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2019.12.31_CCO.p16_ChemoursCorrectiveActionPlan-AppendixB
TR0795 December 2019 APPENDIX B Additional Corrective Action Plan Tables and Figures TR0795 December 2019 APPENDIX B SUPPORTING TABLES, FIGURES, FIELD RECORDS AND LABORATORY REPORTS This document presents supporting documents that include the following: •Figure B-1A: Sample and Flow Measurement Locations September 2019 Event; •Figure B-1B: Cape Fear River Sample Locations September 2019 Event; •Figure B-2: Total Table 3+ Concentrations – September 2019 Event; •Figure B-3: HFPO-DA Concentrations – September 2019 Event; •Figure B-4: Cape Fear River Total Table 3+ Concentrations September 2019 Event; •Figure B-5: Cape Fear River HFPO-DA Concentrations September 2019 Event; •Table B-1: Well Development Stabilized Field Parameters; •Table B-2: Groundwater Sampling Stabilized Field Parameters; •Table B-3: On and Offsite Resampled Groundwater Well Analytical Results – July to November 2019; •Table B-4: September 2019 Mass Loading Model Location Summary; •Table B-5: Analytical Methods and Analyte List; •Table B-6: Analytical Results; •Records of Well Development; •Records of Well Sampling; and •Attachment B: Data Validation Module. * * * * * * * TR0795 FIGURES !( !(!( !(!(!(!( !( !( !( !( !( !( !( #* #* #* #* #* #*#*#* #*#*#* #* #*Ca p e F ea r R i v e r Excess River Water CFR-MILE-76 OUTFALL 002 SEEP-C-1 SEEP-D-1 OLDOF-1 SEEP-A-1SEEP-A-3 SEEP-A-4 SEEP-A-TR1 SEEP-B-1SEEP-B-2 SEEP-B-TR1 SEEP-B-TR2 WC-1 OLDOF-2 W.O. Huske Dam*Old Outfall 002 Willis Creek 1,250 0 1,250625 Feet ³Path: P:\PRJ\Projects\TR0795\Database and GIS\GIS\Corrective Action Plan\TR0795_StreamReaches_FlowMeasurements.mxd Last Revised: 12/13/2019 Author: TIpProjection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US ³Legend #*Flow Measurement Location !(Sample Location Observed Seep Nearby Tributary Site Boundary Notes:* - Flow measurement was taken at W.O. Huske Dam - USGSGauge Site No. 021055001. Flow at Old Outfall 002, Seep A, Seep B and Seep C locationswere measured using flumes.2. Flow at Seep D was measured using salt diultion.3. Flow at Willis Creek and Georgia Branch Creek were measuredusing flow velocity method.4. Results of estimated flow at these locations are provided inTable 5 and Table 7 with supplemental flow measurement dataincluded in Appendix B.5. The outline of Cape Fear River is approximate and is based onopen data from ArcGIS Online and North Carolina Department ofEnvironmental Quality Online GIS. 6. Basemap sources: Esri, DigitalGlobe, GeoEye, EarthstarGeographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN,and the GIS User Community. !(#*GBC-1 G e o r g i a B r a n c h C r e e k ³ 1 0 10.5 Miles ³ 1 2 1 2 Sample and Flow Measurement Locations September 2019 Event Chemours Fayetteville Works, North Carolina Figure B-1ARaleigh 1,000 0 1,000500 Feet December 2019 2,000 0 2,0001,000 Feet !( CFR-BLADEN CFR-MILE-52 CFR-MILE-56 CFR-MILE-68 CFR-MILE-76 Path: P:\PRJ\Projects\TR0795\Database and GIS\GIS\Corrective Action Plan\TR0795_RiverSamples_FlowMeasurements.mxd Last Revised: 2019-12-06 Author: SSomnarainProjection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US Notes:1. Basemap sources: Esri, DigitalGlobe, GeoEye, EarthstarGeographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN,and the GIS User Community. 25 0 2512.5 Miles 1 CFR-KINGS 1 2 0 21 Miles 2 - Downstream 2 Cape Fear River Sample LocationsSeptember 2019 Event Chemours Fayetteville Works, North Carolina Figure B-1BRaleigh 2 0 21 Miles December 2019 Legend Sample Location Site Boundary Cape Fear River !( !( !( !( !(!(!( !( !(!( !( !( !( !( !(Ca p e F e a r R i v e r CFR-MILE-7634 Excess River Water120 OLDOF-1120,000 OUTFALL 002590 SEEP-A-1340,000SEEP-A-3360,000 SEEP-A-4 170,000 SEEP-A-TR1120,000 SEEP-B-1380,000 SEEP-B-2430,000 SEEP-B-TR1 130,000 SEEP-C-1 350,000 SEEP-D-1170,000 WC-12,600 SEEP-B-TR2291,070 Old Outfall 002 Willis Creek 1,250 0 1,250625 Feet ³Path: P:\PRJ\Projects\TR0795\Database and GIS\GIS\Corrective Action Plan\TR0795_StreamReaches_Sept_Tot_Tab_3.mxd Last Revised: 12/13/2019 Author: NBarNahoumProjection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US ³Legend !(Sample Location Observed Seep Nearby Tributary Site Boundary Notes:HFPO-DA - hexafluoropropylene oxide dimer acid 1. All results are in nanograms per liter.2. HFPO-DA is included in the total Table 3+ result, includingHFPO-DA results evaluated by EPA Method 537 Mod.3. Non-detect values were not included in sum of totalTable 3+ results.4. Total Table 3+ results include J-qualified data.5. The outline of Cape Fear River is approximate and is based onopen data from ArcGIS Online and North Carolina Department ofEnvironmental Quality Online GIS.6. Basemap sources: Esri, DigitalGlobe, GeoEye, EarthstarGeographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN,and the GIS User Community. !(GBC-12,100 G e o r g i a B r a n c h C r e e k ³ 1 0 10.5 Miles 1 2 2,000 0 2,0001,000 Feet ³2 1 1,250 0 1,250625 Feet Total Table 3+ Concentrations – September 2019 Event Chemours Fayetteville Works, North Carolina Figure Raleigh 1,000 0 1,000500 Feet December 2019 B-2 !( !( !(!( !( !( !(!(!( !( !(!( !( !( !(Ca pe Fe a r R i v e r Excess River Water26 CFR-MILE-764.5 OUTFALL 00281 J SEEP-C-138,000 SEEP-D-116,000 J OLDOF-17,700 SEEP-A-137,000SEEP-A-343,000 J SEEP-A-419,000 SEEP-A-TR123,000 SEEP-B-125,000SEEP-B-244,000 J SEEP-B-TR118,000 SEEP-B-TR2 41,000 J WC-1400 Old Outfall 002 Willis Creek 1,250 0 1,250625 Feet ³Path: P:\PRJ\Projects\TR0795\Database and GIS\GIS\Corrective Action Plan\TR0795_StreamReaches_Sept_HFPODA.mxd Last Revised: 12/13/2019 Author: NBarNahoumProjection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US ³Legend !(Sample Location Observed Seep Nearby Tributary Site Boundary Notes:J - estimate valueHFPO-DA - hexafluoropropylene oxide dimer acid 1. All results are in nanograms per liter.2. The outline of Cape Fear River is approximate and is based onopen data from ArcGIS Online and North Carolina Department ofEnvironmental Quality Online GIS. 3. Basemap sources: Esri, DigitalGlobe, GeoEye, EarthstarGeographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN,and the GIS User Community. !(GBC-1520 G e o r g i a B r a n c h C r e e k ³ 1 0 10.5 Miles ³ 1 2 1 2 HFPO-DA Concentrations – September 2019 Event Chemours Fayetteville Works, North Carolina Figure Raleigh 1,000 0 1,000500 Feet December 2019 2,000 0 2,0001,000 Feet B-3 CFR-BLADEN410 CFR-MILE-52 36 CFR-MILE-5632 CFR-MILE-68 26 CFR-MILE-76 34 Path: P:\PRJ\Projects\TR0795\Database and GIS\GIS\Corrective Action Plan\TR0795_RiverSamples_Tot_Tab_3.mxd Last Revised: 2019-12-06 Author: SSomnarainProjection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US Notes:HFPO-DA - hexafluoropropylene oxide dimer acid 1. All results are in nanograms per liter.2. HFPO-DA is included in the total Table 3+ result, includingHFPO-DA results evaluated by EPA Method 537 Mod.3. Non-detect values were not included in sum of totalTable 3+ results.4. Total Table 3+ results include J-qualified data.5. Basemap sources: Esri, DigitalGlobe, GeoEye, EarthstarGeographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community. 25 0 2512.5 Miles 1 CFR-KINGS 260 1 2 0 21 Miles 2 - Downstream 2 Cape Fear River Total Table 3+ ConcentrationsSeptember 2019 Event Chemours Fayetteville Works, North Carolina Figure Raleigh 2 0 21 Miles December 2019 Legend Sample Location Site Boundary Cape Fear River B-4 CFR-BLADEN39 J CFR-MILE-68<4 CFR-MILE-764.5 CFR-MILE-52 <4 CFR-MILE-56<4 Path: P:\PRJ\Projects\TR0795\Database and GIS\GIS\Corrective Action Plan\TR0795_RiverSamples_HFPODA.mxd Last Revised: 2019-12-06 Author: SSomnarainProjection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US Notes:< - non-detectJ - estimated value HFPO-DA - hexafluoropropylene oxide dimer acid1. All results are in nanograms per liter.2. Basemap sources: Esri, DigitalGlobe, GeoEye, EarthstarGeographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN,and the GIS User Community. 30 0 3015 Miles 1 CFR-KINGS 27 1 2 0 21 Miles 2 2 - Downstream Cape Fear River HFPO-DA ConcentrationsSeptember 2019 Event Chemours Fayetteville Works, North Carolina Figure Raleigh 2 0 21 Miles December 2019 Legend Sample Location Site Boundary Cape Fear River B-5 TR0795 TABLES TABLE B-1WELL DEVELOPMENT STABILIZED FIELD PARAMETERS Chemours Fayetteville Works, North CarolinaGeosyntec Consultants NC P.C.Well ID Date pHDO (mg/L)ORP(mV)Turbididty(NTU)Spec. Cond.(mS/cm)Temp.(°C)PIW-2D 10/31/2019 5.76 5.91 124.4 29 0.071 19.2PIW-4D 10/22/2019 6.29 1.77 68.1 28.2 0.05 18.42PW-02 10/23/2019 4.32 4.48 312.7 119 0.12 18.95PW-03 10/23/2019 5.37 1.07 37 999 0.38 21.99PW-04 10/28/2019 4.01 0.84 297.1 17.4 0.433 19.7PW-07 10/28/2019 7.51 5.98 271.9 61.5 0.09 18.3PW-09 10/18/2019 7.27 1.75 -36.9 127 0.09 17.51PW-10R 10/23/2019 5.73 0.1 20.2 35.4 0.07 18.01PW-12 10/31/2019 5.92 7.02 85.1 21.7 0.051 18.3PW-13 11/5/2019 6.11 0.19 5.3 45.4 0.05 19.32PW-15R 10/30/2019 5.98 19.51 198 4.91 0.014 18.8CUMBERLAND-2D 10/22/2019 6.17 3.38 -11.8 31.1 0.06 20.03CUMBERLAND-4S 10/18/2019 3.47 2.52 162.1 57.8 0.05 26.11CUMBERLAND-4D 10/18/2019 4.97 48.8 80.1 15.5 0.04 19.91CUMBERLAND-5S 10/21/2019 5.55 1.24 -50.7 9.43 0.11 22.61ROBENSON-1S 10/17/2019 -- -- -- -- -- --ROBENSON-1D 10/17/2019 4.98 44.3 102 19.3 0.06 19.99Notes:1.Stabilized field parameters following well development completion reported here.2.Well development forms included in Appendix B of this report.Abbreviations:DO - Dissolved OxygenmS/cm - milli Siemens per centimeterORP - Oxidation Reduction Potential°C - degree celsiusSpec. Cond. - Specific ConductivityTemp. - Temperaturemg/L - milligrams per litermV - millivoltsNTU - Nephelometric Turbidity UnitsOnsite WellsOffsite WellsPage 1 of 1December 2019 TABLE B-2GROUNDWATER SAMPLING STABILIZED FIELD PARAMETERS Chemours Fayetteville Works, North CarolinaGeosyntec Consultants NC P.C.Well ID Sampling Date Sample TimeField Sample IDpHDO (mg/L)ORP(mV)Turbididty (NTU)Spec. Cond. (mS/cm)Temp. (°C)PIW-1D 10/29/2019 12:10GW4Q19-PIW-1D-1029193.4 0.63 290 6 0.17 18PIW-2D 11/1/2019 11:15GW4Q19-PIW-2D-1101195.8 0.43 45 16 0.07 17PIW-3D 10/28/2019 16:35GW4Q19-PIW-3D-1028194 0.76 -91 8.7 0.1 18PIW-4D 10/31/2019 13:25GW4Q19-PIW-4D-1031197.5 0.6 32 61 0.06 20PIW-5S 10/29/2019 11:40GW4Q19-PIW-5S-1029193.7 2.9 440 11 0.13 19PIW-6S 10/29/2019 13:30GW4Q19-PIW-6S-1029194.6 0.55 210 14 0.094 18PIW-7S 10/30/2019 12:00GW4Q19-PIW-7S-1030196.1 0.31 5.3 3.9 0.15 19PIW-7D 10/30/2019 11:15GW4Q19-PIW-7D-1030194.3 0.29 100 0.71 0.09 19PIW-8D 10/30/2019 13:30GW4Q19-PIW-8D-1030194 0.65 190 1 0.2 18PIW-9D 10/23/2019 11:20GW4Q19-PIW-9D-1023194.7 0 170 0 0.14 17PIW-9S 10/23/2019 12:40GW4Q19-PIW-9S-1023194 0.33 11 1.3 0.11 18PIW-10DR 10/30/2019 15:50 GW4Q19-PIW-10DR-103019 5.5 0.24 17 6.9 0.17 19PIW-10S 10/29/2019 15:10GW4Q19-PIW-10S-1029194 3.8 200 1.1 0.05 19PW-01 10/18/2019 13:40GW4Q19-PW-01-1018194.7 5 250 1.1 0.06 22PW-02 11/4/2019 16:10GW4Q19-PW-02-1104194.7 6.7 240 130 0.11 19PW-03 11/6/2019 12:50GW4Q19-PW-03-1106195.4 0.75 -140 1000 0.21 19.00PW-04 10/30/2019 10:00GW4Q19-PW-04-1030194 0.84 300 12 0.43 20.00PW-05 10/30/2019 10:00GW4Q19-PW-05-1030193.9 4.9 400 3.5 0.08 19PW-06 10/29/2019 15:20GW4Q19-PW-06-1029195.1 3.3 220 1.4 0.067 19PW-07 11/8/2019 9:30GW4Q19-PW-07-1108196 5.3 320 83 0.09 21PW-09 10/30/2019 13:35GW4Q19-PW-09-1030199.5 0.05 -130 68 0.13 19PW-10R 11/4/2019 13:40GW4Q19-PW-10R-1104195.4 0.12 43 5 0.06 18PW-11 10/22/2019 16:25GW4Q19-PW-11-1022194.4 0.00 120 0.00 0.5 19PW-12 11/5/2019 13:20GW4Q19-PW-12-1105195.6 0.00 -150 18 0.05 19PW-13 11/8/2019 15:00GW4Q19-PW-13-1108196.4 1.2 -17 97 0.1 17PW-14 10/23/2019 13:55GW4Q19-PW-14-1023194.7 0.00 170 0.00 0.18 23PW-15R 11/6/2019 14:30GW4Q19-PIW-15R-1106195.1 3.2 150 13 0.15 19BLADEN-1D 11/7/2019 14:31 GW4Q19-BLADEN-1D-110719 7.1 0.54 -51 13 0.13 23BLADEN-2S 10/22/2019 12:30 GW4Q19-BLADEN-2S-102219 6.1 0.44 -34 6.6 0.07 25BLADEN-2D 10/29/2019 12:55 GW4Q19-BLADEN-2D-102919 6 0.09 32 28 0.05 21BLADEN-3S 10/28/2019 12:05 GW4Q19-BLADEN-3S-102819 5.3 5 120 0.62 0.02 25BLADEN-3D 10/28/2019 14:30 GW4Q19-BLADEN-3D-102819 5.9 0.2 31 15 0.08 22BLADEN-4S 10/22/2019 16:50 GW4Q19-BLADEN-4S-102219 5.7 0.55 -43 22 0.07 27BLADEN-4D 10/25/2019 12:45 GW4Q19-BLADEN-4D-102519 6.3 0.02 -76 5.5 0.42 22CUMBERLAND-1S 10/24/2019 10:08 GW4Q19-CUMBERLAND-1S-102419 4.6 6.2 320 1 0.11 23CUMBERLAND-1D 10/24/2019 10:55 GW4Q19-CUMBERLAND-1D-102419 5.2 0.34 -130 14 0.13 21CUMBERLAND-2S 10/23/2019 12:00 GW4Q19-CUMBERLAND-2S-102319 5.1 3.6 220 1.2 0.07 23CUMBERLAND-2D 10/25/2019 12:25 GW4Q19-CUMBERLAND-2D-102519 6.8 0.09 -490 20 0.08 22CUMBERLAND-3S 10/22/2019 15:51 GW4Q19-CUMBERLAND-3D-102219 6.4 1.9 -62 8.8 0.18 24CUMBERLAND-3D 10/23/2019 10:37 GW4Q19-CUMBERLAND-3D-102319 7.6 1.1 -230 3.8 0.23 21CUMBERLAND-4S 10/25/2019 13:57 GW4Q19-CUMBERLAND-4S-102519 4.1 0.41 170 10 0.05 27CUMBERLAND-4D 10/24/2019 14:25 GW4Q19-CUMBERLAND-4D-102419 5.4 0.34 71 18 0.04 23Offsite WellsOnsite WellsTR0795Page 1 of 2December 2019 TABLE B-2GROUNDWATER SAMPLING STABILIZED FIELD PARAMETERS Chemours Fayetteville Works, North CarolinaGeosyntec Consultants NC P.C.Well ID Sampling Date Sample TimeField Sample IDpHDO (mg/L)ORP(mV)Turbididty (NTU)Spec. Cond. (mS/cm)Temp. (°C)CUMBERLAND-5S 10/23/2019 14:32 GW4Q19-CUMBERLAND-5S-102319 5.5 1.3 20 4.8 0.12 24ROBENSON-1S 10/31/2019 13:15 GW4Q19-ROBENSON-1S-103119 5.5 2.8 160 5.1 0.08 25ROBENSON-1D 10/31/2019 11:35 GW4Q19-ROBENSON-1D-103119 6.4 0.13 -100 17 0.08 22Notes:1. PIW-1S and Bladen-1S were dry at the time of sampling2. Duplicate samples collected at PIW-4D, Cumberland-1D and PW-15R3. Stabilized field parameters following well purging reported here.4. Well purging and groundwater sampling forms included in Appendix B of this report.Abbreviations:DO - Dissolved OxygenORP - Oxidation Reduction PotentialSpec. Cond. - Specific ConductivityTemp. - Temperaturemg/L - milligrams per litermV - millivoltsNTU - Nephelometric Turbidity UnitsTR0795Page 2 of 2December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Onsite Onsite Onsite Onsite Onsite Onsite Onsite Onsite Onsite Aquifer Black Creek Aquifer Black Creek Aquifer Surficial Aquifer Surficial Aquifer Surficial Aquifer Surficial Aquifer Surficial Aquifer Black Creek Aquifer Black Creek Aquifer Location ID PIW-10DR PIW-10DR PIW-10S PIW-10S PIW-1D PIW-1D PIW-1D PIW-2D PIW-2D Field Sample ID PIW-10DR-091019 GW4Q19-PIW-10DR-103019 GW0619-PIW-10S GW4Q19-PIW-10S-102919 GW0619-PIW-1D GW0619-PIW-1D-D GW4Q19-PIW-1D-102919 PIW-2D-091219 GW4Q19-PIW-2D-110119 Sample Date 9/10/2019 10/30/2019 7/22/2019 10/29/2019 7/19/2019 7/19/2019 10/29/2019 9/12/2019 11/1/2019 QA/QC ----------DUP ------ Sample Matrix LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID SDG 320-54176-1 320-55860-1 320-52621-1 320-55854-1 320-52621-1 320-52621-1 320-55854-1 320-54314-1 320-56112-1 Lab Sample ID 320-54176-1 320-55860-2 320-52621-3 320-55854-9 320-52621-1 320-52621-2 320-55854-4 320-54314-2 320-56112-3 Table 3+ SOP (ng/L) HFPO-DA 19,000 15,000 4,400 3,600 11,000 J 8,700 J 9,500 1,800 1,600 PFMOAA 45,000 47,000 1,500 1,800 14,000 15,000 14,000 14,000 19,000 PFO2HxA 19,000 19,000 3,000 2,400 9,700 9,700 8,200 2,900 3,500 PFO3OA 6,000 6,500 520 450 1,800 1,800 1,300 100 140 PFO4DA 1,200 J 1,200 210 160 300 320 260 <79 <16 PFO5DA <34 UJ <34 <34 17 <34 <34 <6.7 <34 <6.7 PMPA 9,100 10,000 5,700 5,700 9,900 10,000 9,300 1,300 1,100 PEPA 3,400 3,600 2,100 1,900 3,600 3,600 2,900 92 76 PFESA-BP1 <27 <27 <27 <2.7 <27 <27 <5.3 <27 <5.3 PFESA-BP2 160 J 200 150 93 48 51 52 <30 <6.1 Byproduct 4 1,500 1,200 190 200 420 480 400 <160 44 Byproduct 5 6,400 J 5,600 <58 <5.8 <58 <58 <12 <58 16 Byproduct 6 15 18 <15 <2 <15 <15 <3.1 <15 <3.1 NVHOS 510 490 <54 22 150 160 130 110 J 140 EVE Acid <24 <24 <24 <2.4 <24 <24 <4.9 <24 <4.9 Hydro-EVE Acid 790 J 870 <28 12 37 33 30 <28 <5.6 R-EVE 1,200 980 J 130 110 290 J 350 J 270 <70 40 J PES <46 <46 <46 <4.6 <46 <46 <9.2 <46 <9.2 PFECA B <60 <60 <60 <6 <60 <60 <12 <60 <12 PFECA-G <41 <41 <41 <4.1 <41 <41 <8.2 <41 <8.2 Total Table 3+ Lab SOP*110,000 110,000 18,000 16,000 51,000 50,000 46,000 20,000 26,000 Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. TR0795 Page 1 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Onsite Onsite Onsite Onsite Onsite Onsite Onsite Onsite Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Surficial Aquifer Surficial Aquifer Floodplain Deposits PIW-3D PIW-3D PIW-4D PIW-4D PIW-4D PIW-5S PIW-5S PIW-6S GW0619-PIW-3D GW4Q19-PIW-3D-102819 PIW-04D-091119 GW4Q19-PIW-4D-103119 GW4Q19-PIW-4D-103119-Dup GW0619-PIW-5S GW4Q19-PIW-5S-102919 GW0619-PIW-6S 7/18/2019 10/28/2019 9/11/2019 10/31/2019 10/31/2019 7/19/2019 10/29/2019 7/17/2019 --------DUP ------ LIQUID LIQUID Liquid LIQUID LIQUID LIQUID LIQUID LIQUID 320-52464-1 320-55757-1 320-54317-1 320-55909-1 320-55909-1 320-52624-1 320-55854-1 320-52454-1 320-52464-2 320-55757-6 320-54317-2 320-55909-1 320-55909-2 320-52624-5 320-55854-2 320-52454-5 9,600 11,000 6.7 3.6 B 2.9 B 79,000 J 41,000 13,000 5,400 5,200 <210 <5 <5 35,000 61,000 160,000 9,100 7,900 <81 2.3 2.1 38,000 33,000 35,000 1,700 1,400 <58 <2 <2 10,000 7,600 5,000 780 700 <79 <2 <2 8,700 4,700 150 95 97 <34 <2 <2 4,800 1,900 <34 12,000 10,000 <570 <10 <10 100,000 76,000 8,700 4,400 3,600 <47 <20 <20 44,000 31,000 2,300 <2.7 <5.3 <27 <2 <2 4,300 1,300 <27 150 140 <30 <2 <2 1,300 580 31 500 390 <160 <2 <2 4,700 2,900 470 <5.8 <12 <58 <2 <2 16,000 5,000 1,700 5.1 5.2 <15 <2 <2 65 41 <15 83 72 <54 <2 <2 770 680 1,100 <2.4 <4.9 <24 <2 <2 1,800 570 <24 52 48 <28 <2 <2 1,600 820 43 290 220 J <70 <2 UJ <2 UJ 3,000 2,700 490 <4.6 <9.2 <46 <2 <2 <46 <46 <46 <6 <12 <60 <2 <2 <60 <60 <60 <4.1 <8.2 <41 <2 <2 <41 <41 <41 44,000 41,000 6.7 5.9 5.0 350,000 270,000 230,000 TR0795 Page 2 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Onsite Onsite Onsite Onsite Onsite Onsite Onsite Onsite Floodplain Deposits Black Creek Aquifer Black Creek Aquifer Floodplain Deposits Floodplain Deposits Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer PIW-6S PIW-7D PIW-7D PIW-7S PIW-7S PIW-8D PIW-8D PIW-9D GW4Q19-PIW-6S-102919 GW0619-PIW-7D GW4Q19-PIW-7D-103019 GW0619-PIW-7S GW4Q19-PIW-7S-103019 GW0619-PIW-8D GW4Q19-PIW-8D-103019 GW0619-PIW-9D 10/29/2019 7/19/2019 10/30/2019 7/19/2019 10/30/2019 7/19/2019 10/30/2019 7/23/2019 ---------------- LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID 320-55854-1 320-52624-1 320-55860-1 320-52624-1 320-55860-1 320-52624-1 320-55860-1 320-52722-1 320-55854-3 320-52624-3 320-55860-10 320-52624-4 320-55860-1 320-52624-2 320-55860-9 320-52722-1 10,000 11,000 9,400 1,400 6,600 54,000 J 65,000 33,000 190,000 150,000 170,000 12,000 31,000 400,000 400,000 150,000 33,000 27,000 27,000 2,400 8,000 140,000 110,000 41,000 4,400 2,400 2,900 180 1,500 51,000 45,000 12,000 <160 570 590 <79 96 7,200 6,700 3,100 <67 <34 <34 <34 <34 <340 <130 84 9,000 3,500 3,300 1,100 3,800 15,000 15,000 9,900 2,300 530 510 <47 1,200 4,500 4,200 3,400 <53 <27 <27 <27 <27 <270 <110 29 <61 53 67 <30 77 770 860 370 720 280 300 <160 740 4,400 3,300 J 1,900 J 1,900 690 560 <58 <58 10,000 7,200 2,700 <31 <15 <15 <15 <15 <150 120 18 1,100 810 830 88 350 3,600 3,200 1,700 <49 <24 <24 <24 <24 <240 <97 <24 <56 170 J 200 <28 110 3,700 3,900 1,600 610 350 J 380 130 810 4,500 4,900 1,700 <92 <46 <46 <46 <46 <460 <180 <46 <120 <60 <60 <60 <60 <600 <240 <60 <82 <41 <41 <41 <41 <410 <160 <41 250,000 200,000 220,000 17,000 54,000 700,000 670,000 260,000 TR0795 Page 3 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Onsite Onsite Onsite Onsite Onsite Onsite Onsite Onsite Onsite Black Creek Aquifer Surficial Aquifer Surficial Aquifer Perched Zone Perched Zone Perched Zone Surficial Aquifer Surficial Aquifer Surficial Aquifer PIW-9D PIW-9S PIW-9S PW-01 PW-01 PW-01 PW-02 PW-02 PW-03 GW4Q19-PIW-9D-102319 GW0619-PIW-9S GW4Q19-PIW-9S-102319 PW-01-090919 PW-01-090919-D GW4Q19-PW-01-101819 PW-02-091119 GW4Q19-PW-02-110419 PW-03-091119 10/23/2019 7/18/2019 10/23/2019 9/9/2019 9/9/2019 10/18/2019 9/11/2019 11/4/2019 9/11/2019 --------DUP -------- LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID 320-55683-1 320-52464-1 320-55683-1 320-54217-1 320-54217-1 320-55686-1 320-54274-1 320-56112-1 320-54317-1 320-55683-3 320-52464-1 320-55683-6 320-54217-1 320-54217-2 320-55686-1 320-54274-1 320-56112-7 320-54317-1 20,000 7,300 9,700 8,300 7,500 7,500 7,400 7,800 78,000 200,000 150,000 190,000 25,000 23,000 23,000 9,500,000 89,000 5,900 40,000 34,000 35,000 10,000 9,400 10,000 2,800,000 22,000 18,000 11,000 8,400 8,300 2,000 J 1,900 2,300 750,000 6,200 5,800 2,300 1,500 1,400 1,000 J 960 1,200 250,000 2,300 1,800 <170 <34 <34 660 J 540 930 90,000 950 46 8,500 7,500 7,500 4,100 J 3,600 3,800 470,000 4,200 130,000 3,000 2,700 2,500 1,300 1,200 1,300 180,000 1,500 76,000 <130 <27 <27 490 410 480 35,000 480 130 330 170 200 490 J 400 530 43,000 550 750 <790 800 960 610 470 410 75,000 740 11,000 1,900 J 800 1,000 900 J 880 J 700 J 250,000 3,000 47,000 <77 <15 <15 <15 <15 13 1,900 20 93 1,700 1,500 1,700 280 J 270 270 110,000 970 8,000 <120 <24 <24 110 J 100 95 2,200 25 520 1,600 690 740 130 J 110 120 18,000 220 4,900 630 650 900 310 260 260 36,000 580 12,000 <230 <46 <46 <46 <46 <9.2 <2,300 <46 <46 <300 <60 <60 <60 <60 <12 <3,000 <60 <60 <200 <41 <41 <41 <41 <8.2 <2,000 <41 <41 290,000 220,000 260,000 56,000 51,000 53,000 15,000,000 140,000 400,000 TR0795 Page 4 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Onsite Onsite Onsite Onsite Onsite Onsite Onsite Onsite Onsite Surficial Aquifer Surficial Aquifer Surficial Aquifer Surficial Aquifer Surficial Aquifer Surficial Aquifer Surficial Aquifer Surficial Aquifer Surficial Aquifer PW-03 PW-04 PW-04 PW-05 PW-05 PW-06 PW-06 PW-07 PW-07 GW4Q19-PW-03-110619 PW-04-091119 GW4Q19-PW-04-103019 PW-05-090919 GW4Q19-PW-05-103019 PW-06-091019 GW4Q19-PW-06-102919 PW-07-091319 GW4Q19-PW-07-110819 11/6/2019 9/11/2019 10/30/2019 9/9/2019 10/30/2019 