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6301_MooreCounty_MSWLF_CDLF_Oct2021GW_FID1628681_20220105
Electronic Data - Email CD (data loaded: Yes / No ) Doc/Event #: NC DENR I I Environmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. • Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): S&ME, Inc. (Consultant for Moore County) Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Edmund Q.B. Henriques Phone: 336-288-7180 E-mail: ehenriques@smeinc.com NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) Moore County Landfill 456 Turning Leaf Way, 63-01 .0500 October 18-19, 2021 Aberdeen, North Carolina 28315 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring �x Detection Monitoring Assessment Monitoring x❑ Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells ❑ Groundwater monitoring data from private water supply wells x❑ Leachate monitoring data ❑ Surface water monitoring data Methane gas monitoring data Corrective action data (specify) Monitored Natural Attenuation Data Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. x Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Edmund Q.B. Henriques, PG Senior Geologist / S&ME, Inc. 336-312-3330 Facility Representative Name (Print) Title (Area Code) Telephone Numb�ywQvo, rare; 01/05/2022 Affix NC LicQ6s�dL'pr6feiAighi kVVdglogist Seal Signature 0 Date 8646 W. Market Street, Suite 105, Greensboro NC 27409 Facility Representative Address F-0176 NC PE Firm License Number (if applicable effective May 1, 2009) D,, A-4 ai,)nnn a¢� pry. -.. •.••�d c ®: V d = Se,�m M 4 L 2% Pk spy`, ��AR.,e;a &u tkC%6®�6cb L3 PREPARED FOR: Moore County Solid Waste P.O. Box 1927 Carthage, North Carolina 28327 S&ME, Inc. 8646 West Market Street, Suite 105 Greensboro, North Carolina 27409 January 5, 2022 =0 January 5, 2022 Moore County Solid Waste Department P.O. Box 1927 Carthage, North Carolina 28327-1927 Attention: Mr. David Lambert Solid Waste Director via email: dlambert1 @moorecountync.gov Reference: Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 Dear Mr. Lambert: S&ME, Inc. (S&ME) is pleased to submit this report documenting water quality monitoring conducted between October 18, 2021 through October 19, 2021 at the Moore County Solid Waste Facility located in Aberdeen, North Carolina. These services have been performed in general accordance with S&ME Proposal No. 43-2000335Rev1, dated August 3, 2020. One copy of this report is attached for your file and one copy has been delivered electronically on your behalf directly to the North Carolina Department of Environmental Quality - Division of Waste Management, Solid Waste Section. S&ME appreciates the opportunity to provide environmental services to Moore County. Please call us if you have any questions or comments. Sincerely, S&ME, Inc. 4 Edmund Q.B. Henriques, P.G. Senior Geologist/Project Manager ehenriques@smeinc.com Samuel P. Watts, P.G. Senior Environmental Consultant swatts@smeinc.com Jaclynne Drummond, Hydrogeologist, Solid Waste Section, Division of Waste Management, NC DEQ, 2090 US Highway 70, Swannanoa, NC 28778, jaclynne.drunnnnond@ncdenr.gov (electronic copy) Jimmy Brown, Landfill Manager, NC, 5227 Hwy 15-501, P.O. Box 1927, Carthage, North Carolina, 28327 (hard copy & electronic copy) S&ME, Inc. 18646 W. Market St, Ste 105 1 Greensboro, NC 27409 1 p 336.288.7180 1 www.smeinc.com Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 Table of Contents 1.0 Executive Summary..........................................................................................................2 2.0 Background and Compliance History...........................................................................4 2.1 Background.....................................................................................................................................4 2.2 Compliance History....................................................................................................................... 5 3.0 Methods Employed...........................................................................................................8 3.1 Groundwater Sampling.................................................................................................................8 3.2 Surface Water Sampling................................................................................................................9 4.0 Site Hydrogeology............................................................................................................9 4.1 Groundwater Elevations and Flow Direction............................................................................ 9 4.2 Groundwater Flow Velocity.........................................................................................................9 5.0 Analytical Results...........................................................................................................10 5.1 Groundwater Analytical Data - MSW Landfill........................................................................11 5.2 Groundwater Analytical Data - C&D Landfill........................................................................12 5.3 Groundwater Analytical for Monitored Natural Attenuation Parameters ..........................13 5.4 Groundwater Analytical - Private Water Well........................................................................13 5.5 Surface Water Analytical Data...................................................................................................13 5.6 Quality Control.............................................................................................................................14 6.0 Discussion of Results.....................................................................................................15 7.0 References.........................................................................................................................15 List of Figures Figure 1 Groundwater Elevations and Contours - October 2021 Monitoring Event List of Tables Table 1 Active Monitoring Well Construciton Information Table 2 Groundwater Elevation Data Table 3 Groundwater Field Parameter Data Table 4 Groundwater Conductivities, Gradients, and Flow Velocities Table 5 Groundwater Monitoring Analytical Results (Detected Constituents) Table 6 Surface Water Monitoring Analytical Results (Detected Constituents) Appendices Appendix I -Sampling Forms Appendix II - Laboratory Analytical Reports Appendix III - Historical Analytical Results Appendix IV - Time vs Concentration Charts January 5, 2022 1 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 1.0 Executive Summary Between October 18 and October 19, 2021, sixteen monitoring wells and four surface water locations which monitor the Moore County Solid Waste Facility were sampled as part of the first semi-annual monitoring event for 2021. Monitoring wells MW-1, MW-2, MW-3, MW-4, MW-5, MW-6, MW-7, MW-8, MW-9, MW-11SR, MW-11DR, MW-13SR, MW-13DR, MW-14, MW-15R, MW-17S, MW-17D, MW-18 and MW-19 comprise the groundwater monitoring system for the closed municipal solid waste (MSW) landfill and active Construction & Demolition (C&D) landfill. The off -site water supply well at the Blake Residence was sampled in accordance with the approved Water Quality Monitoring Plan. Samples were collected from surface water locations SW-1, SW-2, SW- 3, and SW-4. Groundwater and surface water sampling was conducted according to North Carolina Department of Environmental Quality, Division of Waste Management, Solid Waste Section (NCDEQ-SWS) guidelines. Samples were analyzed by a North Carolina certified laboratory. Samples collected were submitted for analysis in accordance with the facility's current NCDEQ-SWS approved Water Quality Monitoring Plan. Analyses of surface water samples collected detected no target constituent at a concentration exceeding the corresponding 15A NCAC 2B Standards (213 Standards). 1,4-Dioxane was detected at surface water sample locations SW-1, SW-3, and SW-4 at concentrations greater than the corresponding North Carolina In -Stream Target Value for Surface Waters set at 0.35 micrograms per liter (pg/L) for Class WS (I-V) surface waters; however, no surface water standard promulgated by 15A NCAC 2B (213 Standard) currently exists for 1,4- Dioxane. The table below summarizes the MSW landfill monitor well locations where target constituents were detected at concentrations greater than the corresponding 15A NCAC 2L Groundwater Standards (2L Standards) or NCDEQ- SWS Groundwater Protection Standards (GWPS) during the October 2021 monitoring event: October 2021 Groundwater Sampling Event - MSW Landfill Monitoring Wells Constituent Concentrations Detected Greater Than 2L Standard or GWPS MParameter 2L Standards or GWPS MW-2 MW-4 MW-6 MW-7 MW-8 MW-9 1,4-Dioxane 3 25 6.3 48 34 Benzene 1 1.6 1.1 2.1 2.2 Vinyl Chloride 0.03 1.2 1.6 Arsenic 10 43.9 Iron 300 1,130 Note: All concentrations are in micrograms per liter. Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. The 2L Standard exceedances for volatile organic compounds (VOCs) summarized above are generally consistent with historic monitoring results, which previously triggered regulatory requirements for implementation of Corrective Measures for the MSW landfill. In 2018, the NCDEQ-SWS requested all MSW and C&D landfills begin January 5, 2022 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 ! to analyze groundwater samples for 1,4-Dioxane. Thus, the number of observations for this parameter at the facility is currently limited. The table below provides a summary of the C&D landfill monitor well locations where target constituents were detected at concentrations greater than the 2L Standard or GWPS during the October 2021 monitoring event: October 2021 Groundwater Sampling Event - C&D Landfill Monitoring Wells Constituent Concentration Detected Greater Than 2L Standard or GWPS Parameter 2L Standards or GWPS MW- 11SR MW- 11DR MW- 13SR MW- 13DR MW- 14 MW- 17S MW- 17D MW- 18 MW- 19 1,4- Dioxane 3 5.1 3.9 9.2 3.3 17 3.4 7.1 13 Benzene 1 2.6 1.9 1.7 Vinyl Chloride 0.03 3.1 2.3 2.6 1.8 Iron 300 88,200 72,500 58,600 8,430 136,000 48,700 2,200 93,400 305 Manganese 50 259 156 560 71.8 176 181 154 Note: All concentrations are reaorted in microarams Der liter. Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. The above listed exceedances are generally similar to the prior monitoring event, with the exception of 1,4- Dioxane at monitoring well MW-19, located adjacent to the western property line. The concentration for this event was less than the corresponding 2L Standard. It is noteworthy that in late 2020, Moore County initiated negotiations with the adjoining property owner Hope Wilson, proposing a land swap that would increase Moore County's land ownership in the area immediately west of the C&D landfill, west of monitoring wells MW-18 and MW-19. The land swap will increase the potential to delineate groundwater constituents of concern on property owned by the County, should that become necessary. An informal agreement was reached between the Moore County and Hope Wilson, to divide properties for a land swap. In November 2021, the Moore County Board of Commissioners adopted a resolution authorizing the land swap agreement, whereby Moore County would receive a portion of Parcel ID 00057409 from Hope Wilson and Hope Wilson would receive a portion of Parcel ID 00053332 from Moore County. Land surveyors have completed the survey work associated with the land swap. A closing date for the land swap has not been established. The Alternate Source Demonstration (ASD) prepared by Golder dated, February 28, 2017, indicated that VOCs detected in certain C&D landfill monitoring wells were attributed to the MSW landfill. NCDEQ-SWS responded indicating that they would not approve the ASD for VOCs at the C&D Landfill, at that time. NCDEQ-SWS requested that Moore County implement landfill gas and groundwater corrective action at the closed MSW landfill; and commence assessment monitoring at the C&D landfill pursuant to 15A NCAC 13B .0545. January 5, 2022 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 In response to the NCDEQ-SWS request, Moore County commenced with assessment monitoring at the C&D Landfill. At the MSW landfill, a methane cut-off trench was installed in 2018. Solar flares were added to the cut-off trench vents during early 2020. Monitored Natural Attenuation (MNA) was the selected groundwater remedy for the closed MSW landfill. MNA "Performance Monitoring" continues at MSW wells and select C&D wells. Benzene and vinyl chloride in the vicinity of the MSW landfill generally exhibit trends of stable or declining concentrations over time, with a few exceptions. Concentrations of these constituents are not increasing immediately down -gradient of the source area. Due to prior exceedances of the 2L Standard for benzene at monitoring well MW-18, concentration trends overtime will be reexamined during each subsequent monitoring event, to better understand the nature and extent of benzene, west of the C&D landfill. The size of the analytical data set for 1,4-dioxane is currently insufficient for accurate trend analysis. Considering constituent concentration trends, Moore County plans to continue Assessment Monitoring for the C&D landfill and MNA monitoring of the closed MSW landfill; unless evidence of increasing VOCs concentrations are confirmed or unless Moore County is directed by NCDEQ to proceed to the alternate groundwater remedy. Moore County is proactively evaluating options for alternate groundwater corrective actions that may be appropriate for the CAP contingency plan, including options that would aid in the management of landfill gases, which can contribute to groundwater exceedances. In 2021, S&ME assessed thickness of the soil cover system for the MSW landfill. An analysis of landfill settlement and changes needed to increase positive surface drainage off the cover system is pending. It is believed that some focused maintenance of the cover system should reduce surface infiltration of water through the soil cover system and result in reduced landfill gas production. Plans for possible pilot tests designed to assess facility improvements that enhance management of landfill gas are forthcoming. 2.0 Background and Compliance History 2.1 Background Moore County currently operates a solid waste facility at 456 Turning Leaf Road, in Aberdeen, North Carolina. The facility is owned and operated by Moore County under Solid Waste Permit No. 63-01 issued by the NCDEQ-SWS. The facility includes a municipal solid waste (MSW) transfer facility, a closed unlined MSW landfill and an active C&D landfill unit. The C&D landfill unit and closed MSW landfill are regulated in general accordance with NCDEQ-SWS Permit No. 63-10. Moore County performs groundwater and surface water monitoring on a semiannual basis to comply with the requirements of North Carolina Solid Waste Management Rules (Solid Waste Rules), 15A NCAC 13B. S&ME has prepared this report on behalf of Moore County to present the results of the second monitoring event for 2020 as required by § .0600 and .1632 of the Solid Waste Rules. The Golder Associates NC, Inc. (Golder), Water Quality Monitoring Plan — Moore County Landfill, Permit No. 63-10, Volume 2 — Moore County Design Hydrogeological Report and Monitoring Plans (WQMP) dated December 10, 2019, is the current NCDEQ approved WQMP. Based on the WQMP there are two groundwater compliance well networks, with one background monitoring well providing background data for both networks. January 5, 2022 4 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - • The active C&D landfill groundwater monitoring network consists of nine downgradient monitoring wells (MW-4, MW-11SR, MW-11DR, MW-13SR, MW-13DR, MW-14, MW-171D, MW-18 and MW-19). One monitoring well (MW-5) is shared by both the C&D landfill and MSW landfill for monitoring background groundwater quality. • The closed MSW landfill groundwater monitoring network consists of eight downgradient monitoring wells (MW-1, MW-2, MW-3, MW-6, MW-7, MW-8, MW-9 and MW-15R). In addition, two C&D monitoring wells (MW-4, MW-11 SR) are also used as MNA performance monitoring wells to assess groundwater impacts from the MSW landfill. The groundwater monitoring wells represent conditions in the uppermost aquifer underlying the facility, positioned for detection of potential releases from the landfill units; with some wells employed to assess the efficacy of natural attenuation as a corrective measure. Monitoring wells with "D" suffixes to the well identifier, represent wells screened within deeper portions of the surficial aquifer. The WQMP also involves four stream sample locations, one located on Horse Creek upstream of the facility and three sample locations at points downstream of the facility. One private water supply well on a parcel located east of the facility, the Blake residence well, was monitored in accordance with the approved WQMP. The C&D landfill is currently in Assessment Monitoring. The MSW landfill is currently in Corrective Action Monitoring, which includes MNA performance monitoring parameters for most monitoring wells. 2.2 Compliance History Groundwater quality has been monitored at the facility since 1987. Monitoring wells MW-1 through MW-4 monitored down -gradient regions of the MSW landfill, with MW-5 providing background water quality data for the facility. In March 1995, monitoring wells MW-6 through MW-9 were added to monitor the area between the MSW and the C&D landfill. An NCDEQ-SWS letter dated January 23, 1996, presented initial concerns regarding a potential for off -site migration of VOCs from the facility. Moore County voluntarily initiated corrective measure due to concerns of off - site migration of VOCs in groundwater and measured methane gas concentrations. In 1996, the off -site water supply well at the Blake residence (PW-1) was added to the groundwater monitoring program and monitoring of surface water points SW-2 and SW-1, commenced. Additional groundwater monitoring wells (MW-11 S, MW-11 D, MW-125, MW-12D, MW-135, MW-13D, and MW-14) were installed to assess the extent of groundwater impacts, establish monitoring points for the C&D facility, and to collected data to attempt differentiation of MSW groundwater impacts from C&D landfill impacts. Subsequently, monitoring wells MW12S and MW-12D were abandoned due to planned expansion of the C&D landfill, and replaced by monitoring wells MW-16S and MW16D, located further west and downgradient. In November 1999, HDR Engineering Inc. of the Carolinas (HDR) submitted a Work Plan to further investigate groundwater and methane migration concerns, with assessment activities commencing in March 2000. HDR reported the existence of a clay confining unit at depth beneath the landfill, which was reported to limit vertical groundwater contamination. In January 2005, NCDEQ-SWS requested that Moore County complete an assessment of corrective measures and select a remedy in accordance with 15A NCAC 2L .0106. In July 2005, HDR submitted the Assessment of Corrective Measures Report (ACM) to NCDEQ recommending monitored natural attenuation (MNA) as the primary remedy, January 5, 2022 5 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 with a contingency plan for active landfill gas (LFG) remediation if trends of increasing VOC concentrations over time were observed in groundwater. On November 21, 2005, NCDEQ-SWS approved HDR's ACM. In 2005, a shallow trench vent network consisting of a trench and 12 passive LFG vents were installed to address LFG migration concerns. In 2007, the LFG vent network was expanded with the addition of 12 passive LFG vents. In February 2014, three in -waste passive gas vent wells (GV-30, GV-31, and GV-32) were installed as part of the Joyce Engineering, Inc. Contingency Plan Update and Implementation Plan -Revised approved by NCDEQ-SWS on June 5, 2013. HDR prepared a revised Water Quality Monitoring Plan dated July 20, 2006, which was approved by NCDEQ-SWS on October 13, 2006. The 2006 plan involved monitoring all groundwater and surface water monitoring points for North Carolina Appendix I VOCs and the eight Resource Conservation and Recovery Act (RCRA) metals. MNA parameters were added for "performance monitoring" at select wells. In a letter from the NCDEQ-SWS dated April 18, 2008, NCDEQ-SWS agreed to the elimination of hydrogen, carbon dioxide, and volatile fatty acids from the semi-annual monitoring list, and to the completion of groundwater MNA modeling annually. This letter also specified that Moore County collect the full suite of "performance monitoring parameters" in April and October 2011, and present an MNA Corrective Action Evaluation Report (CAER) after completion of the October 2011 sampling event. Golder submitted a CAER report dated May 15, 2012. Subsequently, NCDEQ-SWS granted Moore County permission to continue MNA for another five-year period at the end of which another CAER report was required. Two additional surface water points (SW-3 and SW-4) were added to the compliance monitoring program upon approval of the May 2012 CAER. On March 10, 2016, Moore County met with NCDEQ-SWS to discuss groundwater impacts at the site and the effectiveness of previously implemented corrective actions. In this meeting and in a March 14, 2016, correspondence from NCDEQ-SWS, Moore County was asked to commence assessment monitoring at the C&D landfill or submit an alternate source demonstration (ASD) to demonstrate the impacts observed in the C&D landfill monitoring network were from a source other than the C&D landfill. On behalf of Moore County, Golder submitted the ASD for the Active C&D Landfill, dated February 28, 2017, identifying the upgradient closed MSW landfill as the source of VOCs at downgradient C&D wells. In two letters dated September 28, 2017, the NCDEQ-SWS indicated that they would not approve the ASD for VOCs at the C&D Landfill, at that time. They also requested that Moore County implement landfill gas and groundwater corrective action at the closed MSW landfill; and commence assessment monitoring at the C&D landfill pursuant to 15A NCAC 13B .0545. On December 6, 2017, after additional communications and a meeting with NCDEQ-SWS, Moore County submitted a letter confirming their intention to comply with the NCDEQ-SWS requests and requested an extension to comply, which was approved by NCDEQ-SWS on December 11, 2017. On behalf of Moore County, Golder submitted: A CAER dated October 16, 2017, An Assessment Monitoring Work Plan, dated January 5, 2018. A Landfill Gas Remediation Plan dated January 31, 2018, A Groundwater Corrective Action Milestone Schedule, dated January 31, 2018 (which included the submission of the NC Solid Waste .0500 Groundwater Corrective Action Application), and January 5, 2022 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - In accordance with Golder's Assessment Monitoring Work Plan, dated January 5, 2018, monitoring wells MW-11 SR, MW-11 DR, and MW-15R were subsequently installed to replace monitoring wells MW-11 S, MW-11 D, and MW-15. The replacement wells were sampled in June 2018, as part of the first assessment monitoring event for the C&D landfill. Groundwater samples collected from assessment monitoring wells were analyzed for constituents listed in North Carolina Appendix II and the C&D landfill indicator parameters required by NCDEQ-SWS (e.g., chloride, manganese, sulfate, iron, alkalinity, total dissolved solids (TDS), and tetrahydrofuran). Samples from monitoring wells MW-6 and MW-7 were also analyzed for Appendix II constituents, to further assess whether the groundwater impacts detected at the C&D landfill were attributable to the upgradient MSW landfill. In a letter dated February 22, 2018, NCDEQ approved a request made by Moore County to decommission monitoring wells MW-16S and MW-16D and replace them in the groundwater monitoring network with MW-175, MW-17D, and MW-18 which were to be installed in conjunction with the permitting of new Cell VI of the C&D landfill. Between May 31 and June 4, 2018, monitoring wells MW-175, MW-17D, and MW-18 were installed, and monitoring wells MW-16S and MW-16D were properly abandoned. Monitoring wells MW-17S and MW-17D were first sampled during the routine semi-annual monitoring event conducted during November 2019. Monitoring well MW-18 was first sampled during the routine semi-annual monitoring event conducted in April 2020. During the April 2020 water quality monitoring event, groundwater monitoring was conducted at the closed MSW landfill in accordance with the approved Water Quality Monitoring Plan and Phase I of the Groundwater Corrective Action Milestone Schedule which was approved by NCDEQ-SWS on February 13, 2018. Phase I of the Groundwater Corrective Action Milestone Schedule included the following activities: Installation of the methane cut-off trench to the south of MW-15 (completed November 2, 2078) Replacement of MW-15 with MW-15R (completed June 7, 2078) Conversion of MW-15 to a compliance methane monitoring well (completed December 7, 2018) Continuation of MNA (as detailed in the approved Water Quality Monitoring Plan) In accordance with the approved Water Quality Monitoring Plan, dated December 10, 2019, hereafter referred to as the WQMP, monitoring wells in the MSW compliance network are corrective action MNA monitoring wells and are currently analyzed for VOCs listed in North Carolina Appendix I, RCRA metals, and an approved suite of MNA parameters (which includes chloride, ethane, ethene, methane, nitrate, sulfate, sulfide, total alkalinity, and total organic carbon). In addition, active C&D monitoring wells MW-4, MW-5, and MW-11SR are also sampled as corrective action MNA monitoring wells and analyzed for the same suite of MNA parameters. Analytical results for the April 2020 water quality monitoring event detected benzene at a concentration of 1.6 pg/L in monitoring well MW-18. Based on this apparent exceedance of the corresponding 2L Standard, a verification sampling event was conducted on June 5, 2020, with laboratory analyses reporting 1.2 pg/L Benzene. Based on the verified exceedance of the 2L Standard for benzene, an update of the Assessment Monitoring Program was required. On June 26, 2020, new monitoring well MW-19 was installed down -gradient (in the direction of contaminant migration) of monitoring well MW-18, near the facility boundary. Monitoring well MW- 19 was first sampled during the October 2020, then monitored semi-annually thereafter. The October 2021 monitoring event represents the second semi-annual water quality monitoring event for the facility in 2021. The event was conducted in general conformance with the WQMP, with the addition of sampling monitoring well MW-19, and analyzing the samples for North Carolina Appendix II constituents. January 5, 2022 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - 3.0 Methods Employed 3.1 Groundwater Sampling Groundwater sampling took place on October 18 and October 19, 2021. The groundwater monitoring well locations are shown on Figure 1. S&ME personnel performed sampling in general accordance with the facility's updated WQMP. Groundwater samples were collected from monitor wells MW-2, MW-3, MW-6, MW-7, MW-8, MW-9, and MW-15R representing the closed MSW landfill. Monitoring wells MW-4 and MW-11SR represent C&D monitoring wells also monitored as MNA performance wells for the MSW landfill. Monitoring wells MW-11 DR, MW-13SR, MW-13DR, MW-14, MW-175, MW-17D, MW-18, and MW-19 represent the active C&D landfill. Monitoring well MW-5 was sampled as the background well for both landfills. A groundwater sample was obtained the off -site water supply well located on the Blake property. Details regarding monitoring well construction and monitored aquifer units are shown in Table 1. Prior to collecting groundwater samples, the monitor wells were opened and allowed to equilibrate with atmospheric conditions before gauging the liquid level. Groundwater depths were measured to an accuracy of ±0.01 feet using an electronic water level indicator, which was decontaminated before its initial use and between measurements. The measurements were collected to calculate relative groundwater elevations, to develop a groundwater potentiometric map, and to estimate the hydraulic gradient and groundwater flow direction at the time of the sampling event. Water level measurements are presented in Table 2 and Figure 1. After collection of groundwater levels, low -flow sampling methods were followed to purge and sample groundwater from the monitoring wells. As purging proceeded, an YSI ProPlus0 multi -meter with a flow -through cell was used to measure field parameters that included pH, temperature, specific conductance, oxidation- reduction potential (ORP), and dissolved oxygen (DO). Turbidity was measured separately. The field data collected during sampling was recorded on the Low -Flow Groundwater Sampling Forms, included in Appendix I. A groundwater sample, for laboratory analysis, was collected after field parameters stabilized and the turbidity measurement was approximately 10 Nephelometric Turbidity Units (NTUs) or less. In accordance with the WQMP, water quality field parameters are considered stable once achieved for three consecutive measurements: Ph (+/- 0.2 S.U.), conductivity (+/- 5% of reading), temperature Ph (+/- 0.2 CO), and dissolved oxygen (+/- 10% of reading or 0.2 mg/L whichever is greater). ORP was measured and should fall within +/- 10 mV or reading; however, it was not a required stabilization parameter. Even with use of low -flow sampling methods, turbidity values obtained at some wells remained higher than target criteria. Accordingly, some samples were collected without meeting the turbidity goal. The field parameter measurements obtained are presented in Table 3. Groundwater samples from monitoring wells were collected using a peristaltic pump or bladder pump, and transferred directly into sample containers provided by the laboratory. Once filled, the sample containers were sealed, labeled, and placed in a cooler with ice. The samples were managed under chain -of -custody protocols and shipped to Environmental Conservation Laboratories, Inc. (ENCO), a North Carolina -certified laboratory. One blind duplicate sample and one equipment blank sample were collected for quality assurance and quality control (QA/QC). One trip blank accompanied each laboratory package under standard chain -of -custody procedures delivered from the laboratory and returned to the laboratory. Samples were stored in laboratory January 5, 2022 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - provided coolers with ice immediately after collection. The samples were delivered to ENCO, a NCDEQ certified laboratory for analysis. The samples were maintained under chain -of -custody procedures through delivery to the laboratory. 3.2 Surface Water Sampling Surface water sampling took place on October 19, 2021. Four surface water samples (SW-1, SW-2, SW-3, and SW- 4) were collected from the locations shown in Figure 1. Sample SW-2 was collected from Horse Creek northwest of the C&D landfill, and upstream of the facility. Downstream sample SW-1 was collected from an unnamed tributary of Horse Creek, south of the MSW landfill. Sample SW-3 was collected downstream of SW-1, prior to the tributary discharging into Horse Creek. Sample SW-4 was collected from an unnamed tributary that drains areas north of both the C&D and MSW landfills. After collection, surface water samples were placed in a cooler with ice, placed under chain -of -custody, and submitted for laboratory analyses for North Carolina Appendix I constituents and 1,4-Dioxane. 4.0 Site Hydrogeology 4.1 Groundwater Elevations and Flow Direction The facility is situated within the Inner Coastal Plain Province of North Carolina. The uppermost aquifer beneath the facility is unconfined, approximately 55 feet thick, and consist of sands with thin clay seams, and seams of fine sand; reportedly underlain by a basal restrictive clay layer. The surficial aquifer is recharged by inflow from up - gradient areas and by precipitation infiltration. The uppermost aquifer underlying the landfill is expected to discharge to the local surface water features including Horse Creek and it's unnamed tributaries in the vicinity of the landfill. Shallow monitoring wells were installed in the surficial aquifer. Table 1 summarizes the well construction details for the facility's groundwater monitor wells. Static water level measurements collected during the October 2021 monitoring event (Table 2) were used to calculate the corresponding groundwater elevations based on surveyed top of casing (TOC) elevations. Groundwater elevations for the shallow water table monitoring wells and our interpretation of the groundwater surface expressed as a potentiometric map along with estimated groundwater flow directions shown on Figure 1. Based upon the groundwater potentiometric surface elevations, the overall shallow groundwater flow direction was estimated to be to the west. The hydraulic gradient (i) in the vicinity of a monitoring well was estimated by calculating the vertical difference between the groundwater elevation at a monitoring well and one or more nearby contour lines from Figure 1. This value was then divided by the horizontal distance measured from the well to the selected groundwater elevation contour line, utilizing a line formed perpendicular to the referenced groundwater elevation line. The calculated horizontal hydraulic gradient values determined for select wells are summarized in Table 4. 4.2 Groundwater Flow Velocity An approximate average linear groundwater flow velocity (V) was calculated using the following equation (Freeze and Cherry, 1979): January 5, 2022 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - V=Ki n where: V = Average linear groundwater flow velocity [feet per year (ft/yr.)] K = Hydraulic conductivity (ft/yr.) i = Flow gradient as a ratio (ft/ft) n = Effective soil porosity (percent) Aquifer rising and falling head tests were previously performed at the site by HDR. The aquifer test data were used to estimate the hydraulic conductivity of the sediments in the surficial aquifer intersected by the screened intervals of the monitoring wells tested. The hydraulic conductivity, K, values previously measured at the site ranged from 0.84 feet per day (feet/day) to 16 feet/day. An average hydraulic conductivity value of 12.2 feet/day was used for calculating the site -wide flow velocity. The average hydraulic gradient of 0.01' ft/ft was calculated from data presented in Table 4. An effective soil porosity, n, of 25% was used as the site -wide average. The average groundwater flow velocity, V, for the site, using the equation and input values above, was estimated to be 291 feet/year. The average groundwater flow velocity information is summarized in Table 4. 5.0 Analytical Results In general accordance with the WQMP, background and compliance groundwater monitor wells were sampled during the October 2021 sampling event. The samples were analyzed by ENCO as follows: MSW landfill groundwater samples from monitoring wells MW-2, MW-3, MW-4, MW-6, MW-7, MW-8, MW-9 and MW-15R were analyzed for constituents listed in the 40 CFR 258, Appendix I VOC analyte list using the analytical methods that included EPA Method 826013, 1,4-Dioxane by EPA Method 8260D SIM, the Eight RCRA Metals using EPA Method 6010/6020 and EPA Method 7470A. Analyses for MNA parameters included chloride by EPA Method 300.0, nitrate by EPA Method 353.2, nitrite by EPA Method 353.2, sulfate by EPA Method 300.0, sulfide by EPA Method 300.0, Total Alkalinity by EPA Method 310.2, and Total Organic Carbon by EPA Method 9060A. Carbon Dioxide, Ethane, Ethene, and Methane by RSK 175. The active C&D landfill groundwater samples from monitoring wells MW-11 SR, MW-11 DR, MW-13SR, MW-13DR, MW-14, MW-17D, MW-18, and MW-5 were analyzed for constituents listed in the 40 CFR 258, Appendix I analyte list using analytical methods EPA Method 8260B (VOCs), total metals by EPA Method 6010, 6020 and EPA Method 7470A. Classic chemistry indicator parameters chloride by EPA Method 300.0, sulfate by EPA Method 300.0, sulfide by SM 4500S2-D-2011, Total Alkalinity by EPA Method 310.2 and Total Dissolved Solids by Method SM 2540-C2011. Plus 1,4-Dioxane by EPA Method 8260D SIM. The active C&D landfill groundwater sample from monitoring well MW-19 was analyzed for constituents listed in the 40 CFR 258, Appendix II analyte list using analytical methods EPA Method 8260D (VOCs), EPA Method 8270E (SVOCs), EPA Method 8081B (pesticides), EPA Method 8082A (PCBs), EPA Method 8151A (herbicides), total metals by EPA Method 6010, 6020 and EPA Method 7470A. Classic chemistry indicator parameters chloride by EPA Method 300.0, sulfate by EPA Method 300.0, sulfide by SM 4500S2-D-2011, Total Alkalinity by EPA Method 310.2 and Total Dissolved Solids by Method SM 2540-C2011. Plus 1,4- Dioxane by EPA Method 8260D SIM. January 5, 2022 10 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 In addition, two C&D monitoring wells (MW-4, MW-11SR) are also used as MNA performance monitoring wells to assess groundwater impacts from the MSW landfill. The field measurements obtained are summarized on Table 3. A summary of constituents detected in groundwater is presented in Table 5. For comparison purposes, these results are shown with their respective 2L Standard, which were revised and became effective April 1, 2013. Where target groundwater constituents have no established 2L Standard, the Method Detection Limit (MDL) is the default 2L Standard. However, the NCDEQ-SWS has listed constituent concentrations protective of groundwater, referred to as the Ground Water Protection Standards (GWPS) established in accordance with the Solid Waste Management Rules, Section .1634(h), which are used as the action level for detections where no 2L Standard is established. The chain -of -custody forms and the laboratory reports from ENCO are provided in Appendix II. Copies of the laboratory reports are provided in Appendix II. Effective December 1, 2006, NCDEQ-SWS changed the standard limits for comparing constituent detections in laboratory analysis from the Practical Quantitation Limits (PQLs) established in 1994 to the Solid Waste Reporting Limits (SWRLs). On February 23, 2007, the Section further revised the reporting limits from the SWRL to the Solid Waste Section Limit (SWSL). The SWSL was defined as the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy. In a memo dated May 29, 2018, the NCDEQ-SWS made a statement that technologies have advanced such over the past 12 years that the majority of the SWSLs are outdated. Given the rapid pace of technology, the NCDEQ- SWS decided that their attempt to continuously update and/or maintain the SWSLs is not warranted. As such, the use of SWSLs will be discontinued. According to the laboratory quality control performed by ENCO, detections above the MDL but below the PQL qualified as estimated values designated by the letter "J". 5.1 Groundwater Analytical Data - MSW Landfill The analytical data was reviewed by comparing constituent detections in the background and MSW compliance monitor wells to the laboratory's MDL. Multiple targeted constituents were detected above the MDL in one or more groundwater samples collected during the October 2021 monitoring event. Constituents with concentrations detected above the laboratory MDLs are summarized on Table 5. Appendix III contains a table providing historic groundwater analytical results for constituents with concentration detected above the MDL. The following table provides a summary of the monitoring well locations where target constituents were detected at concentrations greater than the 2L Standard or GWPS during the October 2021 monitoring event: January 5, 2022 11 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina I S&ME Project No. 4358-20-043A, Task 01 ! October 2021 Groundwater Sampling Event Constituent Concentrations Detected Greater Than 2L Standard or GWPS Parameter 2L Standards or GWPS MW-2 MW-4 MW-6 MW-7 MW-8 MW-9 1,4-Dioxane 3 25 6.3 48 34 Benzene 1 1.6 1.1 2.1 2.2 Vinyl Chloride 0.03 1.2 1.6 Arsenic 10 43.9 Iron 300 1,130 Note: All concentration are in microarams oer liter. Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. In accordance with NCDEQ-SWS guidance, where the 2L Standard or GWPS for a substance is less than the PQL, the detection of that substance at or above the PQL constitutes a violation of the 2L Standard or GWPS. The table above was prepared using this framework, which eliminates constituents reported with estimated concentrations ("J" values). Monitoring well MW-4 is located down -gradient of the MSW landfill and immediately upgradient of the C&D landfill. Monitoring well MW-4 is analyzed for the list of constituents applicable to the C&D landfill, to provide background groundwater quality data for the C&D landfill. Iron and manganese are very common constituents in coastal plain sediment; thus, they are naturally occurring in groundwater. The 2L Standard exceedances for the VOCs summarized above are generally consistent with prior detections, several of which historically triggered regulatory requirements for implementation of Corrective Measures for the MSW landfill. In 2018, the NCDEQ-SWS requested that all MSW and C&D landfills begin to analyze samples for 1,4-Dioxane. Thus, historic data for detections of this parameter at the landfill are limited. Appendix IV contains time vs concentration charts for benzene, vinyl chloride, and 1,4-Dioxane. These charts were prepared to examine trends in concentration changes overtime. 5.2 Groundwater Analytical Data - C&D Landfill The analytical data was reviewed by comparing constituent detections in the background and C&D landfill compliance monitor wells to the laboratory's MDL. Multiple targeted constituents were detected above the MDL in one or more groundwater samples collected during the October 2021 monitoring event. Constituent concentrations detected above the laboratory MDLs are summarized on Table 5. Appendix III contains a table providing historic groundwater analytical results for constituents with concentration detected above the MDL. The table below provides a summary of the monitor well locations where target constituents were detected at concentrations greater than the 2L Standard or GWPS during the October 2021 monitoring event: January 5, 2022 12 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 October 2021 Groundwater Sampling Event Constituent Concentration Detected Greater Than 21, Standard or GWPS Parameter 2L MW- MW- MW- MW- MW- MW- MW- MW- MW- Standards 11SR 11DR 13SR 13DR 14 17S 17D 18 19 or GWPS 1,4- 3 5.1 3.9 9.2 3.3 17 3.4 7.1 13 Dioxane Benzene 1 2.6 1.9 1.7 Vinyl 0.03 3.1 2.3 2.6 1.8 Chloride Iron 300 88,200 72,500 58,600 8,430 136,000 48,700 2,200 93,400 305 Manganese 50 259 156 560 71.8 176 181 154 Note: All concentration shown are in micrograms per liter. Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. In accordance with NCDEQ-SWS guidance, where the 2L Standard or GWPS for a substance is less than the PQL, the detection of that substance at or above the PQL constitutes a violation of the 2L Standard or GWPS. The table above was prepared using this framework, which eliminates constituents reported with estimated concentrations ("Y values). Appendix IV contains time vs concentration charts for benzene, vinyl chloride, and 1,4-Dioxane. These charts were prepared to examine trends in concentration changes overtime. 5.3 Groundwater Analytical for Monitored Natural Attenuation Parameters Groundwater analytical results for monitoring wells involved in Performance Monitoring for MNA parameters are summarized in Table S. 5.4 Groundwater Analytical - Private Water Well In accordance with the facility's Water Quality Monitoring Plan, the off -site private water well located on the Blake property to the north of the MSW landfill was sampled during this monitoring event. With the exception of barium, no other target constituents were detected in the sample collected. The detected barium concentration was below the corresponding 2L Standard and likely represents natural background water quality. 5.5 Surface Water Analytical Data Surface water samples were collected from the four designated sample locations illustrated on Figure 1. Horse Creek located west of the landfill is a stream classified by NCDEQ as a WSII, Water Supply. Laboratory analysis of the samples collected were compared to their respective 15A NCAC 2B (revised 6-10-2019) water quality standards for class WS surface waters (213 Standards). Table 6 provides a summary of constituents detected during the October 2021 monitoring event. The following constituents were detected at concentrations greater than their respective 2B Standards during the October 2021 event: January 5, 2022 13 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 October 2021 Surface Water Sampling Event Constituent Concentration Detected Greater Than 2B Standards Sample ID Detected Constituents Above NCAC 2B Standards It is noted that 1,4-Dioxane was detected at surface water sample location SW-1, SW-3, and SW-4, at concentrations of 3.2 pg/L, 3.6 pg/L, and 1.6 pg/L, respectively. These concentrations are greater than the corresponding North Carolina In -Stream Target Value for Surface Waters set at 0.35 pg/L for Class WS (I-V) surface waters; however, no 2B Standards currently exists. 5.6 Quality Control Quality assurance and quality control of field sampling methods and analytical test methods were assessed by collecting and analyzing one duplicate sample, one equipment blank sample, and one trip blank sample. The duplicate and equipment blank samples were analyzed for Appendix I constituents by the same methods and for the same target constituents as the record samples. Duplicate sample analysis documents the consistency of field sampling methods and the consistency of laboratory testing between samples. Equipment blank sample analysis documents the quality of sampling equipment and decontamination procedures used to reduce the potential of cross -contamination or carry-over effects from sampling equipment used on -site. The trip blank is analyzed for VOCs to document the effect of external conditions on samples/sample containers during lab pack preparation and transportation to and from the site. The concentrations of Appendix I VOCs and inorganic compounds detected in the record and in the duplicate samples collected from monitor well MW-15R were within an acceptable tolerance level and indicate a suitable replication of results from the test procedures. No targeted constituents were detected at concentrations above their respective laboratory method detection limits in the equipment blank sample. In the trip blank sample, no targeted constituents were detected above their respective laboratory MDLs. Some technical limitations exist in the laboratory's reporting of MDLs. MDLs for some VOCs and some inorganic constituents are above the applicable standards. The MDL for vinyl chloride (0.32 pg/L), cobalt (1.4 pg/L), and vanadium (1.4 pg/L) in groundwater are greater than the 2L Standard of 0.03 pg/L for vinyl chloride and the GWPSTs of 1.0 pg/L for cobalt and 0.3 pg/L for vanadium. Therefore, vinyl chloride, cobalt, and vanadium may have been present at concentrations above their respective 2L Standard/GWPS, but were reported as being below their respective MDLs. January 5, 2022 14 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - 6.0 Discussion of Results Moore County continues with assessment monitoring at the C&D Landfill. Monitored Natural Attenuation (MNA) is the selected groundwater remedy for the closed MSW landfill monitoring. MNA "Performance Monitoring" continues at MSW wells and select C&D wells. Analytical results of the October 2021 sampling event were generally consistent prior monitoring data, which demonstrated groundwater near the Moore County Landfill had been impacted by a release of waste constituents from the facility. Benzene and vinyl chloride in the vicinity of the MSW landfill generally exhibit trends of stable or declining concentrations over time, with a few exceptions. Concentrations of these constituents are not increasing immediately down -gradient of the source area. The sample size of the groundwater data set for 1,4-dioxane is currently insufficient for reliable trend analysis. Vinyl chloride and 1,4-dioxane detected at monitoring well MW- 18, down -gradient of the C&D landfill, likely originated from the MSW landfill. Following installation of monitoring well MW-18 in 2020, benzene was detected twice at a concentration greater than the 2L Standard; however, it was not detected during the October 2021 event. Due to prior exceedances of the 2L Standard for benzene at monitoring well MW-18, concentration trends overtime will be reexamined during each subsequent monitoring event, to better understand the nature and extent of benzene, west of the C&D landfill. It is noteworthy that benzene and 1,4-dioxane were not detected in C&D landfill monitoring well MW-19, installed immediately down -gradient of MW-18. During this monitoring event 1,4-dioxane was detected in groundwater samples obtained from multiple MSW and C&D monitoring wells. 1,4-dioxane was not detected at monitoring well MW-19, downgradient of MW-18. Furthermore, this monitoring event represent the 3rd consecutive monitoring event where groundwater samples obtained from monitoring well MW-19 were analyzed for the full Appendix II constituent list, to establish a baseline for this well. In consideration of the VOC concentration trends over time, Moore County plans to continue Assessment Monitoring for the C&D landfill and MNA monitoring of the closed MSW landfill; unless evidence of increasing VOCs concentrations are confirmed or unless Moore County is directed by NCDEQ to proceed to the alternate groundwater remedy. Moore County is proactively evaluating options for alternate groundwater corrective actions that may be appropriate for the CAP contingency plan, including options that would aid in the management of landfill gases, which can contribute to groundwater exceedances. 7.0 References Department of Environment and Natural Resources, Division of Water Quality, 75A NC Administrative Code Subchapter 28.0200 Classifications and Water Quality Standards Applicable to Surface Waters and Wetlands of NC, November 2019. Surface Water Standards Tables updated 06-10-2019. Department of Environment and Natural Resources, Division of Water Quality, 75A NC Administrative Code Subchapter 2L .0200 Groundwater Quality Standards, April 2013. January 5, 2022 15 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 Department of Environment and Natural Resources, Division of Waste Management, 75A NC Administrative Code Subchapter 13B .1634(h) Solid Waste Groundwater Protection Standard, Solid Waste Management Rules, November 2004. Golder Associates NC, Inc. (Golder), Alternate Source Demonstration for Active C&D Landfill, Moore County Construction and Demolition Landfill, NC SWP# 63-01, Submitted to NC DEQ: February 28, 2017. Golder Associates NC, Inc. (Golder), Assessment Monitoring Work Plan, Moore County Construction and Demolition Landfill, NC SWP# 63-01, Submitted to NC DEQ: January 5, 2018. Golder Associates NC, Inc. (Golder), Corrective Action Evaluation Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: May 15, 2012. Golder Associates NC, Inc. (Golder), Groundwater Corrective Action Evaluation Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: October 16, 2017. Golder Associates NC, Inc. (Golder), Groundwater Corrective Action Milestone Schedule, Moore County Closed MSW Landfill, NC SWP# 63-01, Submitted to NC DEQ: January 31, 2018. Golder Associates NC, Inc. (Golder), Landfill Gas Remediation Plan, Moore County Closed MSW Landfill, NC SWP# 63-01, Submitted to NC DEQ: January 31, 2018. Golder Associates NC, Inc. (Golder), Request for Extension, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: December 6, 2017. Golder Associates NC, Inc. (Golder), Request for Monitored Natural Attenuation Parameter Modification, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: January 22, 2008. Golder Associates NC, Inc. (Golder), Response to Letters Received from NC DEQ Dated September 28, 2077, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: October 26, 2017. Golder Associates NC, Inc. (Golder), Second Semi -Annual Water Quality Monitoring Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: March 29, 2017. Golder Associates NC, Inc. (Golder), Water Quality Monitoring Plan, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: Submitted to NC DEQ: December 10, 2019. HDR Engineering, Inc. of the Carolinas (HDR), Addendum to Plan to Address Potential Contamination, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: March 20, 2000. HDR Engineering, Inc. of the Carolinas (HDR), Assessment of Corrective Measures Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: July 29, 2005. HDR Engineering, Inc. of the Carolinas (HDR), Phase 1 Environmental Assessment, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: November 30, 1999 January 5, 2022 16 Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - HDR Engineering, Inc. of the Carolinas (HDR), Water Quality Monitoring Plan, Moore County Landfill, NC SWP# 63- 01, Submitted to NC DENR: July 20, 2006. Joyce Engineering, Inc., Contingency Plan Update and Implementation Plan - Revised, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: May 16, 2013. North Carolina Department of Environment, Health, and Natural Resources (NC DEHNR), Division of Solid Waste Management, Water Quality Monitoring at Moore County Sanitary Landfill, Moore County Landfill, NC SWP# 63- 01, NC DEHNR to Moore County: January 23, 1996. North Carolina Department of Environment and Natural Resources (NC DENR), Division of Waste Management, Request for Monitored Natural Attenuation Parameter Modification, Moore County Landfill, NC SWP# 63-01, NC DENR to Moore County: April 18, 2008. North Carolina Department of Environmental Quality (NC DEQ), Solid Waste Section, Division of Waste Management, Alternate Source Demonstration, Moore County Construction and Demolition Landfill, NC SWP# 63- 01, NC DEQ to Moore County: September 28, 2017. North Carolina Department of Environmental Quality (NC DEQ), Solid Waste Section, Division of Waste Management, Groundwater Corrective Action and Landfill Gas Corrective Action, Moore County Closed MSW Landfill, NC SWP# 63-01, NC DEQ to Moore County: September 28, 2017. North Carolina Department of Environmental Quality (NC DEQ), Solid Waste Section, Division of Waste Management, Groundwater Corrective Action Milestone Schedule, Moore County Closed MSW Landfill, NC SWP# 63-01, NC DEQ to Moore County: February 13, 2018. January 5, 2022 17 TABLE 1 Active Monitoring Well Construction Information Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A = 0 III MW-1 OR 06/05/87 & 508605.64 1854636.41 Ground Surface Elevation 390.70 Measuring Point Elevation 392.87 Total Well r- 20 Well Depthinates 370.70 Di:ete 2 Interval 6.97 - 17.07 Interval 383.73 - 373.63 Geology of Screened Interval Sand Monitored Landfill Unit MSW Landfill MW-2 06/06/87 508508.07 1853819.73 373.39 375.50 20 353.39 2 7.52-17.77 365.87 - 355.62 Sand MSW Landfill MW-3 06/06/87 508781.79 1852845.34 362.00 363.82 16.5 345.50 2 5.75 - 15.88 356.25 - 346.12 Sand and Silty Clay MSW Landfill MW-4 06/06/87 509793.80 1853641.22 363.40 366.19 15 348.40 2 4.28 -14.09 359.12 - 349.31 Sand and Silty Clay C&D Landfill MW-5 06/06/87 510970.55 1853091.84 384.06 386.61 20 364.06 2 6.96-17.21 377.10 - 366.85 Sand and Clayey Sand Background MW-6 03/06/95 510385.96 1853881.79 403.50 405.86 20 383.50 2 5.00 - 20.00 398.50 - 383.50 Sand to Silty Sand MSW Landfill MW-7 03/06/95 509783.24 1853820.43 399.20 402.01 20 379.20 2 4.00 - 19.00 395.20 - 380.20 Sand, Silt, Silty Sand, Clay MSW Landfill MW-8 03/06/95 509384.99 1853844.10 395.20 397.85 20 375.20 2 5.00 - 20.00 390.20 - 375.20 Sand, Silt, Silty Sand, Clay MSW Landfill MW-9 03/06/95 508964.80 1854268.28 403.70 406.06 30 373.70 2 15.00 - 30.00 388.70 - 373.70 Silty Sand MSW Landfill MW-11SR 06/01/18 510452.38 1852905.36 383.41 386.13 28 355.41 2 18.00 - 28.00 358.13 - 368.13 Clayey Sand C&D Landfill MW-11DR 05/31/18 510453.00 1852911.56 383.41 386.36 44 339.41 2 34.00 - 44.00 342.36 - 332.36 Sand C&D Landfill MW-13SR 06/24/20 509541.34 1853156.68 383.87 386.57 20 363.87 2 10.00-20.00 373.87 - 363.87 Sand C&D Landfill MW-13SD 06/24/20 509549.23 1853164.04 383.31 385.99 40 343.31 2 30.00-40.00 353.31-343.31 Sand/Clay C&D Landfill MW-14 09/16/96 510056.32 1853641.99 397.88 400.58 20 377.88 2 5.00 - 20.00 392.88 - 377.88 Sand to Silty Sand Upgradient of C&D Landfill MW-15 09/19/96 510597.22 1854401.13 429.31 431.10 35 394.31 2 20.00 - 35.00 409.31 - 394.31 Sand to Silty Sand MSW Landfill MW-15R 05/29/18 510589.03 1854391.51 428.81 431.48 47 381.81 2 37.00 - 47.00 384.48 - 374.48 Sand MSW Landfill MW-17S 05/31/18 509704.03 1852096.70 371.45 374.16 18 353.45 2 8.00 - 18.00 363.45 - 353.45 Sand C&D Landfill MW-17D 06/01/18 509693.71 1852101.52 372.05 374.56 34 338.05 2 29.00 - 34.00 343.05 - 338.05 Clay/Sandy-Clay C&D Landfill MW-18 06/04/18 509369.85 1852249.28 365.35 368.50 13 352.35 2 5.00 - 13.00 360.35 - 352.35 Gravelly Sand, Sand, Sandy Clay C&D Landfill MW-19 06/25/20 509324.26 1852158.78 363.95 366.67 13 350.95 2 5.00-13.00 358.95 - 350.95 Sand C&D Landfill GP-10R 06/25/20 508889.16 1855952.87 431.90 434.21 15 416.90 2 5.00-15.00 426.90 - 416.90 Sand MSW Landfill GP-13R 05/31/18 509405.06 1852208.08 367.1 370.29 10 357.10 2 3.00-10.00 364.10 - 357.10 Sand C&D Landfill GP-14R 05/30/18 509680.01 1852109.63 372.05 374.78 10 362.05 2 3.00 - 10.00 369.05 - 362.05 Clayey Sand to Sand C&D Landfill GP-15R 06/04/18 510038.89 1852041.09 364.85 367.73 10 354.85 2 3.00 -10.00 361.85 - 354.85 Sandy Clay, Gravelly Sand C&D Landfill GP-19 06/25/20 510494.25 1853794.49 397.08 399.33 10 387.08 2 5.00-10.00 393.08 - 387.07 Sand MSW Landfill Notes: 1.) ft AMSL = feet above mean sea level 2.) ft BGS = feet below ground surface 3.) Well construction information for monitoring wells MW-1 through MW-16S/D collected from boring logs and well construction records from HDR Engineering, Inc. of the Carolinas July 2006 Water Quality Monitoring Plan. TOC and Ground Elevations are taken from the July 2005 Assessment of Corrective Measures Report and/or well records where available. 4) Well construction information for monitoring well MW-19 obtained from boring logs and well construction records from Golder, Inc. 11�2022 Active C&D Groundwater Monitoring Network Well ID MW-4 MW-11SR ,r MW-11DR MW-13SR MW-13DR aaaa�� MW-14 aaaaaa�,MW-17S MW-17D MW-18 MW-19 TOC Elevation (ft AMSL) 3��366.19 386.1' 386.36 386.57 385.9' 400.58� 374.16 374.56 368.50 366.67 Measurement Date GWE DTW GWE bTW GWE DTW GWE DTW GWE §DTW GWE DTW' GWE DTW GWE DTW GWE DTW GWE DTW (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL) (ft) Background Well 10"W Groundwater Monitoring Network - Well ID MW-5 MW-1 MW-2 WW-6 , MIIW-8 MW-9 MW-15 TOC Elevation 386.61 392.87 375.50 M05.86 , 406.06 431.38 (ft AMSL) _ Measurement Date GWE DTW GWE DTW GWE �F DTWj GWE ' DTW GWE DTW WE DTW GWE DTW GWE DTV (ft AMSL) (ft) (ft AMSL) (ft) (ft AMSL)IF (ft) (ft AMSL) (ft) (ft AMSL) (ft) ■TMSL) ME SL) (ft) (ft AMSL) (ft`1ft AMSL) (ft) TABLE 3 Groundwater Field Parameter Data Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 = �r Aberdeen, Moore County, North Carolina E S&ME Project No. 4358-20-043A Notes: 1.) mg/L = milligrams per liter 2.) ND = not detected at or above the laboratory reporting limit 8) NS = Not Sampled 3.) NM = not measured 4.) pS/cm = microseimens per centimeter 5.) NTU = Nephelometric Turbidity Units 6.) S.U. = Standard Units 7.) Samples collected using low -flow purge and sample techniques (when possible). r�uv�amlecta�zozowsse-zogaan Moore county—.. arc a—Mo i—gus- -—-I WQ Mo 1ro g—0-10---- TABLE 4 Groundwater Conductivities, Gradients and Calculated Flow Velocities Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project Number 4358-20-043A =0 Well Hydraulic Cond. Eff. Porosity MW-1 1.6E+01 25% October Gradient 0.022 Flow Velocity 512 MW-2 1.6E+01 25% 0.023 538 MW-3 3.4E+00 25% 0.023 111 MW-4 7.7E+00 25% 0.013 145 MW-5 7.1 E+00 25% 0.020 211 MW-6 9.8E+00 25% 0.019 277 MW-7 8.4E-01 25% 0.016 19 MW-8 1.8E+01 25% 0.013 340 MW-9 4.2E+01 25% 0.011 663 MW-14 8.8E+00 25% 0.019 246 MW-15R 4.8E+00 25% 0.020 137 Mean Values = 1.22E+01 25% 0.018 291 Notes: (1) Hydraulic Conductivity was calculated from slug tests performed by HDR (2) Effective porosity is an estimated value, actual values will vary (3) Hydraulic gradient calculated by measuring linear feet along a line between selected monitor well and contour line. (4) Seepage velocity v = (K*i)/ne (5) WNM = Well Not Monitored During This Event TAMAProjeoLM20\4358-20-043A Moore County Ra Ine LFQ&WQ Monitoring\Phase 03-SemFM—I WO M-tonng 2021-2022\Fa11 202112021-10 WQMR T.N. DRAFT.A.. 1/5/2022 TABLE 5 Groundwater Analytical Results (Detected Constituents) Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A or Detected Constituent/Parameter 11 ate 1qrL 10 GWPS 10 Background MW-5 .=W NO NO NO MW-1301 ND :D Monitoring MW-14 NO Wells MW-17S NO MW-17D ND MW-18 NO MW-19 ND :D Performance for the Closed MW-4 NO Wells MSW Landfill MW-11SR NO MW-11 NO Closed MW-2 NO MSW Monitoring MW-3 NO Wells & MNA MW-6 NO Performance Monitoring MW-7 MW-8 NO NO Wells �,Private MW-9 1=6A 43.9 NO Off -site Well JE NO Arsenic u /L 10/19/21 7.6 Barium u /L 10/19/21 1.1 10 700 21.6 51.9 22.9 39.6 44.7 84.2 36.4 78.1 19.8 35.8 67.1 23.7 63.0 36.7 42.3 33.6 80.0 99.9 42.2 15.8 Chromium u /L 10/19/21 1.4 10 10 NO ND NO ND NO NO 3.04 NO ND 1.91 J NO NO NO NO NO NO NO NO NO NO Copper u /L 10/19/21 1.6 10 1000 NO ND NO ND NO NO ND NO ND 2.20 J NO ANR ANR ANR ANR ANR ANR ANR ANR ANR Vanadium u /L 10/19/21 1.4 10 0.3 NO ND NO ND NO NO ND NO ND 2.2 J NO ANR ANR ANR ANR ANR ANR ANR ANR NO Zinc u /L 10/19/21 4.4 10 1000 NO NO 26.8 J NO NO NO NO ND NO NO NO ANR ANR ANR ANR ANR ANR ANR ANR ANR Iron u /L 10/19/21 22 50 300 NO 72,500 58,600 8,430 136,000 48,700 2,200 93,400 305 1,130 88,200 ANR ANR ANR ANR ANR ANR ANR ANR ANR Manganese u /L 10/19/21 1.5 10 50 2.13 J 156 560 71.8 176 181 19.4 154 2.52 J 34.0 259 ANR ANR ANR ANR ANR ANR ANR ANR ANR Acetone u /L 10/19/21 10.0 20 6000 NO ND NO ND NO NO ND 18 J ND NO ND NO NO NO 27 270 NO NO NO NO Benzene u /L 10/19/21 0.15 1 1 NO 1.9 NO ND 1.7 NO ND NO ND NO 2.6 NO NO NO 1.6 1.1 2.1 2.2 NO NO Chlorobenzene u /L 10/19/21 0.17 1 50 NO 1.2 NO ND 5.2 NO ND 0.93 J ND NO 1.2 NS 2.6 NO 1.7 1.9 J 6.7 6.2 NO NO 1,2-Dichlorobenzene u /L 10/19/21 0.19 1 20 NO ND NO ND 1.8 NO ND NO ND NO NO NO NO NO NO NO 0.91 JI NO NO NO 1,4-Dichlorobenzene u /L 10/19/21 0.19 1 6 NO ND ND ND 4.5 NO ND NO ND NO 2.6 NO NO NO 1.5 0.84 J 5.1 NO NO NO 1,1,-Dichloroethane u /L 10/19/21 0.13 1 6 NO ND NO ND NO NO ND NO ND NO NO NO NO NO 0.41 J NO NO J NO NO NO cis-1,2-Dichloroethene ug/L 10/19/21 0.15 1 70 NO 3.3 1.0 ND NO 1.3 ND 1.8 ND NO 1.0 NO 0.68 J NO 2.2 0.98 J NO J NO 2.4 NO Toluene ug/L 10/19/21 0.14 1 600 NO NO NO ND NO NO ND NO ND NO NO NO NO NO 0.61 J 1.3 0.67 J 0.52 J NO NO Vinyl chloride ug/L 10/19/21 0.32 1 0.03 NO 2.3 NO ND 2.6 1.8 ND 0.98 J ND NO J 3.1 NO NO NO 1.2 1.6 NO NO NO NO 1,4-Dioxane ug/L 10/19/21 0.8 2.0 3 NO 3.9 9.2 3.3 17 3.4 7.1 13 2.9 1.6 J 5.1 NO 25 1.6 J 1.8 J 6.3 48 34 NO NO Tetrahydrofuran ug/L 10/19/21 0.53 1.0 NS ND 3.4 ND ND ND ND ND NO ND NO 6.3 ANR ANR ANR ANR ANR ANR ANR ANR ANR Sulfide mg/L 10/19/21 0.01 0.100 NA NO 0.038 J 0.020 J ND 0.160 ND ND 0.056 J ND 0.066 J 0.053 J NS NO ND 0.190 0.460 0.140 0.300 0.290 J ANR Chloride m /L 10/19/21 2.2 5 NA 3.50 J 18 1.60 7.0 61 27 3 J 44 13 10.0 26 2.7 J 93 7.8 13 25 110 D 120 D 3.30 J ANR Nitrate as N mg/L 10/19/21 0.41 1.0 NA 0.94 ANR ANR ANR ANR ANR ANR ANR ANR 0.11 0.15 760 4.6 D 0.35 0 0.14 0.094 J 0.100 0.110 ANR Nitrite as N m /L 10/19/21 0.017 0.100 NA NO ANR ANR ANR ANR ANR ANR ANR ANR 0.021 NO NO NO NO NO NO NO NO NO ANR Total Dissolved Solids m /L 10/19/21 10 10 NA NO 200 78 ND 250 380 150 410 8 130 540 ANR ANR ANR ANR ANR ANR ANR ANR ANR Sulfate as SO4 m /L 10/19/21 2.9 5.0 NA 2.90 J 11 18 8.0 7.0 95 30 42 10 35.0 NO 8.6 17 11 6.5 NO NO NO 9.60 ANR Total Alkalinity as CaCO3 m /L 10/19/21 14 15 NA NO 210 D 43 2.6 220 190 97 31 D 45 D 60.0 470 D NO 320 D NO 21 D 89 D 310 D 900 D 40 ANR Total Organic Carbon m /L 10/19/21 0.9 1 NA NO ANR ANR ANR ANR ANR ANR ANR ANR 14.0 21 1.3 13 1.7 18 28 26 39 2.2 ANR Nitrate/Nitrite as N m /L 10/19/21 0.41 1.000 NA 0.94 ANR ANR ANR ANR ANR ANR ANR ANR 0.130 150 760 4.6 D 350 0.12 140 94 J 100 110 ANR Ethane m /L 10/19/21 0.0051 0.006 NA NO ANR ANR ANR ANR ANR ANR ANR ANR ANR NO NO NO NO NO NO NO NO NO ANR Ethene m /L 10/19/21 0.0051 0.006 NA NO ANR ANR ANR ANR ANR ANR ANR ANR ANR NO NO NO NO NO NO NO NO NO ANR Methane m /L 10/19/21 0.0051 0.006 NA NO ANR ANR ANR ANR ANR ANR ANR ANR 0.480 DI 2.44 NO 0.824 NO 1 2.84 D 2.78 DI 3.93 D 0.52 1 1.52 ANR Carbon dioxide m /L 10/19/21 2.07 2.5 NA 22.5 ANR ANR ANR ANR ANR ANR ANR ANR 73 D 448 D 60.2 1 259 D 82 1 239 D 243 D 314 D 179 1 216 1 ANR Ferrous Iron (Field Measure) mg/L 10/19/21 1 1 NA 0.00 ANR ANR ANR ANR ANR ANR ANR ANR 0 0 0 0 0 7 3 4 7 7 ANR Notes: 1.) ug/L = Micrograms per liter 2.) NO = Not detected at the stated reporting limit 3.) NA = Not Applicable 4.) J = Estimated concentration reported below Solid Waste Section Limit 5.) ANR = Analysis Not Requested 6.) Bold and highlighted in yellow = Concentration above the current 15A NCAC 02L Groundwater Standard, 7.) NS = Not Sampled 8.) GWPS = Solid Waste Section Groundwater Protection Standard 9.) PQL = Practical quantitation limit - lab specific limit 10.) MDL = Method Detection Limit 15A NCAC 2L IMAC Groundwater Standard, or NC Solid Waste Section Groundwater Protection Standards (GW PS) TAEN\AProjeofe=04135 20- MMoore County Roud-LFG& WG MmltonngTh.. 