 0.6 20
0.044 89.891.60.0450.050mg/KgChloroethane 33-149 1.9 20
0.041 83.286.00.0430.050mg/KgChloroform 73-127 3.3 20
0.046 92.496.20.0480.050mg/KgChloromethane 45-143 4.0 20
0.049 99.61020.0510.050mg/Kg2-Chlorotoluene 67-124 2.5 20
0.050 1001020.0500.050mg/Kg4-Chlorotoluene 71-126 1.5 20
0.046 92.893.60.0460.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.8 20
0.058 1161160.0570.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 0.3 20
0.049 99.099.00.0490.050mg/Kg1,2-Dibromoethane 70-132 0.0 20
0.044 89.889.80.0440.050mg/KgDibromomethane 74-133 0.0 20
0.050 1011010.0500.050mg/Kg1,2-Dichlorobenzene 72-123 0.0 20
0.050 1011010.0500.050mg/Kg1,3-Dichlorobenzene 71-120 0.3 20
0.050 1021020.0500.050mg/Kg1,4-Dichlorobenzene 71-123 0.1 20
0.049 99.41030.0510.050mg/KgDichlorodifluoromethane 26-146 3.9 20
Page 21 of 46Date:10/01/2021 12:25 PM
Page 126 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8480
LCS-V8480 LCSD-V8480Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.043 87.090.00.0450.050mg/Kg1,1-Dichloroethane 74-127 3.3 20
0.043 87.488.80.0440.050mg/Kg1,2-Dichloroethane 68-128 1.5 20
0.045 91.494.00.0470.050mg/Kg1,1-Dichloroethene 67-149 2.8 20
0.043 86.888.80.0440.050mg/Kgcis-1,2-Dichloroethene 76-134 2.2 20
0.044 88.290.60.0450.050mg/Kgtrans-1,2-Dichloroethene 73-132 2.6 20
0.044 88.689.60.0440.050mg/Kg1,2-Dichloropropane 73-130 1.1 20
0.048 97.896.80.0480.050mg/Kg1,3-Dichloropropane 75-124 1.0 20
0.042 84.086.80.0430.050mg/Kg2,2-Dichloropropane 50-142 3.2 20
0.042 85.287.80.0430.050mg/Kg1,1-Dichloropropene 71-130 3.0 20
0.043 87.889.20.0440.050mg/Kgcis-1,3-Dichloropropene 71-125 1.5 20
0.044 89.690.60.0450.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.1 20
0.046 92.494.80.0470.050mg/KgEthylbenzene 74-128 2.5 20
0.091 91.391.80.0910.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.5 20
0.048 97.81000.0500.050mg/KgHexachlorobutadiene 64-125 2.6 20
0.044 88.093.00.0460.050mg/Kgn-Hexane 70-130 5.5 20
0.050 1011110.0550.050mg/Kg2-Hexanone 61-157 8.8 20
0.050 1001030.0510.050mg/KgIsopropylbenzene 68-126 2.5 20
0.050 1011030.0510.050mg/Kg4-Isopropyl toluene 68-129 2.1 20
0.050 1021160.0580.050mg/KgMethyl Ethyl Ketone (MEK)63-149 13.2 20
0.045 90.691.00.0450.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.4 20
0.051 1021020.0500.050mg/Kg4-Methyl-2-Pentanone 57-162 0.3 20
0.043 86.887.40.0430.050mg/KgMethylene Chloride 74-129 0.6 20
0.057 1151120.0560.050mg/KgNaphthalene 57-157 2.2 20
0.050 1011040.0510.050mg/Kgn-Propylbenzene 67-130 2.3 20
0.048 96.697.60.0480.050mg/KgStyrene 77-121 1.0 20
0.047 95.096.40.0480.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.4 20
Page 22 of 46Date:10/01/2021 12:25 PM
Page 127 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8480
LCS-V8480 LCSD-V8480Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.055 1101080.0530.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.2 20
0.041 83.886.80.0430.050mg/KgTetrachloroethene 68-130 3.5 20
0.042 85.086.80.0430.050mg/KgToluene 71-129 2.0 20
0.052 1051040.0520.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.9 20
0.052 1051040.0510.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.9 20
0.041 83.887.40.0430.050mg/Kg1,1,1-Trichloroethane 67-131 4.2 20
0.049 98.297.40.0480.050mg/Kg1,1,2-Trichloroethane 70-133 0.8 20
0.042 85.086.80.0430.050mg/KgTrichloroethene 75-133 2.0 20
0.046 92.897.40.0480.050mg/KgTrichlorofluoromethane 44-146 4.8 20
0.054 1081090.0540.050mg/Kg1,2,3-Trichloropropane 60-137 1.1 20
0.050 1001030.0510.050mg/Kg1,3,5-Trimethylbenzene 69-128 2.5 20
0.040 80.477.20.0380.050mg/KgVinyl Acetate 60-140 4.0 20
0.046 92.296.80.0480.050mg/KgVinyl Chloride 48-147 4.8 20
0.047 94.695.40.0470.050mg/Kgo-Xylene 74-126 0.8 20
0.094 94.897.40.0970.100mg/Kgm,p-Xylene 75-124 2.7 20
1031024-Bromofluorobenzene (S)70-130
102102Dibromofluoromethane (S)84-123
109108Toluene-d8 (S)76-129
Page 23 of 46Date:10/01/2021 12:25 PM
Page 128 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8614QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V8613
Associated Lab Samples: 94717, 94718, 94719, 94720, 94721
LRB-V8613 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/10/21 03:335.001.80<1.80µg/LAcetone
09/10/21 03:335.002.00<2.00µg/LAcrolein
09/10/21 03:335.000.230<0.230µg/LAcrylonitrile
09/10/21 03:330.5000.180<0.180µg/LBenzene
09/10/21 03:330.5000.210<0.210µg/LBromobenzene
09/10/21 03:331.000.420<0.420µg/LBromochloromethane
09/10/21 03:330.5000.160<0.160µg/LBromodichloromethane
09/10/21 03:335.001.50<1.50µg/LBromoform
09/10/21 03:331.000.280<0.280µg/LBromomethane
09/10/21 03:331.000.185<0.185µg/Ln-Butylbenzene
09/10/21 03:330.5000.200<0.200µg/Lsec-Butyl benzene
09/10/21 03:332.000.920<0.920µg/Ltert-Butyl benzene
09/10/21 03:335.000.150<0.150µg/LCarbon Disulfide
09/10/21 03:330.5000.180<0.180µg/LCarbon Tetrachloride
09/10/21 03:330.5000.190<0.190µg/LChlorobenzene
09/10/21 03:330.5000.190<0.190µg/LChlorodibromomethane
09/10/21 03:331.000.430<0.430µg/LChloroethane
09/10/21 03:330.5000.220<0.220µg/LChloroform
09/10/21 03:330.5000.220<0.220µg/LChloromethane
09/10/21 03:330.5000.200<0.200µg/L2-Chlorotoluene
09/10/21 03:330.5000.200<0.200µg/L4-Chlorotoluene
09/10/21 03:335.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
09/10/21 03:332.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
09/10/21 03:330.5000.200<0.200µg/L1,2-Dibromoethane
09/10/21 03:330.5000.230<0.230µg/LDibromomethane
09/10/21 03:330.5000.220<0.220µg/L1,2-Dichlorobenzene
09/10/21 03:330.5000.190<0.190µg/L1,3-Dichlorobenzene
Page 24 of 46Date:10/01/2021 12:25 PM
Page 129 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8614QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V8613
Associated Lab Samples: 94717, 94718, 94719, 94720, 94721
LRB-V8613 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/10/21 03:330.5000.210<0.210µg/L1,4-Dichlorobenzene
09/10/21 03:335.001.20<1.20µg/LDichlorodifluoromethane
09/10/21 03:330.5000.240<0.240µg/L1,1-Dichloroethane
09/10/21 03:330.5000.150<0.150µg/L1,2-Dichloroethane
09/10/21 03:330.5000.150<0.150µg/L1,1-Dichloroethene
09/10/21 03:330.5000.200<0.200µg/Lcis-1,2-Dichloroethene
09/10/21 03:330.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
09/10/21 03:330.5000.190<0.190µg/L1,2-Dichloropropane
09/10/21 03:330.5000.130<0.130µg/L1,3-Dichloropropane
09/10/21 03:332.000.210<0.210µg/L2,2-Dichloropropane
09/10/21 03:330.5000.200<0.200µg/L1,1-Dichloropropene
09/10/21 03:330.5000.210<0.210µg/Lcis-1,3-Dichloropropene
09/10/21 03:330.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
09/10/21 03:330.5000.170<0.170µg/LEthylbenzene
09/10/21 03:3310.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
09/10/21 03:332.000.350<0.350µg/LHexachlorobutadiene
09/10/21 03:3310.01.30<1.30µg/Ln-Hexane
09/10/21 03:335.000.380<0.380µg/L2-Hexanone
09/10/21 03:335.000.180<0.180µg/LIsopropylbenzene
09/10/21 03:330.5000.089<0.089µg/L4-Isopropyl toluene
09/10/21 03:335.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
09/10/21 03:330.5000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
09/10/21 03:335.001.00<1.00µg/L4-Methyl-2-Pentanone
09/10/21 03:331.000.330<0.330µg/LMethylene Chloride
09/10/21 03:331.000.470<0.470µg/LNaphthalene
09/10/21 03:330.5000.190<0.190µg/Ln-Propylbenzene
09/10/21 03:330.5000.220<0.220µg/LStyrene
Page 25 of 46Date:10/01/2021 12:25 PM
Page 130 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8614QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V8613
Associated Lab Samples: 94717, 94718, 94719, 94720, 94721
LRB-V8613 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/10/21 03:330.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
09/10/21 03:330.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
09/10/21 03:330.5000.220<0.220µg/LTetrachloroethene
09/10/21 03:330.5000.220<0.220µg/LToluene
09/10/21 03:332.000.380<0.380µg/L1,2,3-Trichlorobenzene
09/10/21 03:331.000.310<0.310µg/L1,2,4-Trichlorobenzene
09/10/21 03:330.5000.160<0.160µg/L1,1,1-Trichloroethane
09/10/21 03:330.5000.096<0.096µg/L1,1,2-Trichloroethane
09/10/21 03:330.5000.180<0.180µg/LTrichloroethene
09/10/21 03:330.5000.180<0.180µg/LTrichlorofluoromethane
09/10/21 03:331.000.270<0.270µg/L1,2,3-Trichloropropane
09/10/21 03:330.5000.180<0.180µg/L1,3,5-Trimethylbenzene
09/10/21 03:332.001.00<1.00µg/LVinyl Acetate
09/10/21 03:330.5000.170<0.170µg/LVinyl Chloride
09/10/21 03:330.5000.210<0.210µg/Lo-Xylene
09/10/21 03:331.000.420<0.420µg/Lm,p-Xylene
09/10/21 03:334-Bromofluorobenzene (S)105 80-124
09/10/21 03:33Dibromofluoromethane (S)103 75-129
09/10/21 03:331,2-Dichloroethane - d4 (S)96.2 63-136
09/10/21 03:33Toluene-d8 (S)99.6 77-123
LCS-V8613 LCSD-V8613Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
50.1 12513152.240.0µg/LAcetone 40-166 4.1 20.0
36.9 92.290.536.240.0µg/LAcrolein 70-130 1.9 20.0
Page 26 of 46Date:10/01/2021 12:25 PM
Page 131 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8614QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V8613
LCS-V8613 LCSD-V8613Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
41.3 10399.239.740.0µg/LAcrylonitrile 81-127 3.9 20.0
18.4 92.093.518.720.0µg/LBenzene 77-128 1.6 20.0
17.2 86.084.016.820.0µg/LBromobenzene 78-129 2.3 20.0
19.1 95.599.019.820.0µg/LBromochloromethane 78-135 3.5 20.0
18.6 93.092.518.520.0µg/LBromodichloromethane 76-138 0.5 20.0
19.3 96.593.518.720.0µg/LBromoform 71-135 3.1 20.0
17.3 86.588.017.620.0µg/LBromomethane 41-168 1.7 20.0
16.4 82.082.016.420.0µg/Ln-Butylbenzene 68-134 0.0 20.0
16.2 81.081.516.320.0µg/Lsec-Butyl benzene 71-131 0.6 20.0
16.7 83.582.516.520.0µg/Ltert-Butyl benzene 70-132 1.2 20.0
15.9 79.581.516.320.0µg/LCarbon Disulfide 59-135 2.4 20.0
17.6 88.087.017.420.0µg/LCarbon Tetrachloride 72-142 1.1 20.0
17.3 86.587.517.520.0µg/LChlorobenzene 78-119 1.1 20.0
19.2 96.094.518.920.0µg/LChlorodibromomethane 75-134 1.5 20.0
18.4 92.093.518.720.0µg/LChloroethane 57-142 1.6 20.0
18.3 91.590.018.020.0µg/LChloroform 77-130 1.6 20.0
16.2 81.081.016.220.0µg/LChloromethane 47-145 0.0 20.0
17.2 86.084.516.920.0µg/L2-Chlorotoluene 74-126 1.7 20.0
17.2 86.086.017.220.0µg/L4-Chlorotoluene 78-129 0.0 20.0
19.0 95.095.519.120.0µg/LDi-Isopropyl Ether (DIPE)60-154 0.5 20.0
19.0 95.099.019.820.0µg/L1,2-Dibromo-3-Chloropropane 63-134 4.1 20.0
18.8 94.095.519.120.0µg/L1,2-Dibromoethane 77-135 1.5 20.0
19.0 95.095.519.120.0µg/LDibromomethane 76-138 0.5 20.0
16.9 84.585.017.020.0µg/L1,2-Dichlorobenzene 78-128 0.5 20.0
16.3 81.582.016.420.0µg/L1,3-Dichlorobenzene 77-125 0.6 20.0
16.2 81.081.016.220.0µg/L1,4-Dichlorobenzene 75-126 0.0 20.0
Page 27 of 46Date:10/01/2021 12:25 PM
Page 132 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8614QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V8613
LCS-V8613 LCSD-V8613Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
15.3 76.579.515.920.0µg/LDichlorodifluoromethane 28-163 3.8 20.0
18.4 92.092.018.420.0µg/L1,1-Dichloroethane 70-130 0.0 20.0
17.6 88.088.517.720.0µg/L1,2-Dichloroethane 68-131 0.5 20.0
18.3 91.593.518.720.0µg/L1,1-Dichloroethene 70-154 2.1 20.0
18.7 93.593.018.620.0µg/Lcis-1,2-Dichloroethene 76-141 0.5 20.0
17.7 88.589.517.920.0µg/Ltrans-1,2-Dichloroethene 76-135 1.1 20.0
18.7 93.595.519.120.0µg/L1,2-Dichloropropane 77-130 2.1 20.0
18.8 94.094.518.920.0µg/L1,3-Dichloropropane 76-132 0.5 20.0
14.9 74.582.516.520.0µg/L2,2-Dichloropropane 29-149 10.1 20.0
18.4 92.092.518.520.0µg/L1,1-Dichloropropene 71-136 0.5 20.0
18.7 93.591.018.220.0µg/Lcis-1,3-Dichloropropene 65-140 2.7 20.0
18.7 93.591.018.220.0µg/Ltrans-1,3-Dichloropropene 67-140 2.7 20.0
16.9 84.584.016.820.0µg/LEthylbenzene 80-127 0.5 20.0
38.7 96.797.739.140.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 1.0 20.0
18.1 90.589.017.820.0µg/LHexachlorobutadiene 61-134 1.6 20.0
14.8 74.074.014.820.0µg/Ln-Hexane 70-130 0.0 20.0
22.3 11211122.220.0µg/L2-Hexanone 64-137 0.4 20.0
17.3 86.587.017.420.0µg/LIsopropylbenzene 70-130 0.5 20.0
16.2 81.079.515.920.0µg/L4-Isopropyl toluene 69-132 1.8 20.0
20.6 10392.018.420.0µg/LMethyl Ethyl Ketone (MEK)71-134 11.2 20.0
19.1 95.596.019.220.0µg/LMethyl tert-butyl ether (MTBE)68-135 0.5 20.0
19.5 97.595.019.020.0µg/L4-Methyl-2-Pentanone 69-134 2.5 20.0
18.2 91.090.518.120.0µg/LMethylene Chloride 73-131 0.5 20.0
19.9 99.510320.520.0µg/LNaphthalene 64-136 2.9 20.0
16.4 82.081.516.320.0µg/Ln-Propylbenzene 72-132 0.6 20.0
17.7 88.589.017.820.0µg/LStyrene 78-129 0.5 20.0
Page 28 of 46Date:10/01/2021 12:25 PM
Page 133 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8614QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V8613
LCS-V8613 LCSD-V8613Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.5 87.591.518.320.0µg/L1,1,1,2-Tetrachloroethane 79-134 4.4 20.0
16.9 84.587.017.420.0µg/L1,1,2,2-Tetrachloroethane 62-127 2.9 20.0
17.3 86.587.017.420.0µg/LTetrachloroethene 80-129 0.5 20.0
18.2 91.091.018.220.0µg/LToluene 76-131 0.0 20.0
21.1 10610921.820.0µg/L1,2,3-Trichlorobenzene 58-144 3.2 20.0
19.8 99.010320.520.0µg/L1,2,4-Trichlorobenzene 66-139 3.4 20.0
18.2 91.092.518.520.0µg/L1,1,1-Trichloroethane 75-135 1.6 20.0
18.9 94.597.519.520.0µg/L1,1,2-Trichloroethane 70-140 3.1 20.0
19.0 95.093.518.720.0µg/LTrichloroethene 77-133 1.5 20.0
18.0 90.090.018.020.0µg/LTrichlorofluoromethane 62-148 0.0 20.0
17.1 85.590.018.020.0µg/L1,2,3-Trichloropropane 71-127 5.1 20.0
16.5 82.583.516.720.0µg/L1,3,5-Trimethylbenzene 75-131 1.2 20.0
14.8 74.066.513.320.0µg/LVinyl Acetate 34-167 10.6 20.0
17.7 88.587.517.520.0µg/LVinyl Chloride 57-141 1.1 20.0
17.7 88.589.017.820.0µg/Lo-Xylene 78-128 0.5 20.0
35.5 88.789.535.840.0µg/Lm,p-Xylene 77-133 0.8 20.0
1011024-Bromofluorobenzene (S)80-124
102103Dibromofluoromethane (S)75-129
97.297.01,2-Dichloroethane - d4 (S)63-136
100100Toluene-d8 (S)77-123
Page 29 of 46Date:10/01/2021 12:25 PM
Page 134 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8592QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V8443
Associated Lab Samples: 94717, 94718, 94719, 94720, 94721
LRB-V8443 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 19:5720.07.12<7.12µg/LAcenaphthene
09/07/21 19:5720.06.94<6.94µg/LAcenaphthylene
09/07/21 19:5750.07.13<7.13µg/LAniline
09/07/21 19:5710.06.57<6.57µg/LAnthracene
09/07/21 19:5710.05.65<5.65µg/LBenzo(a)anthracene
09/07/21 19:5710.04.67<4.67µg/LBenzo(a)pyrene
09/07/21 19:5710.04.52<4.52µg/LBenzo(b)fluoranthene
09/07/21 19:5710.04.24<4.24µg/LBenzo(g,h,i)perylene
09/07/21 19:5710.04.68<4.68µg/LBenzo(k)fluoranthene
09/07/21 19:5710011.5<11.5µg/LBenzoic Acid
09/07/21 19:5710.08.60<8.60µg/LBenzyl alcohol
09/07/21 19:5710.05.67<5.67µg/LBis(2-Chloroethoxy)methane
09/07/21 19:5710.07.30<7.30µg/LBis(2-Chloroethyl)ether
09/07/21 19:5710.06.59<6.59µg/LBis(2-Chloroisopropyl)ether
09/07/21 19:5710.08.80<8.80µg/LBis(2-ethylhexyl)phthalate
09/07/21 19:5720.06.26<6.26µg/L4-Bromophenyl phenyl ether
09/07/21 19:5710.02.94<2.94µg/LButyl benzyl phthalate
09/07/21 19:5710.05.23<5.23µg/L4-Chloro-3-methylphenol
09/07/21 19:5710.05.42<5.42µg/L4-Chloroaniline
09/07/21 19:5720.07.38<7.38µg/L2-Chloronaphthalene
09/07/21 19:5710.06.58<6.58µg/L2-Chlorophenol
09/07/21 19:5720.06.99<6.99µg/L4-Chlorophenyl phenyl ether
09/07/21 19:5710.05.38<5.38µg/LChrysene
09/07/21 19:5720.06.01<6.01µg/LDibenz(a,h)anthracene
09/07/21 19:5720.05.08<5.08µg/LDibenzofuran
09/07/21 19:5710.05.91<5.91µg/L1,2-Dichlorobenzene
09/07/21 19:5710.05.83<5.83µg/L1,3-Dichlorobenzene
Page 30 of 46Date:10/01/2021 12:25 PM
Page 135 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8592QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V8443
Associated Lab Samples: 94717, 94718, 94719, 94720, 94721
LRB-V8443 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 19:5710.05.91<5.91µg/L1,4-Dichlorobenzene
09/07/21 19:5710.06.60<6.60µg/L3,3'-Dichlorobenzidine
09/07/21 19:5710.05.54<5.54µg/L2,4-Dichlorophenol
09/07/21 19:5720.09.35<9.35µg/LDiethyl phthalate
09/07/21 19:5710.07.82<7.82µg/LDimethyl phthalate
09/07/21 19:5720.010.9<10.9µg/L2,4-Dimethylphenol
09/07/21 19:5710.07.35<7.35µg/LDi-n-butyl phthalate
09/07/21 19:5730.09.92<9.92µg/L4,6-Dinitro-2-methylphenol
09/07/21 19:5730.010.6<10.6µg/L2,4-Dinitrophenol
09/07/21 19:5710.05.20<5.20µg/L2,4-Dinitrotoluene
09/07/21 19:5720.05.90<5.90µg/L2,6-Dinitrotoluene
09/07/21 19:5710.05.01<5.01µg/LDi-n-Octyl Phthalate
09/07/21 19:5710.06.03<6.03µg/LFluoranthene
09/07/21 19:5710.07.27<7.27µg/LFluorene
09/07/21 19:5720.05.75<5.75µg/LHexachlorobenzene
09/07/21 19:5720.05.88<5.88µg/LHexachlorobutadiene
09/07/21 19:5720.05.90<5.90µg/LHexachlorocyclopentadiene
09/07/21 19:5710.05.22<5.22µg/LHexachloroethane
09/07/21 19:5710.06.20<6.20µg/LIndeno(1,2,3-cd)pyrene
09/07/21 19:5710.06.71<6.71µg/LIsophorone
09/07/21 19:5710.07.33<7.33µg/L1-Methylnaphthalene
09/07/21 19:5710.06.92<6.92µg/L2-Methylnaphthalene
09/07/21 19:5710.05.26<5.26µg/L2-Methylphenol
09/07/21 19:5710.02.47<2.47µg/L3&4 Methylphenol
09/07/21 19:5710.07.88<7.88µg/LNaphthalene
09/07/21 19:5710.04.92<4.92µg/L2-Nitroaniline
09/07/21 19:5710.04.55<4.55µg/L3-Nitroaniline
Page 31 of 46Date:10/01/2021 12:25 PM
Page 136 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8592QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V8443
Associated Lab Samples: 94717, 94718, 94719, 94720, 94721
LRB-V8443 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 19:5710.05.10<5.10µg/L4-Nitroaniline
09/07/21 19:5710.07.88<7.88µg/LNitrobenzene
09/07/21 19:5710.05.49<5.49µg/L2-Nitrophenol
09/07/21 19:5710.02.81<2.81µg/L4-Nitrophenol
09/07/21 19:5710.06.49<6.49µg/LN-Nitrosodimethylamine
09/07/21 19:5720.010.9<10.9µg/LN-Nitrosodiphenylamine
09/07/21 19:5720.08.10<8.10µg/LN-Nitroso-di-n-propylamine
09/07/21 19:5750.09.73<9.73µg/LPentachlorophenol
09/07/21 19:5710.06.34<6.34µg/LPhenanthrene
09/07/21 19:5710.02.86<2.86µg/LPhenol
09/07/21 19:5710.05.42<5.42µg/LPyrene
09/07/21 19:5710.05.32<5.32µg/LPyridine
09/07/21 19:5710.06.25<6.25µg/L1,2,4-Trichlorobenzene
09/07/21 19:5720.05.81<5.81µg/L2,4,5-Trichlorophenol
09/07/21 19:5720.06.29<6.29µg/L2,4,6-Trichlorophenol
09/07/21 19:572-Fluorobiphenyl (S)88.4 44-119
09/07/21 19:572-Fluorophenol (S)44.4 19-119
09/07/21 19:57Nitrobenzene-d5 (S)78.2 44-120
09/07/21 19:574-Terphenyl-d14 (S)108 50-134
09/07/21 19:572,4,6-Tribromophenol (S)105 43-140
09/07/21 19:57Phenol-d5 (S)30.3 11-100
LCS-V8443Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
91.245.650.0µg/LAcenaphthene 38-117
93.846.950.0µg/LAcenaphthylene 41-130
Page 32 of 46Date:10/01/2021 12:25 PM
Page 137 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8592QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V8443
LCS-V8443Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
0.0*34.050.0µg/LAniline 12-197
97.048.550.0µg/LAnthracene 57-123
96.648.350.0µg/LBenzo(a)anthracene 58-125
11255.950.0µg/LBenzo(a)pyrene 54-128
10552.450.0µg/LBenzo(b)fluoranthene 53-131
96.248.150.0µg/LBenzo(g,h,i)perylene 50-134
92.846.450.0µg/LBenzo(k)fluoranthene 53-131
0.0*14.150.0µg/LBenzoic Acid 10-125
64.632.350.0µg/LBenzyl alcohol 31-112
94.247.150.0µg/LBis(2-Chloroethoxy)methane 48-120