9/10/2019 10/29/2019 9/13/2019 11/8/2019 ------------------ LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID Liquid Liquid LIQUID 320-56117-1 320-54294-1 320-55860-1 320-54174-1 320-55860-1 320-54231-1 320-55854-1 320-54328-1 320-56173-1 320-56117-6 320-54294-4 320-55860-4 320-54174-1 320-55860-3 320-54231-1 320-55854-1 320-54328-2 320-56173-7 61,000 940 1,000 1,600 1,200 950 1,300 1,100 790 J 6,300 270 360 J <210 230 <210 250 400 310 J 18,000 770 950 730 690 510 690 1,000 880 5,700 280 330 73 73 74 110 140 110 1,700 66 70 130 120 <79 71 87 54 <34 <2 <2 <34 UJ <2 UJ <34 <2 UJ <2 5.7 150,000 710 1,100 1,600 1,300 1,100 1,400 1,400 1,400 76,000 310 450 430 410 380 490 440 380 J 94 <2 <2 <27 <2 <27 <2 <2 <2 800 8.4 16 50 59 <30 40 5.1 7.4 10,000 120 200 J <160 36 <160 50 41 23 37,000 4.4 3.6 J <58 <2 <58 <2 <2 9.1 110 <2 <2 <15 <2 <15 <2 <2 <2 8,400 6.7 10 <54 6.4 <54 7.5 9.1 9.1 500 <2 <2 <24 <2 <24 <2 <2 <2 5,300 5.9 10 <28 17 <28 9.3 6.4 6.5 12,000 47 65 J <70 17 <70 22 13 9.5 J <46 <2 <2 <46 <2 <46 <2 <2 <2 <60 <2 <2 <60 <2 <60 <2 <2 <2 <41 <2 <2 <41 <2 <41 <2 <2 <2 390,000 3,500 4,600 4,600 4,200 3,000 4,400 4,600 4,000 TR0795 Page 5 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Onsite Onsite Onsite Onsite Onsite Onsite Onsite Onsite Onsite Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer PW-09 PW-09 PW-10R PW-10R PW-11 PW-11 PW-12 PW-12 PW-13 PW-09-091119 GW4Q19-PW-09-103019 GW0619-PW-10R GW4Q19-PW-10R-110419 PW-11-091019 GW4Q19-PW-11-102319 PW-12-091119 GW4Q19-PW-12-110519 PW-13-091019 9/11/2019 10/30/2019 9/19/2019 11/4/2019 9/10/2019 10/23/2019 9/11/2019 11/5/2019 9/10/2019 ------------------ LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID Liquid LIQUID LIQUID 320-54274-1 320-55860-1 320-54522-1 320-56112-1 320-54231-1 320-55683-1 320-54299-1 320-56112-1 320-54231-1 320-54274-2 320-55860-5 320-54522-1 320-56112-4 320-54231-2 320-55683-2 320-54299-4 320-56112-10 320-54231-3 <4 <2 9,900 5,200 16,000 12,000 <4 <2 <15 <210 <5 130,000 150,000 280,000 190,000 <5 <5 <210 170 J <2 23,000 24,000 56,000 J 36,000 <2 <2 <81 <58 <2 1,100 1,000 32,000 J 18,000 <2 <2 <58 <79 <2 <79 <79 16,000 11,000 <2 <2 <79 <34 <2 <34 34 670 J 1,100 <2 <2 <34 1,600 <10 3,200 3,500 8,200 6,000 15 <10 <570 220 <20 440 490 3,100 2,400 <20 <20 <47 160 J <2 <27 <27 410 440 <2 <2 <27 81 <2 <30 <30 910 980 <2 <2 <30 <160 <2 <160 <160 1,400 1,100 <2 <2 <160 94 <2 160 170 3,200 2,000 J <2 <2 <58 <15 <2 <15 <15 93 <77 <2 <2 <15 <54 <2 680 820 3,000 1,800 <2 <2 <54 <24 <2 <24 <24 <120 <120 <2 <2 <24 <28 <2 <28 <28 940 590 <2 <2 <28 <70 <2 230 150 540 <350 <2 <2 <70 <46 <2 <46 <46 <230 <230 <2 <2 <46 <60 <2 <60 <60 <300 <300 <2 <2 <60 <41 <2 <41 <41 <200 <200 <2 <2 <41 2,300 ND 170,000 190,000 420,000 280,000 15 ND ND TR0795 Page 6 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Onsite Onsite Onsite Onsite Onsite Onsite Onsite Offsite Offsite Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer PW-13 PW-14 PW-14 PW-15R PW-15R PW-15R PW-15R BLADEN-1D BLADEN-1D GW4Q19-PW-13-110819 PW-14-091119 GW4Q19-PW-14-102319 GW0619-PW-15R GW0619-PW-15R-D GW4Q19-PW-15R-110619 GW4Q19-PW-15R-110619-D BLADEN-1D-082719 DUP-1-082719 11/8/2019 9/11/2019 10/23/2019 9/19/2019 9/19/2019 11/6/2019 11/6/2019 8/27/2019 8/27/2019 --------DUP --DUP --DUP LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID 320-56173-1 320-54274-1 320-55683-1 320-54519-1 320-54519-1 320-56117-1 320-56117-1 280-127778-1 280-127778-1 320-56173-8 320-54274-3 320-55683-8 320-54519-1 320-54519-2 320-56117-4 320-56117-5 280-127778-1 280-127778-2 <2 22,000 17,000 8,700 J 11,000 J 11,000 11,000 180 190 <5 9,500,000 95,000 330,000 340,000 450,000 460,000 33 30 <2 3,400,000 27,000 63,000 64,000 76,000 77,000 81 80 <2 1,100,000 8,100 14,000 14,000 16,000 17,000 6.2 6.2 <2 610,000 4,800 2,200 2,200 2,000 2,300 <2 <2 <2 390,000 2,900 <67 <67 <170 <170 <2 <2 <10 1,400,000 13,000 36,000 36,000 50,000 50,000 330 330 <20 390,000 3,400 8,900 9,300 11,000 11,000 110 110 <2 6,000 52 3,300 4,100 2,300 2,400 <2 <2 <2 250,000 2,500 640 J 670 470 480 0.48 J 0.48 J <2 150,000 1,200 1,500 J 1,800 J 2,200 2,400 13 J 11 J <2 190,000 2,400 J 19,000 21,000 27,000 27,000 <2 <2 <2 5,000 42 270 34 <77 <77 <2 <2 <2 96,000 840 3,500 3,500 4,600 4,800 2.2 1.9 J <2 <2,400 25 250 J 190 <120 <120 <2 <2 <2 210,000 2,000 550 J 510 400 430 <2 0.31 J <2 130,000 1,200 700 J 560 930 890 6.2 5.7 <2 <4,600 <46 210 <92 <230 <230 <2 <2 <2 <6,000 <60 220 <120 <300 <300 <2 <2 <2 <4,100 <41 210 <82 <200 <200 <2 <2 ND 18,000,000 180,000 490,000 510,000 650,000 670,000 760 770 TR0795 Page 7 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Offsite Offsite Offsite Offsite Offsite Offsite Offsite Offsite Black Creek Aquifer Black Creek Aquifer Black Creek Aquifer Surficial Aquifer Surficial Aquifer Black Creek Aquifer Black Creek Aquifer Surficial Aquifer BLADEN-1D BLADEN-2D BLADEN-2D BLADEN-2S BLADEN-2S BLADEN-3D BLADEN-3D BLADEN-3S GW4Q19-BLADEN-1D-110719 BLADEN-2D-082719 GW4Q19-Bladen-2D-102919 BLADEN-2S-082719 GW4Q19-BLADEN-2S-102219 BLADEN-3D-082819 GW4Q19-BLADEN-3D-102819 BLADEN-3S-082819 11/7/2019 8/27/2019 10/29/2019 8/27/2019 10/22/2019 8/28/2019 10/28/2019 8/28/2019 ---------------- LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID LIQUID 320-56173-1 280-127778-1 320-55854-1 280-127778-1 320-55686-1 280-127778-1 320-55757-1 280-127778-1 320-56173-3 280-127778-4 320-55854-5 280-127778-3 320-55686-4 280-127778-6 320-55757-4 280-127778-5 140 11 <2 4.6 8.5 B 2.2 J <2 12 24 J <5 <5 11 22 J <5 <5 15 87 6.3 <2 19 J 31 1.3 J <2 31 7.3 0.96 J <2 1.8 J <2 <2 <2 3.8 <2 <2 <2 1.5 J <2 <2 <2 3.1 <2 <2 <2 UJ 0.53 <2 <2 <2 0.98 J 370 77 J <10 68 60 14 <10 39 110 12 J <20 6.8 J <20 2.1 J <20 5.6 J <2 <2 <2 <2 <2 <2 <2 <2 <2 3.9 <2 14 11 0.63 J <2 3.6 7 <2 <2 <2 5.2 <2 <2 1.9 J <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 2 <2 <2 1.5 J <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 0.36 <2 <2 <2 0.46 J 4.2 <2 <2 <2 3.5 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 750 110 ND 130 130 20 ND 120 TR0795 Page 8 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Offsite Offsite Offsite Offsite Offsite Offsite Offsite Surficial Aquifer Black Creek Aquifer Black Creek Aquifer Surficial Aquifer Surficial Aquifer Black Creek Aquifer Black Creek Aquifer BLADEN-3S BLADEN-4D BLADEN-4D BLADEN-4S BLADEN-4S CUMBERLAND-1D CUMBERLAND-1D GW4Q19-BLADEN-3S-102819 BLADEN-4D-082819 GW4Q19-BLADEN-4D-102519 BLADEN-4S-082819 GW4Q19-BLADEN-4S-102219 CUMBER-1D-09162019 GW4Q19-CUMBERLAND-1D-102419 10/28/2019 8/28/2019 10/25/2019 8/28/2019 10/22/2019 9/16/2019 10/24/2019 -------------- LIQUID Liquid LIQUID Liquid LIQUID Liquid LIQUID 320-55757-1 280-127778-1 320-55754-1 280-127778-1 320-55686-1 320-54439-1 320-55761-1 320-55757-3 280-127778-7 320-55754-1 280-127778-10 320-55686-6 320-54439-2 320-55761-1 29 <3.6 <2 <3.7 2.7 B <3.8 5 21 <5 UJ <5 UJ <5 <5 UJ <5 UJ <5 59 <2 <2 3 3.1 <2 <2 5.7 <2 <2 <2 <2 <2 <2 3.9 <2 <2 <2 <2 <2 <2 <2 <2 UJ <2 <2 <2 <2 UJ <2 93 9.2 J <10 12 <10 <10 <10 <20 <20 <20 <20 <20 <20 <20 <2 <2 <2 <2 <2 <2 <2 8.3 <2 <2 1.5 J <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 2.5 J <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 UJ <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 220 9.2 ND 17 3 ND 7.5 TR0795 Page 9 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Offsite Offsite Offsite Offsite Offsite Offsite Black Creek Aquifer Surficial Aquifer Surficial Aquifer Black Creek Aquifer Black Creek Aquifer Surficial Aquifer CUMBERLAND-1D CUMBERLAND-1S CUMBERLAND-1S CUMBERLAND-2D Cumberland-2D CUMBERLAND-2S GW4Q19-CUMBERLAND-1D-102419-D CUMBER-1S-09162019 GW4Q19-CUMBERLAND-1S-102419 Cumber-2D-09162019 GW4Q19-CUMBERLAND-2D-102519 Cumber-2S-09162019 10/24/2019 9/16/2019 10/24/2019 9/16/2019 10/25/2019 9/16/2019 DUP ---------- LIQUID Liquid LIQUID Liquid LIQUID Liquid 320-55761-1 320-54439-1 320-55761-1 320-54378-1 320-55754-1 320-54378-1 320-55761-2 320-54439-1 320-55761-3 320-54378-8 320-55754-2 320-54378-7 4.8 <3.7 <2 <4 UJ <2 <4 UJ <5 <5 <5 UJ <5 <5 22 <2 11 8.5 <2 <2 4.3 <2 1.9 J <2 <2 <2 <2 <2 0.81 J <2 <2 <2 <2 <2 <2 UJ <2 <2 <2 <2 <10 13 16 10 <10 20 <20 <20 <20 <20 <20 <20 <2 <2 <2 <2 <2 <2 <2 1.8 J 2.3 <2 <2 <2 <2 <2 <2 <2 <2 <2 2.4 J <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 7.2 29 27 10 ND 46 TR0795 Page 10 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Offsite Offsite Offsite Offsite Offsite Offsite Surficial Aquifer Black Creek Aquifer Black Creek Aquifer Surficial Aquifer Surficial Aquifer Black Creek Aquifer Cumberland-2S CUMBERLAND-3D Cumberland-3D CUMBERLAND-3S CUMBERLAND-3S CUMBERLAND-4D GW4Q19-CUMBERLAND-2S-102319 Cumber-3D-09162019 GW4Q19-CUMBERLAND-3D-102319 Cumber-3S-09162019 GW4Q19-CUMBERLAND-3S-102219 Cumber-4D-09162019 10/23/2019 9/16/2019 10/23/2019 9/16/2019 10/22/2019 9/16/2019 ------------ LIQUID Liquid LIQUID Liquid LIQUID Liquid 320-55683-1 320-54378-1 320-55683-1 320-54378-1 320-55686-1 320-54378-1 320-55683-1 320-54378-6 320-55683-5 320-54378-5 320-55686-5 320-54378-1 <86 <4 UJ <86 10 J 16 B <4 UJ <210 17 J <210 30 13 J <5 <81 <2 <81 63 40 <2 <58 <2 <58 9.8 J 3 <2 <79 <2 <79 8.7 <2 <2 38 <2 <34 7.6 <2 <2 <570 12 <570 44 61 12 <47 <20 <47 <20 <20 <20 <27 <2 <27 <2 <2 <2 <30 <2 <30 4 5.1 <2 <160 <2 <160 20 J <2 2.7 J <58 <2 <58 <2 <2 <2 <15 <2 <15 <2 <2 <2 <54 <2 <54 <2 <2 <2 <24 <2 <24 <2 <2 <2 <28 <2 <28 <2 <2 <2 <70 <2 <70 11 J 2.3 <2 <46 <2 <46 <2 <2 <2 <60 <2 <60 <2 <2 <2 <41 <2 <41 <2 <2 <2 38 29 ND 210 120 15 TR0795 Page 11 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Offsite Offsite Offsite Offsite Offsite Offsite Black Creek Aquifer Surficial Aquifer Surficial Aquifer Surficial Aquifer Surficial Aquifer Black Creek Aquifer CUMBERLAND-4D CUMBERLAND-4S CUMBERLAND-4S CUMBERLAND-5S Cumberland-5S ROBESON-1D GW4Q19-CUMBERLAND-4D-102419 Cumber-4S-09162019 GW4Q19-CUMBERLAND-4S-102519 Cumber-5S-09162019 GW4Q19-CUMBERLAND-5S-102319 ROBESON-1D-091219 10/24/2019 9/16/2019 10/25/2019 9/16/2019 10/23/2019 9/12/2019 ------------ LIQUID Liquid LIQUID Liquid LIQUID Liquid 320-55761-1 320-54378-1 320-55761-1 320-54378-1 320-55683-1 280-128413-1 320-55761-4 320-54378-2 320-55761-5 320-54378-4 320-55683-7 280-128413-2 <2 110 J 76 <4 UJ <86 6 J <5 39 15 J 22 <210 <5 <2 110 78 J <2 <81 2.8 <2 18 14 <2 <58 <2 <2 5.1 7.3 <2 <79 <2 <2 <2 <2 <2 50 <2 UJ <10 140 120 J 14 <570 35 <20 42 31 <20 <47 <20 <2 <2 <2 <2 <27 <2 <2 4.8 5.6 <2 <30 3 <2 74 J 30 J <2 <160 <2 <2 <2 <2 <2 <58 <2 <2 <2 <2 <2 <15 <2 <2 2.1 <2 <2 <54 <2 <2 <2 <2 <2 <24 <2 <2 <2 <2 <2 <28 <2 <2 18 J 7.6 J <2 <70 <2 <2 <2 <2 <2 <46 <2 <2 <2 <2 <2 <60 <2 <2 <2 <2 <2 <41 <2 ND 560 380 36 50 47 TR0795 Page 12 of 13 December 2019 TABLE B-3 ON AND OFFSITE RESAMPLED GROUNDWATER WELL ANALYTICAL RESULTS - JULY TO NOVEMBER 2019 Chemours Fayetteville Works, North Carolina Geosyntec Consultants of NC P.C. Area Aquifer Location ID Field Sample ID Sample Date QA/QC Sample Matrix SDG Lab Sample ID Table 3+ SOP (ng/L) HFPO-DA PFMOAA PFO2HxA PFO3OA PFO4DA PFO5DA PMPA PEPA PFESA-BP1 PFESA-BP2 Byproduct 4 Byproduct 5 Byproduct 6 NVHOS EVE Acid Hydro-EVE Acid R-EVE PES PFECA B PFECA-G Total Table 3+ Lab SOP* Notes: * - Total Table 3+ was calculated using HFPO- DA from EPA Method 537 Mod and J qualified data, but not non-detect data. The total is rounded to two significant figures. Bold - Analyte detected above associated reporting limit B - analyte detected in an associated blank EPA - Environmental Protection Agency J - Analyte detected. Reported value may not be accurate or precise ng/L - nanograms per liter QA/QC - Quality assurance/ quality control SDG - Sample Delivery Group SOP - standard operating procedure UJ – Analyte not detected. Reporting limit may not be accurate or precise. < - Analyte not detected above associated reporting limit. Offsite Offsite Offsite Black Creek Aquifer Surficial Aquifer Surficial Aquifer ROBESON-1D ROBESON-1S ROBESON-1S GW4Q19-ROBESON-1D-103119 ROBESON-1S-091219 GW4Q19-ROBESON-1S-103119 10/31/2019 9/12/2019 10/31/2019 ------ LIQUID Liquid LIQUID 320-55909-1 280-128413-1 320-55909-1 320-55909-3 280-128413-1 320-55909-4 3.6 B <4 UJ <2 <5 6.3 7.4 <2 6.2 4.9 <2 <2 <2 <2 <2 <2 <2 <2 UJ <2 11 34 18 <20 <20 <20 <2 <2 <2 <2 7.1 8.7 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 11 54 39 TR0795 Page 13 of 13 December 2019 TABLE B-4SEPTEMBER 2019 MASS LOADING MODEL LOCATION SUMMARYChemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Sample Collection Flow MeasurementSep-19Sep-19OLDOF-1Old Outfall 002 Location 1Y--OLDOF-2Old Outfall 002 Location 2--YSEEP-A-1Seep A Location 1YYSEEP-A-3Seep A Location 3YYSEEP-A-4Seep A Location 4YYSEEP-A-TR1 Seep A Tributary 1YYSEEP-B-1Seep B Location 1YYSEEP-B-2Seep B Location 2YYSEEP-B-TR1 Seep B Tributary 1YYSEEP-B-TR2 Seep B Tributary 2YYSEEP-C-1Seep C Location 1YYSEEP-D-1 (2)Seep D Location 1YYWC-1Willis Creek Location 1YYGBC-1Georgia Branch Creek Location 1YYCFR-MILE-52 Cape Fear River Mile 52Y--CFR-MILE-56 Cape Fear River Mile 56Y--CFR-MILE-68 Cape Fear River Mile 68Y--CFR-MILE-76 Cape Fear River Mile 76Y--CFR-BLADEN Cape Fear River at Bladen BluffsY--CFR-KINGS Cape Fear River at Kings BluffY--W.O. Huske Dam USGS Gauge Site No. 02105500--YExcess River Water Excess River WaterYYOutfall 002 Outfall 002 location YYNotes:1. Flow at Old Outfall 002, Seep A, Seep B and Seep C locations were measured using flumes.2. Flow at Seep D was measured using salt diultion.3. Flow at Willis Creek and Georgia Branch Creek were measured using flow velocity method.Y - Sampling or flow measurement was conductedLocation IDLocation Description4. Results of estimated flow at these locations are provided in Table 6 and supplemental flow measurement data is included in Attachment C.TR0795Page 1 of 1 December 2019 TABLE B-5 ANALYTICAL METHODS AND ANALYTE LIST Chemours Fayetteville Works, North Carolina Geosyntec Consultants NC P.C. Analytical Method Common Name Chemical Name CASN Chemical Formula HFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 C6HF11O3 PEPA Perfluoroethoxypropylcarboxylic acid 267239-61-2 C5HF9O3 PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 C12H9F9O3S PFMOAA Perfluoro-2-methoxyacetic acid 674-13-5 C3HF5O3 PFO2HxA Perfluoro(3,5-dioxahexanoic) acid 39492-88-1 C4HF7O4 PFO3OA Perfluoro(3,5,7-trioxaoctanoic)acid 39492-89-2 C5HF9O5 PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic)acid 39492-90-5 C6HF11O6 PMPA 2,3,3,3-Tetrafluoro-2-(trifluoromethoxy)propanoic 13140-29-9 C4HF7O3 Hydro-EVE Acid Hydro-EVE Acid 773804-62-9 C8H2F14O4 EVE Acid Perfluoroethoxypropionicacid 69087-46-3 C8HF13O4 PFECA B Perfluoro-3,6-dioxaheptanoic acid 151772-58-6 C5HF9O4 R-EVE R-EVE EVS1428 C8H2F12O5 PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 C7HF13O7 Byproduct 4 Byproduct 4 EVS1429 C7H2F12O6S Byproduct 5 Byproduct 6 EVS1430 C6H2F12O4S Byproduct 6 Byproduct 5 EVS1431 C7H3F11O7S NVHOS NVHOS 1132933-86-8 C4H2F8O4S PES PES 113507-82-7 C4HF9O4S PFESA-BP1 PFESA-BP1 29311-67-9 C7HF13O5S PFESA-BP2 PFESA-BP2 749836-20-2 C7H2F14O5S PFBA Perfluorobutanoic acid 375-22-4 C4HF7O2 PFDA Perfluorodecanoic acid 335-76-2 C10HF19O2 PFDoA Perfluorododecanoic acid 307-55-1 C12HF23O2 PFHpA Perfluoroheptanoic acid 375-85-9 C7HF13O2 PFNA Perfluorononanoic acid 375-95-1 C9HF17O2 PFOA Perfluorooctanoic acid 335-67-1 C8HF15O PFHxA Perfluorohexanoic acid 307-24-4 C6HF11O2 PFPeA Perfluoropentanoic acid 2706-90-3 C5HF9O2 PFTeA Perfluorotetradecanoic acid 376-06-7 C14HF27O2 PFTriA Perfluorotridecanoic acid 72629-94-8 C13HF25O2 PFUnA Perfluoroundecanoic acid 2058-94-8 C11HF21O2 PFBS Perfluorobutanesulfonate 375-73-5 C4HF9SO PFDS Perfluorodecanesulfonate 335-77-3 C10HF21O3S PFHpS Perfluoroheptanesulfonic acid 375-92-8 C7HF15O3S PFHxS Perfluorohexanesulfonic acid 355-46-4 C6HF13SO3 PFNS Perfluorononanesulfonate 68259-12-1 C9HF19O3S PFOS Perfluorosulfonic acid 1763-23-1 C8HF17SO3 PFPeS Perfluoropentane sulfonic acid 2706-91-4 C5HF11O3S 10:2 FTS Fluorotelomer sulfonate 10:2 120226-60-0 C12H5F21O3 4:2 FTS Fluorotelomer sulfonate 4:2 757124-72-4 C6H5F9O3S 6:2 FTS Fluorotelomer sulfonate 6:2 27619-97-2 C8H5F13SO3 8:2 FTS Fluorotelomer sulfonate 8:2 39108-34-4 C10H5F17O3S NEtFOSAA N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 C12H8F17NO4S NEtPFOSA N-ethylperfluoro-1-octanesulfonamide 4151-50-2 C10H6F17NO2S NEtPFOSAE N-ethyl perfluorooctane sulphonamidoethanol 1691-99-2 C12H10F17NO3S NMeFOSAA N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 C11H6F17NO4S NMePFOSA N-methyl perfluoro-1-octanesulfonamide 31506-32-8 C9H4F17NO2S NMePFOSAE N-methyl perfluorooctane sulfonamidoethanol 24448-09-7 C11H8F17NO3S PFDOS Perfluorododecanesulfonic acid 79780-39-5 C12HF25O3S PFHxDA Perfluorohexadecanoic acid 67905-19-5 C16HF31O2 PFODA Perfluorooctadecanoic acid 16517-11-6 C18HF35O2 PFOSA Perfluorooctane Sulfonamide 754-91-6 C8H2F17NO2S F-53B Major F-53B Major 73606-19-6 C8HClF16O4S F-53B Minor F-53B Minor 83329-89-9 C10HClF20O4S ADONA 4,8-dioxa-3H-perfluorononanoate 958445-44-8 C7H2F12O4 NaDONA NaDONA EVS1361 -- DONA DONA 919005-14-4 -- Notes: Abbreviations: EPA - Environmental Protection Agency ng/L - nanograms per liter PFAS - Per- and Polyfluoroalkyl substances SOP - Standard Operating Procedure Table 3+ Lab SOP EPA Method 537 Mod TR0795 Page 1 of 1 December 2019 TABLE B-6ANALYTICAL RESULTS Chemours Fayetteville Works, North CarolinaGeosyntec Consultants NC P.C.Location ID CFR-BLADENCFR-KINGSCFR-KINGSCFR-MILE-52 CFR-MILE-56 CFR-MILE-68 CFR-MILE-76Excess River WaterField Sample ID CFR-BLADEN-091819 CFR-KINGS-091819 CFR-KINGS-091819-D CFR-RM-52-091719 CFR-RM-56-091719 CFR-RM-68-091719 CFR-RM-76-091719 EXCESS RIVER WATER-091719Sample Date 9/18/20199/17/20199/17/20199/17/20199/17/20199/17/20199/17/20199/17/2019QA/QC----Dup----------Lab Sample ID 320-54536-4320-54545-3320-54545-4320-54545-2320-54545-1320-54536-3320-54544-2320-54544-3HFPO-DA39 J2726<4<4<44.526PFMOAA150 J8285<5 UJ<5<5 UJ<58 JPFO2HxA593334<2<2<24.5 B15 BPFO3OA137.17.6<2<2<2<22.2PFO4DA4.42.32.4<2<2<2<2<2PFO5DA2.2<2<2<2<2<2<2<2PMPA533635<10<10<102042PEPA<20<20<20<20<20<20<20<20PFESA-BP12.8<2<2<2<2<2<2<2PFESA-BP23.222.1<2<2<2<2<2Byproduct 418 J23 J9.6 J16 J15 J12 J<216 JByproduct 546 J33 J32 J4.5 J4.6 J3 J<22.7 JByproduct 6<2<2<2<2<2<2<2<2NVHOS7.14.55.4139.46.84.74.4EVE Acid<2<2<2<2<2<2<2<2Hydro-EVE Acid<2<2<2<2<2<2<2<2R-EVE7.4 J15 J6.9 J2.2 J3.1 J4.4 J<27.1 JPES<2 <2 <2 <2<2<2<2 <2PFECA B<2 <2 <2 <2<2<2<2 <2PFECA-G<2 <2 <2 <2<2<2<2 <2Total Table 3+ SOP4102602503632263412010:2 Fluorotelomer sulfonate<2<2<2<2<2<2<2<21H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)<20<20<20<20<20<20<20<201H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)<20<20<20<20<20<20<20<202-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol<2<2<2<2<2<2<2<22-(N-methyl perfluoro-1-octanesulfonamido)-ethanol<4<4<4<4<4<4<4<46:2 Fluorotelomer sulfonate<20<20<20<20<20<20<20<20N-ethyl perfluorooctane sulfonamidoacetic acid<20<20<20<20<20<20<20<20N-ethylperfluoro-1-octanesulfonamide<2<2<2<2<2<2<2<2N-methyl perfluoro-1-octanesulfonamide<2<2<2<2<2<2<2<2N-methyl perfluorooctane sulfonamidoacetic acid<20<20<20<20<20<20<20<20Perfluorobutane Sulfonic Acid4.62.92.84.85.34.64.74.2Perfluorobutanoic Acid9.95.35.51514109.49.6Perfluorodecane Sulfonic Acid<2<2<2<2<2<2<2<2Perfluorodecanoic Acid<2<2<2<2<2<2<2<2Perfluorododecane sulfonic acid (PFDoS)<2<2<2<2<2<2<2<2Perfluorododecanoic Acid<2<2<2<2<2<2<2<2Perfluoroheptane sulfonic acid (PFHpS)<2<2<2<2<2<2<2<2Perfluoroheptanoic Acid167.17.22827161616Perfluorohexadecanoic acid (PFHxDA)<2<2<2<2<2<2<2<2Perfluorohexane Sulfonic Acid6.565.97.176.666.4Perfluorohexanoic Acid23109.93938242223Perfluorononanesulfonic acid<2<2<2<2<2<2<2<2Perfluorononanoic Acid<2<2<2<2<2<2<2<2Perfluorooctadecanoic acid<2<2<2<2<2<2<2<2Perfluorooctane Sulfonamide<2<2<2<2<2<2<2<2Perfluoropentane sulfonic acid (PFPeS)<2<2<2<2<2<2<2<2Perfluoropentanoic Acid2310124039252323Perfluorotetradecanoic Acid<2<2<2<2<2<2<2<2Perfluorotridecanoic Acid<2<2<2<2<2<2<2<2Perfluoroundecanoic Acid<2<2<2<2<2<2<2<2PFOA6.94.74.799.27.27.18.2PFOS1313131716131315Analytical MethodMethod 537 Table 3+ Lab SOP (ng/L)TR0795Page 1 of 5December 2019 TABLE B-6ANALYTICAL RESULTS Chemours Fayetteville Works, North CarolinaGeosyntec Consultants NC P.C.Location IDField Sample IDSample DateQA/QCLab Sample IDHFPO-DAPFMOAAPFO2HxAPFO3OAPFO4DAPFO5DAPMPAPEPAPFESA-BP1PFESA-BP2Byproduct 4Byproduct 5Byproduct 6NVHOSEVE AcidHydro-EVE AcidR-EVEPESPFECA BPFECA-GTotal Table 3+ SOP10:2 Fluorotelomer sulfonate1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol6:2 Fluorotelomer sulfonateN-ethyl perfluorooctane sulfonamidoacetic acidN-ethylperfluoro-1-octanesulfonamideN-methyl perfluoro-1-octanesulfonamideN-methyl perfluorooctane sulfonamidoacetic acidPerfluorobutane Sulfonic AcidPerfluorobutanoic AcidPerfluorodecane Sulfonic AcidPerfluorodecanoic AcidPerfluorododecane sulfonic acid (PFDoS)Perfluorododecanoic AcidPerfluoroheptane sulfonic acid (PFHpS)Perfluoroheptanoic AcidPerfluorohexadecanoic acid (PFHxDA)Perfluorohexane Sulfonic AcidPerfluorohexanoic AcidPerfluorononanesulfonic acidPerfluorononanoic AcidPerfluorooctadecanoic acidPerfluorooctane SulfonamidePerfluoropentane sulfonic acid (PFPeS)Perfluoropentanoic AcidPerfluorotetradecanoic AcidPerfluorotridecanoic AcidPerfluoroundecanoic AcidPFOAPFOSAnalytical MethodMethod 537 Table 3+ Lab SOP (ng/L)GBC-1OLDOF-1OUTFALL 002SEEP-A-1SEEP-A-3SEEP-A-3SEEP-A-4SEEP-A-TR1SEEP-B-1GBC-1-091719 OLDOF-1-091719 OUTFALL 002-091719 SEEP-A-1-091719 SEEP-A-3-091719 SEEP-A-3-091719-D SEEP-A-4-091719 SEEP-A-TR1-091719 SEEP-B-1-0917199/17/2019 9/17/20199/17/20199/17/20199/17/20199/17/20199/17/20199/17/20199/17/2019----------Dup------320-54543-3 320-54543-2320-54536-2320-54543-4 320-54491-3320-54491-4320-54491-2320-54491-1320-54489-45207,70081 J37,00043,000 J52,000 J19,00023,00025,0008882,00073 J130,000140,000150,00063,00035,000200,00032017,0006555,00056,00061,00027,00024,00046,000444,3002018,00018,00020,0006,5005,3009,100131,3009.89,60011,00010,0002,600 J1,500 