03-Semi-Annual WO Monitoring 2021-202ZFdl 2021M21-10 WGMR Tables_DRAFT.bsn Page 5of6 TABLE 6 Surface Water Monitoring Analytical Results (Detected Constituents) Water Quality Monitoring Report, October 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project Number 4358-20-043A Notes: 1.) MDL = Method Detection Limit 2.) ug/L = micrograms per liter 3.) ND = Not detected at or above MDL 4.) J = Estimated value 5.) -- = Not applicable 6.) Shaded = Constituent exceeds applicable Surface Water Standard 7.) Blanks = Field, trip and method blanks 8.) Surface Water Standards based on WS-II, High Quality Water Classification for Horse Creek and its tributary per 15A NCAC 02B. 9.) SW Standard for lead is a Narrative Standard per 15A NCAC 02B .0211 10.) Upstream and downstream designations based on inspection of site conditions and flow regimes. Reports prior to October 2009 had the designations inadvertently switched. 11.) For standards based on hardness dependent calculations, acute and chronic values shown are based on a worse -case 25 mg/L hardness 12.) NC Protective values are listed within 15A NCAC 02B, but they are not 2B Standards r P Njeda12020W353-20-0 Mows County Routine LFG&WQ Manlbnngl ... 03-Semi-Mn-I WQ Monilw 2-1022-12021-21-10 WQMR Tabba_DRAFT... Appendices Appendix I -Sampling Forms Moore County Landfill I _� Project Name: Project Location: Project Number: 4358-20-043A phase 11 Purge Date: October 19, 2021 Source Well: MW-1 Purge Time: 30 Minutes Locked?: Yes Sample Date: October 19, 2021 Sampled By: Gary Simcox Sample Time: 11:40 Weather: Sunny Air Temp: 65° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 11:35 0.8 100 12.06 19.2 4.7 47 3.0 224 5.5 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 11:40 Sample End Time: 11:55 Analytical Data Name (1) Gary Simcox Signature Date 10/22/2021 Notes: I tested for Ferrous Iron using a HACH Model IR-18 (0.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 11.79 ft-TOC Total Well Depth: 19.30 ft-TOC Height of Water Column: 7.51 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.2 Gal 3 *Well Volume 3.68 Gal 5 *Well Volume 6.13 Gal Purge Method: Peristaltic Pump Start Time: 11:05 End Time: 11:35 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 15.0 ft-TOC Water Column Above Pump Intake: 3.21 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 12.59 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 11:05 0.0 --- --- --- --- --- --- --- --- Start Purging 11:10 0.1 100 11.93 18.6 5.8 198 2.8 116 6.54 11:15 0.3 100 11.98 19.0 5.1 86 3.2 160 5.70 11:20 0.4 100 12.03 19.2 4.8 63 3.1 199 5.90 11:25 0.5 100 12.04 19.2 4.8 54 3.1 211 6.63 11:30 0.7 100 12.05 19.2 4.7 50 3.3 216 5.74 11:35 0.8 100 12.06 19.2 4.7 47 3.0 224 5.45 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Moore County Landfill I _� Project Name: Project Location: Project Number: 4358-20-043A phase 11 Purge Date: October 19, 2021 Source Well: MW-2 Purge Time: 30 Minutes Locked?: Yes Sample Date: October 19, 2021 Sampled By: Gary Simcox Sample Time: 9:50 Weather: Sunny Air Temp: 50° F Water Level & Well Data We Purging Information Fie Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 09:45 0.8 100 8.60 18.1 6.2 936 6.2 108 3.0 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 09:50 Sample End Time: 10:05 Analytical Data Name (1) Gary Simcox Signature Date 10/22/2021 Notes: I tested for Ferrous Iron using a HACH Model IR-18 (0.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 8.56 ft-TOC Total Well Depth: 18.80 ft-TOC Height of Water Column: 10.24 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.7 Gal 3 *Well Volume 5.01 Gal 5 *Well Volume 8.36 Gal Purge Method: Peristaltic Pump Start Time: 9:15 End Time: 9:45 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 14.0 ft-TOC Water Column Above Pump Intake: 5.44 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 9.92 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 09:15 0.0 --- --- --- --- --- --- --- --- Start Purging 09:20 0.1 100 8.59 17.3 6.1 765 7.6 112 6.01 09:25 0.3 100 8.58 17.6 6.2 863 7.3 110 7.51 09:30 0.4 100 8.60 17.9 6.2 900 6.8 110 4.89 09:35 0.5 100 8.59 17.9 6.2 917 6.5 110 3.68 09:40 0.7 100 8.59 18.0 6.2 923 6.3 109 3.61 09:45 0.8 100 8.60 18.1 6.2 936 6.2 108 2.99 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Moore County Landfill I _� Project Name: Project Location: Project Number: 4358-20-043A phase 11 Purge Date: October 19, 2021 Source Well: MW-3 Purge Time: 30 Minutes Locked?: Yes Sample Date: October 19, 2021 Sampled By: Gary Simcox Sample Time: 8:30 Weather: Sunny Air Temp: 45° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 08:25 0.8 100 7.19 17.7 4.6 71 1.8 221 2.8 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 08:30 Sample End Time: 08:45 Analytical Data Name (1) Gary Simcox Signature Date 10/22/2021 Notes: I tested for Ferrous Iron using a HACH Model IR-18 (0.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 7.11 ft-TOC Total Well Depth: 18.10 ft-TOC Height of Water Column: 10.99 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.8 Gal 3 *Well Volume 5.38 Gal 5 *Well Volume 8.97 Gal Purge Method: Peristaltic Pump Start Time: 7:55 End Time: 8:25 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 13.0 ft-TOC Water Column Above Pump Intake: 5.89 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 8.58 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 07:55 0.0 --- --- --- --- --- --- --- --- Start Purging 08:00 0.1 100 7.18 17.1 5.7 152 1.9 18 13.9 08:05 0.3 100 7.18 17.4 4.9 82 1.8 112 5.82 08:10 0.4 100 7.19 17.4 4.8 74 1.9 149 2.66 08:15 0.5 100 7.18 17.7 4.7 74 1.7 175 2.44 08:20 0.7 100 7.18 17.7 4.6 70 1.6 195 2.47 08:25 0.8 100 7.19 17.7 4.6 71 1.8 221 2.80 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 70 ■ Project Name: Project Location: ■ •■ , 11111,11 IL, 111 11 1111Z'' Moore County Landfill 456 Turning Leaf Way Aberdeen, NC S 13 i I I I S Project Number: 4358-20-043A Phase 03 Purge Date: October 18, 2021 Source Well: MW-4 Purge Time: 125 Minutes Locked?: Yes Sample Date: October 18, 2021 Sampled By: James Waters Sample Time: 17:30 Weather: Sunny Air Temp: 75° F ater Level & WellData Measuring Point: Top of Casing Well Volume Well Diameter 2 inch Water Volume 1.6 Gal 3 *Well Volume 4.90 Gal S *Well Volume 8.17 Gal Time: 15:20 17:25 End Time: (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 11.5 ft-TOC Water Column Above Pump Intake: 4.96 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 7.78 ft-TOC Comments: Final Volume Purged: 3.3 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Volume Depth to Dissolved Time Purged Flow Rate Water Temp pH Spec. Cond. Oxygen ORP* Turbidity Comment (gal) (ml/min) (ft) (°C) (s.u.) (p5/cm) (mg/L) (mV) (NTU) 15:20 0.0 - - Start Purging 1 0.3 100 6.78 20.3 6.0 104 1.9 120 92.0 15:35 0.4 100 6.81 20.3 5.9 104 1.9 121 100 15:40 0.5 100 6.83 20.2 6.0 114 1.7 123 74.7 15:45 0.7 100 6.86 20.2 6.0 137 1.1 124 55.1 15:50 0.8 100 6.89 20.2 6.0 137 1.1 12a 50.5 1555 0.9 100 6.91 20.1 6.0 151 0.8 44.1 16:00 1.1 100 6.91 20.1 6.0 153 0.8 125 42.4 16:05 1.2 100 6.91 20.1 6.0 162 0.6 125 39.0 16:10 1.3 100 6.91 20.1 6.0 164 0.6 124 34.6 16:15 1.5 100 6.91 20.0 6.0 178 0.5 123 34.9 16:20 1.6 100 6.91 20.0 6.1 179 0.5 123 35.5 16:25 1.7 100 6.91 20.0 6.1 187 0.5 112 33.1 16:30 1.8 100 6.91 20.1 6.0 194 0.494 34.4 16:35 2.0 100 6.91 20.1 6.1 202 0.4 89 32.9 16:40 2.1 100 6.91 19.9 6.1 219 0.3 80 29.8 16:45 2.2 100 6.91 19.9 6.1 222 0.3 78 30.7 16:50 2.4 100 6.91 19.8 6.1 239 0.3 74 27.4 16:55 2.5 100 6.91 19.8 6.1 240 0.3 73 23.7 17:00 2.6 100 6.91 19.9 6.1 241 0.3 73 21.6 17:05 2.8 100 6.91 19.8 6.1 246 0.3 72 25.8 17:10 2.9 100 6.91 19.8 6.1 254 0.2 72 23.6 17:15 3.0 100 6.91 19.8 6.1 259 0.2 21.2 17:20 3.2 100 6.91 19.8 6.1 264 0.2 i0 23.5 17:25 3.3 100 6.91 19.8 6.1 267 0.2 70 22.7 17:25 3.3 100 6.91 19.8 6.1 267 0.2 70 22.7 End of Purging Form Revision Date: 2/12/18 16:00 Time: 15:20 17:25 End Time: (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 11.5 ft-TOC Water Column Above Pump Intake: 4.96 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 7.78 ft-TOC Comments: Final Volume Purged: 3.3 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Volume Depth to Dissolved Time Purged Flow Rate Water Temp pH Spec. Cond. Oxygen ORP* Turbidity Comment (gal) (ml/min) (ft) (°C) (s.u.) (p5/cm) (mg/L) (mV) (NTU) 15:20 0.0 - - Start Purging 1 0.3 100 6.78 20.3 6.0 104 1.9 120 92.0 15:35 0.4 100 6.81 20.3 5.9 104 1.9 121 100 15:40 0.5 100 6.83 20.2 6.0 114 1.7 123 74.7 15:45 0.7 100 6.86 20.2 6.0 137 1.1 124 55.1 15:50 0.8 100 6.89 20.2 6.0 137 1.1 12a 50.5 1555 0.9 100 6.91 20.1 6.0 151 0.8 44.1 16:00 1.1 100 6.91 20.1 6.0 153 0.8 125 42.4 16:05 1.2 100 6.91 20.1 6.0 162 0.6 125 39.0 16:10 1.3 100 6.91 20.1 6.0 164 0.6 124 34.6 16:15 1.5 100 6.91 20.0 6.0 178 0.5 123 34.9 16:20 1.6 100 6.91 20.0 6.1 179 0.5 123 35.5 16:25 1.7 100 6.91 20.0 6.1 187 0.5 112 33.1 16:30 1.8 100 6.91 20.1 6.0 194 0.494 34.4 16:35 2.0 100 6.91 20.1 6.1 202 0.4 89 32.9 16:40 2.1 100 6.91 19.9 6.1 219 0.3 80 29.8 16:45 2.2 100 6.91 19.9 6.1 222 0.3 78 30.7 16:50 2.4 100 6.91 19.8 6.1 239 0.3 74 27.4 16:55 2.5 100 6.91 19.8 6.1 240 0.3 73 23.7 17:00 2.6 100 6.91 19.9 6.1 241 0.3 73 21.6 17:05 2.8 100 6.91 19.8 6.1 246 0.3 72 25.8 17:10 2.9 100 6.91 19.8 6.1 254 0.2 72 23.6 17:15 3.0 100 6.91 19.8 6.1 259 0.2 21.2 17:20 3.2 100 6.91 19.8 6.1 264 0.2 i0 23.5 17:25 3.3 100 6.91 19.8 6.1 267 0.2 70 22.7 17:25 3.3 100 6.91 19.8 6.1 267 0.2 70 22.7 End of Purging Form Revision Date: 2/12/18 16:00 Volume Depth to Dissolved Time Purged Flow Rate Water Temp pH Spec. Cond. Oxygen ORP* Turbidity Comment (gal) (ml/min) (ft) (°C) (s.u.) (p5/cm) (mg/L) (mV) (NTU) 15:20 0.0 - - Start Purging 1 0.3 100 6.78 20.3 6.0 104 1.9 120 92.0 15:35 0.4 100 6.81 20.3 5.9 104 1.9 121 100 15:40 0.5 100 6.83 20.2 6.0 114 1.7 123 74.7 15:45 0.7 100 6.86 20.2 6.0 137 1.1 124 55.1 15:50 0.8 100 6.89 20.2 6.0 137 1.1 12a 50.5 1555 0.9 100 6.91 20.1 6.0 151 0.8 44.1 16:00 1.1 100 6.91 20.1 6.0 153 0.8 125 42.4 16:05 1.2 100 6.91 20.1 6.0 162 0.6 125 39.0 16:10 1.3 100 6.91 20.1 6.0 164 0.6 124 34.6 16:15 1.5 100 6.91 20.0 6.0 178 0.5 123 34.9 16:20 1.6 100 6.91 20.0 6.1 179 0.5 123 35.5 16:25 1.7 100 6.91 20.0 6.1 187 0.5 112 33.1 16:30 1.8 100 6.91 20.1 6.0 194 0.494 34.4 16:35 2.0 100 6.91 20.1 6.1 202 0.4 89 32.9 16:40 2.1 100 6.91 19.9 6.1 219 0.3 80 29.8 16:45 2.2 100 6.91 19.9 6.1 222 0.3 78 30.7 16:50 2.4 100 6.91 19.8 6.1 239 0.3 74 27.4 16:55 2.5 100 6.91 19.8 6.1 240 0.3 73 23.7 17:00 2.6 100 6.91 19.9 6.1 241 0.3 73 21.6 17:05 2.8 100 6.91 19.8 6.1 246 0.3 72 25.8 17:10 2.9 100 6.91 19.8 6.1 254 0.2 72 23.6 17:15 3.0 100 6.91 19.8 6.1 259 0.2 21.2 17:20 3.2 100 6.91 19.8 6.1 264 0.2 i0 23.5 17:25 3.3 100 6.91 19.8 6.1 267 0.2 70 22.7 17:25 3.3 100 6.91 19.8 6.1 267 0.2 70 22.7 End of Purging Form Revision Date: 2/12/18 16:00 Form Revision Date: 2/12/18 16:00 Project Name: Project Location: Moore County Landfill 456 Turning Leaf Way Aberdeen, INC - rl� Project Number: 4358-20-043A Phase 03 Purge Date: October 19, 2021 Source Well: MW-5 Purge Time: 30 Minutes Locked?: Yes Sample Date: October 19, 2021 Sampled By: James Waters Sample Time: 12:50 Weather: Sunny Air Temp: 75° F Water Level & WellData e urging n ormation FieldParameters (Taken at time intervals >_ minutes an purge volumes >_ flow -through ce volume) Final: 12:45 0.8 100 10.33 4.6 26 4.5 253 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 12:50 Sample End Time: 13:05 Analytical Data Name (1) James Waters Signature - p�j. �QJL2h�]. ate 10/19/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. *Took a ferrous iron reading at MW-5. Ferrous Iron reading is non -detect. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 10.32 ft-TOC Total Well Depth: 19.85 ft-TOC Height of Water Column: 9.53 feet Screen Length: 10 feet Stickup: 2.6 ft-GRD Well Volume Well Diamete 2 inch Water Volume 1.6 Gal 3 *Well Volume 4.67 Gal 5 *Well Volume 7.78 Gal Purge Method: Peristaltic Pump Start Time: 12:15 End Time: 12:45 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 15.0 ft-TOC Water Column Above Pump Intake: 4.68 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 11.49 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/Cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 12:15 0.0 --- --- --- --- --- --- --- --- Start Purginr 12:20 0.1 100 10.33 21.0 4.8 26 4.0 195 3.96 12:25 0.3 100 10.33 21.1 4.8 26 4.0 201 3.32 12:30 0.4 100 10.33 20.9 4.7 26 4.7 234 3.61 12:35 0.5 100 10.33 20.8 4.7 26 4.6 237 2.80 12:40 0.7 100 10.33 20.9 4.7 26 4.6 245 2.62 12:45 0.8 100 10.33 20.8 4.6 26 4.5 253 2.28 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Moore County Landfill I _� Project Name: Project Location: Project Number: 4358-20-043A phase 11 Purge Date: October 19, 2021 Source Well: MW-6 Purge Time: 35 Minutes Locked?: Yes Sample Date: October 19, 2021 Sampled By: Gary Simcox Sample Time: 15:00 Weather: Sunny Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 14:55 0.9 100 18.76 21.8 6.2 942 2.1 -87 11.9 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 15:00 Sample End Time: 15:15 Analytical Data Name (1) Gary Simcox Signature Date 10/22/2021 Notes: I tested for Ferrous Iron using a HACH Model IR-18 (7.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 17.99 ft-TOC Total Well Depth: 22.50 ft-TOC Height of Water Column: 4.51 feet Screen Length: 15 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 0.7 Gal 3 *Well Volume 2.21 Gal 5 *Well Volume 3.68 Gal Purge Method: Peristaltic Pump Start Time: 14:20 End Time: 14:55 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 20.0 ft-TOC Water Column Above Pump Intake: 2.01 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 18.49 ft-TOC Comments: Final Volume Purged: 0.9 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 14:20 0.0 --- --- --- --- --- --- --- --- Start Purging 14:25 0.1 100 18.61 21.8 6.2 919 2.7 -84 46.3 14:30 0.3 100 18.71 21.6 6.2 919 2.6 -84 16.8 14:35 0.4 100 18.78 22.6 6.2 920 2.5 -84 15.1 14:40 0.5 100 18.76 22.8 6.2 924 2.4 -85 13.7 14:45 0.7 100 18.76 21.9 6.2 932 2.3 -86 13.3 14:50 0.8 100 18.75 21.9 6.2 939 2.2 -87 12.6 14:55 0.9 100 18.76 21.8 6.2 942 2.1 -87 11.9 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Project Name: Project Location: Moore County Landfill 456 Turning Leaf Way Aberdeen, NC - rl� Project Number: 4358-20-043A Phase 03 Purge Date: October 19, 2021 Source Well: MW-7 Purge Time: 45 Minutes Locked?: Yes Sample Date: October 19, 2021 Sampled By: James Waters Sample Time: 14:35 Weather: Sunny Air Temp: 75° F Water Level & WellData e urging n ormation FieldParameters (Taken at time intervals >_ minutes an purge volumes >_ flow -through cellvolume) Final: 14:30 0.8 50 19.90 6.2 668 0.3 -98 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 14:35 Sample End Time: 15:00 Analytical Data Name (1) James Waters Signature 1j. ate 10/19/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. The water level dropped rapidly purging at 100 mL per minute. Slowed purging to 50 mL per minute and recorded parameters eve 10 minutes. *Took a ferrous iron read in at MW-7. Ferrous iron is 3 mg/L. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 17.52 ft-TOC Total Well Depth: 22.00 ft-TOC Height of Water Column: 4.48 feet Screen Length: 15 feet Stickup: 2.7 ft-GRD Well Volume Well Diamete 2 inch Water Volume 0.7 Gal 3 *Well Volume 2.19 Gal 5 *Well Volume 3.66 Gal Purge Method: Peristaltic Pump Start Time: 13:45 End Time: 14:30 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 21.5 ft-TOC Water Column Above Pump Intake: 3.98 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 18.52 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 50 mL/min Well Purged Dry?: Yes (Yes/No) Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/Cm) Dissolved Oxygen (mg/L) ORP' (mV) Turbidity (NTU) Comment 13:45 0.0 --- --- --- --- --- --- --- --- Start Purginr 13:50 0.1 100 18.04 22.8 5.7 261 0.7 15 22.5 13:55 0.3 100 18.66 22.6 5.7 254 0.5 12 12.7 14:00 0.4 100 19.01 24.2 6.1 623 0.9 -77 20.7 14:10 0.5 50 19.15 24.2 6.3 698 0.4 -97 14.5 14:20 0.7 50 19.60 24.7 6.3 692 0.3 -101 12.6 14:30 0.8 50 19.90 24.0 6.2 668 0.3 -98 9.94 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RS K-175 Project Name: Project Location: Moore County Landfill 456 Turning Leaf Way Aberdeen, NC - rl� Project Number: 4358-20-043A Phase 3 Purge Date: October 19, 2021 Source Well: MW-8 Purge Time: 45 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: James Waters Sample Time: Weather: Sunny Air Temp: 75° F Water Level & WellData e urging n ormation FieldParameters (Taken at time intervals >_ minutes an purge volumes >_ flow -through cellvolume) Final: 16:10 1. 100 16.63 6.3 1,272 0.2 -106 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 16:15 Sample End Time: 16:30 Analytical Data Name (1) James Waters'. Signature ^'"' �' ate 10/19/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. *Took a ferrous iron reading at MW-8. Ferrous iron is 4 mg/L. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 16.08 ft-TOC Total Well Depth: 22.00 ft-TOC Height of Water Column: 5.92 feet Screen Length: 15 feet Stickup: 2.6 ft-GRD Well Volume Well Diamete 2 inch Water Volume 1.0 Gal 3 *Well Volume 2.90 Gal 5 *Well Volume 4.83 Gal Purge Method: Peristaltic Pump Start Time: 15:25 End Time: 16:10 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 19.0 ft-TOC Water Column Above Pump Intake: 2.92 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 16.81 ft-TOC Comments: Final Volume Purged: 1.2 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/Cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 15:25 0.0 --- --- --- --- --- --- --- --- Start Purginr 15:30 0.1 100 16.60 21.8 6.2 936 D.5 -80 16.4 15:35 0.3 100 16.63 21.8 6.2 816 0.4 -85 45.2 15:40 0.4 100 16.63 21.7 6.3 1,076 0.3 -99 24.9 15:45 0.5 100 16.63 21.8 6.3 1,092 0.3 -100 21.7 15:50 0.7 100 16.63 21.8 6.3 1,118 0.3 -101 18.9 15:55 0.8 100 16.63 21.5 6.3 1,182 0.2 -101 16.5 16:00 0.9 100 16.63 21.6 6.4 1,230 0.2 -104 12.2 16:05 1.1 100 16.63 21.6 6.3 1,249 0.2 -105 10.5 16:10 1.2 100 16.63 21.6 6.3 1,272 0.2 -106 9.32 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RS K-175 Moore County Landfill E 456 Turning Leaf Way Aberdeen, NC Project Name: Project Location: Project Number: 4358-20-043A phase 11 Purge Date: October 14, 2020 Source Well: MW-9 Purge Time: 35 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: James Waters Sample Time: 13:15 Weather: Sunny Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 13:10 0.9 100 23.85 22.8 6.5 2,143 0.3 -101 4.3 End of Purging Sample Method: Bladder Pump Sample Start Time: 13:15 Sample End Time: 13:30 Analytical Data Name Signature Date (1) James Waters 10/22/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. At the beginning of purging, black liquid came from the well. I tested for Ferrous Iron using a HACH Model I R 18 7.0 m L Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 23.86 ft-TOC Total Well Depth: 32.00 ft-TOC Height of Water Column: 8.14 feet Screen Length: 15 feet Stickup: 2.3 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.3 Gal 3 *Well Volume 3.99 Gal 5 *Well Volume 6.64 Gal Purge Method: Peristaltic Pump Start Time: 12:35 End Time: 13:10 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 28.0 ft-TOC Water Column Above Pump Intake: 4.14 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 24.90 ft-TOC Comments: Final Volume Purged: 0.9 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 12:35 0.0 --- --- --- --- --- --- --- --- Start Purging 12:40 0.1 100 23.88 22.1 6.5 2,142 0.4 -108 4.55 12:45 0.3 100 23.86 22.3 6.5 2,147 0.4 -95 4.61 12:50 0.4 100 23.86 22.5 6.5 2,149 0.3 -99 4.35 12:55 0.5 100 23.85 22.7 6.5 2,150 0.3 -104 4.06 13:00 0.7 100 23.85 22.6 6.5 2,154 0.3 -108 4.57 13:05 0.8 100 23.85 22.9 6.5 2,144 0.3 -107 4.34 13:10 0.9 100 23.85 22.8 6.5 2,143 0.3 -101 4.25 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Project Name: Project Location: Moore County Landfill 456 Turning Leaf Way Aberdeen, INC - rl� Project Number: 4358-20-043A Phase 03 Purge Date: October 19, 2021 Source Well: MW-11SR Purge Time: 35 Minutes Locked?: Yes Sample Date: October 19, 2021 Sampled By: James Waters Sample Time: 8:25 Weather: Sunny Air Temp: 55° F Water Level & WellData e urging n ormation FieldParameters (Taken at time intervals >_ minutes an purge volumes >_ flow -through cellvolume) Final: 08:20 0.9 100 15.61 6.5 1,497 0.3 -99 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 0825 Sample End Time: 08:40 Analytical Data Name (1) James Waters Signature �n� a. +� ate 10/19/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. *Took a ferrous iron reading at MW-11SR. Ferrous Iron reading is reading 7 mg/L on the scale. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 15.61 ft-TOC Total Well Depth: 31.20 ft-TOC Height of Water Column: 15.59 feet Screen Length: 10 feet Stickup: 2.2 ft-GRD Well Volume Well Diamete 2 inch Water Volume 2.5 Gal 3 *Well Volume 7.63 Gal 5 *Well Volume 12.72 Gal Purge Method: Peristaltic Pump Start Time: 7:45 End Time: 8:20 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 26.0 ft-TOC Water Column Above Pump Intake: 10.39 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 18.21 ft-TOC Comments: Final Volume Purged: 0.9 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/Cm) Dissolved Oxygen (mg/L) ORP' (mV) Turbidity (NTU) Comment 07:45 OD --- --- --- --- --- --- - --- Start Purginr 07:55 100 15.61 16.9 6.5 1,447 0.8 2.86 08:00 0.4 100 15.61 17.3 6.5 1,476 0.8 -82 3.07 08:05 0.5 100 15.61 17.1 6.5 1,498 0.6 -88 2.35 08:10 0.7 100 15.61 17.3 6.5 1,493 0.4 -94 2.19 08:15 0.8 100 15.61 17.2 6.5 1,499 0.3 -97 '.85 08:20 0.9 100 15.61 17.1 6.5 1,497 0.3 -99 1.58 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Project Name: Project Location: Moore County Landfill 456 Turning Leaf Way Aberdeen, INC - rl� Project Number: 4358-20-043A Phase 03 Purge Date: October 19, 2021 Source Well: MW-11 DR Purge Time: 30 Minutes Locked?: Yes Sample Date: October 19, 2021 Sampled By: James Waters Sample Time: 9:20 Weather: Sunny Air Temp: 60° F Water Level & WellData e urging n ormation FieldParameters (Taken at time intervals >_ minutes an purge volumes >_ flow -through ce volume) Final: 09:15 0.8 100 15.99 6.4 735 0.3 -85 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 0920 Sample End Time: 09:35 Analytical Data Name (1) James Waters signature y`l Pam' �• "`"�" ate 10/19/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 15.93 ft-TOC Total Well Depth: 42.20 ft-TOC Height of Water Column: 26.27 feet Screen Length: 10 feet Stickup: 2.6 ft-GRD Well Volume Well Diamete 2 inch Water Volume 4.3 Gal 3 *Well Volume 12.86 Gal 5 *Well Volume 21.43 Gal Purge Method: Peristaltic Pump Start Time: 8:45 End Time: 9:15 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 38.0 ft-TOC Water Column Above Pump Intake: 22.07 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 21.45 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/Cm) Dissolved Oxygen (mg/L) ORP' (mV) Turbidity (NTU) Comment 08:45 0.0 --- --- --- --- --- --- - --- Start Purginr 08:50 0.1 100 15.99 16.3 6.4 729 D.8 9.48 08:55 0.3 100 15.99 17.1 6.4 732 0.5 -71 7.83 09:00 0.4 100 15.99 17.4 6.4 757 0.4 -78 6.05 09:05 0.5 100 15.99 17.5 6.4 734 0.4 -81 4.91 09:10 0.7 100 15.99 17.7 6.4 756 0.3 -84 3.07 09:15 0.8 100 15.99 17.7 6.4 735 0.3 -85 2.91 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Project Name: Project Location: Moore County Landfill 456 Turning Leaf Way Aberdeen, INC - rl� Project Number: 4358-20-043A Phase 03 Purge Date: October 19, 2021 Source Well: MW-13SR Purge Time: 55 Minutes Locked?: Yes Sample Date: October 19, 2021 Sampled By: James Waters Sample Time: 10:55 Weather: Sunny Air Temp: 60° F Water Level & WellData e urging n ormation FieldParameters (Taken at time intervals >_ minutes an purge volumes >_ flow -through cellvolume) Final: 10:50 1.S 100 13.20 350 0.2 -47 8. End of Purging Sample Method: Peristaltic Pump Sample Start Time: 10:55 Sample End Time: 11:10 Analytical Data Name (1) James Waters/LI/mQ� signature W�llWtidl. ate 10/19/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 13.16 ft-TOC Total Well Depth: 22.50 ft-TOC Height of Water Column: 9.34 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diamete 2 inch Water Volume 1.5 Gal 3 *Well Volume 4.57 Gal 5 *Well Volume 7.62 Gal Purge Method: Peristaltic Pump Start Time: 9:55 End Time: 10:50 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 17.0 ft-TOC Water Column Above Pump Intake: 3.84 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 14.12 ft-TOC Comments: Final Volume Purged: 1.5 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/Cm) Dissolved Oxygen (mg/L) ORP' (mV) Turbidity (NTU) Comment 09:55 0.0 --- --- --- --- --- --- --- --- Start Purginr 10:00 0.1 100 13.19 17.5 6.1 347 0.5 -17 25.5 10:05 0.3 100 13.20 17.7 6.1 342 0.4 -21 43.2 10:10 0.4 100 13.20 17.6 6.1 336 0.4 -24 84.2 10:15 0.5 100 13.20 18.0 6.1 337 0.3 -28 81.9 10:20 0.7 100 13.20 18.0 6.1 342 0.3 -34 52.1 10:25 0.8 100 13.20 18.2 6.1 344 0.3 -37 40.3 10:30 0.9 100 13.20 18.4 6.1 346 0.2 -39 31.4 10:35 1.1 100 13.20 18.5 6.1 349 0.2 -42 20.3 10:40 1.2 100 13.20 18.6 6.1 349 0.2 -45 15.5 10:45 1.3 100 13.20 18.7 6.1 350 0.2 -46 11.2 10:50 1.5 100 13.20 18.7 6.1 350 0.2 -47 8.58 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Project Name: Project Location: Moore County Landfill 456 Turning Leaf Way Aberdeen, INC - rl� Project Number: 4358-20-043A Phase 03 Purge Date: October 19, 2021 Source Well: MW-13DR Purge Time: 30 Minutes Locked?: Yes Sample Date: October 19, 2021 Sampled By: James Waters Sample Time: 11:50 Weather: Sunny Air Temp: 65° F Water Level & WellData e urging n ormation FieldParameters (Taken at time intervals >_ minutes an purge volumes >_ flow -through cellvolume) Final: 11:45 0.8 100 13.63 5.4 93 0.3 90 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 11:50 Sample End Time: 12:05 Analytical Data Name (1) James Waters signature ��' +✓c' `� `�'� ate 10/19/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 13.60 ft-TOC Total Well Depth: 43.50 ft-TOC Height of Water Column: 29.90 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diamete 2 inch Water Volume 4.9 Gal 3 *Well Volume 14.64 Gal 5 *Well Volume 24.40 Gal Purge Method: Peristaltic Pump Start Time: 11:15 End Time: 11:45 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 38.0 ft-TOC Water Column Above Pump Intake: 24.40 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 19.70 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/Cm) Dissolved Oxygen (mg/L) ORP' (mV) Turbidity (NTU) Comment 11:15 0.0 --- --- --- --- --- --- - --- Start Purginr 11:20 0.1 100 13.63 17.9 5.5 0.7 26.9 11:25 0.3 100 13.63 18.1 5.4 93 0.3 89 11.6 11:30 0.4 100 13.63 18.0 5.4 93 0.3 89 8.44 11:35 0.5 100 13.63 18.2 5.4 93 0.3 90 5.90 11:40 0.7 100 13.63 18.0 5.4 93 0.3 90 4.63 11:45 0.8 100 13.63 18.0 5.4 93 0.3 90 3.55 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Moore County Landfill 456 Turning Leaf Way Aberdeen, NC E Project Name: Project Location: Project Number: 4358-20-043A phase 11 Purge Date: October 18, 2021 Source Well: MW-14 Purge Time: 30 Minutes Locked?: Yes Sample Date: October 18, 2021 Sampled By: Gary Simcox Sample Time: 18:10 Weather: Sunny Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 18:05 0.8 100 18.61 20.0 6.4 1,061 0.2 -95 5.9 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 18:10 Sample End Time: 18:25 Analytical Data Name (1) Gary Simcox Signature Date 10/22/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 18.31 ft-TOC Total Well Depth: 23.00 ft-TOC Height of Water Column: 4.69 feet Screen Length: 15 feet Stickup: 1.9 ft-GRD Well Volume Well Diameter 2 inch Water Volume 0.8 Gal 3 *Well Volume 2.30 Gal 5 *Well Volume 3.83 Gal Purge Method: Peristaltic Pump Start Time: 17:35 End Time: 18:05 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 19.5 ft-TOC Water Column Above Pump Intake: 1.19 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 18.61 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 17:35 0.0 --- --- --- --- --- --- --- --- Start Purging 17:40 0.1 100 18.61 20.8 6.4 1,040 0.5 -80 11.6 17:45 0.3 100 18.61 20.7 6.4 1,049 0.3 -85 8.95 17:50 0.4 100 18.61 20.5 6.4 1,053 0.3 -88 6.13 17:55 0.5 100 18.62 20.4 6.4 1,056 0.2 -90 5.67 18:00 0.7 100 18.61 20.2 6.4 1,060 0.3 -93 6.94 18:05 0.8 100 18.61 20.0 6.4 1,061 0.2 -95 5.94 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Moore County Landfill I 4358-20-043A phase 11 Purge Date: October 18, 2021 Project Name: Project Location: Project Number: Source Well: MW-15R Purge Time: 40 Minutes Locked?: Yes Sample Date: October 18, 2021 Sampled By: Gary Simcox Sample Time: 16:45 Weather: Sunny I Air Temp: 75° F Water Level Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow-throughcellvolume) Final: 16:40 1.1 100 33.24 19.2 6.1 314 0.2 -36 5.0 End of Purging Sample Method: Bladder Pump Sample Start Time: 16:45 Sample End Time: 17:00 Analytical Data (1) Gary Simcox 1012212021 Notes: Duplicate collected at this location. (Sample time recorded as 0700 hrs) I tested for Ferrous Iron using a HACH Model IR-18 (7.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 33.21 ft-TOC Total Well Depth: 50.20 ft-TOC Height of Water Column: 16.99 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 2.8 Gal 3 *Well Volume 8.32 Gal 5 *Well Volume 13.86 Gal Purge Method: Peristaltic Pump Start Time: 16:00 End Time: 16:40 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 45.0 ft-TOC Water Column Above Pump Intake: 11.79 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 36.16 ft-TOC Comments: Final Volume Purged: 1.1 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 16:00 0.0 --- --- --- --- --- --- --- --- Start Purging 16:10 0.3 100 33.24 19.5 6.0 338 0.5 -36 34.9 16:20 0.5 100 33.23 19.5 6.1 321 0.3 -37 14.9 16:30 0.8 100 33.23 19.3 6.1 314 0.2 -36 6.69 16:40 1.1 100 33.24 19.2 6.1 314 0.2 -36 4.95 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Moore County Landfill I _� Project Name: Project Location: Project Number: 4358-20-043A phase 11 Purge Date: October 18, 2021 Source Well: MW-17D Purge Time: 110 Minutes Locked?: Yes Sample Date: October 18, 2021 Sampled By: Gary Simcox Sample Time: 15:10 Weather: Sunny Air Temp: 65° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 15:05 2.9 100 16.68 20.7 7.2 292 1.8 -61 35.9 End of Purging Sample Method: Bladder Pump Sample Start Time: 15:10 Sample End Time: 15:25 Analytical Data Name (1) Gary Simcox Signature Date 10/22/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 11.98 ft-TOC Total Well Depth: 37.30 ft-TOC Height of Water Column: 25.32 feet Screen Length: 5 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 4.1 Gal 3 *Well Volume 12.40 Gal 5 *Well Volume 20.66 Gal Purge Method: Peristaltic Pump Start Time: 13:15 End Time: 15:05 (If Used) Bladder Pump Control Settings: On (sec): 5 Off (sec): 30 Pressure: 25 psi Pump Intake Depth from Top of Casing: 35.0 ft-TOC Water Column Above Pump Intake: 23.02 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 17.74 ft-TOC Comments: Final Volume Purged: 2.9 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 13:15 0.0 --- --- --- --- --- --- --- --- Start Purging 13:25 0.3 100 12.65 20.7 7.1 282 5.4 8 93.3 13:35 0.5 100 13.04 20.6 7.3 305 4.2 -35 150 13:45 0.8 100 13.54 20.4 7.3 303 3.4 -56 158 13:55 1.1 100 14.03 20.0 7.3 299 3.0 -63 115 14:05 1.3 100 14.42 20.4 7.3 297 2.8 -65 87.9 14:15 1.6 100 14.80 20.3 7.3 295 2.5 -65 61.6 14:25 1.8 100 15.25 20.3 7.2 293 2.4 -64 47.8 14:35 2.1 100 15.66 20.4 7.2 293 2.1 -64 41.6 14:45 2.4 100 15.99 20.4 7.2 292 2.0 -63 38.8 14:55 2.6 100 16.31 20.6 7.2 292 1.9 -62 37.4 15:05 2.9 100 16.68 20.7 7.2 292 1.8 -61 35.9 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 a Project Name: a •a � a• � s Moore County Landfill 456 Turning Leaf Way Aberdeen, INC I I I E 4358-20-043A Phase 03 Purge Date: October 18, 2021 Project Location: Project Number: Source Well: MW-17S Purge Time: 60 Minutes Locked?: Yes Sample Date: October 18, 2021 Sampled By: James Waters Sample Time: 11:05 Weather: Sunny I Air Temp:1 65° F Water Level & WellData Well Purging Information FieldParameters (Taken at time intervals _> minutes an purge volumes 2: flow -through cellvo ume Final: 11:00 1.6 100 12.31 21.8 6.3 769 2.5 11 9.3 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 11:05 Sample End Time: 11:20 kna ytica Data N� , _. Date (1) James Waters �� VL . ' " 10/18/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 12.19 ft-TOC Total Well Depth: 21.40 ft-TOC Height of Water Column: 9.21 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.5 Gal 3 *Well Volume 4.51 Gal 5 *Well Volume 7.51 Gal Purge Method: Peristaltic Pump Start Time: 10:00 End Time: 11:00 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 19.0 ft-TOC Water Column Above Pump Intake: 6.81 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 13.89 ft-TOC Comments: Final Volume Purged: 1.6 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Dept W ter ) Temp (°C) pH (s.u.) Spec. Cond. (p5/cm' Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 10:00 0.0 --- --- --- --- --- --- --- --- Start Purging 10:05 0.1 100 12.27 20.1 5.8 358 8.2 159 52.5 10:10 0.3 100 12.30 20.9 5.9 380 4.3 116 30.2 10:15 0.4 100 12.31 21.1 6.0 410 3.8 89 22.7 10:20 0.5 100 12.31 21.2 6.1 463 3.7 57 20.4 10:25 0.7 100 12.31 21.3 6.1 512 2.9 40 16.9 10:30 0.8 100 12.31 21.4 6.2 562 2.9 24 14.1 10:35 0.9 100 12.31 21.4 6.2 611 3.1 12 11.6 10:40 1.1 100 12.31 21.4 6.3 703 2.8 -4 12.7 10:45 1.2 100 12.31 21.5 6.3 705 2.7 5 13.2 10:50 1.3 100 12.31 21.6 6.3 739 2.7 -10 14.5 10:55 1.5 100 12.31 21.3 6.3 748 2.8 -10 11.5 11:00 1.6 100 12.31 21.8 6.3 769 2.5 -11 9.30 Method City Container Preservative Method C1ty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 a Project Name: a •a � a• � s Moore County Landfill 456 Turning Leaf Way Aberdeen, INC I I I E 4358-20-043A Phase 03 Purge Date: October 18, 2021 Project Location: Project Number: Source Well: MW-18 Purge Time: 120 Minutes Locked?: Yes Sample Date: October 18, 2021 Sampled By: James Waters Sample Time: 13:55 Weather: Sunny Air Temp: 70° F Water Level & WellData Measuring Point: Top of Casing Well Volume Well Diameter 2 inch Water Volume 1.4 Gal 3 *Well Volume 4.30 Gal 5 *Well Volume 7.16 Gal Time: 13:50 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure] Pump Intake Depth from Top of Casing: 14.0 ft-TOC Water Column Above Pump Intake: 6.58 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 9.07 ft-TOC Comments: Final Volume Purged: 3.2 Gallons Used YSI Pro psi Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Volume Depth to Dissolved Time Purged Flow Rate Water Temp pH Spec. Cond. Oxygen ORP* Turbidity Comment (gal) (mL/min) (ft) (°C) (s.u.) (p5/cm' (mg/L) (mV) (NTU) 11:50 0.0 --- --- --- --- --- --- --- --- Start Purging 12:00 0.3 100 7.47 21.9 6.2 480 0.5 0 82.7 12:05 0.4 100 7.48 21.8 6.3 528 0.4 -20 65.2 12:10 0.5 100 7.48 21.9 6.3 600 0.4 -39 49.3 12:15 0.7 100 7.48 22.1 6.3 628 0.3 -47 43.9 12:20 0.8 100 7.48 22.0 6.3 686 0.3 -53 35.6 12:25 0.9 100 7.48 22.0 6.3 732 0.3 -57 38.8 12:30 1.1 100 7.48 21.9 6.4 786 0.3 -61 33.2 12:35 1.2 100 7.48 21.9 6.4 801 0.3 -63 34.4 12:40 1.3 100 7.48 21.9 6.4 811 0.3 -65 27.4 12:45 1.5 100 7.48 21.9 6.4 869 0.3 -71 27.3 12:50 1.6 100 7.48 21.9 6.4 868 0.3 -71 25.1 12:55 1.7 100 7.48 21.7 6.4 900 0.3 -75 26.9 1300 1.8 100 7.48 21.8 6.4 901 0.3 -75 23.8 1305 2.0 100 7.48 21.9 6.4 931 0.3 -73 18.7 1310 2.1 100 7.48 21.9 6.4 945 0.2 72 21.513:15 2.2 100 7.48 21.8 6.4 976 0.2 -81 16.4 13:20 2.4 100 7.48 21.7 6.4 973 0.2 -83 16.4 13:25 2.5 100 7.48 21.7 6.4 1,012 0.2 -81 13.4 13:30 2.6 100 7.48 21.7 6.4 1,016 0.2 -81 11.1 13:35 2.8 100 7.48 21.6 6.4 1,013 0.2 -80 12.5 13:40 2.9 100 7.48 21.5 6.4 1,020 0.2 -81 11.1 13:45 3.0 100 7.48 21.5 6.4 1,023 0.2 -81 10.4 13:50 3.2 100 7.48 21.5 6.4 1,029 0.2 -82 9.10 13:50 3.2 100 7.48 21.5 6.4 1,029 0.2 -82 9.1 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 13:55 Sample End Time: 15:00 Method City Container Preservative Method Qty Containe Preservative 8260B 300 8260 D-SIM SIM 450052 D-20' 6010/6020 310.2 7470 SIM 2540C-201 Time: 13:50 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure] Pump Intake Depth from Top of Casing: 14.0 ft-TOC Water Column Above Pump Intake: 6.58 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 9.07 ft-TOC Comments: Final Volume Purged: 3.2 Gallons Used YSI Pro psi Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Volume Depth to Dissolved Time Purged Flow Rate Water Temp pH Spec. Cond. Oxygen ORP* Turbidity Comment (gal) (mL/min) (ft) (°C) (s.u.) (p5/cm' (mg/L) (mV) (NTU) 11:50 0.0 --- --- --- --- --- --- --- --- Start Purging 12:00 0.3 100 7.47 21.9 6.2 480 0.5 0 82.7 12:05 0.4 100 7.48 21.8 6.3 528 0.4 -20 65.2 12:10 0.5 100 7.48 21.9 6.3 600 0.4 -39 49.3 12:15 0.7 100 7.48 22.1 6.3 628 0.3 -47 43.9 12:20 0.8 100 7.48 22.0 6.3 686 0.3 -53 35.6 12:25 0.9 100 7.48 22.0 6.3 732 0.3 -57 38.8 12:30 1.1 100 7.48 21.9 6.4 786 0.3 -61 33.2 12:35 1.2 100 7.48 21.9 6.4 801 0.3 -63 34.4 12:40 1.3 100 7.48 21.9 6.4 811 0.3 -65 27.4 12:45 1.5 100 7.48 21.9 6.4 869 0.3 -71 27.3 12:50 1.6 100 7.48 21.9 6.4 868 0.3 -71 25.1 12:55 1.7 100 7.48 21.7 6.4 900 0.3 -75 26.9 1300 1.8 100 7.48 21.8 6.4 901 0.3 -75 23.8 1305 2.0 100 7.48 21.9 6.4 931 0.3 -73 18.7 1310 2.1 100 7.48 21.9 6.4 945 0.2 72 21.513:15 2.2 100 7.48 21.8 6.4 976 0.2 -81 16.4 13:20 2.4 100 7.48 21.7 6.4 973 0.2 -83 16.4 13:25 2.5 100 7.48 21.7 6.4 1,012 0.2 -81 13.4 13:30 2.6 100 7.48 21.7 6.4 1,016 0.2 -81 11.1 13:35 2.8 100 7.48 21.6 6.4 1,013 0.2 -80 12.5 13:40 2.9 100 7.48 21.5 6.4 1,020 0.2 -81 11.1 13:45 3.0 100 7.48 21.5 6.4 1,023 0.2 -81 10.4 13:50 3.2 100 7.48 21.5 6.4 1,029 0.2 -82 9.10 13:50 3.2 100 7.48 21.5 6.4 1,029 0.2 -82 9.1 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 13:55 Sample End Time: 15:00 Method City Container Preservative Method Qty Containe Preservative 8260B 300 8260 D-SIM SIM 450052 D-20' 6010/6020 310.2 7470 SIM 2540C-201 Volume Depth to Dissolved Time Purged Flow Rate Water Temp pH Spec. Cond. Oxygen ORP* Turbidity Comment (gal) (mL/min) (ft) (°C) (s.u.) (p5/cm' (mg/L) (mV) (NTU) 11:50 0.0 --- --- --- --- --- --- --- --- Start Purging 12:00 0.3 100 7.47 21.9 6.2 480 0.5 0 82.7 12:05 0.4 100 7.48 21.8 6.3 528 0.4 -20 65.2 12:10 0.5 100 7.48 21.9 6.3 600 0.4 -39 49.3 12:15 0.7 100 7.48 22.1 6.3 628 0.3 -47 43.9 12:20 0.8 100 7.48 22.0 6.3 686 0.3 -53 35.6 12:25 0.9 100 7.48 22.0 6.3 732 0.3 -57 38.8 12:30 1.1 100 7.48 21.9 6.4 786 0.3 -61 33.2 12:35 1.2 100 7.48 21.9 6.4 801 0.3 -63 34.4 12:40 1.3 100 7.48 21.9 6.4 811 0.3 -65 27.4 12:45 1.5 100 7.48 21.9 6.4 869 0.3 -71 27.3 12:50 1.6 100 7.48 21.9 6.4 868 0.3 -71 25.1 12:55 1.7 100 7.48 21.7 6.4 900 0.3 -75 26.9 1300 1.8 100 7.48 21.8 6.4 901 0.3 -75 23.8 1305 2.0 100 7.48 21.9 6.4 931 0.3 -73 18.7 1310 2.1 100 7.48 21.9 6.4 945 0.2 72 21.513:15 2.2 100 7.48 21.8 6.4 976 0.2 -81 16.4 13:20 2.4 100 7.48 21.7 6.4 973 0.2 -83 16.4 13:25 2.5 100 7.48 21.7 6.4 1,012 0.2 -81 13.4 13:30 2.6 100 7.48 21.7 6.4 1,016 0.2 -81 11.1 13:35 2.8 100 7.48 21.6 6.4 1,013 0.2 -80 12.5 13:40 2.9 100 7.48 21.5 6.4 1,020 0.2 -81 11.1 13:45 3.0 100 7.48 21.5 6.4 1,023 0.2 -81 10.4 13:50 3.2 100 7.48 21.5 6.4 1,029 0.2 -82 9.10 13:50 3.2 100 7.48 21.5 6.4 1,029 0.2 -82 9.1 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 13:55 Sample End Time: 15:00 Method City Container Preservative Method Qty Containe Preservative 8260B 300 8260 D-SIM SIM 450052 D-20' 6010/6020 310.2 7470 SIM 2540C-201 Method City Container Preservative Method Qty Containe Preservative 8260B 300 8260 D-SIM SIM 450052 D-20' 6010/6020 310.2 7470 SIM 2540C-201 Moore County Landfill I _� Project Name: Project Location: Project Number: 4358-20-043A phase 11 Purge Date: October 18, 2021 Source Well: MW-19 Purge Time: 95 Minutes Locked?: Yes Sample Date: October 18, 2021 Sampled By: Gary Simcox Sample Time: 11:45 Weather: Sunny Air Temp: 52° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 11:40 2.5 100 7.38 20.1 6.5 197 3.8 87 10.1 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 11:45 Sample End Time: 12:30 Analytical Data Name (1) Gary Simcox Signature Date 10/22/2021 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 7.28 ft-TOC Total Well Depth: 15.70 ft-TOC Height of Water Column: 8.42 feet Screen Length: 8 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.4 Gal 3 *Well Volume 4.12 Gal 5 *Well Volume 6.87 Gal Purge Method: Peristaltic Pump Start Time: 10:05 End Time: 11:40 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 13.5 ft-TOC Water Column Above Pump Intake: 6.22 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 8.84 ft-TOC Comments: Final Volume Purged: 2.5 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 10:05 0.0 --- --- --- --- --- --- --- --- Start Purging 10:10 0.1 100 7.35 18.7 6.6 185 4.6 131 66.0 10:15 0.3 100 7.35 19.1 6.5 186 4.4 132 77.9 10:20 0.4 100 7.36 19.3 6.5 183 4.3 132 85.3 10:30 0.7 100 7.38 19.5 6.5 179 3.8 131 120 10:40 0.9 100 7.38 19.4 6.5 188 4.1 107 69.3 10:50 1.2 100 7.37 19.4 6.5 190 3.9 101 55.5 11:00 1.5 100 7.37 19.6 6.5 193 3.9 87 34.9 11:10 1.7 100 7.38 19.8 6.5 196 4.0 85 22.8 11:20 2.0 100 7.37 19.9 6.5 197 3.9 85 17.1 11:30 2.2 100 7.37 20.1 6.5 197 3.8 89 13.2 11:40 2.5 100 7.38 20.1 6.5 197 3.8 87 10.1 Method Qty Container Preservative Method Qty Container Preservative Full App II SIM 450052 D-2011 8260 D-SIM 310.2 7470 SIM 2540C-2011 300 Moore County Landfill 356 Turning Leaf Way, Aberdeen, NC 4358-20-043A phase 01 Sample Date: i i E Thursday, October 15, 2020 Project Name: Project Location: Project Number: Client Name/Contact: Water Supply Well ID: PW-1 Weather: Sunny Well Address: Air Temp (°F): 70 ° F Owner Name: Blake POE Present (Y/N): No IOwner Phone No.: Equipment Calibration Information: Equipment Date Time Calibration Solution Calibration Check PH 10/18/21 08:30 4.00, 7.00, 10.00 4.00 7.00 10.00 Conductivity 10/18/21 08:30 1413 Units 1 1,413 Units I Purging Information Purge Rate (GPM): 5.0 Purge Start Time: 18:25 Volume Purged (Gal): 75.0 Purge End Time: 18:40 Parameters and Sampling Total Volume (Gal) Time pH (s.u.) Temperature °C Conductivity PS/cm 75.00 18:40 5.01 17.1 12 Turbidity (NTU) Dissolved Oxygen (mg/L) ORP (mV) 0.45 9.25 141 Sample ID Sample Location Sample Date Sample Time PW-1 Spigot on well house 10/19/2021 18:40 Method Qty Container Pres. Method Qty Container Pres. VOCs 6200 3 40mL VOAs HCl Additional Comments (description of location of sample port, water well, filters, etc.) Site Sketch Signature Simcox Well / System Photographs Date 10/22/2021 Revision: 9/1/17 13:30 Moore County Landfill I 4358-20-043A phase 11 Purge Date: October 19, 2021 Project Name: Project Location: Project Number: Source Well: SW-1 Purge Time: 5 Minutes Locked?: No Sample Date: October 19, 2021 Sampled By: Gary Simcox Sample Time: 17:45 Weather: Sunny Air Temp: 70 ° F Water Level Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow-throughcellvolume) Final: 17:45 17.2 6.4 209 6.7 -18 9.5 End of Purging Sample Method: Sample Start Time: 17:45 Sample End Time: Analytical Data (1) Gary Simcox 1012212021 Notes: Drive on the dirt road to wel MW-2. Park at MW-2 and walk south down a path to the creek. I collected sample SWA at a location marked with 1" vc and red ribbon. The creek has a red tint but good flow. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: ft-TOC Total Well Depth: ft-TOC Height of Water Column: feet Screen Length: feet Stickup: ft-GRID Well Volume Well Diameter 2 inch Water Volume Gal 3 *Well Volume Gal 5 *Well Volume Gal Purge Method: Peristaltic Pump Start Time: 17:40 End Time: 17:45 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: Gallons Used YSI Pro Plus, Final Volume Purge Rate: mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 17:40 0.0 --- --- --- --- --- --- --- --- Start Purging 17:45 17.2 6.4 209 6.7 -18 9.51 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Moore County Landfill I 4358-20-043A phase 11 Purge Date: October 19, 2021 Project Name: Project Location: Project Number: Source Well: SW-2 Purge Time: 10 Minutes Locked?: No Sample Date: October 19, 2021 Sampled By: Gary Simcox Sample Time: 16:55 Weather: Sunny Air Temp: 75 ° F Water Level Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow-throughcellvolume) Final: 16:55 17.6 6.1 31 5.4 127 3.3 End of Purging Sample Method: Sample Start Time: 16:55 Sample End Time: Analytical Data (1) Gary Simcox 1012212021 Notes: I collected sample SW-2 at the end of the trail past the mulch piles. There is a 1" pvc stake with red ribbon marking the location. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: ft-TOC Total Well Depth: ft-TOC Height of Water Column: feet Screen Length: feet Stickup: ft-GRID Well Volume Well Diameter 2 inch Water Volume Gal 3 *Well Volume Gal 5 *Well Volume Gal Purge Method: Peristaltic Pump Start Time: 16:45 End Time: 16:55 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: Gallons Used YSI Pro Plus, Final Volume Purge Rate: mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (pS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 16:45 0.0 --- --- --- --- --- --- --- --- Start Purging 16:55 17.6 6.1 31 5.4 127 3.25 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Project Name: Moore County Landfill I I Project Location: Project Number: 4358-20-043A phase 11 Purge Date: October 19, 2021 Source Well: SW-3 Purge Time: 5 Minutes Locked?: No Sample Date: October 19, 2021 Sampled By: Gary Simcox Sample Time: 17:30 Weather: Sunny Air Temp: 70 ° F Water Level Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow-throughcellvolume) Final: 17:30 17.3 6.5 190 6.0 -25 53.5 End of Purging Sample Method: Sample Start Time: 17:30 Sample End Time: Analytical Data Name Signature Date (1) Gary Simcox 1012212021 Notes: I collected sample SW-3 at a location marked with pink flagging. Drive on the dirt road SE past MW-3 toward MW-2. About 200 yards past MW-3 there is a path marked with ink flagging. Park and walk in another 200 yards to the creek. The creek has a red tint but good flow. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: ft-TOC Total Well Depth: ft-TOC Height of Water Column: feet Screen Length: feet Stickup: ft-GRD Well Volume Well Diameter 2 inch Water Volume Gal 3 *Well Volume Gal 5 *Well Volume Gal Purge Method: Peristaltic Pump Start Time: 17:25 End Time: 17:30 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: Gallons Used YSI Pro Plus, Final Volume Purge Rate: mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 17:25 0.0 --- --- --- --- --- --- --- --- Start Purging 17:30 17.3 6.5 190 6.0 -25 53.5 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Moore County Landfill I 4358-20-043A phase 11 Purge Date: October 19, 2021 Project Name: Project Location: Project Number: Source Well: SW-4 Purge Time: 5 Minutes Locked?: No Sample Date: October 19, 2021 Sampled By: Gary Simcox Sample Time: 17:10 Weather: Sunny Air Temp: 70 ° F Water Level Well Data We Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow-throughcellvolume) Final: 17:10 17.5 6.3 164 7.2 1 9.6 End of Purging Sample Method: Sample Start Time: 17:10 Sample End Time: Analytical Data (1) Gary Simcox 1012212021 Notes: Walked down the slope at Outfall #1. 1 located the surface water (creek) flowing from NE to SW. I collected sample SW-4 approximatley 100' SW of the intersection of Outfall #1 and the creek. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: ft-TOC Total Well Depth: ft-TOC Height of Water Column: feet Screen Length: feet Stickup: ft-GRID Well Volume Well Diameter 2 inch Water Volume Gal 3 *Well Volume Gal 5 *Well Volume Gal Purge Method: Peristaltic Pump Start Time: 17:05 End Time: 17:10 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: Gallons Used YSI Pro Plus, Final Volume Purge Rate: mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (pS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 17:05 0.0 --- --- --- --- --- --- --- --- Start Purging 17:10 17.5 6.3 164 7.2 1 9.56 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Appendix II - Laboratory Analytical Reports 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, November 10, 2021 S&ME, Inc. (SM004) Attn: Edmund Henriques 8646 West Market Street, Suite 105 Greensboro, NC 27409 RE: Laboratory Results for Project Number: 4358-20-043, Project Name/Desc: Moore County Active C & D LF - Fall ENCO Workorder(s): CE16213 Dear Edmund Henriques, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, October 20, 2021. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 0"6LC'=-:;tA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 44 PROJECT NARRATIVE Client: S&ME, Inc. (SM004) Project: Moore County Active C & D LF - Fall Lab ID: CE16213 (� �Eo www.encolabs.com Overview Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on an acceptable LCS recovery (QM-07). Post -digestion spike did not meet method requirements due to confirmed matrix effects (QM-08). Precision between duplicate metrix spikes of the same sample was outside acceptance limits (QM-11). Quality Control Remarks The associated CCV standard exhibited high bias; since the result is ND, there is no impact (QV-01). Other Comments The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Chuck Smith Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 44 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MWS Lab ID: CE16213-01 Sampled: 10/19/21 12:50 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/22/21 00:21 EPA 310.2 NO PREP 11/02/21 10/27/21 14:18 10/27/21 16:26 EPA 353.2 NO PREP 10/21/21 12:50 10/20/21 15:44 10/20/21 17:04 EPA 353.2 [CALC] 10/21/21 12:50 11/02/21 09:11 11/02/21 13:05 EPA 353.2 NO PREP 11/16/21 11/02/21 09:11 11/02/21 13:05 EPA 6010D EPA 3005A 04/17/22 10/26/21 13:10 10/27/21 13:55 EPA 6020E EPA 3005A 04/17/22 11/01/21 05:54 11/04/21 00:52 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:26 10/22/21 08:41 EPA 8260D EPA 503013_MS 11/02/21 10/26/21 11:30 10/26/21 13:09 EPA 8260D EPA 503013_MS 11/02/21 10/29/21 15:00 10/30/21 03:13 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 12:32 SM 254OC-2011 NO PREP 10/26/21 10/25/21 18:14 10/25/21 18:14 SM 4500S2 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MWS Lab ID: CE16213-01RE1 Sampled: 10/19/21 12:50 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 9060A NO PREP 11/16/21 10/27/21 07:24 10/27/21 16:01 Client ID: 6301-MW13SR Lab ID: CE16213-02 Sampled: 10/19/21 10:55 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/22/21 00:39 EPA 310.2 NO PREP 11/02/21 10/27/21 14:18 10/27/21 16:27 EPA 6010D EPA 3005A 04/17/22 10/26/21 13:10 10/27/21 13:57 EPA 6020E EPA 3005A 04/17/22 11/01/21 05:54 11/04/21 00:57 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:26 10/22/21 09:05 EPA 8260D EPA 503013_MS 11/02/21 10/26/21 11:30 10/26/21 13:35 EPA 8260D EPA 503013_MS 11/02/21 10/28/21 12:00 10/30/21 15:36 SM 254OC-2011 NO PREP 10/26/21 10/25/21 18:14 10/25/21 18:14 SM 4500S2 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MW13DR Lab ID: CE16213-03 Sampled: 10/19/21 11:50 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/22/21 00:57 EPA 310.2 NO PREP 11/02/21 10/27/21 14:18 10/27/21 16:28 EPA 6010D EPA 3005A 04/17/22 10/26/21 13:10 10/27/21 14:00 EPA 6020E EPA 3005A 04/17/22 11/01/21 05:54 11/04/21 01:01 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:26 10/22/21 09:06 EPA 8260D EPA 503013_MS 11/02/21 10/26/21 11:30 10/26/21 14:01 EPA 8260D EPA 5030B_MS 11/02/21 10/28/21 12:00 10/30/21 16:03 SM 2540C-2011 NO PREP 10/26/21 10/25/21 18:14 10/25/21 18:14 SM 4500S2 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-SW1 Lab ID: CE16213-04 Sampled: 10/19/21 17:45 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 04/17/22 10/26/21 13:10 10/27/21 14:02 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:26 10/22/21 09:08 EPA 8260D EPA 503013_MS 11/02/21 10/26/21 11:30 10/26/21 14:27 EPA 8260D EPA 5030B_MS 11/02/21 10/28/21 12:00 10/30/21 16:31 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 44 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-SW2 Lab ID: CE16213-05 Sampled: 10/19/21 16:55 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 04/17/22 10/26/21 13:10 10/27/21 14:05 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:26 10/22/21 09:10 EPA 8260D EPA 503013_MS 11/02/21 10/26/21 11:30 10/26/21 14:52 EPA 8260D EPA 503013_MS 11/02/21 10/27/21 17:00 10/28/21 04:06 Client ID: 6301-SW3 Lab ID: CE16213-06 Sampled: 10/19/21 17:30 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 04/17/22 10/27/21 06:21 10/28/21 12:46 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:26 10/22/21 09:12 EPA 8260D EPA 503013_MS 11/02/21 10/26/21 11:30 10/26/21 15:18 EPA 8260D EPA 503013_MS 11/02/21 10/27/21 17:00 10/28/21 04:35 Client ID: 6301-SW4 Lab ID: CE16213-07 Sampled: 10/19/21 17:10 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 04/17/22 10/27/21 06:21 10/28/21 12:49 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:26 10/22/21 09:13 EPA 8260D EPA 503013_MS 11/02/21 10/26/21 11:30 10/26/21 15:44 EPA 8260D EPA 5030B_MS 11/02/21 10/27/21 17:00 10/28/21 05:04 Client ID: 6301-FB Lab ID: CE16213-08 Sampled: 10/19/21 12:00 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 11/02/21 10/26/21 11:30 10/26/21 16:09 EPA 8260D EPA 503013_MS 11/02/21 10/27/21 17:00 10/27/21 22:15 Client ID: 6301-TRIP Lab ID: CE16213-09 Sampled: 10/19/21 10:55 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/02/21 10/27/21 17:00 10/27/21 21:45 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 44 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MWS Lab ID: CE16213-01 Analvte Results Flag MDL Q Units Method Notes Barium - Total 21.6 1.10 10.0 ug/L EPA 6010D Carbon dioxide 22.5 2.07 2.50 mg/L RSK 175 Chloride 3.5 J 2.2 5.0 mg/L EPA 300.0 Manganese - Total 2.13 J 1.50 10.0 ug/L EPA 6010D Nitrate as N 0.94 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.94 0.041 0.10 mg/L EPA 353.2 Sulfate as SO4 2.9 1 2.9 5.0 mg/L EPA 300.0 Client ID: 6301-MW13SR Lab ID: CE16213-02 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 9.2 0.80 2.0 ug/L EPA 8260D Barium - Total 22.9 1.10 10.0 ug/L EPA 6010D Chloride 16 2.2 5.0 mg/L EPA 300.0 cis-1,2-Dichloroethene 1.0 0.15 1.0 ug/L EPA 8260D Iron - Total 58600 22.0 50.0 ug/L EPA 6010D Manganese - Total 560 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 18 2.9 5.0 mg/L EPA 300.0 Sulfide 0.020 J 0.010 0.10 mg/L SM 4500S2 D-2011 Total Alkalinity as CaCO3 43 14 15 mg/L EPA 310.2 Total Dissolved Solids 78 50 50 mg/L SM 2540C-2011 Zinc - Total 26.8 4.40 10.0 ug/L EPA 6010D Client ID: 6301-MW13DR Lab ID: CE16213-03 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 3.3 0.80 2.0 ug/L EPA 8260D Barium - Total 39.6 1.10 10.0 ug/L EPA 6010D Chloride 7.0 2.2 5.0 mg/L EPA 300.0 Iron - Total 8430 22.0 50.0 ug/L EPA 6010D Manganese - Total 71.8 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 8.0 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 26 14 15 mg/L EPA 310.2 Client ID: 6301-SW3 Lab ID: CE16213-04 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 3.2 0.80 2.0 ug/L EPA 8260D Barium - Total 22.4 1.10 10.0 ug/L EPA 6010D Client ID: 6301-SW2 Lab ID: CE16213-05 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 10.7 1.10 10.0 ug/L EPA 6010D Client ID: 6301-SW3 Lab ID: CE16213-06 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 3.6 0.80 2.0 ug/L EPA 8260D Barium - Total 22.8 1.10 10.0 ug/L EPA 6010D Chlorobenzene 0.57 J 0.17 1.0 ug/L EPA 8260D Client ID: 6301-SW4 Lab ID: CE16213-07 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 1.6 1 0.80 2.0 ug/L EPA 8260D Barium - Total 26.6 1.10 10.0 ug/L EPA 6010D Client ID: 6301-FB Lab ID: CE16213-08 Analvte Results Flag MDL PQL Units Method Notes Acetone 10 1 10 20 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 44 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW5 Lab Sample ID:CE16213-01 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 12:50 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1129020 EPA 8260D 10/30/21 03:13 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1129020 EPA 8260D 10/30/21 03:13 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1129020 EPA 8260D 10/30/21 03:13 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1129020 EPA 8260D 10/30/21 03:13 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1129020 EPA 8260D 10/30/21 03:13 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1129020 EPA 8260D 10/30/21 03:13 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1129020 EPA 8260D 10/30/21 03:13 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Naphthalene [91-20-3]^ 0.11 u ug/L 1 0.11 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Tetrahydrofuran [109-99-9]^ 0.53 u ug/L 1 0.53 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1129020 EPA 8260D 10/30/21 03:13 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1129020 EPA 8260D 10/30/21 03:13 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW5 Lab Sample ID:CE16213-01 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 12:50 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1J29020 EPA 8260D 10/30/21 03:13 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J29020 EPA 8260D 10/30/21 03:13 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 61 1 50.0 122 % 53-136 IJ29020 EPA 6260D 10130121 03:13 RKY Dibromofluoromethane 56 1 50.0 112 % 67-129 IJ29020 EPA 6260D 10130121 03:13 RKY Toluene-d8 53 1 50.0 106 % 59-134 IJ29020 EPA 6260D 10130121 03:13 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20029 EPA 7470A 10/22/21 08:41 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1KO1005 EPA 6020B 11/04/21 00:52 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J26004 EPA 6010D 10/27/21 13:55 JDH Barium [7440-39-3]^ 21.6 ug/L 1 1.10 10.0 1126004 EPA 6010D 10/27/21 13:55 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1J26004 EPA 6010D 10/27/21 13:55 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J26004 EPA 6010D 10/27/21 13:55 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:55 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:55 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1J26004 EPA 6010D 10/27/21 13:55 JDH Iron [7439-89-6]^ 22.0 U ug/L 1 22.0 50.0 1J26004 EPA 6010D 10/27/21 13:55 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J26004 EPA 6010D 10/27/21 13:55 JDH Manganese [7439-96-5]^ 2.13 J ug/L 1 1.50 10.0 1126004 EPA 6010D 10/27/21 13:55 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1J26004 EPA 6010D 10/27/21 13:55 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1KO1005 EPA 6020B 11/04/21 00:52 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J26004 EPA 6010D 10/27/21 13:55 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1KO1005 EPA 6020B 11/04/21 00:52 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:55 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1J26004 EPA 6010D 10/27/21 13:55 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 3.5 J mg/L 1 2.2 5.0 1121002 EPA 300.0 10/22/21 00:21 ZGW Nitrate as N [14797-55-8] 0.94 mg/L 1 0.041 0.10 [CALC] EPA 353.2 11/02/21 13:05 JAH Nitrate/Nitrite as N^ 0.94 mg/L 1 0.041 0.10 1K02006 EPA 353.2 11/02/21 13:05 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1J20032 EPA 353.2 10/20/21 17:04 JAH Sulfate as SO4 [14808-79-B]^ 2.9 J mg/L 1 2.9 5.0 1121002 EPA 300.0 10/22/21 00:21 ZGW Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1J22004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 14 U mg/L 1 14 15 1J27021 EPA 310.2 10/27/21 16:26 JAH Total Dissolved Solids^ 50 U mg/L 1 50 50 1J25026 SM 254OC-2011 10/25/21 18:14 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW5 Lab Sample ID:CE16213-01 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 12:50 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J26022 EPA 8260D 10/26/21 13:09 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.3 1 5.00 106 % 75-125 V26022 EPA 6260D 10126121 13:09 KKW Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 22.5 mg/L 1 2.07 2.50 1126005 RSK 175 10/26/21 12:32 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 12:32 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 12:32 JMW Methane [74-82-8] 0.00400 U mg/L 1 0.00400 0.00500 1J26005 RSK 175 10/26/21 12:32 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Total Organic Carbon^ 0.90 U mg/L 1 0.90 1.0 1J27005 EPA 9060A 10/27/21 16:01 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 44 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13SR Lab Sample ID:CE16213-02 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 10:55 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 u ug/L 1 0.23 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 u ug/L 1 0.48 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,2-Dibromoethane [106-93-4]A 0.66 u ug/L 1 0.66 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 u ug/L 1 0.19 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,2-Dichloroethane [107-06-2]A 0.21 u ug/L 1 0.21 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,2-Dichloropropane [78-87-5]A 0.10 u ug/L 1 0.10 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 u ug/L 1 0.19 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1128036 EPA 8260D 10/30/21 15:36 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1128036 EPA 8260D 10/30/21 15:36 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 u ug/L 1 1.1 5.0 1128036 EPA 8260D 10/30/21 15:36 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1128036 EPA 8260D 10/30/21 15:36 RKY Acrylonitrile [107-13-1]A 3.5 u ug/L 1 3.5 10 1128036 EPA 8260D 10/30/21 15:36 RKY Benzene [71-43-2]A 0.15 u ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Bromoform [75-25-2]A 0.22 u ug/L 1 0.22 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1128036 EPA 8260D 10/30/21 15:36 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Chloroform [67-66-3]A 0.18 u ug/L 1 0.18 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY cis-1,2-Dichloroethene [156-59-2]A 1.0 ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Iodomethane [74-88-4]A 1.7 u ug/L 1 1.7 5.0 1128036 EPA 8260D 10/30/21 15:36 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Tetrahydrofuran [109-99-9]A 0.53 u ug/L 1 0.53 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Toluene [108-88-3]A 0.14 u ug/L 1 0.14 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 u ug/L 1 0.21 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Trichloroethene [79-01-6]A 0.15 u ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Trichlorofluoromethane [75-69-4]A 0.24 u ug/L 1 0.24 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1128036 EPA 8260D 10/30/21 15:36 RKY Vinyl chloride [75-01-4]A 0.32 u ug/L 1 0.32 1.0 1128036 EPA 8260D 10/30/21 15:36 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13SR Lab Sample ID:CE16213-02 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 10:55 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J28036 EPA 8260D 10/30/21 15:36 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 61 1 50.0 121 % 53-136 IJ28036 EPA 6260D 10130121 15:36 RKY Dlbromofluoromethane 52 1 50.0 105 % 67-129 IJ28036 EPA 6260D 10130121 15:36 RKY Toluene-c48 49 1 50.0 98 % 59-134 1J28036 EPA 6260D 10130121 15:36 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed gy Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20029 EPA 7470A 10/22/21 09:05 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed By Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1KO1005 EPA 6020B 11/04/21 00:57 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J26004 EPA 6010D 10/27/21 13:57 JDH Barium [7440-39-3]^ 22.9 ug/L 1 1.10 10.0 1126004 EPA 6010D 10/27/21 13:57 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1J26004 EPA 6010D 10/27/21 13:57 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J26004 EPA 6010D 10/27/21 13:57 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:57 