72.036.050.0µg/LBis(2-Chloroethyl)ether 43-118
72.836.450.0µg/LBis(2-Chloroisopropyl)ether 37-130
12160.650.0µg/LBis(2-ethylhexyl)phthalate 55-135
92.646.350.0µg/L4-Bromophenyl phenyl ether 55-124
11055.150.0µg/LButyl benzyl phthalate 53-134
93.046.550.0µg/L4-Chloro-3-methylphenol 52-119
73.436.750.0µg/L4-Chloroaniline 33-117
87.843.950.0µg/L2-Chloronaphthalene 40-116
72.036.050.0µg/L2-Chlorophenol 38-117
93.646.850.0µg/L4-Chlorophenyl phenyl ether 53-121
99.849.950.0µg/LChrysene 59-123
73.436.750.0µg/LDibenz(a,h)anthracene 51-134
92.446.250.0µg/LDibenzofuran 53-118
71.235.650.0µg/L1,2-Dichlorobenzene 32-111
69.034.550.0µg/L1,3-Dichlorobenzene 28-110
67.033.550.0µg/L1,4-Dichlorobenzene 29-112
10452.050.0µg/L3,3'-Dichlorobenzidine 27-129
Page 33 of 46* QC Fail Date:10/01/2021 12:25 PM
Page 138 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8592QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V8443
LCS-V8443Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
90.445.250.0µg/L2,4-Dichlorophenol 47-121
10050.250.0µg/LDiethyl phthalate 56-125
94.047.050.0µg/LDimethyl phthalate 45-127
90.045.050.0µg/L2,4-Dimethylphenol 31-124
11356.450.0µg/LDi-n-butyl phthalate 59-127
86.243.150.0µg/L4,6-Dinitro-2-methylphenol 44-137
79.439.750.0µg/L2,4-Dinitrophenol 23-143
10050.050.0µg/L2,4-Dinitrotoluene 57-128
10251.250.0µg/L2,6-Dinitrotoluene 57-124
11256.050.0µg/LDi-n-Octyl Phthalate 51-140
97.648.850.0µg/LFluoranthene 57-128
95.847.950.0µg/LFluorene 52-124
93.046.550.0µg/LHexachlorobenzene 53-125
76.638.350.0µg/LHexachlorobutadiene 22-124
61.630.850.0µg/LHexachlorocyclopentadiene 32-117
67.633.850.0µg/LHexachloroethane 21-115
94.847.450.0µg/LIndeno(1,2,3-cd)pyrene 52-134
71.035.550.0µg/LIsophorone 42-124
83.241.650.0µg/L1-Methylnaphthalene 41-119
84.842.450.0µg/L2-Methylnaphthalene 40-121
73.036.550.0µg/L2-Methylphenol 30-117
56.228.150.0µg/L3&4 Methylphenol 29-110
79.039.550.0µg/LNaphthalene 40-121
97.248.650.0µg/L2-Nitroaniline 55-127
87.043.550.0µg/L3-Nitroaniline 41-128
98.849.450.0µg/L4-Nitroaniline 45-135
75.437.750.0µg/LNitrobenzene 45-121
Page 34 of 46Date:10/01/2021 12:25 PM
Page 139 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8592QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V8443
LCS-V8443Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
79.439.750.0µg/L2-Nitrophenol 47-123
47.423.750.0µg/L4-Nitrophenol 10-105
36.218.150.0µg/LN-Nitrosodimethylamine 10-119
11657.950.0µg/LN-Nitrosodiphenylamine 51-123
77.838.950.0µg/LN-Nitroso-di-n-propylamine 49-119
0.0*49.050.0µg/LPentachlorophenol 35-138
98.649.350.0µg/LPhenanthrene 59-120
27.213.650.0µg/LPhenol 12-58
10150.650.0µg/LPyrene 57-126
35.417.750.0µg/LPyridine 10-80
74.637.350.0µg/L1,2,4-Trichlorobenzene 29-126
88.844.450.0µg/L2,4,5-Trichlorophenol 53-123
91.245.650.0µg/L2,4,6-Trichlorophenol 50-125
86.82-Fluorobiphenyl (S)44-119
41.52-Fluorophenol (S)19-119
74.6Nitrobenzene-d5 (S)44-120
1034-Terphenyl-d14 (S)50-134
1042,4,6-Tribromophenol (S)43-140
29.9Phenol-d5 (S)11-100
Page 35 of 46* QC Fail Date:10/01/2021 12:25 PM
Page 140 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8596QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8456
Associated Lab Samples: 94722, 94723, 94724, 94725, 94726
LRB-V8456 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 15:510.6600.116<0.116mg/KgAcenaphthene
09/07/21 15:510.6600.105<0.105mg/KgAcenaphthylene
09/07/21 15:510.6600.152<0.152mg/KgAniline
09/07/21 15:510.6600.143<0.143mg/KgAnthracene
09/07/21 15:510.6600.139<0.139mg/KgBenzo(a)anthracene
09/07/21 15:510.6600.147<0.147mg/KgBenzo(a)pyrene
09/07/21 15:510.6600.146<0.146mg/KgBenzo(b)fluoranthene
09/07/21 15:510.6600.136<0.136mg/KgBenzo(g,h,i)perylene
09/07/21 15:510.6600.137<0.137mg/KgBenzo(k)fluoranthene
09/07/21 15:512.000.580<0.580mg/KgBenzoic Acid
09/07/21 15:510.6600.105<0.105mg/KgBenzyl alcohol
09/07/21 15:510.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
09/07/21 15:510.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
09/07/21 15:510.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
09/07/21 15:510.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
09/07/21 15:510.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
09/07/21 15:510.3300.113<0.113mg/KgButyl benzyl phthalate
09/07/21 15:510.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
09/07/21 15:510.3300.112<0.112mg/Kg4-Chloroaniline
09/07/21 15:510.6600.116<0.116mg/Kg2-Chloronaphthalene
09/07/21 15:510.6600.098<0.098mg/Kg2-Chlorophenol
09/07/21 15:511.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
09/07/21 15:510.6600.142<0.142mg/KgChrysene
09/07/21 15:510.6600.230<0.230mg/KgDibenz(a,h)anthracene
09/07/21 15:510.6600.119<0.119mg/KgDibenzofuran
09/07/21 15:510.6600.094<0.094mg/Kg1,2-Dichlorobenzene
09/07/21 15:510.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 36 of 46Date:10/01/2021 12:25 PM
Page 141 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8596QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8456
Associated Lab Samples: 94722, 94723, 94724, 94725, 94726
LRB-V8456 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 15:510.3300.097<0.097mg/Kg1,4-Dichlorobenzene
09/07/21 15:510.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
09/07/21 15:510.6600.095<0.095mg/Kg2,4-Dichlorophenol
09/07/21 15:510.6600.180<0.180mg/KgDiethyl phthalate
09/07/21 15:510.6600.174<0.174mg/KgDimethyl phthalate
09/07/21 15:510.3300.108<0.108mg/Kg2,4-Dimethylphenol
09/07/21 15:510.6600.107<0.107mg/KgDi-n-butyl phthalate
09/07/21 15:511.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
09/07/21 15:511.500.520<0.520mg/Kg2,4-Dinitrophenol
09/07/21 15:510.6600.096<0.096mg/Kg2,4-Dinitrotoluene
09/07/21 15:510.6600.108<0.108mg/Kg2,6-Dinitrotoluene
09/07/21 15:510.3300.143<0.143mg/KgDi-n-Octyl Phthalate
09/07/21 15:510.6600.123<0.123mg/KgFluoranthene
09/07/21 15:510.6600.128<0.128mg/KgFluorene
09/07/21 15:510.6600.106<0.106mg/KgHexachlorobenzene
09/07/21 15:510.6600.097<0.097mg/KgHexachlorobutadiene
09/07/21 15:510.6600.157<0.157mg/KgHexachlorocyclopentadiene
09/07/21 15:510.6600.079<0.079mg/KgHexachloroethane
09/07/21 15:510.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
09/07/21 15:510.6600.191<0.191mg/KgIsophorone
09/07/21 15:510.6600.106<0.106mg/Kg1-Methylnaphthalene
09/07/21 15:510.6600.100<0.100mg/Kg2-Methylnaphthalene
09/07/21 15:510.6600.097<0.097mg/Kg2-Methylphenol
09/07/21 15:510.6600.084<0.084mg/Kg3&4 Methylphenol
09/07/21 15:510.6600.144<0.144mg/KgNaphthalene
09/07/21 15:510.6600.096<0.096mg/Kg2-Nitroaniline
09/07/21 15:510.6600.120<0.120mg/Kg3-Nitroaniline
Page 37 of 46Date:10/01/2021 12:25 PM
Page 142 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8596QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8456
Associated Lab Samples: 94722, 94723, 94724, 94725, 94726
LRB-V8456 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 15:510.3300.093<0.093mg/Kg4-Nitroaniline
09/07/21 15:510.3300.116<0.116mg/KgNitrobenzene
09/07/21 15:510.6600.088<0.088mg/Kg2-Nitrophenol
09/07/21 15:510.6600.117<0.117mg/Kg4-Nitrophenol
09/07/21 15:510.6600.263<0.263mg/KgN-Nitrosodimethylamine
09/07/21 15:510.6600.181<0.181mg/KgN-Nitrosodiphenylamine
09/07/21 15:510.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
09/07/21 15:511.000.347<0.347mg/KgPentachlorophenol
09/07/21 15:510.6600.208<0.208mg/KgPhenanthrene
09/07/21 15:510.6600.112<0.112mg/KgPhenol
09/07/21 15:510.6600.134<0.134mg/KgPyrene
09/07/21 15:510.3300.079<0.079mg/KgPyridine
09/07/21 15:510.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
09/07/21 15:510.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
09/07/21 15:510.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
09/07/21 15:512-Fluorobiphenyl (S)85.6 44-115
09/07/21 15:512-Fluorophenol (S)85.5 35-115
09/07/21 15:51Nitrobenzene-d5 (S)78.4 37-122
09/07/21 15:514-Terphenyl-d14 (S)94.6 54-127
09/07/21 15:512,4,6-Tribromophenol (S)97.5 39-132
09/07/21 15:51Phenol-d5 (S)82.5 34-121
LCS-V8456Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
83.81.401.67mg/KgAcenaphthene 40-123
88.61.481.67mg/KgAcenaphthylene 32-132
Page 38 of 46Date:10/01/2021 12:25 PM
Page 143 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8596QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8456
LCS-V8456Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
58.50.9781.67mg/KgAniline 12-197
88.61.481.67mg/KgAnthracene 47-123
88.01.471.67mg/KgBenzo(a)anthracene 49-126
1031.721.67mg/KgBenzo(a)pyrene 45-129
91.61.531.67mg/KgBenzo(b)fluoranthene 45-132
88.61.481.67mg/KgBenzo(g,h,i)perylene 43-134
89.21.491.67mg/KgBenzo(k)fluoranthene 47-132
0.0*1.471.67mg/KgBenzoic Acid 10-83
80.81.351.67mg/KgBenzyl alcohol 29-122
91.01.521.67mg/KgBis(2-Chloroethoxy)methane 36-121
89.21.491.67mg/KgBis(2-Chloroethyl)ether 31-120
73.61.231.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1051.751.67mg/KgBis(2-ethylhexyl)phthalate 51-133
83.81.401.67mg/Kg4-Bromophenyl phenyl ether 46-124
96.41.611.67mg/KgButyl benzyl phthalate 48-132
94.61.581.67mg/Kg4-Chloro-3-methylphenol 45-122
72.41.211.67mg/Kg4-Chloroaniline 17-106
82.01.371.67mg/Kg2-Chloronaphthalene 41-114
80.21.341.67mg/Kg2-Chlorophenol 34-121
88.01.471.67mg/Kg4-Chlorophenyl phenyl ether 45-121
88.01.471.67mg/KgChrysene 50-124
67.61.131.67mg/KgDibenz(a,h)anthracene 45-134
87.41.461.67mg/KgDibenzofuran 44-120
71.21.191.67mg/Kg1,2-Dichlorobenzene 33-117
68.81.151.67mg/Kg1,3-Dichlorobenzene 30-115
68.81.151.67mg/Kg1,4-Dichlorobenzene 31-115
87.41.461.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 39 of 46* QC Fail Date:10/01/2021 12:25 PM
Page 144 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8596QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8456
LCS-V8456Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
88.61.481.67mg/Kg2,4-Dichlorophenol 40-122
92.81.551.67mg/KgDiethyl phthalate 50-124
88.61.481.67mg/KgDimethyl phthalate 48-124
91.61.531.67mg/Kg2,4-Dimethylphenol 30-127
1001.671.67mg/KgDi-n-butyl phthalate 51-128
0.0*1.431.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
0.0*1.491.67mg/Kg2,4-Dinitrophenol 27-129
94.01.571.67mg/Kg2,4-Dinitrotoluene 48-126
95.21.591.67mg/Kg2,6-Dinitrotoluene 46-124
1011.691.67mg/KgDi-n-Octyl Phthalate 45-140
88.61.481.67mg/KgFluoranthene 50-127
89.81.501.67mg/KgFluorene 43-125
86.21.441.67mg/KgHexachlorobenzene 45-122
74.81.251.67mg/KgHexachlorobutadiene 32-123
58.60.9791.67mg/KgHexachlorocyclopentadiene 32-117
71.81.201.67mg/KgHexachloroethane 28-117
89.81.501.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
67.61.131.67mg/KgIsophorone 30-122
81.41.361.67mg/Kg1-Methylnaphthalene 40-119
82.61.381.67mg/Kg2-Methylnaphthalene 38-122
82.61.381.67mg/Kg2-Methylphenol 32-122
73.01.221.67mg/Kg3&4 Methylphenol 34-119
76.61.281.67mg/KgNaphthalene 35-123
90.41.511.67mg/Kg2-Nitroaniline 44-127
85.61.431.67mg/Kg3-Nitroaniline 33-119
92.81.551.67mg/Kg4-Nitroaniline 63-147
73.61.231.67mg/KgNitrobenzene 34-122
Page 40 of 46* QC Fail Date:10/01/2021 12:25 PM
Page 145 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8596QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8456
LCS-V8456Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
79.01.321.67mg/Kg2-Nitrophenol 36-123
1071.791.67mg/Kg4-Nitrophenol 30-132
59.81.001.67mg/KgN-Nitrosodimethylamine 10-146
1051.761.67mg/KgN-Nitrosodiphenylamine 38-127
74.81.251.67mg/KgN-Nitroso-di-n-propylamine 36-120
91.61.531.67mg/KgPentachlorophenol 25-133
89.21.491.67mg/KgPhenanthrene 50-121
73.61.231.67mg/KgPhenol 34-121
90.41.511.67mg/KgPyrene 47-127
41.60.6951.67mg/KgPyridine 10-80
73.61.231.67mg/Kg1,2,4-Trichlorobenzene 34-118
86.21.441.67mg/Kg2,4,5-Trichlorophenol 41-124
85.61.431.67mg/Kg2,4,6-Trichlorophenol 39-126
80.82-Fluorobiphenyl (S)44-115
81.02-Fluorophenol (S)35-115
73.0Nitrobenzene-d5 (S)37-122
91.04-Terphenyl-d14 (S)54-127
94.82,4,6-Tribromophenol (S)39-132
78.9Phenol-d5 (S)34-121
V 94532-MS-V8456 V 94532-MSD-V8456Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.34 80.21.271.671.67<0.116mg/KgAcenaphthene 76.0 40-123 5.3 20
1.39 83.21.321.671.67<0.105mg/KgAcenaphthylene 79.0 32-132 5.1 20
1.13 67.61.111.671.67<0.152mg/KgAniline 66.4 12-197 1.7 20
Page 41 of 46Date:10/01/2021 12:25 PM
Page 146 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8596QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8456
V 94532-MS-V8456 V 94532-MSD-V8456Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.41 84.41.361.671.67<0.143mg/KgAnthracene 81.4 47-123 3.6 20
1.36 81.41.291.671.67<0.139mg/KgBenzo(a)anthracene 77.2 49-126 5.2 20
1.55 92.81.501.671.67<0.147mg/KgBenzo(a)pyrene 89.8 45-129 3.2 20
1.39 83.21.371.671.67<0.146mg/KgBenzo(b)fluoranthene 82.0 45-132 1.4 20
1.36 81.41.311.671.67<0.136mg/KgBenzo(g,h,i)perylene 78.4 43-134 3.7 20
1.33 79.61.251.671.67<0.137mg/KgBenzo(k)fluoranthene 74.8 47-132 6.2 20
1.24 0.0*1.111.671.67<0.580mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.31 78.41.251.671.67<0.105mg/KgBenzyl alcohol 74.8 29-122 4.6 20
1.48 88.61.411.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 84.4 36-121 4.8 20
1.04 62.20.9791.671.67<0.107mg/KgBis(2-Chloroethyl)ether 58.6 31-120 6.0 20
1.19 71.21.141.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 68.2 33-131 4.2 20
1.59 95.21.521.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 91.0 51-133 4.5 20
1.32 79.01.281.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 76.6 46-124 3.0 20
1.50 89.81.421.671.67<0.113mg/KgButyl benzyl phthalate 85.0 48-132 5.4 20
1.43 85.61.351.671.67<0.092mg/Kg4-Chloro-3-methylphenol 80.8 45-122 5.7 20
1.17 70.01.131.671.67<0.112mg/Kg4-Chloroaniline 67.6 17-106 3.4 20
1.32 79.01.241.671.67<0.116mg/Kg2-Chloronaphthalene 74.2 41-114 6.2 20
1.28 76.61.231.671.67<0.098mg/Kg2-Chlorophenol 73.6 34-121 3.9 20
1.35 80.81.271.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 76.0 45-121 6.1 20
1.38 82.61.311.671.67<0.142mg/KgChrysene 78.4 50-124 5.2 20
1.06 63.41.001.671.67<0.230mg/KgDibenz(a,h)anthracene 59.8 45-134 5.8 20
1.34 80.21.281.671.67<0.119mg/KgDibenzofuran 76.6 44-120 4.5 20
1.19 71.21.121.671.67<0.094mg/Kg1,2-Dichlorobenzene 67.0 33-117 6.0 20
1.16 69.41.081.671.67<0.097mg/Kg1,3-Dichlorobenzene 64.6 30-115 7.1 20
1.14 68.21.081.671.67<0.097mg/Kg1,4-Dichlorobenzene 64.6 31-115 5.4 20
1.36 81.41.291.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 77.2 22-121 5.2 20
Page 42 of 46* QC Fail Date:10/01/2021 12:25 PM
Page 147 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8596QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8456
V 94532-MS-V8456 V 94532-MSD-V8456Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.43 85.61.351.671.67<0.095mg/Kg2,4-Dichlorophenol 80.8 40-122 5.7 20
1.39 83.21.341.671.67<0.180mg/KgDiethyl phthalate 80.2 50-124 3.6 20
1.34 80.21.281.671.67<0.174mg/KgDimethyl phthalate 76.6 48-124 4.5 30
1.43 85.61.371.671.67<0.108mg/Kg2,4-Dimethylphenol 82.0 30-127 4.2 20
1.57 94.01.521.671.67<0.107mg/KgDi-n-butyl phthalate 91.0 51-128 3.2 20
1.26 0.0*1.201.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
1.25 0.0*1.161.671.67<0.520mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.43 85.61.341.671.67<0.096mg/Kg2,4-Dinitrotoluene 80.2 48-126 6.4 20
1.43 85.61.361.671.67<0.108mg/Kg2,6-Dinitrotoluene 81.4 46-124 5.0 20
1.52 91.01.491.671.67<0.143mg/KgDi-n-Octyl Phthalate 89.2 45-140 1.9 20
1.40 83.81.341.671.67<0.123mg/KgFluoranthene 80.2 50-127 4.3 20
1.38 82.61.331.671.67<0.128mg/KgFluorene 79.6 43-125 3.6 20
1.36 81.41.291.671.67<0.106mg/KgHexachlorobenzene 77.2 45-122 5.2 20
1.24 74.21.181.671.67<0.097mg/KgHexachlorobutadiene 70.6 32-123 4.9 20
1.02 61.00.9401.671.67<0.157mg/KgHexachlorocyclopentadiene 56.2 32-117 8.1 20
1.14 68.21.071.671.67<0.079mg/KgHexachloroethane 64.0 28-117 6.3 20
1.35 80.81.321.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 79.0 45-133 2.2 20
1.08 64.61.041.671.67<0.191mg/KgIsophorone 62.2 30-122 3.7 20
1.33 79.61.241.671.67<0.106mg/Kg1-Methylnaphthalene 74.2 40-119 7.0 20
1.35 80.81.271.671.67<0.100mg/Kg2-Methylnaphthalene 76.0 38-122 6.1 20
1.33 79.61.261.671.67<0.097mg/Kg2-Methylphenol 75.4 32-122 5.4 20
1.16 69.41.111.671.67<0.084mg/Kg3&4 Methylphenol 66.4 34-119 4.4 20
1.23 73.61.191.671.67<0.144mg/KgNaphthalene 71.2 35-123 3.3 20
1.45 86.81.361.671.67<0.096mg/Kg2-Nitroaniline 81.4 44-127 6.4 20
1.29 77.21.261.671.67<0.120mg/Kg3-Nitroaniline 75.4 33-119 2.3 20
1.47 88.01.351.671.67<0.093mg/Kg4-Nitroaniline 80.8 63-147 8.5 20
Page 43 of 46* QC Fail Date:10/01/2021 12:25 PM
Page 148 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8596QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8456
V 94532-MS-V8456 V 94532-MSD-V8456Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.21 72.41.131.671.67<0.116mg/KgNitrobenzene 67.6 34-122 6.8 20
1.30 77.81.231.671.67<0.088mg/Kg2-Nitrophenol 73.6 32-123 5.5 20
1.61 96.41.541.671.67<0.117mg/Kg4-Nitrophenol 92.2 30-132 4.4 20
0.954 57.10.9161.671.67<0.263mg/KgN-Nitrosodimethylamine 54.8 10-146 4.0 30
1.74 1041.661.671.67<0.181mg/KgN-Nitrosodiphenylamine 99.4 38-127 4.7 20
1.22 73.01.151.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 68.8 36-120 5.9 20
1.42 85.01.361.671.67<0.347mg/KgPentachlorophenol 81.4 25-133 4.3 20
1.43 85.61.371.671.67<0.208mg/KgPhenanthrene 82.0 50-121 4.2 20
1.19 71.21.131.671.67<0.112mg/KgPhenol 67.6 34-121 5.1 20
1.39 83.21.351.671.67<0.134mg/KgPyrene 80.8 47-127 2.9 20
0.699 41.80.7031.671.67<0.079mg/KgPyridine 42.0 10-80 0.5 20
1.21 72.41.131.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 67.6 34-118 6.8 20
1.30 77.81.241.671.67<0.096mg/Kg2,4,5-Trichlorophenol 74.2 41-124 4.7 20
1.36 81.41.281.671.67<0.096mg/Kg2,4,6-Trichlorophenol 76.6 39-126 6.0 20
76.02-Fluorobiphenyl (S)72.4 44-115
77.42-Fluorophenol (S)74.1 35-115
70.0Nitrobenzene-d5 (S)67.0 37-122
82.04-Terphenyl-d14 (S)79.0 54-127
87.02,4,6-Tribromophenol (S)81.6 39-132
75.6Phenol-d5 (S)72.3 34-121
Page 44 of 46Date:10/01/2021 12:25 PM
Page 149 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
Dry Weight Determination
SW-DRYWT
V8412QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94421-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/03/21 17:050.421.121.0%Moisture
V 94729-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/03/21 17:059.716.114.6%Moisture
Page 45 of 46Date:10/01/2021 12:25 PM
Page 150 of 154
Quality Control Data
21-242-0018Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
Dry Weight Determination
SW-DRYWT
V8549QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94692-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/08/21 17:271.314.214.4%Moisture
V 94722-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/08/21 17:270.325.225.3%Moisture
Page 46 of 46Date:10/01/2021 12:25 PM
Page 151 of 154
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-242-0018
NOVA Engineering & Environmental
01151
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 5.4 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:09/02/2021 16:36:36
Special precautions or instructions included?
Comments:
Page 152 of 154
Page 153 of 154
Page 154 of 154

