5002_JacksonCounty_MSWLF_Oct21GW_FID1646953_20220303

DENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No) Doc/Event #:
NC DENR I IEnvironmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Anchor QEA of North Carolina, PLLC
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Chuck Pippin Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Jackson County Municipal Solid US Highway 441 50-02 .1600 October 19 and 20, 2021
Waste Landfill Dillsboro, North Carolina 28725
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑ Detection Monitoring ❑X Assessment Monitoring ❑ Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑
Groundwater monitoring data from private water supply wells ❑X
Leachate monitoring data ❑
Surface water monitoring data
Methane gas monitoring data
Corrective action data (specify) Natural Attenuation Parameters
Other(specifv
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Chuck Pippin, P.G. Project Manager 828-281-3350
Facility Representat' a Title (Area Code) Telephone Number
3/3/2022 Affix NC Licensed/ Professional Geologist Seal
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Signature Date �� CQR
•Q.� �GEN"
231 Haywood Street Asheville, North Carolina 28801 O
Facility Representative Address * S AL €�
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P-1649 3/3/223
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NC PE Firm License Number (if applicable effective May 1, 2009) �.,��Q� Q\Ap
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Revised 6/2009 ,�,y�'�l+'

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February 2022 ANCHOR
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02 QEA
Fall 2021
Semiannual Water Quality Monitoring Report
Prepared for Jackson County Solid Waste Department

February 2022
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
Fall 2021
Semiannual Water Quality Monitoring Report
Prepared for
Jackson County Solid Waste Department
401 Grindstaff Cove Road
Sylva, North Carolina 28779
Chuck Pippin, PG
Project Geologist
Prepared by
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Steve Colquhoun
Staff Professional
i
Project Number: C01480-01.02
\\Athena\Asheville\Projects\Jackson County\ -Reports - Groundwater\2021\02_Fall 2021\Deliverables\Final Submittal\Jackson County -Semiannual Water
Quality Report_Fall_2021.docx

Table of Contents
Table of Contents
Abbreviations
1 Introduction
1
2 Semiannual Monitoring...........................................................................................................3
2.1 Groundwater, Surface Water, Domestic Well, and Leachate Sampling..........................................3
2.1.1 Monitoring Well Purging and Sampling Methods.................................................................3
2.1.2 Surface Water Sampling Methods................................................................................................4
2.1.3 Leachate Sampling Methods..........................................................................................................4
2.1.4 Domestic Well Sampling Methods...............................................................................................5
2.2 Sample Handling, Documentation, and Analysis....................................................................................5
3 Findings........................................................................................................................................7
3.1
Groundwater.........................................................................................................................................................7
3.1.1 Field Parameters..................................................................................................................................8
3.1.2 Appendix II Metals (Total)................................................................................................................8
3.1.3 Appendix II Metals (Dissolved).......................................................................................................9
3.1.4 Appendix II VOCs and 1,4-Dioxane..............................................................................................9
3.1.5 Natural Attenuation Parameters.................................................................................................
10
3.2
Surface Water....................................................................................................................................................
10
3.2.1 Field Parameters...............................................................................................................................
10
3.2.2 Appendix II Metals...........................................................................................................................
11
3.2.3 Appendix II VOCs and 1,4-Dioxane...........................................................................................
11
3.3
Leachate...............................................................................................................................................................11
3.4
Domestic Well....................................................................................................................................................
12
3.4.1 Field Parameters...............................................................................................................................
12
3.4.2 VOCs......................................................................................................................................................
12
3.5
Groundwater Flow Directions......................................................................................................................
12
4 Summary....................................................................................................................................13
4.1 Groundwater Quality...................................................................................................................................... 13
4.1.1 Appendix II Metals........................................................................................................................... 13
4.1.2 Appendix II Volatile Organic Compounds and 1,4-Dioxane............................................ 13
4.1.3 Field Parameters and Other Constituents............................................................................... 13
Fall 2021 Semiannual
Water Quality Monitoring Report i February 2022

4.2 Surface Water Quality..................................................................................................................................... 14
4.3 Leachate Quality............................................................................................................................................... 14
4.4 Domestic Well Water Quality...................................................................................................................... 14
5 Future Activities
6 References
TABLES
Table 1 Summary of Laboratory Analyses Performed on Samples
Table 2 Well Construction Details and Corresponding Elevations
Table 3 Analytical Summary
Table 4 Mass Removal Calculations for VOCs Detected in the Leachate Sample (LT-01)
FIGURES
Figure 1
Site Location Map
Figure 2
Site Layout Map
Figure 3
Generalized Groundwater Flow Direction
Figure 4
Hydrograph and Constituents of Concern Versus Time —
MW-01
Figure 5
Hydrograph and Constituents of Concern Versus Time —
MW-02
Figure 6
Hydrograph and Constituents of Concern Versus Time —
MW-03
Figure 7
Hydrograph and Constituents of Concern Versus Time —
MW-04
Figure 8
Hydrograph and Constituents of Concern Versus Time —
MW-05R
Figure 9
Hydrograph and Constituents of Concern Versus Time —
MW-06
Figure 10
Hydrograph and Constituents of Concern Versus Time —
MW-07
APPENDICES
Appendix A Well Sampling Logs, and Equipment Documentation and Instrument Calibration
Data Sheets
Appendix B Reports of Laboratory Analysis, Chain -of -Custody Documentation,
and Certificates of Analysis
15
16
Fall 2021 Semiannual
Water Quality Monitoring Report ii February 2022

Abbreviations
pg/L
micrograms per liter
pmhos/cm
micromhos per centimeter
2L standard
15A NCAC 2L.0202 Groundwater Standard
CAER
Five -Year Corrective Action Evaluation Report
CAP
Corrective Action Plan
DEQ
North Carolina Department of Environmental Quality
DO
dissolved oxygen
EPA
U.S. Environmental Protection Agency
IMAC
interim maximum allowable concentration
J
joule
MDL
method detection limit
mg/L
milligrams per liter
MNA
monitored natural attenuation
mV
millivolts
NCAC
North Carolina Administrative Code
NTU
nephelometric turbidity unit
ORP
oxidation reduction potential
PWR
partially weathered rock
SC
specific conductivity
Site
closed Municipal Solid Waste Landfill
SM
Standard Method
SU
standard unit
SWS
Solid Waste Section
TWSA
Tuckasegee Water & Sewer Authority
VOC
volatile organic compound
Fall 2021 Semiannual
Water Quality Monitoring Report iii February 2022

1 Introduction
The Jackson County Solid Waste Department maintains a closed Municipal Solid Waste Landfill (Site)
approximately 0.75 mile west of Dillsboro, North Carolina, on the northeast side of
Old Dillsboro Road (Old U.S. Highway 74; Figure 1). Water quality monitoring at the landfill is
governed by the North Carolina Department of Environmental Quality (DEQ), Division of Waste
Management, Solid Waste Section (SWS), under Permit No. 50-02 issued to Jackson County. The
landfill permit requires semiannual monitoring of groundwater and surface water quality.
Since October 2007, when Anchor QEA of North Carolina, PLLC, began performing water quality
monitoring events at the Site, groundwater quality monitoring has indicated persistent low-level
concentrations of constituents that exceeded groundwater quality standards. In response to the
continued exceedances of the analyzed constituents, an Assessment of Corrective Measures was
submitted to the North Carolina Department of Environment and Natural Resources (now DEQ) on
September 7, 2010 (Altamont 2010). A Corrective Action Plan (CAP; Altamont 2011) was implemented
upon approval by the North Carolina Department of Environmental and Natural Resources, as
recorded in the September 1, 2011 letter regarding "Approval of the County's Corrective Action Plan"
(DENR 2011). The implemented remedy includes the extraction of leachate through dedicated
submersible pumps installed within landfill gas extraction wells and disposal of the leachate into the
Tuckasegee Water & Sewer Authority (TWSA) collection system. In addition to the leachate
extraction, groundwater natural attenuation parameters are monitored, and natural attenuation
processes are evaluated. As discussed in the CAP, a corrective action evaluation report is prepared
every 5 years. The evaluation report analyzes the progress of the approved corrective action remedy
based on semiannual water quality monitoring data. The remedy was implemented in a phased
approach, with full implementation occurring on September 6, 2013. The first Five -Year Corrective
Action Evaluation Report (CAER), submitted by Altamont on October 31, 2016 (Altamont 2016),
concluded that the current conditions of the monitored natural attenuation (MNA) parameters and
Site geochemical parameters allow for the slow degradation of the select contaminants identified in
the CAER. The second CAER was submitted by Anchor QEA on January 13, 2022, and concluded that
the leachate extraction system has improved but still does not align with the anticipated
performance as modeled in the CAP.
This report serves as the second semiannual water quality monitoring report for 2021. The report
provides an evaluation of groundwater and surface water quality. The water quality monitoring
network is presented in Figure 2. The generalized groundwater flow direction in the upper parts of
the underlying aquifer system is provided in Figure 3. In addition to groundwater and surface water
monitoring, this report includes analysis of the extracted leachate and two domestic water wells. The
water samples collected from selected monitoring points during the spring sampling event were
analyzed for a range of parameters, as presented in Section 2.2 and Table 1. The fall 2021 sampling
Fall 2021 Semiannual
Water Quality Monitoring Report 1 February 2022

event was performed on October 19 and 20, 2021, and is being reported in accordance with
requirements stipulated in the DEQ Solid Waste Management Rules codified under Title 15A,
Subchapter 13B of the North Carolina Administrative Code (NCAC).
Fall 2021 Semiannual
Water Quality Monitoring Report 2 February 2022

2 Semiannual Monitoring
2.1 Groundwater, Surface Water, Domestic Well, and Leachate
Sampling
The Site monitoring wells (MW-01, MW-02, MW-03, MW-04, MW-05R, MW-06, and MW-07), surface
water sample locations (SW-01 and SW-02), leachate sample location (LT-01), and domestic wells
(DW-01 and DW-02) were sampled on October 19 and 20, 2021, by Anchor QEA. Static groundwater
level measurements and field parameter data are included on the sampling logs presented in
Appendix A. Field equipment calibration logs for the YSI Professional Plus Multiparameter Water
Quality Meter and the Hach 2100Q Turbidimeter are also provided in Appendix A. The full suite of
groundwater and surface water laboratory analytical results is presented in the laboratory analysis
reports in Appendix B.
Monitoring wells MW-01 and MW-06 are considered to be the Site's upgradient monitoring wells;
MW-03 and MW-05R are located in the midgradient portion of the Site; and MW-02, MW-04, and
MW-07 monitor downgradient portions of the Site. As summarized in Table 2, the total depths of the
monitoring wells range from 40 to 110 feet below ground surface. The geology of the screened
intervals of the monitoring wells is as follows:
• Saprolite': MW-04 and MW-05R
• Partially weathered rock (PWR)z: MW-03
• Bedrock3: MW-01, MW-02, MW-06, and MW-07
The locations of the monitoring wells, surface water samples, leachate, and domestic well sample
locations are shown in Figure 2.
2.1. 7 Monitoring Well Purging and Sampling Methods
Before the monitoring wells were sampled, the static water level was gauged in each well, and an
initial round of field parameters was measured (consisting of pH, specific conductivity [SC], dissolved
oxygen [DO], turbidity, temperature, and oxidation reduction potential [ORP]).
Anchor QEA personnel used either low -flow techniques or disposable bailers to purge the
monitoring wells and collect groundwater samples. The total depth, condition of the casing, and
groundwater recharge rate determined the purging and sample collection method employed at each
monitoring well.
Saprolite is the result of in -place weathering that produces soil -like material that retains relict features of the parent rock.
z PWR is generally found above the bedrock and is softer than bedrock, but not as soft as saprolite.
3 Bedrock is solid competent rock that underlies Saprolite and partially weathered rock.
Fall 2021 Semiannual
Water Quality Monitoring Report 3 February 2022

Four of the monitoring wells (MW-03, MW-04, MW-06, and MW-07) were purged using low -flow
techniques in accordance with the procedures described by the U.S. Environmental Protection
Agency (EPA) in Low -Flow (Minimal Drawdown) Ground -Water Sampling Procedures (EPA 1996).
During purging, the field parameters (pH, SC, DO, ORP, turbidity, and temperature) were measured
and recorded approximately every 3 minutes. Well purging continued until these parameters had
generally stabilized for three consecutive readings. The required stabilization criteria are determined
by the EPA Region 4 Science and Ecosystem Support Division in Operating Procedure: Groundwater
Sampling (EPA 2017) and are summarized as follows:
• pH values within ±0.1 standard unit (SU)
• SC values within ±5%
• Temperature, DO, and turbidity values within ±10%
• ORP values within ±10 millivolts (mV)
Once the parameters had stabilized, a groundwater sample was collected by field personnel wearing
a new pair of nitrile gloves, using laboratory -supplied sample containers.
Because of their slow recharge rates, monitoring wells MW-01, MW-02, and MW-05R were purged
and sampled using disposable bailers. The wells were purged of three successive well volumes or
purged dry, whichever occurred first. Monitoring well MW-02 was purged dry on October 19 and
sampled on October 20, 2021, after the well had sufficient time to recharge. Monitoring well
MW-05R was purged dry in the morning on October 19, 2021, and sampled later that day after the
well had sufficient time to recharge. Monitoring well MW-01 was purged and sampled on
October 20, 2021. A round of field parameters was measured and recorded at the start of purging
and after each consecutive well volume had been purged.
Field parameter data are shown in the well sampling logs included in Appendix A.
2.1.2 Surface Water Sampling Methods
Surface water samples SW-01 and SW-02 were collected on October 19, 2021, at designated
locations from the Tuckasegee River, which is adjacent to and southwest of the landfill (Figure 2).
Sampling location SW-01 is assumed to represent surface water quality upstream of the landfill, and
sampling location SW-02 is assumed to represent surface water quality downstream of the landfill.
One round of field parameters was measured and recorded at each surface water sampling location
immediately prior to collecting the sample (Appendix A). The surface water samples were collected in
laboratory -provided sample containers by a technician wearing a new pair of nitrile gloves.
2.1.3 Leachate Sampling Methods
Dedicated bottom -loading air -powered pumps, air pressure lines, and a leachate force main
collection system are installed at the landfill. Pumps are installed in landfill gas extraction wells
Fall 2021 Semiannual
Water Quality Monitoring Report 4 February 2022

EW-1 R, EW-2R, EW-3R, EW-4, EW-5, EW-6, EW-7, EW-8, EW-9, and EW-10. The gas extraction well
locations are presented in Figure 2. The leachate is pumped from the wells into a flow equalization
tank, which is connected to the TWSA wastewater collection system.
The flow equalization tank is east of the landfill, adjacent to the existing landfill gas flare. A grab
sample of leachate (LT-01) was acquired on October 20, 2021, by collecting a sample as the leachate
entered the flow equalization tank. One round of field parameters was measured and recorded after
the sample was collected (Appendix A).
2.7.4 Domestic Well Sampling Methods
The domestic well water samples (DW-01 and DW-02) were collected on October 20, 2021, from an
outside spigot at the residence located at 318 Joe Wilkey Road (DW-01) and 138 Joe Wilkey Road
(DW-02), bordering the northern boundary of the landfill (Figure 2). The wells were purged of
30 gallons prior to sample collection. One round of field parameters was measured and recorded
after the 30 gallons had been purged. The domestic well water samples were collected in laboratory -
provided sample containers by field personnel wearing new nitrile gloves.
2.2 Sample Handling, Documentation, and Analysis
It should be noted that during most semiannual sampling events at the Jackson County Landfill,
water quality samples are submitted for Appendix I parameters only. A larger suite of Appendix II
parameters as noted below are analyzed for during the fall sampling event only on a biannual basis.
Field parameters and additional observations pertaining to the Site sampling locations are provided
in the sampling logs (Appendix A). Following sample collection, each groundwater, surface water,
leachate, and domestic well water sample was immediately placed on ice in a sample cooler for
transport to Waypoint Analytical Laboratories, a North Carolina -certified laboratory in Charlotte,
North Carolina. The groundwater samples collected from the monitoring wells were analyzed for the
following parameters (Table 1):
• Appendix II metals, including mercury, using EPA Methods 6020B and 7470A
• Appendix II volatile organic compounds (VOCs) using EPA Method 8260D
• Appendix II semivolatile organic compounds using EPA Method 8270D
• 1,4-dioxane using EPA Method 8260DSIM
• MNA parameters:
— Alkalinity using Standard Method (SM) 2320B
— Biochemical oxygen demand (5-day) using SM 5210B
— Chemical oxygen demand using SM 5220D
— Chloride, nitrate, and sulfate using EPA Method 9056A
— Ferrous iron using SM 3500-Fe D
Fall 2021 Semiannual
Water Quality Monitoring Report 5 February 2022

— Sulfide using SM 4500-5 F
— Total organic carbon using SM 9060A
— Nitrate as N, chloride, and sulfate using EPA Method 9056A
The surface water samples were analyzed for the following parameters:
• Appendix II metals, including mercury, using EPA Methods 6020B and 7470A
• Appendix II VOCs using EPA Method 8260D
• 1,4-dioxane using EPA Method 8260DSIM
• Hardness using SM2340C
The leachate sample was analyzed for the following parameters:
• Appendix II VOCs, using EPA Method 8260D
• 1,4-dioxane, using EPA Method 8260DSIM
• Appendix II metals using EPA Method 6020B
The domestic well samples were analyzed for the following parameters:
• VOCs using EPA Method 524.2
Proper chain -of -custody documentation procedures were followed during collection and
transportation of each sample (Appendix B). Two trip blank samples for quality control/quality
assurance purposes were included in the sample coolers and analyzed for Appendix II VOCs when
applicable. The reports of the laboratory analyses are provided in Appendix B. Laboratory analyses
performed on the samples are summarized in Table 1.
Fall 2021 Semiannual
Water Quality Monitoring Report 6 February 2022

3 Findings
The field parameter data and laboratory analytical results for the groundwater samples (from
monitoring wells MW-01 through MW-07), surface water samples (SW-01 and SW-02), leachate
sample (LT-01), and domestic well samples (DW-01 and DW-02) collected at the landfill are included
in Appendices A and B. The results are also submitted separately to the DEQ Division of Waste
Management SWS in the Electronic Data Deliverable format (DEQ 2020).
The laboratory analytical results were reported and appropriately qualified as follows:
• Non -Detections: Non -detections are values reported by the laboratory as less than the
method detection limits (MDLs). They are tabulated in Table 3 and flagged with a "U" qualifier.
The MDL is the minimum concentration of a substance that can be measured and reported by
a laboratory with 99% confidence that the constituent concentration is greater than zero.
• Estimated or "J" Qualified: A "J" qualifier is used by the laboratory for parameters that are
detected at estimated concentrations greater than the MDL but less than the laboratory's
method reporting limit. The method reporting limit is the minimum concentration of a target
analyte that can be accurately determined by the referenced method.
• Groundwater Quality Standard: Detected concentrations of constituents in groundwater
samples were compared to applicable North Carolina groundwater quality standards. For
most constituents, this standard is defined in the 15A NCAC 2L.0202 Groundwater Standard
15A NCAC 2L.0202 (2L standard). Detected concentrations of analytes in groundwater with no
established 2L standard were compared to the interim maximum allowable concentrations
(IMACs) for Class GA and GSA groundwater (in accordance with 15A NCAC 02L.0202 [c]). For
the purposes of this report, groundwater standards were taken from the October 15, 2018 list
published by the North Carolina SWS (DEQ 2018).
• 2B Standard: Detections of analytes in surface water samples were compared to the surface
water quality standards defined in 15A NCAC 2B (213 standards). Hardness -dependent 2B
surface water standards were calculated using the average analyzed hardness value
(calculated from the upstream and downstream surface water sampling location results) via
the most stringent hardness -dependent metal calculation.
Table 3 summarizes detected concentrations of analytes that exceeded their respective 2L standard,
IMAC, or 2B standard.
3.1 Groundwater
Measured field parameters and analytical results for groundwater samples collected from the
monitoring wells during the fall 2021 sampling event are discussed in the following sections and
summarized in Table 3.
Fall 2021 Semiannual
Water Quality Monitoring Report 7 February 2022

3.1.7 Field Parameters
Field parameter measurements were obtained from all site monitoring wells (MW-01, MW-02,
MW-03, MW-04, MW-05R, MW-06, and MW-07). Field parameters are presented in Table 3 and
summarized below:
• pH: The pH readings ranged from 4.6 SU in MW-06 to 6.8 SU in MW-05R. Of these monitoring
wells, the pH values for MW-01, MW-02, MW-03, MW-04, MW-06, and MW-07 were less than
the 2L standard pH range of 6.5 to 8.5 SU.
• Turbidity: Turbidity ranged from 1.06 nephelometric turbidity units (NTUs) in MW-04 to
594 NTU in MW-02. Generally, the higher values were measured at the monitoring wells
(MW-01, MW-02, and MW-05R) that were purged and sampled using the bailer method
(Section 2.1.1). The bailers were lowered gently to minimize water column disturbance when
the samples were collected.
• Dissolved Oxygen (DO): DO concentrations at the Site ranged from 0.83 milligram per liter
(mg/L) in monitoring well MW-03 to 5.92 mg/L in monitoring well MW-02.
• SC: SC concentrations at the Site ranged from 56.8 micromhos per centimeter (pmhos/cm) in
monitoring well MW-06 to 828 pmhos/cm in monitoring well MW-07.
• Oxidation/Reduction Potential: ORP concentrations at the Site ranged from -111.1 mV in
monitoring well MW-05R to 545.8 mV in monitoring well MW-03.
3.1.2 Appendix 11 Metals (Total)
Thirteen metals were detected in one or more of the monitoring well samples. Five of these metals
(cadmium, chromium, cobalt, thallium, and vanadium) were detected at concentrations above their
respective NC21- and/or IMAC water quality standards in one or more of the groundwater samples. A
summary of the detections is provided below.
• Cadmium (21L standard of 2 micrograms per liter [pg/L]): Cadmium was detected in MW-01 at
a concentration of 8.81 pg/L.
• Chromium (21- standard of 10 pg/L): Chromium was detected in MW-02 at a concentration of
20.6 pg/L.
• Cobalt (21L standard of 1 pg/L): Cobalt was detected in MW-01, MW-02, MW-03, MW-04,
MW-05R, MW-06, and MW-07. Cobalt concentrations in these samples ranged from an
estimated 1.60 pg/L (MW-07) to 139 pg/L (MW-01). As noted in Section 2.1, monitoring well
MW-01 is considered to represent upgradient conditions. The second upgradient well
(MW-06) also showed an exceedance of cobalt (11.6 pg/L). Historically, cobalt has been
present at concentrations that exceeded its applicable water quality standard in groundwater
samples from each of the seven monitoring wells.
• Thallium (21L standard of 0.2 pg/L): Thallium was detected in MW-01 at a concentration of
1.42 joules (J) pg/L.
Fall 2021 Semiannual
Water Quality Monitoring Report 8 February 2022

• Vanadium (2L standard of 0.3 pg/L): Vanadium was detected in MW-01 (6.16 pg/L), MW-02
(28.8 pg/L), MW-03 (2.09 J pg/L), MW-05R (1.97 J pg/L), and MW-07 (1.55 J pg/L).
These metals have historically been present at concentrations exceeding their water quality standard
in samples collected from multiple groundwater monitoring wells at the Site. However, the elevated
turbidity value (549 NTU) measured in the MW-02 sample may have affected the metal
concentrations reported here. During the spring 2020 sampling event, MW-02 showed a turbidity of
15.5 NTU with consistently lower concentrations of these metals (Anchor QEA 2020).
3.1.3 Appendix 11 Metals (Dissolved)
Laboratory -filtered analysis of Appendix II metals were performed for monitoring well samples
MW-01, MW-02, MW-03, and MW-05R because of their elevated turbidity readings (27.2, 594, 10.7,
and 60.5 NTU, respectively) during sample collection. The reported concentrations for the dissolved
metals were consistently lower than the total unfiltered metals analytical results in all monitoring
wells. The only exceedance for a laboratory -filtered analysis was for cobalt (Table 3).
3.1.4 Appendix 11 VOCs and 1,4-Dioxane
Seventeen VOCs were detected in one or more of the monitoring wells (Table 3). Four of these VOCs
(1,4-dichlorobenzene; 1,4-dioxane; benzene; and vinyl chloride) were detected at concentrations that
exceeded their respective 2L standards in the groundwater samples collected from one or more
monitoring wells. Concentration -versus -time graphs (trend plots) were created for the monitoring
wells that have historically exhibited the following VOC concentrations that exceeded the associated
2L standards (Figures 4 through 10):
• 1-4-dichlorobenzene (2L standard of 6 pg/L): The detected concentration of
1,4-dichlorobenzene exceeded its 2L standard in monitoring wells MW-01 (7.76 pg/L),
MW-05R (6.13 pg/L), and MW-07 (7.05 pg/L). The historical 1,4-dichlorobenzene
concentration trend in MW-01 remains relatively stable (Figure 4). Historical 1,4-
dichlorobenzene concentrations in MW-05R have consistently fluctuated (Figure 6).
• 1,4-dioxane (2L standard of 3 pg/L): The detected concentrations of 1,4-dioxane exceeded its
2L standard in MW-03 (5.96 pg/L), MW-04 (5.56 pg/L), MW-05R (4.34 pg/L), and MW-07
(13.7 pg/L). 1,4-dioxane was not detected in monitoring wells MW-01 or MW-06. 1,4-dioxane
was detected under the 2L standard in MW-02. A trend plot for 1,4-dioxane concentrations in
MW-07 shows stable concentrations since sampling for this compound began in October
2018 (Figure 7).
• Benzene (2L standard of 1 pg/L): Benzene was detected at concentrations that exceeded its 2L
standard in MW-01 (1.11 pg/L), MW-03 (1.19 pg/L), MW-05R (2.38 pg/L), and MW-07
(1.82 pg/L). Overall, historic benzene concentrations in monitoring well MW-01 shows a
generalized downward trend since April 2007 (Figure 5). Benzene concentrations at MW-5R
Fall 2021 Semiannual
Water Quality Monitoring Report 9 February 2022

have fluctuated consistently since 2012 (Figure 7). Benzene concentrations at MW-07 have
been relatively stable since 2011 (Figure 10).
• Vinyl chloride (21L standard of 0.03 pg/L): The concentration of vinyl chloride in the sample
collected from one monitoring well, MW-05R (1.52 pg/L), exceeded the compound's 2L
standard. A trend plot for vinyl chloride concentrations in MW-05R shows consistently
fluctuating concentrations (Figure 8).
A review of historical groundwater data indicates the VOCs (1,4-dichlorobenzene; 1,4-dioxane;
benzene; and vinyl chloride) exhibiting concentrations that exceeded the 2L standards during the fall
2021 sampling event have been detected at relatively consistent concentrations for the past several
years. As described in Section 3.2.3, historical surface water samples from the Tuckasegee River,
which may receive discharge from the saprolite groundwater -bearing zone, have consistently shown
no detections of these compounds, or other VOCs.
3.7.5 Natural Attenuation Parameters
During this sampling event, the groundwater samples were analyzed for MNA parameters as
described in Section 2.2 (Table 1). The results of these analyses are summarized in Table 3. These
parameters were detected in one or more groundwater samples collected from the monitoring wells.
Many of these parameters do not have established groundwater standards. Of the parameters that
do have established groundwater standards (chloride and sulfate), there were no exceedances. An
in-depth analysis of the MNA parameters that apply to the Site's select contaminants was presented
in the first CAER (Altamont 2016). The first CAER concluded that the MNA data provide evidence that
reductive degradation and aerobic degradation are occurring in different portions of the Site. The
dataset of the MNA parameters collected from spring 2017 to fall 2021 was used in the second CAER
(Anchor QEA 2022), which concluded that evidence that reductive degradation and aerobic
degradation are occurring in different portions of the Site.
3.2 Surface Water
The following sections summarize the measured field parameters and analytical results associated
with the two surface water samples collected during the fall 2021 sampling event.
3.2.7 Field Parameters
Field parameters are presented in Table 3 and summarized below:
• pH: The pH readings for the upstream (SW-01) and downstream (SW-02) surface water
samples collected during the fall 2021 sampling event were 5.8 and 5.9 SU, respectively. The
pH readings for both surface water samples were less than the 2B standard range of 6.0 to
9.0 SU.
Fall 2021 Semiannual
Water Quality Monitoring Report 10 February 2022

• Turbidity: The turbidity values measured in SW-01 (4.47 NTU) and SW-02 (4.68 NTU) were less
than the 2B standard, which is established at less than or equal to 50 NTU for the receiving
water in streams not designated as trout waters.
• DO: DO was measured at a concentration of 9.39 mg/L in SW-01 and 10.75 mg/L in SW-02.
The 2B standard is established as greater than or equal to 6 mg/L; thus, each sample is within
the acceptable DO range.
• SC: SC concentrations in surface water samples SW-01 and SW-02 were recorded at 25.3 and
24.3 pmhos/cm, respectively. These concentrations of SC are consistent with historical data for
both surface water samples.
• ORP: ORP values for SW-01 and SW-02 were 314.5 and 320.2 mV, respectively. Compared to
historical surface water samples, the concentrations of ORP are elevated by approximately
100 mV.
3.2.2 Appendix Il Metals
Four metals were detected in both surface water sampling locations. Of these metals, none exceeded
the established 2B standards. These results are consistent with historical sample results, with the
exception of lead. In the past, lead has been detected above 2B standards at both the upstream and
downstream sampling locations. Now, lead is a non -detection.
3.2.3 Appendix 1/ VOCs and 7,4-Dioxane
Acetone was the only VOC detected in the surface water samples and was also detected in similar
concentrations in the trip blank sample included with the surface water samples.
3.3 Leachate
Five metals (arsenic [4.0 J pg/L], barium [372 pg/L], cobalt [5.83 J pg/L], nickel [24.2 pg/L], and
vanadium [3.42 J pg/L]) were detected in the leachate sample (LT-01).
Eleven VOCs (1,4-dichlorobenzene [3.85 pg/L]; 1,4-dioxane [48.8 pg/L]; acetone [8.14 pg/L];
benzene [2.45 pg/L]; chlorobenzene [4.28 pg/L]; ethylbenzene [0.838 pg/L]; m,p-xylene [1.17 pg/L];
naphthalene [13.6 pg/L]; o-xylene [1.64 pg/L]; total xylene [2.81 pg/L]; and tetrahydrofuran
[203 pg/L]) were detected in the leachate sample (LT-01).
On September 1, 2012, leachate extraction was initiated following installation of leachate extraction
pumps in the 10 landfill gas extraction wells at the Site (Figure 2). Based on readings taken from the
leachate totalizer during the October 2021 monitoring events, approximately 62,651 gallons of
leachate were discharged through a permanent connection to the TWSA between October 14, 2020,
and October 20, 2021.
Fall 2021 Semiannual
Water Quality Monitoring Report 11 February 2022

In fall 2013, the active portion of the approved corrective action remedy was initiated. Based on the
leachate analytical results for the sample collected on October 20, 2021, Anchor QEA estimates that
approximately 0.15 pounds of VOCs was removed with the extracted leachate between the
October 2020 and October 2021 sampling events. Mass removal calculations through October 2021
are included in Table 4.
3.4 Domestic Well
The following sections summarize measured field parameters and analytical results associated with
the domestic well water sample collected during the fall 2021 sampling event.
3.4.7 Field Parameters
The pH reading for the domestic well samples for DW-01 and DW-02 were 6.3 and 5.2 SU,
respectively, which are outside the 2L standard range of 6.5 to 8.5 SU.
Turbidity measured in DW-01 was 9.8 NTU. DO was measured at a concentration of 7.24 mg/L in
DW-01. SC and ORP values in DW-01 were recorded at 59.3 pmhos/cm and 157.5 mV, respectively.
These parameters do not have established water quality standards.
3.4.2 VOCs
No VOCs were detected at concentrations that exceeded their respective MDLs in the domestic well
water samples.
3.5 Groundwater Flow Directions
Groundwater levels in the saprolite, PWR, and bedrock are monitored at the Site. Three of the
bedrock monitoring wells (MW-01, MW-02, and MW-06) are located in the northern and
northwestern portions of the Site (Figure 3; Table 2). The fourth bedrock monitoring well (MW-07) is
located southwest of the landfill (Figure 3). The fall 2021 water level data collected from these four
bedrock wells were used to determine the generalized bedrock groundwater flow direction, which is
to the southwest (Figure 3).
PWR monitoring well MW-03 and saprolite monitoring wells MW-04 and MW-05R (Figure 3) are
located in the south-central and southern parts of the landfill, respectively. The fall 2021 water level
data collected from monitoring wells MW-03, MW-04, and MW-05R (Table 2) indicate that
groundwater flow direction in the combined saprolite and PWR zones is generally to the south-
southwest, toward the Tuckasegee River (Figure 3).
Fall 2021 Semiannual
Water Quality Monitoring Report 12 February 2022

4 Summary
The second semiannual water quality monitoring event of 2021 for the Site was performed on
October 19 and 20, 2021. Appendices A and B and Table 3 provide detailed analytical results and
field data summarizing the groundwater, surface water, and leachate quality at the landfill.
4.1 Groundwater Quality
4. 7. 7 Appendix ll Metals
Five metals (cadmium, chromium, cobalt, thallium, and vanadium) were detected at concentrations
that exceeded their associated groundwater quality standards in one or more of the monitoring wells
(Table 3). Cadmium and thallium concentrations exceeded 2L standards in MW-01. Chromium
concentrations exceeded their 2L standard in MW-02. Cobalt concentrations exceeded their
2L standard in all the collected groundwater samples. Vanadium exceeded its 2L concentration
MW -01, MW-02, MW-03, MW-05R, and MW-06. These results are consistent with historical data.
The results for groundwater samples from MW-01, MW-02, MW-03, and MW-05R, submitted for
dissolved filtered metals, show consistently lower metals concentrations than the total unfiltered
samples, indicating turbidity likely affects metal concentrations in these wells.
4. 7.2 Appendix 11 Volatile Organic Compounds and 1,4-Dioxane
Four VOCs (1,4-dichlorobenzene; benzene; vinyl chloride; and 1,4-dioxane) were detected at
concentrations that exceeded their respective 2L standards (Table 3) in one or more monitoring
wells, including 1,4-dichlorobenzene and benzene, in the upgradient monitoring well MW-01. Trend
plots for samples from monitoring wells that had VOC concentrations that exceeded their
2L standards (Figures 4 through 10) show relatively stable concentrations with time.
4. 7.3 Field Parameters and Other Constituents
Six of the seven samples collected from the monitoring wells had pH readings outside of the
2L standard range (6.5 to 8.5 SU). These results are consistent with historical data and are
characteristic of the natural groundwater quality of the region. Turbidity readings ranged from
1.06 NTU (MW-04) to 594 NTU (MW-02).
Natural attenuation parameters (alkalinity, biochemical oxygen demand, chemical oxygen demand,
chloride, cyanide, nitrate as N, sulfate, sulfide, total organic carbon, and ferrous iron) were detected
at various concentrations in groundwater samples collected from one or more of the monitoring
wells. Natural attenuation parameters are being monitored to fulfill CAP requirements; further
evaluation of these parameters was performed in the second CAER (Anchor QEA 2022) and
concluded that conditions exist for anaerobic and aerobic degradation of chlorinated solvents.
Fall 2021 Semiannual
Water Quality Monitoring Report 13 February 2022

4.2 Surface Water Quality
No concentrations for metals or VOCs exceeded 2B standards for surface water during this
monitoring event. Field parameters measured in both surface water samples, including turbidity and
DO, were within the 2B standards established for these parameters. The pH measured at both surface
water locations were outside the range of 2B standards. Based on these data, the groundwater
migrating from the landfill toward the Tuckasegee River does not appear to be impacting surface
water quality with regard to metals and VOCs.
4.3 Leachate Quality
The leachate sample (LT-01) was collected from the flow equalization tank and analyzed for
Appendix I VOCs and 1,4-dioxane. Eleven VOCs were detected in the leachate sample (Table 3).
There are no established water quality standards for leachate. 1,4-dioxane was detected at 48.8 pg/L,
which is higher than the detected concentrations of the compound in the monitoring well
groundwater samples. This is the third sampling event where 1,4 dioxane was analyzed for in the
leachate.
4.4 Domestic Well Water Quality
No VOCs were detected at concentrations that exceeded their respective MDLs in the domestic well
water samples.
Fall 2021 Semiannual
Water Quality Monitoring Report 14 February 2022

5 Future Activities
Anchor QEA will continue to monitor the water quality on a semiannual basis at the Site. During
spring 2022, domestic well owners will be contacted, and groundwater samples will be collected
from domestic wells if permitted by the well owner, and if possible, based on well pump operability.
Domestic well samples will be analyzed for VOCs only. Samples will be collected from the monitoring
wells, surface water monitoring points, and leachate flow equalization tank during spring 2022 and
fall 2022. Starting in spring 2022, a third surface water sampling location will be added between the
upstream and downstream locations. In addition to the MNA parameters that were added to the
monitoring requirements as part of the CAP, the analytical suites associated with the current and
future sampling events are outlined in the 2011 CAP (Altamont 2011), the first CAER (Altamont 2016),
and the second CAER (Anchor QEA 2022). The upcoming sampling event parameters are as follows:
Analytical Suite
Sampling Event (not inclusive of natural attenuation parameters)
Appendix I VOCs (including 1,4-dioxane)
Spring 2022 Appendix I Metals
Sulfide
Appendix II VOCs (including 1,4-dioxane)
Appendix II Metals
Fall 2022 Appendix II semivolatile organic compounds
Appendix II herbicides
Appendix II pesticides
Fall 2021 Semiannual
Water Quality Monitoring Report 15 February 2022

6 References
Altamont (Altamont Environmental, Inc.), 2010. Assessment of Corrective Measures. Prepared for
North Carolina Department of Environment and Natural Resources. September 7, 2010.
Altamont, 2011. Corrective Action Plan. Prepared for North Carolina Department of Environment and
Natural Resources. June 30, 2011.
Altamont, 2016. Five -Year Corrective Action Evaluation Report. Prepared for North Carolina
Department of Environmental Quality. October 31, 2016.
Anchor QEA (Anchor QEA of North Carolina, PLLC), 2020. Spring 2020 Semiannual Water Quality
Monitoring Report. Prepared for Jackson County Solid Waste Department. June 2020.
Anchor QEA, 2022. Five -Year Corrective Action Evaluation Report. Prepared for North Carolina
Department of Environmental Quality. January 13, 2022.
DENR (North Carolina Department of Environmental and Natural Resources), 2011. Letter to:
Altamont Environmental, Inc. Regarding: Approval of the County's Corrective Action Plan.
September 1, 2011.
DEQ, 2018. "Groundwater Protection Compliance Standards — Constituents List". Last modified
October 15, 2018. Available at:
https://edocs.deq.nc.gov/WasteManagement/0/edoc/1257181/SWS EnviroMonitoring Const
ituents List.pdf?searchid=13f8efbl-eel 1-485a-b03f-718f2287b271.
DEQ, 2020. Memorandum to: Solid Waste Directors, Landfill Owners/Operators, and North Carolina
Certified Laboratories. Regarding: New Electronic Data Deliverable (EDD) Format.
July 20, 2020.
EPA (U.S. Environmental Protection Agency), 1996. Low -Flow (Minimal Drowdown) Ground -Water
Sampling Procedures. Office of Land and Emergency Management, EPA/540/5-95/504.
EPA, 2017. Science and Ecosystem Support Division. Operating Procedure: Groundwater Sampling.
April 26, 2017.
Fall 2021 Semiannual
Water Quality Monitoring Report 16 February 2022

Tables

Table 1
Summary of Laboratory Analyses Performed on Samples
Groundwater Samples
Location ID
Date
I Collected
Sample ID
Appendix II
VOCs
1,4-Dioxane
Appendix II
Metals
Mercury
Appendix II
SVOCs
EPA 8260D
EPA 8260D
SIM
EPA 6020B
EPA 7470A
EPA 8270D
MW-01
10/20/2021
MW-01-20211020
X
X
X'
X
X
MW-02
10/20/2021
MW-02-20211020
X
X
X1
X
X
MW-03
10/20/2021
MW-03-20211020
X
X
X'
X
X
MW-04
10/19/2021
MW-04-20211019
X
X
X
X
X
MW-05R
10/19/2021
MW-05R-20211019
X
X
X1
X
X
MW-06
10/20/2021
MW-06-20211020
X
X
X
X
X
MW-07
F10/19/2021
MW-07-20211019
X
X
X
X
X
Surface Water,
Leachate,
Domestic Well, and
Quality Control
Samples
Location ID
Date
Collected
Sample ID
Appendix II
VOCs
1,4-Dioxane
Appendix II
Metals
Mercury
Calcium,
Magnesium, and
Hardness
Appendix II
SVOCs
VOCs
EPA 8260D
EPA 8260D
SIM
EPA 6020B
EPA 7470A
EPA 200.7
EPA 8270D
EPA 524.2
DW-01
10/20/2021
DW-01-20211020
X
DW-02
10/20/2021
DW-02-20211020
X
LT-01
10/20/2021
LT-01-20211020
X
X
X
SW-01
10/19/2021
SW-01-20211019
X
X
X
X
X
X
SW-02
10/19/2021
SW-02-20211019
X
X
X
X
X
X
TB-20211019A
10/19/2021
TB-20211019A
X
TB-20211019B
10/19/2021
TB-20211019B
X
TB-20211019C
10/19/2021
TB-20211019C
X
TB-20211020A
10/20/2021
TB-20211020A
X
TB-20211020B
10/20/2021
1 TB-20211020B
X
TB-20211020C
10/20/2021
TB-20211020C
I X
T13-20211020D
10/20/2021
TB-20211020D
I X
Groundwater and Surface Water Samples: Monitored Natural Attenuation Parameters
Location ID
Date
Collected
Sample ID
COD
BOD
Ferrous Iron
Total
Alkalinity
to pH 4.5
Nitrate
as N
Chloride
Sulfate
TOC
Sulfide
Cyanide
SM 5220D
SM 5210B
SM 3500-Fe D
SM 2320B
EPA 9056A
SM 9060A
SM4500-S F
SM 4500-CN-E
MW-01
10/20/2021
MW-01-20211020
X
X
X
X
X
X
X
X
X
X
MW-02
10/20/2021
MW-02-20211020
X
X
X
X
X
X
X
X
X
X
MW-03
10/20/2021
MW-03-20211020
X
X
X
X
X
X
X
X
X
X
MW-04
10/19/2021
MW-04-20211019
X
X
X
X
X
X
X
X
X
X
MW-05R
10/19/2021
MW-05R-20211019
X
X
X
X
X
X
X
X
X
X
MW-06
10/20/2021
MW-06-20211020
X
X
X
X
X
X
X
X
X
X
MW-07
10/19/2021
MW-07-20211019
X
X
X
X
X
X
X
X
X
X
Notes:
1: An additional sample was collected for a laboratory -filtered dissolved metals analysis.
Appendix II constituents were analyzed per Title 40 Code of Federal Regulations, Part 258.
Blank cell: Analysis was not performed on that sample.
BOD: biochemical oxygen demand
COD: chemical oxygen demand
EPA: U.S. Environmental Protection Agency (method)
SIM: selective ion monitoring
SM: Standard Method
SVOC: semivolatile organic compound
TB: trip blank
TOO total organic carbon
VOC: volatile organic compound
Fall 2021 Semiannual Water Quality Monitoring Report Page 1 of 1
Jackson County Closed Municipal Solid Waste Landfill February 2022

Table 2
Well Construction Details and Corresponding Elevations
Stick Up
Depth to
Depth to
Elevation of
Ground
(feet
Depth to
Approximate
Approximate
Top of
Bottom of
Top Elevation
Bottom of
Surface
TOC
above
Total Well
Water
Depth to
Top of Bedrock
Screened
Screened
of Screened
Screened
Geology of
Source of Well
Facility
Elevation
Elevation
ground
Depth
(feet below
Groundwater
Bedrock
Elevation
Interval
Interval
Interval
Interval
Screened
Construction
Permit
Well ID
Date Drilled
(feet)
(feet)
surface)
(feet bgs)
TOC)
Elevation (feet)
(feet bgs)
(feet)
(feet bgs)
(feet bgs)
(feet)
(feet)
Interval
Information
MW-01
04/23/1992
2,169.40
2,171.42
1 2.0
110.5
95.62
2,075.80
83.0
2,086.40
95.0
110.0
2,074.40
2,059.40
Bedrock
MW-02
04/22/1992
2,013.15
2,015.38
2.3
60.7
40.16
1,975.22
13.0
2,000.15
45.0
60.0
1,968.15
1,953.15
Bedrock
Partially
S&ME, Inc.
MW-03
04/21/1992
2,044.16
2,045.53
1.3
65.5
48.00
1,997.53
57.0
1,987.16
48.5
63.5
1,995.66
1,980.66
50-02
weathered rock
MW-04
04/21/1992
1,978.68
1,980.77
2.0
43.0
25.80
1,954.97
NA
NA
25.0
40.0
1,953.68
1,938.68
Saprolite
MW-05R
01/26/2012
2,027.98
2,030.95
2.8
54.0
46.14
1,984.81
NA
NA
44.0
54.0
1,983.98
1,973.98
Saprolite
MW-06
03/23/2004
2,136.58
2,139.57
3.0
94.0
79.95
2,059.62
47.6
2,088.98
84.6
94.6
2,051.98
2,041.98
Bedrock
Altamont
Environmental, Inc.
MW-07
07/30/2010
1,978.71
1,981.29
2.6
95.0
31.37
1,949.92
44.0
1,935.00
70.0
95.0
1,908.71
1,883.71
Bedrock
Notes:
Elevations associated with wells MW-01, MW-02, MW-03, MW-04, and MW-06 are measured relative to mean sea level and are based on surveying completed by Davenport & Associates, Inc.
Elevations associated with wells MW-05R and MW-07 are measured relative to horizontal North American Datum 83 and are based on surveying completed by Wes Cole Land Surveying, PA.
Depth to water was measured on October 19 and 20, 2021 (Appendix A).
Depth to bedrock and screened interval for MW-01 through MW-04 was taken from S&ME, Inc., with boring logs completed on April 21 through 23, 1992.
Depth to bedrock and screened interval for MW-06 was taken from an Altamont Environmental, Inc., with boring log completed on March 23, 2004.
Depth to bedrock and screened interval for MW-07 was taken from an Altamont Environmental, Inc., with boring log completed on July 30, 2010.
Depth to bedrock and screened interval for MW-05R was taken from an Altamont Environmental, Inc., with boring log completed on January 26, 2012.
Monitoring well MW-05 was abandoned on January 26, 2012, by NYEG Drilling, LLC. Monitoring well MW-05R was installed by NYEG Drilling, LLC, on January 26, 2012, as a replacement to MW-05.
Monitoring well MW-05R was surveyed by Wes Cole Land Surveying, PA, on September 28, 2012.
bgs: below ground surface
NA: not applicable
TOC: top of casing
Fall 2020 Semiannual Water Quality Monitoring Report Page 1 of 1
Jackson County Closed Municipal Solid Waste Landfill February 2021

Table 3
Analytical Summary
Location ID
DW-01
DW-02
LT-01
MW-01
MW-02
MW-03
MW-04
MW-05R
MW-06
MW-07
SW-01
SW-02
FieIdQC
FieIdQC
FieIdQC
FieIdQC
FieIdQC
FieIdQC
Sample ID
DW-01-
20211020
DW-02-
20211020
LT-01-
20211020
MW-01-
20211020
MW-02-
20211020
MW-03-
20211020
MW-04-
20211019
MW-0511-
20211019
MW-06-
20211020
MW-07-
20211019
SW-01-
20211019
SW-02-
20211019
TB-
20211019A
TB-
20211019B
TB-
20211019C
TB-
20211020A
TB-
20211020B
TB-
20211020C
Sample Date
10/20/2021
10/20/2021
10/20/2021
10/20/2021
10/20/2021
10/20/2021
10/19/2021
10/19/2021
10/20/2021
10/19/2021
10/19/2021
10/19/2021
10/19/2021
10/19/2021
10/19/2021
10/20/2021
10/20/2021
10/20/2021
Sample Type
N
N
N
N
N
N
N
N
N
N
N
N
TB
TB
TB
TB
TB
TB
Matrix
WG
WG
WG
WG
WG
WG
WG
WG
WG
WG
WS
WS
WQ
WQ
WQ
WQ
WQ
WQ
NC2L NC2L
Chemical Method (2013) IMAC NC 213
Conventional Parameters
Water level depth (feet)
95.62
40.16
48.00
25.80
46.14
79.95
31.37
Temperature (°C)
Field
15.2
14.6
20.1
16.6
12.7
15.2
15.3
22
15.5
15.6
14.7
15
--
--
--
Dissolved oxygen (field)
Field
>_6
3.38
5.3
1.48
2.07
5.92
0.83
5.62
1.11
5.7
1.36
9.39
10.75
--
--
--
Specific conductivity (field)
Field
53.6
46.7
4560
214.9
204.1
254.1
655
702
56.6
828
25.3
24.3
--
--
--
pH (SU)
Field
6.5-8.5
6.0-9.0
6.3
5.24
6.9
5.6
5.2
5.2
5.7
6.8
4.6
6.0
5.8
5.9
--
--
--
ORP (mV)
Field
180.8
184.1
-91.8
27.1
407.6
545.8
518.3
-111.1
334.5
139.6
314.5
320.2
--
--
--
Turbidity (NTU)
Field
10
7.4
1.89
2.95
27.2
594
10.7
1.06
60.5
2.44
4.37
4.47
4.68
--
--
--
Hardness as Ca and Mg (mg/L)
SM2340C
--
--
--
--
--
--
--
--
--
8 J
8.11
--
--
--
MNA Parameters (mg/L)
Alkalinity, total as CaCO3
SM2320B
--
--
81
58
51
103
203
25
258
--
--
--
--
--
Biochemical oxygen demand
SM5210B
--
--
8.8
2 U
2 U
2
15.5
2 U
2 U
--
--
--
--
--
Chemical oxygen demand
SM5220C
--
--
74
38 J
41 J
34 J
101
191
29 J
--
--
--
--
--
Chloride
SW9056A
250
--
--
0.866 J
20.1
32.5
61.7
66.5
0.888 J
81.6
--
--
--
--
--
Cyanide
9014
0.07
--
--
--
--
--
0.0038 U
0.0038 U
--
0.0038 U
--
--
--
--
--
--
Nitrate as nitrogen
SW9056A
10
--
--
0.076 U
0.255
3.71
1.76
0.076 U
0.076 U
0.076 U
--
--
--
--
--
--
Sulfate
SW9056A
250
--
--
--
0.54 U
27
1
124
0.54 U
0.54 U
23
--
--
--
--
--
--
Sulfide
SM4500S2F
--
--
--
0.83 U
4
0.83 U
0.83 U
0.83 U
0.83 U
0.83 U
--
--
--
--
--
--
--
Ferrous iron
SM3500FEB
--
--
--
32.9
0.080 J
0.05 U
0.05 U
7.64
0.060 J
0.37
--
--
--
--
--
--
--
Total organic carbon
SM5310B
--
--
--
1.89
1.45
2.41
2.39
5.36
0.788 J
3.13
--
--
--
--
--
--
--
Metals (Ng/L)
Arsenic
SW6020
10
10
--
--
4 J
0.549 J
2.99
0.359 J
0.17 U
0.418 J
0.17 U
0.172 J
0.17 U
0.181 J
--
--
--
--
--
--
Barium
SW6020
700
21000
--
--
372
130
154
199
72.1
116
48.9
420
13.3
11.9
--
--
--
--
--
--
Beryllium
SW6020
4
--
--
0.95 U
0.19 U
0.611 J
0.19 U
0.19 U
0.19 U
0.19 U
0.19 U
0.19 U
0.19 U
--
--
--
--
--
--
Cadmium
SW6020
2
*0.06
--
--
0.8 U
8.81
0.16 U
0.486 J
0.33 J
0.16 U
0.16 U
0.16 U
0.16 U
0.16 U
--
--
--
--
--
--
Chromium
SW6020
10
*9.37
--
--
3.95 U
5.6
20.6
1.05 J
0.79 U
3.83
0.79 U
0.79 U
0.79 U
0.79 U
--
--
--
--
--
--
Cobalt
SW6020
1
1.6
--
--
5.83 J
139
28.1
6.28
2.97
12.5
11.6
1.6 J
0.52 U
0.52 U
--
--
--
--
--
--
Copper
SW6020
1000
*1.03
--
--
19 U
27.9
22.6
3.8 U
3.8 U
3.8 U
3.8 U
3.8 U
3.8 U
3.8 U
--
--
--
--
--
--
Lead
SW6020
15
*0.15
--
--
1.3 U
2.6
5.96
0.26 U
0.26 U
0.612 J
0.26 U
0.26 U
0.26 U
0.26 U
--
--
--
--
--
--
Mercury
SW7470
1
0.012
--
--
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
--
--
--
--
--
--
Nickel
SW6020
100
*6.14
--
--
24.2
18.3
14.6
4.88
3.51
3.26
5.31
6.77
0.51 U
0.51 U
--
--
--
--
--
--
Selenium
SW6020
20
5
--
--
3.7 U
0.74 U
0.912 J
0.74 U
0.921 J
0.74 U
0.74 U
0.74 U
0.958 J
0.74 U
--
--
--
--
--
--
Thallium
SW6020
0.2
2
--
--
2.85 U
1.42 J
0.57 U
0.57 U
0.57 U
0.57 U
0.57 U
0.57 U
0.57 U
0.57 U
--
--
--
--
--
--
Vanadium
SW6020
0.3
--
--
3.42 J
6.16
28.8
2.09 J
7.3 U
1.97 J
1.55 J
7.3 U
1.3 U
1.38 J
--
--
--
--
--
--
Zinc
SW6020
1000
*13.79
--
--
34.5 U
169
55.5
10.9 J
6.9 U
10.1 J
13.2 J
6.9 U
6.9 U
6.9 U
--
--
--
--
--
--
Metals Dissolved L
Arsenic
SW6020
10
10
--
--
--
0.17 U
0.17 U
0.17 U
--
0.17 U
--
--
--
--
--
--
--
--
--
--
Barium
SW6020
700
21000
--
--
--
105
39.2
186
--
59.9
--
--
--
--
--
--
--
--
--
Cadmium
SW6020
2
*0.06
--
--
--
0.16 U
0.16 U
0.421 J
--
0.16 U
--
--
--
--
--
--
--
--
--
Chromium
SW6020
10
*9.37
--
--
--
0.79 U
0.79 U
0.79 U
--
0.79 U
--
--
--
--
--
--
--
--
--
Cobalt
SW6020
1
1.6
--
--
--
121
19.1
3.59
9.14
--
--
--
--
--
--
--
--
--
Copper
SW6020
1000
*1.03
--
--
--
3.8 U
3.8 U
3.8 U
--
3.8 U
--
--
--
--
--
--
--
--
--
--
Lead
SW6020
15
*0.15
--
--
--
0.26 U
0.26 U
0.26 U
--
0.26 U
--
--
--
--
--
--
--
--
--
--
Mercury
SW7470
1
0.012
--
--
--
0.09 J
0.07 J
0.08 J
--
0.07 U
--
--
--
--
--
--
--
--
--
--
Nickel
SW6020
100
*6.14
--
--
--
13.6
18.3
4.12
--
1.81 J
--
--
--
--
--
--
--
--
--
--
Selenium
SW6020
20
5
--
--
--
0.74 U
0.74 U
0.74 U
--
0.74 U
--
--
--
--
--
--
--
--
--
--
Thallium
SW6020
0.2
2
--
--
--
0.573 J
0.57 U
0.57 U
--
0.57 U
--
--
--
--
--
--
--
--
--
--
Vanadium
SW6020
0.3
--
--
--
1.3 U
1.3 U
1.3 U
--
1.3 U
--
--
--
--
--
--
--
--
--
--
Zinc
SW6020
1000
*13.79
--
--
--
6.9 U
6.9 U
8.2 J
--
6.9 U
--
--
--
--
--
--
--
--
--
--
Fall 2021 Semiannual Water Quality Monitoring Report 1 of 2
Jackson County Closed Municipal Solid Waste Landfill February 2022

Table 3
Analytical Summary
Location ID
DW-01
DW-02
LT-01
MW-01
MW-02
MW-03
MW-04
MW-05R
MW-06
MW-07
SW-01
SW-02
FieIdQC
FieIdQC
FieIdQC
FieIdQC
FieIdQC
FieIdQC
Sample ID
DW-01-
20211020
DW-02-
20211020
LT-01-
20211020
MW-01-
20211020
MW-02-
20211020
MW-03-
20211020
MW-04-
20211019
MW-05R-
20211019
MW-06-
20211020
MW-07-
20211019
SW-01-
20211019
SW-02-
20211019
TB-
20211019A
TB-
20211019B
TB-
20211019C
TB-
20211020A
TB-
20211020B
TB-
20211020C
Sample Date
10/20/2021
10/20/2021
10/20/2021
10/20/2021
10/20/2021
10/20/2021
10/19/2021
10/19/2021
10/20/2021
10/19/2021
10/19/2021
10/19/2021
10/19/2021
10/19/2021
10/19/2021
10/20/2021
10/20/2021
10/20/2021
Sample Type
N
N
N
N
N
N
N
N
N
N
N
N
TB
TB
TB
TB
TB
TB
Matrix
WG
WG
WG
WG
WG
WG
WG
WG
WG
WG
WS
WS
WQ
WQ
WQ
WQ
WQ
WQ
NC2L NC2L
Chemical Method (2013) IMAC NC 2B
Volatile Orcianics L
1,1-dichloroethane
SW8260
6
100
--
--
0.24 U
2.34
0.24 U
0.781
0.24 U
0.24 U
0.833
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
1,2-dichloroethene, cis-
SW8260
70
720
0.33 U
0.33 U
0.2 U
3.24
0.2 U
2.18
1.17
2.1
0.676
2.73
0.2 U
0.2 U
0.2 U
0.2 U
0.2 U
0.2 U
0.2 U
0.2 U
1,4-dichlorobenzene
SW8267
6
56
0.3 U
0.3 U
3.85
7.76
0.21 U
5.19
1.27 J
6.13
1.43
7.05
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
1,4-dioxane
SW8260SIM
3
80
--
--
48.8
0.139 U
1.7 J
5.96
5.56
4.34
0.139 U
13.7
0.139 U
0.139 U
--
--
--
--
--
--
Acetone
SW8260
6000
2000
--
--
8.14
4.9 J
1.8 U
1.92 J
1.8 U
5.07
1.8 U
1.8 U
2.96 J
2.96 J
1.8 U
2.57 J
2.27 J
1.8 U
1.8 U
1.8 U
Allyl chloride
SW8260
--
--
0.579 U
0.579 U
0.579 U
0.579 U
0.579 U
0.579 U
0.579 U
0.579 U
0.579 U
0.617 J
0.579 U
0.579 U
0.579 U
0.579 U
0.579 U
0.579 U
Benzene
SW8260
1
51
0.4 U
0.4 U
2.45
1.11
0.18 U
1.19
0.568
2.38
0.18 U
1.82
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
Chlorobenzene
SW8260
50
140
0.26 U
0.26 U
4.28
1.14
0.19 U
10.2
2.6
8.02
0.19 U
6.25
0.19 U
0.19 U
0.19 U
0.19 U
0.19 U
0.19 U
0.19 U
0.19 U
Ethylbenzene
SW8260
600
97
0.23 U
0.23 U
0.838
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
0.17 U
m,p-xylene
SW8260
500
550
--
--
1.17
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
Methyl ethyl ketone (2-butanone)
SW8260
4000
26000
--
--
0.71 U
0.71 U
0.71 U
0.969 J
0.71 U
0.71 U
0.71 U
0.71 U
0.71 U
0.71 U
0.71 U
0.71 U
0.71 U
0.71 U
0.71 U
0.71 U
Naphthalene
SW8260
6
12
--
--
13.6
0.96 J
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
o-xylene
SW8260
500
400
--
--
1.64
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
Tetrachloroethene (PCE)
SW8260
0.7
3.3
0.26 U
0.26 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
Tetrahydrofuran
SW8260
2000
110000
--
--
203
1.5 U
1.5 U
1.5 U
1.5 U
3.6 J
1.5 U
1.5 U
1.5 U
1.5 U
1.5 U
1.5 U
1.5 U
1.5 U
1.5 U
1.5 U
Total xylene
SW8260
--
--
2.81
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
Trichloroethene (TCE)
SW8260
3
30
0.26 U
0.26 U
0.18 U
0.517
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
0.18 U
Vinyl chloride
SW8260
0.03
2.4
0.72 U
0.72 U
0.77 U
0.77 U
0.77 U
0.77 U
0.77 U
1.52
0.77 U
0.77 U
0.17 U
0.17 U
0.77 U
0.77 U
0.77 U 4
0.77 U
0.77 U
0.77 U
Semivolatile Or anics L
1,4-dichlorobenzene
SW8270
6
56
0.3 U
0.3 U
--
3.72 J
1.38 U
2.84 J
3.02
2.64 J
0.822 J
2.48 J
--
--
--
--
--
--
--
--
Dibenzofuran
SW8270
28
--
--
--
0.431 U
1.01 U
0.431 U
0.444 U
0.533 J
0.427 U
0.444 U
--
--
--
--
--
--
--
--
Diethyl phthalate
SW8270
6000
--
--
--
0.651 J
4.41 J
0.596 U
0.615 U
3.48 J
0.59 U
0.615 U
--
--
--
--
--
--
--
--
Fluorene
SW8270
300
70
--
--
--
0.452 U
1.06 U
0.452 U
0.468 U
0.523 J
0.448 U
0.468 U
--
--
--
--
--
--
--
--
Notes:
indicates the detected concentration is greater than the NCH (2013) or NC2L IMAC (2013) screening level.
indicates the detected concentration is greater than the NC213 screening level.
Bold indicates a detected result.
Italicized indicates non -detected concentration is above one or more identified screening levels
*: 2B surface water standard calculated using average analyzed hardness value (calculated from the upstream and downstream sampling location results) via the most stringent hardness -dependent metal calculation per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface
Water and Wetland Standards (last amended September 2017).
All nondetect results are reported at the method detection limit.
Horizontal coordinate datum is North American Datum of 1983 State Plane North Carolina FIPS 3200 (US Survev Feet).
--: compound not analyzed for the sample
pg/L: micrograms per liter
2B: surface water standard per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards (last amended in September 2017) or the standard obtained from the U.S. Environmental Protection Agency Nationally Recommended Water Quality Criteria
for Aquatic Life and Human Health
2L: Subchapter 2L - Groundwater Classifications and Standards, Department of Environmental Quality (Amended April 1, 2013); groundwater standard from North Carolina Administrative Code, Title 15A
Appendix I: indicates volatile organic compounds and metals per 40 Code of Federal Regulations Part 258
IMAC: interim maximum allowable concentration (listed in 2L Appendix 1)
J: estimated value
mg/L: milligrams per liter
mV: millivolts
N: normal environmental sample
NTU: nephelometric turbidity unit
PCE: perch loroethylene
SM: Standard Method
su: standard units
TB: trip blank
U: compound analyzed for but not detected above detection limit
umhos/cm: microsiemens per centimeter
Fall 2021 Semiannual Water Quality Monitoring Report 2 of 2
Jackson County Closed Municipal Solid Waste Landfill February 2022