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:57 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1J26004 EPA 6010D 10/27/21 13:57 JDH Iron [7439-89-6]^ 58600 ug/L 1 22.0 50.0 1126004 EPA 6010D 10/27/21 13:57 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J26004 EPA 6010D 10/27/21 13:57 JDH Manganese [7439-96-5]^ 560 ug/L 1 1.50 10.0 1126004 EPA 6010D 10/27/21 13:57 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1J26004 EPA 6010D 10/27/21 13:57 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1KO1005 EPA 6020B 11/04/21 00:57 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J26004 EPA 6010D 10/27/21 13:57 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1KO1005 EPA 6020B 11/04/21 00:57 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:57 JDH Zinc [7440-66-6]^ 26.8 ug/L 1 4.40 10.0 1126004 EPA 6010D 10/27/21 13:57 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed By Notes Chloride [16887-00-6]^ 16 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/22/21 00:39 ZGW Sulfate as SO4 [14808-79-B]^ 18 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/22/21 00:39 ZGW Sulfide [18496-25-8]^ 0.020 J mg/L 1 0.010 0.10 1122004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 43 mg/L 1 14 15 1127021 EPA 310.2 10/27/21 16:27 JAH Total Dissolved Solids^ 78 mg/L 1 50 50 1125026 SM 254OC-2011 10/25/21 18:14 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13SR Lab Sample ID:CE16213-02 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 10:55 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 9.2 ug/L 1 0.80 2.0 1326022 EPA 8260D 10/26/21 13:35 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.4 1 5.00 107 % 75-125 V26022 EPA 6260D 10126121 13:35 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 44 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13DR Lab Sample ID:CE16213-03 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 11:50 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1128036 EPA 8260D 10/30/21 16:03 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1128036 EPA 8260D 10/30/21 16:03 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1128036 EPA 8260D 10/30/21 16:03 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1128036 EPA 8260D 10/30/21 16:03 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1128036 EPA 8260D 10/30/21 16:03 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1128036 EPA 8260D 10/30/21 16:03 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1128036 EPA 8260D 10/30/21 16:03 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Tetrahydrofuran [109-99-9]^ 0.53 u ug/L 1 0.53 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1128036 EPA 8260D 10/30/21 16:03 RKY Vinyl chloride [75-01-4]^ 0.32 u ug/L 1 0.32 1.0 1128036 EPA 8260D 10/30/21 16:03 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13DR Lab Sample ID:CE16213-03 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 11:50 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J28036 EPA 8260D 10/30/21 16:03 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 59 1 50.0 119 % 53-136 IJ28036 EPA 6260D 10130121 16:03 RKY Dlbromofluoromethane 59 1 50.0 117 % 67-129 IJ28036 EPA 6260D 10130121 16:03 RKY Toluene-c48 50 1 50.0 101 % 59-134 1J28036 EPA 6260D 10130121 16:03 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed gy Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20029 EPA 7470A 10/22/21 09:06 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed By Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1KO1005 EPA 6020B 11/04/21 01:01 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J26004 EPA 6010D 10/27/21 14:00 JDH Barium [7440-39-3]^ 39.6 ug/L 1 1.10 10.0 1126004 EPA 6010D 10/27/21 14:00 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1J26004 EPA 6010D 10/27/21 14:00 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J26004 EPA 6010D 10/27/21 14:00 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 14:00 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 14:00 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1J26004 EPA 6010D 10/27/21 14:00 JDH Iron [7439-89-6]^ 8430 ug/L 1 22.0 50.0 1126004 EPA 6010D 10/27/21 14:00 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J26004 EPA 6010D 10/27/21 14:00 JDH Manganese [7439-96-S]^ 71.8 ug/L 1 1.50 10.0 1126004 EPA 6010D 10/27/21 14:00 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1J26004 EPA 6010D 10/27/21 14:00 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1KO1005 EPA 6020B 11/04/21 01:01 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J26004 EPA 6010D 10/27/21 14:00 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1KO1005 EPA 6020B 11/04/21 01:01 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 14:00 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1J26004 EPA 6010D 10/27/21 14:00 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed By Notes Chloride [16887-00-6]^ 7.0 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/22/21 00:57 ZGW Sulfate as SO4 [14808-79-B]^ 8.0 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/22/21 00:57 ZGW Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1J22004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 26 mg/L 1 14 15 1127021 EPA 310.2 10/27/21 16:28 JAH Total Dissolved Solids^ 50 U mg/L 1 50 50 1J25026 SM 254OC-2011 10/25/21 18:14 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13DR Lab Sample ID:CE16213-03 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 11:50 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 3.3 ug/L 1 0.80 2.0 1326022 EPA 8260D 10/26/21 14:01 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.4 1 5.00 108 % 75-125 V26022 EPA 6260D 10126121 14:01 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 44 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW1 Lab Sample ID:CE16213-04 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 17:45 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1128036 EPA 8260D 10/30/21 16:31 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1128036 EPA 8260D 10/30/21 16:31 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1128036 EPA 8260D 10/30/21 16:31 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1128036 EPA 8260D 10/30/21 16:31 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1128036 EPA 8260D 10/30/21 16:31 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1128036 EPA 8260D 10/30/21 16:31 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Ethylbenzene [500-41-4]A 0.13 u ug/L 1 0.13 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1128036 EPA 8260D 10/30/21 16:31 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Naphthalene [91-20-3]^ 0.11 u ug/L 1 0.11 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Tetrahydrofuran [109-99-9]^ 0.53 u ug/L 1 0.53 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1128036 EPA 8260D 10/30/21 16:31 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1128036 EPA 8260D 10/30/21 16:31 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SWI Lab Sample ID:CE16213-04 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 17:45 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1J28036 EPA 8260D 10/30/21 16:31 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J28036 EPA 8260D 10/30/21 16:31 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 58 1 50.0 117 % 53-136 IJ28036 EPA 6260D 10130121 16:31 RKY Dibromofluoromethane 56 1 50.0 112 % 67-129 IJ28036 EPA 6260D 10130121 16:31 RKY Toluene-d8 52 1 50.0 103 % 59-134 1J28036 EPA 6260D 10130121 16:31 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20029 EPA 7470A 10/22/21 09:08 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J26004 EPA 6010D 10/27/21 14:02 JDH Barium [7440-39-3]^ 22.4 ug/L 1 1.10 10.0 1126004 EPA 6010D 10/27/21 14:02 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J26004 EPA 6010D 10/27/21 14:02 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 14:02 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J26004 EPA 6010D 10/27/21 14:02 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J26004 EPA 6010D 10/27/21 14:02 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J26004 EPA 6010D 10/27/21 14:02 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 3.2 ug/L 1 0.80 2.0 1126022 EPA 8260D 10/26/21 14:27 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.1 1 5.00 101 % 75-125 IJ26022 EPA 8260D 10126121 14:27 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 44 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW2 Lab Sample ID:CE16213-05 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 16:55 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analvte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1127031 EPA 8260D 10/28/21 04:06 RKY QV-01 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1127031 EPA 8260D 10/28/21 04:06 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1127031 EPA 8260D 10/28/21 04:06 RKY QV-01 Acetone [67-64-1]A 10 u ug/L 1 10 20 1127031 EPA 8260D 10/28/21 04:06 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1127031 EPA 8260D 10/28/21 04:06 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY QV-01 Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1127031 EPA 8260D 10/28/21 04:06 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY QV-01 Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY QV-01 Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1127031 EPA 8260D 10/28/21 04:06 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY QV-01 Naphthalene [91-20-3]^ 0.11 u ug/L 1 0.11 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Tetrahydrofuran [109-99-9]^ 0.53 u ug/L 1 0.53 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1127031 EPA 8260D 10/28/21 04:06 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1127031 EPA 8260D 10/28/21 04:06 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW2 Lab Sample ID:CE16213-05 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 16:55 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1J27031 EPA 8260D 10/28/21 04:06 RKY QV-01 Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27031 EPA 8260D 10/28/21 04:06 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 100 % 53-136 IJ27031 EPA 6260D 10128121 04:06 RKY Dibromofluoromethane 50 1 50.0 100 % 67-129 IJ27031 EPA 6260D 10128121 04:06 RKY Toluene-d8 51 1 50.0 102 % 59-134 IJ27031 EPA 6260D 10126121 04:06 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20029 EPA 7470A 10/22/21 09:10 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J26004 EPA 6010D 10/27/21 14:05 JDH Barium [7440-39-3]^ 10.7 ug/L 1 1.10 10.0 1126004 EPA 6010D 10/27/21 14:05 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J26004 EPA 6010D 10/27/21 14:05 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 14:05 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J26004 EPA 6010D 10/27/21 14:05 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J26004 EPA 6010D 10/27/21 14:05 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J26004 EPA 6010D 10/27/21 14:05 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte MAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J26022 EPA 8260D 10/26/21 14:52 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.4 1 5.00 108 % 75-125 IJ26022 EPA 8260D 10126121 14:52 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 44 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW3 Lab Sample ID:CE16213-06 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 17:30 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 1,2-Dibromoethane [106-93-4]A 0.66 u ug/L 1 0.66 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 1,2-Dichloroethane [107-06-2]A 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 1,2-Dichloropropane [78-87-5]A 0.10 u ug/L 1 0.10 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1127031 EPA 8260D 10/28/21 04:35 RKY QV-01 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1127031 EPA 8260D 10/28/21 04:35 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 u ug/L 1 1.1 5.0 1127031 EPA 8260D 10/28/21 04:35 RKY QV-01 Acetone [67-64-1]A 10 u ug/L 1 10 20 1127031 EPA 8260D 10/28/21 04:35 RKY Acrylonitrile [107-13-1]A 3.5 u ug/L 1 3.5 10 1127031 EPA 8260D 10/28/21 04:35 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY QV-01 Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY QV-01 Bromoform [75-25-2]A 0.22 u ug/L 1 0.22 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1127031 EPA 8260D 10/28/21 04:35 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY QV-01 Chlorobenzene [108-90-7]A 0.57 J ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Chloroform [67-66-3]A 0.18 u ug/L 1 0.18 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY QV-01 Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY cis-1,2-Dichloroethene [156-59-2]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Iodomethane [74-88-4]A 1.7 u ug/L 1 1.7 5.0 1127031 EPA 8260D 10/28/21 04:35 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY QV-01 Naphthalene [91-20-3]A 0.11 u ug/L 1 0.11 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Tetrahydrofuran [109-99-9]A 0.53 u ug/L 1 0.53 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Toluene [108-88-3]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Trichloroethene [79-01-6]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Trichlorofluoromethane [75-69-4]A 0.24 u ug/L 1 0.24 1.0 1127031 EPA 8260D 10/28/21 04:35 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1127031 EPA 8260D 10/28/21 04:35 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW3 Lab Sample ID:CE16213-06 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 17:30 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1J27031 EPA 8260D 10/28/21 04:35 RKY QV-01 Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27031 EPA 8260D 10/28/21 04:35 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 51 1 50.0 101 % 53-136 IJ27031 EPA 6260D 10128121 04:35 RKY Dibromofluoromethane 50 1 50.0 100 % 67-129 IJ27031 EPA 6260D 10128121 04:35 RKY Toluene-d8 51 1 50.0 103 % 59-134 IJ27031 EPA 6260D 10126121 04:35 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20029 EPA 7470A 10/22/21 09:12 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J27004 EPA 6010D 10/28/21 12:46 JDH Barium [7440-39-3]^ 22.8 ug/L 1 1.10 10.0 1127004 EPA 6010D 10/28/21 12:46 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J27004 EPA 6010D 10/28/21 12:46 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J27004 EPA 6010D 10/28/21 12:46 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J27004 EPA 6010D 10/28/21 12:46 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J27004 EPA 6010D 10/28/21 12:46 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J27004 EPA 6010D 10/28/21 12:46 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 3.6 ug/L 1 0.80 2.0 1126022 EPA 8260D 10/26/21 15:18 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.0 1 5.00 101 % 75-125 1J26022 EPA 8260D 10126121 15:18 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 44 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW4 Lab Sample ID:CE16213-07 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 17:10 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1127031 EPA 8260D 10/28/21 05:04 RKY QV-01 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1127031 EPA 8260D 10/28/21 05:04 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1127031 EPA 8260D 10/28/21 05:04 RKY QV-01 Acetone [67-64-1]A 10 u ug/L 1 10 20 1127031 EPA 8260D 10/28/21 05:04 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1127031 EPA 8260D 10/28/21 05:04 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY QV-01 Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1127031 EPA 8260D 10/28/21 05:04 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY QV-01 Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY QV-01 Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1127031 EPA 8260D 10/28/21 05:04 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY QV-01 Naphthalene [91-20-3]^ 0.11 u ug/L 1 0.11 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Tetrahydrofuran [109-99-9]^ 0.53 u ug/L 1 0.53 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1127031 EPA 8260D 10/28/21 05:04 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1127031 EPA 8260D 10/28/21 05:04 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW4 Lab Sample ID:CE16213-07 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 17:10 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1J27031 EPA 8260D 10/28/21 05:04 RKY QV-01 Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27031 EPA 8260D 10/28/21 05:04 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 101 % 53-136 IJ27031 EPA 6260D 10128121 05:04 RKY Dibromofluoromethane 50 1 50.0 101 % 67-129 IJ27031 EPA 6260D 10128121 05:04 RKY Toluene-d8 52 1 50.0 103 % 59-134 IJ27031 EPA 6260D 10126121 05:04 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20029 EPA 7470A 10/22/21 09:13 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J27004 EPA 6010D 10/28/21 12:49 JDH Barium [7440-39-3]^ 26.6 ug/L 1 1.10 10.0 1127004 EPA 6010D 10/28/21 12:49 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J27004 EPA 6010D 10/28/21 12:49 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J27004 EPA 6010D 10/28/21 12:49 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J27004 EPA 6010D 10/28/21 12:49 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J27004 EPA 6010D 10/28/21 12:49 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J27004 EPA 6010D 10/28/21 12:49 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.6 J ug/L 1 0.80 2.0 1126022 EPA 8260D 10/26/21 15:44 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.4 1 5.00 108 % 75-125 1J26022 EPA 8260D 10126121 15:44 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 44 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-FB Lab Sample ID:CE16213-08 Received: 10/20/21 10:20 Matrix: Water Sampled:10/19/21 12:00 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 1,2-Dibromoethane [106-93-4]A 0.66 u ug/L 1 0.66 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 1,2-Dichloroethane [107-06-2]A 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 1,2-Dichloropropane [78-87-5]A 0.10 u ug/L 1 0.10 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1127031 EPA 8260D 10/27/21 22:15 RKY QV-01 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1127031 EPA 8260D 10/27/21 22:15 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 u ug/L 1 1.1 5.0 1127031 EPA 8260D 10/27/21 22:15 RKY QV-01 Acetone [67-64-1]A 10 J ug/L 1 10 20 1127031 EPA 8260D 10/27/21 22:15 RKY Acrylonitrile [107-13-1]A 3.5 u ug/L 1 3.5 10 1127031 EPA 8260D 10/27/21 22:15 RKY Benzene [71-43-2]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY QV-01 Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY QV-01 Bromoform [75-25-2]A 0.22 u ug/L 1 0.22 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1127031 EPA 8260D 10/27/21 22:15 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY QV-01 Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Chloroform [67-66-3]A 0.18 u ug/L 1 0.18 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY QV-01 Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY cis-1,2-Dichloroethene [156-59-2]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Iodomethane [74-88-4]A 1.7 u ug/L 1 1.7 5.0 1127031 EPA 8260D 10/27/21 22:15 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY QV-01 Naphthalene [91-20-3]A 0.11 u ug/L 1 0.11 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Tetrahydrofuran [109-99-9]A 0.53 u ug/L 1 0.53 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Toluene [108-88-3]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Trichloroethene [79-01-6]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Trichlorofluoromethane [75-69-4]A 0.24 u ug/L 1 0.24 1.0 1127031 EPA 8260D 10/27/21 22:15 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1127031 EPA 8260D 10/27/21 22:15 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-FB Lab Sample ID:CE16213-08 Received: 10/20/21 10:20 Matrix: Water Sampled:10/19/21 12:00 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1J27031 EPA 8260D 10/27/21 22:15 RKY QV-01 Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27031 EPA 8260D 10/27/21 22:15 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 51 1 50.0 101 % 53-136 IJ27031 EPA 6260D 10127121 22:15 RKY Dibromofluoromethane 49 1 50.0 98 % 67-129 IJ27031 EPA 6260D 10127121 22:15 RKY Toluene-d8 51 1 50.0 103 % 59-134 IJ27031 EPA 6260D 10127121 22:15 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J26022 EPA 8260D 10/26/21 16:09 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.3 1 5.00 106 % 75-125 IJ26022 EPA 8260D 10126121 16:09 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 44 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-TRIP Lab Sample ID:CE16213-09 Received: 10/20/21 10:20 Matrix: Water Sampled:10/19/21 10:55 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1127031 EPA 8260D 10/27/21 21:45 RKY QV-01 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1127031 EPA 8260D 10/27/21 21:45 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1127031 EPA 8260D 10/27/21 21:45 RKY QV-01 Acetone [67-64-1]A 10 u ug/L 1 10 20 1127031 EPA 8260D 10/27/21 21:45 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1127031 EPA 8260D 10/27/21 21:45 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY QV-01 Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1127031 EPA 8260D 10/27/21 21:45 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY QV-01 Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY QV-01 Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Ethylbenzene [500-41-4]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1127031 EPA 8260D 10/27/21 21:45 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY QV-01 Naphthalene [91-20-3]^ 0.11 u ug/L 1 0.11 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Tetrahydrofuran [109-99-9]^ 0.53 u ug/L 1 0.53 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1127031 EPA 8260D 10/27/21 21:45 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1127031 EPA 8260D 10/27/21 21:45 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 44 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-TRIP Lab Sample ID:CE16213-09 Received: 10/20/21 10:20 Matrix: Water Sampled:10/19/21 10:55 Work Order: CE16213 Project: Moore County Active C & D LF - Fall Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1J27031 EPA 8260D 10/27/21 21:45 RKY QV-01 Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27031 EPA 8260D 10/27/21 21:45 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 101 % 53-136 IJ27031 EPA 6260D 10127121 21:45 RKY Dlbromofluoromethane 50 1 50.0 100 % 67-129 IJ27031 EPA 6260D 10127121 21:45 RKY Toluene-d8 51 1 50.0 101 % 59-134 IJ27031 EPA 6260D 10127121 21:45 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 44 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1127031 - EPA 5030B MS Blank (1327031-BLK1) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 20:47 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 44 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1127031 - EPA 5030B MS - Continued (� �Eo www.encolabs.com Blank (1327031-BLK1) Continued Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 20:47 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 50 u91L 50.0 99 53-136 Dibromofluoromethane 49 u91L 50.0 98 67-129 Toluene-d8 50 u91L 50.0 101 59-134 LCS (1327031-BS1) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 18:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 24 1.0 ug/L 20.0 122 75-133 Benzene 24 1.0 ug/L 20.0 120 80-134 Chlorobenzene 19 1.0 ug/L 20.0 95 80-120 Toluene 20 1.0 ug/L 20.0 99 71-120 Trichloroethene 21 1.0 ug/L 20.0 107 74-120 Matrix Spike (1J27031-MS1) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 19:19 Source: CE16369-11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 24 1.0 ug/L 20.0 0.21 U 118 75-133 Benzene 23 1.0 ug/L 20.0 0.15 U 117 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 97 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 99 71-120 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 108 74-120 Matrix Spike Dup (1J27031-MSD1) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 19:48 Source: CE16369-11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 25 1.0 ug/L 20.0 0.21 U 123 75-133 4 20 Benzene 24 1.0 ug/L 20.0 0.15 U 118 80-134 0.6 17 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 98 80-120 0.8 16 Toluene 20 1.0 ug/L 20.0 0.14 U 99 71-120 0.4 17 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 110 74-120 2 22 Batch 1128036 - EPA 5030B MS Blank (1328036-BLK1) Prepared: 10/28/2021 12:00 Analyzed: 10/30/2021 08:15 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 44 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IJ28036 - EPA 5030B MS - Continued Blank (1328036-BLK1) Continued Prepared: 10/28/2021 12:00 Analyzed: 10/30/2021 08:15 Analvte Result Flaq POL Units 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 60 u91L 50.0 121 53-136 Dibromofluoromethane 55 u91L 50.0 109 67-129 Toluene-d8 50 u91L 50.0 100 59-134 LCS (1328036-BS1) Prepared: 10/28/2021 12:00 Analyzed: 10/30/2021 06:25 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 92 75-133 Benzene 16 1.0 ug/L 20.0 82 80-134 Chlorobenzene 18 1.0 ug/L 20.0 92 80-120 Toluene 22 1.0 ug/L 20.0 110 71-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 29 of 44 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1128036 - EPA 5030B MS - Continued LCS (1328036-BS1) Continued Prepared: 10/28/2021 12:00 Analyzed: 10/30/2021 06:25 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Trichloroethene 17 1.0 ug/L 20.0 87 74-120 Matrix Spike (1728036-MS1) Prepared: 10/28/2021 12:00 Analyzed: 10/30/2021 06:53 Source: CE16369-12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 0.21 U 108 75-133 Benzene 19 1.0 ug/L 20.0 0.15 U 93 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 94 80-120 Toluene 22 1.0 ug/L 20.0 0.14 U 110 71-120 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 99 74-120 Matrix Spike Dup (1328036-MSD1) Prepared: 10/28/2021 12:00 Analyzed: 10/30/2021 07:20 Source: CE16369-12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 99 75-133 8 20 Benzene 18 1.0 ug/L 20.0 0.15 U 90 80-134 3 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 90 80-120 5 16 Toluene 22 1.0 ug/L 20.0 0.14 U 108 71-120 2 17 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 93 74-120 6 22 Batch 1129020 - EPA 5030B MS Blank (1129020-BLK3) Prepared: 10/29/2021 15:00 Analyzed: 10/29/2021 18:58 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 30 of 44 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IJ29020 - EPA 5030B MS - Continued Blank (1329020-BLK1) Continued Prepared: 10/29/2021 15:00 Analyzed: 10/29/2021 18:58 Analvte Result Flaq POL Units Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 59 u9/L 50.0 119 53-136 Dlbromofluoromethane 58 u9/L 50.0 115 67-129 Toluene-d8 52 u9/L 50.0 104 59-134 LCS (1729020-BS1) Prepared: 10/29/2021 15:00 Analyzed: 10/29/2021 17:07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 96 75-133 Benzene 17 1.0 ug/L 20.0 86 80-134 Chlorobenzene 18 1.0 ug/L 20.0 92 80-120 Toluene 21 1.0 ug/L 20.0 107 71-120 Trichloroethene 19 1.0 ug/L 20.0 95 74-120 Matrix Spike (1329020-MS1) Prepared: 10/29/2021 15:00 Analyzed: 10/29/2021 17:35 Source: CE16465-08 Spike Source %REC Analvte Result Flaq POL Units Level Result %REC Limits RPD 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 98 75-133 Benzene 20 1.0 ug/L 20.0 0.15 U 100 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 100 80-120 Toluene 23 1.0 ug/L 20.0 0.14 U 114 71-120 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 99 74-120 RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 31 of 44 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1129020 - EPA 5030B MS - Continued (� �Eo www.encolabs.com Matrix Spike Dup (1329020-MSDI) Prepared: 10/29/2021 15:00 Analyzed: 10/29/2021 18:03 Source: CE16465-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 97 75-133 1 20 Benzene 18 1.0 ug/L 20.0 0.15 U 88 80-134 12 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 95 80-120 4 16 Toluene 23 1.0 ug/L 20.0 0.14 U 115 71-120 0.3 17 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 96 74-120 3 22 Metals by EPA 6000/7000 Series Methods - Quality Control Batch V20019 - EPA 245.1 Blank (1320029-BLK3) Prepared: 10/20/2021 15:26 Analyzed: 10/22/2021 08:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L LCS (1J20029-BSI) Prepared: 10/20/2021 15:26 Analyzed: 10/22/2021 08:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.07 0.200 ug/L 5.00 101 80-120 Matrix Spike (1320029-MS1) Prepared: 10/20/2021 15:26 Analyzed: 10/22/2021 08:45 Source: CE16213-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.79 0.200 ug/L 5.00 0.150 U 96 75-125 Matrix Spike Dup (1320029-MSD1) Prepared: 10/20/2021 15:26 Analyzed: 10/22/2021 08:47 Source: CE16213-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.99 0.200 ug/L 5.00 0.150 U 100 75-125 4 25 Post Spike (1320029-PS1) Prepared: 10/20/2021 15:26 Analyzed: 10/22/2021 08:49 Source: CE16213-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.53 0.200 ug/L 4.76 0.00533 116 75-125 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1116004 - EPA 3005A Blank (1126004-BLK3) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:06 Analvte Result Flaq POL Units Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Beryllium 0.160 U 1.00 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Cobalt 1.40 U 10.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 32 of 44 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch IJ26004 - EPA 3005A - Continued Blank (1326004-BLK1) Continued Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Manganese 1.50 U 10.0 ug/L Nickel 2.20 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L Vanadium 1.40 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (1326004-BS1) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 201 10.0 ug/L 200 100 80-120 Barium 203 10.0 ug/L 200 101 80-120 Beryllium 19.5 1.00 ug/L 20.0 98 80-120 Cadmium 20.0 1.00 ug/L 20.0 100 80-120 Chromium 196 10.0 ug/L 200 98 80-120 Cobalt 201 10.0 ug/L 200 101 80-120 Copper 193 10.0 ug/L 200 97 80-120 Iron 988 50.0 ug/L 1000 99 80-120 Lead 198 10.0 ug/L 200 99 80-120 Manganese 194 10.0 ug/L 200 97 80-120 Nickel 202 10.0 ug/L 200 101 80-120 Selenium 201 10.0 ug/L 200 101 80-120 Silver 197 10.0 ug/L 200 99 80-120 Vanadium 192 10.0 ug/L 200 96 80-120 Zinc 206 10.0 ug/L 200 103 80-120 Matrix Spike (1326004-MS1) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:14 Source: CE15202-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 193 10.0 ug/L 200 7.60 U 97 75-125 Barium 241 10.0 ug/L 200 45.7 97 75-125 Beryllium 18.9 1.00 ug/L 20.0 0.160 U 95 75-125 Cadmium 19.1 1.00 ug/L 20.0 0.360 U 96 75-125 Chromium 190 10.0 ug/L 200 1.40 U 95 75-125 Cobalt 194 10.0 ug/L 200 1.40 U 97 75-125 Copper 186 10.0 ug/L 200 1.60 U 93 75-125 Iron 1110 50.0 ug/L 1000 152 96 75-125 Lead 193 10.0 ug/L 200 3.10 U 97 75-125 Manganese 213 10.0 ug/L 200 24.7 94 75-125 Nickel 196 10.0 ug/L 200 2.20 U 98 75-125 Selenium 189 10.0 ug/L 200 6.20 U 95 75-125 Silver 191 10.0 ug/L 200 1.90 U 95 75-125 Vanadium 186 10.0 ug/L 200 1.40 U 93 75-125 Zinc 199 10.0 ug/L 200 4.40 U 99 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 33 of 44 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch IJ26004 - EPA 3005A - Continued Matrix Spike Dup (1326004-MSDI) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:16 Source: CE15202-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 192 10.0 ug/L 200 7.60 U 96 75-125 0.9 20 Barium 243 10.0 ug/L 200 45.7 98 75-125 0.8 20 Beryllium 19.2 1.00 ug/L 20.0 0.160 U 96 75-125 1 20 Cadmium 19.5 1.00 ug/L 20.0 0.360 U 97 75-125 2 20 Chromium 192 10.0 ug/L 200 1.40 U 96 75-125 1 20 Cobalt 195 10.0 ug/L 200 1.40 U 98 75-125 0.6 20 Copper 189 10.0 ug/L 200 1.60 U 95 75-125 2 20 Iron 1130 50.0 ug/L 1000 152 98 75-125 2 20 Lead 193 10.0 ug/L 200 3.10 U 97 75-125 0.03 20 Manganese 216 10.0 ug/L 200 24.7 96 75-125 2 20 Nickel 198 10.0 ug/L 200 2.20 U 99 75-125 1 20 Selenium 195 10.0 ug/L 200 6.20 U 97 75-125 3 20 Silver 194 10.0 ug/L 200 1.90 U 97 75-125 2 20 Vanadium 188 10.0 ug/L 200 1.40 U 94 75-125 1 20 Zinc 201 10.0 ug/L 200 4.40 U 100 75-125 0.9 20 Post Spike (1326004-PS1) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:19 Source: CE15202-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.195 0.0100 mg/L 0.200 0.00236 96 80-120 Barium 0.245 0.0100 mg/L 0.200 0.0457 100 80-120 Beryllium 0.0194 0.00100 mg/L 0.0200 5.99E-6 97 80-120 Cadmium 0.0198 0.00100 mg/L 0.0200 2.87E-5 99 80-120 Chromium 0.195 0.0100 mg/L 0.200 -0.000188 97 80-120 Cobalt 0.199 0.0100 mg/L 0.200 0.000139 99 80-120 Copper 0.193 0.0100 mg/L 0.200 -0.000286 96 80-120 Iron 1.13 0.0500 mg/L 1.00 0.152 98 80-120 Lead 0.197 0.0100 mg/L 0.200 -0.00153 99 80-120 Manganese 0.218 0.0100 mg/L 0.200 0.0247 97 80-120 Nickel 0.201 0.0100 mg/L 0.200 0.000521 100 80-120 Selenium 0.201 0.0100 mg/L 0.200 -0.00717 101 80-120 Silver 0.198 0.0100 mg/L 0.200 0.000123 99 80-120 Vanadium 0.191 0.0100 mg/L 0.200 0.000419 95 80-120 Zinc 0.212 0.0100 mg/L 0.200 0.00232 105 80-120 Batch IJ27004 - EPA 3005A Blank (1327004-BLKI) Prepared: 10/27/2021 06:21 Analyzed: 10/28/2021 11:34 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Lead 3.10 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 34 of 44 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch IJ27004 - EPA 3005A - Continued LCS (1327004-BSI) Prepared: 10/27/2021 06:21 Analyzed: 10/28/2021 11:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 200 10.0 ug/L 200 100 80-120 Barium 207 10.0 ug/L 200 104 80-120 Cadmium 20.3 1.00 ug/L 20.0 102 80-120 Chromium 198 10.0 ug/L 200 99 80-120 Lead 203 10.0 ug/L 200 101 80-120 Selenium 210 10.0 ug/L 200 105 80-120 Silver 201 10.0 ug/L 200 100 80-120 Matrix Spike (1327004-MS1) Prepared: 10/27/2021 06:21 Analyzed: 10/28/2021 11:42 Source: CE16233-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 189 10.0 ug/L 200 7.60 U 94 75-125 Barium 807 10.0 ug/L 200 618 94 75-125 Cadmium 18.6 1.00 ug/L 20.0 0.360 U 93 75-125 Chromium 198 10.0 ug/L 200 1.40 U 99 75-125 Lead 194 10.0 ug/L 200 3.10 U 97 75-125 Selenium 196 10.0 ug/L 200 6.20 U 98 75-125 Silver 200 10.0 ug/L 200 1.90 U 100 75-125 Matrix Spike Dup (1]27004-MSDI) Prepared: 10/27/2021 06:21 Analyzed: 10/28/2021 12:39 Source: CE16233-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 189 10.0 ug/L 200 7.60 U 95 75-125 0.2 20 Barium 803 10.0 ug/L 200 618 93 75-125 0.4 20 Cadmium 18.7 1.00 ug/L 20.0 0.360 U 93 75-125 0.4 20 Chromium 197 10.0 ug/L 200 1.40 U 99 75-125 0.3 20 Lead 198 10.0 ug/L 200 3.10 U 99 75-125 2 20 Selenium 204 10.0 ug/L 200 6.20 U 102 75-125 4 20 Silver 201 10.0 ug/L 200 1.90 U 100 75-125 0.7 20 Post Spike (1327004-PS1) Prepared: 10/27/2021 06:21 Analyzed: 10/28/2021 12:41 Source: CE16233-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.171 0.0100 mg/L 0.200 -0.0138 86 80-120 Barium 0.794 0.0100 mg/L 0.200 0.618 88 80-120 Cadmium 0.0169 0.00100 mg/L 0.0200 -0.00102 84 80-120 Chromium 0.181 0.0100 mg/L 0.200 0.000873 90 80-120 Lead 0.176 0.0100 mg/L 0.200 -0.00139 88 80-120 Selenium 0.179 0.0100 mg/L 0.200 -0.0125 90 80-120 Silver 0.184 0.0100 mg/L 0.200 -0.000426 92 80-120 Batch 1KO1005 - EPA 3005A Blank (1K03005-BLK1) Prepared: 11/01/2021 05:54 Analyzed: 11/03/2021 21:30 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 0.370 U 1.00 ug/L Selenium 0.910 U 1.00 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 35 of 44 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch IK01005 - EPA 3005A - Continued Blank (SK01005-BLKS) Continued Prepared: 11/01/2021 05:54 Analyzed: 11/03/2021 21:30 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Thallium 0.110 U 1.00 ug/L LCS (1K01005-BS3) Prepared: 11/01/2021 05:54 Analyzed: 11/03/2021 21:34 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 24.3 1.00 ug/L 20.0 121 80-120 Selenium 23.1 1.00 ug/L 20.0 115 80-120 Thallium 23.9 1.00 ug/L 20.0 120 80-120 Matrix Spike (1K01005-MS3) Prepared: 11/01/2021 05:54 Analyzed: 11/03/2021 21:38 Source: CE15945-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 51.2 2.00 ug/L 40.0 0.740 U 128 75-125 QM-07 Selenium 49.4 2.00 ug/L 40.0 1.82 U 123 75-125 Thallium 49.9 2.00 ug/L 40.0 0.220 U 125 75-125 Matrix Spike Dup (1K03005-MSD3) Prepared: 11/01/2021 05:54 Analyzed: 11/03/2021 21:42 Source: CE15945-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 52.9 2.00 ug/L 40.0 0.740 U 132 75-125 3 20 QM-07 Selenium 51.1 2.00 ug/L 40.0 1.82 U 128 75-125 3 20 QM-07 Thallium 50.3 2.00 ug/L 40.0 0.220 U 126 75-125 0.7 20 QM-07 Post Spike (1K01005-PS3) Prepared: 11/01/2021 05:54 Analyzed: 11/03/2021 21:47 Source: CE15945-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 26.3 1.00 ug/L 20.0 0.0497 131 75-125 QM-08 Selenium 26.1 1.00 ug/L 20.0 -0.0416 131 75-125 QM-08 Thallium 25.2 1.00 ug/L 20.0 0.0358 126 75-125 QM-08 Classical Chemistry Parameters - Quality Control Batch IJ20032 - NO PREP Blank (1320032-BLK1) Prepared: 10/20/2021 15:44 Analyzed: 10/20/2021 16:49 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L LCS (1320032-BS3) Prepared: 10/20/2021 15:44 Analyzed: 10/20/2021 17:06 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 100 90-110 Matrix Spike (1320032-MS3) Prepared: 10/20/2021 15:44 Analyzed: 10/20/2021 16:51 Source: CE15205-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 36 of 44 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch IJ20032 - NO PREP - Continued (� �Eo www.encolabs.com Matrix Spike (1320032-MS3) Continued Prepared: 10/20/2021 15:44 Analyzed: 10/20/2021 16:51 Source: CE15205-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.99 0.10 mg/L 1.00 0.017 U 99 90-110 Matrix Spike (1720032-MS2) Prepared: 10/20/2021 15:44 Analyzed: 10/20/2021 16:54 Source: CE15205-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.96 0.10 mg/L 1.00 0.017 U 96 90-110 Matrix Spike Dup (I]20032-MSDi) Prepared: 10/20/2021 15:44 Analyzed: 10/20/2021 16:52 Source: CE15205-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 100 90-110 0.6 10 Batch IJ21002 - NO PREP Blank (1321002-BLK1) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 16:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L Sulfate as SO4 2.9 U 5.0 mg/L LCS (1321002-BSI) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 16:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 51 5.0 mg/L 50.0 102 90-110 Sulfate as SO4 51 5.0 mg/L 50.0 102 90-110 Matrix Spike (1723002-MS3) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:17 Source: CE35554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 30 5.0 mg/L 20.0 10 99 90-110 Sulfate as SO4 56 5.0 mg/L 20.0 35 108 90-110 Matrix Spike (1323002-MS2) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:52 Source: CE15554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 46 5.0 mg/L 20.0 26 98 90-110 Sulfate as SO4 19 5.0 mg/L 20.0 2.9 U 97 90-110 Matrix Spike Dup (I]23002-MSDi) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:35 Source: CE35554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 32 5.0 mg/L 20.0 10 108 90-110 6 10 Sulfate as SO4 57 5.0 mg/L 20.0 35 113 90-110 2 10 QM-07 Batch IJ22004 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 37 of 44 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1122004 - NO PREP - Continued Blank (1322004-BLK1) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L LCS (1722004-BS3) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.38 0.10 mg/L 0.401 94 80-120 Duplicate (1122004-DUP3) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.055 J 0.10 mg/L 0.053 4 25 Matrix Spike (1322004-MS3) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.29 0.10 mg/L 0.401 0.053 58 80-120 QM-07 Matrix Spike Dup (1722004-MSD1) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.29 0.10 mg/L 0.401 0.053 59 80-120 1 25 QM-07 Batch 1125026 - NO PREP Blank (1325026-BLK3) Prepared & Analyzed: 10/25/2021 18:14 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 50 U 50 mg/L LCS (1325026-BS1) Prepared & Analyzed: 10/25/2021 18:14 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 920 50 mg/L 1000 92 80-120 Duplicate (1325026-DUPl) Prepared & Analyzed: 10/25/2021 18:14 Source: CE33958-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 2200 100 mg/L 2300 4 20 Duplicate (1325026-DUP2) Prepared & Analyzed: 10/25/2021 18:14 Source: CE33958-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 2100 100 mg/L 2200 4 20 Batch 1127021 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 38 of 44 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch IJ27021 - NO PREP - Continued (� �Eo www.encolabs.com Blank (1327021-BLK1) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (1327021-BS3) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 99 15 mg/L 100 99 80-120 Matrix Spike (1J27021-MS3) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:12 Source: CE15554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 110 15 mg/L 37.8 60 140 80-120 QM-07 Matrix Spike Dup (1327021-MSDI) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:12 Source: CE15554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 110 15 mg/L 37.8 60 137 80-120 1 25 QM-07 Batch 1KO2006 - NO PREP Blank (1K02006-BLK1) Prepared: 11/02/2021 09:11 Analyzed: 11/02/2021 12:25 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (1K02006-BS3) Prepared: 11/02/2021 09:11 Analyzed: 11/02/2021 12:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.2 0.10 mg/L 1.25 93 90-110 Matrix Spike (11<02006-MS1) Prepared: 11/02/2021 09:11 Analyzed: 11/02/2021 12:30 Source: CE15741-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.52 0.10 mg/L 0.521 0.045 91 90-110 Matrix Spike (1K02006-MS2) Prepared: 11/02/2021 09:11 Analyzed: 11/02/2021 12:35 Source: CE15741-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.58 0.10 mg/L 0.521 0.041 U 111 90-110 QM-07 Matrix Spike Dup (1K02006-MSD3) Prepared: 11/02/2021 09:11 Analyzed: 11/02/2021 12:32 Source: CE15741-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.52 0.10 mg/L 0.521 0.045 92 90-110 0.9 10 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 1.726022 - EPA 5030B MS FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 39 of 44 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 1126022 - EPA 5030B MS - Continued Blank (1326022-BLK1) Prepared: 10/26/2021 00:00 Analyzed: 10/26/2021 11:18 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-& 5.0 ug/L 5.00 101 75-125 LCS (1326022-BS1) Prepared: 10/26/2021 00:00 Analyzed: 10/26/2021 10:52 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 102 80-133 Toluene-d8 5.3 ug/L 5.00 106 75-125 Matrix Spike (1326022-MS1) Prepared: 10/26/2021 00:00 Analyzed: 10/26/2021 20:26 Source: AE08465-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 26 2.0 ug/L 25.0 0.80 U 105 80-133 Toluene-d8 5.1 ug/L 5.00 101 75-125 Matrix Spike Dup (1326022-MSD1) Prepared: 10/26/2021 00:00 Analyzed: 10/26/2021 20:51 Source: AE08465-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 0.80 U 101 80-133 4 19 Toluene-d8 5.4 ug/L 5.00 108 75-125 Dissolved Gases by GC - Quality Control Batch 1.726005 - Same Blank (1326005-BLK3) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:34 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 2.07 U 2.50 mg/L Ethane 0.00510 U 0.00600 mg/L Ethene 0.00510 U 0.00600 mg/L Methane 0.00400 U 0.00500 mg/L LCS (1326005-BSI) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 46.0 2.50 mg/L 45.8 100 70-130 Ethane 0.321 0.00600 mg/L 0.323 99 70-130 Ethene 0.315 0.00600 mg/L 0.302 104 70-130 Methane 0.168 0.00500 mg/L 0.174 97 70-130 LCS Dup (1326005-BSD1) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 50.3 2.50 mg/L 45.8 110 70-130 9 30 Ethane 0.353 0.00600 mg/L 0.323 109 70-130 9 30 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 40 of 44 QUALITY CONTROL DATA Dissolved Gases by GC - Quality Control Batch 1126005 - Same - Continued (� �Eo www.encolabs.com LCS Dup (1326005-BSD3) Continued Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Ethene 0.349 0.00600 mg/L 0.302 116 70-130 10 30 Methane 0.188 0.00500 mg/L 0.174 108 70-130 11 30 Duplicate (1326005-DUP1) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 13:37 Source: CE16213-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 22.1 2.50 mg/L 22.5 2 30 Ethane 0.00510 U 0.00600 mg/L 0.00510 U 30 Ethene 0.00510 U 0.00600 mg/L 0.00510 U 30 Methane 0.00400 U 0.00500 mg/L 0.00400 U 30 Classical Chemistry Parameters - Quality Control Batch 1.726001 - NO PREP Blank (1326001-BLK3) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 09:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 0.90 U 1.0 mg/L LCS (1326001-BS1) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 09:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 49 1.0 mg/L 50.0 97 85-115 Matrix Spike (1326001-MS3) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 10:24 Source: AE08470-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 51 1.0 mg/L 50.0 2.4 97 85-115 Matrix Spike (1326001-MS2) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 18:44 Source: AE08497-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 52 1.0 mg/L 50.0 2.9 98 85-115 Matrix Spike Dup (1326001-MSDI) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 10:47 Source: AE08470-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 50 1.0 mg/L 50.0 2.4 95 85-115 2 21 Matrix Spike Dup (1326001-MSD2) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 19:08 Source: AE08497-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 51 1.0 mg/L 50.0 2.9 97 85-115 2 21 Batch 1127005 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 41 of 44 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch IJ27005 - NO PREP - Continued Matrix Spike (1327005-MS2) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 18:34 Source: AE08497-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 55 1.0 mg/L 50.0 3.3 104 85-115 Matrix Spike Dup (1727005-MSD2) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 18:57 Source: AE08497-03 Analvte Total Organic Carbon Spike Source %REC Result Flaq POL Units Level Result %REC Limits RPD 36 1.0 mg/L 50.0 3.3 66 85-115 42 RPD Limit Notes 21 QM-07, QM-11 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 42 of 44 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test). QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 43 of 44 E 0 V qA 0 V i Q) C � E y N I O f-- a C Q CEi a V F c CJ} Lu a a w N ; Q u v ca Q) 0 tM 1 r 0 Z � � J V0906 001 x a S-flQSpWS apl_laS x X. x 4i OCl£ ajeAns cx X x x m a ZOO + 91 L }Jsa x Z'£9£ ?CON x 6H x X x x x x x x S Z L v m Ie10l opluefi0 P U �QY5Z4VlS Sclfooc WPONot-ow 4ullvmly x x >1l `o # m ookems aas'r=r F N ee P1441 OU Ppooiuo'Z-mc 4u!I"ry l V 1 � a c u' CA 0) C 5' h J U u ��y �n V n � V r� V III or C m I) [� C yr� x o L EN E c C� m= a G E _ g m U fl 4 ti N aw � titi1 U 66 C V a n m Q co co Rf z co a [t7 r r Cb .� .0 2CD Ui C SLI.: � ty E c r e— La W� N " w 11 �+ny mto U 4 U FL � vl r-) Q N � C E E m E m m 0` m N ¢_a 10 c U c U 7 ti J O m � m m a m y �r 4 r 0 m Q E m E fi O m m V1 m r N n v -N r. Q S S U c m a � C (� U 0 m V 0 W U � � m � U r Uaz`flr LL N 0 U s z a U N W_ cr- O p a it 0��� m�� J n C,3 z _ u� 4 a 0 m M C� a N � Q w z O U J z Wo z N � 0��� cc ry a z C o w 6 0 E i µ - 0 m tf C E N N " U) r. n Q 0 H L cn W 07a `o U m m � 47 � n ❑ � o a � m z � � J V0906 001 s S-00917WS apWnS 00£ ajejnS W 4ZOO + 9x AS a E ' ZE9£ XON $ m g 2 fi 6H x x x y C V 606 10101 ON MAD a O U �O1�iWS sai'oo£ oNxq NJ'rri4e AvuII041V o i� OOKZWS gcu,z"E9£ F IV N GIMIN'00£ OPP0143'rM R11u11eX V ae c � � U J Go m N E o ❑ CA ❑ 0 0 m = m U � 1 a` a` IL ¢ m rn �- co O O a C& co N ++ to c CD C4 b � m m Of EzLU w00 � m n r 0 0 r 0 rr 0 m m 6 Q U Mm U) W m ro Q U _\\ N E E: m a o 0 R � 'y �7 m � ¢ U U t r� a v U 1 � m m m ^\ U cc 0 m E m E m E a t v 0 m m ai n F m � o� m E a m m � m � m a a x m n m E Sample Preservation Verification ENCO Cary Work Order: CE16213 Project: Moore County Active C &JD LF - Fall Client: S&ME, Inc. (SM004) Project #: 4358-20-043 Logged In: 20-Oct-21 11:08 Logged By: Rachel Ann Yo jsh Preservation Check Performed By: Date/Time: =0 CE16213-01 Cant Type Pres (pH) Requirement pH Checked / In Control pH Adjusted Date[Time Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 I N / NA Y / NA C 250mLP+ZnAc+NaOH >9 N / NA Y /n NA D 250mLP+H2SO4 <2 Y N/ NA Y/ N NA CE16213-02 Cont Type Pres (pH) pH Checked / Requirement In Control pH Adjusted DatelTime Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 1 N I NA Y 104 NA C 250mLP+ZnAc+NaOH >9 Y N/ NA Y /W NA +h CE16213-03 �k Y ti 'font Type Pres (pH) pH Checked I Requirement In Control Date/Timeyp Adjusted pH AdAdjusted Reagent Used/Comments B 250mLP+HNO3 <2 / NA Y /NA C 250mLP+ZnAc+NaOH RY/N >9 N I NA Y N NA CE16213-04 Cont Type Pres (pH) Requirement pH CheckedF In Control pH Adjusted Date/Ttme Adjusted Reagent Used/Comments A 250mLP+HNO3 <2 Y j N I NA Y 1` N ',/ NA I CE16213-05 Cont Type Pres (pH) fequirement pH Checked 1 In Control pH Adjusted DateMime Adjusted Reagent Used/Comments A 250mLP+HNO3 1 2 Y " N / NA I Y /' N NA CE16213-06 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted DateiTime I Adjusted Reagent Used/Comments A 25OmLP+HNO3 <2 Y I N I NA Y I N r NA JkCE16213-07 pe Pres (pH) pH Checked/ pH Adjusted Date�me Reagent Used/Comments Requirement In Control Adjusted F=25OmLP+HNO3 <2 Y N/ NA Y! N NA C:lelmntlPrinftko—PreservationCheck, rpt Page 1 c,f Sample Preservation Verification ENCO Cary �uco Work Order: CE16213 Client: S&ME, Inc. (SM004) Logged In: 20-Oct-21 11:08 Logged By: Rachel Ann Yoni h Preservation Check Performed By: _ Date/Time: �la-i Zi I Rea ent Name ID 1 2 Project: Moore County Active C & D LF - Fall Project #: 4358-20-043 Reacient Name ID 3 4 Reagent Name ID 5 6 pH Strip ID: PH Strips COF0555 4 C:lelmntlPririLlWr(o_rreservanont,,neCK.rpt Page 2 of 2 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, December 7, 2021 S&ME, Inc. (SM004) Attn: Edmund Henriques 8646 West Market Street, Suite 105 Greensboro, NC 27409 RE: Laboratory Results for Project Number: 4358-20-043, Project Name/Desc: Moore County Active C & D LF - Fall ENCO Workorder(s): CE15554 Dear Edmund Henriques, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, October 19, 2021. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 4P 0 ee Bill Scott For Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 82 PROJECT NARRATIVE Client: S&ME, Inc. (SM004) Project: Moore County Active C & D LF - Fall Lab ID: CE15554 Rev (� �Eo www.encolabs.com Overview This report is a revision to the original data report dated 11/10/2. This report was revised to include volatile compounds benzene and vinyl chloride that were missing for samples MW 11 SR and MW11 DR. Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples The associated LCS exhibited high bias; since the result is ND, there is no impact (QL-02). The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on an acceptable LCS recovery (QM-07). Post -digestion spike did not meet method requirements due to confirmed matrix effects (QM-08). Precision between duplicate metrix spikes of the same sample was outside acceptance limits (QM-11). Quality Control Remarks Analyte biased low in LCS but detected in the reporting limit standard. Since the analyte is in the associated sample was not detected, there is no impact on data Quality (A-07). Result may be biased high. Associated CV standard exceeded the upper control limit (J-04). Result may be biased low. Associated CV standard did not meet the minimum control limit (J-05). The associated LCS exhibited low bias; the reported result should be considered to be a minimum estimate (J-06). Samples MW-18 and MW-19 were re -extracted outside of the 8270 holding time due to failing QC. Both sets of data have been reported (0-05). Surrogate recovery oustide acceptance limits (QS-03). The associated CCV standard exhibited high bias; since the result is ND, there is no impact (QV-01) The sample was diluted due to the presence of high levels of non -target analytes resulting in elevated reporting limits (R-05). Other Comments The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Chuck Smith Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 82 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW4 Lab ID: CE15554-01 Sampled: 10/18/21 17:30 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/15/21 10/21/21 06:21 10/21/21 18:10 EPA 310.2 NO PREP 11/01/21 10/27/21 14:18 10/27/21 16:11 EPA 353.2 NO PREP 10/20/21 17:30 10/19/21 15:56 10/19/21 17:40 EPA 353.2 [CALC] 10/20/21 17:30 10/26/21 09:55 10/29/21 15:07 EPA 6010D EPA 3005A 04/16/22 10/20/21 11:28 10/27/21 14:48 EPA 6010D EPA 3005A 04/16/22 10/21/21 16:13 10/25/21 10:54 EPA 6020E EPA 3005A 04/16/22 10/29/21 06:14 11/02/21 23:31 EPA 7470A EPA 245.1 11/15/21 10/20/21 15:21 10/22/21 07:57 EPA 8260D EPA 503013_MS 11/01/21 10/25/21 08:55 10/25/21 10:47 EPA 8260D EPA 503013_MS 11/01/21 10/27/21 16:42 10/29/21 07:05 EPA 9060A NO PREP 11/15/21 10/26/21 07:08 10/26/21 14:56 RSK 175 Same 11/01/21 10/26/21 08:00 10/26/21 12:48 SM 2540C-2011 NO PREP 10/25/21 10/25/21 18:14 10/25/21 18:14 SM 4500S2 D-2011 NO PREP 10/25/21 10/20/21 16:27 10/20/21 16:45 Client ID: 6301-MW4 Lab ID: CE15554-OIRE1 Sampled: 10/18/21 17:30 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 353.2 NO PREP 11/15/21 10/26/21 09:55 10/29/21 15:07 Client ID: 6301-MW11SR Lab ID: CE15554-02 Sampled: 10/19/21 08:25 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/21/21 18:28 EPA 353.2 NO PREP 10/21/21 08:25 10/19/21 15:56 10/19/21 17:43 EPA 353.2 [CALC] 10/21/21 08:25 10/26/21 09:55 10/29/21 13:27 EPA 353.2 NO PREP 11/16/21 10/26/21 09:55 10/29/21 13:27 EPA 6010D EPA 3005A 04/17/22 10/20/21 11:28 10/27/21 14:51 EPA 6010D EPA 3005A 04/17/22 10/21/21 16:13 10/25/21 10:21 EPA 6020E EPA 3005A 04/17/22 10/29/21 06:14 11/02/21 23:35 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:21 10/22/21 07:59 EPA 8260D EPA 5030B_MS 11/02/21 10/25/21 08:55 10/25/21 11:13 EPA 8260D EPA 503013_MS 11/02/21 10/27/21 17:00 10/28/21 02:09 EPA 9060A NO PREP 11/16/21 10/26/21 07:08 10/26/21 15:17 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 13:04 SM 2540C-2011 NO PREP 10/26/21 10/25/21 18:14 10/25/21 18:14 SM 4500S2 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MW11SR Lab ID: CE15554-02RE3 Sampled: 10/19/21 08:25 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 11/02/21 11/01/21 09:50 11/01/21 13:49 Client ID: 6301-MW11DR Lab ID: CE15554-03 Sampled: 10/19/21 09:20 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/21/21 19:21 EPA 310.2 NO PREP 11/02/21 10/27/21 14:18 10/27/21 16:15 EPA 6010D EPA 3005A 04/17/22 10/20/21 11:28 10/27/21 14:53 EPA 6010D EPA 3005A 04/17/22 10/21/21 16:13 10/25/21 10:57 EPA 6020E EPA 3005A 04/17/22 10/29/21 06:14 11/02/21 23:39 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:21 10/22/21 08:04 EPA 8260D EPA 503013_MS 11/02/21 10/25/21 08:55 10/25/21 11:38 EPA 8260D EPA 503013_MS 11/02/21 10/27/21 17:00 10/28/21 02:38 SM 254OC-2011 NO PREP 10/26/21 10/25/21 18:14 10/25/21 18:14 SM 4500S2 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 82 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW34 Lab ID: CE15554-04 Sampled: 10/18/21 18:10 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/15/21 10/21/21 06:21 10/21/21 19:39 EPA 310.2 NO PREP 11/01/21 10/27/21 14:18 10/27/21 16:16 EPA 6010D EPA 3005A 04/16/22 10/21/21 16:13 10/25/21 10:59 EPA 6020B EPA 3005A 04/16/22 10/29/21 06:14 11/02/21 23:43 EPA 7470A EPA 245.1 11/15/21 10/20/21 15:21 10/22/21 08:06 EPA 8260D EPA 5030B_MS 11/01/21 10/25/21 08:55 10/25/21 12:04 EPA 8260D EPA 5030B_MIS 11/01/21 10/27/21 16:42 10/29/21 07:32 SM 254OC-2011 NO PREP 10/25/21 10/25/21 18:14 10/25/21 18:14 SM 450052 D-2011 NO PREP 10/25/21 10/20/21 16:27 10/20/21 16:45 Client ID: 6301-MW14 Lab ID: CE15554-04RE1 Sampled: 10/18/21 18:10 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/01/21 11/01/21 13:31 11/01/21 20:56 Client ID: 6301-MW17S Lab ID: CE15554-05 Sampled: 10/18/21 11:05 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(sl Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/15/21 10/21/21 06:21 10/21/21 19:56 EPA 310.2 NO PREP 11/01/21 10/27/21 14:18 10/27/21 16:18 EPA 6010D EPA 3005A 04/16/22 10/21/21 16:13 10/25/21 11:02 EPA 6020E EPA 3005A 04/16/22 10/29/21 06:14 11/02/21 23:53 EPA 7470A EPA 245.1 11/15/21 10/20/21 15:21 10/22/21 08:13 EPA 8260D EPA 503013_MS 11/01/21 10/25/21 08:55 10/25/21 12:30 EPA 8260D EPA 503013_MS 11/01/21 10/27/21 16:42 10/29/21 08:00 SM 2540C-2011 NO PREP 10/25/21 10/25/21 18:14 10/25/21 18:14 SM 450052 D-2011 NO PREP 10/25/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MW17S Lab ID: CE15554-OSRE1 Sampled: 10/18/21 11:05 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/01/21 11/01/21 13:31 11/01/21 21:23 Client ID: 6301-MW17D Lab ID: CE15554-06 Sampled: 10/18/21 15:10 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/15/21 10/21/21 06:21 10/21/21 20:14 EPA 310.2 NO PREP 11/01/21 10/27/21 14:18 10/27/21 16:18 EPA 6010D EPA 3005A 04/16/22 10/21/21 16:13 10/25/21 11:04 EPA 6020E EPA 3005A 04/16/22 10/29/21 06:14 11/02/21 23:58 EPA 7470A EPA 245.1 11/15/21 10/20/21 15:21 10/22/21 08:15 EPA 8260D EPA 503013_MS 11/01/21 10/25/21 08:55 10/25/21 12:55 EPA 8260D EPA 503013_MS 11/01/21 10/27/21 16:42 10/29/21 08:28 SM 2540C-2011 NO PREP 10/25/21 10/25/21 18:14 10/25/21 18:14 SM 450052 D-2011 NO PREP 10/25/21 10/22/21 09:58 10/22/21 10:16 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 82 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW38 Lab ID: CE15554-07 Sampled: 10/18/21 13:55 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/15/21 10/21/21 06:21 10/21/21 20:32 EPA 310.2 NO PREP 11/01/21 10/27/21 14:18 10/27/21 16:19 EPA 6010D EPA 3005A 04/16/22 10/21/21 16:13 10/25/21 11:15 EPA 6020B EPA 3005A 04/16/22 10/29/21 06:14 11/03/21 00:02 EPA 7470A EPA 245.1 11/15/21 10/20/21 15:21 10/22/21 08:17 EPA 8081E EPA 3510C 10/25/21 12/02/21 10/23/21 15:01 10/27/21 13:57 EPA 8082A EPA 3510C 10/18/22 12/02/21 10/23/21 15:09 10/27/21 13:57 EPA 8151A EPA 3510C 10/25/21 12/04/21 10/25/21 15:30 10/27/21 19:24 EPA 8260D EPA 503013_MS 11/01/21 10/25/21 08:55 10/25/21 13:21 EPA 8260D EPA 503013_MS 11/01/21 10/27/21 16:42 10/29/21 08:55 EPA 8270E EPA 3510C—MS 10/25/21 12/04/21 10/25/21 10:05 10/27/21 15:21 EPA 9014 Same 11/01/21 10/25/21 14:10 10/26/21 13:08 SM 2540C-2011 NO PREP 10/25/21 10/25/21 18:14 10/25/21 18:14 SM 4500S2 D-2011 NO PREP 10/25/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MW18 Lab ID: CE15554-07RE1 Sampled: 10/18/21 13:55 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/01/21 11/01/21 13:31 11/01/21 21:51 EPA 8270E EPA 3510C MS 10/25/21 12/11/21 11/01/21 08:29 11/01/21 18:42 Client ID: 6301-MW19 Lab ID: CE15554-08 Sampled: 10/18/21 11:45 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/15/21 10/21/21 06:21 10/21/21 20:49 EPA 310.2 NO PREP 11/01/21 10/27/21 14:18 10/27/21 16:20 EPA 6010D EPA 3005A 04/16/22 10/21/21 16:13 10/25/21 11:17 EPA 6020B EPA 3005A 04/16/22 10/29/21 06:14 11/03/21 00:06 EPA 7470A EPA 245.1 11/15/21 10/20/21 15:21 10/22/21 08:18 EPA 8081E EPA 3510C 10/25/21 12/02/21 10/23/21 15:01 10/27/21 14:10 EPA 8082A EPA 3510C 10/18/22 12/02/21 10/23/21 15:09 10/27/21 14:10 EPA 8260D EPA 5030B_MS 11/01/21 10/25/21 08:55 10/25/21 13:47 EPA 8260D EPA 503013_MS 11/01/21 10/27/21 16:42 10/29/21 09:23 EPA 8270E EPA 3510C—MS 10/25/21 12/04/21 10/25/21 10:05 10/27/21 15:52 EPA 9014 Same 11/01/21 10/25/21 14:10 10/26/21 13:09 SM 2540C-2011 NO PREP 10/25/21 10/25/21 18:14 10/25/21 18:14 SM 4500S2 D-2011 NO PREP 10/25/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MW19 Lab ID: CE15554-08RE1 Sampled: 10/18/21 11:45 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8151A EPA 3510C 10/25/21 12/08/21 10/29/21 07:30 11/01/21 14:04 EPA 8270E EPA 3510C MS 10/25/21 12/11/21 11/01/21 08:29 11/01/21 19:13 Client ID: 6301-DUPLICATE Lab ID: CE15554-09 Sampled: 10/18/21 00:00 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/15/21 10/21/21 06:21 10/21/21 21:07 EPA 6010D EPA 3005A 04/16/22 10/21/21 16:13 10/25/21 11:20 EPA 6020B EPA 3005A 04/16/22 10/29/21 06:14 11/03/21 00:10 EPA 7470A EPA 245.1 11/15/21 10/20/21 15:21 10/22/21 08:20 EPA 8260D EPA 5030B_MS 11/01/21 10/25/21 08:55 10/25/21 14:12 EPA 8260D EPA 503013_MS 11/01/21 10/27/21 16:42 10/29/21 09:50 SM 254OC-2011 NO PREP 10/25/21 10/25/21 18:14 10/25/21 18:14 SM 4500S2 D-2011 NO PREP 10/25/21 10/22/21 09:58 10/22/21 10:16 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5 Of 82 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-DUPLICATE Lab ID: CE15554-09RE1 Sampled: 10/18/21 00:00 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) EPA 310.2 NO PREP 11/01/21 Prep Date/Time(s) Analysis Date/Time(s) 11/01/21 09:50 11/01/21 12:23 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 82 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW4 Lab ID: CE15554-01 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 1.6 J 0.80 2.0 ug/L EPA 8260D Barium - Total 35.8 1.10 10.0 ug/L EPA 6010D Carbon dioxide 72.5 D 10.4 12.5 mg/L RSK 175 Chloride 10 2.2 5.0 mg/L EPA 300.0 Chromium - Total 1.91 J 1.40 10.0 ug/L EPA 6010D Copper - Total 2.20 J 1.60 10.0 ug/L EPA 6010D Iron - Total 1130 22.0 50.0 ug/L EPA 6010D Manganese - Total 34.0 1.50 10.0 ug/L EPA 6010D Methane 0.0480 D 0.0200 0.0250 mg/L RSK 175 Nitrate as N 0.11 0.041 0.10 mg/L EPA 353.2 Nitrite as N 0.021 J 0.017 0.10 mg/L EPA 353.2 Sulfate as SO4 35 2.9 5.0 mg/L EPA 300.0 Sulfide 0.066 J 0.010 0.10 mg/L SM 4500S2 D-2011 Total Alkalinity as CaCO3 60 14 15 mg/L EPA 310.2 Total Dissolved Solids 130 50 50 mg/L SM 2540C-2011 Total Organic Carbon 14 0.90 1.0 mg/L EPA 9060A Vanadium - Total 2.20 1 1.40 10.0 uq/L EPA 6010D I Client ID: 6301-MW4 Lab ID: CE15554-01RE1 Analvte Results Flag MDL Q Units Method Notes Nitrate/Nitrite as N 0.13 0.041 0.10 mg/L EPA 353.2 Client ID: 6301-MW11SR Lab ID: CE15554-02 Analvte Results Flag MDL Q Units Method Notes 1,4-Dichlorobenzene 2.6 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 5.1 0.80 2.0 ug/L EPA 8260D Barium - Total 67.1 1.10 10.0 ug/L EPA 6010D Benzene 2.6 0.15 1.0 ug/L EPA 8260D 3-04 Carbon dioxide 448 D 43.5 52.5 mg/L RSK 175 Chloride 26 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.2 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.0 0.15 1.0 ug/L EPA 8260D Iron - Total 88200 22.0 50.0 ug/L EPA 6010D Manganese - Total 259 1.50 10.0 ug/L EPA 6010D Methane 2.44 D 0.0840 0.105 mg/L RSK 175 Nitrate as N 0.15 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.15 0.041 0.10 mg/L EPA 353.2 Sulfide 0.053 J 0.010 0.10 mg/L SM 4500S2 D-2011 Tetrahydrofuran 6.3 0.53 1.0 ug/L EPA 8260D Total Dissolved Solids 540 50 50 mg/L SM 2540C-2011 Total Organic Carbon 21 0.90 1.0 mg/L EPA 9060A Vinyl chloride 3.1 0.32 1.0 ug/L EPA 8260D 3-04 Client ID: 6301-MW11SR Lab ID: CE35554-02RE3 Analvte Results Flag MDL Q Units Method Notes Total Alkalinity as CaCO3 470 D 70 75 mg/L EPA 310.2 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 Of 82 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW11DR Lab ID: CE15554-03 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 3.9 0.80 2.0 ug/L EPA 8260D Barium - Total 51.9 1.10 10.0 ug/L EPA 6010D Benzene 1.9 0.15 1.0 ug/L EPA 8260D 3-04 Chloride 18 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.2 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 3.3 0.15 1.0 ug/L EPA 8260D Iron - Total 72500 22.0 50.0 ug/L EPA 6010D Manganese - Total 156 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 11 2.9 5.0 mg/L EPA 300.0 Sulfide 0.038 J 0.010 0.10 mg/L SM 4500S2 D-2011 Tetrahydrofuran 3.4 0.53 1.0 ug/L EPA 8260D Total Alkalinity as CaCO3 210 D 70 75 mg/L EPA 310.2 Total Dissolved Solids 200 50 50 mg/L SM 2540C-2011 Vinyl chloride 2.3 0.32 1.0 ug/L EPA 8260D 3-04 Client ID: 6301-MW34 Lab ID: CE15554-04 Analvte Results Flag MDL Q Units Method Notes 1,2-Dichlorobenzene 1.8 0.19 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 4.5 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 17 0.80 2.0 ug/L EPA 8260D Barium - Total 44.7 1.10 10.0 ug/L EPA 6010D Benzene 1.7 0.15 1.0 ug/L EPA 8260D Chloride 61 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 5.2 0.17 1.0 ug/L EPA 8260D Iron - Total 136000 22.0 50.0 ug/L EPA 6010D Manganese - Total 176 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 7.0 2.9 5.0 mg/L EPA 300.0 Sulfide 0.16 0.010 0.10 mg/L SM 4500S2 D-2011 Total Alkalinity as CaCO3 220 D 70 75 mg/L EPA 310.2 Total Dissolved Solids 250 50 50 mg/L SM 2540C-2011 Client ID: 6301-MW34 Lab ID: CE15554-04RE1 Analvte Results Flag MDL Q Units Method Notes Vinyl chloride 2.6 0.32 1.0 ug/L EPA 8260D Client ID: 6301-MW17S Lab ID: CE15554-05 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 3.4 0.80 2.0 ug/L EPA 8260D Barium - Total 84.2 1.10 10.0 ug/L EPA 6010D Chloride 27 2.2 5.0 mg/L EPA 300.0 cis-1,2-Dichloroethene 1.3 0.15 1.0 ug/L EPA 8260D Iron - Total 48700 22.0 50.0 ug/L EPA 6010D Manganese - Total 181 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 95 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 190 14 15 mg/L EPA 310.2 Total Dissolved Solids 380 50 50 mg/L SM 2540C-2011 Client ID: 6301-MW17S Lab ID: CE15554-05RE1 Analvte Results Flag MDL Q Units Method Notes Vinyl chloride 1.8 0.32 1.