APPENDIX D

SOIL GAS ANALYTICAL

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

9/10/2021
NOVA Engineering & Environmental Steven Aldis
417 Minuet Lane Suite D Charlotte, NC, 28217
Ref: Analytical Testing
Lab Report Number: 21-242-0017 Client Project Description: Doggette Site
Dear Steven Aldis:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/2/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 45
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-242-0017
Page 2 of 45
Report Number:
Sample Summary Table
Client Project Description:
21-242-0017
Doggette Site
Lab No Client Sample ID Matrix Date Collected Date Received
09/01/2021 14:59Air 94709 SV-1 09/02/2021 16:00
09/01/2021 14:03Air 94710 SV-2 09/02/2021 16:00
09/01/2021 12:31Air 94711 SV-3 09/02/2021 16:00
09/01/2021 12:50Air 94712 SV-4 09/02/2021 16:00
09/01/2021 13:30Air 94713 SV-5 09/02/2021 16:00
09/01/2021 13:12Air 94714 SV-6 09/02/2021 16:00
09/01/2021 14:21Air 94715 SV-7 09/02/2021 16:00
09/01/2021Air 94716 DUP-1 09/02/2021 16:00
Page 3 of 45
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-242-0017
Report Limit
Project:Doggette Site
V 94709SV-1
33.4 09/07/2021 17:47TO-15 Acetone µg/m3 0.202
J1.41 09/07/2021 17:47TO-15 Benzene µg/m3 0.0733
J0.380 09/07/2021 17:47TO-15 Carbon Disulfide µg/m3 0.0608
J0.547 09/07/2021 17:47TO-15 Carbon Tetrachloride µg/m3 0.155
J0.747 09/07/2021 17:47TO-15 Chloromethane µg/m3 0.0673
J3.09 09/07/2021 17:47TO-15 Cyclohexane µg/m3 0.161
3.10 09/07/2021 17:47TO-15 Dichlorodifluoromethane µg/m3 0.134
J0.560 09/07/2021 17:47TO-15 Ethylbenzene µg/m3 0.106
J0.613 09/07/2021 17:47TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
J0.680 09/07/2021 17:47TO-15 Heptane µg/m3 0.143
J1.06 09/07/2021 17:47TO-15 n-Hexane µg/m3 0.0472
JB4.88 09/07/2021 17:47TO-15 Isopropyl Alchohol µg/m3 0.139
3.26 09/07/2021 17:47TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J1.12 09/07/2021 17:47TO-15 Methyl tert-butyl ether (MTBE)µg/m3 0.0336
J0.664 09/07/2021 17:47TO-15 4-Methyl-2-Pentanone µg/m3 0.121
J1.01 09/07/2021 17:47TO-15 Methylene Chloride µg/m3 0.489
2.58 09/07/2021 17:47TO-15 Propene µg/m3 0.242
13.1 09/07/2021 17:47TO-15 Styrene µg/m3 0.124
J2.00 09/07/2021 17:47TO-15 Tetrachloroethene µg/m3 0.181
J1.79 09/07/2021 17:47TO-15 Toluene µg/m3 0.0901
J2.43 09/07/2021 17:47TO-15 Trichlorofluoromethane µg/m3 0.130
J0.547 09/07/2021 17:47TO-15 o-Xylene µg/m3 0.157
J1.24 09/07/2021 17:47TO-15 m,p-Xylene µg/m3 0.217
J1.79 09/07/2021 17:47TO-15 Xylene (Total)µg/m3 0.157
V 94710SV-2
138 09/03/2021 17:42TO-15 Acetone µg/m3 4.04
66.5 09/03/2021 17:42TO-15 Benzene µg/m3 1.46
J70.1 09/03/2021 17:42TO-15 Carbon Disulfide µg/m3 1.22
J50.2 09/03/2021 17:42TO-15 Cyclohexane µg/m3 3.22
518 09/03/2021 17:42TO-15 Ethylbenzene µg/m3 2.12
J33.6 09/03/2021 17:42TO-15 4-Ethyltoluene µg/m3 2.56
112 09/03/2021 17:42TO-15 Heptane µg/m3 2.86
46.7 09/03/2021 17:42TO-15 n-Hexane µg/m3 0.943
J14.7 09/03/2021 17:42TO-15 Isopropyl Alchohol µg/m3 2.78
J19.9 09/03/2021 17:42TO-15 Methyl Ethyl Ketone (MEK)µg/m3 4.48
J13.4 09/03/2021 17:42TO-15 4-Methyl-2-Pentanone µg/m3 2.42
Page 4 of 45
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-242-0017
Report Limit
Project:Doggette Site
V 94710SV-2
J11.7 09/03/2021 17:42TO-15 Naphthalene µg/m3 3.66
298 09/03/2021 17:42TO-15 Propene µg/m3 4.84
4330 09/03/2021 17:42TO-15 Tetrachloroethene µg/m3 3.62
J11.0 09/03/2021 17:42TO-15 Tetrahydrofuran µg/m3 2.14
460 09/03/2021 17:42TO-15 Toluene µg/m3 1.80
J32.6 09/03/2021 17:42TO-15 1,2,4-Trimethylbenzene µg/m3 2.20
115 09/03/2021 17:42TO-15 1,3,5-Trimethylbenzene µg/m3 4.72
412 09/03/2021 17:42TO-15 o-Xylene µg/m3 3.14
911 09/03/2021 17:42TO-15 m,p-Xylene µg/m3 4.34
1320 09/03/2021 17:42TO-15 Xylene (Total)µg/m3 3.14
V 94711SV-3
78.3 09/07/2021 18:40TO-15 Acetone µg/m3 0.202
29.1 09/07/2021 18:40TO-15 Benzene µg/m3 0.0733
14.9 09/07/2021 18:40TO-15 Carbon Disulfide µg/m3 0.0608
J0.585 09/07/2021 18:40TO-15 Carbon Tetrachloride µg/m3 0.155
1.37 09/07/2021 18:40TO-15 Chloroethane µg/m3 0.164
J1.87 09/07/2021 18:40TO-15 Chloroform µg/m3 0.0864
J0.599 09/07/2021 18:40TO-15 Chloromethane µg/m3 0.0673
7.48 09/07/2021 18:40TO-15 Cyclohexane µg/m3 0.161
13.7 09/07/2021 18:40TO-15 1,4-Dichlorobenzene µg/m3 0.186
2.78 09/07/2021 18:40TO-15 Dichlorodifluoromethane µg/m3 0.134
2.93 09/07/2021 18:40TO-15 trans-1,2-Dichloroethene µg/m3 0.108
8.08 09/07/2021 18:40TO-15 Ethylbenzene µg/m3 0.106
J0.796 09/07/2021 18:40TO-15 4-Ethyltoluene µg/m3 0.128
5.60 09/07/2021 18:40TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
13.7 09/07/2021 18:40TO-15 Heptane µg/m3 0.143
13.5 09/07/2021 18:40TO-15 n-Hexane µg/m3 0.0472
9.25 09/07/2021 18:40TO-15 Isopropyl Alchohol µg/m3 0.139
12.8 09/07/2021 18:40TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J1.20 09/07/2021 18:40TO-15 Methyl tert-butyl ether (MTBE)µg/m3 0.0336
3.41 09/07/2021 18:40TO-15 4-Methyl-2-Pentanone µg/m3 0.121
J0.973 09/07/2021 18:40TO-15 Methylene Chloride µg/m3 0.489
75.8 09/03/2021 18:20TO-15 Propene µg/m3 4.84
3.48 09/07/2021 18:40TO-15 Styrene µg/m3 0.124
1650 09/03/2021 18:20TO-15 Tetrachloroethene µg/m3 3.62
153 09/03/2021 18:20TO-15 Toluene µg/m3 1.80
Page 5 of 45
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-242-0017
Report Limit
Project:Doggette Site
V 94711SV-3
J1.59 09/07/2021 18:40TO-15 Trichloroethene µg/m3 0.199
12.0 09/07/2021 18:40TO-15 Trichlorofluoromethane µg/m3 0.130
J1.95 09/07/2021 18:40TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J0.826 09/07/2021 18:40TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
J0.828 09/07/2021 18:40TO-15 Vinyl Chloride µg/m3 0.127
6.12 09/07/2021 18:40TO-15 o-Xylene µg/m3 0.157
20.8 09/07/2021 18:40TO-15 m,p-Xylene µg/m3 0.217
26.9 09/07/2021 18:40TO-15 Xylene (Total)µg/m3 0.157
V 94712SV-4
254 09/07/2021 16:53TO-15 Acetone µg/m3 10.1
J34.3 09/07/2021 16:53TO-15 Benzene µg/m3 3.66
J12709/07/2021 16:53TO-15 Carbon Disulfide µg/m3 3.04
1600 09/07/2021 16:53TO-15 Cyclohexane µg/m3 8.05
1210 09/07/2021 16:53TO-15 Ethylbenzene µg/m3 5.32
3800 09/07/2021 16:53TO-15 Heptane µg/m3 7.12
115 09/07/2021 16:53TO-15 n-Hexane µg/m3 2.36
J82.1 09/07/2021 16:53TO-15 Isopropyl Alchohol µg/m3 6.96
J55.6 09/07/2021 16:53TO-15 Methyl Ethyl Ketone (MEK)µg/m3 11.2
360 09/07/2021 16:53TO-15 Propene µg/m3 12.1
1400 09/07/2021 16:53TO-15 Tetrachloroethene µg/m3 9.07
432 09/07/2021 16:53TO-15 Toluene µg/m3 4.50
479 09/07/2021 16:53TO-15 o-Xylene µg/m3 7.88
1170 09/07/2021 16:53TO-15 m,p-Xylene µg/m3 10.8
1650 09/07/2021 16:53TO-15 Xylene (Total)µg/m3 7.88
V 94713SV-5
117 09/03/2021 19:37TO-15 Acetone µg/m3 4.04
J23.3 09/03/2021 19:37TO-15 Benzene µg/m3 1.46
J16.7 09/03/2021 19:37TO-15 Carbon Disulfide µg/m3 1.22
J53.6 09/03/2021 19:37TO-15 Cyclohexane µg/m3 3.22
667 09/03/2021 19:37TO-15 Ethylbenzene µg/m3 2.12
J35.9 09/03/2021 19:37TO-15 4-Ethyltoluene µg/m3 2.56
128 09/03/2021 19:37TO-15 Heptane µg/m3 2.86
J12.3 09/03/2021 19:37TO-15 n-Hexane µg/m3 0.943
J12.2 09/03/2021 19:37TO-15 Isopropyl Alchohol µg/m3 2.78
3020 09/03/2021 19:37TO-15 Tetrachloroethene µg/m3 3.62
367 09/03/2021 19:37TO-15 Toluene µg/m3 1.80
Page 6 of 45
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-242-0017
Report Limit
Project:Doggette Site
V 94713SV-5
J9.33 09/03/2021 19:37TO-15 Trichlorofluoromethane µg/m3 2.60
J29.1 09/03/2021 19:37TO-15 1,2,4-Trimethylbenzene µg/m3 2.20
117 09/03/2021 19:37TO-15 1,3,5-Trimethylbenzene µg/m3 4.72
520 09/03/2021 19:37TO-15 o-Xylene µg/m3 3.14
1130 09/03/2021 19:37TO-15 m,p-Xylene µg/m3 4.34
1650 09/03/2021 19:37TO-15 Xylene (Total)µg/m3 3.14
V 94714SV-6
99.0 09/03/2021 20:15TO-15 Acetone µg/m3 4.04
34.6 09/03/2021 20:15TO-15 Benzene µg/m3 1.46
176 09/03/2021 20:15TO-15 Carbon Disulfide µg/m3 1.22
J16.5 09/03/2021 20:15TO-15 Chloroform µg/m3 1.73
J9.37 09/03/2021 20:15TO-15 Chloromethane µg/m3 1.34
164 09/03/2021 20:15TO-15 Cyclohexane µg/m3 3.22
J12.0 09/03/2021 20:15TO-15 1,4-Dichlorobenzene µg/m3 3.72
1310 09/03/2021 20:15TO-15 Ethylbenzene µg/m3 2.12
J25.0 09/03/2021 20:15TO-15 4-Ethyltoluene µg/m3 2.56
561 09/03/2021 20:15TO-15 Heptane µg/m3 2.86
J34.1 09/03/2021 20:15TO-15 n-Hexane µg/m3 0.943
J11.7 09/03/2021 20:15TO-15 Isopropyl Alchohol µg/m3 2.78
J13.5 09/03/2021 20:15TO-15 Methyl Ethyl Ketone (MEK)µg/m3 4.48
J15.1 09/03/2021 20:15TO-15 Methylene Chloride µg/m3 9.75
179 09/03/2021 20:15TO-15 Propene µg/m3 4.84
2470 09/03/2021 20:15TO-15 Tetrachloroethene µg/m3 3.62
478 09/03/2021 20:15TO-15 Toluene µg/m3 1.80
J9.21 09/03/2021 20:15TO-15 Trichlorofluoromethane µg/m3 2.60
J13.6 09/03/2021 20:15TO-15 1,2,4-Trimethylbenzene µg/m3 2.20
72.8 09/03/2021 20:15TO-15 1,3,5-Trimethylbenzene µg/m3 4.72
819 09/03/2021 20:15TO-15 o-Xylene µg/m3 3.14
1880 09/03/2021 20:15TO-15 m,p-Xylene µg/m3 4.34
2700 09/03/2021 20:15TO-15 Xylene (Total)µg/m3 3.14
V 94715SV-7
J90.1 09/03/2021 20:53TO-15 Acetone µg/m3 4.04
J10.4 09/03/2021 20:53TO-15 Benzene µg/m3 1.46
J8.41 09/03/2021 20:53TO-15 Carbon Disulfide µg/m3 1.22
J32.1 09/03/2021 20:53TO-15 Cyclohexane µg/m3 3.22
409 09/03/2021 20:53TO-15 Ethylbenzene µg/m3 2.12
Page 7 of 45
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-242-0017
Report Limit
Project:Doggette Site
V 94715SV-7
J34.1 09/03/2021 20:53TO-15 4-Ethyltoluene µg/m3 2.56
67.0 09/03/2021 20:53TO-15 Heptane µg/m3 2.86
J14.1 09/03/2021 20:53TO-15 Isopropyl Alchohol µg/m3 2.78
J6.43 09/03/2021 20:53TO-15 Methyl Ethyl Ketone (MEK)µg/m3 4.48
2210 09/03/2021 20:53TO-15 Tetrachloroethene µg/m3 3.62
221 09/03/2021 20:53TO-15 Toluene µg/m3 1.80
J35.6 09/03/2021 20:53TO-15 1,2,4-Trimethylbenzene µg/m3 2.20
116 09/03/2021 20:53TO-15 1,3,5-Trimethylbenzene µg/m3 4.72
349 09/03/2021 20:53TO-15 o-Xylene µg/m3 3.14
745 09/03/2021 20:53TO-15 m,p-Xylene µg/m3 4.34
1090 09/03/2021 20:53TO-15 Xylene (Total)µg/m3 3.14
V 94716DUP-1
119 09/03/2021 21:32TO-15 Acetone µg/m3 4.04
J24.0 09/03/2021 21:32TO-15 Benzene µg/m3 1.46
J17.9 09/03/2021 21:32TO-15 Carbon Disulfide µg/m3 1.22
J58.5 09/03/2021 21:32TO-15 Cyclohexane µg/m3 3.22
710 09/03/2021 21:32TO-15 Ethylbenzene µg/m3 2.12
J37.3 09/03/2021 21:32TO-15 4-Ethyltoluene µg/m3 2.56
165 09/03/2021 21:32TO-15 Heptane µg/m3 2.86
J12.0 09/03/2021 21:32TO-15 n-Hexane µg/m3 0.943
J11.5 09/03/2021 21:32TO-15 Isopropyl Alchohol µg/m3 2.78
J12.5 09/03/2021 21:32TO-15 Methyl Ethyl Ketone (MEK)µg/m3 4.48
3070 09/03/2021 21:32TO-15 Tetrachloroethene µg/m3 3.62
376 09/03/2021 21:32TO-15 Toluene µg/m3 1.80
J31.8 09/03/2021 21:32TO-15 1,2,4-Trimethylbenzene µg/m3 2.20
125 09/03/2021 21:32TO-15 1,3,5-Trimethylbenzene µg/m3 4.72
558 09/03/2021 21:32TO-15 o-Xylene µg/m3 3.14
1210 09/03/2021 21:32TO-15 m,p-Xylene µg/m3 4.34
1770 09/03/2021 21:32TO-15 Xylene (Total)µg/m3 3.14
Page 8 of 45