Table 4
Mass Removal Calculations for VOCs Detected in the Leachate Sample (LT-01)
Sample Dates
Detected VOCs
Concentration
in LT-01
(mg/L)
Cumulative
Flow at Gauge
(gal)
Differential
Flow (gal)
Mass
Removed
(lb)
Estimated Cumulative
Mass Removed (lb)
Beginning
Ending
9/1/2012
10/25/2012
1,4-dichlorobenzene
0.0034
11,500
11,500
0.00033
4-meth I-2- entanone (MIBK)
0.0021
J
0.00020
Acetone
0.0292
0.00280
Benzene
0.0021
0.00020
Chlorobenzene
0.0029
0.00028
cis- 1,2-dichloroethene
0.00063
J
0.00006
Dichlorodifluoro-methane
0.00093
J
0.00009
Eth (benzene
0.0102
0.00098
Naphthalene
0.0069
0.00066
Styrene
0.00033
J
0.00003
Toluene
10.003
0.00029
Total x lenes
10.0094
0.00090
Total:
0.00681
0.00681
10/26/2012
4/11/2013
1,4-dichlorobenzene
0.006
65,500
54,000
0.00270
Acetone
0.012
J
0.00540
Benzene
0.0011
0.00049
Carbon disulfide
0.0067
J
0.00301
Chlorobenzene
0.0024
J
0.00108
cis- 1,2-dichloroethene
10.00058
1 J
0.00026
Eth (benzene
10.0083
1
0.00373
Toluene
10.00059
1 J
0.00027
Total x lenes
10.0078
1
0.00351
Total:
0.02045
0.02726
4/12/2013
10/8/2013
1,4-dichlorobenzene
0.0055
114,737
49,237
0.00226
4-meth I-2- entanone (MIBK)
0.0012
J
0.00049
Benzene
0.0020
0.00082
Chlorobenzene
0.0039
0.00160
cis- 1,2-dichloroethene
0.00080
J
0.00033
Eth (benzene
0.0151
0.00619
Naphthalene
0.0184
0.00754
Toluene
0.0012
0.00049
Total x lenes
0.0090
0.00369
Total:
0.02341
0.05067
10/9/2013
4 8 2014
1,4-dichlorobenzene
0.0056
164,437
49,700
0.00232
Benzene
0.0018
0.00075
Chlorobenzene
0.0051
0.00211
cis- 1,2-dichloroethene
0.00049
J
0.00020
Eth (benzene
10.0047
0.00195
Toluene
10.00041
1 J
0.00017
Total x lenes
10.0021
1 J
0.00087
Total:
0.00836
0.05903
4/8/2014
10 23 2014
1,4-dichlorobenzene
0.0053
200,148
1
35,710
0.00158
Benzene
0.0014
0.00042
Chlorobenzene
0.003
0.00089
cis- 1,2-dichloroethene
0.00049
J
0.00015
Eth (benzene
0.0027
0.00080
Toluene
10.00051
1 J
0.00015
Total x lenes
10.0014
J
0.00042
Total:
0.00440
0.06343
10/23/2014
4/21/2015
1,2,3-trimeth (benzene
0.00062
241,700
41,552
0.00021
1,2,4-trimeth (benzene
0.00076
0.00026
2-chlorotoluene
0.00067
0.00023
1,4-dichlorobenzene
0.0059
Acetone
0.00790
Benzene
0.0022
0.00076
Chlorobenzene
0.003
0.00104
Eth (benzene
0.0056
0.00194
Isopropyl benzene
0.0013
0.00045
Methy tert-but I -ether
0.0013
0.00045
Na thalene
0.024
0.00831
n-propylbenzene
0.00088
0.00030
Tetrah drofuran
0.089
0.03080
Toluene
0.00054
J
0.00019
Vinyl chloride
0.00038
Total x lenes
10.0030
0.00104
Total:
0.05089
0.11432
4/21/2015
10/13/2015
1,4-dichlorobenzene
0.00600
278,420
36,720
0.00183
2-butanone
0.00960
J
0.00294
Benzene
0.00210
0.00064
Chlorobenzene
0.0040
0.00122
Eth (benzene
0.00710
0.00217
Na hthalene
0.021
0.00642
Tetrah drofuran
0.062
0.01896
Toluene
0.00058
J
0.00018
Total x lenes
0.0031
J
0.00095
Total:
0.03531
0.14963
10/13/2015
4/5/2016
1,4-dichlorobenzene
0.00590
337,398
58,978
1
0.00290
Benzene
0.00170
0.00083
Chlorobenzene
0.0038
0.00187
Eth (benzene
0.00500
0.00246
Toluene
0.00063
J
0.00031
Total x lenes
10.0025
J
0.00123
Total:
0.00959
0.15922
4/5/2016 10 11 20162 No detected compounds 352,745
15,347
0.00000
Total:
0.00000
0.15922
Fall 2021 Semiannual Water Quality Monitoring Report Page 1 of 2
Jackson County Closed Municipal Solid Waste Landfill February 2022

Table 4
Mass Removal Calculations for VOCs Detected in the Leachate Sample (LT-01)
Sample Dates
Detected VOCs
Concentration
in LT-01
(mg/L)
Cumulative
Flow at Gauge
(gal)
Differential
Flow (gal)
Mass
Removed
(Ib)
Estimated Cumulative
Mass Removed (Ib)
Beginning
Ending
10/11/2016
3/21/2017
1,4-dichlorobenzene
0.0046
355,947
3,202
0.00012
Acetone
0.0094
J
0.00025
Benzene
0.0015
0.00004
Chlorobenzene
0.0043
0.00011
Eth (benzene
0.0014
0.00004
Tetrah drofuran
10.066
0.00176
Total x lenes
10.0015
71
0.00004
Total:
0.00237
0.16159
3/21/2017
10/11/2017
1,4-dichlorobenzene
0.0041
386,495
1 30,548
0.00104
Acetone
0.0067
J
1
0.00170
Acetonitrile
0.008
J
0.00204
Benzene
0.00061
0.00016
Chlorobenzene
0.0012
0.00031
Eth (benzene
10.00087
1
0.00022
Naphthalene
10.0012
0 3
Tetrah drofuran
10.12
5
Total:
0.03630
0.19789
10/12/2017
10/18/20183
1,4-dichlorobenzene
0.0028
398,872
12,377
0.00029
Acetone
0.017
1
0.00175
Benzene
0.0012
0.00012
Chlorobenzene
0.0024
0.00025
Eth (benzene
0.0018
0.00019
Meth lene chloride
10.00034
1 J
0.00004
Total x lenes
10.00098
1 J
0.00010
Total:
0.0027
0.20062
10/18/2018
10/22 20193
1,4-dichlorobenzene
0.0037
407,807
8,936
0.00028
Acetone
0.006
0.00045
Benzene
0.0017
0.00013
Chlorobenzene
0.0038
0.00028
Eth (benzene
0.0016
0.00012
Toluene
10.00039
J
0.00003
Total xylenes
10.0017
J
0.00013
Total:
0.0014
0.20203
10/22/2019
3 18 20203
1,4-dichlorobenzene
0.0056
539,644
1 131,836
0.00615
1,4-dioxane
0.06
0.06585
Acetone
0.0064
0.00702
Benzene
0.0013
0.00143
Chlorobenzene
0.0032
0.00351
Eth (benzene
0.0027
0.00296
Methyl isobutyl ketone
0.00079
J
0.00087
Toluene
0.00070
0.00077
Total x lenes
10.00209
J
0.00229
Total:
0.0886
0.29058
3/18/2020
10 14 20203
1,2-dichloroethene, cis-
0.00029
J
639,343
99,699
0.00024
1,3-dichlorobenzene
0.00027
J
0.00022
1,4-dichlorobenzene
0.0048
0.00398
1,4-dioxane
0.058
0.04814
Acetone
0.011
0.00913
Acetonitri e (et anenitri e)
0.0047
J
0.00390
Benzene
0.0024
0.00199
Chlorobenzene
0.0044
0.00365
Chloroethane
0.00047
J
0.00039
Eth (benzene
0.0018
0.00149
Na hthalene
0.013
0.01079
Tetrah drofuran
0.094
0.07802
Toluene
0.00079
0.00066
Total xylenes
0.0037
0.00307
Vinyl chloride
0.00022
J
0.00018
Total:
0.1659
0.45645
10/14/2020
10/20/2021
1,4-dichlorobenzene
0.00385
701,994
1 62,651
0.00201
1,4-dioxane
0.0488
0.02546
Acetone
0.00814
0.00425
Benzene
TUU745
0.00128
Chlorobenzene
0.00428
0.00223
Eth (benzene
0.000838
0.00044
Naphthalene
0.0136
0.00710
Tetrah drofuran
TTO3
0.10592
Total x lenes
0.00281
0.00147
Total:
0.1501
0.60659
N otes:
Total xylenes represent the sum of m,p-xylenes and o-xylenes.
Only detected VOCs in leachate sample LT-01 are included in the mass removal calculation.
Leachate extraction at the landfill was initiated on September 1, 2012. Connection to the TWSA sewer was completed on September 6, 2013. Up until the connection to the TWSA sewer,
leachate was pumped into a temporary collection tank and then hauled off site. Extraction volume measurements for leachate hauled off site were recorded and provided by Jackson County
ctaff
Anchor QEA bases mass removal calculations on the assumption that the VOCs concentration in one sampling event is representative of leachate quality until the next sampling event
occurs and that the leachate removal system has a 100% removal and treatment efficiency.
Differential flow represents the total flow between the LT-01 sample dates.
Estimated cumulative mass removed and treated is estimated based upon a conversion of milligrams to pounds and liters to gallons and the multiplication of the concentration by the
differential flow for the specified period. Formula: ((concentration[mg/L])*(2.2e-6 Ib)/(0.264 gal))*(differential flow).
1. Totalizer readings were not recorded during the sampling event, and the differential flow was calculated based on an interpolated totalizer reading using monthly readings taken by
TWSA for 3 months before and after the sample date.
2. No VOCs were detected in the leachate sample collected during the October 2016 sampling event.
3. In March 2018, the totalizer at the TWSA connection was replaced. During the March 2018 sampling event, Anchor QEA began reading an incorrect totalizer for the volume of extracted
the leachate. Differential flow was calculated for the sample dates in the same manner as Note 1. This table has been updated to reflect the updated totalizer readings from previous
groundwater monitoring reports.
gal: gallon
J: indicates laboratory estimated concentration is above the adjusted method detection limit and below the adjusted reporting limit
lb: pound
mg/L: milligrams per liter
TWSA: Tuckaseigee Water and Sewer Authority
VOC: volatile organic compound
Fall 2021 Semiannual Water Quality Monitoring Report Page 2 of 2
Jackson County Closed Municipal Solid Waste Landfill February 2022

Figures

1-0
60VIrIPI a �. E.
r
LEGEND: SOURCES:
1. BasemaU.S. Geological Survey Topographic
® Site Parcel Boundary Maps - Gree ens Creek and Whittier 7.5-minute
Quadrangles
2. Parcel: Jackson County GIS 0 2,000
Feet
Publish Date: 2022/02/14, 11:05 PM I User: scolquhoun
Filepath: Q:\Jobs\JacksonCounty_NC_1480\Maps\2021\FaIIWQ\AQ_Fig01_JacksonCounty_FaIIWQ2021_SiteLocationMap.mxd
kZANCHOR Figure 1
QEA Site Location Map
Fall 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill

LEGEND:
DW-02
Saprolite Monitoring Well
® PWR Monitoring Well
® Bedrock Monitoring Well
Domestic Well Sampling Location
Leachate Sample Location and Flow
Equalization Tank
\�OL
® Surface Water Sample Location
+ Leachate/Landfill Gas Extraction Well
- Compliance Boundary
SW-02
F
• • • Edge of Waste
a
— Stream
Q Property Boundary
MW-06
— Road
® MW-01 DW-01
®
—Elevation Contour (20-Foot Interval)
WOO �� I
I....Y'• ♦ram
.
EW-7
` EW-5 �•
MW-02 1 •��'•.• EW-31R •�
® EW-1R,
y� EW-9 '0-
'•`
:L
EW-21R
EW-10•• ��.`♦♦
PQ .%
�Q • �.
ZZ
MW-03 : '. ♦
NOTES:
1.Contours, roads, and parcel boundaries are
c1j
'•.�
from Jackson County GIS.
2. Monitoring well locations are approximate.
012
•�.•••"
3. Basemap provided by Esri.
• :••
G •�'.
PWR: Partially Weathered Rock
,
-A MW-05R100,
�.001
MW-07 (N MW-04
I
�
SW-01 L
- �pOO y0
APR 0 300
Feet
Publish Date: 2022/02/14, 11:00 PM I User: scolquhoun
Filepath: Q:\JobsVacksonCounty_NC_1480\Maps\2021\FaIIWQ\AQ_Fig02_JacksonCounty_FaIIWQ2021_SampleLocationMap.mxd
kZANCHOR Figure 2
QEA Site Layout Map
Fall 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill

C'* �'•
lea �`°o o •.
MW-03
(1,997.53) cue L
,a 0• •.
Publish Date: 2022/02/14, 11:08 PM I User: scolquhoun
Filepath: Q:\Jobs\JacksonCounty_NC_1480\Maps\2021\FaIIWQ\AQ_Fig03_JacksonCounty_FaIIWQ2021_GroundwaterElevationMap.mxd
kZANCHOR
QEA
LEGEND:
Saprolite Monitoring Well
PWR Monitoring Well
Bedrock Monitoring Well
Leachate Sample Location and Flow
Equalization Tank
Edge of Waste
Generalized GW Flow Direction for
} PWR/Saprolite
Generalized GW Flow Direction for Bedrock
Stream
Property Boundary
Road
Elevation Contour (20-Foot Interval)
NOTES:
1.Contours, roads, and parcel boundaries are
from Jackson County GIS.
2. Monitoring well locations are approximate.
3. Groundwater elevations and flow direction
are updated on a semiannual basis every April
and October following the sample collection
events.
4. Groundwater flow direction is based on
groundwater elevations in feet in monitoring
wells MW-01, MW-02, MW-03, MW-04, MW-
05R, MW-06, and MW-07. Direction is
calculated based on depth to water measured
on October 19 and 20, 2021.
5. Last names of property owners are shown in
parcels that border the landfill property.
GW: Groundwater
PWR: Partially Weathered Rock
0
0 200
Feet
Figure 3
Generalized Groundwater Flow Direction
Fall 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill

Tetrachloroethene (PCE)
5
4
�3
c
0
M
c
2
c
0
v
1
0 I Q CT'1
2008 2010 2012 2014 2016 2018 2020
Date
14
12
10
c
0 8
M
c
6
c
0
U
4
2
0
Trichloroethene (TCE)
zee;
2077
2075 $
c
0
2073 a'>i
w
2071
3
2069 o
IMI
2067
2065
J 4
\
c
0
3
c
v
o 2
U
1
0
2008 2010 2012 2014 2016 2018 2020
Date
2079
ZU.0
2077
17.5
15.0
2075
�
o
.2
J
\
0)
12.5
2073
T
LL,
o
—
10.0
2071
c
7.5
2069
Do
�7
5.0
2067
2.5
2065
0.0
2008 2010 2012 2014 2016 2018 2020 2008 2010 2012 2014 2016 2018 2020
Date Date
Benzene 1,4-Dichlorobenzene
Notes:
1. Dashed horizontal lines represent the 2L groundwater standard.
2. Dashed vertical lines represent the start of leachate extraction.
3. Non -detects are plotted as an open symbol at the method detection limit.
4. Data presented are from semiannual sampling events from 2007 to 2021.
µg/L: micrograms per liter
ft:feet
Publish Date: 02/15/2022 16:00 PM I User: SYR-SCOL
File Path: \\athena\Asheville\Projects\Jackson County`Reports - Groundwater\python\JacksonCounty-GW-Evaluation.py
kZANCHOR
QEA
611M
2077
2075 $
01
2073 v
w
2071
3
2069 0
A,
2067
2065
40
35
30
J
25
c
0
20
c
c 15
0
V
10
5
0
Cis- 1,2-Dichloroethene
2008 2010 2012 2014 2016 2018 2020
Date
2079
20.0
2077
17.5
15.0
2075
=
0
0)
12.5
i
2073
v
I=
w
0
-
10.0
'
2071
c
7.5
2069
0
U
5.0
;
2067
i 1
2.5
------------------ - --
2065
0.0
2008 2010 2012 2014 2016 2018 2020
Date
1,4-Dioxane
2079
101
2077
2075
$
�
o
J
2073
>
100�
w
0
2071
3
U
c
0
2069
Do
10-1
2067
2065
79
77
75
c
0
73 rO
v
LL,
71
3
c
69 o
y
67
65
Vinyl Chloride
i
2008 2010 2012 2014 2016 2018 2020
Date
Constituent Key with 2L Standards
f Tetrachloroethene (PCE) (0.70 µg/L)
Trichloroethene (TCE) (3 µg/L)
cis-1,2-Dichloroethene (70 µg/L)
f Vinyl Chloride (0.03 µg/L)
f Benzene (1 µg/L)
f 1,4-Dichlorobenzene (6 µg/L)
1,4-Dioxane (3 µg/L)
Groundwater Elevation (ft)
Leachate Extraction Start Date
2079
2077
2075 $
c
0
2073
w
2071
3
2069 0
0
2067
2065
Figure 4
Hydrograph and Constituents of Concern Versus Time - MW-01
Fall 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landifll

Tetrachloroethene (PCE)
5
4
0,
�3
c
0
M
c
2
c
0
U
1
H
2008 2010 2012 2014 2016 2018 2020
Date
14
12
10
c
0 8
c
0 6
c
0
U
4
2
0
2008 2010 2012 2014 2016 2018 2020
Date
Benzene
Notes:
1. Dashed horizontal lines represent the 2L groundwater standard.
2. Dashed vertical lines represent the start of leachate extraction.
3. Non -detects are plotted as an open symbol at the method detection limit.
4. Data presented are from semiannual sampling events from 2007 to 2021.
µg/L: micrograms per liter
ft:feet
1990
1988
1986
1984
1982 .o
1980 >
w
1978
1976
1974
O
1972
1970
1968
1966
J 4
\
c
0
3
c
v
o 2
U
1
0
Trichloroethene (TCE)
1
I
1
1
1
1
i
I
1
I
1
1
1
1
I
1
I
1
2008 2010 2012 2014 2016 2018 2020
Date
90 ZU.0 ,
1
58 17.5
B6
1
B4 15.0
1
c � �
B2 .L 01
12.5
BO a'� ;
LU o
78 10.0
2 1
76 0
1
1
� U 7.5 ;
74 0 0
OU---------------1------------- -- -- -----
72 5.0
1
70
1
58 2.5 ;
56
0.0
2008 2010 2012 2014 2016 2018 2020
Date
1,4-Dichlorobenzene
Publish Date: 02/15/2022 16:00 PM I User: SYR-SCOL
File Path: \\athena\Asheville\Projects\Jackson County`Reports - Groundwater\python\JacksonCounty-GW-Evaluation.py
kZANCHOR
QEA
1990
1988
1986
1984
1982 .o
1980 v
1978 v
1976 3
1974
O
1972
1970
1968
1966
40
35
30
J
25
c
0
20
2
c
15
0
U
10
5
0
Cis- 1,2-Dichloroethene
2008 2010 2012 2014 2016 2018 2020
Date
1990
20.0
1988
17.5
'
1986
;
1984 FS
15.0
1
1982 .o
12.5
1980 v
;
w
O
'
1978
10.0
1976 3
v
1974
0 7.5
p
O
U
I
1972
5.0
1970
1968
2.5
---------------------------- ---
1966
0.01
'
2008 2010 2012 2014 2016 2018 2020
Date
1,4-Dioxane
1990
101
1988
1986
1984
�
1982 .o
J
1980 >
10°
w
r
1978
2'
1976
1974 0
U
0
O
U
1972
10-1
1970
1968
1966
84
82 0
M
80 v
w
78
76
74
O
72 0
70
68
66
Vinyl Chloride
I
1
1
1
1
1
1
--------------------------------
1
2008 2010 2012 2014 2016 2018 2020
Date
Constituent Key with 2L Standards
f Tetrachloroethene (PCE) (0.70 µg/L)
Trichloroethene (TCE) (3 µg/L)
cis-1,2-Dichloroethene (70 µg/L)
f Vinyl Chloride (0.03 µg/L)
f Benzene (1 µg/L)
f 1,4-Dichlorobenzene (6 µg/L)
1,4-Dioxane (3 µg/L)
Groundwater Elevation (ft)
Leachate Extraction Start Date
1990
1988
1986
1984
1982 .o
1980
1978
1976
1974
0
1972 0
1970
1968
1966
Figure 5
Hydrograph and Constituents of Concern Versus Time - MW-02
Fall 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landifll

5
4
J
�3
c
0
M
c
2
c
0
U
1
a
14
12
10
c
0 8
M
c
(tj 6
c
0
U
4
2
0
Tetrachloroethene (PCE)
i
2008 2010 2012 2014 2016 2018 2020
Date
2009
2007
2005 $
2003 0
2001 >)
w
1999 a5
1997
c
1995 0
6
1993
1991
1989
Trichloroethene (TCE)
6
5
J 4
c
0
3
c
v
o 2
U
1 V J \
V
0
2008 2010 2012 2014 2016 2018 2020
Date
LU.0
2009
2007
17.5
2005
15.0
2003
0
12.5
2001
> >
0)
�
LL,
o
1999
a5
a
10.0
1997
�
2
c
c
7.5
1995
0
0
U
�7
5.0
1993
1991
2.5
1989
0.0
2008 2010 2012 2014 2016 2018 2020 2008 2010 2012 2014 2016 2018 2020
Date Date
Benzene 1,4-Dichlorobenzene
Notes:
1. Dashed horizontal lines represent the 2L groundwater standard.
2. Dashed vertical lines represent the start of leachate extraction.
3. Non -detects are plotted as an open symbol at the method detection limit.
4. Data presented are from semiannual sampling events from 2007 to 2021.
µg/L: micrograms per liter
ft:feet
Publish Date: 02/15/2022 16:00 PM I User: SYR-SCOL
File Path: \\athena\Asheville\Projects\Jackson County`Reports - Groundwater\python\JacksonCounty-GW-Evaluation.py
kZANCHOR
QEA
2009
2007
2005 $
2003 0
M
2001 v
w
1999 v
1997
c
1995 0
6
1993
1991
1989
40
35
30
25
c
0
20
2
c
a�
c 15
0
U
10
5
0
Cis- 1,2-Dichloroethene
2008 2010 2012 2014 2016 2018 2020
Date
2
0.0
2009
2007
17.5
2005
15.0
2003 0
12.5
2001 >
'E�
;
w
0
1999 v
o 10.0
�
1997
c
7.5
1995 o
U
t7
5.0
1993
1991
2.5
'
1989
0.0
2008 2010 2012 2014 2016 2018 2020
Date
1,4-Dioxane
2009
101
2007
2005
$
2003 0
10°
2001 >
w
1999 a,
P
�
1997
c
0
1995 0
U
L7
10-1
1993
1991
1989
09
07
05
03 0
0%
91
89
Vinyl Chloride
2008 2010 2012 2014 2016 2018 2020
Date
Constituent Key with 2L Standards
f Tetrachloroethene (PCE) (0.70 µg/L)
Trichloroethene (TCE) (3 µg/L)
cis-1,2-Dichloroethene (70 µg/L)
f Vinyl Chloride (0.03 µg/L)
f Benzene (1 µg/L)
f 1,4-Dichlorobenzene (6 µg/L)
1,4-Dioxane (3 µg/L)
Groundwater Elevation (ft)
Leachate Extraction Start Date
2009
2007
2005 $
2003 0
2001
w
1999
1997
c
1995 0
1993
1991
1989
Figure 6
Hydrograph and Constituents of Concern Versus Time - MW-03
Fall 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landifll

5
4
J
�3
c
O
M
R
14
12
10
c
O 8
M
c
(tj 6
c
O
U
4
2
0
Tetrachloroethene (PCE)
1958
6
5
1956 $
o
J
4
a>i
�
1954LU
3
�
3
c
v
_0
D
0
U
rZ
O 2
O
U
1952
1
1950
0
Trichloroethene (TCE)
2008 2010 2012 2014 2016 2018 2020 2008 2010 2012 2014 2016 2018 2020
Date Date
1958
20.0
17.5
1956_
15.0
�
o
J
�
0)
12.5
a>i
�
1954
�
10.0
�
c
U
7.5
O
o
U
1952
5.0
2.5
1950
0.0
2008 2010 2012 2014 2016 2018 2020 2008 2010 2012 2014 2016 2018 2020
Date Date
Benzene 1,4-Dichlorobenzene
Notes:
1. Dashed horizontal lines represent the 2L groundwater standard.
2. Dashed vertical lines represent the start of leachate extraction.
3. Non -detects are plotted as an open symbol at the method detection limit.
4. Data presented are from semiannual sampling events from 2007 to 2021.
µg/L: micrograms per liter
ft:feet
Publish Date: 02/15/2022 16:00 PM I User: SYR-SCOL
File Path: \\athena\Asheville\Projects\Jackson County`Reports - Groundwater\python\JacksonCounty-GW-Evaluation.py
kZANCHOR
QEA
1958
40
35
1956 $
30
C
0
25
1954
20
�
c
c
O
15
O
U
1952
10
5
1950
0
Cis- 1,2-Dichloroethene
2008 2010 2012 2014 2016 2018 2020
Date
1958
20.0
17.5
1956
15.0
o
0) 12.5
v
LU
1954
10.0
�
c
7.5
O
O
U
i
1952
5.0
2.5
-------------------
1950
0.0
2008 2010 2012 2014 2016 2018 2020
Date
1,4-Dioxane
1958
101
1956 $
C
o
�
>
100
v
�
1954
�
3
c
U
�
C
U
0
O
1952 6
U
10-1
1950
f:
c
O
i2 0
0
Vinyl Chloride
I-q--------- -------------------
2008 2010 2012 2014 2016 2018 2020
Date
Constituent Key with 2L Standards
f Tetrachloroethene (PCE) (0.70 µg/L)
Trichloroethene (TCE) (3 µg/L)
cis-1,2-Dichloroethene (70 µg/L)
f Vinyl Chloride (0.03 µg/L)
f Benzene (1 µg/L)
f 1,4-Dichlorobenzene (6 µg/L)
1,4-Dioxane (3 µg/L)
Groundwater Elevation (ft)
Leachate Extraction Start Date
1958
1956
c
O
a�
1954
3
C
Z)
O
1952 6
1950
Figure 7
Hydrograph and Constituents of Concern Versus Time - MW-04
Fall 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landifll

J
a
c
0
c
U
c
0
U
5
0
2008 2010 2012 2014 2016 2018 2020
Date
14
12
10
c
0 8
M
c
0 6
c
0
U
4
2
0
Trichloroethene (TCE)
B9
57
79
77
J 4
c
0
3
c
v
o 2
U
1
0
2008 2010 2012 2014 2016 2018 2020
Date
I yjbj
LU.0
17.5
1987
15.0
1985
0
.2
12.5
a>i
0)
�
LL,
o
1983
�
10.0
�
2
c
1981
_0
0
c
0
7.5
0
U
�7
5.0
1979
2.5
1977
0.0
2008 2010 2012 2014 2016 2018 2020 2008 2010 2012 2014 2016 2018 2020
Date Date
Benzene 1,4-Dichlorobenzene
Notes:
1. Dashed horizontal lines represent the 2L groundwater standard.
2. Dashed vertical lines represent the start of leachate extraction.
3. Non -detects are plotted as an open symbol at the method detection limit.
4. Data presented are from semiannual sampling events from 2007 to 2021.
µg/L: micrograms per liter
ft:feet
Publish Date: 02/15/2022 16:00 PM I User: SYR-SCOL
File Path: \\athena\Asheville\Projects\Jackson County`Reports - Groundwater\python\JacksonCounty-GW-Evaluation.py
kZANCHOR
QEA
1989
1987
1985 0
v
w
1983
3
1981
O
A,
1979
1977
40
35
30
25
c
0
20
2
c
15
U
10
5
0
Cis- 1,2-Dichloroethene
2008 2010 2012 2014 2016 2018 2020
Date
1989
20.0
i
17.5
i
1987
15.0
1985
0
LD
12.5
v
0)
w
g
1983
10.0
�
c
1981
7.5
O
O
U
t7
5.0
1979
-------------- {----------- - - --
2.5
1977
0.0
2008 2010 2012 2014 2016 2018 2020
Date
1,4-Dioxane
1989
101
1987
1985
0
>
100
v
w
rZ
1983
0
1981
0
0
10-1
1979
1977
87
85
c
O
v
83 w
79
Vinyl Chloride
i
2008 2010 2012 2014 2016 2018 2020
Date
Constituent Key with 2L Standards
f Tetrachloroethene (PCE) (0.70 µg/L)
Trichloroethene (TCE) (3 µg/L)
cis-1,2-Dichloroethene (70 µg/L)
f Vinyl Chloride (0.03 µg/L)
f Benzene (1 µg/L)
f 1,4-Dichlorobenzene (6 µg/L)
1,4-Dioxane (3 µg/L)
Groundwater Elevation (ft)
Leachate Extraction Start Date
1989
1987
1985 0
a�
w
1983
1981 ZS
0
1979
1977
Figure 8
Hydrograph and Constituents of Concern Versus Time - MW-05R
Fall 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landifll

5
4
�3
c
O
M
c
2
c
O
U
1
H
14
12
10
c
0 8
M
c
(tj 6
c
0
U
4
2
0
Tetrachloroethene (PCE)
2008 2010 2012 2014 2016 2018 2020
Date
Trichloroethene (TCE)
cis- 1,2-Dichloroethene
2066
6
2066
40
2066
101
2064
2064
2064
35
2062
5
2062
2062
2060 $
2060 $
30
2060 $
4
2058
2058
0)
25
2058 0
10o
>�
°
i
>
°
>
2056 "'
3
------- - ------ --- --- ----- - _.
2056 "'
20
2056 LU
2054 3
v
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2054
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2052
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2052
c
0
15
'
2052
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0
0
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0
U
2050
2050
10
2050 0
10-1
1
2048
2048
5
2048
2046
2046
2046
0
0
2008 2010 2012 2014 2016 2018 2020
2008 2010 2012 2014 2016 2018 2020
Date
Date
LUbb
LU.0
2064
17.5
2062
Y
15.0
2060
J
o
2058
\
12.5
o
LL
2056 u
�
10.0
2054
c
7.5
2052 o
U
2050
5.0
2048
2.5
2046
0.0
2008 2010 2012 2014 2016 2018 2020 2008 2010 2012 2014 2016 2018 2020
Date Date
Benzene 1,4-Dichlorobenzene
Notes:
1. Dashed horizontal lines represent the 2L groundwater standard.
2. Dashed vertical lines represent the start of leachate extraction.
3. Non -detects are plotted as an open symbol at the method detection limit.
4. Data presented are from semiannual sampling events from 2007 to 2021.
µg/L: micrograms per liter
ft:feet
Publish Date: 02/15/2022 16:00 PM I User: SYR-SCOL
File Path: \\athena\Asheville\Projects\Jackson County`Reports - Groundwater\python\JacksonCounty-GW-Evaluation.py
kZANCHOR
QEA
2066
20.0
2064
17.5
,
2062
15.0
2060
J
0
2058
12.5
v
°
2056 w
10.0
2054 3
v
7.5
,
2052 0
U
2050 0
5.0
2048
2.5
-- --- ----------- -- --
2046
0.0
2008 2010 2012 2014 2016 2018 2020
Date
1,4-Dioxane
64
62
60
58 0
56
a,
54 3
52
O
50
48
46
Vinyl Chloride
i\\/II
-------------------------
2008 2010 2012 2014 2016 2018 2020
Date
Constituent Key with 2L Standards
f Tetrachloroethene (PCE) (0.70 µg/L)
Trichloroethene (TCE) (3 µg/L)
cis-1,2-Dichloroethene (70 µg/L)
f Vinyl Chloride (0.03 µg/L)
f Benzene (1 µg/L)
f 1,4-Dichlorobenzene (6 µg/L)
1,4-Dioxane (3 µg/L)
Groundwater Elevation (ft)
Leachate Extraction Start Date
2066
2064
2062
2060
0
2058
a�
2056
a�
2054 3
2052
0
2050
2048
2046
Figure 9
Hydrograph and Constituents of Concern Versus Time - MW-06
Fall 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landifll

Tetrachloroethene (PCE)
5
4
J
�3
c
O
M
c
2
c
O
U
1
0
2008 2010 2012 2014 2016 2018 2020
Date
14
12
10
c
O 8
M
c
6
c
O
U
4
2
0
Trichloroethene (TCE)
1954
6
5
1952
0
4
w
O
3
3
qj
v
1950
�
rZ
2
0
1
1948
0
2008 2010 2012 2014 2016 2018 2020
Date
1954
20.0
17.5
15.0
1952
0
.2
12.5
a>i
0)
�
12
10.0
�
c
u
1950
0
7.5
O
U
�7
5.0
2.5
1948
0.0
1954
40
35
$
30
1952
0
25
°J
w
o
— 20
3
1950
0 15
O
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t7
10
5
1948
0
1954
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17.5
15.0
1952
0
.2
12.5
v
0)
�
—
10.0
o
�
c
v
1950
0
7.5
O
U
5.0
2.5
1948
0.0
Cis- 1,2-Dichloroethene
2008 2010 2012 2014 2016 2018 2020
Date
2008 2010 2012 2014 2016 2018 2020 2008 2010 2012 2014 2016 2018 2020 2008 2010 2012 2014 2016 2018 2020
Date Date Date
Benzene 1,4-Dichlorobenzene 1,4-Dioxane
Notes:
1. Dashed horizontal lines represent the 2L groundwater standard.
2. Dashed vertical lines represent the start of leachate extraction.
3. Non -detects are plotted as an open symbol at the method detection limit.
4. Data presented are from semiannual sampling events from 2007 to 2021.
µg/L: micrograms per liter
ft:feet
Publish Date: 02/15/2022 16:00 PM I User: SYR-SCOL
File Path: \\athena\Asheville\Projects\Jackson County`Reports - Groundwater\python\JacksonCounty-GW-Evaluation.py
kZANCHOR
QEA
1954
101
1952 0
>
10°
v
w
�
O
3
0
1950 �
rZ
0
0
O
U
0
10-1
1948
1952
c
O
Y
1948
Vinyl Chloride
2008 2010 2012 2014 2016 2018 2020
Date
Constituent Key with 2L Standards
f Tetrachloroethene (PCE) (0.70 µg/L)
Trichloroethene (TCE) (3 µg/L)
cis-1,2-Dichloroethene (70 µg/L)
f Vinyl Chloride (0.03 µg/L)
f Benzene (1 µg/L)
f 1,4-Dichlorobenzene (6 µg/L)
1,4-Dioxane (3 µg/L)
Groundwater Elevation (ft)
Leachate Extraction Start Date
1954
F_
1952 0
1948
a�
w
Me
Figure 10
Hydrograph and Constituents of Concern Versus Time - MW-07
Fall 2021 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landifll

Appendix A
Well Sampling Logs, and Equipment
Documentation and Instrument
Calibration Data Sheets

Anchor QEA of North Carolina, PLLC
231 Haywood Street
k ANCHOR
QEA u
Asheville. North Carolina 28801
Well Sampling Log
Well ID: MW-01
Project Name:
Jackson County Landfill
Date: ld /'Lo,"Zo
Project Number.
C11480-01.02
Weather. "7eq si/hs,
Project Location:
Dillsboro, NC
Facility ID or Permit # (if applicable): 50-02
Sample Collector(s):
gG
Sample ID (on COC): MW-01-ZF Z 1 irk 2_-0
Well Diameter:
2
in Sample Time:
Screen Interval:
N/A
ft bgs
Measuring Point:
TOC
Well Depth (WD): 110.5
ft TOC
Well Type:
NStick Up oFlush Mount
Water Level in Feet (WL):
ft TOC
Comments: .4 0, o (
Length of Water Column (LWQ: ' �
ft; (WD - WL)
^
One Casing Volume:
gallons; (LWC x WCV)
Three Casing Volumes: 7 f
gallons aG bl
Actual Volume Purged:
gallons
Tagged Bottom:
, . 7 ft at (time): Three Casing Volumes:
gallons
Well Casing Volumes (WCV)
1" = 0.04 Gal/Ft 2" = 0.16 Gal/Ft 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft
Purge Method:
Bailer-Dis Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other:
Bailer-Dis Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other.
Sample Method:
Oxidation
Dissolved
Specific
pH (S.U.)
Reduction
Gallons
Temperature
Oxygen
Conductivity
report to 0.1
Potential
Turbidity
Reading
Time
Purged
(°C)
(mg/L)
(pmhos/cm)
S.U.
(mv)
(NTU)
Comments
1
r
1 1I/r.�-i
V
2ID
I
i
PJ
,
O
3
!
s
4
p
�/
5
6
7M
:..
8
9
10
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
1 L Glass
Other
Protective Casing: J
Pad: Lock: VegetationVVj_V Access:
Sample Analysts
Sample
Signature:
Analysts OLVI �St�i Date:
Name:
_K_ L.J`�^'L
b
Notes:
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% nd turbidity, +/- 3% Conductivity, +/- 0.1 pH unit; +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
Abbreviations: Method Reference:
°C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter ft: feet Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter in: inches DO: SM 4500 0 G-2011
mV: millivolt bgs: below ground surface pH: SM 4500-H` B-2011
NTU: nephelometric turbidity units TOC: top of casing Turbidity: SM 2130 B-2011
Page 1 of 1

ANCHOR
At
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Well Sampling Log
Well ID: MW-02
Project Name: Jackson County Landfill
Date:
f alle(lZ J`Z (— i
Project Number. C11480-01.02
Weather:
_3 6'd= ,r 1,;iX All
R�J
Project Location: Dillsboro, NC
Facility ID or Permit # (if applicable):
50-02
Sample Collector(s): 5 Cr /e in
�T
Sample ID (on COQ
MW-02-
Well Diameter. 2
in Sample Time:
Screen Interval: N/A
ft bgs
Measuring Point: TOC
Well Depth (WD):
60.7
ft TOC
Well Type: XStick Up ❑Flush Mount
Water Level in Feet (WL):
"(o, ! jj
ft TOC
/
Comments: aJ'� r p��>!vo
Length of Water Column (LWQ:
Z 0, S— �%
ft; (WD - WL)
A IX JhAll,
One Casing Volume:
Z . .)_ cy
gallons; (LWC x WCV)
—WA,aj,
A
c Three Casing Volumes: �� gall s+b b6t,c� 5
1
��_[[��}}
6f�'
, G1 Actual Volume Purged:
a �� ,
Ilons
fagged Bottom: L. �Z ft at (time):
p �l S Three Casing Volumes:
gallons
Well Casing Volumes (WCV)
1" = 0.04 Gal/Ft 2" = 0.16 Gal/Ft 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft
8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft
Purge Method: Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos
Other:
Sample Method: Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos
Other.
Oxidation
Dissolved
Specific
pH (S.U.)
Reduction
Gallons
Temperature
Oxyge
Conductivity
report to 0.1
Potential
Turbidity
Reading
Time
Purged
(°C)
(
(pmhos/cm)
S.U.
(mv)
(NTU)
Comments
1
0l0
4�
2
tfi
S-A
0 1 4
3
L0
1
14 AC4.
4
fill'0
4
�.
tJ�Vs
0 v,.
5
2 .
S,
D1. I
S 2
L+
• U
6
7
8
9
10
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
1 L Glass
Other
Protective Casing: Pad: Lock: Vegetation: Access:
Sample Analysts
Sample
Signature
Analysts 1 Date:
Name: 'Q S t�
Notes: U
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity, +/- 3% Conductivity; +/- 0,1 pH unit; +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
Abbreviations:
°C: degrees Celsius S.U: standard units
pmhos/cm: micromhos per centimeter ft: feet
mg/L: milligrams per liter in: inches
mv: millivolt bgs: below ground surface
NTU: nephelometric turbidity units TOC: top of casing
i0ivI ��o J\ . b W w
rUL)
® r, 11)( d()M 1
Method Reference:
Temperature: SM 2550 B-2010�tA!?� r• "^'� `^ J
Specific conductivity: EPA Method 120.1, Rev. 1982 �•� o, to �) on
DO:SM 4500 O G-2011 V�
pH:SM 4500-H' B-2011
��� �� SVt)6f V}0Q' is a� OY{ Page 1ofl

ANCHOR
QEA u
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Low -Flow Sampling Log
Well ID: MW--03.
Project Name: Jackson County Landfill
Project Number. C11480-01.02
Project Location: Dillsboro, NC
Sample Collector(s): S •I P
Well Diameter: 2
Screen Interval: 48.5-63.5
Well Depth (as constructed): 65.5
Depth to Water. �/r'.60
Measuring Point: TOC
Depth of Pump Intake: 960-
Pump Used (circle): Peristaltic Bladder
Comments: Start microsee j 1. _
Stop microSeep:
Date: _10.At) AV R 1
Weather: S�F�
Facility ID or Permit # (if applicable): 50-02 USJ
Sample ID (on COC): MW-03-
in Arrive at Well:y Gj ,� 2j
ft bgs StartTime: tvzt _
ft bgs Sample Time: U01TO
ft Leave Well:
Well Type: XS/tick Up ❑Flush Mount
�
ft Tagged Bottom: 1FJ�" ft at (time): d cl s
Other (describe): Purge Rate:
_ Total Volume Purged:
Pump Speed: 0- [.3 N: 37
Time
DTW (feet)
Temperature (°C)
Dissolved Oxygen
(mg/L)
Specific
Conductivity
(pmhos/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (m1)
Turbidity (NTU)
- 2
N - 0
117
2't ff, `(
t 31 D
1,04
q c
44A
tc�3o
7
�.,. ^ (
. 7
Z 3. y
Sal
t0�
Ir
Sample Analyst Signature:
Sample Analyst
Name:
Date:
cold I
Notes: U
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 70% DO and turbidity +/- 3% Conductivity, +/- 0.1 pH unit +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
5. 1 pmho/cm = 1 pS/cm
Abbreviations:
Method Reference:
°C: degrees Celsius S.U.: standard units
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter ft: feet
Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter in: inches
DO: SM 4500 O G-2011
mv: millivolt bgs: below ground surface
pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units TOC: top of casing
Turbidity: SM 2130 B-2011
�ti o Art lrD1 �' P 0 +C'1 �o S� c��A-"� °&` F
Sptn V1'4AI
.Vow �bs�cv�d @tip ,piA. Do
� 10 .
tt : biv (� ylf�c"
crud ""— Page 1 of 1

ANCHOR
�► QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Low -Flow Sampling Log
IWO ID: MW-04
Project Name: Jackson County Landfill
Project Number. C11480-01.02
Project Location: Dillsboro, INC
Sample Collector(s): A
Well Diameter. 2
Screen Interval: 25 - 40
Well Depth (as constructed): 43
Depth to Water. X '
Measuring Point: TOC
Depth of Pump Intake: 35
Pump Used (circle):^ Peristaltic Bladder
Comments: Start MiCroSeer i 7T. �fl
Stop micrOSeep: i 'j,�') } _
Date: iC/ f e( /2_02-
Weather: �SE'/'.✓,�.1u
Facility ID or Permit * (if applicable): 50-02
Sample ID (on COQ: MW-U4-
in Arrive at Well: ( CjO_¢r
ft bgs Start Time: (0 ,3+Y
ft bgs Sample Time: i 0,57y
ft Leave Well:
Well Type: KStick Up ❑Flush Mount f +�
ft Tagged Bottom: y Z - t•(X ft at (time):
Other (describe): Purge Rate: 360 %..,yq
�( T %s wm'rtt Total Volume Purged:
Pump Speed: 0.,r
Time
DTW (feet)
Temperature (°C)
Dissolved Oxygen
(mg/L)
Specific
Conductivity
(pmhos/cm)
PH (S.U.)
report to o.f S.U.
Oxidation
Reduction
Potential (mV)
Turbidity (NTU)
1, 3r
2,6- • l .-
rY . 7
S 6®
d Y 7
S y
f:7
.211. zz
,031
26. 053
4(1 Y.
,a 7
6,11
sS
zs7
213
to -to
2G- LS
d n
1 3
6 11
3 2Z. ?
(.gam
b�i3
2�. osi
l ty,
61 F, 0
9-7
yam. 0
1. `f i
l0"IL
2_6.nf
IS'.
'. �
(���
S17
YsLt. V
'0 `
l I
SS Yv
`f
57 7
'YqS,°7
la y:
I�SZ
z6,L)
.
. 7`i
�S�_s`
5(_ 7
s 0q.0
)t'
i05
& s-
5`.7
.S /_3
1 0
Sample Analyst Signature:
Sample Analyst
Name:
p
e Su
Date:
'w
1 O d W
Notes: U
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity, +/- 3% Conductivity,* +/- 0.1 pHunit; +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
5. 1 pmho/cm = 1 pS/cm
Abbreviations:
°C: degrees Celsius
S.U.: standard units
pmhos/cm: micromhos per centimeter
ft: feet
mg/L: milligrams per liter
in: inches
mv: millivolt
bgs: below ground surface
NTU: nephelometric turbidity units
TOC: top of casing
fu wv? o n OCR to, a�
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
PH: SM 4500-H' B-2011
Turbidity: SM 2130 B-2011
Page 1 of 1

ANCHOR.
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Well Sampling Log
Well ID: MW-05R
Project Name: Jackson County Landfill
Date:
Project Number. C11480-01.02
Weather:
■j
Project Location: Dillsboro, NC
Facility ID or Permit # (if applicable): 50-02
Sample Collector(s): SC)' i _?
Sample ID (on COC): MW-OSR-
Well Diameter: 2
in Sample Time: ; 6 0S-
Screen Interval: N/A
ft bgs
Measuring Point: TOC
Well Depth (WD): 54
ft TOC
Well Type: §Stick Up ❑Flush Mount
Water Level in Feet (WL): 'I (p, 14
ft TOC
I i
:omments: _I��2 F:i y t) �, I r (j., . c< Length of Water Column (LWQ: -4 , 'bCa
ft; (WD - WL)
ipiv�
One Casing Volume: l , A LOP
gallons; (LWC x WCV)
Sct sta
Three Casing Volumes: —4 -
gallons ((D b c4aS'
0'rV/ : J , ( �U
Actual Volume Purged: ay
gallons
_
Tagged Bottom: (� (a —1ft at (time): © Three Casing Volumes:
gallons
Well Casing Volumes (WCV)
1" = 0.04 Gal/ F 2" = 0.16 Gal/Ft 3" = 0.37 Gal/Ft 4" = 0.65 Gal/Ft 6" = 1.47 Gal/Ft 8" = 2.61 Gal/Ft 12" = 5.87 Gal/Ft
Purge Method: U Hailer-Disp. I Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other:
zdmple Method: Bailer-Disp. Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other:
Oxidation
_ 7D-31,1
Dissolved
Specific
pH (S.U.)
Reduction
Gallons
Temperature
Oxygen
Conductivity
report to 0. i
Pptential
Turbidity
Reading
Time
Purged
CQ
(mg/L)
(Nmhos/cm)
S.U.
(mV) o
(NTU)
Comments
1
's ®
t
DVS
(�i^i
7
(`._i+�
171
ry♦ r
11
3
loa
1
7Z7
s7
1 O
4
�I
-�.
7 Oq ro
5
6
�r
.i7
t
ICE
7
8
9
10
Sampling Container
Number of containers
Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
1 L Glass
Other
Protective Casing: Pad: . Lock Vegetation: Access:_
Sample Analysts
Signature: f
amp e
Analysts
..4.,y(� j iC/��� Date:
7
`011 `e61 Zj
Name: 'L
Notes:
,..Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity, +/- 3% Conductivity, +/- 0.1 pH unit,' +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection. \QA_ot,,�
P
1 �� W % � , -r� ( P ,� J TZ
4. NC Field Laboratory Certificate Number 5445 1i (J f" >] (k�
Abbreviations: Method Reference:
°C: degrees Celsius S.U.: standard units Temperature: SM 2550 B-2010
umhos/cm: micromhos per centimeter ft: feet Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter in: inches DO: SM 4500 0 G-2011
mv: millivolt bgs: below ground surface pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units r� [[TOC: top fof casing Turbidity: SM 2130 B-2011 l i , D, " ,,� nq,
(� a �J� vxku Tu SA, � �dmtS �Rt�lt V1 A—) IDd_e.'�til. Page 1 of 1
wb lS r ��>� i ra C 1P'� �-` v �i'`re.`a" Gbl.�-� �t—

ANCHOR
.-v QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Low -Flow Sampling Log
Well ID: MW-06
Project Name: Jackson County Landfill
Project Number. C11480-01.02
Project Location: Dillsboro, NC
Sample Collector(s): G ►��
Well Diameter. 2
Screen Interval: 84-94
Well Depth (as constructed): 94
Depth to Water: J:q,GJ5
Measuring Point: TOC
Depth of Pump Intake: 91
Pump Used (circle): Peristaltic Bladder
Comments: start mlcroseep:: % A3 3
stop microseep: d cyr, j
Date:
Weather: E &wl
Facility ID or Permit # (if applicable): 50-02
Sample ID (on COQ: MW-06-
in Arrive at Well: ,45
ft bgs Start Time:
ft bgs Sample Time: t 3,3
ft Leave Well:
Well Type: KStick� Up ❑Flush Mount
/71— ft at (time): �r
ft Tagged Bottom: 1°l
Other (describe): Purge Rate: 2.06
Total Volume Purged:
_ Pump Speed:Zy=ems
Time
DTW (feet)
Temperature (*Q
Dissolved Oxygen
(mg/L)
Specific
Conductivity
(pmhos/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (m1)
Turbidity (NFU)
Is fp
. I J
lr S
1 : 7
Ls®a .i
L.[`/]_
-3 221 2—
ZS
v�°'QQa
y
�`j
(%
/ti
P
i3z
8D<r{,
l5 -6
; ,(
-57, V
3d 1.3
il37z
011,i7
l �
!
vT?•
3TL*.7
3p3f3
[32-,2
rt%
�7
/
LLc
�7r3
y:S
Cr
33 1. 6
( 330
M 17
S`, (,6
S7>
Al. S_
33 J. 6
,
Sample Analyst Signature:
Sample Analyst
Name:
1� �-,- i.e re S S lcq Date:
10 p2 '
Notes:
1: Stabilization (3 successive readings, 3 minutes apart): within +/- 10% DO and turbidity, +/- 3% Conductivity,' +/- 0.7 pH unit; +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is.still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
S. 1 Nmho/cm = 1 pS/cm
Abbreviations:
Method Reference:
°C: degrees Celsius S.U.: standard units
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter ft: feet
Specific conductivity: EPA Method 1201, Rev. 19.82
mg/L: milligrams per liter in: inches
DO: SM 4500 O G-2011
mV: millivolt bgs: below ground surface
pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units TOC: top of casing
Turbidity: SM 2130 B-2011
Page 1 of 1

ANCHOR
._i QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Low -Flow Sampling Log
well ID: MW-07
Project Name: Jackson County Landfill Date:
Project Number. C11480-01.02 Weather.. rj
Project Location: Dillsboro, NC Facility ID or Permit # (if applicable): 50-02
Sample Collector(s): (� Sample ID (on COC): MW-07-
Well Diameter: 2 in Arrive at Well: %
Screen Interval: 70 - 95 ft bgs Start Time:
Well Depth (as constructed): 95 ft bgs Sample Time:
Depth to Water. ?� F;. ft Leave Well:+-�^ s
Measuring Point: TOC _ Well Type: Atick Up ❑Flush Mount
Depth of Pump Intake: 85 ft Tagged Bottom: ft at (time):
Pump Used (circle): Peristaltic Bladder Min Other (describe): Purge Rate:
Comments: start microseep e " Total Volume Purged:
�'_� �P�t l� � f�f1V11-� g
stop microseep: Jc4 Z Pump Speed: 1A 2,49
Time
DTW (feet)
Temperature ('C)
Dissolved Oxygen
(mg/L)
Specific
Conductivity
(Nmhos/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (m1)
Turbidity (NTU)
itj
-71 5 T
4-
i o Y
0, 47
3114C4f
�,� a
gt 7
6:r G
l 7 .• '
(r
'
3 if."o
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F22
Geo
170,7
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,7J-
IA3
f 2zs
6.o
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.3
6
3
�
i �
S'2 7
6.0
16 (, -7
9 . Y 4`
` �
7S
V � r
j CSS
(cl V•'
Si ?.
6.0
1 3'
T. y,J
£5L
Gco
f
19053?
51,q 1
[S IL
34-L
5ze.
6
�3
Sample Analyst Signature:
Sample Analyst
Name:,S(_P_
j t�J�
Date:
Notes:
1: Stabilization (3 successive readings, 3 minutes apart): within +/-.10% DO and turbidity; +/- 3% Conductivity, +/- 0.7 pH unii; +/- 70 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2017)
2. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
3. Samples are analyzed immediately upon collection.
4. NC Field Laboratory Certificate Number 5445
S. 1 pmho/cm = 1 pS/cm
Abbreviations:
Method Reference:
°C: degrees Celsius S.U.: standard units
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter ft: feet
Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter in: inches
DO: SM 4500 O G-2011
mV: millivolt bgs: below ground surface
pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units TOC: top of casing
Turbidity: SM 2130 B-2011
%
d\klCto -3a o��AA t
P
Page 1 of 1

ANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Surface Water Sampling Log
Location ID: SW-01
Project Name:
Jackson County Landfill
Date:
Project Number:
C11480-01.02
Weather:
Project Location:
Dillsboro, NC
Facility ID or Permit # (if applicable):
50-02
Sample Collector(s): '(: r. 0
Sample ID (on COC):
SW-01-0 P
Comments:
Upstream of landfill
Sample Method (circle
Grab Syringe
Pump
Bailer Disp.
Other:
one)
Specific
Oxidation
Temperature
Dissolved
Conductivity
pH (S.U.)
Reduction
Turbidity
Time
CC)
Oxygen (mg/L)
(pmhos/cm)
report to 0.1 S.U.
Potential (mV)
(NTU)
Comments
0s
t .�-
q�3�1
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
J 0
1 L Glass
Other
Vegetation: Nr7t � A U Ir1 Access: ML—h
Sample Analyst `
Sample Analyst Signature: Name: Mf—I /� P ! L 1 Date: ip 11 "1 I X 01
1. Documentation errors are to be crossed out with a sinale line, so the
2. Samples are analyzed immediately upon collection.
3. NC Field Laboratory Certificate Number 5445
Abbreviations:
°C: degrees Celsius
pmhos/cm: micromhos per centimeter
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
text is still legible, followed by the staff members initials and date
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
PH: SM 4500-H* B-2011
Turbiditv: SM 2130 B-2011
Page 1 of 1

ANCHOR
QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Surface Water Sampling Log
Location ID: SW-02
Project Name: Jackson County Landfill
Project Number: C11480-01.02
Project Location: Dillsboro, NC
Sample Collector(s): SC, W
Comments: Downstream of landfill
Date: aDC j t
Weather: J u47-r
Facility ID or Permit # (if applicable): 50-02
Sample ID (on COC): SW-02-
Sample Method (circle
one):
Grab
Q
Syringe
Pump
Bailer-Disp. Other:
Time
Temperature
VQ
Dissolved
Oxygen (mg/L)
Specific
Conductivity
(pmhos/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (mV)
Turbidity
(NTU)
Comments
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
' �S
125 mL Plastic
40 mL Glass
ko
1 L Glass
Other
Vegetation: Access: 6-rf"��
Sample Analyst
1. Documentation errors are to be crossed out with a single line, so the
2. Samples are analyzed immediately upon collection.
3. NC Field Laboratory Certificate Number 5445
Abbreviations:
°C: degrees Celsius
pmhos/cm: micromhos per centimeter
mg/L: milligrams per liter
mV: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Sample Analyst t' 'c
Name: F O ` � 9 W S �� Date: 1 V
text is still legible, followed by the staff members initials and date
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 0 G-2011
pH: SM 4500-H* B-2011
Turbidity: SM 2130 B-2011
Page 1 of 1

ANCHOR
Q EA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Sampling Log - Grab
Location ID: LT-01
Project Name:
Project Number:
Project Location:
Sample Collector(s):
Comments:
Jackson County Landfill
C11480-01.02
Dillsboro, NC
nn
Date: `o d
Weather.
Facility ID or Permit # (if applicable): 50-02
Sample ID (on COQ LT-01- jbo)1 O
Ir ire
Sample Method (circle one): Grab
Syringe
Pump Bailer-Disp.
Other.
Time
Temperature
VQ
Dissolved
Oxygen
(mg/L)
Specific
Conductivity
(Nmhos/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (mV)
Turbidity
(NTU)
Comments
Lts oo
4q
-Cl► '%
a .q5
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
V1 r
125 mL Plastic
40 mL Glass
VD
d A D S 1^ rn
1 L Glass
I =r
Vegetation: � A Access: La� - i n IVW
- ^ Sample Analyst
Sample Analyst Signature: Analyst
I t ` C S S Date:
Notes:
1. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
2. Samples are analyzed immediately upon collection.
3. NC Field Laboratory Certificate Number 5445
Abbreviations:
"C: degrees Celsius
Nmhos/cm: micromhos per centimeter
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
pH: SM 4500-H` B-2011
Turbidity: SM 2130 B-2011
Page 1 of 1

ANCHOR
L-vQEA`
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
_Sampling Log - Grab
Location ID: DW-01
Project Name:
Project Number:
Project Location:
Sample Collector(s):
Comments:
Jackson County Landfill Date:;
C11480-01.02 Weather.
Dillsboro, NC Facility ID or Permit # (if applicable):
�i�� Sample ID (on COC):
Purged 30 gallons prior to sampling. Wilkey residence.
Q G ._ u n n
50-02
DW-01-� d
Sample Method (circle one): Grab
Syringe
Pump
Bailer-Disp. Other.
Time
Temperature
VQ
Dissolved
Oxygen
(mg/L)
Specific
Conductivity
(Nmhos/cm)
pH (S.U.)
report to 0.1 S.U.
Oxidation
Reduction
Potential (mV)
Turbidity
(NTU)
Comments
�� �
► �
3,38
1`3, 6
63
&9�5
7,1-(
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
1 L Glass
er
Vegetation: N N
Access:
Sample Analyst Sample Analyst Signature: A� Name: eo Ae, �_„ h'L'9 " Date:
Notes:
1. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
2. Samples are analyzed immediately upon collection.
3. NC Field Laboratory Certificate Number 5445
Abbreviations:
°C: degrees Celsius
pmhos/cm: micromhos per centimeter
mg/L: milligrams per liter
mV: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
PH: SM 4500-H' B-2011
Turbidity: SM 2130 B-2011
Page 1 of 1

A. -.ANCHOR
QEA «"
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Surface Water Sampling Log
Location ID:
Project Name:
4Sc,^
C."f � L'
//'
F,` f f
Date:
C0/Zc�'/Z-vZ
Project Number:
C —©1 r 0 Z
Weather:
. Jr _ ck
Project Location:
Facility ID or Permit # (if applicable):
tj 6-0 �f
Sample Collector(s):
Sample ID (on COC):
t,✓—C? 2 ZJ Z f (r7 j
Comments:
Sample Method (circle
one):
Grab
Syringe
Pump
Bailer-Disp.
Other:
Specific
Oxidation
Temperature
Dissolved
Conductivity
pH (S.U.)
Reduction
Turbidity
Time
(°C)
Oxygen (mg/L)
(pmhos/cm)
report to 0.1 S.U.
Potential (mV)
(NTU)
Comments
D
7:f
�. � `A
I
Sampling Container
Number of Containers
Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
3
ti0 ('
1 L Glass
Other
Vegetation: A_� ``10 � 144WA)
Access: V' 4'a -/
Sample Analyst
Sample Analyst Signature: J`( —ule— (i c,L(I Name: Date: Gy12 ®rZJ
Notes:
1. Documentation errors are to be crossed out with a single line, so the original text is still leoible, followed by the staff members initials and date
2. Samples are analyzed immediately upon collection.
3. NC Field Laboratory Certificate Number 5445
Abbreviations:
Method Reference:
°C: degrees Celsius
Temperature: SM 2550 B-2010
pmhos/cm: micromhos per centimeter
Specific conductivity: EPA Method 120.1, Rev. 1982
mg/L: milligrams per liter
DO: SM 4500 O G-2011
mv: millivolt
pH: SM 4500-H' B-2011
NTU: nephelometric turbidity units
Turbidity: SM 2130 B-2011
S.U.: standard units
Page 1 of 1