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 8 Of 82 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW17D Lab ID: CE15554-06 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 7.1 0.80 2.0 ug/L EPA 8260D Barium - Total 36.4 1.10 10.0 ug/L EPA 6010D Chloride 3.0 J 2.2 5.0 mg/L EPA 300.0 Chromium - Total 3.04 J 1.40 10.0 ug/L EPA 6010D Iron - Total 2200 22.0 50.0 ug/L EPA 6010D Manganese - Total 19.4 1.50 10.0 ug/L EPA 6010D Nickel - Total 2.92 J 2.20 10.0 ug/L EPA 6010D Sulfate as SO4 30 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 97 14 15 mg/L EPA 310.2 Total Dissolved Solids 150 50 50 mg/L SM 2540C-2011 Client ID: 6301-MW38 Lab ID: CE15554-07 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 13 0.80 2.0 ug/L EPA 8260D Barium - Total 78.1 1.10 10.0 ug/L EPA 6010D Chloride 44 2.2 5.0 mg/L EPA 300.0 cis-1,2-Dichloroethene 2.3 0.15 1.0 ug/L EPA 8260D Iron - Total 93400 22.0 50.0 ug/L EPA 6010D Manganese - Total 154 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 42 2.9 5.0 mg/L EPA 300.0 Sulfide 0.056 J 0.010 0.10 mg/L SM 450052 D-2011 Total Alkalinity as CaCO3 310 D 70 75 mg/L EPA 310.2 Total Dissolved Solids 410 50 50 mq/L SM 2540C-2011 Client ID: 6301-MW38 Lab ID: CE15554-07RE3 Analvte Results Flag MDL PQL Units Method Notes Acetone 18 1 10 20 ug/L EPA 8260D Chlorobenzene 0.93 1 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.8 0.15 1.0 ug/L EPA 8260D Vinyl chloride 0.98 J 0.32 1.0 ug/L EPA 8260D Client ID: 6301-MW39 Lab ID: CE15554-08 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 2.9 0.80 2.0 ug/L EPA 8260D Barium - Total 19.8 1.10 10.0 ug/L EPA 6010D Chloride 13 2.2 5.0 mg/L EPA 300.0 Iron - Total 305 22.0 50.0 ug/L EPA 6010D Manganese - Total 2.52 J 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 9.5 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 45 14 15 mg/L EPA 310.2 Total Dissolved Solids 80 50 50 mg/L SM 2540C-2011 Client ID: 6301-MW39 Lab ID: CE15554-08RE1 Analvte Results Flag MDL PQL Units Method Notes Bis(2-ethylhexyl)phthalate 4.0 J 1.9 5.0 ug/L EPA 8270E 0-05 Client ID: 6301-DUPLICATE Lab ID: CE15554-09 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 13 0.80 2.0 ug/L EPA 8260D Barium - Total 78.6 1.10 10.0 ug/L EPA 6010D Benzene 0.93 1 0.15 1.0 ug/L EPA 8260D Chloride 44 2.2 5.0 mg/L EPA 300.0 cis-1,2-Dichloroethene 2.0 0.15 1.0 ug/L EPA 8260D Iron - Total 93900 22.0 50.0 ug/L EPA 6010D Manganese - Total 155 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 42 2.9 5.0 mg/L EPA 300.0 Sulfide 0.037 J 0.010 0.10 mg/L SM 450052 D-2011 Total Dissolved Solids 480 50 50 mg/L SM 2540C-2011 Client ID: 6301-DUPLICATE Lab ID: CE15554-09RE1 Analvte Results Flag MDL PQL Units Method Notes Total Alkalinity as CaCO3 340 D 70 75 mg/L EPA 310.2 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 9 Of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW4 Lab Sample ID:CE15554-01 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 17:30 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1127025 EPA 8260D 10/29/21 07:05 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1127025 EPA 8260D 10/29/21 07:05 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1127025 EPA 8260D 10/29/21 07:05 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1127025 EPA 8260D 10/29/21 07:05 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1127025 EPA 8260D 10/29/21 07:05 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1127025 EPA 8260D 10/29/21 07:05 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1127025 EPA 8260D 10/29/21 07:05 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Tetrahydrofuran [109-99-9]^ 0.53 u ug/L 1 0.53 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1127025 EPA 8260D 10/29/21 07:05 RKY Vinyl chloride [75-01-4]^ 0.32 u ug/L 1 0.32 1.0 1127025 EPA 8260D 10/29/21 07:05 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 10 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW4 Lab Sample ID:CE15554-01 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 17:30 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27025 EPA 8260D 10/29/21 07:05 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 59 1 50.0 117 % 53-136 IJ27025 EPA 6260D 10129121 07:05 RKY Dibromofluoromethane 55 1 50.0 111 % 67-129 IJ27025 EPA 6260D 10129121 07:05 RKY Toluene-c48 52 1 50.0 104 % 59-134 IJ27025 EPA 6260D 10129121 07:05 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 07:57 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1J29005 EPA 6020B 11/02/21 23:31 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J21030 EPA 6010D 10/25/21 10:54 JDH Barium [7440-39-3]^ 35.8 ug/L 1 1.10 10.0 1121030 EPA 6010D 10/25/21 10:54 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1J21030 EPA 6010D 10/25/21 10:54 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 10:54 JDH Chromium [7440-47-3]^ 1.91 J ug/L 1 1.40 10.0 1121030 EPA 6010D 10/25/21 10:54 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 10:54 JDH Copper[7440-50-8]^ 2.20 J ug/L 1 1.60 10.0 1121030 EPA 6010D 10/25/21 10:54 JDH Iron [7439-89-6]^ 1130 ug/L 1 22.0 50.0 1120014 EPA 6010D 10/27/21 14:48 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 10:54 JDH Manganese [7439-96-5]^ 34.0 ug/L 1 1.50 10.0 1121030 EPA 6010D 10/25/21 10:54 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1J21030 EPA 6010D 10/25/21 10:54 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1J29005 EPA 6020B 11/02/21 23:31 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 10:54 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1J29005 EPA 6020B 11/02/21 23:31 RLF Vanadium [7440-62-2]^ 2.20 J ug/L 1 1.40 10.0 1121030 EPA 6010D 10/25/21 10:54 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1J21030 EPA 6010D 10/25/21 10:54 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 30 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 18:10 ZGW Nitrate as N [14797-55-8] 0.11 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/29/21 15:07 JAH Nitrate/Nitrite as N^ 0.13 mg/L 1 0.041 0.10 1126014 EPA 353.2 10/29/21 15:07 JAH Nitrite as N [14797-65-0]^ 0.021 J mg/L 1 0.017 0.10 1119028 EPA 353.2 10/19/21 17:40 JAH Sulfate as SO4 [14808-79-B]^ 35 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/21/21 18:10 ZGW Sulfide [18496-25-8]^ 0.066 J mg/L 1 0.010 0.10 1120023 iM 4500S2 D-2011 10/20/21 16:45 JOC Total Alkalinity as CaCO3 [471-34-1]^ 60 mg/L 1 14 15 1127021 EPA 310.2 10/27/21 16:11 JAH Total Dissolved Solids^ 130 mg/L 1 50 50 1125026 SM 254OC-2011 10/25/21 18:14 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 11 of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW4 Lab Sample ID:CE15554-01 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 17:30 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 1.6 J ug/L 1 0.80 2.0 1325015 EPA 8260D 10/25/21 10:47 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.5 1 5.00 110 % 75-125 V25015 EPA 6260D 10125121 10:47 KKW Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 72.5 D mg/L 5 10.4 12.5 1126005 RSK 175 10/26/21 12:48 JMW Ethane [74-84-0] 0.0255 UD mg/L 5 0.0255 0.0300 1J26005 RSK 175 10/26/21 12:48 JMW Ethene [74-85-1] 0.0255 UD mg/L 5 0.0255 0.0300 1J26005 RSK 175 10/26/21 12:48 JMW Methane [74-82-8] 0.0480 D mg/L 5 0.0200 0.0250 1126005 RSK 175 10/26/21 12:48 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MOIL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 14 mg/L 1 0.90 1.0 1126001 EPA 9060A 10/26/21 14:56 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 12 of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11SR Lab Sample ID:CE15554-02 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2108:25 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 1,4-Dichlorobenzene [306-46-7]^ 2.6 ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1127031 EPA 8260D 10/28/21 02:09 RKY QV-01 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1127031 EPA 8260D 10/28/21 02:09 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1127031 EPA 8260D 10/28/21 02:09 RKY QV-01 Acetone [67-64-1]^ 10 U ug/L 1 10 20 1127031 EPA 8260D 10/28/21 02:09 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1127031 EPA 8260D 10/28/21 02:09 RKY Benzene [71-43-2]A 2.6 ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY 3-04 Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY QV-01 Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1127031 EPA 8260D 10/28/21 02:09 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY QV-01 Chlorobenzene [108-90-7]A 1.2 ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY QV-01 Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY cis-1,2-Dichloroethene [156-59-2]A 1.0 ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1127031 EPA 8260D 10/28/21 02:09 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY QV-01 Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Tetrahydrofuran [109-99-9]A 6.3 ug/L 1 0.53 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1127031 EPA 8260D 10/28/21 02:09 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1127031 EPA 8260D 10/28/21 02:09 RKY QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. r Page 13 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11SR Lab Sample ID:CE15554-02 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2108:25 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 3.1 ug/L 1 0.32 1.0 1327031 EPA 8260D 10/28/21 02:09 RKY J-04 Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27031 EPA 8260D 10/28/21 02:09 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 61 1 50.0 122 % 53-136 IJ27031 EPA 6260D 10128121 02:09 RKY Dibromofluoromethane 52 1 50.0 104 % 67-129 IJ27031 EPA 6260D 10128121 02:09 RKY Toluene-d8 50 1 50.0 101 % 59-134 IJ27031 EPA 6260D 10126121 02:09 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed By Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 07:59 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1J29005 EPA 6020B 11/02/21 23:35 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J21030 EPA 6010D 10/25/21 10:21 JDH Barium [7440-39-3]^ 67.1 ug/L 1 1.10 10.0 1121030 EPA 6010D 10/25/21 10:21 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1J21030 EPA 6010D 10/25/21 10:21 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 10:21 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 10:21 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 10:21 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1J21030 EPA 6010D 10/25/21 10:21 JDH Iron [7439-89-6]^ 88200 ug/L 1 22.0 50.0 1120014 EPA 6010D 10/27/21 14:51 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 10:21 JDH Manganese [7439-96-5]^ 259 ug/L 1 1.50 10.0 1121030 EPA 6010D 10/25/21 10:21 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1J21030 EPA 6010D 10/25/21 10:21 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1J29005 EPA 6020B 11/02/21 23:35 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 10:21 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1J29005 EPA 6020B 11/02/21 23:35 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 10:21 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1J21030 EPA 6010D 10/25/21 10:21 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 26 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 18:28 ZGW Nitrate as N [14797-55-8] 0.15 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/29/21 13:27 JAH Nitrate/Nitrite as N^ 0.15 mg/L 1 0.041 0.10 1126014 EPA 353.2 10/29/21 13:27 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1J19028 EPA 353.2 10/19/21 17:43 JAH Sulfate as SO4 [14808-79-8]^ 2.9 U mg/L 1 2.9 5.0 1J21002 EPA 300.0 10/21/21 18:28 ZGW Sulfide [18496-25-8]^ 0.053 J mg/L 1 0.010 0.10 1122004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 470 D mg/L 5 70 75 1KO1020 EPA 310.2 11/01/21 13:49 JAH Total Dissolved Solids^ 540 mg/L 1 50 50 1125026 SM 254OC-2011 10/25/21 18:14 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 14 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11SR Lab Sample ID:CE15554-02 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2108:25 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 5.1 ug/L 1 0.80 2.0 1325015 EPA 8260D 10/25/21 11:13 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.2 1 5.00 104 % 75-125 V25015 EPA 6260D 10125121 11:13 KKW Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 448 D mg/L 21 43.5 52.5 1126005 RSK 175 10/26/21 13:04 JMW Ethane [74-84-0] 0.107 UD mg/L 21 0.107 0.126 1J26005 RSK 175 10/26/21 13:04 JMW Ethene [74-85-1] 0.107 UD mg/L 21 0.107 0.126 1J26005 RSK 175 10/26/21 13:04 JMW Methane [74-82-8] 2.44 D mg/L 21 0.0840 0.105 1126005 RSK 175 10/26/21 13:04 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MOIL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 21 mg/L 1 0.90 1.0 1126001 EPA 9060A 10/26/21 15:17 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 15 of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11DR Lab Sample ID:CE15554-03 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2109:20 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 1127031 EPA 8260D 10/28/21 02:38 RKY QV-01 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1127031 EPA 8260D 10/28/21 02:38 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 1127031 EPA 8260D 10/28/21 02:38 RKY QV-01 Acetone [67-64-1]A 10 U ug/L 1 10 20 1127031 EPA 8260D 10/28/21 02:38 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 1127031 EPA 8260D 10/28/21 02:38 RKY Benzene [71-43-2]^ 1.9 ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 3-04 Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY QV-01 Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 1127031 EPA 8260D 10/28/21 02:38 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY QV-01 Chlorobenzene [108-90-7]^ 1.2 ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY QV-01 Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY cis-1,2-Dichloroethene [156-59-2]^ 3.3 ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 1127031 EPA 8260D 10/28/21 02:38 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY QV-01 Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Tetrahydrofuran [109-99-9]^ 3.4 ug/L 1 0.53 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 1127031 EPA 8260D 10/28/21 02:38 RKY QV-01 Vinyl chloride [75-01-4]^ 2.3 ug/L 1 0.32 1.0 1127031 EPA 8260D 10/28/21 02:38 RKY 3-04 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 16 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11DR Lab Sample ID:CE15554-03 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2109:20 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27031 EPA 8260D 10/28/21 02:38 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 100 % 53-136 IJ27031 EPA 6260D 10128121 02:38 RKY Dibromofluoromethane 49 1 50.0 98 % 67-129 IJ27031 EPA 6260D 10128121 02:38 RKY Toluene-c48 51 1 50.0 103 % 59-134 IJ27031 EPA 6260D 10128121 02:38 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:04 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1J29005 EPA 6020B 11/02/21 23:39 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J21030 EPA 6010D 10/25/21 10:57 JDH Barium [7440-39-3]^ 51.9 ug/L 1 1.10 10.0 1121030 EPA 6010D 10/25/21 10:57 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1J21030 EPA 6010D 10/25/21 10:57 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 10:57 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 10:57 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 10:57 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1J21030 EPA 6010D 10/25/21 10:57 JDH Iron [7439-89-6]^ 72500 ug/L 1 22.0 50.0 1120014 EPA 6010D 10/27/21 14:53 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 10:57 JDH Manganese [7439-96-5]^ 156 ug/L 1 1.50 10.0 1121030 EPA 6010D 10/25/21 10:57 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1J21030 EPA 6010D 10/25/21 10:57 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1J29005 EPA 6020B 11/02/21 23:39 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 10:57 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1J29005 EPA 6020B 11/02/21 23:39 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 10:57 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1J21030 EPA 6010D 10/25/21 10:57 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 18 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 19:21 ZGW Sulfate as SO4 [14808-79-B]^ 11 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/21/21 19:21 ZGW Sulfide [18496-25-8]^ 0.038 J mg/L 1 0.010 0.10 1122004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 210 D mg/L 5 70 75 1127021 EPA 310.2 10/27/21 16:15 JAH Total Dissolved Solids^ 200 mg/L 1 50 50 1125026 SM 254OC-2011 10/25/21 18:14 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 17 Of $2 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11DR Lab Sample ID:CE15554-03 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2109:20 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 3.9 ug/L 1 0.80 2.0 1325015 EPA 8260D 10/25/21 11:38 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.2 1 5.00 104 % 75-125 V25015 EPA 6260D 10125121 11:38 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 18 Of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW14 Lab Sample ID:CE15554-04 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 18:10 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,2-Dichlorobenzene [95-50-1]A 1.8 ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 1,4-Dichlorobenzene [306-46-7]^ 4.5 ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1127025 EPA 8260D 10/29/21 07:32 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1127025 EPA 8260D 10/29/21 07:32 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1127025 EPA 8260D 10/29/21 07:32 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1127025 EPA 8260D 10/29/21 07:32 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1127025 EPA 8260D 10/29/21 07:32 RKY Benzene [71-43-2]A 1.7 ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1127025 EPA 8260D 10/29/21 07:32 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Chlorobenzene [108-90-7]A 5.2 ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1127025 EPA 8260D 10/29/21 07:32 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Styrene[100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1127025 EPA 8260D 10/29/21 07:32 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1127025 EPA 8260D 10/29/21 07:32 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 19 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW14 Lab Sample ID:CE15554-04 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 18:10 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Vinyl chloride [75-01-4]^ 2.6 ug/L 1 0.32 1.0 1KO1035 EPA 8260D 11/01/21 20:56 ref Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27025 EPA 8260D 10/29/21 07:32 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 61 1 50.0 121 % 53-136 IJ27025 EPA 6260D 10129121 0732 RKY 4-Bromofluorobenzene 53 1 50.0 107 % 53-136 IK01035 EPA 6260D 11101121 20:56 ref Dibromofluoromethane 62 1 50.0 124 % 67-129 IJ27025 EPA 6260D 10129121 0732 RKY Dibromofluoromethane 56 1 50.0 112 % 67-129 IK01035 EPA 8260D 11101121 20:56 ref Toluene-c48 52 1 50.0 105 % 59-134 IJ27025 EPA 8260D 10129121 0732 RKY Toluene-c48 57 1 50.0 114 % 59-134 IK01035 EPA 6260D 11101121 20:56 ref Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed gy Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:06 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony[7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1J29005 EPA 6020B 11/02/21 23:43 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J21030 EPA 6010D 10/25/21 10:59 JDH Barium [7440-39-3]^ 44.7 ug/L 1 1.10 10.0 1121030 EPA 6010D 10/25/21 10:59 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1J21030 EPA 6010D 10/25/21 10:59 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 10:59 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 10:59 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 10:59 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1J21030 EPA 6010D 10/25/21 10:59 JDH Iron [7439-89-6]^ 136000 ug/L 1 22.0 50.0 1121030 EPA 6010D 10/25/21 10:59 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 10:59 JDH Manganese [7439-96-5]^ 176 ug/L 1 1.50 10.0 1121030 EPA 6010D 10/25/21 10:59 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1J21030 EPA 6010D 10/25/21 10:59 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1J29005 EPA 6020B 11/02/21 23:43 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 10:59 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1J29005 EPA 6020B 11/02/21 23:43 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 10:59 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1J21030 EPA 6010D 10/25/21 10:59 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 61 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 19:39 ZGW Sulfate as SO4 [14808-79-8]^ 7.0 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/21/21 19:39 ZGW Sulfide [18496-25-8]^ 0.16 mg/L 1 0.010 0.10 1120023 iM 4500S2 D-2011 10/20/21 16:45 JOC Total Alkalinity as CaCO3 [471-34-1]^ 220 D mg/L 5 70 75 1127021 EPA 310.2 10/27/21 16:16 JAH Total Dissolved Solids^ 250 mg/L 1 50 50 1125026 SM 254OC-2011 10/25/21 18:14 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 20 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW14 Lab Sample ID:CE15554-04 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 18:10 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 17 ug/L 1 0.80 2.0 1325015 EPA 8260D 10/25/21 12:04 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.2 1 5.00 103 % 75-125 V25015 EPA 6260D 10125121 12:04 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 21 of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17S Lab Sample ID:CE15554-05 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:05 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 1127025 EPA 8260D 10/29/21 08:00 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1127025 EPA 8260D 10/29/21 08:00 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 1127025 EPA 8260D 10/29/21 08:00 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 1127025 EPA 8260D 10/29/21 08:00 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 1127025 EPA 8260D 10/29/21 08:00 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 1127025 EPA 8260D 10/29/21 08:00 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Chlorobenzene [108-90-7]A 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY cis-1,2-Dichloroethene [156-59-2]A 1.3 ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 1127025 EPA 8260D 10/29/21 08:00 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Tetrahydrofuran [109-99-9]A 0.53 U ug/L 1 0.53 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 1127025 EPA 8260D 10/29/21 08:00 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 1127025 EPA 8260D 10/29/21 08:00 RKY Vinyl chloride [75-01-4]A 1.8 ug/L 1 0.32 1.0 IK01035 EPA 8260D 11/01/21 21:23 ref FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 22 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17S Lab Sample ID:CE15554-05 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:05 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27025 EPA 8260D 10/29/21 08:00 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 54 1 50.0 108 % 53-136 IJ27025 EPA 6260D 10129121 08:00 RKY 4-Bromofluorobenzene 55 1 50.0 110 % 53-136 IK01035 EPA 6260D 11101121 21:23 ref Dibromofluoromethane 62 1 50.0 124 % 67-129 IJ27025 EPA 6260D 10129121 08:00 RKY Dibromofluoromethane 57 1 50.0 115 % 67-129 IK01035 EPA 8260D 11101121 21:23 ref Toluene-d8 51 1 50.0 102 % 59-134 IJ27025 EPA 8260D 10129121 08:00 RKY Toluene-d8 58 1 50.0 116 % 59-134 IK01035 EPA 6260D 11101121 21:23 ref Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:13 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1J29005 EPA 6020B 11/02/21 23:53 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J21030 EPA 6010D 10/25/21 11:02 JDH Barium [7440-39-3]^ 84.2 ug/L 1 1.10 10.0 1121030 EPA 6010D 10/25/21 11:02 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1J21030 EPA 6010D 10/25/21 11:02 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 11:02 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:02 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:02 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1J21030 EPA 6010D 10/25/21 11:02 JDH Iron [7439-89-6]^ 48700 ug/L 1 22.0 50.0 1121030 EPA 6010D 10/25/21 11:02 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 11:02 JDH Manganese [7439-96-5]^ 181 ug/L 1 1.50 10.0 1121030 EPA 6010D 10/25/21 11:02 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1J21030 EPA 6010D 10/25/21 11:02 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1J29005 EPA 6020B 11/02/21 23:53 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 11:02 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1J29005 EPA 6020B 11/02/21 23:53 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:02 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1J21030 EPA 6010D 10/25/21 11:02 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 27 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 19:56 ZGW Sulfate as SO4 [14808-79-B]^ 95 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/21/21 19:56 ZGW Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1J22004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 190 mg/L 1 14 15 1127021 EPA 310.2 10/27/21 16:18 JAH Total Dissolved Solids^ 380 mg/L 1 50 50 1125026 SM 254OC-2011 10/25/21 18:14 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 23 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17S Lab Sample ID:CE15554-05 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:05 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 3.4 ug/L 1 0.80 2.0 1325015 EPA 8260D 10/25/21 12:30 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.5 1 5.00 110 % 75-125 V25015 EPA 6260D 10125121 12:30 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 24 Of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17D Lab Sample ID:CE15554-06 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 15:10 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1127025 EPA 8260D 10/29/21 08:28 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1127025 EPA 8260D 10/29/21 08:28 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1127025 EPA 8260D 10/29/21 08:28 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1127025 EPA 8260D 10/29/21 08:28 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1127025 EPA 8260D 10/29/21 08:28 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1127025 EPA 8260D 10/29/21 08:28 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1127025 EPA 8260D 10/29/21 08:28 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Tetrahydrofuran [109-99-9]^ 0.53 u ug/L 1 0.53 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1127025 EPA 8260D 10/29/21 08:28 RKY Vinyl chloride [75-01-4]^ 0.32 u ug/L 1 0.32 1.0 1127025 EPA 8260D 10/29/21 08:28 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 25 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17D Lab Sample ID:CE15554-06 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 15:10 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27025 EPA 8260D 10/29/21 08:28 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 60 1 50.0 121 % 53-136 IJ27025 EPA 6260D 10129121 08:28 RKY Dibromofluoromethane 58 1 50.0 115 % 67-129 IJ27025 EPA 6260D 10129121 08:28 RKY Toluene-c48 53 1 50.0 107 % 59-134 IJ27025 EPA 6260D 10129121 08:28 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MOIL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:15 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1J29005 EPA 6020B 11/02/21 23:58 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J21030 EPA 6010D 10/25/21 11:04 JDH Barium [7440-39-3]^ 36.4 ug/L 1 1.10 10.0 1121030 EPA 6010D 10/25/21 11:04 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1J21030 EPA 6010D 10/25/21 11:04 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 11:04 JDH Chromium [7440-47-3]^ 3.04 J ug/L 1 1.40 10.0 1121030 EPA 6010D 10/25/21 11:04 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:04 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1J21030 EPA 6010D 10/25/21 11:04 JDH Iron [7439-89-6]^ 2200 ug/L 1 22.0 50.0 1121030 EPA 6010D 10/25/21 11:04 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 11:04 JDH Manganese [7439-96-5]1 19.4 ug/L 1 1.50 10.0 1121030 EPA 6010D 10/25/21 11:04 JDH Nickel[7440-02-O]^ 2.92 J ug/L 1 2.20 10.0 1121030 EPA 6010D 10/25/21 11:04 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1J29005 EPA 6020B 11/02/21 23:58 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 11:04 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1J29005 EPA 6020B 11/02/21 23:58 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:04 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1J21030 EPA 6010D 10/25/21 11:04 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 3.0 J mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 20:14 ZGW Sulfate as SO4 [14808-79-B]^ 30 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/21/21 20:14 ZGW Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1J22004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 97 mg/L 1 14 15 1127021 EPA 310.2 10/27/21 16:18 JAH Total Dissolved Solids^ 150 mg/L 1 50 50 1125026 SM 254OC-2011 10/25/21 18:14 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 26 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17D Lab Sample ID:CE15554-06 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 15:10 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 7.1 ug/L 1 0.80 2.0 1325015 EPA 8260D 10/25/21 12:55 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.5 1 5.00 109 % 75-125 V25015 EPA 6260D 10125121 12:55 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 27 Of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE15554-07 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 13:55 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,1-Dichloropropene [563-58-6]A 0.15 U ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,1-Dichloropropene [563-58-6]A 0.15 U ug/L 1 0.15 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,2,4-Trichlorobenzene [120-82-1]A 0.14 U ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,2,4-Trichlorobenzene [120-82-1]A 0.14 U ug/L 1 0.14 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,3-Dichlorobenzene [541-73-1]A 0.15 U ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,3-Dichlorobenzene [541-73-1]A 0.15 U ug/L 1 0.15 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,3-Dichloropropane [142-28-9]A 0.16 U ug/L 1 0.16 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,3-Dichloropropane [142-28-9]A 0.16 U ug/L 1 0.16 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 2,2-Dichloropropane [594-20-7]A 0.28 U ug/L 1 0.28 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 2,2-Dichloropropane [594-20-7]A 0.28 U ug/L 1 0.28 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref QV-01 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 1127025 EPA 8260D 10/29/21 08:55 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1127025 EPA 8260D 10/29/21 08:55 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 3-Chloropropene [107-05-1]A 0.11 U ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY 3-Chloropropene [107-05-1]A 0.11 U ug/L 1 0.11 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 1127025 EPA 8260D 10/29/21 08:55 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Acetone [67-64-1]A 10 U ug/L 1 10 20 1127025 EPA 8260D 10/29/21 08:55 RKY Acetone [67-64-1]A 16 J ug/L 1 10 20 IK01035 EPA 8260D 11/01/21 21:51 ref Acetonitrile [75-05-8]A 5.0 U ug/L 1 5.0 10 1127025 EPA 8260D 10/29/21 08:55 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 28 Of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE15554-07 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 13:55 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes Acetonitrile [75-05-8]^ 5.0 u ug/L 1 5.0 10 1KO1035 EPA 8260D 11/01/21 21:51 ref Acrolein [107-02-8]^ 4.0 u ug/L 1 4.0 10 1127025 EPA 8260D 10/29/21 08:55 RKY Acrolein [107-02-8]^ 4.0 u ug/L 1 4.0 10 1KO1035 EPA 8260D 11/01/21 21:51 ref Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1127025 EPA 8260D 10/29/21 08:55 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1KO1035 EPA 8260D 11/01/21 21:51 ref Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Benzene [71-43-2]^ 0.15 u ug/L 1 0.15 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 1127025 EPA 8260D 10/29/21 08:55 RKY Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Chlorobenzene [108-90-7]^ 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Chlorobenzene [308-90-7]^ 0.93 J ug/L 1 0.17 1.0 IK01035 EPA 8260D 11/01/21 21:51 ref Chloroethane [75-00-3]^ 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Chloroethane [75-00-3]^ 0.23 u ug/L 1 0.23 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Chloroprene [126-99-8]^ 0.64 u ug/L 1 0.64 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Chloroprene [126-99-8]^ 0.64 u ug/L 1 0.64 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref cis-1,2-Dichloroethene [156-59-2]^ 2.3 ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY cis-1,2-Dichloroethene [156-59-2]^ 1.8 ug/L 1 0.15 1.0 IK01035 EPA 8260D 11/01/21 21:51 ref cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Dichlorodifluoromethane [75-71-8]^ 0.20 u ug/L 1 0.20 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Dichlorodifluoromethane [75-71-8]^ 0.20 u ug/L 1 0.20 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Ethyl Methacrylate [97-63-2]^ 0.38 u ug/L 1 0.38 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Ethyl Methacrylate [97-63-2]^ 0.38 u ug/L 1 0.38 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Ethylbenzene [100-41-4]^ 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Ethylbenzene [100-41-4]^ 0.13 u ug/L 1 0.13 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Hexachlorobutadiene [87-68-3]^ 0.22 u ug/L 1 0.22 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Hexachlorobutadiene [87-68-3]^ 0.22 u ug/L 1 0.22 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1127025 EPA 8260D 10/29/21 08:55 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1KO1035 EPA 8260D 11/01/21 21:51 ref FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 29 Of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE15554-07 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 13:55 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:lames Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes Isobutyl alcohol [78-83-1]A 11 U ug/L 1 11 50 1127025 EPA 8260D 10/29/21 08:55 RKY QL-02 Isobutyl alcohol [78-83-1]A 11 U ug/L 1 11 50 1KO1035 EPA 8260D 11/01/21 21:51 ref QL-02 Methacrylonitrile [126-98-7]A 4.9 U ug/L 1 4.9 10 1127025 EPA 8260D 10/29/21 08:55 RKY Methacrylonitrile [126-98-7]A 4.9 U ug/L 1 4.9 10 1KO1035 EPA 8260D 11/01/21 21:51 ref Methyl Methacrylate [80-62-6]A 0.51 U ug/L 1 0.51 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Methyl Methacrylate [80-62-6]A 0.51 U ug/L 1 0.51 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Naphthalene [91-20-3]A 0.11 U ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Naphthalene [91-20-3]A 0.11 U ug/L 1 0.11 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Propionitrile [107-12-0]A 5.0 U ug/L 1 5.0 10 1127025 EPA 8260D 10/29/21 08:55 RKY Propionitrile [107-12-0]A 5.0 U ug/L 1 5.0 10 1KO1035 EPA 8260D 11/01/21 21:51 ref Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Tetrahydrofuran [109-99-9]A 0.53 U ug/L 1 0.53 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 1127025 EPA 8260D 10/29/21 08:55 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 1127025 EPA 8260D 10/29/21 08:55 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Vinyl chloride [75-01-4]A 0.98 J ug/L 1 0.32 1.0 IK01035 EPA 8260D 11/01/21 21:51 ref Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 1127025 EPA 8260D 10/29/21 08:55 RKY Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 1KO1035 EPA 8260D 11/01/21 21:51 ref Surrogates Results DF Spikev/ %Rec %RecLimits Batch Method Analvzed " Notes 4-Bromofluorobenzene 59 1 50.0 118 % 53-136 IJ27025 EPA 8260D 10129121 08:55 RKY 4-Bromofluorobenzene 53 1 50.0 107 % 53-136 IK01035 EPA 8260D 11101121 21:51 ref Dibromofluoromethane 59 1 50.0 117 % 67-129 IJ27025 EPA 8260D 10129121 08:55 RKY Dibromofluoromethane 55 1 50.0 109 % 67-129 IK01035 EPA 8260D 11/01/2121:51 ref Toluene-& 53 1 50.0 106 % 59-134 IJ27025 EPA 8260D 10129121 08:55 RKY Toluene-& 56 1 50.0 113 % 59-134 IK01035 EPA 8260D 11101121 21:51 ref FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 30 Of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE15554-07 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 13:55 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte iCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed By Notes 1,2,4,5-Tetrachlorobenzene [95-94-3]A 3.4 U ug/L 1 3.4 10 1125011 EPA 8270E 10/27/21 15:21 DFM 1,2,4,5-Tetrachlorobenzene [95-94-3]A 3.4 U ug/L 1 3.4 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 1,3,5-Trinitrobenzene [99-35-4]A 3.0 U ug/L 1 3.0 10 1125011 EPA 8270E 10/27/21 15:21 DFM 1,3,5-Trinitrobenzene [99-35-4]A 3.0 U ug/L 1 3.0 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 1,3-Dinitrobenzene [99-65-0]A 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:21 DFM 1,3-Dinitrobenzene [99-65-0]A 2.5 U ug/L 1 2.5 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 1,4-Naphthoquinone [130-15-4]A 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:21 DFM 1,4-Naphthoquinone [130-15-4]A 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 1,4-Phenylenediamine [106-50-3]A 4.0 U ug/L 1 4.0 10 1125011 EPA 8270E 10/27/21 15:21 DFM 1,4-Phenylenediamine [106-50-3]A 4.0 U ug/L 1 4.0 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 1-Naphthylamine [134-32-7]A 2.2 U ug/L 1 2.2 10 1125011 EPA 8270E 10/27/21 15:21 DFM 1-Naphthylamine [134-32-7]A 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2,3,4,6-Tetrachlorophenol[58-90-2]A 2.4 U ug/L 1 2.4 10 1325011 EPA 8270E 10/27/21 15:21 DFM 2,3,4,6-Tetrachlorophenol[58-90-2]A 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2,4,5-Trichlorophenol[95-95-4]A 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2,4,5-Trichlorophenol[95-95-4]A 2.5 U ug/L 1 2.5 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 2,4,6-Trichlorophenol[88-06-2]A 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2,4,6-Trichlorophenol[88-06-2]A 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2,4-Dichlorophenol[120-83-2]A 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2,4-Dichlorophenol[120-83-2]A 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2,4-Dimethylphenol [105-67-9]A 2.3 U ug/L 1 2.3 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2,4-Dimethylphenol [105-67-9]A 2.3 U ug/L 1 2.3 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2,4-Dinitrophenol [51-28-5]A 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2,4-Dinitrophenol [51-28-5]A 2.6 U ug/L 1 2.6 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 2,4-Dinitrotoluene [121-14-2]A 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2,4-Dinitrotoluene [121-14-2]A 2.6 U ug/L 1 2.6 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 2,6-Dichlorophenol [87-65-0]A 2.0 U ug/L 1 2.0 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2,6-Dichlorophenol [87-65-0]A 2.0 U ug/L 1 2.0 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2,6-Dinitrotoluene [606-20-2]A 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2,6-Dinitrotoluene [606-20-2]A 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2-AcetylaminoFluorene [53-96-3]A 3.1 U ug/L 1 3.1 10 1325011 EPA 8270E 10/27/21 15:21 DFM 2-AcetylaminoFluorene [53-96-3]A 3.1 U ug/L 1 3.1 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2-Chloronaphthalene [91-58-7]A 2.8 U ug/L 1 2.8 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2-Chloronaphthalene [91-58-7]A 2.8 U ug/L 1 2.8 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 2-Chlorophenol[95-57-8]A 2.2 U ug/L 1 2.2 10 1125011 EPA 8270E 10/27/21 15:21 DFM A-07 2-Chlorophenol[95-57-8]A 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2-Methyl-4,6-dinitrophenol[534-52-1]A 3.3 U ug/L 1 3.3 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2-Methyl-4,6-dinitrophenol [534-52-1]A 3.3 U ug/L 1 3.3 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2-Methylnaphthalene [91-57-6]A 2.8 U ug/L 1 2.8 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2-Methylnaphthalene [91-57-6]A 2.8 U ug/L 1 2.8 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2-Methylphenol[95-48-7]A 2.0 U ug/L 1 2.0 10 1325011 EPA 8270E 10/27/21 15:21 DFM 2-Methylphenol[95-48-7]A 2.0 U ug/L 1 2.0 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2-Naphthylamine [91-59-8]A 3.0 U ug/L 1 3.0 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2-Naphthylamine [91-59-8]A 3.0 U ug/L 1 3.0 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2-Nitroaniline [88-74-4]A 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:21 DFM 2-Nitroaniline [88-74-4]A 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2-Nitrophenol[88-75-5]A 1.1 U ug/L 1 1.1 10 1125011 EPA 8270E 10/27/21 15:21 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 31 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE15554-07 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 13:55 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes 2-Nitrophenol[88-75-5]^ 1.1 U ug/L 1 1.1 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 3 & 4-Methylphenol[108-39-4/106-44-5]^ 2.1 U ug/L 1 2.1 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 3 & 4-Methylphenol[108-39-4/106-44-5]^ 2.1 U ug/L 1 2.1 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 3,3'-Dichlorobenzidine [91-94-1]^ 3.5 U ug/L 1 3.5 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 3,3'-Dichlorobenzidine [91-94-1]^ 3.5 U ug/L 1 3.5 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 3,3'-Dimethylbenzidine [119-93-7]^ 2.2 U ug/L 1 2.2 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 3,3'-Dimethylbenzidine [119-93-7]^ 2.2 U ug/L 1 2.2 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 3-Methylcholanthrene [56-49-5]^ 1.3 U ug/L 1 1.3 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 3-Methylcholanthrene [56-49-5]^ 1.3 U ug/L 1 1.3 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 3-Nitroaniline [99-09-2]^ 2.6 U ug/L 1 2.6 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 3-Nitroaniline [99-09-2]^ 2.6 U ug/L 1 2.6 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 4-Aminobiphenyl [92-67-1]^ 3.5 U ug/L 1 3.5 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 4-Aminobiphenyl[92-67-1]^ 3.5 U ug/L 1 3.5 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 4-Bromophenyl-phenylether[101-55-3]^ 2.4 U ug/L 1 2.4 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 4-Bromophenyl-phenylether[101-55-3]^ 2.4 U ug/L 1 2.4 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 4-Chloro-3-methylphenol[59-50-7]^ 2.4 U ug/L 1 2.4 10 1J25011 EPA 8270E 10/27/21 15:21 DFM A-07 4-Chloro-3-methylphenol[59-50-7]^ 2.4 U ug/L 1 2.4 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 4-Chloroaniline [106-47-8]^ 2.0 U ug/L 1 2.0 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 4-Chloroaniline [106-47-8]^ 2.0 U ug/L 1 2.0 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 4-Chlorophenyl-phenylether[7005-72-3]^ 2.6 U ug/L 1 2.6 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 4-Chlorophenyl-phenylether[7005-72-3]^ 2.6 U ug/L 1 2.6 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 4-Nitroaniline [100-01-6]^ 3.2 U ug/L 1 3.2 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 4-Nitroaniline [100-01-6]^ 3.2 U ug/L 1 3.2 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 4-Nitrophenol [100-02-7]^ 2.8 U ug/L 1 2.8 10 1J25011 EPA 8270E 10/27/21 15:21 DFM A-07 4-Nitrophenol[100-02-7]^ 2.8 U ug/L 1 2.8 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 5-Nitro-o-toluidine [99-55-8]^ 3.2 U ug/L 1 3.2 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 5-Nitro-o-toluidine [99-55-8]^ 3.2 U ug/L 1 3.2 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 7,12-Di methyl benz(a)anth racene 1.4 U ug/L 1 1.4 10 1J25011 EPA 8270E 10/27/21 15:21 DFM [57-97-6]^ 7,12-Di methyl benz(a)anth racene 1.4 U ug/L 1 1.4 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 [57-97-6]^ a,a-Dimethylphenethylamine [122-09-8]^ 3.5 U ug/L 1 3.5 10 1J25011 EPA 8270E 10/27/21 15:21 DFM a,a-Dimethylphenethylamine [122-09-8]^ 3.5 U ug/L 1 3.5 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Acenaphthene [83-32-9]^ 2.7 U ug/L 1 2.7 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Acenaphthene [83-32-9]^ 2.7 U ug/L 1 2.7 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Acenaphthylene[208-96-8]^ 2.6 U ug/L 1 2.6 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Acenaphthylene [208-96-8]^ 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Acetophenone[98-86-2]^ 2.0 U ug/L 1 2.0 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Acetophenone [98-86-2]^ 2.0 U ug/L 1 2.0 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Anthracene [120-12-7]^ 2.4 U ug/L 1 2.4 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Anthracene [120-12-7]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Benzo(a)anthracene [56-55-3]^ 2.4 U ug/L 1 2.4 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Benzo(a)anthracene [56-55-3]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Benzo(a)pyrene [50-32-8]^ 2.2 U ug/L 1 2.2 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Benzo(a)pyrene [50-32-8]^ 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Benzo(b)fluoranthene [205-99-2]^ 2.8 U ug/L 1 2.8 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Benzo(b)fluoranthene [205-99-2]^ 2.8 U ug/L 1 2.8 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 32 of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE15554-07 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 13:55 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Semivolatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed By Notes Benzo(g,h,i)perylene [191-24-2]^ 2.4 U ug/L 1 2.4 10 1125011 EPA 8270E 10/27/21 15:21 DFM Benzo(g,h,i)perylene [191-24-2]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Benzo(k)Fluoranthene[207-08-9]^ 2.4 U ug/L 1 2.4 10 1125011 EPA 8270E 10/27/21 15:21 DFM Benzo(k)Fluoranthene[207-08-9]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Benzyl alcohol [100-51-6]^ 2.4 U ug/L 1 2.4 10 1125011 EPA 8270E 10/27/21 15:21 DFM Benzyl alcohol [100-51-6]^ 2.4 U ug/L 1 2.4 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Bis(2-chloroethoxy)methane [111-91-1]^ 2.4 U ug/L 1 2.4 10 1125011 EPA 8270E 10/27/21 15:21 DFM Bis(2-chloroethoxy)methane [111-91-1]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Bis(2-chloroethyl)ether [111-44-4]^ 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:21 DFM Bis(2-chloroethyl)ether [111-44-4]^ 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Bis(2-chloroisopropyl)ether [108-60-1]^ 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:21 DFM Bis(2-chloroisopropyl)ether[108-60-1]^ 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Bis(2-ethylhexyl)phthalate [117-81-7]^ 1.9 U ug/L 1 1.9 5.0 1125011 EPA 8270E 10/27/21 15:21 DFM QV-01 Bis(2-ethylhexyl)phthalate [117-81-7]^ 1.9 U ug/L 1 1.9 5.0 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Butylbenzylphthalate [85-68-7]^ 3.8 U ug/L 1 3.8 10 1125011 EPA 8270E 10/27/21 15:21 DFM Butylbenzylphthalate [85-68-7]^ 3.8 U ug/L 1 3.8 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Chlorobenzilate [510-15-6]^ 2.4 U ug/L 1 2.4 10 1125011 EPA 8270E 10/27/21 15:21 DFM Chlorobenzilate [510-15-6]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Chrysene [218-01-9]^ 2.2 U ug/L 1 2.2 10 1125011 EPA 8270E 10/27/21 15:21 DFM Chrysene [218-01-9]^ 2.2 U ug/L 1 2.2 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Diallate [2303-16-4]^ 1.9 U ug/L 1 1.9 10 1125011 EPA 8270E 10/27/21 15:21 DFM Diallate [2303-16-4]^ 1.9 U ug/L 1 1.9 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Dibenzo(a,h)anthracene [53-70-3]^ 2.3 U ug/L 1 2.3 10 1125011 EPA 8270E 10/27/21 15:21 DFM Dibenzo(a,h)anthracene [53-70-3]^ 2.3 U ug/L 1 2.3 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Dibenzofuran [132-64-9]^ 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:21 DFM Dibenzofuran [132-64-9]^ 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Diethylphthalate [84-66-2]^ 2.4 U ug/L 1 2.4 10 1125011 EPA 8270E 10/27/21 15:21 DFM Diethylphthalate [84-66-2]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Dimethoate [60-51-5]^ 2.3 U ug/L 1 2.3 10 1125011 EPA 8270E 10/27/21 15:21 DFM Dimethoate [60-51-5]^ 2.3 U ug/L 1 2.3 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Dimethylphthalate [131-11-3]^ 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:21 DFM Dimethylphthalate [131-11-3]^ 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Di-n-butylphthalate [84-74-2]^ 2.8 U ug/L 1 2.8 10 1125011 EPA 8270E 10/27/21 15:21 DFM Di-n-butylphthalate [84-74-2]^ 2.8 U ug/L 1 2.8 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Di-n-octylphthalate [117-84-0]^ 3.1 U ug/L 1 3.1 10 1125011 EPA 8270E 10/27/21 15:21 DFM Di-n-octylphthalate [117-84-0]^ 3.1 U ug/L 1 3.1 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Disulfoton [298-04-4]^ 2.0 U ug/L 1 2.0 10 1125011 EPA 8270E 10/27/21 15:21 DFM Disulfoton [298-04-4]^ 2.0 U ug/L 1 2.0 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Ethyl methanesulfonate [62-50-0]^ 2.2 U ug/L 1 2.2 10 1125011 EPA 8270E 10/27/21 15:21 DFM Ethyl methanesulfonate [62-50-0]^ 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Famphur[52-85-7]^ 2.7 U ug/L 1 2.7 10 1125011 EPA 8270E 10/27/21 15:21 DFM Famphur[52-85-7]^ 2.7 U ug/L 1 2.7 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Fluoranthene[206-44-0]^ 3.1 U ug/L 1 3.1 10 1125011 EPA 8270E 10/27/21 15:21 DFM Fluoranthene[206-44-0]^ 3.1 U ug/L 1 3.1 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Fluorene [86-73-7]^ 2.5 U ug/L 1 2.5 10 1325011 EPA 8270E 10/27/21 15:21 DFM Fluorene [86-73-7]^ 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Hexachlorobenzene [118-74-1]^ 2.3 U ug/L 1 2.3 10 1125011 EPA 8270E 10/27/21 15:21 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 33 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE15554-07 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 13:55 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Hexachlorobenzene [118-74-1]^ 2.3 U ug/L 1 2.3 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Hexachlorobutadiene [87-68-3]^ 2.8 U ug/L 1 2.8 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Hexachlorobutadiene [87-68-3]^ 2.8 U ug/L 1 2.8 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Hexachlorocyclopentadiene [77-47-4]^ 2.7 U ug/L 1 2.7 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Hexachlorocyclopentadiene [77-47-4]^ 2.7 U ug/L 1 2.7 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Hexachloroethane [67-72-1]^ 2.6 U ug/L 1 2.6 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Hexachloroethane [67-72-1]^ 2.6 U ug/L 1 2.6 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Hexachloropropene [1888-71-7]^ 6.8 U ug/L 1 6.8 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Hexachloropropene [1888-71-7]^ 6.8 U ug/L 1 6.8 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Indeno(1,2,3-cd)pyrene [193-39-5]^ 2.2 U ug/L 1 2.2 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Indeno(1,2,3-cd)pyrene [193-39-5]^ 2.2 U ug/L 1 2.2 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Isodrin [465-73-6]^ 1.5 U ug/L 1 1.5 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Isodrin [465-73-6]^ 1.5 U ug/L 1 1.5 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Isophorone [78-59-1]^ 2.5 U ug/L 1 2.5 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Isophorone [78-59-1]^ 2.5 U ug/L 1 2.5 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Isosafrole [120-58-1]^ 2.2 U ug/L 1 2.2 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Isosafrole [120-58-1]^ 2.2 U ug/L 1 2.2 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 Kepone[143-50-0]^ 7.2 U ug/L 1 7.2 20 1J25011 EPA 8270E 10/27/21 15:21 DFM J-05 Kepone [143-50-0]^ 7.2 U ug/L 1 7.2 20 1K01006 EPA 8270E 11/01/21 18:42 DFM 1-05, 0-05 Methapyrilene [91-80-5]^ Methapyrilene [91-80-5]^ Methyl Methanesulfonate [66-27-3]^ Methyl Methanesulfonate [66-27-3]^ Methyl parathion [298-00-0]^ Methyl parathion [298-00-0]^ Nitrobenzene [98-95-3]^ Nitrobenzene [98-95-3]^ N-Nitrosodiethylamine [55-18-5]^ N-Nitrosodiethylamine [55-18-5]^ N-Nitrosodimethylamine [62-75-9]^ N-Nitrosodimethylamine [62-75-9]^ N-Nitrosodi-n-butylamine [924-16-3]^ N-Nitrosodi-n-butylamine [924-16-3]^ N-Nitroso-di-n-propylamine [621-64-7]^ N-Nitroso-di-n-propylamine [621-64-7]^ N-nitrosod i phenyla mine/Di phenylam i ne [86-30-6/122-39-4]^ N-nitrosodiphenylamine/Diphenylamine [86-30-6/122-39-4]^ N-Nitrosomethylethylamine [10595-95-6]^ N-Nitrosomethylethylamine [10595-95-6]^ N-Nitrosopiperidine [100-75-4]^ N-Nitrosopiperidine [100-75-4]^ N-Nitrosopyrrolidine [930-55-2]^ N-Nitrosopyrrolidine [930-55-2]^ 0,0,0-Triethyl phosphorothioate [126-68-1]^ 4.8 U ug/L 1 4.8 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 4.8 U ug/L 1 4.8 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2.2 U ug/L 1 2.2 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2.5 U ug/L 1 2.5 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2.5 U ug/L 1 2.5 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2.1 U ug/L 1 2.1 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 2.1 U ug/L 1 2.1 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 1.9 U ug/L 1 1.9 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 1.9 U ug/L 1 1.9 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2.0 U ug/L 1 2.0 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 2.0 U ug/L 1 2.0 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2.3 U ug/L 1 2.3 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 2.3 U ug/L 1 2.3 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 2.5 U ug/L 1 2.5 10 1J25011 EPA 8270E 10/27/21 15:21 DFM 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 1.9 U ug/L 1 1.9 10 1325011 EPA 8270E 10/27/21 15:21 DFM 1.9 U ug/L 1 1.9 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 2.1 U ug/L 1 2.1 10 1325011 EPA 8270E 10/27/21 15:21 DFM 2.1 U ug/L 1 2.1 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 1.9 U ug/L 1 1.9 10 1325011 EPA 8270E 10/27/21 15:21 DFM 1.9 U ug/L 1 1.9 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 2.2 U ug/L 1 2.2 10 1325011 EPA 8270E 10/27/21 15:21 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 34 of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE15554-07 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 13:55 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 0,0,0-Triethylphosphorothioate 2.2 U ug/L 1 2.2 10 1K01006 EPA 8270E 11/01/21 18:42 DFM 0-05 [126-68-1]^ o-Toluidine [95-53-4]^ 1.6 U ug/L 1 1.6 10 1J25011 EPA 8270E 10/27/21 15:21 DFM o-Toluidine [95-53-4]^ 1.6 U ug/L 1 1.6 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Parathion [56-38-2]^ 1.7 U ug/L 1 1.7 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Parathion [56-38-2]^ 1.7 U ug/L 1 1.7 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 p-Dimethylaminoazobenzene [60-11-7]^ 2.6 U ug/L 1 2.6 10 1J25011 EPA 8270E 10/27/21 15:21 DFM p-Dimethylaminoazobenzene [60-11-7]^ 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Pentachlorobenzene [608-93-5]^ 2.7 U ug/L 1 2.7 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Pentachlorobenzene [608-93-5]^ 2.7 U ug/L 1 2.7 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Pentachloronitrobenzene [82-68-8]^ 1.9 U ug/L 1 1.9 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Pentachloronitrobenzene [82-68-8]^ 1.9 U ug/L 1 1.9 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Phenacetin [62-44-2]^ 2.7 U ug/L 1 2.7 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Phenacetin [62-44-2]^ 2.7 U ug/L 1 2.7 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Phenanthrene[85-01-8]^ 2.6 U ug/L 1 2.6 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Phenanthrene [85-01-8]^ 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Phenol[108-95-2]^ 1.7 U ug/L 1 1.7 10 1J25011 EPA 8270E 10/27/21 15:21 DFM A-07 Phenol[108-95-2]^ 1.7 U ug/L 1 1.7 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Phorate [298-02-2]^ 2.1 U ug/L 1 2.1 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Phorate [298-02-2]^ 2.1 U ug/L 1 2.1 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Pronamide [23950-58-5]^ 1.7 U ug/L 1 1.7 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Pronamide [23950-58-5]^ 1.7 U ug/L 1 1.7 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Pyrene [129-00-0]^ 3.5 U ug/L 1 3.5 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Pyrene [129-00-0]^ 3.5 U ug/L 1 3.5 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Safrole [94-59-7]^ 2.2 U ug/L 1 2.2 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Safrole [94-59-7]^ 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Thionazin [297-97-2]^ 2.3 U ug/L 1 2.3 10 1J25011 EPA 8270E 10/27/21 15:21 DFM Thionazin [297-97-2]^ 2.3 U ug/L 1 2.3 10 1KO1006 EPA 8270E 11/01/21 18:42 DFM 0-05 Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 2,4,6-Tribromophenol 55 1 100 55 % 10-179 IJ25011 EPA 8270E 10127121 15:21 DFM 2,4,6-Tribromophenol 73 1 100 73 % 10-179 1KO1006 EPA 8270E 11101121 18:42 DFM 0-05 2-Fluorobiphenyl 34 1 50.0 69 % 10-149 IJ25011 EPA 8270E 10127121 15:21 DFM 2-Fluorobiphenyl 41 1 50.0 81 % 10-149 1KO1006 EPA 8270E 11101121 18:42 DFM 0-05 2-Fluorophenol 27 1 100 27 % 10-110 IJ25011 EPA 8270E 10127121 15:21 DFM 2-Fluorophenol 55 1 100 55 % 10-110 1KO1006 EPA 8270E 11101121 18:42 DFM 0-05 Nitrobenzene-d5 33 1 50.0 66 % 10-149 IJ25011 EPA 8270E 10127121 15:21 DFM Nitrobenzene-d5 34 1 50.0 67 % 10-149 1KO1006 EPA 8270E 11101121 18:42 DFM 0-05 Phenol-d5 38 1 100 38 % 10-88 IJ25011 EPA 8270E 10127121 15:21 DFM Phenol-d5 50 1 100 50 % 10-88 1KO1006 EPA 8270E 11101121 18:42 DFM 0-05 Terphenyl-d14 38 1 50.0 76 % 10-166 IJ25011 EPA 8270E 10127121 15:21 DFM Terphenyl-d14 42 1 50.0 84 % 10-166 1KO1006 EPA 8270E 11101121 16:42 DFM 0-05 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 35 of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE15554-07 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 13:55 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:lames Waters Organochlorine Pesticides by GC ^ - ENCO Cary rertified analyte [NC 591] Analvte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 4,4'-DDD [72-54-8]^ 0.044 U ug/L 1 0.044 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK 4,4'-DDE [72-55-9]^ 0.048 U ug/L 1 0.048 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK 4,4'-DDT [50-29-3]A 0.049 U ug/L 1 0.049 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Aldrin [309-00-2]^ 0.041 U ug/L 1 0.041 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK alpha-BHC [319-84-6]^ 0.036 U ug/L 1 0.036 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK beta-BHC [319-85-7]A 0.041 U ug/L 1 0.041 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Chlordane (tech) [12789-03-6]^ 0.37 U ug/L 1 0.37 0.50 1123005 EPA 8081E 10/27/21 13:57 LSK Chlordane -alpha [5103-71-9]^ 0.048 U ug/L 1 0.048 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Chlordane -gamma [5103-74-2]^ 0.042 U ug/L 1 0.042 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK delta-BHC [319-86-8]^ 0.048 U ug/L 1 0.048 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Dieldrin [60-57-1]A 0.045 U ug/L 1 0.045 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Endosulfan I [959-98-8]^ 0.045 U ug/L 1 0.045 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Endosulfan II[33213-65-9]^ 0.038 U ug/L 1 0.038 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Endosulfan sulfate [1031-07-8]^ 0.032 U ug/L 1 0.032 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Endrin [72-20-8]A 0.041 U ug/L 1 0.041 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Endrin aldehyde [7421-93-4]^ 0.049 U ug/L 1 0.049 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK gamma-BHC [58-89-9]A 0.034 U ug/L 1 0.034 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Heptachlor[76-44-8]A 0.047 U ug/L 1 0.047 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK QM-07 Heptachlor epoxide [1024-57-3]^ 0.037 U ug/L 1 0.037 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Methoxychlor[72-43-5]^ 0.048 U ug/L 1 0.048 0.050 1123005 EPA 8081E 10/27/21 13:57 LSK Toxaphene [8001-35-2]^ 0.28 U ug/L 1 0.28 1.0 1123005 EPA 8081E 10/27/21 13:57 LSK Surrogates Results DF Spike L v/ % Rec % Rec Limits Batch Method Analyzed By Notes 2,4,5,E-TCMX 0.95 1 1,00 95 % 10-139 IJ23005 EPA 8081B 10127121 13:57 LSK Decachlorobiphenyl 0.74 1 1,00 74 % 10-122 IJ23005 EPA 8081B 10127121 13:57 LSK Polychlorinated Biphenyls by GC ^ - ENCO Cary certified analyte [NC 5911 Analvte rCAS Numberl Results Flaa Units DF MDL I.2 Batch Method Analyzed By Notes PCB-1016/1242 [12674-11-2/53469-21-9]^ 0.48 u ug/L 1 0.48 0.50 1J23006 EPA 8082A 10/27/21 13:57 LSK PCB-1221 [11104-28-2]^ 0.43 u ug/L 1 0.43 0.50 1J23006 EPA 8082A 10/27/21 13:57 LSK PCB-1232 [11141-16-5]^ 0.50 u ug/L 1 0.50 0.50 1J23006 EPA 8082A 10/27/21 13:57 LSK PCB-1248 [12672-29-6]^ 0.45 u ug/L 1 0.45 0.50 1323006 EPA 8082A 10/27/21 13:57 LSK PCB-1254 [11097-69-1]^ 0.43 u ug/L 1 0.43 0.50 1J23006 EPA 8082A 10/27/21 13:57 LSK PCB-1260 [11096-82-5]^ 0.47 u ug/L 1 0.47 0.50 1J23006 EPA 8082A 10/27/21 13:57 LSK Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 2,4,5,E-TCMX 0.59 1 1.00 59 % 10-128 IJ23006 EPA 80824 10127121 13:57 LSK Decachlorobiphenyl 0.40 1 1.00 40 % 10-129 IJ23006 EPA 80824 10127121 13:57 LSK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 36 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE15554-07 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 13:55 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:17 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1J29005 EPA 6020B 11/03/21 00:02 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J21030 EPA 6010D 10/25/21 11:15 JDH Barium [7440-39-3]^ 78.1 ug/L 1 1.10 10.0 1321030 EPA 6010D 10/25/21 11:15 JDH Beryllium [7440-41-7]1 0.160 U ug/L 1 0.160 1.00 1J21030 EPA 6010D 10/25/21 11:15 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 11:15 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:15 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:15 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1J21030 EPA 6010D 10/25/21 11:15 JDH Iron [7439-89-6]^ 93400 ug/L 1 22.0 50.0 1321030 EPA 6010D 10/25/21 11:15 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 11:15 JDH Manganese [7439-96-5]^ 154 ug/L 1 1.50 10.0 1321030 EPA 6010D 10/25/21 11:15 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1J21030 EPA 6010D 10/25/21 11:15 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1J29005 EPA 6020B 11/03/21 00:02 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 11:15 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1J29005 EPA 6020B 11/03/21 00:02 RLF Tin [7440-31-5]^ 2.90 U ug/L 1 2.90 10.0 1J21030 EPA 6010D 10/25/21 11:15 JDH Vanadium [7440-62-2]1 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:15 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1J21030 EPA 6010D 10/25/21 11:15 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 44 mg/L 1 2.2 5.0 1321002 EPA 300.0 10/21/21 20:32 ZGW Cyanide (total) [57-12-5]^ 0.0049 U mg/L 1 0.0049 0.010 1J25024 EPA 9014 10/26/21 13:08 JAH Sulfate as SO4 [14808-79-8]^ 42 mg/L 1 2.9 5.0 1321002 EPA 300.0 10/21/21 20:32 ZGW Sulfide [18496-25-8]^ 0.056 J mg/L 1 0.010 0.10 1322004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 310 D mg/L 5 70 75 1327021 EPA 310.2 10/27/21 16:19 JAH Total Dissolved Solids^ 410 mg/L 1 50 50 1325026 SM 2540C-2011 10/25/21 18:14 DMJ Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 13 ug/L 1 0.80 2.0 1325015 EPA 8260D 10/25/21 13:21 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-c48 5.5 1 5.00 110 % 75-125 IJ25015 EPA 6260D 10125121 13:21 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 37 of $2 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CE15554-07 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 13:55 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Chlorinated Herbicides by GC A - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 2,4,5-T [93-76-5]^ 0.28 U ug/L 1 0.28 0.50 1J25043 EPA 8151A 10/27/21 19:24 FCV 2,4,5-TP (silvex) [93-72-1]^ 0.44 U ug/L 1 0.44 0.50 1J25043 EPA 8151A 10/27/21 19:24 FCV 2,4-D [94-75-7]^ 0.27 U ug/L 1 0.27 0.50 1J25043 EPA 8151A 10/27/21 19:24 FCV Dinoseb [88-85-7]^ 0.32 U ug/L 1 0.32 0.50 1J25043 EPA 8151A 10/27/21 19:24 FCV Pentachlorophenol[87-86-5]^ 0.19 U ug/L 1 0.19 0.50 1J25043 EPA 8151A 10/27/21 19:24 FCV Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 2,4-DCAA 1.2 1 2,00 60 % 37-134 V25043 EPA 6151A 10127121 19:24 FCV FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 38 of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE15554-08 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:45 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,1-Dichloropropene [563-58-6]^ 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,2,4-Trichlorobenzene [120-82-1]^ 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,3-Dichlorobenzene [541-73-1]^ 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,3-Dichloropropane [142-28-9]^ 0.16 u ug/L 1 0.16 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 2,2-Dichloropropane [594-20-7]^ 0.28 u ug/L 1 0.28 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1127025 EPA 8260D 10/29/21 09:23 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1127025 EPA 8260D 10/29/21 09:23 RKY 3-Chloropropene [107-05-1]A 0.11 u ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1127025 EPA 8260D 10/29/21 09:23 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1127025 EPA 8260D 10/29/21 09:23 RKY Acetonitrile [75-05-8]A 5.0 u ug/L 1 5.0 10 1127025 EPA 8260D 10/29/21 09:23 RKY Acrolein [107-02-8]A 4.0 u ug/L 1 4.0 10 1127025 EPA 8260D 10/29/21 09:23 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1127025 EPA 8260D 10/29/21 09:23 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1127025 EPA 8260D 10/29/21 09:23 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Chloroprene [126-99-8]A 0.64 u ug/L 1 0.64 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Dichlorodifluoromethane [75-71-8]A 0.20 u ug/L 1 0.20 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Ethyl Methacrylate [97-63-2]^ 0.38 u ug/L 1 0.38 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Hexachlorobutadiene [87-68-3]A 0.22 u ug/L 1 0.22 1.0 1127025 EPA 8260D 10/29/21 09:23 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1127025 EPA 8260D 10/29/21 09:23 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 39 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE15554-08 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:45 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed AX Notes Isobutyl alcohol [78-83-1]^ 11 U ug/L 1 11 50 1J27025 EPA 8260D 10/29/21 09:23 RKY QL-02 Methacrylonitrile [126-98-7]^ 4.9 U ug/L 1 4.9 10 1J27025 EPA 8260D 10/29/21 09:23 RKY Methyl Methacrylate [80-62-6]^ 0.51 U ug/L 1 0.51 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Propionitrile [107-12-0]^ 5.0 U ug/L 1 5.0 10 1J27025 EPA 8260D 10/29/21 09:23 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27025 EPA 8260D 10/29/21 09:23 RKY Surrogates Results DF Spike LN % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 61 1 50.0 123 % 53-136 IJ27025 EPA 6260D 10129121 09:23 RKY Dibromofluoromethane 58 1 50.0 117 % 67-129 IJ27025 EPA 6260D 10129121 09:23 RKY Toluene-d8 52 1 50.0 104 % 59-134 IJ27025 EPA 6260D 10129121 09:23 RKY Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,2,4,5-Tetrachlorobenzene [95-94-3]^ 3.4 U ug/L 1 3.4 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 1,2,4,5-Tetrachlorobenzene [95-94-3]^ 3.4 U ug/L 1 3.