Client: NOVA Engineering & Environmental CASE NARRATIVE
Project: Doggette Site Lab Report Number: 21-242-0017
Date: 9/9/2021
Volatile Organic Compounds in Air- GC/MS Method TO-15 Sample 94712 (SV-4) Analyte: 4-Bromofluorobenzene
QC Batch No: V8577/V8576 Surrogate(s) was flagged for recovery outside QC limits in this project sample. This sample was re-analyzed for
verification, and/or dilution of target analytes. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.

Page 9 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-1
94709 Matrix:
9/1/2021 14:59
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8576 09/07/21 09:00
33.4 µg/m3 0.202 4.75Acetone 1 09/07/21 17:47 V8577ANG
1.41 J µg/m3 0.0733 1.60Benzene 1 09/07/21 17:47 V8577ANG
<0.148 µg/m3 0.148 10.4Benzyl Chloride 1 09/07/21 17:47 V8577ANG
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 09/07/21 17:47 V8577ANG
<0.153 µg/m3 0.153 5.17Bromoform 1 09/07/21 17:47 V8577ANG
<0.115 µg/m3 0.115 1.94Bromomethane 1 09/07/21 17:47 V8577ANG
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 09/07/21 17:47 V8577ANG
0.380 J µg/m3 0.0608 6.23Carbon Disulfide 1 09/07/21 17:47 V8577ANG
0.547 J
µg/m3 0.155 3.15
Carbon Tetrachloride 1 09/07/21 17:47 V8577ANG
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 09/07/21 17:47 V8577ANG
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 09/07/21 17:47 V8577ANG
<0.164 µg/m3 0.164 1.32Chloroethane 1 09/07/21 17:47 V8577ANG
<0.0864 µg/m3 0.0864 2.44Chloroform 1 09/07/21 17:47 V8577ANG
0.747 J µg/m3 0.0673 1.03Chloromethane 1 09/07/21 17:47 V8577ANG
3.09 J µg/m3 0.161 3.44Cyclohexane 1 09/07/21 17:47 V8577ANG
<0.151 µg/m3 0.151 3.84
1,2-Dibromoethane 1 09/07/21 17:47 V8577ANG
<0.0963 µg/m3 0.0963 3.011,2-Dichlorobenzene 1 09/07/21 17:47 V8577ANG
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 09/07/21 17:47 V8577ANG
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 09/07/21 17:47 V8577ANG
3.10 µg/m3 0.134 2.47Dichlorodifluoromethane 1 09/07/21 17:47 V8577ANG
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 09/07/21 17:47 V8577ANG
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 09/07/21 17:47 V8577ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-1
94709 Matrix:
9/1/2021 14:59
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8576 09/07/21 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 09/07/21 17:47 V8577ANG
<0.0955 µg/m3 0.0955 1.98cis-1,2-Dichloroethene 1 09/07/21 17:47 V8577ANG
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 09/07/21 17:47 V8577ANG
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 09/07/21 17:47 V8577ANG
<0.623 µg/m3 0.623 3.501,2-Dichlorotetrafluoroethane 1 09/07/21 17:47 V8577ANG
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 09/07/21 17:47 V8577ANG
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 09/07/21 17:47 V8577ANG
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 09/07/21 17:47 V8577ANG
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 09/07/21 17:47 V8577ANG
0.560 J µg/m3 0.106 2.17Ethylbenzene 1 09/07/21 17:47 V8577ANG
<0.128 µg/m3 0.128 2.464-Ethyltoluene 1 09/07/21 17:47 V8577ANG
0.613 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 09/07/21 17:47 V8577ANG
0.680 J µg/m3 0.143 2.05Heptane 1 09/07/21 17:47 V8577ANG
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 09/07/21 17:47 V8577ANG
1.06 J µg/m3 0.0472 1.76n-Hexane 1 09/07/21 17:47 V8577ANG
<0.285 µg/m3 0.285 2.05
2-Hexanone 1 09/07/21 17:47 V8577ANG
4.88 JB µg/m3 0.139 4.92Isopropyl Alchohol 1 09/07/21 17:47 V8577ANG
3.26 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 09/07/21 17:47 V8577ANG
1.12 J µg/m3 0.0336 1.80Methyl tert-butyl ether (MTBE)1 09/07/21 17:47 V8577ANG
0.664 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 09/07/21 17:47 V8577ANG
1.01 J µg/m3 0.489 1.74Methylene Chloride 1 09/07/21 17:47 V8577ANG
<0.183 µg/m3 0.183 2.62Naphthalene 1 09/07/21 17:47 V8577ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-1
94709 Matrix:
9/1/2021 14:59
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8576 09/07/21 09:00
2.58 µg/m3 0.242 0.861Propene 1 09/07/21 17:47 V8577ANG
13.1 µg/m3 0.124 2.13Styrene 1 09/07/21 17:47 V8577ANG
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 09/07/21 17:47 V8577ANG
2.00 J µg/m3 0.181 3.39Tetrachloroethene 1 09/07/21 17:47 V8577ANG
<0.107 µg/m3 0.107 1.47Tetrahydrofuran 1 09/07/21 17:47 V8577ANG
1.79 J µg/m3 0.0901 1.88Toluene 1 09/07/21 17:47 V8577ANG
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 09/07/21 17:47 V8577ANG
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 09/07/21 17:47 V8577ANG
<0.0877 µg/m3 0.0877 2.73
1,1,2-Trichloroethane 1 09/07/21 17:47 V8577ANG
<0.199 µg/m3 0.199 2.15Trichloroethene 1 09/07/21 17:47 V8577ANG
2.43 J µg/m3 0.130 2.81Trichlorofluoromethane 1 09/07/21 17:47 V8577ANG
<0.110 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 09/07/21 17:47 V8577ANG
<0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 09/07/21 17:47 V8577ANG
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 09/07/21 17:47 V8577ANG
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 09/07/21 17:47 V8577ANG
0.547 J
µg/m3 0.157 2.17
o-Xylene 1 09/07/21 17:47 V8577ANG
1.24 J µg/m3 0.217 5.65m,p-Xylene 1 09/07/21 17:47 V8577ANG
1.79 J µg/m3 0.157 2.17Xylene (Total)1 09/07/21 17:47 V8577
Surrogate: 4-Bromofluorobenzene 94.7 Limits: 70-130%09/07/21 17:471 ANG V8577
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-2
94710 Matrix:
9/1/2021 14:03
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
138 µg/m3 4.04 95.0Acetone 20 09/03/21 17:42 V8587ANG
66.5 µg/m3 1.46 31.9Benzene 20 09/03/21 17:42 V8587ANG
<2.94 µg/m3 2.94 207Benzyl Chloride 20 09/03/21 17:42 V8587ANG
<3.00 µg/m3 3.00 67.0Bromodichloromethane 20 09/03/21 17:42 V8587ANG
<3.05 µg/m3 3.05 103Bromoform 20 09/03/21 17:42 V8587ANG
<2.30 µg/m3 2.30 38.8Bromomethane 20 09/03/21 17:42 V8587ANG
<6.53 µg/m3 6.53 22.11,3-Butadiene 20 09/03/21 17:42 V8587ANG
70.1 J µg/m3 1.22 125Carbon Disulfide 20 09/03/21 17:42 V8587ANG
<3.10 µg/m3 3.10 62.9
Carbon Tetrachloride 20 09/03/21 17:42 V8587ANG
<2.14 µg/m3 2.14 46.0Chlorobenzene 20 09/03/21 17:42 V8587ANG
<4.16 µg/m3 4.16 85.2Chlorodibromomethane 20 09/03/21 17:42 V8587ANG
<3.28 µg/m3 3.28 26.4Chloroethane 20 09/03/21 17:42 V8587ANG
<1.73 µg/m3 1.73 48.8Chloroform 20 09/03/21 17:42 V8587ANG
<1.34 µg/m3 1.34 20.6Chloromethane 20 09/03/21 17:42 V8587ANG
50.2 J µg/m3 3.22 68.8Cyclohexane 20 09/03/21 17:42 V8587ANG
<3.02 µg/m3 3.02 76.8
1,2-Dibromoethane 20 09/03/21 17:42 V8587ANG
<1.92 µg/m3 1.92 60.11,2-Dichlorobenzene 20 09/03/21 17:42 V8587ANG
<3.48 µg/m3 3.48 2411,3-Dichlorobenzene 20 09/03/21 17:42 V8587ANG
<3.72 µg/m3 3.72 60.11,4-Dichlorobenzene 20 09/03/21 17:42 V8587ANG
<2.68 µg/m3 2.68 49.4Dichlorodifluoromethane 20 09/03/21 17:42 V8587ANG
<2.02 µg/m3 2.02 40.51,1-Dichloroethane 20 09/03/21 17:42 V8587ANG
<2.58 µg/m3 2.58 40.51,2-Dichloroethane 20 09/03/21 17:42 V8587ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-2
94710 Matrix:
9/1/2021 14:03
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
<2.14 µg/m3 2.14 39.61,1-Dichloroethene 20 09/03/21 17:42 V8587ANG
<1.91 µg/m3 1.91 39.6cis-1,2-Dichloroethene 20 09/03/21 17:42 V8587ANG
<2.16 µg/m3 2.16 39.6trans-1,2-Dichloroethene 20 09/03/21 17:42 V8587ANG
<4.10 µg/m3 4.10 46.21,2-Dichloropropane 20 09/03/21 17:42 V8587ANG
<12.4 µg/m3 12.4 69.91,2-Dichlorotetrafluoroethane 20 09/03/21 17:42 V8587ANG
<3.56 µg/m3 3.56 45.4cis-1,3-Dichloropropene 20 09/03/21 17:42 V8587ANG
<3.56 µg/m3 3.56 45.4trans-1,3-Dichloropropene 20 09/03/21 17:42 V8587ANG
<8.69 µg/m3 8.69 36.01,4-Dioxane 20 09/03/21 17:42 V8587ANG
<2.72 µg/m3 2.72 36.0
Ethyl Acetate 20 09/03/21 17:42 V8587ANG
518 µg/m3 2.12 43.4Ethylbenzene 20 09/03/21 17:42 V8587ANG
33.6 J µg/m3 2.56 49.24-Ethyltoluene 20 09/03/21 17:42 V8587ANG
<11.2 µg/m3 11.2 76.61,1,2-Trichloro-1,2,2-trifluoroethane 20 09/03/21 17:42 V8587ANG
112 µg/m3 2.86 41.0Heptane 20 09/03/21 17:42 V8587ANG
<6.62 µg/m3 6.62 107Hexachlorobutadiene 20 09/03/21 17:42 V8587ANG
46.7 µg/m3 0.943 35.2n-Hexane 20 09/03/21 17:42 V8587ANG
<5.71 µg/m3 5.71 41.0
2-Hexanone 20 09/03/21 17:42 V8587ANG
14.7 J µg/m3 2.78 98.3Isopropyl Alchohol 20 09/03/21 17:42 V8587ANG
19.9 J µg/m3 4.48 29.5Methyl Ethyl Ketone (MEK)20 09/03/21 17:42 V8587ANG
<0.673 µg/m3 0.673 36.1Methyl tert-butyl ether (MTBE)20 09/03/21 17:42 V8587ANG
13.4 J µg/m3 2.42 41.04-Methyl-2-Pentanone 20 09/03/21 17:42 V8587ANG
<9.75 µg/m3 9.75 34.7Methylene Chloride 20 09/03/21 17:42 V8587ANG
11.7 J µg/m3 3.66 52.4Naphthalene 20 09/03/21 17:42 V8587ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-2
94710 Matrix:
9/1/2021 14:03
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
298 µg/m3 4.84 17.2Propene 20 09/03/21 17:42 V8587ANG
<2.48 µg/m3 2.48 42.6Styrene 20 09/03/21 17:42 V8587ANG
<2.08 µg/m3 2.08 68.61,1,2,2-Tetrachloroethane 20 09/03/21 17:42 V8587ANG
4330 µg/m3 3.62 67.8Tetrachloroethene 20 09/03/21 17:42 V8587ANG
11.0 J µg/m3 2.14 29.5Tetrahydrofuran 20 09/03/21 17:42 V8587ANG
460 µg/m3 1.80 37.7Toluene 20 09/03/21 17:42 V8587ANG
<4.18 µg/m3 4.18 74.21,2,4-Trichlorobenzene 20 09/03/21 17:42 V8587ANG
<2.88 µg/m3 2.88 54.61,1,1-Trichloroethane 20 09/03/21 17:42 V8587ANG
<1.75 µg/m3 1.75 54.6
1,1,2-Trichloroethane 20 09/03/21 17:42 V8587ANG
<3.98 µg/m3 3.98 43.0Trichloroethene 20 09/03/21 17:42 V8587ANG
<2.60 µg/m3 2.60 56.2Trichlorofluoromethane 20 09/03/21 17:42 V8587ANG
32.6 J µg/m3 2.20 49.21,2,4-Trimethylbenzene 20 09/03/21 17:42 V8587ANG
115 µg/m3 4.72 49.21,3,5-Trimethylbenzene 20 09/03/21 17:42 V8587ANG
<4.48 µg/m3 4.48 35.2Vinyl Acetate 20 09/03/21 17:42 V8587ANG
<2.54 µg/m3 2.54 25.6Vinyl Chloride 20 09/03/21 17:42 V8587ANG
412 µg/m3 3.14 43.4
o-Xylene 20 09/03/21 17:42 V8587ANG
911 µg/m3 4.34 113m,p-Xylene 20 09/03/21 17:42 V8587ANG
1320 µg/m3 3.14 43.4Xylene (Total)20 09/03/21 17:42 V8587
Surrogate: 4-Bromofluorobenzene 74.6 Limits: 70-130%09/03/21 17:4220 ANG V8587
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-3
94711 Matrix:
9/1/2021 12:31
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8576 09/07/21 09:00 V8585 09/03/21 09:00
78.3 µg/m3 0.202 4.75Acetone 1 09/07/21 18:40 V8577ANG
29.1 µg/m3 0.0733 1.60Benzene 1 09/07/21 18:40 V8577ANG
<0.148 µg/m3 0.148 10.4Benzyl Chloride 1 09/07/21 18:40 V8577ANG
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 09/07/21 18:40 V8577ANG
<0.153 µg/m3 0.153 5.17Bromoform 1 09/07/21 18:40 V8577ANG
<0.115 µg/m3 0.115 1.94Bromomethane 1 09/07/21 18:40 V8577ANG
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 09/07/21 18:40 V8577ANG
14.9 µg/m3 0.0608 6.23Carbon Disulfide 1 09/07/21 18:40 V8577ANG
0.585 J
µg/m3 0.155 3.15
Carbon Tetrachloride 1 09/07/21 18:40 V8577ANG
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 09/07/21 18:40 V8577ANG
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 09/07/21 18:40 V8577ANG
1.37 µg/m3 0.164 1.32Chloroethane 1 09/07/21 18:40 V8577ANG
1.87 J µg/m3 0.0864 2.44Chloroform 1 09/07/21 18:40 V8577ANG
0.599 J µg/m3 0.0673 1.03Chloromethane 1 09/07/21 18:40 V8577ANG
7.48 µg/m3 0.161 3.44Cyclohexane 1 09/07/21 18:40 V8577ANG
<0.151 µg/m3 0.151 3.84
1,2-Dibromoethane 1 09/07/21 18:40 V8577ANG
<0.0963 µg/m3 0.0963 3.011,2-Dichlorobenzene 1 09/07/21 18:40 V8577ANG
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 09/07/21 18:40 V8577ANG
13.7 µg/m3 0.186 3.011,4-Dichlorobenzene 1 09/07/21 18:40 V8577ANG
2.78 µg/m3 0.134 2.47Dichlorodifluoromethane 1 09/07/21 18:40 V8577ANG
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 09/07/21 18:40 V8577ANG
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 09/07/21 18:40 V8577ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-3
94711 Matrix:
9/1/2021 12:31
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8576 09/07/21 09:00 V8585 09/03/21 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 09/07/21 18:40 V8577ANG
<0.0955 µg/m3 0.0955 1.98cis-1,2-Dichloroethene 1 09/07/21 18:40 V8577ANG
2.93 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 09/07/21 18:40 V8577ANG
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 09/07/21 18:40 V8577ANG
<0.623 µg/m3 0.623 3.501,2-Dichlorotetrafluoroethane 1 09/07/21 18:40 V8577ANG
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 09/07/21 18:40 V8577ANG
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 09/07/21 18:40 V8577ANG
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 09/07/21 18:40 V8577ANG
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 09/07/21 18:40 V8577ANG
8.08 µg/m3 0.106 2.17Ethylbenzene 1 09/07/21 18:40 V8577ANG
0.796 J µg/m3 0.128 2.464-Ethyltoluene 1 09/07/21 18:40 V8577ANG
5.60 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 09/07/21 18:40 V8577ANG
13.7 µg/m3 0.143 2.05Heptane 1 09/07/21 18:40 V8577ANG
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 09/07/21 18:40 V8577ANG
13.5 µg/m3 0.0472 1.76n-Hexane 1 09/07/21 18:40 V8577ANG
<0.285 µg/m3 0.285 2.05
2-Hexanone 1 09/07/21 18:40 V8577ANG
9.25 µg/m3 0.139 4.92Isopropyl Alchohol 1 09/07/21 18:40 V8577ANG
12.8 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 09/07/21 18:40 V8577ANG
1.20 J µg/m3 0.0336 1.80Methyl tert-butyl ether (MTBE)1 09/07/21 18:40 V8577ANG
3.41 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 09/07/21 18:40 V8577ANG