ANCHOR
►� QEA cc
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
E ui ment Documentation and Instrument Calibration Data Sheet
Analyst Conducting Calibration: fir- S Project Name: i
Project Number. 4 ' 1 ; Date of Calibration: Apt 18_1^0d
Project Location: I( it (' d y o o l J Date of Field Measurements: 1
Facility ID or Permit # (if applicable): SC) '6!A
EQUIPMENT DOCUMENTATION
Rental sample analysis equipment or meters used to take measurements:
Equipment Type Brand Serial Number Date of Use Rental Company
IL..� 1 f4l i _ IG_Oi30_ ID I 1 __4__
Select Turbidimeter® Hach 21000 (s/n 151006045207)
HF Scientific MicroTPW Win 200601045)
Instrument Readings
Instrument Readings
(Hach 21000)
(HF Scientific MicroTPVO
Cal Std Information
10 NTU
20 NTU
100 NTU
800 Nm
1,000 NTU
10.0 NTU
0.02 NTU
Lot
2,
ti'-Oa 9 9O
iration Date:
Cal ( 1
Cal gq�
Cal ( u /•7
vl
Cal (NTU):
Cal (NTU):
Cal (NT
Time: (p g �3
•7
Tim ) ^
w
rgI4
Tim
Time:
Time:
Time:
Calibration
*Pre -Analysis
Result TLI)/:
jw3D
Time:
*Pre -Analysis
Res U):
Time:
Verification:
Check (10 NTU):
.
Check (10 NTU •
*Post -Analysis
Result NTU):
Time: i
•Post -An "s
Result (NTU):
Time:
Check (10 NTU):
`, ,
C 10 NTU):
YSI Professional Plus Muhipammater Matey Isla 185101802)
Cal Still Information
p g+, IQ,Strument Readings
6_11
�8
Date
� Date
r/
Opened
Dissolved Oxygen
Initial (%):
Cal 1%1:
mmHg: '']�f`��
-1 q"I
Temperature (°C):
Time:
(% saturation)
I a
p
DO (Site #2,
Initial (%i
Cal (%):
m g�
Tem ratur °C).
TimOe: db
H a licable *
,
}
QC** Check: DO
Time:
Result (%): �!'�
Tim �p
Resul %:
Time:
Result (%):
601Wl
i
PH 7 S.U.
Initial: �Yy
pHmV:
�
Cal (S.U.): `
pHmV:
Time,
9A
report to 0. 7 S. U.
LO. —19
,.
, i
k -lV , 5
PH 4 S.U.
Initi
pHmV'
Cal
.U.):
pHmV:
Time: � ((
!yvl424-4
�� ��
a
report to0.7S.U.
�,fm'
PH 10 S.U.
Initial:
pHmV:
Cal (S.U.):
pHmV:
a,.�
Time:
(Not
�w
�W'
report to 0.7 S.U.
, Q�
QC** PH 7 S.U.
Time:�LO
Result (S.U.):
TimYYe: s
Result U.):
Time:
Result (S.U.):
pp
AI
t�1
r ort to a s.U.
Vty
•©
r c
V
V1
Spec. Cond.
Initial: t7��
—
Cal (pmhoos/cm):
Os/) 0
Time: 2
L
f�'
1,000 mhos/cm
1 u
�.J
2�
% Recovery=
QC** Spec. Cond.
Time: �t7l1A
Result (pmhos/cm):
Time:
Result (pmhos/cm):
Time:
Result (pmhos/cm):
1
! Dla►I
1,000 pmhos/cm
10PLt
V V
a 3°I
% Recovery=
ORP 200 mV
Initial: `�
_40
Cal
fTemperature
LI;
3
.SYI ,A
`opi
,�/,,
UW
qJ
Analyst SignatumcKAnalyst Name: Date: (NJ
Notes: (�
Revision 6, 12/20/20, MAK
1. Instruments shall be calibrated in accordance with the manufacturer's operation manual.
2. Specific Conductivity should be calibrated according to values representative of historic range.
3. Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORR QC checks.
4. *When performing DO analyses at multiple sample sites (i.e. project/facility locations), the DO probe must be calibrated at each sample site prior to analysis.
5. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the instrument needs to be recalibrated.
6. ** QC check must be performed prior to sampling and following completion of sampling, at a minimum. QC checks must be performed with calibration standard from a separate lot n as the initial QC.
7. % Recovery = (Value Obtained, pmhos/cm , True Value, pmhos/cm) x 100
8. NC Field Laboratory Certificate Number 544S
9. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
10. Unless otherwise noted, all DO calibrations and measurements are performed at 0 ppt Salinity.
11. 1 pmho/cm = 1 p5/cm
Abbreviations: Method Reference:
pmhos/cm: micromhos per centimeter NTU: nephelometric turbidity units Temperature: SM 2550 B-2010
°C: degrees Celsius ORP: oxidation reduction potential Specific conductivity EPA Method 120.1, Rev. 1982
DO: dissolved oxygen s/n: serial number DO: SM 4S00 0 G-2011
mg/L: milligrams per liter S.U.: standard units pH: SM 4500-H* B-2011
.V. millivolt Spec. Cond.: Specific Conductivity Turbidity, SM 2130 B-2011
Page 1 of 1

k4ANCHOR
IDEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
liui ment Documentation and Instrument Calibration Data Sheet
Project Name: ' _li Analyst Conducting Calibration: Qi
Project Number. Date of Calibration:
Project Location: Date of Field Measurements: tL
Facility ID or Permit # (if applicable):
EQUIPMENT DOCUMENTATION
Rental sample analysis equipment or meters used to take measurements:
Equi ment Type I Brand I Serial Number I Date of Use Rental Company
Select Turbidimeter. Hach 21000 (s/n 151006045207)
HF Scientific MicroTPW (s/n 20060104S)
Instrument Readings
instrument Readings
(Hach 2100Q)
(HF Scientific MicroTPVY)
Cal Still Information
10 NTU
20 NTU
100 NTU
800 NTU
1,000 NTU
10.0 NTU
0.02 NTU
Lot #:
i
Expiration Date
I
t
Cal (NTU} p� -�
Cal (IyTW:�
Cal (N
Cal (NTU):
Cal (NTU):
Ca U):
Tim : 112WI
Time: r I
Time: ttnl-� Idt
Tme:
Time:
Time:
Calibration
*Pre -Analysis
Result (NTUJ:
I
Time:r,
*Pre -Analysis
Result ):
Time:
Ve�cation•
Check (10 NTU):
i © . k
�l4
©V
Check (10 NTU):
*Post -Analysis
Result (NTU):
Time:
'Post -Anal
Result (NTU):
Time:
Check (10 NTU):
Ch NTU):
YSI Professional Plus Multiparemeter Meter (s/n 186101802)
Cal Still Information
Instrument Readings
Lot#
Date
Ex . Data
P
0 period
Dissolved Oxygen
(% saturation)
Initial (%):
121, 1
Cal )�
� C . U
Tempera ure (° ):
r
Time: of AC
9V1
I
DO (Site #2,
Ini ' I :
Cal (%`` )'
m
Temp to (C):
Time -
i
if a applicable)
400
r
QC" Check DO
Time: �'' I
Result:` 7
��fJ L
Time: � � �� (�
Res�l© ):
s
Time:
Result (%):
PH 7 S.U.
Initial:
pHmV: r
Cal (S.U.):
pHmV:
Time:
3
I
11U
report to 0.7 S.U.
r ` j r
,Time
'
r 1
PH 4 S.U.
Initia •
pHmV:
Cal (S.U.):
pHmV:
-
1
report(
to 0.1 S.U.
a
rit.,I
PH S.U.
Initial:
pH� : 1 �
Cal (Sii��.1U1.):
pHm
Time
(P
to
report to 0.7 S.U.
t
I
V :
f•
QC` PH 7 S.U.
Time: rat 130h j
Result is U.:
b
Time:
Resu�ty(S.U.):
Time: V/`+l�
Result S.U.):
��
_
re ortto0.1 S.U.
C)f0 ACt
I t
t
T •
I Z, '7
Spar Cond.
1,000 mhos/cm
Initial:
O
Cal (pmhos/cm):
Tim`{e:532
Y�J�
[Yt��
1
U
% Recovery=
QC— SpecCond.
Time:(o`•t,.Erji
Result(pmhos/cm):
Time:ib,Zi1Z4
Resultt((pmhos/cm):
`f
Time:
Result(pmhos/cm):
•`�"�
i
^�
1,000 mhos/,.
�
( rA 1
a a
O
0�as
% Recovery=
DRIP 200 mV
Initial:
q r,fl r
CT V1�
Cal:
Tem erature (°C):
t�
p(
Time:
1 ( �rn
ferg
Analyst Signature: Analyst Name:W Date:
Notes:
Revision 6, 12/20/20, MAK
1. Instruments shall be calibrated in accordance with the manufacturer's operation manual.
2. Specific Conductivity should be calibrated according to values representative of historic range.
3. Order of Calibration is as follows: Specific Conductivity, pH 7. PH 4, pH 10, DO, ORP, QC checks.
4. When Performing DO analyses at multiple sample sites 0-e. project/facility locations), the DO probe must be calibrated at
each sample site prior to analysis.
5. QC Acceptable Ranges: PH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the
instrument needs to be recalibrated.
6. •' QC check mist be performed prior to sampling and following completion of sampling, at a minimum. QC checks must be performed with calibration standard from a separate lot # as the initial QC.
7. % Recovery = (Value Obtained, pmhos/cm + True Value, pmhos/cm) x 100
8. NC Field Laboratory Certificate Number 5445
9. Documentation errors are to be crossed out with a single line, so the original text is still legible, followed by the staff members initials and date
10. Unless otherwise noted, all DO calibrations and measurements are performed at 0 ppt Salinity.
11. 1 pmho/cm = 1 pS/cm
Abbreviations:
Method Reference:
pmhos/cm: micromhos per centimeter NTU: nephelometric turbidity units
Temperature: SM 2550 B•2010
°C: degrees Celsius ORP: oxidation reduction potential
Specific conductivity. EPA Method 120.1, Rev. 1982
DO: dissolved oxygen s/n: serial number
DO: SM 4500 0 G-2011
mg/L: milligrams per liter S.U.: standard units
PH: SM 4500-H' 5-2011
mV: millivolt Spec. Cond.: Specific Conductivity
Turbidity: SM 2130 0-2011
Page 1 of 1

Appendix B
Reports of Laboratory Analysis,
Chain -of -Custody Documentation,
and Certificates of Analysis

Waypointo
ANALYTICAL
12/21 /2021
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville, NC, 28801
Ref: Analytical Testing
Lab Report Number: 21-294-8011
Client Project Description: Jackson County
Site: 58-02
Project Number: 58-02
Dear Chuck Pippin:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/21/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
J* /I OA-2--
Kyle N. Collins
General Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 105

0
Waypoint.
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2022
North Carolina
State Program
402
12/31/2021
South Carolina
State Program
99012
07/31/2022
South Carolina
State Program
99012
12/31/2021
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2022
Arkansas
State Program
88-0650
02/07/2022
California
State Program
2904
06/30/2022
Florida
State Program
- NELAP
E871157
06/30/2022
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2022
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2021
Louisiana
State Program
- NELAP
LA037
12/31/2021
Louisiana
State Program
- NELAP
04015
06/30/2022
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2021
Pennsylvania
State Program
- NELAP
68-03195
05/31/2022
South Carolina
State Program
84002
06/30/2022
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2022
Virginia
State Program
- NELAP
460181
09/14/2022
Page 1 of 1 00016/21-294-8011
Page 2 of 105

Waypoint. (2)
ANALYTICAL
Sample
Report Number: 21-294-8011
Client Project Description: Jackson County
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca I som
Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
97850
MW-07-20211019
Aqueous
10/19/2021
13:08
10/21/2021
11:35
97850
MW-07-20211019
Aqueous
10/19/2021
13:08
10/21/2021
11:35
8270D
WP MTN
97850
MW-07-20211019
Aqueous
10/19/2021
13:08
10/21/2021
11:35
531OC-2011
WP MTN
97850
MW-07-20211019
Aqueous
10/19/2021
13:08
10/21/2021
11:35
8270D
WP MTN
97850
MW-07-20211019
Aqueous
10/19/2021
13:08
10/21/2021
11:35
8270C
WP MTN
97851
SW-01-20211019
Aqueous
10/19/2021
14:55
10/21/2021
11:35
97852
SW-02-20211019
Aqueous
10/19/2021
15:30
10/21/2021
11:35
97853
TB-20211019B
Aqueous
10/19/2021
10/21/2021
11:35
97854
MW-04-20211019
Aqueous
10/19/2021
10:58
10/21/2021
11:35
97854
MW-04-20211019
Aqueous
10/19/2021
10:58
10/21/2021
11:35
531OC-2011
WP MTN
97855
MW-05R-20211019
Aqueous
10/19/2021
16:05
10/21/2021
11:35
97855
MW-05R-20211019
Aqueous
10/19/2021
16:05
10/21/2021
11:35
531OC-2011
WP MTN
97856
TB-20211019A
Aqueous
10/19/2021
10/21/2021
11:35
97858
MW-04-20211019
Aqueous
10/19/2021
10:58
10/21/2021
11:35
8270D
WP MTN
97858
MW-04-20211019
Aqueous
10/19/2021
10:58
10/21/2021
11:35
8270D
WP MTN
97858
MW-04-20211019
Aqueous
10/19/2021
10:58
10/21/2021
11:35
8270C
WP MTN
97859
MW-05R-20211019
Aqueous
10/19/2021
16:05
10/21/2021
11:35
8270C
WP MTN
97859
MW-05R-20211019
Aqueous
10/19/2021
16:05
10/21/2021
11:35
8270D
WP MTN
97859
MW-05R-20211019
Aqueous
10/19/2021
16:05
10/21/2021
11:35
8270D
WP MTN
97860
TB-20211019C
Aqueous
10/19/2021
10/21/2021
11:35
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 105

Waypoint.(2)
ANALYTICAL
Project: Jackson County
Report Number: 21-294-8011
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Summary of Detected
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
MW-07-20211019
V 97850
2320B-2011
Alkalinity (as CaCO3)
5220D-2011
COD (Chemical Oxygen Demand)
5310C-2011
TOC
6020B
Arsenic
6020B
Barium
6020B
Cobalt
6020B
Nickel
8260D
Benzene
8260D
Chlorobenzene
8260D
1,4-Dichlorobenzene
8260D
cis-1,2-Dichloroethene
8260D SIM
1,4-Dioxane
8270D
1,4-Dichlorobenzene
9056A
Chloride
9056A
Sulfate
SM-3500-Fe-B
Ferrous Iron
SW-01-20211019
V 97851
2340C-2011
Hardness
6020B
Barium
6020B
Selenium
8260D
Acetone
SW-02-20211019
V 97852
2340C-2011
Hardness
6020B
Arsenic
6020B
Barium
6020B
Vanadium
8260D
Acetone
8260D
Allyl Chloride
TB-20211019B
V 97853
8260D
Acetone
MW-04-20211019
V 97854
2320B-2011
Alkalinity (as CaCO3)
5210B-2016
Biochemical Oxygen Demand (5-day)
5220D-2011
COD (Chemical Oxygen Demand)
258000
pq/L
800
10/27/202110:20
29000
Ng/L
11000
10/25/2021 11:16 1
3130
uq/L
500
10/27/2021 00:05
0.172
Ng/L
0.170
11/03/202104:42 1
420
uq/L
0.810
11/03/202104:42
1.60
Ng/L
0.520
11/03/202104:42 1
6.77
uq/L
0.510
11/03/202104:42
1.82
pg/L
0.180
11 /01 /2021 06:37
6.25
uq/L
0.190
11/01/202106:37
7.05
pg/L
0.210
11 /01 /2021 06:37
2.73
pq/L
0.200
11/01/202106:37
13.7
Ng/L
0.139
10/25/202114:28
2.48
pq/L
0.610
10/25/202117:59 1
81600
pg/L
370
10/21/202114:57
23000
uq/L
540
10/21/2021 14:57
370
Ng/L
50.0
10/21/202116:01
8000
pq/L
1140
10/28/202110:10 1
13.3
Ng/L
0.810
11/03/202104:49
0.958
uq/L
0.740
11/03/202119:56 1
2.96
Ng/L
1.80
11 /01 /2021 07:02 1
8000
pq/L
1140
10/28/202110:10 1
0.181
Ng/L
0.170
11/03/202105:09 1
11.9
uq/L
0.810
11/03/202105:09
1.38
pg/L
1.30
11/03/202120:16 1
2.96
pq/L
1.80
11/01/202107:26 1
0.617
Ng/L
0.579
11 /01 /2021 07:26 1
2.57
pq/L
1.80
111011202103:20 1
103000
Ng/L
800
10/27/2021 10:20
2000
pq/L
2000
10/21/202115:53 H
34000
Ng/L
11000
10/25/2021 11:16 1
Page 4 of 105

Waypoint.(2)
ANALYTICAL
Project: Jackson County
Report Number: 21-294-8011
Client Sample ID Lab Sample ID
Method Parameters
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lytica Isom
Summary of Detected
Result Units Report Limit Analyzed
MW-04-20211019
V 97854
5310C-2011
TOC
2390
pq/L
500
10/28/202117:12
6020B
Barium
72.1
Ng/L
0.810
10/29/202103:18
6020B
Cadmium
0.330
uq/L
0.160
10/29/202103:18
6020B
Cobalt
2.97
Ng/L
0.520
10/29/202103:18
6020B
Nickel
3.51
uq/L
0.510
10/29/202103:18
6020B
Selenium
0.921
Ng/L
0.740
10/29/202103:18
8260D
Benzene
0.568
uq/L
0.180
11/01/202107:51
8260D
Chlorobenzene
2.60
pg/L
0.190
11/01/202107:51
8260D
1,4-Dichlorobenzene
3.02
uq/L
0.210
11/01/202107:51
8260D
cis- 1,2-Dichloroethene
1.17
pg/L
0.200
11/01/202107:51
8260D SIM
1,4-Dioxane
5.56
pq/L
0.139
10/25/2021
15:44
9056A
Chloride
61700
Ng/L
370
10/21/202114:41
9056A
Nitrate (NO3-N)
1760
pq/L
76.0
10/21/2021
14:41
9056A
Sulfate
124000
Ng/L
540
10/21/202114:41
MW-05R-20211019
V 97855
2320B-2011
Alkalinity (as CaCO3)
203000
pq/L
800
10/27/2021
10:20
5210B-2016
Biochemical Oxygen Demand (5-day)
15500
Ng/L
2000
10/21/2021
15:53
5220D-2011
COD (Chemical Oxygen Demand)
101000
uq/L
11000
10/25/2021
11:16
5310C-2011
TOC
5360
Ng/L
500
10/28/2021
18:29
6020B
Arsenic
0.418
uq/L
0.170
10/29/202103:25
6020B
Barium
116
Ng/L
0.810
10/29/202103:25
6020B
Dissolved Barium
59.9
uq/L
0.810
11/05/2021
13:52
6020B
Chromium
3.83
Ng/L
0.790
10/29/202103:25
6020B
Cobalt
12.5
uq/L
0.520
10/29/202103:25
6020B
Dissolved Cobalt
9.14
Ng/L
0.520
11/05/2021
13:52
6020B
Lead
0.612
uq/L
0.260
10/29/202103:25
6020B
Dissolved Nickel
1.81
Ng/L
0.510
11/05/2021
13:52
6020B
Nickel
3.26
uq/L
0.510
10/29/202103:25
6020B
Vanadium
1.97
Ng/L
1.30
11/08/202116:57
6020B
Zinc
10.1
uq/L
6.90
10/29/202103:25
8260D
Acetone
5.07
Ng/L
1.80
11/01/202108:15
8260D
Benzene
2.38
uq/L
0.180
11/01/202108:15
8260D
Chlorobenzene
8.02
Ng/L
0.190
11/01/202108:15
8260D
1,4-Dichlorobenzene
6.13
uq/L
0.210
11/01/202108:15
8260D
cis- 1,2-Dichloroethene
2.10
Ng/L
0.200
11/01/202108:15
8260D
Tetrahydrofuran
3.60
pg/L
1.50
11/01/202108:15
Qualifiers
Ill
J
0
I
JB
J
0
Page 5 of 105

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Summary of Detected Analytes
Project: Jackson County
Report Number: 21-294-8011
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
MW-05R-20211019
V 97855
8260D
Vinyl Chloride
8260D SIM
1,4-Dioxane
9056A
Chloride
SM-3500-Fe-B
Ferrous Iron
MW-04-20211019
V 97858
8270D
1,4-Dichlorobenzene
MW-05R-20211019
V 97859
8270D
Dibenzofuran
8270D
1,4-Dichlorobenzene
8270D
Diethyl phthalate
8270D
Fluorene
TB-20211019C
V 97860
8260D
Acetone
1.52
pq/L
0.170
11/01/202108:15
4.34
Ng/L
0.139
10/25/202116:09
66500
pq/L
370
10/21/2021 14:26
7640
pg/L
250
10/21/202116:01
1.27
pg/L
0.610
10/25/202118:21 1
0.533
Ng/L
0.423
10/25/202118:42 1
2.64
pq/L
0.580
10/25/202118:42 1
3.48
Ng/L
0.585
10/25/202118:42 1
0.523
pq/L
0.444
10/25/202118:42 1
PANIA
pg/L 1.80 11 /01 /2021 04:09 1
Page 6 of 105

Waypointo
ANALYTICAL
Client: Anchor QEA of North Carolina, PLLC
Project: Jackson County
Lab Report Number: 21-294-8011
Date: 12/21 /2021
Ferrous Iron Method SM-3500-Fe-B
QC Batch No: V10584
MS/MSD failure.
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
CASE NARRATIVE
Biochemical Oxygen Demand (BOD) Method 521OB-2016
QC Batch No: V10821
The BOD glucose-glutamic acid (GGA) check standard did not meet the criteria established by the reference
method. The acceptance range provided in the reference method is 167.5 - 228.5 mg/L. The GGA result
obtained for this analytical batch was mg/L.
The BOD glucose-glutamic acid (GGA) check standard did not meet the criteria established by the reference
method. The acceptance range provided in the reference method is 167.5 - 228.5 mg/L. The GGA result
obtained for this analytical batch was 121.5 mg/L.
Sample 97855 (MW-05R-20211019)
QC Batch No: V10821
Dup did not meet RPD requirements.
Metals Analyses Method 6020B
Analyte: Beryllium
QC Batch No: V11308/V10665/V11161
LLICV failed high. Sample concentration BRL or 10X concentration.
Analyte: Antimony
QC Batch No: V10786/V10665/V11161
LLICV, ICV and CCB failed high. Sample concentration BRL.
Analyte: Selenium
QC Batch No: V11077/V10665/V11161
LLICV failed high. Sample concentration BRL.
Analyte: Selenium
QC Batch No: V11081/V10665/V11161
LLICV and LRB failed high. Results may be high bias.
Analyte: Selenium
QC Batch No: V11233/V10665/V11161
LLICV failed high. Sample concentration BRL.
Analyte: Vanadium
QC Batch No: V10908/V10665/V11161
LLICV failed high. Concentration BRL.
Analyte: Vanadium
QC Batch No: V11077/V10665/V11161
Page 7 of 105

Waypointo
ANALYTICAL
ICB, LLICV and CCB failed high. Results may be high bias.
Sample 97850 (MW-07-20211019)
Analyte: Vanadium
QC Batch No: V11123/V10665
LLICV failed high. Sample concentration BRL.
Sample 97851 (SW-01-20211019)
Analyte: Vanadium
QC Batch No: V 11 123/V1 0665
LLICV failed high. Sample concentration BRL.
Analyte: Vanadium
QC Batch No: V11233/V10665/V11161
LLICV failed high. Sample concentration BRL.
Sample 97893
Analyte: Antimony
QC Batch No: V10908/V10701
ICV, LLICV and CCB failed high
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Sample concentration BRL.
Sample 97852 (SW-02-20211019)
Analyte: Vanadium
QC Batch No: V11123/V10735
LLICV failed high. Result may be high bias.
Sample 98018
Analyte: Barium
QC Batch No: V1 1240/V1 1166
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Total Aqueous Mercury Analysis - CVAA Method 7470A
Sample 97855 (MW-05R-20211019)
Analyte: Mercury
QC Batch No: V11256/V11199/V11161
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected.
Revised Report — This a revised report combining three reports to represent all the samples that were taken on
10/19/21.
Page 8 of 105

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-294-8011
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/21/2021
Lab No : 97850
Matrix: Aqueous
Sample ID: MW-07-20211019
Sampled:
10/19/2021
13:08
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ferrous Iron
370
Ng/L
50.0
200
1
10/21/21 16:01
SMW
SM-3500-Fe-B
1,4-Dioxane
13.7
ug/L
0.139
2.00
1
10/25/21 14:28
TBL
8260D SIM
1,4-Naphthoquinone
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
1-Naphthylamine
<10.5
ug/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
2-Acetylaminofluorene
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
2-Naphthylamine
<10.5
ug/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
3-Methylcholanthrene
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
4-Aminobiphenyl
<10.5
ug/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
5-Nitro-o-toluidine
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
7,12-Dimethyl benz(a)anth racene <10.5
ug/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
Diallate
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
Hexachloropropene
<10.5 M
ug/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
Isosafrole
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
Methapyrilene
<10.5
ug/L
10.5
10.5
1
10/25/21 17:59
BGV
8270D
N-Nitrosomethylethylamine
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
N-Nitrosomorpholine
<10.5
ug/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
N-Nitrosopyrrolidine
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
N-Nitrosopiperidine
<10.5
ug/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
0,0,0-Triethyl Phosphorothioate <0.346
Ng/L
0.346
1.05
1
10/26/21 02:43
VBW
8270C
o-Toluidine
<10.5
ug/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
p-Dimethylaminoazobenzene
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
p-Phenylenediamine
<10.5 M
ug/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
Pronamide
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
8270D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 9 of 105

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-294-8011
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/21/2021
Lab No : 97850
Matrix: Aqueous
Sample ID: MW-07-20211019
Sampled:
10/19/2021
13:08
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Safrole
<10.5
Ng/L
10.5
10.5
1
10/25/2117:59
VBW
8270D
Thionazine
<0.346
ug/L
0.346
1.05
1
10/26/2102:43
VBW
8270C
Alkalinity (as CaCO3)
258000
Ng/L
800
5000
1
10/27/21 10:20
CLB
2320B-2011
Biochemical Oxygen Demand (5-day) <2000 H
ug/L
2000
2000
1
10/21/21 15:53
SLO
521OB-2016
Chloride
81600
Ng/L
370
1000
1
10/21/21 14:57
CEG
9056A
Cyanide, Total
<3.80
ug/L
3.80
10.0
1
10/27/21 09:30
ENM
450OCNE-2016
COD (Chemical Oxygen Demand) 290003
Ng/L
11000
50000
1
10/25/21 11:16
ENM
5220D-2011
Nitrate (NO3-N)
<76.0
ug/L
76.0
200
1
10/21/21 14:57
CEG
9056A
TOC
3130
Ng/L
500
1000
1
10/27/21 00:05
TJS
531OC-2011
Sulfate
23000
ug/L
540
1000
1
10/21/21 14:57
CEG
9056A
Sulfide
<830
Ng/L
2000
1
10/26/2109:45
ENM
4500S2F-2011
Antimony
<0.490
ug/L
0.490
2.00
1
11/03/2104:42
EDV
6020B
Arsenic
0.1723
Ng/L
0.170
1.00
1
11/03/2104:42
EDV
6020B
Barium
420
ug/L
0.810
10.0
1
11/03/2104:42
EDV
6020B
Beryllium
<0.190
Ng/L
0.190
1.00
1
11/03/2119:49
EDV
6020B
Cadmium
<0.160
ug/L
0.160
1.00
1
11/03/2104:42
EDV
6020B
Chromium
<0.790
Ng/L
0.790
2.00
1
11/03/2104:42
EDV
6020B
Cobalt
1.60 J
ug/L
0.520
2.00
1
11/03/21 04:42
EDV
6020B
Copper
<3.80
Ng/L
3.80
10.0
1
11/03/21 04:42
EDV
6020B
Lead
<0.260
ug/L
0.260
1.00
1
11/03/21 04:42
EDV
6020B
Mercury (Total)
<0.0700
Ng/L
0.0700
0.200
1
10/27/21 18:50
EDV
7470A
Nickel
6.77
ug/L
0.510
3.00
1
11/03/2104:42
EDV
6020B
Selenium
<0.740
Ng/L
0.740
5.00
1
11/03/2104:42
EDV
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 10 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97850
Sample ID: MW-07-20211019
Matrix: Aqueous
Sampled: 10/19/2021 13:08
Test
Results
Units
MDL
MQL
DF
Date / Time By Analytical
Analyzed Method
Silver
<0.110
Ng/L
0.110
1.00
1
11/03/2104:42 EDV 6020E
Tin
<1.80
ug/L
1.80
5.00
1
11/03/2104:42 EDV 6020B
Thallium
<0.570
Ng/L
0.570
2.00
1
11/03/2104:42 EDV 6020B
Vanadium
<1.30
ug/L
1.30
5.00
1
11/03/2119:49 EDV 6020B
Zinc
<6.90
Ng/L
6.90
20.0
1
11/03/2104:42 EDV 6020B
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 11 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97850
Matrix: Aqueous
Sample ID: MW-07-20211019
Sampled:
10/19/2021
13:08
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
Ng/L
1.80
5.00
1
11/01/21 06:37
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 06:37
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 06:37
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 06:37
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 06:37
JLB
V11000
Benzene
1.82
ug/L
0.180
0.500
1
11/01/21 06:37
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 06:37
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 06:37
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 06:37
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 06:37
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 06:37
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 06:37
JLB
V11000
Chlorobenzene
6.25
Ng/L
0.190
0.500
1
11/01/21 06:37
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 06:37
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 06:37
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 06:37
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 06:37
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 06:37
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 06:37
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 06:37
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 06:37
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 06:37
JLB
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 12 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
REPORT OF ANAL YSIS
Lab No : 97850 Matrix: Aqueous
Sample ID: MW-07-20211019 Sampled: 10/19/2021 13:08
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 06:37
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 06:37
JLB
V11000
1,4-Dichlorobenzene
7.05
Ng/L
0.210
0.500
1
11/01/21 06:37
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 06:37
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 06:37
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 06:37
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 06:37
JLB
V11000
cis- 1,2-Dich loroethene
2.73
ug/L
0.200
0.500
1
11/01/21 06:37
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 06:37
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 06:37
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 06:37
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 06:37
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 06:37
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 06:37
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 06:37
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 06:37
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 06:37
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 06:37
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 06:37
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 06:37
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 06:37
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 06:37
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 13 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97850
Matrix: Aqueous
Sample ID: MW-07-20211019
Sampled:
10/19/2021
13:08
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 06:37
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 06:37
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 06:37
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 06:37
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 06:37
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 06:37
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 06:37
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 06:37
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 06:37
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 06:37
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 06:37
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 06:37
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 06:37
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 06:37
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 06:37
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 06:37
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 06:37
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 06:37
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 06:37
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 06:37
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 06:37
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 14 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97850
Matrix: Aqueous
Sample ID: MW-07-20211019
Sampled:
10/19/2021
13:08
Analytical Method:
8270C
Prep Batch(es):
L580965
10/25/21 10:30
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Dimethoate
<0.748
Ng/L
0.748
1.05
1
10/26/21 02:43
VBW
L581161
Disulfoton
<0.489
ug/L
0.489
1.05
1
10/26/21 02:43
VBW
L581161
Ethyl Parathion
<0.596
Ng/L
0.596
1.05
1
10/26/21 02:43
VBW
L581161
Famphur
<0.537
u9/L
0.537
1.05
1
10/26/21 02:43
VBW
L581161
Methyl Parathion
<0.845
Ng/L
0.845
1.05
1
10/26/21 02:43
VBW
L581161
Phorate
<0.691
ug/L
0.691
1.05
1
10/26/21 02:43
VBW
L581161
Analytical Method:
8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dinitrobenzene
<0.949
ug/L
0.949
10.5
1
10/25/21 17:59
VBW
L581160
1,3,5-Trinitrobenzene
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
L581162
Acenaphthene
<0.445
ug/L
0.445
2.11
1
10/25/21 17:59
VBW
L581160
Acenaphthylene
<0.452
Ng/L
0.452
2.11
1
10/25/21 17:59
VBW
L581160
Acetophenone
<0.721
ug/L
0.721
5.26
1
10/25/21 17:59
VBW
L581160
Anthracene
<0.492
Ng/L
0.492
2.11
1
10/25/21 17:59
VBW
L581160
Benzo(a)anthracene
<0.450
ug/L
0.450
2.11
1
10/25/21 17:59
VBW
L581160
Benzo(a)pyrene
<1.06
Ng/L
1.06
2.11
1
10/25/21 17:59
VBW
L581160
Benzo(b)fluoranthene
<0.992
ug/L
0.992
2.11
1
10/25/21 17:59
VBW
L581160
Benzo(g,h,i)perylene
<1.43
Ng/L
1.43
2.11
1
10/25/21 17:59
VBW
L581160
Benzo(k)fluoranthene
<0.793
ug/L
0.793
2.11
1
10/25/21 17:59
VBW
L581160
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 15 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97850
Matrix: Aqueous
Sample ID: MW-07-20211019
Sampled:
10/19/2021
13:08
Analytical Method: 8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzyl alcohol
<3.16
Ng/L
3.16
10.5
1
10/25/21 17:59
VBW
L581160
Bis(2-Chloroethoxy)methane
<0.455
ug/L
0.455
5.26
1
10/25/21 17:59
VBW
L581160
Bis(2-Chloroethyl)ether
<0.470
Ng/L
0.470
5.26
1
10/25/21 17:59
VBW
L581160
Bis(2-Chloroisopropyl)ether
<0.574
ug/L
0.574
5.26
1
10/25/21 17:59
VBW
L581160
Bis(2-ethylhexyl)phthalate
<3.85
Ng/L
3.85
5.26
1
10/25/21 17:59
VBW
L581160
4-Bromophenyl phenyl ether
<0.526
ug/L
0.526
5.26
1
10/25/21 17:59
VBW
L581160
Butyl benzyl phthalate
<4.83
Ng/L
4.83
5.26
1
10/25/21 17:59
VBW
L581160
4-Chloro-3-methylphenol
<0.529
ug/L
0.529
5.26
1
10/25/21 17:59
VBW
L581160
4-Chloroaniline
<0.553
Ng/L
0.553
5.26
1
10/25/21 17:59
VBW
L581160
Chlorobenzilate
<2.00
ug/L
2.00
5.26
1
10/25/21 17:59
VBW
L581160
2-Chloronaphthalene
<0.500
Ng/L
0.500
5.26
1
10/25/21 17:59
VBW
L581160
2-Chlorophenol
<0.774
ug/L
0.774
5.26
1
10/25/21 17:59
VBW
L581160
4-Chlorophenyl phenyl ether
<0.503
Ng/L
0.503
5.26
1
10/25/21 17:59
VBW
L581160
Chrysene
<0.771
ug/L
0.771
2.11
1
10/25/21 17:59
VBW
L581160
Dibenz(a,h)anthracene
<0.265
Ng/L
0.265
2.11
1
10/25/21 17:59
VBW
L581160
Dibenzofuran
<0.444
ug/L
0.444
5.26
1
10/25/21 17:59
VBW
L581160
1,2-Dichlorobenzene
<0.661
Ng/L
0.661
5.26
1
10/25/21 17:59
VBW
L581160
1,3-Dichlorobenzene
<0.516
ug/L
0.516
5.26
1
10/25/21 17:59
VBW
L581160
1,4-Dichlorobenzene
2.48 3
Ng/L
0.610
5.26
1
10/25/21 17:59
VBW
L581160
3,3'-Dichlorobenzidine
<3.93
ug/L
3.93
10.5
1
10/25/21 17:59
VBW
L581160
2,4-Dichlorophenol
<1.60
Ng/L
1.60
5.26
1
10/25/21 17:59
VBW
L581160
2,6-Dichlorophenol
<0.739
ug/L
0.739
5.26
1
10/25/21 17:59
VBW
L581160
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 16 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97850
Matrix: Aqueous
Sample ID: MW-07-20211019
Sampled:
10/19/2021
13:08
Analytical Method: 8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.615
Ng/L
0.615
5.26
1
10/25/21 17:59
VBW
L581160
Dimethyl phthalate
<0.536
ug/L
0.536
5.26
1
10/25/21 17:59
VBW
L581160
3,3' Dimethylbenzidine
<1.97
Ng/L
1.97
10.5
1
10/25/21 17:59
VBW
L581160
2,4-Dimethylphenol
<0.709
ug/L
0.709
5.26
1
10/25/21 17:59
VBW
L581160
Di-n-butyl phthalate
<1.66
Ng/L
1.66
5.26
1
10/25/21 17:59
VBW
L581160
4,6- Din itro-2- methyl phenol
<3.64
ug/L
3.64
10.5
1
10/25/21 17:59
VBW
L581160
2,4-Dinitrophenol
<5.09
Ng/L
5.09
10.5
1
10/25/21 17:59
VBW
L581160
2,4-Dinitrotoluene
<0.423
ug/L
0.423
5.26
1
10/25/21 17:59
VBW
L581160
2,6-Dinitrotoluene
<0.434
Ng/L
0.434
5.26
1
10/25/21 17:59
VBW
L581160
Di-n-Octyl Phthalate
<1.81
u9/L
1.81
5.26
1
10/25/21 17:59
VBW
L581160
Ethyl methanesulfonate
<0.751
Ng/L
0.751
5.26
1
10/25/21 17:59
VBW
L581160
Fluoranthene
<0.428
ug/L
0.428
2.11
1
10/25/21 17:59
VBW
L581160
Fluorene
<0.468
Ng/L
0.468
2.11
1
10/25/21 17:59
VBW
L581160
Hexachlorobenzene
<2.70
ug/L
2.70
5.26
1
10/25/21 17:59
VBW
L581160
Hexachlorobutadiene
<0.426
Ng/L
0.426
5.26
1
10/25/21 17:59
VBW
L581160
Hexachlorocyclopentadiene
<2.46
ug/L
2.46
5.26
1
10/25/21 17:59
VBW
L581160
Hexachloroethane
<0.291
Ng/L
0.291
5.26
1
10/25/21 17:59
VBW
L581160
Indeno(1,2,3-cd)pyrene
<1.07
ug/L
1.07
2.11
1
10/25/21 17:59
VBW
L581160
Isodrin
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
L581162
Isophorone
<0.378
ug/L
0.378
5.26
1
10/25/21 17:59
VBW
L581160
Kepone
<10.5
Ng/L
10.5
10.5
1
10/25/21 17:59
VBW
L581162
Methyl methanesulfonate
<0.650
ug/L
0.650
5.26
1
10/25/21 17:59
VBW
L581160
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 17 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97850
Matrix: Aqueous
Sample ID: MW-07-20211019
Sampled:
10/19/2021
13:08
Analytical Method: 8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Methylnaphthalene
<0.511
Ng/L
0.511
2.11
1
10/25/21 17:59
VBW
L581160
2-Methylphenol
<0.758
ug/L
0.758
5.26
1
10/25/21 17:59
VBW
L581160
3&4 Methylphenol
<0.726
Ng/L
0.726
5.26
1
10/25/21 17:59
VBW
L581160
Naphthalene
<0.510
ug/L
0.510
2.11
1
10/25/21 17:59
VBW
L581160
2-Nitroaniline
<0.603
Ng/L
0.603
5.26
1
10/25/21 17:59
VBW
L581160
3-Nitroaniline
<1.61
ug/L
1.61
10.5
1
10/25/21 17:59
VBW
L581160
4-Nitroaniline
<0.778
Ng/L
0.778
5.26
1
10/25/21 17:59
VBW
L581160
Nitrobenzene
<0.558
ug/L
0.558
5.26
1
10/25/21 17:59
VBW
L581160
2-Nitrophenol
<0.637
Ng/L
0.637
5.26
1
10/25/21 17:59
VBW
L581160
4-Nitrophenol
<1.46
ug/L
1.46
10.5
1
10/25/21 17:59
VBW
L581160
N-Nitrosodimethylamine
<0.261
Ng/L
0.261
5.26
1
10/25/21 17:59
VBW
L581160
N-Nitrosodiphenylamine
<0.822
ug/L
0.822
10.5
1
10/25/21 17:59
VBW
L581160
N-Nitrosodiethylamine
<0.420
Ng/L
0.420
5.26
1
10/25/21 17:59
VBW
L581160
N-Nitroso-di-n-butylamine
<0.791
ug/L
0.791
5.26
1
10/25/21 17:59
VBW
L581160
N-Nitroso-di-n-propylamine
<0.351
Ng/L
0.351
5.26
1
10/25/21 17:59
VBW
L581160
Pentachlorobenzene
<0.481
u9/L
0.481
10.5
1
10/25/21 17:59
VBW
L581160
Pentachloronitrobenzene
<1.21
Ng/L
1.21
5.26
1
10/25/21 17:59
VBW
L581160
Pentachlorophenol
<2.57
ug/L
2.57
10.5
1
10/25/21 17:59
VBW
L581160
Phenacetin
<1.35
Ng/L
1.35
5.26
1
10/25/21 17:59
VBW
L581160
Phenanthrene
<0.489
ug/L
0.489
2.11
1
10/25/21 17:59
VBW
L581160
Phenol
<0.409
Ng/L
0.409
5.26
1
10/25/21 17:59
VBW
L581160
Pyrene
<1.10
ug/L
1.10
2.11
1
10/25/21 17:59
VBW
L581160
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 18 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
Lab No : 97850
Sample ID: MW-07-20211019
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 10/19/2021 13:08
Analytical Method: 8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2,4,5-Tetrachlorobenzene
<0.333
Ng/L
0.333
5.26
1
10/25/2117:59
VBW
L581160
2,3,4,6-Tetrachlorophenol
<0.373
ug/L
0.373
5.26
1
10/25/2117:59
VBW
L581160
1,2,4-Trichlorobenzene
<0.507
Ng/L
0.507
5.26
1
10/25/2117:59
VBW
L581160
2,4,5-Trichlorophenol
<0.368
ug/L
0.368
5.26
1
10/25/2117:59
VBW
L581160
2,4,6-Trichlorophenol
<0.361
Ng/L
0.361
5.26
1
10/25/2117:59
VBW
L581160
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
M Minimum value MQL Method Quantitation Limit
Page 19 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97851
Sample ID: SW-01-20211019
Matrix: Aqueous
Sampled: 10/19/2021 14:55
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Hardness
80003
Ng/L
1140
10000
1
10/28/21 10:10
CLB
2340C-2011
1,4-Dioxane
<0.139
ug/L
0.139
2.00
1
10/25/21 14:53
TBL
8260D SIM
Antimony
<0.490
Ng/L
0.490
2.00
1
11/03/2104:49
EDV
6020B
Arsenic
<0.170
ug/L
0.170
1.00
1
11/03/2104:49
EDV
6020B
Barium
13.3
Ng/L
0.810
10.0
1
11/03/2104:49
EDV
6020B
Beryllium
<0.190
ug/L
0.190
1.00
1
11/03/2119:56
EDV
6020B
Cadmium
<0.160
Ng/L
0.160
1.00
1
11/03/2104:49
EDV
6020B
Chromium
<0.790
ug/L
0.790
2.00
1
11/03/2104:49
EDV
6020B
Cobalt
<0.520
Ng/L
0.520
2.00
1
11/03/2104:49
EDV
6020B
Copper
<3.80
ug/L
3.80
10.0
1
11/03/21 04:49
EDV
6020B
Lead
<0.260
Ng/L
0.260
1.00
1
11/03/21 04:49
EDV
6020E
Mercury (Total)
<0.0700
ug/L
0.0700
0.200
1
10/27/21 18:53
EDV
7470A
Nickel
<0.510
Ng/L
0.510
3.00
1
11/03/2104:49
EDV
6020E
Selenium
0.9583
ug/L
0.740
5.00
1
11/03/21 19:56
EDV
6020B
Silver
<0.110
Ng/L
0.110
1.00
1
11/03/2104:49
EDV
6020E
Tin
<1.80
ug/L
1.80
5.00
1
11/03/2104:49
EDV
6020B
Thallium
<0.570
Ng/L
0.570
2.00
1
11/03/2104:49
EDV
6020B
Vanadium
<1.30
ug/L
1.30
5.00
1
11/03/2119:56
EDV
6020B
Zinc
<6.90
Ng/L
6.90
20.0
1
11/03/2104:49
EDV
6020B
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 20 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97851
Matrix: Aqueous
Sample ID: SW-01-20211019
Sampled:
10/19/2021
14:55
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
2.963
Ng/L
1.80
5.00
1
11/01/21 07:02
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 07:02
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 07:02
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 07:02
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 07:02
JLB
V11000
Benzene
<0.180
ug/L
0.180
0.500
1
11/01/21 07:02
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 07:02
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 07:02
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 07:02
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 07:02
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 07:02
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 07:02
JLB
V11000
Chlorobenzene
<0.190
Ng/L
0.190
0.500
1
11/01/21 07:02
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 07:02
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 07:02
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 07:02
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 07:02
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 07:02
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 07:02
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 07:02
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 07:02
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 07:02
JLB
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 21 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
REPORT OF ANAL YSIS
Lab No : 97851 Matrix: Aqueous
Sample ID: SW-01-20211019 Sampled: 10/19/2021 14:55
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 07:02
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 07:02
JLB
V11000
1,4-Dichlorobenzene
<0.210
Ng/L
0.210
0.500
1
11/01/21 07:02
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 07:02
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 07:02
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 07:02
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 07:02
JLB
V11000
cis- 1,2-Dich loroethene
<0.200
ug/L
0.200
0.500
1
11/01/21 07:02
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 07:02
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 07:02
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 07:02
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 07:02
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 07:02
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 07:02
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 07:02
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 07:02
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 07:02
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 07:02
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 07:02
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 07:02
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 07:02
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 07:02
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 22 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97851
Matrix: Aqueous
Sample ID: SW-01-20211019
Sampled:
10/19/2021
14:55
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 07:02
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 07:02
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 07:02
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 07:02
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 07:02
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 07:02
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 07:02
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 07:02
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 07:02
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 07:02
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 07:02
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 07:02
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 07:02
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 07:02
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 07:02
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 07:02
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 07:02
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 07:02
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 07:02
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 07:02
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 07:02
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 23 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97852
Sample ID: SW-02-20211019
Matrix: Aqueous
Sampled: 10/19/2021 15:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Hardness
80003
Ng/L
1140
10000
1
10/28/21 10:10
CLB
2340C-2011
1,4-Dioxane
<0.139
ug/L
0.139
2.00
1
10/25/21 15:19
TBL
8260D SIM
Antimony
<0.490
Ng/L
0.490
2.00
1
11/03/2105:09
EDV
6020B
Arsenic
0.181 J
ug/L
0.170
1.00
1
11/03/21 05:09
EDV
6020B
Barium
11.9
Ng/L
0.810
10.0
1
11/03/2105:09
EDV
6020B
Beryllium
<0.190
ug/L
0.190
1.00
1
11/03/2120:16
EDV
6020B
Cadmium
<0.160
Ng/L
0.160
1.00
1
11/08/2116:43
EDV
6020B
Chromium
<0.790
ug/L
0.790
2.00
1
11/03/2105:09
EDV
6020B
Cobalt
<0.520
Ng/L
0.520
2.00
1
11/03/2105:09
EDV
6020B
Copper
<3.80
ug/L
3.80
10.0
1
11/03/21 05:09
EDV
6020B
Lead
<0.260
Ng/L
0.260
1.00
1
11/03/21 05:09
EDV
6020E
Mercury (Total)
<0.0700
ug/L
0.0700
0.200
1
10/27/21 18:55
EDV
7470A
Nickel
<0.510
Ng/L
0.510
3.00
1
11/03/2105:09
EDV
6020E
Selenium
<0.740
ug/L
0.740
5.00
1
11/03/2105:09
EDV
6020B
Silver
<0.110
Ng/L
0.110
1.00
1
11/03/2105:09
EDV
6020E
Tin
<1.80
ug/L
1.80
5.00
1
11/03/2105:09
EDV
6020B
Thallium
<0.570
Ng/L
0.570
2.00
1
11/03/2105:09
EDV
6020B
Vanadium
1.38 J
ug/L
1.30
5.00
1
11/03/21 20:16
EDV
6020B
Zinc
<6.90
Ng/L
6.90
20.0
1
11/03/2105:09
EDV
6020B
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 24 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97852
Matrix: Aqueous
Sample ID: SW-02-20211019
Sampled:
10/19/2021
15:30
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
2.963
Ng/L
1.80
5.00
1
11/01/21 07:26
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 07:26
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 07:26
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 07:26
JLB
V11000
Allyl Chloride
0.6173
Ng/L
0.579
10.0
1
11/01/21 07:26
JLB
V11000
Benzene
<0.180
ug/L
0.180
0.500
1
11/01/21 07:26
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 07:26
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 07:26
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 07:26
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 07:26
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 07:26
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 07:26
JLB
V11000
Chlorobenzene
<0.190
Ng/L
0.190
0.500
1
11/01/21 07:26
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 07:26
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 07:26
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 07:26
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 07:26
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 07:26
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 07:26
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 07:26
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 07:26
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 07:26
JLB
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 25 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
REPORT OF ANAL YSIS
Lab No : 97852 Matrix: Aqueous
Sample ID: SW-02-20211019 Sampled: 10/19/2021 15:30
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 07:26
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 07:26
JLB
V11000
1,4-Dichlorobenzene
<0.210
Ng/L
0.210
0.500
1
11/01/21 07:26
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 07:26
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 07:26
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 07:26
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 07:26
JLB
V11000
cis- 1,2-Dich loroethene
<0.200
ug/L
0.200
0.500
1
11/01/21 07:26
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 07:26
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 07:26
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 07:26
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 07:26
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 07:26
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 07:26
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 07:26
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 07:26
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 07:26
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 07:26
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 07:26
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 07:26
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 07:26
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 07:26
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 26 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97852
Matrix: Aqueous
Sample ID: SW-02-20211019
Sampled:
10/19/2021
15:30
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 07:26
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 07:26
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 07:26
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 07:26
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 07:26
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 07:26
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 07:26
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 07:26
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 07:26
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 07:26
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 07:26
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 07:26
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 07:26
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 07:26
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 07:26
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 07:26
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 07:26
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 07:26
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 07:26
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 07:26
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 07:26
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 27 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97853
Matrix: Aqueous
Sample ID : TB-20211019B
Sampled:
10/19/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
2.573
Ng/L
1.80
5.00
1
11/01/21 03:20
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 03:20
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 03:20
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 03:20
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 03:20
JLB
V11000
Benzene
<0.180
ug/L
0.180
0.500
1
11/01/21 03:20
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 03:20
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 03:20
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 03:20
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 03:20
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 03:20
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 03:20
JLB
V11000
Chlorobenzene
<0.190
Ng/L
0.190
0.500
1
11/01/21 03:20
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 03:20
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 03:20
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 03:20
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 03:20
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 03:20
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 03:20
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 03:20
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 03:20
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 03:20
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 28 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
REPORT OF ANAL YSIS
Lab No : 97853 Matrix: Aqueous
Sample ID : TB-20211019B Sampled: 10/19/2021 0:00
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 03:20
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 03:20
JLB
V11000
1,4-Dichlorobenzene
<0.210
Ng/L
0.210
0.500
1
11/01/21 03:20
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 03:20
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 03:20
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 03:20
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 03:20
JLB
V11000
cis- 1,2-Dich loroethene
<0.200
ug/L
0.200
0.500
1
11/01/21 03:20
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 03:20
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 03:20
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 03:20
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 03:20
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 03:20
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 03:20
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 03:20
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 03:20
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 03:20
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 03:20
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 03:20
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 03:20
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 03:20
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 03:20
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 29 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97853
Matrix: Aqueous
Sample ID : TB-20211019B
Sampled:
10/19/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 03:20
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 03:20
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 03:20
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 03:20
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 03:20
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 03:20
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 03:20
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 03:20
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 03:20
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 03:20
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 03:20
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 03:20
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 03:20
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 03:20
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 03:20
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 03:20
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 03:20
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 03:20
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 03:20
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 03:20
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 03:20
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 30 of 105

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-294-8011
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/21/2021
Lab No : 97854
Matrix: Aqueous
Sample ID: MW-04-20211019
Sampled:
10/19/2021
10:58
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ferrous Iron
<50.0
Ng/L
50.0
200
1
10/21/21 16:01
SMW
SM-3500-Fe-B
1,4-Dioxane
5.56
ug/L
0.139
2.00
1
10/25/21 15:44
TBL
8260D SIM
Alkalinity (as CaCO3)
103000
Ng/L
800
5000
1
10/27/21 10:20
CLB
2320B-2011
Biochemical Oxygen Demand (5-day) 2000 H
ug/L
2000
2000
1
10/21/21 15:53
SLO
521OB-2016
Chloride
61700
Ng/L
370
1000
1
10/21/2114:41
CEG
9056A
Cyanide, Total
<3.80
ug/L
3.80
10.0
1
10/27/21 09:30
ENM
450OCNE-2016
COD (Chemical Oxygen Demand) 340003
Ng/L
11000
50000
1
10/25/21 11:16
ENM
5220D-2011
Nitrate (NO3-N)
1760
ug/L
76.0
200
1
10/21/21 14:41
CEG
9056A
TOC
2390
Ng/L
500
1000
1
10/28/21 17:12
JW2
531OC-2011
Sulfate
124000
ug/L
540
1000
1
10/21/2114:41
CEG
9056A
Sulfide
<830
Ng/L
2000
1
10/26/2109:45
ENM
4500S2F-2011
Antimony
<0.490
ug/L
0.490
2.00
1
11/03/2108:15
EDV
6020B
Arsenic
<0.170
Ng/L
0.170
1.00
1
10/29/2103:18
EDV
6020B
Barium
72.1
ug/L
0.810
10.0
1
10/29/2103:18
EDV
6020B
Beryllium
<0.190
Ng/L
0.190
1.00
1
10/29/2103:18
EDV
6020B
Cadmium
0.3303
ug/L
0.160
1.00
1
10/29/2103:18
EDV
6020B
Chromium
<0.790
Ng/L
0.790
2.00
1
10/29/2103:18
EDV
6020B
Cobalt
2.97
ug/L
0.520
2.00
1
10/29/2103:18
EDV
6020B
Copper
<3.80
Ng/L
3.80
10.0
1
10/29/21 03:18
EDV
6020B
Lead
<0.260
ug/L
0.260
1.00
1
10/29/21 03:18
EDV
6020B
Mercury (Total)
<0.0700
Ng/L
0.0700
0.200
1
10/27/21 18:58
EDV
7470A
Nickel
3.51
ug/L
0.510
3.00
1
10/29/2103:18
EDV
6020B
Selenium
0.9213
Ng/L
0.740
5.00
1
10/29/2103:18
EDV
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 31 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97854
Sample ID: MW-04-20211019
Matrix: Aqueous
Sampled: 10/19/2021 10:58
Test
Results
Units
MDL
MQL
DF
Date / Time By Analytical
Analyzed Method
Silver
<0.110
Ng/L
0.110
1.00
1
10/29/2103:18 EDV 6020E
Tin
<1.80
ug/L
1.80
5.00
1
10/29/2103:18 EDV 6020B
Thallium
<0.570
Ng/L
0.570
2.00
1
10/29/2103:18 EDV 6020B
Vanadium
<1.30
ug/L
1.30
5.00
1
11/08/2116:50 EDV 6020B
Zinc
<6.90
Ng/L
6.90
20.0
1
10/29/2103:18 EDV 6020B
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 32 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97854
Matrix: Aqueous
Sample ID: MW-04-20211019
Sampled:
10/19/2021
10:58
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
Ng/L
1.80
5.00
1
11/01/21 07:51
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 07:51
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 07:51
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 07:51
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 07:51
JLB
V11000
Benzene
0.568
ug/L
0.180
0.500
1
11/01/21 07:51
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 07:51
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 07:51
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 07:51
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 07:51
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 07:51
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 07:51
JLB
V11000
Chlorobenzene
2.60
Ng/L
0.190
0.500
1
11/01/21 07:51
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 07:51
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 07:51
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 07:51
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 07:51
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 07:51
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 07:51
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 07:51
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 07:51
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 07:51
JLB
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 33 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
REPORT OF ANAL YSIS
Lab No : 97854 Matrix: Aqueous
Sample ID: MW-04-20211019 Sampled: 10/19/2021 10:58
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 07:51
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 07:51
JLB
V11000
1,4-Dichlorobenzene
3.02
Ng/L
0.210
0.500
1
11/01/21 07:51
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 07:51
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 07:51
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 07:51
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 07:51
JLB
V11000
cis- 1,2-Dich loroethene
1.17
ug/L
0.200
0.500
1
11/01/21 07:51
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 07:51
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 07:51
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 07:51
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 07:51
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 07:51
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 07:51
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 07:51
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 07:51
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 07:51
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 07:51
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 07:51
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 07:51
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 07:51
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 07:51
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 34 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97854
Matrix: Aqueous
Sample ID: MW-04-20211019
Sampled:
10/19/2021
10:58
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 07:51
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 07:51
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 07:51
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 07:51
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 07:51
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 07:51
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 07:51
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 07:51
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 07:51
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 07:51
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 07:51
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 07:51
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 07:51
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 07:51
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 07:51
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 07:51
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 07:51
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 07:51
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 07:51
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 07:51
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 07:51
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 35 of 105

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-294-8011
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/21/2021
Lab No : 97855
Matrix: Aqueous
Sample ID: MW-05R-20211019
Sampled:
10/19/2021
16:05
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ferrous Iron
7640
Ng/L
250
1000
1
10/21/21 16:01
SMW
SM-3500-Fe-B
1,4-Dioxane
4.34
ug/L
0.139
2.00
1
10/25/21 16:09
TBL
8260D SIM
Alkalinity (as CaCO3)
203000
Ng/L
800
5000
1
10/27/21 10:20
CLB
2320B-2011
Biochemical Oxygen Demand (5-day) 15500
ug/L
2000
2000
1
10/21/21 15:53
SLO
521OB-2016
Chloride
66500
Ng/L
370
1000
1
10/21/21 14:26
CEG
9056A
Cyanide, Total
<3.80
ug/L
3.80
10.0
1
10/27/21 09:30
ENM
450OCNE-2016
COD (Chemical Oxygen Demand) 101000
Ng/L
11000
50000
1
10/25/21 11:16
ENM
5220D-2011
Nitrate (NO3-N)
<76.0
ug/L
76.0
200
1
10/21/21 14:26
CEG
9056A
TOC
5360
Ng/L
500
1000
1
10/28/21 18:29
JW2
531OC-2011
Sulfate
<540
ug/L
540
1000
1
10/21/21 14:26
CEG
9056A
Sulfide
<830
Ng/L
2000
1
10/26/2109:45
ENM
4500S2F-2011
Antimony
<0.490
ug/L
0.490
2.00
1
11/03/2108:22
EDV
6020B
Dissolved Antimony
<0.490
Ng/L
0.490
2.00
1
11/05/21 13:52
EDV
6020B
Arsenic
0.418 J
ug/L
0.170
1.00
1
10/29/21 03:25
EDV
6020B
Dissolved Arsenic
<0.170
Ng/L
0.170
1.00
1
11/05/21 13:52
EDV
6020B
Barium
116
ug/L
0.810
10.0
1
10/29/2103:25
EDV
6020B
Dissolved Barium
59.9
Ng/L
0.810
10.0
1
11/05/21 13:52
EDV
6020B
Beryllium
<0.190
ug/L
0.190
1.00
1
10/29/2103:25
EDV
6020B
Dissolved Beryllium
<0.190
Ng/L
0.190
1.00
1
11/05/21 13:52
EDV
6020B
Cadmium
<0.160
ug/L
0.160
1.00
1
10/29/2103:25
EDV
6020B
Dissolved Cadmium
<0.160
Ng/L
0.160
1.00
1
11/05/21 13:52
EDV
6020B
Chromium
3.83
ug/L
0.790
2.00
1
10/29/2103:25
EDV
6020B
Dissolved Chromium
<0.790
Ng/L
0.790
2.00
1
11/05/21 13:52
EDV
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 36 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97855
Matrix: Aqueous
Sample ID: MW-05R-20211019
Sampled:
10/19/2021
16:05
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Cobalt
12.5
Ng/L
0.520
2.00
1
10/29/2103:25
EDV
6020B
Dissolved Cobalt
9.14
ug/L
0.520
2.00
1
11/05/21 13:52
EDV
6020B
Copper
<3.80
Ng/L
3.80
10.0
1
10/29/2103:25
EDV
6020E
Dissolved Copper
<3.80
ug/L
3.80
10.0
1
11/05/21 13:52
EDV
6020B
Lead
0.6123
Ng/L
0.260
1.00
1
10/29/21 03:25
EDV
6020E
Dissolved Lead
<0.260
ug/L
0.260
1.00
1
11/05/21 13:52
EDV
6020B
Mercury (Total)
<0.0700
Ng/L
0.0700
0.200
1
10/27/21 19:01
EDV
7470A
Dissolved Mercury
<0.0700
ug/L
0.0700
0.200
1
11/06/21 12:13
EDV
7470A
Dissolved Nickel
1.813
Ng/L
0.510
3.00
1
11/05/21 13:52
EDV
6020E
Nickel
3.26
ug/L
0.510
3.00
1
10/29/2103:25
EDV
6020B
Selenium
<0.740
Ng/L
0.740
5.00
1
10/29/2103:25
EDV
6020E
Dissolved Selenium
<0.740
ug/L
0.740
5.00
1
11/05/21 13:52
EDV
6020B
Silver
<0.110
Ng/L
0.110
1.00
1
10/29/2103:25
EDV
6020E
Dissolved Silver
<0.110
ug/L
0.110
1.00
1
11/05/21 13:52
EDV
6020B
Tin
<1.80
Ng/L
1.80
5.00
1
10/29/2103:25
EDV
6020B
Dissolved Tin
<1.80
ug/L
1.80
5.00
1
11/05/21 13:52
EDV
6020B
Thallium
<0.570
Ng/L
0.570
2.00
1
10/29/2103:25
EDV
6020B
Dissolved Thallium
<0.570
ug/L
0.570
2.00
1
11/05/21 13:52
EDV
6020B
Vanadium
1.97 36
Ng/L
1.30
5.00
1
11/08/21 16:57
EDV
6020B
Dissolved Vanadium
<1.30
ug/L
1.30
5.00
1
11/05/21 13:52
EDV
6020B
Zinc
10.13
Ng/L
6.90
20.0
1
10/29/2103:25
EDV
6020B
Dissolved Zinc
<6.90
ug/L
6.90
20.0
1
11/05/21 13:52
EDV
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 37 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97855
Matrix: Aqueous
Sample ID: MW-05R-20211019
Sampled:
10/19/2021
16:05
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
5.07
Ng/L
1.80
5.00
1
11/01/21 08:15
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 08:15
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 08:15
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 08:15
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 08:15
JLB
V11000
Benzene
2.38
ug/L
0.180
0.500
1
11/01/21 08:15
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 08:15
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 08:15
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 08:15
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 08:15
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 08:15
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 08:15
JLB
V11000
Chlorobenzene
8.02
Ng/L
0.190
0.500
1
11/01/21 08:15
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 08:15
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 08:15
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 08:15
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 08:15
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 08:15
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 08:15
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 08:15
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 08:15
JLB
V11000
trans-1,4-Dichloro-2-butene
< 1.30
ug/L
1.30
10.0
1
11/01/21 08:15
JLB
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 38 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
REPORT OF ANAL YSIS
Lab No : 97855 Matrix: Aqueous
Sample ID: MW-05R-20211019 Sampled: 10/19/2021 16:05
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 08:15
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 08:15
JLB
V11000
1,4-Dichlorobenzene
6.13
Ng/L
0.210
0.500
1
11/01/21 08:15
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 08:15
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 08:15
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 08:15
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 08:15
JLB
V11000
cis- 1,2-Dich loroethene
2.10
ug/L
0.200
0.500
1
11/01/21 08:15
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 08:15
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 08:15
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 08:15
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 08:15
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 08:15
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 08:15
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 08:15
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 08:15
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 08:15
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 08:15
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 08:15
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 08:15
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 08:15
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 08:15
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 39 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97855
Matrix: Aqueous
Sample ID: MW-05R-20211019
Sampled:
10/19/2021
16:05
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 08:15
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 08:15
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 08:15
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 08:15
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 08:15
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 08:15
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 08:15
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 08:15
JLB
V11000
Tetrahydrofuran
3.603
Ng/L
1.50
10.0
1
11/01/21 08:15
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 08:15
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 08:15
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 08:15
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 08:15
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 08:15
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 08:15
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 08:15
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 08:15
JLB
V11000
Vinyl Chloride
1.52
ug/L
0.170
0.500
1
11/01/21 08:15
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 08:15
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 08:15
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 08:15
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 40 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97856
Matrix: Aqueous
Sample ID : TB-20211019A
Sampled:
10/19/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
Ng/L
1.80
5.00
1
11/01/21 03:45
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 03:45
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 03:45
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 03:45
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 03:45
JLB
V11000
Benzene
<0.180
ug/L
0.180
0.500
1
11/01/21 03:45
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 03:45
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 03:45
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 03:45
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 03:45
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 03:45
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 03:45
JLB
V11000
Chlorobenzene
<0.190
Ng/L
0.190
0.500
1
11/01/21 03:45
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 03:45
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 03:45
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 03:45
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 03:45
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 03:45
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 03:45
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 03:45
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 03:45
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 03:45
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 41 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
REPORT OF ANAL YSIS
Lab No : 97856 Matrix: Aqueous
Sample ID : TB-20211019A Sampled: 10/19/2021 0:00
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 03:45
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 03:45
JLB
V11000
1,4-Dichlorobenzene
<0.210
Ng/L
0.210
0.500
1
11/01/21 03:45
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 03:45
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 03:45
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 03:45
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 03:45
JLB
V11000
cis- 1,2-Dich loroethene
<0.200
ug/L
0.200
0.500
1
11/01/21 03:45
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 03:45
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 03:45
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 03:45
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 03:45
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 03:45
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 03:45
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 03:45
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 03:45
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 03:45
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 03:45
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 03:45
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 03:45
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 03:45
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 03:45
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 42 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97856
Matrix: Aqueous
Sample ID : TB-20211019A
Sampled:
10/19/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 03:45
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 03:45
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 03:45
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 03:45
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 03:45
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 03:45
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 03:45
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 03:45
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 03:45
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 03:45
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 03:45
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 03:45
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 03:45
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 03:45
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 03:45
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 03:45
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 03:45
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 03:45
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 03:45
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 03:45
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 03:45
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 43 of 105