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 1,3,5-Trinitrobenzene [99-35-4]^ 3.0 U ug/L 1 3.0 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 1,3,5-Trinitrobenzene [99-35-4]^ 3.0 U ug/L 1 3.0 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 1,3-Dinitrobenzene [99-65-0]^ 2.5 U ug/L 1 2.5 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 1,3-Dinitrobenzene [99-65-0]^ 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 1,4-Naphthoquinone [130-15-4]^ 2.5 U ug/L 1 2.5 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 1,4-Naphthoquinone [130-15-4]^ 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 1,4-Phenylenediamine [106-50-3]^ 4.0 U ug/L 1 4.0 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 1,4-Phenylenediamine [106-50-3]^ 4.0 U ug/L 1 4.0 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 1-Naphthylamine [134-32-7]^ 2.2 U ug/L 1 2.2 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 1-Naphthylamine [134-32-7]^ 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2,3,4,6-Tetrachlorophenol[58-90-2]^ 2.4 U ug/L 1 2.4 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 2,3,4,6-Tetrachlorophenol[58-90-2]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2,4,5-Trichlorophenol[95-95-4]^ 2.5 U ug/L 1 2.5 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 2,4,5-Trichlorophenol[95-95-4]^ 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2,4,6-Trichlorophenol[88-06-2]^ 2.6 U ug/L 1 2.6 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 2,4,6-Trichlorophenol[88-06-2]^ 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2,4-Dichlorophenol[120-83-2]^ 2.6 U ug/L 1 2.6 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 2,4-Dichlorophenol[120-83-2]^ 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 40 of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE15554-08 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:45 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed By Notes 2,4-Dimethylphenol [105-67-9]^ 2.3 U ug/L 1 2.3 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2,4-Dimethylphenol [105-67-9]^ 2.3 U ug/L 1 2.3 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2,4-Dinitrophenol [51-28-5]^ 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2,4-Dinitrophenol [51-28-5]^ 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2,4-Dinitrotoluene [121-14-2]^ 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2,4-Dinitrotoluene [121-14-2]^ 2.6 U ug/L 1 2.6 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 2,6-Dichlorophenol [87-65-0]^ 2.0 U ug/L 1 2.0 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2,6-Dichlorophenol [87-65-0]^ 2.0 U ug/L 1 2.0 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2,6-Dinitrotoluene [606-20-2]^ 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2,6-Dinitrotoluene [606-20-2]^ 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2-AcetylaminoFluorene [53-96-3]^ 3.1 U ug/L 1 3.1 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2-AcetylaminoFluorene [53-96-3]^ 3.1 U ug/L 1 3.1 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2-Chloronaphthalene [91-58-7]^ 2.8 U ug/L 1 2.8 10 1325011 EPA 8270E 10/27/21 15:52 DFM 2-Chloronaphthalene [91-58-7]^ 2.8 U ug/L 1 2.8 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2-Chlorophenol[95-57-8]^ 2.2 U ug/L 1 2.2 10 1125011 EPA 8270E 10/27/21 15:52 DFM A-07 2-Chlorophenol[95-57-8]^ 2.2 U ug/L 1 2.2 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 2-Methyl-4,6-dinitrophenol[534-52-1]^ 3.3 U ug/L 1 3.3 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2-Methyl-4,6-dinitrophenol[534-52-1]^ 3.3 U ug/L 1 3.3 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2-Methylnaphthalene [91-57-6]^ 2.8 U ug/L 1 2.8 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2-Methylnaphthalene [91-57-6]^ 2.8 U ug/L 1 2.8 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2-Methylphenol[95-48-7]^ 2.0 U ug/L 1 2.0 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2-Methylphenol[95-48-7]^ 2.0 U ug/L 1 2.0 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 2-Naphthylamine [91-59-8]^ 3.0 U ug/L 1 3.0 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2-Naphthylamine [91-59-8]^ 3.0 U ug/L 1 3.0 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 2-Nitroaniline [88-74-4]^ 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2-Nitroaniline [88-74-4]^ 2.5 U ug/L 1 2.5 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 2-Nitrophenol[88-75-5]^ 1.1 U ug/L 1 1.1 10 1125011 EPA 8270E 10/27/21 15:52 DFM 2-Nitrophenol[88-75-5]^ 1.1 U ug/L 1 1.1 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 3 & 4-Methylphenol[108-39-4/106-44-5]^ 2.1 U ug/L 1 2.1 10 1125011 EPA 8270E 10/27/21 15:52 DFM 3 & 4-Methylphenol[108-39-4/106-44-5]^ 2.1 U ug/L 1 2.1 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 3,3'-Dichlorobenzidine [91-94-1]^ 3.5 U ug/L 1 3.5 10 1325011 EPA 8270E 10/27/21 15:52 DFM 3,3'-Dichlorobenzidine [91-94-1]^ 3.5 U ug/L 1 3.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 3,3'-Dimethylbenzidine [119-93-7]^ 2.2 U ug/L 1 2.2 10 1125011 EPA 8270E 10/27/21 15:52 DFM 3,3'-Dimethylbenzidine [119-93-7]^ 2.2 U ug/L 1 2.2 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 3-Methylcholanthrene [56-49-5]^ 1.3 U ug/L 1 1.3 10 1125011 EPA 8270E 10/27/21 15:52 DFM 3-Methylcholanthrene [56-49-5]^ 1.3 U ug/L 1 1.3 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 3-Nitroaniline [99-09-2]^ 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:52 DFM 3-Nitroaniline [99-09-2]^ 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 4-Aminobiphenyl[92-67-1]^ 3.5 U ug/L 1 3.5 10 1125011 EPA 8270E 10/27/21 15:52 DFM 4-Aminobiphenyl[92-67-1]^ 3.5 U ug/L 1 3.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 4-Bromophenyl-phenylether[101-55-3]^ 2.4 U ug/L 1 2.4 10 1325011 EPA 8270E 10/27/21 15:52 DFM 4-Bromophenyl-phenylether[101-55-3]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 4-Chloro-3-methylphenol[59-50-7]^ 2.4 U ug/L 1 2.4 10 1125011 EPA 8270E 10/27/21 15:52 DFM A-07 4-Chloro-3-methylphenol[59-50-7]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 4-Chloroaniline [106-47-8]^ 2.0 U ug/L 1 2.0 10 1125011 EPA 8270E 10/27/21 15:52 DFM 4-Chloroaniline [106-47-8]^ 2.0 U ug/L 1 2.0 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 4-Chlorophenyl-phenylether[7005-72-3]^ 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:52 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 41 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE15554-08 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:45 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 4-Chlorophenyl-phenylether[7005-72-3]^ 2.6 U ug/L 1 2.6 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 4-Nitroaniline [100-01-6]^ 3.2 U ug/L 1 3.2 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 4-Nitroaniline [100-01-6]^ 3.2 U ug/L 1 3.2 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 4-Nitrophenol[100-02-7]^ 2.8 U ug/L 1 2.8 10 1J25011 EPA 8270E 10/27/21 15:52 DFM A-07 4-Nitrophenol[100-02-7]^ 2.8 U ug/L 1 2.8 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 5-Nitro-o-toluidine [99-55-8]^ 3.2 U ug/L 1 3.2 10 1J25011 EPA 8270E 10/27/21 15:52 DFM 5-Nitro-o-toluidine [99-55-8]^ 3.2 U ug/L 1 3.2 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 7,12-Di methyl benz(a)anth racene 1.4 U ug/L 1 1.4 10 1J25011 EPA 8270E 10/27/21 15:52 DFM [57-97-6]^ 7,12-Di methyl benz(a)a nth racene 1.4 U ug/L 1 1.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 [57-97-6]^ a,a-Dimethylphenethylamine [122-09-8]^ 3.5 U ug/L 1 3.5 10 1J25011 EPA 8270E 10/27/21 15:52 DFM a,a-Dimethylphenethylamine [122-09-8]^ 3.5 U ug/L 1 3.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Acenaphthene [83-32-9]^ 2.7 U ug/L 1 2.7 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Acenaphthene [83-32-9]^ 2.7 U ug/L 1 2.7 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Acenaphthylene[208-96-8]^ 2.6 U ug/L 1 2.6 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Acenaphthylene [208-96-8]^ 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Acetophenone[98-86-2]^ 2.0 U ug/L 1 2.0 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Acetophenone [98-86-2]^ 2.0 U ug/L 1 2.0 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Anthracene [120-12-7]^ 2.4 U ug/L 1 2.4 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Anthracene [120-12-7]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Benzo(a)anthracene [56-55-3]^ 2.4 U ug/L 1 2.4 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Benzo(a)anthracene [56-55-3]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Benzo(a)pyrene [50-32-8]^ 2.2 U ug/L 1 2.2 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Benzo(a)pyrene [50-32-8]^ 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Benzo(b)fluoranthene [205-99-2]^ 2.8 U ug/L 1 2.8 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Benzo(b)fluoranthene [205-99-2]^ 2.8 U ug/L 1 2.8 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Benzo(g,h,i)perylene [191-24-2]^ 2.4 U ug/L 1 2.4 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Benzo(g,h,i)perylene [191-24-2]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Benzo(k)fluoranthene [207-08-9]^ 2.4 U ug/L 1 2.4 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Benzo(k)fluoranthene [207-08-9]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Benzylalcohol [100-51-6]^ 2.4 U ug/L 1 2.4 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Benzylalcohol [100-51-6]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Bis(2-chloroethoxy)methane [111-91-1]^ 2.4 U ug/L 1 2.4 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Bis(2-chloroethoxy)methane [111-91-1]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Bis(2-chloroethyl)ether[111-44-4]^ 2.6 U ug/L 1 2.6 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Bis(2-chloroethyl)ether[111-44-4]^ 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Bis(2-chloroisopropyl)ether[108-60-1]^ 2.5 U ug/L 1 2.5 10 1J25011 EPA 8270E 10/27/21 15:52 DFM Bis(2-chloroisopropyl)ether[108-60-1]^ 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Bis(2-ethylhexyl)phthalate [117-81-7]^ 1.9 U ug/L 1 1.9 5.0 1J25011 EPA 8270E 10/27/21 15:52 DFM QV-01 Bis(2-ethylhexyl)phthalate 4.0 J ug/L 1 1.9 5.0 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 [117-81-7]^ Butyl benzylphtha late [85-68-7]^ 3.8 U ug/L 1 3.8 10 1325011 EPA 8270E 10/27/21 15:52 DFM Butyl benzylphtha late [85-68-7]^ 3.8 U ug/L 1 3.8 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 Chlorobenzilate [510-15-6]^ 2.4 U ug/L 1 2.4 10 1325011 EPA 8270E 10/27/21 15:52 DFM Chlorobenzilate [510-15-6]^ 2.4 U ug/L 1 2.4 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 Chrysene [218-01-9]^ 2.2 U ug/L 1 2.2 10 1325011 EPA 8270E 10/27/21 15:52 DFM Chrysene [218-01-9]^ 2.2 U ug/L 1 2.2 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 42 of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE15554-08 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:45 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Semivolatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed By Notes Diallate [2303-16-4]^ 1.9 U ug/L 1 1.9 10 1125011 EPA 8270E 10/27/21 15:52 DFM Diallate [2303-16-4]^ 1.9 U ug/L 1 1.9 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Dibenzo(a,h)anthracene [53-70-3]^ 2.3 U ug/L 1 2.3 10 1125011 EPA 8270E 10/27/21 15:52 DFM Dibenzo(a,h)anthracene [53-70-3]^ 2.3 U ug/L 1 2.3 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Dibenzofuran [132-64-9]^ 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:52 DFM Dibenzofuran [132-64-9]^ 2.6 U ug/L 1 2.6 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 Diethylphthalate [84-66-2]^ 2.4 U ug/L 1 2.4 10 1125011 EPA 8270E 10/27/21 15:52 DFM Diethylphthalate [84-66-2]^ 2.4 U ug/L 1 2.4 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Dimethoate [60-51-5]^ 2.3 U ug/L 1 2.3 10 1125011 EPA 8270E 10/27/21 15:52 DFM Dimethoate [60-51-5]^ 2.3 U ug/L 1 2.3 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Dimethylphthalate [131-11-3]^ 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:52 DFM Dimethylphthalate [131-11-3]^ 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Di-n-butylphthalate [84-74-2]^ 2.8 U ug/L 1 2.8 10 1325011 EPA 8270E 10/27/21 15:52 DFM Di-n-butylphthalate [84-74-2]^ 2.8 U ug/L 1 2.8 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Di-n-octylphthalate [117-84-0]^ 3.1 U ug/L 1 3.1 10 1125011 EPA 8270E 10/27/21 15:52 DFM Di-n-octylphthalate [117-84-0]^ 3.1 U ug/L 1 3.1 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 Disulfoton [298-04-4]^ 2.0 U ug/L 1 2.0 10 1125011 EPA 8270E 10/27/21 15:52 DFM Disulfoton [298-04-4]^ 2.0 U ug/L 1 2.0 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Ethyl methanesulfonate [62-50-0]^ 2.2 U ug/L 1 2.2 10 1125011 EPA 8270E 10/27/21 15:52 DFM Ethyl methanesulfonate [62-50-0]^ 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Famphur[52-85-7]^ 2.7 U ug/L 1 2.7 10 1125011 EPA 8270E 10/27/21 15:52 DFM Famphur[52-85-7]^ 2.7 U ug/L 1 2.7 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Fluoranthene[206-44-0]^ 3.1 U ug/L 1 3.1 10 1125011 EPA 8270E 10/27/21 15:52 DFM Fluoranthene[206-44-0]^ 3.1 U ug/L 1 3.1 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 Fluorene [86-73-7]^ 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:52 DFM Fluorene [86-73-7]^ 2.5 U ug/L 1 2.5 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 Hexachlorobenzene [118-74-1]^ 2.3 U ug/L 1 2.3 10 1125011 EPA 8270E 10/27/21 15:52 DFM Hexachlorobenzene[118-74-1]^ 2.3 U ug/L 1 2.3 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Hexachlorobutadiene [87-68-3]^ 2.8 U ug/L 1 2.8 10 1125011 EPA 8270E 10/27/21 15:52 DFM Hexachlorobutadiene [87-68-3]^ 2.8 U ug/L 1 2.8 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Hexachlorocyclopentadiene [77-47-4]^ 2.7 U ug/L 1 2.7 10 1325011 EPA 8270E 10/27/21 15:52 DFM Hexachlorocyclopentadiene [77-47-4]^ 2.7 U ug/L 1 2.7 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Hexachloroethane [67-72-1]^ 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:52 DFM Hexachloroethane [67-72-1]^ 2.6 U ug/L 1 2.6 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 Hexachloropropene [1888-71-7]^ 6.8 U ug/L 1 6.8 10 1125011 EPA 8270E 10/27/21 15:52 DFM Hexachloropropene [1888-71-7]^ 6.8 U ug/L 1 6.8 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Indeno(1,2,3-cd)pyrene [193-39-5]^ 2.2 U ug/L 1 2.2 10 1125011 EPA 8270E 10/27/21 15:52 DFM Indeno(1,2,3-cd)pyrene [193-39-5]^ 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Isodrin [465-73-6]^ 1.5 U ug/L 1 1.5 10 1125011 EPA 8270E 10/27/21 15:52 DFM Isodrin [465-73-6]^ 1.5 U ug/L 1 1.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Isophorone [78-59-1]^ 2.5 U ug/L 1 2.5 10 1325011 EPA 8270E 10/27/21 15:52 DFM Isophorone[78-59-1]^ 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Isosafrole [120-58-1]^ 2.2 U ug/L 1 2.2 10 1125011 EPA 8270E 10/27/21 15:52 DFM Isosafrole [120-58-1]^ 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Kepone[143-50-0]^ 7.2 U ug/L 1 7.2 20 1125011 EPA 8270E 10/27/21 15:52 DFM 3-05 Kepone[143-50-0]^ 7.2 U ug/L 1 7.2 20 1KO1006 EPA 8270E 11/01/21 19:13 DFM 3-05, 0-05 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 43 Of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE15554-08 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:45 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Semivolatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes Methapyrilene [91-80-5]A 4.8 U ug/L 1 4.8 10 1125011 EPA 8270E 10/27/21 15:52 DFM Methapyrilene [91-80-5]A 4.8 U ug/L 1 4.8 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Methyl Methanesulfonate [66-27-3]A 2.2 U ug/L 1 2.2 10 1125011 EPA 8270E 10/27/21 15:52 DFM Methyl Methanesulfonate [66-27-3]A 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Methyl parathion [298-00-0]A 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:52 DFM Methyl parathion [298-00-0]A 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Nitrobenzene [98-95-3]A 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:52 DFM Nitrobenzene [98-95-3]A 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 N-Nitrosodiethylamine [55-18-5]A 2.1 U ug/L 1 2.1 10 1125011 EPA 8270E 10/27/21 15:52 DFM N-Nitrosodiethylamine [55-18-5]A 2.1 U ug/L 1 2.1 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 N-Nitrosodimethylamine [62-75-9]A 1.9 U ug/L 1 1.9 10 1125011 EPA 8270E 10/27/21 15:52 DFM N-Nitrosodimethylamine [62-75-9]A 1.9 U ug/L 1 1.9 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 N-Nitrosodi-n-butylamine [924-16-3]A 2.0 U ug/L 1 2.0 10 1125011 EPA 8270E 10/27/21 15:52 DFM N-Nitrosodi-n-butylamine [924-16-3]A 2.0 U ug/L 1 2.0 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 N-Nitroso-di-n-propylamine [621-64-7]A 2.3 U ug/L 1 2.3 10 1125011 EPA 8270E 10/27/21 15:52 DFM N-Nitroso-di-n-propylamine [621-64-7]A 2.3 U ug/L 1 2.3 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 N-nitrosodiphenylamine/Diphenylamine 2.5 U ug/L 1 2.5 10 1125011 EPA 8270E 10/27/21 15:52 DFM [86-30-6/122-39-4]A N-nitrosodiphenylamine/Diphenylamine 2.5 U ug/L 1 2.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 [86-30-6/122-39-4]A N-Nitrosomethylethylamine [10595-95-6]A 1.9 U ug/L 1 1.9 10 1325011 EPA 8270E 10/27/21 15:52 DFM N-Nitrosomethylethylamine [10595-95-6]A 1.9 U ug/L 1 1.9 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 N-Nitrosopiperidine [100-75-4]A 2.1 U ug/L 1 2.1 10 1325011 EPA 8270E 10/27/21 15:52 DFM N-Nitrosopiperidine [100-75-4]A 2.1 U ug/L 1 2.1 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 N-Nitrosopyrrolidine [930-55-2]A 1.9 U ug/L 1 1.9 10 1J25011 EPA 8270E 10/27/21 15:52 DFM N-Nitrosopyrrolidine [930-55-2]A 1.9 U ug/L 1 1.9 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 0,0,0-Triethylphosphorothioate 2.2 U ug/L 1 2.2 10 1325011 EPA 8270E 10/27/21 15:52 DFM [126-68-1]A 0,0,0-Triethylphosphorothioate 2.2 U ug/L 1 2.2 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 [126-68-1]A o-Toluidine [95-53-4]A 1.6 U ug/L 1 1.6 10 1125011 EPA 8270E 10/27/21 15:52 DFM o-Toluidine [95-53-4]A 1.6 U ug/L 1 1.6 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Parathion [56-38-2]A 1.7 U ug/L 1 1.7 10 1125011 EPA 8270E 10/27/21 15:52 DFM Parathion [56-38-2]A 1.7 U ug/L 1 1.7 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 p-Dimethylaminoazobenzene [60-11-7]A 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:52 DFM p-Dimethylaminoazobenzene [60-11-7]A 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Pentachlorobenzene [608-93-5]A 2.7 U ug/L 1 2.7 10 1125011 EPA 8270E 10/27/21 15:52 DFM Pentachlorobenzene [608-93-5]A 2.7 U ug/L 1 2.7 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Pentachloronitrobenzene [82-68-8]A 1.9 U ug/L 1 1.9 10 1125011 EPA 8270E 10/27/21 15:52 DFM Pentachloronitrobenzene [82-68-8]A 1.9 U ug/L 1 1.9 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Phenacetin [62-44-2]A 2.7 U ug/L 1 2.7 10 1125011 EPA 8270E 10/27/21 15:52 DFM Phenacetin [62-44-2]A 2.7 U ug/L 1 2.7 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Phenanthrene [85-01-8]A 2.6 U ug/L 1 2.6 10 1125011 EPA 8270E 10/27/21 15:52 DFM Phenanthrene [85-01-8]A 2.6 U ug/L 1 2.6 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Phenol[108-95-2]A 1.7 U ug/L 1 1.7 10 1125011 EPA 8270E 10/27/21 15:52 DFM A-07 Phenol[108-95-2]A 1.7 U ug/L 1 1.7 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Phorate [298-02-2]A 2.1 U ug/L 1 2.1 10 1125011 EPA 8270E 10/27/21 15:52 DFM Phorate [298-02-2]A 2.1 U ug/L 1 2.1 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 44 Of 82 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE15554-08 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:45 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:lames Waters Semivolatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analvte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed By Notes Pronamide [23950-58-5]A 1.7 u ug/L 1 1.7 10 1125011 EPA 8270E 10/27/21 15:52 DFM Pronamide [23950-58-5]A 1.7 u ug/L 1 1.7 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Pyrene [129-00-0]A 3.5 u ug/L 1 3.5 10 1125011 EPA 8270E 10/27/21 15:52 DFM Pyrene [129-00-0]A 3.5 u ug/L 1 3.5 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Safrole [94-59-7]A 2.2 u ug/L 1 2.2 10 1125011 EPA 8270E 10/27/21 15:52 DFM Safrole [94-59-7]A 2.2 u ug/L 1 2.2 10 1K01006 EPA 8270E 11/01/21 19:13 DFM 0-05 Thionazin [297-97-2]A 2.3 u ug/L 1 2.3 10 1125011 EPA 8270E 10/27/21 15:52 DFM Thionazin [297-97-2]A 2.3 u ug/L 1 2.3 10 1KO1006 EPA 8270E 11/01/21 19:13 DFM 0-05 Surrogates Results DF Spike L v/ % Rec % Rec Limits Batch Method Analyzed " Notes 2,4,6-Tribromophenol 11 1 100 11 % 10-179 IJ25011 EPA 8270E 10127121 15:52 DFM 2,4,6-Tribromophenol 67 1 100 67 % 10-179 IK01006 EPA 8270E 11101121 19:13 DFM 0-05 2-Fluorobiphenyl 43 1 50.0 87 % 10-149 IJ25011 EPA 8270E 10127121 15:52 DFM 2-Fluorobiphenyl 34 1 50.0 67 % 10-149 IK01006 EPA 8270E 11/01/11 19:13 DFM 0-05 1-Fluorophenol 9.1 1 100 9 % 10-110 IJ25011 EPA 8270E 10127121 15:52 DFM Q5-03 1-Fluorophenol 43 1 100 43 % 10-110 IK01006 EPA 8270E 11101121 19:13 DFM 0-05 Nitrobenzene-d5 42 1 50.0 84 % 10-149 IJ25011 EPA 8270E 10127121 15:52 DFM Nitrobenzene-d5 28 1 50.0 57 % 10-149 IK01006 EPA 8170E 11/01/11 19:13 DFM 0-05 Phenol-d5 8.8 1 100 9 % 10-88 IJ25011 EPA 8170E 10127121 15:52 DFM Q5-03 Phenol-d5 43 1 100 43 % 10-88 IK01006 EPA 8270E 11/01/11 19:13 DFM 0-05 Terphenyl-d14 44 1 50.0 88 % 10-188 IJ25011 EPA 8170E 10127121 15:52 DFM Terphenyl-d14 38 1 50.0 76 % 10-188 IK01006 EPA 8270E 11/01/11 19:13 DFM 0-05 IOrganochlorine Pesticides by GC ' ^ - ENCO Cary certified analyte [NC 591] Analvte rCAS Numberl Results Flaa Units DF MDL I•Q Batch Method Analyzed By Notes 4,4'-DDD [72-54-8]A 0.044 u ug/L 1 0.044 0.050 1323005 EPA 8081B 10/27/21 14:10 LSK 4,4'-DDE [72-55-9]A 0.048 u ug/L 1 0.048 0.050 1J23005 EPA 8081B 10/27/21 14:10 LSK 4,4'-DDT [50-29-3]A 0.049 u ug/L 1 0.049 0.050 1J23005 EPA 8081B 10/27/21 14:10 LSK Aldrin [309-00-2]A 0.041 u ug/L 1 0.041 0.050 1J23005 EPA 8081B 10/27/21 14:10 LSK alpha-BHC [319-84-6]A 0.036 u ug/L 1 0.036 0.050 1323005 EPA 8081B 10/27/21 14:10 LSK beta-BHC [319-85-7]A 0.041 u ug/L 1 0.041 0.050 1323005 EPA 8081B 10/27/21 14:10 LSK Chlordane (tech) [12789-03-6]A 0.37 u ug/L 1 0.37 0.50 1323005 EPA 8081B 10/27/21 14:10 LSK Chlordane -alpha [5103-71-9]A 0.048 u ug/L 1 0.048 0.050 1J23005 EPA 8081B 10/27/21 14:10 LSK Chlordane -gamma [5103-74-2]A 0.042 u ug/L 1 0.042 0.050 1J23005 EPA 8081B 10/27/21 14:10 LSK delta-BHC [319-86-8]A 0.048 u ug/L 1 0.048 0.050 1J23005 EPA 8081B 10/27/21 14:10 LSK Dieldrin [60-57-1]A 0.045 u ug/L 1 0.045 0.050 1323005 EPA 8081E 10/27/21 14:10 LSK Endosulfan I[959-98-8]A 0.045 u ug/L 1 0.045 0.050 1323005 EPA 8081E 10/27/21 14:10 LSK Endosulfan II[33213-65-9]A 0.038 u ug/L 1 0.038 0.050 1J23005 EPA 8081E 10/27/21 14:10 LSK Endosulfan sulfate [1031-07-8]A 0.032 u ug/L 1 0.032 0.050 1323005 EPA 8081E 10/27/21 14:10 LSK Endrin [72-20-8]A 0.041 u ug/L 1 0.041 0.050 1323005 EPA 8081E 10/27/21 14:10 LSK Endrin aldehyde [7421-93-4]A 0.049 u ug/L 1 0.049 0.050 1J23005 EPA 8081E 10/27/21 14:10 LSK gamma-BHC [58-89-9]A 0.034 u ug/L 1 0.034 0.050 1J23005 EPA 8081B 10/27/21 14:10 LSK Heptachlor[76-44-8]A 0.047 u ug/L 1 0.047 0.050 1J23005 EPA 8081B 10/27/21 14:10 LSK Heptachlor epoxide [1024-57-3]A 0.037 u ug/L 1 0.037 0.050 1323005 EPA 8081B 10/27/21 14:10 LSK Methoxychlor[72-43-5]A 0.048 u ug/L 1 0.048 0.050 1J23005 EPA 8081B 10/27/21 14:10 LSK Toxaphene [8001-35-2]A 0.28 u ug/L 1 0.28 1.0 1J23005 EPA 8081E 10/27/21 14:10 LSK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 45 of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE15554-08 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:45 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Organochlorine Pesticides by GC ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Snike Lv/ % Rec % Rec Limits Batch Method Ana/vzed Notes 2,4,5,6-TCMX 1.1 1 1.00 109 % 10-139 IJ23005 EPA 6081E 10127121 14:10 LSK Decachlorobiphenyl 0.56 1 1.00 56 % 10-122 IJ23005 EPA 6081E 10127121 14:10 LSK Polychlorinated Biphenyls by GC ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes PCB-1016/1242 [12674-11-2/53469-21-9]^ 0.48 U ug/L 1 0.48 0.50 1323006 EPA 8082A 10/27/21 14:10 LSK PCB-1221 [11104-28-2]^ 0.43 U ug/L 1 0.43 0.50 1323006 EPA 8082A 10/27/21 14:10 LSK PCB-1232 [11141-16-5]^ 0.50 U ug/L 1 0.50 0.50 1323006 EPA 8082A 10/27/21 14:10 LSK PCB-1248[12672-29-6]^ 0.45 U ug/L 1 0.45 0.50 1323006 EPA 8082A 10/27/21 14:10 LSK PCB-1254[11097-69-1]^ 0.43 U ug/L 1 0.43 0.50 1323006 EPA 8082A 10/27/21 14:10 LSK PCB-1260 [11096-82-5]^ 0.47 U ug/L 1 0.47 0.50 1323006 EPA 8082A 10/27/21 14:10 LSK Surrogates Results DF Snike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 2,4,5,E-TCMX 0.64 1 1.00 64 % 10-128 IJ23006 EPA 60624 10127121 14:10 LSK Decachlorobiphenyl 0.52 1 1.00 52 % 10-129 IJ23006 EPA 60624 10127121 14:10 LSK Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:18 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1J29005 EPA 6020B 11/03/21 00:06 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J21030 EPA 6010D 10/25/21 11:17 JDH Barium [7440-39-3]^ 19.8 ug/L 1 1.10 10.0 1121030 EPA 6010D 10/25/21 11:17 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1J21030 EPA 6010D 10/25/21 11:17 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 11:17 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:17 JDH Cobalt [7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:17 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1J21030 EPA 6010D 10/25/21 11:17 JDH Iron [7439-89-6]^ 305 ug/L 1 22.0 50.0 1121030 EPA 6010D 10/25/21 11:17 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 11:17 JDH Manganese [7439-96-5]^ 2.52 J ug/L 1 1.50 10.0 1121030 EPA 6010D 10/25/21 11:17 JDH Nickel [7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1J21030 EPA 6010D 10/25/21 11:17 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1J29005 EPA 6020B 11/03/21 00:06 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 11:17 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1J29005 EPA 6020B 11/03/21 00:06 RLF Tin [7440-31-5]^ 2.90 U ug/L 1 2.90 10.0 1J21030 EPA 6010D 10/25/21 11:17 JDH Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:17 JDH Zinc [7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1J21030 EPA 6010D 10/25/21 11:17 JDH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 46 of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CE15554-08 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 11:45 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 13 mg/L 1 2.2 5.0 1321002 EPA 300.0 10/21/21 20:49 ZGW Cyanide (total) [57-12-5]^ 0.0049 U mg/L 1 0.0049 0.010 1J25024 EPA 9014 10/26/21 13:09 JAH Sulfate as SO4 [14808-79-8]^ 9.5 mg/L 1 2.9 5.0 1321002 EPA 300.0 10/21/21 20:49 ZGW Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1J22004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 45 mg/L 1 14 15 1327021 EPA 310.2 10/27/21 16:20 JAH Total Dissolved Solids^ 80 mg/L 1 50 50 1325026 SM 2540C-2011 10/25/21 18:14 DMJ Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 2.9 ug/L 1 0.80 2.0 1125015 EPA 8260D 10/25/21 13:47 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.6 1 5.00 112 % 75-125 V25015 EPA 6260D 10125121 13:47 KKW Chlorinated Herbicides by GC ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 2,4,5-T [93-76-5]^ 0.28 U ug/L 1 0.28 0.50 1J29001 EPA 8151A 11/01/21 14:04 FCV 2,4,5-TP (Silvex) [93-72-1]^ 0.44 U ug/L 1 0.44 0.50 1J29001 EPA 8151A 11/01/21 14:04 FCV 2,4-D [94-75-7]^ 0.27 U ug/L 1 0.27 0.50 1J29001 EPA 8151A 11/01/21 14:04 FCV Dinoseb [88-85-7]^ 0.32 U ug/L 1 0.32 0.50 1J29001 EPA 8151A 11/01/21 14:04 FCV Pentachlorophenol[87-86-5]^ 0.19 U ug/L 1 0.19 0.50 1J29001 EPA 8151A 11/01/21 14:04 FCV Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes 2, 4-DCAA 1.6 1 2,00 80 % 37-134 V29001 EPA 8151A 11101121 14:04 FCV FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 47 Of $2 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-DUPLICATE Lab Sample ID:CE15554-09 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/18/2100:00 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 u ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,2-Dibromoethane [106-93-4]A 0.66 u ug/L 1 0.66 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 u ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,2-Dichloroethane [107-06-2]A 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,2-Dichloropropane [78-87-5]A 0.10 u ug/L 1 0.10 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 u ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1127025 EPA 8260D 10/29/21 09:50 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1127025 EPA 8260D 10/29/21 09:50 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 u ug/L 1 1.1 5.0 1127025 EPA 8260D 10/29/21 09:50 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1127025 EPA 8260D 10/29/21 09:50 RKY Acrylonitrile [107-13-1]A 3.5 u ug/L 1 3.5 10 1127025 EPA 8260D 10/29/21 09:50 RKY Benzene [71-43-2]A 0.93 J ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Bromoform [75-25-2]A 0.22 u ug/L 1 0.22 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1127025 EPA 8260D 10/29/21 09:50 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Chloroform [67-66-3]A 0.18 u ug/L 1 0.18 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY cis-1,2-Dichloroethene [156-59-2]A 2.0 ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Iodomethane [74-88-4]A 1.7 u ug/L 1 1.7 5.0 1127025 EPA 8260D 10/29/21 09:50 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Naphthalene [91-20-3]A 0.11 u ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Tetrahydrofuran [109-99-9]A 0.53 u ug/L 1 0.53 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Toluene [108-88-3]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Trichloroethene [79-01-6]A 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Trichlorofluoromethane [75-69-4]A 0.24 u ug/L 1 0.24 1.0 1127025 EPA 8260D 10/29/21 09:50 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1127025 EPA 8260D 10/29/21 09:50 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 48 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-DUPLICATE Lab Sample ID:CE15554-09 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/18/2100:00 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1J27025 EPA 8260D 10/29/21 09:50 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1J27025 EPA 8260D 10/29/21 09:50 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 60 1 50.0 120 % 53-136 IJ27025 EPA 6260D 10129121 09:50 RKY Dibromofluoromethane 62 1 50.0 123 % 67-129 IJ27025 EPA 6260D 10129121 09:50 RKY Toluene-d8 56 1 50.0 111 % 59-134 IJ27025 EPA 6260D 10129121 09:50 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:20 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 1J29005 EPA 6020B 11/03/21 00:10 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J21030 EPA 6010D 10/25/21 11:20 JDH Barium [7440-39-3]^ 78.6 ug/L 1 1.10 10.0 1121030 EPA 6010D 10/25/21 11:20 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 1J21030 EPA 6010D 10/25/21 11:20 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 11:20 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:20 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:20 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 1J21030 EPA 6010D 10/25/21 11:20 JDH Iron [7439-89-6]^ 93900 ug/L 1 22.0 50.0 1121030 EPA 6010D 10/25/21 11:20 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 11:20 JDH Manganese [7439-96-5]^ 155 ug/L 1 1.50 10.0 1121030 EPA 6010D 10/25/21 11:20 JDH Nickel[7440-02-0]^ 2.20 U ug/L 1 2.20 10.0 1J21030 EPA 6010D 10/25/21 11:20 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 1J29005 EPA 6020B 11/03/21 00:10 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 11:20 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 1J29005 EPA 6020B 11/03/21 00:10 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:20 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 1J21030 EPA 6010D 10/25/21 11:20 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 44 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 21:07 ZGW Sulfate as SO4 [14808-79-B]^ 42 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/21/21 21:07 ZGW Sulfide [18496-25-8]^ 0.037 J mg/L 1 0.010 0.10 1122004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 340 D mg/L 5 70 75 1KO1020 EPA 310.2 11/01/21 12:23 JAH Total Dissolved Solids^ 480 mg/L 1 50 50 1125026 SM 254OC-2011 10/25/21 18:14 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 49 Of 82 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-DUPLICATE Lab Sample ID:CE15554-09 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/18/2100:00 Work Order: CE15554 Project: Moore County Active C & D LF - Fall Sampled By: James Waters Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 13 ug/L 1 0.80 2.0 1325015 EPA 8260D 10/25/21 14:12 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.0 1 5.00 101 % 75-125 V25015 EPA 6260D 10125121 14:12 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 50 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IJ27025 - EPA 5030B MS Blank (1327025-BLK1) Prepared: 10/27/2021 16:42 Analyzed: 10/29/2021 03:52 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,1-Dichloropropene 0.15 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2,4-Trichlorobenzene 0.14 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,3-Dichlorobenzene 0.15 U 1.0 ug/L 1,3-Dichloropropane 0.16 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2,2-Dichloropropane 0.28 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 3-Chloropropene 0.11 U 1.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acetonitrile 5.0 U 10 ug/L Acrolein 4.0 U 10 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L Chloroprene 0.64 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Dichlorodifluoromethane 0.20 U 1.0 ug/L Ethyl Methacrylate 0.38 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Hexachlorobutadiene 0.22 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Isobutyl alcohol 11 U 50 ug/L Methacrylonitrile 4.9 U 10 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 51 of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IJ27025 - EPA 5030B MS - Continued Blank (1327025-BLK1) Continued Prepared: 10/27/2021 16:42 Analyzed: 10/29/2021 03:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Methyl Methacrylate 0.51 U 1.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Propionitrile 5.0 U 10 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 58 u91L 50.0 116 53-136 Dibromofluoromethane 53 u91L 50.0 106 67-129 Toluene-d8 52 u91L 50.0 103 59-134 LCS (1327025-BS1) Prepared: 10/27/2021 16:42 Analyzed: 10/29/2021 02:02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 88 75-133 Benzene 17 1.0 ug/L 20.0 85 80-134 Chlorobenzene 18 1.0 ug/L 20.0 91 80-120 Toluene 21 1.0 ug/L 20.0 106 71-120 Trichloroethene 18 1.0 ug/L 20.0 88 74-120 4-Bromofluorobenzene 60 u91L 50.0 119 53-136 Dibromofluoromethane 48 u91L 50.0 95 67-129 Toluene-d8 53 u91L 50.0 105 59-134 Matrix Spike (1327025-MS1) Prepared: 10/27/2021 16:42 Analyzed: 10/29/2021 02:29 Source: CE16369-09 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 97 75-133 Benzene 18 1.0 ug/L 20.0 0.15 U 92 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 Toluene 24 1.0 ug/L 20.0 0.14 U 120 71-120 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 98 74-120 4-Bromofluorobenzene 56 u91L 50.0 115 53-136 Dibromofluoromethane 50 u91L 50.0 101 67-129 Toluene-d8 50 u91L 50.0 100 59-134 Matrix Spike Dup (1327025-MSD1) Prepared: 10/27/2021 16:42 Analyzed: 10/29/2021 02:57 Source: CE16369-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 52 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IJ27025 - EPA 5030B MS - Continued Matrix Spike Dup (1327025-MSDI) Continued Prepared: 10/27/2021 16:42 Analyzed: 10/29/2021 02:57 Source: CE16369-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 91 75-133 6 20 Benzene 16 1.0 ug/L 20.0 0.15 U 81 80-134 13 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 90 80-120 7 16 Toluene 21 1.0 ug/L 20.0 0.14 U 104 71-120 15 17 Trichloroethene 16 1.0 ug/L 20.0 0.15 U 81 74-120 19 22 4-Bromofluorobenzene 61 u91L 50.0 121 53-136 Dibromofluoromethane 51 u91L 50.0 102 67-129 Toluene-d8 52 u91L 50.0 103 59-134 Batch 1J27031 - EPA 5030E MS Blank (1327031-BLK3) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 20:47 Analvte Result Flaq POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 53 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1127031 - EPA 5030B MS - Continued Blank (1327031-BLK1) Continued Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 20:47 Analvte Result Flaq POL Units Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 50 u91L 50.0 99 53-136 Dlbromofluoromethane 49 u91L 50.0 98 67-129 Toluene-d8 50 u91L 50.0 101 59-134 LCS (1727031-BS1) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 18:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 24 1.0 ug/L 20.0 122 75-133 Benzene 24 1.0 ug/L 20.0 120 80-134 Chlorobenzene 19 1.0 ug/L 20.0 95 80-120 Toluene 20 1.0 ug/L 20.0 99 71-120 Trichloroethene 21 1.0 ug/L 20.0 107 74-120 Matrix Spike (1327031-MS1) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 19:19 Source: CE16369-11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 24 1.0 ug/L 20.0 0.21 U 118 75-133 Benzene 23 1.0 ug/L 20.0 0.15 U 117 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 97 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 99 71-120 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 108 74-120 Matrix Spike Dup (1327031-MSD1) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 19:48 Source: CE16369-11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 25 1.0 ug/L 20.0 0.21 U 123 75-133 4 20 Benzene 24 1.0 ug/L 20.0 0.15 U 118 80-134 0.6 17 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 98 80-120 0.8 16 Toluene 20 1.0 ug/L 20.0 0.14 U 99 71-120 0.4 17 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 110 74-120 2 22 Batch 1KO1035 - EPA 50308 MS FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 54 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1 K01035 - EPA 5030B MS - Continued Blank (1K03035-BLKS) Prepared: 11/01/2021 13:31 Analyzed: 11/01/2021 17:39 Analvte Result Flaq POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,1-Dichloropropene 0.15 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2,4-Trichlorobenzene 0.14 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,3-Dichlorobenzene 0.15 U 1.0 ug/L 1,3-Dichloropropane 0.16 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2,2-Dichloropropane 0.28 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 3-Chloropropene 0.11 U 1.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acetonitrile 5.0 U 10 ug/L Acrolein 4.0 U 10 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L Chloroprene 0.64 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Dichlorodifluoromethane 0.20 U 1.0 ug/L Ethyl Methacrylate 0.38 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Hexachlorobutadiene 0.22 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Isobutyl alcohol 11 U 50 ug/L Methacrylonitrile 4.9 U 10 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 55 Of 82 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK01035 - EPA 5030E MS - Continued Blank (1K01035-BLK1) Continued Prepared: 11/01/2021 13:31 Analyzed: 11/01/2021 17:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Methyl Methacrylate 0.51 U 1.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Propionitrile 5.0 U 10 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 46 u91L 50.0 93 53-136 Dibromofluoromethane 41 u91L 50.0 81 67-129 Toluene-d8 44 u91L 50.0 87 59-134 LCS (1K01035-BS1) Prepared: 11/01/2021 13:31 Analyzed: 11/01/2021 15:50 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 107 75-133 Benzene 20 1.0 ug/L 20.0 102 80-134 Chlorobenzene 19 1.0 ug/L 20.0 95 80-120 Toluene 19 1.0 ug/L 20.0 96 71-120 Trichloroethene 19 1.0 ug/L 20.0 97 74-120 4-Bromofluorobenzene 47 u91L 50.0 94 53-136 Dibromofluoromethane 42 u91L 50.0 84 67-129 Toluene-d8 42 u91L 50.0 85 59-134 Matrix Spike (1K01035-MS1) Prepared: 11/01/2021 13:31 Analyzed: 11/01/2021 16:18 Source: CE16332-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 99 D 5.0 ug/L 100 1.0 U 99 75-133 Benzene 390 D 5.0 ug/L 100 310 81 80-134 Chlorobenzene 120 D 5.0 ug/L 100 37 78 80-120 QM-07 Toluene 110 D 5.0 ug/L 100 23 88 71-120 Trichloroethene 96 D 5.0 ug/L 100 0.75 U 96 74-120 4-Bromofluorobenzene 47 u91L 50.0 94 53-136 Dibromofluoromethane 43 u91L 50.0 86 67-129 Toluene-& 41 u91L 50.0 81 59-134 Matrix Spike Dup (1K01035-MSD1) Prepared: 11/01/2021 13:31 Analyzed: 11/01/2021 16:45 Source: CE16332-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 110 D 5.0 ug/L 100 1.0 U 109 75-133 10 20 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 56 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1 K01035 - EPA 5030B MS - Continued Matrix Spike Dup (1K03035-MSD1) Continued Prepared: 11/01/2021 13:31 Analyzed: 11/01/2021 16:45 Source: CE16332-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Benzene 420 D 5.0 ug/L 100 310 106 80-134 6 17 Chlorobenzene 130 D 5.0 ug/L 100 37 90 80-120 10 16 Toluene 120 D 5.0 ug/L 100 23 100 71-120 10 17 Trichloroethene 100 D 5.0 ug/L 100 0.75 U 103 74-120 7 22 4-Bromofluorobenzene 48 u91L 50.0 96 53-136 Dibromofluoromethane 39 u91L 50.0 79 67-129 Toluene-d8 42 u91L 50.0 83 59-134 Semivolatile Organic Compounds by GCMS - Quality Control Batch IJ25011 - EPA 3510C MS Blank (1125011-BLK3) Prepared: 10/25/2021 10:05 Analyzed: 10/27/2021 14:19 Analvte Result Flaq POL Units 1,2,4,5-Tetrachlorobenzene 3.4 U 10 ug/L 1,3,5-Trinitrobenzene 3.0 U 10 ug/L 1,3-Dinitrobenzene 2.5 U 10 ug/L 1,4-Naphthoquinone 2.5 U 10 ug/L 1,4-Phenylenediamine 4.0 U 10 ug/L 1-Naphthylamine 2.2 U 10 ug/L 2,3,4,6-TetrachIorophen o1 2.4 U 10 ug/L 2,4,5-Trichlorophenol 2.5 U 10 ug/L 2,4,6-Trichlorophenol 2.6 U 10 ug/L 2,4-Dichlorophenol 2.6 U 10 ug/L 2,4-Di methyl phenol 2.3 U 10 ug/L 2,4-Dinitrophenol 2.6 U 10 ug/L 2,4-Dinitrotoluene 2.6 U 10 ug/L 2,6-Dichlorophenol 2.0 U 10 ug/L 2,6-Dinitrotoluene 2.5 U 10 ug/L 2-Acetylaminofluorene 3.1 U 10 ug/L 2-Chloronaphthalene 2.8 U 10 ug/L 2-Chlorophenol 2.2 U 10 ug/L 2-Methyl-4,6-dinitrophenol 3.3 U 10 ug/L 2- Methyl naphthalene 2.8 U 10 ug/L 2-Methylphenol 2.0 U 10 ug/L 2-Naphthylamine 3.0 U 10 ug/L 2-Nitroaniline 2.5 U 10 ug/L 2-Nitrophenol 1.1 U 10 ug/L 3 & 4-Methylphenol 2.1 U 10 ug/L 3,3'-Dichlorobenzidine 3.5 U 10 ug/L 3,3'-Dimethylbenzidine 2.2 U 10 ug/L 3-Methylcholanthrene 1.3 U 10 ug/L 3-Nitroaniline 2.6 U 10 ug/L 4-Aminobiphenyl 3.5 U 10 ug/L 4-Bromophenyl-phenylether 2.4 U 10 ug/L 4-Chloro-3-methylphenol 2.4 U 10 ug/L 4-Chloroaniline 2.0 U 10 ug/L 4-Chlorophenyl-phenylether 2.6 U 10 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 57 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 1125011 - EPA 3510C MS - Continued Blank (1325011-BLK1) Continued Prepared: 10/25/2021 10:05 Analyzed: 10/27/2021 14:19 Analvte Result Flaq POL Units 4-Nitroaniline 3.2 U 10 ug/L 4-Nitrophenol 2.8 U 10 ug/L 5-Nitro-o-toluidine 3.2 U 10 ug/L 7,12-Di methyl benz(a)anth racene 1.4 U 10 ug/L a,a-Dimethylphenethylamine 3.5 U 10 ug/L Acenaphthene 2.7 U 10 ug/L Acenaphthylene 2.6 U 10 ug/L Acetophenone 2.0 U 10 ug/L Anthracene 2.4 U 10 ug/L Benzo(a)anthracene 2.4 U 10 ug/L Benzo(a)pyrene 2.2 U 10 ug/L Benzo(b)fluoranthene 2.8 U 10 ug/L Benzo(g,h,i)perylene 2.4 U 10 ug/L Benzo(k)fluoranthene 2.4 U 10 ug/L Benzyl alcohol 2.4 U 10 ug/L Bis(2-chloroethoxy)methane 2.4 U 10 ug/L Bis(2-chloroethyl)ether 2.6 U 10 ug/L Bis(2-chloroisopropyl)ether 2.5 U 10 ug/L Bis(2-ethylhexyl)phthalate 1.9 U 5.0 ug/L Butyl benzylphtha late 3.8 U 10 ug/L Chlorobenzilate 2.4 U 10 ug/L Chrysene 2.2 U 10 ug/L Diallate 1.9 U 10 ug/L Dibenzo(a,h)anthracene 2.3 U 10 ug/L Dibenzofuran 2.6 U 10 ug/L Diethylphtha late 2.4 U 10 ug/L Dimethoate 2.3 U 10 ug/L Dimethylphthalate 2.5 U 10 ug/L Di-n-butylphthalate 2.8 U 10 ug/L Di-n-octylphthalate 3.1 U 10 ug/L Disulfoton 2.0 U 10 ug/L Ethyl methanesulfonate 2.2 U 10 ug/L Famphur 2.7 U 10 ug/L Fluoranthene 3.1 U 10 ug/L Fluorene 2.5 U 10 ug/L Hexachlorobenzene 2.3 U 10 ug/L Hexachlorobutadiene 2.8 U 10 ug/L Hexachlorocyclopentadiene 2.7 U 10 ug/L Hexachloroethane 2.6 U 10 ug/L Hexachloropropene 6.8 U 10 ug/L Indeno(1,2,3-cd)pyrene 2.2 U 10 ug/L Isodrin 1.5 U 10 ug/L Isophorone 2.5 U 10 ug/L Isosafrole 2.2 U 10 ug/L Kepone 7.2 U 20 ug/L Methapyrilene 4.8 U 10 ug/L Methyl Methanesulfonate 2.2 U 10 ug/L Methyl parathion 2.5 U 10 ug/L Nitrobenzene 2.5 U 10 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes J-04 QV-01 J-05 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 58 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 1125011 - EPA 3510C MS - Continued Blank (1325011-BLK1) Continued Prepared: 10/25/2021 10:05 Analyzed: 10/27/2021 14:19 Analvte Result Flaq POL Units N-Nitrosodiethylamine 2.1 U 10 ug/L N-Nitrosodimethylamine 1.9 U 10 ug/L N-Nitrosodi-n-butylamine 2.0 U 10 ug/L N-Nitroso-di-n-propylamine 2.3 U 10 ug/L N-nitrosodiphenylamine/Diphenylamine 2.5 U 10 ug/L N-Nitrosomethylethylamine 1.9 U 10 ug/L N-Nitrosopiperidine 2.1 U 10 ug/L N-Nitrosopyrrolidine 1.9 U 10 ug/L 0,0,0-Triethylphosphorothioate 2.2 U 10 ug/L o-Toluidine 1.6 U 10 ug/L Parathion 1.7 U 10 ug/L p-Dimethylaminoazobenzene 2.6 U 10 ug/L Pentachlorobenzene 2.7 U 10 ug/L Pentachloronitrobenzene 1.9 U 10 ug/L Phenacetin 2.7 U 10 ug/L Phenanthrene 2.6 U 10 ug/L Phenol 1.7 U 10 ug/L Phorate 2.1 U 10 ug/L Pronamide 1.7 U 10 ug/L Pyrene 3.5 U 10 ug/L Safrole 2.2 U 10 ug/L Thionazin 2.3 U 10 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 2,4,6-Tribromophenol 79 u91L 100 79 10-179 2-Fluorobiphenyl 42 u91L 50.0 85 10-149 2-Fluorophenol 52 u91L 100 52 10-110 Nitrobenzene-d5 43 u91L 50.0 86 10-149 Phenol-d5 45 u91L 100 45 10-88 TerphenyhdM 53 u91L 50.0 106 10-188 LCS (1325011-BS1) Prepared: 10/25/2021 10:05 Analyzed: 10/27/2021 14:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Chorophenol 2.2 U 10 ug/L 50.0 40-109 3-06 4-Chloro-3-methylphenol 11 10 ug/L 50.0 23 58-121 3-06 4-Nitrophenol 2.8 U 10 ug/L 50.0 33-105 J-06 Acenaphthene 42 10 ug/L 50.0 84 39-125 N-Nitroso-di-n-propylamine 39 10 ug/L 50.0 79 48-126 Phenol 2.4 J 10 ug/L 50.0 5 19-78 J-06 Pyrene 50 10 ug/L 50.0 100 44-137 2,4,6-Tribromophenol 0.54 u91L 100 0.5 10-179 Q5-03 2-Fluorobiphenyl 43 u91L 50.0 86 10-149 2-Fluorophenol 0.61 u91L 100 0.6 10-110 Q5-03 Nitrobenzene-d5 45 u91L 50.0 90 10-149 Phenol-d5 5.0 u91L 100 5 10-88 QS-03 Terphenyl-dM 43 u91L 50.0 87 10-188 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 59 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch IJ25011 - EPA 3510C MS - Continued Matrix Spike (1325011-MS3) Prepared: 10/25/2021 10:05 Analyzed: 10/27/2021 22:02 Source: CE15045-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Chlorophenol 39 JD 50 ug/L 50.0 11 U 77 40-109 J-06, R-05 4-Chloro-3-methylphenol 200 D 50 ug/L 50.0 12 U 396 58-121 J-06, R-05 4-Nitrophenol 23 JD 50 ug/L 50.0 14 U 45 33-105 J-06, R-05 Acenaphthene 44 JD 50 ug/L 50.0 14 U 88 39-125 R-05 N-Nitroso-di-n-propylamine 38 JD 50 ug/L 50.0 12 U 76 48-126 R-05 Phenol 32 JD 50 ug/L 50.0 8.5 U 63 19-78 J-06, R-05 Pyrene 33 JD 50 ug/L 50.0 18 U 67 44-137 R-05 2,4,6-Tribromophenol 76 ug/L 100 76 10-179 R-05 2-Fluoroblphenyl 38 ug/L 50.0 76 10-149 R-05 2-Fluorophenol 58 u91L 100 58 10-110 R-05 Nitrobenzene-d5 41 u91L 50.0 82 10-149 R-05 Phenol-d5 60 u91L 100 60 10-88 R-05 Terphenyhd14 27 u91L 50.0 53 10-188 R-05 Batch IK01006 - EPA 3510C MS Blank (1K03006-BLKS) Prepared: 11/01/2021 08:29 Analyzed: 11/01/2021 16:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,2,4,5-Tetrachlorobenzene 3.4 U 10 ug/L 1,3,5-Trinitrobenzene 3.0 U 10 ug/L 1,3-Dinitrobenzene 2.5 U 10 ug/L 1,4-Naphthoquinone 2.5 U 10 ug/L 1,4-Phenylenediamine 4.0 U 10 ug/L 1-Naphthylamine 2.2 U 10 ug/L 2,3,4,6-Tetrachlorophenol 2.4 U 10 ug/L 2,4,5-Trichlorophenol 2.5 U 10 ug/L 2,4,6-Trichlorophenol 2.6 U 10 ug/L 2,4-Dichlorophenol 2.6 U 10 ug/L 2,4-Di methyl phenol 2.3 U 10 ug/L 2,4-Dinitrophenol 2.6 U 10 ug/L 2,4-Dinitrotoluene 2.6 U 10 ug/L 2,6-Dichlorophenol 2.0 U 10 ug/L 2,6-Dinitrotoluene 2.5 U 10 ug/L 2-Acetylaminofluorene 3.1 U 10 ug/L 2-Chloronaphthalene 2.8 U 10 ug/L 2-Chlorophenol 2.2 U 10 ug/L 2-Methyl-4,6-dinitrophenol 3.3 U 10 ug/L 2- Methyl naphthalene 2.8 U 10 ug/L 2-Methylphenol 2.0 U 10 ug/L 2-Naphthylamine 3.0 U 10 ug/L 2-Nitroaniline 2.5 U 10 ug/L 2-Nitrophenol 1.1 U 10 ug/L 3 & 4-Methylphenol 2.1 U 10 ug/L 3,3'-Dichlorobenzidine 3.5 U 10 ug/L 3,3'-Dimethylbenzidine 2.2 U 10 ug/L 3-Methylcholanthrene 1.3 U 10 ug/L 3-Nitroaniline 2.6 U 10 ug/L 4-Aminobiphenyl 3.5 U 10 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 60 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 1 K01006 - EPA 3510C MS - Continued Blank (SK03006-BLKS) Continued Prepared: 11/01/2021 08:29 Analyzed: 11/01/2021 16:08 Analvte Result Flaq POL Units 4-Bromophenyl-phenylether 2.4 U 10 ug/L 4-Chloro-3-methylphenol 2.4 U 10 ug/L 4-Chloroaniline 2.0 U 10 ug/L 4-Chlorophenyl-phenylether 2.6 U 10 ug/L 4-Nitroaniline 3.2 U 10 ug/L 4-Nitrophenol 2.8 U 10 ug/L 5-Nitro-o-toluidine 3.2 U 10 ug/L 7,12-Di methyl benz(a)anth racene 1.4 U 10 ug/L a,a-Dimethylphenethylamine 3.5 U 10 ug/L Acenaphthene 2.7 U 10 ug/L Acenaphthylene 2.6 U 10 ug/L Acetophenone 2.0 U 10 ug/L Anthracene 2.4 U 10 ug/L Benzo(a)anthracene 2.4 U 10 ug/L Benzo(a)pyrene 2.2 U 10 ug/L Benzo(b)fluoranthene 2.8 U 10 ug/L Benzo(g,h,i)perylene 2.4 U 10 ug/L Benzo(k)fluoranthene 2.4 U 10 ug/L Benzyl alcohol 2.4 U 10 ug/L Bis(2-chloroethoxy)methane 2.4 U 10 ug/L Bis(2-chloroethyl)ether 2.6 U 10 ug/L Bis(2-chloroisopropyl)ether 2.5 U 10 ug/L Bis(2-ethylhexyl)phthalate 1.9 U 5.0 ug/L Butyl benzylphtha late 3.8 U 10 ug/L Chlorobenzilate 2.4 U 10 ug/L Chrysene 2.2 U 10 ug/L Diallate 1.9 U 10 ug/L Dibenzo(a,h)anthracene 2.3 U 10 ug/L Dibenzofuran 2.6 U 10 ug/L Diethylphtha late 2.4 U 10 ug/L Dimethoate 2.3 U 10 ug/L Dimethylphthalate 2.5 U 10 ug/L Di-n-butylphthalate 2.8 U 10 ug/L Di-n-octylphthalate 3.1 U 10 ug/L Disulfoton 2.0 U 10 ug/L Ethyl methanesulfonate 2.2 U 10 ug/L Famphur 2.7 U 10 ug/L Fluoranthene 3.1 U 10 ug/L Fluorene 2.5 U 10 ug/L Hexachlorobenzene 2.3 U 10 ug/L Hexachlorobutadiene 2.8 U 10 ug/L Hexachlorocyclopentadiene 2.7 U 10 ug/L Hexachloroethane 2.6 U 10 ug/L Hexachloropropene 6.8 U 10 ug/L Indeno(1,2,3-cd)pyrene 2.2 U 10 ug/L Isodrin 1.5 U 10 ug/L Isophorone 2.5 U 10 ug/L Isosafrole 2.2 U 10 ug/L Kepone 7.2 U 20 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes J-05 Page 61 of 82 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 1 K01006 - EPA 3510C MS - Continued Blank (SK03006-BLKS) Continued Prepared: 11/01/2021 08:29 Analyzed: 11/01/2021 16:08 Analvte Result Flaq POL Units Methapyrilene 4.8 U 10 ug/L Methyl Methanesulfonate 2.2 U 10 ug/L Methyl parathion 2.5 U 10 ug/L Nitrobenzene 2.5 U 10 ug/L N-Nitrosodiethylamine 2.1 U 10 ug/L N-Nitrosodimethylamine 1.9 U 10 ug/L N-Nitrosodi-n-butylamine 2.0 U 10 ug/L N-Nitroso-di-n-propylamine 2.3 U 10 ug/L N-nitrosodiphenylamine/Diphenylamine 2.5 U 10 ug/L N-Nitrosomethylethylamine 1.9 U 10 ug/L N-Nitrosopiperidine 2.1 U 10 ug/L N-Nitrosopyrrolidine 1.9 U 10 ug/L 0,0,0-Triethyl phosphorothioate 2.2 U 10 ug/L o-Toluidine 1.6 U 10 ug/L Parathion 1.7 U 10 ug/L p-Dimethylaminoazobenzene 2.6 U 10 ug/L Pentachlorobenzene 2.7 U 10 ug/L Pentachloronitrobenzene 1.9 U 10 ug/L Phenacetin 2.7 U 10 ug/L Phenanthrene 2.6 U 10 ug/L Phenol 1.7 U 10 ug/L Phorate 2.1 U 10 ug/L Pronamide 1.7 U 10 ug/L Pyrene 3.5 U 10 ug/L Safrole 2.2 U 10 ug/L Thionazin 2.3 U 10 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 2,4,6-Tribromopheno/ 79 ug/L 100 79 10-179 2-Fluorobiphenyl 46 ug/L 50.0 92 10-149 2-Fluorophenol 69 ug/L 100 69 10-110 Nitrobenzene-d5 39 ug/L 50.0 79 10-149 Phenol-d5 63 ug/L 100 63 10-88 Terphenyl-dM 50 ug/L 50.0 101 10-166 LCS (1K01006-BS1) Prepared: 11/01/2021 08:29 Analyzed: 11/01/2021 16:38 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Chlorophenol 41 10 ug/L 50.0 82 40-109 4-Chloro-3-methylphenol 45 10 ug/L 50.0 90 58-121 4-Nitrophenol 45 10 ug/L 50.0 89 33-105 Acenaphthene 47 10 ug/L 50.0 95 39-125 N-Nitroso-di-n-propylamine 40 10 ug/L 50.0 80 48-126 Phenol 32 10 ug/L 50.0 65 19-78 Pyrene 45 10 ug/L 50.0 91 44-137 2,4,6-Tribromopheno/ 91 ug/L 100 91 10-179 2-Fluorobiphenyl 46 ug/L 50.0 92 10-149 2-Fluorophenol 72 ug/L 100 72 10-110 Nitrobenzene-d5 41 ug/L 50.0 81 10-149 Phenohd5 68 ug/L 100 68 10-68 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 62 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 1 K01006 - EPA 3510C MS - Continued LCS (1K01006-BS3) Continued Prepared: 11/01/2021 08:29 Analyzed: 11/01/2021 16:38 Analvte Terphenyl-d14 Result Flaq 43 POL Units u91L Spike Level 50.0 Source Result %REC 65 %REC Limits RPD 10-188 RPD Limit Notes Matrix Spike (1K01006-MS3) Prepared: 11/01/2021 08:29 Analyzed: 11/01/2021 17:09 Source: CE35678-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Chlorophenol 38 10 ug/L 50.0 2.2 U 75 40-109 4-Chloro-3-methylphenol 38 10 ug/L 50.0 2.4 U 76 58-121 4-Nitrophenol 37 10 ug/L 50.0 2.8 U 74 33-105 Acenaphthene 45 10 ug/L 50.0 2.7 U 89 39-125 N-Nitroso-di-n-propylamine 36 10 ug/L 50.0 2.3 U 72 48-126 Phenol 29 10 ug/L 50.0 1.7 U 58 19-78 Pyrene 42 10 ug/L 50.0 3.5 U 85 44-137 2,4,6-Tribromopheno/ 84 u91L 100 84 10-179 2-Fluorobiphenyl 46 u91L 50.0 93 10-149 2-Fluorophenol 68 u91L 100 68 10-110 Nitrobenzene-d5 38 u91L 50.0 76 10-149 Phenohd5 61 u91L 100 61 10-88 Terphenyl-d14 41 u91L 50.0 82 10-166 Matrix Spike Dup (1K03006-MSD3) Prepared: 11/01/2021 08:29 Analyzed: 11/01/2021 17:40 Source: CE35678-06 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 2-Chlorophenol 36 10 ug/L 50.0 2.2 U 72 40-109 5 22 4-Chloro-3-methylphenol 37 10 ug/L 50.0 2.4 U 74 58-121 3 22 4-Nitrophenol 37 10 ug/L 50.0 2.8 U 74 33-105 0.2 27 Acenaphthene 42 10 ug/L 50.0 2.7 U 84 39-125 6 25 N-Nitroso-di-n-propylamine 34 10 ug/L 50.0 2.3 U 69 48-126 5 23 Phenol 27 10 ug/L 50.0 1.7 U 54 19-78 6 18 Pyrene 39 10 ug/L 50.0 3.5 U 77 44-137 9 24 2,4,6-Tribromopheno/ 79 u91L 100 79 10-179 2-Fluorobiphenyl 43 u91L 50.0 86 10-149 2-Fluorophenol 64 u91L 100 64 10-110 Nitrobenzene-d5 36 u91L 50.0 72 10-149 Phenohd5 58 u91L 100 58 10-68 Terphenyl-d14 35 u91L 50.0 71 10-186 Organochlorine Pesticides by GC - Quality Control Batch V23005 - EPA 3510C Blank (1323005-BLK3) Prepared: 10/23/2021 15:01 Analyzed: 10/27/2021 12:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4,4'-DDD 0.044 U 0.050 ug/L 4,4'-DDE 0.048 U 0.050 ug/L 4,4'-DDT 0.049 U 0.050 ug/L Aldrin 0.041 U 0.050 ug/L alpha-BHC 0.036 U 0.050 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 63 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Organochlorine Pesticides by GC - Quality Control Batch 1123005 - EPA 3510C - Continued Blank (1323005-BLK1) Continued Prepared: 10/23/2021 15:01 Analyzed: 10/27/2021 12:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes beta-BHC 0.041 U 0.050 ug/L Chlordane (tech) 0.37 U 0.50 ug/L Chlordane -alpha 0.048 U 0.050 ug/L Chlordane -gamma 0.042 U 0.050 ug/L delta-BHC 0.048 U 0.050 ug/L Dieldrin 0.045 U 0.050 ug/L Endosulfan I 0.045 U 0.050 ug/L Endosulfan II 0.038 U 0.050 ug/L Endosulfan sulfate 0.032 U 0.050 ug/L Endrin 0.041 U 0.050 ug/L Endrin aldehyde 0.049 U 0.050 ug/L gamma-BHC 0.034 U 0.050 ug/L Heptachlor 0.047 U 0.050 ug/L Heptachlor epoxide 0.037 U 0.050 ug/L Methoxychlor 0.048 U 0.050 ug/L Toxaphene 0.28 U 1.0 ug/L 2,4,5,E-TCMX 0.78 u91L 1.00 78 10-139 Decachlorobiphenyl 0.51 u91L 1.00 51 10-122 LCS (1323005-BSI) Prepared: 10/23/2021 15:01 Analyzed: 10/27/2021 12:25 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4,4'-DDT 1.1 0.050 ug/L 1.00 113 37-139 Dieldrin 1.0 0.050 ug/L 1.00 101 46-132 Endrin 1.0 0.050 ug/L 1.00 100 43-133 2,4,5,6-TCMX 0.88 ug/L 1.00 88 10-139 Decachlorobiphenyl 0.57 u91L 1.00 57 10-122 Matrix Spike (1723005-MS3) Prepared: 10/23/2021 15:01 Analyzed: 10/27/2021 12:38 Source: CE15554-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4,4'-DDT 1.2 0.050 ug/L 1.00 0.049 U 123 37-139 Dieldrin 0.94 0.050 ug/L 1.00 0.045 U 94 46-132 Endrin 0.98 0.050 ug/L 1.00 0.041 U 98 43-133 2,4,5,E-TCMX 0.84 u91L 1.00 84 10-139 Decachlorobiphenyl 0.39 ug/L 1.00 39 10-122 Matrix Spike Dup (1123005-MSD1) Prepared: 10/23/2021 15:01 Analyzed: 10/27/2021 12:52 Source: CE15554-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4,4'-DDT 1.1 0.050 ug/L 1.00 0.049 U 110 37-139 11 26 Dieldrin 1.1 0.050 ug/L 1.00 0.045 U 106 46-132 12 27 Endrin 1.1 0.050 ug/L 1.00 0.041 U 108 43-133 10 26 2,4,5,6-TCMX 0.92 ug/L 1.00 92 10-139 Decachlorobiphenyl 0.44 u91L 1.00 44 10-122 Polychlorinated Biphenyls by GC - Quality Control FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 64 Of S2 (� �Eo www.encolabs.com QUALITY CONTROL DATA Polychlorinated Biphenyls by GC - Quality Control Batch V23006 - EPA 3510C Blank (1323006-BLK3) Prepared: 10/23/2021 15:09 Analyzed: 10/27/2021 13:05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes PCB-1016/1242 0.48 U 0.50 ug/L PCB-1221 0.43 U 0.50 ug/L PCB-1232 0.50 U 0.50 ug/L PCB-1248 0.45 U 0.50 ug/L PCB-1254 0.43 U 0.50 ug/L PCB-1260 0.47 U 0.50 ug/L 2,4,5,E-TCMX 0.47 U91L 1.00 47 10-128 Decachlorobiphenyl 0.41 u91L 1.00 41 10-129 LCS (1323006-BSI) Prepared: 10/23/2021 15:09 Analyzed: 10/27/2021 13:18 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes PCB-1016/1242 6.2 0.50 ug/L 10.0 62 43-123 PCB-1260 5.1 0.50 ug/L 10.0 51 41-125 2,4,5,E-TCMX 0.56 u91L 1.00 56 10-128 Decachlorobiphenyl 0.34 u91L 1.00 34 10-129 Matrix Spike (1323006-MS1) Prepared: 10/23/2021 15:09 Analyzed: 10/27/2021 13:31 Source: CE15554-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes PCB-1016/1242 5.8 0.50 ug/L 10.0 0.48 U 58 43-123 PCB-1260 5.5 0.50 ug/L 10.0 0.47 U 55 41-125 2,4,5,6-TCMX 0.46 u91L 1.00 46 10-128 Decachlorobiphenyl 0.54 u91L 1.00 54 10-129 Matrix Spike Dup (1323006-MSD1) Prepared: 10/23/2021 15:09 Analyzed: 10/27/2021 13:44 Source: CE15554-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes PCB-1016/1242 6.1 0.50 ug/L 10.0 0.48 U 61 43-123 6 23 PCB-1260 5.6 0.50 ug/L 10.0 0.47 U 56 41-125 2 31 2,4,5,E-TCMX 0.45 u91L 1.00 45 10-128 Decachlorobiphenyl 0.48 u91L 1.00 46 10-129 Metals by EPA 6000/7000 Series Methods - Quality Control Batch IJ20028 - EPA 245.1 Blank (1320028-BLK3) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:33 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L Blank (1320028-BLK2) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:35 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 3.00 U 4.00 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 65 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch 112002E - EPA 245.1 - Continued LCS (1320028-BSI) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.46 0.200 ug/L 5.00 109 80-120 Matrix Spike (1320028-MS1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:44 Source: CE35555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.96 0.200 ug/L 5.00 0.150 U 99 75-125 Matrix Spike Dup (1J20028-MSD1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:46 Source: CE35555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.99 0.200 ug/L 5.00 0.150 U 100 75-125 0.8 25 Post Spike (IJ20028-PS1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:48 Source: CE35555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.02 0.200 ug/L 4.76 -0.000286 105 75-125 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1120014 - EPA 3005A Blank (1320014-BLK1) Prepared: 10/20/2021 11:28 Analyzed: 10/27/2021 14:17 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Iron 22.0 U 50.0 ug/L LCS (1320014-BS3) Prepared: 10/20/2021 11:28 Analyzed: 10/27/2021 14:22 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Iron 1010 50.0 ug/L 1000 101 80-120 Matrix Spike (1J20014-MS1) Prepared: 10/20/2021 11:28 Analyzed: 10/27/2021 14:24 Source: CE16094-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Iron 2150 50.0 ug/L 1000 1150 99 75-125 Matrix Spike Dup (1320014-MSDI) Prepared: 10/20/2021 11:28 Analyzed: 10/27/2021 14:27 Source: CE16094-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Iron 2190 50.0 ug/L 1000 1150 103 75-125 2 20 Post Spike (1J20014-PS1) Prepared: 10/20/2021 11:28 Analyzed: 10/27/2021 14:30 Source: CE16094-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Iron 2.13 0.0500 mg/L 1.00 1.15 97 80-120 Batch 1.721030 - EPA 3005A FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 66 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1121030 - EPA 3005A - Continued Blank (1321030-BLK1) Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:17 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Beryllium 0.160 U 1.00 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Cobalt 1.40 U 10.0 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Manganese 1.50 U 10.0 ug/L Nickel 2.