0.973 J µg/m3 0.489 1.74Methylene Chloride 1 09/07/21 18:40 V8577ANG
<0.183 µg/m3 0.183 2.62Naphthalene 1 09/07/21 18:40 V8577ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-3
94711 Matrix:
9/1/2021 12:31
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8576 09/07/21 09:00 V8585 09/03/21 09:00
75.8 µg/m3 4.84 17.2Propene 20 09/03/21 18:20 V8587ANG
3.48 µg/m3 0.124 2.13Styrene 1 09/07/21 18:40 V8577ANG
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 09/07/21 18:40 V8577ANG
1650 µg/m3 3.62 67.8Tetrachloroethene 20 09/03/21 18:20 V8587ANG
<0.107 µg/m3 0.107 1.47Tetrahydrofuran 1 09/07/21 18:40 V8577ANG
153 µg/m3 1.80 37.7Toluene 20 09/03/21 18:20 V8587ANG
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 09/07/21 18:40 V8577ANG
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 09/07/21 18:40 V8577ANG
<0.0877 µg/m3 0.0877 2.73
1,1,2-Trichloroethane 1 09/07/21 18:40 V8577ANG
1.59 J µg/m3 0.199 2.15Trichloroethene 1 09/07/21 18:40 V8577ANG
12.0 µg/m3 0.130 2.81Trichlorofluoromethane 1 09/07/21 18:40 V8577ANG
1.95 J µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 09/07/21 18:40 V8577ANG
0.826 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 09/07/21 18:40 V8577ANG
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 09/07/21 18:40 V8577ANG
0.828 J µg/m3 0.127 1.28Vinyl Chloride 1 09/07/21 18:40 V8577ANG
6.12 µg/m3 0.157 2.17
o-Xylene 1 09/07/21 18:40 V8577ANG
20.8 µg/m3 0.217 5.65m,p-Xylene 1 09/07/21 18:40 V8577ANG
26.9 µg/m3 0.157 2.17Xylene (Total)1 09/07/21 18:40 V8577
Surrogate: 4-Bromofluorobenzene 93.6 Limits: 70-130%09/07/21 18:401 ANG V8577
Surrogate: 4-Bromofluorobenzene 94.1 Limits: 70-130%09/03/21 18:2020 ANG V8587
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-4
94712 Matrix:
9/1/2021 12:50
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8576 09/07/21 09:00
254 µg/m3 10.1 238Acetone 50 09/07/21 16:53 V8577ANG
34.3 J µg/m3 3.66 79.9Benzene 50 09/07/21 16:53 V8577ANG
<7.35 µg/m3 7.35 518Benzyl Chloride 50 09/07/21 16:53 V8577ANG
<7.52 µg/m3 7.52 168Bromodichloromethane 50 09/07/21 16:53 V8577ANG
<7.64 µg/m3 7.64 258Bromoform 50 09/07/21 16:53 V8577ANG
<5.75 µg/m3 5.75 97.1Bromomethane 50 09/07/21 16:53 V8577ANG
<16.3 µg/m3 16.3 55.31,3-Butadiene 50 09/07/21 16:53 V8577ANG
127 J µg/m3 3.04 311Carbon Disulfide 50 09/07/21 16:53 V8577ANG
<7.74 µg/m3 7.74 157
Carbon Tetrachloride 50 09/07/21 16:53 V8577ANG
<5.35 µg/m3 5.35 115Chlorobenzene 50 09/07/21 16:53 V8577ANG
<10.4 µg/m3 10.4 213Chlorodibromomethane 50 09/07/21 16:53 V8577ANG
<8.20 µg/m3 8.20 66.0Chloroethane 50 09/07/21 16:53 V8577ANG
<4.32 µg/m3 4.32 122Chloroform 50 09/07/21 16:53 V8577ANG
<3.36 µg/m3 3.36 51.6Chloromethane 50 09/07/21 16:53 V8577ANG
1600 µg/m3 8.05 172Cyclohexane 50 09/07/21 16:53 V8577ANG
<7.55 µg/m3 7.55 192
1,2-Dibromoethane 50 09/07/21 16:53 V8577ANG
<4.80 µg/m3 4.80 1501,2-Dichlorobenzene 50 09/07/21 16:53 V8577ANG
<8.70 µg/m3 8.70 6021,3-Dichlorobenzene 50 09/07/21 16:53 V8577ANG
<9.28 µg/m3 9.28 1501,4-Dichlorobenzene 50 09/07/21 16:53 V8577ANG
<6.72 µg/m3 6.72 124Dichlorodifluoromethane 50 09/07/21 16:53 V8577ANG
<5.04 µg/m3 5.04 1011,1-Dichloroethane 50 09/07/21 16:53 V8577ANG
<6.44 µg/m3 6.44 1011,2-Dichloroethane 50 09/07/21 16:53 V8577ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-4
94712 Matrix:
9/1/2021 12:50
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8576 09/07/21 09:00
<5.35 µg/m3 5.35 99.11,1-Dichloroethene 50 09/07/21 16:53 V8577ANG
<4.77 µg/m3 4.77 99.1cis-1,2-Dichloroethene 50 09/07/21 16:53 V8577ANG
<5.40 µg/m3 5.40 99.1trans-1,2-Dichloroethene 50 09/07/21 16:53 V8577ANG
<10.3 µg/m3 10.3 1161,2-Dichloropropane 50 09/07/21 16:53 V8577ANG
<31.1 µg/m3 31.1 1751,2-Dichlorotetrafluoroethane 50 09/07/21 16:53 V8577ANG
<8.86 µg/m3 8.86 113cis-1,3-Dichloropropene 50 09/07/21 16:53 V8577ANG
<8.86 µg/m3 8.86 113trans-1,3-Dichloropropene 50 09/07/21 16:53 V8577ANG
<21.8 µg/m3 21.8 90.11,4-Dioxane 50 09/07/21 16:53 V8577ANG
<6.80 µg/m3 6.80 90.1
Ethyl Acetate 50 09/07/21 16:53 V8577ANG
1210 µg/m3 5.32 109Ethylbenzene 50 09/07/21 16:53 V8577ANG
<6.41 µg/m3 6.41 1234-Ethyltoluene 50 09/07/21 16:53 V8577ANG
<28.1 µg/m3 28.1 1921,1,2-Trichloro-1,2,2-trifluoroethane 50 09/07/21 16:53 V8577ANG
3800 µg/m3 7.12 102Heptane 50 09/07/21 16:53 V8577ANG
<16.5 µg/m3 16.5 267Hexachlorobutadiene 50 09/07/21 16:53 V8577ANG
115 µg/m3 2.36 88.1n-Hexane 50 09/07/21 16:53 V8577ANG
<14.2 µg/m3 14.2 102
2-Hexanone 50 09/07/21 16:53 V8577ANG
82.1 J µg/m3 6.96 246Isopropyl Alchohol 50 09/07/21 16:53 V8577ANG
55.6 J µg/m3 11.2 73.7Methyl Ethyl Ketone (MEK)50 09/07/21 16:53 V8577ANG
<1.68 µg/m3 1.68 90.1Methyl tert-butyl ether (MTBE)50 09/07/21 16:53 V8577ANG
<6.03 µg/m3 6.03 1024-Methyl-2-Pentanone 50 09/07/21 16:53 V8577ANG
<24.4 µg/m3 24.4 86.8Methylene Chloride 50 09/07/21 16:53 V8577ANG
<9.15 µg/m3 9.15 131Naphthalene 50 09/07/21 16:53 V8577ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-4
94712 Matrix:
9/1/2021 12:50
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8576 09/07/21 09:00
360 µg/m3 12.1 43.0Propene 50 09/07/21 16:53 V8577ANG
<6.17 µg/m3 6.17 106Styrene 50 09/07/21 16:53 V8577ANG
<5.21 µg/m3 5.21 1721,1,2,2-Tetrachloroethane 50 09/07/21 16:53 V8577ANG
1400 µg/m3 9.07 170Tetrachloroethene 50 09/07/21 16:53 V8577ANG
<5.35 µg/m3 5.35 73.7Tetrahydrofuran 50 09/07/21 16:53 V8577ANG
432 µg/m3 4.50 94.2Toluene 50 09/07/21 16:53 V8577ANG
<10.5 µg/m3 10.5 1861,2,4-Trichlorobenzene 50 09/07/21 16:53 V8577ANG
<7.18 µg/m3 7.18 1361,1,1-Trichloroethane 50 09/07/21 16:53 V8577ANG
<4.37 µg/m3 4.37 136
1,1,2-Trichloroethane 50 09/07/21 16:53 V8577ANG
<9.91 µg/m3 9.91 107Trichloroethene 50 09/07/21 16:53 V8577ANG
<6.48 µg/m3 6.48 140Trichlorofluoromethane 50 09/07/21 16:53 V8577ANG
<5.50 µg/m3 5.50 1231,2,4-Trimethylbenzene 50 09/07/21 16:53 V8577ANG
<11.8 µg/m3 11.8 1231,3,5-Trimethylbenzene 50 09/07/21 16:53 V8577ANG
<11.2 µg/m3 11.2 88.0Vinyl Acetate 50 09/07/21 16:53 V8577ANG
<6.35 µg/m3 6.35 63.9Vinyl Chloride 50 09/07/21 16:53 V8577ANG
479 µg/m3 7.88 109
o-Xylene 50 09/07/21 16:53 V8577ANG
1170 µg/m3 10.8 282m,p-Xylene 50 09/07/21 16:53 V8577ANG
1650 µg/m3 7.88 109Xylene (Total)50 09/07/21 16:53 V8577
Surrogate: 4-Bromofluorobenzene 60.3 *Limits: 70-130%09/07/21 16:5350 ANG V8577
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-5
94713 Matrix:
9/1/2021 13:30
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
117 µg/m3 4.04 95.0Acetone 20 09/03/21 19:37 V8587ANG
23.3 J µg/m3 1.46 31.9Benzene 20 09/03/21 19:37 V8587ANG
<2.94 µg/m3 2.94 207Benzyl Chloride 20 09/03/21 19:37 V8587ANG
<3.00 µg/m3 3.00 67.0Bromodichloromethane 20 09/03/21 19:37 V8587ANG
<3.05 µg/m3 3.05 103Bromoform 20 09/03/21 19:37 V8587ANG
<2.30 µg/m3 2.30 38.8Bromomethane 20 09/03/21 19:37 V8587ANG
<6.53 µg/m3 6.53 22.11,3-Butadiene 20 09/03/21 19:37 V8587ANG
16.7 J µg/m3 1.22 125Carbon Disulfide 20 09/03/21 19:37 V8587ANG
<3.10 µg/m3 3.10 62.9
Carbon Tetrachloride 20 09/03/21 19:37 V8587ANG
<2.14 µg/m3 2.14 46.0Chlorobenzene 20 09/03/21 19:37 V8587ANG
<4.16 µg/m3 4.16 85.2Chlorodibromomethane 20 09/03/21 19:37 V8587ANG
<3.28 µg/m3 3.28 26.4Chloroethane 20 09/03/21 19:37 V8587ANG
<1.73 µg/m3 1.73 48.8Chloroform 20 09/03/21 19:37 V8587ANG
<1.34 µg/m3 1.34 20.6Chloromethane 20 09/03/21 19:37 V8587ANG
53.6 J µg/m3 3.22 68.8Cyclohexane 20 09/03/21 19:37 V8587ANG
<3.02 µg/m3 3.02 76.8
1,2-Dibromoethane 20 09/03/21 19:37 V8587ANG
<1.92 µg/m3 1.92 60.11,2-Dichlorobenzene 20 09/03/21 19:37 V8587ANG
<3.48 µg/m3 3.48 2411,3-Dichlorobenzene 20 09/03/21 19:37 V8587ANG
<3.72 µg/m3 3.72 60.11,4-Dichlorobenzene 20 09/03/21 19:37 V8587ANG
<2.68 µg/m3 2.68 49.4Dichlorodifluoromethane 20 09/03/21 19:37 V8587ANG
<2.02 µg/m3 2.02 40.51,1-Dichloroethane 20 09/03/21 19:37 V8587ANG
<2.58 µg/m3 2.58 40.51,2-Dichloroethane 20 09/03/21 19:37 V8587ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-5
94713 Matrix:
9/1/2021 13:30
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
<2.14 µg/m3 2.14 39.61,1-Dichloroethene 20 09/03/21 19:37 V8587ANG
<1.91 µg/m3 1.91 39.6cis-1,2-Dichloroethene 20 09/03/21 19:37 V8587ANG
<2.16 µg/m3 2.16 39.6trans-1,2-Dichloroethene 20 09/03/21 19:37 V8587ANG
<4.10 µg/m3 4.10 46.21,2-Dichloropropane 20 09/03/21 19:37 V8587ANG
<12.4 µg/m3 12.4 69.91,2-Dichlorotetrafluoroethane 20 09/03/21 19:37 V8587ANG
<3.56 µg/m3 3.56 45.4cis-1,3-Dichloropropene 20 09/03/21 19:37 V8587ANG
<3.56 µg/m3 3.56 45.4trans-1,3-Dichloropropene 20 09/03/21 19:37 V8587ANG
<8.69 µg/m3 8.69 36.01,4-Dioxane 20 09/03/21 19:37 V8587ANG
<2.72 µg/m3 2.72 36.0
Ethyl Acetate 20 09/03/21 19:37 V8587ANG
667 µg/m3 2.12 43.4Ethylbenzene 20 09/03/21 19:37 V8587ANG
35.9 J µg/m3 2.56 49.24-Ethyltoluene 20 09/03/21 19:37 V8587ANG
<11.2 µg/m3 11.2 76.61,1,2-Trichloro-1,2,2-trifluoroethane 20 09/03/21 19:37 V8587ANG
128 µg/m3 2.86 41.0Heptane 20 09/03/21 19:37 V8587ANG
<6.62 µg/m3 6.62 107Hexachlorobutadiene 20 09/03/21 19:37 V8587ANG
12.3 J µg/m3 0.943 35.2n-Hexane 20 09/03/21 19:37 V8587ANG
<5.71 µg/m3 5.71 41.0
2-Hexanone 20 09/03/21 19:37 V8587ANG
12.2 J µg/m3 2.78 98.3Isopropyl Alchohol 20 09/03/21 19:37 V8587ANG
<4.48 µg/m3 4.48 29.5Methyl Ethyl Ketone (MEK)20 09/03/21 19:37 V8587ANG
<0.673 µg/m3 0.673 36.1Methyl tert-butyl ether (MTBE)20 09/03/21 19:37 V8587ANG
<2.42 µg/m3 2.42 41.04-Methyl-2-Pentanone 20 09/03/21 19:37 V8587ANG
<9.75 µg/m3 9.75 34.7Methylene Chloride 20 09/03/21 19:37 V8587ANG
<3.66 µg/m3 3.66 52.4Naphthalene 20 09/03/21 19:37 V8587ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-5
94713 Matrix:
9/1/2021 13:30
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
<4.84 µg/m3 4.84 17.2Propene 20 09/03/21 19:37 V8587ANG
<2.48 µg/m3 2.48 42.6Styrene 20 09/03/21 19:37 V8587ANG
<2.08 µg/m3 2.08 68.61,1,2,2-Tetrachloroethane 20 09/03/21 19:37 V8587ANG
3020 µg/m3 3.62 67.8Tetrachloroethene 20 09/03/21 19:37 V8587ANG
<2.14 µg/m3 2.14 29.5Tetrahydrofuran 20 09/03/21 19:37 V8587ANG
367 µg/m3 1.80 37.7Toluene 20 09/03/21 19:37 V8587ANG
<4.18 µg/m3 4.18 74.21,2,4-Trichlorobenzene 20 09/03/21 19:37 V8587ANG
<2.88 µg/m3 2.88 54.61,1,1-Trichloroethane 20 09/03/21 19:37 V8587ANG
<1.75 µg/m3 1.75 54.6
1,1,2-Trichloroethane 20 09/03/21 19:37 V8587ANG
<3.98 µg/m3 3.98 43.0Trichloroethene 20 09/03/21 19:37 V8587ANG
9.33 J µg/m3 2.60 56.2Trichlorofluoromethane 20 09/03/21 19:37 V8587ANG
29.1 J µg/m3 2.20 49.21,2,4-Trimethylbenzene 20 09/03/21 19:37 V8587ANG
117 µg/m3 4.72 49.21,3,5-Trimethylbenzene 20 09/03/21 19:37 V8587ANG
<4.48 µg/m3 4.48 35.2Vinyl Acetate 20 09/03/21 19:37 V8587ANG
<2.54 µg/m3 2.54 25.6Vinyl Chloride 20 09/03/21 19:37 V8587ANG
520 µg/m3 3.14 43.4
o-Xylene 20 09/03/21 19:37 V8587ANG
1130 µg/m3 4.34 113m,p-Xylene 20 09/03/21 19:37 V8587ANG
1650 µg/m3 3.14 43.4Xylene (Total)20 09/03/21 19:37 V8587
Surrogate: 4-Bromofluorobenzene 74.6 Limits: 70-130%09/03/21 19:3720 ANG V8587
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-6
94714 Matrix:
9/1/2021 13:12
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
99.0 µg/m3 4.04 95.0Acetone 20 09/03/21 20:15 V8587ANG
34.6 µg/m3 1.46 31.9Benzene 20 09/03/21 20:15 V8587ANG
<2.94 µg/m3 2.94 207Benzyl Chloride 20 09/03/21 20:15 V8587ANG
<3.00 µg/m3 3.00 67.0Bromodichloromethane 20 09/03/21 20:15 V8587ANG
<3.05 µg/m3 3.05 103Bromoform 20 09/03/21 20:15 V8587ANG
<2.30 µg/m3 2.30 38.8Bromomethane 20 09/03/21 20:15 V8587ANG
<6.53 µg/m3 6.53 22.11,3-Butadiene 20 09/03/21 20:15 V8587ANG
176 µg/m3 1.22 125Carbon Disulfide 20 09/03/21 20:15 V8587ANG
<3.10 µg/m3 3.10 62.9
Carbon Tetrachloride 20 09/03/21 20:15 V8587ANG
<2.14 µg/m3 2.14 46.0Chlorobenzene 20 09/03/21 20:15 V8587ANG
<4.16 µg/m3 4.16 85.2Chlorodibromomethane 20 09/03/21 20:15 V8587ANG
<3.28 µg/m3 3.28 26.4Chloroethane 20 09/03/21 20:15 V8587ANG
16.5 J µg/m3 1.73 48.8Chloroform 20 09/03/21 20:15 V8587ANG
9.37 J µg/m3 1.34 20.6Chloromethane 20 09/03/21 20:15 V8587ANG
164 µg/m3 3.22 68.8Cyclohexane 20 09/03/21 20:15 V8587ANG
<3.02 µg/m3 3.02 76.8
1,2-Dibromoethane 20 09/03/21 20:15 V8587ANG
<1.92 µg/m3 1.92 60.11,2-Dichlorobenzene 20 09/03/21 20:15 V8587ANG
<3.48 µg/m3 3.48 2411,3-Dichlorobenzene 20 09/03/21 20:15 V8587ANG
12.0 J µg/m3 3.72 60.11,4-Dichlorobenzene 20 09/03/21 20:15 V8587ANG
<2.68 µg/m3 2.68 49.4Dichlorodifluoromethane 20 09/03/21 20:15 V8587ANG
<2.02 µg/m3 2.02 40.51,1-Dichloroethane 20 09/03/21 20:15 V8587ANG
<2.58 µg/m3 2.58 40.51,2-Dichloroethane 20 09/03/21 20:15 V8587ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-6
94714 Matrix:
9/1/2021 13:12
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
<2.14 µg/m3 2.14 39.61,1-Dichloroethene 20 09/03/21 20:15 V8587ANG
<1.91 µg/m3 1.91 39.6cis-1,2-Dichloroethene 20 09/03/21 20:15 V8587ANG
<2.16 µg/m3 2.16 39.6trans-1,2-Dichloroethene 20 09/03/21 20:15 V8587ANG
<4.10 µg/m3 4.10 46.21,2-Dichloropropane 20 09/03/21 20:15 V8587ANG
<12.4 µg/m3 12.4 69.91,2-Dichlorotetrafluoroethane 20 09/03/21 20:15 V8587ANG
<3.56 µg/m3 3.56 45.4cis-1,3-Dichloropropene 20 09/03/21 20:15 V8587ANG
<3.56 µg/m3 3.56 45.4trans-1,3-Dichloropropene 20 09/03/21 20:15 V8587ANG
<8.69 µg/m3 8.69 36.01,4-Dioxane 20 09/03/21 20:15 V8587ANG
<2.72 µg/m3 2.72 36.0
Ethyl Acetate 20 09/03/21 20:15 V8587ANG
1310 µg/m3 2.12 43.4Ethylbenzene 20 09/03/21 20:15 V8587ANG
25.0 J µg/m3 2.56 49.24-Ethyltoluene 20 09/03/21 20:15 V8587ANG