J1,2002.38009.26,7008,7008,7002,1002103108005,1004024,00024,00025,00029,00020,00036,0002401,800<209,5009,1009,50012,0007,20014,000<253417,9008,90010,000100 J<271,10022320461,8002,1002,20046029068037 J39026 J3,1003,2003,4001,3009903,900<2970150 J28,00030,00033,0003,600250 J30,000<2<15<28589952215632.77609.7 J1,7001,6001,8006504702,800<2<246.81,5001,7001,900<24<241,400<21902.22,3002,7002,7005102501,90018 J2206 J1,6001,6001,8008706802,600<2<46<2<46<46<46<46<46<92<2<60<2<60<60<60<60<60<120<2<41<2<41<41<41<41<41<822,100120,000590340,000360,000390,000170,000120,000380,000<18<18<2<19<18<18<18<19<18<190<190<20<200<190<190<190<200<190<500<490<24<520<490<490<500<520<500<82<80<4<84<79<80<82<85<82<130<130<6.5<140<130<130<140<140<130<190<190<20<200<190<190<190<200<190<180<180<20<190<180<180<180<190<180<84<82<4.1<86<81<82<84<87<84<41<41<2<43<40<41<42<43<41<300<290<20<310<290<290<300<310<300100894.29387100130140130<34689.9350370370380130460<31<30<2<32<30<30<31<32<31<30<29<2<31<29<29<30<31<30<43<43<2.1<45<42<42<44<45<43<53<52<2.6<55<51<52<53<55<53<18<18<2<19<18<18<18<19<18<2431171401401306547160<86<84<4.1<88<83<84<86<90<86<16<165.8<17<16<16<16<17<16<56<5524<586364<56<58<56<15<15<2<16<15<15<15<16<15<26<26<2<273028<26<27<26<44<44<2.1<46<43<43<44<46<44<34<33<2<35<33<33<34<35<34<29<28<2<30<28<28<29<30<29<47160238007908704803201,200<28<27<2<29<27<27<28<29<28<130<120<6.1<130<120<120<130<130<130<110<100<5.1<110<100<100<110<110<110<82<807.2<84<79<80<82<85<82<52<5114<54<50<51<52<54<52TR0795Page 2 of 5December 2019 TABLE B-6ANALYTICAL RESULTS Chemours Fayetteville Works, North CarolinaGeosyntec Consultants NC P.C.Location IDField Sample IDSample DateQA/QCLab Sample IDHFPO-DAPFMOAAPFO2HxAPFO3OAPFO4DAPFO5DAPMPAPEPAPFESA-BP1PFESA-BP2Byproduct 4Byproduct 5Byproduct 6NVHOSEVE AcidHydro-EVE AcidR-EVEPESPFECA BPFECA-GTotal Table 3+ SOP10:2 Fluorotelomer sulfonate1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol6:2 Fluorotelomer sulfonateN-ethyl perfluorooctane sulfonamidoacetic acidN-ethylperfluoro-1-octanesulfonamideN-methyl perfluoro-1-octanesulfonamideN-methyl perfluorooctane sulfonamidoacetic acidPerfluorobutane Sulfonic AcidPerfluorobutanoic AcidPerfluorodecane Sulfonic AcidPerfluorodecanoic AcidPerfluorododecane sulfonic acid (PFDoS)Perfluorododecanoic AcidPerfluoroheptane sulfonic acid (PFHpS)Perfluoroheptanoic AcidPerfluorohexadecanoic acid (PFHxDA)Perfluorohexane Sulfonic AcidPerfluorohexanoic AcidPerfluorononanesulfonic acidPerfluorononanoic AcidPerfluorooctadecanoic acidPerfluorooctane SulfonamidePerfluoropentane sulfonic acid (PFPeS)Perfluoropentanoic AcidPerfluorotetradecanoic AcidPerfluorotridecanoic AcidPerfluoroundecanoic AcidPFOAPFOSAnalytical MethodMethod 537 Table 3+ Lab SOP (ng/L)SEEP-B-2SEEP-B-TR1SEEP-B-TR2SEEP-C-1SEEP-D-1WC-1EBEBEBFBLKSEEP-B-2-091719 SEEP-B-TR1-091719 SEEP-B-TR2-091719 SEEP-C-1-091719 SEEP D-1-091719 WC-1-091719 EQBLK-091719-01 EQBLK-091719-02 EB-01-091819 FBLK-0917199/17/20199/17/20199/17/20199/17/20199/17/2019 9/17/2019 9/17/20199/17/2019 9/18/2019 9/17/2019------------ Equipment Blank Equipment Blank Equipment BlankField Blank320-54489-3 320-54489-2 320-54489-1320-54544-1 320-54536-1 320-54543-1 320-54544-6 320-54544-5 320-54536-6 320-54544-444,000 J 18,000 41,000 J38,00016,000 J400<4<4<4 UJ<4190,00061,00092,000210,000100,000690 J36<5<5<545,00017,00027,00056,00028,0003806.7<2<2<29,3003,8004,60015,0007,10058<2<2<2<21,5001,3001,2003,4002,10013<2<2<2<24301,500540<1702403<2<2<2<249,00017,00041,00012,0008,100540<10<10<10<1022,0006,00019,0004,1002,700130<20<20<20<202,200<272,100<130<27<2<2<2<2<21,3005801,60053035013<2<2<2<26,1007406,5001,7001,10061 J<2<2<2<245,0004,30038,0002,800 B2,000300 J2.1<2<2<2110<15130<7716<2<2<2<2<24,1005804,5001,90090013<2<2<2<22,800<241,500<120<24<2<2<2<2<23,6003205,0002,2001,4005.9<2<2<2<24,600390 J5,4002,0001,100 J34 J<2<2<2<2<92<46<46<230<46<2<2<2<2<2<120<60<60<300<60<2<2<2<2<2<82<41<41<200<41<2<2<2<2<2430,000130,000290,000350,000170,0002,60045<19<18<18<18<17<19<2<2<2<2<200<190<190<190<180<200<20<20<20<20<510<490<490<500<470<520<20<20<20<20<84<80<80<81<77<86<2<2<2<2<140<130<130<130<130<140<4<4<4<4<200<190<190<190<180<200<20<20<20<20<190<180<180<180<170<190<20<20<20<20<85<82<82<83<78<88<2<2<2<2<42<40<40<41<39<43<2<2<2<2<300<290<290<300<280<310<20<20<20<20100110130<19<18220<2<2<2<2780450800380210<35<2<2<2<2<31<30<30<31<29<32<2<2<2<2<30<29<29<30<28<31<2<2<2<2<44<42<42<43<41<45<2<2<2<2<54<52<52<53<50<55<2<2<2<2<19<18<18<18<17<19<2<2<2<223070240240110<25<2<2<2<2<87<84<84<85<80<90<2<2<2<2<17<16<16<16<15<17<2<2<2<262<546384<52<58<2<2<2<2<16<15<15<15<14<16<2<2<2<2<27<25<25<26<24<27<2<2<2<2<45<43<43<44<41<46<2<2<2<2<34<33<33<33<32<35<2<2<2<2<29<28<28<29<27<30<2<2<2<21,9005702,1001,900790<49<2<2<2<2<28<27<27<28<26<29<2<2<2<2<130<120<120<120<120<130<2<2<2<2<110<100<100<110<99<110<2<2<2<2<84<80<80<81<77<86<2<2<2<2<53<51<51<52<49<54<2<2<2<2TR0795Page 3 of 5December 2019 TABLE B-6ANALYTICAL RESULTS Chemours Fayetteville Works, North CarolinaGeosyntec Consultants NC P.C.Location IDField Sample IDSample DateQA/QCLab Sample IDHFPO-DAPFMOAAPFO2HxAPFO3OAPFO4DAPFO5DAPMPAPEPAPFESA-BP1PFESA-BP2Byproduct 4Byproduct 5Byproduct 6NVHOSEVE AcidHydro-EVE AcidR-EVEPESPFECA BPFECA-GTotal Table 3+ SOP10:2 Fluorotelomer sulfonate1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol6:2 Fluorotelomer sulfonateN-ethyl perfluorooctane sulfonamidoacetic acidN-ethylperfluoro-1-octanesulfonamideN-methyl perfluoro-1-octanesulfonamideN-methyl perfluorooctane sulfonamidoacetic acidPerfluorobutane Sulfonic AcidPerfluorobutanoic AcidPerfluorodecane Sulfonic AcidPerfluorodecanoic AcidPerfluorododecane sulfonic acid (PFDoS)Perfluorododecanoic AcidPerfluoroheptane sulfonic acid (PFHpS)Perfluoroheptanoic AcidPerfluorohexadecanoic acid (PFHxDA)Perfluorohexane Sulfonic AcidPerfluorohexanoic AcidPerfluorononanesulfonic acidPerfluorononanoic AcidPerfluorooctadecanoic acidPerfluorooctane SulfonamidePerfluoropentane sulfonic acid (PFPeS)Perfluoropentanoic AcidPerfluorotetradecanoic AcidPerfluorotridecanoic AcidPerfluoroundecanoic AcidPFOAPFOSAnalytical MethodMethod 537 Table 3+ Lab SOP (ng/L)FBLKFB-01-0918199/18/2019Field Blank320-54536-5<4Notes:<51. Bold - Analyte detected above associated reporting limit<22. F53B-Major, F53B-Minor, DONA, ADONA and NaDONA were not reported by the laboratory at the time of this analysis.<2Abbreviations: <2B - analyte detected in an associated blank<2J - Analyte detected. Reported value may not be accurate or precise<10ng/L - nanograms per liter<20QA/QC - Quality assurance/ quality control<2SOP - standard operating procedure<2UJ – Analyte not detected. Reporting limit may not be accurate or precise. <2< - Analyte not detected above associated reporting limit. <2<2<2<2<2<2<2<2<2<2<20<20<2<4<20<20<2<2<20<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2<2TR0795Page 4 of 5December 2019 TR0795 RECORD OF WELL DEVELOPMENT Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-21-2019 Time:13:56 Water Volume = 5.41 58.45 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 14:26 6.00 7500.00 36.00 5.67 51.10 41.20 995.00 Cloudy No 14:40 6.10 7500.00 30.00 6.24 52.10 9.30 547.00 Cloudy No 14:50 6.15 7500.00 30.00 6.32 51.60 8.90 447.00 Cloudy No 15:10 6.20 7500.00 30.00 6.4 56.50 8.70 162.00 Cloudy No 15:25 6.21 7500.00 30.00 6.45 57.10 9.30 79.70 Semi cloudy No 15:35 6.25 7500.00 20.00 6.45 56.60 8.80 86.00 Semi cloudy No 15:45 6.30 7500.00 20.00 6.45 56.40 8.40 66.00 Slightly cloudy No 15:55 6.33 7500.00 20.00 6.43 55.40 8.30 64.00 Clear No Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: 0.07 19.67 0.07 19.68 0.07 19.70 0.08 19.91 0.08 20.20 0.08 19.82 RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well Cumberland-2D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.08 20.46 Initial Depth to Water (ft.): Temperature (F): 8.486Low Flow: SS Monsoon Pump Temp.(oC)PFAS19.70 Screen Interval: 47 - 57 6.43pH STABILIZED PARAMETERS 0.07 64.00 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 55.40 8.30 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.08 20.21 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-22-2019 Time:10:40 Water Volume = 5.44 58.2 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 10:45 5.20 11250.00 45.00 7.08 2.14 -70.00 116.00 Semi cloudy Sulfuric 11:00 6.22 11250.00 45.00 6.74 2.57 -36.00 74.30 Semi cloudy Sulfuric 11:15 6.30 11250.00 45.00 6.3 3.04 -17.70 51.90 Semi cloudy Sulfuric 11:30 6.32 11250.00 45.00 6.19 3.38 -7.20 38.60 Clear No 11:45 6.35 11250.00 45.00 6.19 3.38 -11.10 33.10 Clear No 12:00 6.40 11250.00 45.00 6.17 3.38 -11.80 31.10 Clear No Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: 0.06 20.03 0.06 19.60 0.06 19.80 0.06 20.00 RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well Cumberland-2D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.08 19.90 Initial Depth to Water (ft.): Temperature (F): 8.442Low Flow: SS Monsoon Pump Temp.(oC)PFAS20.03 Screen Interval: 47 - 57 6.17pH STABILIZED PARAMETERS 0.06 31.10 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 3.38 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.07 19.70 Cloudy Rain Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-18-2019 Time:11:02 Water Volume = 13.9 68.7 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:17 16.65 7500.00 30.00 5.58 59.00 84.50 Cloudy Sulfuric smell 11:30 17.80 7500.00 26.00 5.06 63.30 69.80 404.00 Cliudy Sulfuric odor 11:45 16.85 7500.00 30.00 5.14 83.30 82.10 583.00 Cloudy Sulfuric odor 12:00 16.90 7500.00 30.00 5.13 53.80 80.10 316.00 Cloudy Sulfuric odor 12:15 16.90 7500.00 30.00 5.17 51.20 88.20 77.00 Cloudy Sulfuric odor 14:10 16.35 7500.00 6.00 5.14 59.80 94.30 373.00 Cloudy Sulfuric odor 14:20 16.68 7500.00 20.00 4.92 48.00 75.50 92.60 Clear Sulfuric odor 14:35 16.80 7500.00 5 50.60 80.70 34.70 Clear Sulfuric odor 14:50 16.90 7500.00 30.00 5 48.60 78.80 18.80 Clear Sulfuric odor 15:05 16.90 7500.00 30.00 4.97 48.80 80.10 15.50 Clear Sulfuric odor Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: 0.04 19.98 0.04 19.91 0.05 20.00 0.04 19.97 0.04 20.06 0.04 20.05 0.04 20.19 0.04 19.79 RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE Nick charles WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well Cumberland-4D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.07 20.55 Initial Depth to Water (ft.): Temperature (F): 8.768Low Flow: SS Monsoon Pump Temp.(oC)PFAS19.91 Screen Interval: 57 - 67 4.97pH STABILIZED PARAMETERS 0.04 15.50 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 48.80 80.10 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Turbidity over range 0.05 19.80 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-18-2019 Time:11:13 Water Volume = 7.65 20.3 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:44 14.75 7900.00 72.00 3.44 0.00 233.00 69.10 Cloudy Sulfuric 12:06 14.72 7900.00 108.00 3.36 0.56 236.00 58.50 Cloudy Sulfuric 12:18 14.64 7900.00 104.00 3.43 0.36 232.00 58.00 Slightly cloudy Sulfuric 14:18 14.02 7900.00 128.00 3.51 0.70 234.00 60.20 Clear Sulfuric 14:47 12.45 7900.00 158.00 3.78 6.70 225.00 140.00 Slightly cloudy Sulfuric 15:02 14.48 7900.00 178.00 3.64 3.67 131.80 78.10 Clear None 15:20 14.63 7900.00 208.00 3.52 3.06 149.00 51.40 Red/orange No 15:38 14.65 7900.00 226.00 3.47 2.52 162.10 57.80 Yellow,orang e None Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: 0.05 26.77 0.05 27.18 0.05 26.11 0.04 27.64 0.04 27.65 0.00 28.17 Fluctuating dtw from 8.8 to ~14 RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well Cumberland-4S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.04 27.69 Initial Depth to Water (ft.): Temperature (F): 2.024Low Flow: SS Monsoon Pump Temp.(oC)PFAS26.11 Screen Interval: 10 - 20 3.47pH STABILIZED PARAMETERS 0.05 57.80 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 2.52 162.10 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.04 27.65 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-21-2019 Time:11:20 Water Volume = 7.59 20.91 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:43 10.85 11.00 5.55 67.10 101.30 114.00 Orange Sulfuric 12:00 10.52 9.00 4.52 56.60 142.50 469.00 Orange Sulfuric 12:15 9.70 7.50 4.3 56.60 163.30 41.50 Orange Sulfuric 12:30 10.70 7.50 4.31 56.90 168.40 25.60 Orange Sulfuric 12:45 9.60 7.50 4.27 55.90 169.20 17.30 Orange Sulfuric Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: 0.05 25.93 0.05 25.89 0.05 25.81 RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well Cumberland-4S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.09 26.74 Initial Depth to Water (ft.): Temperature (F): 2.131Low Flow: SS Monsoon Pump Temp.(oC)PFAS25.81 Screen Interval: 10 - 20 4.27pH STABILIZED PARAMETERS 0.05 17.30 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 55.90 169.20 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.06 25.89 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-21-2019 Time:11:04 Water Volume = 4.48 23.23 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:30 4.59 9000.00 5.63 8.66 -28.60 984.00 Tan Yes 11:50 4.63 9000.00 5.8 2.10 -20.60 325.00 Light tan Yes 12:05 4.64 9000.00 5.69 1.46 -21.00 652.00 Tan Yes 12:20 4.64 9000.00 5.63 1.59 -69.40 402.00 Light tan Yes 12:35 4.64 9000.00 5.63 1.22 -59.60 218.00 Light tan Yes 12:50 4.64 9000.00 5.64 1.45 -66.40 235.00 Cloudy Yes 13:05 4.64 9000.00 5.64 1.46 -8.90 130.00 Cloudy Yes 13:20 4.64 9000.00 5.63 1.50 -68.40 66.60 Cloudy Yes 13:24 4.64 9000.00 5.62 1.60 -69.50 55.10 Cloudy Yes 16:10 4.60 9000.00 5.68 2.26 -67.50 145.00 Cloudy Yes 16:20 4.62 9000.00 5.61 1.71 -59.90 64.40 Cloudy Yes 16:30 4.62 9000.00 5.61 1.59 10.60 34.70 Cloudy Yes 16:40 4.64 9000.00 5.59 1.70 46.20 21.60 Clear Yes 16:50 4.64 9000.00 5.52 1.72 -34.70 19.30 Clear Yes 16:00 4.64 9000.00 5.63 1.43 -44.50 14.70 Clear Yes 17:10 4.64 9000.00 5.59 1.14 -54.70 11.40 Clear Yes 17:20 4.64 9000.00 5.6 1.26 -51.70 9.66 Clear Yes 17:30 4.64 9000.00 5.5 1.25 -50.20 9.33 Clear Yes 17:40 4.64 9000.00 5.55 1.24 -50.70 9.43 Clear Yes Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: 0.11 22.63 0.11 22.61 Odor, possible petroleum contamination from gas station 0.12 22.63 0.11 22.50 0.11 22.64 0.11 22.80 0.11 22.72 0.11 22.83 0.11 23.22 0.12 23.26 0.11 22.88 0.12 22.87 0.11 22.91 0.11 22.78 0.12 22.67 0.12 22.68 0.12 22.75 RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER Justin Hobart WATER VOLUME CALCULATION Other Tracy Ovbey bottom of well Cumberland-5S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp.oC 0.12 22.95 Initial Depth to Water (ft.): Temperature (F): 3Conventional: SS Monsoon Pump Temp.(oC)PFAS22.61 Screen Interval: 14 - 24 5.55pH STABILIZED PARAMETERS 0.11 9.43 Spec. Cond.(mS/cm) Turbidity (NTU) 61.00 250 mL poly NP DO (mg/L) ORP (mV) 1.24 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.13 23.07 Partly Cloudy None Wind (mph)5 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-28-2019 Time:14:10 Water Volume = 36.75 53 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 14:25 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: RECORD OF WELL DEVELOPMENT Well ran dry = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LAUREN LACY WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PIW-2D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC Initial Depth to Water (ft.): Temperature (F): 2.6Electric Submersible Pump Temp.(oC)PFAS Screen Interval: 40 - 50 pH STABILIZED PARAMETERS Spec. Cond.(mS/cm) Turbidity (NTU) 80.00 250 mL poly NP DO (mg/L) ORP (mV) WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Well went dry before readings could be taken. Let recharge 30 minutes Sunny None Wind (mph)9 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-29-2019 Time:10:46 Water Volume = 36.9 53 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:00 50.55 6.18 11.20 106.50 832.00 Cloudy No 13:38 Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: RECORD OF WELL DEVELOPMENT Well ran dry = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PIW-2D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.09 18.62 Initial Depth to Water (ft.): Temperature (F): 2.576Electric Submersible Pump Temp.(oC)PFAS Screen Interval: 40 - 50 pH STABILIZED PARAMETERS Spec. Cond.(mS/cm) Turbidity (NTU) 65.00 250 mL poly NP DO (mg/L) ORP (mV) WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Well went dry at 1103 Developed until dry for the third time. Cloudy None Wind (mph)8 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-22-2019 Time:14:51 Water Volume = Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 14:53 8500.00 6.51 2.53 55.30 1000.00 Grey present 15:10 8500.00 6.21 1.25 52.00 152.00 Cloudy no 15:29 8500.00 6.2 1.77 52.90 82.30 Slightly cloudy Strong 15:48 8500.00 5.9 1.61 81.50 67.20 Clear Strong 15:59 8500.00 6.01 1.31 64.90 36.60 Clear Strong 16:07 8500.00 6.24 1.62 62.90 32.50 Clear Strong 16:13 8500.00 6.29 1.78 65.70 29.50 Clear Strong 16:21 8500.00 6.29 1.77 68.10 28.20 Clear Strong Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: 0.05 18.98 0.05 18.76 0.05 18.42 About 250 gal purged. 0.06 20.21 0.05 19.56 0.05 19.02 RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 CHARLES PACE WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PIW-4D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.06 19.44 Initial Depth to Water (ft.): Temperature (F): 0Electric Submersible Pump Temp.(oC)PFAS18.42 Screen Interval: 32.3 - 37.3 6.29pH STABILIZED PARAMETERS 0.05 28.20 Spec. Cond.(mS/cm) Turbidity (NTU) 81.00 250 mL poly NP DO (mg/L) ORP (mV) 1.77 68.10 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.05 19.80 Partly Cloudy None Wind (mph)9 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-23-2019 Time:10:20 Water Volume = 56.64 63.49 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 10:38 58.45 4.99 3.92 174.50 484.00 10:45 56.78 4.76 4.15 228.70 430.00 11:10 58.45 4.61 4.03 249.40 350.00 11:25 4.47 3.79 272.00 244.00 11:40 58.42 4.43 4.22 283.00 216.00 11:55 59.15 4.84 4.36 242.70 245.00 12:10 59.23 4.49 4.67 267.30 200.00 12:25 59.29 4.41 4.63 290.00 192.00 12:40 59.31 4.37 4.42 299.40 184.00 12:55 59.32 4.33 4.28 305.90 157.00 13:10 59.34 4.32 4.28 309.70 131.00 13:25 59.35 4.32 4.48 312.70 119.00 Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: 0.12 18.95 Tank full stop purging at 250 gal 0.12 18.91 0.12 18.82 0.12 18.86 0.12 19.26 0.12 19.01 0.12 18.96 0.12 19.57 0.12 0.12 19.12 RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 Alli Vo, Brandon Peach WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PW-02 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.13 19.28 Initial Depth to Water (ft.): Temperature (F): 1.096 Electric Submersible Pump Temp.(oC)PFAS18.95 Screen Interval: 50 - 60 4.32pH STABILIZED PARAMETERS 0.12 119.00 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 4.48 312.70 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.12 19.25 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-23-2019 Time:13:00 Water Volume = 42.46 48.65 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:35 42.60 4800.00 6.7 1.30 -19.70 999.00 Dark gray None 13:50 43.50 4800.00 6.54 -0.20 25.10 999.00 Dark gray None 16:05 42.65 4800.00 5.37 1.07 37.00 999.00 Dark grey No Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: RECORD OF WELL DEVELOPMENT Well ran dry = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PW-03 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 2.97Total Volume Purged (gallons): Temperature (F): 0.99 70.00 250 mL poly NP 0.38 21.99 3 well volumes purged, about 3 gallons in total Conventional: SS Monsoon Pump Temp.(oC)PFAS21.99 Screen Interval: 35 - 45 5.37pH STABILIZED PARAMETERS 0.38 999.00 Spec. Cond.(mS/cm) Turbidity (NTU) Temp.oC 0.39 21.33 Initial Depth to Water (ft.): DO (mg/L) ORP (mV) 1.07 37.00 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.35 22.97 Decided to read depth to water right before turning pump on Sunny None Wind (mph)4 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-28-2019 Time:11:30 Water Volume = 29.52 30.87 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:38 3.84 4.35 99.10 Cloudy No 11:54 30.84 2.94 1.47 157.60 36.40 Clear No Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: RECORD OF WELL DEVELOPMENT Well ran dry = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PW-04 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.40 22.70 Initial Depth to Water (ft.): Temperature (F): 0.216Peristaltic Pump Temp.(oC)PFAS23.94 Screen Interval: 17 - 27 2.94pH STABILIZED PARAMETERS 0.02 36.40 Spec. Cond.(mS/cm) Turbidity (NTU) 73.00 250 mL poly NP DO (mg/L) ORP (mV) 1.47 157.60 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Turbidity OR 0.02 23.94 Went dry at 12:00 Sunny None Wind (mph)9 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-28-2019 Time:13:06 Water Volume = 39.89 41.83 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:25 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: RECORD OF WELL DEVELOPMENT Well ran dry = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PW-07 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC Initial Depth to Water (ft.): Temperature (F): 0.31Electric Submersible Pump Temp.(oC)PFAS Screen Interval: 28 - 38 pH STABILIZED PARAMETERS Spec. Cond.(mS/cm) Turbidity (NTU) 77.00 250 mL poly NP DO (mg/L) ORP (mV) WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Well went dry before any readings could be taken Sunny None Wind (mph)5 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-29-2019 Time:10:09 Water Volume = 39.6 41 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 10:32 40.60 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: RECORD OF WELL DEVELOPMENT Well ran dry = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PW-07 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC Initial Depth to Water (ft.): Temperature (F): 0.224Electric Submersible Pump Temp.(oC)PFAS Screen Interval: 28 - 38 pH STABILIZED PARAMETERS Spec. Cond.