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L Tin 2.90 U 10.0 ug/L Vanadium 1.40 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (1321030-BS1) Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:23 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 195 10.0 ug/L 200 98 80-120 Barium 203 10.0 ug/L 200 101 80-120 Beryllium 19.4 1.00 ug/L 20.0 97 80-120 Cadmium 19.4 1.00 ug/L 20.0 97 80-120 Chromium 193 10.0 ug/L 200 96 80-120 Cobalt 199 10.0 ug/L 200 99 80-120 Copper 192 10.0 ug/L 200 96 80-120 Iron 990 50.0 ug/L 1000 99 80-120 Lead 197 10.0 ug/L 200 98 80-120 Manganese 193 10.0 ug/L 200 96 80-120 Nickel 205 10.0 ug/L 200 102 80-120 Silver 196 10.0 ug/L 200 98 80-120 Tin 197 10.0 ug/L 200 98 80-120 Vanadium 193 10.0 ug/L 200 97 80-120 Zinc 203 10.0 ug/L 200 101 80-120 Matrix Spike (1323030-MS1) Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:26 Source: CE15554-02 Spike Source %REC Analvte Result Flaq POL Units Level Result %REC Limits RPD Arsenic 182 10.0 ug/L 200 7.60 U 91 75-125 Barium 264 10.0 ug/L 200 67.1 99 75-125 Beryllium 18.5 1.00 ug/L 20.0 0.160 U 92 75-125 Cadmium 17.7 1.00 ug/L 20.0 0.360 U 88 75-125 Chromium 189 10.0 ug/L 200 1.40 U 94 75-125 Cobalt 193 10.0 ug/L 200 1.40 U 96 75-125 Copper 181 10.0 ug/L 200 1.60 U 90 75-125 Iron 102000 50.0 ug/L 1000 100000 183 75-125 Lead 192 10.0 ug/L 200 3.10 U 96 75-125 Manganese 454 10.0 ug/L 200 259 97 75-125 RPD Limit Notes QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 67 of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1121030 - EPA 3005A - Continued Matrix Spike (1323030-MS3) Continued Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:26 Source: CE15554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nickel 196 10.0 ug/L 200 2.20 U 98 75-125 Silver 196 10.0 ug/L 200 1.90 U 98 75-125 Tin 188 10.0 ug/L 200 2.90 U 94 75-125 Vanadium 190 10.0 ug/L 200 1.40 U 95 75-125 Zinc 199 10.0 ug/L 200 4.40 U 99 75-125 Matrix Spike Dup (1]23030-MSD1) Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:29 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 188 10.0 ug/L 200 7.60 U 94 75-125 4 20 Barium 272 10.0 ug/L 200 67.1 103 75-125 3 20 Beryllium 19.0 1.00 ug/L 20.0 0.160 U 95 75-125 3 20 Cadmium 18.1 1.00 ug/L 20.0 0.360 U 90 75-125 2 20 Chromium 194 10.0 ug/L 200 1.40 U 97 75-125 3 20 Cobalt 199 10.0 ug/L 200 1.40 U 99 75-125 3 20 Copper 186 10.0 ug/L 200 1.60 U 93 75-125 3 20 Iron 105000 50.0 ug/L 1000 100000 471 75-125 3 20 QM-07 Lead 198 10.0 ug/L 200 3.10 U 99 75-125 3 20 Manganese 467 10.0 ug/L 200 259 104 75-125 3 20 Nickel 203 10.0 ug/L 200 2.20 U 101 75-125 3 20 Silver 203 10.0 ug/L 200 1.90 U 102 75-125 3 20 Tin 195 10.0 ug/L 200 2.90 U 97 75-125 3 20 Vanadium 195 10.0 ug/L 200 1.40 U 98 75-125 3 20 Zinc 205 10.0 ug/L 200 4.40 U 102 75-125 3 20 Post Spike (i]21030-PS1) Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:31 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.188 0.0100 mg/L 0.200 -0.0113 94 80-120 Barium 0.274 0.0100 mg/L 0.200 0.0671 104 80-120 Beryllium 0.0191 0.00100 mg/L 0.0200 -0.000654 95 80-120 Cadmium 0.0187 0.00100 mg/L 0.0200 -0.00127 93 80-120 Chromium 0.196 0.0100 mg/L 0.200 -0.00223 98 80-120 Cobalt 0.201 0.0100 mg/L 0.200 0.000105 101 80-120 Copper 0.189 0.0100 mg/L 0.200 -0.0110 95 80-120 Iron 104 0.0500 mg/L 1.00 100 362 80-120 QM-08 Lead 0.197 0.0100 mg/L 0.200 -0.000820 99 80-120 Manganese 0.466 0.0100 mg/L 0.200 0.259 104 80-120 Nickel 0.200 0.0100 mg/L 0.200 -0.000195 100 80-120 Silver 0.203 0.0100 mg/L 0.200 -0.00117 102 80-120 Tin 0.196 0.0100 mg/L 0.200 -0.00262 98 80-120 Vanadium 0.197 0.0100 mg/L 0.200 -0.00122 99 80-120 Zinc 0.208 0.0100 mg/L 0.200 0.00236 103 80-120 Batch 1129005 - EPA 3005A FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 68 of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1129005 - EPA 3005A - Continued Blank (1329005-BLK1) Prepared: 10/29/2021 06:14 Analyzed: 11/02/2021 22:24 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 0.370 U 1.00 ug/L Selenium 0.910 U 1.00 ug/L Thallium 0.110 U 1.00 ug/L LCS (1329005-BS1) Prepared: 10/29/2021 06:14 Analyzed: 11/02/2021 22:28 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 21.3 1.00 ug/L 20.0 107 80-120 Selenium 20.5 1.00 ug/L 20.0 103 80-120 Thallium 21.7 1.00 ug/L 20.0 109 80-120 Matrix Spike (1329005-MS3) Prepared: 10/29/2021 06:14 Analyzed: 11/02/2021 22:32 Source: CE15177-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 42.8 2.00 ug/L 40.0 0.740 U 107 75-125 Selenium 46.4 2.00 ug/L 40.0 1.82 U 116 75-125 Thallium 41.8 2.00 ug/L 40.0 0.220 U 105 75-125 Matrix Spike Dup (1329005-MSDI) Prepared: 10/29/2021 06:14 Analyzed: 11/02/2021 22:36 Source: CE15177-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 41.8 2.00 ug/L 40.0 0.740 U 104 75-125 2 20 Selenium 40.5 2.00 ug/L 40.0 1.82 U 101 75-125 14 20 Thallium 40.7 2.00 ug/L 40.0 0.220 U 102 75-125 3 20 Classical Chemistry Parameters - Quality Control Batch 1.719028 - NO PREP Blank (1319028-BLK3) Prepared: 10/19/2021 15:56 Analyzed: 10/19/2021 17:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L LCS (1319028-BS1) Prepared: 10/19/2021 15:56 Analyzed: 10/19/2021 18:14 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 100 90-110 Matrix Spike (1319028-MS3) Prepared: 10/19/2021 15:56 Analyzed: 10/19/2021 17:41 Source: CE15554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.021 98 90-110 Matrix Spike (1J19028-MS2) Prepared: 10/19/2021 15:56 Analyzed: 10/19/2021 17:44 Source: CE15554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 69 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 111902E - NO PREP - Continued Matrix Spike (1319028-MS2) Continued Prepared: 10/19/2021 15:56 Analyzed: 10/19/2021 17:44 Source: CE15554-02 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Nitrite as N 0.83 0.10 mg/L 1.00 0.017 U 83 90-110 QM-07 Matrix Spike Dup (1719028-MSD1) Prepared: 10/19/2021 15:56 Analyzed: 10/19/2021 17:42 Source: CE15554-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Nitrite as N 0.99 0.10 mg/L 1.00 0.021 97 90-110 0.5 10 Batch 1120023 - NO PREP Blank (1120023-BLK3) Prepared: 10/20/2021 16:27 Analyzed: 10/20/2021 16:45 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L LCS (1320023-BS1) Prepared: 10/20/2021 16:27 Analyzed: 10/20/2021 16:45 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Sulfide 0.38 0.10 mg/L 0.401 95 80-120 Duplicate (1320023-DUPl) Prepared: 10/20/2021 16:27 Analyzed: 10/20/2021 16:45 Source: CE15371-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L 0.010 U 25 Matrix Spike (1J20023-MS3) Prepared: 10/20/2021 16:27 Analyzed: 10/20/2021 16:45 Source: CE15371-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Sulfide 0.38 0.10 mg/L 0.401 0.010 U 95 80-120 Matrix Spike Dup (1320023-MSDl) Prepared: 10/20/2021 16:27 Analyzed: 10/20/2021 16:45 Source: CE15371-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Sulfide 0.38 0.10 mg/L 0.401 0.010 U 94 80-120 0.5 25 Batch V21002 - NO PREP Blank (1321002-BLK3) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 16:42 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L Sulfate as SO4 2.9 U 5.0 mg/L LCS (1321002-BS1) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 16:59 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Chloride 51 5.0 mg/L 50.0 102 90-110 Sulfate as SO4 51 5.0 mg/L 50.0 102 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 70 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1121002 - NO PREP - Continued Matrix Spike (1323002-MS3) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:17 Source: CE15554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 30 5.0 mg/L 20.0 10 99 90-110 Sulfate as SO4 56 5.0 mg/L 20.0 35 108 90-110 Matrix Spike (1J23002-MS2) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:52 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 46 5.0 mg/L 20.0 26 98 90-110 Sulfate as SO4 19 5.0 mg/L 20.0 2.9 U 97 90-110 Matrix Spike Dup (1J23002-MSD1) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:35 Source: CE35554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 32 5.0 mg/L 20.0 10 108 90-110 6 10 Sulfate as SO4 57 5.0 mg/L 20.0 35 113 90-110 2 10 QM-07 Batch 1122004 - NO PREP Blank (1322004-BLK1) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L LCS (1322004-BS3) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.38 0.10 mg/L 0.401 94 80-120 Duplicate (1122004-DUP3) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.055 J 0.10 mg/L 0.053 4 25 Matrix Spike (1322004-MS1) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE15554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.29 0.10 mg/L 0.401 0.053 58 80-120 QM-07 Matrix Spike Dup (1322004-MSD1) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.29 0.10 mg/L 0.401 0.053 59 80-120 1 25 QM-07 Batch 1.725024 - Same Blank (1125024-BLK3) Prepared: 10/25/2021 14:10 Analyzed: 10/26/2021 12:54 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 71 of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch IJ25024 - Same - Continued Blank (1325024-BLK1) Continued Prepared: 10/25/2021 14:10 Analyzed: 10/26/2021 12:54 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Cyanide (total) 0.0049 U 0.010 mg/L LCS (1325024-BS3) Prepared: 10/25/2021 14:10 Analyzed: 10/26/2021 12:59 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Cyanide (total) 0.14 0.010 mg/L 0.150 94 85-115 Matrix Spike (1J25024-MS3) Prepared: 10/25/2021 14:10 Analyzed: 10/26/2021 13:02 Source: CE15240-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Cyanide (total) 0.13 0.010 mg/L 0.150 0.0049 U 85 85-115 Matrix Spike Dup (1325024-MSDI) Prepared: 10/25/2021 14:10 Analyzed: 10/26/2021 13:04 Source: CE15240-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Cyanide (total) 0.11 0.010 mg/L 0.150 0.0049 U 73 85-115 15 20 QM-07 Batch V25026 - NO PREP Blank (1325026-BLK3) Prepared & Analyzed: 10/25/2021 18:14 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Dissolved Solids 50 U 50 mg/L LCS (1325026-BSI) Prepared & Analyzed: 10/25/2021 18:14 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Dissolved Solids 920 50 mg/L 1000 92 80-120 Duplicate (1325026-DUPl) Prepared & Analyzed: 10/25/2021 18:14 Source: CE13958-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Dissolved Solids 2200 100 mg/L 2300 4 20 Duplicate (1325026-DUP2) Prepared & Analyzed: 10/25/2021 18:14 Source: CE13958-02 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Dissolved Solids 2100 100 mg/L 2200 4 20 Batch 1.726014 - NO PREP Blank (1126014-BLK3) Prepared: 10/26/2021 09:55 Analyzed: 10/29/2021 12:59 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 72 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1126014 - NO PREP - Continued LCS (1326014-BS1) Prepared: 10/26/2021 09:55 Analyzed: 10/29/2021 13:00 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.2 0.10 mg/L 1.25 98 90-110 Matrix Spike (1326014-MS3) Prepared: 10/26/2021 09:55 Analyzed: 10/29/2021 13:04 Source: CE35235-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.1 0.20 mg/L 1.00 0.18 92 90-110 Matrix Spike (1326014-MS2) Prepared: 10/26/2021 09:55 Analyzed: 10/29/2021 13:09 Source: CE35235-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 3.2 E 0.10 mg/L 0.521 2.6 111 90-110 QM-07 Matrix Spike Dup (1326014-MSDI) Prepared: 10/26/2021 09:55 Analyzed: 10/29/2021 13:06 Source: CE15235-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.1 0.20 mg/L 1.00 0.18 93 90-110 0.3 10 Batch 1127021 - NO PREP Blank (1327021-BLK3) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (1327021-BSI) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 99 15 mg/L 100 99 80-120 Matrix Spike (1327021-MS3) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:12 Source: CE15554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 110 15 mg/L 37.8 60 140 80-120 QM-07 Matrix Spike Dup (1327021-MSD1) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:12 Source: CE15554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 110 15 mg/L 37.8 60 137 80-120 1 25 QM-07 Batch .1K01020 - NO PREP Blank (1K03020-BLKI) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 73 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1K01020 - NO PREP - Continued LCS (1K01020-BS1) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 100 15 mg/L 100 100 80-120 Matrix Spike (1K01020-MS3) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:14 Source: CE15194-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 88 15 mg/L 37.8 39 129 80-120 QM-07 Matrix Spike Dup (1K03020-MSD3) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:15 Source: CE15194-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 89 15 mg/L 37.8 39 133 80-120 2 25 QM-07 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 1.725015 - EPA 5030B MS Blank (1125015-BLK3) Prepared: 10/25/2021 00:00 Analyzed: 10/25/2021 08:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-& 5.4 ug/L 5.00 107 75-125 LCS (1325015-BS1) Prepared: 10/25/2021 00:00 Analyzed: 10/25/2021 08:33 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 109 80-133 Toluene-& 5.7 ug/L 5.00 114 75-125 Matrix Spike (1325015-MS3) Prepared: 10/25/2021 00:00 Analyzed: 10/25/2021 18:04 Source: AE08430-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 50 2.0 ug/L 25.0 25 101 80-133 Toluene-& 5.4 u91L 5.00 108 75-125 Matrix Spike Dup (1325015-MSD1) Prepared: 10/25/2021 00:00 Analyzed: 10/25/2021 18:29 Source: AE08430-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 50 2.0 ug/L 25.0 25 101 80-133 0.2 19 Toluene-d8 5.4 ug/L 5.00 109 75-125 Chlorinated Herbicides by GC - Quality Control Batch IJ25043 - EPA 3510C Blank (1325043-BLK1) Prepared: 10/25/2021 15:30 Analyzed: 10/27/2021 15:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 74 of S2 (� �Eo www.encolabs.com QUALITY CONTROL DATA Chlorinated Herbicides by GC - Quality Control Batch IJ25043 - EPA 3510C - Continued Blank (1325043-BLK1) Continued Prepared: 10/25/2021 15:30 Analyzed: 10/27/2021 15:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 2,4,5-T 0.28 U 0.50 ug/L 2,4,5-TP (Silvex) 0.44 U 0.50 ug/L 2,4-D 0.27 U 0.50 ug/L Dinoseb 0.32 U 0.50 ug/L Pentachlorophenol 0.19 U 0.50 ug/L 2,4-DC,4A 1.8 u91L 2.00 88 37-134 LCS (1325043-BSI) Prepared: 10/25/2021 15:30 Analyzed: 10/27/2021 15:36 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 2,4,5-TP (Silvex) 1.4 0.50 ug/L 2.00 70 24-135 2,4-D 1.5 0.50 ug/L 2.00 74 20-134 2,4-DCAA 2.0 u91L 2.00 100 37-134 Matrix Spike (1725043-MS3) Prepared: 10/25/2021 15:30 Analyzed: 10/27/2021 16:01 Source: AE08497-01 Spike Source O/oREC RPD Analvte Result Flaa Q Units Level Result O/oREC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.55 0.50 ug/L 2.00 0.44 U 28 24-135 2,4-D 0.69 0.50 ug/L 2.00 0.27 U 34 20-134 2, 4-DCAA 0.62 u91L 2.00 41 37-134 Matrix Spike Dup (1725043-MSD1) Prepared: 10/25/2021 15:30 Analyzed: 10/27/2021 16:27 Source: AE08497-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.86 0.50 ug/L 2.00 0.44 U 43 24-135 44 19 QM-11 2,4-D 0.71 0.50 ug/L 2.00 0.27 U 36 20-134 3 19 2, 4-DCAA 1.0 u91L 2.00 51 37-134 Batch IJ29001 - EPA 3510C Blank (1329001-BLK1) Prepared: 10/29/2021 07:30 Analyzed: 11/01/2021 11:58 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 2,4,5-T 0.28 U 0.50 ug/L 2,4,5-TP (Silvex) 0.44 U 0.50 ug/L 2,4-D 0.27 U 0.50 ug/L Dinoseb 0.32 U 0.50 ug/L Pentachlorophenol 0.19 U 0.50 ug/L 2,4-DC.4A[2C] 1.6 u91L 2.00 79 37-134 LCS (1329001-BS1) Prepared: 10/29/2021 07:30 Analyzed: 11/01/2021 12:23 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 2,4,5-TP (Silvex) 1.4 0.50 ug/L 2.00 68 24-135 2,4-D 1.5 0.50 ug/L 2.00 75 20-134 2,4-DC,4A[2C] 1.4 u91L 2.00 68 37-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 75 Of 82 (� �Eo www.encolabs.com QUALITY CONTROL DATA Chlorinated Herbicides by GC - Quality Control Batch 1129001 - EPA 3510C - Continued Matrix Spike (1329001-MS3) Prepared: 10/29/2021 07:30 Analyzed: 11/01/2021 12:48 Source: AE08497-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 1.2 0.50 ug/L 2.00 0.44 U 59 24-135 2,4-D 1.3 0.50 ug/L 2.00 0.27 U 66 20-134 2,4-DC,4A [2C] 1.2 u91L 2.00 62 37-134 Matrix Spike Dup (1129001-MSD3) Prepared: 10/29/2021 07:30 Analyzed: 11/01/2021 13:13 Source: AE08497-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 1.5 0.50 ug/L 2.00 0.44 U 76 24-135 25 19 QM-11 2,4-D 2.0 0.50 ug/L 2.00 0.27 U 98 20-134 40 19 QM-11 2, 4-OCAA [2C] 1.8 u91L 2.00 92 37-134 Dissolved Gases by GC - Quality Control Batch 2126005 - Same LCS Dup (1726005-BSD3) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 50.3 2.50 mg/L 45.8 110 70-130 9 30 Ethane 0.353 0.00600 mg/L 0.323 109 70-130 9 30 Ethene 0.349 0.00600 mg/L 0.302 116 70-130 10 30 Methane 0.188 0.00500 mg/L 0.174 108 70-130 11 30 Duplicate (1726005-DUPl) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 13:37 Source: AE08472-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 22.1 2.50 mg/L 22.5 2 30 Ethane 0.00510 U 0.00600 mg/L 0.00510 U 30 Ethene 0.00510 U 0.00600 mg/L 0.00510 U 30 Methane 0.00400 U 0.00500 mg/L 0.00400 U 30 Classical Chemistry Parameters - Quality Control Batch 1116001 - NO PREP Blank (1326001-BLK3) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 09:08 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 0.90 U 1.0 mg/L LCS (1326001-BSI) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 09:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 49 1.0 mg/L 50.0 97 85-115 Matrix Spike (1726001-MS3) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 10:24 Source: AE08470-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 76 of 82 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1126001 - NO PREP - Continued (� �Eo www.encolabs.com Matrix Spike (1326001-MS1) Continued Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 10:24 Source: AE08470-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 51 1.0 mg/L 50.0 2.4 97 85-115 Matrix Spike (1726001-MS2) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 18:44 Source: AE08497-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 52 1.0 mg/L 50.0 2.9 98 85-115 Matrix Spike Dup (1]26001-MSDi) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 10:47 Source: AE08470-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 50 1.0 mg/L 50.0 2.4 95 85-115 2 21 Matrix Spike Dup (1326001-MSD2) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 19:08 Source: AE08497-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 51 1.0 mg/L 50.0 2.9 97 85-115 2 21 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 77 Of 82 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. A-07 Analyte biased low in LCS but detected in the reporting limit standard. Since the analyte in the associated sample was not detected, there is no impact on data quality. 3-04 Result may be biased high. Associated calibration verification standard exceeded the upper control limit. 1-05 Result may be biased low. Associated calibration verification standard did not meet the minimum control limit. 1-06 The associated laboratory control sample exhibited low bias; the reported result should be considered to be a minimum estimate. 0-05 This sample was extracted outside of the EPA recommended holding time. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test). QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QS-03 Surrogate recovery outside acceptance limits QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. R-05 The sample was diluted due to the presence of high levels of non -target analytes resulting in elevated reporting limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 78 Of 82 E 0 a 0 U W cc 0 0 In D U LL 0 Z a 2 U N W cc 0 a Q 0 m a J Z 0 9M a: W N Z 0 U LJ r Z CW C Z 0 z W 14 6 1. ro a -2 O A u (9 � V U N ELO co g 0 QJ H co LU N � 0. E-r E a 7 w / E ro CC Z Q _a td C U a,'gd'JO`pO'e8`Sy'6b x °a Q :XI o e>Z n'[1'as'gS 4d'!N'uW'8�'ryo'�O'o'J`Po`efl' i' x X X X x X x X X o 0 o X X til? 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N d H E C co 5o ELu v o co U Cb ❑ 3 [V m � c u C' •� G r IEiv W E E m 3 n O _ Z i ¢ IL o m U C 66 (�1 ¢ E m Ay a c fiw) co N �v Q o 0 �W G z to a a � z h W fr7 w g 3 •/ rI©� ♦/�� m C 82 F Page 80 of U ¢ Sample Preservation Verification ENCO Cary 99- MOD Work Order: CE15554 Project: Moore County Active C &rD LF - Fall Client: S&ME, Inc. (SM004) Project #: 4358-20-043 Logged In: 19-Oct-21 14:11 Logged By: Rachel A ur�y sh c�2IPreservation Check Performed By: Date/TimeCt EilNi C E 15554-01 Cant Type Pres (pH) Requirement. pH Checked / In Control pH ,adjusted Date/Time Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y N I NA Y I 1 NA C 250mLP+ZnAc+NaOH ?9 Y I N I NA Y NA D 250mLP+H2SO4 <2 Y I N I NA Y I NA CE15554-02 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 1' N 1 NA Y / NA C 250mLP+ZnAc+NaOH >9 Y N / NA Y / NA D 250mLP+H2SO4 <2 Y N I NA Y N/ NA CE15554-03 Cont Type Pres (pH) pH Checked / Requirement In Control pH Adjusted DatelTime Adiusted Reagent Used/Comments B250mLP+HNO3 <2 Y 11 N / NA Y NA C 250mLP+ZnAc+NaOH >9 Y/ N/ NA Y N I NA E15554-04 CuntP250mLP+HNO3 Pres (pH) Requirement pH Checked 1 In Control pH Adjusted DatelTme Adjusted Reagent Used/Comments B <2 I N! NA Y I 1 NA CmLP+ZnAc+NaOH >9 YIN / NA Y N NA CE15554-05 Cant Type Pres (pH) pH Checked / In Control pH Adjusted Date�me Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y / N / NA Y / NA C 250mLP+ZnAc+NaOH >9 Y N/ NA Y/ N I NA CE15554-06 Cont Type Pres (pH) pH Checked / PH Adjusted Date�me Reagent Used/Comments Requirement In Control Adjusted B 250mLP+HNO3 <2 Y 1 N/ NA Y 1 / NA C 250mLP+ZnAc+NaOH >9 YIN / NA Y NA ku.. IelmntlPrintlwko_Preservation Check. rpt Page 81 of 82 Sample Preservation Verification ENCO Cary Work Order: CE15554 Client: S&ME, Inc. (SM004) Project: Moore County Active C & D LF - Fall Project #: 4358-20-043 Logged In: 19-Oct-21 14:11 Logged By: Rachel Ann Y ish Preservation Check Performed By: _ DatelTime: U 1i 17 CE15554-07 Cont Type Pres (pH) Requirement pH Checked I In Control pH Adjusted DatetTime Adjusted Reagent Used/Comments C 250mLA (PEST) Pest pH 5-9 I N I NA Y ! NA G 250mLP+HNO3 <2 N I NA Y I N/ NA H 250mLP+ZnAc+NaOH >9 Y N I NA Y I 1 NA I 250mLP+NaOH >12 Y N/ NA Y I N/ NA El5554-08 C,;. 250MLA (PEST) Pres (pH) pH Checked/ Requirement In Control pH Adjusted Datel time Adjusted Reagent Used/Comments Pest pH 5-9 / N 1 NA Y 1 / NA G 250mLP+HNO3 <2 Y N/ NA Y I NA H 250mLP+ZnAc+NaOH >9 Y 1 N / NA YIN NA 1 250mLP+NaOH >12 Y N/ NA Y 0 NA ti CE15554-09 Cont YP Type Pres (pH) Requirement pH Checked / In Control DateTme pH Adjusted Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 I N/ NA Y 1 NA C 250mLP+ZnAc+NaOH >9 Y N/ NA Y N NA Rea ent Name ID 1 2 Rea ent Name ID 3 4 Rea ent Name ID 5 6 pH Strip ID: PH Strips C0F0555 r C:lelmntlPrii,,,..,\u_rjcacrvanonuneCK.rpt Page 82 of 82 2 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, November 10, 2021 S&ME, Inc. (SM004) Attn: Edmund Henriques 8646 West Market Street, Suite 105 Greensboro, NC 27409 RE: Laboratory Results for Project Number: 4358-20-043, Project Name/Desc: Moore County Closed LF CA ENCO Workorder(s): CE15555 Dear Edmund Henriques, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, October 19, 2021. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 0"6LC'=-:;tA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 29 PROJECT NARRATIVE Client: S&ME, Inc. (SM004) Project: Moore County Closed LF CA Lab ID: CE15555 (� �Eo www.encolabs.com Overview Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on an acceptable LCS recovery (QM-07). Post -digestion spike did not meet method requirements due to confirmed matrix effects (QM-08). Precision between duplicate matrix spikes of the same sample was outside acceptance limits (QM-11). Quality Control Remarks The associated CCV standard exhibited high bias; since the result is ND, there is no impact (QV-01). Other Comments The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Chuck Smith Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 29 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW2 Lab ID: CE15555-01 Sampled: 10/19/21 09:50 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/21/21 21:25 EPA 353.2 NO PREP 10/21/21 09:50 10/19/21 15:56 10/19/21 17:46 EPA 353.2 [CALC] 10/21/21 09:50 10/26/21 09:54 10/29/21 14:58 EPA 6010D EPA 3005A 04/17/22 10/21/21 16:13 10/25/21 11:22 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:21 10/22/21 07:37 EPA 8260D EPA 503013_MS 11/02/21 10/25/21 08:55 10/25/21 09:30 EPA 8260D EPA 5030B_MIS 11/02/21 10/27/21 17:00 10/28/21 03:07 EPA 9060A NO PREP 11/16/21 10/26/21 07:08 10/26/21 14:00 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 10:22 SM 4500S2 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MW2 Lab ID: CE15555-01RE1 Sampled: 10/19/21 09:50 Received: 10/19/21 13:00 Parameter Preoaration Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 11/02/21 11/01/21 09:50 11/01/21 12:24 EPA 353.2 NO PREP 11/16/21 10/26/21 09:54 10/29/21 14:58 EPA 8260D EPA 5030B_MIS 11/02/21 11/01/21 15:32 11/02/21 06:02 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 13:53 Client ID: 6301-MW3 Lab ID: CE15555-02 Sampled: 10/19/21 08:30 Received: 10/19/21 13:00 Parameter Preoaration Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/21/21 21:42 EPA 310.2 NO PREP 11/02/21 10/27/21 14:18 10/27/21 16:22 EPA 353.2 NO PREP 10/21/21 08:30 10/19/21 15:56 10/19/21 17:47 EPA 353.2 [CALC] 10/21/21 08:30 10/26/21 09:54 10/29/21 12:15 EPA 353.2 NO PREP 11/16/21 10/26/21 09:54 10/29/21 12:15 EPA 6010D EPA 3005A 04/17/22 10/21/21 16:13 10/25/21 11:25 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:21 10/22/21 08:22 EPA 8260D EPA 503013_MS 11/02/21 10/25/21 08:55 10/25/21 09:55 EPA 8260D EPA 503013_MS 11/02/21 10/27/21 17:00 10/28/21 03:36 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 10:38 SM 4500S2 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MW3 Lab ID: CE15555-02RE1 Sampled: 10/19/21 08:30 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/02/21 11/01/21 15:32 11/02/21 06:29 EPA 9060A NO PREP 11/16/21 10/27/21 07:24 10/27/21 13:36 Client ID: 6301-MW15R Lab ID: CE15555-03 Sampled: 10/18/21 16:45 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/15/21 10/21/21 06:21 10/21/21 22:00 EPA 310.2 NO PREP 11/01/21 10/27/21 14:18 10/27/21 16:22 EPA 353.2 NO PREP 10/20/21 16:45 10/19/21 15:56 10/19/21 17:48 EPA 353.2 [CALC] 10/20/21 16:45 10/26/21 09:54 10/29/21 12:19 EPA 353.2 NO PREP 11/15/21 10/26/21 09:54 10/29/21 12:19 EPA 6010D EPA 3005A 04/16/22 10/21/21 16:13 10/25/21 11:27 EPA 7470A EPA 245.1 11/15/21 10/20/21 15:21 10/22/21 08:24 EPA 8260D EPA 503013_MS 11/01/21 10/25/21 08:55 10/25/21 10:21 EPA 8260D EPA 5030B_MS 11/01/21 10/27/21 16:42 10/29/21 10:18 RSK 175 Same 11/01/21 10/26/21 08:00 10/26/21 10:54 SM 4500S2 D-2011 NO PREP 10/25/21 10/22/21 09:58 10/22/21 10:16 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 29 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW15R Lab ID: CE15555-03RE3 Sampled: 10/18/21 16:45 Received: 10/19/21 13:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 9060A NO PREP 11/15/21 RSK 175 Same 11/01/21 10/27/21 07:24 10/27/21 13:54 10/26/21 08:00 10/26/21 14:09 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 29 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW2 Lab ID: CE15555-01 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 25 0.80 2.0 ug/L EPA 8260D Barium - Total 63.0 1.10 10.0 ug/L EPA 6010D Chloride 93 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 2.6 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 0.68 J 0.15 1.0 ug/L EPA 8260D Methane 0.0824 0.00400 0.00500 mg/L RSK 175 Nitrate as N 4.6 D 0.41 1.0 mg/L EPA 353.2 Sulfate as SO4 17 2.9 5.0 mg/L EPA 300.0 Total Organic Carbon 13 0.90 1.0 mq/L EPA 9060A Client ID: 6301-MW2 Lab ID: CE15555-01RE3 Analvte Results Flag MDL PQL Units Method Notes Carbon dioxide 259 D 10.4 12.5 mg/L RSK 175 Nitrate/Nitrite as N 4.6 D 0.41 1.0 mg/L EPA 353.2 Total Alkalinity as CaCO3 320 D 70 75 mg/L EPA 310.2 Client ID: 6301-MW3 Lab ID: CE15555-02 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 1.6 J 0.80 2.0 ug/L EPA 8260D Barium - Total 36.7 1.10 10.0 ug/L EPA 6010D Carbon dioxide 81.8 2.07 2.50 mg/L RSK 175 Chloride 7.8 2.2 5.0 mg/L EPA 300.0 Nitrate as N 0.35 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.35 0.041 0.10 mg/L EPA 353.2 Sulfate as SO4 11 2.9 5.0 mg/L EPA 300.0 Client ID: 6301-MW3 Lab ID: CE15555-02RE3 Analvte Results Flag MDL PQL Units Method Notes Total Organic Carbon 1.7 0.90 1.0 mg/L EPA 9060A Client ID: 6301-MW15R Lab ID: CE15555-03 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 42.2 1.10 10.0 ug/L EPA 6010D Chloride 3.3 1 2.2 5.0 mg/L EPA 300.0 cis-1,2-Dichloroethene 2.4 0.15 1.0 ug/L EPA 8260D Nitrate as N 0.11 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.11 0.041 0.10 mg/L EPA 353.2 Sulfate as SO4 9.6 2.9 5.0 mg/L EPA 300.0 Sulfide 0.029 J 0.010 0.10 mg/L SM 4500S2 D-2011 Total Alkalinity as CaCO3 40 14 15 mg/L EPA 310.2 Client ID: 6301-MW15R Lab ID: CE15555-03RE3 Analvte Results Flag MDL PQL Units Method Notes Carbon dioxide 216 D 31.0 37.5 mg/L RSK 175 Methane 1.52 D 0.0600 0.0750 mg/L RSK 175 Total Organic Carbon 2.2 0.90 1.0 mg/L EPA 9060A FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 29 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW2 Lab Sample ID:CE15555-01 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2109:50 Work Order: CE15555 Project: Moore County Closed LF CA Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 1127031 EPA 8260D 10/28/21 03:07 RKY QV-01 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1127031 EPA 8260D 10/28/21 03:07 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 1127031 EPA 8260D 10/28/21 03:07 RKY QV-01 Acetone [67-64-1]A 10 U ug/L 1 10 20 1127031 EPA 8260D 10/28/21 03:07 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 1127031 EPA 8260D 10/28/21 03:07 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY QV-01 Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 1127031 EPA 8260D 10/28/21 03:07 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY QV-01 Chlorobenzene [108-90-7]A 2.6 ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY QV-01 Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY cis-1,2-Dichloroethene [156-59-2]A 0.68 J ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 1127031 EPA 8260D 10/28/21 03:07 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY QV-01 Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 1127031 EPA 8260D 10/28/21 03:07 RKY QV-01 Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 1127031 EPA 8260D 10/28/21 03:07 RKY QV-01 Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 1127031 EPA 8260D 10/28/21 03:07 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 29 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW2 Lab Sample ID:CE15555-01 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2109:50 Work Order: CE15555 Project: Moore County Closed LF CA Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffly Notes 4-Bromofluorobenzene 51 1 50.0 101 % 53-136 IJ27031 EPA 8260D 10128121 03:07 RKY 4-Bromofluorobenzene 55 1 50.0 110 % 53-136 1K01036 EPA 8260D 11102121 06:02 ref Dibromofluoromethane 50 1 50.0 99 % 67-129 IJ27031 EPA 8260D 10128121 03:07 RKY Dibromofluoromethane 55 1 50.0 110 % 67-129 1K01036 EPA 8260D 11102121 06:02 ref Toluene-d8 51 1 50.0 102 % 59-134 IJ27031 EPA 8260D 10128121 03:07 RKY Toluene-d8 58 1 50.0 116 % 59-134 1K01036 EPA 8260D 11102121 06:02 ref Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 07:37 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J21030 EPA 6010D 10/25/21 11:22 JDH Barium [7440-39-3]^ 63.0 ug/L 1 1.10 10.0 1321030 EPA 6010D 10/25/21 11:22 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 11:22 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:22 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 11:22 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J21030 EPA 6010D 10/25/21 11:22 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 11:22 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 93 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 21:25 ZGW Nitrate as N [14797-55-8] 4.6 D mg/L 10 0.41 1.0 [CALC] EPA 353.2 10/29/21 14:58 JAH Nitrate/Nitrite as N^ 4.6 D mg/L 10 0.41 1.0 1326013 EPA 353.2 10/29/21 14:58 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1J19028 EPA 353.2 10/19/21 17:46 JAH Sulfate as SO4 [14808-79-8]^ 17 mg/L 1 2.9 5.0 1321002 EPA 300.0 10/21/21 21:25 ZGW Sulfide [18496-25-8]^ 0.010 u mg/L 1 0.010 0.10 1J22004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 320 D mg/L 5 70 75 1KO1020 EPA 310.2 11/01/21 12:24 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed AX Notes 1,4-Dioxane [123-91-1]^ 25 ug/L 1 0.80 2.0 1325015 EPA 8260D 10/25/21 09:30 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.5 1 5.00 111 % 75-125 IJ25015 EPA 6260D 10125121 09:30 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 29 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW2 Lab Sample ID:CE15555-01 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2109:50 Work Order: CE15555 Project: Moore County Closed LF CA Sampled By: Gary Simcox Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 259 D mg/L 5 10.4 12.5 1326005 RSK 175 10/26/21 13:53 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 10:22 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 10:22 JMW Methane [74-82-8] 0.0824 mg/L 1 0.00400 0.00500 1326005 RSK 175 10/26/21 10:22 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 13 mg/L 1 0.90 1.0 1326001 EPA 9060A 10/26/21 14:00 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 29 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW3 Lab Sample ID:CE15555-02 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2108:30 Work Order: CE15555 Project: Moore County Closed LF CA Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1127031 EPA 8260D 10/28/21 03:36 RKY QV-01 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1127031 EPA 8260D 10/28/21 03:36 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1127031 EPA 8260D 10/28/21 03:36 RKY QV-01 Acetone [67-64-1]A 10 u ug/L 1 10 20 1127031 EPA 8260D 10/28/21 03:36 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1127031 EPA 8260D 10/28/21 03:36 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY QV-01 Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1127031 EPA 8260D 10/28/21 03:36 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY QV-01 Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY QV-01 Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1127031 EPA 8260D 10/28/21 03:36 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1KO1036 EPA 8260D 11/02/21 06:29 ref Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1127031 EPA 8260D 10/28/21 03:36 RKY QV-01 Vinyl chloride [75-01-4]^ 0.32 u ug/L 1 0.32 1.0 1127031 EPA 8260D 10/28/21 03:36 RKY QV-01 Xylenes (Total) [1330-20-7]A 0.45 Ll ug/L 1 0.45 3.0 1127031 EPA 8260D 10/28/21 03:36 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 29 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW3 Lab Sample ID:CE15555-02 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2108:30 Work Order: CE15555 Project: Moore County Closed LF CA Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 51 1 50.0 102 % 53-136 V27031 EPA 6260D 10128121 03:36 RKY 4-Bromofluorobenzene 54 1 50.0 109 % 53-136 IK01036 EPA 6260D 11102121 06:29 ref Dibromofluoromethane 48 1 50.0 96 % 67-129 V27031 EPA 6260D 10126121 03:36 RKY Dibromofluoromethane 56 1 50.0 113 % 67-129 IK01036 EPA 6260D 11102121 06:29 ref Toluene-d8 51 1 50.0 101 % 59-134 V27031 EPA 6260D 10126121 03:36 RKY Toluene-d8 58 1 50.0 117 % 59-134 IK01036 EPA 6260D 11102121 06:29 ref Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:22 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 IJ21030 EPA 6010D 10/25/21 11:25 JDH Barium [7440-39-3]^ 36.7 ug/L 1 1.10 10.0 1121030 EPA 6010D 10/25/21 11:25 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 11:25 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:25 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 11:25 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J21030 EPA 6010D 10/25/21 11:25 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 11:25 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 7.8 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 21:42 ZGW Nitrate as N [14797-55-8] 0.35 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/29/21 12:15 JAH Nitrate/Nitrite as N^ 0.35 mg/L 1 0.041 0.10 1126013 EPA 353.2 10/29/21 12:15 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1J19028 EPA 353.2 10/19/21 17:47 JAH Sulfate as SO4 [14808-79-B]^ 11 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/21/21 21:42 ZGW Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1J22004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 14 U mg/L 1 14 15 1J27021 EPA 310.2 10/27/21 16:22 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.6 J ug/L 1 0.80 2.0 1125015 EPA 8260D 10/25/21 09:55 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes Toluene-d8 5.4 1 5.00 107 % 75-125 V25015 EPA 8260D 10125121 09:55 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 29 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW3 Lab Sample ID:CE15555-02 Received: 10/19/21 13:00 Matrix: Ground Water Sampled: 10/19/2108:30 Work Order: CE15555 Project: Moore County Closed LF CA Sampled By: Gary Simcox Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 81.8 mg/L 1 2.07 2.50 1326005 RSK 175 10/26/21 10:38 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 10:38 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 10:38 JMW Methane [74-82-8] 0.00400 U mg/L 1 0.00400 0.00500 1J26005 RSK 175 10/26/21 10:38 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Total Organic Carbon^ 1.7 mg/L 1 0.90 1.0 1327005 EPA 9060A 10/27/21 13:36 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 29 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW15R Lab Sample ID:CE15555-03 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 16:45 Work Order: CE15555 Project: Moore County Closed LF CA Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 u ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,2-Dibromoethane [106-93-4]A 0.66 u ug/L 1 0.66 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 u ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,2-Dichloroethane [107-06-2]A 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,2-Dichloropropane [78-87-5]A 0.10 u ug/L 1 0.10 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 u ug/L 1 0.19 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1127025 EPA 8260D 10/29/21 10:18 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1127025 EPA 8260D 10/29/21 10:18 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 u ug/L 1 1.1 5.0 1127025 EPA 8260D 10/29/21 10:18 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1127025 EPA 8260D 10/29/21 10:18 RKY Acrylonitrile [107-13-1]A 3.5 u ug/L 1 3.5 10 1127025 EPA 8260D 10/29/21 10:18 RKY Benzene [71-43-2]A 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Bromoform [75-25-2]A 0.22 u ug/L 1 0.22 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1127025 EPA 8260D 10/29/21 10:18 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Chloroform [67-66-3]A 0.18 u ug/L 1 0.18 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY cis-1,2-Dichloroethene [156-59-2]A 2.4 ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Iodomethane [74-88-4]A 1.7 u ug/L 1 1.7 5.0 1127025 EPA 8260D 10/29/21 10:18 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Toluene [108-88-3]A 0.14 u ug/L 1 0.14 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 u ug/L 1 0.21 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Trichloroethene [79-01-6]A 0.15 u ug/L 1 0.15 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Trichlorofluoromethane [75-69-4]A 0.24 u ug/L 1 0.24 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1127025 EPA 8260D 10/29/21 10:18 RKY Vinyl chloride [75-01-4]A 0.32 u ug/L 1 0.32 1.0 1127025 EPA 8260D 10/29/21 10:18 RKY Xylenes (Total) [1330-20-7]A 0.45 Ll ug/L 1 0.45 3.0 1127025 EPA 8260D 10/29/21 10:18 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 29 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW15R Lab Sample ID:CE15555-03 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 16:45 Work Order: CE15555 Project: Moore County Closed LF CA Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 62 1 50.0 123 % 53-136 V27025 EPA 6260D 10129121 10:18 RKY Dibromofluoromethane 59 1 50.0 119 % 67-129 V27025 EPA 6260D 10129121 10:18 RKY Toluene-d8 53 1 50.0 107 % 59-134 V27025 EPA 6260D 10129121 10:18 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:24 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J21030 EPA 6010D 10/25/21 11:27 JDH Barium [7440-39-3]^ 42.2 ug/L 1 1.10 10.0 1121030 EPA 6010D 10/25/21 11:27 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J21030 EPA 6010D 10/25/21 11:27 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J21030 EPA 6010D 10/25/21 11:27 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J21030 EPA 6010D 10/25/21 11:27 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J21030 EPA 6010D 10/25/21 11:27 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J21030 EPA 6010D 10/25/21 11:27 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 3.3 J mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 22:00 ZGW Nitrate as N [14797-55-8] 0.11 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/29/21 12:19 JAH Nitrate/Nitrite as N^ 0.11 mg/L 1 0.041 0.10 1126013 EPA 353.2 10/29/21 12:19 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1J19028 EPA 353.2 10/19/21 17:48 JAH Sulfate as SO4 [14808-79-B]^ 9.6 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/21/21 22:00 ZGW Sulfide [18496-25-8]^ 0.029 J mg/L 1 0.010 0.10 1122004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 40 mg/L 1 14 15 1127021 EPA 310.2 10/27/21 16:22 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J25015 EPA 8260D 10/25/21 10:21 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.1 1 5.00 102 % 75-125 V25015 EPA 8260D 10125121 10:21 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 29 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW15R Lab Sample ID:CE15555-03 Received: 10/19/21 13:00 Matrix: Ground Water Sampled:10/18/21 16:45 Work Order: CE15555 Project: Moore County Closed LF CA Sampled By: Gary Simcox Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 216 D mg/L 15 31.0 37.5 1326005 RSK 175 10/26/21 14:09 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 10:54 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 10:54 JMW Methane [74-82-8] 1.52 D mg/L 15 0.0600 0.0750 1326005 RSK 175 10/26/21 14:09 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Total Organic Carbon^ 2.2 mg/L 1 0.90 1.0 1327005 EPA 9060A 10/27/21 13:54 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 29 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IJ27025 - EPA 5030B MS Blank (1327025-BLK1) Prepared: 10/27/2021 16:42 Analyzed: 10/29/2021 03:52 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 58 u9/L 50.0 116 53-136 Dibromofluoromethane 53 u9/L 50.0 106 67-129 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 29 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1127025 - EPA 5030B MS - Continued Blank (1327025-BLK1) Continued Prepared: 10/27/2021 16:42 Analyzed: 10/29/2021 03:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Toluene-d8 52 u91L 50.0 103 59-134 LCS (1727025-BS1) Prepared: 10/27/2021 16:42 Analyzed: 10/29/2021 02:02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 88 75-133 Benzene 17 1.0 ug/L 20.0 85 80-134 Chlorobenzene 18 1.0 ug/L 20.0 91 80-120 Toluene 21 1.0 ug/L 20.0 106 71-120 Trichloroethene 18 1.0 ug/L 20.0 88 74-120 Matrix Spike (1327025-MS1) Prepared: 10/27/2021 16:42 Analyzed: 10/29/2021 02:29 Source: CE16369-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 97 75-133 Benzene 18 1.0 ug/L 20.0 0.15 U 92 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 Toluene 24 1.0 ug/L 20.0 0.14 U 120 71-120 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 98 74-120 Matrix Spike Dup (1]27025-MSD1) Prepared: 10/27/2021 16:42 Analyzed: 10/29/2021 02:57 Source: CE16369-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 91 75-133 6 20 Benzene 16 1.0 ug/L 20.0 0.15 U 81 80-134 13 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 90 80-120 7 16 Toluene 21 1.0 ug/L 20.0 0.14 U 104 71-120 15 17 Trichloroethene 16 1.0 ug/L 20.0 0.15 U 81 74-120 19 22 Batch 1127031 - EPA 5030E MS Blank (1]27031-BLK3) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 20:47 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 29 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1127031 - EPA 5030B MS - Continued Blank (1327031-BLK1) Continued Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 20:47 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 50 u91L 50.0 99 53-136 Dibromofluoromethane 49 u91L 50.0 96 67-129 Toluene-d8 50 u91L 50.0 101 59-134 LCS (1327031-BSI) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 18:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 24 1.0 ug/L 20.0 122 75-133 Benzene 24 1.0 ug/L 20.0 120 80-134 Chlorobenzene 19 1.0 ug/L 20.0 95 80-120 Toluene 20 1.0 ug/L 20.0 99 71-120 Trichloroethene 21 1.0 ug/L 20.0 107 74-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 29 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1127031 - EPA 5030B MS - Continued Matrix Spike (1327031-MS3) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 19:19 Source: CE16369-11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 24 1.0 ug/L 20.0 0.21 U 118 75-133 Benzene 23 1.0 ug/L 20.0 0.15 U 117 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 97 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 99 71-120 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 108 74-120 Matrix Spike Dup (1]27031-MSD1) Prepared: 10/27/2021 17:00 Analyzed: 10/27/2021 19:48 Source: CE16369-11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 25 1.0 ug/L 20.0 0.21 U 123 75-133 4 20 Benzene 24 1.0 ug/L 20.0 0.15 U 118 80-134 0.6 17 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 98 80-120 0.8 16 Toluene 20 1.0 ug/L 20.0 0.14 U 99 71-120 0.4 17 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 110 74-120 2 22 Batch IKO1036 - EPA 50308 MS Blank (1K03036-BLK1) Prepared: 11/01/2021 15:32 Analyzed: 11/02/2021 05:34 Analvte Result Flaq POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 29 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1K01036 - EPA 5030B MS - Continued (� �Eo www.encolabs.com Blank (SK03036-BLKS) Continued Prepared: 11/01/2021 15:32 Analyzed: 11/02/2021 05:34 Analvte Result Flaq POL Units cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 55 ug/L 50.0 109 53-136 Dibromofluoromethane 55 ug/L 50.0 111 67-129 Toluene-d8 58 ug/L 50.0 116 59-134 LCS (iK01036-BS1) Prepared: 11/01/2021 15:32 Analyzed: 11/02/2021 03:46 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 107 75-133 Benzene 22 1.0 ug/L 20.0 109 80-134 Chlorobenzene 20 1.0 ug/L 20.0 98 80-120 Toluene 19 1.0 ug/L 20.0 97 71-120 Trichloroethene 20 1.0 ug/L 20.0 102 74-120 Matrix Spike (1K01036-MS1) Prepared: 11/01/2021 15:32 Analyzed: 11/02/2021 04:13 Source: CE16465-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 100 75-133 Benzene 22 1.0 ug/L 20.0 0.15 U 109 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 100 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 102 71-120 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 111 74-120 Matrix Spike Dup (1K01036-MSD1) Prepared: 11/01/2021 15:32 Analyzed: 11/02/2021 04:40 Source: CE16465-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 104 75-133 4 20 Benzene 20 1.0 ug/L 20.0 0.15 U 102 80-134 7 17 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 100 80-120 0.4 16 Toluene 19 1.0 ug/L 20.0 0.14 U 97 71-120 4 17 Trichloroethene 23 1.0 ug/L 20.0 0.15 U 113 74-120 2 22 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 29 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch V20028 - EPA 245.1 Blank (1320028-BLK3) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:33 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L Blank (1120028-BLK2) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:35 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 3.00 U 4.00 ug/L LCS (1320028-BS1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.46 0.200 ug/L 5.00 109 80-120 Matrix Spike (1720028-MS1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:44 Source: CE15555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.96 0.200 ug/L 5.00 0.150 U 99 75-125 Matrix Spike Dup (1]20028-MSD1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:46 Source: CE15555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.99 0.200 ug/L 5.00 0.150 U 100 75-125 0.8 25 Post Spike (1]20028-PS1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:48 Source: CE15555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.02 0.200 ug/L 4.76 -0.000286 105 75-125 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch IJ21030 - EPA 3005A Blank (1321030-BLK1) Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:17 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Lead 3.10 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L LCS (1721030-BS1) Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:23 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 195 10.0 ug/L 200 98 80-120 Barium 203 10.0 ug/L 200 101 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 29 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1121030 - EPA 3005A - Continued LCS (1321030-BS1) Continued Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:23 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Cadmium 19.4 1.00 ug/L 20.0 97 80-120 Chromium 193 10.0 ug/L 200 96 80-120 Lead 197 10.0 ug/L 200 98 80-120 Selenium 202 10.0 ug/L 200 101 80-120 Silver 196 10.0 ug/L 200 98 80-120 Matrix Spike (1323030-MS1) Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:26 Source: CE35554-02 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Arsenic 182 10.0 ug/L 200 7.60 U 91 75-125 Barium 264 10.0 ug/L 200 67.1 99 75-125 Cadmium 17.7 1.00 ug/L 20.0 0.360 U 88 75-125 Chromium 189 10.0 ug/L 200 1.40 U 94 75-125 Lead 192 10.0 ug/L 200 3.10 U 96 75-125 Selenium 139 10.0 ug/L 200 6.20 U 70 75-125 QM-07 Silver 196 10.0 ug/L 200 1.90 U 98 75-125 Matrix Spike Dup (1323030-MSD1) Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:29 Source: CE15554-02 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Arsenic 188 10.0 ug/L 200 7.60 U 94 75-125 4 20 Barium 272 10.0 ug/L 200 67.1 103 75-125 3 20 Cadmium 18.1 1.00 ug/L 20.0 0.360 U 90 75-125 2 20 Chromium 194 10.0 ug/L 200 1.40 U 97 75-125 3 20 Lead 198 10.0 ug/L 200 3.10 U 99 75-125 3 20 Selenium 141 10.0 ug/L 200 6.20 U 71 75-125 1 20 QM-07 Silver 203 10.0 ug/L 200 1.90 U 102 75-125 3 20 Post Spike (1323030-PS3) Prepared: 10/21/2021 16:13 Analyzed: 10/25/2021 10:31 Source: CE35554-02 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Arsenic 0.188 0.0100 mg/L 0.200 -0.0113 94 80-120 Barium 0.274 0.0100 mg/L 0.200 0.0671 104 80-120 Cadmium 0.0187 0.00100 mg/L 0.0200 -0.00127 93 80-120 Chromium 0.196 0.0100 mg/L 0.200 -0.00223 98 80-120 Lead 0.197 0.0100 mg/L 0.200 -0.000820 99 80-120 Selenium 0.147 0.0100 mg/L 0.200 -0.0580 73 80-120 QM-08 Silver 0.203 0.0100 mg/L 0.200 -0.00117 102 80-120 Classical Chemistry Parameters - Quality Control Batch V19028 - NO PREP Blank (1319028-BLK3) Prepared: 10/19/2021 15:56 Analyzed: 10/19/2021 17:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 29 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 111902E - NO PREP - Continued LCS (1319028-BS1) Prepared: 10/19/2021 15:56 Analyzed: 10/19/2021 18:14 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 100 90-110 Matrix Spike (1319028-MS3) Prepared: 10/19/2021 15:56 Analyzed: 10/19/2021 17:41 Source: CE35554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.021 98 90-110 Matrix Spike (1J19028-MS2) Prepared: 10/19/2021 15:56 Analyzed: 10/19/2021 17:44 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.83 0.10 mg/L 1.00 0.017 U 83 90-110 QM-07 Matrix Spike Dup (1339028-MSDI) Prepared: 10/19/2021 15:56 Analyzed: 10/19/2021 17:42 Source: CE15554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.99 0.10 mg/L 1.00 0.021 97 90-110 0.5 10 Batch 1121002 - NO PREP Blank (1321002-BLK3) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 16:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L Sulfate as SO4 2.9 U 5.0 mg/L LCS (1321002-BS1) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 16:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 51 5.0 mg/L 50.0 102 90-110 Sulfate as SO4 51 5.0 mg/L 50.0 102 90-110 Matrix Spike (1J23002-MS3) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:17 Source: CE35554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 30 5.0 mg/L 20.0 10 99 90-110 Sulfate as SO4 56 5.0 mg/L 20.0 35 108 90-110 Matrix Spike (1323002-MS2) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:52 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 46 5.0 mg/L 20.0 26 98 90-110 Sulfate as SO4 19 5.0 mg/L 20.0 2.9 U 97 90-110 Matrix Spike Dup (1323002-MSDI) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:35 Source: CE15554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 32 5.0 mg/L 20.0 10 108 90-110 6 10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 29 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1121002 - NO PREP - Continued Matrix Spike Dup (1323002-MSDI) Continued Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:35 Source: CE15554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfate as SO4 57 5.0 mg/L 20.0 35 113 90-110 2 10 QM-07 Batch 1122004 - NO PREP Blank (1322004-BLK3) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L LCS (1322004-BSI) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.38 0.10 mg/L 0.401 94 80-120 Duplicate (1322004-DUPl) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE15554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.055 3 0.10 mg/L 0.053 4 25 Matrix Spike (1322004-MS3) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.29 0.10 mg/L 0.401 0.053 58 80-120 QM-07 Matrix Spike Dup (1322004-MSDI) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.29 0.10 mg/L 0.401 0.053 59 80-120 1 25 QM-07 Batch 1126013 - NO PREP Blank (1326013-BLK1) Prepared: 10/26/2021 09:54 Analyzed: 10/29/2021 11:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (1326013-BS3) Prepared: 10/26/2021 09:54 Analyzed: 10/29/2021 11:54 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.2 0.10 mg/L 1.25 98 90-110 Matrix Spike (1326013-MS3) Prepared: 10/26/2021 09:54 Analyzed: 10/29/2021 12:08 Source: CE15555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 5.3 E 0.10 mg/L 0.521 4.9 61 90-110 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 29 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch IJ26013 - NO PREP - Continued Matrix Spike (1326013-MS2) Prepared: 10/26/2021 09:54 Analyzed: 10/29/2021 12:17 Source: CE15555-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.88 0.10 mg/L 0.521 0.35 102 90-110 Matrix Spike Dup (1726013-MSD1) Prepared: 10/26/2021 09:54 Analyzed: 10/29/2021 12:10 Source: CE35555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 5.4 E 0.10 mg/L 0.521 4.9 85 90-110 2 10 QM-07 Batch 1127021 - NO PREP Blank (1127021-BLK3) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (1327021-BS1) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 99 15 mg/L 100 99 80-120 Matrix Spike (1727021-MS3) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:12 Source: CE35554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 110 15 mg/L 37.8 60 140 80-120 QM-07 Matrix Spike Dup (1]27021-MSDi) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:12 Source: CE35554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 110 15 mg/L 37.8 60 137 80-120 1 25 QM-07 Batch IK01020 - NO PREP Blank (1K03020-BLKS) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (1K01020-BS3) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 100 15 mg/L 100 100 80-120 Matrix Spike (1K01020-MS3) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:14 Source: CE15194-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 88 15 mg/L 37.8 39 129 80-120 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 29 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1K01020 - NO PREP - Continued Matrix Spike Dup (1K01020-MSD1) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:15 Source: CE15194-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 89 15 mg/L 37.8 39 133 80-120 2 25 QM-07 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch IJ25015 - EPA 5030B MS Blank (1325015-BLK1) Prepared: 10/25/2021 00:00 Analyzed: 10/25/2021 08:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-& 5.4 ug/L 5.00 107 75-125 LCS (1725015-BS1) Prepared: 10/25/2021 00:00 Analyzed: 10/25/2021 08:33 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 109 80-133 Toluene-d8 5.7 ug/L 5.00 114 75-125 Matrix Spike (1325015-MS1) Prepared: 10/25/2021 00:00 Analyzed: 10/25/2021 18:04 Source: CE15555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 50 2.0 ug/L 25.0 25 101 80-133 Toluene-d8 5.4 u91L 5.00 108 75-125 Matrix Spike Dup (1725015-MSD1) Prepared: 10/25/2021 00:00 Analyzed: 10/25/2021 18:29 Source: CE35555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 50 2.0 ug/L 25.0 25 101 80-133 0.2 19 Toluene-d8 5.4 u91L 5.00 109 75-125 Dissolved Gases by GC - Quality Control Batch 1126005 - Same Blank (1326005-BLK3) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:34 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 2.07 U 2.50 mg/L Ethane 0.00510 U 0.00600 mg/L Ethene 0.00510 U 0.00600 mg/L Methane 0.00400 U 0.00500 mg/L LCS (1326005-BSI) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 46.0 2.50 mg/L 45.8 100 70-130 Ethane 0.321 0.00600 mg/L 0.323 99 70-130 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 29 QUALITY CONTROL DATA Dissolved Gases by GC - Quality Control Batch 1126005 - Same - Continued (� �Eo www.encolabs.com LCS (1326005-BSI) Continued Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Ethene 0.315 0.00600 mg/L 0.302 104 70-130 Methane 0.168 0.00500 mg/L 0.174 97 70-130 LCS Dup (1J26005-BSD1) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:19 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Carbon dioxide 50.3 2.50 mg/L 45.8 110 70-130 9 30 Ethane 0.353 0.00600 mg/L 0.323 109 70-130 9 30 Ethene 0.349 0.00600 mg/L 0.302 116 70-130 10 30 Methane 0.188 0.00500 mg/L 0.174 108 70-130 11 30 Duplicate (1326005-DUPl) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 13:37 Source: AE08472-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Carbon dioxide 22.1 2.50 mg/L 22.5 2 30 Ethane 0.00510 U 0.00600 mg/L 0.00510 U 30 Ethene 0.00510 U 0.00600 mg/L 0.00510 U 30 Methane 0.00400 U 0.00500 mg/L 0.00400 U 30 Classical Chemistry Parameters - Quality Control Batch 1126001 - NO PREP Blank (1326001-BLK1) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 09:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 0.90 U 1.0 mg/L LCS (1326001-BS3) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 09:43 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 49 1.0 mg/L 50.0 97 85-115 Matrix Spike (1J26001-MS3) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 10:24 Source: AE08470-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 51 1.0 mg/L 50.0 2.4 97 85-115 Matrix Spike (1J26001-MS2) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 18:44 Source: AE08497-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 52 1.0 mg/L 50.0 2.9 98 85-115 Matrix Spike Dup (1J26001-MSD1) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 10:47 Source: AE08470-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 50 1.0 mg/L 50.0 2.4 95 85-115 2 21 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 29 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1126001 - NO PREP - Continued Matrix Spike Dup (1326001-MSD2) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 19:08 Source: AE08497-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 51 1.0 mg/L 50.0 2.9 97 85-115 2 21 Batch V27005 - NO PREP Blank (1327005-BLK3) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 09:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 0.90 u 1.0 mg/L LCS (1327005-BSI) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 09:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 49 1.0 mg/L 50.0 99 85-115 Matrix Spike (1327005-MS3) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 10:33 Source: AE08497-02RE1 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 50 1.0 mg/L 50.0 3.1 95 85-115 Matrix Spike (1327005-MS2) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 18:34 Source: AE08497-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 55 1.0 mg/L 50.0 3.3 104 85-115 Matrix Spike Dup (1327005-MSDI) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 10:56 Source: AE08497-02REI Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 55 1.0 mg/L 50.0 3.1 104 85-115 9 21 Matrix Spike Dup (1327005-MSD2) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 18:57 Source: AE08497-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 36 1.0 mg/L 50.0 3.3 66 85-115 42 21 QM-07, QM-11 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 29 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test). QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 29 E LJ a) •o ° m z' o a �_ ca w E i n _ F8 NN w C CD . m `� X a>LOv� O U I.0 y ¢ a W D ff m m Q% i ? 4 ) C U) a 3 Z n *1�w ✓✓✓ @ J ` 0906 001 x >,I f t f x a S-O05tWS aR!MnS x x A x OO£ a;eAnS x x x = m U zoo } 9L � )qsa x x >x m Z'E9£ XON > x x x ff in 6H > x x > > x m fl% Tm N se aWlIN'OOE eR.JON3'Z-OLC AIIUIIIIIY x x X X > x m a> 0 C) — eS'gd'JO'p3'eg'SV'6y X x x X> x 70- al WIS C109Zs' 6 xlpueddd a09ZIR x x x V a � r 2 cc U U �\ LL pN � N JNWj w' 80 N .0 4 V C O 0 O z 18 m a D m o 4 �E w m E a a a o a rr _ m O N • O CCi a � - W co pN U v 1 yyn� co O LD LL� g C] U a k O `✓ CO R E CV _ m 2 (! CL p p m (o . CD CD CD CD CD v (1)90� �1 9 D co v m / Q m U 1 U C � C) n •� ❑ ❑ N a N V C Q c Al I •, ` "� 3 � -, ow v S ff a: E € E t a E E v a u vp 0 rm m h d y n a � C nE 7 C CE � C ff: W 8 v 00 � m � 2 m a Y G E ai E E 100 Sample Preservation Verification ■11■ ENCO Cary Work Order: CE15555 Project: Moore County Closed LFCA Client: S&ME, Inc. (SM004) Project #: 4358-20-043 Logged In: 19-Oct-21 14:05 Logged By: Rachel Ann Yonish Preservation Check Performed By: _ (126 Date/Time: U991-1 1 (A9t� CE15555-01 Cont Type y Pres (pH) Requirement pH Checked/ In Control Date/Time PH Adjusted Adjusted Reagent Used/Comments B 250mLP+HNO3 <2I. Y 1 N/ NA Y 1� N/ NA C 250mLP+ZnAc+NaOH >9 R@J Y N I NA D 250mLP+H2SO4 <2 Y/ NA CE15555-02 Gant Type Pres (pH) Requirement ,� pH Checked I ..._.In Control pH Adjusted DatefTime Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y 'l N I NA YNA C 250mLP+ZnAc+NaOH >9 Y/ N 1 NA Y 1W NA D 250mLP+H2SO4 <2 Y N / NA Y / N / NA CE15555-03 Cont Type Pres (pH) Requirement pH Checked / In Control Date/TimeYP PH Adjusted Adjusted Reagent Used/Comments B 250ml-P+-HNO3 <2 Y I N/ NA Y 1 N' 1 NA C 250mLP+ZnAc+NaOH >9 Y I N I NA Y 'N / NA D n0mLP+H2SO4 <2 YIN / NA Y N NA Rea ent Name ID b Rea ent Name ID 3 4 Reagent Name ID 5 6 pH Strip 1D: PH Strips COF0555 C:lelmnt\Prii ,,,,Yi%u_; 1 UQc1 YC2L1U1 nLi =L r,. i pt Page 1 of 1 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, November 10, 2021 S&ME, Inc. (SM004) Attn: Edmund Henriques 8646 West Market Street, Suite 105 Greensboro, NC 27409 RE: Laboratory Results for Project Number: 4358-20-043, Project Name/Desc: Moore County Closed LF CA ENCO Workorder(s): CE16209 Dear Edmund Henriques, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, October 20, 2021. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 0"6LC'=-:;tA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 37 PROJECT NARRATIVE Client: S&ME, Inc. (SM004) Project: Moore County Closed LF CA Lab ID: CE16209 Overview (� �Eo www.encolabs.com Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on an acceptable LCS recovery (QM-07). Precision between duplicate matrix spikes of the same sample was outside acceptance limits (QM-11). Quality Control Remarks The associated CCV standard exhibited high bias; since the result is ND, there is no impact (QV-01). Other Comments The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Chuck Smith Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 37 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW3 Lab ID: CE16209-01 Sampled: 10/19/21 11:40 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/21/21 22:53 EPA 353.2 NO PREP 10/21/21 11:40 10/20/21 15:44 10/20/21 16:59 EPA 353.2 [CALC] 10/21/21 11:40 10/26/21 09:55 10/29/21 13:34 EPA 353.2 NO PREP 11/16/21 10/26/21 09:55 10/29/21 13:34 EPA 6010D EPA 3005A 04/17/22 10/26/21 13:10 10/27/21 13:20 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:21 10/22/21 08:29 EPA 8260D EPA 5030B_MIS 11/02/21 10/25/21 10:26 10/26/21 04:20 EPA 8260D EPA 503013_MS 11/02/21 10/28/21 13:21 10/29/21 00:59 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 11:10 SM 4500S2 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MW1 Lab ID: CE16209-01RE1 Sampled: 10/19/21 11:40 Received: 10/20/21 10:20 Parameter Preoaration Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 11/02/21 11/01/21 09:50 11/01/21 12:30 EPA 9060A NO PREP 11/16/21 10/27/21 07:24 10/27/21 15:43 Client ID: 6301-MW6 Lab ID: CE16209-02 Sampled: 10/19/21 15:00 Received: 10/20/21 10:20 Parameter Preoaration Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/21/21 23:11 EPA 310.2 NO PREP 11/02/21 10/27/21 14:19 10/27/21 16:34 EPA 353.2 NO PREP 10/21/21 15:00 10/20/21 15:44 10/20/21 17:00 EPA 353.2 [CALC] 10/21/21 15:00 10/26/21 09:55 10/29/21 13:37 EPA 353.2 NO PREP 11/16/21 10/26/21 09:55 10/29/21 13:37 EPA 6010D EPA 3005A 04/17/22 10/26/21 13:10 10/27/21 13:45 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:21 10/22/21 08:34 EPA 8260D EPA 503013_MS 11/02/21 10/25/21 10:26 10/26/21 04:46 EPA 8260D EPA 503013_MS 11/02/21 10/28/21 13:21 10/29/21 01:29 EPA 9060A NO PREP 11/16/21 10/26/21 07:08 10/26/21 15:57 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 11:28 SM 4500S2 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MW6 Lab ID: CE16209-02RE1 Sampled: 10/19/21 15:00 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 11/02/21 11/01/21 13:31 11/01/21 22:18 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 14:25 Client ID: 6301-MW7 Lab ID: CE16209-03 Sampled: 10/19/21 14:35 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/21/21 23:28 EPA 310.2 NO PREP 11/02/21 10/27/21 14:18 10/27/21 16:23 EPA 353.2 NO PREP 10/21/21 14:35 10/20/21 15:44 10/20/21 17:00 EPA 353.2 [CALC] 10/21/21 14:35 10/26/21 09:55 10/29/21 13:38 EPA 353.2 NO PREP 11/16/21 10/26/21 09:55 10/29/21 13:38 EPA 6010D EPA 3005A 04/17/22 10/26/21 13:10 10/27/21 13:47 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:26 10/22/21 08:59 EPA 8260D EPA 503013_MS 11/02/21 10/25/21 10:26 10/26/21 05:11 EPA 8260D EPA 503013_MS 11/02/21 10/28/21 13:21 10/29/21 01:58 EPA 9060A NO PREP 11/16/21 10/26/21 07:08 10/26/21 17:00 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 11:44 SM 4500S2 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 37 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW7 Lab ID: CE16209-03RE3 Sampled: 10/19/21 14:35 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/02/21 11/01/21 13:31 11/01/21 22:47 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 14:41 Client ID: 6301-MW8 Lab ID: CE16209-04 Sampled: 10/19/21 16:15 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/21/21 23:46 EPA 310.2 NO PREP 11/02/21 10/27/21 14:18 10/27/21 16:24 EPA 353.2 NO PREP 10/21/21 16:15 10/20/21 15:44 10/20/21 17:01 EPA 353.2 [CALC] 10/21/21 16:15 10/26/21 09:55 10/29/21 13:39 EPA 353.2 NO PREP 11/16/21 10/26/21 09:55 10/29/21 13:39 EPA 6010D EPA 3005A 04/17/22 10/26/21 13:10 10/27/21 13:50 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:26 10/22/21 09:01 EPA 8260D EPA 503013_MS 11/02/21 10/25/21 10:26 10/26/21 05:37 EPA 8260D EPA 503013_MS 11/02/21 10/29/21 15:00 10/30/21 02:18 EPA 9060A NO PREP 11/16/21 10/26/21 07:08 10/26/21 17:22 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 12:00 SM 450052 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MW8 Lab ID: CE16209-04RE1 Sampled: 10/19/21 16:15 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/22/21 07:11 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 14:57 Client ID: 6301-MW9 Lab ID: CE16209-05 Sampled: 10/19/21 13:15 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/22/21 00:04 EPA 310.2 NO PREP 11/02/21 10/27/21 14:18 10/27/21 16:26 EPA 353.2 NO PREP 10/21/21 13:15 10/20/21 15:44 10/20/21 17:03 EPA 353.2 [CALC] 10/21/21 13:15 10/26/21 09:55 10/29/21 13:40 EPA 353.2 NO PREP 11/16/21 10/26/21 09:55 10/29/21 13:40 EPA 6010D EPA 3005A 04/17/22 10/26/21 13:10 10/27/21 13:52 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:26 10/22/21 09:03 EPA 8260D EPA 503013_MS 11/02/21 10/25/21 10:26 10/26/21 06:03 EPA 8260D EPA 5030B_MIS 11/02/21 10/29/21 15:00 10/30/21 02:46 EPA 9060A NO PREP 11/16/21 10/26/21 07:08 10/26/21 17:44 RSK 175 Same 11/02/21 10/26/21 08:00 10/26/21 12:16 SM 450052 D-2011 NO PREP 10/26/21 10/22/21 09:58 10/22/21 10:16 Client ID: 6301-MW9 Lab ID: CE16209-OSRE1 Sampled: 10/19/21 13:15 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/16/21 10/21/21 06:21 10/22/21 07:28 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 37 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW3 Lab ID: CE16209-01 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 23.7 1.10 10.0 ug/L EPA 6010D Carbon dioxide 60.2 2.07 2.50 mg/L RSK 175 Chloride 2.7 3 2.2 5.0 mg/L EPA 300.0 Nitrate as N 0.76 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.76 0.041 0.10 mg/L EPA 353.2 Sulfate as SO4 8.6 2.9 5.0 mg/L EPA 300.0 Client ID: 6301-MW3 Lab ID: CE16209-01RE1 Analvte Results Flag MDL PQL Units Method Notes Total Organic Carbon 1.3 0.90 1.0 mg/L EPA 9060A Client ID: 6301-MW6 Lab ID: CE16209-02 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 0.41 3 0.13 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 1.5 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 1.8 3 0.80 2.0 ug/L EPA 8260D Barium - Total 42.3 1.10 10.0 ug/L EPA 6010D Chloride 13 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.7 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 2.2 0.15 1.0 ug/L EPA 8260D Nitrate as N 0.12 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.12 0.041 0.10 mg/L EPA 353.2 Sulfate as SO4 6.5 2.9 5.0 mg/L EPA 300.0 Sulfide 0.19 0.010 0.10 mg/L SM 4500S2 D-2011 Toluene 0.61 3 0.14 1.0 ug/L EPA 8260D Total Alkalinity as CaCO3 210 D 70 75 mg/L EPA 310.2 Total Organic Carbon 18 0.90 1.0 mg/L EPA 9060A Client ID: 6301-MW6 Lab ID: CE16209-02RE1 Analvte Results Flag MDL PQL Units Method Notes Acetone 27 10 20 ug/L EPA 8260D Benzene 1.6 0.15 1.0 ug/L EPA 8260D Carbon dioxide 239 D 145 175 mg/L RSK 175 Methane 2.84 D 0.280 0.350 mg/L RSK 175 Vinyl chloride 1.2 0.32 1.0 uq/L EPA 8260D I Client ID: 6301-MW7 Lab ID: CE16209-03 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 0.84 3 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 6.3 0.80 2.0 ug/L EPA 8260D Barium - Total 33.6 1.10 10.0 ug/L EPA 6010D Chloride 25 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.9 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 0.98 3 0.15 1.0 ug/L EPA 8260D Nitrate as N 0.14 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.14 0.041 0.10 mg/L EPA 353.2 Sulfide 0.46 0.010 0.10 mg/L SM 4500S2 D-2011 Toluene 1.3 0.14 1.0 ug/L EPA 8260D Total Alkalinity as CaCO3 89 D 70 75 mg/L EPA 310.2 Total Organic Carbon 28 0.90 1.0 mg/L EPA 9060A Client ID: 6301-MW7 Lab ID: CE16209-03RE1 Analvte Results Flag MDL PQL Units Method Notes 2-Butanone 9.3 1.3 5.0 ug/L EPA 8260D Acetone 270 10 20 ug/L EPA 8260D Benzene 1.1 0.15 1.0 ug/L EPA 8260D Carbon dioxide 243 D 108 130 mg/L RSK 175 Methane 2.78 D 0.208 0.260 mg/L RSK 175 Vinyl chloride 1.6 0.32 1.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 37 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW8 Lab ID: CE16209-04 Analvte Results Flag MDL Q Units Method Notes 1,2-Dichlorobenzene 0.91 3 0.19 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 5.1 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 48 0.80 2.0 ug/L EPA 8260D Barium - Total 80.0 1.10 10.0 ug/L EPA 6010D Benzene 2.1 0.15 1.0 ug/L EPA 8260D Chlorobenzene 6.7 0.17 1.0 ug/L EPA 8260D Nitrate as N 0.094 3 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.094 3 0.041 0.10 mg/L EPA 353.2 Sulfide 0.14 0.010 0.10 mg/L SM 4500S2 D-2011 Toluene 0.67 3 0.14 1.0 ug/L EPA 8260D Total Alkalinity as CaCO3 310 D 70 75 mg/L EPA 310.2 Total Organic Carbon 26 0.90 1.0 mg/L EPA 9060A Client ID: 6301-MW8 Lab ID: CE16209-04RE3 Analvte Results Flag MDL Q Units Method Notes Carbon dioxide 314 D 72.4 87.5 mg/L RSK 175 Chloride 110 D 4.4 10 mg/L EPA 300.0 Methane 3.93 D 0.140 0.175 mg/L RSK 175 Client ID: 6301-MW9 Lab ID: CE16209-05 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 34 0.80 2.0 ug/L EPA 8260D Arsenic - Total 43.9 7.60 10.0 ug/L EPA 6010D Barium - Total 99.9 1.10 10.0 ug/L EPA 6010D Benzene 2.2 0.15 1.0 ug/L EPA 8260D Carbon dioxide 179 2.07 2.50 mg/L RSK 175 Chloride 120 D 4.4 10 mg/L EPA 300.0 Chlorobenzene 6.2 0.17 1.0 ug/L EPA 8260D Methane 0.517 0.00400 0.00500 mg/L RSK 175 Nitrate as N 0.10 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.10 0.041 0.10 mg/L EPA 353.2 Sulfide 0.30 0.010 0.10 mg/L SM 4500S2 D-2011 Toluene 0.52 3 0.14 1.0 ug/L EPA 8260D Total Alkalinity as CaCO3 900 D 70 75 mg/L EPA 310.2 Total Organic Carbon 39 0.90 1.0 mg/L EPA 9060A FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 37 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW1 Lab Sample ID:CE16209-01 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 11:40 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1128031 EPA 8260D 10/29/21 00:59 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 Acetone [67-64-1]A 10 u ug/L 1 10 20 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1128031 EPA 8260D 10/29/21 00:59 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1128031 EPA 8260D 10/29/21 00:59 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 Vinyl chloride [75-01-4]^ 0.32 u ug/L 1 0.32 1.0 1128031 EPA 8260D 10/29/21 00:59 RKY QV-01 Xylenes (Total) [1330-20-7]A 0.45 Ll ug/L 1 0.45 3.0 1128031 EPA 8260D 10/29/21 00:59 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 37 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW1 Lab Sample ID:CE16209-01 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 11:40 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 51 1 50.0 102 % 53-136 V28031 EPA 6260D 10129121 00:59 RKY Dibromofluoromethane 50 1 50.0 99 % 67-129 V28031 EPA 6260D 10129121 00:59 RKY Toluene-d8 52 1 50.0 103 % 59-134 V28031 EPA 6260D 10129121 00:59 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:29 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J26004 EPA 6010D 10/27/21 13:20 JDH Barium [7440-39-3]^ 23.7 ug/L 1 1.10 10.0 1126004 EPA 6010D 10/27/21 13:20 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J26004 EPA 6010D 10/27/21 13:20 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:20 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J26004 EPA 6010D 10/27/21 13:20 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J26004 EPA 6010D 10/27/21 13:20 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J26004 EPA 6010D 10/27/21 13:20 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 2.7 J mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 22:53 ZGW Nitrate as N [14797-55-8] 0.76 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/29/21 13:34 JAH Nitrate/Nitrite as N^ 0.76 mg/L 1 0.041 0.10 1126014 EPA 353.2 10/29/21 13:34 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1J20032 EPA 353.2 10/20/21 16:59 JAH Sulfate as SO4 [14808-79-8]^ 8.6 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/21/21 22:53 ZGW Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 1J22004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 14 U mg/L 1 14 15 1KO1020 EPA 310.2 11/01/21 12:30 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J25020 EPA 8260D 10/26/21 04:20 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.3 1 5.00 105 % 75-125 V25020 EPA 8260D 10126121 04:20 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 37 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW1 Lab Sample ID:CE16209-01 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 11:40 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By: James Waters Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 60.2 mg/L 1 2.07 2.50 1326005 RSK 175 10/26/21 11:10 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 11:10 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 11:10 JMW Methane [74-82-8] 0.00400 U mg/L 1 0.00400 0.00500 1J26005 RSK 175 10/26/21 11:10 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Total Organic Carbon^ 1.3 mg/L 1 0.90 1.0 1327005 EPA 9060A 10/27/21 15:43 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 37 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW6 Lab Sample ID:CE16209-02 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 15:00 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY 1,1-Dichloroethane [75-34-3]A 0.41 J ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY 1,4-Dichlorobenzene [306-46-7]^ 1.5 ug/L 1 0.19 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1128031 EPA 8260D 10/29/21 01:29 RKY QV-01 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1128031 EPA 8260D 10/29/21 01:29 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1128031 EPA 8260D 10/29/21 01:29 RKY QV-01 Acetone [67-64-1]A 27 ug/L 1 10 20 IK01035 EPA 8260D 11/01/21 22:18 ref Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1128031 EPA 8260D 10/29/21 01:29 RKY QV-01 Benzene [71-43-2]A 1.6 ug/L 1 0.15 1.0 IK01035 EPA 8260D 11/01/21 22:18 ref Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1128031 EPA 8260D 10/29/21 01:29 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Chlorobenzene [108-90-7]A 1.7 ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY QV-01 Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY cis-1,2-Dichloroethene [156-59-2]A 2.2 ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1128031 EPA 8260D 10/29/21 01:29 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY QV-01 Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Toluene [108-88-3]A 0.61 J ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY QV-01 Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1128031 EPA 8260D 10/29/21 01:29 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1128031 EPA 8260D 10/29/21 01:29 RKY QV-01 Vinyl chloride [75-01-4]A 1.2 ug/L 1 0.32 1.0 IK01035 EPA 8260D 11/01/21 22:18 ref Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1128031 EPA 8260D 10/29/21 01:29 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 37 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW6 Lab Sample ID:CE16209-02 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 15:00 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 51 1 50.0 101 % 53-136 V28031 EPA 6260D 10129121 01:29 RKY 4-Bromofluorobenzene 54 1 50.0 108 % 53-136 IK01035 EPA 6260D 11101121 22:18 ref Dibromofluoromethane 50 1 50.0 101 % 67-129 V28031 EPA 6260D 10129121 01:29 RKY Dibromofluoromethane 57 1 50.0 114 % 67-129 IK01035 EPA 6260D 11101121 22:18 ref Toluene-d8 51 1 50.0 103 % 59-134 V28031 EPA 8260D 10129121 01:29 RKY Toluene-d8 58 1 50.0 116 % 59-134 IK01035 EPA 8260D 11101121 22:18 ref Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:34 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J26004 EPA 6010D 10/27/21 13:45 JDH Barium [7440-39-3]^ 42.3 ug/L 1 1.10 10.0 1126004 EPA 6010D 10/27/21 13:45 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J26004 EPA 6010D 10/27/21 13:45 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:45 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J26004 EPA 6010D 10/27/21 13:45 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J26004 EPA 6010D 10/27/21 13:45 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J26004 EPA 6010D 10/27/21 13:45 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 13 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 23:11 ZGW Nitrate as N [14797-55-8] 0.12 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/29/21 13:37 JAH Nitrate/Nitrite as N^ 0.12 mg/L 1 0.041 0.10 1126014 EPA 353.2 10/29/21 13:37 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1J20032 EPA 353.2 10/20/21 17:00 JAH Sulfate as SO4 [14808-79-B]^ 6.5 mg/L 1 2.9 5.0 1121002 EPA 300.0 10/21/21 23:11 ZGW Sulfide [18496-25-8]^ 0.19 mg/L 1 0.010 0.10 1122004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 210 D mg/L 5 70 75 1127022 EPA 310.2 10/27/21 16:34 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.8 J ug/L 1 0.80 2.0 1125020 EPA 8260D 10/26/21 04:46 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.2 1 5.00 104 % 75-125 V25020 EPA 8260D 10126121 04:46 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 37 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW6 Lab Sample ID:CE16209-02 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 15:00 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By: James Waters Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 239 D mg/L 70 145 175 1326005 RSK 175 10/26/21 14:25 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 11:28 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 11:28 JMW Methane [74-82-8] 2.84 D mg/L 70 0.280 0.350 1326005 RSK 175 10/26/21 14:25 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 18 mg/L 1 0.90 1.0 1326001 EPA 9060A 10/26/21 15:57 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 37 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW7 Lab Sample ID:CE16209-03 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 14:35 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY QV-01 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY 1,4-Dichlorobenzene [106-46-7]A 0.84 J ug/L 1 0.19 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY 2-Butanone [78-93-3]A 9.3 ug/L 1 1.3 5.0 IK01035 EPA 8260D 11/01/21 22:47 ref 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1128031 EPA 8260D 10/29/21 01:58 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 1128031 EPA 8260D 10/29/21 01:58 RKY QV-01 Acetone [67-64-1]A 270 ug/L 1 10 20 IK01035 EPA 8260D 11/01/21 22:47 ref Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 1128031 EPA 8260D 10/29/21 01:58 RKY QV-01 Benzene [71-43-2]A 1.1 ug/L 1 0.15 1.0 IK01035 EPA 8260D 11/01/21 22:47 ref Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 1128031 EPA 8260D 10/29/21 01:58 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Chlorobenzene [108-90-7]A 1.9 ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY QV-01 Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY cis-1,2-Dichloroethene [156-59-2]A 0.98 J ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 1128031 EPA 8260D 10/29/21 01:58 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY QV-01 Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Toluene [108-88-3]A 1.3 ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY QV-01 Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 1128031 EPA 8260D 10/29/21 01:58 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 1128031 EPA 8260D 10/29/21 01:58 RKY QV-01 Vinyl chloride [75-01-4]A 1.6 ug/L 1 0.32 1.0 IK01035 EPA 8260D 11/01/21 22:47 ref Xylenes (Total) [1330-20-7]A 0.45 U ug/L 1 0.45 3.0 1128031 EPA 8260D 10/29/21 01:58 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 37 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW7 Lab Sample ID:CE16209-03 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 14:35 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 100 % 53-136 V28031 EPA 6260D 10129121 01:58 RKY 4-Bromofluorobenzene 53 1 50.0 106 % 53-136 IK01035 EPA 6260D 11101121 22:47 ref Dibromofluoromethane 50 1 50.0 99 % 67-129 V28031 EPA 6260D 10129121 01:58 RKY Dibromofluoromethane 56 1 50.0 112 % 67-129 IK01035 EPA 6260D 11101121 22:47 ref Toluene-d8 52 1 50.0 104 % 59-134 V28031 EPA 6260D 10129121 01:58 RKY Toluene-d8 59 1 50.0 117 % 59-134 IK01035 EPA 6260D 11101121 22:47 ref Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20029 EPA 7470A 10/22/21 08:59 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J26004 EPA 6010D 10/27/21 13:47 JDH Barium [7440-39-3]^ 33.6 ug/L 1 1.10 10.0 1126004 EPA 6010D 10/27/21 13:47 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J26004 EPA 6010D 10/27/21 13:47 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:47 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J26004 EPA 6010D 10/27/21 13:47 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J26004 EPA 6010D 10/27/21 13:47 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J26004 EPA 6010D 10/27/21 13:47 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 25 mg/L 1 2.2 5.0 1121002 EPA 300.0 10/21/21 23:28 ZGW Nitrate as N [14797-55-8] 0.14 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/29/21 13:38 JAH Nitrate/Nitrite as N^ 0.14 mg/L 1 0.041 0.10 1126014 EPA 353.2 10/29/21 13:38 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1J20032 EPA 353.2 10/20/21 17:00 JAH Sulfate as SO4 [14808-79-8]^ 2.9 U mg/L 1 2.9 5.0 1J21002 EPA 300.0 10/21/21 23:28 ZGW Sulfide [18496-25-8]^ 0.46 mg/L 1 0.010 0.10 1122004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 89 D mg/L 5 70 75 1127021 EPA 310.2 10/27/21 16:23 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 6.3 ug/L 1 0.80 2.0 1125020 EPA 8260D 10/26/21 05:11 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes Toluene-d8 5.6 1 5.00 112 % 75-125 V25020 EPA 8260D 10126121 05:11 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 37 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW7 Lab Sample ID:CE16209-03 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 14:35 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By: James Waters Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 243 D mg/L 52 108 130 1326005 RSK 175 10/26/21 14:41 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 11:44 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 11:44 JMW Methane [74-82-8] 2.78 D mg/L 52 0.208 0.260 1326005 RSK 175 10/26/21 14:41 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 28 mg/L 1 0.90 1.0 1326001 EPA 9060A 10/26/21 17:00 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 37 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW8 Lab Sample ID:CE16209-04 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 16:15 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,2-Dichlorobenzene [95-50-1]A 0.91 J ug/L 1 0.19 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 1,4-Dichlorobenzene [106-46-7]^ 5.1 ug/L 1 0.19 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 1129020 EPA 8260D 10/30/21 02:18 RKY 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 1129020 EPA 8260D 10/30/21 02:18 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1129020 EPA 8260D 10/30/21 02:18 RKY Acetone [67-64-1]^ 10 u ug/L 1 10 20 1129020 EPA 8260D 10/30/21 02:18 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1129020 EPA 8260D 10/30/21 02:18 RKY Benzene [71-43-2]A 2.1 ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 1129020 EPA 8260D 10/30/21 02:18 RKY Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Chlorobenzene [108-90-7]A 6.7 ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Chloroethane [75-00-3]^ 0.23 u ug/L 1 0.23 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Ethylbenzene [100-41-4]^ 0.13 u ug/L 1 0.13 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1129020 EPA 8260D 10/30/21 02:18 RKY Methylene chloride [75-09-2]^ 0.23 u ug/L 1 0.23 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Styrene [100-42-5]^ 0.11 u ug/L 1 0.11 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Toluene [108-88-3]A 0.67 J ug/L 1 0.14 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 1129020 EPA 8260D 10/30/21 02:18 RKY Vinyl chloride [75-01-4]^ 0.32 u ug/L 1 0.32 1.0 1129020 EPA 8260D 10/30/21 02:18 RKY Xylenes (Total) [1330-20-7]^ 0.45 Ll ug/L 1 0.45 3.0 1129020 EPA 8260D 10/30/21 02:18 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 37 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW8 Lab Sample ID:CE16209-04 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 16:15 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 61 1 50.0 123 % 53-136 IJ29020 EPA 6260D 10130121 02:18 RKY Dibromofluoromethane 48 1 50.0 96 % 67-129 IJ29020 EPA 6260D 10130121 02:18 RKY Toluene-d8 52 1 50.0 104 % 59-134 IJ29020 EPA 6260D 10130121 02:18 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20029 EPA 7470A 10/22/21 09:01 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J26004 EPA 6010D 10/27/21 13:50 JDH Barium [7440-39-3]^ 80.0 ug/L 1 1.10 10.0 1126004 EPA 6010D 10/27/21 13:50 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J26004 EPA 6010D 10/27/21 13:50 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:50 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J26004 EPA 6010D 10/27/21 13:50 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J26004 EPA 6010D 10/27/21 13:50 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J26004 EPA 6010D 10/27/21 13:50 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 110 D mg/L 2 4.4 10 1121002 EPA 300.0 10/22/21 07:11 ZGW Nitrate as N [14797-55-8] 0.094 J mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/29/21 13:39 JAH Nitrate/Nitrite as N^ 0.094 J mg/L 1 0.041 0.10 1126014 EPA 353.2 10/29/21 13:39 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1J20032 EPA 353.2 10/20/21 17:01 JAH Sulfate as SO4 [14808-79-8]^ 2.9 U mg/L 1 2.9 5.0 1J21002 EPA 300.0 10/21/21 23:46 ZGW Sulfide [18496-25-8]^ 0.14 mg/L 1 0.010 0.10 1122004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 310 D mg/L 5 70 75 1127021 EPA 310.2 10/27/21 16:24 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 48 ug/L 1 0.80 2.0 1125020 EPA 8260D 10/26/21 05:37 KKW Surrogates Toluene-d8 Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes 4.9 1 5.00 98 % 75-125 IJ25020 EPA 8260D 10126121 0527 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 37 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW8 Lab Sample ID:CE16209-04 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 16:15 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By: James Waters Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 314 D mg/L 35 72.4 87.5 1326005 RSK 175 10/26/21 14:57 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 12:00 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 12:00 JMW Methane [74-82-8] 3.93 D mg/L 35 0.140 0.175 1326005 RSK 175 10/26/21 14:57 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 26 mg/L 1 0.90 1.0 1326001 EPA 9060A 10/26/21 17:22 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 37 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW9 Lab Sample ID:CE16209-05 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 13:15 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By:James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 u ug/L 1 0.23 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 u ug/L 1 0.48 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,2-Dibromoethane [106-93-4]A 0.66 u ug/L 1 0.66 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 u ug/L 1 0.19 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,2-Dichloroethane [107-06-2]A 0.21 u ug/L 1 0.21 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,2-Dichloropropane [78-87-5]A 0.10 u ug/L 1 0.10 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 u ug/L 1 0.19 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1129020 EPA 8260D 10/30/21 02:46 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1129020 EPA 8260D 10/30/21 02:46 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 u ug/L 1 1.1 5.0 1129020 EPA 8260D 10/30/21 02:46 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1129020 EPA 8260D 10/30/21 02:46 RKY Acrylonitrile [107-13-1]A 3.5 u ug/L 1 3.5 10 1129020 EPA 8260D 10/30/21 02:46 RKY Benzene [71-43-2]A 2.2 ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Bromoform [75-25-2]A 0.22 u ug/L 1 0.22 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1129020 EPA 8260D 10/30/21 02:46 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Chlorobenzene [108-90-7]A 6.2 ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Chloroform [67-66-3]A 0.18 u ug/L 1 0.18 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY cis-1,2-Dichloroethene [156-59-2]A 0.15 u ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Iodomethane [74-88-4]A 1.7 u ug/L 1 1.7 5.0 1129020 EPA 8260D 10/30/21 02:46 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Toluene [108-88-3]A 0.52 J ug/L 1 0.14 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 u ug/L 1 0.21 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Trichloroethene [79-01-6]A 0.15 u ug/L 1 0.15 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Trichlorofluoromethane [75-69-4]A 0.24 u ug/L 1 0.24 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1129020 EPA 8260D 10/30/21 02:46 RKY Vinyl chloride [75-01-4]A 0.32 u ug/L 1 0.32 1.0 1129020 EPA 8260D 10/30/21 02:46 RKY Xylenes (Total) [1330-20-7]A 0.45 Ll ug/L 1 0.45 3.0 1129020 EPA 8260D 10/30/21 02:46 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 37 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW9 Lab Sample ID:CE16209-05 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 13:15 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By: James Waters Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 61 1 50.0 122 % 53-136 IJ29020 EPA 6260D 10130121 02:46 RKY Dibromofluoromethane 48 1 50.0 97 % 67-129 IJ29020 EPA 6260D 10130121 02:46 RKY Toluene-d8 48 1 50.0 96 % 59-134 IJ29020 EPA 6260D 10130121 02:46 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20029 EPA 7470A 10/22/21 09:03 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic [7440-38-2]^ 43.9 ug/L 1 7.60 10.0 1126004 EPA 6010D 10/27/21 13:52 JDH Barium [7440-39-3]^ 99.9 ug/L 1 1.10 10.0 1126004 EPA 6010D 10/27/21 13:52 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J26004 EPA 6010D 10/27/21 13:52 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:52 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J26004 EPA 6010D 10/27/21 13:52 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J26004 EPA 6010D 10/27/21 13:52 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J26004 EPA 6010D 10/27/21 13:52 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 120 D mg/L 2 4.4 10 1121002 EPA 300.0 10/22/21 00:04 ZGW Nitrate as N [14797-55-8] 0.10 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/29/21 13:40 JAH Nitrate/Nitrite as N^ 0.10 mg/L 1 0.041 0.10 1126014 EPA 353.2 10/29/21 13:40 JAH Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 1J20032 EPA 353.2 10/20/21 17:03 JAH Sulfate as SO4 [14808-79-8]^ 2.9 U mg/L 1 2.9 5.0 1J21002 EPA 300.0 10/22/21 07:28 ZGW Sulfide [18496-25-8]^ 0.30 mg/L 1 0.010 0.10 1122004 iM 4500S2 D-2011 10/22/21 10:16 JOC Total Alkalinity as CaCO3 [471-34-1]^ 900 D mg/L 5 70 75 1127021 EPA 310.2 10/27/21 16:26 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 34 ug/L 1 0.80 2.0 1125020 EPA 8260D 10/26/21 06:03 KKW Surrogates Toluene-d8 Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes 5.6 1 5.00 113 % 75-125 IJ25020 EPA 8260D 10126121 06:03 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 37 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW9 Lab Sample ID:CE16209-05 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 13:15 Work Order: CE16209 Project: Moore County Closed LF CA Sampled By: James Waters Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 179 mg/L 1 2.07 2.50 1326005 RSK 175 10/26/21 12:16 JMW Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 12:16 JMW Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 1J26005 RSK 175 10/26/21 12:16 JMW Methane [74-82-8] 0.517 mg/L 1 0.00400 0.00500 1326005 RSK 175 10/26/21 12:16 JMW Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 39 mg/L 1 0.90 1.0 1326001 EPA 9060A 10/26/21 17:44 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 37 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1128031 - EPA 5030B MS Blank (1328031-BLK1) Prepared: 10/28/2021 13:21 Analyzed: 10/28/2021 17:38 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 50 u91L 50.0 100 53-136 Dibromofluoromethane 49 u91L 50.0 99 67-129 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 37 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1128031 - EPA 5030B MS - Continued Blank (1328031-BLK1) Continued Prepared: 10/28/2021 13:21 Analyzed: 10/28/2021 17:38 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Toluene-d8 51 u91L 50.0 102 59-134 LCS (1328031-BS1) Prepared: 10/28/2021 13:21 Analyzed: 10/28/2021 15:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 117 75-133 Benzene 24 1.0 ug/L 20.0 120 80-134 Chlorobenzene 19 1.0 ug/L 20.0 94 80-120 Toluene 19 1.0 ug/L 20.0 96 71-120 Trichloroethene 22 1.0 ug/L 20.0 108 74-120 Matrix Spike (1328031-MS1) Prepared: 10/28/2021 13:21 Analyzed: 10/28/2021 16:09 Source: CE16465-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 26 1.0 ug/L 20.0 0.21 U 132 75-133 Benzene 26 1.0 ug/L 20.0 0.15 U 130 80-134 Chlorobenzene 21 1.0 ug/L 20.0 0.17 U 103 80-120 Toluene 21 1.0 ug/L 20.0 0.14 U 106 71-120 Trichloroethene 24 1.0 ug/L 20.0 0.15 U 119 74-120 Matrix Spike Dup (1328031-MSD1) Prepared: 10/28/2021 13:21 Analyzed: 10/28/2021 16:38 Source: CE16465-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 106 75-133 22 20 QM-11 Benzene 23 1.0 ug/L 20.0 0.15 U 115 80-134 12 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 94 80-120 9 16 Toluene 19 1.0 ug/L 20.0 0.14 U 95 71-120 11 17 Trichloroethene 21 1.0 ug/L 20.0 0.15 U 104 74-120 14 22 Batch 1129020 - EPA 5030E MS Blank (1329020-BLK3) Prepared: 10/29/2021 15:00 Analyzed: 10/29/2021 18:58 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 37 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IJ29020 - EPA 5030B MS - Continued Blank (1329020-BLK1) Continued Prepared: 10/29/2021 15:00 Analyzed: 10/29/2021 18:58 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 59 u9/L 50.0 119 53-136 Dibromofluoromethane 56 u9/L 50.0 115 67-129 Toluene-d8 52 u9/L 50.0 104 59-134 LCS (1329020-BSI) Prepared: 10/29/2021 15:00 Analyzed: 10/29/2021 17:07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 96 75-133 Benzene 17 1.0 ug/L 20.0 86 80-134 Chlorobenzene 18 1.0 ug/L 20.0 92 80-120 Toluene 21 1.0 ug/L 20.0 107 71-120 Trichloroethene 19 1.0 ug/L 20.0 95 74-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 37 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1129020 - EPA 5030B MS - Continued Matrix Spike (1329020-MS3) Prepared: 10/29/2021 15:00 Analyzed: 10/29/2021 17:35 Source: CE16465-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 98 75-133 Benzene 20 1.0 ug/L 20.0 0.15 U 100 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 100 80-120 Toluene 23 1.0 ug/L 20.0 0.14 U 114 71-120 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 99 74-120 Matrix Spike Dup (1329020-MSD1) Prepared: 10/29/2021 15:00 Analyzed: 10/29/2021 18:03 Source: CE16465-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 97 75-133 1 20 Benzene 18 1.0 ug/L 20.0 0.15 U 88 80-134 12 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 95 80-120 4 16 Toluene 23 1.0 ug/L 20.0 0.14 U 115 71-120 0.3 17 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 96 74-120 3 22 Batch 1KO1035 - EPA 5030E MS Blank (1K03035-BLK1) Prepared: 11/01/2021 13:31 Analyzed: 11/01/2021 17:39 Analvte Result Flaq POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 37 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1 K01035 - EPA 5030B MS - Continued (� �Eo www.encolabs.com Blank (SK03035-BLKS) Continued Prepared: 11/01/2021 13:31 Analyzed: 11/01/2021 17:39 Analvte Result Flaq POL Units cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 46 u91L 50.0 93 53-136 Dibromofluoromethane 41 u91L 50.0 61 67-129 Toluene-d8 44 u91L 50.0 87 59-134 LCS (iK01035-BS1) Prepared: 11/01/2021 13:31 Analyzed: 11/01/2021 15:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 107 75-133 Benzene 20 1.0 ug/L 20.0 102 80-134 Chlorobenzene 19 1.0 ug/L 20.0 95 80-120 Toluene 19 1.0 ug/L 20.0 96 71-120 Trichloroethene 19 1.0 ug/L 20.0 97 74-120 Matrix Spike (1K01035-MS1) Prepared: 11/01/2021 13:31 Analyzed: 11/01/2021 16:18 Source: CE16332-05 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 99 D 5.0 ug/L 100 1.0 U 99 75-133 Benzene 390 D 5.0 ug/L 100 310 81 80-134 Chlorobenzene 120 D 5.0 ug/L 100 37 78 80-120 QM-07 Toluene 110 D 5.0 ug/L 100 23 88 71-120 Trichloroethene 96 D 5.0 ug/L 100 0.75 U 96 74-120 Matrix Spike Dup (1K01035-MSD1) Prepared: 11/01/2021 13:31 Analyzed: 11/01/2021 16:45 Source: CE16332-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 110 D 5.0 ug/L 100 1.0 U 109 75-133 10 20 Benzene 420 D 5.0 ug/L 100 310 106 80-134 6 17 Chlorobenzene 130 D 5.0 ug/L 100 37 90 80-120 10 16 Toluene 120 D 5.0 ug/L 100 23 100 71-120 10 17 Trichloroethene 100 D 5.0 ug/L 100 0.75 U 103 74-120 7 22 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 37 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch V20028 - EPA 245.1 Blank (1320028-BLK3) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:33 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L Blank (1320028-BLK2) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:35 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 3.00 U 4.00 ug/L LCS (1320028-BS1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.46 0.200 ug/L 5.00 109 80-120 Matrix Spike (1320028-MS1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:44 Source: CE15555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.96 0.200 ug/L 5.00 0.150 U 99 75-125 Matrix Spike Dup (1320028-MSD1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:46 Source: CE15555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.99 0.200 ug/L 5.00 0.150 U 100 75-125 0.8 25 Post Spike (1320028-PS1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:48 Source: CE15555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.02 0.200 ug/L 4.76-0.000286 105 75-125 Batch V20029 - EPA 245.1 Blank (1320029-BLK3) Prepared: 10/20/2021 15:26 Analyzed: 10/22/2021 08:40 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L LCS (1320029-BSI) Prepared: 10/20/2021 15:26 Analyzed: 10/22/2021 08:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.07 0.200 ug/L 5.00 101 80-120 Matrix Spike (1320029-MS1) Prepared: 10/20/2021 15:26 Analyzed: 10/22/2021 08:45 Source: CE16213-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.79 0.200 ug/L 5.00 0.150 U 96 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 37 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch 1120029 - EPA 245.1 - Continued Matrix Spike Dup (1320029-MSDI) Prepared: 10/20/2021 15:26 Analyzed: 10/22/2021 08:47 Source: CE16213-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.99 0.200 ug/L 5.00 0.150 U 100 75-125 4 25 Post Spike (1320029-PS1) Prepared: 10/20/2021 15:26 Analyzed: 10/22/2021 08:49 Source: CE16213-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.53 0.200 ug/L 4.76 0.00533 116 75-125 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch V26004 - EPA 3005A Blank (1326004-BLK3) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Lead 3.10 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L LCS (1326004-BSI) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 201 10.0 ug/L 200 100 80-120 Barium 203 10.0 ug/L 200 101 80-120 Cadmium 20.0 1.00 ug/L 20.0 100 80-120 Chromium 196 10.0 ug/L 200 98 80-120 Lead 198 10.0 ug/L 200 99 80-120 Selenium 201 10.0 ug/L 200 101 80-120 Silver 197 10.0 ug/L 200 99 80-120 Matrix Spike (1326004-MS1) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:14 Source: CE15202-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 193 10.0 ug/L 200 7.60 U 97 75-125 Barium 241 10.0 ug/L 200 45.7 97 75-125 Cadmium 19.1 1.00 ug/L 20.0 0.360 U 96 75-125 Chromium 190 10.0 ug/L 200 1.40 U 95 75-125 Lead 193 10.0 ug/L 200 3.10 U 97 75-125 Selenium 189 10.0 ug/L 200 6.20 U 95 75-125 Silver 191 10.0 ug/L 200 1.90 U 95 75-125 Matrix Spike Dup (1326004-MSD1) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:16 Source: CE15202-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 192 10.0 ug/L 200 7.60 U 96 75-125 0.9 20 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 37 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1126004 - EPA 3005A - Continued Matrix Spike Dup (1326004-MSDI) Continued Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:16 Source: CE15202-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Barium 243 10.0 ug/L 200 45.7 98 75-125 0.8 20 Cadmium 19.5 1.00 ug/L 20.0 0.360 U 97 75-125 2 20 Chromium 192 10.0 ug/L 200 1.40 U 96 75-125 1 20 Lead 193 10.0 ug/L 200 3.10 U 97 75-125 0.03 20 Selenium 195 10.0 ug/L 200 6.20 U 97 75-125 3 20 Silver 194 10.0 ug/L 200 1.90 U 97 75-125 2 20 Post Spike (1326004-PS3) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:19 Source: CE15202-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.195 0.0100 mg/L 0.200 0.00236 96 80-120 Barium 0.245 0.0100 mg/L 0.200 0.0457 100 80-120 Cadmium 0.0198 0.00100 mg/L 0.0200 2.87E-5 99 80-120 Chromium 0.195 0.0100 mg/L 0.200 -0.000188 97 80-120 Lead 0.197 0.0100 mg/L 0.200 -0.00153 99 80-120 Selenium 0.201 0.0100 mg/L 0.200 -0.00717 101 80-120 Silver 0.198 0.0100 mg/L 0.200 0.000123 99 80-120 Classical Chemistry Parameters - Quality Control Batch 1120032 - NO PREP Blank (1320032-BLK1) Prepared: 10/20/2021 15:44 Analyzed: 10/20/2021 16:49 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L LCS (1320032-BS3) Prepared: 10/20/2021 15:44 Analyzed: 10/20/2021 17:06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 100 90-110 Matrix Spike (1J20032-MS3) Prepared: 10/20/2021 15:44 Analyzed: 10/20/2021 16:51 Source: CE15205-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.99 0.10 mg/L 1.00 0.017 U 99 90-110 Matrix Spike (1J20032-MS2) Prepared: 10/20/2021 15:44 Analyzed: 10/20/2021 16:54 Source: CE15205-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.96 0.10 mg/L 1.00 0.017 U 96 90-110 Matrix Spike Dup (1J20032-MSD1) Prepared: 10/20/2021 15:44 Analyzed: 10/20/2021 16:52 Source: CE15205-01 Analvte Nitrite as N Batch 1121002 - NO PREP Result Flaq POL 1.0 0.10 Spike Source %REC Units Level Result %REC Limits RPD mg/L 1.00 0.017 U 100 90-110 0.6 RPD Limit Notes 10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 29 of 37 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch IJ21002 - NO PREP - Continued (� �Eo www.encolabs.com Blank (1321002-BLK1) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 16:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L Sulfate as SO4 2.9 U 5.0 mg/L LCS (1323002-BSI) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 16:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 51 5.0 mg/L 50.0 102 90-110 Sulfate as SO4 51 5.0 mg/L 50.0 102 90-110 Matrix Spike (1323002-MS3) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:17 Source: CE35554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 30 5.0 mg/L 20.0 10 99 90-110 Sulfate as SO4 56 5.0 mg/L 20.0 35 108 90-110 Matrix Spike (1323002-MS2) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:52 Source: CE15554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 46 5.0 mg/L 20.0 26 98 90-110 Sulfate as SO4 19 5.0 mg/L 20.0 2.9 U 97 90-110 Matrix Spike Dup (I323002-MSDI) Prepared: 10/21/2021 06:21 Analyzed: 10/21/2021 17:35 Source: CE35554-01 Analvte Result Flaq POL Chloride 32 5.0 Sulfate as SO4 57 5.0 Batch IJ22004 - NO PREP Spike Source %REC RPD Units Level Result %REC Limits RPD Limit mg/L 20.0 10 108 90-110 6 10 mg/L 20.0 35 113 90-110 2 10 Notes QM-07 Blank (1322004-BLK3) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L LCS (1322004-BSI) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.38 0.10 mg/L 0.401 94 80-120 Duplicate (1322004-DUPl) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.055 3 0.10 mg/L 0.053 4 25 Matrix Spike (1322004-MS3) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE35554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 30 of 37 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1122004 - NO PREP - Continued Matrix Spike (1322004-MS3) Continued Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE15554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.29 0.10 mg/L 0.401 0.053 58 80-120 QM-07 Matrix Spike Dup (1322004-MSD1) Prepared: 10/22/2021 09:58 Analyzed: 10/22/2021 10:16 Source: CE15554-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.29 0.10 mg/L 0.401 0.053 59 80-120 1 25 QM-07 Batch 1126014 - NO PREP Blank (1326014-BLK3) Prepared: 10/26/2021 09:55 Analyzed: 10/29/2021 12:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (1326014-BS1) Prepared: 10/26/2021 09:55 Analyzed: 10/29/2021 13:00 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.2 0.10 mg/L 1.25 98 90-110 Matrix Spike (1326014-MS3) Prepared: 10/26/2021 09:55 Analyzed: 10/29/2021 13:04 Source: CE15235-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.1 0.20 mg/L 1.00 0.18 92 90-110 Matrix Spike (1326014-MS2) Prepared: 10/26/2021 09:55 Analyzed: 10/29/2021 13:09 Source: CE15235-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 3.2 E 0.10 mg/L 0.521 2.6 111 90-110 QM-07 Matrix Spike Dup (1326014-MSDI) Prepared: 10/26/2021 09:55 Analyzed: 10/29/2021 13:06 Source: CE15235-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.1 0.20 mg/L 1.00 0.18 93 90-110 0.3 10 Batch V27021 - NO PREP Blank (1327021-BLK3) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:10 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (1327021-BSI) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 99 15 mg/L 100 99 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 31 of 37 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch IJ27021 - NO PREP - Continued Matrix Spike (1327021-MS3) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:12 Source: CE15554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 110 15 mg/L 37.8 60 140 80-120 QM-07 Matrix Spike Dup (1327021-MSD1) Prepared: 10/27/2021 14:18 Analyzed: 10/27/2021 16:12 Source: CE15554-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 110 15 mg/L 37.8 60 137 80-120 1 25 QM-07 Batch 1127022 - NO PREP Blank (1327022-BLK3) Prepared: 10/27/2021 14:19 Analyzed: 10/27/2021 16:28 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (1327022-BS1) Prepared: 10/27/2021 14:19 Analyzed: 10/27/2021 16:29 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 98 15 mg/L 100 98 80-120 Matrix Spike (1327022-MS3) Prepared: 10/27/2021 14:19 Analyzed: 10/27/2021 16:30 Source: CE16264-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 110 15 mg/L 37.8 62 127 80-120 QM-07 Matrix Spike Dup (1327022-MSDi) Prepared: 10/27/2021 14:19 Analyzed: 10/27/2021 16:31 Source: CE16264-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 110 15 mg/L 37.8 62 124 80-120 1 25 QM-07 Batch IK01020 - NO PREP Blank (1K03020-BLKS) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (1K01020-BS3) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 100 15 mg/L 100 100 80-120 Matrix Spike (1K01020-MS3) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:14 Source: CE15194-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 88 15 mg/L 37.8 39 129 80-120 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 32 of 37 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1K01020 - NO PREP - Continued Matrix Spike Dup (1K01020-MSD1) Prepared: 11/01/2021 09:50 Analyzed: 11/01/2021 12:15 Source: CE15194-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 89 15 mg/L 37.8 39 133 80-120 2 25 QM-07 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch IJ25020 - EPA 5030B MS Blank (1325020-BLK1) Prepared: 10/25/2021 10:26 Analyzed: 10/25/2021 21:29 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-& 5.4 ug/L 5.00 107 75-125 LCS (1325020-BS1) Prepared: 10/25/2021 10:26 Analyzed: 10/25/2021 19:47 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 102 80-133 Toluene-d8 5.2 ug/L 5.00 104 75-125 Matrix Spike (1325020-MS1) Prepared: 10/25/2021 10:26 Analyzed: 10/25/2021 20:12 Source: AE08463-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 0.80 U 108 80-133 Toluene-d8 5.3 ug/L 5.00 107 75-125 Matrix Spike Dup (1325020-MSD1) Prepared: 10/25/2021 10:26 Analyzed: 10/25/2021 20:38 Source: AE08463-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 0.80 U 108 80-133 0 19 Toluene-d8 5.3 ug/L 5.00 106 75-125 Dissolved Gases by GC - Quality Control Batch 1126005 - Same Blank (1326005-BLK3) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:34 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 2.07 U 2.50 mg/L Ethane 0.00510 U 0.00600 mg/L Ethene 0.00510 U 0.00600 mg/L Methane 0.00400 U 0.00500 mg/L LCS (1326005-BSI) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 46.0 2.50 mg/L 45.8 100 70-130 Ethane 0.321 0.00600 mg/L 0.323 99 70-130 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 33 of 37 QUALITY CONTROL DATA Dissolved Gases by GC - Quality Control Batch 1126005 - Same - Continued (� �Eo www.encolabs.com LCS (1326005-BSI) Continued Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Ethene 0.315 0.00600 mg/L 0.302 104 70-130 Methane 0.168 0.00500 mg/L 0.174 97 70-130 LCS Dup (1J26005-BSD1) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 09:19 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Carbon dioxide 50.3 2.50 mg/L 45.8 110 70-130 9 30 Ethane 0.353 0.00600 mg/L 0.323 109 70-130 9 30 Ethene 0.349 0.00600 mg/L 0.302 116 70-130 10 30 Methane 0.188 0.00500 mg/L 0.174 108 70-130 11 30 Duplicate (1326005-DUPl) Prepared: 10/26/2021 08:00 Analyzed: 10/26/2021 13:37 Source: AE08472-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Carbon dioxide 22.1 2.50 mg/L 22.5 2 30 Ethane 0.00510 U 0.00600 mg/L 0.00510 U 30 Ethene 0.00510 U 0.00600 mg/L 0.00510 U 30 Methane 0.00400 U 0.00500 mg/L 0.00400 U 30 Classical Chemistry Parameters - Quality Control Batch 1126001 - NO PREP Blank (1326001-BLK1) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 09:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 0.90 U 1.0 mg/L LCS (1326001-BS3) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 09:43 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 49 1.0 mg/L 50.0 97 85-115 Matrix Spike (1J26001-MS3) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 10:24 Source: AE08470-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 51 1.0 mg/L 50.0 2.4 97 85-115 Matrix Spike (1J26001-MS2) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 18:44 Source: AE08497-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 52 1.0 mg/L 50.0 2.9 98 85-115 Matrix Spike Dup (1J26001-MSD1) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 10:47 Source: AE08470-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 50 1.0 mg/L 50.0 2.4 95 85-115 2 21 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 34 of 37 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 1126001 - NO PREP - Continued Matrix Spike Dup (1326001-MSD2) Prepared: 10/26/2021 07:08 Analyzed: 10/26/2021 19:08 Source: AE08497-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 51 1.0 mg/L 50.0 2.9 97 85-115 2 21 Batch V27005 - NO PREP Blank (1327005-BLK3) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 09:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 0.90 u 1.0 mg/L LCS (1327005-BSI) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 09:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 49 1.0 mg/L 50.0 99 85-115 Matrix Spike (1327005-MS3) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 10:33 Source: AE08497-02RE1 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 50 1.0 mg/L 50.0 3.1 95 85-115 Matrix Spike (1327005-MS2) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 18:34 Source: AE08497-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 55 1.0 mg/L 50.0 3.3 104 85-115 Matrix Spike Dup (1327005-MSDI) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 10:56 Source: AE08497-02REI Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 55 1.0 mg/L 50.0 3.1 104 85-115 9 21 Matrix Spike Dup (1327005-MSD2) Prepared: 10/27/2021 07:24 Analyzed: 10/27/2021 18:57 Source: AE08497-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 36 1.0 mg/L 50.0 3.3 66 85-115 42 21 QM-07, QM-11 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 35 of 37 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 36 of 37 (n uj RE 0 a F N 3 � cc N m 0 pp b O m U m a� J ro rNNi � a Z 7 LL 0 a m GPi cc e W U) Z 0 U J F M- o Z O N a N v 0M J N Ld� C � v m Z rz w n LLJ o Q n -0co � y N E v :� x m H L U) W �, a C 7 ¢ U N 0 � s V0906 Doi x x Ix x x x x T Cl S-00/�r JI WS a1 IjlnS x X x X X x / y� N OOE ejejlnS G x x x x x x 4 zoo +q'LNSa xxxxx ro Z'S9C XON x X x x c o 6H x x x x x 2 a Ul C Z'£9E N sa ft.))!N'OOE OPPONO'Z-Ol£ 4ullOXIV x X x x xc 0 eSigd`JO'PD'89'Sy'6a x x x x x X 0 id INIS Q09Zg' L Xtpuaddy (109Z8 x K x x x x V u = t1) 0 LO LO w to 0 Q U _ J N a C7 C o 2 oo E S I1j E c E V .1 a a a w � as m m r T tv U r J N [p g � (N CV c `w � a co G Z � f(1 }G ,jT w 4 a — Urt± �y CV Q CD to "' E E E L m Q a) U E E E y C k n � a 0 0 7 � t O O C] C v t3 v z cc ¢ w m m m o n a ir c CD ra � m v N O. aE i- m C air: C Q m 0 U E d 0 E m cr co �i 0 m 1° m a � " N a_ Y � r! U C E E u C m Sample Preservation Verification T ENCO Cary Work Order: CE16209 Project: Moore County Closed LPJCA Client: S&ME, Inc. (SM004) Project #: 4358-20-043 Logged In: 20-Oct-21 11:02 Logged By: Rachel Ann Yo ish I Preservation Check Performed By: ,� Date/Time: 0 CE16209-01 Cant Type Pres (pH) pH Checked / .Requirement In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y I N/ NA Y N/ NA C 250mLP+ZnAc+NaOH >9 / N / NA Y / NA D 250mLP+H2SO4 <2 Y / N / NA YIN 1 NA CE16209-02 Cont Type Pres (pH) Requirement pH Checked / to Control pH Adjusted Date(Time Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 / N 1 NA Y 16WY NA C 250mLP+ZnAc+NaOH >9 Y/ N I NA Y/ I NA D 250mLP+H2SO4 <2 YIN / NA Y / N NA CE16209-03 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted Date/Time Adiusted Reagent Used/Comments B 250mLP+HNO3 <2 'Y / N 1 NA Y N 1 NA C 250mLP+ZnAc+NaOH >9 Y / N / NA Y NA D Z50mLP+H2SO4 <2 Y/ N/ NA I Y I W1 NA CE16209-04 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent UsedlComments B 250mLP+HNO3 <2 Y/ N I NA Y NA C 250mLP+ZnAc+NaOH >9 N / NA Y / NA Q 250mLP+H2SO4 <2 Y 1 N I NA YIN NA CE16209-05 Cont Type Pres (pH) pH Checked / Requirement in Control pH Adjusted DatelTime Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 • / N / NA Y / ` NA C 250mLP+ZnAc+NaOH >9 I N/ NA Y N NA D 250mLP+H2SO4 <2 Y/ N I NA Y I N NA Rea ent Name ID 1 1 2 Rea ent Name ID 3 4 Reagent Name ID 5 6 pH Strip ID: PH Strips COF0555 C:IelmntlPrimNwKu_rit=Pvauui Pt Page 1 of 1 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, November 10, 2021 S&ME, Inc. (SM004) Attn: Edmund Henriques 8646 West Market Street, Suite 105 Greensboro, NC 27409 RE: Laboratory Results for Project Number: 4358-20-043A Phase 01, Project Name/Desc: Moore County Private Well ENCO Workorder(s): CE15556 Dear Edmund Henriques, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, October 20, 2021. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 0"6LC'=-:;tA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 12 PROJECT NARRATIVE Client: S&ME, Inc. (SM004) Project: Moore County Private Well Lab ID: CE15556 Overview (� �Eo www.encolabs.com Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples Precision between duplicate matrix spikes of the same sample was outside acceptance limits (QM-11). Quality Control Remarks The associated CCV standard exhibited high bias; since the result is ND, there is no impact (QV-01). Other Comments The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Chuck Smith Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 12 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: PW-1 Lab ID: CE15556-01 Sampled: 10/19/21 18:40 Received: 10/20/21 10:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 04/17/22 10/26/21 13:10 10/27/21 13:17 EPA 7470A EPA 245.1 11/16/21 10/20/21 15:21 10/22/21 08:25 EPA 8260D EPA 503013_MS 11/02/21 10/26/21 12:40 10/27/21 03:17 EPA 8260D EPA 503013_MS 11/02/21 10/28/21 13:21 10/29/21 00:30 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 12 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: PW-1 Lab ID: CE15556-01 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 15.8 1.10 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 12 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: PW-1 Lab Sample ID:CE15556-01 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 18:40 Work Order: CE15556 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1128031 EPA 8260D 10/29/21 00:30 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 Acetone [67-64-1]A 10 u ug/L 1 10 20 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1128031 EPA 8260D 10/29/21 00:30 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1128031 EPA 8260D 10/29/21 00:30 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY Vinyl acetate [108-05-4]A 0.95 u ug/L 1 0.95 5.0 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 Vinyl chloride [75-01-4]^ 0.32 u ug/L 1 0.32 1.0 1128031 EPA 8260D 10/29/21 00:30 RKY QV-01 Xylenes (Total) [1330-20-7]A 0.45 u ug/L 1 0.45 3.0 1128031 EPA 8260D 10/29/21 00:30 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 12 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: PW-1 Lab Sample ID:CE15556-01 Received: 10/20/21 10:20 Matrix: Ground Water Sampled:10/19/21 18:40 Work Order: CE15556 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 51 1 50.0 101 % 53-136 IJ28031 EPA 6260D 10129121 00:30 RKY Dibromofluoromethane 50 1 50.0 99 % 67-129 IJ28031 EPA 6260D 10129121 00:30 RKY Toluene-d8 51 1 50.0 101 % 59-134 IJ28031 EPA 6260D 10129121 00:30 RKY Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed AX Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 1J20028 EPA 7470A 10/22/21 08:25 CPH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 1J26004 EPA 6010D 10/27/21 13:17 JDH Barium [7440-39-3]^ 15.8 ug/L 1 1.10 10.0 1126004 EPA 6010D 10/27/21 13:17 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 1J26004 EPA 6010D 10/27/21 13:17 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 1J26004 EPA 6010D 10/27/21 13:17 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 1J26004 EPA 6010D 10/27/21 13:17 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 1J26004 EPA 6010D 10/27/21 13:17 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 1J26004 EPA 6010D 10/27/21 13:17 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO orlandO certified analyte [NC 424] Analyte rCAS Numberl 1,4-Dioxane [123-91-1]^ Surrogates Toluene-d8 Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 0.80 U ug/L 1 0.80 2.0 1J26032 EPA 8260D 10/27/21 03:17 KKW Results DF Soike Lv/ % Rec Vo Rec Limits Batch Method Analyzed ffy Notes 5.0 1 5.00 101 % 75-125 1J26032 EPA 8260D 10127121 03:17 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 12 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1128031 - EPA 5030B MS Blank (1328031-BLK1) Prepared: 10/28/2021 13:21 Analyzed: 10/28/2021 17:38 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 50 u91L 50.0 100 53-136 Dibromofluoromethane 49 u91L 50.0 99 67-129 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 12 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1128031 - EPA 5030B MS - Continued Blank (1328031-BLK1) Continued Prepared: 10/28/2021 13:21 Analyzed: 10/28/2021 17:38 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Toluene-d8 51 u91L 50.0 102 59-134 LCS (1728031-BS1) Prepared: 10/28/2021 13:21 Analyzed: 10/28/2021 15:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 117 75-133 Benzene 24 1.0 ug/L 20.0 120 80-134 Chlorobenzene 19 1.0 ug/L 20.0 94 80-120 Toluene 19 1.0 ug/L 20.0 96 71-120 Trichloroethene 22 1.0 ug/L 20.0 108 74-120 Matrix Spike (1328031-MS1) Prepared: 10/28/2021 13:21 Analyzed: 10/28/2021 16:09 Source: CE16465-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 26 1.0 ug/L 20.0 0.21 U 132 75-133 Benzene 26 1.0 ug/L 20.0 0.15 U 130 80-134 Chlorobenzene 21 1.0 ug/L 20.0 0.17 U 103 80-120 Toluene 21 1.0 ug/L 20.0 0.14 U 106 71-120 Trichloroethene 24 1.0 ug/L 20.0 0.15 U 119 74-120 Matrix Spike Dup (1]28031-MSD1) Prepared: 10/28/2021 13:21 Analyzed: 10/28/2021 16:38 Source: CE16465-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 106 75-133 22 20 QM-11 Benzene 23 1.0 ug/L 20.0 0.15 U 115 80-134 12 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 94 80-120 9 16 Toluene 19 1.0 ug/L 20.0 0.14 U 95 71-120 11 17 Trichloroethene 21 1.0 ug/L 20.0 0.15 U 104 74-120 14 22 Metals by EPA 6000/7000 Series Methods - Quality Control Batch 1120028 - EPA 245.1 Blank (1320028-BLK1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:33 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L Blank (1320028-BLK2) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:35 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Mercury 3.00 U 4.00 ug/L LCS (1320028-BSI) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.46 0.200 ug/L 5.00 109 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 12 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch 112002E - EPA 245.1 - Continued Matrix Spike (1320028-MS3) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:44 Source: CE15555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.96 0.200 ug/L 5.00 0.150 U 99 75-125 Matrix Spike Dup (1720028-MSD1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:46 Source: CE35555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.99 0.200 ug/L 5.00 0.150 U 100 75-125 0.8 25 Post Spike (1320028-PS1) Prepared: 10/20/2021 15:21 Analyzed: 10/22/2021 07:48 Source: CE35555-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.02 0.200 ug/L 4.76-0.000286 105 75-125 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 1.726004 - EPA 3005A Blank (1326004-BLK3) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Lead 3.10 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L LCS (1326004-BS1) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 201 10.0 ug/L 200 100 80-120 Barium 203 10.0 ug/L 200 101 80-120 Cadmium 20.0 1.00 ug/L 20.0 100 80-120 Chromium 196 10.0 ug/L 200 98 80-120 Lead 198 10.0 ug/L 200 99 80-120 Selenium 201 10.0 ug/L 200 101 80-120 Silver 197 10.0 ug/L 200 99 80-120 Matrix Spike (1726004-MS1) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:14 Source: CE15202-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 193 10.0 ug/L 200 7.60 U 97 75-125 Barium 241 10.0 ug/L 200 45.7 97 75-125 Cadmium 19.1 1.00 ug/L 20.0 0.360 U 96 75-125 Chromium 190 10.0 ug/L 200 1.40 U 95 75-125 Lead 193 10.0 ug/L 200 3.10 U 97 75-125 Selenium 189 10.0 ug/L 200 6.20 U 95 75-125 Silver 191 10.0 ug/L 200 1.90 U 95 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 12 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch IJ26004 - EPA 3005A - Continued Matrix Spike Dup (1326004-MSDI) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:16 Source: CE15202-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 192 10.0 ug/L 200 7.60 U 96 75-125 0.9 20 Barium 243 10.0 ug/L 200 45.7 98 75-125 0.8 20 Cadmium 19.5 1.00 ug/L 20.0 0.360 U 97 75-125 2 20 Chromium 192 10.0 ug/L 200 1.40 U 96 75-125 1 20 Lead 193 10.0 ug/L 200 3.10 U 97 75-125 0.03 20 Selenium 195 10.0 ug/L 200 6.20 U 97 75-125 3 20 Silver 194 10.0 ug/L 200 1.90 U 97 75-125 2 20 Post Spike (1326004-PS3) Prepared: 10/26/2021 13:10 Analyzed: 10/27/2021 12:19 Source: CE15202-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.195 0.0100 mg/L 0.200 0.00236 96 80-120 Barium 0.245 0.0100 mg/L 0.200 0.0457 100 80-120 Cadmium 0.0198 0.00100 mg/L 0.0200 2.87E-5 99 80-120 Chromium 0.195 0.0100 mg/L 0.200 -0.000188 97 80-120 Lead 0.197 0.0100 mg/L 0.200 -0.00153 99 80-120 Selenium 0.201 0.0100 mg/L 0.200 -0.00717 101 80-120 Silver 0.198 0.0100 mg/L 0.200 0.000123 99 80-120 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 2126032 - EPA 5030E MS Blank (1326032-BLK3) Prepared: 10/26/2021 12:40 Analyzed: 10/26/2021 23:51 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-d8 5.3 ug/L 5.00 107 75-125 LCS (1326032-BSI) Prepared: 10/26/2021 12:40 Analyzed: 10/26/2021 22:09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 26 2.0 ug/L 25.0 104 80-133 Toluene-d8 5.0 ug/L 5.00 101 75-125 Matrix Spike (1326032-MS1) Prepared: 10/26/2021 12:40 Analyzed: 10/26/2021 22:34 Source: AE08473-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 0.80 U 106 80-133 Toluene-& 5.0 u9/L 5.00 101 75-125 Matrix Spike Dup (1326032-MSD1) Prepared: 10/26/2021 12:40 Analyzed: 10/26/2021 23:00 Source: AE08473-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 0.80 U 107 80-133 0.8 19 Toluene-& 5.1 u9/L 5.00 102 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 12 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 12 3 3 Q) m ro IL M© W O M UJ- v t9 v © C !x9 b LL Nc _ 3 o n 0 U r Z UQ `m LL9Ua O z Q U 0 .Cy o UU _0_N 7 N O a a 2 U') C E cc E �m -0 m s �.ry E F ' C [7 E n N Lo U _ cn w '2 r Y CL 7 ccm d m N N +W Cn o m yN L] C m m m C O C d_ U n o ¢ m cn 0 N Q7 � w ¢ 6H a` c O U 9S'gd'J0`p3'e8'SV'6y x F QI NIS Gogzs' 6 xlpueddy 009Z8 x v o� � C h � U w x � � O 9 � N Z ti m`N a/�V�J 7 Z m Z Um m� oc J}ry[( o o n' `0' J 0 V ill�� = m U a m l0 ❑ � O Q o w _` r N QQ}} (D Cf) LV z CO o 1 p co OLj z zg cp �, it Z od TO b�� rp� Ln Cr7 v a n E E 4 =V H mE U) m U U to m E E E a a v ca a c U D�a p U i � m yip L Z F m m `OE ¢ - fL Gc 0 m E m E f a ¢ C O (3] Cc m d d E nGi m 3 m m a" m v) U3 Y m E m E u] U Sample Preservation Verification ENCO Cary Work Order: CE15556 Project: Moore County Private Well Client: S&ME, Inc. (SM004) Project #: 4358-20-043A Phase 01 Logged In: 20-Oct-21 11:16 ' Logged By: Rachel Ann Yo ish ir Preservation Check Performed By: _ Date/Time: 1 �� CE15556-01 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted ❑ateMme Adjusted Reagent Used/Comments A 250mLP+HNO3 <2 Y ) N / NA Y NIII NA Reagent Name ID ` 2 r „z pH Strip ID: PH Strips COF0555 C:lelmntlPrint\WKo_NreservationCheck. rpt Reagent Name ID 3 4 Reacient Name ID 5 6 Page 1 of I Sample Preservation Verification ENCQ Cary Work Order: CE15556 Project: Moore County Private Well Client: S&ME, Inc. (SM004) Project #: 4358-20-043A Phase 01 Logged In: 20-Oct-21 11:16 Logged By: Rachel Ann Ya ish Preservation Check Performed By: _ Date/Time: wilo 1 CE15556-01 Cont Type Pres (pH) pH Checked / Requirement In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments A 250mLP+HNO3 <2 Y N/ NA Y N I NA Rea ent Name ID 1 2 Reagent Name ID 3 4 Rea ent Name ID 5 6 pH Strip ID: PH Strips C0F0555 