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-294-8011
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/21/2021
Lab No : 97858
Matrix: Aqueous
Sample ID: MW-04-20211019
Sampled:
10/19/2021
10:58
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Methapyrilene
<10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
BGV
8270D
1,4-Naphthoquinone
<10.5
pg/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
1-Naphthylamine
<10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
2-Acetylaminofluorene
<10.5
ug/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
2-Naphthylamine
<10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
3-Methylcholanthrene
<10.5
ug/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
4-Aminobiphenyl
<10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
5-Nitro-o-toluidine
<10.5
ug/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
7,12-Dimethyl benz(a)anth racene <10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
Diallate
<10.5
ug/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
Hexachloropropene
<10.5 M
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
Isosafrole
<10.5
ug/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
N-Nitrosopiperidine
<10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
N-Nitrosomethylethylamine
<10.5
ug/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
N-Nitrosomorpholine
<10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
N-Nitrosopyrrolidine
<10.5
ug/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
0,0,0-Triethyl Phosphorothioate <0.346
Ng/L
0.346
1.05
1
10/26/21 02:55
VBW
8270C
o-Toluidine
<10.5
ug/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
p-Dimethylaminoazobenzene
<10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
p-Phenylenediamine
<10.5 M
ug/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
Pronamide
<10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
Safrole
<10.5
ug/L
10.5
10.5
1
10/25/21 18:21
VBW
8270D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 44 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97858 Matrix: Aqueous
Sample ID: MW-04-20211019 Sampled: 10/19/2021 10:58
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Thionazine <0.346 Ng/L 0.346 1.05 1 10/26/2102:55 VBW 8270C
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 45 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97858
Matrix: Aqueous
Sample ID: MW-04-20211019
Sampled:
10/19/2021
10:58
Analytical Method:
8270C
Prep Batch(es):
L580965
10/25/21 10:30
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Dimethoate
<0.748
Ng/L
0.748
1.05
1
10/26/21 02:55
VBW
L581161
Disulfoton
<0.489
ug/L
0.489
1.05
1
10/26/21 02:55
VBW
L581161
Ethyl Parathion
<0.596
Ng/L
0.596
1.05
1
10/26/21 02:55
VBW
L581161
Famphur
<0.537
ug/L
0.537
1.05
1
10/26/21 02:55
VBW
L581161
Methyl Parathion
<0.845
Ng/L
0.845
1.05
1
10/26/21 02:55
VBW
L581161
Phorate
<0.691
ug/L
0.691
1.05
1
10/26/21 02:55
VBW
L581161
Analytical Method:
8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dinitrobenzene
<0.949
ug/L
0.949
10.5
1
10/25/21 18:21
VBW
L581160
1,3,5-Trinitrobenzene
<10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
L581162
Acenaphthene
<0.445
ug/L
0.445
2.11
1
10/25/21 18:21
VBW
L581160
Acenaphthylene
<0.452
Ng/L
0.452
2.11
1
10/25/21 18:21
VBW
L581160
Acetophenone
<0.721
ug/L
0.721
5.26
1
10/25/21 18:21
VBW
L581160
Anthracene
<0.492
Ng/L
0.492
2.11
1
10/25/21 18:21
VBW
L581160
Benzo(a)anthracene
<0.450
ug/L
0.450
2.11
1
10/25/21 18:21
VBW
L581160
Benzo(a)pyrene
<1.06
Ng/L
1.06
2.11
1
10/25/21 18:21
VBW
L581160
Benzo(b)fluoranthene
<0.992
ug/L
0.992
2.11
1
10/25/21 18:21
VBW
L581160
Benzo(g,h,i)perylene
<1.43
Ng/L
1.43
2.11
1
10/25/21 18:21
VBW
L581160
Benzo(k)fluoranthene
<0.793
ug/L
0.793
2.11
1
10/25/21 18:21
VBW
L581160
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 46 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
REPORT OF ANAL YSIS
Lab No : 97858 Matrix: Aqueous
Sample ID: MW-04-20211019 Sampled: 10/19/2021 10:58
Analytical Method: 8270D Prep Batch(es): L580969 10/25/21 10:30
Prep Method: 3510C
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Benzyl alcohol
<3.16
Ng/L
3.16
10.5
1
10/25/21 18:21
VBW
L581160
Bis(2-Chloroethoxy)methane
<0.455
ug/L
0.455
5.26
1
10/25/21 18:21
VBW
L581160
Bis(2-Chloroethyl)ether
<0.470
Ng/L
0.470
5.26
1
10/25/21 18:21
VBW
L581160
Bis(2-Chloroisopropyl)ether
<0.574
ug/L
0.574
5.26
1
10/25/21 18:21
VBW
L581160
Bis(2-ethylhexyl)phthalate
<3.85
Ng/L
3.85
5.26
1
10/25/21 18:21
VBW
L581160
4-Bromophenyl phenyl ether
<0.526
ug/L
0.526
5.26
1
10/25/21 18:21
VBW
L581160
Butyl benzyl phthalate
<4.83
Ng/L
4.83
5.26
1
10/25/21 18:21
VBW
L581160
4-Chloro-3-methylphenol
<0.529
ug/L
0.529
5.26
1
10/25/21 18:21
VBW
L581160
4-Chloroaniline
<0.553
Ng/L
0.553
5.26
1
10/25/21 18:21
VBW
L581160
Chlorobenzilate
<2.00
ug/L
2.00
5.26
1
10/25/21 18:21
VBW
L581160
2-Chloronaphthalene
<0.500
Ng/L
0.500
5.26
1
10/25/21 18:21
VBW
L581160
2-Chlorophenol
<0.774
ug/L
0.774
5.26
1
10/25/21 18:21
VBW
L581160
4-Chlorophenyl phenyl ether
<0.503
Ng/L
0.503
5.26
1
10/25/21 18:21
VBW
L581160
Chrysene
<0.771
ug/L
0.771
2.11
1
10/25/21 18:21
VBW
L581160
Dibenz(a,h)anthracene
<0.265
Ng/L
0.265
2.11
1
10/25/21 18:21
VBW
L581160
Dibenzofuran
<0.444
ug/L
0.444
5.26
1
10/25/21 18:21
VBW
L581160
1,2-Dichlorobenzene
<0.661
Ng/L
0.661
5.26
1
10/25/21 18:21
VBW
L581160
1,3-Dichlorobenzene
<0.516
ug/L
0.516
5.26
1
10/25/21 18:21
VBW
L581160
1,4-Dichlorobenzene
1.273
Ng/L
0.610
5.26
1
10/25/21 18:21
VBW
L581160
3,3'-Dichlorobenzidine
<3.93
ug/L
3.93
10.5
1
10/25/21 18:21
VBW
L581160
2,4-Dichlorophenol
<1.60
Ng/L
1.60
5.26
1
10/25/21 18:21
VBW
L581160
2,6-Dichlorophenol
<0.739
ug/L
0.739
5.26
1
10/25/21 18:21
VBW
L581160
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 47 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97858
Matrix: Aqueous
Sample ID: MW-04-20211019
Sampled:
10/19/2021
10:58
Analytical Method: 8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.615
Ng/L
0.615
5.26
1
10/25/21 18:21
VBW
L581160
Dimethyl phthalate
<0.536
ug/L
0.536
5.26
1
10/25/21 18:21
VBW
L581160
3,3' Dimethylbenzidine
<1.97
Ng/L
1.97
10.5
1
10/25/21 18:21
VBW
L581160
2,4-Dimethylphenol
<0.709
ug/L
0.709
5.26
1
10/25/21 18:21
VBW
L581160
Di-n-butyl phthalate
<1.66
Ng/L
1.66
5.26
1
10/25/21 18:21
VBW
L581160
4,6- Din itro-2- methyl phenol
<3.64
ug/L
3.64
10.5
1
10/25/21 18:21
VBW
L581160
2,4-Dinitrophenol
<5.09
Ng/L
5.09
10.5
1
10/25/21 18:21
VBW
L581160
2,4-Dinitrotoluene
<0.423
ug/L
0.423
5.26
1
10/25/21 18:21
VBW
L581160
2,6-Dinitrotoluene
<0.434
Ng/L
0.434
5.26
1
10/25/21 18:21
VBW
L581160
Di-n-Octyl Phthalate
<1.81
u9/L
1.81
5.26
1
10/25/21 18:21
VBW
L581160
Ethyl methanesulfonate
<0.751
Ng/L
0.751
5.26
1
10/25/21 18:21
VBW
L581160
Fluoranthene
<0.428
ug/L
0.428
2.11
1
10/25/21 18:21
VBW
L581160
Fluorene
<0.468
Ng/L
0.468
2.11
1
10/25/21 18:21
VBW
L581160
Hexachlorobenzene
<2.70
ug/L
2.70
5.26
1
10/25/21 18:21
VBW
L581160
Hexachlorobutadiene
<0.426
Ng/L
0.426
5.26
1
10/25/21 18:21
VBW
L581160
Hexachlorocyclopentadiene
<2.46
ug/L
2.46
5.26
1
10/25/21 18:21
VBW
L581160
Hexachloroethane
<0.291
Ng/L
0.291
5.26
1
10/25/21 18:21
VBW
L581160
Indeno(1,2,3-cd)pyrene
<1.07
ug/L
1.07
2.11
1
10/25/21 18:21
VBW
L581160
Isodrin
<10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
L581162
Isophorone
<0.378
ug/L
0.378
5.26
1
10/25/21 18:21
VBW
L581160
Kepone
<10.5
Ng/L
10.5
10.5
1
10/25/21 18:21
VBW
L581162
Methyl methanesulfonate
<0.650
ug/L
0.650
5.26
1
10/25/21 18:21
VBW
L581160
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 48 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97858
Matrix: Aqueous
Sample ID: MW-04-20211019
Sampled:
10/19/2021
10:58
Analytical Method: 8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Methylnaphthalene
<0.511
Ng/L
0.511
2.11
1
10/25/21 18:21
VBW
L581160
2-Methylphenol
<0.758
ug/L
0.758
5.26
1
10/25/21 18:21
VBW
L581160
3&4 Methylphenol
<0.726
Ng/L
0.726
5.26
1
10/25/21 18:21
VBW
L581160
Naphthalene
<0.510
ug/L
0.510
2.11
1
10/25/21 18:21
VBW
L581160
2-Nitroaniline
<0.603
Ng/L
0.603
5.26
1
10/25/21 18:21
VBW
L581160
3-Nitroaniline
<1.61
ug/L
1.61
10.5
1
10/25/21 18:21
VBW
L581160
4-Nitroaniline
<0.778
Ng/L
0.778
5.26
1
10/25/21 18:21
VBW
L581160
Nitrobenzene
<0.558
ug/L
0.558
5.26
1
10/25/21 18:21
VBW
L581160
2-Nitrophenol
<0.637
Ng/L
0.637
5.26
1
10/25/21 18:21
VBW
L581160
4-Nitrophenol
<1.46
ug/L
1.46
10.5
1
10/25/21 18:21
VBW
L581160
N-Nitrosodimethylamine
<0.261
Ng/L
0.261
5.26
1
10/25/21 18:21
VBW
L581160
N-Nitrosodiphenylamine
<0.822
ug/L
0.822
10.5
1
10/25/21 18:21
VBW
L581160
N-Nitrosodiethylamine
<0.420
Ng/L
0.420
5.26
1
10/25/21 18:21
VBW
L581160
N-Nitroso-di-n-butylamine
<0.791
u9/L
0.791
5.26
1
10/25/21 18:21
VBW
L581160
N-Nitroso-di-n-propylamine
<0.351
Ng/L
0.351
5.26
1
10/25/21 18:21
VBW
L581160
Pentachlorobenzene
<0.481
u9/L
0.481
10.5
1
10/25/21 18:21
VBW
L581160
Pentachloronitrobenzene
<1.21
Ng/L
1.21
5.26
1
10/25/21 18:21
VBW
L581160
Pentachlorophenol
<2.57
ug/L
2.57
10.5
1
10/25/21 18:21
VBW
L581160
Phenacetin
<1.35
Ng/L
1.35
5.26
1
10/25/21 18:21
VBW
L581160
Phenanthrene
<0.489
ug/L
0.489
2.11
1
10/25/21 18:21
VBW
L581160
Phenol
<0.409
Ng/L
0.409
5.26
1
10/25/21 18:21
VBW
L581160
Pyrene
<1.10
ug/L
1.10
2.11
1
10/25/21 18:21
VBW
L581160
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 49 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
Lab No : 97858
Sample ID: MW-04-20211019
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 10/19/2021 10:58
Analytical Method: 8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2,4,5-Tetrachlorobenzene
<0.333
Ng/L
0.333
5.26
1
10/25/2118:21
VBW
L581160
2,3,4,6-Tetrachlorophenol
<0.373
ug/L
0.373
5.26
1
10/25/2118:21
VBW
L581160
1,2,4-Trichlorobenzene
<0.507
Ng/L
0.507
5.26
1
10/25/2118:21
VBW
L581160
2,4,5-Trichlorophenol
<0.368
ug/L
0.368
5.26
1
10/25/2118:21
VBW
L581160
2,4,6-Trichlorophenol
<0.361
Ng/L
0.361
5.26
1
10/25/2118:21
VBW
L581160
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
M Minimum value MQL Method Quantitation Limit
Page 50 of 105

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-294-8011
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/21/2021
Lab No : 97859
Matrix: Aqueous
Sample ID: MW-05R-20211019
Sampled:
10/19/2021
16:05
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Methapyrilene
<10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
BGV
8270D
1,4-Naphthoquinone
<10.0
pg/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
1-Naphthylamine
<10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
2-Acetylaminofluorene
<10.0
ug/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
2-Naphthylamine
<10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
3-Methylcholanthrene
<10.0
ug/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
4-Aminobiphenyl
<10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
5-Nitro-o-toluidine
<10.0
ug/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
7,12-Dimethyl benz(a)anth racene <10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
Diallate
<10.0
ug/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
Hexachloropropene
<10.0 M
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
Isosafrole
<10.0
ug/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
N-Nitrosopiperidine
<10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
N-Nitrosomethylethylamine
<10.0
ug/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
N-Nitrosomorpholine
<10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
N-Nitrosopyrrolidine
<10.0
ug/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
0,0,0-Triethyl Phosphorothioate <0.330
Ng/L
0.330
1.00
1
10/26/21 03:06
VBW
8270C
o-Toluidine
<10.0
ug/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
p-Dimethylaminoazobenzene
<10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
p-Phenylenediamine
<10.0 M
ug/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
Pronamide
<10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
Safrole
<10.0
ug/L
10.0
10.0
1
10/25/21 18:42
VBW
8270D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 51 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97859 Matrix: Aqueous
Sample ID: MW-05R-20211019 Sampled: 10/19/2021 16:05
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Thionazine <0.330 Ng/L 0.330 1.00 1 10/26/2103:06 VBW 8270C
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 52 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97859
Matrix: Aqueous
Sample ID: MW-05R-20211019
Sampled:
10/19/2021
16:05
Analytical Method:
8270C
Prep Batch(es):
L580965
10/25/21 10:30
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Dimethoate
<0.713
Ng/L
0.713
1.00
1
10/26/21 03:06
VBW
L581161
Disulfoton
<0.466
ug/L
0.466
1.00
1
10/26/21 03:06
VBW
L581161
Ethyl Parathion
<0.568
Ng/L
0.568
1.00
1
10/26/21 03:06
VBW
L581161
Famphur
<0.512
ug/L
0.512
1.00
1
10/26/21 03:06
VBW
L581161
Methyl Parathion
<0.805
Ng/L
0.805
1.00
1
10/26/21 03:06
VBW
L581161
Phorate
<0.659
ug/L
0.659
1.00
1
10/26/21 03:06
VBW
L581161
Analytical Method:
8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dinitrobenzene
<0.904
ug/L
0.904
10.0
1
10/25/21 18:42
VBW
L581160
1,3,5-Trinitrobenzene
<10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
L581162
Acenaphthene
<0.422
ug/L
0.422
2.00
1
10/25/21 18:42
VBW
L581160
Acenaphthylene
<0.429
Ng/L
0.429
2.00
1
10/25/21 18:42
VBW
L581160
Acetophenone
<0.686
ug/L
0.686
5.00
1
10/25/21 18:42
VBW
L581160
Anthracene
<0.467
Ng/L
0.467
2.00
1
10/25/21 18:42
VBW
L581160
Benzo(a)anthracene
<0.427
ug/L
0.427
2.00
1
10/25/21 18:42
VBW
L581160
Benzo(a)pyrene
<1.00
Ng/L
1.00
2.00
1
10/25/21 18:42
VBW
L581160
Benzo(b)fluoranthene
<0.941
u9/L
0.941
2.00
1
10/25/21 18:42
VBW
L581160
Benzo(g,h,i)perylene
<1.36
Ng/L
1.36
2.00
1
10/25/21 18:42
VBW
L581160
Benzo(k)fluoranthene
<0.752
ug/L
0.752
2.00
1
10/25/21 18:42
VBW
L581160
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 53 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
REPORT OF ANAL YSIS
Lab No : 97859 Matrix: Aqueous
Sample ID: MW-05R-20211019 Sampled: 10/19/2021 16:05
Analytical Method: 8270D Prep Batch(es): L580969 10/25/21 10:30
Prep Method: 3510C
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Benzyl alcohol
<3.01
Ng/L
3.01
10.0
1
10/25/21 18:42
VBW
L581160
Bis(2-Chloroethoxy)methane
<0.433
ug/L
0.433
5.00
1
10/25/21 18:42
VBW
L581160
Bis(2-Chloroethyl)ether
<0.447
Ng/L
0.447
5.00
1
10/25/21 18:42
VBW
L581160
Bis(2-Chloroisopropyl)ether
<0.546
ug/L
0.546
5.00
1
10/25/21 18:42
VBW
L581160
Bis(2-ethylhexyl)phthalate
<3.66
Ng/L
3.66
5.00
1
10/25/21 18:42
VBW
L581160
4-Bromophenyl phenyl ether
<0.500
ug/L
0.500
5.00
1
10/25/21 18:42
VBW
L581160
Butyl benzyl phthalate
<4.59
Ng/L
4.59
5.00
1
10/25/21 18:42
VBW
L581160
4-Chloro-3-methylphenol
<0.503
ug/L
0.503
5.00
1
10/25/21 18:42
VBW
L581160
4-Chloroaniline
<0.526
Ng/L
0.526
5.00
1
10/25/21 18:42
VBW
L581160
Chlorobenzilate
<1.90
ug/L
1.90
5.00
1
10/25/21 18:42
VBW
L581160
2-Chloronaphthalene
<0.476
Ng/L
0.476
5.00
1
10/25/21 18:42
VBW
L581160
2-Chlorophenol
<0.736
ug/L
0.736
5.00
1
10/25/21 18:42
VBW
L581160
4-Chlorophenyl phenyl ether
<0.479
Ng/L
0.479
5.00
1
10/25/21 18:42
VBW
L581160
Chrysene
<0.731
ug/L
0.731
2.00
1
10/25/21 18:42
VBW
L581160
Dibenz(a,h)anthracene
<0.252
Ng/L
0.252
2.00
1
10/25/21 18:42
VBW
L581160
Dibenzofuran
0.533 J
ug/L
0.423
5.00
1
10/25/21 18:42
VBW
L581160
1,2-Dichlorobenzene
<0.629
Ng/L
0.629
5.00
1
10/25/21 18:42
VBW
L581160
1,3-Dichlorobenzene
<0.491
ug/L
0.491
5.00
1
10/25/21 18:42
VBW
L581160
1,4-Dichlorobenzene
2.64 J
Ng/L
0.580
5.00
1
10/25/21 18:42
VBW
L581160
3,3'-Dichlorobenzidine
<3.74
ug/L
3.74
10.0
1
10/25/21 18:42
VBW
L581160
2,4-Dichlorophenol
<1.52
Ng/L
1.52
5.00
1
10/25/21 18:42
VBW
L581160
2,6-Dichlorophenol
<0.703
ug/L
0.703
5.00
1
10/25/21 18:42
VBW
L581160
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 54 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
REPORT OF ANAL YSIS
Lab No : 97859 Matrix: Aqueous
Sample ID: MW-05R-20211019 Sampled: 10/19/2021 16:05
Analytical Method: 8270D Prep Batch(es): L580969 10/25/21 10:30
Prep Method: 3510C
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Diethyl phthalate
3.483
Ng/L
0.585
5.00
1
10/25/21 18:42
VBW
L581160
Dimethyl phthalate
<0.510
ug/L
0.510
5.00
1
10/25/21 18:42
VBW
L581160
3,3' Dimethylbenzidine
<1.88
Ng/L
1.88
10.0
1
10/25/21 18:42
VBW
L581160
2,4-Dimethylphenol
<0.674
ug/L
0.674
5.00
1
10/25/21 18:42
VBW
L581160
Di-n-butyl phthalate
<1.58
Ng/L
1.58
5.00
1
10/25/21 18:42
VBW
L581160
4,6- Din itro-2- methyl phenol
<3.47
u9/L
3.47
10.0
1
10/25/21 18:42
VBW
L581160
2,4-Dinitrophenol
<4.85
Ng/L
4.85
10.0
1
10/25/21 18:42
VBW
L581160
2,4-Dinitrotoluene
<0.403
ug/L
0.403
5.00
1
10/25/21 18:42
VBW
L581160
2,6-Dinitrotoluene
<0.413
Ng/L
0.413
5.00
1
10/25/21 18:42
VBW
L581160
Di-n-Octyl Phthalate
<1.72
u9/L
1.72
5.00
1
10/25/21 18:42
VBW
L581160
Ethyl methanesulfonate
<0.714
Ng/L
0.714
5.00
1
10/25/21 18:42
VBW
L581160
Fluoranthene
<0.406
ug/L
0.406
2.00
1
10/25/21 18:42
VBW
L581160
Fluorene
0.5233
Ng/L
0.444
2.00
1
10/25/21 18:42
VBW
L581160
Hexachlorobenzene
<2.57
ug/L
2.57
5.00
1
10/25/21 18:42
VBW
L581160
Hexachlorobutadiene
<0.405
Ng/L
0.405
5.00
1
10/25/21 18:42
VBW
L581160
Hexachlorocyclopentadiene
<2.34
ug/L
2.34
5.00
1
10/25/21 18:42
VBW
L581160
Hexachloroethane
<0.277
Ng/L
0.277
5.00
1
10/25/21 18:42
VBW
L581160
Indeno(1,2,3-cd)pyrene
<1.01
ug/L
1.01
2.00
1
10/25/21 18:42
VBW
L581160
Isodrin
<10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
L581162
Isophorone
<0.360
ug/L
0.360
5.00
1
10/25/21 18:42
VBW
L581160
Kepone
<10.0
Ng/L
10.0
10.0
1
10/25/21 18:42
VBW
L581162
Methyl methanesulfonate
<0.618
ug/L
0.618
5.00
1
10/25/21 18:42
VBW
L581160
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 55 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97859
Matrix: Aqueous
Sample ID: MW-05R-20211019
Sampled:
10/19/2021
16:05
Analytical Method: 8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Methylnaphthalene
<0.485
Ng/L
0.485
2.00
1
10/25/21 18:42
VBW
L581160
2-Methylphenol
<0.721
u9/L
0.721
5.00
1
10/25/21 18:42
VBW
L581160
3&4 Methylphenol
<0.691
Ng/L
0.691
5.00
1
10/25/21 18:42
VBW
L581160
Naphthalene
<0.484
ug/L
0.484
2.00
1
10/25/21 18:42
VBW
L581160
2-Nitroaniline
<0.574
Ng/L
0.574
5.00
1
10/25/21 18:42
VBW
L581160
3-Nitroaniline
<1.53
ug/L
1.53
10.0
1
10/25/21 18:42
VBW
L581160
4-Nitroaniline
<0.740
Ng/L
0.740
5.00
1
10/25/21 18:42
VBW
L581160
Nitrobenzene
<0.531
ug/L
0.531
5.00
1
10/25/21 18:42
VBW
L581160
2-Nitrophenol
<0.606
Ng/L
0.606
5.00
1
10/25/21 18:42
VBW
L581160
4-Nitrophenol
<1.39
ug/L
1.39
10.0
1
10/25/21 18:42
VBW
L581160
N-Nitrosodimethylamine
<0.249
Ng/L
0.249
5.00
1
10/25/21 18:42
VBW
L581160
N-Nitrosodiphenylamine
<0.783
ug/L
0.783
10.0
1
10/25/21 18:42
VBW
L581160
N-Nitrosodiethylamine
<0.400
Ng/L
0.400
5.00
1
10/25/21 18:42
VBW
L581160
N-Nitroso-di-n-butylamine
<0.752
ug/L
0.752
5.00
1
10/25/21 18:42
VBW
L581160
N-Nitroso-di-n-propylamine
<0.334
Ng/L
0.334
5.00
1
10/25/21 18:42
VBW
L581160
Pentachlorobenzene
<0.459
ug/L
0.459
10.0
1
10/25/21 18:42
VBW
L581160
Pentachloronitrobenzene
<1.15
Ng/L
1.15
5.00
1
10/25/21 18:42
VBW
L581160
Pentachlorophenol
<2.45
ug/L
2.45
10.0
1
10/25/21 18:42
VBW
L581160
Phenacetin
<1.28
Ng/L
1.28
5.00
1
10/25/21 18:42
VBW
L581160
Phenanthrene
<0.464
ug/L
0.464
2.00
1
10/25/21 18:42
VBW
L581160
Phenol
<0.389
Ng/L
0.389
5.00
1
10/25/21 18:42
VBW
L581160
Pyrene
<1.04
ug/L
1.04
2.00
1
10/25/21 18:42
VBW
L581160
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 56 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
Lab No : 97859
Sample ID: MW-05R-20211019
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 10/19/2021 16:05
Analytical Method: 8270D
Prep Batch(es):
L580969
10/25/21 10:30
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2,4,5-Tetrachlorobenzene
<0.317
Ng/L
0.317
5.00
1
10/25/2118:42
VBW
L581160
2,3,4,6-Tetrachlorophenol
<0.355
ug/L
0.355
5.00
1
10/25/2118:42
VBW
L581160
1,2,4-Trichlorobenzene
<0.482
Ng/L
0.482
5.00
1
10/25/2118:42
VBW
L581160
2,4,5-Trichlorophenol
<0.350
ug/L
0.350
5.00
1
10/25/2118:42
VBW
L581160
2,4,6-Trichlorophenol
<0.344
Ng/L
0.344
5.00
1
10/25/2118:42
VBW
L581160
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
M Minimum value MQL Method Quantitation Limit
Page 57 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97860
Matrix: Aqueous
Sample ID : TB-20211019C
Sampled:
10/19/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
2.273
Ng/L
1.80
5.00
1
11/01/21 04:09
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 04:09
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 04:09
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 04:09
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 04:09
JLB
V11000
Benzene
<0.180
ug/L
0.180
0.500
1
11/01/21 04:09
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 04:09
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 04:09
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 04:09
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 04:09
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 04:09
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 04:09
JLB
V11000
Chlorobenzene
<0.190
Ng/L
0.190
0.500
1
11/01/21 04:09
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 04:09
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 04:09
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 04:09
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 04:09
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 04:09
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 04:09
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 04:09
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 04:09
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 04:09
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 58 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011
REPORT OF ANAL YSIS
Lab No : 97860 Matrix: Aqueous
Sample ID : TB-20211019C Sampled: 10/19/2021 0:00
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 04:09
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 04:09
JLB
V11000
1,4-Dichlorobenzene
<0.210
Ng/L
0.210
0.500
1
11/01/21 04:09
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 04:09
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 04:09
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 04:09
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 04:09
JLB
V11000
cis- 1,2-Dich loroethene
<0.200
ug/L
0.200
0.500
1
11/01/21 04:09
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 04:09
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 04:09
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 04:09
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 04:09
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 04:09
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 04:09
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 04:09
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 04:09
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 04:09
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 04:09
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 04:09
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 04:09
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 04:09
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 04:09
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 59 of 105

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/21/2021
Asheville , NC 28801
Report Number : 21-294-8011 REPOR T OF A NA L YSIS
Lab No : 97860
Matrix: Aqueous
Sample ID : TB-20211019C
Sampled:
10/19/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 04:09
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 04:09
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 04:09
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 04:09
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 04:09
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 04:09
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 04:09
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 04:09
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 04:09
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 04:09
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 04:09
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 04:09
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 04:09
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 04:09
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 04:09
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 04:09
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 04:09
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 04:09
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 04:09
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 04:09
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 04:09
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 60 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-294-8011
QC Analytical Batch:
V10803
Analysis Method:
2320B-2011
Analysis Description:
Alkalinity
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples:
97850, 97854, 97855
Blank MDL
MQL
Analyzed
Parameter
Units
Result
Alkalinity (as CaCO3)
pg/L
<800 800
5000
10/27/21 10:20
Laboratory Control Sample
LCS
Spike
LCS
LCS %Rec % Rec
Parameter
Units
Conc.
Result
Limits
Alkalinity (as CaCO3)
pg/L
250000
250000
100 90-110
Duplicate
V 98019-DUP
Result DUP
RPD Max RPD
Analyzed
Parameter
Units
Result
Alkalinity (as CaCO3)
pg/L
51000 52000
1.9 20
10/27/21 10:20
Date: 12/21/2021 12:58 PM Page 1 of 41
Page 61 of 105

•
Waypoint,
449 Springbrook
Charlotte, NC 28217
Rd, Ch
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Analytical Batch: V10861
Analysis Method: 2340C-2011
Analysis Description: Total Hardness
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples: 97851, 97852
Blank MDL
MQL
Analyzed
Parameter Units
Result
Hardness pg/L
<570 570
5000
10/28/21 10:10
Laboratory Control Sample
LCS
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Hardness pg/L
50000
50000
100 90-110
Duplicate
V 98125-DUP
Result DUP
RPD Max RPD
Analyzed
Parameter Units
Result
Hardness pg/L
108000 108000
0.0 20
10/28/21 10:10
Matrix Spike & Matrix Spike Duplicate
V 98125-MS V 98125-MSD
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Hardness pg/L
108000 20000
20000 128000
130000 100 110 80-120 1.5 20
Date: 12/21/2021 12:58 PM Page 2 of 41
Page 62 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-294-8011
QC Analytical Batch:
V10788
Analysis Method:
450OCNE-2016
Analysis Description:
Total Cyanide
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples:
97850, 97854, 97855
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Cyanide, Total
pg/L
<3.80
3.80
10.0
10/27/21 09:30
Laboratory Control Sample
LCS
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Cyanide, Total
pg/L
100
89.6
90.0
85-115
Matrix Spike & Matrix Spike Duplicate
V 97850-MS V 97850-MSD
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result
Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Cyanide, Total
pg/L
<3.80
100
100 94.8
94.6 95.0
95.0 80-120 0.2 20
Date: 12/21/2021 12:58 PM Page 3 of 41
Page 63 of 105

•
Waypoint,
449 Springbrook
Charlotte, NC 28217
Rd, Ch
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Analytical Batch: V10772
Analysis Method: 4500S2F-2011
Analysis Description: Sulfide
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples: 97850, 97854, 97855
Blank
MQL
Analyzed
Parameter Units
Result
Sulfide pg/L
<2000
2000
10/26/2109:45
Laboratory Control Sample
LCS
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Sulfide pg/L
10000
9000
90.0 70-122
Matrix Spike
V 97992-MS
MS Spike
MSD MS Result
MSD MS %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec Limits RPD
Conc.
Sulfide pg/L
<2000 10000
7000
70.0 70-130
Date: 12/21/2021 12:58 PM Page 4 of 41
Page 64 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Analytical Batch: V10821
Analysis Method: 521OB-2016
Analysis Description: Biochemical Oxygen Demand (BOD)
Glucose-Glutamic Acid GGA
Result Range Analyzed
Parameter Units
Biochemical Oxygen Demand (5-day) Ng/L 122* 167.5-228.E 10/21/21 15:53
Duplicate V 97855-DUP
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Biochemical Oxygen Demand (5-day) Ng/L 15500 25300 48.0* 30 10/21/21 15:53
* QC Fail Date: 12/21/2021 12:58 PM Page 5 of 41
Page 65 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Analytical Batch: V10695
Analysis Method: 5220D-2011
Analysis Description: Chemical Oxygen Demand (COD)
Lab Reagent Blank LRB
Matrix: AQU
Associated Lab Samples: 97850, 97854, 97855
Blank MDL
MQL
Analyzed
Parameter Units Result
COD (Chemical Oxygen Demand) pg/L <11000 11000
50000
10/25/21 11:16
Laboratory Control Sample LCS
Spike
LCS
LCS %Rec
% Rec
Parameter Units Conc.
Result
Limits
COD (Chemical Oxygen Demand) pg/L 500000
526000
105
90-110
Matrix Spike & Matrix Spike Duplicate V 97861-MS V 97861-MSD
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter Units Result Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
COD (Chemical Oxygen Demand) pg/L 82000 500000
500000 587000
555000 101
95.0 80-120 5.6 20
Date: 12/21/2021 12:58 PM Page 6 of 41
Page 66 of 105

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality
Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: L581378
QC Analytical Batch(es): L581383
QC Prep Batch Method: 5310C-2011
Analysis Method:
5310C-2011
Analysis Description:
Total Organic Carbon
Lab Reagent Blank
LRB-L581378
Matrix: AQU
Associated Lab Samples: 97850
Blank MDL
MQL
Analyzed
Parameter Units
Result
TOC pg/L
<500 500
1000
10/26/2111:26
Laboratory Control Sample
LCS-L581378
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
TOC pg/L
5000
5040
101 85-115
Duplicate
G 62988-DUP-L581378
Result DUP
RPD Max RPD
Analyzed
Parameter Units
Result
TOC pg/L
<1000 <1000
0.0 20
10/26/2120:16
Matrix Spike
V 97850-MS-L581378
MS Spike
MSD MS Result
MSD MS %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec Limits RPD
Conc.
TOC pg/L
3130 5260
8450
101 70-130
Date: 12/21/2021 12:58 PM Page 7 of 41
Page 67 of 105

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality
Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: L581990
QC Analytical Batch(es): L582004
QC Prep Batch Method: 5310C-2011
Analysis Method:
5310C-2011
Analysis Description:
Total Organic Carbon
Lab Reagent Blank
LRB-L581990
Matrix: AQU
Associated Lab Samples: 97854, 97855
Blank MDL
MQL
Analyzed
Parameter Units
Result
TOC pg/L
<500 500
1000
10/28/2112:01
Laboratory Control Sample
LCS-L581990
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
TOC pg/L
5000
5060
101 85-115
Duplicate
V 97854-DUP-L581990
Result DUP
RPD Max RPD
Analyzed
Parameter Units
Result
TOC pg/L
2390 2520
5.2 20
10/28/21 17:50
Matrix Spike
L 96060-MS-L581990
MS Spike
MSD MS Result
MSD MS %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec Limits RPD
Conc.
TOC pg/L
2630 5260
7910
100 70-130
Date: 12/21/2021 12:58 PM Page 8 of 41
Page 68 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V10665 QC Analytical Batch(es): V10786,V11077
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Lab Reagent Blank LRB-V10665 Matrix: AQU
Associated Lab Samples: 97850, 97851
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Antimony
pg/L
<0.490
0.490
2.00
10/27/2102:41
Arsenic
pg/L
<0.170
0.170
1.00
10/27/2102:41
Barium
pg/L
<0.810
0.810
10.0
10/27/2102:41
Beryllium
pg/L
<0.190
0.190
1.00
10/27/2102:41
Cadmium
pg/L
<0.160
0.160
1.00
10/27/2102:41
Chromium
pg/L
<0.790
0.790
2.00
10/27/2102:41
Cobalt
pg/L
<0.520
0.520
2.00
10/27/2102:41
Copper
pg/L
<3.80
3.80
10.0
10/27/2102:41
Lead
pg/L
<0.260
0.260
1.00
10/27/2102:41
Nickel
pg/L
<0.510
0.510
3.00
10/27/2102:41
Selenium
pg/L
<0.740
0.740
5.00
10/27/2102:41
Silver
pg/L
<0.110
0.110
1.00
10/27/2102:41
Tin
pg/L
<1.80
1.80
5.00
10/27/2102:41
Thallium
pg/L
<0.570
0.570
2.00
10/27/2102:41
Vanadium
pg/L
<1.30
1.30
5.00
10/27/2102:41
Zinc
pg/L
<6.90
6.90
20.0
10/27/2102:41
Laboratory Control Sample
LCS-V10665
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Antimony
pg/L
100
115
115
80-120
Arsenic
pg/L
100
99.7
100
80-120
Barium
pg/L
100
102
102
80-120
Beryllium
pg/L
100
108
108
80-120
Cadmium
pg/L
100
101
101
80-120
Chromium
pg/L
100
103
103
80-120
Cobalt
pg/L
100
103
103
80-120
Date:
12/21/2021 12:58 PM
Page 9 of 41
Page 69 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V10665 QC Analytical Batch(es): V10786,V11077
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Laboratory Control Sample LCS-V10665
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Copper
pg/L
100
104
104
80-120
Lead
pg/L
100
103
103
80-120
Nickel
pg/L
100
103
103
80-120
Selenium
pg/L
100
105
105
80-120
Silver
pg/L
100
102
102
80-120
Tin
pg/L
100
102
102
80-120
Thallium
pg/L
100
99.1
99.0
80-120
Vanadium
pg/L
100
104
104
80-120
Zinc
pg/L
100
102
102
80-120
Matrix Spike & Matrix Spike Duplicate
Parameter Units
V 97831-MS-V10665
MS Spike
Result Conc.
V 97831-MSD-V10665
MSD MS Result
Spike
Conc.
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Antimony
pg/L
< 0.490
100
100
108
109
108
109
75-125
0.9
20.0
Arsenic
pg/L
< 0.170
100
100
96.0
95.8
96.0
96.0
75-125
0.2
20.0
Barium
pg/L
37.0
100
100
146
140
109
103
75-125
4.1
20.0
Beryllium
pg/L
< 0.190
100
100
96.8
94.8
97.0
95.0
75-125
2.0
20.0
Cadmium
pg/L
0.290
100
100
99.1
100
99.0
100
75-125
0.9
20.0
Chromium
pg/L
< 0.790
100
100
95.1
96.0
95.0
96.0
75-125
0.9
20.0
Cobalt
pg/L
< 0.520
100
100
96.5
97.1
97.0
97.0
75-125
0.6
20.0
Copper
pg/L
< 3.80
100
100
96.2
97.7
96.0
98.0
75-125
1.5
20.0
Lead
pg/L
< 0.260
100
100
100
99.1
100
99.0
75-125
0.9
20.0
Nickel
pg/L
< 0.510
100
100
95.3
97.0
95.0
97.0
75-125
1.7
20.0
Selenium
pg/L
< 0.740
100
100
99.1
99.7
99.0
100
75-125
0.6
20.0
Silver
pg/L
< 0.110
100
100
99.9
98.8
100
99.0
75-125
1.1
20.0
Tin
pg/L
< 1.80
100
100
98.5
99.4
99.0
99.0
75-125
0.9
20.0
Date: 12/21/2021 12:58 PM Page 10 of 41
Page 70 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-294-8011
QC Prep:
V10665
QC Analytical Batch(es): V10786,V11077
QC Prep Batch Method:
3005A
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Matrix Spike & Matrix Spike
Duplicate
V 97831-MS-V10665
V 97831-MSD-V10665
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Thallium
pg/L
< 0.570 100
100 92.1
92.3 92.0
92.0 75-125 0.2 20.0
Vanadium
pg/L
3.00 100
100 102
103 102
103 75-125 0.9 20.0
Zinc
pg/L
< 6.90 100
100 97.0
99.4 97.0
99.0 75-125 2.4 20.0
Post Digestion Spike
V 97831-PDS-V10665
PDS
%
Analyzed
Parameter
Units
Result Recovery
Antimony
pg/L
51.9
104
11/03/2102:16
Arsenic
pg/L
48.1
96.0
11/03/2102:16
Barium
pg/L
70.1
102
11/03/2102:16
Beryllium
pg/L
46.1
92.0
11/03/2102:16
Cadmium
pg/L
50.8
102
11/03/2102:16
Chromium
pg/L
49.2
98.0
11/03/2102:16
Cobalt
pg/L
48.1
96.0
11/03/2102:16
Copper
pg/L
47.5
95.0
11/03/2102:16
Lead
pg/L
49.8
100
11/03/2102:16
Nickel
pg/L
47.8
96.0
11/03/2102:16
Selenium
pg/L
50.6
101
11/03/2102:16
Silver
pg/L
49.0
98.0
11/03/2102:16
Tin
pg/L
50.2
100
11/03/2102:16
Thallium
pg/L
50.7
101
11/03/2102:16
Vanadium
pg/L
53.9
108
11/03/2102:16
Zinc
pg/L
48.7
97.0
11/03/2102:16
Date: 12/21/2021 12:58 PM Page 11 of 41
Page 71 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V10701 QC Analytical Batch(es): V10908
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Lab Reagent Blank LRB-V10701 Matrix: AQU
Associated Lab Samples: 97854, 97855
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Antimony
pg/L
<0.490
0.490
2.00
10/29/2102:18
Arsenic
pg/L
<0.170
0.170
1.00
10/29/2102:18
Barium
pg/L
<0.810
0.810
10.0
10/29/2102:18
Beryllium
pg/L
<0.190
0.190
1.00
10/29/2102:18
Cadmium
pg/L
<0.160
0.160
1.00
10/29/2102:18
Chromium
pg/L
<0.790
0.790
2.00
10/29/2102:18
Cobalt
pg/L
<0.520
0.520
2.00
10/29/2102:18
Copper
pg/L
<3.80
3.80
10.0
10/29/2102:18
Lead
pg/L
<0.260
0.260
1.00
10/29/2102:18
Nickel
pg/L
<0.510
0.510
3.00
10/29/2102:18
Selenium
pg/L
<0.740
0.740
5.00
10/29/2102:18
Silver
pg/L
<0.110
0.110
1.00
10/29/2102:18
Tin
pg/L
<1.80
1.80
5.00
10/29/2102:18
Thallium
pg/L
<0.570
0.570
2.00
10/29/2102:18
Vanadium
pg/L
2.50
1.30
5.00
10/29/2102:18
Zinc
pg/L
<6.90
6.90
20.0
10/29/2102:18
Laboratory Control Sample
LCS-V10701
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Antimony
pg/L
100
113
113
80-120
Arsenic
pg/L
100
95.3
95.0
80-120
Barium
pg/L
100
99.5
100
80-120
Beryllium
pg/L
100
103
103
80-120
Cadmium
pg/L
100
97.6
98.0
80-120
Chromium
pg/L
100
99.1
99.0
80-120
Cobalt
pg/L
100
99.8
100
80-120
Date:
12/21/2021 12:58 PM
Page 12 of 41
Page 72 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V10701 QC Analytical Batch(es): V10908
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Laboratory Control Sample LCS-V10701
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Copper
pg/L
100
97.3
97.0
80-120
Lead
pg/L
100
98.9
99.0
80-120
Nickel
pg/L
100
97.5
98.0
80-120
Selenium
pg/L
100
97.8
98.0
80-120
Silver
pg/L
100
98.4
98.0
80-120
Tin
pg/L
100
99.3
99.0
80-120
Thallium
pg/L
100
98.1
98.0
80-120
Vanadium
pg/L
100
102
102
80-120
Zinc
pg/L
100
98.4
98.0
80-120
Matrix Spike & Matrix Spike Duplicate
Parameter Units
V 97893-MS-V10701
MS Spike
Result Conc.
V 97893-MSD-V10701
MSD MS Result
Spike
Conc.
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Antimony
pg/L
< 0.490
100
100
116
115
116
115
75-125
0.8
20.0
Arsenic
pg/L
0.394
100
100
96.9
96.2
97.0
96.0
75-125
0.7
20.0
Barium
pg/L
32.1
100
100
133
134
101
102
75-125
0.7
20.0
Beryllium
pg/L
0.196
100
100
100
96.5
100
97.0
75-125
3.5
20.0
Cadmium
pg/L
< 0.160
100
100
100
101
100
101
75-125
0.9
20.0
Chromium
pg/L
< 0.790
100
100
102
101
102
101
75-125
0.9
20.0
Cobalt
pg/L
0.742
100
100
100
101
100
101
75-125
0.9
20.0
Copper
pg/L
< 3.80
100
100
101
100
101
100
75-125
0.9
20.0
Lead
pg/L
1.19
100
100
102
101
101
100
75-125
0.9
20.0
Nickel
pg/L
0.797
100
100
98.3
99.6
98.0
100
75-125
1.3
20.0
Selenium
pg/L
< 0.740
100
100
101
99.7
101
100
75-125
1.2
20.0
Silver
pg/L
< 0.110
100
100
100
99.3
100
99.0
75-125
0.7
20.0
Tin
pg/L
< 1.80
100
100
102
101
102
101
75-125
0.9
20.0
Date: 12/21/2021 12:58 PM Page 13 of 41
Page 73 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-294-8011
QC Prep:
V10701
QC Analytical Batch(es): V10908
QC Prep Batch Method:
3005A
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Matrix Spike & Matrix Spike
Duplicate
V 97893-MS-V10701
V 97893-MSD-V10701
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Thallium
pg/L
< 0.570 100
100 99.5
99.4 100
99.0 75-125 0.1 20.0
Vanadium
pg/L
2.69 100
100 105
104 105
104 75-125 0.9 20.0
Zinc
pg/L
< 6.90 100
100 102
100 102
100 75-125 1.9 20.0
Post Digestion Spike
V 97893-PDS-V10701
PDS
%
Analyzed
Parameter
Units
Result Recovery
Antimony
pg/L
57.1
114
10/29/2102:51
Arsenic
pg/L
50.4
101
10/29/2102:51
Barium
pg/L
65.9
100
10/29/2102:51
Beryllium
pg/L
51.1
102
10/29/2102:51
Cadmium
pg/L
50.9
102
10/29/2102:51
Chromium
pg/L
51.4
103
10/29/2102:51
Cobalt
pg/L
51.6
103
10/29/2102:51
Copper
pg/L
51.2
102
10/29/2102:51
Lead
pg/L
50.8
100
10/29/2102:51
Nickel
pg/L
50.6
101
10/29/2102:51
Selenium
pg/L
50.2
100
10/29/2102:51
Silver
pg/L
50.5
101
10/29/2102:51
Tin
pg/L
50.5
101
10/29/2102:51
Thallium
pg/L
49.9
100
10/29/2102:51
Vanadium
pg/L
53.3
107
10/29/2102:51
Zinc
pg/L
51.6
103
10/29/2102:51
Date: 12/21/2021 12:58 PM Page 14 of 41
Page 74 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V10735 QC Analytical Batch(es): V11081,V11123
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Lab Reagent Blank LRB-V10735 Matrix: AQU
Associated Lab Samples: 97852
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Antimony
pg/L
<0.490
0.490
2.00
11/03/2104:56
Arsenic
pg/L
<0.170
0.170
1.00
11/03/2104:56
Barium
pg/L
<0.810
0.810
10.0
11/03/2104:56
Beryllium
pg/L
<0.190
0.190
1.00
11/03/2120:02
Cadmium
pg/L
<0.160
0.160
1.00
11/03/2104:56
Chromium
pg/L
<0.790
0.790
2.00
11/03/2104:56
Cobalt
pg/L
<0.520
0.520
2.00
11/03/2104:56
Copper
pg/L
<3.80
3.80
10.0
11/03/2104:56
Lead
pg/L
<0.260
0.260
1.00
11/03/2104:56
Nickel
pg/L
<0.510
0.510
3.00
11/03/2104:56
Selenium
pg/L
0.786
0.740
5.00
11/03/2104:56
Silver
pg/L
<0.110
0.110
1.00
11/03/2104:56
Tin
pg/L
<1.80
1.80
5.00
11/03/2104:56
Thallium
pg/L
<0.570
0.570
2.00
11/03/2104:56
Vanadium
pg/L
<1.30
1.30
5.00
11/03/2120:02
Zinc
pg/L
<6.90
6.90
20.0
11/03/2104:56
Laboratory Control Sample
LCS-V10735
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Antimony
pg/L
100
101
101
80-120
Arsenic
pg/L
100
89.9
90.0
80-120
Barium
pg/L
100
97.1
97.0
80-120
Beryllium
pg/L
100
89.7
90.0
80-120
Cadmium
pg/L
100
95.8
96.0
80-120
Chromium
pg/L
100
95.2
95.0
80-120
Cobalt
pg/L
100
93.8
94.0
80-120
Date:
12/21/2021 12:58 PM
Page 15 of 41
Page 75 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V10735 QC Analytical Batch(es): V11081,V11123
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Laboratory Control Sample LCS-V10735
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Copper
pg/L
100
92.8
93.0
80-120
Lead
pg/L
100
96.7
97.0
80-120
Nickel
pg/L
100
92.6
93.0
80-120
Selenium
pg/L
100
90.3
90.0
80-120
Silver
pg/L
100
95.5
96.0
80-120
Tin
pg/L
100
96.0
96.0
80-120
Thallium
pg/L
100
91.9
92.0
80-120
Vanadium
pg/L
100
100
100
80-120
Zinc
pg/L
100
91.4
91.0
80-120
Matrix Spike & Matrix Spike Duplicate
Parameter Units
V 97852-MS-V10735
MS Spike
Result Conc.
V 97852-MSD-V10735
MSD MS Result
Spike
Conc.
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Antimony
pg/L
< 0.490
100
100
103
107
103
107
75-125
3.8
20.0
Arsenic
pg/L
0.181
100
100
90.9
93.3
91.0
93.0
75-125
2.6
20.0
Barium
pg/L
11.9
100
100
109
108
97.0
96.0
75-125
0.9
20.0
Beryllium
pg/L
< 0.190
100
100
94.1
93.4
94.0
93.0
75-125
0.7
20.0
Cadmium
pg/L
< 0.160
100
100
98.5
98.4
99.0
98.0
75-125
0.1
20.0
Chromium
pg/L
< 0.790
100
100
97.9
97.5
98.0
98.0
75-125
0.4
20.0
Cobalt
pg/L
< 0.520
100
100
95.6
96.5
96.0
97.0
75-125
0.9
20.0
Copper
pg/L
< 3.80
100
100
93.8
96.3
94.0
96.0
75-125
2.6
20.0
Lead
pg/L
< 0.260
100
100
99.4
99.2
99.0
99.0
75-125
0.2
20.0
Nickel
pg/L
< 0.510
100
100
95.7
95.6
96.0
96.0
75-125
0.1
20.0
Selenium
pg/L
< 0.740
100
100
90.4
97.1
90.0
97.0
75-125
7.1
20.0
Silver
pg/L
< 0.110
100
100
98.1
98.6
98.0
99.0
75-125
0.5
20.0
Tin
pg/L
< 1.80
100
100
97.0
99.3
97.0
99.0
75-125
2.3
20.0
Date: 12/21/2021 12:58 PM Page 16 of 41
Page 76 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-294-8011
QC Prep:
V10735
QC Analytical Batch(es): V11081,V11123
QC Prep Batch Method:
3005A
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Matrix Spike & Matrix Spike
Duplicate
V 97852-MS-V10735
V 97852-MSD-V10735
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Thallium
pg/L
< 0.570 100
100 95.4
95.7 95.0
96.0 75-125 0.3 20.0
Vanadium
pg/L
3.74 100
100 102
103 102
103 75-125 0.9 20.0
Zinc
pg/L
< 6.90 100
100 93.2
94.8 93.0
95.0 75-125 1.7 20.0
Post Digestion Spike
V 97852-PDS-V10735
PDS
%
Analyzed
Parameter
Units
Result Recovery
Antimony
pg/L
52.0
104
11/03/2105:29
Arsenic
pg/L
46.4
93.0
11/03/2105:29
Barium
pg/L
54.8
98.0
11/03/2105:29
Beryllium
pg/L
47.8
96.0
11/03/2120:35
Cadmium
pg/L
49.6
99.0
11/03/2105:29
Chromium
pg/L
48.8
98.0
11/03/2105:29
Cobalt
pg/L
47.6
95.0
11/03/2105:29
Copper
pg/L
46.6
93.0
11/03/2105:29
Lead
pg/L
50.3
101
11/03/21 05:29
Nickel
pg/L
47.2
94.0
11/03/2105:29
Selenium
pg/L
48.1
96.0
11/03/2105:29
Silver
pg/L
48.9
98.0
11/03/2105:29
Tin
pg/L
51.1
102
11/03/2105:29
Thallium
pg/L
50.5
101
11/03/2105:29
Vanadium
pg/L
53.7
107
11/03/2105:29
Zinc
pg/L
47.7
95.0
11/03/2105:29
Date: 12/21/2021 12:58 PM Page 17 of 41
Page 77 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V11166 QC Analytical Batch(es): V11233,V11240
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Lab Reagent Blank LRB-V11166 Matrix: AQU
Associated Lab Samples: 97855
Parameter
Units
Blank
Result
MDL
MQL
Analyzed
Dissolved Antimony
pg/L
<0.490
0.490
2.00
11/05/21 13:39
Dissolved Arsenic
pg/L
<0.170
0.170
1.00
11/05/21 13:39
Dissolved Barium
pg/L
<0.810
0.810
10.0
11/05/21 13:39
Dissolved Beryllium
pg/L
<0.190
0.190
1.00
11/05/21 13:39
Dissolved Cadmium
pg/L
<0.160
0.160
1.00
11/05/21 13:39
Dissolved Chromium
pg/L
<0.790
0.790
2.00
11/05/21 13:39
Dissolved Cobalt
pg/L
<0.520
0.520
2.00
11/05/21 13:39
Dissolved Copper
pg/L
<3.80
3.80
10.0
11/05/21 13:39
Dissolved Lead
pg/L
<0.260
0.260
1.00
11/05/21 13:39
Dissolved Nickel
pg/L
<0.510
0.510
3.00
11/05/21 13:39
Dissolved Selenium
pg/L
<0.740
0.740
5.00
11/05/21 13:39
Dissolved Silver
pg/L
<0.110
0.110
1.00
11/05/21 13:39
Dissolved Tin
pg/L
<1.80
1.80
5.00
11/05/21 13:39
Dissolved Thallium
pg/L
<0.570
0.570
2.00
11/05/21 13:39
Dissolved Vanadium
pg/L
<1.30
1.30
5.00
11/05/21 13:39
Dissolved Zinc
pg/L
<6.90
6.90
20.0
11/05/21 13:39
Laboratory Control Sample LCS-V11166
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Dissolved Antimony
pg/L
100
100
100
80-120
Dissolved Arsenic
pg/L
100
92.7
93.0
80-120
Dissolved Barium
pg/L
100
101
101
80-120
Dissolved Beryllium
pg/L
100
91.4
91.0
80-120
Dissolved Cadmium
pg/L
100
96.2
96.0
80-120
Dissolved Chromium
pg/L
100
94.7
95.0
80-120
Dissolved Cobalt
pg/L
100
91.9
92.0
80-120
Date: 12/21/2021 12:58 PM Page 18 of 41
Page 78 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V11166 QC Analytical Batch(es): V11233,V11240
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Laboratory Control Sample LCS-V11166
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Dissolved Copper
pg/L
100
91.4
91.0
80-120
Dissolved Lead
pg/L
100
98.3
98.0
80-120
Dissolved Nickel
pg/L
100
90.7
91.0
80-120
Dissolved Selenium
pg/L
100
97.3
97.0
80-120
Dissolved Silver
pg/L
100
94.9
95.0
80-120
Dissolved Tin
pg/L
100
93.4
93.0
80-120
Dissolved Thallium
pg/L
100
96.9
97.0
80-120
Dissolved Vanadium
pg/L
100
94.1
94.0
80-120
Dissolved Zinc
pg/L
100
96.9
97.0
80-120
Matrix Spike & Matrix Spike Duplicate
Parameter Units
V 98018-V11161-MS-V11166
MS Spike MSD
Result Conc. Spike
Conc.
V 98018-VIII61-MSD-VIII66
MS Result MSD MS
Result %Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Dissolved Antimony
pg/L
< 0.490
100
100
106
107
106
107
75-125
0.9
20.0
Dissolved Arsenic
pg/L
< 0.170
100
100
95.7
93.9
96.0
94.0
75-125
1.8
20.0
Dissolved Barium
pg/L
39.2
100
100
286
280
247*
241*
75-125
2.1
20.0
Dissolved Beryllium
pg/L
< 0.190
100
100
95.3
95.5
95.0
96.0
75-125
0.2
20.0
Dissolved Cadmium
pg/L
< 0.160
100
100
101
98.7
101
99.0
75-125
2.3
20.0
Dissolved Chromium
pg/L
< 0.790
100
100
95.4
94.6
95.0
95.0
75-125
0.8
20.0
Dissolved Cobalt
pg/L
19.1
100
100
98.7
96.1
80.0
77.0
75-125
2.6
20.0
Dissolved Copper
pg/L
< 3.80
100
100
95.3
92.4
95.0
92.0
75-125
3.0
20.0
Dissolved Lead
pg/L
< 0.260
100
100
98.6
98.7
99.0
99.0
75-125
0.1
20.0
Dissolved Nickel
pg/L
18.3
100
100
97.1
94.0
79.0
76.0
75-125
3.2
20.0
Dissolved Selenium
pg/L
< 0.740
100
100
102
102
102
102
75-125
0.0
20.0
Dissolved Silver
pg/L
< 0.110
100
100
80.9
80.5
81.0
81.0
75-125
0.4
20.0
Dissolved Tin
pg/L
< 1.80
100
100
95.6
96.6
96.0
97.0
75-125
1.0
20.0
* QC Fail Date: 12/21/2021 12:58 PM Page 19 of 41
Page 79 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-294-8011
QC Prep:
V11166
QC Analytical Batch(es): V11233,V11240
QC Prep Batch Method:
3005A
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Matrix Spike & Matrix Spike
Duplicate
V 98018-V11161-MS-V11166 V 98018-V11161-MSD-V11166
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Dissolved Thallium
pg/L
< 0.570 100
100 98.1
96.9 98.0
97.0 75-125 1.2 20.0
Dissolved Vanadium
pg/L
< 1.30 100
100 95.7
93.4 96.0
93.0 75-125 2.4 20.0
Dissolved Zinc
pg/L
< 6.90 100
100 106
104 106
104 75-125 1.9 20.0
Post Digestion Spike
V 98018-V11161-PDS-V11166
PDS
%
Analyzed
Parameter
Units
Result
Recovery
Dissolved Antimony
pg/L
55.4
111
11/05/21 20:07
Dissolved Arsenic
pg/L
50.7
101
11/05/21 20:07
Dissolved Barium
pg/L
72.8
105
11/05/21 20:07
Dissolved Beryllium
pg/L
47.5
95.0
11/05/21 20:07
Dissolved Cadmium
pg/L
52.3
105
11/05/21 20:07
Dissolved Chromium
pg/L
51.2
102
11/05/21 20:07
Dissolved Cobalt
pg/L
58.9
99.0
11/05/21 20:07
Dissolved Copper
pg/L
48.6
97.0
11/05/21 20:07
Dissolved Lead
pg/L
50.9
102
11/05/21 20:07
Dissolved Nickel
pg/L
58.6
99.0
11/05/21 20:07
Dissolved Selenium
pg/L
52.7
105
11/05/21 20:07
Dissolved Silver
pg/L
51.3
103
11/05/21 20:07
Dissolved Tin
pg/L
51.3
103
11/05/21 20:07
Dissolved Thallium
pg/L
49.8
100
11/05/21 20:07
Dissolved Vanadium
pg/L
50.5
101
11/05/21 20:07
Dissolved Zinc
pg/L
50.9
102
11/05/21 20:07
Date: 12/21/2021 12:58 PM Page 20 of 41
Page 80 of 105

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V10826
QC Analytical Batch(es): V10857
QC Prep Batch Method: 7470A
Analysis Method:
7470A
Analysis Description:
Total Aqueous Mercury Analysis - CVAA
Lab Reagent Blank
LRB-V10826
Matrix: AQU
Associated Lab Samples: 97850, 97851, 97852, 97854, 97855
Blank MDL
MQL
Analyzed
Parameter Units
Result
Mercury (Total) pg/L
<0.0700 0.0700
0.200
10/27/21 18:12
Laboratory Control Sample
LCS-V10826
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Mercury (Total) pg/L
9.38
9.62
103 80-120
Matrix Spike & Matrix Spike Duplicate
V 97687-MS-V10826
V 97687-MSD-V10826
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Mercury (Total) pg/L
<0.0700 9.38
9.38 8.95
8.93 95.0 95.0 80-120 0.2 20
Post Digestion Spike
V 97687-PDS-V10826
PDS
%
Analyzed
Parameter Units
Result
Recovery
Mercury (Total) pg/L
4.51
96.0
10/27/21 18:30
Date: 12/21/2021 12:58 PM Page 21 of 41
Page 81 of 105