(mS/cm) Turbidity (NTU) 63.00 250 mL poly NP DO (mg/L) ORP (mV) WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Well too dry to pump water all the way out. Pumped what we could and Cloudy None Wind (mph)9 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-01-2019 Time:09:19 Water Volume = 40.1 41.85 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min. gal.mg/L mV NTU 09:31 40.10 6.75 75.60 66.60 265.00 Muddy Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: RECORD OF WELL DEVELOPMENT Well ran dry = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey PW-07 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 0.5Total Volume Purged (gallons): Temp. oC 0.07 16.40 Initial Depth to Water (ft.): Temperature (F): 0.28 Temp.(oC)PFAS16.40 Screen Interval: 28 - 38 6.75pH STABILIZED PARAMETERS 0.07 265.00 Spec. Cond.(mS/cm) Turbidity (NTU) 46.00 250 mL poly NP DO (mg/L) ORP (mV) 75.60 66.60 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Bailer Sunny None Wind (mph)11 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-05-2019 Time:09:19 Water Volume = 39.99 41.77 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 09:20 39.99 0.25 9.1 6.23 171.60 120.00 Cloudy None Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PW-07 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp.oC 0.10 18.50 Initial Depth to Water (ft.): Temperature (F): 0.285 Temp.(oC)PFAS18.50 Screen Interval: 28 - 38 9.10pH STABILIZED PARAMETERS 0.10 120.00 Spec. Cond.(mS/cm) Turbidity (NTU) 59.00 250 mL poly NP DO (mg/L) ORP (mV) 6.23 171.60 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Using bailer to develop well dry, second time. Sunny None Wind (mph)1 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-18-2019 Time:10:59 Water Volume = 25.33 57.71 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:20 9.21 3.92 33.90 613.00 Cloudy No 11:45 9.32 3.47 38.80 496.00 Cloudy No 12:30 9.03 2.29 14.80 289.00 Cloudy No 13:00 8.11 1.85 -23.10 201.00 Cloudy No 13:15 7.78 1.76 -38.00 171.00 Cloudy No 13:30 7.61 1.86 -46.00 153.00 Cloudy No 13:45 7.54 1.88 -49.70 148.00 Cloudy No 14:00 7.51 1.87 -32.00 142.00 Cloudy No 14:20 7.31 1.68 -35.90 128.00 Cloudy No 14:25 7.27 1.75 -36.90 127.00 Cloudy No Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: 0.09 17.50 0.09 17.51 0.09 17.59 0.09 17.48 0.09 17.50 0.11 17.43 Have not been steadily pumping, will let recharge then pump dry 0.10 17.62 0.09 17.52 RECORD OF WELL DEVELOPMENT Well ran dry = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 CHARLES PACE WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PW-09 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.14 17.63 Initial Depth to Water (ft.): Temperature (F): 5.181Electric Submersible Pump Temp.(oC)PFAS17.51 Screen Interval: 44 - 54 7.27pH STABILIZED PARAMETERS 0.09 127.00 Spec. Cond.(mS/cm) Turbidity (NTU) 59.00 250 mL poly NP DO (mg/L) ORP (mV) 1.75 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.13 17.52 Well is running dry but recharging quickly, we are pumping dry and Sunny None Wind (mph)8 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-23-2019 Time:11:46 Water Volume = 27.83 70.53 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 12:39 52.16 4800.00 11.60 6.03 27.50 28.00 793.00 Grey Sulfuric smell 12:44 54.13 4800.00 15.00 5.99 8.40 10.90 755.00 15.00 Grey 12:49 54.48 4800.00 5.00 6 6.10 6.70 728.00 Grey Sulfuric smell 12:54 54.94 4800.00 5.00 5.98 6.00 5.10 507.00 Grey Sulfuric smell 12:59 54.97 4800.00 5.00 5.96 5.30 5.80 238.00 Light grey Sulfuric smell 13:04 54.89 4800.00 5.00 5.95 4.80 5.40 157.00 Light grey Sulfuric smell 13:10 54.85 4800.00 5.00 5.93 4.30 6.70 224.00 Light grey Sulfuric smell 13:15 55.02 4800.00 5.00 5.93 0.31 6.30 124.00 Clear Sulfuric smell 13:20 55.15 4800.00 5.00 5.91 0.26 7.30 106.00 Clear No 13:25 55.16 4800.00 5.00 5.89 0.27 8.10 90.30 Clear No 14:18 52.28 4800.00 10.00 5.71 0.19 23.10 139.00 Clear No odor 14:23 53.68 4800.00 5.00 5.83 0.19 15.30 169.00 Clear Sulfuric smell 14:29 54.22 4800.00 5.00 5.82 0.12 15.00 117.00 Clear Sulfuric smell 14:34 55.02 4800.00 5.00 5.82 0.15 15.00 133.00 Light grey No odor 14:39 55.44 4800.00 5.00 5.81 0.17 15.20 106.00 Clear Sulfuric smell 14:44 55.75 4800.00 5.00 5.83 0.14 15.20 91.00 Clear Same odor 14:49 55.58 4800.00 5.00 5.81 0.15 15.10 176.00 Clear Same odor 14:55 55.30 4800.00 5.00 5.79 0.12 15.80 70.50 Clear No odor 15:01 55.36 4800.00 5.00 5.78 0.16 16.10 60.10 Clear Same odor 15:05 55.38 4800.00 5.00 5.78 0.26 16.20 52.60 Clear Same odor 15:11 55.39 4800.00 5.00 5.77 0.01 16.60 47.10 Clear Same odor 15:14 4800.00 5.00 5.76 -0.31 17.50 Clear Same odor 16:07 50.28 4800.00 5.00 5.8 1.34 24.10 123.00 Clear Sulfuric smell 16:15 52.78 4800.00 8.00 5.8 0.50 22.10 94.00 Clear Same odor 16:21 53.40 4800.00 5.00 5.78 0.28 21.50 81.30 Clear No 16:25 53.57 4800.00 5.00 5.77 0.18 21.30 66.50 Clear Same odor 16:31 53.70 4800.00 6.00 5.76 0.15 20.90 57.20 Clear Same odor 16:38 53.75 4800.00 8.00 5.75 0.14 20.50 46.50 Clear Same odor 16:43 53.82 4800.00 5.00 5.74 0.10 20.40 42.50 Clear Same odor 16:49 54.19 4800.00 6.00 5.74 0.11 20.60 42.80 Clear Same odor 16:54 54.16 4800.00 5.00 5.73 0.11 20.40 37.10 Clear Same odor 16:59 54.11 4800.00 5.00 5.73 0.10 20.20 35.40 Clear Same odor Sampling Data Zero HS: Method:Date: Time: Field Parameters 0.07 18.01 0.07 18.01 0.07 18.01 1700 stopped purging. Turbidity under 50 NTU for four readings and 0.07 18.01 0.07 18.01 0.07 18.01 0.07 18.00 0.07 18.01 0.07 18.01 0.07 18.05 0.07 18.06 Pump cut off at 15:14. No depth to water and turbidity reading was 0.07 17.99 Pump reconnected at 1602. Initial water level = 28.09 ft from top of 0.07 18.04 0.07 18.04 0.07 18.04 0.07 18.04 0.07 18.03 0.07 18.04 0.07 18.04 169.00 0.07 18.05 0.07 18.04 0.08 18.07 0.08 18.07 Cut off the pump and dump IDW water. 0.08 18.05 Started pumping at 1408. Initial water level was at 28.07 ft from top 0.08 18.10 DO input unit is percent but not mg/l 0.08 18.08 0.08 18.11 DO unit switched from percentage to mg/l 0.07 18.03 0.07 18.04 0.07 18.07 RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 KEN STUART Michael Wang WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen PW-10R Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.07 17.97 Initial Depth to Water (ft.): 6.832Electric Submersible Pump Screen Interval: 5.73pH STABILIZED PARAMETERS 0.07Spec. Cond.(mS/cm) Comments SAMPLE SET PFAS Parameter Method EPA 537 Modified Bottle 2-250 mL poly NP Pres. DO unit is percent not mg/l throughout the readings below. 0.07 18.01 Sulfuric smell Sample ID: DuplicateID: Temperature (F): Temp.(oC)PFAS18.01 57 - 6735.40Turbidity (NTU) 68.00 250 mL poly NP DO (mg/L) ORP (mV) 0.10 20.20 WEATHER CONDITIONS Table 3+ PFAS Table 3250 mL poly NP Sunny None Wind (mph)5 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-01-2019 Time:09:45 Water Volume = 29.76 131.25 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min. gal.mg/L mV NTU 10:30 33.92 360.00 1.44 10.11 0.23 -218.10 1000.00 Cloudy No odor 10:45 38.55 360.00 1.44 9.98 0.20 -206.90 1000.00 Cloudy No odor 11:00 41.41 360.00 1.44 9.22 0.18 -203.60 1000.00 Cloudy No odor 11:15 42.88 360.00 1.44 8.26 0.16 -174.80 1000.00 Cloudy No odor 11:30 43.66 360.00 1.44 7.31 0.19 -134.70 1000.00 Cloudy No odor 11:45 44.17 360.00 1.44 6.92 0.23 -114.30 1000.00 Cloudy NA 12:00 44.45 360.00 1.44 6.87 0.26 -120.10 1000.00 Cloudy No odor 12:15 44.77 360.00 1.44 6.69 0.22 -115.80 880.00 Cloudy No odor 12:30 44.92 360.00 1.44 6.59 0.22 -115.50 783.00 Cloudy No odor 12:45 44.95 360.00 1.44 6.56 0.20 -116.50 626.00 Cloudy No odor 13:00 44.95 360.00 1.44 6.52 0.19 -119.80 591.00 Cloudy No odor 13:15 45.08 360.00 1.44 6.47 0.02 -120.40 506.00 Cloudy No odor 13:30 45.21 360.00 1.44 6.45 0.18 -122.10 532.00 Cloudy No odor 13:45 45.28 360.00 1.44 6.44 0.04 -126.90 469.00 Cloudy No odor 14:00 45.28 360.00 1.44 6.42 0.25 -128.20 479.00 Cloudy No odor 14:15 45.29 360.00 1.44 6.33 0.17 -127.90 452.10 Cloudy No odor Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: 0.10 19.79 0.09 19.62 0.10 19.58 0.10 19.47 0.10 19.58 0.10 19.62 0.10 19.59 0.10 19.62 0.12 19.15 Slightly less turbid but still exceeds limits of meter 0.11 19.52 0.11 19.52 0.20 19.24 Turbidity meter maxed out 0.15 19.10 0.13 19.16 Turbidity meter maxed out RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE Ali Vo WATER VOLUME CALCULATION Quarterly Tracy Ovbey 131.2 bottom of well PW-13 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.31 18.03 Initial Depth to Water (ft.): Temperature (F): 16.238Double valve pump Temp.(oC)PFAS19.62 Screen Interval: 120 - 130 6.33pH STABILIZED PARAMETERS 0.09 452.10 Spec. Cond.(mS/cm) Turbidity (NTU) 44.00 250 mL poly NP DO (mg/L) ORP (mV) 0.17 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Turbidity meter maxed out 0.29 18.89 Sunny None Wind (mph)10 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-04-2019 Time:15:10 Water Volume = 33.32 130.81 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min. gal.mg/L mV NTU 15:40 62.88 3000.00 11.88 9.64 0.86 16.50 999.00 Gray None 15:55 66.40 3000.00 10.30 7.46 0.44 -84.30 999.00 Gray None 16:10 55.78 3000.00 9.51 6.79 0.29 -39.00 822.00 Brown None 16:25 53.31 3000.00 11.88 6.49 0.27 -18.70 492.00 Cloudy brown None 16:40 52.73 3000.00 11.88 6.38 0.23 -11.80 345.00 Cloudy brown None Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: 0.10 19.19 0.10 19.14 Flow rate back at 3000ml/min 0.10 19.11 Last reading for today, will continue developing in the morning RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER K. Stuart WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PW-13 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.25 19.42 Initial Depth to Water (ft.): Temperature (F): 15.598 Electric Submersible Pump Temp.(oC)PFAS19.11 Screen Interval: 120 - 130 6.38pH STABILIZED PARAMETERS 0.10 345.00 Spec. Cond.(mS/cm) Turbidity (NTU) 67.00 250 mL poly NP DO (mg/L) ORP (mV) 0.23 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.12 19.34 Slowed pump rate from 3000 to 2400 ml/min Sunny None Wind (mph)2 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-05-2019 Time:09:56 Water Volume = 31.24 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 10:05 51.58 3840.00 5.94 7.17 1.63 40.60 999.00 Gray None 10:20 56.37 3840.00 17.83 6.43 1.04 26.20 478.00 Grayish tan None 10:35 55.98 3840.00 17.83 6.2 2.17 20.10 211.00 Light tan None 10:50 54.71 3840.00 17.83 6.27 1.28 26.50 347.00 Light tan None 11:05 55.21 3840.00 15.22 6.1 1.28 23.80 172.00 Light tan None 11:20 55.11 3840.00 15.22 6.06 1.33 23.40 111.00 Light tan None 11:35 53.51 3840.00 15.22 6.05 1.33 22.20 98.80 Light tan None 13:45 34.16 3840.00 5.94 6.19 1.66 82.90 606.00 Light brown None 14:00 51.59 3840.00 17.83 5.69 1.21 63.60 421.00 Light tan None 14:15 51.96 3840.00 17.83 5.79 1.28 50.90 139.00 Light tan None 14:30 52.31 3840.00 17.83 5.81 1.32 46.40 111.00 Light tan None 14:45 51.24 3840.00 17.83 5.85 1.30 41.30 86.60 Light tan None 15:00 52.58 3840.00 17.83 5.87 1.28 37.60 77.60 Cloudy None 15:15 52.38 3840.00 17.83 5.89 1.25 34.70 60.30 Cloudy None 15:30 52.03 3840.00 17.83 5.92 1.17 31.80 66.00 Cloudy None 16:00 50.10 3840.00 11.09 5.64 0.48 76.00 273.00 Light tan None 16:10 51.89 3840.00 11.09 5.78 0.56 55.40 123.00 Light tan None 16:20 51.91 3840.00 11.09 5.86 0.70 47.30 83.80 Cloudy None 16:30 51.89 3840.00 11.09 5.88 0.86 42.80 69.40 Cloudy None 16:40 51.88 3840.00 11.09 5.89 0.95 39.80 63.70 Cloudy None Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: 0.07 19.30 0.07 19.30 0.07 19.30 0.07 19.30 Stopped developing to empty tote. 0.08 19.30 Pump rate 4200ml/min 0.07 19.30 0.07 19.30 0.07 19.30 0.07 19.30 0.08 19.40 0.07 19.30 0.07 19.30 0.08 19.30 0.07 19.30 Break for lunch after this reading 0.08 19.40 Back from lunch, flow rate is now 4500ml/min 0.08 19.20 0.08 19.30 0.08 19.30 RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER K. Stuart WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PW-13 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp.oC 0.10 19.30 Initial Depth to Water (ft.): Temperature (F): -4.998Electric Submersible Pump Temp.(oC)PFAS19.30 Screen Interval: 120 - 130 5.89pH STABILIZED PARAMETERS 0.07 63.70 Spec. Cond.(mS/cm) Turbidity (NTU) 61.00 250 mL poly NP DO (mg/L) ORP (mV) 0.95 39.80 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Flow rate at 4500ml/min 0.08 19.30 Sunny NonePrecipitation: Sky: Wind (mph)1 Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10/17/2019 Time:1233 Water Volume = 11.54 28.23 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr. ft. ml/min. gal.mg/L mV NTU 1233 6375.00 1253 16.97 1258 16.70 1318 15.13 5.00 8.46 167.00 42.10 1333 1338 4.89 7.45 170.00 8.40 1353 1507 11.49 1510 1523 11.55 5.06 6.67 155.00 0.00 1525 1530 1545 1550 1615 5.3 5.29 122.70 5.20 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: Temperature (F): Wind (mph) Sky: Precipitation: WEATHER CONDITIONS ORP (mV)122.70 5.20 17-27 PFAS 250 mL poly Spec. Cond.(mS/cm)0.05 Screen Interval:PFAS 2-250 mL poly NP EPA 537 Modified DO (mg/L)5.29 NP Table 3 Temp.(oC)21.55 PFAS 250 mL poly NP Table 3+ Turbidity (NTU) STABILIZED PARAMETERS SAMPLE SET pH 5.30 Parameter Bottle Pres.Method Total Volume Purged (gallons): 220 0.054 21.55 disconnected and purged reconnected disconnected and purged reconnected started pumping 0.049 22.85 disconnected the pump cutt off the pump 0.046 22.81 recoonected the pump reconnected the pump 0.050 22.64 reconected. Started purging. cut the pump off, purge the well Initial Depth to Water (ft.): Depth to Well Bottom (ft.): Spec. Cond. Temp.Comments mS/cm oC WATER VOLUME CALCULATION = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot RECORD OF DEVELOPMENT Chemours Fayetteville Robeson-1S Michael Wang Project Manager: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-17-2019 Time:12:32 Water Volume = 13.5 54.4 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:11 14.58 6000.00 67.20 7.6 0.00 55.10 Cloudy No 13:29 14.63 6000.00 96.00 6.13 42.50 36.30 Cloudy Sulfuric 13:51 14.70 6000.00 128.00 5.88 38.20 53.70 75.50 Clear Sulfuric 15:26 14.55 6000.00 158.00 5.68 60.60 87.80 178.00 Clear Sulfuric 15:41 14.55 6000.00 188.00 5.1 45.20 106.20 8.87 Clear Sulfuric 15:56 14.62 6000.00 218.00 5.3 46.80 93.20 737.00 Cloudy Sulfuric 16:11 14.65 6000.00 248.00 5.04 44.00 99.30 104.00 Clear Sulfuric 16:26 14.69 6000.00 278.00 4.98 44.30 102.00 19.30 Clear Sulfuric Sampling Data Zero HS: Method:Date: Time:Field Parameters Sample ID: DuplicateID: 0.06 20.13 0.06 20.35 0.06 19.99 0.07 20.11 0.07 20.80 0.06 20.69 RECORD OF WELL DEVELOPMENT = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE Nick Charles WATER VOLUME CALCULATION Quarterly Tracy Ovbey 50 bottom of well Robeson-1D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.16 20.27 Initial Depth to Water (ft.): Temperature (F): 54.4Low Flow: SS Monsoon Pump Temp.(oC)PFAS19.99 Screen Interval: 42.75 - 52.75 4.98pH STABILIZED PARAMETERS 0.06 19.30 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 44.30 102.00 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Turbidity exceeded detection limit 0.09 20.53 Turbidity over range Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10/31/2019 Time:1400 Water Volume = 36.85 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr. ft. ml/min. gal.mg/L mV NTU 1415 35.61 6.24 11.47 138.30 278.00 1420 38.95 5.81 9.80 165.00 263.00 1425 40.43 150.00 5.63 9.73 159.10 201.00 1435 40.39 150.00 5.8 9.63 137.00 142.00 1440 -150.00 5.8 8.86 131.70 58.70 1445 40.97 150.00 5.8 8.07 130.00 58.60 1450 41.01 150.00 5.79 7.63 129.20 54.60 1455 41.07 150.00 5.79 7.70 128.30 33.80 1500 -150.00 5.79 7.19 128.00 31.80 1505 41.13 150.00 5.76 7.01 128.10 31.90 1510 41.17 150.00 5.75 6.73 128.70 28.50 1515 -150.00 5.75 6.10 126.70 25.00 1520 -150.00 5.77 6.03 124.80 25.10 1525 -150.00 5.76 5.91 124.40 29.00 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: RECORD OF DEVELOPMENT Chemours Fayetteville PIW-2D Brandon Peach and Savannah Volkoff Project Manager: Initial Depth to Water (ft.): Depth to Well Bottom (ft.): Spec. Cond. Temp.Comments mS/cm oC WATER VOLUME CALCULATION = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot 0.082 19.00 0.078 19.40 0.09 20.50 0.085 19.20 0.074 19.30 0.072 19.20 0.075 19.30 0.075 19.20 0.071 19.20 0.072 19.20 0.071 19.20 0.071 19.20 0.071 19.20 0.071 19.20 Total Volume Purged (gallons): STABILIZED PARAMETERS SAMPLE SET pH 5.76 Parameter Bottle Pres.Method Spec. Cond.(mS/cm)0.07 Screen Interval:PFAS 2-250 mL poly NP EPA 537 Modified DO (mg/L)5.91 NP Table 3 Temp.(oC)19.20 PFAS 250 mL poly NP Table 3+ Turbidity (NTU)29.00 PFAS 250 mL poly WEATHER CONDITIONS ORP (mV)124.40 Temperature (F): Wind (mph) Sky: Precipitation: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10/31/2019 Time:9:55 Water Volume = 58.4 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr. ft. ml/min. gal.mg/L mV NTU 0955 1005 58.20 575.00 5.57 5.77 141.40 441.00 1020 58.14 500.00 5.73 5.89 118.10 242.00 1035 58.10 500.00 5.76 6.43 110.00 148.00 1050 58.12 500.00 5.81 6.47 100.40 88.60 1105 58.10 500.00 5.83 6.76 96.80 78.50 1120 58.10 500.00 5.84 6.51 93.80 50.80 1135 58.10 500.00 5.86 6.73 91.30 37.90 1150 58.10 500.00 5.88 6.87 89.10 29.80 1155 58.10 500.00 5.88 7.02 88.30 27.40 1200 58.20 500.00 5.89 7.20 88.10 26.20 1205 58.10 500.00 5.89 7.03 87.50 23.20 1210 58.10 500.00 5.91 7.40 86.20 24.60 1215 58.10 500.00 5.92 7.29 85.80 22.00 1220 58.10 500.00 5.91 7.77 85.00 22.40 1225 58.10 500.00 5.92 7.49 82.40 21.80 1230 58.10 500.00 5.92 7.02 85.10 21.70 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: 0.051 18.50 0.051 18.30 0.051 18.30 0.051 18.30 0.051 18.30 0.052 18.60 0.051 18.60 = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville Brandon Peach and Savannah Volkoff WATER VOLUME CALCULATION PW-12 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.052 18.50 Temperature (F): Temp.(oC)PFAS18.30 Screen Interval: 5.92pH STABILIZED PARAMETERS 0.05 21.70 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 7.02 85.10 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.052 18.40 Wind (mph) Precipitation: Sky: RECORD OF DEVELOPMENT 0.051 0.051 0.051 0.051 0.051 18.30 18.40 18.30 18.30 18.30 Initial Depth to Water (ft.): 0.051 18.30 0.051 18.50 Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10/30/2019 Time:1510 Water Volume = 54.32 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr. ft. ml/min. gal.mg/L mV NTU 1520 60.47 800.00 7.48 2.01 46.40 184.00 1535 59.63 750.00 6.37 4.72 74.30 65.50 1550 61.27 750.00 5.7 16.50 134.40 96.00 1609 61.05 750.00 5.25 23.60 140.10 15.00 1615 61.27 750.00 5.99 18.58 143.10 9.75 1620 61.25 750.00 5.55 18.11 141.60 8.55 1625 61.31 750.00 5.43 19.09 148.30 13.90 1630 60.91 750.00 5.42 18.54 147.60 13.60 1635 61.30 750.00 5.48 19.51 148.00 4.91 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: RECORD OF DEVELOPMENT Chemours Fayetteville P1W-15R Brandon Peach and Savannah Volkoff Project Manager: Initial Depth to Water (ft.): Depth to Well Bottom (ft.): Spec. Cond. Temp.Comments mS/cm oC WATER VOLUME CALCULATION = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot 18.70 18.80 19.00 19.00 18.80 18.20 18.80 18.90 18.80 Total Volume Purged (gallons): STABILIZED PARAMETERS SAMPLE SET pH 5.48 Parameter Bottle Pres.Method Spec. Cond.(mS/cm)Screen Interval:PFAS 2-250 mL poly NP EPA 537 Modified DO (mg/L)19.51 NP Table 3 Temp.(oC)18.80 PFAS 250 mL poly NP Table 3+ Turbidity (NTU)4.91 PFAS 250 mL poly WEATHER CONDITIONS ORP (mV)148.00 Temperature (F): Wind (mph) Sky: Precipitation: TR0795 RECORD OF WELL SAMPLING Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-22-2019 Time:10:50 Water Volume = Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 18:12 Sampling Data Zero HS: Method:Date: Time:18:12 Field Parameters Sample ID: DuplicateID: RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER Justin Hobart WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen Bladen-1S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp.oC Initial Depth to Water (ft.): Temperature (F): 0 10-22-2019 Low Flow: Geo Pump Temp.(oC)PFAS Screen Interval: 5 - 10 pH STABILIZED PARAMETERS Spec. Cond.(mS/cm) Turbidity (NTU) 68.00 250 mL poly NP DO (mg/L) ORP (mV) GW4Q19-Bladen-1S WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Well is dry Cloudy None Wind (mph)2 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-07-2019 Time:13:30 Water Volume = 19.75 38.7 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:45 19.79 100.00 8.78 0.78 149.70 50.10 Clear 13:51 19.79 100.00 8.84 0.54 87.20 34.70 Clear 13:54 19.79 100.00 8.7 0.51 57.30 25.70 Clear Sulfur like odor 14:00 19.79 100.00 8.33 0.50 -34.90 20.70 Clear Sulfur 14:05 19.79 100.00 7.95 0.53 -56.70 18.10 Clear 14:10 19.79 100.00 7.57 0.54 -56.00 17.30 Clear Sulfur like odor 14:15 19.79 100.00 7.45 0.53 -66.50 18.00 Clear Sulfur like smell 14:20 19.79 100.00 7.33 0.57 -56.30 14.00 Clear Sulfur like odor 14:25 19.79 100.00 7.18 0.58 -54.70 15.20 Clear Sulfur like odor 14:30 19.79 100.00 7.08 0.54 -51.40 13.00 Clear Sulfur like odor Sampling Data Zero HS: Method:Date: Time:14:31 Field Parameters Sample ID: DuplicateID: 0.12 22.40 0.13 22.60 0.13 22.40 0.13 22.50 0.13 22.70 0.13 23.10 0.13 22.40 0.13 22.20 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER K. Stuart WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen Bladen-1D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp.oC 0.14 21.60 Initial Depth to Water (ft.): Temperature (F): 3.032 11-07-2019 Low Flow: Geo Pump Temp.(oC)PFAS22.60 Screen Interval: 37 - 47 7.08pH STABILIZED PARAMETERS 0.13 13.00 Spec. Cond.