<11.2 µg/m3 11.2 76.61,1,2-Trichloro-1,2,2-trifluoroethane 20 09/03/21 20:15 V8587ANG
561 µg/m3 2.86 41.0Heptane 20 09/03/21 20:15 V8587ANG
<6.62 µg/m3 6.62 107Hexachlorobutadiene 20 09/03/21 20:15 V8587ANG
34.1 J µg/m3 0.943 35.2n-Hexane 20 09/03/21 20:15 V8587ANG
<5.71 µg/m3 5.71 41.0
2-Hexanone 20 09/03/21 20:15 V8587ANG
11.7 J µg/m3 2.78 98.3Isopropyl Alchohol 20 09/03/21 20:15 V8587ANG
13.5 J µg/m3 4.48 29.5Methyl Ethyl Ketone (MEK)20 09/03/21 20:15 V8587ANG
<0.673 µg/m3 0.673 36.1Methyl tert-butyl ether (MTBE)20 09/03/21 20:15 V8587ANG
<2.42 µg/m3 2.42 41.04-Methyl-2-Pentanone 20 09/03/21 20:15 V8587ANG
15.1 J µg/m3 9.75 34.7Methylene Chloride 20 09/03/21 20:15 V8587ANG
<3.66 µg/m3 3.66 52.4Naphthalene 20 09/03/21 20:15 V8587ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-6
94714 Matrix:
9/1/2021 13:12
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
179 µg/m3 4.84 17.2Propene 20 09/03/21 20:15 V8587ANG
<2.48 µg/m3 2.48 42.6Styrene 20 09/03/21 20:15 V8587ANG
<2.08 µg/m3 2.08 68.61,1,2,2-Tetrachloroethane 20 09/03/21 20:15 V8587ANG
2470 µg/m3 3.62 67.8Tetrachloroethene 20 09/03/21 20:15 V8587ANG
<2.14 µg/m3 2.14 29.5Tetrahydrofuran 20 09/03/21 20:15 V8587ANG
478 µg/m3 1.80 37.7Toluene 20 09/03/21 20:15 V8587ANG
<4.18 µg/m3 4.18 74.21,2,4-Trichlorobenzene 20 09/03/21 20:15 V8587ANG
<2.88 µg/m3 2.88 54.61,1,1-Trichloroethane 20 09/03/21 20:15 V8587ANG
<1.75 µg/m3 1.75 54.6
1,1,2-Trichloroethane 20 09/03/21 20:15 V8587ANG
<3.98 µg/m3 3.98 43.0Trichloroethene 20 09/03/21 20:15 V8587ANG
9.21 J µg/m3 2.60 56.2Trichlorofluoromethane 20 09/03/21 20:15 V8587ANG
13.6 J µg/m3 2.20 49.21,2,4-Trimethylbenzene 20 09/03/21 20:15 V8587ANG
72.8 µg/m3 4.72 49.21,3,5-Trimethylbenzene 20 09/03/21 20:15 V8587ANG
<4.48 µg/m3 4.48 35.2Vinyl Acetate 20 09/03/21 20:15 V8587ANG
<2.54 µg/m3 2.54 25.6Vinyl Chloride 20 09/03/21 20:15 V8587ANG
819 µg/m3 3.14 43.4
o-Xylene 20 09/03/21 20:15 V8587ANG
1880 µg/m3 4.34 113m,p-Xylene 20 09/03/21 20:15 V8587ANG
2700 µg/m3 3.14 43.4Xylene (Total)20 09/03/21 20:15 V8587
Surrogate: 4-Bromofluorobenzene 75.1 Limits: 70-130%09/03/21 20:1520 ANG V8587
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-7
94715 Matrix:
9/1/2021 14:21
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
90.1 J µg/m3 4.04 95.0Acetone 20 09/03/21 20:53 V8587ANG
10.4 J µg/m3 1.46 31.9Benzene 20 09/03/21 20:53 V8587ANG
<2.94 µg/m3 2.94 207Benzyl Chloride 20 09/03/21 20:53 V8587ANG
<3.00 µg/m3 3.00 67.0Bromodichloromethane 20 09/03/21 20:53 V8587ANG
<3.05 µg/m3 3.05 103Bromoform 20 09/03/21 20:53 V8587ANG
<2.30 µg/m3 2.30 38.8Bromomethane 20 09/03/21 20:53 V8587ANG
<6.53 µg/m3 6.53 22.11,3-Butadiene 20 09/03/21 20:53 V8587ANG
8.41 J µg/m3 1.22 125Carbon Disulfide 20 09/03/21 20:53 V8587ANG
<3.10 µg/m3 3.10 62.9
Carbon Tetrachloride 20 09/03/21 20:53 V8587ANG
<2.14 µg/m3 2.14 46.0Chlorobenzene 20 09/03/21 20:53 V8587ANG
<4.16 µg/m3 4.16 85.2Chlorodibromomethane 20 09/03/21 20:53 V8587ANG
<3.28 µg/m3 3.28 26.4Chloroethane 20 09/03/21 20:53 V8587ANG
<1.73 µg/m3 1.73 48.8Chloroform 20 09/03/21 20:53 V8587ANG
<1.34 µg/m3 1.34 20.6Chloromethane 20 09/03/21 20:53 V8587ANG
32.1 J µg/m3 3.22 68.8Cyclohexane 20 09/03/21 20:53 V8587ANG
<3.02 µg/m3 3.02 76.8
1,2-Dibromoethane 20 09/03/21 20:53 V8587ANG
<1.92 µg/m3 1.92 60.11,2-Dichlorobenzene 20 09/03/21 20:53 V8587ANG
<3.48 µg/m3 3.48 2411,3-Dichlorobenzene 20 09/03/21 20:53 V8587ANG
<3.72 µg/m3 3.72 60.11,4-Dichlorobenzene 20 09/03/21 20:53 V8587ANG
<2.68 µg/m3 2.68 49.4Dichlorodifluoromethane 20 09/03/21 20:53 V8587ANG
<2.02 µg/m3 2.02 40.51,1-Dichloroethane 20 09/03/21 20:53 V8587ANG
<2.58 µg/m3 2.58 40.51,2-Dichloroethane 20 09/03/21 20:53 V8587ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-7
94715 Matrix:
9/1/2021 14:21
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
<2.14 µg/m3 2.14 39.61,1-Dichloroethene 20 09/03/21 20:53 V8587ANG
<1.91 µg/m3 1.91 39.6cis-1,2-Dichloroethene 20 09/03/21 20:53 V8587ANG
<2.16 µg/m3 2.16 39.6trans-1,2-Dichloroethene 20 09/03/21 20:53 V8587ANG
<4.10 µg/m3 4.10 46.21,2-Dichloropropane 20 09/03/21 20:53 V8587ANG
<12.4 µg/m3 12.4 69.91,2-Dichlorotetrafluoroethane 20 09/03/21 20:53 V8587ANG
<3.56 µg/m3 3.56 45.4cis-1,3-Dichloropropene 20 09/03/21 20:53 V8587ANG
<3.56 µg/m3 3.56 45.4trans-1,3-Dichloropropene 20 09/03/21 20:53 V8587ANG
<8.69 µg/m3 8.69 36.01,4-Dioxane 20 09/03/21 20:53 V8587ANG
<2.72 µg/m3 2.72 36.0
Ethyl Acetate 20 09/03/21 20:53 V8587ANG
409 µg/m3 2.12 43.4Ethylbenzene 20 09/03/21 20:53 V8587ANG
34.1 J µg/m3 2.56 49.24-Ethyltoluene 20 09/03/21 20:53 V8587ANG
<11.2 µg/m3 11.2 76.61,1,2-Trichloro-1,2,2-trifluoroethane 20 09/03/21 20:53 V8587ANG
67.0 µg/m3 2.86 41.0Heptane 20 09/03/21 20:53 V8587ANG
<6.62 µg/m3 6.62 107Hexachlorobutadiene 20 09/03/21 20:53 V8587ANG
<0.943 µg/m3 0.943 35.2n-Hexane 20 09/03/21 20:53 V8587ANG
<5.71 µg/m3 5.71 41.0
2-Hexanone 20 09/03/21 20:53 V8587ANG
14.1 J µg/m3 2.78 98.3Isopropyl Alchohol 20 09/03/21 20:53 V8587ANG
6.43 J µg/m3 4.48 29.5Methyl Ethyl Ketone (MEK)20 09/03/21 20:53 V8587ANG
<0.673 µg/m3 0.673 36.1Methyl tert-butyl ether (MTBE)20 09/03/21 20:53 V8587ANG
<2.42 µg/m3 2.42 41.04-Methyl-2-Pentanone 20 09/03/21 20:53 V8587ANG
<9.75 µg/m3 9.75 34.7Methylene Chloride 20 09/03/21 20:53 V8587ANG
<3.66 µg/m3 3.66 52.4Naphthalene 20 09/03/21 20:53 V8587ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:SV-7
94715 Matrix:
9/1/2021 14:21
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
<4.84 µg/m3 4.84 17.2Propene 20 09/03/21 20:53 V8587ANG
<2.48 µg/m3 2.48 42.6Styrene 20 09/03/21 20:53 V8587ANG
<2.08 µg/m3 2.08 68.61,1,2,2-Tetrachloroethane 20 09/03/21 20:53 V8587ANG
2210 µg/m3 3.62 67.8Tetrachloroethene 20 09/03/21 20:53 V8587ANG
<2.14 µg/m3 2.14 29.5Tetrahydrofuran 20 09/03/21 20:53 V8587ANG
221 µg/m3 1.80 37.7Toluene 20 09/03/21 20:53 V8587ANG
<4.18 µg/m3 4.18 74.21,2,4-Trichlorobenzene 20 09/03/21 20:53 V8587ANG
<2.88 µg/m3 2.88 54.61,1,1-Trichloroethane 20 09/03/21 20:53 V8587ANG
<1.75 µg/m3 1.75 54.6
1,1,2-Trichloroethane 20 09/03/21 20:53 V8587ANG
<3.98 µg/m3 3.98 43.0Trichloroethene 20 09/03/21 20:53 V8587ANG
<2.60 µg/m3 2.60 56.2Trichlorofluoromethane 20 09/03/21 20:53 V8587ANG
35.6 J µg/m3 2.20 49.21,2,4-Trimethylbenzene 20 09/03/21 20:53 V8587ANG
116 µg/m3 4.72 49.21,3,5-Trimethylbenzene 20 09/03/21 20:53 V8587ANG
<4.48 µg/m3 4.48 35.2Vinyl Acetate 20 09/03/21 20:53 V8587ANG
<2.54 µg/m3 2.54 25.6Vinyl Chloride 20 09/03/21 20:53 V8587ANG
349 µg/m3 3.14 43.4
o-Xylene 20 09/03/21 20:53 V8587ANG
745 µg/m3 4.34 113m,p-Xylene 20 09/03/21 20:53 V8587ANG
1090 µg/m3 3.14 43.4Xylene (Total)20 09/03/21 20:53 V8587
Surrogate: 4-Bromofluorobenzene 79.6 Limits: 70-130%09/03/21 20:5320 ANG V8587
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:DUP-1
94716 Matrix:
9/1/2021 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
119 µg/m3 4.04 95.0Acetone 20 09/03/21 21:32 V8587ANG
24.0 J µg/m3 1.46 31.9Benzene 20 09/03/21 21:32 V8587ANG
<2.94 µg/m3 2.94 207Benzyl Chloride 20 09/03/21 21:32 V8587ANG
<3.00 µg/m3 3.00 67.0Bromodichloromethane 20 09/03/21 21:32 V8587ANG
<3.05 µg/m3 3.05 103Bromoform 20 09/03/21 21:32 V8587ANG
<2.30 µg/m3 2.30 38.8Bromomethane 20 09/03/21 21:32 V8587ANG
<6.53 µg/m3 6.53 22.11,3-Butadiene 20 09/03/21 21:32 V8587ANG
17.9 J µg/m3 1.22 125Carbon Disulfide 20 09/03/21 21:32 V8587ANG
<3.10 µg/m3 3.10 62.9
Carbon Tetrachloride 20 09/03/21 21:32 V8587ANG
<2.14 µg/m3 2.14 46.0Chlorobenzene 20 09/03/21 21:32 V8587ANG
<4.16 µg/m3 4.16 85.2Chlorodibromomethane 20 09/03/21 21:32 V8587ANG
<3.28 µg/m3 3.28 26.4Chloroethane 20 09/03/21 21:32 V8587ANG
<1.73 µg/m3 1.73 48.8Chloroform 20 09/03/21 21:32 V8587ANG
<1.34 µg/m3 1.34 20.6Chloromethane 20 09/03/21 21:32 V8587ANG
58.5 J µg/m3 3.22 68.8Cyclohexane 20 09/03/21 21:32 V8587ANG
<3.02 µg/m3 3.02 76.8
1,2-Dibromoethane 20 09/03/21 21:32 V8587ANG
<1.92 µg/m3 1.92 60.11,2-Dichlorobenzene 20 09/03/21 21:32 V8587ANG
<3.48 µg/m3 3.48 2411,3-Dichlorobenzene 20 09/03/21 21:32 V8587ANG
<3.72 µg/m3 3.72 60.11,4-Dichlorobenzene 20 09/03/21 21:32 V8587ANG
<2.68 µg/m3 2.68 49.4Dichlorodifluoromethane 20 09/03/21 21:32 V8587ANG
<2.02 µg/m3 2.02 40.51,1-Dichloroethane 20 09/03/21 21:32 V8587ANG
<2.58 µg/m3 2.58 40.51,2-Dichloroethane 20 09/03/21 21:32 V8587ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:DUP-1
94716 Matrix:
9/1/2021 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
<2.14 µg/m3 2.14 39.61,1-Dichloroethene 20 09/03/21 21:32 V8587ANG
<1.91 µg/m3 1.91 39.6cis-1,2-Dichloroethene 20 09/03/21 21:32 V8587ANG
<2.16 µg/m3 2.16 39.6trans-1,2-Dichloroethene 20 09/03/21 21:32 V8587ANG
<4.10 µg/m3 4.10 46.21,2-Dichloropropane 20 09/03/21 21:32 V8587ANG
<12.4 µg/m3 12.4 69.91,2-Dichlorotetrafluoroethane 20 09/03/21 21:32 V8587ANG
<3.56 µg/m3 3.56 45.4cis-1,3-Dichloropropene 20 09/03/21 21:32 V8587ANG
<3.56 µg/m3 3.56 45.4trans-1,3-Dichloropropene 20 09/03/21 21:32 V8587ANG
<8.69 µg/m3 8.69 36.01,4-Dioxane 20 09/03/21 21:32 V8587ANG
<2.72 µg/m3 2.72 36.0
Ethyl Acetate 20 09/03/21 21:32 V8587ANG
710 µg/m3 2.12 43.4Ethylbenzene 20 09/03/21 21:32 V8587ANG
37.3 J µg/m3 2.56 49.24-Ethyltoluene 20 09/03/21 21:32 V8587ANG
<11.2 µg/m3 11.2 76.61,1,2-Trichloro-1,2,2-trifluoroethane 20 09/03/21 21:32 V8587ANG
165 µg/m3 2.86 41.0Heptane 20 09/03/21 21:32 V8587ANG
<6.62 µg/m3 6.62 107Hexachlorobutadiene 20 09/03/21 21:32 V8587ANG
12.0 J µg/m3 0.943 35.2n-Hexane 20 09/03/21 21:32 V8587ANG
<5.71 µg/m3 5.71 41.0
2-Hexanone 20 09/03/21 21:32 V8587ANG
11.5 J µg/m3 2.78 98.3Isopropyl Alchohol 20 09/03/21 21:32 V8587ANG
12.5 J µg/m3 4.48 29.5Methyl Ethyl Ketone (MEK)20 09/03/21 21:32 V8587ANG
<0.673 µg/m3 0.673 36.1Methyl tert-butyl ether (MTBE)20 09/03/21 21:32 V8587ANG
<2.42 µg/m3 2.42 41.04-Methyl-2-Pentanone 20 09/03/21 21:32 V8587ANG
<9.75 µg/m3 9.75 34.7Methylene Chloride 20 09/03/21 21:32 V8587ANG
<3.66 µg/m3 3.66 52.4Naphthalene 20 09/03/21 21:32 V8587ANG
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28217
21-242-0017
01151
NOVA Engineering & Environmental
417 Minuet Lane Suite D
Steven Aldis
Charlotte
Received : 09/02/2021
Doggette Site
Report Date : 09/10/2021
Sample ID :
Lab No :
Sampled:DUP-1
94716 Matrix:
9/1/2021 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V8585 09/03/21 09:00
<4.84 µg/m3 4.84 17.2Propene 20 09/03/21 21:32 V8587ANG
<2.48 µg/m3 2.48 42.6Styrene 20 09/03/21 21:32 V8587ANG
<2.08 µg/m3 2.08 68.61,1,2,2-Tetrachloroethane 20 09/03/21 21:32 V8587ANG
3070 µg/m3 3.62 67.8Tetrachloroethene 20 09/03/21 21:32 V8587ANG
<2.14 µg/m3 2.14 29.5Tetrahydrofuran 20 09/03/21 21:32 V8587ANG
376 µg/m3 1.80 37.7Toluene 20 09/03/21 21:32 V8587ANG
<4.18 µg/m3 4.18 74.21,2,4-Trichlorobenzene 20 09/03/21 21:32 V8587ANG
<2.88 µg/m3 2.88 54.61,1,1-Trichloroethane 20 09/03/21 21:32 V8587ANG
<1.75 µg/m3 1.75 54.6
1,1,2-Trichloroethane 20 09/03/21 21:32 V8587ANG
<3.98 µg/m3 3.98 43.0Trichloroethene 20 09/03/21 21:32 V8587ANG
<2.60 µg/m3 2.60 56.2Trichlorofluoromethane 20 09/03/21 21:32 V8587ANG
31.8 J µg/m3 2.20 49.21,2,4-Trimethylbenzene 20 09/03/21 21:32 V8587ANG
125 µg/m3 4.72 49.21,3,5-Trimethylbenzene 20 09/03/21 21:32 V8587ANG
<4.48 µg/m3 4.48 35.2Vinyl Acetate 20 09/03/21 21:32 V8587ANG
<2.54 µg/m3 2.54 25.6Vinyl Chloride 20 09/03/21 21:32 V8587ANG
558 µg/m3 3.14 43.4
o-Xylene 20 09/03/21 21:32 V8587ANG
1210 µg/m3 4.34 113m,p-Xylene 20 09/03/21 21:32 V8587ANG
1770 µg/m3 3.14 43.4Xylene (Total)20 09/03/21 21:32 V8587
Surrogate: 4-Bromofluorobenzene 74.3 Limits: 70-130%09/03/21 21:3220 ANG V8587
Qualifiers/
Definitions
Analyte detected in blankBOutside QC Limit*
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 45
Quality Control Data
21-242-0017Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V8577QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V8576
Associated Lab Samples: 94709, 94711, 94712
LRB-V8576 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 11:494.750.2020.558µg/m3Acetone
09/07/21 11:491.600.0733<0.0733µg/m3Benzene
09/07/21 11:4910.40.148<0.148µg/m3Benzyl Chloride
09/07/21 11:493.350.150<0.150µg/m3Bromodichloromethane
09/07/21 11:495.170.153<0.153µg/m3Bromoform
09/07/21 11:491.940.115<0.115µg/m3Bromomethane
09/07/21 11:491.110.328<0.328µg/m31,3-Butadiene
09/07/21 11:496.230.0608<0.0608µg/m3Carbon Disulfide
09/07/21 11:493.150.155<0.155µg/m3Carbon Tetrachloride
09/07/21 11:492.300.107<0.107µg/m3Chlorobenzene
09/07/21 11:494.260.208<0.208µg/m3Chlorodibromomethane
09/07/21 11:491.320.164<0.164µg/m3Chloroethane
09/07/21 11:492.440.0864<0.0864µg/m3Chloroform
09/07/21 11:491.030.0673<0.0673µg/m3Chloromethane
09/07/21 11:493.440.161<0.161µg/m3Cyclohexane
09/07/21 11:493.840.151<0.151µg/m31,2-Dibromoethane
09/07/21 11:493.010.0963<0.0963µg/m31,2-Dichlorobenzene
09/07/21 11:4912.00.174<0.174µg/m31,3-Dichlorobenzene
09/07/21 11:493.010.186<0.186µg/m31,4-Dichlorobenzene
09/07/21 11:492.470.134<0.134µg/m3Dichlorodifluoromethane
09/07/21 11:492.020.101<0.101µg/m31,1-Dichloroethane
09/07/21 11:492.020.129<0.129µg/m31,2-Dichloroethane
09/07/21 11:491.980.107<0.107µg/m31,1-Dichloroethene
09/07/21 11:491.980.0955<0.0955µg/m3cis-1,2-Dichloroethene
09/07/21 11:491.980.108<0.108µg/m3trans-1,2-Dichloroethene
09/07/21 11:492.310.205<0.205µg/m31,2-Dichloropropane
09/07/21 11:493.500.623<0.623µg/m31,2-Dichlorotetrafluoroethane
Page 1 of 10Date:09/10/2021 11:50 AM
Page 34 of 45
Quality Control Data