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V11199
QC Analytical Batch(es): V11256
QC Prep Batch Method: 7470A
Analysis Method:
7470A
Analysis Description:
Total Aqueous Mercury Analysis - CVAA
Lab Reagent Blank
LRB-V11199
Matrix: AQU
Associated Lab Samples: 97855
Blank MDL
MQL
Analyzed
Parameter Units
Result
Dissolved Mercury pg/L
0.000 0.000
0.200
11/06/21 12:07
Laboratory Control Sample
LCS-V11199
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Dissolved Mercury pg/L
9.38
9.00
96.0 80-120
Matrix Spike & Matrix Spike Duplicate
V 97855-V11161-MS-V11199 V 97855-V11161-MSD-V11199
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Dissolved Mercury pg/L
<0.0700 9.38
9.38 5.76
5.83 61.0* 62.0* 80-120 1.2 20
Post Digestion Spike
V 97855-V11161-PDS-V11199
PDS
%
Analyzed
Parameter Units
Result
Recovery
Dissolved Mercury pg/L
3.70
79.0*
11/06/21 12:22
* QC Fail Date: 12/21/2021 12:58 PM Page 22 of 41
Page 82 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-294-8011
QC Prep:
V10685
QC Analytical Batch(es): V10686
QC Prep Batch Method:
5030B
Analysis Method:
8260D SIM
Analysis Description:
Volatile Organic Compounds -
GC/MS
Lab Reagent Blank
LRB-V10685
Matrix: AQU
Associated Lab Samples:
97850, 97851, 97852, 97854, 97855
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
1,4-Dioxane
pg/L
<0.139 0.139
2.00
10/25/2112:22
4-Bromofluorobenzene (S)
10/25/21 12:22
109
70-130
Laboratory Control Sample
LCS-V10685
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
1,4-Dioxane
pg/L
50.0
49.2
98.4
70-130
4-Bromofluorobenzene (S)
116
70-130
Matrix Spike & Matrix Spike Duplicate
V 97985-MS-V10685
V 97985-MSD-V10685
MS Spike
MSD MS Result
MSD MS
MSD
%Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec
Limits RPD
Conc.
1,4-Dioxane
pg/L
< 0.139 50.0
50.0 49.1
53.0 98.2
106
70-130
4-Bromofluorobenzene (S)
125
116
70-130
Date: 12/21/2021 12:58 PM Page 23 of 41
Page 83 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V10999
QC Prep Batch Method: 5030B
QC Analytical Batch(es): V11000
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V10999 Matrix: AQU
Associated Lab Samples: 97850, 97851, 97852, 97853, 97854, 97855, 97856, 97860
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
pg/L
<1.80
1.80
5.00
11/01/2102:07
Acetonitrile
pg/L
<20.3
20.3
10.0
11/01/2102:07
Acrolein
pg/L
<2.00
2.00
5.00
11/01/2102:07
Acrylonitrile
pg/L
<0.230
0.230
5.00
11/01/2102:07
Allyl Chloride
pg/L
<0.579
0.579
10.0
11/01/2102:07
Benzene
pg/L
<0.180
0.180
0.500
11/01/2102:07
Bromochloromethane
pg/L
<0.420
0.420
1.00
11/01/2102:07
Bromodichloromethane
pg/L
<0.160
0.160
0.500
11/01/2102:07
Bromoform
pg/L
<1.50
1.50
5.00
11/01/2102:07
Bromomethane
pg/L
<0.280
0.280
1.00
11/01/2102:07
Carbon Disulfide
pg/L
<0.150
0.150
5.00
11/01/2102:07
Carbon Tetrachloride
pg/L
<0.180
0.180
0.500
11/01/21 02:07
Chlorobenzene
pg/L
<0.190
0.190
0.500
11/01/2102:07
Chlorodibromomethane
pg/L
<0.190
0.190
0.500
11/01/2102:07
Chloroethane
pg/L
<0.430
0.430
1.00
11/01/2102:07
Chloroform
pg/L
<0.220
0.220
0.500
11/01/2102:07
Chloromethane
pg/L
<0.220
0.220
0.500
11/01/2102:07
Chloroprene
pg/L
<0.450
0.450
10.0
11/01/2102:07
1,2-Dibromo-3-Chloropropane
pg/L
<1.10
1.10
2.00
11/01/2102:07
1,2-Dibromoethane
pg/L
<0.200
0.200
0.500
11/01/2102:07
Dibromomethane
pg/L
<0.230
0.230
0.500
11/01/2102:07
trans-1,4-Dichloro-2-butene
pg/L
< 1.30
1.30
10.0
11/01/21 02:07
1,2-Dichlorobenzene
pg/L
<0.220
0.220
0.500
11/01/2102:07
1,3-Dichlorobenzene
pg/L
<0.190
0.190
0.500
11/01/2102:07
1,4-Dichlorobenzene
pg/L
<0.210
0.210
0.500
11/01/2102:07
Dichlorodifluoromethane
pg/L
<1.20
1.20
5.00
11/01/2102:07
1,1-Dichloroethane
pg/L
<0.240
0.240
0.500
11/01/2102:07
Date:
12/21/2021 12:58 PM
Page 24 of 41
Page 84 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V10999
QC Prep Batch Method: 5030B
QC Analytical Batch(es): V11000
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V10999 Matrix: AQU
Associated Lab Samples: 97850, 97851, 97852, 97853, 97854, 97855, 97856, 97860
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,2-Dichloroethane
pg/L
<0.150
0.150
0.500
11/01/2102:07
1,1-Dichloroethene
pg/L
<0.150
0.150
0.500
11/01/2102:07
cis-1,2-Dichloroethene
pg/L
<0.200
0.200
0.500
11/01/2102:07
trans-1,2-Dichloroethene
pg/L
<0.180
0.180
0.500
11/01/2102:07
1,2-Dichloropropane
pg/L
<0.190
0.190
0.500
11/01/2102:07
1,3-Dichloropropane
pg/L
<0.130
0.130
0.500
11/01/2102:07
2,2-Dichloropropane
pg/L
<0.210
0.210
2.00
11/01/2102:07
1,1-Dichloropropene
pg/L
<0.200
0.200
0.500
11/01/2102:07
cis-1,3-Dichloropropene
pg/L
<0.210
0.210
0.500
11/01/2102:07
trans-1,3-Dichloropropene
pg/L
<0.150
0.150
0.500
11/01/2102:07
Ethyl Methacrylate
pg/L
<1.62
1.62
10.0
11/01/21 02:07
Ethylbenzene
pg/L
<0.170
0.170
0.500
11/01/2102:07
Hexachlorobutadiene
pg/L
<0.350
0.350
2.00
11/01/2102:07
2-Hexanone
pg/L
<0.380
0.380
5.00
11/01/2102:07
Iodomethane
pg/L
<0.054
0.054
0.500
11/01/2102:07
Methyl Ethyl Ketone (MEK)
pg/L
<0.710
0.710
5.00
11/01/2102:07
Methacrylonitrile
pg/L
<12.6
12.6
10.0
11/01/2102:07
4-Methyl-2-Pentanone
pg/L
<1.00
1.00
5.00
11/01/2102:07
Methylene Chloride
pg/L
<0.330
0.330
1.00
11/01/2102:07
Naphthalene
pg/L
<0.470
0.470
1.00
11/01/2102:07
Propionitrile
pg/L
<23.7
23.7
10.0
11/01/2102:07
Styrene
pg/L
<0.220
0.220
0.500
11/01/2102:07
1,1,1,2-Tetrachloroethane
pg/L
<0.160
0.160
0.500
11/01/2102:07
1,1,2,2-Tetrachloroethane
pg/L
<0.160
0.160
0.500
11/01/2102:07
Tetrachloroethene
pg/L
<0.220
0.220
0.500
11/01/2102:07
Tetrahydrofuran
pg/L
<1.50
1.50
10.0
11/01/2102:07
Toluene
pg/L
<0.220
0.220
0.500
11/01/2102:07
Date:
12/21/2021 12:58 PM
Page 25 of 41
Page 85 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep:
V10999
QC Analytical Batch(es): V11000
QC Prep Batch Method:
5030B
Analysis
Method:
8260D
Analysis Description:
Volatile Organic Compounds - GC/MS
Lab Reagent Blank
LRB-V10999
Matrix: AQU
Associated Lab Samples:
97850, 97851, 97852, 97853,
97854, 97855,
97856, 97860
Blank
MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
1,2,4-Trichlorobenzene
pg/L
<0.310
0.310
1.00
11/01/2102:07
1,1,1-Trichloroethane
pg/L
<0.160
0.160
0.500
11/01/2102:07
1,1,2-Trichloroethane
pg/L
<0.096
0.096
0.500
11/01/2102:07
Trichloroethene
pg/L
<0.180
0.180
0.500
11/01/2102:07
Trichlorofluoromethane
pg/L
<0.180
0.180
0.500
11/01/2102:07
1,2,3-Trichloropropane
pg/L
<0.270
0.270
1.00
11/01/2102:07
Vinyl Acetate
pg/L
<1.00
1.00
2.00
11/01/2102:07
Vinyl Chloride
pg/L
<0.170
0.170
0.500
11/01/2102:07
o-Xylene
pg/L
<0.210
0.210
0.500
11/01/2102:07
m,p-Xylene
pg/L
<0.420
0.420
1.00
11/01/2102:07
4-Bromofluorobenzene (S)
11/01/2102:07
100
80-124
Dibromofluoromethane (S)
11/01/2102:07
99.2
75-129
1,2-Dichloroethane - d4 (S)
11/01/2102:07
101
63-136
Toluene-d8 (S)
11/01/2102:07
96.8
77-123
Laboratory Control Sample & LCSD
LCS-V10999 LCSD-V10999
Spike
LCS
LCSD
LCS LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec a/o Rec
Limits
RPD
Max
RPD
Acetone
pg/L
40.0
48.8
49.4
122 124
40-166
1.2
20.0
Acetonitrile
pg/L
20.0
<20.3
<20.3
94.0 84.0
40-160
11.2
20.0
Acrolein
pg/L
40.0
39.8
41.1
99.5 103
70-130
3.2
20.0
Acrylonitrile
pg/L
40.0
46.9
49.3
117 123
81-127
4.9
20.0
Allyl Chloride
pg/L
20.0
19.5
18.7
97.5 93.5
40-160
4.1
20.0
Benzene
pg/L
20.0
24.1
23.7
121 119
77-128
1.6
20.0
Bromochloromethane
pg/L
20.0
24.8
23.5
124 118
78-135
5.3
20.0
Bromodichloromethane
pg/L
20.0
23.7
23.4
119 117
76-138
1.2
20.0
Date: 12/21/2021 12:58 PM Page 26 of 41
Page 86 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V10999 QC Analytical Batch(es): V11000
QC Prep Batch Method: 5030B Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V10999 LCSD-V10999
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Bromoform
pg/L
20.0
22.6
22.6
113
113
71-135
0.0
20.0
Bromomethane
pg/L
20.0
24.6
25.4
123
127
41-168
3.2
20.0
Carbon Disulfide
pg/L
20.0
21.3
20.4
107
102
59-135
4.3
20.0
Carbon Tetrachloride
pg/L
20.0
24.1
23.1
121
116
72-142
4.2
20.0
Chlorobenzene
pg/L
20.0
21.4
20.8
107
104
78-119
2.8
20.0
Chlorodibromomethane
pg/L
20.0
21.9
21.8
110
109
75-134
0.4
20.0
Chloroethane
pg/L
20.0
24.0
23.1
120
116
57-142
3.8
20.0
Chloroform
pg/L
20.0
22.9
22.5
115
113
77-130
1.7
20.0
Chloromethane
pg/L
20.0
24.0
22.9
120
115
47-145
4.6
20.0
Chloroprene
pg/L
20.0
19.4
18.8
97.0
94.0
40-160
3.1
20.0
1,2-Dibromo-3-Chloropropane
pg/L
20.0
21.3
21.5
107
108
63-134
0.9
20.0
1,2-Dibromoethane
pg/L
20.0
21.8
21.4
109
107
77-135
1.8
20.0
Dibromomethane
pg/L
20.0
23.9
24.1
120
121
76-138
0.8
20.0
trans-1,4-Dichloro-2-butene
pg/L
20.0
15.3
16.2
76.5
81.0
70-130
5.7
20.0
1,2-Dichlorobenzene
pg/L
20.0
19.8
19.7
99.0
98.5
78-128
0.5
20.0
1,3-Dichlorobenzene
pg/L
20.0
19.8
19.3
99.0
96.5
77-125
2.5
20.0
1,4-Dichlorobenzene
pg/L
20.0
19.6
19.0
98.0
95.0
75-126
3.1
20.0
Dichlorodifluoromethane
pg/L
20.0
21.2
20.5
106
103
28-163
3.3
20.0
1,1-Dichloroethane
pg/L
20.0
24.8
23.6
124
118
70-130
4.9
20.0
1,2-Dichloroethane
pg/L
20.0
23.2
22.9
116
115
68-131
1.3
20.0
1,1-Dichloroethene
pg/L
20.0
23.4
22.2
117
111
70-154
5.2
20.0
cis-1,2-Dichloroethene
pg/L
20.0
23.2
22.3
116
112
76-141
3.9
20.0
trans-1,2-Dichloroethene
pg/L
20.0
23.7
22.6
119
113
76-135
4.7
20.0
1,2-Dichloropropane
pg/L
20.0
23.4
23.1
117
116
77-130
1.2
20.0
1,3-Dichloropropane
pg/L
20.0
21.7
21.5
109
108
76-132
0.9
20.0
2,2-Dichloropropane
pg/L
20.0
21.1
20.6
106
103
29-149
2.3
20.0
Date: 12/21/2021 12:58 PM Page 27 of 41
Page 87 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: V10999 QC Analytical Batch(es): V11000
QC Prep Batch Method: 5030B Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V10999 LCSD-V10999
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
1,1-Dichloropropene
pg/L
20.0
24.0
22.9
120
115
71-136
4.6
20.0
cis-1,3-Dichloropropene
pg/L
20.0
23.6
23.1
118
116
65-140
2.1
20.0
trans-1,3-Dichloropropene
pg/L
20.0
23.3
23.0
117
115
67-140
1.2
20.0
Ethyl Methacrylate
pg/L
20.0
20.0
19.1
100
95.5
40-160
4.6
20.0
Ethylbenzene
pg/L
20.0
21.7
20.8
109
104
80-127
4.2
20.0
Hexachlorobutadiene
pg/L
20.0
21.8
19.8
109
99.0
61-134
9.6
20.0
2-Hexanone
pg/L
20.0
22.2
23.1
111
116
64-137
3.9
20.0
Iodomethane
pg/L
20.0
18.8
19.3
94.0
96.5
70-130
2.6
20.0
Methyl Ethyl Ketone (MEK)
pg/L
20.0
22.5
22.9
113
115
71-134
1.7
20.0
Methacrylonitrile
pg/L
20.0
24.8
25.1
124
126
40-160
1.2
20.0
4-Methyl-2-Pentanone
pg/L
20.0
24.7
24.9
124
125
69-134
0.8
20.0
Methylene Chloride
pg/L
20.0
23.2
22.5
116
113
73-131
3.0
20.0
Naphthalene
pg/L
20.0
20.7
19.8
104
99.0
64-136
4.4
20.0
Propionitrile
pg/L
20.0
<23.7
<23.7
102
95.0
40-160
7.1
20.0
Styrene
pg/L
20.0
22.3
21.9
112
110
78-129
1.8
20.0
1,1,1,2-Tetrachloroethane
pg/L
20.0
21.5
21.2
108
106
79-134
1.4
20.0
1,1,2,2-Tetrachloroethane
pg/L
20.0
19.0
18.7
95.0
93.5
62-127
1.5
20.0
Tetrachloroethene
pg/L
20.0
21.1
20.7
106
104
80-129
1.9
20.0
Tetrahydrofuran
pg/L
20.0
23.4
22.3
117
112
70-130
4.8
20.0
Toluene
pg/L
20.0
23.9
23.2
120
116
76-131
2.9
20.0
1,2,4-Trichlorobenzene
pg/L
20.0
21.0
20.3
105
102
66-139
3.3
20.0
1,1,1-Trichloroethane
pg/L
20.0
24.4
23.0
122
115
75-135
5.9
20.0
1,1,2-Trichloroethane
pg/L
20.0
23.4
23.7
117
119
70-140
1.2
20.0
Trichloroethene
pg/L
20.0
25.2
24.4
126
122
77-133
3.2
20.0
Trichlorofluoromethane
pg/L
20.0
23.8
23.4
119
117
62-148
1.6
20.0
1,2,3-Trichloropropane
pg/L
20.0
19.7
19.4
98.5
97.0
71-127
1.5
20.0
Date: 12/21/2021 12:58 PM Page 28 of 41
Page 88 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-294-8011
QC Prep:
V10999
QC Analytical Batch(es): V11000
QC Prep Batch Method:
5030B
Analysis Method:
8260D
Analysis Description:
Volatile Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V10999 LCSD-V10999
Spike
LCS LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result Result
%Rec
% Rec
Limits
RPD
Max
RPD
Vinyl Acetate
pg/L
20.0
18.8 18.4
94.0
92.0
34-167
2.1
20.0
Vinyl Chloride
pg/L
20.0
23.0 22.3
115
112
57-141
3.0
20.0
o-Xylene
pg/L
20.0
21.8 21.3
109
107
78-128
2.3
20.0
m,p-Xylene
pg/L
40.0
46.0 43.8
115
110
77-133
4.8
20.0
4-Bromofluorobenzene (S)
96.4
96.0
80-124
Dibromofluoromethane (S)
96.6
96.8
75-129
1,2-Dichloroethane - d4 (S)
94.4
95.4
63-136
Toluene-d8(S)
92.2
90.4
77-123
Date: 12/21/2021 12:58 PM Page 29 of 41
Page 89 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: L580965
QC Prep Batch Method: 3510C
Lab Reagent Blank
LRB-L580965
Associated Lab Samples:
97850, 97858, 97859
Blank
MDL
Parameter
Units
Result
Dimethoate
pg/L
<0.713
0.713
Disulfoton
pg/L
<0.466
0.466
Ethyl Parathion
pg/L
<0.568
0.568
Famphur
pg/L
<0.512
0.512
Methyl Parathion
pg/L
<0.805
0.805
Phorate
pg/L
<0.659
0.659
Tributyl phosphate (S)
Triphenyl phosphate (S)
Laboratory Control Sample & LCSD LCS-L580965 L
Spike
Parameter Units Conc.
QC Analytical Batch(es): L581161
Analysis Method: 8270C
Analysis Description: Organophosphorus Pesticides by GC/MS
Matrix: AQU
MQL
Analyzed
0/0
Recovery
1.00
10/25/21 18:37
1.00
10/25/21 18:37
1.00
10/25/21 18:37
1.00
10/25/21 18:37
1.00
10/25/21 18:37
1.00
10/25/21 18:37
10/25/21 18:37
67.0
10/25/21 18:37
68.5
CSD-L580965
LCS LCSD LCS LCSD % Rec
Result Result %Rec % Rec Limits
Dimethoate
pg/L
20.0
11.1
11.4
55.5
57.0
40-140
Disulfoton
pg/L
20.0
12.9
13.1
64.5
65.5
40-140
Ethyl Parathion
pg/L
20.0
13.7
13.0
68.5
65.0
40-140
Famphur
pg/L
20.0
18.5
15.9
92.5
79.5
40-140
Methyl Parathion
pg/L
20.0
13.7
13.9
68.5
69.5
40-140
Phorate
pg/L
20.0
14.1
14.0
70.5
70.0
40-140
Tributyl phosphate (S)
72.0
71.5
50-150
Triphenyl phosphate (S)
80.0
65.5
50-150
Rec
Limits
50-150
50-150
RPD Max
RPD
2.6 20.0
1.5 20.0
5.2 20.0
15.1 20.0
1.4 20.0
0.7 20.0
Date: 12/21/2021 12:58 PM
Page 90 of 105
Page 30 of 41

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: L580969
QC Prep Batch Method: 3510C
Lab Reagent Blank LRB-L580969
Associated Lab Samples: 97850, 97858, 97859
QC Analytical Batch(es): L581160
Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix: AQU
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,3-Dinitrobenzene
pg/L
<0.904
0.904
10.0
10/25/21 15:48
Acenaphthene
pg/L
<0.422
0.422
2.00
10/25/21 15:48
Acenaphthylene
pg/L
<0.429
0.429
2.00
10/25/21 15:48
Acetophenone
pg/L
<0.686
0.686
5.00
10/25/21 15:48
Anthracene
pg/L
<0.467
0.467
2.00
10/25/21 15:48
Benzo(a)anthracene
pg/L
<0.427
0.427
2.00
10/25/21 15:48
Benzo(a)pyrene
pg/L
<1.00
1.00
2.00
10/25/21 15:48
Benzo(b)fluoranthene
pg/L
<0.941
0.941
2.00
10/25/21 15:48
Benzo(g,h,i)perylene
pg/L
<1.36
1.36
2.00
10/25/21 15:48
Benzo(k)fluoranthene
pg/L
<0.752
0.752
2.00
10/25/21 15:48
Benzyl alcohol
pg/L
<3.01
3.01
10.0
10/25/21 15:48
Bis(2-Chloroethoxy)methane
pg/L
<0.433
0.433
5.00
10/25/21 15:48
Bis(2-Chloroethyl)ether
pg/L
<0.447
0.447
5.00
10/25/21 15:48
Bis(2-Chloroisopropyl)ether
pg/L
<0.546
0.546
5.00
10/25/21 15:48
Bis(2-ethylhexyl)phthalate
pg/L
<3.66
3.66
5.00
10/25/21 15:48
4-Bromophenyl phenyl ether
pg/L
<0.500
0.500
5.00
10/25/21 15:48
Butyl benzyl phthalate
pg/L
<4.59
4.59
5.00
10/25/21 15:48
4-Chloro-3-methylphenol
pg/L
<0.503
0.503
5.00
10/25/21 15:48
4-Chloroaniline
pg/L
<0.526
0.526
5.00
10/25/21 15:48
Chlorobenzilate
pg/L
<1.90
1.90
5.00
10/25/21 15:48
2-Chloronaphthalene
pg/L
<0.476
0.476
5.00
10/25/21 15:48
2-Chlorophenol
pg/L
<0.736
0.736
5.00
10/25/21 15:48
4-Chlorophenyl phenyl ether
pg/L
<0.479
0.479
5.00
10/25/21 15:48
Chrysene
pg/L
<0.731
0.731
2.00
10/25/21 15:48
Dibenz(a,h)anthracene
pg/L
<0.252
0.252
2.00
10/25/21 15:48
Dibenzofuran
pg/L
<0.423
0.423
5.00
10/25/21 15:48
1,2-Dichlorobenzene
pg/L
<0.629
0.629
5.00
10/25/21 15:48
Date:
12/21/2021 12:58 PM
Page 31 of 41
Page 91 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: L580969
QC Prep Batch Method: 3510C
Lab Reagent Blank LRB-L580969
Associated Lab Samples: 97850, 97858, 97859
QC Analytical Batch(es): L581160
Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix: AQU
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,3-Dichlorobenzene
pg/L
<0.491
0.491
5.00
10/25/21 15:48
1,4-Dichlorobenzene
pg/L
<0.580
0.580
5.00
10/25/21 15:48
3,3'-Dichlorobenzidine
pg/L
<3.74
3.74
10.0
10/25/21 15:48
2,4-Dichlorophenol
pg/L
<1.52
1.52
5.00
10/25/21 15:48
2,6-Dichlorophenol
pg/L
<0.703
0.703
5.00
10/25/21 15:48
Diethyl phthalate
pg/L
<0.585
0.585
5.00
10/25/21 15:48
Dimethyl phthalate
pg/L
<0.510
0.510
5.00
10/25/21 15:48
3,3' Dimethylbenzidine
pg/L
<1.88
1.88
10.0
10/25/21 15:48
2,4-Dimethylphenol
pg/L
<0.674
0.674
5.00
10/25/21 15:48
Di-n-butyl phthalate
pg/L
<1.58
1.58
5.00
10/25/21 15:48
4,6- Din itro-2-methylphenol
pg/L
<3.47
3.47
10.0
10/25/21 15:48
2,4-Dinitrophenol
pg/L
<4.85
4.85
10.0
10/25/21 15:48
2,4-Dinitrotoluene
pg/L
<0.403
0.403
5.00
10/25/21 15:48
2,6-Dinitrotoluene
pg/L
<0.413
0.413
5.00
10/25/21 15:48
Di-n-Octyl Phthalate
pg/L
<1.72
1.72
5.00
10/25/21 15:48
Ethyl methanesulfonate
pg/L
<0.714
0.714
5.00
10/25/21 15:48
Fluoranthene
pg/L
<0.406
0.406
2.00
10/25/21 15:48
Fluorene
pg/L
<0.444
0.444
2.00
10/25/21 15:48
Hexachlorobenzene
pg/L
<2.57
2.57
5.00
10/25/21 15:48
Hexachlorobutadiene
pg/L
<0.405
0.405
5.00
10/25/21 15:48
Hexachlorocyclopentadiene
pg/L
<2.34
2.34
5.00
10/25/21 15:48
Hexachloroethane
pg/L
<0.277
0.277
5.00
10/25/21 15:48
Indeno(1,2,3-cd)pyrene
pg/L
<1.01
1.01
2.00
10/25/21 15:48
Isophorone
pg/L
<0.360
0.360
5.00
10/25/21 15:48
Methyl methanesulfonate
pg/L
<0.618
0.618
5.00
10/25/21 15:48
2-Methylnaphthalene
pg/L
<0.485
0.485
2.00
10/25/21 15:48
2-Methylphenol
pg/L
<0.721
0.721
5.00
10/25/21 15:48
Date:
12/21/2021 12:58 PM
Page 32 of 41
Page 92 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: L580969 QC Analytical Batch(es): L581160
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-L580969 Matrix: AQU
Associated Lab Samples: 97850, 97858, 97859
Blank
MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
3&4 Methylphenol
pg/L
<0.691
0.691
5.00
10/25/21 15:48
Naphthalene
pg/L
<0.484
0.484
2.00
10/25/21 15:48
2-Nitroaniline
pg/L
<0.574
0.574
5.00
10/25/21 15:48
3-Nitroaniline
pg/L
<1.53
1.53
10.0
10/25/21 15:48
4-Nitroaniline
pg/L
<0.740
0.740
5.00
10/25/21 15:48
Nitrobenzene
pg/L
<0.531
0.531
5.00
10/25/21 15:48
2-Nitrophenol
pg/L
<0.606
0.606
5.00
10/25/21 15:48
4-Nitrophenol
pg/L
<1.39
1.39
10.0
10/25/21 15:48
N-Nitrosodimethylamine
pg/L
<0.249
0.249
5.00
10/25/21 15:48
N-Nitrosodiphenylamine
pg/L
<0.783
0.783
10.0
10/25/21 15:48
N-Nitrosodiethylamine
pg/L
<0.400
0.400
5.00
10/25/21 15:48
N-Nitroso-di-n-butylamine
pg/L
<0.752
0.752
5.00
10/25/21 15:48
N-Nitroso-di-n-propylamine
pg/L
<0.334
0.334
5.00
10/25/21 15:48
Pentachloronitrobenzene
pg/L
<1.15
1.15
5.00
10/25/21 15:48
Pentachlorophenol
pg/L
<2.45
2.45
10.0
10/25/21 15:48
Phenacetin
pg/L
<1.28
1.28
5.00
10/25/21 15:48
Phenanthrene
pg/L
<0.464
0.464
2.00
10/25/21 15:48
Phenol
pg/L
<0.389
0.389
5.00
10/25/21 15:48
Pyrene
pg/L
<1.04
1.04
2.00
10/25/21 15:48
1,2,4,5-Tetrachlorobenzene
pg/L
<0.317
0.317
5.00
10/25/21 15:48
2,3,4,6-Tetrachlorophenol
pg/L
<0.355
0.355
5.00
10/25/21 15:48
1,2,4-Trichlorobenzene
pg/L
<0.482
0.482
5.00
10/25/21 15:48
2,4,5-Trichlorophenol
pg/L
<0.350
0.350
5.00
10/25/21 15:48
2,4,6-Trichlorophenol
pg/L
<0.344
0.344
5.00
10/25/21 15:48
2-Fluorobiphenyl(S)
10/25/21 15:48
55.2
24-93
2-Fluorophenol(S)
10/25/21 15:48
20.7
10-44
Nitrobenzene-d5 (S)
10/25/21 15:48
57.1
20-91
Date:
12/21/2021 12:58 PM
Page 33 of 41
Page 93 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-294-8011
QC Prep:
L580969
QC Analytical Batch(es): L581160
QC Prep Batch Method:
3510C
Analysis Method:
8270D
Analysis Description:
Semivolatile
Organic Compounds -
GC/MS
Lab Reagent Blank
LRB-L580969
Matrix: AQU
Associated Lab Samples: 97850, 97858, 97859
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
Phenol-d6 (S)
10/25/21 15:48
14.8
7-32
4-Terphenyl-d14 (S)
10/25/21 15:48
94.0
35-126
2,4,6-Tribromophenol (S)
10/25/21 15:48
72.2
39-110
Laboratory Control Sample & LCSD
LCS-1-580969 LCSD-L580969
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
1,3-Dinitrobenzene
pg/L
50.0
44.2
41.6
88.4
83.2
45-135
6.0
20.0
Acenaphthene
pg/L
50.0
33.4
30.5
66.8
61.0
38-117
9.0
20.0
Acenaphthylene
pg/L
50.0
29.6
27.9
59.2
55.8
37-114
5.9
20.0
Acetophenone
pg/L
50.0
26.8
25.8
53.6
51.6
25-108
3.8
20.0
Anthracene
pg/L
50.0
43.0
38.0
86.0
76.0
34-128
12.3
20.0
Benzo(a)anthracene
pg/L
50.0
44.7
39.1
89.4
78.2
36-127
13.3
20.0
Benzo(a)pyrene
pg/L
50.0
46.9
40.0
93.8
80.0
34-131
15.8
20.0
Benzo(b)fluoranthene
pg/L
50.0
46.3
42.3
92.6
84.6
36-131
9.0
20.0
Benzo(g,h,i)perylene
pg/L
50.0
41.3
39.9
82.6
79.8
26-123
3.4
20.0
Benzo(k)fluoranthene
pg/L
50.0
56.1
43.4
112
86.8
32-132
25.5*
20.0
Benzyl alcohol
pg/L
50.0
19.5
17.6
39.0
35.2
20-109
10.2
20.0
Bis(2-Chloroethoxy)methane
pg/L
50.0
30.2
27.1
60.4
54.2
20-126
10.8
20.0
Bis(2-Chloroethyl)ether
pg/L
50.0
23.0
22.1
46.0
44.2
16-122
3.9
20.0
Bis(2-Chloroisopropyl)ether
pg/L
50.0
19.3
18.5
38.6
37.0
28-108
4.2
20.0
Bis(2-ethylhexyl)phthalate
pg/L
50.0
42.8
39.5
85.6
79.0
21-162
8.0
20.0
4-Bromophenyl phenyl ether
pg/L
50.0
45.7
41.0
91.4
82.0
31-124
10.8
20.0
Butyl benzyl phthalate
pg/L
50.0
47.7
43.8
95.4
87.6
33-142
8.5
20.0
4-Chloro-3-methyl phenol
pg/L
50.0
31.4
27.9
62.8
55.8
35-117
11.8
20.0
4-Chloroaniline
pg/L
50.0
28.1
25.1
56.2
50.2
24-127
11.2
20.0
* QC Fail Date: 12/21/2021 12:58 PM Page 34 of 41
Page 94 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: L580969 QC Analytical Batch(es): L581160
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-L580969 LCSD-L580969
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Chlorobenzilate
pg/L
50.0
51.3
48.0
103
96.0
35-118
6.6
20.0
2-Chloronaphthalene
pg/L
50.0
31.6
29.0
63.2
58.0
29-137
8.5
20.0
2-Chlorophenol
pg/L
50.0
20.8
19.4
41.6
38.8
27-102
6.9
20.0
4-Chlorophenyl phenyl ether
pg/L
50.0
40.5
36.4
81.0
72.8
39-110
10.6
20.0
Chrysene
pg/L
50.0
39.5
35.4
79.0
70.8
30-124
10.9
20.0
Dibenz(a,h)anthracene
pg/L
50.0
39.7
38.8
79.4
77.6
27-124
2.2
20.0
Dibenzofuran
pg/L
50.0
36.4
34.6
72.8
69.2
40-108
5.0
20.0
1,2-Dichlorobenzene
pg/L
50.0
23.1
22.3
46.2
44.6
26-100
3.5
20.0
1,3-Dichlorobenzene
pg/L
50.0
22.1
21.3
44.2
42.6
21-102
3.6
20.0
1,4-Dichlorobenzene
pg/L
50.0
22.3
21.5
44.6
43.0
24-99
3.6
20.0
3,3'-Dichlorobenzidine
pg/L
150
170
139
113
92.6
6-192
20.0*
20.0
2,4-Dichlorophenol
pg/L
50.0
22.9
20.2
45.8
40.4
32-110
12.5
20.0
2,6-Dichlorophenol
pg/L
50.0
31.3
28.2
62.6
56.4
25-112
10.4
20.0
Diethyl phthalate
pg/L
50.0
44.1
39.8
88.2
79.6
36-130
10.2
20.0
Dimethyl phthalate
pg/L
50.0
41.6
38.9
83.2
77.8
34-123
6.7
20.0
3,3' Dimethylbenzidine
pg/L
200
97.6
87.2
48.8
43.6
6-192
11.2
20.0
2,4-Dimethylphenol
pg/L
50.0
27.5
24.7
55.0
49.4
34-105
10.7
20.0
Di-n-butyl phthalate
pg/L
50.0
45.8
41.3
91.6
82.6
19-158
10.3
20.0
4,6- Din itro-2-methylphenol
pg/L
50.0
60.2
57.8
120
116
27-128
4.0
20.0
2,4-Dinitrophenol
pg/L
150
117
114
78.0
76.0
10-132
2.5
20.0
2,4-Dinitrotoluene
pg/L
50.0
43.0
40.0
86.0
80.0
24-147
7.2
20.0
2,6-Dinitrotoluene
pg/L
50.0
43.1
40.1
86.2
80.2
36-125
7.2
20.0
Di-n-Octyl Phthalate
pg/L
50.0
45.1
37.9
90.2
75.8
29-136
17.3
20.0
Ethyl methanesulfonate
pg/L
50.0
24.7
23.2
49.4
46.4
20-121
6.2
20.0
Fluoranthene
pg/L
50.0
44.1
38.8
88.2
77.6
28-127
12.7
20.0
Fluorene
pg/L
50.0
38.5
35.3
77.0
70.6
41-116
8.6
20.0
* QC Fail Date: 12/21/2021 12:58 PM Page 35 of 41
Page 95 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: L580969 QC Analytical Batch(es): L581160
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-L580969 LCSD-L580969
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Hexachlorobenzene
pg/L
50.0
48.8
44.3
97.6
88.6
18-136
9.6
20.0
Hexachlorobutadiene
pg/L
50.0
27.0
24.2
54.0
48.4
22-109
10.9
20.0
Hexachlorocyclopentadiene
pg/L
50.0
7.50
7.04
15.0
14.0
10-102
6.3
20.0
Hexachloroethane
pg/L
50.0
22.5
21.6
45.0
43.2
16-107
4.0
20.0
Indeno(1,2,3-cd)pyrene
pg/L
50.0
39.8
40.2
79.6
80.4
22-126
1.0
20.0
Isophorone
pg/L
50.0
22.1
20.0
44.2
40.0
31-116
9.9
20.0
Methyl methanesulfonate
pg/L
50.0
14.4
13.7
28.8
27.4
15-82
4.9
20.0
2-Methylnaphthalene
pg/L
50.0
30.0
26.8
60.0
53.6
34-108
11.2
20.0
2-Methylphenol
pg/L
50.0
18.5
17.3
37.0
34.6
22-97
6.7
20.0
3&4 Methylphenol
pg/L
50.0
19.3
17.9
38.6
35.8
21-96
7.5
20.0
Naphthalene
pg/L
50.0
28.5
27.0
57.0
54.0
33-108
5.4
20.0
2-Nitroaniline
pg/L
50.0
41.0
37.8
82.0
75.6
32-127
8.1
20.0
3-Nitroaniline
pg/L
50.0
34.5
31.5
69.0
63.0
28-142
9.0
20.0
4-Nitroaniline
pg/L
50.0
46.9
43.5
93.8
87.0
23-139
7.5
20.0
Nitrobenzene
pg/L
50.0
26.7
25.0
53.4
50.0
27-117
6.5
20.0
2-Nitrophenol
pg/L
50.0
28.9
26.7
57.8
53.4
25-114
7.9
20.0
4-Nitrophenol
pg/L
50.0
17.2
15.4
34.4
30.8
1-76
11.0
20.0
N-Nitrosodimethylamine
pg/L
50.0
12.5
12.2
25.0
24.4
14-84
2.4
20.0
N-Nitrosodiphenylamine
pg/L
50.0
35.6
32.4
71.2
64.8
45-135
9.4
20.0
N-Nitrosodiethylamine
pg/L
50.0
24.1
23.1
48.2
46.2
25-107
4.2
20.0
N-Nitroso-di-n-butylamine
pg/L
50.0
30.3
27.0
60.6
54.0
25-126
11.5
20.0
N-Nitroso-di-n-propylamine
pg/L
50.0
25.9
23.6
51.8
47.2
29-114
9.2
20.0
Pentachloronitrobenzene
pg/L
50.0
50.9
45.7
102
91.4
34-135
10.7
20.0
Pentachlorophenol
pg/L
50.0
55.0
49.1
110
98.2
17-142
11.3
20.0
Phenacetin
pg/L
50.0
42.1
37.7
84.2
75.4
29-141
11.0
20.0
Phenanthrene
pg/L
50.0
44.5
40.7
89.0
81.4
40-120
8.9
20.0
Date: 12/21/2021 12:58 PM Page 36 of 41
Page 96 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: L580969 QC Analytical Batch(es): L581160
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-L580969 LCSD-L580969
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max
RPD
Phenol
pg/L
50.0
7.92
7.40
15.8
14.8
11-55
6.7
20.0
Pyrene
pg/L
50.0
53.8
52.0
108
104
20-154
3.4
20.0
1,2,4,5-Tetrachlorobenzene
pg/L
50.0
31.8
30.3
63.6
60.6
28-110
4.8
20.0
2,3,4,6-Tetrachlorophenol
pg/L
50.0
38.4
35.4
76.8
70.8
28-118
8.1
20.0
1,2,4-Trichlorobenzene
pg/L
50.0
27.3
24.9
54.6
49.8
23-106
9.1
20.0
2,4,5-Trichlorophenol
pg/L
50.0
36.3
34.5
72.6
69.0
26-118
5.0
20.0
2,4,6-Trichlorophenol
pg/L
50.0
38.2
34.4
76.4
68.8
26-115
10.4
20.0
2-Fluorobiphenyl (S)
53.8
51.1
24-93
2-Fluorophenol (S)
18.5
18.1
10-44
Nitrobenzene-d5 (S)
51.9
49.0
20-91
Phenol-d6 (S)
14.7
13.7
7-32
4-Terphenyl-d14(S)
107
102
35-126
2,4,6-Tribromophenol (S)
90.8
80.6
39-110
Date: 12/21/2021 12:58 PM Page 37 of 41
Page 97 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: L580970 QC Analytical Batch(es): L581162
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: 8270 Extended List
Lab Reagent Blank LRB-L580970 Matrix: AQU
Associated Lab Samples: 97850, 97858, 97859
Blank MDL MQL Analyzed
Parameter Units Result
1,3,5-Trinitrobenzene
pg/L
<10.0
10.0
10.0
10/25/2115:48
Isodrin
pg/L
<10.0
10.0
10.0
10/25/2115:48
Kepone
pg/L
<10.0
10.0
10.0
10/25/21 15:48
1,4-Naphthoquinone
pg/L
<10.0
10.0
10.0
10/25/2115:48
1-Naphthylamine
pg/L
<10.0
10.0
10.0
10/25/2115:48
2-Acetylaminofluorene
pg/L
<10.0
10.0
10.0
10/25/2115:48
2-Naphthylamine
pg/L
<10.0
10.0
10.0
10/25/2115:48
3-Methylcholanthrene
pg/L
<10.0
10.0
10.0
10/25/2115:48
4-Aminobiphenyl
pg/L
<10.0
10.0
10.0
10/25/2115:48
5-Nitro-o-toluidine
pg/L
<10.0
10.0
10.0
10/25/2115:48
7,12-Di methyl benz(a)anth racene
pg/L
<10.0
10.0
10.0
10/25/2115:48
Diallate
pg/L
<10.0
10.0
10.0
10/25/2115:48
Hexachloropropene
pg/L
<10.0
10.0
10.0
10/25/2115:48
Isosafrole
pg/L
<10.0
10.0
10.0
10/25/2115:48
Methapyrilene
pg/L
<10.0
10.0
20.0
10/25/2115:48
N-Nitrosomethylethylamine
pg/L
<10.0
10.0
10.0
10/25/2115:48
N-Nitrosomorpholine
pg/L
<10.0
10.0
10.0
10/25/2115:48
N-Nitrosopiperidine
pg/L
<10.0
10.0
10.0
10/25/2115:48
N-Nitrosopyrrolidine
pg/L
<10.0
10.0
10.0
10/25/2115:48
o-Toluidine
pg/L
<10.0
10.0
10.0
10/25/2115:48
p-Dimethylaminoazobenzene
pg/L
<10.0
10.0
10.0
10/25/2115:48
p-Phenylenediamine
pg/L
<10.0
10.0
10.0
10/25/2115:48
Pronamide
pg/L
<10.0
10.0
10.0
10/25/2115:48
Safrole
pg/L
<10.0
10.0
10.0
10/25/2115:48
Date: 12/21/2021 12:58 PM Page 38 of 41
Page 98 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-294-8011
QC Prep: L580970 QC Analytical Batch(es): L581162
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: 8270 Extended List
Laboratory Control Sample & LCSD LCS-L580970 LCSD-L580970
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
1,3,5-Trinitrobenzene
pg/L
50.0
38.1
32.8
76.2
65.6
20-120
14.9
20.0
Isodrin
pg/L
50.0
38.4
36.9
76.8
73.8
20-120
3.9
20.0
Kepone
pg/L
50.0
45.1
45.2
90.2
90.4
20-120
0.2
20.0
1,4-Naphthoquinone
pg/L
50.0
22.1
20.2
44.2
40.4
20-120
8.9
20.0
1-Naphthylamine
pg/L
50.0
10.7
10.2
21.4
20.4
20-120
4.7
20.0
2-Acetylaminofluorene
pg/L
50.0
31.7
32.1
63.4
64.2
20-120
1.2
20.0
2-Naphthylamine
pg/L
50.0
10.0
<10.0
20.0
0.0*
20-120
0.0
20.0
3-Methylcholanthrene
pg/L
50.0
32.0
32.7
64.0
65.4
20-120
2.1
20.0
4-Aminobiphenyl
pg/L
50.0
18.0
17.0
36.0
34.0
20-120
5.7
20.0
5-Nitro-o-toluidine
pg/L
50.0
31.7
29.2
63.4
58.4
20-120
8.2
20.0
7,12-Di methyl benz(a)anth racene
pg/L
50.0
37.6
32.3
75.2
64.6
20-120
15.1
20.0
Diallate
pg/L
50.0
31.3
32.5
62.6
65.0
20-120
3.7
20.0
Hexachloropropene
pg/L
50.0
<10.0
<10.0
0.0*
0.0*
20-120
0.0
20.0
Isosafrole
pg/L
50.0
29.1
27.2
58.2
54.4
20-120
6.7
20.0
Methapyrilene
pg/L
50.0
38.3
50.9
76.6
102
20-120
28.2*
20.0
N-Nitrosomethylethylamine
pg/L
50.0
16.4
15.6
32.8
31.2
20-120
5.0
20.0
N-Nitrosomorpholine
pg/L
50.0
19.2
18.7
38.4
37.4
20-120
2.6
20.0
N-Nitrosopiperidine
pg/L
50.0
22.1
21.8
44.2
43.6
20-120
1.3
20.0
N-Nitrosopyrrolidine
pg/L
50.0
21.6
21.3
43.2
42.6
20-120
1.3
20.0
o-Toluidine
pg/L
50.0
19.2
19.4
38.4
38.8
20-120
1.0
20.0
p-Dimethylaminoazobenzene
pg/L
50.0
38.6
41.3
77.2
82.6
20-120
6.7
20.0
p-Phenylenediamine
pg/L
50.0
<10.0
<10.0
0.0*
0.0*
20-120
0.0
20.0
Pronamide
pg/L
50.0
37.7
36.0
75.4
72.0
20-120
4.6
20.0
Safrole
pg/L
50.0
24.9
24.1
49.8
48.2
20-120
3.2
20.0
* QC Fail Date: 12/21/2021 12:58 PM Page 39 of 41
Page 99 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-294-8011
QC Prep:
V10654
QC Analytical Batch(es): V10700
QC Prep Batch Method:
SW-9056A (PREP)
Analysis Method:
9056A
Analysis Description:
Anions by Ion Chromatography
Lab Reagent Blank
LRB-V10654
Matrix: AQU
Associated Lab Samples:
97850, 97854, 97855
Blank MDL
MQL
Analyzed
Parameter
Units
Result
Chloride
pg/L
<370 370
1000
10/21/21 16:32
Nitrate (NO3-N)
pg/L
<76.0 76.0
200
10/21/21 16:32
Sulfate
pg/L
664 540
1000
10/21/21 16:32
Laboratory Control Sample
LCS-V10654
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Chloride
pg/L
40000
39800
100
80-120
Nitrate (NO3-N)
pg/L
4000
3770
94.0
80-120
Sulfate
pg/L
40000
42000
105
80-120
Matrix Spike & Matrix Spike Duplicate
V 97849-MS-V10654
V 97849-MSD-V10654
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Chloride
pg/L
500000 40000
40000 564000
607000 160*
268* 80-120 7.3 20
* QC Fail Date: 12/21/2021 12:58 PM Page 40 of 41
Page 100 of 105

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-294-8011
QC Analytical Batch:
V10584
Analysis Method:
SM-3500-Fe-13
Analysis Description:
Ferrous Iron
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples:
97850, 97854, 97855
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Ferrous Iron
pg/L
<50.0
50.0
200
10/21/21 16:01
Laboratory Control Sample
LCS
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Ferrous Iron
pg/L
2000
1930
97.0
90-110
Matrix Spike & Matrix Spike Duplicate
V 97850-MS V 97850-MSD
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result
Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Ferrous Iron
pg/L
370
2000
2000 2880
2830 125*
123* 80-120 1.7 20
* QC Fail Date: 12/21/2021 12:58 PM Page 41 of 41
Page 101 of 105

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01015
Customer Name: Anchor QEA of North Carolina, PLLC
Report Number: 21-294-8011
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client # Courier
0 Other:
Thermometer ID:
IRT-15 5.5 C
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
3
Custody seals intact on shipping container/cooler?
Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample Iabel(s)?
(0) Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
U Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
U Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
U N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: ngela D Overcash Date & Time: 12/21/2021 11:31:52
Page 102 of 105

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Page 105 of 105

Waypointo
ANALYTICAL
12/21 /2021
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville, NC, 28801
Ref: Analytical Testing
Lab Report Number: 21-295-8005
Client Project Description: Jackson County
Site: 58-02
Project Number: 58-02
Dear Chuck Pippin:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/22/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
J* /I OA-2--
Kyle N. Collins
General Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 129

0
Waypoint.
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2022
North Carolina
State Program
402
12/31/2021
South Carolina
State Program
99012
07/31/2022
South Carolina
State Program
99012
12/31/2021
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2022
Arkansas
State Program
88-0650
02/07/2022
California
State Program
2904
06/30/2022
Florida
State Program
- NELAP
E871157
06/30/2022
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2022
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2021
Louisiana
State Program
- NELAP
LA037
12/31/2021
Louisiana
State Program
- NELAP
04015
06/30/2022
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2021
Pennsylvania
State Program
- NELAP
68-03195
05/31/2022
South Carolina
State Program
84002
06/30/2022
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2022
Virginia
State Program
- NELAP
460181
09/14/2022
Page 1 of 1 00016/21-295-8005
Page 2 of 129

Waypoint.(2)
ANALYTICAL
Report Number: 21-295-8005
Client Project Description: Jackson County
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
97909
DW-01-20211020
Aqueous
10/20/2021
10/22/2021
06:50
524.2
97910
DW-02-20211020
Aqueous
10/20/2021
10/22/2021
06:50
524.2
97911
TB-20211020D
Aqueous
10/20/2021
10/22/2021
06:50
524.2
97987
MW-01-20211020
Aqueous
10/20/2021
16:34
10/22/2021
06:50
97987
MW-01-20211020
Aqueous
10/20/2021
16:34
10/22/2021
06:50
531OC-2011
97988
MW-06-20211020
Aqueous
10/20/2021
13:36
10/22/2021
06:50
97988
MW-06-20211020
Aqueous
10/20/2021
13:36
10/22/2021
06:50
531OC-2011
97989
TB-20211020A
Aqueous
10/20/2021
10/22/2021
06:50
98018
MW-02-20211020
Aqueous
10/20/2021
09:15
10/22/2021
06:50
98018
MW-02-20211020
Aqueous
10/20/2021
09:15
10/22/2021
06:50
531OC-2011
98019
MW-03-20211020
Aqueous
10/20/2021
10:40
10/22/2021
06:50
98019
MW-03-20211020
Aqueous
10/20/2021
10:40
10/22/2021
06:50
531OC-2011
98020
TB-20211020B
Aqueous
10/20/2021
10/22/2021
06:50
98021
MW-02-20211020
Aqueous
10/20/2021
19:10
10/22/2021
06:50
98021
MW-02-20211020
Aqueous
10/20/2021
19:10
10/22/2021
06:50
8270D
98021
MW-02-20211020
Aqueous
10/20/2021
19:10
10/22/2021
06:50
8270C
98021
MW-02-20211020
Aqueous
10/20/2021
19:10
10/22/2021
06:50
8270D
98022
MW-03-20211020
Aqueous
10/20/2021
10:40
10/22/2021
06:50
8270C
98022
MW-03-20211020
Aqueous
10/20/2021
10:40
10/22/2021
06:50
8270D
98022
MW-03-20211020
Aqueous
10/20/2021
10:40
10/22/2021
06:50
8270D
98023
MW-01-20211020
Aqueous
10/20/2021
16:34
10/22/2021
06:50
8270C
98023
MW-01-20211020
Aqueous
10/20/2021
16:34
10/22/2021
06:50
8270D
98023
MW-01-20211020
Aqueous
10/20/2021
16:34
10/22/2021
06:50
8270D
98024
MW-06-20211020
Aqueous
10/20/2021
13:36
10/22/2021
06:50
8270C
98024
MW-06-20211020
Aqueous
10/20/2021
13:36
10/22/2021
06:50
8270D
98024
MW-06-20211020
Aqueous
10/20/2021
13:36
10/22/2021
06:50
8270D
98025
LT-01-20211020
Aqueous
10/20/2021
17:25
10/22/2021
06:50
: Pace Analytical - Huntersville, NC, Huntersville, NC
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
WP MTN
Page 3 of 129

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Sample Summary Table
Report Number: 21-295-8005
Client Project Description: Jackson County
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
98026 TB-20211020C Aqueous 10/20/2021 10/22/2021 06:50
: Pace Analytical - Huntersville, NC, Huntersville, NC
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 4 of 129

Waypoint (D 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytica Isom
Summary of Detected Analytes
Project: Jackson County
Report Number: 21-295-8005
Client Sample ID
Method
Lab Sample ID
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
MW-01-20211020
V 97987
2320B-2011
Alkalinity (as CaCO3)
81000
pg/L
800
10/27/2021 10:20
5210E-2016
Biochemical Oxygen Demand (5-day)
8800
Ng/L
2000
10/22/2021 10:46
5220D-2011
COD (Chemical Oxygen Demand)
74000
pg/L
11000
10/25/2021 11:16
5310C-2011
TOC
1890
Ng/L
500
10/29/2021 01:29
6020E
Arsenic
0.549
pg/L
0.170
11/03/202107:42
1
6020E
Barium
130
Ng/L
0.810
11/03/202107:42
6020E
Dissolved Barium
105
pg/L
0.810
11/05/2021 14:12
6020E
Cadmium
8.81
Ng/L
0.160
11/03/202107:42
6020E
Chromium
5.60
pg/L
0.790
11/03/202107:42
6020E
Cobalt
139
Ng/L
0.520
11/03/202107:42
6020E
Dissolved Cobalt
121
pg/L
0.520
11/05/2021 14:12
6020E
Copper
27.9
Ng/L
3.80
11/03/202107:42
6020E
Lead
2.60
pg/L
0.260
11/03/202107:42
6020E
Dissolved Nickel
13.6
pg/L
0.510
11/05/2021 14:12
6020E
Nickel
18.3
pg/L
0.510
11/03/202107:42
6020E
Thallium
1.42
Ng/L
0.570
11/03/202107:42
1
6020E
Dissolved Thallium
0.573
pg/L
0.570
11/05/2021 14:12
1
6020E
Vanadium
6.16
Ng/L
1.30
11/03/202122:35
6020E
Zinc
169
pg/L
6.90
11/03/202107:42
7470A
Dissolved Mercury
0.0900
Ng/L
0.0700
11/06/2021 12:32
1
8260D
Acetone
4.90
pg/L
1.80
11/01/202109:29
1
8260D
Benzene
1.11
Ng/L
0.180
11/01/202109:29
8260D
Chlorobenzene
1.14
pg/L
0.190
11/01/202109:29
8260D
1,4-Dichlorobenzene
7.76
Ng/L
0.210
11/01/202109:29
8260D
1,1-Dichloroethane
2.34
pg/L
0.240
11/01/202109:29
8260D
cis- 1,2-Dichloroethene
3.24
Ng/L
0.200
11/01/202109:29
8260D
Naphthalene
0.960
pg/L
0.470
11/01/202109:29
1
8260D
Trichloroethene
0.517
Ng/L
0.180
11/01/202109:29
9056A
Chloride
866
pg/L
370
10/22/202113:22
1
SM-3500-Fe-B
Ferrous Iron
32900
Ng/L
1250
10/25/2021 15:56
MW-06-20211020
V 97988
2320E-2011
Alkalinity (as CaCO3)
25000
pg/L
800
10/27/2021 10:20
5220D-2011
COD (Chemical Oxygen Demand)
19000
Ng/L
11000
10/25/2021 11:16
1
5310C-2011
TOC
788
pg/L
500
10/30/202113:22
1
6020E
Barium
48.9
Ng/L
0.810
11/03/202107:49
6020E
Cobalt
11.6
pg/L
0.520
11/03/202107:49
Page 5 of 129

(D
Waypoint 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
AN LYT I CAL www.waypointanalytica l.com
Summary of Detected Analytes
Project: Jackson County
Report Number: 21-295-8005
Client Sample ID Lab Sample ID
Method Parameters
Result Units Report Limit Analyzed
MW-06-20211020
V 97988
6020B
Nickel
5.31
pg/L
0.510
11/03/202107:49
6020E
Vanadium
1.55
pg/L
1.30
11/03/202122:41
6020E
Zinc
13.2
pg/L
6.90
11/03/202107:49
8260D
1,4-Dichlorobenzene
1.43
pg/L
0.210
11/01/202109:54
8260D
1,1-Dichloroethane
0.833
pg/L
0.240
11/01/202109:54
8260D
cis- 1,2-Dichloroethene
0.676
pg/L
0.200
11/01/202109:54
9056A
Chloride
888
pg/L
370
10/22/202113:06
SM-3500-Fe-B
Ferrous Iron
60.0
pg/L
50.0
10/25/2021 15:56
MW-02-20211020
V 98018
2320E-2011
Alkalinity (as CaCO3)
58000
pg/L
800
10/27/2021 10:20
4500S2F-2011
Sulfide
4.00
mg/L
0.83
10/26/202109:45
5220D-2011
COD (Chemical Oxygen Demand)
38000
pg/L
11000
10/25/2021 11:16
5310C-2011
TOC
1450
pg/L
500
10/30/2021 14:38
6020E
Arsenic
2.99
pg/L
0.170
11/02/202121:24
6020B
Barium
154
pg/L
0.810
11/02/202121:24
6020B
Dissolved Barium
39.2
pg/L
0.810
11/05/2021 13:58
6020B
Beryllium
0.611
pg/L
0.190
11/02/202121:24
6020B
Chromium
20.6
pg/L
0.790
11/02/202121:24
6020B
Cobalt
28.1
pg/L
0.520
11/02/202121:24
6020B
Dissolved Cobalt
19.1
pg/L
0.520
11/05/2021 13:58
6020B
Copper
22.6
pg/L
3.80
11/02/202121:24
6020B
Lead
5.96
pg/L
0.260
11/02/202121:24
6020B
Dissolved Nickel
18.3
pg/L
0.510
11/05/2021 13:58
6020E
Nickel
14.6
pg/L
0.510
11/02/202121:24
6020B
Selenium
0.912
pg/L
0.740
11/08/202117:23
6020B
Vanadium
28.8
pg/L
1.30
11/08/202117:23
6020B
Zinc
55.5
pg/L
6.90
11/02/202121:24
7470A
Dissolved Mercury
0.0700
pg/L
0.0700
11/06/2021 12:27
8260D SIM
1,4-Dioxane
1.70
pg/L
0.139
10/27/2021 10:02
9056A
Chloride
20100
pg/L
370
10/22/202115:01
9056A
Sulfate
27000
pg/L
540
10/22/202115:01
SM-3500-Fe-13
Ferrous Iron
80.0
pg/L
50.0
10/25/2021 15:56
MW-03-20211020
V 98019
2320B-2011
Alkalinity (as CaCO3)
51000
pg/L
800
10/27/2021 10:20
5220D-2011
COD (Chemical Oxygen Demand)
41000
pg/L
11000
10/25/2021 11:16
5310C-2011
TOC
2410
pg/L
500
10/30/2021 15:16
Qualifiers
I
I
0
0
0
I
IJ
I
Page 6 of 129

Waypoint.(2)
ANALYTICAL
Project: Jackson County
Report Number: 21-295-8005
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Summary of Detected
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
MW-03-20211020
V 98019
6020B
Arsenic
6020B
Barium
6020B
Dissolved Barium
6020B
Cadmium
6020B
Dissolved Cadmium
6020B
Chromium
6020B
Cobalt
6020B
Dissolved Cobalt
6020B
Dissolved Nickel
6020B
Nickel
6020B
Vanadium
6020B
Zinc
6020B
Dissolved Zinc
7470A
Dissolved Mercury
8260D
Acetone
8260D
Benzene
8260D
Chlorobenzene
8260D
1,4-Dichlorobenzene
8260D
1,1-Dichloroethane
8260D
cis-1,2-Dichloroethene
8260D
Methyl Ethyl Ketone (MEK)
8260D SIM
1,4-Dioxane
9056A
Chloride
9056A
Nitrate (NO3-N)
9056A
Sulfate
MW-02-20211020
V 98021
8270D
Diethyl phthalate
9056A
Nitrate (NO3-N)
MW-03-20211020
V 98022
8270D
1,4-Dichlorobenzene
MW-01-20211020
V 98023
8270D
1,4-Dichlorobenzene
8270D
Diethyl phthalate
0.359
pq/L
0.170
111021202121:31
1
199
Ng/L
0.810
11/02/202121:31
186
pq/L
0.810
11/05/202114:05
0.486
pg/L
0.160
11/02/202121:31
1
0.421
pq/L
0.160
11/05/202114:05
1
1.05
pg/L
0.790
11/02/202121:31
1
6.28
pq/L
0.520
11/02/202121:31
3.59
pg/L
0.520
11/05/202114:05
4.12
pq/L
0.510
11/05/202114:05
4.88
pg/L
0.510
11/02/202121:31
2.09
pq/L
1.30
11/08/202117:30
1
10.9
pg/L
6.90
11/02/202121:31
1
8.20
pq/L
6.90
11/05/202114:05
1
0.0800
pg/L
0.0700
11/06/202112:30
1
1.92
pq/L
1.80
11/01/202109:05
1
1.19
Ng/L
0.180
11 /01 /2021
09:05
10.2
pq/L
0.190
111011202109:05
5.19
pg/L
0.210
11 /01 /2021
09:05
0.781
pq/L
0.240
111011202109:05
2.18
Ng/L
0.200
11 /01 /2021
09:05
0.969
pq/L
0.710
111011202109:05
1
5.96
Ng/L
0.139
10/27/202110:27
32500
pq/L
370
101221202115:16
3710
Ng/L
76.0
10/22/202115:16
1000
pq/L
540
101221202115:16
B
4.41
Ng/L
1.39
10/27/202122:38
1
255
pq/L
76.0
10/22/202116:04
2.84
pg/L
0.591
10/27/202123:00
1
3.72
pq/L
0.591
10/27/202123:22
1
0.651
Ng/L
0.596
10/27/202123:22
1
Page 7 of 129

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Summary of Detected Analytes
Project: Jackson County
Report Number: 21-295-8005
Client Sample ID Lab Sample ID
Method Parameters Result Units Report Limit Analyzed Qualifiers
MW-06-20211020
V 98024
8270D
1,4-Dichlorobenzene
0.822
pq/L
LT-01-20211020
V 98025
6020B
Arsenic
4.00
Ng/L
6020B
Barium
372
pq/L
6020B
Cobalt
5.83
Ng/L
6020B
Nickel
24.2
uq/L
6020B
Vanadium
3.42
Ng/L
8260D
Acetone
8.14
uq/L
8260D
Benzene
2.45
Ng/L
8260D
Chlorobenzene
4.28
uq/L
8260D
1,4-Dichlorobenzene
3.85
Ng/L
8260D
Ethylbenzene
0.838
uq/L
8260D
Naphthalene
13.6
Ng/L
8260D
Tetrahydrofuran
203
uq/L
8260D
o-Xylene
1.64
Ng/L
8260D
m,p-Xylene
1.17
uq/L
8260D
Xylene (Total)
2.81
Ng/L
8260D SIM
1,4-Dioxane
48.8
pq/L
0.585
10/27/2021 23:44 1
0.850
11 /02/2021 21:38 1
4.05
11/02/2021 21:38
2.60
11 /02/2021 21:38 1
2.55
11/02/2021 21:38
1.30
11 /08/2021 17:49 1
1.80
11/01/2021 10:19
0.180
11 /01 /2021 10:19
0.190
11/01/2021 10:19
0.210
11 /01 /2021 10:19
0.170
11/01/2021 10:19
0.470
11 /01 /2021 10:19
15.0
11 /01 /2021 19:07
0.210
11 /01 /2021 10:19
0.420
11 /01 /2021 10:19
0.210
11 /01 /2021 10:19
0.139
10/28/2021 12:24
Page 8 of 129

Waypointo
ANALYTICAL
Client: Anchor QEA of North Carolina, PLLC
Project: Jackson County
Lab Report Number: 21-295-8005
Date: 12/21 /2021
Metals Analyses Method 6020B
Sample 97852
Analyte: Vanadium
QC Batch No: V1 1 123/V1 0735
LLICV failed high. Result may be high bias.
Sample 97988 (MW-06-20211020)
Analyte: Vanadium
QC Batch No: V11123/V10735
LLICV failed high. Result may be high bias.
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
CASE NARRATIVE
Sample 98025 (LT-01-20211020)
QC Batch No: V11101/V10864
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 97383
Analyte: Selenium
QC Batch No: V11068/V10864
LLICV failed high. Sample results are BRL.
Sample 98018 (MW-02-20211020)
Analyte: Barium
QC Batch No: V1 1240N1 1 166/V1 1161
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Beryllium
QC Batch No: V11308/V11166/V11161
LLICV failed high. Sample concentration BRL or 10X concentration.
Analyte: Selenium
QC Batch No: V11081/V11166/V11161
LLICV and LRB failed high. Results may be high bias.
Analyte: Selenium
QC Batch No: V11101/V11166/V11161
LLICV failed high. Sample concentration BRL.
Sample 98018 (MW-02-20211020)
Analyte: Selenium
QC Batch No: V11101/V11166/V11161
LLICV failed high. Results may be high bias.
Analyte: Selenium
QC Batch No: V11232/V11166/V11161
Page 9 of 129

Waypointo
ANALYTICAL
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
LLICV failed high. Sample concentration BRL or 1 OX concentration
Analyte: Selenium
QC Batch No: V11233/V11166/V11161
LLICV failed high. Sample concentration BRL.
Analyte: Selenium
QC Batch No: V11240N11166/V11161
LLICV failed high. Sample concentration BRL.
Analyte: Vanadium
QC Batch No: V11101/V11166/V11161
LLICV, ICB and CCB failed high. Results may be high bias.
Sample 97987 (MW-01-20211020)
Analyte: Vanadium
QC Batch No: V1 1 123/V1 1 166/V1 1161
LLICV failed high. Result may be high bias.
Analyte: Vanadium
QC Batch No: V11233/V11166/V11161
LLICV failed high. Sample concentration BRL.
Analyte: Vanadium
QC Batch No: V11240/V11166/V11161
LLICV failed high. Sample concentration BRL.
Total Aqueous Mercury Analysis - CVAA Method 7470A
Sample 98049
Analyte: Mercury
QC Batch No: V10964/V10945
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Sample 97996
Analyte: Mercury
QC Batch No: V11111/V11049
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 97855
Analyte: Mercury
QC Batch No: V11256/V11199
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected.
Revised Report — This a revised report combining five reports to represent all the samples that were taken on
10/20/21.
Page 10 of 129