(mS/cm) Turbidity (NTU) 74.00 250 mL poly NP DO (mg/L) ORP (mV) 0.54 GW4Q19-Bladen-1D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.14 22.90 Sunny None Wind (mph)3 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-22-2019 Time:11:27 Water Volume = 7.39 19.73 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:55 8.40 120.00 5.83 1.13 38.50 8.93 Clear None 11:58 8.61 120.00 5.82 0.72 10.10 7.54 Clear None 12:03 8.69 120.00 5.84 0.64 -4.20 8.69 Clear None 12:08 8.72 120.00 5.9 0.57 -14.50 8.08 Clear None 12:13 8.73 120.00 5.96 0.59 -11.40 6.90 Clear None 12:18 8.75 120.00 6.03 0.47 -29.20 7.07 Clear None 12:22 8.76 120.00 6.06 0.48 -29.40 6.35 Clear None 12:28 8.78 120.00 6.1 0.44 -33.50 6.64 Sampling Data Zero HS: Method:Date: Time:12:30 Field Parameters Sample ID: DuplicateID: 0.06 24.75 0.07 24.62 0.07 24.70 0.06 24.84 0.06 24.90 0.06 24.75 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER Justin Hobart WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen Bladen-2S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp.oC 0.06 24.51 Initial Depth to Water (ft.): Temperature (F): 1.974 10-22-2019 Low Flow: Geo Pump Temp.(oC)PFAS24.70 Screen Interval: 10 - 20 6.10pH STABILIZED PARAMETERS 0.07 6.64 Spec. Cond.(mS/cm) Turbidity (NTU) 70.00 250 mL poly NP DO (mg/L) ORP (mV) 0.44 GW4Q19-Bladen-2S WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.05 24.71 Cloudy None Wind (mph)5 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-28-2019 Time:11:24 Water Volume = 10.51 44.68 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 12:00 13.25 400.00 6.22 1.20 54.20 127.00 Cloudy None 12:05 13.91 400.00 5.9 0.70 56.10 153.00 Cloudy None 12:10 14.22 400.00 5.86 0.51 52.60 159.00 Cloudy None 12:15 14.51 400.00 5.89 0.48 44.60 83.30 Cloudy None 12:20 14.63 400.00 5.88 0.54 42.00 62.60 Cloudy None 12:25 14.75 400.00 5.87 0.56 42.60 46.80 Cloudy None 12:30 14.84 400.00 5.86 0.56 41.80 41.00 Cloudy None 12:35 14.90 400.00 5.84 0.53 42.70 46.70 Cloudy None 12:40 14.93 400.00 5.84 0.54 42.60 38.00 Cloudy None 12:45 14.97 400.00 5.83 0.31 41.70 35.60 Cloudy None 12:52 14.99 400.00 5.78 0.30 42.50 30.40 Cloudy None 13:00 15.05 400.00 5.8 0.32 41.50 27.10 Cloudy None 13:05 15.02 400.00 5.82 0.30 39.40 23.50 Cloudy None 13:12 15.26 400.00 5.8 0.29 41.40 23.00 Clear None 13:15 15.23 400.00 5.79 0.30 41.60 24.30 Clear None 13:20 15.28 400.00 5.8 3.05 46.90 24.60 Clear None 13:30 15.11 400.00 5.79 0.86 49.30 18.40 Clear None 13:50 14.85 400.00 6.08 0.39 23.80 21.20 Clear None 13:55 12.67 400.00 5.97 0.26 30.30 21.50 Clear None 13:55 12.98 400.00 5.88 0.30 35.80 35.20 Clear None 14:00 13.68 400.00 5.83 0.46 39.60 36.50 Clear None 14:05 13.30 400.00 5.83 0.27 37.00 26.80 Clear None 14:10 12.71 400.00 5.89 0.20 33.00 26.50 Clear None 14:15 12.51 400.00 5.88 0.19 32.50 21.40 Clear None 14:20 12.44 400.00 5.88 0.19 32.00 20.00 Clear None 14:25 12.40 400.00 5.88 0.19 31.00 15.80 Clear None 14:29 12.34 400.00 5.87 0.20 31.00 15.40 Clear None Sampling Data Zero HS: Method:Date: Time:14:30 Field Parameters 0.08 21.70 0.08 22.00 0.08 22.00 0.08 21.80 0.08 20.90 0.08 21.90 0.08 21.90 Changed flow to 5 secs every 25 secs to reduce draw down 0.10 20.90 Compressor turns off and couldn’t sample last 15 mins. 0.09 21.10 0.08 21.10 0.09 20.50 0.09 20.40 0.08 21.00 0.09 20.60 0.09 20.60 0.08 20.50 0.09 20.70 0.08 20.60 0.09 20.70 0.10 20.70 0.09 20.70 0.09 20.70 0.10 21.20 0.10 20.80 0.10 20.70 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER B.Peach WATER VOLUME CALCULATION Quarterly Tracy Ovbey 37.7 within screen Bladen-3D Project Manager: Depth to Well Bottom (ft.): Dedicated tubing Spec. Cond. mS/cm 9.06Total Volume Purged (gallons): Temp.oC 0.11 21.00 Initial Depth to Water (ft.): 5.467 10-28-2019 Double valve pump Temp.(oC)PFAS21.70 Screen Interval: 33.75 - 43.75 5.87pH STABILIZED PARAMETERS 0.08 15.40 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L)0.20 Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.10 20.90 Sample ID: DuplicateID: Temperature (F):74.00 ORP (mV)31.00 GW4Q19-Bladen-3D WEATHER CONDITIONS Sunny None Wind (mph)2 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-28-2019 Time:11:25 Water Volume = 9.58 14.51 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:45 9.58 180.00 7.94 5.63 61.40 1.14 11:53 9.59 180.00 5.82 5.26 114.70 1.10 11:57 9.58 180.00 5.25 4.69 122.80 1.23 12:00 9.60 180.00 5.31 4.82 121.30 1.03 12:05 9.61 180.00 5.31 4.98 124.40 0.62 Sampling Data Zero HS: Method:Date: Time:12:05Field Parameters Sample ID: DuplicateID: 0.02 25.70 0.03 25.55 0.02 25.07 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER A. Vo WATER VOLUME CALCULATION Quarterly Tracy Ovbey 12 within screen Bladen-3S Project Manager: Depth to Well Bottom (ft.): Peristaltic Pump Spec. Cond. mS/cm 1.03Total Volume Purged (gallons): Temp.oC 0.05 26.53 Initial Depth to Water (ft.): Temperature (F): 0.789 10-28-2019 Low Flow: Geo Pump Temp.(oC)PFAS25.07 Screen Interval: 5 - 15 5.31pH STABILIZED PARAMETERS 0.02 0.62 Spec. Cond.(mS/cm) Turbidity (NTU) 74.00 250 mL poly NP DO (mg/L) ORP (mV) 4.98 124.40 GW4Q19-Bladen-3S WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.03 25.70 Sunny None Wind (mph)2 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-25-2019 Time:11:13 Water Volume = 1.41 51.72 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 12:15 1.62 640.00 6.29 0.03 -69.90 32.00 Clear None 12:20 1.81 640.00 6.27 0.02 -69.10 25.60 Clear None 12:25 1.80 640.00 6.31 0.02 -74.00 19.20 Clear None 12:30 1.82 640.00 6.31 0.02 -75.30 13.90 Clear Nonw 12:35 1.83 640.00 6.31 0.02 -76.30 9.29 Clear None 12:40 1.83 640.00 6.26 0.02 -76.30 5.49 Clear None Sampling Data Zero HS: Method:Date: Time:12:45 Field Parameters a Sample ID: DuplicateID: 0.42 21.91 0.42 22.02 0.42 21.98 0.42 21.80 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER S. Volkoff WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen Bladen-4D Project Manager: Depth to Well Bottom (ft.): Dedicated tubing Spec. Cond. mS/cm 5.11Total Volume Purged (gallons): Temp.oC 0.43 22.15 Initial Depth to Water (ft.): Temperature (F): 8.05 10-25-2019 Double valve pump Temp.(oC)PFAS21.91 Screen Interval: 46.75 - 51.75 6.26pH STABILIZED PARAMETERS 0.42 5.49 Spec. Cond.(mS/cm) Turbidity (NTU) 77.00 250 mL poly NP DO (mg/L) ORP (mV) 0.02 GW4Q19-Bladen-4D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.42 22.13 Sunny None Wind (mph)3 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-22-2019 Time:13:12 Water Volume = 5.74 14.99 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:42 5.74 170.00 5.78 2.85 20.30 32.90 Clear None 13:47 5.75 170.00 5.76 1.60 4.90 28.90 Clear None 13:52 5.75 170.00 5.75 1.04 -7.00 24.60 Clear None 13:57 5.75 170.00 5.74 0.98 -8.30 24.50 Clear None 14:02 5.75 170.00 5.73 0.81 -18.60 23.40 Clear None 14:07 5.75 170.00 5.73 0.82 -24.80 22.20 Clear None 14:12 5.75 170.00 5.74 0.83 -26.30 21.80 Clear None 14:17 5.75 170.00 5.74 0.71 -25.90 21.80 Clear None 14:22 5.75 170.00 5.73 0.64 -30.80 22.20 Clear None 14:27 5.75 170.00 5.72 0.66 -31.50 22.00 Clear None 14:32 5.75 170.00 5.72 0.60 -33.30 22.40 Clear None 14:37 5.75 170.00 5.71 0.65 -34.80 22.40 Clear None 14:42 5.75 170.00 5.72 0.65 -36.70 22.30 Clear None 14:47 5.75 170.00 5.71 0.55 -37.30 22.20 Clear None 14:52 5.75 170.00 5.71 0.55 -38.90 22.50 Clear None 14:57 5.75 170.00 5.71 0.57 -38.80 22.30 Clear None 15:02 5.75 170.00 5.7 0.59 -39.30 21.80 Clear None 15:07 5.75 170.00 5.7 0.57 -39.20 22.20 Clear None 15:12 5.75 170.00 5.71 0.58 -40.10 23.20 Clear None 15:17 5.75 170.00 5.7 0.55 -40.60 22.20 Clear None 15:22 5.75 170.00 5.71 0.55 -40.40 22.30 Clear None 15:27 5.75 170.00 5.71 0.51 -40.20 22.50 Clear None 15:32 5.75 170.00 5.71 0.54 -40.10 22.50 Clear None 15:37 5.75 170.00 5.7 0.58 -41.30 22.80 Clear None 15:42 5.75 170.00 5.69 0.57 -40.10 22.30 Clear None 15:47 5.75 170.00 5.69 0.58 -38.80 22.90 Clear None 15:52 5.75 170.00 5.69 0.56 -38.00 22.60 Clear None 15:57 5.75 170.00 5.69 0.55 -39.80 22.00 Clear None 16:02 5.75 170.00 5.68 0.50 -38.90 22.50 Clear None 16:07 5.75 170.00 5.69 0.61 -38.00 29.30 Clear None 16:12 5.75 170.00 5.69 0.59 -40.30 22.90 Clear None 16:17 5.75 170.00 5.69 0.56 -38.60 22.90 Clear None 16:22 5.75 170.00 5.69 0.57 -39.10 22.90 Clear None 16:27 5.75 170.00 5.68 0.55 -39.80 22.40 Clear None 16:32 5.75 170.00 5.68 0.57 -40.40 22.50 Clear None 16:37 5.75 170.00 5.68 0.56 -41.30 22.30 Clear None 16:42 5.75 170.00 5.68 0.55 -42.40 22.50 Clear None 16:46 5.75 170.00 5.68 0.55 -42.70 22.20 Clear None Comments 0.08 27.35 Initial Depth to Water (ft.): 1.48Low Flow: Geo Pump RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER Justin Hobart WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen Bladen-4S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Temp.oC 0.08 27.29 0.08 27.38 0.07 27.33 0.07 27.37 0.07 27.37 0.07 27.42 0.07 27.52 0.07 27.60 0.07 27.59 0.07 27.49 0.07 27.60 Start pumping 5x well volume, due to high turb but stable parameters 0.07 27.67 0.07 27.65 0.07 27.54 0.07 27.61 0.07 27.52 0.07 27.49 0.07 27.57 0.07 27.52 0.07 27.42 0.07 27.39 0.07 27.29 0.07 27.29 0.07 27.29 0.07 27.29 0.07 27.27 0.07 27.22 0.06 27.21 0.07 27.24 Accidentally hit flow cell, iron precipitate floating around cell 0.07 27.20 0.07 27.19 0.07 27.24 0.07 27.19 0.07 27.20 0.07 27.28 0.07 27.36 0.07 27.26 Purged 5x well volume, sampled Sampling Data Zero HS: Method:Date: Time:16:50 Field Parameters Sample ID: DuplicateID: Cloudy None Wind (mph)6 Precipitation: Sky: SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. DO (mg/L) ORP (mV) 0.55 GW4Q19-Bladen-4S WEATHER CONDITIONS 76.00 250 mL poly NP Temperature (F): 10-22-2019 Temp.(oC)PFAS27.26 Screen Interval: 4.75 - 14.75 5.68pH STABILIZED PARAMETERS 0.07 22.20 Spec. Cond.(mS/cm) Turbidity (NTU) Total Volume Purged (gallons): Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-24-2019 Time:09:20 Water Volume = 7.28 50.36 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 10:10 7.68 480.00 5.29 1.18 -39.90 297.00 Cloudy Yes 10:15 7.45 480.00 5.28 0.88 -95.50 117.00 Cloudy Yes 10:20 7.51 480.00 5.3 0.68 -119.40 73.50 Cloudy Yes 10:25 7.45 480.00 5.31 0.59 -132.90 44.50 Cloudy Yes 10:30 7.45 480.00 5.3 0.47 -137.90 39.80 Cloudy Yes 10:35 7.50 480.00 5.27 0.38 -142.60 30.20 Cloudy Yes 10:40 7.47 480.00 5.26 0.37 -144.10 20.50 Cloudy Yes 10:45 7.48 480.00 5.22 0.35 -136.90 16.30 Clear Yes 10:50 7.48 480.00 5.15 0.34 -128.60 14.10 Clear Yes Sampling Data Zero HS: Method:Date: Time:10:55Field Parameters Sample ID: DuplicateID: 0.13 20.90 Sulfur smell 0.13 20.73 0.13 20.76 0.13 20.78 0.13 20.59 0.13 20.66 Sulfur smell 0.13 20.71 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER Mike Wang WATER VOLUME CALCULATION Quarterly Tracy Ovbey 45 within screen Cumberland-1D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 5.9Total Volume Purged (gallons): Temp.oC 0.13 20.40 Initial Depth to Water (ft.): Temperature (F): 6.893 10-24-2019 Double valve pump Temp.(oC)PFAS20.90 Screen Interval: 40 - 50 5.15pH STABILIZED PARAMETERS 0.13 14.10 Spec. Cond.(mS/cm) Turbidity (NTU) 51.00 250 mL poly NP DO (mg/L) ORP (mV) 0.34 -128.60 GW4Q19-Cumberland-1D WEATHER CONDITIONS GW4Q19-Cumberland-1D-D Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.12 20.63 Sunny None Wind (mph)5 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-24-2019 Time:09:23 Water Volume = 7.12 25.2 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 09:45 7.20 175.00 0.23 4.91 5.67 281.30 1.50 Clear No 09:50 7.20 175.00 0.23 4.73 6.86 293.60 1.10 Clear No 09:55 7.21 175.00 0.23 4.63 6.34 304.60 0.92 Clear No 10:00 7.21 175.00 0.23 4.61 6.15 313.40 0.86 Clear No 10:05 7.22 175.00 0.23 4.59 6.20 323.20 1.00 Clear No Sampling Data Zero HS: Method:Date: Time:10:08 Field Parameters Sample ID: DuplicateID: Sunny None Wind (mph) Precipitation: Sky: Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.11 23.10 DO (mg/L) ORP (mV) 6.20 323.20 GW4Q19-Cumberland-1S WEATHER CONDITIONS 250 mL poly NP Initial Depth to Water (ft.): Temperature (F): 2.893 10-24-2019 Peristaltic Pump Temp.(oC)PFAS23.20 Screen Interval: 15 - 25 4.59pH STABILIZED PARAMETERS 0.11 1.00 Spec. Cond.(mS/cm) Turbidity (NTU) RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey 20 within screen Cumberland-1S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 1.31Total Volume Purged (gallons): Temp. oC 0.11 22.90 0.11 23.10 0.11 23.10 0.11 23.20 Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-25-2019 Time:09:21 Water Volume = 5.32 57.55 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 10:00 5.35 150.00 0.20 6.64 0.44 -108.00 136.00 Cloudy Sulfuric 10:05 5.31 150.00 0.20 6.7 0.27 -132.60 117.00 Semi cloudy Sulfuric 10:10 5.35 150.00 0.20 6.73 0.29 -149.30 107.00 Slightly cloudy Sulfuric 10:15 5.35 150.00 0.20 6.76 0.22 -162.40 98.10 Slightly cloudy Sulfuric 10:20 5.31 150.00 0.20 6.78 0.32 -177.90 94.60 Slightly cloudy Sulfuric 10:25 5.32 150.00 0.20 6.77 0.34 -183.60 83.60 Slightly cloudy Sulfuric 10:30 5.32 150.00 0.20 6.78 0.27 -192.40 79.10 Clear Sulfuric 10:35 5.32 150.00 0.20 6.77 0.19 -199.30 70.80 Clear Sulfuric 10:40 5.32 150.00 0.20 6.72 0.21 -209.60 68.60 Clear Sulfuric 10:45 5.32 150.00 0.20 6.74 0.19 -231.50 65.00 Clear Sulfuric 10:50 5.32 150.00 0.20 6.78 0.16 -251.70 64.70 Clear Sulfuric 10:55 5.33 150.00 0.20 6.8 0.21 -274.80 62.60 Semi cloudy No odor 11:00 5.32 150.00 0.20 6.8 0.18 -305.90 66.30 Clear Sulfuric 11:05 5.33 150.00 0.20 6.82 0.16 -335.80 57.40 Clear Sulfuric 11:10 5.35 150.00 0.20 6.8 0.19 -370.40 52.10 Clear No 11:15 5.33 150.00 0.20 6.79 0.16 -380.80 48.20 Clear No 11:20 5.33 150.00 0.20 6.79 0.15 -410.20 42.60 Clear No 11:25 5.35 150.00 0.20 6.81 0.12 -420.30 41.30 Clear No 11:30 5.33 150.00 0.20 6.79 0.13 -423.10 37.00 Clear No 11:35 5.33 150.00 0.20 6.78 0.13 -421.60 41.20 Clear No 11:40 5.34 150.00 0.20 6.75 0.13 -440.90 35.60 Clear No 11:45 5.35 150.00 0.20 6.79 0.10 -479.90 32.90 Clear No 11:50 5.33 150.00 0.20 6.81 0.07 -477.30 29.70 Clear No 11:55 5.35 150.00 0.20 6.76 0.09 -490.20 24.40 Clear No 12:00 5.33 150.00 0.20 6.87 0.09 -490.30 19.80 Clear No 12:05 5.32 150.00 0.20 6.85 0.09 -484.90 18.20 Clear No 12:10 5.33 150.00 0.20 6.8 0.09 -485.30 19.90 Clear No Sampling Data Zero HS: Method:Date: Time:12:25Field Parameters a Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.10 21.00 DO (mg/L) ORP (mV) 0.09 250 mL poly NP Initial Depth to Water (ft.): 8.357 10-25-2019 Double valve pump Temp.(oC)PFAS21.60 Screen Interval: 47 - 57 6.80pH STABILIZED PARAMETERS 0.08 19.90 Spec. Cond.(mS/cm) Turbidity (NTU) RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey 52 within screen Cumberland-2D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 5.15Total Volume Purged (gallons): Temp. oC 0.10 20.80 0.10 21.00 0.10 21.10 0.10 21.30 0.09 21.90 0.09 20.80 0.09 20.70 0.09 20.70 0.09 21.00 0.09 21.20 0.09 21.20 0.09 21.30 0.08 21.20 0.08 20.90 0.08 20.80 0.08 21.30 0.08 21.10 0.08 21.50 0.08 22.10 0.08 21.20 0.08 22.00 0.08 21.90 0.08 21.60 0.08 21.90 0.08 21.20 0.08 21.50 Sample ID: DuplicateID: Sunny None Wind (mph) Precipitation: Sky: GW4Q19-Cumberland-2D WEATHER CONDITIONS Temperature (F): Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-23-2019 Time:11:15 Water Volume = 5.2 16.75 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:35 5.20 165.00 0.22 5.52 4.26 193.80 1.57 Clear No 11:40 5.20 165.00 0.22 5.28 4.60 196.30 1.16 Clear No 11:45 5.20 165.00 0.22 5.16 3.79 205.10 2.34 Clear No 11:50 5.19 165.00 0.22 5.08 3.83 212.10 1.46 Clear No 11:55 5.19 165.00 0.22 5.08 3.64 218.10 1.18 Clear No Sampling Data Zero HS: Method:Date: Time:12:00 Field Parameters Sample ID: DuplicateID: 0.07 23.00 0.07 23.10 0.07 23.10 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey 12 within screen Cumberland-2S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 1.1Total Volume Purged (gallons): Temp. oC 0.06 23.00 Initial Depth to Water (ft.): Temperature (F): 1.848 10-23-2019 Peristaltic Pump Temp.(oC)PFAS23.10 Screen Interval: 7 - 17 5.08pH STABILIZED PARAMETERS 0.07 1.18 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 3.64 218.10 GW4Q19-Cumberland-2S WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.07 23.10 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-23-2019 Time:09:54 Water Volume = 8.09 27.06 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 10:05 8.10 175.00 0.23 8.04 4.39 -197.80 10.60 Clear No 10:10 8.10 175.00 0.23 7.85 1.75 -207.80 9.74 Clear No 10:15 8.10 175.00 0.23 7.76 1.30 -215.10 8.85 Clear No 10:20 8.10 175.00 0.23 7.7 1.26 -219.70 7.16 Clear No 10:25 8.10 175.00 0.23 7.66 1.14 -223.50 5.34 Clear No 10:30 8.10 175.00 0.23 7.62 1.12 -224.60 4.95 Clear No 10:35 8.10 175.00 0.23 7.6 1.08 -226.00 3.77 Clear No Sampling Data Zero HS: Method:Date: Time:10:37 Field Parameters Sample ID: DuplicateID: 0.23 21.00 0.23 21.00 0.23 21.00 0.23 21.00 0.23 21.00 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey 24.5 within screen Cumberland-3D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 1.61Total Volume Purged (gallons): Temp. oC 0.23 21.10 Initial Depth to Water (ft.): Temperature (F): 3.035 10-23-2019 Peristaltic Pump Temp.(oC)PFAS21.00 Screen Interval: 22 - 27 7.60pH STABILIZED PARAMETERS 0.23 3.77 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 1.08 GW4Q19-Cumberland-3D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.23 21.00 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-22-2019 Time:14:52 Water Volume = 8.54 14.18 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 15:05 8.55 175.00 0.23 6.32 1.83 -51.70 10.30 Clear No 15:10 8.55 175.00 0.23 6.32 1.65 -51.80 10.50 Clear No 15:15 8.56 175.00 0.23 6.32 1.41 -53.70 12.30 Clear No 15:20 8.55 175.00 0.23 6.23 2.12 -41.70 10.20 Clear No 15:25 8.55 175.00 0.23 6.28 2.60 -40.70 9.48 Clear No 15:30 8.55 175.00 0.23 6.34 2.41 -48.60 9.08 Clear No 15:35 8.55 175.00 0.23 6.39 2.18 -54.80 8.68 Clear No 15:40 8.55 175.00 0.23 6.43 2.12 -58.30 9.05 Clear No 15:45 8.55 175.00 0.23 6.43 1.96 -60.60 9.06 Clear No 15:50 8.60 175.00 0.23 6.44 1.93 -61.50 8.75 Clear No Sampling Data Zero HS: Method:Date: Time:15:51 Field Parameters Sample ID: DuplicateID: 0.18 24.30 0.18 24.10 0.18 24.40 0.18 24.40 0.17 24.30 0.08 24.30 0.13 24.20 0.18 24.20 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey 11.5 within screen Cumberland-3S Project Manager: Depth to Well Bottom (ft.): Peristaltic Pump Spec. Cond. mS/cm 2.66Total Volume Purged (gallons): Temp. oC 0.08 24.20 Initial Depth to Water (ft.): Temperature (F): 0.902 10-22-2019 Peristaltic Pump Temp.(oC)PFAS24.10 Screen Interval: 9 - 14 6.44pH STABILIZED PARAMETERS 0.18 8.75 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 1.93 GW4Q19-Cumberland-3S WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.08 24.30 Partly Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-24-2019 Time:13:09 Water Volume = 13.95 68.45 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:50 14.00 225.00 0.30 5.4 1.54 107.30 114.00 Slightly cloudy No 13:55 13.99 225.00 0.30 5.43 1.22 98.50 138.00 Slightly cloudy No 14:00 14.00 225.00 0.30 5.41 1.17 94.70 121.00 Slightly cloudy No 14:05 14.00 225.00 0.30 5.41 1.16 91.70 89.50 Slightly cloudy No 14:10 14.00 225.00 0.30 5.41 1.18 89.90 87.30 Clear No 14:15 14.00 225.00 0.30 5.39 1.00 87.70 89.80 Clear No 14:20 14.00 225.00 0.30 5.35 0.92 87.00 78.90 Clear No 14:25 14.00 225.00 0.30 5.35 0.78 85.20 70.20 Clear No 14:30 14.00 225.00 0.30 5.34 0.67 83.80 64.30 Clear No 14:35 14.00 225.00 0.30 5.34 0.56 81.70 53.80 Clear No 14:40 14.00 225.00 0.30 5.36 0.50 79.50 55.90 Clear No 14:45 14.00 225.00 0.30 5.37 0.48 77.23 45.60 Clear No 14:50 14.00 225.00 0.30 5.37 0.42 76.80 38.60 Clear No 14:55 14.00 225.00 0.30 5.36 0.41 77.00 34.80 Clear No 15:00 14.00 225.00 0.30 5.34 0.39 77.30 29.80 Clear No 15:05 14.00 225.00 0.30 5.32 0.37 77.80 31.60 Clear No 15:10 14.00 225.00 0.30 5.32 0.36 77.10 24.60 Clear No 15:15 14.00 225.00 0.30 5.32 0.34 76.70 19.80 Clear No 15:20 14.00 225.00 0.30 5.38 0.35 71.90 19.60 Clear No 15:25 14.00 225.00 0.30 5.38 0.34 71.10 17.90 Clear No Sampling Data Zero HS: Method:Date: Time:14:25 Field Parameters Sample ID: DuplicateID: 0.04 22.80 0.04 22.90 0.04 22.80 0.04 22.30 0.04 22.30 0.04 22.40 0.04 22.80 0.04 22.60 0.04 22.50 0.04 22.50 0.04 22.80 0.04 22.70 0.04 22.60 0.04 22.60 0.04 22.50 0.04 23.00 0.04 23.00 0.04 23.00 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen Cumberland-4D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 6Total Volume Purged (gallons): Temp. oC 0.04 23.10 Initial Depth to Water (ft.): Temperature (F): 8.72 10-24-2019 Double valve pump Temp.(oC)PFAS22.80 Screen Interval: 57 - 67 5.38pH STABILIZED PARAMETERS 0.04 17.90 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 0.34 71.10 GW4Q19-Cumberland-4D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.04 23.10 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-25-2019 Time:13:14 Water Volume = 7.7 20.9 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:35 7.85 200.00 0.27 4.04 0.54 187.90 11.50 Orange No 13:40 7.85 200.00 0.27 4.02 0.45 183.20 9.84 Oramge No 13:45 7.86 200.00 0.27 4.05 0.42 178.50 10.00 Orange No 13:50 7.86 200.00 0.27 4.05 0.41 175.80 9.59 Orange No 13:55 7.87 200.00 0.27 4.08 0.41 173.80 10.20 Orange No Sampling Data Zero HS: Method:Date: Time:13:57 Field Parameters a Sample ID: DuplicateID: 0.05 26.50 0.05 26.50 0.05 26.50 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen Cumberland-4S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 1.62Total Volume Purged (gallons): Temp. oC 0.05 26.50 Initial Depth to Water (ft.): Temperature (F): 2.112 10-25-2019 Peristaltic Pump Temp.