21-242-0017Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V8577QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V8576
Associated Lab Samples: 94709, 94711, 94712
LRB-V8576 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 11:492.270.178<0.178µg/m3cis-1,3-Dichloropropene
09/07/21 11:492.270.178<0.178µg/m3trans-1,3-Dichloropropene
09/07/21 11:491.800.435<0.435µg/m31,4-Dioxane
09/07/21 11:491.800.136<0.136µg/m3Ethyl Acetate
09/07/21 11:492.170.106<0.106µg/m3Ethylbenzene
09/07/21 11:492.460.128<0.128µg/m34-Ethyltoluene
09/07/21 11:493.830.561<0.561µg/m31,1,2-Trichloro-1,2,2-trifluoroethane
09/07/21 11:492.050.143<0.143µg/m3Heptane
09/07/21 11:495.330.330<0.330µg/m3Hexachlorobutadiene
09/07/21 11:491.760.0472<0.0472µg/m3n-Hexane
09/07/21 11:492.050.285<0.285µg/m32-Hexanone
09/07/21 11:494.920.1390.531µg/m3Isopropyl Alchohol
09/07/21 11:491.470.224<0.224µg/m3Methyl Ethyl Ketone (MEK)
09/07/21 11:491.800.0336<0.0336µg/m3Methyl tert-butyl ether (MTBE)
09/07/21 11:492.050.121<0.121µg/m34-Methyl-2-Pentanone
09/07/21 11:491.740.489<0.489µg/m3Methylene Chloride
09/07/21 11:492.620.183<0.183µg/m3Naphthalene
09/07/21 11:490.8610.242<0.242µg/m3Propene
09/07/21 11:492.130.124<0.124µg/m3Styrene
09/07/21 11:493.430.104<0.104µg/m31,1,2,2-Tetrachloroethane
09/07/21 11:493.390.181<0.181µg/m3Tetrachloroethene
09/07/21 11:491.470.107<0.107µg/m3Tetrahydrofuran
09/07/21 11:491.880.0901<0.0901µg/m3Toluene
09/07/21 11:493.710.209<0.209µg/m31,2,4-Trichlorobenzene
09/07/21 11:492.730.144<0.144µg/m31,1,1-Trichloroethane
09/07/21 11:492.730.0877<0.0877µg/m31,1,2-Trichloroethane
09/07/21 11:492.150.199<0.199µg/m3Trichloroethene
Page 2 of 10Date:09/10/2021 11:50 AM
Page 35 of 45
Quality Control Data
21-242-0017Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V8577QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V8576
Associated Lab Samples: 94709, 94711, 94712
LRB-V8576 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/07/21 11:492.810.130<0.130µg/m3Trichlorofluoromethane
09/07/21 11:492.460.110<0.110µg/m31,2,4-Trimethylbenzene
09/07/21 11:492.460.236<0.236µg/m31,3,5-Trimethylbenzene
09/07/21 11:491.760.224<0.224µg/m3Vinyl Acetate
09/07/21 11:491.280.127<0.127µg/m3Vinyl Chloride
09/07/21 11:492.170.157<0.157µg/m3o-Xylene
09/07/21 11:495.650.217<0.217µg/m3m,p-Xylene
09/07/21 11:494-Bromofluorobenzene (S)95.2 70-130
LCS-V8576Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10412.411.9µg/m3Acetone 70-130
10817.216.0µg/m3Benzene 70-130
11229.025.9µg/m3Benzyl Chloride 70-130
10936.533.5µg/m3Bromodichloromethane 70-130
11258.051.7µg/m3Bromoform 70-130
10921.219.4µg/m3Bromomethane 70-130
11112.311.1µg/m31,3-Butadiene 70-130
11618.115.6µg/m3Carbon Disulfide 70-130
10432.731.5µg/m3Carbon Tetrachloride 70-130
11326.123.0µg/m3Chlorobenzene 70-130
11348.242.6µg/m3Chlorodibromomethane 70-130
10413.713.2µg/m3Chloroethane 70-130
10726.224.4µg/m3Chloroform 70-130
11011.310.3µg/m3Chloromethane 70-130
95.316.417.2µg/m3Cyclohexane 70-130
Page 3 of 10Date:09/10/2021 11:50 AM
Page 36 of 45
Quality Control Data
21-242-0017Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V8577QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V8576
LCS-V8576Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
11343.538.4µg/m31,2-Dibromoethane 70-130
10832.430.1µg/m31,2-Dichlorobenzene 70-130
10732.230.1µg/m31,3-Dichlorobenzene 70-130
10431.430.1µg/m31,4-Dichlorobenzene 70-130
10225.324.7µg/m3Dichlorodifluoromethane 70-130
11022.220.2µg/m31,1-Dichloroethane 70-130
10721.620.2µg/m31,2-Dichloroethane 70-130
11422.619.8µg/m31,1-Dichloroethene 70-130
11222.119.8µg/m3cis-1,2-Dichloroethene 70-130
11122.019.8µg/m3trans-1,2-Dichloroethene 70-130
10925.123.1µg/m31,2-Dichloropropane 70-130
10336.135.0µg/m31,2-Dichlorotetrafluoroethane 70-130
11025.022.7µg/m3cis-1,3-Dichloropropene 70-130
11025.022.7µg/m3trans-1,3-Dichloropropene 70-130
94.417.018.0µg/m31,4-Dioxane 70-130
10518.918.0µg/m3Ethyl Acetate 70-130
11023.921.7µg/m3Ethylbenzene 70-130
11428.124.6µg/m34-Ethyltoluene 70-130
10941.838.3µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 70-130
11122.820.5µg/m3Heptane 70-130
11259.853.3µg/m3Hexachlorobutadiene 70-130
10919.217.6µg/m3n-Hexane 70-130
10120.820.5µg/m32-Hexanone 70-130
99.112.212.3µg/m3Isopropyl Alchohol 70-130
10515.614.8µg/m3Methyl Ethyl Ketone (MEK)70-130
10619.118.0µg/m3Methyl tert-butyl ether (MTBE)70-130
10521.520.5µg/m34-Methyl-2-Pentanone 70-130
Page 4 of 10Date:09/10/2021 11:50 AM
Page 37 of 45
Quality Control Data
21-242-0017Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V8577QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V8576
LCS-V8576Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10618.517.4µg/m3Methylene Chloride 70-130
11931.226.2µg/m3Naphthalene 70-130
1008.648.61µg/m3Propene 70-130
11123.621.3µg/m3Styrene 70-130
10937.334.3µg/m31,1,2,2-Tetrachloroethane 70-130
11237.833.9µg/m3Tetrachloroethene 70-130
10815.914.7µg/m3Tetrahydrofuran 70-130
11020.618.8µg/m3Toluene 70-130
11141.137.1µg/m31,2,4-Trichlorobenzene 70-130
10227.927.3µg/m31,1,1-Trichloroethane 70-130
11030.127.3µg/m31,1,2-Trichloroethane 70-130
10728.926.9µg/m3Trichloroethene 70-130
11030.928.1µg/m3Trichlorofluoromethane 70-130
11327.724.6µg/m31,2,4-Trimethylbenzene 70-130
11428.024.6µg/m31,3,5-Trimethylbenzene 70-130
10217.917.6µg/m3Vinyl Acetate 70-130
10813.812.8µg/m3Vinyl Chloride 70-130
11023.921.7µg/m3o-Xylene 70-130
11248.443.4µg/m3m,p-Xylene 70-130
1034-Bromofluorobenzene (S)70-130
Page 5 of 10Date:09/10/2021 11:50 AM
Page 38 of 45
Quality Control Data
21-242-0017Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V8587QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V8585
Associated Lab Samples: 94710, 94711, 94713, 94714, 94715, 94716
LRB-V8585 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/03/21 14:314.750.2020.330µg/m3Acetone
09/03/21 14:311.600.0733<0.0733µg/m3Benzene
09/03/21 14:3110.40.148<0.148µg/m3Benzyl Chloride
09/03/21 14:313.350.150<0.150µg/m3Bromodichloromethane
09/03/21 14:315.170.153<0.153µg/m3Bromoform
09/03/21 14:311.940.115<0.115µg/m3Bromomethane
09/03/21 14:311.110.328<0.328µg/m31,3-Butadiene
09/03/21 14:316.230.0608<0.0608µg/m3Carbon Disulfide
09/03/21 14:313.150.155<0.155µg/m3Carbon Tetrachloride
09/03/21 14:312.300.107<0.107µg/m3Chlorobenzene
09/03/21 14:314.260.208<0.208µg/m3Chlorodibromomethane
09/03/21 14:311.320.164<0.164µg/m3Chloroethane
09/03/21 14:312.440.0864<0.0864µg/m3Chloroform
09/03/21 14:311.030.0673<0.0673µg/m3Chloromethane
09/03/21 14:313.440.161<0.161µg/m3Cyclohexane
09/03/21 14:313.840.151<0.151µg/m31,2-Dibromoethane
09/03/21 14:313.010.0963<0.0963µg/m31,2-Dichlorobenzene
09/03/21 14:3112.00.174<0.174µg/m31,3-Dichlorobenzene
09/03/21 14:313.010.186<0.186µg/m31,4-Dichlorobenzene
09/03/21 14:312.470.134<0.134µg/m3Dichlorodifluoromethane
09/03/21 14:312.020.101<0.101µg/m31,1-Dichloroethane
09/03/21 14:312.020.129<0.129µg/m31,2-Dichloroethane
09/03/21 14:311.980.107<0.107µg/m31,1-Dichloroethene
09/03/21 14:311.980.0955<0.0955µg/m3cis-1,2-Dichloroethene
09/03/21 14:311.980.108<0.108µg/m3trans-1,2-Dichloroethene
09/03/21 14:312.310.205<0.205µg/m31,2-Dichloropropane
09/03/21 14:313.500.623<0.623µg/m31,2-Dichlorotetrafluoroethane
Page 6 of 10Date:09/10/2021 11:50 AM
Page 39 of 45
Quality Control Data
21-242-0017Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V8587QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V8585
Associated Lab Samples: 94710, 94711, 94713, 94714, 94715, 94716
LRB-V8585 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/03/21 14:312.270.178<0.178µg/m3cis-1,3-Dichloropropene
09/03/21 14:312.270.178<0.178µg/m3trans-1,3-Dichloropropene
09/03/21 14:311.800.435<0.435µg/m31,4-Dioxane
09/03/21 14:311.800.136<0.136µg/m3Ethyl Acetate
09/03/21 14:312.170.106<0.106µg/m3Ethylbenzene
09/03/21 14:312.460.128<0.128µg/m34-Ethyltoluene
09/03/21 14:313.830.561<0.561µg/m31,1,2-Trichloro-1,2,2-trifluoroethane
09/03/21 14:312.050.143<0.143µg/m3Heptane
09/03/21 14:315.330.330<0.330µg/m3Hexachlorobutadiene
09/03/21 14:311.760.0472<0.0472µg/m3n-Hexane
09/03/21 14:312.050.285<0.285µg/m32-Hexanone
09/03/21 14:314.920.1390.383µg/m3Isopropyl Alchohol
09/03/21 14:311.470.224<0.224µg/m3Methyl Ethyl Ketone (MEK)
09/03/21 14:311.800.0336<0.0336µg/m3Methyl tert-butyl ether (MTBE)
09/03/21 14:312.050.121<0.121µg/m34-Methyl-2-Pentanone
09/03/21 14:311.740.489<0.489µg/m3Methylene Chloride
09/03/21 14:312.620.183<0.183µg/m3Naphthalene
09/03/21 14:310.8610.242<0.242µg/m3Propene
09/03/21 14:312.130.124<0.124µg/m3Styrene
09/03/21 14:313.430.104<0.104µg/m31,1,2,2-Tetrachloroethane
09/03/21 14:313.390.181<0.181µg/m3Tetrachloroethene
09/03/21 14:311.470.107<0.107µg/m3Tetrahydrofuran
09/03/21 14:311.880.0901<0.0901µg/m3Toluene
09/03/21 14:313.710.209<0.209µg/m31,2,4-Trichlorobenzene
09/03/21 14:312.730.144<0.144µg/m31,1,1-Trichloroethane
09/03/21 14:312.730.0877<0.0877µg/m31,1,2-Trichloroethane
09/03/21 14:312.150.199<0.199µg/m3Trichloroethene
Page 7 of 10Date:09/10/2021 11:50 AM
Page 40 of 45
Quality Control Data
21-242-0017Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V8587QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V8585
Associated Lab Samples: 94710, 94711, 94713, 94714, 94715, 94716
LRB-V8585 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/03/21 14:312.810.130<0.130µg/m3Trichlorofluoromethane
09/03/21 14:312.460.110<0.110µg/m31,2,4-Trimethylbenzene
09/03/21 14:312.460.236<0.236µg/m31,3,5-Trimethylbenzene
09/03/21 14:311.760.224<0.224µg/m3Vinyl Acetate
09/03/21 14:311.280.127<0.127µg/m3Vinyl Chloride
09/03/21 14:312.170.157<0.157µg/m3o-Xylene
09/03/21 14:315.650.217<0.217µg/m3m,p-Xylene
09/03/21 14:314-Bromofluorobenzene (S)98.3 70-130
LCS-V8585Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
95.711.411.9µg/m3Acetone 70-130
10917.516.0µg/m3Benzene 70-130
11429.625.9µg/m3Benzyl Chloride 70-130
10735.733.5µg/m3Bromodichloromethane 70-130
11157.551.7µg/m3Bromoform 70-130
10620.619.4µg/m3Bromomethane 70-130
10511.611.1µg/m31,3-Butadiene 70-130
10616.515.6µg/m3Carbon Disulfide 70-130
10332.631.5µg/m3Carbon Tetrachloride 70-130
11326.023.0µg/m3Chlorobenzene 70-130
11147.142.6µg/m3Chlorodibromomethane 70-130
96.912.813.2µg/m3Chloroethane 70-130
11127.024.4µg/m3Chloroform 70-130
10310.610.3µg/m3Chloromethane 70-130
97.016.717.2µg/m3Cyclohexane 70-130
Page 8 of 10Date:09/10/2021 11:50 AM
Page 41 of 45
Quality Control Data
21-242-0017Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V8587QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V8585
LCS-V8585Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
11343.238.4µg/m31,2-Dibromoethane 70-130
11033.030.1µg/m31,2-Dichlorobenzene 70-130
10631.930.1µg/m31,3-Dichlorobenzene 70-130
10331.030.1µg/m31,4-Dichlorobenzene 70-130
96.723.924.7µg/m3Dichlorodifluoromethane 70-130
10721.620.2µg/m31,1-Dichloroethane 70-130
10821.820.2µg/m31,2-Dichloroethane 70-130
10721.119.8µg/m31,1-Dichloroethene 70-130
10821.419.8µg/m3cis-1,2-Dichloroethene 70-130
10620.919.8µg/m3trans-1,2-Dichloroethene 70-130
10824.923.1µg/m31,2-Dichloropropane 70-130
98.034.335.0µg/m31,2-Dichlorotetrafluoroethane 70-130
10924.822.7µg/m3cis-1,3-Dichloropropene 70-130
10924.822.7µg/m3trans-1,3-Dichloropropene 70-130
95.017.118.0µg/m31,4-Dioxane 70-130
10418.718.0µg/m3Ethyl Acetate 70-130
11424.721.7µg/m3Ethylbenzene 70-130
11628.624.6µg/m34-Ethyltoluene 70-130
10540.438.3µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 70-130
11022.520.5µg/m3Heptane 70-130
11058.753.3µg/m3Hexachlorobutadiene 70-130
10618.717.6µg/m3n-Hexane 70-130
10020.520.5µg/m32-Hexanone 70-130
95.111.712.3µg/m3Isopropyl Alchohol 70-130
99.314.714.8µg/m3Methyl Ethyl Ketone (MEK)70-130
10318.518.0µg/m3Methyl tert-butyl ether (MTBE)70-130
10120.820.5µg/m34-Methyl-2-Pentanone 70-130
Page 9 of 10Date:09/10/2021 11:50 AM
Page 42 of 45
Quality Control Data
21-242-0017Report No:
Project Description:
Client ID:NOVA Engineering & Environmental
Doggette Site
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V8587QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V8585
LCS-V8585Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.817.217.4µg/m3Methylene Chloride 70-130
11931.326.2µg/m3Naphthalene 70-130
95.18.198.61µg/m3Propene 70-130
11223.921.3µg/m3Styrene 70-130
11338.634.3µg/m31,1,2,2-Tetrachloroethane 70-130
11238.133.9µg/m3Tetrachloroethene 70-130
10515.414.7µg/m3Tetrahydrofuran 70-130
11120.818.8µg/m3Toluene 70-130
11442.237.1µg/m31,2,4-Trichlorobenzene 70-130
10428.527.3µg/m31,1,1-Trichloroethane 70-130
11130.427.3µg/m31,1,2-Trichloroethane 70-130
11029.626.9µg/m3Trichloroethene 70-130
10429.228.1µg/m3Trichlorofluoromethane 70-130
11428.124.6µg/m31,2,4-Trimethylbenzene 70-130
11628.524.6µg/m31,3,5-Trimethylbenzene 70-130
11119.517.6µg/m3Vinyl Acetate 70-130
10413.312.8µg/m3Vinyl Chloride 70-130
11424.721.7µg/m3o-Xylene 70-130
11549.843.4µg/m3m,p-Xylene 70-130
1064-Bromofluorobenzene (S)70-130
Page 10 of 10Date:09/10/2021 11:50 AM
Page 43 of 45
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-242-0017
NOVA Engineering & Environmental
01151
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:NA
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:09/02/2021 16:23:58
Special precautions or instructions included?
Comments:
Page 44 of 45
Page 45 of 45