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-295-8005
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/22/2021
Lab No : 97987
Matrix: Aqueous
Sample ID: MW-01-20211020
Sampled:
10/20/2021 16:34
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ferrous Iron
32900
Ng/L
1250
5000
1
10/25/21 15:56
ENM
SM-3500-Fe-B
1,4-Dioxane
<0.139
ug/L
0.139
2.00
1
10/28/21 11:34
TBL
8260D SIM
Alkalinity (as CaCO3)
81000
Ng/L
800
5000
1
10/27/21 10:20
CLB
2320B-2011
Biochemical Oxygen Demand (5-day)
8800
ug/L
2000
2000
1
10/22/21 10:46
SLO
521OB-2016
Chloride
8663
Ng/L
370
1000
1
10/22/21 13:22
CEG
9056A
COD (Chemical Oxygen Demand)
74000
ug/L
11000
50000
1
10/25/21 11:16
ENM
5220D-2011
Nitrate (NO3-N)
<76.0
Ng/L
76.0
200
1
10/22/21 13:22
CEG
9056A
TOC
1890
ug/L
500
1000
1
10/29/2101:29
JW2
531OC-2011
Sulfate
<540
Ng/L
540
1000
1
10/22/21 13:22
CEG
9056A
Sulfide
<830
ug/L
2000
1
10/26/2109:45
ENM
4500S2F-2011
Antimony
<0.490
Ng/L
0.490
2.00
1
11/03/2107:42
EDV
6020B
Dissolved Antimony
<0.490
ug/L
0.490
2.00
1
11/05/21 14:12
EDV
6020B
Arsenic
0.5493
Ng/L
0.170
1.00
1
11/03/2107:42
EDV
6020B
Dissolved Arsenic
<0.170
ug/L
0.170
1.00
1
11/05/21 14:12
EDV
6020B
Barium
130
Ng/L
0.810
10.0
1
11/03/2107:42
EDV
6020B
Dissolved Barium
105
ug/L
0.810
10.0
1
11/05/21 14:12
EDV
6020B
Beryllium
<0.190
Ng/L
0.190
1.00
1
11/03/2122:35
EDV
6020B
Dissolved Beryllium
<0.190
ug/L
0.190
1.00
1
11/05/21 14:12
EDV
6020B
Cadmium
8.81
Ng/L
0.160
1.00
1
11/03/2107:42
EDV
6020B
Dissolved Cadmium
<0.160
ug/L
0.160
1.00
1
11/05/21 14:12
EDV
6020B
Chromium
5.60
Ng/L
0.790
2.00
1
11/03/2107:42
EDV
6020B
Dissolved Chromium
<0.790
ug/L
0.790
2.00
1
11/05/21 14:12
EDV
6020B
Cobalt
139
Ng/L
0.520
2.00
1
11/03/2107:42
EDV
6020B
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
L Limit Exceeded
M
Minimum
value
MQL Method Quantitation Limit
Page 11 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 97987
Matrix: Aqueous
Sample ID: MW-01-20211020
Sampled:
10/20/2021 16:34
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Dissolved Cobalt
121
Ng/L
0.520
2.00
1
11/05/21 14:12
EDV
6020B
Copper
27.9
ug/L
3.80
10.0
1
11/03/21 07:42
EDV
6020B
Dissolved Copper
<3.80
Ng/L
3.80
10.0
1
11/05/21 14:12
EDV
6020B
Lead
2.60
ug/L
0.260
1.00
1
11/03/2107:42
EDV
6020B
Dissolved Lead
<0.260
Ng/L
0.260
1.00
1
11/05/21 14:12
EDV
6020E
Mercury (Total)
<0.0700
ug/L
0.0700
0.200
1
10/29/21 20:48
EDV
7470A
Dissolved Mercury
0.09003
Ng/L
0.0700
0.200
1
11/06/21 12:32
EDV
7470A
Dissolved Nickel
13.6
pg/L
0.510
3.00
1
11/05/21 14:12
EDV
6020B
Nickel
18.3
Ng/L
0.510
3.00
1
11/03/2107:42
EDV
6020B
Selenium
<0.740
pg/L
0.740
5.00
1
11/03/2107:42
EDV
6020B
Dissolved Selenium
<0.740
Ng/L
0.740
5.00
1
11/05/21 14:12
EDV
6020B
Silver
<0.110
pg/L
0.110
1.00
1
11/03/2107:42
EDV
6020B
Dissolved Silver
<0.110
Ng/L
0.110
1.00
1
11/05/21 14:12
EDV
6020B
Tin
<1.80
pg/L
1.80
5.00
1
11/03/2107:42
EDV
6020B
Dissolved Tin
<1.80
Ng/L
1.80
5.00
1
11/05/21 14:12
EDV
6020B
Thallium
1.421
ug/L
0.570
2.00
1
11/03/2107:42
EDV
6020B
Dissolved Thallium
0.5733
Ng/L
0.570
2.00
1
11/05/21 14:12
EDV
6020B
Vanadium
6.16
ug/L
1.30
5.00
1
11/03/2122:35
EDV
6020B
Dissolved Vanadium
<1.30
Ng/L
1.30
5.00
1
11/05/21 14:12
EDV
6020B
Zinc
169
ug/L
6.90
20.0
1
11/03/2107:42
EDV
6020B
Dissolved Zinc
<6.90
Ng/L
6.90
20.0
1
11/05/21 14:12
EDV
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 12 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 97987
Matrix: Aqueous
Sample ID: MW-01-20211020
Sampled:
10/20/2021
16:34
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
4.903
Ng/L
1.80
5.00
1
11/01/21 09:29
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 09:29
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 09:29
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 09:29
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 09:29
JLB
V11000
Benzene
1.11
ug/L
0.180
0.500
1
11/01/21 09:29
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 09:29
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 09:29
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 09:29
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 09:29
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 09:29
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 09:29
JLB
V11000
Chlorobenzene
1.14
Ng/L
0.190
0.500
1
11/01/21 09:29
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 09:29
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 09:29
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 09:29
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 09:29
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 09:29
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 09:29
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 09:29
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 09:29
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 09:29
JLB
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 13 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 97987 Matrix: Aqueous
Sample ID: MW-01-20211020 Sampled: 10/20/2021 16:34
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 09:29
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 09:29
JLB
V11000
1,4-Dichlorobenzene
7.76
Ng/L
0.210
0.500
1
11/01/21 09:29
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 09:29
JLB
V11000
1,1-Dichloroethane
2.34
Ng/L
0.240
0.500
1
11/01/21 09:29
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 09:29
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 09:29
JLB
V11000
cis- 1,2-Dich loroethene
3.24
ug/L
0.200
0.500
1
11/01/21 09:29
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 09:29
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 09:29
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 09:29
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 09:29
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 09:29
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 09:29
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 09:29
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 09:29
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 09:29
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 09:29
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 09:29
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 09:29
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 09:29
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 09:29
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 14 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 97987
Matrix: Aqueous
Sample ID: MW-01-20211020
Sampled:
10/20/2021
16:34
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 09:29
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 09:29
JLB
V11000
Naphthalene
0.9603
Ng/L
0.470
1.00
1
11/01/21 09:29
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 09:29
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 09:29
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 09:29
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 09:29
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 09:29
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 09:29
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 09:29
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 09:29
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 09:29
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 09:29
JLB
V11000
Trichloroethene
0.517
ug/L
0.180
0.500
1
11/01/21 09:29
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 09:29
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 09:29
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 09:29
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 09:29
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 09:29
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 09:29
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 09:29
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 15 of 129

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-295-8005
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/22/2021
Lab No : 97988
Matrix: Aqueous
Sample ID: MW-06-20211020
Sampled:
10/20/2021 13:36
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ferrous Iron
60.03
Ng/L
50.0
200
1
10/25/21 15:56
ENM
SM-3500-Fe-B
1,4-Dioxane
<0.139
ug/L
0.139
2.00
1
10/28/21 11:59
TBL
8260D SIM
Alkalinity (as CaCO3)
25000
Ng/L
800
5000
1
10/27/21 10:20
CLB
2320B-2011
Biochemical Oxygen Demand (5-day) <2000
ug/L
2000
2000
1
10/22/21 10:46
SLO
521OB-2016
Chloride
8883
Ng/L
370
1000
1
10/22/21 13:06
CEG
9056A
COD (Chemical Oxygen Demand) 190003
ug/L
11000
50000
1
10/25/21 11:16
ENM
5220D-2011
Nitrate (NO3-N)
<76.0
Ng/L
76.0
200
1
10/22/21 13:06
CEG
9056A
TOC
7883
pg/L
500
1000
1
10/30/21 13:22
JW2
531OC-2011
Sulfate
<540
Ng/L
540
1000
1
10/22/21 13:06
CEG
9056A
Sulfide
<830
ug/L
2000
1
10/26/2109:45
ENM
4500S2F-2011
Antimony
<0.490
Ng/L
0.490
2.00
1
11/03/2107:49
EDV
6020B
Arsenic
<0.170
ug/L
0.170
1.00
1
11/03/2107:49
EDV
6020B
Barium
48.9
Ng/L
0.810
10.0
1
11/03/2107:49
EDV
6020B
Beryllium
<0.190
ug/L
0.190
1.00
1
11/03/2122:41
EDV
6020B
Cadmium
<0.160
Ng/L
0.160
1.00
1
11/03/2107:49
EDV
6020B
Chromium
<0.790
ug/L
0.790
2.00
1
11/03/2107:49
EDV
6020B
Cobalt
11.6
Ng/L
0.520
2.00
1
11/03/2107:49
EDV
6020B
Copper
<3.80
ug/L
3.80
10.0
1
11/03/21 07:49
EDV
6020B
Lead
<0.260
Ng/L
0.260
1.00
1
11/03/21 07:49
EDV
6020B
Mercury (Total)
<0.0700
ug/L
0.0700
0.200
1
10/29/21 20:51
EDV
7470A
Nickel
5.31
Ng/L
0.510
3.00
1
11/03/2107:49
EDV
6020B
Selenium
<0.740
ug/L
0.740
5.00
1
11/03/2107:49
EDV
6020B
Silver
<0.110
Ng/L
0.110
1.00
1
11/03/2107:49
EDV
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 16 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 97988
Sample ID: MW-06-20211020
Matrix: Aqueous
Sampled: 10/20/2021 13:36
Test
Results
Units
MDL
MQL
DF
Date / Time By Analytical
Analyzed Method
Tin
<1.80
Ng/L
1.80
5.00
1
11/03/2107:49 EDV 6020B
Thallium
<0.570
ug/L
0.570
2.00
1
11/03/2107:49 EDV 6020B
Vanadium
1.553
Ng/L
1.30
5.00
1
11/03/21 22:41 EDV 6020B
Zinc
13.23
ug/L
6.90
20.0
1
11/03/2107:49 EDV 6020B
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 17 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 97988
Matrix: Aqueous
Sample ID: MW-06-20211020
Sampled:
10/20/2021
13:36
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
Ng/L
1.80
5.00
1
11/01/21 09:54
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 09:54
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 09:54
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 09:54
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 09:54
JLB
V11000
Benzene
<0.180
ug/L
0.180
0.500
1
11/01/21 09:54
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 09:54
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 09:54
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 09:54
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 09:54
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 09:54
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 09:54
JLB
V11000
Chlorobenzene
<0.190
Ng/L
0.190
0.500
1
11/01/21 09:54
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 09:54
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 09:54
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 09:54
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 09:54
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 09:54
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 09:54
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 09:54
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 09:54
JLB
V11000
trans-1,4-Dichloro-2-butene
< 1.30
ug/L
1.30
10.0
1
11/01/21 09:54
JLB
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation
Limit
Page 18 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 97988 Matrix: Aqueous
Sample ID: MW-06-20211020 Sampled: 10/20/2021 13:36
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 09:54
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 09:54
JLB
V11000
1,4-Dichlorobenzene
1.43
Ng/L
0.210
0.500
1
11/01/21 09:54
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 09:54
JLB
V11000
1,1-Dichloroethane
0.833
Ng/L
0.240
0.500
1
11/01/21 09:54
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 09:54
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 09:54
JLB
V11000
cis- 1,2-Dich loroethene
0.676
ug/L
0.200
0.500
1
11/01/21 09:54
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 09:54
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 09:54
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 09:54
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 09:54
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 09:54
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 09:54
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 09:54
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 09:54
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 09:54
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 09:54
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 09:54
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 09:54
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 09:54
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 09:54
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation
Limit
Page 19 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 97988
Matrix: Aqueous
Sample ID: MW-06-20211020
Sampled:
10/20/2021
13:36
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 09:54
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 09:54
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 09:54
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 09:54
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 09:54
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 09:54
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 09:54
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 09:54
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 09:54
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 09:54
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 09:54
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 09:54
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 09:54
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 09:54
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 09:54
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 09:54
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 09:54
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 09:54
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 09:54
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 09:54
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 09:54
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation
Limit
Page 20 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 97989
Matrix: Aqueous
Sample ID : TB-20211020A
Sampled:
10/20/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
Ng/L
1.80
5.00
1
11/01/21 02:31
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 02:31
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 02:31
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 02:31
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 02:31
JLB
V11000
Benzene
<0.180
ug/L
0.180
0.500
1
11/01/21 02:31
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 02:31
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 02:31
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 02:31
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 02:31
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 02:31
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 02:31
JLB
V11000
Chlorobenzene
<0.190
Ng/L
0.190
0.500
1
11/01/21 02:31
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 02:31
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 02:31
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 02:31
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 02:31
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 02:31
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 02:31
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 02:31
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 02:31
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 02:31
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 21 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 97989 Matrix: Aqueous
Sample ID : TB-20211020A Sampled: 10/20/2021 0:00
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 02:31
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 02:31
JLB
V11000
1,4-Dichlorobenzene
<0.210
Ng/L
0.210
0.500
1
11/01/21 02:31
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 02:31
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 02:31
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 02:31
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 02:31
JLB
V11000
cis- 1,2-Dich loroethene
<0.200
ug/L
0.200
0.500
1
11/01/21 02:31
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 02:31
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 02:31
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 02:31
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 02:31
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 02:31
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 02:31
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 02:31
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 02:31
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 02:31
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 02:31
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 02:31
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 02:31
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 02:31
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 02:31
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 22 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 97989
Matrix: Aqueous
Sample ID : TB-20211020A
Sampled:
10/20/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 02:31
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 02:31
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 02:31
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 02:31
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 02:31
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 02:31
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 02:31
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 02:31
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 02:31
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 02:31
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 02:31
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 02:31
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 02:31
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 02:31
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 02:31
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 02:31
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 02:31
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 02:31
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 02:31
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 02:31
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 02:31
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 23 of 129

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-295-8005
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/22/2021
Lab No : 98018
Matrix: Aqueous
Sample ID: MW-02-20211020
Sampled:
10/20/2021 9:15
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ferrous Iron
80.03
Ng/L
50.0
200
1
10/25/21 15:56
ENM
SM-3500-Fe-B
1,4-Dioxane
1.70 J
ug/L
0.139
2.00
1
10/27/21 10:02
TBL
8260D SIM
Alkalinity (as CaCO3)
58000
Ng/L
800
5000
1
10/27/21 10:20
CLB
2320B-2011
Chloride
20100
ug/L
370
1000
1
10/22/21 15:01
CEG
9056A
COD (Chemical Oxygen Demand) 380003
Ng/L
11000
50000
1
10/25/21 11:16
ENM
5220D-2011
Nitrate (NO3-N)
<76.0 H
ug/L
76.0
200
1
10/22/21 15:01
CEG
9056A
TOC
1450
Ng/L
500
1000
1
10/30/21 14:38
JW2
531OC-2011
Sulfate
27000
ug/L
540
1000
1
10/22/21 15:01
CEG
9056A
Sulfide
4.00
mg/L
2.00
1
10/26/2109:45
ENM
4500S2F-2011
Antimony
<0.490
ug/L
0.490
2.00
1
11/02/2121:24
EDV
6020B
Dissolved Antimony
<0.490
Ng/L
0.490
2.00
1
11/05/21 13:58
EDV
6020B
Arsenic
2.99
ug/L
0.170
1.00
1
11/02/2121:24
EDV
6020B
Dissolved Arsenic
<0.170
Ng/L
0.170
1.00
1
11/05/21 13:58
EDV
6020B
Barium
154
ug/L
0.810
10.0
1
11/02/2121:24
EDV
6020B
Dissolved Barium
39.2
Ng/L
0.810
10.0
1
11/05/21 13:58
EDV
6020B
Beryllium
0.6113
ug/L
0.190
1.00
1
11/02/21 21:24
EDV
6020B
Dissolved Beryllium
<0.190
Ng/L
0.190
1.00
1
11/05/21 13:58
EDV
6020B
Cadmium
<0.160
ug/L
0.160
1.00
1
11/02/2121:24
EDV
6020B
Dissolved Cadmium
<0.160
Ng/L
0.160
1.00
1
11/05/21 13:58
EDV
6020B
Chromium
20.6
ug/L
0.790
2.00
1
11/02/2121:24
EDV
6020B
Dissolved Chromium
<0.790
Ng/L
0.790
2.00
1
11/05/21 13:58
EDV
6020B
Cobalt
28.1
ug/L
0.520
2.00
1
11/02/2121:24
EDV
6020B
Dissolved Cobalt
19.1
Ng/L
0.520
2.00
1
11/05/21 13:58
EDV
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 24 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98018
Matrix: Aqueous
Sample ID: MW-02-20211020
Sampled:
10/20/2021 9:15
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Copper
22.6
Ng/L
3.80
10.0
1
11/02/21 21:24
EDV
6020B
Dissolved Copper
<3.80
ug/L
3.80
10.0
1
11/05/21 13:58
EDV
6020B
Lead
5.96
Ng/L
0.260
1.00
1
11/02/21 21:24
EDV
6020E
Dissolved Lead
<0.260
ug/L
0.260
1.00
1
11/05/21 13:58
EDV
6020B
Mercury (Total)
<0.0700
Ng/L
0.0700
0.200
1
11/02/21 18:21
EDV
7470A
Dissolved Mercury
0.0700 J
ug/L
0.0700
0.200
1
11/06/21 12:27
EDV
7470A
Dissolved Nickel
18.3
Ng/L
0.510
3.00
1
11/05/21 13:58
EDV
6020E
Nickel
14.6
ug/L
0.510
3.00
1
11/02/2121:24
EDV
6020B
Selenium
0.912 J
Ng/L
0.740
5.00
1
11/08/21 17:23
EDV
6020E
Dissolved Selenium
<0.740
ug/L
0.740
5.00
1
11/05/21 13:58
EDV
6020B
Silver
<0.110
Ng/L
0.110
1.00
1
11/02/2121:24
EDV
6020E
Dissolved Silver
<0.110
ug/L
0.110
1.00
1
11/05/21 13:58
EDV
6020B
Tin
<1.80
Ng/L
1.80
5.00
1
11/05/2114:45
EDV
6020B
Dissolved Tin
<1.80
ug/L
1.80
5.00
1
11/05/21 13:58
EDV
6020B
Thallium
<0.570
Ng/L
0.570
2.00
1
11/02/2121:24
EDV
6020B
Dissolved Thallium
<0.570
ug/L
0.570
2.00
1
11/05/21 13:58
EDV
6020B
Vanadium
28.8
Ng/L
1.30
5.00
1
11/08/2117:23
EDV
6020B
Dissolved Vanadium
<1.30
ug/L
1.30
5.00
1
11/05/21 13:58
EDV
6020B
Zinc
55.5
Ng/L
6.90
20.0
1
11/02/2121:24
EDV
6020B
Dissolved Zinc
<6.90
ug/L
6.90
20.0
1
11/05/21 13:58
EDV
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 25 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98018
Matrix: Aqueous
Sample ID: MW-02-20211020
Sampled:
10/20/2021
9:15
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
Ng/L
1.80
5.00
1
11/01/21 08:40
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 08:40
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 08:40
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 08:40
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 08:40
JLB
V11000
Benzene
<0.180
ug/L
0.180
0.500
1
11/01/21 08:40
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 08:40
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 08:40
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 08:40
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 08:40
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 08:40
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 08:40
JLB
V11000
Chlorobenzene
<0.190
Ng/L
0.190
0.500
1
11/01/21 08:40
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 08:40
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 08:40
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 08:40
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 08:40
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 08:40
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 08:40
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 08:40
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 08:40
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 08:40
JLB
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 26 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98018 Matrix: Aqueous
Sample ID: MW-02-20211020 Sampled: 10/20/2021 9:15
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 08:40
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 08:40
JLB
V11000
1,4-Dichlorobenzene
<0.210
Ng/L
0.210
0.500
1
11/01/21 08:40
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 08:40
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 08:40
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 08:40
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 08:40
JLB
V11000
cis- 1,2-Dich loroethene
<0.200
ug/L
0.200
0.500
1
11/01/21 08:40
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 08:40
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 08:40
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 08:40
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 08:40
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 08:40
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 08:40
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 08:40
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 08:40
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 08:40
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 08:40
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 08:40
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 08:40
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 08:40
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 08:40
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 27 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98018
Matrix: Aqueous
Sample ID: MW-02-20211020
Sampled:
10/20/2021
9:15
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 08:40
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 08:40
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 08:40
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 08:40
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 08:40
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 08:40
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 08:40
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 08:40
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 08:40
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 08:40
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 08:40
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 08:40
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 08:40
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 08:40
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 08:40
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 08:40
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 08:40
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 08:40
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 08:40
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 08:40
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 08:40
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 28 of 129

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-295-8005
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/22/2021
Lab No : 98019
Matrix: Aqueous
Sample ID: MW-03-20211020
Sampled:
10/20/2021 10:40
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ferrous Iron
<50.0
Ng/L
50.0
200
1
10/25/21 15:56
ENM
SM-3500-Fe-B
1,4-Dioxane
5.96
ug/L
0.139
2.00
1
10/27/21 10:27
TBL
8260D SIM
Alkalinity (as CaCO3)
51000
Ng/L
800
5000
1
10/27/21 10:20
CLB
2320B-2011
Biochemical Oxygen Demand (5-day)
<2000
ug/L
2000
2000
1
10/22/21 10:46
SLO
521OB-2016
Chloride
32500
Ng/L
370
1000
1
10/22/21 15:16
CEG
9056A
COD (Chemical Oxygen Demand)
41000 J
ug/L
11000
50000
1
10/25/21 11:16
ENM
5220D-2011
Nitrate (NO3-N)
3710
Ng/L
76.0
200
1
10/22/21 15:16
CEG
9056A
TOC
2410
ug/L
500
1000
1
10/30/21 15:16
JW2
531OC-2011
Sulfate
1000 B
Ng/L
540
1000
1
10/22/21 15:16
CEG
9056A
Sulfide
<0.83
mg/L
2.00
1
10/26/2109:45
ENM
4500S2F-2011
Antimony
<0.490
Ng/L
0.490
2.00
1
11/02/2121:31
EDV
6020B
Dissolved Antimony
<0.490
ug/L
0.490
2.00
1
11/05/21 14:05
EDV
6020B
Arsenic
0.359 J
Ng/L
0.170
1.00
1
11/02/2121:31
EDV
6020B
Dissolved Arsenic
<0.170
ug/L
0.170
1.00
1
11/05/21 14:05
EDV
6020B
Barium
199
Ng/L
0.810
10.0
1
11/02/2121:31
EDV
6020B
Dissolved Barium
186
ug/L
0.810
10.0
1
11/05/21 14:05
EDV
6020B
Beryllium
<0.190
Ng/L
0.190
1.00
1
11/02/2121:31
EDV
6020B
Dissolved Beryllium
<0.190
ug/L
0.190
1.00
1
11/05/21 14:05
EDV
6020B
Cadmium
0.486 J
Ng/L
0.160
1.00
1
11/02/2121:31
EDV
6020B
Dissolved Cadmium
0.4213
ug/L
0.160
1.00
1
11/05/21 14:05
EDV
6020B
Chromium
1.05 J
Ng/L
0.790
2.00
1
11/02/2121:31
EDV
6020B
Dissolved Chromium
<0.790
ug/L
0.790
2.00
1
11/05/21 14:05
EDV
6020B
Cobalt
6.28
Ng/L
0.520
2.00
1
11/02/2121:31
EDV
6020B
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
L Limit Exceeded
M
Minimum
value
MQL Method Quantitation Limit
Page 29 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98019
Matrix: Aqueous
Sample ID: MW-03-20211020
Sampled:
10/20/2021 10:40
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Dissolved Cobalt
3.59
Ng/L
0.520
2.00
1
11/05/21 14:05
EDV
6020B
Copper
<3.80
ug/L
3.80
10.0
1
11/02/2121:31
EDV
6020B
Dissolved Copper
<3.80
Ng/L
3.80
10.0
1
11/05/21 14:05
EDV
6020E
Lead
<0.260
ug/L
0.260
1.00
1
11/02/2121:31
EDV
6020B
Dissolved Lead
<0.260
Ng/L
0.260
1.00
1
11/05/21 14:05
EDV
6020E
Mercury (Total)
<0.0700
ug/L
0.0700
0.200
1
11/02/21 18:24
EDV
7470A
Dissolved Mercury
0.08003
Ng/L
0.0700
0.200
1
11/06/21 12:30
EDV
7470A
Dissolved Nickel
4.12
ug/L
0.510
3.00
1
11/05/21 14:05
EDV
6020B
Nickel
4.88
Ng/L
0.510
3.00
1
11/02/2121:31
EDV
6020E
Selenium
<0.740
ug/L
0.740
5.00
1
11/02/2121:31
EDV
6020B
Dissolved Selenium
<0.740
Ng/L
0.740
5.00
1
11/05/21 14:05
EDV
6020E
Silver
<0.110
ug/L
0.110
1.00
1
11/02/2121:31
EDV
6020B
Dissolved Silver
<0.110
Ng/L
0.110
1.00
1
11/05/21 14:05
EDV
6020E
Tin
<1.80
ug/L
1.80
5.00
1
11/05/2114:51
EDV
6020B
Dissolved Tin
<1.80
Ng/L
1.80
5.00
1
11/05/21 14:05
EDV
6020B
Thallium
<0.570
ug/L
0.570
2.00
1
11/02/2121:31
EDV
6020B
Dissolved Thallium
<0.570
Ng/L
0.570
2.00
1
11/05/21 14:05
EDV
6020B
Vanadium
2.09 J
ug/L
1.30
5.00
1
11/08/21 17:30
EDV
6020B
Dissolved Vanadium
<1.30
Ng/L
1.30
5.00
1
11/05/21 14:05
EDV
6020B
Zinc
10.91
ug/L
6.90
20.0
1
11/02/21 21:31
EDV
6020B
Dissolved Zinc
8.203
Ng/L
6.90
20.0
1
11/05/21 14:05
EDV
6020B
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 30 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98019
Matrix: Aqueous
Sample ID: MW-03-20211020
Sampled:
10/20/2021
10:40
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
1.923
Ng/L
1.80
5.00
1
11/01/21 09:05
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 09:05
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 09:05
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 09:05
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 09:05
JLB
V11000
Benzene
1.19
ug/L
0.180
0.500
1
11/01/21 09:05
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 09:05
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 09:05
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 09:05
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 09:05
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 09:05
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 09:05
JLB
V11000
Chlorobenzene
10.2
Ng/L
0.190
0.500
1
11/01/21 09:05
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 09:05
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 09:05
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 09:05
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 09:05
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 09:05
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 09:05
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 09:05
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 09:05
JLB
V11000
trans-1,4-Dichloro-2-butene
< 1.30
ug/L
1.30
10.0
1
11/01/21 09:05
JLB
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 31 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98019 Matrix: Aqueous
Sample ID: MW-03-20211020 Sampled: 10/20/2021 10:40
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 09:05
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 09:05
JLB
V11000
1,4-Dichlorobenzene
5.19
Ng/L
0.210
0.500
1
11/01/21 09:05
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 09:05
JLB
V11000
1,1-Dichloroethane
0.781
Ng/L
0.240
0.500
1
11/01/21 09:05
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 09:05
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 09:05
JLB
V11000
cis- 1,2-Dich loroethene
2.18
ug/L
0.200
0.500
1
11/01/21 09:05
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 09:05
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 09:05
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 09:05
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 09:05
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 09:05
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 09:05
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 09:05
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 09:05
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 09:05
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 09:05
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 09:05
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 09:05
JLB
V11000
Methyl Ethyl Ketone (MEK)
0.9693
Ng/L
0.710
5.00
1
11/01/21 09:05
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 09:05
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 32 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98019
Matrix: Aqueous
Sample ID: MW-03-20211020
Sampled:
10/20/2021
10:40
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 09:05
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 09:05
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 09:05
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 09:05
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 09:05
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 09:05
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 09:05
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 09:05
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 09:05
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 09:05
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 09:05
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 09:05
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 09:05
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 09:05
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 09:05
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 09:05
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 09:05
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 09:05
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 09:05
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 09:05
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 09:05
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 33 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98020
Matrix: Aqueous
Sample ID : TB-20211020B
Sampled:
10/20/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
Ng/L
1.80
5.00
1
11/01/21 04:34
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 04:34
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 04:34
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 04:34
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 04:34
JLB
V11000
Benzene
<0.180
ug/L
0.180
0.500
1
11/01/21 04:34
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 04:34
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 04:34
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 04:34
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 04:34
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 04:34
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 04:34
JLB
V11000
Chlorobenzene
<0.190
Ng/L
0.190
0.500
1
11/01/21 04:34
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 04:34
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 04:34
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 04:34
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 04:34
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 04:34
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 04:34
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 04:34
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 04:34
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 04:34
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation
Limit
Page 34 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98020 Matrix: Aqueous
Sample ID : TB-20211020B Sampled: 10/20/2021 0:00
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 04:34
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 04:34
JLB
V11000
1,4-Dichlorobenzene
<0.210
Ng/L
0.210
0.500
1
11/01/21 04:34
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 04:34
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 04:34
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 04:34
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 04:34
JLB
V11000
cis- 1,2-Dich loroethene
<0.200
ug/L
0.200
0.500
1
11/01/21 04:34
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 04:34
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 04:34
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 04:34
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 04:34
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 04:34
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 04:34
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 04:34
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 04:34
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 04:34
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 04:34
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 04:34
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 04:34
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 04:34
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 04:34
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation
Limit
Page 35 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98020
Matrix: Aqueous
Sample ID : TB-20211020B
Sampled:
10/20/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 04:34
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 04:34
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 04:34
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 04:34
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 04:34
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 04:34
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 04:34
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 04:34
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 04:34
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 04:34
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 04:34
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 04:34
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 04:34
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 04:34
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 04:34
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 04:34
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 04:34
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 04:34
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 04:34
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 04:34
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 04:34
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation
Limit
Page 36 of 129

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-295-8005
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/22/2021
Lab No : 98021
Matrix: Aqueous
Sample ID: MW-02-20211020
Sampled:
10/20/2021
19:10
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Methapyrilene
<23.8
Ng/L
23.8
47.6
1
10/27/21 22:38
VBW
8270D
1,4-Naphthoquinone
<23.8
ug/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
1-Naphthylamine
<23.8
Ng/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
2-Acetylaminofluorene
<23.8
ug/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
2-Naphthylamine
<23.8
Ng/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
3-Methylcholanthrene
<23.8
ug/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
4-Aminobiphenyl
<23.8
Ng/L
23.8
23.8
1
10/27/2122:38
VBW
8270D
5-Nitro-o-toluidine
<23.8
ug/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
7,12-Dimethyl benz(a)anth racene <23.8
Ng/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
Diallate
<23.8
pg/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
Hexachloropropene
<23.8 M
Ng/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
Isosafrole
<23.8
pg/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
N-Nitrosopiperidine
<23.8
Ng/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
N-Nitrosomethylethylamine
<23.8
pg/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
N-Nitrosomorpholine
<23.8
Ng/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
N-Nitrosopyrrolidine
<23.8
ug/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
0,0,0-Triethyl Phosphorothioate <0.785
Ng/L
0.785
2.38
1
10/27/21 18:39
VBW
8270C
o-Toluidine
<23.8
ug/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
p-Dimethylaminoazobenzene
<23.8
Ng/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
p-Phenylenediamine
<23.8 M
ug/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
Pronamide
<23.8
Ng/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
Safrole
<23.8
ug/L
23.8
23.8
1
10/27/21 22:38
VBW
8270D
Thionazine
<0.785
Ng/L
0.785
2.38
1
10/27/2118:39
VBW
8270C
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 37 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98021 Matrix: Aqueous
Sample ID: MW-02-20211020 Sampled: 10/20/2021 19:10
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Biochemical Oxygen Demand (5-day)
Nitrate (NO3-N)
<2000 Ng/L 2000 2000
255 Pg/L 76.0 200
1 10/22/21 10:46 SLO 5210E-2016
1 10/22/21 16:04 CEG 9056A
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 38 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98021 Matrix: Aqueous
Sample ID: MW-02-20211020 Sampled: 10/20/2021 19:10
Analytical Method: 8270C Prep Batch(es): L581531 10/27/21 16:00
Prep Method: 3510C
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Dimethoate
<1.70
Ng/L
1.70
2.38
1
10/27/21 18:39
VBW
L581686
Disulfoton
<1.11
u9/L
1.11
2.38
1
10/27/21 18:39
VBW
L581686
Ethyl Parathion
<1.35
Ng/L
1.35
2.38
1
10/27/21 18:39
VBW
L581686
Famphur
<1.22
ug/L
1.22
2.38
1
10/27/21 18:39
VBW
L581686
Methyl Parathion
<1.92
Ng/L
1.92
2.38
1
10/27/21 18:39
VBW
L581686
Phorate
<1.57
u9/L
1.57
2.38
1
10/27/21 18:39
VBW
L581686
Analytical Method:
8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dinitrobenzene
<2.15
ug/L
2.15
23.8
1
10/27/21 22:38
VBW
L581684
1,3,5-Trinitrobenzene
<23.8
Ng/L
23.8
23.8
1
10/27/21 22:38
VBW
L581685
Acenaphthene
<1.00
ug/L
1.00
4.76
1
10/27/21 22:38
VBW
L581684
Acenaphthylene
<1.02
Ng/L
1.02
4.76
1
10/27/21 22:38
VBW
L581684
Acetophenone
<1.63
ug/L
1.63
11.9
1
10/27/21 22:38
VBW
L581684
Anthracene
<1.11
Ng/L
1.11
4.76
1
10/27/21 22:38
VBW
L581684
Benzo(a)anthracene
<1.02
u9/L
1.02
4.76
1
10/27/21 22:38
VBW
L581684
Benzo(a)pyrene
<2.38
Ng/L
2.38
4.76
1
10/27/21 22:38
VBW
L581684
Benzo(b)fluoranthene
<2.24
u9/L
2.24
4.76
1
10/27/21 22:38
VBW
L581684
Benzo(g,h,i)perylene
<3.23
Ng/L
3.23
4.76
1
10/27/21 22:38
VBW
L581684
Benzo(k)fluoranthene
<1.79
ug/L
1.79
4.76
1
10/27/21 22:38
VBW
L581684
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 39 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98021 Matrix: Aqueous
Sample ID: MW-02-20211020 Sampled: 10/20/2021 19:10
Analytical Method: 8270D Prep Batch(es): L581529 10/27/21 16:00
Prep Method: 3510C
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Benzyl alcohol
<7.15
Ng/L
7.15
23.8
1
10/27/21 22:38
VBW
L581684
Bis(2-Chloroethoxy)methane
<1.03
ug/L
1.03
11.9
1
10/27/21 22:38
VBW
L581684
Bis(2-Chloroethyl)ether
<1.06
Ng/L
1.06
11.9
1
10/27/21 22:38
VBW
L581684
Bis(2-Chloroisopropyl)ether
<1.30
ug/L
1.30
11.9
1
10/27/21 22:38
VBW
L581684
Bis(2-ethylhexyl)phthalate
<8.71
Ng/L
8.71
11.9
1
10/27/21 22:38
VBW
L581684
4-Bromophenyl phenyl ether
<1.19
ug/L
1.19
11.9
1
10/27/21 22:38
VBW
L581684
Butyl benzyl phthalate
<10.9
Ng/L
10.9
11.9
1
10/27/21 22:38
VBW
L581684
4-Chloro-3-methylphenol
<1.20
ug/L
1.20
11.9
1
10/27/21 22:38
VBW
L581684
4-Chloroaniline
<1.25
Ng/L
1.25
11.9
1
10/27/21 22:38
VBW
L581684
Chlorobenzilate
<4.52
u9/L
4.52
11.9
1
10/27/21 22:38
VBW
L581684
2-Chloronaphthalene
<1.13
Ng/L
1.13
11.9
1
10/27/21 22:38
VBW
L581684
2-Chlorophenol
<1.75
ug/L
1.75
11.9
1
10/27/21 22:38
VBW
L581684
4-Chlorophenyl phenyl ether
<1.14
Ng/L
1.14
11.9
1
10/27/21 22:38
VBW
L581684
Chrysene
<1.74
ug/L
1.74
4.76
1
10/27/21 22:38
VBW
L581684
Dibenz(a,h)anthracene
<0.599
Ng/L
0.599
4.76
1
10/27/21 22:38
VBW
L581684
Dibenzofuran
<1.01
u9/L
1.01
11.9
1
10/27/21 22:38
VBW
L581684
1,2-Dichlorobenzene
<1.50
Ng/L
1.50
11.9
1
10/27/21 22:38
VBW
L581684
1,3-Dichlorobenzene
<1.17
ug/L
1.17
11.9
1
10/27/21 22:38
VBW
L581684
1,4-Dichlorobenzene
<1.38
Ng/L
1.38
11.9
1
10/27/21 22:38
VBW
L581684
3,3'-Dichlorobenzidine
<8.90
ug/L
8.90
23.8
1
10/27/21 22:38
VBW
L581684
2,4-Dichlorophenol
<3.62
Ng/L
3.62
11.9
1
10/27/21 22:38
VBW
L581684
2,6-Dichlorophenol
<1.67
ug/L
1.67
11.9
1
10/27/21 22:38
VBW
L581684
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 40 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98021 Matrix: Aqueous
Sample ID: MW-02-20211020 Sampled: 10/20/2021 19:10
Analytical Method: 8270D Prep Batch(es): L581529 10/27/21 16:00
Prep Method: 3510C
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Diethyl phthalate
4.413
Ng/L
1.39
11.9
1
10/27/21 22:38
VBW
L581684
Dimethyl phthalate
<1.21
u9/L
1.21
11.9
1
10/27/21 22:38
VBW
L581684
3,3' Dimethylbenzidine
<4.47
Ng/L
4.47
23.8
1
10/27/21 22:38
VBW
L581684
2,4-Dimethylphenol
<1.60
ug/L
1.60
11.9
1
10/27/21 22:38
VBW
L581684
Di-n-butyl phthalate
<3.75
Ng/L
3.75
11.9
1
10/27/21 22:38
VBW
L581684
4,6- Din itro-2- methyl phenol
<8.26
ug/L
8.26
23.8
1
10/27/21 22:38
VBW
L581684
2,4-Dinitrophenol
<11.5
Ng/L
11.5
23.8
1
10/27/21 22:38
VBW
L581684
2,4-Dinitrotoluene
<0.959
ug/L
0.959
11.9
1
10/27/21 22:38
VBW
L581684
2,6-Dinitrotoluene
<0.982
Ng/L
0.982
11.9
1
10/27/21 22:38
VBW
L581684
Di-n-Octyl Phthalate
<4.10
ug/L
4.10
11.9
1
10/27/21 22:38
VBW
L581684
Ethyl methanesulfonate
<1.70
Ng/L
1.70
11.9
1
10/27/21 22:38
VBW
L581684
Fluoranthene
<0.966
ug/L
0.966
4.76
1
10/27/21 22:38
VBW
L581684
Fluorene
<1.06
Ng/L
1.06
4.76
1
10/27/21 22:38
VBW
L581684
Hexachlorobenzene
<6.12
u9/L
6.12
11.9
1
10/27/21 22:38
VBW
L581684
Hexachlorobutadiene
<0.963
Ng/L
0.963
11.9
1
10/27/21 22:38
VBW
L581684
Hexachlorocyclopentadiene
<5.57
u9/L
5.57
11.9
1
10/27/21 22:38
VBW
L581684
Hexachloroethane
<0.659
Ng/L
0.659
11.9
1
10/27/21 22:38
VBW
L581684
Indeno(1,2,3-cd)pyrene
<2.41
ug/L
2.41
4.76
1
10/27/21 22:38
VBW
L581684
Isodrin
<23.8
Ng/L
23.8
23.8
1
10/27/21 22:38
VBW
L581685
Isophorone
<0.856
ug/L
0.856
11.9
1
10/27/21 22:38
VBW
L581684
Kepone
<23.8
Ng/L
23.8
23.8
1
10/27/21 22:38
VBW
L581685
Methyl methanesulfonate
<1.47
ug/L
1.47
11.9
1
10/27/21 22:38
VBW
L581684
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 41 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98021 Matrix: Aqueous
Sample ID: MW-02-20211020 Sampled: 10/20/2021 19:10
Analytical Method: 8270D Prep Batch(es): L581529 10/27/21 16:00
Prep Method: 3510C
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
2-Methylnaphthalene
<1.15
Ng/L
1.15
4.76
1
10/27/21 22:38
VBW
L581684
2-Methylphenol
<1.72
u9/L
1.72
11.9
1
10/27/21 22:38
VBW
L581684
3&4 Methylphenol
<1.64
Ng/L
1.64
11.9
1
10/27/21 22:38
VBW
L581684
Naphthalene
<1.15
ug/L
1.15
4.76
1
10/27/21 22:38
VBW
L581684
2-Nitroaniline
<1.37
Ng/L
1.37
11.9
1
10/27/21 22:38
VBW
L581684
3-Nitroaniline
<3.64
ug/L
3.64
23.8
1
10/27/21 22:38
VBW
L581684
4-Nitroaniline
<1.76
Ng/L
1.76
11.9
1
10/27/21 22:38
VBW
L581684
Nitrobenzene
<1.26
ug/L
1.26
11.9
1
10/27/21 22:38
VBW
L581684
2-Nitrophenol
<1.44
Ng/L
1.44
11.9
1
10/27/21 22:38
VBW
L581684
4-Nitrophenol
<3.31
ug/L
3.31
23.8
1
10/27/21 22:38
VBW
L581684
N-Nitrosodimethylamine
<0.592
Ng/L
0.592
11.9
1
10/27/21 22:38
VBW
L581684
N-Nitrosodiphenylamine
<1.86
ug/L
1.86
23.8
1
10/27/21 22:38
VBW
L581684
N-Nitrosodiethylamine
<0.952
Ng/L
0.952
11.9
1
10/27/21 22:38
VBW
L581684
N-Nitroso-di-n-butylamine
<1.79
ug/L
1.79
11.9
1
10/27/21 22:38
VBW
L581684
N-Nitroso-di-n-propylamine
<0.794
Ng/L
0.794
11.9
1
10/27/21 22:38
VBW
L581684
Pentachlorobenzene
<1.09
ug/L
1.09
23.8
1
10/27/21 22:38
VBW
L581684
Pentachloronitrobenzene
<2.74
Ng/L
2.74
11.9
1
10/27/21 22:38
VBW
L581684
Pentachlorophenol
<5.83
ug/L
5.83
23.8
1
10/27/21 22:38
VBW
L581684
Phenacetin
<3.05
Ng/L
3.05
11.9
1
10/27/21 22:38
VBW
L581684
Phenanthrene
<1.10
ug/L
1.10
4.76
1
10/27/21 22:38
VBW
L581684
Phenol
<0.925
Ng/L
0.925
11.9
1
10/27/21 22:38
VBW
L581684
Pyrene
<2.48
ug/L
2.48
4.76
1
10/27/21 22:38
VBW
L581684
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 42 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
Lab No : 98021
Sample ID: MW-02-20211020
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 10/20/2021 19:10
Analytical Method: 8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2,4,5-Tetrachlorobenzene
<0.754
Ng/L
0.754
11.9
1
10/27/2122:38
VBW
L581684
2,3,4,6-Tetrachlorophenol
<0.844
u9/L
0.844
11.9
1
10/27/2122:38
VBW
L581684
1,2,4-Trichlorobenzene
<1.15
Ng/L
1.15
11.9
1
10/27/2122:38
VBW
L581684
2,4,5-Trichlorophenol
<0.833
ug/L
0.833
11.9
1
10/27/2122:38
VBW
L581684
2,4,6-Trichlorophenol
<0.818
Ng/L
0.818
11.9
1
10/27/2122:38
VBW
L581684
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
M Minimum value MQL Method Quantitation Limit
Page 43 of 129

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-295-8005
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/22/2021
Lab No : 98022
Matrix: Aqueous
Sample ID: MW-03-20211020
Sampled:
10/20/2021
10:40
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Methapyrilene
<10.2
Ng/L
10.2
20.4
1
10/27/2123:00
VBW
8270D
1,4-Naphthoquinone
<10.2
ug/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
1-Naphthylamine
<10.2
Ng/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
2-Acetylaminofluorene
<10.2
ug/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
2-Naphthylamine
<10.2
Ng/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
3-Methylcholanthrene
<10.2
ug/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
4-Aminobiphenyl
<10.2
Ng/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
5-Nitro-o-toluidine
<10.2
ug/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
7,12-Dimethyl benz(a)anth racene <10.2
Ng/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
Diallate
<10.2
pg/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
Hexachloropropene
<10.2 M
Ng/L
10.2
10.2
1
10/27/21 23:00
VBW
8270D
Isosafrole
<10.2
pg/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
N-Nitrosopiperidine
<10.2
Ng/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
N-Nitrosomethylethylamine
<10.2
pg/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
N-Nitrosomorpholine
<10.2
Ng/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
N-Nitrosopyrrolidine
<10.2
ug/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
0,0,0-Triethyl Phosphorothioate <0.336
Ng/L
0.336
1.02
1
10/27/21 18:50
VBW
8270C
o-Toluidine
<10.2
ug/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
p-Dimethylaminoazobenzene
<10.2
Ng/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
p-Phenylenediamine
<10.2 M
ug/L
10.2
10.2
1
10/27/21 23:00
VBW
8270D
Pronamide
<10.2
Ng/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
Safrole
<10.2
ug/L
10.2
10.2
1
10/27/2123:00
VBW
8270D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 44 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98022 Matrix: Aqueous
Sample ID: MW-03-20211020 Sampled: 10/20/2021 10:40
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Thionazine <0.336 Ng/L 0.336 1.02 1 10/27/2118:50 VBW 8270C
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 45 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98022
Matrix: Aqueous
Sample ID: MW-03-20211020
Sampled:
10/20/2021
10:40
Analytical Method:
8270C
Prep Batch(es):
L581531
10/27/21 16:00
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Dimethoate
<0.727
Ng/L
0.727
1.02
1
10/27/21 18:50
VBW
L581686
Disulfoton
<0.475
ug/L
0.475
1.02
1
10/27/21 18:50
VBW
L581686
Ethyl Parathion
<0.579
Ng/L
0.579
1.02
1
10/27/21 18:50
VBW
L581686
Famphur
<0.522
ug/L
0.522
1.02
1
10/27/21 18:50
VBW
L581686
Methyl Parathion
<0.821
Ng/L
0.821
1.02
1
10/27/21 18:50
VBW
L581686
Phorate
<0.672
ug/L
0.672
1.02
1
10/27/21 18:50
VBW
L581686
Analytical Method:
8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dinitrobenzene
<0.922
ug/L
0.922
10.2
1
10/27/21 23:00
VBW
L581684
1,3,5-Trinitrobenzene
<10.2
Ng/L
10.2
10.2
1
10/27/21 23:00
VBW
L581685
Acenaphthene
<0.430
ug/L
0.430
2.04
1
10/27/21 23:00
VBW
L581684
Acenaphthylene
<0.437
Ng/L
0.437
2.04
1
10/27/21 23:00
VBW
L581684
Acetophenone
<0.699
ug/L
0.699
5.10
1
10/27/21 23:00
VBW
L581684
Anthracene
<0.476
Ng/L
0.476
2.04
1
10/27/21 23:00
VBW
L581684
Benzo(a)anthracene
<0.435
ug/L
0.435
2.04
1
10/27/21 23:00
VBW
L581684
Benzo(a)pyrene
<1.02
Ng/L
1.02
2.04
1
10/27/21 23:00
VBW
L581684
Benzo(b)fluoranthene
<0.959
ug/L
0.959
2.04
1
10/27/21 23:00
VBW
L581684
Benzo(g,h,i)perylene
<1.38
Ng/L
1.38
2.04
1
10/27/21 23:00
VBW
L581684
Benzo(k)fluoranthene
<0.767
ug/L
0.767
2.04
1
10/27/21 23:00
VBW
L581684
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 46 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98022 Matrix: Aqueous
Sample ID: MW-03-20211020 Sampled: 10/20/2021 10:40
Analytical Method: 8270D Prep Batch(es): L581529 10/27/21 16:00
Prep Method: 3510C
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Benzyl alcohol
<3.07
Ng/L
3.07
10.2
1
10/27/21 23:00
VBW
L581684
Bis(2-Chloroethoxy)methane
<0.441
ug/L
0.441
5.10
1
10/27/21 23:00
VBW
L581684
Bis(2-Chloroethyl)ether
<0.455
Ng/L
0.455
5.10
1
10/27/21 23:00
VBW
L581684
Bis(2-Chloroisopropyl)ether
<0.556
ug/L
0.556
5.10
1
10/27/21 23:00
VBW
L581684
Bis(2-ethylhexyl)phthalate
<3.73
Ng/L
3.73
5.10
1
10/27/21 23:00
VBW
L581684
4-Bromophenyl phenyl ether
<0.510
ug/L
0.510
5.10
1
10/27/21 23:00
VBW
L581684
Butyl benzyl phthalate
<4.69
Ng/L
4.69
5.10
1
10/27/21 23:00
VBW
L581684
4-Chloro-3-methylphenol
<0.513
ug/L
0.513
5.10
1
10/27/21 23:00
VBW
L581684
4-Chloroaniline
<0.536
Ng/L
0.536
5.10
1
10/27/21 23:00
VBW
L581684
Chlorobenzilate
<1.94
ug/L
1.94
5.10
1
10/27/21 23:00
VBW
L581684
2-Chloronaphthalene
<0.485
Ng/L
0.485
5.10
1
10/27/21 23:00
VBW
L581684
2-Chlorophenol
<0.750
ug/L
0.750
5.10
1
10/27/21 23:00
VBW
L581684
4-Chlorophenyl phenyl ether
<0.488
Ng/L
0.488
5.10
1
10/27/21 23:00
VBW
L581684
Chrysene
<0.745
ug/L
0.745
2.04
1
10/27/21 23:00
VBW
L581684
Dibenz(a,h)anthracene
<0.257
Ng/L
0.257
2.04
1
10/27/21 23:00
VBW
L581684
Dibenzofuran
<0.431
ug/L
0.431
5.10
1
10/27/21 23:00
VBW
L581684
1,2-Dichlorobenzene
<0.641
Ng/L
0.641
5.10
1
10/27/21 23:00
VBW
L581684
1,3-Dichlorobenzene
<0.500
ug/L
0.500
5.10
1
10/27/21 23:00
VBW
L581684
1,4-Dichlorobenzene
2.843
Ng/L
0.591
5.10
1
10/27/21 23:00
VBW
L581684
3,3'-Dichlorobenzidine
<3.81
ug/L
3.81
10.2
1
10/27/21 23:00
VBW
L581684
2,4-Dichlorophenol
<1.55
Ng/L
1.55
5.10
1
10/27/21 23:00
VBW
L581684
2,6-Dichlorophenol
<0.717
ug/L
0.717
5.10
1
10/27/21 23:00
VBW
L581684
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 47 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98022
Matrix: Aqueous
Sample ID: MW-03-20211020
Sampled:
10/20/2021
10:40
Analytical Method: 8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.596
Ng/L
0.596
5.10
1
10/27/21 23:00
VBW
L581684
Dimethyl phthalate
<0.520
ug/L
0.520
5.10
1
10/27/21 23:00
VBW
L581684
3,3' Dimethylbenzidine
<1.92
Ng/L
1.92
10.2
1
10/27/21 23:00
VBW
L581684
2,4-Dimethylphenol
<0.687
ug/L
0.687
5.10
1
10/27/21 23:00
VBW
L581684
Di-n-butyl phthalate
<1.61
Ng/L
1.61
5.10
1
10/27/21 23:00
VBW
L581684
4,6- Din itro-2- methyl phenol
<3.54
ug/L
3.54
10.2
1
10/27/21 23:00
VBW
L581684
2,4-Dinitrophenol
<4.95
Ng/L
4.95
10.2
1
10/27/21 23:00
VBW
L581684
2,4-Dinitrotoluene
<0.411
ug/L
0.411
5.10
1
10/27/21 23:00
VBW
L581684
2,6-Dinitrotoluene
<0.421
Ng/L
0.421
5.10
1
10/27/21 23:00
VBW
L581684
Di-n-Octyl Phthalate
<1.76
ug/L
1.76
5.10
1
10/27/21 23:00
VBW
L581684
Ethyl methanesulfonate
<0.728
Ng/L
0.728
5.10
1
10/27/21 23:00
VBW
L581684
Fluoranthene
<0.414
ug/L
0.414
2.04
1
10/27/21 23:00
VBW
L581684
Fluorene
<0.452
Ng/L
0.452
2.04
1
10/27/21 23:00
VBW
L581684
Hexachlorobenzene
<2.62
ug/L
2.62
5.10
1
10/27/21 23:00
VBW
L581684
Hexachlorobutadiene
<0.413
Ng/L
0.413
5.10
1
10/27/21 23:00
VBW
L581684
Hexachlorocyclopentadiene
<2.39
ug/L
2.39
5.10
1
10/27/21 23:00
VBW
L581684
Hexachloroethane
<0.282
Ng/L
0.282
5.10
1
10/27/21 23:00
VBW
L581684
Indeno(1,2,3-cd)pyrene
<1.03
ug/L
1.03
2.04
1
10/27/21 23:00
VBW
L581684
Isodrin
<10.2
Ng/L
10.2
10.2
1
10/27/21 23:00
VBW
L581685
Isophorone
<0.367
ug/L
0.367
5.10
1
10/27/21 23:00
VBW
L581684
Kepone
<10.2
Ng/L
10.2
10.2
1
10/27/21 23:00
VBW
L581685
Methyl methanesulfonate
<0.630
ug/L
0.630
5.10
1
10/27/21 23:00
VBW
L581684
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 48 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98022
Matrix: Aqueous
Sample ID: MW-03-20211020
Sampled:
10/20/2021
10:40
Analytical Method: 8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Methylnaphthalene
<0.494
Ng/L
0.494
2.04
1
10/27/21 23:00
VBW
L581684
2-Methylphenol
<0.735
ug/L
0.735
5.10
1
10/27/21 23:00
VBW
L581684
3&4 Methylphenol
<0.704
Ng/L
0.704
5.10
1
10/27/21 23:00
VBW
L581684
Naphthalene
<0.493
ug/L
0.493
2.04
1
10/27/21 23:00
VBW
L581684
2-Nitroaniline
<0.585
Ng/L
0.585
5.10
1
10/27/21 23:00
VBW
L581684
3-Nitroaniline
<1.56
ug/L
1.56
10.2
1
10/27/21 23:00
VBW
L581684
4-Nitroaniline
<0.754
Ng/L
0.754
5.10
1
10/27/21 23:00
VBW
L581684
Nitrobenzene
<0.541
ug/L
0.541
5.10
1
10/27/21 23:00
VBW
L581684
2-Nitrophenol
<0.618
Ng/L
0.618
5.10
1
10/27/21 23:00
VBW
L581684
4-Nitrophenol
<1.42
ug/L
1.42
10.2
1
10/27/21 23:00
VBW
L581684
N-Nitrosodimethylamine
<0.253
Ng/L
0.253
5.10
1
10/27/21 23:00
VBW
L581684
N-Nitrosodiphenylamine
<0.798
ug/L
0.798
10.2
1
10/27/21 23:00
VBW
L581684
N-Nitrosodiethylamine
<0.408
Ng/L
0.408
5.10
1
10/27/21 23:00
VBW
L581684
N-Nitroso-di-n-butylamine
<0.767
ug/L
0.767
5.10
1
10/27/21 23:00
VBW
L581684
N-Nitroso-di-n-propylamine
<0.340
Ng/L
0.340
5.10
1
10/27/21 23:00
VBW
L581684
Pentachlorobenzene
<0.468
ug/L
0.468
10.2
1
10/27/21 23:00
VBW
L581684
Pentachloronitrobenzene
<1.17
Ng/L
1.17
5.10
1
10/27/21 23:00
VBW
L581684
Pentachlorophenol
<2.50
ug/L
2.50
10.2
1
10/27/21 23:00
VBW
L581684
Phenacetin
<1.31
Ng/L
1.31
5.10
1
10/27/21 23:00
VBW
L581684
Phenanthrene
<0.473
ug/L
0.473
2.04
1
10/27/21 23:00
VBW
L581684
Phenol
<0.396
Ng/L
0.396
5.10
1
10/27/21 23:00
VBW
L581684
Pyrene
<1.06
ug/L
1.06
2.04
1
10/27/21 23:00
VBW
L581684
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 49 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
Lab No : 98022
Sample ID: MW-03-20211020
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 10/20/2021 10:40
Analytical Method: 8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2,4,5-Tetrachlorobenzene
<0.323
Ng/L
0.323
5.10
1
10/27/2123:00
VBW
L581684
2,3,4,6-Tetrachlorophenol
<0.362
ug/L
0.362
5.10
1
10/27/2123:00
VBW
L581684
1,2,4-Trichlorobenzene
<0.491
Ng/L
0.491
5.10
1
10/27/2123:00
VBW
L581684
2,4,5-Trichlorophenol
<0.357
ug/L
0.357
5.10
1
10/27/2123:00
VBW
L581684
2,4,6-Trichlorophenol
<0.350
Ng/L
0.350
5.10
1
10/27/2123:00
VBW
L581684
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
M Minimum value MQL Method Quantitation Limit
Page 50 of 129

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-295-8005
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/22/2021
Lab No : 98023
Matrix: Aqueous
Sample ID: MW-01-20211020
Sampled:
10/20/2021
16:34
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Methapyrilene
<10.2
Ng/L
10.2
20.4
1
10/27/2123:22
VBW
8270D
1,4-Naphthoquinone
<10.2
ug/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
1-Naphthylamine
<10.2
Ng/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
2-Acetylaminofluorene
<10.2
ug/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
2-Naphthylamine
<10.2
Ng/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
3-Methylcholanthrene
<10.2
ug/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
4-Aminobiphenyl
<10.2
Ng/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
5-Nitro-o-toluidine
<10.2
ug/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
7,12-Dimethyl benz(a)anth racene <10.2
Ng/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
Diallate
<10.2
pg/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
Hexachloropropene
<10.2 M
Ng/L
10.2
10.2
1
10/27/21 23:22
VBW
8270D
Isosafrole
<10.2
pg/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
N-Nitrosopiperidine
<10.2
Ng/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
N-Nitrosomethylethylamine
<10.2
pg/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
N-Nitrosomorpholine
<10.2
Ng/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
N-Nitrosopyrrolidine
<10.2
ug/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
0,0,0-Triethyl Phosphorothioate <0.336
Ng/L
0.336
1.02
1
10/27/21 19:02
VBW
8270C
o-Toluidine
<10.2
ug/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
p-Dimethylaminoazobenzene
<10.2
Ng/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
p-Phenylenediamine
<10.2 M
ug/L
10.2
10.2
1
10/27/21 23:22
VBW
8270D
Pronamide
<10.2
Ng/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
Safrole
<10.2
ug/L
10.2
10.2
1
10/27/2123:22
VBW
8270D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 51 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98023 Matrix: Aqueous
Sample ID: MW-01-20211020 Sampled: 10/20/2021 16:34
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Thionazine <0.336 Ng/L 0.336 1.02 1 10/27/2119:02 VBW 8270C
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 52 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98023
Matrix: Aqueous
Sample ID: MW-01-20211020
Sampled:
10/20/2021
16:34
Analytical Method:
8270C
Prep Batch(es):
L581531
10/27/21 16:00
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Dimethoate
<0.727
Ng/L
0.727
1.02
1
10/27/21 19:02
VBW
L581686
Disulfoton
<0.475
ug/L
0.475
1.02
1
10/27/21 19:02
VBW
L581686
Ethyl Parathion
<0.579
Ng/L
0.579
1.02
1
10/27/21 19:02
VBW
L581686
Famphur
<0.522
ug/L
0.522
1.02
1
10/27/21 19:02
VBW
L581686
Methyl Parathion
<0.821
Ng/L
0.821
1.02
1
10/27/21 19:02
VBW
L581686
Phorate
<0.672
ug/L
0.672
1.02
1
10/27/21 19:02
VBW
L581686
Analytical Method:
8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dinitrobenzene
<0.922
ug/L
0.922
10.2
1
10/27/21 23:22
VBW
L581684
1,3,5-Trinitrobenzene
<10.2
Ng/L
10.2
10.2
1
10/27/21 23:22
VBW
L581685
Acenaphthene
<0.430
ug/L
0.430
2.04
1
10/27/21 23:22
VBW
L581684
Acenaphthylene
<0.437
Ng/L
0.437
2.04
1
10/27/21 23:22
VBW
L581684
Acetophenone
<0.699
ug/L
0.699
5.10
1
10/27/21 23:22
VBW
L581684
Anthracene
<0.476
Ng/L
0.476
2.04
1
10/27/21 23:22
VBW
L581684
Benzo(a)anthracene
<0.435
ug/L
0.435
2.04
1
10/27/21 23:22
VBW
L581684
Benzo(a)pyrene
<1.02
Ng/L
1.02
2.04
1
10/27/21 23:22
VBW
L581684
Benzo(b)fluoranthene
<0.959
ug/L
0.959
2.04
1
10/27/21 23:22
VBW
L581684
Benzo(g,h,i)perylene
<1.38
Ng/L
1.38
2.04
1
10/27/21 23:22
VBW
L581684
Benzo(k)fluoranthene
<0.767
ug/L
0.767
2.04
1
10/27/21 23:22
VBW
L581684
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 53 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98023 Matrix: Aqueous
Sample ID: MW-01-20211020 Sampled: 10/20/2021 16:34
Analytical Method: 8270D Prep Batch(es): L581529 10/27/21 16:00
Prep Method: 3510C
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Benzyl alcohol
<3.07
Ng/L
3.07
10.2
1
10/27/21 23:22
VBW
L581684
Bis(2-Chloroethoxy)methane
<0.441
ug/L
0.441
5.10
1
10/27/21 23:22
VBW
L581684
Bis(2-Chloroethyl)ether
<0.455
Ng/L
0.455
5.10
1
10/27/21 23:22
VBW
L581684
Bis(2-Chloroisopropyl)ether
<0.556
ug/L
0.556
5.10
1
10/27/21 23:22
VBW
L581684
Bis(2-ethylhexyl)phthalate
<3.73
Ng/L
3.73
5.10
1
10/27/21 23:22
VBW
L581684
4-Bromophenyl phenyl ether
<0.510
ug/L
0.510
5.10
1
10/27/21 23:22
VBW
L581684
Butyl benzyl phthalate
<4.69
Ng/L
4.69
5.10
1
10/27/21 23:22
VBW
L581684
4-Chloro-3-methylphenol
<0.513
ug/L
0.513
5.10
1
10/27/21 23:22
VBW
L581684
4-Chloroaniline
<0.536
Ng/L
0.536
5.10
1
10/27/21 23:22
VBW
L581684
Chlorobenzilate
<1.94
ug/L
1.94
5.10
1
10/27/21 23:22
VBW
L581684
2-Chloronaphthalene
<0.485
Ng/L
0.485
5.10
1
10/27/21 23:22
VBW
L581684
2-Chlorophenol
<0.750
ug/L
0.750
5.10
1
10/27/21 23:22
VBW
L581684
4-Chlorophenyl phenyl ether
<0.488
Ng/L
0.488
5.10
1
10/27/21 23:22
VBW
L581684
Chrysene
<0.745
ug/L
0.745
2.04
1
10/27/21 23:22
VBW
L581684
Dibenz(a,h)anthracene
<0.257
Ng/L
0.257
2.04
1
10/27/21 23:22
VBW
L581684
Dibenzofuran
<0.431
ug/L
0.431
5.10
1
10/27/21 23:22
VBW
L581684
1,2-Dichlorobenzene
<0.641
Ng/L
0.641
5.10
1
10/27/21 23:22
VBW
L581684
1,3-Dichlorobenzene
<0.500
ug/L
0.500
5.10
1
10/27/21 23:22
VBW
L581684
1,4-Dichlorobenzene
3.723
Ng/L
0.591
5.10
1
10/27/21 23:22
VBW
L581684
3,3'-Dichlorobenzidine
<3.81
ug/L
3.81
10.2
1
10/27/21 23:22
VBW
L581684
2,4-Dichlorophenol
<1.55
Ng/L
1.55
5.10
1
10/27/21 23:22
VBW
L581684
2,6-Dichlorophenol
<0.717
ug/L
0.717
5.10
1
10/27/21 23:22
VBW
L581684
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 54 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98023 Matrix: Aqueous
Sample ID: MW-01-20211020 Sampled: 10/20/2021 16:34
Analytical Method: 8270D Prep Batch(es): L581529 10/27/21 16:00
Prep Method: 3510C
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Diethyl phthalate
0.6513
Ng/L
0.596
5.10
1
10/27/21 23:22
VBW
L581684
Dimethyl phthalate
<0.520
ug/L
0.520
5.10
1
10/27/21 23:22
VBW
L581684
3,3' Dimethylbenzidine
<1.92
Ng/L
1.92
10.2
1
10/27/21 23:22
VBW
L581684
2,4-Dimethylphenol
<0.687
ug/L
0.687
5.10
1
10/27/21 23:22
VBW
L581684
Di-n-butyl phthalate
<1.61
Ng/L
1.61
5.10
1
10/27/21 23:22
VBW
L581684
4,6- Din itro-2- methyl phenol
<3.54
ug/L
3.54
10.2
1
10/27/21 23:22
VBW
L581684
2,4-Dinitrophenol
<4.95
Ng/L
4.95
10.2
1
10/27/21 23:22
VBW
L581684
2,4-Dinitrotoluene
<0.411
ug/L
0.411
5.10
1
10/27/21 23:22
VBW
L581684
2,6-Dinitrotoluene
<0.421
Ng/L
0.421
5.10
1
10/27/21 23:22
VBW
L581684
Di-n-Octyl Phthalate
<1.76
ug/L
1.76
5.10
1
10/27/21 23:22
VBW
L581684
Ethyl methanesulfonate
<0.728
Ng/L
0.728
5.10
1
10/27/21 23:22
VBW
L581684
Fluoranthene
<0.414
ug/L
0.414
2.04
1
10/27/21 23:22
VBW
L581684
Fluorene
<0.452
Ng/L
0.452
2.04
1
10/27/21 23:22
VBW
L581684
Hexachlorobenzene
<2.62
ug/L
2.62
5.10
1
10/27/21 23:22
VBW
L581684
Hexachlorobutadiene
<0.413
Ng/L
0.413
5.10
1
10/27/21 23:22
VBW
L581684
Hexachlorocyclopentadiene
<2.39
ug/L
2.39
5.10
1
10/27/21 23:22
VBW
L581684
Hexachloroethane
<0.282
Ng/L
0.282
5.10
1
10/27/21 23:22
VBW
L581684
Indeno(1,2,3-cd)pyrene
<1.03
ug/L
1.03
2.04
1
10/27/21 23:22
VBW
L581684
Isodrin
<10.2
Ng/L
10.2
10.2
1
10/27/21 23:22
VBW
L581685
Isophorone
<0.367
ug/L
0.367
5.10
1
10/27/21 23:22
VBW
L581684
Kepone
<10.2
Ng/L
10.2
10.2
1
10/27/21 23:22
VBW
L581685
Methyl methanesulfonate
<0.630
ug/L
0.630
5.10
1
10/27/21 23:22
VBW
L581684
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 55 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98023
Matrix: Aqueous
Sample ID: MW-01-20211020
Sampled:
10/20/2021
16:34
Analytical Method: 8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Methylnaphthalene
<0.494
Ng/L
0.494
2.04
1
10/27/21 23:22
VBW
L581684
2-Methylphenol
<0.735
ug/L
0.735
5.10
1
10/27/21 23:22
VBW
L581684
3&4 Methylphenol
<0.704
Ng/L
0.704
5.10
1
10/27/21 23:22
VBW
L581684
Naphthalene
<0.493
ug/L
0.493
2.04
1
10/27/21 23:22
VBW
L581684
2-Nitroaniline
<0.585
Ng/L
0.585
5.10
1
10/27/21 23:22
VBW
L581684
3-Nitroaniline
<1.56
ug/L
1.56
10.2
1
10/27/21 23:22
VBW
L581684
4-Nitroaniline
<0.754
Ng/L
0.754
5.10
1
10/27/21 23:22
VBW
L581684
Nitrobenzene
<0.541
ug/L
0.541
5.10
1
10/27/21 23:22
VBW
L581684
2-Nitrophenol
<0.618
Ng/L
0.618
5.10
1
10/27/21 23:22
VBW
L581684
4-Nitrophenol
<1.42
ug/L
1.42
10.2
1
10/27/21 23:22
VBW
L581684
N-Nitrosodimethylamine
<0.253
Ng/L
0.253
5.10
1
10/27/21 23:22
VBW
L581684
N-Nitrosodiphenylamine
<0.798
ug/L
0.798
10.2
1
10/27/21 23:22
VBW
L581684
N-Nitrosodiethylamine
<0.408
Ng/L
0.408
5.10
1
10/27/21 23:22
VBW
L581684
N-Nitroso-di-n-butylamine
<0.767
u9/L
0.767
5.10
1
10/27/21 23:22
VBW
L581684
N-Nitroso-di-n-propylamine
<0.340
Ng/L
0.340
5.10
1
10/27/21 23:22
VBW
L581684
Pentachlorobenzene
<0.468
ug/L
0.468
10.2
1
10/27/21 23:22
VBW
L581684
Pentachloronitrobenzene
<1.17
Ng/L
1.17
5.10
1
10/27/21 23:22
VBW
L581684
Pentachlorophenol
<2.50
ug/L
2.50
10.2
1
10/27/21 23:22
VBW
L581684
Phenacetin
<1.31
Ng/L
1.31
5.10
1
10/27/21 23:22
VBW
L581684
Phenanthrene
<0.473
ug/L
0.473
2.04
1
10/27/21 23:22
VBW
L581684
Phenol
<0.396
Ng/L
0.396
5.10
1
10/27/21 23:22
VBW
L581684
Pyrene
<1.06
ug/L
1.06
2.04
1
10/27/21 23:22
VBW
L581684
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 56 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
Lab No : 98023
Sample ID: MW-01-20211020
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 10/20/2021 16:34
Analytical Method: 8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2,4,5-Tetrachlorobenzene
<0.323
Ng/L
0.323
5.10
1
10/27/2123:22
VBW
L581684
2,3,4,6-Tetrachlorophenol
<0.362
ug/L
0.362
5.10
1
10/27/2123:22
VBW
L581684
1,2,4-Trichlorobenzene
<0.491
Ng/L
0.491
5.10
1
10/27/2123:22
VBW
L581684
2,4,5-Trichlorophenol
<0.357
ug/L
0.357
5.10
1
10/27/2123:22
VBW
L581684
2,4,6-Trichlorophenol
<0.350
Ng/L
0.350
5.10
1
10/27/2123:22
VBW
L581684
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
M Minimum value MQL Method Quantitation Limit
Page 57 of 129