(oC)PFAS26.50 Screen Interval: 10 - 20 4.08pH STABILIZED PARAMETERS 0.05 10.20 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 0.41 173.80 GW4Q19-Cumberland-4S WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.05 26.50 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-23-2019 Time:13:15 Water Volume = 4.46 23.45 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:30 4.45 175.00 0.23 5.4 1.95 73.10 5.78 Clear Sulfuric 13:35 4.49 175.00 0.23 5.4 1.61 62.90 6.30 Clear Sulfuric 13:41 4.48 175.00 0.23 5.44 1.46 52.60 5.54 Clear Sulfuric 13:45 4.48 175.00 0.23 5.46 1.41 45.00 5.95 Clear Sulfuric 13:50 4.47 175.00 0.23 5.48 1.36 38.30 5.83 Clear No 13:55 4.48 175.00 0.23 5.48 1.36 34.30 5.49 Clear No 14:00 4.48 175.00 2.30 5.5 1.36 30.80 4.96 Clear No 14:05 4.48 175.00 2.30 5.4 1.37 27.80 5.02 Clear Sulfuric 14:10 4.48 175.00 0.23 5.51 1.53 24.90 6.77 Clear Sulfuric 14:15 4.49 175.00 0.23 5.46 1.48 24.40 6.80 Clear No 14:20 4.48 175.00 0.23 5.48 1.42 21.50 4.96 Clear No 14:25 4.48 175.00 0.23 5.47 1.36 21.50 5.16 Clear No 14:30 4.48 175.00 0.23 5.47 1.33 20.20 4.82 Clear No Sampling Data Zero HS: Method:Date: Time:14:32Field Parameters Sample ID: DuplicateID: Sunny None Wind (mph) Precipitation: Sky: Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.13 23.90 DO (mg/L) ORP (mV) 1.33 20.20 GW4Q19-Cumberland-5S WEATHER CONDITIONS 250 mL poly NP Initial Depth to Water (ft.): Temperature (F): 3.038 10-23-2019 Peristaltic Pump Temp.(oC)PFAS23.50 Screen Interval: 14 - 24 5.47pH STABILIZED PARAMETERS 0.12 4.82 Spec. Cond.(mS/cm) Turbidity (NTU) RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey 19 within screen Cumberland-5S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 3.45Total Volume Purged (gallons): Temp. oC 0.14 24.00 0.13 23.80 0.13 23.80 0.13 23.80 0.13 23.70 0.13 23.70 0.13 23.70 0.13 23.60 0.12 23.50 0.13 23.70 0.13 23.50 0.13 23.70 Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-29-2019 Time:11:16 Water Volume = 19.63 31.78 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:37 19.70 300.00 3.36 32.98 198.80 85.10 Cloudy None 11:42 19.71 300.00 3.38 2.22 223.50 88.50 Clear No 11:47 19.72 300.00 3.41 1.25 244.40 16.60 Clear No 11:51 19.73 300.00 3.41 0.83 256.70 9.04 Clear No 11:54 19.73 300.00 3.42 0.64 272.60 7.27 Clear No 12:00 19.73 300.00 3.42 0.65 279.00 18.20 Clear No 12:06 19.73 300.00 3.42 0.63 287.30 5.98 Clear No Sampling Data Zero HS: Method:Date: Time:12:10 Field Parameters Sample ID: DuplicateID: 0.17 18.20 0.17 18.27 0.17 18.20 0.17 18.22 0.17 18.19 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PIW-1D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.16 18.63 Initial Depth to Water (ft.): Temperature (F): 1.944 10-29-2019 Peristaltic Pump Temp.(oC)PFAS18.27 Screen Interval: 24.5 to 29.5 3.42pH STABILIZED PARAMETERS 0.17 5.98 Spec. Cond.(mS/cm) Turbidity (NTU) 66.00 250 mL poly NP DO (mg/L) ORP (mV) 0.63 287.30 GW4Q19-PIW-1D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.17 18.25 Cloudy None Wind (mph)8 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-29-2019 Time:13:28 Water Volume = 22 22 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:30 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey PIW-1S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC Initial Depth to Water (ft.): Temperature (F): 0 Temp.(oC)PFAS Screen Interval: 7.8 - 17.8 pH STABILIZED PARAMETERS Spec. Cond.(mS/cm) Turbidity (NTU) 68.00 250 mL poly NP DO (mg/L) ORP (mV) GW4Q19-PIW-1S WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Completely dry. Cloudy Rain Wind (mph)4 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-01-2019 Time:09:43 Water Volume = 36.8 53 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min. gal.mg/L mV NTU 10:15 37.80 150.00 6.27 2.84 67.50 104.00 Cloudy None 10:20 37.81 150.00 6.17 1.52 66.30 101.00 Cloudy 10:25 37.87 150.00 6.04 1.48 66.80 99.00 Cloudy 10:30 38.02 150.00 6 0.58 59.40 68.10 Cloudy 10:35 37.90 150.00 5.99 0.56 56.20 53.60 Cloudy 10:40 37.87 150.00 5.89 0.50 55.60 37.80 Cloudy 10:45 38.05 150.00 5.88 0.51 49.70 24.20 Clear 10:50 37.85 150.00 5.89 0.49 49.10 22.50 Clear 10:55 37.95 150.00 1.50 5.87 0.48 47.80 20.50 Clear 11:00 38.15 150.00 5.84 0.40 45.70 17.50 Clear 11:05 38.00 150.00 5.82 0.40 46.60 17.20 Clear 11:11 38.10 150.00 1.75 5.82 0.43 45.10 16.20 Clear None Sampling Data Zero HS: Method:Date: Time:11:15 Field Parameters Sample ID: DuplicateID: 0.07 16.50 0.07 16.10 0.07 16.40 0.07 16.14 0.07 15.76 0.07 16.09 0.07 15.74 0.08 15.65 0.08 16.06 0.07 15.46 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen PIW-2D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 1.75Total Volume Purged (gallons): Temp. oC 0.08 15.94 Initial Depth to Water (ft.): Temperature (F): 2.592 11-01-2019 Double valve pump Temp.(oC)PFAS16.50 Screen Interval: 40 - 50 5.82pH STABILIZED PARAMETERS 0.07 16.20 Spec. Cond.(mS/cm) Turbidity (NTU) 47.00 250 mL poly NP DO (mg/L) ORP (mV) 0.43 45.10 GW4Q19-PIW-2D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.08 15.76 Sunny None Wind (mph)11 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-28-2019 Time:16:09 Water Volume = 17.6 26.86 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 16:07 18.00 250.00 4.2 2.77 53.90 105.00 Cloudy None 16:12 18.10 250.00 3.83 1.20 47.50 17.40 Clear None 16:17 18.12 250.00 3.8 1.00 -68.40 13.40 Clear No 16:22 18.15 250.00 3.82 0.83 -75.50 10.70 Clear None 16:27 18.16 250.00 3.9 0.82 -85.70 7.97 Clear None 16:32 18.15 250.00 3.99 0.76 -90.80 8.72 Clearr None Sampling Data Zero HS: Method:Date: Time:16:35 Field Parameters Sample ID: DuplicateID: 0.10 18.37 0.10 18.61 0.10 18.60 0.10 18.43 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PIW-3D Project Manager: Depth to Well Bottom (ft.): Peristaltic Pump Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.10 18.93 Initial Depth to Water (ft.): Temperature (F): 1.482 10-28-2019 Peristaltic Pump Temp.(oC)PFAS18.37 Screen Interval: 19 - 24 3.99pH STABILIZED PARAMETERS 0.10 8.72 Spec. Cond.(mS/cm) Turbidity (NTU) 81.00 250 mL poly NP DO (mg/L) ORP (mV) 0.76 GW4Q19-PIW-3D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.10 18.80 Sunny None Wind (mph)9 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-30-2019 Time:15:13 Water Volume = 11.25 41.77 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 18:00 11.29 250.00 5.74 0.75 28.60 74.40 Clear None 16:05 11.30 250.00 5.84 0.51 20.50 66.50 Clear None 16:10 11.29 250.00 5.85 0.43 17.10 66.10 Clear None Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: 0.06 28.25 Last reading for the day. Left tubing in well and will restart tomorrow. RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen PIW-4D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.06 18.31 Initial Depth to Water (ft.): Temperature (F): 4.883Double valve pump Temp.(oC)PFAS28.25 Screen Interval: 32.3 - 37.3 5.85pH STABILIZED PARAMETERS 0.06 66.10 Spec. Cond.(mS/cm) Turbidity (NTU) 77.00 250 mL poly NP DO (mg/L) ORP (mV) 0.43 17.10 GW4Q19-PIW-4D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.06 28.41 Cloudy None Wind (mph)3 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-31-2019 Time:10:51 Water Volume = 11.29 41.77 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 10:50 11.29 280.00 7.65 2.35 87.50 52.50 Clear None 10:55 11.29 280.00 7.14 1.35 84.00 34.50 Clear None 11:00 11.25 280.00 6.99 0.84 64.70 46.80 Clear None 11:05 11.25 280.00 7.18 0.72 44.60 57.50 Clear none 11:10 11.25 280.00 7.35 0.60 28.30 59.60 Cloudy None 11:15 11.25 280.00 7.39 0.58 26.30 62.00 Clear None 11:20 11.25 280.00 7.39 0.59 26.00 62.80 Clear None 11:25 11.25 280.00 7.38 0.61 26.30 63.70 Clear None 11:35 11.25 280.00 7.09 1.69 46.20 65.40 Clear None 11:40 11.25 280.00 7.46 0.22 22.00 83.90 Clear None 11:45 11.25 280.00 7.51 0.27 20.60 80.30 Cloudy None 11:50 11.25 280.00 7.51 0.29 19.80 78.20 Cloudy None 11:55 11.25 280.00 7.52 0.25 18.30 81.80 Cloudy None 11:59 11.25 280.00 7.5 0.20 19.00 82.60 Cloudy None 12:05 11.25 280.00 6.97 0.89 52.90 86.80 Cloudy None 12:10 11.25 280.00 7.12 1.11 45.60 90.70 Cloudy None 12:15 11.25 280.00 7.26 2.05 40.90 93.40 Cloudy None 12:20 11.26 280.00 7.29 2.14 37.10 93.60 Cloudy None 12:25 11.26 280.00 7.37 0.47 34.40 96.20 Cloudy None 12:30 11.27 280.00 7.45 3.38 33.30 96.70 Cloudy None 12:35 11.29 280.00 7.38 2.47 36.60 96.10 Cloudy None 12:40 11.29 280.00 7.36 3.09 37.70 97.20 Cloudy None 12:45 11.29 280.00 7.4 1.32 36.60 87.60 Cloudy None 12:50 11.29 280.00 7.45 2.80 36.70 87.20 Cloudy None 12:55 11.29 280.00 7.43 1.37 36.60 78.10 Cloudy None 13:00 11.29 280.00 7.38 3.29 41.20 71.20 Cloudy Yes, methane 13:05 11.30 280.00 7.39 1.50 37.70 69.80 Cloudy Yes, methane 13:10 11.29 280.00 7.47 2.26 36.00 71.90 Cloudy Yes, methane 13:15 11.29 280.00 7.5 1.57 34.30 59.20 Cloudy Yes, methane 13:20 11.29 280.00 7.5 0.60 32.10 60.50 Cloudy Yes, methane Sampling Data Zero HS: Method:Date: Time:13:25 Field Parameters 0.06 19.68 0.05 17.69 0.05 19.09 0.05 19.63 0.05 17.75 0.05 17.70 0.05 17.59 0.05 17.58 0.05 17.58 0.05 17.57 0.05 17.70 0.05 17.59 0.05 17.64 0.05 17.62 0.05 17.64 0.05 17.59 0.06 20.15 0.06 20.67 0.06 0.72 0.06 17.72 55.60 19.53 0.06 19.77 0.06 18.75 0.06 18.69 0.05 18.62 0.06 18.70 0.06 18.59 0.06 18.82 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen PIW-4D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.06 18.87 Initial Depth to Water (ft.): 4.877 10-31-2019 Double valve pump Temp.(oC)PFAS19.68 Screen Interval: 32.3 - 37.3 7.50pH STABILIZED PARAMETERS 0.06 60.50 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.06 18.86 Sample ID: DuplicateID: Temperature (F):79.00 DO (mg/L) ORP (mV) 0.60 32.10 GW4Q19-PIW-4D WEATHER CONDITIONS GW4Q19-PIW-4D-D Partly Sunny None Wind (mph)12 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-30-2019 Time:10:23 Water Volume = 5.87 38.1 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 10:50 5.90 4.29 1.26 87.70 5.29 Clear None 10:55 5.90 4.17 0.83 99.40 2.68 Clear None 11:00 5.90 4.12 0.55 105.30 2.03 Clear None 10:05 5.90 4.11 0.45 105.90 1.71 Clear None 11:10 5.90 4.12 0.45 106.70 1.25 Clear None 11:15 5.90 4.11 0.39 106.80 0.96 Clear None 11:20 5.90 4.12 0.38 106.60 0.92 Clear None 11:25 5.90 4.1 0.34 106.40 0.72 Clear None 11:30 5.90 4.13 0.29 104.60 0.86 Clear None 11:35 5.90 4.11 0.30 105.10 0.89 Clear None 11:40 5.90 4.3 0.29 102.10 0.71 Clear None Sampling Data Zero HS: Method:Date: Time:11:15Field Parameters Sample ID: DuplicateID: 0.09 18.60 0.09 18.34 0.09 18.50 0.09 18.38 0.09 18.45 0.09 18.50 0.09 18.54 0.09 18.64 0.09 18.49 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey PIW-7D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.09 18.88 Initial Depth to Water (ft.): Temperature (F): 5.157 10-30-2019 Temp.(oC)PFAS18.50 Screen Interval: 29 - 34 4.30pH STABILIZED PARAMETERS 0.09 0.71 Spec. Cond.(mS/cm) Turbidity (NTU) 70.00 250 mL poly NP DO (mg/L) ORP (mV) 0.29 102.10 GW4Q19-PIW-7D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.09 19.08 Cloudy None Wind (mph)10 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-30-2019 Time:12:30 Water Volume = 7.3 42 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 12:45 7.39 250.00 3.85 1.74 155.50 25.50 Clear None 12:50 7.39 250.00 3.93 1.42 154.50 12.80 Clear None 12:55 7.37 250.00 3.97 0.76 157.40 7.71 Clear None 12:59 7.37 250.00 3.98 0.71 162.60 4.45 Clear None 13:06 7.39 250.00 3.97 1.19 170.20 2.23 Clear None 13:10 7.39 250.00 3.98 0.70 173.80 1.94 Clear None 13:15 7.39 250.00 3.98 0.61 179.10 1.46 Clear None 13:20 7.39 250.00 3.98 0.60 182.40 1.81 Clear None 13:25 7.39 250.00 3.98 0.65 185.40 1.02 Clear None Sampling Data Zero HS: Method:Date: Time:13:30 Field Parameters Sample ID: DuplicateID: 0.20 18.39 0.20 18.37 0.20 18.33 0.20 18.29 0.20 18.31 0.20 18.24 0.20 18.38 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen PIW-8D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.20 18.44 Initial Depth to Water (ft.): Temperature (F): 5.552 10-30-2019 Double valve pump Temp.(oC)PFAS18.39 Screen Interval: 35.5 - 45.5 3.98pH STABILIZED PARAMETERS 0.20 1.02 Spec. Cond.(mS/cm) Turbidity (NTU) 72.00 250 mL poly NP DO (mg/L) ORP (mV) 0.65 185.40 GW4Q19-PIW-8D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.20 18.40 Cloudy Rain Wind (mph)5 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-23-2019 Time:09:55 Water Volume = 37.34 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 10:30 37.51 310.00 10.02 3.54 -2.00 0.00 Clear No 10:35 37.51 310.00 7.65 0.00 7.00 0.00 Clear No 10:40 37.42 310.00 5.85 0.00 83.00 0.00 Clear No 10:45 37.50 310.00 5.33 0.00 112.00 0.00 Clear No 10:50 37.50 310.00 5.11 0.00 128.00 0.00 Clear No 10:55 37.50 310.00 5.03 0.00 136.00 0.00 Clear No 11:00 37.50 310.00 4.96 0.00 147.00 0.00 Clear No 11:05 37.50 310.00 4.8 0.00 160.00 0.00 Clear No 11:10 37.50 310.00 4.75 0.00 167.00 0.00 Clear No 11:15 37.50 310.00 4.71 0.00 171.00 0.00 Clear No Sampling Data Zero HS: Method:Date: Time:11:20 Field Parameters Sample ID: DuplicateID: 0.15 17.39 0.14 17.40 0.15 17.33 0.15 17.32 0.15 17.35 0.18 17.27 0.16 17.28 0.16 17.30 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 CHARLES PACE WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen PIW-9D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.33 17.32 Initial Depth to Water (ft.): Temperature (F): -5.974 10-23-2019 Double valve pump Temp.(oC)PFAS17.40 Screen Interval: 40 - 45 4.71pH STABILIZED PARAMETERS 0.14Spec. Cond.(mS/cm) Turbidity (NTU) 60.00 250 mL poly NP DO (mg/L) ORP (mV)171.00 GW4Q19-PIW-9D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.21 17.33 Sunny None Wind (mph)8 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-23-2019 Time:09:56 Water Volume = 30.43 33.11 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:10 30.62 200.00 4.52 1.70 173.50 33.10 Clear None 11:15 30.65 200.00 4.2 1.10 114.00 25.70 Clear None 11:20 30.66 200.00 3.98 0.87 86.80 13.10 Clear None 11:25 30.66 200.00 3.96 0.79 65.60 6.70 Clear None 11:30 30.66 200.00 3.97 0.79 49.80 11:35 30.72 200.00 3.99 0.54 41.60 11:40 30.71 200.00 3.99 0.48 32.60 3.73 Clear None 11:45 30.71 200.00 3.98 0.47 29.00 2.42 Clear None 11:50 30.71 200.00 3.98 0.46 26.30 2.08 Clear None 11:55 30.71 200.00 3.98 0.43 22.60 1.61 Clear None 12:00 30.70 200.00 4 0.41 17.10 2.00 Clear None 12:05 30.70 200.00 3.98 0.35 16.90 1.42 Clear None 12:10 30.70 200.00 3.99 0.39 15.40 1.44 Clear None 12:15 30.69 200.00 3.99 0.35 14.30 1.23 Clear None 12:20 30.69 200.00 4.02 0.42 13.10 1.27 Clear None 12:25 30.60 200.00 4.04 0.33 11.01 1.20 Clear None 12:30 30.69 200.00 4.04 0.32 11.50 1.39 Clear None 12:35 30.69 200.00 4.04 0.33 10.90 1.25 Clear None Sampling Data Zero HS: Method:Date: Time:12:40 Field Parameters Sample ID: DuplicateID: 0.11 17.90 0.11 18.01 0.11 17.96 0.11 17.98 0.11 17.90 0.11 17.94 0.11 17.97 0.11 17.77 0.11 17.82 0.11 17.87 0.11 17.77 No turbidity taken 0.11 17.78 0.11 17.79 0.11 17.78 0.11 17.68 0.11 17.67 No turbidity taken RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER Charles Pace WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen PIW-9S Project Manager: Depth to Well Bottom (ft.): Peristaltic Pump Spec. Cond. mS/cm 4.49Total Volume Purged (gallons): Temp.oC 0.11 18.04 Initial Depth to Water (ft.): Temperature (F): 0.429 10-23-2019 Low Flow: Geo Pump Temp.(oC)PFAS17.90 Screen Interval: 24.8 - 29.8 4.04pH STABILIZED PARAMETERS 0.11 1.25 Spec. Cond.(mS/cm) Turbidity (NTU) 61.00 250 mL poly NP DO (mg/L) ORP (mV) 0.33 10.90 GW4Q19-PIW-9S WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.11 17.87 Sunny None Wind (mph)5 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-30-2019 Time:15:10 Water Volume = 14.68 61.95 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 15:15 14.68 200.00 0.27 5.67 0.51 -2.20 56.80 Clear No odor 15:20 14.70 200.00 0.27 5.54 0.36 7.90 36.80 Clear No odor 15:25 14.70 200.00 0.27 5.49 0.41 15.30 18.90 Clear No odor 15:30 14.70 200.00 0.27 5.49 0.39 16.30 14.90 Clear No odor 15:35 14.69 200.00 0.27 5.48 0.28 15.60 11.70 Clear No odor 15:40 14.68 200.00 0.27 5.48 0.26 16.40 8.77 Clear No odor 15:45 14.68 200.00 0.27 5.47 0.25 15.80 8.01 Clear No odor 15:50 14.68 200.00 0.27 5.46 0.24 16.60 6.91 Clear No odor Sampling Data Zero HS: Method:Date: Time:15:50 Field Parameters Sample ID: DuplicateID: 0.17 19.45 0.17 19.42 0.17 19.29 0.17 19.22 0.17 19.30 0.17 19.23 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey 55.5 within screen PIW-10DR Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 2.13Total Volume Purged (gallons): Temp. oC 0.18 19.45 Initial Depth to Water (ft.): Temperature (F): 7.563 10-30-2019 Double valve pump Temp.(oC)PFAS19.29 Screen Interval: 53 - 58 5.46pH STABILIZED PARAMETERS 0.17 6.91 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 0.24 16.60 GW4Q19-PIW-10DR WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.17 19.48 Partly Cloudy None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-29-2019 Time:14:13 Water Volume = 18.9 20.19 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 14:40 19.30 250.00 3.96 14.06 186.90 61.40 Cloudy None 14:45 19.25 250.00 3.97 7.06 189.70 15.30 Clear None 14:52 19.25 250.00 3.98 4.61 195.20 5.42 Clear None 14:57 19.25 250.00 3.99 3.76 198.70 2.60 Clear None 15:02 19.25 250.00 3.98 3.75 202.10 1.58 Clear None 15:07 19.25 250.00 3.99 3.80 204.80 1.12 Clear None Sampling Data Zero HS: Method:Date: Time:15:10 Field Parameters Sample ID: DuplicateID: 0.05 19.20 0.05 19.22 0.05 19.19 0.05 19.23 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 LUKE TART WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PIW-10S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.05 19.20 Initial Depth to Water (ft.): Temperature (F): 0.206 10-29-2019 Peristaltic Pump Temp.(oC)PFAS19.20 Screen Interval: 7 - 17 3.99pH STABILIZED PARAMETERS 0.05 1.12 Spec. Cond.(mS/cm) Turbidity (NTU) 68.00 250 mL poly NP DO (mg/L) ORP (mV) 3.80 204.80 GW4Q19-PIW-10S WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.05 19.21 Cloudy Rain Wind (mph)5 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-18-2019 Time:12:49 Water Volume = 16.1 23.39 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:05 16.08 200.00 5.27 2.39 213.00 8.71 Clear None 13:10 16.08 200.00 5.04 2.87 227.60 5.22 Clear None 13:15 16.08 200.00 4.88 3.78 236.90 3.26 Clear None 13:20 16.08 200.00 4.75 4.34 242.80 1.91 Clear None 13:25 16.08 200.00 4.77 4.97 244.00 1.03 Clear None 13:30 16.08 200.00 4.77 4.71 244.10 0.83 Clear None 13:35 16.08 200.00 4.73 4.98 248.70 1.13 Clear None Sampling Data Zero HS: Method:Date: Time:13:40Field Parameters Sample ID: DuplicateID: Sunny None Wind (mph)4 Precipitation: Sky: Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.07 22.17 DO (mg/L) ORP (mV) 4.98 248.70 GW4Q19-PW-01 WEATHER CONDITIONS 65.00 250 mL poly NP Initial Depth to Water (ft.): Temperature (F): 1.166 10-18-2019 Low Flow: Geo Pump Temp.(oC)PFAS21.79 Screen Interval: 11 - 21 4.73pH STABILIZED PARAMETERS 0.06 1.13 Spec. Cond.(mS/cm) Turbidity (NTU) RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER Ally Vo WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen PW-01 Project Manager: Depth to Well Bottom (ft.): Peristaltic Pump Spec. Cond. mS/cm Total Volume Purged (gallons): Temp.oC 0.08 21.97 0.06 21.88 0.06 21.79 0.06 22.20 0.06 21.68 0.06 21.99 Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-04-2019 Time:14:40 Water Volume = 56.6 64.74 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min. gal.mg/L mV NTU 14:45 56.60 200.00 5.48 1.19 186.40 204.00 Cloudy None 15:50 56.60 200.00 5.35 0.77 188.50 231.00 Cloudy None 14:55 56.55 200.00 1.00 5.26 0.62 189.20 221.00 Cloudy None 15:00 56.58 200.00 5.21 0.83 190.70 226.00 Cloudy Nome 15:05 56.65 200.00 5.17 0.83 193.90 230.10 Cloudy No odor 15:15 56.60 200.00 5.14 4.77 197.90 250.00 Cloudy None 15:20 56.70 200.00 5.04 2.41 206.50 213.00 Cloudy None 15:25 56.63 200.00 4.81 6.03 217.80 168.00 Cloudy No odor 15:30 56.61 200.00 4.91 3.22 217.90 159.00 Cloudy No odor 15:35 56.62 200.00 4.92 3.11 219.10 155.00 Cloudy No odor 15:40 56.65 200.00 4.92 2.83 221.20 155.00 Cloudy No odor 15:45 56.59 200.00 4.88 2.89 224.50 141.00 Cloudy None 15:50 56.61 200.00 4.83 6.68 232.10 146.00 Cloudy None 15:55 56.57 200.00 4.8 7.80 233.50 137.00 Cloudy None 16:00 56.66 200.00 4.72 5.03 239.10 133.00 Cloudy Nome 16:05 56.60 200.00 4.73 4.04 242.50 135.00 Cloudy No odor 16:10 56.67 200.00 4.71 6.65 244.80 125.00 Cloudy No odor Sampling Data Zero HS: Method:Date: Time:16:10 Field Parameters Sample ID: DuplicateID: 0.11 18.57 0.11 18.56 0.11 18.54 0.12 18.62 0.12 18.57 0.11 18.57 0.12 18.63 0.12 18.56 0.12 18.66 0.12 18.71 0.12 18.71 0.12 18.67 0.13 18.91 0.13 18.94 0.12 18.91 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE Luke Tart WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen PW-02 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 7.4Total Volume Purged (gallons): Temp. oC 0.13 19.06 Initial Depth to Water (ft.): Temperature (F): 1.302 11-04-2019 Double valve pump Temp.(oC)PFAS18.54 Screen Interval: 50 - 60 4.71pH STABILIZED PARAMETERS 0.11 125.00 Spec. Cond.(mS/cm) Turbidity (NTU) 66.00 250 mL poly NP DO (mg/L) ORP (mV) 6.65 244.80 GW4Q19-PW-02 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.13 18.94 Partly Cloudy None Wind (mph)5 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-05-2019 Time:15:10 Water Volume = 42.26 49.68 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 15:20 43.05 100.00 0.03 6.27 5.45 -135.40 1000.00 murky None 15:25 43.24 100.00 0.03 6.18 1.94 -143.90 1000.00 Cloudy No odor 15:30 43.59 100.00 0.03 6.12 1.69 -142.00 1000.00 Cloudy No odor 15:35 43.85 100.00 0.03 5.98 1.26 -142.40 1000.00 Cloudy No odor 15:40 44.00 100.00 0.03 5.8 2.62 -59.80 1000.00 Cloudy No odor 15:45 44.25 100.00 0.03 5.69 1.11 -89.90 1000.00 Cloudy No odor 15:50 44.35 100.00 0.03 5.6 0.90 -143.50 1000.00 Cloudy No odor 15:55 44.60 100.00 0.03 5.64 0.73 -137.90 1000.00 Cloudy None 16:00 44.55 100.00 0.03 5.79 0.67 -153.20 1000.00 Cloudy No odor 16:05 44.55 100.00 0.03 5.92 0.67 -156.40 1000.00 Cloudy No odor 16:10 44.60 100.00 0.27 5.91 0.64 -161.60 1000.00 Cloudy No odor 16:15 45.48 100.00 0.03 5.88 0.61 -160.00 1000.00 Cloudy No odor 16:20 46.08 100.00 0.27 5.44 0.75 -142.90 1000.00 Murky None Sampling Data Zero HS: Method:Date: Time:15:39Field Parameters Sample ID: DuplicateID: 0.23 20.11 0.21 18.68 0.27 19.77 0.28 19.76 0.25 20.00 0.30 19.78 0.26 19.69 0.26 19.74 0.33 20.72 0.33 20.43 0.31 19.90 RECORD OF WELL SAMPLING Well ran dry = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey 46 within screen PW-03 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.35 21.28 Initial Depth to Water (ft.): Temperature (F): 1.187 11-05-2019 Double valve pump Temp.