APPENDIX E

RISK CALCULATOR RESULTS

DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID:
Exposure Unit ID: SV-1
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 33.4 1.002 -6.5E+03 3.1E-05
71-43-2 Benzene 1.41 0.0423 3.6E-01 6.3E+00 1.2E-07 1.4E-03
75-15-0 Carbon Disulfide 0.38 0.0114 -1.5E+02 1.6E-05
56-23-5 Carbon Tetrachloride 0.547 0.01641 4.7E-01 2.1E+01 3.5E-08 1.6E-04
74-87-3 Chloromethane 0.747 0.02241 -1.9E+01 2.4E-04
110-83-8 Cyclohexene 3.09 0.0927 -2.1E+02 8.9E-05
75-71-8 Dichlorodifluoromethane 3.1 0.093 -2.1E+01 8.9E-04
100-41-4 Ethylbenzene 0.56 0.0168 1.1E+00 2.1E+02 1.5E-08 1.6E-05
142-82-5 Heptane, N-0.68 0.0204 -8.3E+01 4.9E-05
110-54-3 Hexane, N-1.06 0.0318 -1.5E+02 4.4E-05
78-83-1 Isobutyl Alcohol 4.88 0.1464 --
78-93-3 Methyl Ethyl Ketone (2-Butanone)3.26 0.0978 -1.0E+03 1.9E-05
1634-04-4 Methyl tert-Butyl Ether (MTBE)1.12 0.0336 1.1E+01 6.3E+02 3.1E-09 1.1E-05
108-11-2 Methyl-2-Pentanol, 4-0.664 0.01992 - 6.3E+02 6.4E-06
75-09-2 Methylene Chloride 1.01 0.0303 1.0E+02 1.3E+02 3.0E-10 4.8E-05
115-07-1 Propylene 2.58 0.0774 -6.3E+02 2.5E-05
100-42-5 Styrene 13.1 0.393 - 2.1E+02 3.8E-04
127-18-4 Tetrachloroethylene 2 0.06 1.1E+01 8.3E+00 5.6E-09 1.4E-03
108-88-3 Toluene 1.79 0.0537 -1.0E+03 1.0E-05
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-0.613 0.01839 -1.0E+03 3.5E-06
75-69-4 Trichlorofluoromethane 2.43 0.0729 --
1330-20-7 Xylenes 1.79 0.0537 -2.1E+01 5.1E-04
Cumulative: 1.8E-07 5.3E-03
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID:
Exposure Unit ID: SV-2
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 138 4.14 -6.5E+03 1.3E-04
71-43-2 Benzene 66.5 1.995 3.6E-01 6.3E+00 5.5E-06 6.4E-02
75-15-0 Carbon Disulfide 70.1 2.103 -1.5E+02 2.9E-03
56-23-5 Carbon Tetrachloride 4.7E-01 2.1E+01
74-87-3 Chloromethane -1.9E+01
110-83-8 Cyclohexene 50.2 1.506 -2.1E+02 1.4E-03
75-71-8 Dichlorodifluoromethane -2.1E+01
100-41-4 Ethylbenzene 518 15.54 1.1E+00 2.1E+02 1.4E-05 1.5E-02
142-82-5 Heptane, N-112 3.36 -8.3E+01 8.1E-03
110-54-3 Hexane, N-46.7 1.401 -1.5E+02 1.9E-03
78-83-1 Isobutyl Alcohol 14.7 0.441 --
78-93-3 Methyl Ethyl Ketone (2-Butanone)19.9 0.597 -1.0E+03 1.1E-04
1634-04-4 Methyl tert-Butyl Ether (MTBE)1.1E+01 6.3E+02
108-11-2 Methyl-2-Pentanol, 4-13.4 0.402 - 6.3E+02 1.3E-04
75-09-2 Methylene Chloride 1.0E+02 1.3E+02
115-07-1 Propylene 298 8.94 -6.3E+02 2.9E-03
100-42-5 Styrene - 2.1E+02
127-18-4 Tetrachloroethylene 4330 129.9 1.1E+01 8.3E+00 1.2E-05 3.1E+00
108-88-3 Toluene 460 13.8 -1.0E+03 2.6E-03
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2--1.0E+03
75-69-4 Trichlorofluoromethane --
1330-20-7 Xylenes 1320 39.6 -2.1E+01 3.8E-01
Cumulative: 3.1E-05 3.6E+00
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID:
Exposure Unit ID: SV-3
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 78.3 2.349 -6.5E+03 7.3E-05
71-43-2 Benzene 29.1 0.873 3.6E-01 6.3E+00 2.4E-06 2.8E-02
75-15-0 Carbon Disulfide 14.9 0.447 -1.5E+02 6.1E-04
56-23-5 Carbon Tetrachloride 0.585 0.01755 4.7E-01 2.1E+01 3.8E-08 1.7E-04
67-66-3 Chloroform 1.87 0.0561 1.2E-01 2.0E+01 4.6E-07 5.5E-04
74-87-3 Chloromethane 0.599 0.01797 -1.9E+01 1.9E-04
110-83-8 Cyclohexene 7.48 0.2244 -2.1E+02 2.2E-04
106-46-7 Dichlorobenzene, 1,4-13.7 0.411 2.6E-01 1.7E+02 1.6E-06 4.9E-04
75-71-8 Dichlorodifluoromethane 2.78 0.0834 -2.1E+01 8.0E-04
156-60-5 Dichloroethylene, trans-1,2-2.93 0.0879 -8.3E+00 2.1E-03
100-41-4 Ethylbenzene 8.08 0.2424 1.1E+00 2.1E+02 2.2E-07 2.3E-04
111-71-7 Heptanal, n-13.7 0.411 -6.3E-01 1.3E-01
110-54-3 Hexane, N-13.5 0.405 -1.5E+02 5.5E-04
78-83-1 Isobutyl Alcohol 9.25 0.2775 --
78-93-3 Methyl Ethyl Ketone (2-Butanone)12.8 0.384 -1.0E+03 7.4E-05
1634-04-4 Methyl tert-Butyl Ether (MTBE)1.2 0.036 1.1E+01 6.3E+02 3.3E-09 1.2E-05
108-11-2 Methyl-2-Pentanol, 4-3.41 0.1023 - 6.3E+02 3.3E-05
75-09-2 Methylene Chloride 0.973 0.02919 1.0E+02 1.3E+02 2.9E-10 4.7E-05
115-07-1 Propylene 75.8 2.274 -6.3E+02 7.3E-04
100-42-5 Styrene 3.48 0.1044 - 2.1E+02 1.0E-04
127-18-4 Tetrachloroethylene 1650 49.5 1.1E+01 8.3E+00 4.6E-06 1.2E+00
108-88-3 Toluene 153 4.59 -1.0E+03 8.8E-04
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-5.6 0.168 -1.0E+03 3.2E-05
79-01-6 Trichloroethylene 1.59 0.0477 4.8E-01 4.2E-01 1.0E-07 2.3E-02
75-69-4 Trichlorofluoromethane 12 0.36 --
95-63-6 Trimethylbenzene, 1,2,4-1.95 0.0585 -1.3E+01 9.3E-04
108-67-8 Trimethylbenzene, 1,3,5-0.826 0.02478 -1.3E+01 4.0E-04
75-01-4 Vinyl Chloride 0.828 0.02484 1.7E-01 2.1E+01 1.5E-07 2.4E-04
1330-20-7 Xylenes 26.9 0.807 -2.1E+01 7.7E-03
Cumulative: 9.6E-06 1.4E+00
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID:
Exposure Unit ID: SV-4
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 254 7.62 -6.5E+03 2.4E-04
71-43-2 Benzene 34.3 1.029 3.6E-01 6.3E+00 2.9E-06 3.3E-02
75-15-0 Carbon Disulfide 127 3.81 -1.5E+02 5.2E-03
56-23-5 Carbon Tetrachloride 4.7E-01 2.1E+01
74-87-3 Chloromethane -1.9E+01
110-83-8 Cyclohexene 1600 48 -2.1E+02 4.6E-02
75-71-8 Dichlorodifluoromethane -2.1E+01
100-41-4 Ethylbenzene 1210 36.3 1.1E+00 2.1E+02 3.2E-05 3.5E-02
142-82-5 Heptane, N--8.3E+01
110-54-3 Hexane, N-115 3.45 -1.5E+02 4.7E-03
78-83-1 Isobutyl Alcohol 82.1 2.463 --
78-93-3 Methyl Ethyl Ketone (2-Butanone)55.6 1.668 -1.0E+03 3.2E-04
1634-04-4 Methyl tert-Butyl Ether (MTBE)1.1E+01 6.3E+02
108-11-2 Methyl-2-Pentanol, 4-- 6.3E+02
75-09-2 Methylene Chloride 1.0E+02 1.3E+02
115-07-1 Propylene 360 10.8 -6.3E+02 3.5E-03
100-42-5 Styrene - 2.1E+02
127-18-4 Tetrachloroethylene 1400 42 1.1E+01 8.3E+00 3.9E-06 1.0E+00
108-88-3 Toluene 432 12.96 -1.0E+03 2.5E-03
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2--1.0E+03
75-69-4 Trichlorofluoromethane --
1330-20-7 Xylenes 1650 49.5 -2.1E+01 4.7E-01
Cumulative: 3.9E-05 1.6E+00
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID:
Exposure Unit ID: SV-5
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 254 7.62 -6.5E+03 2.4E-04
71-43-2 Benzene 34.3 1.029 3.6E-01 6.3E+00 2.9E-06 3.3E-02
75-15-0 Carbon Disulfide 127 3.81 -1.5E+02 5.2E-03
56-23-5 Carbon Tetrachloride 4.7E-01 2.1E+01
74-87-3 Chloromethane -1.9E+01
110-83-8 Cyclohexene 1600 48 -2.1E+02 4.6E-02
75-71-8 Dichlorodifluoromethane -2.1E+01
100-41-4 Ethylbenzene 1210 36.3 1.1E+00 2.1E+02 3.2E-05 3.5E-02
142-82-5 Heptane, N-3800 114 -8.3E+01 2.7E-01
110-54-3 Hexane, N-115 3.45 -1.5E+02 4.7E-03
78-83-1 Isobutyl Alcohol 82.1 2.463 --
78-93-3 Methyl Ethyl Ketone (2-Butanone)55.6 1.668 -1.0E+03 3.2E-04
1634-04-4 Methyl tert-Butyl Ether (MTBE)1.1E+01 6.3E+02
108-11-2 Methyl-2-Pentanol, 4-- 6.3E+02
75-09-2 Methylene Chloride 1.0E+02 1.3E+02
115-07-1 Propylene 360 10.8 -6.3E+02 3.5E-03
100-42-5 Styrene - 2.1E+02
127-18-4 Tetrachloroethylene 1400 42 1.1E+01 8.3E+00 3.9E-06 1.0E+00
108-88-3 Toluene 432 12.96 -1.0E+03 2.5E-03
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2--1.0E+03
75-69-4 Trichlorofluoromethane --
1330-20-7 Xylenes 1650 49.5 -2.1E+01 4.7E-01
Cumulative: 3.9E-05 1.9E+00
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID:
Exposure Unit ID: SV-6
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 99 2.97 -6.5E+03 9.2E-05
71-43-2 Benzene 34.6 1.038 3.6E-01 6.3E+00 2.9E-06 3.3E-02
75-15-0 Carbon Disulfide 176 5.28 -1.5E+02 7.2E-03
67-66-3 Chloroform 16.5 0.495 1.2E-01 2.0E+01 4.1E-06 4.8E-03
74-87-3 Chloromethane 9.37 0.2811 -1.9E+01 3.0E-03
110-83-8 Cyclohexene 164 4.92 -2.1E+02 4.7E-03
106-46-7 Dichlorobenzene, 1,4-12 0.36 2.6E-01 1.7E+02 1.4E-06 4.3E-04
100-41-4 Ethylbenzene 1310 39.3 1.1E+00 2.1E+02 3.5E-05 3.8E-02
142-82-5 Heptane, N-561 16.83 -8.3E+01 4.0E-02
110-54-3 Hexane, N-34.1 1.023 -1.5E+02 1.4E-03
78-83-1 Isobutyl Alcohol 11.7 0.351 --
78-93-3 Methyl Ethyl Ketone (2-Butanone)13.5 0.405 -1.0E+03 7.8E-05
75-09-2 Methylene Chloride 15.1 0.453 1.0E+02 1.3E+02 4.5E-09 7.2E-04
115-07-1 Propylene 179 5.37 -6.3E+02 1.7E-03
127-18-4 Tetrachloroethylene 2470 74.1 1.1E+01 8.3E+00 6.9E-06 1.8E+00
108-88-3 Toluene 478 14.34 -1.0E+03 2.8E-03
75-69-4 Trichlorofluoromethane 9.21 0.2763 --
95-63-6 Trimethylbenzene, 1,2,4-13.6 0.408 -1.3E+01 6.5E-03
108-67-8 Trimethylbenzene, 1,3,5-72.8 2.184 -1.3E+01 3.5E-02
1330-20-7 Xylenes 2700 81 -2.1E+01 7.8E-01
Cumulative: 5.0E-05 2.7E+00
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID:
Exposure Unit ID: SV-7
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 90.1 2.703 -6.5E+03 8.4E-05
71-43-2 Benzene 10.4 0.312 3.6E-01 6.3E+00 8.7E-07 1.0E-02
75-15-0 Carbon Disulfide 8.41 0.2523 -1.5E+02 3.5E-04
56-23-5 Carbon Tetrachloride 4.7E-01 2.1E+01
74-87-3 Chloromethane -1.9E+01
110-83-8 Cyclohexene 32.1 0.963 -2.1E+02 9.2E-04
75-71-8 Dichlorodifluoromethane -2.1E+01
100-41-4 Ethylbenzene 409 12.27 1.1E+00 2.1E+02 1.1E-05 1.2E-02
142-82-5 Heptane, N-67 2.01 -8.3E+01 4.8E-03
110-54-3 Hexane, N--1.5E+02
78-83-1 Isobutyl Alcohol 14.1 0.423 --
78-93-3 Methyl Ethyl Ketone (2-Butanone)6.43 0.1929 -1.0E+03 3.7E-05
1634-04-4 Methyl tert-Butyl Ether (MTBE)1.1E+01 6.3E+02
108-11-2 Methyl-2-Pentanol, 4-- 6.3E+02
75-09-2 Methylene Chloride 1.0E+02 1.3E+02
115-07-1 Propylene -6.3E+02
100-42-5 Styrene - 2.1E+02
127-18-4 Tetrachloroethylene 2210 66.3 1.1E+01 8.3E+00 6.1E-06 1.6E+00
108-88-3 Toluene 221 6.63 -1.0E+03 1.3E-03
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2--1.0E+03
75-69-4 Trichlorofluoromethane --
1330-20-7 Xylenes 1090 32.7 -2.1E+01 3.1E-01
Cumulative: 1.8E-05 1.9E+00
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID:
Exposure Unit ID: DUP-1
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 119 3.57 -6.5E+03 1.1E-04
71-43-2 Benzene 24 0.72 3.6E-01 6.3E+00 2.0E-06 2.3E-02
75-15-0 Carbon Disulfide 17.9 0.537 -1.5E+02 7.4E-04
110-83-8 Cyclohexene 58.5 1.755 -2.1E+02 1.7E-03
100-41-4 Ethylbenzene 710 21.3 1.1E+00 2.1E+02 1.9E-05 2.0E-02
142-82-5 Heptane, N-165 4.95 -8.3E+01 1.2E-02
110-54-3 Hexane, N-12 0.36 -1.5E+02 4.9E-04
78-83-1 Isobutyl Alcohol 11.5 0.345 --
78-93-3 Methyl Ethyl Ketone (2-Butanone)12.5 0.375 -1.0E+03 7.2E-05
127-18-4 Tetrachloroethylene 3070 92.1 1.1E+01 8.3E+00 8.5E-06 2.2E+00
108-88-3 Toluene 376 11.28 -1.0E+03 2.2E-03
95-63-6 Trimethylbenzene, 1,2,4-31.8 0.954 -1.3E+01 1.5E-02
108-67-8 Trimethylbenzene, 1,3,5-125 3.75 -1.3E+01 6.0E-02
1330-20-7 Xylenes 1770 53.1 -2.1E+01 5.1E-01
Cumulative: 2.9E-05 2.9E+00
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator

APPENDIX F

RECEPTOR SURVEY
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site:Doggett Street/ West Tremont Avenue Site
Address:305 Doggett Street and 242/306 West Tremont Avenue
City:Charlotte
County:Mecklenburg
Brownfields Project Number:24052-20-060
Date 9/8/2021
Property and Building Characteristics
a. Provide occupancy and use information.
The property is currently unoccupied. Formerly Gas-Fired Products, a manufacturer of space heaters.
305 Doggett Street consists of three (3) buildings. Building one is a 10,200 sf single story brick and CMU
warehouse. Building 2 is a two (2) story brick and CMU manufacturing and office building which is 24,024 sf.
Building 3 is a single story wood garage totaling 600 sf.
306 West Tremont contains one (1) 2-story brick, metal and wood,warehouse building including 11,644 sf.
242 West Tremont contains one (1) 1-story CMU and metal light manufacturing building including 10,370 sf.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
Each of the buildings are slab-on-grade, with concrete construction.
The buildings use roof top package units, and split systems for the offices. The warehouse buildings have area
heaters.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
None
75%
NA
0%
5%
0%
Size of Property (acres)
% of property that is wooded/brush
2.441
0%
5%
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air
return, and design considerations (e.g. positive pressure?).
0%
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the
information requested below. Distances are measured from the site property boundary unless otherwise indicated
by the DEQ Brownfield’s Project Manager (PM).
Current Usage Proposed UsageSurface Conditions
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved 20%
75%
20%
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets
as needed. If numerous buildings are on-site, consult with your PM as only information on specific buildings may
be needed.
b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings
(e.g. windows, bay doors), and height (number of stories).
% of property that is covered by buildings
Rev. 09/2015 Page 1 of 4
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Rev. 09/2015 Page 2 of 4
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
South
East
West
N
Y Adjacent NSEW
N
Utilities
Is there a septic system on-site? (Y or N) _____N____
Please provide the utility providers for the subject property
a. Natural Gas ___Peidmont Natural Gas________________________
b. Sewer __City of Charlotte_________________________
c. Electricity _____Duke Energy______________________
d. Other __________________________
For surrounding properties, please complete the following table with available information.
Y On N & S
Y On N & S
N
Y On N & S
Y On N & S
N
N
Zoning/Land Use Proposed Usage Current Use/Occupant
DirectionDistance
(ft)Address
Unknown
Please provide information on the following land uses in the vicinity of the subject site, including a map of the
surrounding areas. If specific receptors are present, please provide addresses of the facilities.
Commercial and Residential
Commercial
Commercial and Residential
Residential
For the subject property, please provide a map of known buried utilites. If available, include depth to top,
construction material, and diameter of the utilities. In addition, please provide the following information on utilty
providers. If additional assessment is required, the public utility locators should be contacted. This information
can then be added to a site map.
Y/N *
Is a school or daycare center within 1,000 ft of the
Property?
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific
addresses.
Distance
(ft)
See Map
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with
the subject property.
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
Unknown
Unknown
Unknown
Is there a basement within 1,000 ft of the Property
Is there a residence within 1,000 ft of the Property?
Utility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
Is a sanitary sewer within 100 ft of the Property boundary?
Rev. 09/2015 Page 3 of 4
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public Yes___ Private ______
N
N
N
Surface Water & Wetlands
Are there surface water features on the
property? (If yes, please complete a. to d.)
Provide Information regarding Surface Water
and Wetlands
Distance
(ft)Direction Address
a. Is the water body naturally developed or
man-made?
Y/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a
minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if
water supply or irrigation wells may be present. Information from applicable databases can and should be
utilized; however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the
requested radius, please provide a map of the well locations. If needed, please attach a separate table to list all
wells. Please note, the PM may opt for a more extensive water supply well survey if needed.
No
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public,
please include the water providers name.
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property
boundary?Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in
the vicinity of the Property.
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
b. List the uses of the water body.
c. What is the source of the water for the
water body?
d. What is the nature of the bottom of the
water body (e.g., rocky or concrete bottom,
drainage ways or impoundments)
If no on-site surface water features, what is the
nearest surface water body?
Are there any wetlands present on the
property? If no wetlands on-site, are wetlands
suspected on adjoining properties?
Rev. 09/2015 Page 4 of 4

FIGURE
Receptor

SOURCE: Mecklenburg GIS
SCALE: As Shown
COUSINS TREMONT DOGGETT. LP
Doggett Street/West Tremont Avenue
Charlotte, Mecklenburg County, North Carolina
NOVA Project Number 3021011

Residential Properties
1,000’

APPENDIX G

QUALIFICATIONS OF CONCLUSIONS

QUALIFICATIONS OF CONCLUSIONS

The findings and opinions presented are relative to the dates of our site work and
should not be relied on to represent conditions at substantially later dates or
locations not investigated.

The opinions included herein are based on information obtained during the study and
our experience. If additional information becomes available which might impact our
environmental conclusions, we request the opportunity to review the information,
reassess the potential concerns and modify our opinions, if necessary.

Assessments may include interviews, a review of documents prepared by others or
other secondary information sources. NOVA has not verified the provided information
and has no responsibility for the accuracy or completeness of the information.

Although this assessment has attempted to identify the potential for environmental
impacts to the subject property, potential sources of contamination may have
escaped detection due to: (1) the limited scope of this assessment, (2) the
inaccuracy of public records, (3) the presence of undetected or unreported
environmental incidents, (4) inaccessible areas and/or (5) deliberate concealment of
detrimental information. It was not the purpose of this study to determine the actual
presence, degree or extent of contamination at the site, except as specifically
described in the previous sections of this report. This would require additional
exploratory work, including supplemental sampling and laboratory analysis.

This report is intended for the sole use of Cousins Tremont Doggett LP. The scope of
work performed during this study was developed for purposes specifically intended
by Cousins Tremont Doggett LP and may not satisfy other user requirements. Use of
this report or the findings and conclusions by others will be at the sole risk of the
user.

Our professional services have been performed, our findings obtained, our
conclusions derived and our recommendations prepared in accordance with
generally accepted engineering practices and principles. This statement is in lieu of
all other statements or warranties, either expressed or implied.