WavDdibnto
ANALYTICAL
01015
Anchor QEA of North Carolina, PLLC
Chuck Pippin
231 Haywood Street
Asheville , NC 28801
Report Number : 21-295-8005
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Project ID :
Project Jackson County
Information :
REPORT OF ANAL YSIS
Report Date : 12/21/2021
Received : 10/22/2021
Lab No : 98024
Matrix: Aqueous
Sample ID: MW-06-20211020
Sampled:
10/20/2021
13:36
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Methapyrilene
<10.1
Ng/L
10.1
20.2
1
10/27/2123:44
VBW
8270D
1,4-Naphthoquinone
<10.1
ug/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
1-Naphthylamine
<10.1
Ng/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
2-Acetylaminofluorene
<10.1
ug/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
2-Naphthylamine
<10.1
Ng/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
3-Methylcholanthrene
<10.1
ug/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
4-Aminobiphenyl
<10.1
Ng/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
5-Nitro-o-toluidine
<10.1
ug/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
7,12-Dimethyl benz(a)anth racene <10.1
Ng/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
Diallate
<10.1
pg/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
Hexachloropropene
<10.1 M
Ng/L
10.1
10.1
1
10/27/21 23:44
VBW
8270D
Isosafrole
<10.1
pg/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
N-Nitrosopiperidine
<10.1
Ng/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
N-Nitrosomethylethylamine
<10.1
pg/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
N-Nitrosomorpholine
<10.1
Ng/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
N-Nitrosopyrrolidine
<10.1
ug/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
0,0,0-Triethyl Phosphorothioate <0.333
Ng/L
0.333
1.01
1
10/27/21 19:14
VBW
8270C
o-Toluidine
<10.1
ug/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
p-Dimethylaminoazobenzene
<10.1
Ng/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
p-Phenylenediamine
<10.1 M
ug/L
10.1
10.1
1
10/27/21 23:44
VBW
8270D
Pronamide
<10.1
Ng/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
Safrole
<10.1
ug/L
10.1
10.1
1
10/27/2123:44
VBW
8270D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
L
Limit Exceeded
M
Minimum
value
MQL
Method Quantitation Limit
Page 58 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98024 Matrix: Aqueous
Sample ID: MW-06-20211020 Sampled: 10/20/2021 13:36
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Thionazine <0.333 Ng/L 0.333 1.01 1 10/27/2119:14 VBW 8270C
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 59 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98024
Matrix: Aqueous
Sample ID: MW-06-20211020
Sampled:
10/20/2021
13:36
Analytical Method:
8270C
Prep Batch(es):
L581531
10/27/21 16:00
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Dimethoate
<0.720
Ng/L
0.720
1.01
1
10/27/21 19:14
VBW
L581686
Disulfoton
<0.470
ug/L
0.470
1.01
1
10/27/21 19:14
VBW
L581686
Ethyl Parathion
<0.573
Ng/L
0.573
1.01
1
10/27/21 19:14
VBW
L581686
Famphur
<0.517
ug/L
0.517
1.01
1
10/27/21 19:14
VBW
L581686
Methyl Parathion
<0.813
Ng/L
0.813
1.01
1
10/27/21 19:14
VBW
L581686
Phorate
<0.665
ug/L
0.665
1.01
1
10/27/21 19:14
VBW
L581686
Analytical Method:
8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method:
3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,3-Dinitrobenzene
<0.913
ug/L
0.913
10.1
1
10/27/21 23:44
VBW
L581684
1,3,5-Trinitrobenzene
<10.1
Ng/L
10.1
10.1
1
10/27/21 23:44
VBW
L581685
Acenaphthene
<0.426
ug/L
0.426
2.02
1
10/27/21 23:44
VBW
L581684
Acenaphthylene
<0.433
Ng/L
0.433
2.02
1
10/27/21 23:44
VBW
L581684
Acetophenone
<0.692
ug/L
0.692
5.05
1
10/27/21 23:44
VBW
L581684
Anthracene
<0.471
Ng/L
0.471
2.02
1
10/27/21 23:44
VBW
L581684
Benzo(a)anthracene
<0.431
ug/L
0.431
2.02
1
10/27/21 23:44
VBW
L581684
Benzo(a)pyrene
<1.01
Ng/L
1.01
2.02
1
10/27/21 23:44
VBW
L581684
Benzo(b)fluoranthene
<0.950
ug/L
0.950
2.02
1
10/27/21 23:44
VBW
L581684
Benzo(g,h,i)perylene
<1.37
Ng/L
1.37
2.02
1
10/27/21 23:44
VBW
L581684
Benzo(k)fluoranthene
<0.759
ug/L
0.759
2.02
1
10/27/21 23:44
VBW
L581684
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 60 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98024 Matrix: Aqueous
Sample ID: MW-06-20211020 Sampled: 10/20/2021 13:36
Analytical Method: 8270D Prep Batch(es): L581529 10/27/21 16:00
Prep Method: 3510C
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Benzyl alcohol
<3.04
Ng/L
3.04
10.1
1
10/27/21 23:44
VBW
L581684
Bis(2-Chloroethoxy)methane
<0.437
u9/L
0.437
5.05
1
10/27/21 23:44
VBW
L581684
Bis(2-Chloroethyl)ether
<0.451
Ng/L
0.451
5.05
1
10/27/21 23:44
VBW
L581684
Bis(2-Chloroisopropyl)ether
<0.551
ug/L
0.551
5.05
1
10/27/21 23:44
VBW
L581684
Bis(2-ethylhexyl)phthalate
<3.70
Ng/L
3.70
5.05
1
10/27/21 23:44
VBW
L581684
4-Bromophenyl phenyl ether
<0.505
ug/L
0.505
5.05
1
10/27/21 23:44
VBW
L581684
Butyl benzyl phthalate
<4.64
Ng/L
4.64
5.05
1
10/27/21 23:44
VBW
L581684
4-Chloro-3-methylphenol
<0.508
ug/L
0.508
5.05
1
10/27/21 23:44
VBW
L581684
4-Chloroaniline
<0.531
Ng/L
0.531
5.05
1
10/27/21 23:44
VBW
L581684
Chlorobenzilate
<1.92
u9/L
1.92
5.05
1
10/27/21 23:44
VBW
L581684
2-Chloronaphthalene
<0.480
Ng/L
0.480
5.05
1
10/27/21 23:44
VBW
L581684
2-Chlorophenol
<0.743
ug/L
0.743
5.05
1
10/27/21 23:44
VBW
L581684
4-Chlorophenyl phenyl ether
<0.483
Ng/L
0.483
5.05
1
10/27/21 23:44
VBW
L581684
Chrysene
<0.738
ug/L
0.738
2.02
1
10/27/21 23:44
VBW
L581684
Dibenz(a,h)anthracene
<0.254
Ng/L
0.254
2.02
1
10/27/21 23:44
VBW
L581684
Dibenzofuran
<0.427
ug/L
0.427
5.05
1
10/27/21 23:44
VBW
L581684
1,2-Dichlorobenzene
<0.635
Ng/L
0.635
5.05
1
10/27/21 23:44
VBW
L581684
1,3-Dichlorobenzene
<0.495
ug/L
0.495
5.05
1
10/27/21 23:44
VBW
L581684
1,4-Dichlorobenzene
0.8223
Ng/L
0.585
5.05
1
10/27/21 23:44
VBW
L581684
3,3'-Dichlorobenzidine
<3.78
ug/L
3.78
10.1
1
10/27/21 23:44
VBW
L581684
2,4-Dichlorophenol
<1.54
Ng/L
1.54
5.05
1
10/27/21 23:44
VBW
L581684
2,6-Dichlorophenol
<0.710
ug/L
0.710
5.05
1
10/27/21 23:44
VBW
L581684
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 61 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98024
Matrix: Aqueous
Sample ID: MW-06-20211020
Sampled:
10/20/2021
13:36
Analytical Method: 8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Diethyl phthalate
<0.590
Ng/L
0.590
5.05
1
10/27/21 23:44
VBW
L581684
Dimethyl phthalate
<0.515
ug/L
0.515
5.05
1
10/27/21 23:44
VBW
L581684
3,3' Dimethylbenzidine
<1.90
Ng/L
1.90
10.1
1
10/27/21 23:44
VBW
L581684
2,4-Dimethylphenol
<0.680
ug/L
0.680
5.05
1
10/27/21 23:44
VBW
L581684
Di-n-butyl phthalate
<1.59
Ng/L
1.59
5.05
1
10/27/21 23:44
VBW
L581684
4,6- Din itro-2- methyl phenol
<3.50
ug/L
3.50
10.1
1
10/27/21 23:44
VBW
L581684
2,4-Dinitrophenol
<4.90
Ng/L
4.90
10.1
1
10/27/21 23:44
VBW
L581684
2,4-Dinitrotoluene
<0.407
ug/L
0.407
5.05
1
10/27/21 23:44
VBW
L581684
2,6-Dinitrotoluene
<0.417
Ng/L
0.417
5.05
1
10/27/21 23:44
VBW
L581684
Di-n-Octyl Phthalate
<1.74
ug/L
1.74
5.05
1
10/27/21 23:44
VBW
L581684
Ethyl methanesulfonate
<0.721
Ng/L
0.721
5.05
1
10/27/21 23:44
VBW
L581684
Fluoranthene
<0.410
ug/L
0.410
2.02
1
10/27/21 23:44
VBW
L581684
Fluorene
<0.448
Ng/L
0.448
2.02
1
10/27/21 23:44
VBW
L581684
Hexachlorobenzene
<2.60
ug/L
2.60
5.05
1
10/27/21 23:44
VBW
L581684
Hexachlorobutadiene
<0.409
Ng/L
0.409
5.05
1
10/27/21 23:44
VBW
L581684
Hexachlorocyclopentadiene
<2.36
ug/L
2.36
5.05
1
10/27/21 23:44
VBW
L581684
Hexachloroethane
<0.279
Ng/L
0.279
5.05
1
10/27/21 23:44
VBW
L581684
Indeno(1,2,3-cd)pyrene
<1.02
ug/L
1.02
2.02
1
10/27/21 23:44
VBW
L581684
Isodrin
<10.1
Ng/L
10.1
10.1
1
10/27/21 23:44
VBW
L581685
Isophorone
<0.363
ug/L
0.363
5.05
1
10/27/21 23:44
VBW
L581684
Kepone
<10.1
Ng/L
10.1
10.1
1
10/27/21 23:44
VBW
L581685
Methyl methanesulfonate
<0.624
ug/L
0.624
5.05
1
10/27/21 23:44
VBW
L581684
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 62 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98024
Matrix: Aqueous
Sample ID: MW-06-20211020
Sampled:
10/20/2021
13:36
Analytical Method: 8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Methylnaphthalene
<0.489
Ng/L
0.489
2.02
1
10/27/21 23:44
VBW
L581684
2-Methylphenol
<0.728
ug/L
0.728
5.05
1
10/27/21 23:44
VBW
L581684
3&4 Methylphenol
<0.697
Ng/L
0.697
5.05
1
10/27/21 23:44
VBW
L581684
Naphthalene
<0.488
ug/L
0.488
2.02
1
10/27/21 23:44
VBW
L581684
2-Nitroaniline
<0.579
Ng/L
0.579
5.05
1
10/27/21 23:44
VBW
L581684
3-Nitroaniline
<1.55
ug/L
1.55
10.1
1
10/27/21 23:44
VBW
L581684
4-Nitroaniline
<0.747
Ng/L
0.747
5.05
1
10/27/21 23:44
VBW
L581684
Nitrobenzene
<0.536
ug/L
0.536
5.05
1
10/27/21 23:44
VBW
L581684
2-Nitrophenol
<0.612
Ng/L
0.612
5.05
1
10/27/21 23:44
VBW
L581684
4-Nitrophenol
<1.40
ug/L
1.40
10.1
1
10/27/21 23:44
VBW
L581684
N-Nitrosodimethylamine
<0.251
Ng/L
0.251
5.05
1
10/27/21 23:44
VBW
L581684
N-Nitrosodiphenylamine
<0.790
ug/L
0.790
10.1
1
10/27/21 23:44
VBW
L581684
N-Nitrosodiethylamine
<0.404
Ng/L
0.404
5.05
1
10/27/21 23:44
VBW
L581684
N-Nitroso-di-n-butylamine
<0.759
ug/L
0.759
5.05
1
10/27/21 23:44
VBW
L581684
N-Nitroso-di-n-propylamine
<0.337
Ng/L
0.337
5.05
1
10/27/21 23:44
VBW
L581684
Pentachlorobenzene
<0.463
ug/L
0.463
10.1
1
10/27/21 23:44
VBW
L581684
Pentachloronitrobenzene
<1.16
Ng/L
1.16
5.05
1
10/27/21 23:44
VBW
L581684
Pentachlorophenol
<2.47
ug/L
2.47
10.1
1
10/27/21 23:44
VBW
L581684
Phenacetin
<1.29
Ng/L
1.29
5.05
1
10/27/21 23:44
VBW
L581684
Phenanthrene
<0.468
ug/L
0.468
2.02
1
10/27/21 23:44
VBW
L581684
Phenol
<0.392
Ng/L
0.392
5.05
1
10/27/21 23:44
VBW
L581684
Pyrene
<1.05
ug/L
1.05
2.02
1
10/27/21 23:44
VBW
L581684
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 63 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
Lab No : 98024
Sample ID: MW-06-20211020
REPOR T OF A NA L YSIS
Matrix: Aqueous
Sampled: 10/20/2021 13:36
Analytical Method: 8270D
Prep Batch(es):
L581529
10/27/21 16:00
Prep Method: 3510C
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2,4,5-Tetrachlorobenzene
<0.320
Ng/L
0.320
5.05
1
10/27/2123:44
VBW
L581684
2,3,4,6-Tetrachlorophenol
<0.358
ug/L
0.358
5.05
1
10/27/2123:44
VBW
L581684
1,2,4-Trichlorobenzene
<0.486
Ng/L
0.486
5.05
1
10/27/2123:44
VBW
L581684
2,4,5-Trichlorophenol
<0.353
ug/L
0.353
5.05
1
10/27/2123:44
VBW
L581684
2,4,6-Trichlorophenol
<0.347
Ng/L
0.347
5.05
1
10/27/2123:44
VBW
L581684
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
M Minimum value MQL Method Quantitation Limit
Page 64 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98025
Sample ID: LT-01-20211020
Matrix: Aqueous
Sampled: 10/20/2021 17:25
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
1,4-Dioxane
48.8
Ng/L
0.139
2.00
1
10/28/21 12:24
TBL
8260D SIM
Antimony
<2.45
ug/L
2.45
10.0
5
11/02/21 21:38
EDV
6020B
Arsenic
4.003
Ng/L
0.850
5.00
5
11/02/21 21:38
EDV
6020B
Barium
372
ug/L
4.05
50.0
5
11/02/21 21:38
EDV
6020B
Beryllium
<0.950
Ng/L
0.950
5.00
5
11/02/21 21:38
EDV
6020B
Cadmium
<0.800
ug/L
0.800
5.00
5
11/02/21 21:38
EDV
6020B
Chromium
<3.95
Ng/L
3.95
10.0
5
11/02/21 21:38
EDV
6020B
Cobalt
5.833
ug/L
2.60
10.0
5
11/02/21 21:38
EDV
6020B
Copper
<19.0
Ng/L
19.0
50.0
5
11/02/21 21:38
EDV
6020B
Lead
<1.30
ug/L
1.30
5.00
5
11/02/21 21:38
EDV
6020B
Mercury (Total)
<0.0700
Ng/L
0.0700
0.200
1
11/02/21 18:26
EDV
7470A
Nickel
24.2
ug/L
2.55
15.0
5
11/02/21 21:38
EDV
6020B
Selenium
<3.70
Ng/L
3.70
25.0
5
11/02/21 21:38
EDV
6020B
Silver
<0.550
ug/L
0.550
5.00
5
11/02/21 21:38
EDV
6020B
Tin
<1.80
Ng/L
1.80
5.00
1
11/05/2114:58
EDV
6020B
Thallium
<2.85
ug/L
2.85
10.0
5
11/02/21 21:38
EDV
6020B
Vanadium
3.423
Ng/L
1.30
5.00
1
11/08/21 17:49
EDV
6020B
Zinc
<34.5
ug/L
34.5
100
5
11/02/21 21:38
EDV
6020B
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time J Estimated value
L Limit Exceeded M Minimum value
MQL Method Quantitation Limit
Page 65 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98025
Matrix: Aqueous
Sample ID: LT-01-20211020
Sampled:
10/20/2021
17:25
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
V11027
11/01/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
8.14
Ng/L
1.80
5.00
1
11/01/21 10:19
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 10:19
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 10:19
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 10:19
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 10:19
JLB
V11000
Benzene
2.45
ug/L
0.180
0.500
1
11/01/21 10:19
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 10:19
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 10:19
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 10:19
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 10:19
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 10:19
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 10:19
JLB
V11000
Chlorobenzene
4.28
Ng/L
0.190
0.500
1
11/01/21 10:19
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 10:19
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 10:19
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 10:19
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 10:19
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 10:19
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 10:19
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 10:19
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 10:19
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 10:19
JLB
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 66 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98025 Matrix: Aqueous
Sample ID: LT-01-20211020 Sampled: 10/20/2021 17:25
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00 V11027 11/01/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 10:19
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 10:19
JLB
V11000
1,4-Dichlorobenzene
3.85
Ng/L
0.210
0.500
1
11/01/21 10:19
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 10:19
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 10:19
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 10:19
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 10:19
JLB
V11000
cis- 1,2-Dich loroethene
<0.200
ug/L
0.200
0.500
1
11/01/21 10:19
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 10:19
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 10:19
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 10:19
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 10:19
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 10:19
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 10:19
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 10:19
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 10:19
JLB
V11000
Ethylbenzene
0.838
Ng/L
0.170
0.500
1
11/01/21 10:19
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 10:19
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 10:19
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 10:19
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 10:19
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 10:19
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 67 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98025
Matrix: Aqueous
Sample ID: LT-01-20211020
Sampled:
10/20/2021
17:25
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
V11027
11/01/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 10:19
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 10:19
JLB
V11000
Naphthalene
13.6
Ng/L
0.470
1.00
1
11/01/21 10:19
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 10:19
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 10:19
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 10:19
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 10:19
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 10:19
JLB
V11000
Tetrahydrofuran
203
Ng/L
15.0
100
10
11/01/21 19:07
JLB
V11028
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 10:19
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 10:19
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 10:19
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 10:19
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 10:19
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 10:19
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 10:19
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 10:19
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 10:19
JLB
V11000
o-Xylene
1.64
Ng/L
0.210
0.500
1
11/01/21 10:19
JLB
V11000
m,p-Xylene
1.17
ug/L
0.420
1.00
1
11/01/21 10:19
JLB
V11000
Xylene (Total)
2.81
Ng/L
0.210
0.500
1
11/01/21 10:19
V11000
Qualifiers/ B Analyte detected in blank
DF
Dilution Factor
Definitions H Beyond holding
time
J
Estimated value
M Minimum value
MQL
Method Quantitation Limit
Page 68 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98026
Matrix: Aqueous
Sample ID : TB-20211020C
Sampled:
10/20/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<1.80
Ng/L
1.80
5.00
1
11/01/21 05:23
JLB
V11000
Acetonitrile
<20.3
ug/L
20.3
10.0
1
11/01/21 05:23
JLB
V11000
Acrolein
<2.00
Ng/L
2.00
5.00
1
11/01/21 05:23
JLB
V11000
Acrylonitrile
<0.230
ug/L
0.230
5.00
1
11/01/21 05:23
JLB
V11000
Allyl Chloride
<0.579
Ng/L
0.579
10.0
1
11/01/21 05:23
JLB
V11000
Benzene
<0.180
ug/L
0.180
0.500
1
11/01/21 05:23
JLB
V11000
Bromochloromethane
<0.420
Ng/L
0.420
1.00
1
11/01/21 05:23
JLB
V11000
Bromodichloromethane
<0.160
ug/L
0.160
0.500
1
11/01/21 05:23
JLB
V11000
Bromoform
<1.50
Ng/L
1.50
5.00
1
11/01/21 05:23
JLB
V11000
Bromomethane
<0.280
ug/L
0.280
1.00
1
11/01/21 05:23
JLB
V11000
Carbon Disulfide
<0.150
Ng/L
0.150
5.00
1
11/01/21 05:23
JLB
V11000
Carbon Tetrachloride
<0.180
ug/L
0.180
0.500
1
11/01/21 05:23
JLB
V11000
Chlorobenzene
<0.190
Ng/L
0.190
0.500
1
11/01/21 05:23
JLB
V11000
Chlorodibromomethane
<0.190
ug/L
0.190
0.500
1
11/01/21 05:23
JLB
V11000
Chloroethane
<0.430
Ng/L
0.430
1.00
1
11/01/21 05:23
JLB
V11000
Chloroform
<0.220
ug/L
0.220
0.500
1
11/01/21 05:23
JLB
V11000
Chloromethane
<0.220
Ng/L
0.220
0.500
1
11/01/21 05:23
JLB
V11000
Chloroprene
<0.450
ug/L
0.450
10.0
1
11/01/21 05:23
JLB
V11000
1,2-Dibromo-3-Chloropropane
<1.10
Ng/L
1.10
2.00
1
11/01/21 05:23
JLB
V11000
1,2-Dibromoethane
<0.200
ug/L
0.200
0.500
1
11/01/21 05:23
JLB
V11000
Dibromomethane
<0.230
Ng/L
0.230
0.500
1
11/01/21 05:23
JLB
V11000
trans-1,4-Dichloro-2-butene
<1.30
ug/L
1.30
10.0
1
11/01/21 05:23
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 69 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005
REPORT OF ANAL YSIS
Lab No : 98026 Matrix: Aqueous
Sample ID : TB-20211020C Sampled: 10/20/2021 0:00
Analytical Method: 8260D Prep Batch(es): V10999 10/31/21 09:00
Prep Method: 5030E
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,2-Dichlorobenzene
<0.220
Ng/L
0.220
0.500
1
11/01/21 05:23
JLB
V11000
1,3-Dichlorobenzene
<0.190
ug/L
0.190
0.500
1
11/01/21 05:23
JLB
V11000
1,4-Dichlorobenzene
<0.210
Ng/L
0.210
0.500
1
11/01/21 05:23
JLB
V11000
Dichlorodifluoromethane
<1.20
ug/L
1.20
5.00
1
11/01/21 05:23
JLB
V11000
1,1-Dichloroethane
<0.240
Ng/L
0.240
0.500
1
11/01/21 05:23
JLB
V11000
1,2-Dichloroethane
<0.150
ug/L
0.150
0.500
1
11/01/21 05:23
JLB
V11000
1,1-Dichloroethene
<0.150
Ng/L
0.150
0.500
1
11/01/21 05:23
JLB
V11000
cis- 1,2-Dich loroethene
<0.200
ug/L
0.200
0.500
1
11/01/21 05:23
JLB
V11000
trans-1,2-Dichloroethene
<0.180
Ng/L
0.180
0.500
1
11/01/21 05:23
JLB
V11000
1,2-Dichloropropane
<0.190
ug/L
0.190
0.500
1
11/01/21 05:23
JLB
V11000
1,3-Dichloropropane
<0.130
Ng/L
0.130
0.500
1
11/01/21 05:23
JLB
V11000
2,2-Dichloropropane
<0.210
ug/L
0.210
2.00
1
11/01/21 05:23
JLB
V11000
1,1-Dichloropropene
<0.200
Ng/L
0.200
0.500
1
11/01/21 05:23
JLB
V11000
cis- 1,3-Dich loropropene
<0.210
ug/L
0.210
0.500
1
11/01/21 05:23
JLB
V11000
trans-1,3-Dichloropropene
<0.150
Ng/L
0.150
0.500
1
11/01/21 05:23
JLB
V11000
Ethyl Methacrylate
<1.62
ug/L
1.62
10.0
1
11/01/21 05:23
JLB
V11000
Ethylbenzene
<0.170
Ng/L
0.170
0.500
1
11/01/21 05:23
JLB
V11000
Hexachlorobutadiene
<0.350
ug/L
0.350
2.00
1
11/01/21 05:23
JLB
V11000
2-Hexanone
<0.380
Ng/L
0.380
5.00
1
11/01/21 05:23
JLB
V11000
Iodomethane
<0.054
ug/L
0.054
0.500
1
11/01/21 05:23
JLB
V11000
Methyl Ethyl Ketone (MEK)
<0.710
Ng/L
0.710
5.00
1
11/01/21 05:23
JLB
V11000
Methacrylonitrile
<12.6
ug/L
12.6
10.0
1
11/01/21 05:23
JLB
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 70 of 129

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
01015 Project ID
Anchor QEA of North Carolina, PLLC Project Jackson County
Chuck Pippin Report Date : 12/21/2021
231 Haywood Street Information : Received : 10/22/2021
Asheville , NC 28801
Report Number : 21-295-8005 REPOR T OF A NA L YSIS
Lab No : 98026
Matrix: Aqueous
Sample ID : TB-20211020C
Sampled:
10/20/2021
0:00
Analytical Method: 8260D
Prep Batch(es):
V10999
10/31/21 09:00
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
4-Methyl-2-Pentanone
<1.00
Ng/L
1.00
5.00
1
11/01/21 05:23
JLB
V11000
Methylene Chloride
<0.330
ug/L
0.330
1.00
1
11/01/21 05:23
JLB
V11000
Naphthalene
<0.470
Ng/L
0.470
1.00
1
11/01/21 05:23
JLB
V11000
Propionitrile
<23.7
ug/L
23.7
10.0
1
11/01/21 05:23
JLB
V11000
Styrene
<0.220
Ng/L
0.220
0.500
1
11/01/21 05:23
JLB
V11000
1,1,1,2-Tetrachloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 05:23
JLB
V11000
1,1,2,2-Tetrachloroethane
<0.160
Ng/L
0.160
0.500
1
11/01/21 05:23
JLB
V11000
Tetrachloroethene
<0.220
ug/L
0.220
0.500
1
11/01/21 05:23
JLB
V11000
Tetrahydrofuran
<1.50
Ng/L
1.50
10.0
1
11/01/21 05:23
JLB
V11000
Toluene
<0.220
ug/L
0.220
0.500
1
11/01/21 05:23
JLB
V11000
1,2,4-Trichlorobenzene
<0.310
Ng/L
0.310
1.00
1
11/01/21 05:23
JLB
V11000
1,1,1-Trichloroethane
<0.160
ug/L
0.160
0.500
1
11/01/21 05:23
JLB
V11000
1,1,2-Trichloroethane
<0.096
Ng/L
0.096
0.500
1
11/01/21 05:23
JLB
V11000
Trichloroethene
<0.180
ug/L
0.180
0.500
1
11/01/21 05:23
JLB
V11000
Trichlorofluoromethane
<0.180
Ng/L
0.180
0.500
1
11/01/21 05:23
JLB
V11000
1,2,3-Trichloropropane
<0.270
ug/L
0.270
1.00
1
11/01/21 05:23
JLB
V11000
Vinyl Acetate
<1.00
Ng/L
1.00
2.00
1
11/01/21 05:23
JLB
V11000
Vinyl Chloride
<0.170
ug/L
0.170
0.500
1
11/01/21 05:23
JLB
V11000
o-Xylene
<0.210
Ng/L
0.210
0.500
1
11/01/21 05:23
JLB
V11000
m,p-Xylene
<0.420
ug/L
0.420
1.00
1
11/01/21 05:23
JLB
V11000
Xylene (Total)
<0.21
Ng/L
0.210
0.500
1
11/01/21 05:23
V11000
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions H
Beyond holding time
J
Estimated value
M
Minimum value
MQL
Method Quantitation Limit
Page 71 of 129

lacioAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
November 01, 2021
Robbi A. Jones
Prism Laboratories, Inc.
P.O. Box 240543
Charlotte, NC 28224
RE: Project: DW VOC
Pace Project No.: 92568536
Dear Robbi Jones:
Enclosed are the analytical results for sample(s) received by the laboratory on October 25, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Angela Overcash, Prism
V AtQ
REPORT OF LABORATORY ANALYSIS
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B ;
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I
Project: DW VOC
Pace Project No.: 92568536
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
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Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: DW VOC
Pace Project No.: 92568536
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92568536001 DW-01
EPA 524.2
CLT
24
PASI-O
92568536002 DW-02
EPA 524.2
CLT
24
PASI-O
92568536003 TB
EPA 524.2
CLT
24
PASI-O
PASI-O = Pace Analytical Services - Ormond Beach
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ANALYTICAL RESULTS
Project: DW VOC
Pace Project No.: 92568536
Sample: DW-01 Lab ID: 92568536001 Collected: 10/20/21 00:00 Received: 10/25/21 09:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
524.2 MSV
Analytical Method: EPA 524.2
Pace Analytical
Services - Ormond
Beach
Benzene
ND
mg/L
0.00050
1
10/29/21 14:34
71-43-2
Carbon tetrachloride
ND
mg/L
0.00050
1
10/29/21 14:34
56-23-5
Chlorobenzene
ND
mg/L
0.00050
1
10/29/21 14:34
108-90-7
1,2-Dichlorobenzene
ND
mg/L
0.00050
1
10/29/21 14:34
95-50-1
1,4-Dichlorobenzene
ND
mg/L
0.00050
1
10/29/21 14:34
106-46-7
1,2-Dichloroethane
ND
mg/L
0.00050
1
10/29/21 14:34
107-06-2
1,1-Dichloroethene
ND
mg/L
0.00050
1
10/29/21 14:34
75-35-4
cis-1,2-Dichloroethene
ND
mg/L
0.00050
1
10/29/21 14:34
156-59-2
trans- 1 2- Dich loroethene
ND
mg/L
0.00050
1
10/29/21 14:34
156-60-5
1,2-Dichloropropane
ND
mg/L
0.00050
1
10/29/21 14:34
78-87-5
Ethylbenzene
ND
mg/L
0.00050
1
10/29/21 14:34
100-41-4
Methylene Chloride
ND
mg/L
0.0010
1
10/29/21 14:34
75-09-2
Styrene
ND
mg/L
0.00050
1
10/29/21 14:34
100-42-5
Tetrachloroethene
ND
mg/L
0.00050
1
10/29/21 14:34
127-18-4
Toluene
ND
mg/L
0.00050
1
10/29/21 14:34
108-88-3
1,2,4-Trichlorobenzene
ND
mg/L
0.00050
1
10/29/21 14:34
120-82-1
1,1,1-Trichloroethane
ND
mg/L
0.00050
1
10/29/21 14:34
71-55-6
1,1,2-Trichloroethane
ND
mg/L
0.00050
1
10/29/21 14:34
79-00-5
Trichloroethene
ND
mg/L
0.00050
1
10/29/21 14:34
79-01-6
Vinyl chloride
ND
mg/L
0.00050
1
10/29/21 14:34
75-01-4
Xylene (Total)
ND
mg/L
0.0010
1
10/29/21 14:34
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
91
%
70-130
1
10/29/21 14:34
460-00-4
Toluene-d8 (S)
102
%
70-130
1
10/29/21 14:34
2037-26-5
1,2-Dichlorobenzene-d4 (S)
102
%
70-130
1
10/29/21 14:34
2199-69-1
Sample: DW-02 Lab ID: 92568536002 Collected: 10/20/21 00:00 Received: 10/25/21 09:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
524.2 MSV
Analytical Method: EPA 524.2
Pace Analytical
Services - Ormond
Beach
Benzene
ND
mg/L
0.00050
1
10/29/21 14:58
71-43-2
Carbon tetrachloride
ND
mg/L
0.00050
1
10/29/21 14:58
56-23-5
Chlorobenzene
ND
mg/L
0.00050
1
10/29/21 14:58
108-90-7
1,2-Dichlorobenzene
ND
mg/L
0.00050
1
10/29/21 14:58
95-50-1
1,4-Dichlorobenzene
ND
mg/L
0.00050
1
10/29/21 14:58
106-46-7
1,2-Dichloroethane
ND
mg/L
0.00050
1
10/29/21 14:58
107-06-2
1,1-Dichloroethene
ND
mg/L
0.00050
1
10/29/21 14:58
75-35-4
cis- 1,2-Dichloroethene
ND
mg/L
0.00050
1
10/29/21 14:58
156-59-2
trans- 1 2- Dich loroethene
ND
mg/L
0.00050
1
10/29/21 14:58
156-60-5
1,2-Dichloropropane
ND
mg/L
0.00050
1
10/29/21 14:58
78-87-5
Ethylbenzene
ND
mg/L
0.00050
1
10/29/21 14:58
100-41-4
Methylene Chloride
ND
mg/L
0.0010
1
10/29/21 14:58
75-09-2
Styrene
ND
mg/L
0.00050
1
10/29/21 14:58
100-42-5
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: DW VOC
Pace Project No.: 92568536
Sample: DW-02 Lab ID: 92568536002 Collected: 10/20/21 00:00 Received: 10/25/21 09:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
524.2 MSV
Tetrachloroethene
Toluene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichlorobenzene-d4 (S)
Analytical Method: EPA 524.2
Pace Analytical Services - Ormond Beach
ND
mg/L
0.00050
ND
mg/L
0.00050
ND
mg/L
0.00050
ND
mg/L
0.00050
ND
mg/L
0.00050
ND
mg/L
0.00050
ND
mg/L
0.00050
ND
mg/L
0.0010
91
%
70-130
101
%
70-130
102
%
70-130
1 10/29/21 14:58
127-18-4
1 10/29/21 14:58
108-88-3
1 10/29/21 14:58
120-82-1
1 10/29/21 14:58
71-55-6
1 10/29/21 14:58
79-00-5
1 10/29/21 14:58
79-01-6
1 10/29/21 14:58
75-01-4
1 10/29/21 14:58
1330-20-7
1 10/29/21 14:58
460-00-4
1 10/29/21 14:58
2037-26-5
1 10/29/21 14:58
2199-69-1
Sample: TB Lab ID: 92568536003 Collected: 10/20/21 00:00 Received: 10/25/21 09:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
524.2 MSV
Analytical Method: EPA 524.2
Pace Analytical
Services - Ormond
Beach
Benzene
ND
mg/L
0.00050
1
10/29/21 15:22
71-43-2
Carbon tetrachloride
ND
mg/L
0.00050
1
10/29/21 15:22
56-23-5
Chlorobenzene
ND
mg/L
0.00050
1
10/29/21 15:22
108-90-7
1,2-Dichlorobenzene
ND
mg/L
0.00050
1
10/29/21 15:22
95-50-1
1,4-Dichlorobenzene
ND
mg/L
0.00050
1
10/29/21 15:22
106-46-7
1,2-Dichloroethane
ND
mg/L
0.00050
1
10/29/21 15:22
107-06-2
1,1-Dichloroethene
ND
mg/L
0.00050
1
10/29/21 15:22
75-35-4
cis- 1,2-Dichloroethene
ND
mg/L
0.00050
1
10/29/21 15:22
156-59-2
trans- 1 2- Dich loroethene
ND
mg/L
0.00050
1
10/29/21 15:22
156-60-5
1,2-Dichloropropane
ND
mg/L
0.00050
1
10/29/21 15:22
78-87-5
Ethylbenzene
ND
mg/L
0.00050
1
10/29/21 15:22
100-41-4
Methylene Chloride
ND
mg/L
0.0010
1
10/29/21 15:22
75-09-2
Styrene
ND
mg/L
0.00050
1
10/29/21 15:22
100-42-5
Tetrachloroethene
ND
mg/L
0.00050
1
10/29/21 15:22
127-18-4
Toluene
ND
mg/L
0.00050
1
10/29/21 15:22
108-88-3
1,2,4-Trichlorobenzene
ND
mg/L
0.00050
1
10/29/21 15:22
120-82-1
1,1,1-Trichloroethane
ND
mg/L
0.00050
1
10/29/21 15:22
71-55-6
1,1,2-Trichloroethane
ND
mg/L
0.00050
1
10/29/21 15:22
79-00-5
Trichloroethene
ND
mg/L
0.00050
1
10/29/21 15:22
79-01-6
Vinyl chloride
ND
mg/L
0.00050
1
10/29/21 15:22
75-01-4
Xylene (Total)
ND
mg/L
0.0010
1
10/29/21 15:22
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
93
%
70-130
1
10/29/21 15:22
460-00-4
Toluene-d8 (S)
100
%
70-130
1
10/29/21 15:22
2037-26-5
1,2-Dichlorobenzene-d4 (S)
103
%
70-130
1
10/29/21 15:22
2199-69-1
Date: 11/01/2021 01:22 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: DW VOC
Pace Project No.: 92568536
QC Batch: 773685 Analysis Method: EPA 524.2
QC Batch Method: EPA 524.2 Analysis Description: 524.2 MSV
Laboratory: Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92568536001, 92568536002, 92568536003
METHOD BLANK: 4235070 Matrix:
Associated Lab Samples: 92568536001, 92568536002, 92568536003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed Qualifiers
1,1,1-Trichloroethane
mg/L
ND
0.00050
10/29/21 13:21
1,1,2-Trichloroethane
mg/L
ND
0.00050
10/29/21 13:21
1,1-Dichloroethene
mg/L
ND
0.00050
10/29/21 13:21
1,2,4-Trichlorobenzene
mg/L
ND
0.00050
10/29/21 13:21
1,2-Dichlorobenzene
mg/L
ND
0.00050
10/29/21 13:21
1,2-Dichloroethane
mg/L
ND
0.00050
10/29/21 13:21
1,2-Dichloropropane
mg/L
ND
0.00050
10/29/21 13:21
1,4-Dichlorobenzene
mg/L
ND
0.00050
10/29/21 13:21
Benzene
mg/L
ND
0.00050
10/29/21 13:21
Carbon tetrachloride
mg/L
ND
0.00050
10/29/21 13:21
Chlorobenzene
mg/L
ND
0.00050
10/29/21 13:21
cis-1,2-Dichloroethene
mg/L
ND
0.00050
10/29/21 13:21
Ethylbenzene
mg/L
ND
0.00050
10/29/21 13:21
Methylene Chloride
mg/L
ND
0.0010
10/29/21 13:21
Styrene
mg/L
ND
0.00050
10/29/21 13:21
Tetrachloroethene
mg/L
ND
0.00050
10/29/21 13:21
Toluene
mg/L
ND
0.00050
10/29/21 13:21
trans- 1 2- Dich loroethene
mg/L
ND
0.00050
10/29/21 13:21
Trichloroethene
mg/L
ND
0.00050
10/29/21 13:21
Vinyl chloride
mg/L
ND
0.00050
10/29/21 13:21
Xylene (Total)
mg/L
ND
0.0010
10/29/21 13:21
1,2-Dichlorobenzene-d4(S)
%
104
70-130
10/29/21 13:21
4-Bromofluorobenzene (S)
%
90
70-130
10/29/21 13:21
Toluene-d8 (S)
%
99
70-130
10/29/21 13:21
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
4235071
Units
Spike
Conc.
4235072
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
1,1,1-Trichloroethane
mg/L
0.02
0.018
0.018
91
89
70-130
2
20
1,1,2-Trichloroethane
mg/L
0.02
0.020
0.020
99
98
70-130
2
20
1,1-Dichloroethene
mg/L
0.02
0.019
0.018
93
91
70-130
2
20
1,2,4-Trichlorobenzene
mg/L
0.02
0.017
0.017
84
86
70-130
2
20
1,2-Dichlorobenzene
mg/L
0.02
0.020
0.020
99
99
70-130
0
20
1,2-Dichloroethane
mg/L
0.02
0.019
0.018
93
90
70-130
2
20
1,2-Dichloropropane
mg/L
0.02
0.019
0.018
95
92
70-130
3
20
1,4-Dichlorobenzene
mg/L
0.02
0.020
0.020
101
100
70-130
1
20
Benzene
mg/L
0.02
0.019
0.019
95
93
70-130
2
20
Carbon tetrachloride
mg/L
0.02
0.019
0.019
94
93
70-130
2
20
Chlorobenzene
mg/L
0.02
0.018
0.018
90
88
70-130
2
20
Results presented on this page are in the units indicated
by the "Units"
column except where an alternate unit is
presented to the right of the
result.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA
Project: DW VOC
Pace Project No.: 92568536
LABORATORY CONTROL SAMPLE & LCSD:
4235071
4235072
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
cis-1,2-Dichloroethene
mg/L
0.02
0.019
0.019
94
95
70-130
2
20
Ethylbenzene
mg/L
0.02
0.019
0.019
94
93
70-130
1
20
Methylene Chloride
mg/L
0.02
0.020
0.020
102
99
70-130
2
20
Styrene
mg/L
0.02
0.020
0.020
98
98
70-130
1
20
Tetrachloroethene
mg/L
0.02
0.018
0.018
92
90
70-130
3
20
Toluene
mg/L
0.02
0.018
0.018
91
90
70-130
1
20
trans- 1 2- Dich loroethene
mg/L
0.02
0.018
0.018
91
89
70-130
2
20
Trichloroethene
mg/L
0.02
0.018
0.018
92
90
70-130
2
20
Vinyl chloride
mg/L
0.02
0.019
0.019
95
94
70-130
1
20
Xylene (Total)
mg/L
0.06
0.059
0.058
98
97
70-130
1
20
1,2-Dichlorobenzene-d4(S)
%
98
98
70-130
4-Bromofluorobenzene (S)
%
95
95
70-130
Toluene-d8 (S)
%
101
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11 /01 /2021 01:22 PM without the written consent of Pace Analytical Services, LLC.
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[phone]
QUALIFIERS
Project: DW VOC
Pace Project No.: 92568536
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DW VOC
Pace Project No.: 92568536
Lab ID
Sample ID
QC Batch Method
QC Batch
92568536001
DW-01
EPA 524.2
773685
92568536002
DW-02
EPA 524.2
773685
92568536003
TB
EPA 524.2
773685
Date: 11/01/2021 01:22 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 9 of 12
Page 80 of 129

Document Name: Document Revised: October 28, 2020
WCeAnalytical' Sample Condition Upon Recelpt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F•CAR-CS•033•Rev,07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[]Greenwood ❑ Huntersville Raleigh _ Mechaniicsviile AtlantaFl Kernersu,illeEl
ConditionSample Client Name:
Upon ReceiptPrc WO# : 92568536
❑Courier. ❑Fed Ex ❑UPS ❑U5P5 aClient 111111111111111 IIII �II
Commercial [:]Pace Other:
/ 82566536
Custody Seal Present? Dyes []No Seals Intact? []Yes QNo 1 /
Date/tnRlalsFersan Examining Contents:/ i]1J 57(V
Packing Material: ❑Bubble Wrap ❑Bubble Bags []None❑ Other Biological Tissue Frozen?
Thermometer: Des ❑No []N/A
I-1 iR G-,P in• 't , r,1,9 [ Net ❑BSue ❑None
'~ J YPe a ice: —' -
r 4 C 'C-Correction Factor:
Cooler Temp: -- I t) Add/Subtract (°Cj ' Temp should be above freezing to 6°C
(q / ❑Samplesaut of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected -(°,Cf)•� has begun
USDA Regulated Sall ( [ /A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC {check maps)? Did sampes originate from a foreign source (InternaVonalfy,
f lyes FlNo . n..
L-J
Comments/Discrepancy:
Chain of Custody Present?
dyes
[--]No
❑NSA
1.
-Samples Arrived within Hold Time?
Short Hold Time Analysis <7I hr.)?
Efyes
Elves
[]NO
ONo
❑N/A
❑N/A
2.
3.
Rush Turn Around Time Requested?
❑Yes
�o
❑N/A
4.
Sufficient Volume?
Yes
❑Na
INA
5,
Correct Containers Used?
-Pace Containers Used?
[7 es
Yes
❑No
❑No
❑N/A
❑N/A
6.
Containers Intact?
Lyres
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
[:]No
4/A
g.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
f fres
❑No
❑N/A
4.
Headspace in VOA Vials (>5-5mm)?
❑Yes
No
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
©Yes
❑Yes
❑No
011s0
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of splilcontainers:
CLIENT NOTIFICATION/RESC)LUTION
Person -cunt -acted; Datum
Project Manager SCURF Review:
Project Manager SRF Review:
Date:
Date:
Field Data Required? []yes []NO
Page 81 of 129

Document Name: Document Revised' October 28, 2020
Condition Upon Receipt(SOUR) Page 2 of 2
Document No.: Issuing AutharitV:
F-CAR-C"33-Aev.07 Para ('Arnlinac (]nality Office
*Check mark top half of box If pH and/or dechlorination is Pro- WO ; g2568536
verified and within the acceptance range for preservation
samn es. PM: MWB Due Date: 1I/oi /7i
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (waterl DOC, LLHg CLIENT: 92—Prism
"Bottom Ralf of box is to list number of bottles
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot a
Note: -When eve rthere-iMdiscrepancy-affecting-North-C-arol ina-[Umpliane�samples,-a eopy-of4his-form-wilVbe-sent-to.the-Nurth-Carolina [J6HNR-Gertiflcatian DFTice [I,a.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 82 of 129

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Page 12 of 12
Page 83 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-295-8005
QC Analytical Batch:
V10803
Analysis Method:
2320B-2011
Analysis Description:
Alkalinity
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples:
97987, 97988, 98018,
98019
Blank MDL
MQL
Analyzed
Parameter
Units
Result
Alkalinity (as CaCO3)
pg/L
<800 800
5000
10/27/21 10:20
Laboratory Control Sample
LCS
Spike
LCS
LCS %Rec % Rec
Parameter
Units
Conc.
Result
Limits
Alkalinity (as CaCO3)
pg/L
250000
250000
100 90-110
Duplicate
V 98019-DUP
Result DUP
RPD Max RPD
Analyzed
Parameter
Units
Result
Alkalinity (as CaCO3)
pg/L
51000 52000
1.9 20
10/27/21 10:20
Date: 12/21/2021 12:58 PM Page 1 of 40
Page 84 of 129

•
Waypoint,
449 Springbrook
Charlotte, NC 28217
Rd, Ch
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Analytical Batch: V10772
Analysis Method: 4500S2F-2011
Analysis Description: Sulfide
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples: 97987, 97988, 98018, 98019
Blank
MQL
Analyzed
Parameter Units
Result
Sulfide pg/L
<2000
2000
10/26/2109:45
Laboratory Control Sample
LCS
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Sulfide pg/L
10000
9000
90.0 70-122
Matrix Spike
V 97992-MS
MS Spike
MSD MS Result
MSD MS %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec Limits RPD
Conc.
Sulfide pg/L
<2000 10000
7000
70.0 70-130
Date: 12/21/2021 12:58 PM Page 2 of 40
Page 85 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Analytical Batch: V10823
Analysis Method: 5210B-2016
Analysis Description: Biochemical Oxygen Demand (BOD)
Glucose-Glutamic Acid GGA
Result Range Analyzed
Parameter Units
Biochemical Oxygen Demand (5-day) Ng/L 180 167.5-228.E 10/22/21 10:46
Duplicate V 97874-DUP
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Biochemical Oxygen Demand (5-day) Ng/L 14200 11900 17.6 30 10/22/21 10:46
Date: 12/21/2021 12:58 PM Page 3 of 40
Page 86 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Analytical Batch: V10695
Analysis Method: 5220D-2011
Analysis Description: Chemical Oxygen Demand (COD)
Lab Reagent Blank LRB
Matrix: AQU
Associated Lab Samples: 97987, 97988, 98018, 98019
Blank MDL
MQL
Analyzed
Parameter Units Result
COD (Chemical Oxygen Demand) pg/L <11000 11000
50000
10/25/21 11:16
Laboratory Control Sample LCS
Spike
LCS
LCS %Rec
% Rec
Parameter Units Conc.
Result
Limits
COD (Chemical Oxygen Demand) pg/L 500000
526000
105
90-110
Matrix Spike & Matrix Spike Duplicate V 97861-MS V 97861-MSD
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter Units Result Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
COD (Chemical Oxygen Demand) pg/L 82000 500000
500000 587000
555000 101
95.0 80-120 5.6 20
Date: 12/21/2021 12:58 PM Page 4 of 40
Page 87 of 129

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality
Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: L581990
QC Analytical Batch(es): L582004
QC Prep Batch Method: 5310C-2011
Analysis Method:
5310C-2011
Analysis Description:
Total Organic Carbon
Lab Reagent Blank
LRB-L581990
Matrix: AQU
Associated Lab Samples: 97987
Blank MDL
MQL
Analyzed
Parameter Units
Result
TOC pg/L
<500 500
1000
10/28/2112:01
Laboratory Control Sample
LCS-L581990
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
TOC pg/L
5000
5060
101 85-115
Duplicate
V 97854-DUP-L581990
Result DUP
RPD Max RPD
Analyzed
Parameter Units
Result
TOC pg/L
2390 2520
5.2 20
10/28/21 17:50
Matrix Spike
L 96060-MS-L581990
MS Spike
MSD MS Result
MSD MS %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec Limits RPD
Conc.
TOC pg/L
2630 5260
7910
100 70-130
Date: 12/21/2021 12:58 PM Page 5 of 40
Page 88 of 129

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality
Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-295-8005
QC Prep:
L582163
QC Analytical Batch(es): L582178
QC Prep Batch Method:
5310C-2011
Analysis Method:
5310C-2011
Analysis Description:
Total Organic Carbon
Lab Reagent Blank
LRB-L582163
Matrix: AQU
Associated Lab Samples:
97988, 98018, 98019
Blank MDL
MQL
Analyzed
Parameter
Units
Result
TOC
pg/L
<500 500
1000
10/30/21 10:11
Laboratory Control Sample
LCS-L582163
Spike
LCS
LCS %Rec % Rec
Parameter
Units
Conc.
Result
Limits
TOC
pg/L
5000
5010
100 85-115
Duplicate
V 97988-DUP-L582163
Result DUP
RPD Max RPD
Analyzed
Parameter
Units
Result
TOC
pg/L
<1000 <1000
0.0 20
10/30/2114:00
Matrix Spike
Q 95500-MS-L582163
MS Spike
MSD MS Result
MSD MS %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec Limits RPD
Conc.
TOC
pg/L
11900 5260
16400
86.0 70-130
Date: 12/21/2021 12:58 PM Page 6 of 40
Page 89 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V10735 QC Analytical Batch(es): V11081,V11123
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Lab Reagent Blank LRB-V10735 Matrix: AQU
Associated Lab Samples: 97987, 97988
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Antimony
pg/L
<0.490
0.490
2.00
11/03/2104:56
Arsenic
pg/L
<0.170
0.170
1.00
11/03/2104:56
Barium
pg/L
<0.810
0.810
10.0
11/03/2104:56
Beryllium
pg/L
<0.190
0.190
1.00
11/03/2120:02
Cadmium
pg/L
<0.160
0.160
1.00
11/03/2104:56
Chromium
pg/L
<0.790
0.790
2.00
11/03/2104:56
Cobalt
pg/L
<0.520
0.520
2.00
11/03/2104:56
Copper
pg/L
<3.80
3.80
10.0
11/03/2104:56
Lead
pg/L
<0.260
0.260
1.00
11/03/2104:56
Nickel
pg/L
<0.510
0.510
3.00
11/03/2104:56
Selenium
pg/L
0.786
0.740
5.00
11/03/2104:56
Silver
pg/L
<0.110
0.110
1.00
11/03/2104:56
Tin
pg/L
<1.80
1.80
5.00
11/03/2104:56
Thallium
pg/L
<0.570
0.570
2.00
11/03/2104:56
Vanadium
pg/L
<1.30
1.30
5.00
11/03/2120:02
Zinc
pg/L
<6.90
6.90
20.0
11/03/2104:56
Laboratory Control Sample
LCS-V10735
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Antimony
pg/L
100
101
101
80-120
Arsenic
pg/L
100
89.9
90.0
80-120
Barium
pg/L
100
97.1
97.0
80-120
Beryllium
pg/L
100
89.7
90.0
80-120
Cadmium
pg/L
100
95.8
96.0
80-120
Chromium
pg/L
100
95.2
95.0
80-120
Cobalt
pg/L
100
93.8
94.0
80-120
Date:
12/21/2021 12:58 PM
Page 7 of 40
Page 90 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V10735 QC Analytical Batch(es): V11081,V11123
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Laboratory Control Sample LCS-V10735
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Copper
pg/L
100
92.8
93.0
80-120
Lead
pg/L
100
96.7
97.0
80-120
Nickel
pg/L
100
92.6
93.0
80-120
Selenium
pg/L
100
90.3
90.0
80-120
Silver
pg/L
100
95.5
96.0
80-120
Tin
pg/L
100
96.0
96.0
80-120
Thallium
pg/L
100
91.9
92.0
80-120
Vanadium
pg/L
100
100
100
80-120
Zinc
pg/L
100
91.4
91.0
80-120
Matrix Spike & Matrix Spike Duplicate
Parameter Units
V 97852-MS-V10735
MS Spike
Result Conc.
V 97852-MSD-V10735
MSD MS Result
Spike
Conc.
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Antimony
pg/L
< 0.490
100
100
103
107
103
107
75-125
3.8
20.0
Arsenic
pg/L
0.181
100
100
90.9
93.3
91.0
93.0
75-125
2.6
20.0
Barium
pg/L
11.9
100
100
109
108
97.0
96.0
75-125
0.9
20.0
Beryllium
pg/L
< 0.190
100
100
94.1
93.4
94.0
93.0
75-125
0.7
20.0
Cadmium
pg/L
< 0.160
100
100
98.5
98.4
99.0
98.0
75-125
0.1
20.0
Chromium
pg/L
< 0.790
100
100
97.9
97.5
98.0
98.0
75-125
0.4
20.0
Cobalt
pg/L
< 0.520
100
100
95.6
96.5
96.0
97.0
75-125
0.9
20.0
Copper
pg/L
< 3.80
100
100
93.8
96.3
94.0
96.0
75-125
2.6
20.0
Lead
pg/L
< 0.260
100
100
99.4
99.2
99.0
99.0
75-125
0.2
20.0
Nickel
pg/L
< 0.510
100
100
95.7
95.6
96.0
96.0
75-125
0.1
20.0
Selenium
pg/L
< 0.740
100
100
90.4
97.1
90.0
97.0
75-125
7.1
20.0
Silver
pg/L
< 0.110
100
100
98.1
98.6
98.0
99.0
75-125
0.5
20.0
Tin
pg/L
< 1.80
100
100
97.0
99.3
97.0
99.0
75-125
2.3
20.0
Date: 12/21/2021 12:58 PM Page 8 of 40
Page 91 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-295-8005
QC Prep:
V10735
QC Analytical Batch(es): V11081,V11123
QC Prep Batch Method:
3005A
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Matrix Spike & Matrix Spike
Duplicate
V 97852-MS-V10735
V 97852-MSD-V10735
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Thallium
pg/L
< 0.570 100
100 95.4
95.7 95.0
96.0 75-125 0.3 20.0
Vanadium
pg/L
3.74 100
100 102
103 102
103 75-125 0.9 20.0
Zinc
pg/L
< 6.90 100
100 93.2
94.8 93.0
95.0 75-125 1.7 20.0
Post Digestion Spike
V 97852-PDS-V10735
PDS
%
Analyzed
Parameter
Units
Result Recovery
Antimony
pg/L
52.0
104
11/03/2105:29
Arsenic
pg/L
46.4
93.0
11/03/2105:29
Barium
pg/L
54.8
98.0
11/03/2105:29
Beryllium
pg/L
47.8
96.0
11/03/2120:35
Cadmium
pg/L
49.6
99.0
11/03/2105:29
Chromium
pg/L
48.8
98.0
11/03/2105:29
Cobalt
pg/L
47.6
95.0
11/03/2105:29
Copper
pg/L
46.6
93.0
11/03/2105:29
Lead
pg/L
50.3
101
11/03/21 05:29
Nickel
pg/L
47.2
94.0
11/03/2105:29
Selenium
pg/L
48.1
96.0
11/03/2105:29
Silver
pg/L
48.9
98.0
11/03/2105:29
Tin
pg/L
51.1
102
11/03/2105:29
Thallium
pg/L
50.5
101
11/03/2105:29
Vanadium
pg/L
53.7
107
11/03/2105:29
Zinc
pg/L
47.7
95.0
11/03/2105:29
Date: 12/21/2021 12:58 PM Page 9 of 40
Page 92 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep:
V10864
QC Analytical Batch(es): V11068,V11101
QC Prep Batch Method:
3005A
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Lab Reagent Blank
LRB-V10864
Matrix: AQU
Associated Lab Samples:
98018, 98019, 98025
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Antimony
pg/L
<0.490
0.490
2.00
11/02/21 13:41
Arsenic
pg/L
<0.170
0.170
1.00
11/02/21 13:41
Barium
pg/L
<0.810
0.810
10.0
11/02/21 13:41
Beryllium
pg/L
<0.190
0.190
1.00
11/02/21 13:41
Cadmium
pg/L
<0.160
0.160
1.00
11/02/21 13:41
Chromium
pg/L
<0.790
0.790
2.00
11/02/21 13:41
Cobalt
pg/L
<0.520
0.520
2.00
11/02/21 13:41
Copper
pg/L
<3.80
3.80
10.0
11/02/21 13:41
Lead
pg/L
<0.260
0.260
1.00
11/02/21 13:41
Nickel
pg/L
<0.510
0.510
3.00
11/02/21 13:41
Selenium
pg/L
<0.740
0.740
5.00
11/02/21 13:41
Silver
pg/L
<0.110
0.110
1.00
11/02/21 13:41
Thallium
pg/L
<0.570
0.570
2.00
11/02/21 13:41
Vanadium
pg/L
<1.30
1.30
5.00
11/02/21 13:41
Zinc
pg/L
<6.90
6.90
20.0
11/02/21 13:41
Laboratory Control Sample LCS-V10864
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Antimony
pg/L
100
104
104
80-120
Arsenic
pg/L
100
96.9
97.0
80-120
Barium
pg/L
100
102
102
80-120
Beryllium
pg/L
100
97.6
98.0
80-120
Cadmium
pg/L
100
98.0
98.0
80-120
Chromium
pg/L
100
99.7
100
80-120
Cobalt
pg/L
100
101
101
80-120
Copper
pg/L
100
101
101
80-120
Date: 12/21/2021 12:58 PM Page 10 of 40
Page 93 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V10864 QC Analytical Batch(es): V11068,V11101
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Laboratory Control Sample LCS-V10864
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Lead
pg/L
100
102
102
80-120
Nickel
pg/L
100
100
100
80-120
Selenium
pg/L
100
97.1
97.0
80-120
Silver
pg/L
100
99.0
99.0
80-120
Thallium
pg/L
100
100
100
80-120
Vanadium
pg/L
100
102
102
80-120
Zinc
pg/L
100
100
100
80-120
Matrix Spike & Matrix Spike Duplicate
Parameter Units
V 97383-MS-V10864
MS Spike
Result Conc.
V 97383-MSD-V10864
MSD MS Result
Spike
Conc.
MSD
Result
MS
%Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Antimony
pg/L
< 0.490
100
100
107
106
107
106
75-125
0.9
20.0
Arsenic
pg/L
0.302
100
100
98.3
95.8
98.0
96.0
75-125
2.5
20.0
Barium
pg/L
62.8
100
100
167
159
104
96.0
75-125
4.9
20.0
Beryllium
pg/L
< 0.190
100
100
99.6
99.4
100
99.0
75-125
0.2
20.0
Cadmium
pg/L
< 0.160
100
100
101
99.3
101
99.0
75-125
1.6
20.0
Chromium
pg/L
1.50
100
100
101
98.5
101
99.0
75-125
2.5
20.0
Cobalt
pg/L
2.23
100
100
103
100
101
98.0
75-125
2.9
20.0
Copper
pg/L
< 3.80
100
100
101
99.4
101
99.0
75-125
1.5
20.0
Lead
pg/L
0.794
100
100
101
99.4
101
99.0
75-125
1.5
20.0
Nickel
pg/L
1.24
100
100
102
99.1
102
99.0
75-125
2.8
20.0
Selenium
pg/L
< 0.740
100
100
102
102
102
102
75-125
0.0
20.0
Silver
pg/L
< 0.110
100
100
101
100
101
100
75-125
0.9
20.0
Thallium
pg/L
< 0.570
100
100
99.5
97.6
100
98.0
75-125
1.9
20.0
Vanadium
pg/L
4.66
100
100
106
105
106
105
75-125
0.9
20.0
Zinc
pg/L
< 6.90
100
100
102
101
102
101
75-125
0.9
20.0
Date: 12/21/2021 12:58 PM Page 11 of 40
Page 94 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V10864 QC Analytical Batch(es): V11068,V11101
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Post Digestion Spike V 97383-PDS-V10864
Parameter
Units
PDS
Result
%
Recovery
Analyzed
Antimony
pg/L
52.4
105
11/02/21 19:25
Arsenic
pg/L
49.8
100
11/02/21 19:25
Barium
Ng/L
83.3
102
11/02/21 19:25
Beryllium
pg/L
51.4
103
11/02/21 19:25
Cadmium
pg/L
49.4
99.0
11/02/21 19:25
Chromium
pg/L
50.4
101
11/02/21 19:25
Cobalt
Ng/L
50.9
100
11/02/21 19:25
Copper
pg/L
50.2
100
11/02/21 19:25
Lead
Ng/L
50.0
100
11/02/21 19:25
Nickel
Ng/L
50.0
100
11/02/21 19:25
Selenium
pg/L
48.8
98.0
11/02/21 19:25
Silver
pg/L
49.5
99.0
11/02/21 19:25
Thallium
Ng/L
50.5
101
11/02/21 19:25
Vanadium
pg/L
54.3
109
11/02/21 19:25
Zinc
Ng/L
50.8
102
11/02/21 19:25
Date: 12/21/2021 12:58 PM Page 12 of 40
Page 95 of 129