(oC)PFAS18.68 Screen Interval: 35 - 45 5.44pH STABILIZED PARAMETERS 0.21 1000.00 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 0.75 GW4Q19-PW-03 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.33 21.03 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-30-2019 Time:09:30 Water Volume = 29.33 79.6 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 09:35 29.43 225.00 0.30 4.07 5.58 364.50 36.60 Clear No odor 09:45 29.45 225.00 0.30 3.98 4.90 414.70 8.61 Clear No odor 09:55 29.45 225.00 0.30 3.83 4.92 404.10 4.23 Clear No odor 10:00 29.45 225.00 0.30 3.93 4.89 402.80 3.47 Clear No odor Sampling Data Zero HS: Method:Date: Time:10:00Field Parameters Sample ID: DuplicateID: 0.08 19.45 0.08 19.36 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey 74 within screen PW-05 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 1.8Total Volume Purged (gallons): Temp. oC 0.07 19.50 Initial Depth to Water (ft.): Temperature (F): 8.043 10-30-2019 Double valve pump Temp.(oC)PFAS19.36 Screen Interval: 65 - 75 3.93pH STABILIZED PARAMETERS 0.08 3.47 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 4.89 402.80 GW4Q19-PW-05 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.08 19.35 Cloudy None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-30-2019 Time:11:17 Water Volume = 25.33 58.31 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:23 26.50 180.00 0.24 11.38 0.41 -113.10 45.40 Clear No odor 11:28 26.51 180.00 0.24 11.33 0.52 -119.90 28.50 Clear No odor 11:32 26.50 180.00 0.24 11.57 0.23 -144.70 17.80 Clear No odor 11:37 26.50 180.00 0.24 11.62 0.21 -187.90 21.50 Clear No odor 11:42 26.50 180.00 0.24 11.36 0.18 -168.90 62.10 Clear No odor 11:47 26.51 180.00 0.24 10.74 0.16 -123.70 75.20 Clear No odor 11:52 26.49 180.00 0.24 10.61 0.16 -65.60 79.30 Clear No odor 11:57 26.49 180.00 0.24 10.35 0.18 -72.90 75.50 Clear No odor 12:02 26.49 180.00 0.24 10.22 0.12 -69.30 77.20 Clear No odor 12:07 26.48 180.00 0.24 10.14 0.13 -83.70 80.60 Clear No odor 12:12 26.48 180.00 0.24 10.08 0.12 -98.10 80.70 Clear No odor 12:17 26.49 180.00 0.24 9.96 0.12 -100.10 83.10 Clear No odor 12:22 26.50 180.00 0.24 9.98 0.12 -101.10 84.90 Clear No odor 12:27 26.49 180.00 0.24 9.88 0.12 -97.90 85.00 Clear No odor 12:32 26.50 180.00 0.24 9.89 0.12 -108.60 84.40 Clear No odor 12:37 26.50 180.00 0.24 9.86 0.12 -108.50 85.50 Clear No odor 12:42 26.49 180.00 0.24 9.81 0.10 -116.90 79.80 Clear No odor 12:47 26.50 180.00 0.24 9.78 0.09 -120.10 77.40 Clear No odor 12:52 26.50 180.00 0.24 9.73 0.09 -120.50 76.30 Clear No odor 12:57 26.49 180.00 0.24 9.67 0.09 -124.60 72.80 Clear No odor 13:02 26.49 180.00 0.24 9.62 0.07 -129.10 75.90 Clear No odor 13:07 26.49 180.00 0.24 9.6 0.05 -130.30 72.40 Clear No odor 13:12 26.49 180.00 0.24 9.57 0.05 -132.90 71.10 Clear No odor 13:17 26.49 180.00 0.24 9.54 0.05 -124.10 69.80 Clear No odor 13:23 26.49 180.00 0.24 9.51 0.05 -127.50 68.80 Clear No odor 13:28 26.48 180.00 0.24 9.49 0.05 -124.50 66.80 Clear No odor 13:33 26.49 180.00 0.24 9.48 0.05 -126.50 67.50 Clear No odor Sampling Data Zero HS: Method:Date: Time:01:35Field Parameters 0.13 18.62 Turbidity stabilized around 68 NTU for half hour period. 0.13 18.39 0.14 18.39 0.13 18.42 0.14 18.35 0.14 18.41 0.14 18.44 0.16 18.30 0.15 18.30 0.15 18.26 0.17 18.34 0.17 18.38 0.17 18.34 0.18 18.48 0.17 18.39 0.17 18.40 0.20 18.45 0.19 18.41 0.19 18.54 0.28 18.49 0.25 18.51 0.22 18.47 0.80 18.56 0.68 18.51 0.61 18.43 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey 51 within screen PW-09 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 6.53Total Volume Purged (gallons): Temp. oC 0.51 18.28 Initial Depth to Water (ft.): 5.277 10-30-2019 Double valve pump Temp.(oC)PFAS18.62 Screen Interval: 44 - 54 9.48pH STABILIZED PARAMETERS 0.13 67.50 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 0.05 Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.61 18.40 Sample ID: DuplicateID: Temperature (F): GW4Q19-PW-09 WEATHER CONDITIONS Cloudy None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-04-2019 Time:12:30 Water Volume = 27.64 69.1 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min. gal.mg/L mV NTU 12:40 27.80 200.00 0.27 5.43 0.51 84.90 28.50 Clear None 12:45 27.82 200.00 0.27 5.4 0.19 75.80 7.30 Clear None 12:50 27.90 200.00 0.27 5.41 0.17 65.70 6.98 Clear None 12:55 27.80 200.00 5.42 0.22 61.40 7.61 Clear None 13:00 27.80 200.00 0.27 5.4 0.39 58.20 4.68 Clear None 13:05 27.82 200.00 5.39 0.35 56.60 3.47 Clear None 13:10 27.90 200.00 2.50 5.4 0.29 52.50 3.91 Clear None 13:15 27.80 200.00 5.4 0.18 50.70 3.46 Clear None 13:20 27.90 200.00 3.00 5.4 0.18 47.60 4.39 Clear Nome 13:26 27.85 200.00 5.39 0.13 45.90 5.15 Clear None 13:30 27.86 200.00 0.27 5.39 0.12 43.60 3.66 Clear None 13:35 27.86 200.00 4.00 5.39 0.12 42.80 4.99 Clear None Sampling Data Zero HS: Method:Date: Time:13:40 Field Parameters Sample ID: DuplicateID: 0.06 18.05 0.06 17.92 0.06 17.99 0.06 17.99 0.06 17.87 0.06 17.89 0.06 18.00 0.06 17.88 0.06 17.91 0.06 17.88 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE Luke Tart WATER VOLUME CALCULATION Quarterly Tracy Ovbey 62 within screen PW-10R Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 4.3Total Volume Purged (gallons): Temp. oC 0.07 18.13 Initial Depth to Water (ft.): Temperature (F): 6.634 11-04-2019 Double valve pump Temp.(oC)PFAS18.05 Screen Interval: 57 - 67 5.39pH STABILIZED PARAMETERS 0.06 4.99 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 0.12 42.80 GW4Q19-PW-10R WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.07 17.88 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-22-2019 Time:15:07 Water Volume = 33.68 67.57 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 15:50 33.97 450.00 3.85 24.27 181.00 0.00 Clear 15:55 33.98 450.00 3.83 3.02 168.00 0.00 Clear 16:00 33.98 450.00 3.96 2.40 154.00 0.00 16:05 33.98 450.00 4.09 0.00 144.00 0.00 16:10 33.98 450.00 4.22 0.00 127.00 0.00 16:15 33.98 450.00 4.35 0.00 118.00 0.30 16:18 33.97 450.00 4.43 0.00 115.00 0.00 Sampling Data Zero HS: Method:Date: Time:16:25 Field Parameters Sample ID: DuplicateID: 0.49 18.75 0.50 18.78 0.50 19.06 0.50 19.03 0.50 18.91 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 STEVEN BOOR Brandon - Geosyntec WATER VOLUME CALCULATION Other Tracy Ovbey within screen PW-11 Project Manager: Depth to Well Bottom (ft.): Other Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.50 19.23 Initial Depth to Water (ft.): Temperature (F): 5.422 10-22-2019 Double valve pump Temp.(oC)PFAS18.78 Screen Interval: 53 - 63 4.43pH STABILIZED PARAMETERS 0.50Spec. Cond.(mS/cm) Turbidity (NTU) 80.00 250 mL poly NP DO (mg/L) ORP (mV)115.00 GW4Q19-PW-11 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.51 18.93 Partly Sunny Rain Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-05-2019 Time:11:00 Water Volume = 58.14 124.34 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:10 58.21 200.00 0.27 5.93 -0.73 -116.70 495.00 Cloudy No odor 11:15 58.20 200.00 0.27 5.77 -0.60 -116.50 279.00 Cloudy No odor 11:20 58.21 200.00 0.27 5.68 -0.48 -119.00 207.00 Cloudy No odor 11:25 58.20 200.00 0.27 5.66 -0.44 -118.70 193.00 Cloudy No odor 11:30 58.20 200.00 0.27 5.67 -0.34 -125.50 153.00 Cloudy No odor 11:35 58.20 200.00 0.27 5.66 -0.28 -128.00 120.00 Cloudy No odor 11:40 58.20 200.00 0.27 5.66 -0.26 -132.10 108.00 Cloudy No odor 11:45 58.20 200.00 0.27 5.66 -0.22 -133.80 97.40 Cloudy No odor 11:50 58.20 200.00 0.27 5.67 -0.20 -136.50 83.90 Cloudy No odor 11:55 58.20 200.00 0.27 5.61 -0.24 -143.50 75.00 Cloudy None 12:00 58.20 200.00 0.27 5.57 2.11 -148.20 68.00 Cloudy None 12:05 58.20 200.00 0.27 5.54 1.34 -147.90 61.60 Cloudy None 12:10 58.20 200.00 0.27 5.51 0.96 -150.10 59.20 Cloudy No odor 12:15 58.20 200.00 0.27 5.48 0.78 -148.50 55.30 Clear No odor 12:20 58.20 200.00 0.27 5.42 0.73 -150.50 47.30 Clear No odor 12:25 19.15 200.00 0.27 5.41 0.67 -146.80 38.40 Cloudy None 12:30 58.20 200.00 0.27 5.48 -0.52 -153.00 28.10 Clear None 12:35 58.20 200.00 0.27 5.54 -0.40 -142.80 25.30 Clear No odor 12:40 58.20 200.00 0.27 5.6 -0.32 -149.00 21.80 Clear None 12:45 58.20 200.00 0.27 5.73 -0.14 -93.60 23.50 Cloudy None 12:50 58.20 200.00 0.27 5.69 -0.14 -115.80 26.40 Clear None 12:55 58.20 200.00 0.27 5.66 -0.14 -128.60 26.90 Clear None 13:00 58.20 200.00 0.27 5.65 -0.14 -141.10 24.40 Cloudy None 13:05 58.20 200.00 0.27 5.65 -0.14 -146.20 25.70 Clear None 13:10 58.20 200.00 0.27 5.63 -0.14 -150.60 20.80 Clear None 13:15 58.20 200.00 0.27 5.62 -0.14 -152.20 18.60 Clear No odor 13:20 58.20 200.00 0.27 5.61 -0.14 -152.50 17.80 Clear None Sampling Data Zero HS: Method:Date: Time:13:20Field Parameters 0.05 19.25 0.05 19.36 0.05 19.47 0.05 19.43 0.05 19.53 0.05 19.32 0.05 19.30 0.05 19.41 0.05 19.31 0.05 19.96 0.05 19.09 0.05 19.17 0.05 19.19 0.05 19.33 0.05 19.16 0.05 19.05 0.05 19.72 0.05 19.64 0.05 19.52 0.05 19.48 0.05 19.65 0.05 19.63 0.05 19.32 0.05 19.40 0.05 19.50 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE WATER VOLUME CALCULATION Quarterly Tracy Ovbey 116 within screen PW-12 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 6.93Total Volume Purged (gallons): Temp. oC 0.05 19.18 Initial Depth to Water (ft.): 10.592 11-05-2019 Double valve pump Temp.(oC)PFAS19.25 Screen Interval: 109 - 119 5.61pH STABILIZED PARAMETERS 0.05 17.80 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.05 19.26 Sample ID: DuplicateID: Temperature (F): GW4Q19-PW-12 WEATHER CONDITIONS Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-23-2019 Time:12:58 Water Volume = 61.15 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:30 61.15 195.00 5.51 0.00 117.00 295.00 Grey No 13:35 61.18 195.00 5.26 0.00 125.00 84.50 Murky No 13:40 61.15 195.00 4.72 0.00 164.00 1.00 Clear No 13:45 61.15 195.00 4.71 0.00 166.00 0.00 Clear No 13:50 61.15 195.00 4.67 0.00 167.00 0.00 Clear No Sampling Data Zero HS: Method:Date: Time:13:55 Field Parameters Sample ID: DuplicateID: 0.18 22.77 0.18 22.20 0.18 23.01 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 CHARLES PACE WATER VOLUME CALCULATION Quarterly Tracy Ovbey within screen PW-14 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 1.03Total Volume Purged (gallons): Temp. oC 0.20 22.78 Initial Depth to Water (ft.): Temperature (F): -9.784 10-23-2019 Double valve pump Temp.(oC)PFAS23.01 Screen Interval: 136 - 146 4.67pH STABILIZED PARAMETERS 0.18Spec. Cond.(mS/cm) Turbidity (NTU) 71.00 250 mL poly NP DO (mg/L) ORP (mV)167.00 GW4Q19-PW-14 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.19 23.39 Sunny None Wind (mph)8 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-31-2019 Time:10:25 Water Volume = 14.28 54.88 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 10:30 14.30 200.00 0.27 6.13 0.62 -29.90 25.00 Clear No odor 10:35 14.30 200.00 0.27 6.1 0.36 -48.30 68.10 Clear No odor 10:40 14.30 200.00 0.27 6.25 0.26 -64.20 65.10 Clear No odor 10:45 14.31 200.00 0.27 6.38 0.24 -78.00 48.00 Clear No odor 10:50 14.30 200.00 0.27 6.42 0.28 -85.60 43.60 Clear No odor 10:55 14.31 200.00 0.27 6.42 0.25 -89.50 36.10 Clear No odor 11:00 14.31 200.00 0.27 6.42 0.19 -87.60 31.10 Clear No odor 11:05 14.31 200.00 0.27 6.42 0.19 -93.90 29.10 Clear No odor 11:10 14.32 200.00 0.27 6.43 0.19 -97.50 25.40 Clear No odor 11:15 14.32 200.00 0.27 6.41 0.19 -96.70 25.60 Clear No odor 11:20 14.31 200.00 0.27 6.4 0.13 -101.10 22.80 Clear No odor 11:25 14.31 200.00 0.27 6.42 0.13 -100.50 19.50 Clear No odor 11:30 14.31 200.00 0.27 6.41 0.13 -101.50 19.60 Clear No odor 11:35 14.31 200.00 0.27 6.39 0.13 -102.10 17.20 Clear No odor Sampling Data Zero HS: Method:Date: Time:11:35 Field Parameters Sample ID: DuplicateID: 0.08 22.43 0.08 22.42 0.08 22.43 0.08 22.42 0.08 22.39 0.08 22.39 0.08 22.50 0.08 22.45 0.08 22.45 0.08 22.68 0.08 22.74 0.08 22.62 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE Ali Vo WATER VOLUME CALCULATION Quarterly Tracy Ovbey 47.7 within screen Robeson-1D Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 3.73Total Volume Purged (gallons): Temp. oC 0.08 22.97 Initial Depth to Water (ft.): Temperature (F): 6.496 10-31-2019 Double valve pump Temp.(oC)PFAS22.43 Screen Interval: 42.75 - 52.75 6.39pH STABILIZED PARAMETERS 0.08 17.20 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 0.13 GW4Q19-Robeson-1D WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.08 22.80 Partly Cloudy None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10-31-2019 Time:13:00 Water Volume = 12.06 28.65 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:05 12.19 120.00 0.16 5.5 3.13 165.40 7.72 Clear No odor 13:10 12.20 120.00 0.16 5.46 2.98 168.20 6.03 Clear No odor 13:15 12.20 120.00 0.16 5.51 2.82 161.30 5.05 Clear No odor Sampling Data Zero HS: Method:Date: Time:13:15 Field Parameters Sample ID: DuplicateID: 0.08 25.48 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE Ali Vo WATER VOLUME CALCULATION Quarterly Tracy Ovbey 22 within screen Robeson-1S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 0.48Total Volume Purged (gallons): Temp. oC 0.08 25.80 Initial Depth to Water (ft.): Temperature (F): 2.654 10-31-2019 Peristaltic Pump Temp.(oC)PFAS25.48 Screen Interval: 17 - 27 5.51pH STABILIZED PARAMETERS 0.08 5.05 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 2.82 161.30 GW4Q19-Robeson-1S WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.08 25.62 Partly Cloudy None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-06-2019 Time:14:00 Water Volume = 59.47 124 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 14:05 59.58 125.00 6.04 7.75 89.10 97.50 Clear None 14:10 59.64 125.00 0.17 5.55 3.54 92.50 38.60 Clear None 14:15 59.68 125.00 0.17 5.48 3.25 127.60 28.80 Clear None 14:20 59.66 125.00 0.17 5.3 3.25 143.10 26.00 Clear None 14:25 59.65 125.00 0.17 5.14 3.24 149.10 19.50 Clear None 14:30 59.69 125.00 0.17 5.12 3.22 149.00 12.80 Clear None Sampling Data Zero HS: Method:Date: Time:14:30Field Parameters a a Sample ID: DuplicateID: Sunny None Wind (mph) Precipitation: Sky: Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.17 19.50 DO (mg/L) ORP (mV) 3.22 149.00 GW4Q19-PW-15R WEATHER CONDITIONS GW4Q19-PW-15R-D 250 mL poly NP Initial Depth to Water (ft.): Temperature (F): 10.325 11-06-2019 PFC Free Bladder Pump Temp.(oC)PFAS19.40 Screen Interval: 110 - 120 5.12pH STABILIZED PARAMETERS 0.15 12.80 Spec. Cond.(mS/cm) Turbidity (NTU) RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE Danielle Delgado WATER VOLUME CALCULATION Quarterly Tracy Ovbey 120 within screen PW-15R Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 1Total Volume Purged (gallons): Temp. oC 0.18 19.50 0.15 19.40 0.16 19.40 0.16 19.60 0.15 19.40 Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-08-2019 Time:13:10 Water Volume = 34.2 133.05 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 13:20 34.44 125.00 0.17 9.91 4.14 212.10 293.00 Cloudy None 13:25 34.38 125.00 0.17 8.63 1.07 127.70 246.00 Cloudy None 13:30 34.45 125.00 0.17 7.97 0.89 53.80 209.00 Cloudy None 13:35 34.44 125.00 0.17 7.56 0.86 18.40 170.00 Cloudy None 13:40 34.42 125.00 0.17 7.23 0.82 0.70 157.00 Cloudy None 13:45 34.44 125.00 0.17 7.08 0.82 -12.60 141.00 Cloudy None 13:50 34.44 125.00 0.17 6.99 0.83 -21.70 132.00 Cloudy None 13:55 34.40 125.00 0.17 6.9 0.83 -26.30 113.00 Cloudy None 14:00 34.42 125.00 0.17 6.89 0.80 -32.00 107.00 Cloudy None 14:05 34.44 125.00 0.17 6.85 0.81 -32.90 97.00 Cloudy None 14:11 34.44 125.00 0.17 8.7 0.81 -30.10 95.00 Cloudy None 14:15 34.44 125.00 0.17 6.7 0.88 -26.20 89.00 Cloudy None 14:20 34.44 125.00 0.17 6.63 0.97 -23.10 87.00 Cloudy None 14:25 34.44 125.00 0.17 6.55 0.98 -23.40 86.80 Cloudy None 14:30 34.44 125.00 0.17 6.54 1.00 -23.00 83.30 Cloudy None 14:35 34.44 125.00 0.17 6.48 1.10 -20.00 94.00 Cloudy None 14:40 34.44 125.00 0.17 6.46 1.10 -19.70 99.10 Cloudy None 14:45 34.44 125.00 0.17 6.42 1.09 -19.50 98.10 Cloudy None 14:50 34.44 125.00 0.17 6.39 1.19 -18.40 103.00 Cloudy None 14:55 34.44 125.00 0.17 6.38 1.19 -17.00 97.20 Cloudy None Sampling Data Zero HS: Method:Date: Time:15:00 Field Parameters a Sample ID: DuplicateID: 0.10 18.00 0.10 17.60 0.10 17.10 0.10 17.80 0.10 17.90 0.10 18.10 0.11 17.70 0.10 16.70 0.10 17.90 0.11 18.20 0.11 17.90 0.11 17.60 0.11 17.30 0.11 18.00 0.11 17.70 0.13 18.00 0.12 17.90 0.12 18.20 RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE Danielle delgado WATER VOLUME CALCULATION Quarterly Tracy Ovbey 129 within screen PW-13 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm 3.33Total Volume Purged (gallons): Temp. oC 0.35 18.70 Initial Depth to Water (ft.): Temperature (F): 15.816 11-08-2019 Double valve pump Temp.(oC)PFAS17.10 Screen Interval: 120 - 130 6.38pH STABILIZED PARAMETERS 0.10 97.20 Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) 1.19 GW4Q19-PW-13 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.15 17.40 Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-07-2019 Time:11:14 Water Volume = 40.04 41.77 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU 11:20 40.04 0.25 5.97 5.29 316.90 83.10 Cloudy None Sampling Data Zero HS: Method:Date: Time:11:28 Field Parameters Sample ID: DuplicateID: RECORD OF WELL SAMPLING Well ran dry = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BRANDON WEIDNER K. Stuart WATER VOLUME CALCULATION Quarterly Tracy Ovbey bottom of well PW-07 Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp.oC 0.09 21.30 Initial Depth to Water (ft.): Temperature (F): 0.277 11-07-2019 Temp.(oC)PFAS21.30 Screen Interval: 28 - 38 5.97pH STABILIZED PARAMETERS 0.09 83.10 Spec. Cond.(mS/cm) Turbidity (NTU) 71.00 250 mL poly NP DO (mg/L) ORP (mV) 5.29 316.90 GW4Q19-PW-07 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Went dry before we could sample water Sunny None Wind (mph)2 Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:11-08-2019 Time:09:17 Water Volume = 40.15 41.75 Time DTW Pump Rate Vol.pH DO Redox Turbidity Color Odor 24 hr.ft.ml/min.gal.mg/L mV NTU Sampling Data Zero HS: Method:Date: Time:09:30Field Parameters a Sample ID: DuplicateID: RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 BEN KRAUSE Danielle Delgado WATER VOLUME CALCULATION Quarterly Tracy Ovbey PW-07 Project Manager: Depth to Well Bottom (ft.): Grab Spec. Cond. mS/cm 0Total Volume Purged (gallons): Temp. oC Initial Depth to Water (ft.): Temperature (F): 0.256 11-08-2019 Temp.(oC)PFAS Screen Interval: 28 - 38 pH STABILIZED PARAMETERS Spec. Cond.(mS/cm) Turbidity (NTU) 250 mL poly NP DO (mg/L) ORP (mV) GW4Q19-PW-07 WEATHER CONDITIONS Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. Sunny None Wind (mph) Precipitation: Sky: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10/29/2019 Time:1235 Water Volume = 14.52 31.54 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr. ft. ml/min. gal.mg/L mV NTU 1235 1240 15.07 175.00 4.52 0.83 251.40 30.30 1246 15.14 185.00 4.50 0.63 247.70 33.50 1251 15.23 185.00 4.46 0.61 240.90 30.50 1256 15.20 175.00 4.52 0.48 237.10 35.90 1304 15.20 175.00 4.65 0.46 215.00 33.50 1309 15.26 -4.64 0.46 210.80 24.10 1314 15.25 -4.63 0.52 210.90 20.50 1319 15.29 -4.61 0.56 213.20 31.70 1324 15.31 -4.6 0.55 210.20 14.20 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: Temperature (F): Wind (mph) Sky: Precipitation: WEATHER CONDITIONS ORP (mV)210.20 14.20 18-28 PFAS 250 mL poly Spec. Cond.(mS/cm)0.09 Screen Interval:PFAS 2-250 mL poly NP EPA 537 Modified DO (mg/L)0.55 NP Table 3 Temp.(oC)18.00 PFAS 250 mL poly NP Table 3+ Turbidity (NTU) STABILIZED PARAMETERS SAMPLE SET pH 4.60 Parameter Bottle Pres.Method Total Volume Purged (gallons): 0.093 18.0 0.093 18.0 0.093 18.1 0.093 18.1 0.094 18.3 0.093 18.1 0.094 18.4 0.094 18.3 BEGIN PURGING 0.094 18.5 Initial Depth to Water (ft.): Depth to Well Bottom (ft.): Spec. Cond. Temp.Comments mS/cm oC `23 WATER VOLUME CALCULATION = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot RECORD OF WELL SAMPLING Chemours Fayetteville PIW-6S 2 Brandon Peach and Savannah Volkoff Project Manager: Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10/31/2019 Time:1100 Water Volume = 5.73 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr. ft. ml/min. gal.mg/L mV NTU 1100 5.40 150.00 5.88 0.81 68.10 19.10 1106 5.70 200.00 5.87 0.49 50.10 26.10 1111 5.60 200.00 5.86 0.48 40.20 20.30 1116 5.90 200.00 5.89 0.37 30.40 19.70 1121 6.00 200.00 5.93 0.39 23.00 19.29 1126 6.00 200.00 5.97 0.38 17.90 6.85 1130 6.01 200.00 6.01 0.35 13.70 4.46 1135 5.90 200.00 6.03 0.40 11.00 6.97 1140 6.00 200.00 6.05 0.35 8.80 4.83 1145 6.00 200.00 6.06 0.35 7.50 2.86 1150 6.00 200.00 6.07 0.31 6.10 2.49 1155 6.01 200.00 6.08 0.34 5.90 2.70 1200 6.00 200.00 6.08 0.31 5.30 3.92 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: 0.152 18.9 Wind (mph) Precipitation: Sky: 250 mL poly NP Comments SAMPLE SET Table 3+ PFAS Parameter Method EPA 537 Modified PFAS Bottle Table 3 2-250 mL poly 250 mL poly NP NP Pres. 0.015 19.3 DO (mg/L) ORP (mV) 0.31 5.30 WEATHER CONDITIONS Initial Depth to Water (ft.): Temperature (F): Temp.(oC)PFAS18.90 Screen Interval: 7-17=10FT 6.08pH STABILIZED PARAMETERS 0.15 3.92 Spec. Cond.(mS/cm) Turbidity (NTU) RECORD OF WELL SAMPLING = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot Chemours Fayetteville 2 Brandon Peach and Savannah Volkoff WATER VOLUME CALCULATION`12 PIW-7S Project Manager: Depth to Well Bottom (ft.): Spec. Cond. mS/cm Total Volume Purged (gallons): Temp. oC 0.145 19.7 0.146 19.1 0.015 18.9 0.152 18.9 0.153 18.9 0.154 18.9 0.154 18.9 0.153 18.9 0.155 18.8 0.155 18.8 0.154 18.9 Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10/29/2019 Time:1635 Water Volume = 28.25 30.8 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr. ft. ml/min. gal.mg/L mV NTU 1635 28.78 50.00 4.02 1.32 316.40 8.3 1640 29.31 50.00 3.96 0.87 320.90 16.7 1645 29.68 25.00 3.96 0.78 315.40 46.9 1650 29.90 25.00 3.90 0.76 306.80 24.6 1655 30.20 25.00 4.00 0.81 300.50 18.0 1700 30.64 25.00 4.01 0.84 297.10 12.4 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: Temperature (F): Wind (mph) Sky: Precipitation: WEATHER CONDITIONS ORP (mV)297.10 12.40 10 PFAS 250 mL poly Spec. Cond.(mS/cm)0.43 Screen Interval:PFAS 2-250 mL poly NP EPA 537 Modified DO (mg/L)0.84 NP Table 3 Temp.(oC)19.70 PFAS 250 mL poly NP Table 3+ Turbidity (NTU) STABILIZED PARAMETERS SAMPLE SET pH 4.01 Parameter Bottle Pres.Method Total Volume Purged (gallons): 0.426 19.8 0.433 19.7 0.401 19.7 1629 begin purge 0.416 19.7 0.417 19.7 1625 stop and cut new tubing 30ft Initial Depth to Water (ft.): Depth to Well Bottom (ft.): Spec. Cond. Temp.Comments RECORD OF WELL SAMPLING Chemours Fayetteville PW-04 2 Brandon Peach and Savannah Volkoff Project Manager: mS/cm oC 22 WATER VOLUME CALCULATION = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot 0.442 19.7 1620 begin purge Site Name:Well ID: Well Diameter: Inches Samplers:Event: Purging Data Pump Depth: Pump Loc: Method:Date:10/29/2019 Time:1420 Water Volume = 19.54 32.84 Time DTW Pump Rate Vol. pH DO Redox Turbidity Color Odor 24 hr. ft. ml/min. gal.mg/L mV NTU 1420 1425 20.20 175.00 3.94 3.00 392.40 2.23 1430 20.23 75.00 4.03 2.58 380.00 1.41 1435 20.20 -4.27 2.24 330.50 1.19 1440 20.26 125.00 4.37 3.30 319.80 1.15 1445 20.30 125.00 4.50 3.28 301.20 1.01 1450 20.31 125.00 4.67 3.11 179.10 1.71 1455 20.34 125.00 4.76 3.46 265.30 1.22 1500 20.27 125.00 4.92 2.56 242.50 1.52 1505 20.27 125.00 4.98 3.29 235.40 1.27 1510 20.29 125.00 4.99 3.06 228.20 1.25 1515 125.00 5.12 3.29 216.70 1.38 Sampling Data Zero HS: Method:Date: Time: Field Parameters Sample ID: DuplicateID: Temperature (F): Wind (mph) Sky: Precipitation: WEATHER CONDITIONS ORP (mV)216.70 1.38 10 PFAS 250 mL poly Spec. Cond.(mS/cm)0.07 Screen Interval:PFAS 2-250 mL poly NP EPA 537 Modified DO (mg/L)3.29 NP Table 3 Temp.(oC)19.00 PFAS 250 mL poly NP Table 3+ Turbidity (NTU) STABILIZED PARAMETERS SAMPLE SET pH 5.12 Parameter Bottle Pres.Method Total Volume Purged (gallons): 0.066 18.9 0.067 19.0 0.066 19.0 0.066 19.0 0.066 19.0 0.065 19.0 0.071 19.0 0.068 19.0 0.084 19.1 0.074 19.1 BEGIN PURGING 0.087 19.1 Initial Depth to Water (ft.): Depth to Well Bottom (ft.): Spec. Cond. Temp.Comments mS/cm oC 14 WATER VOLUME CALCULATION = (Total Depth of Well - Depth To Water ) x Casing Volume per Foot RECORD OF WELL SAMPLING Chemours Fayetteville PW-06 2 Brandon Peach and Savannah Volkoff Project Manager: TR0795 DATA REVIEW NARRATIVES AND LABORATORY REPORTS DATA REVIEW NARRATIVES AND LABORATORY REPORTS Data review narratives are included in this appendix. Due to file size limits, analytical laboratory reports will be provided separately with the hard copy of the report. All analytical data were reviewed using the Data Verification Module (DVM) within the LocusTM Environmental Information Management (EIM) system, which is a commercial software program used to manage data. Following the DVM process, a manual review of the data was conducted. The DVM and the manual review results were combined in a data review narrative report for each set of sample results, which were consistent with Stage 2b of the EPA Guidance for Labeling Externally Validated Laboratory Analytical Data for Superfund Use (EPA-540-R-08-005 2009). The narrative report summarizes which samples were qualified (if any), the specific reasons for the qualification, and any potential bias in reported results. The data usability, in view of the project’s data quality objectives (DQOs), was assessed and the data were entered into the EIM system. The data were evaluated by the DVM against the following data usability checks: Hold time criteria; Field and laboratory blank contamination; Completeness of QA/QC samples; MS/MSD recoveries and the relative percent differences (RPDs) between these spikes; Laboratory control sample/control sample duplicate recoveries and the RPD between these spikes; Surrogate spike recoveries for organic analyses; and RPD between field duplicate sample pairs. ADQM Data Review Narrative - FAY Creeks Seeps Old Outfall 002 919 rev.doc 1 of 3 ADQM DATA REVIEW NARRATIVE Site Chemours FAY – Fayetteville Project Creeks Seeps Old Outfall 002 9/19 Project Reviewer Michael Aucoin, AECOM as a Chemours contractor Sampling Dates September 17 - 18, 2019 Analytical Protocol Laboratory Analytical Method Parameter(s) TestAmerica - Sacramento 537 Modified PFAS1 TestAmerica - Sacramento Cl. Spec. Table 3 Compound SOP Table 3+ compounds 1 Perfluoroalkylsubstances, a list of 33 compounds including HFPO-DA. Sample Receipt The following items are noted for this data set: All samples were received in satisfactory condition and within EPA temperature guidelines on September 19, 2019 Data Review The electronic data submitted for this project was reviewed via the Data Verification Module (DVM) process. Overall the data is acceptable for use without qualification, except as noted below: •Some table 3+ results in three water samples were qualified B and the reported results may bebiased high, or false positives, due to a comparable concentration found in the associatedequipment blank. Byproduct 5 and PFMOAA results in sample ID EXCESS RIVER WATER- 091719 were also impacted by an MS RPR outside criteria indicating estimated results but the Bqualifier supercedes the J qualifier. •Several analytical results have been qualified J as estimated, and non-detect results qualified UJindicating an estimated reporting limit, due to a poor laboratory matrix spike; sample analysiswhich exceeded the laboratory preparation hold time; and poor field duplicate or lab replicate precision. See the Data Verification Module (DVM) Narrative Report for which samples werequalified, the specific reasons for qualification, and potential bias in reported results. ADQM Data Review Narrative - FAY Creeks Seeps Old Outfall 002 919 rev.doc 2 of 3 Attachments The DVM Narrative report is attached. The lab reports due to a large page count are stored on an AECOM network shared drive and are available to be posted on external shared drives, or on a flash drive. ADQM Data Review Narrative - FAY Creeks Seeps Old Outfall 002 919 rev.doc 3 of 3 Data Verification Module (DVM) The DVM is an internal review process used by the ADQM group to assist with the determination of data usability. The electronic data deliverables received from the laboratory are loaded into the Locus EIM™ database and processed through a series of data quality checks, which are a combination of software (Locus EIM™ database Data Verification Module (DVM)) and manual reviewer evaluations. The data is evaluated against the following data usability checks: • Field and laboratory blank contamination • US EPA hold time criteria • Missing Quality Control (QC) samples • Matrix spike(MS)/matrix spike duplicate (MSD) recoveries and the relative percent differences (RPDs) between these spikes • Laboratory control sample(LCS)/control sample duplicate (LCSD) recoveries and the RPD between these spikes • Surrogate spike recoveries for organic analyses • RPD between field duplicate sample pairs • RPD between laboratory replicates for inorganic analyses • Difference / percent difference between total and dissolved sample pairs. There are two qualifier fields in EIM: Lab Qualifier is the qualifier assigned by the lab and may not reflect the usability of the data. This qualifier may have many different meanings and can vary between labs and over time within the same lab. Please refer to the laboratory report for a description of the lab qualifiers. As they are lab descriptors they are not to be used when evaluating the data. Validation Qualifier is the 3rd party formal validation qualifier if this was performed. Otherwise this field contains the qualifier resulting from the ADQM DVM review process. This qualifier assesses the usability of the data and may not equal the lab qualifier. The DVM applies the following data evaluation qualifiers to analysis results, as warranted: Qualifier Definition B Not detected substantially above the level reported in the laboratory or field blanks. R Unusable result. Analyte may or may not be present in the sample. J Analyte present. Reported value may not be accurate or precise. UJ Not detected. Reporting limit may not be accurate or precise. The Validation Status Code field is set to “DVM” if the ADQM DVM process has been performed. If the DVM has not been run, the field will be blank. If the DVM has been run (Validation Status Code equals “DVM”), use the Validation Qualifier. DVM Narrative ReportContamination detected in equipment blank(s). Sample result does not differ significantly from the analyte concentration detected in the associatedequipment blank(s).LABSTATSValidation Options:Validation ReasonFayettevilleSite:Sampling Program:Creeks Seeps Old Outfall 002 9/19AnalyticalMethodAnalyteDateSampledPQLValidationQualifierLab Sample IDPre-prepMDLResult TypeField Sample IDPrepUnitsEXCESS RIVER WATER-09171909/17/2019 320-54544-3Byproduct 50.0027 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.0020PQLEXCESS RIVER WATER-09171909/17/2019 320-54544-3Byproduct 50.0027 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.0020PQLEXCESS RIVER WATER-09171909/17/2019 320-54544-3PFO2HxA0.015 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.0020PQLEXCESS RIVER WATER-09171909/17/2019 320-54544-3PFO2HxA0.015 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.0020PQLEXCESS RIVER WATER-09171909/17/2019 320-54544-3PFMOAA0.0080 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.0050PQLEXCESS RIVER WATER-09171909/17/2019 320-54544-3PFMOAA0.0079 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.0050PQLSEEP-C-1-091719 09/17/2019 320-54544-1Byproduct 52.8 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.29PQLSEEP-C-1-091719 09/17/2019 320-54544-1Byproduct 53.1 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.29PQLCFR-RM-76-091719 09/17/2019 320-54544-2PFO2HxA0.0045 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.0020PQLCFR-RM-76-091719 09/17/2019 320-54544-2PFO2HxA0.0050 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.0020PQLPage 1 of 11 Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidation Options:Validation ReasonFayettevilleSite:Sampling Program:Creeks Seeps Old Outfall 002 9/19AnalyticalMethodAnalyteDateSampledPQLValidationQualifierLab Sample IDPre-prepMDLResult TypeField Sample IDPrepUnitsCFR-RM-52-091719 09/17/2019 320-54545-2PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLCFR-RM-52-091719 09/17/2019 320-54545-2PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLCFR-RM-68-091719 09/17/2019 320-54536-3PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLCFR-RM-68-091719 09/17/2019 320-54536-3PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLPage 2 of 11 The preparation hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidation Options:Validation ReasonFayettevilleSite:Sampling Program:Creeks Seeps Old Outfall 002 9/19AnalyticalMethodAnalyteDateSampledPQLValidationQualifierLab Sample IDPre-prepMDLResult TypeField Sample IDPrepUnitsEB-01-09181909/18/2019 320-54536-6Hfpo Dimer Acid0.0040 UG/L537 ModifiedUJ3535_PFC0.0040PQLPage 3 of 11 Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidation Options:Validation ReasonFayettevilleSite:Sampling Program:Creeks Seeps Old Outfall 002 9/19AnalyticalMethodAnalyteDateSampledPQLValidationQualifierLab Sample IDPre-prepMDLResult TypeField Sample IDPrepUnitsCFR-RM-68-091719 09/17/2019 320-54536-3R-EVE0.0044 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-68-091719 09/17/2019 320-54536-3R-EVE0.0043 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-68-091719 09/17/2019 320-54536-3Byproduct 40.012 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-68-091719 09/17/2019 320-54536-3Byproduct 40.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-68-091719 09/17/2019 320-54536-3Byproduct 50.0030 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-68-091719 09/17/2019 320-54536-3Byproduct 50.0031 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-52-091719 09/17/2019 320-54545-2R-EVE0.0022 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-52-091719 09/17/2019 320-54545-2R-EVE0.0022 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-52-091719 09/17/2019 320-54545-2Byproduct 40.016 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-52-091719 09/17/2019 320-54545-2Byproduct 40.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-52-091719 09/17/2019 320-54545-2Byproduct 50.0045 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-56-091719 09/17/2019 320-54545-1R-EVE0.0031 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-56-091719 09/17/2019 320-54545-1R-EVE0.0030 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-56-091719 09/17/2019 320-54545-1Byproduct 40.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-56-091719 09/17/2019 320-54545-1Byproduct 50.0046 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-56-091719 09/17/2019 320-54545-1Byproduct 50.0049 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 4 of 11 Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidation Options:Validation ReasonFayettevilleSite:Sampling Program:Creeks Seeps Old Outfall 002 9/19AnalyticalMethodAnalyteDateSampledPQLValidationQualifierLab Sample IDPre-prepMDLResult TypeField Sample IDPrepUnitsCFR-BLADEN-091819 09/18/2019 320-54536-4R-EVE0.0074 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-BLADEN-091819 09/18/2019 320-54536-4R-EVE0.0082 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-BLADEN-091819 09/18/2019 320-54536-4Byproduct 40.018 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-BLADEN-091819 09/18/2019 320-54536-4Byproduct 40.020 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-BLADEN-091819 09/18/2019 320-54536-4Byproduct 50.046 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-BLADEN-091819 09/18/2019 320-54536-4Byproduct 50.049 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-KINGS-091819 09/17/2019 320-54545-3R-EVE0.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-KINGS-091819 09/17/2019 320-54545-3Byproduct 40.023 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-KINGS-091819 09/17/2019 320-54545-3Byproduct 50.033 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-KINGS-091819 09/17/2019 320-54545-3Byproduct 50.033 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-KINGS-091819-D 09/17/2019 320-54545-4Byproduct 50.032 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-KINGS-091819-D 09/17/2019 320-54545-4Byproduct 50.034 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWC-1-09171909/17/2019 320-54543-1PFMOAA0.69 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLWC-1-09171909/17/2019 320-54543-1PFMOAA0.67 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLWC-1-09171909/17/2019 320-54543-1R-EVE0.034 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWC-1-09171909/17/2019 320-54543-1R-EVE0.034 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWC-1-09171909/17/2019 320-54543-1Byproduct 40.061 UG/LCl. Spec. Table 3CompoundJPFAS_DI_Prep0.0020PQLPage 5 of 11 Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidation Options:Validation ReasonFayettevilleSite:Sampling Program:Creeks Seeps Old Outfall 002 9/19AnalyticalMethodAnalyteDateSampledPQLValidationQualifierLab Sample IDPre-prepMDLResult TypeField Sample IDPrepUnitsSOPWC-1-09171909/17/2019 320-54543-1Byproduct 40.059 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWC-1-09171909/17/2019 320-54543-1Byproduct 50.30 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWC-1-09171909/17/2019 320-54543-1Byproduct 50.28 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLEXCESS RIVER WATER-09171909/17/2019 320-54544-3R-EVE0.0071 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLEXCESS RIVER WATER-09171909/17/2019 320-54544-3R-EVE0.0072 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLEXCESS RIVER WATER-09171909/17/2019 320-54544-3Byproduct 40.016 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLGBC-1-09171909/17/2019 320-54543-3R-EVE0.018 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLGBC-1-09171909/17/2019 320-54543-3R-EVE0.018 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLGBC-1-09171909/17/2019 320-54543-3Byproduct 40.037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLGBC-1-09171909/17/2019 320-54543-3Byproduct 40.037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLOUTFALL 002-091719 09/17/2019 320-54536-2Byproduct 40.026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLOUTFALL 002-091719 09/17/2019 320-54536-2Byproduct 40.027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLOUTFALL 002-091719 09/17/2019 320-54536-2Byproduct 50.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 6 of 11 High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidation Options:Validation ReasonFayettevilleSite:Sampling Program:Creeks Seeps Old Outfall 002 9/19AnalyticalMethodAnalyteDateSampledPQLValidationQualifierLab Sample IDPre-prepMDLResult TypeField Sample IDPrepUnitsCFR-KINGS-091819 09/17/2019 320-54545-3R-EVE0.014 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-KINGS-091819 09/17/2019 320-54545-3Byproduct 40.023 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-KINGS-091819-D 09/17/2019 320-54545-4R-EVE0.0069 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-KINGS-091819-D 09/17/2019 320-54545-4R-EVE0.0069 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-KINGS-091819-D 09/17/2019 320-54545-4Byproduct 40.0096 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-KINGS-091819-D 09/17/2019 320-54545-4Byproduct 40.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 7 of 11 Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidation Options:Validation ReasonFayettevilleSite:Sampling Program:Creeks Seeps Old Outfall 002 9/19AnalyticalMethodAnalyteDateSampledPQLValidationQualifierLab Sample IDPre-prepMDLResult TypeField Sample IDPrepUnitsCFR-RM-52-091719 09/17/2019 320-54545-2Byproduct 50.0056 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLCFR-RM-56-091719 09/17/2019 320-54545-1Byproduct 40.017 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLEXCESS RIVER WATER-09171909/17/2019 320-54544-3Byproduct 40.018 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLOUTFALL 002-091719 09/17/2019 320-54536-2NVHOS0.0097 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLOUTFALL 002-091719 09/17/2019 320-54536-2NVHOS0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLOUTFALL 002-091719 09/17/2019 320-54536-2R-EVE0.0060 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLOUTFALL 002-091719 09/17/2019 320-54536-2R-EVE0.0071 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLOUTFALL 002-091719 09/17/2019 320-54536-2Byproduct 50.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLSEEP D-1-091719 09/17/2019 320-54536-1R-EVE1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLSEEP D-1-091719 09/17/2019 320-54536-1R-EVE1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLSEEP-A-3-091719 09/17/2019 320-54491-3PerfluorobutaneSulfonic Acid (trial)0.087 UG/L537 ModifiedJ3535_PFC0.019PQLSEEP-A-4-091719 09/17/2019 320-54491-2PFESA-BP10.10 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLSEEP-A-4-091719 09/17/2019 320-54491-2PFESA-BP10.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLSEEP-A-4-091719 09/17/2019 320-54491-2PFO4DA2.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLSEEP-A-4-091719 09/17/2019 320-54491-2PFO4DA3.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLSEEP-A-TR1-091719 09/17/2019 320-54491-1PFO4DA1.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLSEEP-A-TR1-091719 09/17/2019 320-54491-1PFO4DA1.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLPage 8 of 11 Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidation Options:Validation ReasonFayettevilleSite:Sampling Program:Creeks Seeps Old Outfall 002 9/19AnalyticalMethodAnalyteDateSampledPQLValidationQualifierLab Sample IDPre-prepMDLResult TypeField Sample IDPrepUnitsSEEP-A-TR1-091719 09/17/2019 320-54491-1Byproduct 50.25 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLSEEP-A-TR1-091719 09/17/2019 320-54491-1Byproduct 50.29 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLSEEP-B-TR1-091719 09/17/2019 320-54489-2R-EVE0.39 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLSEEP-B-TR1-091719 09/17/2019 320-54489-2R-EVE0.43 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLPage 9 of 11 Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit but above the rejection limit. Thereported result may be biased low.LABSTATSValidation Options:Validation ReasonFayettevilleSite:Sampling Program:Creeks Seeps Old Outfall 002 9/19AnalyticalMethodAnalyteDateSampledPQLValidationQualifierLab Sample IDPre-prepMDLResult TypeField Sample IDPrepUnitsCFR-BLADEN-091819 09/18/2019 320-54536-4PFMOAA0.15 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLCFR-BLADEN-091819 09/18/2019 320-54536-4PFMOAA0.15 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLOUTFALL 002-091719 09/17/2019 320-54536-2PFMOAA0.073 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLOUTFALL 002-091719 09/17/2019 320-54536-2PFMOAA0.080 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLPage 10 of 11 The preparation hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidation Options:Validation ReasonFayettevilleSite:Sampling Program:Creeks Seeps Old Outfall 002 9/19AnalyticalMethodAnalyteDateSampledPQLValidationQualifierLab Sample IDPre-prepMDLResult TypeField Sample IDPrepUnitsCFR-BLADEN-091819 09/18/2019 320-54536-4Hfpo Dimer Acid0.039 UG/L537 ModifiedJ3535_PFC0.0040PQLOUTFALL 002-091719 09/17/2019 320-54536-2Hfpo Dimer Acid0.081 UG/L537 ModifiedJ3535_PFC0.0040PQLSEEP D-1-091719 09/17/2019 320-54536-1Hfpo Dimer Acid16 UG/L537 ModifiedJ3535_PFC0.14PQLPage 11 of 11