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V11089
QC Analytical Batch(es): V11232,V11242
QC Prep Batch Method: 3005A
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Lab Reagent Blank
LRB-V11089
Matrix: AQU
Associated Lab Samples: 98018, 98019, 98025
Blank MDL
MQL
Analyzed
Parameter Units
Result
Tin pg/L
<1.80 1.80
5.00
11/05/2114:18
Laboratory Control Sample
LCS-V11089
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Tin pg/L
100
99.6
100 80-120
Matrix Spike & Matrix Spike Duplicate
V 97383-MS-V11089
V 97383-MSD-V11089
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Tin pg/L
< 1.80 100
100 100
99.1 100 99.0 75-125 0.9 20.0
Post Digestion Spike
V 97383-PDS-V11089
PDS
%
Analyzed
Parameter Units
Result
Recovery
Tin pg/L
50.9
102
11/05/21 17:42
Date: 12/21/2021 12:58 PM Page 13 of 40
Page 96 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V11166 QC Analytical Batch(es): V11233,V11240
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Lab Reagent Blank LRB-V11166 Matrix: AQU
Associated Lab Samples: 97987, 98018, 98019
Parameter
Units
Blank
Result
MDL
MQL
Analyzed
Dissolved Antimony
pg/L
<0.490
0.490
2.00
11/05/21 13:39
Dissolved Arsenic
pg/L
<0.170
0.170
1.00
11/05/21 13:39
Dissolved Barium
pg/L
<0.810
0.810
10.0
11/05/21 13:39
Dissolved Beryllium
pg/L
<0.190
0.190
1.00
11/05/21 13:39
Dissolved Cadmium
pg/L
<0.160
0.160
1.00
11/05/21 13:39
Dissolved Chromium
pg/L
<0.790
0.790
2.00
11/05/21 13:39
Dissolved Cobalt
pg/L
<0.520
0.520
2.00
11/05/21 13:39
Dissolved Copper
pg/L
<3.80
3.80
10.0
11/05/21 13:39
Dissolved Lead
pg/L
<0.260
0.260
1.00
11/05/21 13:39
Dissolved Nickel
pg/L
<0.510
0.510
3.00
11/05/21 13:39
Dissolved Selenium
pg/L
<0.740
0.740
5.00
11/05/21 13:39
Dissolved Silver
pg/L
<0.110
0.110
1.00
11/05/21 13:39
Dissolved Tin
pg/L
<1.80
1.80
5.00
11/05/21 13:39
Dissolved Thallium
pg/L
<0.570
0.570
2.00
11/05/21 13:39
Dissolved Vanadium
pg/L
<1.30
1.30
5.00
11/05/21 13:39
Dissolved Zinc
pg/L
<6.90
6.90
20.0
11/05/21 13:39
Laboratory Control Sample LCS-V11166
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Dissolved Antimony
pg/L
100
100
100
80-120
Dissolved Arsenic
pg/L
100
92.7
93.0
80-120
Dissolved Barium
pg/L
100
101
101
80-120
Dissolved Beryllium
pg/L
100
91.4
91.0
80-120
Dissolved Cadmium
pg/L
100
96.2
96.0
80-120
Dissolved Chromium
pg/L
100
94.7
95.0
80-120
Dissolved Cobalt
pg/L
100
91.9
92.0
80-120
Date: 12/21/2021 12:58 PM Page 14 of 40
Page 97 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V11166 QC Analytical Batch(es): V11233,V11240
QC Prep Batch Method: 3005A Analysis Method: 6020B
Analysis Description: Metals Analyses
Laboratory Control Sample LCS-V11166
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Dissolved Copper
pg/L
100
91.4
91.0
80-120
Dissolved Lead
pg/L
100
98.3
98.0
80-120
Dissolved Nickel
pg/L
100
90.7
91.0
80-120
Dissolved Selenium
pg/L
100
97.3
97.0
80-120
Dissolved Silver
pg/L
100
94.9
95.0
80-120
Dissolved Tin
pg/L
100
93.4
93.0
80-120
Dissolved Thallium
pg/L
100
96.9
97.0
80-120
Dissolved Vanadium
pg/L
100
94.1
94.0
80-120
Dissolved Zinc
pg/L
100
96.9
97.0
80-120
Matrix Spike & Matrix Spike Duplicate
Parameter Units
V 98018-V11161-MS-V11166
MS Spike MSD
Result Conc. Spike
Conc.
V 98018-VIII61-MSD-VIII66
MS Result MSD MS
Result %Rec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Dissolved Antimony
pg/L
< 0.490
100
100
106
107
106
107
75-125
0.9
20.0
Dissolved Arsenic
pg/L
< 0.170
100
100
95.7
93.9
96.0
94.0
75-125
1.8
20.0
Dissolved Barium
pg/L
39.2
100
100
286
280
247*
241*
75-125
2.1
20.0
Dissolved Beryllium
pg/L
< 0.190
100
100
95.3
95.5
95.0
96.0
75-125
0.2
20.0
Dissolved Cadmium
pg/L
< 0.160
100
100
101
98.7
101
99.0
75-125
2.3
20.0
Dissolved Chromium
pg/L
< 0.790
100
100
95.4
94.6
95.0
95.0
75-125
0.8
20.0
Dissolved Cobalt
pg/L
19.1
100
100
98.7
96.1
80.0
77.0
75-125
2.6
20.0
Dissolved Copper
pg/L
< 3.80
100
100
95.3
92.4
95.0
92.0
75-125
3.0
20.0
Dissolved Lead
pg/L
< 0.260
100
100
98.6
98.7
99.0
99.0
75-125
0.1
20.0
Dissolved Nickel
pg/L
18.3
100
100
97.1
94.0
79.0
76.0
75-125
3.2
20.0
Dissolved Selenium
pg/L
< 0.740
100
100
102
102
102
102
75-125
0.0
20.0
Dissolved Silver
pg/L
< 0.110
100
100
80.9
80.5
81.0
81.0
75-125
0.4
20.0
Dissolved Tin
pg/L
< 1.80
100
100
95.6
96.6
96.0
97.0
75-125
1.0
20.0
* QC Fail Date: 12/21/2021 12:58 PM Page 15 of 40
Page 98 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-295-8005
QC Prep:
V11166
QC Analytical Batch(es): V11233,V11240
QC Prep Batch Method:
3005A
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Matrix Spike & Matrix Spike
Duplicate
V 98018-V11161-MS-V11166 V 98018-V11161-MSD-V11166
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Dissolved Thallium
pg/L
< 0.570 100
100 98.1
96.9 98.0
97.0 75-125 1.2 20.0
Dissolved Vanadium
pg/L
< 1.30 100
100 95.7
93.4 96.0
93.0 75-125 2.4 20.0
Dissolved Zinc
pg/L
< 6.90 100
100 106
104 106
104 75-125 1.9 20.0
Post Digestion Spike
V 98018-V11161-PDS-V11166
PDS
%
Analyzed
Parameter
Units
Result
Recovery
Dissolved Antimony
pg/L
55.4
111
11/05/21 20:07
Dissolved Arsenic
pg/L
50.7
101
11/05/21 20:07
Dissolved Barium
pg/L
72.8
105
11/05/21 20:07
Dissolved Beryllium
pg/L
47.5
95.0
11/05/21 20:07
Dissolved Cadmium
pg/L
52.3
105
11/05/21 20:07
Dissolved Chromium
pg/L
51.2
102
11/05/21 20:07
Dissolved Cobalt
pg/L
58.9
99.0
11/05/21 20:07
Dissolved Copper
pg/L
48.6
97.0
11/05/21 20:07
Dissolved Lead
pg/L
50.9
102
11/05/21 20:07
Dissolved Nickel
pg/L
58.6
99.0
11/05/21 20:07
Dissolved Selenium
pg/L
52.7
105
11/05/21 20:07
Dissolved Silver
pg/L
51.3
103
11/05/21 20:07
Dissolved Tin
pg/L
51.3
103
11/05/21 20:07
Dissolved Thallium
pg/L
49.8
100
11/05/21 20:07
Dissolved Vanadium
pg/L
50.5
101
11/05/21 20:07
Dissolved Zinc
pg/L
50.9
102
11/05/21 20:07
Date: 12/21/2021 12:58 PM Page 16 of 40
Page 99 of 129

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V10945
QC Analytical Batch(es): V10964
QC Prep Batch Method: 7470A
Analysis Method:
7470A
Analysis Description:
Total Aqueous Mercury Analysis - CVAA
Lab Reagent Blank
LRB-V10945
Matrix: AQU
Associated Lab Samples: 97987, 97988
Blank MDL
MQL
Analyzed
Parameter Units
Result
Mercury (Total) pg/L
<0.0700 0.0700
0.200
10/29/21 19:36
Laboratory Control Sample
LCS-V10945
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Mercury (Total) pg/L
9.38
9.64
103 80-120
Matrix Spike & Matrix Spike Duplicate
V 98049-MS-V10945
V 98049-MSD-V10945
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Mercury (Total) pg/L
<0.0700 9.38
9.38 2.41
2.37 26.0* 25.0* 80-120 1.6 20
Post Digestion Spike
V 98049-PDS-V10945
PDS
%
Analyzed
Parameter Units
Result
Recovery
Mercury (Total) pg/L
2.15
46.0*
10/29/21 19:50
* QC Fail Date: 12/21/2021 12:58 PM Page 17 of 40
Page 100 of 129

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V11049
QC Analytical Batch(es): V11111
QC Prep Batch Method: 7470A
Analysis Method:
7470A
Analysis Description:
Total Aqueous Mercury Analysis - CVAA
Lab Reagent Blank
LRB-V11049
Matrix: AQU
Associated Lab Samples: 98018, 98019, 98025
Blank MDL
MQL
Analyzed
Parameter Units
Result
Mercury (Total) pg/L
<0.0700 0.0700
0.200
11/02/21 17:44
Laboratory Control Sample
LCS-V11049
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Mercury (Total) pg/L
9.38
9.51
101 80-120
Matrix Spike & Matrix Spike Duplicate
V 97996-MS-V11049
V 97996-MSD-V11049
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Mercury (Total) pg/L
<0.0700 9.38
9.38 6.91
6.85 74.0* 73.0* 80-120 0.8 20
Post Digestion Spike
V 97996-PDS-V11049
PDS
%
Analyzed
Parameter Units
Result
Recovery
Mercury (Total) pg/L
4.29
92.0
11/02/21 17:59
* QC Fail Date: 12/21/2021 12:58 PM Page 18 of 40
Page 101 of 129

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V11199
QC Analytical Batch(es): V11256
QC Prep Batch Method: 7470A
Analysis Method:
7470A
Analysis Description:
Total Aqueous Mercury Analysis - CVAA
Lab Reagent Blank
LRB-V11199
Matrix: AQU
Associated Lab Samples: 97987, 98018, 98019
Blank MDL
MQL
Analyzed
Parameter Units
Result
Dissolved Mercury pg/L
0.000 0.000
0.200
11/06/21 12:07
Laboratory Control Sample
LCS-V11199
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Dissolved Mercury pg/L
9.38
9.00
96.0 80-120
Matrix Spike & Matrix Spike Duplicate
V 97855-V11161-MS-V11199 V 97855-V11161-MSD-V11199
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Dissolved Mercury pg/L
<0.0700 9.38
9.38 5.76
5.83 61.0* 62.0* 80-120 1.2 20
Post Digestion Spike
V 97855-V11161-PDS-V11199
PDS
%
Analyzed
Parameter Units
Result
Recovery
Dissolved Mercury pg/L
3.70
79.0*
11/06/21 12:22
* QC Fail Date: 12/21/2021 12:58 PM Page 19 of 40
Page 102 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-295-8005
QC Prep:
V10781
QC Analytical Batch(es): V10782
QC Prep Batch Method:
5030B
Analysis Method:
8260D SIM
Analysis Description:
Volatile Organic Compounds -
GC/MS
Lab Reagent Blank
LRB-V10781
Matrix: AQU
Associated Lab Samples:
98018, 98019
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
1,4-Dioxane
pg/L
<0.139 0.139
2.00
10/27/2109:11
4-Bromofluorobenzene (S)
10/27/21 09:11
105
70-130
Laboratory Control Sample
LCS-V10781
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
1,4-Dioxane
pg/L
50.0
54.8
110
70-130
4-Bromofluorobenzene (S)
115
70-130
Matrix Spike & Matrix Spike Duplicate
V 98008-MS-V10781
V 98008-MSD-V10781
MS Spike
MSD MS Result
MSD MS
MSD
%Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec
Limits RPD
Conc.
1,4-Dioxane
pg/L
< 0.139 50.0
50.0 54.5
57.7 109
115
70-130
4-Bromofluorobenzene (S)
115
110
70-130
Date: 12/21/2021 12:58 PM Page 20 of 40
Page 103 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-295-8005
QC Prep:
V10873
QC Analytical Batch(es): V10875
QC Prep Batch Method:
5030B
Analysis Method:
8260D SIM
Analysis Description:
Volatile Organic Compounds -
GC/MS
Lab Reagent Blank
LRB-V10873
Matrix: AQU
Associated Lab Samples:
97987, 97988, 98025
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
1,4-Dioxane
pg/L
<0.139 0.139
2.00
10/28/2109:53
4-Bromofluorobenzene (S)
10/28/21 09:53
102
70-130
Laboratory Control Sample
LCS-V10873
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
1,4-Dioxane
pg/L
50.0
47.5
95.0
70-130
4-Bromofluorobenzene (S)
98.2
70-130
Matrix Spike & Matrix Spike Duplicate
V 98011-MS-V10873
V 98011-MSD-V10873
MS Spike
MSD MS Result
MSD MS
MSD
%Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec
Limits RPD
Conc.
1,4-Dioxane
pg/L
< 0.139 50.0
50.0 47.2
45.7 94.4
91.4
70-130
4-Bromofluorobenzene (S)
98.4
91.4
70-130
Date: 12/21/2021 12:58 PM Page 21 of 40
Page 104 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V10999
QC Prep Batch Method: 5030B
QC Analytical Batch(es): V11000
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V10999 Matrix: AQU
Associated Lab Samples: 97987, 97988, 97989, 98018, 98019, 98020, 98025, 98026
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
pg/L
<1.80
1.80
5.00
11/01/2102:07
Acetonitrile
pg/L
<20.3
20.3
10.0
11/01/2102:07
Acrolein
pg/L
<2.00
2.00
5.00
11/01/2102:07
Acrylonitrile
pg/L
<0.230
0.230
5.00
11/01/2102:07
Allyl Chloride
pg/L
<0.579
0.579
10.0
11/01/2102:07
Benzene
pg/L
<0.180
0.180
0.500
11/01/2102:07
Bromochloromethane
pg/L
<0.420
0.420
1.00
11/01/2102:07
Bromodichloromethane
pg/L
<0.160
0.160
0.500
11/01/2102:07
Bromoform
pg/L
<1.50
1.50
5.00
11/01/2102:07
Bromomethane
pg/L
<0.280
0.280
1.00
11/01/2102:07
Carbon Disulfide
pg/L
<0.150
0.150
5.00
11/01/2102:07
Carbon Tetrachloride
pg/L
<0.180
0.180
0.500
11/01/21 02:07
Chlorobenzene
pg/L
<0.190
0.190
0.500
11/01/2102:07
Chlorodibromomethane
pg/L
<0.190
0.190
0.500
11/01/2102:07
Chloroethane
pg/L
<0.430
0.430
1.00
11/01/2102:07
Chloroform
pg/L
<0.220
0.220
0.500
11/01/2102:07
Chloromethane
pg/L
<0.220
0.220
0.500
11/01/2102:07
Chloroprene
pg/L
<0.450
0.450
10.0
11/01/2102:07
1,2-Dibromo-3-Chloropropane
pg/L
<1.10
1.10
2.00
11/01/2102:07
1,2-Dibromoethane
pg/L
<0.200
0.200
0.500
11/01/2102:07
Dibromomethane
pg/L
<0.230
0.230
0.500
11/01/2102:07
trans-1,4-Dichloro-2-butene
pg/L
< 1.30
1.30
10.0
11/01/21 02:07
1,2-Dichlorobenzene
pg/L
<0.220
0.220
0.500
11/01/2102:07
1,3-Dichlorobenzene
pg/L
<0.190
0.190
0.500
11/01/2102:07
1,4-Dichlorobenzene
pg/L
<0.210
0.210
0.500
11/01/2102:07
Dichlorodifluoromethane
pg/L
<1.20
1.20
5.00
11/01/2102:07
1,1-Dichloroethane
pg/L
<0.240
0.240
0.500
11/01/2102:07
Date:
12/21/2021 12:58 PM
Page 22 of 40
Page 105 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V10999
QC Prep Batch Method: 5030B
QC Analytical Batch(es): V11000
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V10999 Matrix: AQU
Associated Lab Samples: 97987, 97988, 97989, 98018, 98019, 98020, 98025, 98026
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,2-Dichloroethane
pg/L
<0.150
0.150
0.500
11/01/2102:07
1,1-Dichloroethene
pg/L
<0.150
0.150
0.500
11/01/2102:07
cis-1,2-Dichloroethene
pg/L
<0.200
0.200
0.500
11/01/2102:07
trans-1,2-Dichloroethene
pg/L
<0.180
0.180
0.500
11/01/2102:07
1,2-Dichloropropane
pg/L
<0.190
0.190
0.500
11/01/2102:07
1,3-Dichloropropane
pg/L
<0.130
0.130
0.500
11/01/2102:07
2,2-Dichloropropane
pg/L
<0.210
0.210
2.00
11/01/2102:07
1,1-Dichloropropene
pg/L
<0.200
0.200
0.500
11/01/2102:07
cis-1,3-Dichloropropene
pg/L
<0.210
0.210
0.500
11/01/2102:07
trans-1,3-Dichloropropene
pg/L
<0.150
0.150
0.500
11/01/2102:07
Ethyl Methacrylate
pg/L
<1.62
1.62
10.0
11/01/21 02:07
Ethylbenzene
pg/L
<0.170
0.170
0.500
11/01/2102:07
Hexachlorobutadiene
pg/L
<0.350
0.350
2.00
11/01/2102:07
2-Hexanone
pg/L
<0.380
0.380
5.00
11/01/2102:07
Iodomethane
pg/L
<0.054
0.054
0.500
11/01/2102:07
Methyl Ethyl Ketone (MEK)
pg/L
<0.710
0.710
5.00
11/01/2102:07
Methacrylonitrile
pg/L
<12.6
12.6
10.0
11/01/2102:07
4-Methyl-2-Pentanone
pg/L
<1.00
1.00
5.00
11/01/2102:07
Methylene Chloride
pg/L
<0.330
0.330
1.00
11/01/2102:07
Naphthalene
pg/L
<0.470
0.470
1.00
11/01/2102:07
Propionitrile
pg/L
<23.7
23.7
10.0
11/01/2102:07
Styrene
pg/L
<0.220
0.220
0.500
11/01/2102:07
1,1,1,2-Tetrachloroethane
pg/L
<0.160
0.160
0.500
11/01/2102:07
1,1,2,2-Tetrachloroethane
pg/L
<0.160
0.160
0.500
11/01/2102:07
Tetrachloroethene
pg/L
<0.220
0.220
0.500
11/01/2102:07
Tetrahydrofuran
pg/L
<1.50
1.50
10.0
11/01/2102:07
Toluene
pg/L
<0.220
0.220
0.500
11/01/2102:07
Date:
12/21/2021 12:58 PM
Page 23 of 40
Page 106 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep:
V10999
QC Analytical Batch(es): V11000
QC Prep Batch Method:
5030B
Analysis
Method:
8260D
Analysis Description:
Volatile Organic Compounds - GC/MS
Lab Reagent Blank
LRB-V10999
Matrix: AQU
Associated Lab Samples:
97987, 97988, 97989, 98018,
98019, 98020,
98025, 98026
Blank
MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
1,2,4-Trichlorobenzene
pg/L
<0.310
0.310
1.00
11/01/2102:07
1,1,1-Trichloroethane
pg/L
<0.160
0.160
0.500
11/01/2102:07
1,1,2-Trichloroethane
pg/L
<0.096
0.096
0.500
11/01/2102:07
Trichloroethene
pg/L
<0.180
0.180
0.500
11/01/2102:07
Trichlorofluoromethane
pg/L
<0.180
0.180
0.500
11/01/2102:07
1,2,3-Trichloropropane
pg/L
<0.270
0.270
1.00
11/01/2102:07
Vinyl Acetate
pg/L
<1.00
1.00
2.00
11/01/2102:07
Vinyl Chloride
pg/L
<0.170
0.170
0.500
11/01/2102:07
o-Xylene
pg/L
<0.210
0.210
0.500
11/01/2102:07
m,p-Xylene
pg/L
<0.420
0.420
1.00
11/01/2102:07
4-Bromofluorobenzene (S)
11/01/2102:07
100
80-124
Dibromofluoromethane (S)
11/01/2102:07
99.2
75-129
1,2-Dichloroethane - d4 (S)
11/01/2102:07
101
63-136
Toluene-d8 (S)
11/01/2102:07
96.8
77-123
Laboratory Control Sample & LCSD
LCS-V10999 LCSD-V10999
Spike
LCS
LCSD
LCS LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec a/o Rec
Limits
RPD
Max
RPD
Acetone
pg/L
40.0
48.8
49.4
122 124
40-166
1.2
20.0
Acetonitrile
pg/L
20.0
<20.3
<20.3
94.0 84.0
40-160
11.2
20.0
Acrolein
pg/L
40.0
39.8
41.1
99.5 103
70-130
3.2
20.0
Acrylonitrile
pg/L
40.0
46.9
49.3
117 123
81-127
4.9
20.0
Allyl Chloride
pg/L
20.0
19.5
18.7
97.5 93.5
40-160
4.1
20.0
Benzene
pg/L
20.0
24.1
23.7
121 119
77-128
1.6
20.0
Bromochloromethane
pg/L
20.0
24.8
23.5
124 118
78-135
5.3
20.0
Bromodichloromethane
pg/L
20.0
23.7
23.4
119 117
76-138
1.2
20.0
Date: 12/21/2021 12:58 PM Page 24 of 40
Page 107 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V10999 QC Analytical Batch(es): V11000
QC Prep Batch Method: 5030B Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V10999 LCSD-V10999
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Bromoform
pg/L
20.0
22.6
22.6
113
113
71-135
0.0
20.0
Bromomethane
pg/L
20.0
24.6
25.4
123
127
41-168
3.2
20.0
Carbon Disulfide
pg/L
20.0
21.3
20.4
107
102
59-135
4.3
20.0
Carbon Tetrachloride
pg/L
20.0
24.1
23.1
121
116
72-142
4.2
20.0
Chlorobenzene
pg/L
20.0
21.4
20.8
107
104
78-119
2.8
20.0
Chlorodibromomethane
pg/L
20.0
21.9
21.8
110
109
75-134
0.4
20.0
Chloroethane
pg/L
20.0
24.0
23.1
120
116
57-142
3.8
20.0
Chloroform
pg/L
20.0
22.9
22.5
115
113
77-130
1.7
20.0
Chloromethane
pg/L
20.0
24.0
22.9
120
115
47-145
4.6
20.0
Chloroprene
pg/L
20.0
19.4
18.8
97.0
94.0
40-160
3.1
20.0
1,2-Dibromo-3-Chloropropane
pg/L
20.0
21.3
21.5
107
108
63-134
0.9
20.0
1,2-Dibromoethane
pg/L
20.0
21.8
21.4
109
107
77-135
1.8
20.0
Dibromomethane
pg/L
20.0
23.9
24.1
120
121
76-138
0.8
20.0
trans-1,4-Dichloro-2-butene
pg/L
20.0
15.3
16.2
76.5
81.0
70-130
5.7
20.0
1,2-Dichlorobenzene
pg/L
20.0
19.8
19.7
99.0
98.5
78-128
0.5
20.0
1,3-Dichlorobenzene
pg/L
20.0
19.8
19.3
99.0
96.5
77-125
2.5
20.0
1,4-Dichlorobenzene
pg/L
20.0
19.6
19.0
98.0
95.0
75-126
3.1
20.0
Dichlorodifluoromethane
pg/L
20.0
21.2
20.5
106
103
28-163
3.3
20.0
1,1-Dichloroethane
pg/L
20.0
24.8
23.6
124
118
70-130
4.9
20.0
1,2-Dichloroethane
pg/L
20.0
23.2
22.9
116
115
68-131
1.3
20.0
1,1-Dichloroethene
pg/L
20.0
23.4
22.2
117
111
70-154
5.2
20.0
cis-1,2-Dichloroethene
pg/L
20.0
23.2
22.3
116
112
76-141
3.9
20.0
trans-1,2-Dichloroethene
pg/L
20.0
23.7
22.6
119
113
76-135
4.7
20.0
1,2-Dichloropropane
pg/L
20.0
23.4
23.1
117
116
77-130
1.2
20.0
1,3-Dichloropropane
pg/L
20.0
21.7
21.5
109
108
76-132
0.9
20.0
2,2-Dichloropropane
pg/L
20.0
21.1
20.6
106
103
29-149
2.3
20.0
Date: 12/21/2021 12:58 PM Page 25 of 40
Page 108 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: V10999 QC Analytical Batch(es): V11000
QC Prep Batch Method: 5030B Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V10999 LCSD-V10999
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
1,1-Dichloropropene
pg/L
20.0
24.0
22.9
120
115
71-136
4.6
20.0
cis-1,3-Dichloropropene
pg/L
20.0
23.6
23.1
118
116
65-140
2.1
20.0
trans-1,3-Dichloropropene
pg/L
20.0
23.3
23.0
117
115
67-140
1.2
20.0
Ethyl Methacrylate
pg/L
20.0
20.0
19.1
100
95.5
40-160
4.6
20.0
Ethylbenzene
pg/L
20.0
21.7
20.8
109
104
80-127
4.2
20.0
Hexachlorobutadiene
pg/L
20.0
21.8
19.8
109
99.0
61-134
9.6
20.0
2-Hexanone
pg/L
20.0
22.2
23.1
111
116
64-137
3.9
20.0
Iodomethane
pg/L
20.0
18.8
19.3
94.0
96.5
70-130
2.6
20.0
Methyl Ethyl Ketone (MEK)
pg/L
20.0
22.5
22.9
113
115
71-134
1.7
20.0
Methacrylonitrile
pg/L
20.0
24.8
25.1
124
126
40-160
1.2
20.0
4-Methyl-2-Pentanone
pg/L
20.0
24.7
24.9
124
125
69-134
0.8
20.0
Methylene Chloride
pg/L
20.0
23.2
22.5
116
113
73-131
3.0
20.0
Naphthalene
pg/L
20.0
20.7
19.8
104
99.0
64-136
4.4
20.0
Propionitrile
pg/L
20.0
<23.7
<23.7
102
95.0
40-160
7.1
20.0
Styrene
pg/L
20.0
22.3
21.9
112
110
78-129
1.8
20.0
1,1,1,2-Tetrachloroethane
pg/L
20.0
21.5
21.2
108
106
79-134
1.4
20.0
1,1,2,2-Tetrachloroethane
pg/L
20.0
19.0
18.7
95.0
93.5
62-127
1.5
20.0
Tetrachloroethene
pg/L
20.0
21.1
20.7
106
104
80-129
1.9
20.0
Tetrahydrofuran
pg/L
20.0
23.4
22.3
117
112
70-130
4.8
20.0
Toluene
pg/L
20.0
23.9
23.2
120
116
76-131
2.9
20.0
1,2,4-Trichlorobenzene
pg/L
20.0
21.0
20.3
105
102
66-139
3.3
20.0
1,1,1-Trichloroethane
pg/L
20.0
24.4
23.0
122
115
75-135
5.9
20.0
1,1,2-Trichloroethane
pg/L
20.0
23.4
23.7
117
119
70-140
1.2
20.0
Trichloroethene
pg/L
20.0
25.2
24.4
126
122
77-133
3.2
20.0
Trichlorofluoromethane
pg/L
20.0
23.8
23.4
119
117
62-148
1.6
20.0
1,2,3-Trichloropropane
pg/L
20.0
19.7
19.4
98.5
97.0
71-127
1.5
20.0
Date: 12/21/2021 12:58 PM Page 26 of 40
Page 109 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-295-8005
QC Prep:
V10999
QC Analytical Batch(es): V11000
QC Prep Batch Method:
5030B
Analysis Method:
8260D
Analysis Description:
Volatile Organic Compounds - GC/MS
Laboratory Control Sample
& LCSD
LCS-V10999 LCSD-V10999
Spike
LCS LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result Result
%Rec
% Rec
Limits
RPD
Max
RPD
Vinyl Acetate
pg/L
20.0
18.8 18.4
94.0
92.0
34-167
2.1
20.0
Vinyl Chloride
pg/L
20.0
23.0 22.3
115
112
57-141
3.0
20.0
o-Xylene
pg/L
20.0
21.8 21.3
109
107
78-128
2.3
20.0
m,p-Xylene
pg/L
40.0
46.0 43.8
115
110
77-133
4.8
20.0
4-Bromofluorobenzene (S)
96.4
96.0
80-124
Dibromofluoromethane (S)
96.6
96.8
75-129
1,2-Dichloroethane - d4 (S)
94.4
95.4
63-136
Toluene-d8(S)
92.2
90.4
77-123
Date: 12/21/2021 12:58 PM Page 27 of 40
Page 110 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-295-8005
QC Prep:
V11027
QC Analytical Batch(es): V11028
QC Prep Batch Method:
5030B
Analysis Method:
8260D
Analysis Description:
Volatile Organic Compounds - GC/MS
Lab Reagent Blank
LRB-V11027
Matrix: AQU
Associated Lab Samples:
98025
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
Tetrahydrofuran
pg/L
<1.50 1.50
10.0
11/01/21 13:40
4-Bromofluorobenzene (S)
11/01/21 13:40
96.8
80-124
Dibromofluoromethane (S)
11/01/21 13:40
97.8
75-129
1,2-Dichloroethane - d4 (S)
11/01/21 13:40
91.0
63-136
Toluene-d8 (S)
11/01/21 13:40
90.6
77-123
Laboratory Control Sample & LCSD
LCS-V11027 LCSD-VII027
Spike
LCS LCSD
LCS LCSD
% Rec
Parameter
Units
Conc.
Result Result
%Rec a/o Rec
Limits
RPD Max
RPD
Tetrahydrofuran
pg/L
20.0
22.9 24.2
115 121
70-130
5.5 20.0
4-Bromofluorobenzene (S)
97.4 95.2
80-124
Dibromofluoromethane (S)
95.4 96.0
75-129
1,2-Dichloroethane - d4 (S)
92.0 95.0
63-136
Toluene-d8(S)
89.4 90.2
77-123
Date: 12/21/2021 12:58 PM Page 28 of 40
Page 111 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: L581531
QC Prep Batch Method: 3510C
Lab Reagent Blank
LRB-L581531
Associated Lab Samples:
98021, 98022, 98023, 98024
Blank
MDL
Parameter
Units
Result
Dimethoate
pg/L
<0.713
0.713
Disulfoton
pg/L
<0.466
0.466
Ethyl Parathion
pg/L
<0.568
0.568
Famphur
pg/L
<0.512
0.512
Methyl Parathion
pg/L
<0.805
0.805
Phorate
pg/L
<0.659
0.659
Tributyl phosphate (S)
Triphenyl phosphate (S)
Laboratory Control Sample & LCSD LCS-L581531 L
Spike
Parameter Units Conc.
QC Analytical Batch(es): L581686
Analysis Method: 8270C
Analysis Description: Organophosphorus Pesticides by GC/MS
Matrix: AQU
MQL
Analyzed
0/0
Recovery
1.00
10/27/21 18:27
1.00
10/27/21 18:27
1.00
10/27/21 18:27
1.00
10/27/21 18:27
1.00
10/27/21 18:27
1.00
10/27/21 18:27
10/27/21 18:27
69.0
10/27/21 18:27
60.0
CSD-L581531
LCS LCSD LCS LCSD % Rec
Result Result %Rec % Rec Limits
Dimethoate
pg/L
20.0
11.3
12.5
56.5
62.5
40-140
Disulfoton
pg/L
20.0
14.0
14.9
70.0
74.5
40-140
Ethyl Parathion
pg/L
20.0
13.2
14.3
66.0
71.5
40-140
Famphur
pg/L
20.0
16.0
16.7
80.0
83.5
40-140
Methyl Parathion
pg/L
20.0
13.9
15.6
69.5
78.0
40-140
Phorate
pg/L
20.0
15.0
16.3
75.0
81.5
40-140
Tributyl phosphate (S)
74.5
79.0
50-150
Triphenyl phosphate (S)
64.5
68.5
50-150
Rec
Limits
50-150
50-150
RPD Max
RPD
10.0 20.0
6.2 20.0
8.0 20.0
4.2 20.0
11.5 20.0
8.3 20.0
Date: 12/21/2021 12:58 PM
Page 112 of 129
Page 29 of 40

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: L581529
QC Prep Batch Method: 3510C
Lab Reagent Blank LRB-L581529
Associated Lab Samples: 98021, 98022, 98023, 98024
QC Analytical Batch(es): L581684
Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix: AQU
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,3-Dinitrobenzene
pg/L
<0.904
0.904
10.0
10/27/21 17:09
Acenaphthene
pg/L
<0.422
0.422
2.00
10/27/21 17:09
Acenaphthylene
pg/L
<0.429
0.429
2.00
10/27/21 17:09
Acetophenone
pg/L
<0.686
0.686
5.00
10/27/21 17:09
Anthracene
pg/L
<0.467
0.467
2.00
10/27/21 17:09
Benzo(a)anthracene
pg/L
<0.427
0.427
2.00
10/27/21 17:09
Benzo(a)pyrene
pg/L
<1.00
1.00
2.00
10/27/21 17:09
Benzo(b)fluoranthene
pg/L
<0.941
0.941
2.00
10/27/21 17:09
Benzo(g,h,i)perylene
pg/L
<1.36
1.36
2.00
10/27/21 17:09
Benzo(k)fluoranthene
pg/L
<0.752
0.752
2.00
10/27/21 17:09
Benzyl alcohol
pg/L
<3.01
3.01
10.0
10/27/21 17:09
Bis(2-Chloroethoxy)methane
pg/L
<0.433
0.433
5.00
10/27/21 17:09
Bis(2-Chloroethyl)ether
pg/L
<0.447
0.447
5.00
10/27/21 17:09
Bis(2-Chloroisopropyl)ether
pg/L
<0.546
0.546
5.00
10/27/21 17:09
Bis(2-ethylhexyl)phthalate
pg/L
<3.66
3.66
5.00
10/27/21 17:09
4-Bromophenyl phenyl ether
pg/L
<0.500
0.500
5.00
10/27/21 17:09
Butyl benzyl phthalate
pg/L
<4.59
4.59
5.00
10/27/21 17:09
4-Chloro-3-methylphenol
pg/L
<0.503
0.503
5.00
10/27/21 17:09
4-Chloroaniline
pg/L
<0.526
0.526
5.00
10/27/21 17:09
Chlorobenzilate
pg/L
<1.90
1.90
5.00
10/27/21 17:09
2-Chloronaphthalene
pg/L
<0.476
0.476
5.00
10/27/21 17:09
2-Chlorophenol
pg/L
<0.736
0.736
5.00
10/27/21 17:09
4-Chlorophenyl phenyl ether
pg/L
<0.479
0.479
5.00
10/27/21 17:09
Chrysene
pg/L
<0.731
0.731
2.00
10/27/21 17:09
Dibenz(a,h)anthracene
pg/L
<0.252
0.252
2.00
10/27/21 17:09
Dibenzofuran
pg/L
<0.423
0.423
5.00
10/27/21 17:09
1,2-Dichlorobenzene
pg/L
<0.629
0.629
5.00
10/27/21 17:09
Date:
12/21/2021 12:58 PM
Page 30 of 40
Page 113 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: L581529
QC Prep Batch Method: 3510C
Lab Reagent Blank LRB-L581529
Associated Lab Samples: 98021, 98022, 98023, 98024
QC Analytical Batch(es): L581684
Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix: AQU
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,3-Dichlorobenzene
pg/L
<0.491
0.491
5.00
10/27/21 17:09
1,4-Dichlorobenzene
pg/L
<0.580
0.580
5.00
10/27/21 17:09
3,3'-Dichlorobenzidine
pg/L
<3.74
3.74
10.0
10/27/21 17:09
2,4-Dichlorophenol
pg/L
<1.52
1.52
5.00
10/27/21 17:09
2,6-Dichlorophenol
pg/L
<0.703
0.703
5.00
10/27/21 17:09
Diethyl phthalate
pg/L
<0.585
0.585
5.00
10/27/21 17:09
Dimethyl phthalate
pg/L
<0.510
0.510
5.00
10/27/21 17:09
3,3' Dimethylbenzidine
pg/L
<1.88
1.88
10.0
10/27/21 17:09
2,4-Dimethylphenol
pg/L
<0.674
0.674
5.00
10/27/21 17:09
Di-n-butyl phthalate
pg/L
<1.58
1.58
5.00
10/27/21 17:09
4,6- Din itro-2-methylphenol
pg/L
<3.47
3.47
10.0
10/27/21 17:09
2,4-Dinitrophenol
pg/L
<4.85
4.85
10.0
10/27/21 17:09
2,4-Dinitrotoluene
pg/L
<0.403
0.403
5.00
10/27/21 17:09
2,6-Dinitrotoluene
pg/L
<0.413
0.413
5.00
10/27/21 17:09
Di-n-Octyl Phthalate
pg/L
<1.72
1.72
5.00
10/27/21 17:09
Ethyl methanesulfonate
pg/L
<0.714
0.714
5.00
10/27/21 17:09
Fluoranthene
pg/L
<0.406
0.406
2.00
10/27/21 17:09
Fluorene
pg/L
<0.444
0.444
2.00
10/27/21 17:09
Hexachlorobenzene
pg/L
<2.57
2.57
5.00
10/27/21 17:09
Hexachlorobutadiene
pg/L
<0.405
0.405
5.00
10/27/21 17:09
Hexachlorocyclopentadiene
pg/L
<2.34
2.34
5.00
10/27/21 17:09
Hexachloroethane
pg/L
<0.277
0.277
5.00
10/27/21 17:09
Indeno(1,2,3-cd)pyrene
pg/L
<1.01
1.01
2.00
10/27/21 17:09
Isophorone
pg/L
<0.360
0.360
5.00
10/27/21 17:09
Methyl methanesulfonate
pg/L
<0.618
0.618
5.00
10/27/21 17:09
2-Methylnaphthalene
pg/L
<0.485
0.485
2.00
10/27/21 17:09
2-Methylphenol
pg/L
<0.721
0.721
5.00
10/27/21 17:09
Date:
12/21/2021 12:58 PM
Page 31 of 40
Page 114 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: L581529 QC Analytical Batch(es): L581684
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-L581529 Matrix: AQU
Associated Lab Samples: 98021, 98022, 98023, 98024
Blank
MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
3&4 Methylphenol
pg/L
<0.691
0.691
5.00
10/27/21 17:09
Naphthalene
pg/L
<0.484
0.484
2.00
10/27/21 17:09
2-Nitroaniline
pg/L
<0.574
0.574
5.00
10/27/21 17:09
3-Nitroaniline
pg/L
<1.53
1.53
10.0
10/27/21 17:09
4-Nitroaniline
pg/L
<0.740
0.740
5.00
10/27/21 17:09
Nitrobenzene
pg/L
<0.531
0.531
5.00
10/27/21 17:09
2-Nitrophenol
pg/L
<0.606
0.606
5.00
10/27/21 17:09
4-Nitrophenol
pg/L
<1.39
1.39
10.0
10/27/21 17:09
N-Nitrosodimethylamine
pg/L
<0.249
0.249
5.00
10/27/21 17:09
N-Nitrosodiphenylamine
pg/L
<0.783
0.783
10.0
10/27/21 17:09
N-Nitrosodiethylamine
pg/L
<0.400
0.400
5.00
10/27/21 17:09
N-Nitroso-di-n-butylamine
pg/L
<0.752
0.752
5.00
10/27/21 17:09
N-Nitroso-di-n-propylamine
pg/L
<0.334
0.334
5.00
10/27/21 17:09
Pentachloronitrobenzene
pg/L
<1.15
1.15
5.00
10/27/21 17:09
Pentachlorophenol
pg/L
<2.45
2.45
10.0
10/27/21 17:09
Phenacetin
pg/L
<1.28
1.28
5.00
10/27/21 17:09
Phenanthrene
pg/L
<0.464
0.464
2.00
10/27/21 17:09
Phenol
pg/L
<0.389
0.389
5.00
10/27/21 17:09
Pyrene
pg/L
<1.04
1.04
2.00
10/27/21 17:09
1,2,4,5-Tetrachlorobenzene
pg/L
<0.317
0.317
5.00
10/27/21 17:09
2,3,4,6-Tetrachlorophenol
pg/L
<0.355
0.355
5.00
10/27/21 17:09
1,2,4-Trichlorobenzene
pg/L
<0.482
0.482
5.00
10/27/21 17:09
2,4,5-Trichlorophenol
pg/L
<0.350
0.350
5.00
10/27/21 17:09
2,4,6-Trichlorophenol
pg/L
<0.344
0.344
5.00
10/27/21 17:09
2-Fluorobiphenyl(S)
10/27/21 17:09
64.8
24-93
2-Fluorophenol(S)
10/27/21 17:09
25.8
10-44
Nitrobenzene-d5 (S)
10/27/21 17:09
68.5
20-91
Date:
12/21/2021 12:58 PM
Page 32 of 40
Page 115 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-295-8005
QC Prep:
L581529
QC Analytical Batch(es): L581684
QC Prep Batch Method:
3510C
Analysis Method:
8270D
Analysis Description:
Semivolatile
Organic Compounds -
GC/MS
Lab Reagent Blank
LRB-L581529
Matrix: AQU
Associated Lab Samples: 98021, 98022, 98023, 98024
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
Phenol-d6 (S)
10/27/21 17:09
17.0
7-32
4-Terphenyl-d14 (S)
10/27/21 17:09
93.8
35-126
2,4,6-Tribromophenol (S)
10/27/21 17:09
79.1
39-110
Laboratory Control Sample & LCSD
LCS-1-581529 LCSD-L581529
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
1,3-Dinitrobenzene
pg/L
50.0
50.8
44.2
102
88.4
45-135
13.8
20.0
Acenaphthene
pg/L
50.0
40.3
37.0
80.6
74.0
38-117
8.5
20.0
Acenaphthylene
pg/L
50.0
36.3
33.6
72.6
67.2
37-114
7.7
20.0
Acetophenone
pg/L
50.0
35.9
34.0
71.8
68.0
25-108
5.4
20.0
Anthracene
pg/L
50.0
46.2
38.7
92.4
77.4
34-128
17.6
20.0
Benzo(a)anthracene
pg/L
50.0
48.8
41.5
97.6
83.0
36-127
16.1
20.0
Benzo(a)pyrene
pg/L
50.0
50.3
43.8
101
87.6
34-131
13.8
20.0
Benzo(b)fluoranthene
pg/L
50.0
58.1
43.9
116
87.8
36-131
27.8*
20.0
Benzo(g,h,i)perylene
pg/L
50.0
51.1
44.9
102
89.8
26-123
12.9
20.0
Benzo(k)fluoranthene
pg/L
50.0
46.8
45.6
93.6
91.2
32-132
2.5
20.0
Benzyl alcohol
pg/L
50.0
23.6
22.8
47.2
45.6
20-109
3.4
20.0
Bis(2-Chloroethoxy)methane
pg/L
50.0
38.7
37.3
77.4
74.6
20-126
3.6
20.0
Bis(2-Chloroethyl)ether
pg/L
50.0
31.4
30.3
62.8
60.6
16-122
3.5
20.0
Bis(2-Chloroisopropyl)ether
pg/L
50.0
26.3
26.1
52.6
52.2
28-108
0.7
20.0
Bis(2-ethylhexyl)phthalate
pg/L
50.0
47.0
40.5
94.0
81.0
21-162
14.8
20.0
4-Bromophenyl phenyl ether
pg/L
50.0
52.2
43.9
104
87.8
31-124
17.2
20.0
Butyl benzyl phthalate
pg/L
50.0
51.6
43.7
103
87.4
33-142
16.5
20.0
4-Chloro-3-methyl phenol
pg/L
50.0
37.9
34.8
75.8
69.6
35-117
8.5
20.0
4-Chloroaniline
pg/L
50.0
33.4
31.2
66.8
62.4
24-127
6.8
20.0
* QC Fail Date: 12/21/2021 12:58 PM Page 33 of 40
Page 116 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: L581529 QC Analytical Batch(es): L581684
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-L581529 LCSD-L581529
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Chlorobenzilate
pg/L
50.0
54.4
48.6
109
97.2
35-118
11.2
20.0
2-Chloronaphthalene
pg/L
50.0
39.2
36.9
78.4
73.8
29-137
6.0
20.0
2-Chlorophenol
pg/L
50.0
29.0
28.5
58.0
57.0
27-102
1.7
20.0
4-Chlorophenyl phenyl ether
pg/L
50.0
46.5
41.6
93.0
83.2
39-110
11.1
20.0
Chrysene
pg/L
50.0
41.7
35.5
83.4
71.0
30-124
16.0
20.0
Dibenz(a,h)anthracene
pg/L
50.0
50.3
44.1
101
88.2
27-124
13.1
20.0
Dibenzofuran
pg/L
50.0
44.4
39.6
88.8
79.2
40-108
11.4
20.0
1,2-Dichlorobenzene
pg/L
50.0
32.8
33.3
65.6
66.6
26-100
1.5
20.0
1,3-Dichlorobenzene
pg/L
50.0
30.4
31.1
60.8
62.2
21-102
2.2
20.0
1,4-Dichlorobenzene
pg/L
50.0
30.9
31.1
61.8
62.2
24-99
0.6
20.0
3,3'-Dichlorobenzidine
pg/L
150
170
148
113
98.6
6-192
13.8
20.0
2,4-Dichlorophenol
pg/L
50.0
31.9
30.5
63.8
61.0
32-110
4.4
20.0
2,6-Dichlorophenol
pg/L
50.0
43.0
38.4
86.0
76.8
25-112
11.3
20.0
Diethyl phthalate
pg/L
50.0
46.8
40.7
93.6
81.4
36-130
13.9
20.0
Dimethyl phthalate
pg/L
50.0
45.8
39.8
91.6
79.6
34-123
14.0
20.0
3,3' Dimethylbenzidine
pg/L
200
111
99.4
55.5
49.7
6-192
11.0
20.0
2,4-Dimethylphenol
pg/L
50.0
33.9
33.2
67.8
66.4
34-105
2.0
20.0
Di-n-butyl phthalate
pg/L
50.0
49.5
41.6
99.0
83.2
19-158
17.3
20.0
4,6- Din itro-2-methylphenol
pg/L
50.0
66.7
58.8
133*
118
27-128
12.5
20.0
2,4-Dinitrophenol
pg/L
150
130
121
86.6
80.6
10-132
7.1
20.0
2,4-Dinitrotoluene
pg/L
50.0
45.3
40.3
90.6
80.6
24-147
11.6
20.0
2,6-Dinitrotoluene
pg/L
50.0
49.7
42.9
99.4
85.8
36-125
14.6
20.0
Di-n-Octyl Phthalate
pg/L
50.0
45.1
37.7
90.2
75.4
29-136
17.8
20.0
Ethyl methanesulfonate
pg/L
50.0
32.3
31.3
64.6
62.6
20-121
3.1
20.0
Fluoranthene
pg/L
50.0
49.0
39.6
98.0
79.2
28-127
21.2*
20.0
Fluorene
pg/L
50.0
44.0
39.1
88.0
78.2
41-116
11.7
20.0
* QC Fail Date: 12/21/2021 12:58 PM Page 34 of 40
Page 117 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: L581529 QC Analytical Batch(es): L581684
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-L581529 LCSD-L581529
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Hexachlorobenzene
pg/L
50.0
54.4
46.1
109
92.2
18-136
16.5
20.0
Hexachlorobutadiene
pg/L
50.0
35.5
35.9
71.0
71.8
22-109
1.1
20.0
Hexachlorocyclopentadiene
pg/L
50.0
13.2
12.7
26.4
25.4
10-102
3.8
20.0
Hexachloroethane
pg/L
50.0
31.0
31.6
62.0
63.2
16-107
1.9
20.0
Indeno(1,2,3-cd)pyrene
pg/L
50.0
52.0
46.0
104
92.0
22-126
12.2
20.0
Isophorone
pg/L
50.0
26.1
24.8
52.2
49.6
31-116
5.1
20.0
Methyl methanesulfonate
pg/L
50.0
18.2
17.9
36.4
35.8
15-82
1.6
20.0
2-Methylnaphthalene
pg/L
50.0
39.3
36.8
78.6
73.6
34-108
6.5
20.0
2-Methylphenol
pg/L
50.0
24.0
23.4
48.0
46.8
22-97
2.5
20.0
3&4 Methylphenol
pg/L
50.0
24.9
23.5
49.8
47.0
21-96
5.7
20.0
Naphthalene
pg/L
50.0
39.1
36.7
78.2
73.4
33-108
6.3
20.0
2-Nitroaniline
pg/L
50.0
49.0
42.4
98.0
84.8
32-127
14.4
20.0
3-Nitroaniline
pg/L
50.0
38.5
33.2
77.0
66.4
28-142
14.7
20.0
4-Nitroaniline
pg/L
50.0
58.9
47.4
118
94.8
23-139
21.6*
20.0
Nitrobenzene
pg/L
50.0
44.6
44.7
89.2
89.4
27-117
0.2
20.0
2-Nitrophenol
pg/L
50.0
40.1
38.2
80.2
76.4
25-114
4.8
20.0
4-Nitrophenol
pg/L
50.0
16.4
14.7
32.8
29.4
1-76
10.9
20.0
N-Nitrosodimethylamine
pg/L
50.0
15.3
15.8
30.6
31.6
14-84
3.2
20.0
N-Nitrosodiphenylamine
pg/L
50.0
39.3
34.4
78.6
68.8
45-135
13.2
20.0
N-Nitrosodiethylamine
pg/L
50.0
32.8
31.0
65.6
62.0
25-107
5.6
20.0
N-Nitroso-di-n-butylamine
pg/L
50.0
35.8
32.8
71.6
65.6
25-126
8.7
20.0
N-Nitroso-di-n-propylamine
pg/L
50.0
34.0
31.7
68.0
63.4
29-114
7.0
20.0
Pentachloronitrobenzene
pg/L
50.0
57.0
47.7
114
95.4
34-135
17.7
20.0
Pentachlorophenol
pg/L
50.0
54.4
45.5
109
91.0
17-142
17.8
20.0
Phenacetin
pg/L
50.0
44.8
38.1
89.6
76.2
29-141
16.1
20.0
Phenanthrene
pg/L
50.0
49.1
41.2
98.2
82.4
40-120
17.4
20.0
* QC Fail Date: 12/21/2021 12:58 PM Page 35 of 40
Page 118 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: L581529 QC Analytical Batch(es): L581684
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-L581529 LCSD-L581529
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max
RPD
Phenol
pg/L
50.0
9.93
10.1
19.8
20.2
11-55
1.6
20.0
Pyrene
pg/L
50.0
58.3
53.9
117
108
20-154
7.8
20.0
1,2,4,5-Tetrachlorobenzene
pg/L
50.0
42.2
40.6
84.4
81.2
28-110
3.8
20.0
2,3,4,6-Tetrachlorophenol
pg/L
50.0
43.8
37.2
87.6
74.4
28-118
16.2
20.0
1,2,4-Trichlorobenzene
pg/L
50.0
37.0
36.3
74.0
72.6
23-106
1.9
20.0
2,4,5-Trichlorophenol
pg/L
50.0
43.1
37.7
86.2
75.4
26-118
13.3
20.0
2,4,6-Trichlorophenol
pg/L
50.0
47.8
43.5
95.6
87.0
26-115
9.4
20.0
2-Fluorobiphenyl (S)
62.3
60.6
24-93
2-Fluorophenol (S)
24.4
26.2
10-44
Nitrobenzene-d5 (S)
60.7
64.9
20-91
Phenol-d6 (S)
17.4
17.9
7-32
4-Terphenyl-d14 (S)
94.8
91.8
35-126
2,4,6-Tribromophenol (S)
91.0
80.4
39-110
Date: 12/21/2021 12:58 PM Page 36 of 40
Page 119 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: L581530 QC Analytical Batch(es): L581685
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: 8270 Extended List
Lab Reagent Blank LRB-L581530 Matrix: AQU
Associated Lab Samples: 98021, 98022, 98023, 98024
Blank MDL MQL Analyzed
Parameter Units Result
1,3,5-Trinitrobenzene
pg/L
<10.0
10.0
10.0
10/27/21 17:09
Isodrin
pg/L
<10.0
10.0
10.0
10/27/21 17:09
Kepone
pg/L
<10.0
10.0
10.0
10/27/21 17:09
1,4-Naphthoquinone
pg/L
<10.0
10.0
10.0
10/27/21 17:09
1-Naphthylamine
pg/L
<10.0
10.0
10.0
10/27/21 17:09
2-Acetylaminofluorene
pg/L
<10.0
10.0
10.0
10/27/21 17:09
2-Naphthylamine
pg/L
<10.0
10.0
10.0
10/27/21 17:09
3-Methylcholanthrene
pg/L
<10.0
10.0
10.0
10/27/21 17:09
4-Aminobiphenyl
pg/L
<10.0
10.0
10.0
10/27/21 17:09
5-Nitro-o-toluidine
pg/L
<10.0
10.0
10.0
10/27/21 17:09
7,12-Di methyl benz(a)anth racene
pg/L
<10.0
10.0
10.0
10/27/21 17:09
Diallate
pg/L
<10.0
10.0
10.0
10/27/21 17:09
Hexachloropropene
pg/L
<10.0
10.0
10.0
10/27/21 17:09
Isosafrole
pg/L
<10.0
10.0
10.0
10/27/21 17:09
Methapyrilene
pg/L
<10.0
10.0
20.0
10/27/21 17:09
N-Nitrosomethylethylamine
pg/L
<10.0
10.0
10.0
10/27/21 17:09
N-Nitrosomorpholine
pg/L
<10.0
10.0
10.0
10/27/21 17:09
N-Nitrosopiperidine
pg/L
<10.0
10.0
10.0
10/27/21 17:09
N-Nitrosopyrrolidine
pg/L
<10.0
10.0
10.0
10/27/21 17:09
o-Toluidine
pg/L
<10.0
10.0
10.0
10/27/21 17:09
p-Dimethylaminoazobenzene
pg/L
<10.0
10.0
10.0
10/27/21 17:09
p-Phenylenediamine
pg/L
<10.0
10.0
10.0
10/27/21 17:09
Pronamide
pg/L
<10.0
10.0
10.0
10/27/21 17:09
Safrole
pg/L
<10.0
10.0
10.0
10/27/21 17:09
Date: 12/21/2021 12:58 PM Page 37 of 40
Page 120 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID: Anchor QEA of North Carolina, PLLC
Project Description: Jackson County
Report No: 21-295-8005
QC Prep: L581530 QC Analytical Batch(es): L581685
QC Prep Batch Method: 3510C Analysis Method: 8270D
Analysis Description: 8270 Extended List
Laboratory Control Sample & LCSD LCS-L581530 LCSD-L581530
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
1,3,5-Trinitrobenzene
pg/L
50.0
40.0
38.5
80.0
77.0
20-120
3.8
20.0
Isodrin
pg/L
50.0
37.9
35.3
75.8
70.6
20-120
7.1
20.0
Kepone
pg/L
50.0
45.3
41.6
90.6
83.2
20-120
8.5
20.0
1,4-Naphthoquinone
pg/L
50.0
22.8
21.1
45.6
42.2
20-120
7.7
20.0
1-Naphthylamine
pg/L
50.0
10.0
<10.0
20.0
0.0*
20-120
0.0
20.0
2-Acetylaminofluorene
pg/L
50.0
42.2
35.4
84.4
70.8
20-120
17.5
20.0
2-Naphthylamine
pg/L
50.0
10.0
<10.0
20.0
0.0*
20-120
0.0
20.0
3-Methylcholanthrene
pg/L
50.0
37.8
32.7
75.6
65.4
20-120
14.4
20.0
4-Aminobiphenyl
pg/L
50.0
17.1
15.9
34.2
31.8
20-120
7.2
20.0
5-Nitro-o-toluidine
pg/L
50.0
33.3
32.2
66.6
64.4
20-120
3.3
20.0
7,12-Di methyl benz(a)anth racene
pg/L
50.0
34.0
32.3
68.0
64.6
20-120
5.1
20.0
Diallate
pg/L
50.0
33.7
29.3
67.4
58.6
20-120
13.9
20.0
Hexachloropropene
pg/L
50.0
<10.0
<10.0
0.0*
0.0*
20-120
0.0
20.0
Isosafrole
pg/L
50.0
34.8
24.4
69.6
48.8
20-120
35.1*
20.0
Methapyrilene
pg/L
50.0
36.3
32.7
72.6
65.4
20-120
10.4
20.0
N-Nitrosomethylethylamine
pg/L
50.0
14.3
15.2
28.6
30.4
20-120
6.1
20.0
N-Nitrosomorpholine
pg/L
50.0
16.3
16.9
32.6
33.8
20-120
3.6
20.0
N-Nitrosopiperidine
pg/L
50.0
20.0
20.6
40.0
41.2
20-120
2.9
20.0
N-Nitrosopyrrolidine
pg/L
50.0
19.4
20.1
38.8
40.2
20-120
3.5
20.0
o-Toluidine
pg/L
50.0
16.0
16.0
32.0
32.0
20-120
0.0
20.0
p-Dimethylaminoazobenzene
pg/L
50.0
39.1
37.5
78.2
75.0
20-120
4.1
20.0
p-Phenylenediamine
pg/L
50.0
<10.0
<10.0
0.0*
0.0*
20-120
0.0
20.0
Pronamide
pg/L
50.0
38.6
36.0
77.2
72.0
20-120
6.9
20.0
Safrole
pg/L
50.0
23.4
23.6
46.8
47.2
20-120
0.8
20.0
* QC Fail Date: 12/21/2021 12:58 PM Page 38 of 40
Page 121 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-295-8005
QC Prep:
V10693
QC Analytical Batch(es): V10699
QC Prep Batch Method:
SW-9056A (PREP)
Analysis Method:
9056A
Analysis Description:
Anions by Ion Chromatography
Lab Reagent Blank
LRB-V10693
Matrix: AQU
Associated Lab Samples:
97987, 97988, 98018, 98019, 98021
Blank MDL
MQL
Analyzed
Parameter
Units
Result
Chloride
pg/L
<370 370
1000
10/22/21 12:18
Nitrate (NO3-N)
pg/L
<76.0 76.0
200
10/22/21 12:18
Sulfate
pg/L
786 540
1000
10/22/21 12:18
Laboratory Control Sample
LCS-V10693
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Chloride
pg/L
40000
39100
98.0
80-120
Nitrate (NO3-N)
pg/L
4000
3700
93.0
80-120
Sulfate
pg/L
40000
40200
101
80-120
Matrix Spike & Matrix Spike Duplicate
V 97987-MS-V10693
V 97987-MSD-V10693
MS Spike
MSD MS Result
MSD MS
MSD
%Rec Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec
Limits RPD RPD
Conc.
Chloride
pg/L
866 40000
40000 41000
41400 103
104
80-120 0.9 20
Nitrate (NO3-N)
pg/L
<76.0 4000
4000 3890
3900 97.0
98.0
80-120 0.2 20
Sulfate
pg/L
<540 40000
40000 40600
40800 102
102
80-120 0.4 20
Date: 12/21/2021 12:58 PM Page 39 of 40
Page 122 of 129

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
Anchor QEA of North Carolina, PLLC
Project Description:
Jackson County
Report No:
21-295-8005
QC Analytical Batch:
V10722
Analysis Method:
SM-3500-Fe-13
Analysis Description:
Ferrous Iron
Lab Reagent Blank
LRB
Matrix: AQU
Associated Lab Samples:
97987, 97988, 98018,
98019
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Ferrous Iron
pg/L
<50.0
50.0
200
10/25/21 15:56
Laboratory Control Sample
LCS
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Ferrous Iron
pg/L
2000
1970
99.0
90-110
Matrix Spike & Matrix Spike Duplicate
V 97988-MS V 97988-MSD
MS Spike
MSD MS Result
MSD MS
MSD %Rec Max
Parameter
Units
Result
Conc.
Spike
Result %Rec
%Rec Limits RPD RPD
Conc.
Ferrous Iron
pg/L
<50.0
2000
2000 2020
2030 101
101 80-120 0.4 20
Date: 12/21/2021 12:58 PM Page 40 of 40
Page 123 of 129

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 01015
Customer Name: Anchor QEA of North Carolina, PLLC
Report Number: 21-295-8005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client # Courier
0 Other:
Thermometer ID:
IRT-15 5.7C
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
5
Custody seals intact on shipping container/cooler?
Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample Iabel(s)?
(0) Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
U Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
U Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
U N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: ngela D Overcash Date & Time: 12/21/2021 12:22:42
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