CaelmntlPrintkwKo_Nreservation Check. rpt Page 1 of 1 Appendix III — Historical Analytical Results TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A DetectedActive Const wig ituent/Parameter Antimony NC21- IMAC = 1 ug/L EPA MCL = 6 ug/L Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L D. 06/20/18 11/27/18 04/02/19 11/19/19 04/07/20 10/13/20 04/13/21 10/19/21 0.74 0.74 0.74 0.74 0.74 0.74 0.74 0.74 2 2 2 2 2 2 2 2 -- -- -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND D- ND ND ND C&D Monitoring MW-14 ND ND ND ND ND ND ND ND Wells MW-1 7S -- ND ND ND ND ND MW-17D -- ND ND ND ND ND -- -- ND ND ND ND -- -- ND ND ND ND ND ND ND ND ND ND ND MW-11SR ND ND ND ND ND ND ND ND MW-1 -- -- -- NS NS MW-2 -- -- -- NS NS Closed MSW Monitoring MW-3 -- -- -- NS NS Wells MW-6 ND -- -- ANR ANR & MNA Performance MW-7 ND -- -- ANR ANR Monitoring MW-8 -- -- -- ANR ANR Wells M�= -- -- -- ANR ANR -- -- -- ANR ANR -- -- -- NS NS Arsenic ug/L 03/05/90 ND ND ND ND ND ND NC 2L = 10 ug/L ug/L 03/21/91 ND ND ND ND ND ND EPA MCL = 10 ug/L ug/L 03/10/92 ND ND ND ND ND ND ug/L 04/20/95 ND ND ND ND ND ND ug/L 06/27/95 ND ug/L 09/22/95 ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 ND ND ND ND ND ND ND ND ug/L 04/27/99 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/21/99 ND ND ND 18 ND ND ND ND ug/L 03/14/00 -- ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 ND ND ND ND ND ND ND ND ug/L 10/11/01 ND ND ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 ND 11 19 ND ND 10 ND ND ug/L 04/09/03 ND ND 11 ND ND ND 10 ND ug/L 10/13/03 ND ND 14 17 14 14 11 ND ug/L 04/26/04 ND ND ND ND ND ND 12 ND ug/L 10/25/04 ND ND 15 ND ND ND 14 ND ug/L 04/04/05 10 10 10 15 10 29 10 ND ug/L 10/04/05 ND ND 13 15 12 21 ND ND ug/L 04/28/06 ND 11 ND ND ND ND 12 ND ND 11 16 ND ug/L 10/09/06 ND 13 ND ND ND ND 14 ND ND ND 11 ND ug/L 04/24/07 ND ND ND ND ND ND ND ND ND 38 27 ND ug/L 10/30/07 10 ND ND ND ND ND ND 3.2 J ND ND 6.9 J 7.8 J ND ug/L 04/23/08 10 ND ND ND 3.2 J ND ND ND ND ND ND 2.3 J ND ug/L 10/06/08 10 ND ND ND ND ND ND ND ND ND ND 7.7 J ND ug/L 04/13/09 10 ND 5.1 J ND ND ND ND 8.2 J 17.1 6.6 J 11.4 10.1 J ND ug/L 10/15/09 10 5.30 J 6.47 J 5.54 J 6.53 J 2.86 J ND 8.63 J 18.3 11.6 15.9 12.6 ND ug/L 04/26/10 10 ND 10.8 ND 3.14 J ND 3.50 J 14.2 31.0 8.54 J 13.4 28.5 ND ug/L 10/19/10 10 5.16 J 24.9 ND ND ND ND 29.5 33.0 22.6 28.0 26.6 ND ug/L 04/18/11 10 ND 20.0 ND 3.29 B ND 5.35 B 18.7 14.6 B 16.1 B 19.2 14.6 B 5.39 B ug/L 10/10/11 10 ND ND ND ND ND 2.96 J 5.48 J 4.73 J 5.67 J 19.0 Dry 5.26 J ug/L 04/17/12 10 4.42 B ND ND ND 4.31 B 3.32 B ND 29.4 ND 17.9 B Dry ND ug/L 10/09/12 10 ND 6.36 J ND 2.90 J ND 2.91 J 9.82 J 21.6 9.74 J 10.7 Dry ND ug/L 04/15/13 10 3.97 B ND 5.21 B 2.87 B ND 4.42 B 17.8 ND ND 14.7 B Dry ND ug/L 09/30/13 10 ND 9.62 J ND ND ND ND 24.5 32.0 20.3 18.0 Dry ND ug/L 04/16/14 10 ND 8.25 J ND ND ND ND 23.3 19.7 15.2 19.5 Dry ND ug/L 10/15/14 5.4 10 Dry ND ND ND ND ND 6.99 J 10.8 14.1 38.6 Dry ND ug/L 04/15/15 5.4 -- 10 ND -- ND -- -- -- -- ND -- ND ND ND 20.3 21.8 ND 8.41 J Dry ND ug/L 10/07/15 5.4 10 ND ND ND ND ND ND ND 20.0 ND 32.4 8.73 J ND ug/L 04/11/16 5.4 -- 10 ND -- ND -- -- -- -- ND -- ND ND ND 12.6 27.0 11.3 38.7 29.6 ND ug/L 11/30/16 6.8 -- 10 ND -- 48.1 (ND) -- -- -- -- ND -- ND ND ND 65.8 (ND) 20.4 (ND) 14.9 (ND) 85.6 (41.9) 39.6 (42.4) ND (Dissolved) ug/L 11/30/16 6.8 10 -- -- -- -- 14.4 (Verification Event) ug/L 02/09/17 6.8 -- 10 ND -- -- -- -- -- -- -- -- -- -- -- -- -- -- 40.5 -- (Dissolved) ug/L 02/09/17 6.8 -- 10 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- 39.0 ug/L 04/11/17 6.8 10 ND 7.78 J ND ND ND ND 10.5 8.67 J ND 53.7 31.8 ND ug/L 12/12/17 6.8 10 ND 19.3 ND ND ND ND 25.9 21.5 8.49 J 53.2 25.4 ND ug/L 06/20/18 7.6 -- 10 ND ND 22.7 -- -- -- -- ND ND ND ND ND 22.8 ND ND 38.6 ND -- ug/L 11/27/18 7.6 10 -- ND ND ND -- -- -- -- ND ND ND ND ND ND 14.9 ND 38.4 ND ND ug/L 04/02/19 7.6 10 ND ND ND ND ND ND ND ND ND 11.7 ND ND ND ND ug/L 11/19/19 7.6 10 ND ND ND ND ND ND ND ND ND ND ND ND ND 36.5 ND ND ug/L 04/07/20 7.6 10 ND ND ND ND ND ND ND ND ND ND ND 23.8 ND ug/L 10/13/20 7.6 10 -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 64.8 ND -- ug/L 04/13/21 7.6 10 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/19/21 7.6 10 -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 43.9 ND ND T:-Proj--358-20-043A Moore County R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 AppendixIII- RlsioMc G-21-10 WQMR Tables Fa App,d - Page 1 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells DetectedActive Constituent/Parameter Barium Units ug/L D.MW-5§JrD- 03/05/90 -- -- -- 35 -- -- -- =���E6" -- -- -- 15 MW-11SR -- MW-1 57 MW-2 21 MW-3 13 MW-6 -- MW-7 -- MW-8 -- M�= -- -- ND NC 2L = 700 ug/L ug/L 03/21/91 35 23 73 66 23 ND EPA MCL = 2000 ug/L ug/L 03/10/92 30 23 43 69 12 ND ug/L 04/20/95 ND -- -- -- -- ND ND ND ND ND ug/L 06/27/95 ND ug/L 09/22/95 ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 ND ND ND ND ND ND ND ND ug/L 04/27/99 ND ND ND ND ND ND ND ND ug/L 10/21/99 ND ND ND ND ND ND ND ND ug/L 03/14/00 ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/09/03 ND ND ND ND ND ND ND ND ug/L 10/13/03 ND ND ND ND ND ND ND ND ug/L 04/26/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND ND ND ND ND ND ug/L 10/04/05 ND ND ND ND ND ND ND ND ug/L 04/28/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/24/07 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/30/07 100 13.5 J 44.4 J 52.8 J 46.6 J 65.8 J 13.8 J 40.1 J 17.0 J 60.3 J 80.2 J 15.5 J 14.6 J ug/L 04/23/08 100 11.9 J 42.6 J 31.7 J 57.1 J 55.4 J 12.1 J 59.5 J 26.8 J 52.1 J 81.1 J 12.3 J 14.8 J ug/L 10/06/08 100 12.8 J 45.7 J 41.8 J 40.9 J 58.8 J 13.8 J 42.0 J 31.2 J 51.4 J 83.1 J 12.4 J 15.6 J ug/L 04/13/09 100 11.5 J 51.3 J 56.0 J 49.5 J 65.8 J 17.2 J 42.6 J 36.7 J 81.6 J 89.8 J 14.9 J 14.5 J ug/L 10/15/09 100 13.7 J 44.7 J 72.6 J 28.6 J 66.7 J 19.1 J 40.0 J 33.9 J 67.5 J 78.6 J 20.8 J 14.5 J ug/L 04/26/10 100 9.47 J 49.9 J 54.7 J 43.3 J 66.0 J 19.8 J 39.8 J 33.4 J 67.2 J 80.3 J 11.7 J 14.8 J ug/L 10/19/10 100 16.6 J 42.4 J 29.5 J 31.4 J 52.6 J 14.9 J 29.5 J 25.2 J 53.9 J 69.7 J 13.6 J 11.8 J ug/L 04/18/11 100 13.1 J 48.1 J 41.9 J 48.8 J 64.8 J 21.4 J 40.2 J 28.2 J 70.3 J 81.9 J 17.5 J 15.4 J ug/L 10/10/11 100 14.3 J 47.5 J 71.2 J 46.1 J 66.7 J 22.0 J 39.9 J 30.1 J 71.7 J 74.7 J Dry 15.5 J ug/L 04/17/12 100 19.5 J 52.1 J 40.5 J 62.7 J 75.0 J 21.7 J 39.8 J 30.1 J 67.5 J 84.9 J Dry 15.5 J ug/L 10/09/12 100 15.4 J 54.3 J 10.1 J 52.0 J 68.1 J 18.8 J 39.5 J 39.7 J 64.2 J 73.0 J Dry 14.7 J ug/L 04/15/13 100 14.6 J 49.4 J 26.8 J 40.5 J 60.8 J 20.4 J 42.7 J 36.7 J 78.4 J 86.4 J Dry 14.6 J ug/L 09/30/13 100 12.4 J 56.5 J 24.5 J 35.8 J 38.3 J 21.1 J 50.5 J 47.1 J 65.3 J 90.1 J Dry 14.9 J ug/L 04/16/14 100 13.6 J 47.3 J 15.9 J 35.3 J 41.8 J 15.2 J 42.6 J 28.9 J 60.6 J 102 Dry 16.2 J ug/L 10/15/14 1 100 Dry 50.4 J 25.9 J 33.6 J 46.3 J 25.5 J 49.3 J 31.1 J 103 98.4 J Dry 23.1 J ug/L 04/15/15 1 100 15.6 J 49.2 J 95.6 J 46.6 J 53.3 J 32.9 J 45.0 J 28.4 J 74.7 J 93.7 J Dry 18.2 J ug/L 10/07/15 1 100 14.7 J 45.8 J 21.2 J 30.4 J 52.1 J 25.2 J 36.6 J 28.6 J 88.8 J 92.8 J 12.6 J 15.8 J ug/L 04/11/16 1 100 13.7 J 41.5 J 69.3 J 31.9 J 38.8 J 34.0 J 44.4 J 28.6 J 65.5 J 84.0 J 8.38 J 18.5 J ug/L 11/30/16 1 100 14.4 B 36.7 B 38.3 B 28.6 B 38.2 B 30.0 B 44.5 J 24.2 B 75.1 J 84.2 J 8.70 B 17.8 B ug/L 04/11/17 1 100 14.5 J 45.3 J 28.5 J 29.9 J 54.5 J 32.6 J 45.0 J 26.6 J 99.7 J 106 9.34 J 18.6 J ug/L 12/12/17 1 100 12.9 J 43.5 J 35.6 J 34.8 J 55.6 J 36.8 J 47.9 J 28.6 J 77.3 J 98.2 J 14.5 J 18.7 J ug/L 06/20/18 1.1 -- 100 11.7 J 58.2 J 39.8 J 40.3 J 59.9 J 26.7 J 57.0 J 31.8 J 42.7 J 33.3 J 76.3 J 89.3 J 38.6 J -- ug/L 11/27/18 1.1 10 -- 13.9 53.1 40.4 60.4 68.4 30.5 38.7 31.9 38.9 39.2 50.5 78.8 32.3 20.2 ug/L 04/02/19 1.1 10 15.4 49.0 37.8 54.9 98.0 30.4 38.3 33.5 37.8 40.8 54.2 78.4 38.9 20.8 ug/L 11/19/19 1.1 10 14.5 59.3 56.9 68.3 16.5 -- 53.9 71.2 37.8 54.9 38.5 52.7 38.3 102 117 19.8 20.7 ug/L 04/07/20 1.1 10 12.8 54.7 42.2 91.8 10.6 86.7 -- 43.0 69.3 -- -- -- 42.9 25.7 69 83 40.0 -- ug/L 10/13/20 1.1 10 15.4 52.7 19.1 44.0 44.6 87.9 33.4 83.8 59.5 25.9 72.8 26.7 34.7 33.9 41.0 34.4 75.6 95.5 27.5 19.0 ug/L 04/13/21 1.1 10 32.7 55.0 22 48.3 18.2 136.0 22.4 89.5 103 103.0 89.0 NS NS NS 46.0 38.4 66.6 78.2 25.0 NS ug/L 10/19/21 1.1 10 21.6 51.9 22.9 39.6 44.7 84.2 36.4 78.1 19.8 35.8 67.1 23.7 63 36.7 42.3 33.6 80.0 99.9 42.2 15.8 T:-Proj--358-20-043A Moore County R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 AppendixIII- RlsioMc G-21-10 WQMR Tables Fa App,d - Page 2 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells DetectedActive Constituent/Parameter Cadmium Units ug/L D.MW-501VD-MW-11SR 03/05/90 -- -- -- ND -- -- -- -- -- -- ND -- MW-1 ND MW-2 ND MW-3 ND MW-6 -- MW-7 -- MW-8 -- M�= -- -- ND NC 2L = 2 ug/L ug/L 03/21/91 ND ND ND ND ND ND EPA MCL = 5 ug/L ug/L 03/10/92 ND ND ND ND ND ND ug/L 04/20/95 ND ND ND ND ND ND ug/L 06/27/95 ND ug/L 09/22/95 ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 ND ND ND ND ND ND ND ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 ND ND ND ND ND ND ND ND ug/L 04/27/99 ND ND ND ND ND ND ND ND ug/L 10/21/99 ND ND ND ND ND ND ND ND ug/L 03/14/00 ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 ND ND ND ND ND ND ND ND ug/L 04/09/03 ND ND ND ND ND ND ND ND ug/L 10/13/03 2 ND ND ND ND ND ND ND ug/L 04/26/04 1 ND 1 ND ND ND ND ND ug/L 10/25/04 1 ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND ND ND ND ND ND ug/L 10/04/05 ND ND ND ND ND ND ND ND ug/L 04/28/06 ND ND ND ND ND ND ND 1 ND 1 2 ND ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/24/07 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/30/07 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/23/08 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/06/08 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/15/09 1 ND ND ND ND ND 0.487 J ND ND ND ND ND ND ug/L 04/26/10 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/19/10 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/18/11 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/10/11 1 ND ND ND ND ND ND ND 0.685 J ND ND Dry ND ug/L 04/17/12 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/09/12 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/15/13 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 09/30/13 1 ND ND ND ND ND ND 1.15 0.722 J ND ND Dry ND ug/L 04/16/14 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/15/14 0.36 1 Dry ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/15/15 0.36 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/07/15 0.36 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/11/16 0.36 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/30/16 0.36 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/11/17 0.36 1 ND ND ND ND ND ND 0.585 J ND ND 0.696 J ND ND ug/L 12/12/17 0.36 1 ND -- ND ND ND ND ND ND ND 0.734 J ND ND 0.371 J ug/L 06/20/18 0.36 1 ND 0.500 B ND ND ND ND ND ND ND ND ND ND ND -- ug/L 11/27/18 0.36 1 -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/02/19 0.36 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/19/19 0.36 1 ND ND 0.409 J ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/07/20 0.36 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/13/20 0.36 1 ND 1.09 1.03 ND 1.93 ND ND 1.26 ND ND 1.11 ND ND ND 2.16 1.57 1.67 0.662 J 1.92 ug/L 04/13/21 0.36 1 ND 0.526 J 0.572 J ND ND ND ND 0.811 J ND ND ND NS NS NS 1.04 1.25 0.612 J ND 0.855 J NS ug/L 10/09/21 0.36 1 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS T:—Proj--358-20-043A Moore County R-Im LFG6 WQ Mon1-1,g—, 03-S--Annual WQ 2021-2022Te112021 AppendixIII- RlsioMc G-21-10 WQMR Tables Fa App,d — Page 3of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells DetectedActive Constituent/Parameter Chromium Units ug/L D.MW-501VD-MW-11SR 03/05/90 -- -- -- ND -- -- -- -- -- -- ND -- MW-1 ND MW-2 ND MW-3 ND MW-6 -- MW-7 -- MW-8 -- M�= -- -- ND NC 2L = 10 ug/L ug/L 03/21/91 ND ND ND 12 10 ND EPA MCL = 100 ug/L ug/L 03/10/92 ND ND ND ND ND -- -- ND ug/L 04/20/95 ND ND ND 12 7 ND ug/L 06/27/95 -- -- ND ug/L 09/22/95 ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 ND ND ND ND ND ND ND ND ug/L 04/27/99 ND ND ND ND ND ND ND ND ug/L 10/21/99 ND ND ND ND ND ND ND ND ug/L 03/14/00 ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/09/03 20 ND ND ND ND 11 ND ND ug/L 10/13/03 ND ND ND ND ND ND ND ND ug/L 04/26/04 ND ND ND ND ND 19 ND ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND ND ND ND ND ND ug/L 10/04/05 ND ND ND ND ND ND ND ND ug/L 04/28/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/24/07 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/30/07 10 ND ND 2.4 J ND ND ND ND ND ND ND ND 2.8 J ug/L 04/23/08 10 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/06/08 10 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/13/09 10 ND ND ND ND ND ND ND 1.1 J ND ND ND ND ug/L 10/15/09 10 ND ND ND ND ND 1.02 J ND ND ND ND ND ND ug/L 04/26/10 10 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/19/10 10 5.84 J ND 3.07 J ND ND ND ND ND ND ND ND ND ug/L 04/18/11 10 ND ND 1.02 J 1.90 J ND ND ND ND ND ND ND ND ug/L 10/10/11 10 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/17/12 10 3.10 J ND ND ND ND ND ND ND ND 2.25 J Dry ND ug/L 10/09/12 10 1.65 J ND 3.37 J ND ND ND ND ND ND ND Dry ND ug/L 04/15/13 10 ND ND ND ND ND ND 2.64 B ND ND ND Dry ND ug/L 09/30/13 10 ND ND 2.25 J ND ND ND ND ND ND ND Dry ND ug/L 04/16/14 10 ND ND 1.88 J ND ND ND ND ND ND ND Dry ND ug/L 10/15/14 1.4 10 Dry ND 5.71 J 1.83 J ND ND ND ND ND ND Dry ND ug/L 04/15/15 1.4 10 ND ND ND ND ND 1.64 J ND ND ND ND Dry ND ug/L 10/07/15 1.4 10 ND ND 2.97 J ND ND ND ND ND ND ND ND ND ug/L 04/11/16 1.4 10 ND ND ND ND ND ND ND ND ND ND 4.36 J ND ug/L 11/30/16 1.4 10 ND ND ND ND ND ND ND ND ND ND 1.42 J ND ug/L 04/11/17 1.4 10 ND ND 2.22 J ND ND ND ND ND ND ND ND ND ug/L 12/12/17 1.4 10 ND ND 1.88 J ND ND ND ND ND ND ND ND ND ug/L 06/20/18 1.4 -- 10 ND ND ND 1.55 J ND ND ND ND ND ND ND ND ND ug/L 11/27/18 1.4 10 -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/02/19 1.4 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/19/19 1.4 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/07/20 1.4 10 -- ND ND ND ND ND ND -- 3.46 J 3.68 J -- -- -- ND ND ND ND ND -- ug/L 10/13/20 1.4 10 ND ND ND ND ND ND 1.59 J ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/13/21 1.4 10 -- ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/19/21 1.4 10 -- ND ND ND ND ND ND 3.04 ND ND 1.91 J ND ND ND ND ND ND ND ND ND ND T:-Proj--358-20-043A Moore County R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 AppendixIII- RlsioMc G-21-10 WQMR Tables Fa App,d - Page 4 Of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A DetectedActive Constituent/Parameter Cobalt NC 2L IMAC = 1 ug/L Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L D. 06/20/18 11/27/18 04/02/19 11/19/19 04/07/20 10/13/20 04/13/21 10/19/21 1.4 1.4 1.4 1.4 1.4 1.4 1.4 1.4 -- 10 10 10 10 10 10 10 10 -- ND ND ND ND ND ND ND ND �• 2.13 2.03 2.55 ND ND 1.49 1.63 ND J J J J J ND ND ND D- 1.51 1.43 ND C&D Monitoring MW-14 ND ND ND ND 1.50 J J J ND ND Wells MW-1 7S -- ND ND ND ND ND MW-17D -- ND ND 1.48 J ND ND -- ND ND ND ND -- ND ND ND ND ND ND ND ND ND ND ND MW-11SR ND ND 1.63 J ND ND ND ND ND MW-1 -- NS NS Closed MW-2 -- NS NS MSW Monitoring MW-3 -- NS NS Wells & MW-6 ND ANR ANR MNA Performance MW-7 ND ANR ANR Monitoring MW-8 -- ANR ANR Wells M�= -- ANR ANR -- ANR ANR -- NS NS Copper ug/L 03/05/90 -- -- ND ND 10 ND ND ND NC 2L=1000 ug/L ug/L 03/21/91 ND ND 14 12 ND ND EPA MCL = 1300 ug/L ug/L 03/10/92 ND ND ND 110 ND -- -- ND ug/L 04/20/95 ND -- ND ND 14 11 ND ug/L 06/27/95 -- -- ND ug/L 09/22/95 ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 ND ND ND ND ND ND ND ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/27/99 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/21/99 ND ND ND ND ND ND ND ND ug/L 03/14/00 ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 ND ND ND ND ND ND ND ND ug/L 10/11/01 ND ND ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 ND ND ND ND ND ND ND ND ug/L 04/09/03 ND ND ND ND ND ND ND ND ug/L 10/13/03 ND ND ND ND ND ND ND ND ug/L 04/26/04 ND ND ND ND ND ND ND ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND ND ND ND ND ND ug/L 10/04/05 ND ND ND ND ND ND ND ND ug/L 04/28/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/09/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/24/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/30/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/23/08 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 06/20/18 1.6 -- 10 2.28 B ND ND 5.70 B ND ND ND ug/L 11/27/18 1.6 10 -- ND ND ND 3.17 B ND ug/L 04/02/19 1.6 10 ND ND ND -- 3.37 J ND ug/L 11/19/19 1.6 10 ND ND ND ND 2.96 J 1.76 J ND ug/L 04/07/20 1.6 10 ND ND ND ND ND ND -- 1.75 J ND ug/L 10/13/20 1.6 10 ND ND ND ND 3.26 J ND 2.97 J 1.99 2.03 J 3.81 J ND ug/L 04/13/21 1.6 10 ND ND 1.97 J ND 3.37 J ND ND ND ND ND ND NS NS NS ANR ANR ANR ANR ANR NS ug/L 10/19/21 1.6 10 ND ND ND ND ND ND ND ND ND 2.20 J ND ANR ANR ANR ANR ANR ANR ANR ANR ANR T:-Proj--358-20-043A Moore Cowry R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 AppendixIII- RlsioMc G-21-10 WQMR Tables Fa App,d - Page 5 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells DetectedActive Constituent/Parameter Lead Units ug/L D.MW-501VD-MW-11SR 03/05/90 -- -- -- 16 -- -- -- -- -- -- 14 -- MW-1 7 MW-2 29 MW-3 6 MW-6 -- MW-7 -- MW-8 -- M�= -- -- ND NC 2L = 15 ug/L ug/L 03/21/91 ND ND ND ND ND ND EPA MCL = 15 ug/L* ug/L 03/10/92 14 25 10 39 12 -- -- -- ND ug/L 04/20/95 -- -- -- ND -- -- -- -- -- -- -- -- -- -- -- 7 ND 18 16 -- ND ug/L 06/27/95 -- -- -- ND ug/L 09/22/95 ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND 39 ug/L 04/08/97 ND ND ND ND ND ND ND 34 ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND 70 ug/L 04/30/98 ND ND ND ND ND ND ND 42 ug/L 10/14/98 ND ND ND ND ND ND ND 26 ug/L 04/27/99 ND ND ND ND ND ND 13 166 ug/L 10/21/99 ND ND ND ND ND ND ND 135 ug/L 03/14/00 ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 ND ND ND ND ND ND 10 14 ug/L 10/11/01 ND ND ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 ND ND ND ND ND ND ND ND ug/L 04/09/03 10 ND ND 13 ND ND 19 ND ug/L 10/13/03 ND ND ND ND ND ND ND 11 ug/L 04/26/04 ND ND ND ND ND ND ND ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND 12 ND 14 ND 16 ug/L 10/04/05 ND ND ND 11 ND ND ND 17 ug/L 04/28/06 ND ND ND ND ND ND ND ND ND ND 13 18 ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/24/07 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/30/07 10 ND 3.9 J ND ND ND ND 4.6 J 5.2 J 6.5 J 2.6 J 2.5 J 6.8 J ug/L 04/23/08 10 ND ND ND ND ND ND ND ND ND ND ND 15.8 ug/L 10/06/08 10 ND ND 9.4 J ND ND ND 2.9 J 4.9 J ND ND 2.2 J 13.4 ug/L 04/13/09 10 ND 6.3 J ND ND 2.1 J 2.3 J 5.4 J 5.2 J 6.5 J 6.4 J 5.5 J 10.4 ug/L 10/15/09 10 ND ND ND ND ND ND ND 3.90 J ND ND 2.27 J 3.37 J ug/L 04/26/10 10 ND 3.82 J ND ND 2.47 J ND 3.17 J 4.54 J 3.95 J 3.09 J 3.89 J 2.18 J ug/L 10/19/10 10 4.34 J 2.07 J 3.45 J ND ND ND ND ND 1.92 J ND ND 8.93 J ug/L 04/18/11 10 ND 5.09 J 2.00 J ND ND ND 5.57 J 5.07 J 6.87 J ND 5.19 J 19.0 ug/L 10/10/11 10 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/17/12 10 ND ND 2.26 J ND ND ND ND 4.08 J ND ND Dry 16.6 ug/L 10/09/12 10 ND 3.49 J 2.51 J ND ND ND 3.89 J 2.89 J ND ND Dry 20.6 ug/L 04/15/13 10 ND ND 2.11 J ND ND ND ND ND ND ND Dry 20.4 ug/L 09/30/13 10 ND 4.05 J 2.75 J ND ND ND 6.67 J 5.81 J 5.32 J 3.31 J Dry 37.3 ug/L 04/16/14 10 ND 4.17 J 3.06 J ND ND ND 5.24 J 7.02 J 4.95 J 2.83 J Dry 60.5 ug/L 10/15/14 2.1 10 Dry ND ND ND ND ND ND ND ND ND Dry 18.3 ug/L 04/15/15 2.1 10 ND ND ND ND ND ND ND ND ND ND Dry 26.2 ug/L 10/07/15 2.1 10 ND ND 4.58 J 3.55 J ND ND 3.21 J 4.36 J ND 5.90 J 6.76 J 22.2 ug/L 04/11/16 2.1 10 ND ND ND ND ND ND ND ND ND ND 4.87 J 21.0 ug/L 11/30/16 3.1 10 ND ND ND ND ND ND ND ND ND ND ND 11.5 ug/L 04/11/17 3.1 10 ND ND 4.48 J ND ND ND ND ND ND ND ND 36.0 ug/L 12/12/17 3.1 10 ND 7.48 J ND ND ND ND 7.80 J ND 3.33 J ND 5.91 J 15.6 ug/L 06/20/18 3.1 -- 10 ND ND ND ND ND ND ND ND ND ND ND ND ND -- ug/L 11/27/18 3.1 10 -- ND 3.42 J ND ND ND ND ND ND ND ND ND ND ND 23.7 ug/L 04/02/19 3.1 10 ND ND ND ND ND ND ND ND ND ND ND ND 23.8 22.4 ug/L 11/19/19 3.1 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 26.3 ug/L 04/07/20 3.1 10 ND ND ND ND ND ND ND ND ND ND ND ND ND -- ug/L 10/13/20 3.1 10 ND 6.92 4.49 J ND 11.2 ND ND 7.49 ND ND ND ND ND ND 9.32 J 10.9 9.86 6.58 J 9.94 J 11.4 ug/L 04/13/21 3.1 10 ND 8.39 J 9.88 J ND 7 J 3.98 J ND ND 7.9 J 5.15 J 11.5 NS NS NS 4.25 J 4.39 J 13.9 10.9 13 NS ug/L 10/19/21 3.1 10 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS T:-Proj--358-20-043A Moore County R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 Appendix III -RI51oMc G-21-10 WQMR Tables Fa App,d - Page 6 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells DetectedActive Constituent/Parameter Mercury Units ug/L D.MW-501VD- 03/05/90 -- -- -- 0.5 -- -- -- =���E6" -- -- -- ND MW-11SR -- MW-1 ND MW-2 0.5 MW-3 ND MW-6 -- MW-7 -- MW-8 -- M�= -- -- ND NC 2L = 1 ug/L ug/L 03/21/91 0.6 0.6 0.8 2.4 0.6 ND EPA MCL = 2 ug/L ug/L 03/10/92 0.7 1.1 ND 6 1.3 -- -- ND ug/L 04/20/95 ND -- -- -- ND ND 1.2 0.3 ND ug/L 06/27/95 -- -- ND ug/L 09/22/95 ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/08/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 ND ND ND ND ND ND ND ND ug/L 04/27/99 ND ND ND ND ND ND ND ND ug/L 10/21/99 ND ND ND ND ND ND ND ND ug/L 03/14/00 ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/18/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/09/03 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- 1.01 ND ND ND ND ND ug/L 10/13/03 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/26/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND ND ND ND ND ND ug/L 10/04/05 ND ND ND ND ND ND ND ND ug/L 04/28/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/24/07 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/30/07 0.2 0.17 J 0.12 J 0.24 0.21 0.16 J ND ND ND 0.17 J ND ND ND ug/L 04/23/08 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/06/08 0.2 ND ND ND ND ND 0.21 ND ND ND ND ND ND ug/L 04/13/09 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/15/09 0.2 ND ND ND 0.0952 J ND ND ND ND ND ND ND ND ug/L 04/26/10 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/19/10 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/18/11 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/10/11 0.2 ND ND ND 0.478 ND ND ND ND ND ND Dry ND ug/L 04/17/12 0.2 ND ND ND 0.175 J ND ND ND ND ND ND Dry ND ug/L 10/09/12 0.2 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/15/13 0.2 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 09/30/13 0.2 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/16/14 0.2 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/15/14 0.17 0.2 Dry ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/15/15 0.17 0.2 ND ND 0.0261 J ND ND ND 0.0796 J ND ND ND Dry ND ug/L 10/07/15 0.17 0.2 ND ND ND ND ND ND 0.197 J ND ND ND 0.201 ND ug/L 04/11/16 0.17 0.2 ND ND ND ND ND ND ND 0.274 ND ND 0.219 ND ug/L 11/30/16 0.17 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/11/17 0.17 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 12/12/17 0.10 0.2 ND 0.0990 J ND 0.103 J ND ND ND ND ND 0.118 J 0.111 J ND ug/L 06/20/18 0.15 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/27/18 0.15 0.2 -- 0.281 ND ND ND ND ND ND ND ND 0.338 ND 0.187 J ND ND ug/L 04/02/19 0.15 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/19/19 0.15 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/07/20 0.15 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/13/20 0.15 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/13/21 0.15 0.2 ND ND ND ND ND ND ND ND ND 0.476 ND NS NS NS ND ND ND ND ND NS ug/L 10/19/21 0.15 0.2 -- ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS Nickel Total ug/L 06/20/18 2.2 -- 50 4.03 B 3.14 B ND 2.30 B ND ND ND NC 2L = 100 ug/L ug/L 11/27/18 2.2 10 -- ND ND ND ND ND ug/L 04/02/19 2.2 10 ND ND ND ND ND ug/L 11/19/19 2.2 10 ND ND ND ND ND ND ND ug/L 04/07/20 2.2 10 ND ND ND ND ND ND ND ND ug/L 10/13/20 2.2 10 ND ND ND ND ND ND ND ND ND ND ND ANR ANR ANR ANR ANR ANR ANR ANR ND ug/L 04/13/21 2.2 10 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ANR ANR ANR ANR ANR NS ug/L 10/19/21 2.2 10 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ANR ANR ANR ANR ANR NS T:-Proj--358-20-043A Moore Cowry R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 Appendix III -RI51oMc G-21-10 WQMR Tables Fa App,d - Page 7 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells DetectedActive Constituent/Parameter Selenium Units ug/L D.MW-501VD- 04/28/06 -- -- -- ND -- ND -- =���E6" -- -- -- ND MW-11SR -- MW-1 ND MW-2 ND ND ND ND ND MW-9 ND MW-15/15R ND AM ND NC 2L = 20 ug/L ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND ND ND EPA MCL = 50 ug/L ug/L 04/24/07 -- ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/30/07 -- -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND ug/L 04/23/08 10 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/06/08 -- -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND ug/L 04/13/09 -- -- 10 ND -- 6.4 B -- -- -- -- ND -- ND ND ND 4.7 B 13.9 B ND 14.6 B 15.2 B ND ug/L 10/15/09 10 ND ND ND ND ND ND ND ND 1.02 B 2.47 B ND ND ug/L 04/26/10 -- -- 10 ND -- 1.35 J -- -- -- -- ND -- ND ND ND 1.17 J 1.18 J ND ND 3.22 J ND ug/L 10/19/10 -- -- 10 ND -- ND -- -- -- -- ND -- ND 2.48 J 1.09 J 0.919 J 2.88 J 1.30 J 4.50 J 1.49 J ND ug/L 04/18/11 10 ND ND 4.90 J ND ND ND ND ND ND ND ND ND ug/L 10/10/11 -- -- 10 ND -- ND -- -- -- -- ND -- ND ND 2.71 J ND ND ND ND Dry ND ug/L 04/17/12 10 ND 5.54 (ND) J 2.86 (ND) J ND ND ND 4.55 (ND) J ND ND ND Dry ND ug/L 10/09/12 10 ND ND ND ND ND ND ND ND ND 12.4 Dry ND ug/L 04/15/13 -- -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND Dry ND ug/L 09/30/13 10 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/16/14 -- -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND Dry ND ug/L 10/15/14 5.0 -- 10 Dry -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND Dry ND ug/L 04/15/15 5.0 10 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/07/15 5.0 -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND ug/L 04/11/16 5.0 -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND ug/L 11/30/16 6.2 -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND ug/L 04/11/17 6.2 -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND ug/L 12/12/17 6.2 10 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 06/20/18 6.2 -- 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/27/18 6.2 10 -- ND ND ND -- -- -- -- ND ND ND ND ND ND ND ND ND ND ND ug/L 04/02/19 6.2 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/19/19 6.2 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/07/20 6.2 10 -- ND ND ND ND ND ND -- ND ND NS NS NS ND ND ND ND ND -- ug/L 10/13/20 6.2 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/13/21 6.2 10 -- ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/19/21 6.2 10 -- ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS Silver ug/L 04/28/06 -- -- -- ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND NC 2L = 20 ug/L ug/L 10/09/06 -- -- -- ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND EPA MCL = 100 ug/L" ug/L 04/24/07 -- ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/30/07 -- -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND ug/L 04/23/08 10 2.8 B ND ND ND ND ND ND ND ND ND ND ND ug/L 10/06/08 10 ND ND ND ND ND ND ND ND ND 4.6 B ND ND ug/L 04/13/09 -- -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND ug/L 10/15/09 10 ND ND ND ND ND ND ND ND ND 3.03 J ND ND ug/L 04/26/10 -- -- 10 ND -- 5.35 J -- -- -- -- ND -- ND ND ND 3.86 J 5.70 J 5.29 J 5.55 J 2.17 J ND ug/L 10/19/10 -- -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND ug/L 04/18/11 10 ND 5.35 J ND ND ND ND 5.13 J ND ND 5.64 J 1.95 J ND ug/L 10/10/11 -- -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND 9.37 J ND ND Dry ND ug/L 04/17/12 -- -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND Dry ND ug/L 10/09/12 10 ND ND ND ND ND ND ND 2.66 J ND 2.43 J Dry ND ug/L 04/15/13 -- -- 10 ND -- 2.19 J -- -- -- -- ND -- ND ND ND ND ND ND ND Dry ND ug/L 09/30/13 10 ND 4.10 J ND ND ND ND 4.63 J 5.55 J 4.09 J 2.61 J Dry ND ug/L 04/16/14 10 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/15/14 1.9 -- 10 Dry -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND Dry ND ug/L 04/15/15 1.9 10 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/07/15 1.9 10 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/11/16 1.9 -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND ug/L 11/30/16 1.9 10 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/11/17 1.9 -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND 1.92 J ND ND ND ND ug/L 12/12/17 1.9 -- 10 ND -- ND -- -- -- -- ND -- ND ND ND ND ND 2.43 B ND ND ND ug/L 06/20/18 1.9 -- 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/27/18 1.9 10 -- ND ND ND -- -- -- -- ND ND ND ND ND ND ND ND ND ND ND ug/L 04/02/19 1.9 10 -- ND ND ND -- -- -- -- ND ND ND ND ND ND ND ND ND ND ND ug/L 11/19/19 1.9 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/07/20 1.9 10 -- ND ND ND ND ND ND -- ND ND NS NS NS ND ND ND ND ND NS ug/L 10/13/20 1.9 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/13/21 1.9 10 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/19/21 1.9 10 -- ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS T:-Proj--358-20-043A Moore County R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 AppendixIII- RlsioMc G-21-10 WQMR Tables Fa App,d - Page 8 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A DetectedActive Constituent/Parameter Vanadium Total NC 2L IMAC = 0.3 ug/L Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Date 06/20/18 11/27/18 04/02/19 11/19/19 04/07/20 10/13/20 04/13/21 10/19/21 1.4 1.4 1.4 1.4 1.4 1.4 1.4 1.4 -- 10 10 10 10 10 10 10 25 -- MW-50OW-13SR ND ND ND ND ND ND ND ND 2.86 1.65 1.65 ND ND 1.70 ND ND J J J J 2.15 ND ND MW-13DR ND ND ND C&D MW-14 3.60 1.95 1.65 ND 1.55 4.83 ND ND Monitoring J J J J J Wells MW-1 7S -- -- ND ND ND ND ND MW-17D -- -- ND 2.02 J ND ND ND -- -- ND 2.34 J ND ND -- -- ND ND ND ND ND ND 1.92 ND ND ND 2.2 MW-11SR 3.39 J 2.90 J 2.46 J J ND ND 2.32 J ND J ND MW-1 -- -- ANR NS ANR Closed MW-2 -- -- ANR NS ANR MSW Monitoring MW-3 -- -- ANR NS ANR Wells & MNA MW-6 Jdn"8 4.40 J -- ANR ANR ANR Performance 3.09 J -- ANR ANR ANR Monitoring -- -- ANR ANR ANR Wells M�= -- -- ANR ANR ANR -- -- ANR ANR ANR -- -- ANR NS ND Zinc ug/L 03/05/90 -- -- 34 26 43 79 11 ND NC 2L = 1000 ug/L ug/L 03/21/91 ND ND 24 24 ND ND EPA MCL = 5000 ug/L ug/L 03/10/92 30 31 40 31 21 -- -- -- -- ND ug/L 04/20/95 35 -- -- -- -- 47 60 49 51 ND ug/L 06/27/95 - -- -- -- -- ND ug/L 09/22/95 ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 ND ND ND ND ND ND ND ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/27/99 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/21/99 ND ND ND ND ND ND ND ND ug/L 03/14/00 ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 ND ND ND ND ND ND ND ND ug/L 10/11/01 ND ND ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 ND ND ND ND ND ND ND ND ug/L 04/09/03 ND ND ND ND ND ND ND ND ug/L 10/13/03 ND ND ND ND ND ND ND ND ug/L 04/26/04 ND ND ND ND ND ND ND ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND ND ND ND ND ND ug/L 10/04/05 ND ND ND ND ND ND ND ND ug/L 04/28/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/09/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/24/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/30/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/23/08 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 06/20/18 4.4 -- 10 ND ND ND ND ND ND ND ug/L 11/27/18 4.4 10 -- ND ND ND ND ND ug/L 04/02/19 4.4 10 ND ND ND ND ND ug/L 11/19/19 4.4 10 ND ND 5.24 J ND ND 22.6 ND ug/L 04/07/20 4.4 10 ND 27.7 ND ND ND ND ND ND ug/L 10/13/20 4.4 10 ND ND 455 ND 4.83 J ND ND ND ND ND ND ANR ANR ANR ANR ANR ANR ANR ANR ANR ug/L 04/13/21 4.4 10 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ANR ANR ANR ANR ANR NS ug/L 10/19/21 4.4 10 ND ND 26.8 J ND ND ND ND ND ND ND ND ANR ANR ANR ANR ANR ANR ANR ANR ANR T:-Proj--358-20-043A Moore Cowry R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 Appendix III -RI51oMc G-21-10 WQMR Tables Fa App,d - Page 9 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells DetectedActive Constituent/Parameter Iron Units ug/L Date 03/05/90 -- -- -- MW-501V 1469 MMW 13MSR -- MW-13DR MW-14 -- MW-1 7S -- -- -- -- 419 MW-11SR -- MW-1 239 MW-2 1110 MW-3 394 MW-6 -- MW-7 -- MW-8 -- M�= -- -- ND NC 2L = 300 ug/L ug/L 03/21/91 -- -- -- 7800 -- -- -- -- -- -- 700 -- 2510 17000 6500 -- -- -- -- -- ND EPA MCL = 300 ug/L ug/L 03/10/92 213 463 90 3110 323 -- -- -- -- ND ug/L 04/20/95 -- -- -- 186 -- -- -- -- -- -- -- -- -- -- -- 1340 9600 51200 71500 -- ND ug/L 06/27/95 - -- -- -- -- ND ug/L 09/22/95 ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 ND ND ND ND ND ND ND ND ug/L 04/27/99 ND ND ND ND ND ND ND ND ug/L 10/21/99 ND ND ND ND ND ND ND ND ug/L 03/14/00 ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/09/03 ND ND ND ND ND ND ND ND ug/L 10/13/03 ND ND ND ND ND ND ND ND ug/L 04/26/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/25/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/28/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/09/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/24/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/30/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/23/08 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 06/20/18 22 -- 300 72.9 J 83,700 135,000 1,790 144,000 ug/L 11/27/18 22 50 -- ND 88,300 142,000 417 141,000 ug/L 04/02/19 22 50 ND 82,700 134,000 -- -- 440 129,000 ug/L 11/19/19 22 50 -- ND 75,900 152,000 38,400 181 -- -- 15,500 101,000 -- -- -- -- -- -- -- -- -- ug/L 04/07/20 22 50 ND 52,300 141,000 2,670 448 111,000 2,510 101,000 ug/L 10/13/20 22 50 -- ND 83,800 66,200 7,600 139,000 14,400 2,500 103,000 ND 397 119,000 ANR ANR ANR ANR ANR ANR ANR ANR ANR ug/L 04/13/21 22 50 -- ND 94,700 78,700 8,000 45,900 9,390 1,470 131,000 60,400 19,300 123,000 INS INS INS ANR ANR ANR ANR ANR INS ug/L 10/19/21 22 50 -- ND 72,500 58,600 8,430 136,000 48,700 2,200 93,400 305 1,130 88,200 ANR ANR ANR ANR ANR ANR ANR ANR ANR T:-Proj--358-20-043A Moore County R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 Appendix III -RI51oMc G-21-10 WQMR Tables Fa App,d - Page 10 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells DetectedActive Constituent/Parameter wiiii& Manganese Units ug/L D.MW-501VD- 03/05/90 -- -- -- ND -- -- -- -- -- -- ND MW-11SR -- MW-1 31 MW-2 ND ND -- -- -- M�= -- -- ND NC 2L = 50 ug/L ug/L 03/21/91 -- -- -- 20 -- -- -- -- -- -- 14 -- 50 50 13 -- -- -- -- -- ND EPA MCL = 50 ug/L ug/L 03/10/92 ND ND 47 32 ND -- -- -- -- ND ug/L 04/20/95 ND -- -- 23 23 1020 173 ND ug/L 06/27/95 -- -- -- -- ND ug/L 09/22/95 ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 ND ND ND ND ND ND ND ND ug/L 04/27/99 ND ND ND ND ND ND ND ND ug/L 10/21/99 ND ND ND ND ND ND ND ND ug/L 03/14/00 ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/11/01 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/09/03 ND ND ND ND ND ND ND ND ug/L 10/13/03 ND ND ND ND ND ND ND ND ug/L 04/26/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/25/04 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/04/05 -- -- -- ND -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/28/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/09/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/24/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/30/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/23/08 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 06/20/18 1.5 -- 50 ND 200 186 -- -- -- -- 40.2 J 346 -- -- -- -- -- -- -- -- -- ug/L 11/27/18 1.5 10 -- 1.73 J 203 185 -- -- -- -- 103 384 -- -- -- -- -- -- -- -- -- ug/L 04/02/19 1.5 10 -- 3.52 J 190 174 -- -- -- -- 185 443 -- -- -- -- -- -- -- -- -- ug/L 11/19/19 1.5 10 2.68 J 191 212 114 2.71 J -- 131 248 ug/L 04/07/20 1.5 10 1.59 J 166 229 99.6 8.4 J 228 53 258 ug/L 10/13/20 1.5 10 -- 2.85 J 180 569 123 183 164 47.8 227 ND 11 294 ANR ANR ANR ANR ANR ANR ANR ANR ANR ug/L 04/13/21 1.5 10 -- 4.80 J 178 683 150 68 104 37.3 241 229 327 372 NS NS NS ANR ANR ANR ANR ANR NS ug/L 10/19/21 1.5 10 -- 2.13 J 156 560 71.8 176 181 19.4 154 2.52 J 34 259 ANR ANR ANR ANR ANR ANR ANR ANR ANR T:—Proj--358-20-043A Moore County R-Im LFG6 WQ Mon1-1,g—, 03-S--Annual WQ 2021-2022Te112021 Appendix III -RI51oMc G-21-10 WQMR Tables Fa App,d — Page 11 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituent/Parameter Acetone Units ug/L Sample Date 0:3/05/90 MDL PQL SWSL MW-501V MMW 13MSR MW-13DR MW-14 MW-1 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 MW-9�= NC 2L = 6000 ug/L ug/L 03/21/91 ND ug/L 03/10/92 ND ug/L 04/20/95 ND ug/L 06/27/95 ND ND ND ND ug/L 09/22/95 ND ND ND ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 ND ND ND ND ND ND ND ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 ND ND ND ND 3085 ND ND ND ug/L 04/27/99 ND ND ND 541 ND ND ND ND ug/L 10/21/99 ND ND 335 390 108 ND ND ND ug/L 03/14/00 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/19/00 ND ND ND ND 728 ND 139 ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 ND ND 185 ND 2628 ND ND ND ug/L 10/11/01 ND ND ND ND ND ND ND ND ug/L 04/18/02 ND ND 129 ND ND ND ND ND ug/L 10/08/02 ND ND 422 110 ND ND ND ND ug/L 04/09/03 ND ND ND 192 119 ND ND ND ug/L 10/13/03 ND ND 125 113 361 ND ND ND ug/L 04/26/04 ND ND ND ND ND ND ND ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND 1400 123 ND ND ND ug/L 10/04/05 ND ND ND ND ND ND ND ND ug/L 04/28/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/24/07 ND ND ND ND ND ND ND 138 ND ND ND ND ug/L 10/30/07 100 ND 4.8 J ND ND ND ND 380 60 16 7.7 5.6 ND ug/L 04/23/08 100 ND ND 5.7 J ND ND ND 420 120 220 10 J ND ND ug/L 10/06/08 100 ND 7.6 B ND ND ND ND 1100 160 56 J 20 B 210 ND ug/L 04/13/09 100 ND ND ND ND ND ND 48 J 240 160 ND 45 J ND ug/L 10/15/09 100 ND ND ND ND ND ND ND 78 J ND ND ND ND ug/L 04/26/10 100 ND ND ND ND ND ND 80 J 25 J 77 J 8.9 J 140 ND ug/L 10/19/10 100 ND ND ND ND ND ND 180 1700 ND ND 170 ND ug/L 04/18/11 100 ND ND ND ND ND ND 29 J 36 J ND 36 J ND ND ug/L 10/10/11 100 ND ND ND ND ND ND 15 J -- ND 5.0 J Dry ND ug/L 04/17/12 100 ND ND ND ND ND ND 10 J 56 J 12 J 18 J Dry ND ug/L 10/09/12 100 ND ND ND ND ND ND ND 290 ND 13 J Dry ND ug/L 04/15/13 100 ND ND ND ND ND ND 150 88 J 73 J 12 J Dry ND ug/L 09/30/13 100 ND ND ND ND ND ND 94 J 24 J 9.8 J 5.5 J Dry ND ug/L 04/16/14 100 ND ND ND ND ND ND 280 36 J 6.3 J 15 J Dry ND ug/L 10/15/14 1.2 100 Dry ND ND ND ND ND 16 J 110 6.6 J 12 J Dry ND ug/L 04/15/15 1.2 100 ND ND ND ND ND ND 210 110 16 J 7.0 J Dry ND ug/L 10/07/15 1.2 100 ND ND ND ND ND ND 130 200 6.4 J 2.6 J 98 J ND ug/L 04/11/16 1.2 100 ND ND ND ND ND ND 290 110 ND 55 J 300 ND ug/L 11/30/16 10 100 ND ND ND ND ND ND 46 J 10 J ND 19 J 980 ND ug/L 04/11/17 10 100 ND ND ND ND ND ND ND 20 J ND ND 880 ND ug/L 12/12/17 10 100 ND ND ND ND ND ND ND ND ND 11 J 20 J ND ug/L 06/20/18 10 -- 100 ND ND ND ND ND ND ND ND 20 B 19 B 11 B 20 B ND ND ug/L 11/27/18 10 20 -- ND ND ND ND ND ND ND ND 28 190 56 57 ND ND ug/L 04/02/19 10 20 ND ND ND ND ND ND ND ND 12 J 490 21 ND ND ND ug/L 11/19/19 10 20 ND ND ND ND ND ND ND ND ND ND ND 12 J ND ND 190 ND ug/L 04/07/20 10 20 ND ND ND ND ND ND ND ND NS NS NS 26 59 ND 17 J ND NS ug/L 10/13/20 10 20 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 490 D ND ND ND ND ug/L 04/13/21 10 20 ND ND ND ND 120 ND ND 11 J 22 ND 10 NS NS NS 46 75 ND ND ND NS ug/L 10/19/21 10 20 ND ND ND ND ND ND 18 J ND ND ND ND ND ND 27 270 ND ND ND ND T—Plj--358-20-043A — —ty R-Im LFG & WQ —1-1,g—, 03 - S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11— G-21 -10 WQMR Tables F, App,dk— Page 12 of 31 mBLsSA Record mGroundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April no,Monitoring Event Moore County Landfill, woSolid Waste Permit No. o`-0, Aberdeen, Moore County, North Carolina xmmsProject No. *`58-2o-0*`^ *nz"ne ug/L 0310e9 - - - - - - - - - - - - - - - - - - - ' wo mo'~,ugu ug/L 03/21m1 - - - - - - - - - - - - - - - - - - - - wo :PA MCL~ougu ug/L 03m0/92 - - - - - - - - - - - - - - - - - - - - wo ug/L 04/20m5 - - - - - - - - - - - - - - - - - - - - wo ug/L worm, - - - - - - - - - - - - - - - wo zx uo 9.8 - wo ug/L 09/22m5 - - - wo - - - - - - wo - wo wo wo wo wo o o - wo ug/L 03/28m6 - - - wo - - - - - - - - wo wo - ,o wn , o - wo ug/L 10/29m6 - - - wo - wo - - - - - - - - - wo wo wo o o wo ug/L owomo - - - wo - mo - - - - - - - - - wo wo wo o / wo ug/L 10/29m7 - - - wo - wo - - - - - - - - - , wn wo o., ,, wo ug/L owomo - - - wo - wo - - - - - - - - - wo 6.6 wo 6.4 ,, wo ug/L 10n4/98 - - - wo - wo - - - - - - - - - wo wo wo wo u, wo ug/L 04/27m9 - - - wo - 5.3 - - - - - - - - - wo wn wo 6.2 m wo ug/L 10o1m9 - - - wo - wo - - - - - - - - - wo wo wo wo ,, wo ug/L wmmm - - - wo - wo - - - - wo - wo , wo x wn wo ^ ,, wo ug/L 04m9/00 - - - wo - wo - - - - - - - - - wo wn wo wo zx wo ug/L 10n7/00 - - - wo - wo - - - - - - - - - wo wo , 5.2 9.2 wo ug/L 04m0m1 - - - wo - wo - - - - - - - - - wo wn wo 5.1 ox wo ug/L 10n1m1 - - - wo - wo - - - - - - - - - wo wo wo wo o wo ug/L 04m8/02 - - - wo - wo - - - - - - - - - wo wo , wo wo wo ug/L 10/08/0 - - - wo - wo - - - - - - - - - wo wn wo wo wo wo ug/L owomo - - - wo - wo - - - - - - - - - wo wo wo wo 6.8 wo ug/L 10n3/03 - - - wo - wo - - - - - - - - - wo wo wo wo 8.9 wo ug/L 04/26m4 - - - wo - wo - - - - - - - - - wo wn wo wo 8.4 wo ug/L 10/25m4 - - - wo - wo - - - - - - - - - wo wo wo wo 6.8 wo ug/L owowo - - - wo - wo - - - - - - - - - wo wn wo wo 7.9 wo ug/L 10/04/0 - - - wo - wo - - - - - - - - - wo wn wo wo 6.5 wo ug/L 04/28m6 - - - wo - wo - - - - wo - wo wo wo wo wo wo wo 6.6 wo ug/L 10/09/0 - - - wo - wo - - - - wo - wo wo wo wo wn wo wo 5.5 wo ug/L 04/24m7 - - - wo - - - wo - - - - wo - wo wo wo wo wn ^, `., `.` wo ug/L 10/30/07 - - ` wo - - - e.2 - - - - wo - wo 1.2 wo 3.0 ,., e.7 `.z *.2 wo ug/L 04/23m8 - - ` wo - - - e., - - - - wo - wo nam J wo wo 2.8 mw J ^o wo wo ug/L 10/06/0 - - ' wo - - - wo - - - - wo - wo vyr J wo wo ,^ e.2 ,., u* wo ug/L 04m3/09 - - ' wo - - - e.3 - - - - wo - wo wo wo e.6 wo 3.1 `^ ,v wo ug/L 10n5/09 - - , wo - - - e.2 - - - - o/m J - ,, 1.4 wo 3.4 ,.` e.9 `., 4.0 mn ug/L 04/26n0 - - ' wo - - - e., - - - - wo - wo 1.1 wo e.2 x^ 3.1 3.6 ,, wo ug/L 10n9n0 - - ' wo - - - e.3 - - - - wo - wo 1.0 wo 3.1 wo uo 3.6 4.6 wo ug/L 04m8n1 - - , wo - - - wo - - - - wo - wo wo wo wo 0.80 J uo wn 4.1 mn ug/L 10n0n1 - - ' wo - - - e.2 - - - - wo - wo ,.o wo 3.4 - u* `., mv wo ug/L 04m7n2 - - , wo - - - e.3 - - - - wo - o.m J 1.0 wo `.o ,.z *.3 `.v mv wo ug/L 10/09/2 - - , wo - - - e.0 - - - - wo - o.o^ J 1.2 wo 2.2 2.2 uo ^o mv wo ug/L wmono - - ' wo - - - e.1 - - - - wo - wo 0,4 J wo 2.4 ,, uo ^.z mv wo ug/L omomo - - , wo - - - e.1 - - - - wo - wo n/m J wo 2.2 z., 2.4 `^ mv wo ug/L 04m6w4 - - ' wo - - - e.0 - - - - wo - wo vsr J wo ,.o ,.o 2.8 `.` mv wo ug/L 10n5n4 o.m - ' Dry - - - 1.9 - - - - wo - wo 0.81 J wo ,.o ,.o `y `^ mv wo ug/L wm,w, o.m - , wo - - - 1.2 - - - - wo - wo 0.81 J wo ,., 0.69 J 1.9 2.9 mv wo ug/L 10/07n5 o.m - ' wo - - - e.4 - - - - wo - wo vav J wo 3.9 1.6 3.1 `.o ux wo ug/L 04m1n6 o.m - ' wo - - - e.2 - - - - wo - wo v/w J wo ,.o 0.6* J u, `u 2.8 wo ug/L 11m0/6 o.m - , wo - - - e.0 - - - - wo - wo n/o J wo 2.6 1.4 e.9 2.9 `x wo ug/L 04m1n7 o.m - , wo - - - e.2 - - - - wo - wo 1.2 wo ,.o wo uo ^^ o^ wo ug/L 12n2n7 o.m - ` wo - - - 1.4 - - - - wo - o.m J naw J wo 2^ 1.1 e.7 `., ^^ wo ug/L womo o.m - ` wo ,.z - - 1.6 - - - - wo ,^ wo 1.0 wo 2.5 1.1 ux `^ ,., wo ug/L 11o7/8 o.m , - wo zo - - e.0 - - - - wo ,.o wo wo wo 3.3 o.m J e.3 `.v ,.n wo ug/L ow000 o.m , - wo z, - - 1.6 - - - - wo ,., wo v/m J wo `^ 1.1 J e.7 `^ ,.0 wo ug/L 11n9n9 o.m , - wo ,.o - - e.3 wo wo - - wo ,.o o,m J vyr J wo `.r 1.6 e.9 `u 5.7 wo (Verification Event) ug/L 01m8/20 o.m , - - - - - - - - - - - - - - - - - ' ,., wo ug/L owmoo o.m , - wo ,.o - - 1.7 wo mo 1.6 - wo `., - - - ,^ wo e., `.v ,., wo (Verification Event) ug/L 06/05/20 o.m , - - - - - - - - ,.z - - - wu wu wo - - - ' - wo ug/L 10n3/20 o.m , - wo ,.o wo wo e.2 wo wo uoo J wo wo 3.2 wo 0.54 J wo ,., wo e.8 ^.o 1.2 wo ug/L 04m3o1 0.15 , - wo z, wo wo wo wo wo 1.20 wo wo e.7 wa wu wo 2.6 , 3.2 3.2 0.8 J wo | "n/L | ,m,mu, | o^o | , | - | wo | wo wo ,.r wo wo wo wo | wo wo wo ,.o ,^ o^ 2.2 wo | wo -ty R-Im LFG & WQ -1-1,g-,°- S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11- G-=WQMR �-~Ap�,dk- Page owo TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituent/Parameter Chlorobenzene Units ug/L Sample Date 0:3/05/90 MDL PQL SWSL MW-501V MMW 13MSR MW-13DR MW-14 MW-1 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 MW-9�= NC 2L = 50 ug/L ug/L 03/21/91 ND EPA MCL = 100 ug/L ug/L 03/10/92 ND ug/L 04/20/95 -- ND ug/L 06/27/95 ND ND ND 6.5 ND ug/L 09/22/95 ND ND ND ND ND ND ND ND 6 ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 ND ND ND ND ND 7.5 ND ND ug/L 04/30/98 ND ND ND ND ND 5.4 ND ND ug/L 10/14/98 ND ND ND ND ND 5.1 ND ND ug/L 04/27199 ND ND ND ND ND 6.1 ND ND ug/L 10/21/99 ND ND -- ND ND ND 7.1 ND ND ug/L 03/14/00 ND ND ND ND 3 ND ND ND ND 6 ND ND ug/L 04/19/00 ND ND -- ND ND ND 5.5 ND ND ug/L 10/17/00 ND ND ND ND ND 12 ND ND ug/L 04/10/01 ND ND ND ND ND 7.3 ND ND ug/L 10/11/01 ND ND ND ND ND 13 ND ND ug/L 04/18/02 ND ND ND ND ND 10.5 ND ND ug/L 10/08/02 ND ND ND ND ND 8.6 ND ND ug/L 04/09/03 ND ND ND ND ND 8.6 ND ND ug/L 10/13/03 ND ND ND ND ND 10.8 ND ND ug/L 04/26/04 ND ND ND ND ND 10.9 ND ND ug/L 10/25/04 ND ND ND ND ND 11.9 ND ND ug/L 04/04/05 ND ND ND ND ND 9 ND ND ug/L 10/04/05 ND ND ND ND ND 9.1 ND ND ug/L 04/28/06 ND ND ND ND ND ND ND ND ND 7.8 ND ND ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/24/07 ND ND ND ND 3.2 ND ND ND ND 9.1 ND ND ug/L 10/30/07 3 ND 3.0 ND ND 4.0 ND 0.93 J 0.98 J 2.4 J 9.2 0.48 J ND ug/L 04/23/08 3 ND 2.7 J ND ND 2.5 J ND ND 0.45 J ND 9.9 ND ND ug/L 10/06/08 3 ND 2.1 J ND ND 2.6 J ND ND 0.93 J ND 9.0 ND ND ug/L 04/13/09 3 ND 2.9 J ND ND 3.4 ND 0.71 J ND 1.1 J 11 ND ND ug/L 10/15/09 3 ND 3.2 ND 8.4 3.8 ND 1.2 J 1.0 J 2.9 J 11 0.57 J ND ug/L 04/26/10 3 ND 3.2 ND ND 2.7 J ND 0.81 J 0.61 J 1.0 J 11 ND ND ug/L 10/19/10 3 ND 3.0 ND ND 3.1 ND 0.99 J ND 1.5 J 10 ND ND ug/L 04/18/11 3 ND 3.2 ND ND 2.6 J ND ND 0.81 J 2.7 J 7.8 ND ND ug/L 10/10/11 3 ND 3.9 ND 6.7 3.0 ND 1.6 J -- 3.6 9.6 Dry ND ug/L 04/17/12 3 ND 3.6 ND 6.3 2.8 J ND 1.4 J 0.86 J 2.3 J 12 Dry ND ug/L 10/09/12 3 ND 3.5 ND 5.6 3.1 ND 1.3 J 1.4 J 2.5 J 11 Dry ND ug/L 04/15/13 3 ND 3.1 ND ND 1.9 J ND 1.1 J 0.41 J 1.1 J 10 Dry ND ug/L 09/30/13 3 ND 2.5 J ND ND 1.2 J ND 1.2 J 1.0 J 0.64 J 9.2 Dry ND ug/L 04/16/14 3 ND 3.3 ND ND 1.8 J ND 1.2 J 0.75 J 0.74 J 9.1 Dry ND ug/L 10/15/14 0.17 3 Dry 2.6 J ND 1.6 J 2.1 J ND 0.96 J 1.4 J 3.1 10 Dry ND ug/L 04/15/15 0.17 3 ND 2.7 J ND ND 2.1 J ND 0.69 J ND 1.1 J 10 Dry ND ug/L 10/07/15 0.17 3 ND 2.6 J ND ND 2.3 J ND 1.2 J 1.8 J 3.6 9.9 0.64 J ND ug/L 04/11/16 0.17 3 ND 2.6 J ND ND 1.2 J ND 0.74 J ND 2.1 J 10 ND ND ug/L 11/30/16 0.17 3 ND 2.3 J ND ND 1.4 J ND 1.0 J 1.4 J 3.1 8.4 ND ND ug/L 04/11/17 0.17 3 ND 2.6 J ND ND 3.3 ND 1.4 J ND 4.6 12 ND ND ug/L 12/12/17 0.17 3 ND -- 1.2 J ND -- 7.1 2.1 J ND ND 1.4 J 4.0 10 0.62 J ND ug/L 06/20/18 0.17 3 ND 0.62 J 2.9 J ND 1.3 J ND 2.8 J ND 1.8 J 0.93 J 2.8 J 10 0.40 J ND ug/L 11/27/18 0.17 1 -- ND 0.97 J 3.5 ND 1.0 ND 0.90 J ND 1.6 0.46 J 0.91 J 7.4 ND ND ug/L 04/02/19 0.17 1 ND 1.2 3.4 ND 1.0 ND 1.3 ND 1.4 ND 1.2 9.3 0.44 J ND ug/L 11/19/19 0.17 1 ND 0.90 J 5.1 ND ND -- ND 1.3 3.7 2.6 ND 1.9 4.1 6.1 11 0.91 J ND ug/L 04/07/20 0.17 1 ND ND 5.3 ND ND 1.2 ND 1.6 NS NS NS 1.2 ND 1.9 9.6 ND NS ug/L 10/13/20 0.17 1 ND ND ND ND 5.8 ND ND 0.88 J ND ND 1.9 ND 1.2 ND 1.6 ND 4.3 8.9 ND ND ug/L 04/13/21 0.17 1 ND 1.3 ND ND 1.5 ND ND 0.91 J ND 0.53 J 1.6 NS NS NS 1.5 0.9 J 3.8 10.0 ND NS ug/L 10/19/21 0.17 1 ND 1.2 ND ND 5.2 ND ND 0.93 J ND ND 1.2 NS 2.6 ND 1.7 1.9 J 6.7 6.2 ND ND T-Plj--358-20-043A - County R-Im LFG & WQ -1-1,g-, 03 - S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11- G-21 -10 WQMR Tables F, App,dk- Page 14 of 31 mBLsSA Record mGroundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April no,Monitoring Event Moore County Landfill, woSolid Waste Permit No. o`-0, Aberdeen, Moore County, North Carolina xmmsProject No. *`58-2o-0*`^ NC 2L~3000"g/L ug/L 0310e9 - - - - - - - - - - - - - - - - - - - - - ' wo ug/L 03/21m1 - - - - - ' ' - - - - - - - - - - - - - - - wo ug/L 03m0/92 - - - - - ' ' - - - - - - - - - - - - - - - wo ug/L 04/20m5 - - - - - ' ' - - - - - - - - - - - - - - - wo ug/L worm, - - - - - ' - - - - - - - - - - - 13.3 ^, va u, - wo ug/L 09/22m5 - - - wo - ' - - - - - - wo - wo wo wo o ,* wo wo - wo ug/L 03/28m6 - - - wo - ' - - - - - - - - wo wo - 23 `« wo wo - wo ug/L 10/29m6 - - - wo - ' - wo - - - - - - - - - wo wo wo wo wo wo ug/L owomo - - - wo - ' - wo - - - - - - - - - 23 wo wo wo wo wo ug/L 10/29m7 - - - wo - ' - wo - - - - - - - - - 17 wn wo wo wo wo ug/L owomo - - - wo - ' - wo - - - - - - - - - 19 wo wo wo wo wo ug/L 10n4/98 - - - wo - ' - wo - - - - - - - - - m wo wo wo wo wo ug/L 04/27m9 - - - wo - - - wo - - - - - - - - - m wn wo wo wo wo ug/L 10o1m9 - - - wo - - - wo - - - - - - - - - 11 wo wo wo wo wo ug/L wmmm - - - wo - - - wo - - - - wo - wo wo wo 6 wn wo wo 2 wo ug/L 04m9/00 - - - wo - - - wo - - - - - - - - - wo wn wo wo wo wo ug/L 10n7/00 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L 04m0m1 - - - wo - - - wo - - - - - - - - - wo wn wo wo wo wo ug/L 10n1m1 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L 04m8/02 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L 10/08/0 - - - wo - - - wo - - - - - - - - - wo wn wo wo wo wo ug/L owomo - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L 10n3/03 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L 04/26m4 - - - wo - - - wo - - - - - - - - - wo wn wo wo wo wo ug/L 10/25m4 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L owowo - - - wo - - - wo - - - - - - - - - wo wn wo wo wo wo ug/L 10/04/0 - - - wo - - - wo - - - - - - - - - wo wn wo wo wo wo ug/L 04/28m6 - - - wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L 10/09/0 - - - wo - - - wo - - - - wo - wo wo wo wo wn wo wo wo wo ug/L 04/24m7 - - - wo - - - wo - - - - wo - wo wo wo wo wn wo wo wo wo ug/L 10/30/07 - - `v wo - - - wo - - - - wo - wo wo wo 1.3 J wo wo wo wo wo ug/L 04/23m8 - - `v wo - - - wo - - - - wo - wo wo wo wo wn wo wo wo wo ug/L 10/06/0 - - `v wo - - - 1.2 J - - - - wo - wo wo wo *.8 J o.,, J um J 1.3 J 2.5 J wo ug/L 04m3/09 - - `v wo - - - wo - - - - wo - wo wo wo wo wo 1.1 J wo wo wo ug/L 10n5/09 - - `v wo - - - wo - - - - wo - wo wo wo wo wn wo wo wo mo ug/L 04/26n0 - - `v wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L 10n9n0 - - `v wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L 04m8n1 - - `v wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo mo ug/L 10n0n1 - - `v wo - - - wo - - - - wo - wo wo wo wo - wo wo mv wo ug/L 04m7n2 - - `v wo - - - wo - - - - wo - wo wo wo wo wo mw J wo mv wo ug/L 10/09/2 - - `v wo - - - wo - - - - wo - wo wo wo wo wn wo wo mv wo ug/L wmono - - `v wo - - - ma J - - - - wo - wo wo wo wo wo om J wo mv wo ug/L omomo - - `v wo - - - wo - - - - wo - wo wo wo wo wn wo wo mv wo ug/L 04m6w4 - - `v wo - - - wo - - - - wo - wo wo wo wo wo wo wo mv wo ug/L 10n5n4 0.23 - `v Dry - - - wo - - - - wo - wo wo wo wo wo wo wo mv wo ug/L wm,w, 0.23 - `v wo - - - wo - - - - wo - wo wo wo wo wn wo wo mv wo ug/L 10/07n5 0.23 - `v wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L 04m1n6 0.23 - `v wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L 11m0/6 0.23 - `v wo - - - wo - - - - wo - wo wo wo wo wn wo wo wo wo ug/L 04m1n7 0.23 - `v wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L 12n2n7 0.23 - `v wo - - - wo - - - - wo - wo wo wo wo wn wo wo vs, J wo ug/L womo 0.23 - `v wo wo - - wo - - - - wo wo wo wo wo wo wn wo wo wo wo ug/L 11o7/8 0.23 , - wo wo - - wo - - - - wo wo wo wo wo wo wo wo wo wo wo ug/L ow000 0.23 , - wo wo - - wo - - - - wo wo wo wo wo wo wn wo wo wo wo ug/L 11n9n9 0.23 , - wo wo - - wo wo wo - - wo wo wo wo wo wo wn wo wo wo wo ug/L owmoo 0.23 , - wo wo - - wo wo wo wo - wo wo wu wu wu wo wo wo wo wo wo ug/L 10n3/20 0.23 , - wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo wn wo wo wo wo ug/L 04m3o1 0.23 , - wo wo wo wo wo wo wo wo wo wo wo wo wu wu wo wo wo wo wo wo ug/L | 10n9o1 | 0.23 | , | - | wo | wo wo wo wo wo wo wo wo | wo wo | wo wu wu wo wo wo wo wo | wo —ty R-Im LFG & WQ M.nl-��—.°- WQ --I.g2.21-2022T,11 2021Apndl, III - 11— G—=WQMR �-~Ap�,dk- Page mwo TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells DetectedActive Constituent/Parameter 1,2-Dichlorobenzene Units ug/L D.MW-501VD- 04/24/07 -- -- -- ND -- -- -- ND -- =���E6" -- -- -- ND MW-11SR -- MW-1 ND MW-2 ND ND ND ND ND MW-9 ND MW-1 5/15R ND M ND NC 2L = 20 ug/L ug/L 04/28/07 ND ND ND ND ND ND ND ND ND ND ND ND EPA MCL = 600 ug/L ug/L 10/09/07 -- ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/30/07 5 ND 2.7 J ND ND 0.75 J ND ND ND 0.81 J 0.61 J ND ND ug/L 04/23/08 5 ND 2.1 J ND ND 0.43 J ND ND ND ND 0.69 J ND ND ug/L 10/06/08 5 ND 1.5 J ND ND 0.42 J ND ND ND ND 0.64 J ND ND ug/L 04/13/09 5 ND 2.3 J ND ND 0.64 J ND ND ND ND 0.73 J ND ND ug/L 10/15/09 5 ND 2.2 J ND 0.62 J 0.67 J ND ND ND 0.81 J 0.69 J ND ND ug/L 04/26/10 5 ND 2.0 J ND ND 0.50 J ND ND ND ND 0.82 J ND ND ug/L 10/19/10 5 ND 2.1 J ND ND 0.53 J ND ND ND ND 0.88 J ND ND ug/L 04/18/11 5 ND 2.0 J ND ND 0.43 J ND ND ND 0.51 J 0.67 J ND ND ug/L 10/10/11 5 ND 1.9 J ND 0.47 J 0.49 J ND ND 0.86 J 0.49 J Dry ND ug/L 04/17/12 5 ND 2.0 J ND 0.49 J 0.64 J ND ND ND ND 0.66 J Dry ND ug/L 10/09/12 5 ND 2.0 J ND ND 0.49 J ND ND ND 0.48 J 0.76 J Dry ND ug/L 04/15/13 5 ND 1.7 J ND ND ND ND ND ND ND 0.65 J Dry ND ug/L 09/30/13 5 ND 1.2 J ND ND ND ND ND ND ND 0.72 J Dry ND ug/L 04/16/14 5 ND 1.7 J ND ND ND ND ND ND ND 0.68 J Dry ND ug/L 10/15/14 0.19 5 Dry 1.3 J ND ND ND ND ND ND 0.59 J 0.58 J Dry ND ug/L 04/15/15 0.19 5 ND 1.4 J ND ND ND ND ND ND ND 0.51 J Dry ND ug/L 10/07/15 0.19 5 ND 1.1 J ND ND 0.42 J ND ND ND 0.65 J ND ND ND ug/L 04/11/16 0.19 5 ND 1.0 J ND ND ND ND ND ND ND ND ND ND ug/L 11/30/16 0.19 5 ND 0.92 J ND ND ND ND ND ND ND ND ND ND ug/L 04/11/17 0.19 5 ND 0.94 J ND ND ND ND ND ND 0.57 J ND ND ND ug/L 12/12/17 0.19 5 ND 0.82 J ND 0.44 J ND ND ND ND 0.59 J ND ND ND ug/L 06/20/18 0.19 5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/27/18 0.19 1 -- ND ND 1.1 ND ND ND ND ND ND ND ND ND ND ND ug/L 04/02/19 0.19 1 ND ND 1.1 ND ND ND ND ND ND ND ND ND ND ND ug/L 11/19/19 0.19 1 ND ND 1.8 ND ND -- ND ND ND ND ND ND 0.49 J 0.84 J 0.41 J ND ND ug/L 04/07/20 0.19 1 ND ND 1.3 ND ND 0.55 J ND ND NS NS NS ND ND ND ND ND NS ug/L 10/13/20 0.19 1 ND ND ND ND 1.6 ND ND 0.52 J ND ND ND ND ND ND ND ND 0.54 J ND ND ug/L 04/13/21 0.19 1 ND 0.51 J ND ND ND ND ND 0.55 J ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/19/21 0.19 1 ND ND ND ND 1.8 ND ND ND ND ND ND ND ND ND ND ND 0.91 J ND ND ND T:-Proj--358-20-043A Moore County R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 Appendix III -RI51oMc G-21-10 WQMR Tables Fa App,d - Page 16 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituent/Parameter 1,4-Uichlorobenzene Units ug/L Sample Date 0:3/05/90 MDL PQL SWSL MW-501V MMW 13MSR MW-13DR MW-14 MW-1 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 M�F P N NC 2L = 6 ug/L ug/L 03/21/91 ND EPA MCL = 75 ug/L ug/L 03/10/92 ND ug/L 04/20/95 -- -- -- ND ug/L 06/27/95 ND 3.3 2 7.4 ND ug/L 09/22/95 ND ND ND ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND 6 ND ND ND 7 6 ND ug/L 10/29/97 ND 7.8 ND ND ND 7 6.1 ND ug/L 04/30/98 ND ND ND ND ND 7.1 ND ND ug/L 10/14/98 ND 9.7 ND ND ND 5.2 ND ND ug/L 04/27/99 ND 8.7 ND ND ND 5.9 5.6 ND ug/L 10/21/99 ND ND -- ND ND ND ND 21 ND ug/L 03/14/00 ND 2 ND ND 3 ND ND ND ND 4 ND ND ug/L 04/19/00 ND 7.5 -- ND ND ND ND 6.4 ND ug/L 10/17/00 ND 9.5 ND ND ND 10 6.3 ND ug/L 04/10/01 ND 6.7 ND ND ND 5.1 5.9 ND ug/L 10/11/01 ND ND ND ND ND 5.6 8.3 ND ug/L 04/18/02 ND ND ND ND ND 5.9 ND ND ug/L 10/08/02 ND ND ND ND ND 5.7 ND ND ug/L 04/09/03 ND ND ND ND ND 5.3 7.5 ND ug/L 10/13/03 ND ND ND ND ND 5.8 7.8 ND ug/L 04/26/04 ND 5.1 ND ND ND 5.9 6.9 ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND ND ND ND 6.1 ND ug/L 10/04/05 ND ND ND ND ND ND 6.6 ND ug/L 04/28/06 ND ND ND ND ND ND ND ND ND ND 6.8 ND ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND 6 ND ug/L 04/24/07 ND 5.3 ND ND ND ND ND ND ND 3.5 5.7 ND ug/L 10/30/07 1 ND 5.7 ND ND 1.9 ND 2.0 0.49 J 4.0 3.0 3.3 ND ug/L 04/23/08 1 ND 5.5 ND ND 1.8 ND ND ND ND 4.2 ND ND ug/L 10/06/08 1 ND 4.9 ND ND ND ND ND 1.5 ND 3.6 5.8 ND ug/L 04/13/09 1 ND 6.9 ND ND 2.3 ND 1.6 ND 0.97 J 4.2 5.9 ND ug/L 10/15/09 1 ND 5.5 ND ND 2.6 ND 3.4 1.6 4.1 3.7 5.3 ND ug/L 04/26/10 1 ND 6.0 ND ND 2.0 ND 1.8 1.2 0.67 J 3.9 4.9 ND ug/L 10/19/10 1 ND 4.2 ND ND ND ND ND ND 1.8 3.9 5.3 ND ug/L 04/18/11 1 ND 5.0 ND ND 1.5 ND 1.7 0.92 J 3.0 3.0 5.4 ND ug/L 10/10/11 1 ND 5.1 ND 0.82 J ND ND 4.0 -- 4.1 3.1 Dry ND ug/L 04/17/12 1 ND 5.2 ND ND 2.2 ND 4.3 1.1 2.6 4.0 Dry ND ug/L 10/09/12 1 ND 5.1 ND ND ND ND 3.7 1.8 3.3 4.9 Dry ND ug/L 04/15/13 1 ND 4.7 ND ND 1.9 ND 3.2 0.74 J 1.1 3.9 Dry ND ug/L 09/30/13 1 ND 4.4 ND ND ND ND 3.0 1.4 0.41 J 3.9 Dry ND ug/L 04/16/14 1 ND 4.7 ND ND ND ND 3.1 0.83 J 0.60 J 3.7 Dry ND ug/L 10/15/14 0.19 1 Dry 4.0 ND ND ND ND 2.4 1.6 4.1 3.3 Dry ND ug/L 04/15/15 0.19 1 ND 4.0 0.45 J ND ND ND 1.2 0.58 J 0.72 J 3.4 Dry ND ug/L 10/07/15 0.19 1 ND 3.9 ND ND ND ND 2.3 1.4 5.4 3.3 7.8 ND ug/L 04/11/16 0.19 1 ND 4.8 ND ND ND ND 1.4 ND 2.3 3.1 5.4 ND ug/L 11/30/16 0.19 1 ND 3.5 ND ND ND ND 1.9 1.3 3.5 2.5 4.8 ND ug/L 04/11/17 0.19 1 ND 4.4 ND ND 1.7 ND 2.8 0.63 J 6.1 3.6 5.0 ND ug/L 12/12/17 0.19 1 ND -- 2.7 ND -- 0.97 J 1.2 ND 2.4 1.3 4.6 2.7 5.1 ND ug/L 06/20/18 0.19 1 ND 1.7 4.3 ND 2.8 ND 1.9 ND 2.9 0.72 J 3.4 2.6 0.89 J ND ug/L 11/27/18 0.19 1 -- ND 2.1 4.2 ND 2.3 ND 0.53 J ND 2.6 ND 1.2 2.7 0.89 J ND ug/L 04/02/19 0.19 1 ND 2.9 4.2 ND 2.6 ND 0.74 J ND 2.0 ND 1.2 2.6 1.3 ND ug/L 11/19/19 0.19 1 ND 2.0 5.6 ND ND -- 0.46 J 2.9 0.45 J 1.2 ND 2.3 3.0 6.2 2.9 5.8 ND ug/L 04/07/20 0.19 1 ND 2.1 5.1 ND ND 2.1 ND 2.9 NS NS NS 1.3 ND 2.5 2.6 0.92 J NS ug/L 10/13/20 0.19 1 ND 2.6 ND ND 5.1 ND ND 1.8 ND ND 3.1 ND 0.59 J ND 1.7 ND 5.3 3.1 0.73 J ND ug/L 04/13/21 0.19 1 ND 3.1 ND ND ND ND ND 2.0 ND ND 2.4 NS NS NS 1.6 0.81 J 3.1 2.7 ND NS ug/L 10/19/21 0.19 1 ND ND ND ND 4.5 ND ND ND ND ND 2.6 ND ND ND 1.5 0.84 J 5.1 ND ND ND T-Plj--358-20-043A - County R-Im LFG & WQ -1-1,g-, 03 - S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11- G-21 -10 WQMR Tables F, App,dk- Page 17 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituen �Mll t/Parameter 1,1,-Dichloroethane Units ug/L Sample Date 0:3/05/90 MDL PQL SWSL MW-501V MMW 13MSR MW-13DR MW-14 MW-1 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 M�= NC 2L = 6 ug/L ug/L 03/21/91 ND ug/L 03/10/92 ND ug/L 04/20/95 ND ug/L 06/27/95 7.9 9.3 13.4 9.6 ND ug/L 09/22/95 ND ND ND 9 ND 18 10 19 12 ND ug/L 03/28/96 ND ND 11 ND 14 ND 10 -- ND ug/L 10/29/96 ND ND -- 70 7 ND 7 80 ND ug/L 04/08/97 ND 14 74 5 ND 6 72 ND ug/L 10/29/97 ND 12 64 6.2 8.3 7.5 72 ND ug/L 04/30/98 ND ND 45 8.1 ND 5.3 60 ND ug/L 10/14/98 ND 8.4 50 ND ND ND 46 ND ug/L 04/27/99 ND 9.7 37 ND ND 5.6 39 ND ug/L 10/21/99 ND ND -- 12 ND ND ND 24 ND ug/L 03/14/00 ND ND ND ND 4 ND 12 ND ND ND 20 ND ug/L 04/19/00 ND 5.9 -- 19 ND ND ND 23 ND ug/L 10/17/00 ND ND 909 ND ND ND 24 ND ug/L 04/10/01 ND 5.5 9.2 ND ND ND 23 ND ug/L 10/11/01 ND ND 16 ND 6 ND 22 ND ug/L 04/18/02 ND ND 5.5 ND ND ND ND ND ug/L 10/08/02 ND ND 5.7 ND ND ND ND ND ug/L 04/09/03 ND ND ND ND ND ND 9.5 ND ug/L 10/13/03 ND ND ND ND ND ND 11.7 ND ug/L 04/26/04 ND ND ND ND ND ND 10.7 ND ug/L 10/25/04 ND ND ND ND ND ND 8.5 ND ug/L 04/04/05 ND ND ND ND ND ND 11.5 ND ug/L 10/04/05 ND ND ND ND ND ND 10.7 ND ug/L 04/28/06 ND ND ND ND ND ND ND ND ND ND 10.1 ND ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND 17.7 ND ug/L 04/24/07 ND ND ND ND ND ND ND ND ND ND 5.9 ND ug/L 10/30/07 5 ND 1.0 J 0.69 J ND 1.1 J ND 1.4 J 0.38 J 4.3 J 0.51 J 3.6 J ND ug/L 04/23/08 5 ND 1.2 J ND ND 0.84 J ND ND 0.76 J ND 0.87 J 1.0 J ND ug/L 10/06/08 5 ND 1.2 J ND ND 0.61 J ND ND ND ND 0.83 J 7.4 ND ug/L 04/13/09 5 ND 0.79 J ND ND 0.77 J ND 0.67 J ND 0.65 J 0.74 J 4.7 J ND ug/L 10/15/09 5 ND 0.71 J 0.78 J ND 0.76 J ND 1.1 J ND 1.2 J 0.45 J 2.4 J ND ug/L 04/26/10 5 ND 0.64 J ND ND 0.56 J ND 0.51 J ND 0.86 J 0.49 J 2.8 J ND ug/L 10/19/10 5 ND 0.68 J ND ND 0.59 J ND 0.75 J ND 0.74 J 0.59 J 2.7 J ND ug/L 04/18/11 5 ND 0.69 J ND ND 0.47 J ND 0.51 J ND 1.0 J 0.50 J 2.0 J ND ug/L 10/10/11 5 ND 0.78 J 0.42 J ND 0.53 J ND 0.91 J -- 1.0 J 0.45 J Dry ND ug/L 04/17/12 5 ND 0.66 J ND ND 0.51 J ND 0.87 J ND 1.0 J 0.40 J Dry ND ug/L 10/09/12 5 ND 0.58 J ND ND 0.64 J ND 0.46 J ND 0.75 J 0.55 J Dry ND ug/L 04/15/13 5 ND 0.49 J ND ND ND ND 0.53 J ND 0.85 J 0.45 J Dry ND ug/L 09/30/13 5 ND ND ND ND ND ND 0.49 J 0.42 J ND ND Dry ND ug/L 04/16/14 5 ND ND ND ND ND ND 0.53 J ND 0.45 J 0.42 J Dry ND ug/L 10/15/14 0.13 5 Dry ND ND ND ND ND 0.50 J ND 0.87 J ND Dry ND ug/L 04/15/15 0.13 5 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/07/15 0.13 5 ND 0.73 J ND ND ND ND 0.58 J ND 0.62 J ND 1.1 J ND ug/L 04/11/16 0.13 5 ND 0.66 J ND ND ND ND ND ND 0.61 J ND 0.90 J ND ug/L 11/30/16 0.13 5 ND 0.59 J ND ND ND ND ND ND 0.70 J ND 0.77 J ND ug/L 04/11/17 0.13 5 ND 0.61 J ND ND 0.44 J ND ND ND 1.1 J ND ND ND ug/L 12/12/17 0.13 5 ND ND ND ND ND ND ND ND 0.46 J ND 0.66 J ND ug/L 06/20/18 0.13 5 ND ND ND ND ND ND ND ND ND ND 0.49 J ND ND ND ug/L 11/27/18 0.13 1 -- ND 0.64 J 0.50 J ND ND ND ND ND ND ND ND ND ND ND ug/L 04/02/19 0.13 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/19/19 0.13 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.93 J ND ug/L 04/07/20 0.13 1 ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/13/20 0.13 1 ND 0.43 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.56 J ND ND ND ug/L 04/13121 0.13 1 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND 0.56 J ND ND NS ug/L 10/19/21 0.13 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.41 J ND ND J ND ND ND T-Plj--358-20-043A - County R-Im LFG & WQ -1-1,g-, 03 - S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11- G-21 -10 WQMR Tables F, App,dk- Page 18 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A 2L = 0.4 ug/L ug/L 04/23/08 MCL = 5 ug/L ug/L 10/06/08 ug/L 04/13/09 ug/L 10/15/09 ug/L 04/26/10 ug/L 10/19/10 ug/L 04/18/11 ug/L 10/10/11 ug/L 04/17/12 ug/L 10/09/12 ug/L 04/15/13 ug/L 09/30/13 ug/L 04/16/14 ug/L 10/15/14 ug/L 04/15/15 ug/L 10/07/15 ug/L 04/11/16 ug/L 11/30/16 ug/L 04/11/17 ug/L 12/12/17 ug/L 06/20/18 ug/L 11/27/18 ug/L 04/02/19 ug/L 11/19/19 ug/L 04/07/20 ug/L 10/13/20 ug/L 04/13/21 ug/L 10/19/21 is-1,2-Dichloroethene ug/L 04/28/06 JC 2L = 70 ug/L ug/L 10/09/06 :PA MCL = 70 ug/L ug/L 04/24/07 ug/L 10/30/07 ug/L 04/23/08 ug/L 10/06/08 ug/L 04/13/09 ug/L 10/15/09 ug/L 04/26/10 ug/L 10/19/10 ug/L 04/18/11 ug/L 10/10/11 ug/L 04/17/12 ug/L 10/09/12 ug/L 04/15/13 ug/L 09/30/13 ug/L 04/16/14 ug/L 10/15/14 ug/L 04/15/15 ug/L 10/07/15 ug/L 04/11/16 ug/L 11/30/16 ug/L 04/11/17 ug/L 12/12/17 ug/L 06/20/18 ug/L 11/27/18 ug/L 04/02/19 ug/L 11/19/19 ug/L 04/07/20 ug/L 10/13/20 ug/L 04/13/21 ug/L 10/19/21 -- -- 1 ND -- -- -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND 1 ND ND ND ND ND ND ND ND ND ND ND ND 1 ND ND ND ND ND ND ND ND ND ND ND ND 1 ND ND ND ND ND ND ND ND ND ND ND ND 1 ND ND ND ND ND ND ND ND ND ND ND ND 1 ND ND ND ND ND ND ND ND ND ND ND ND 1 ND ND ND ND ND ND ND ND ND ND ND ND 1 ND ND ND ND ND ND ND ND ND Dry ND 1 ND ND ND ND ND ND ND ND ND ND Dry ND 1 ND ND ND ND ND ND ND ND ND ND Dry ND 1 ND ND ND ND ND ND ND ND ND ND Dry ND 1 ND ND ND ND ND ND ND ND ND ND Dry ND -- 1 ND ND ND ND 1.4 ND ND ND ND ND Dry ND 0.21 1 Dry ND ND ND ND ND ND ND ND ND Dry ND 0.21 1 ND ND ND ND ND ND ND ND ND ND Dry ND 0.21 1 ND ND ND ND ND ND ND ND ND ND ND ND 0.21 1 ND ND ND ND ND ND ND ND ND ND ND ND 0.21 1 ND ND ND ND ND ND ND ND ND ND ND ND 0.21 -- 1 ND -- -- -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND 0.21 -- 1 ND -- -- -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND 0.21 -- 1 ND ND -- -- ND -- -- -- -- ND ND ND ND ND ND ND ND ND ND ND 0.21 1 -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.21 1 -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.21 1 -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.21 1 -- ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS 0.21 1 -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.21 1 -- ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS 0.21 1 -- ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS -- -- -- ND 16.3 ND ND 6.4 ND 19.6 ND ND ND 18.4 NET -- ND 17.3 ND ND 5.1 ND 14.3 9.5 ND 9.3 19.4 ND -- ND 19.3 ND ND ND ND 15.3 ND ND ND 7.3 ND 5 ND 20 4.4 J ND 5.1 0.35 J 14 6.4 3.0 J 1.6 J 17 ND 5 ND 20 ND ND 3.0 J ND 3.8 J 3.1 J ND 2.2 J 3.2 J ND 5 ND 14 ND ND 2.8 J ND 5.1 5.8 ND 2.5 J 12 ND 5 ND - 14 ND ND 3.7 J ND 6.1 ND ND 2.9 J 12 ND 5 ND 17 6.2 1.9 J 4.6 J 0.41 J 15 5.1 5.0 1.8 J 16 ND 5 ND 13 0.60 J ND 2.8 J 0.43 J 7.5 3.2 J ND 2.3 J 7.2 ND 5 ND 13 ND ND 3.0 J ND 8.4 ND ND 2.8 J 10 ND 5 ND 12 ND ND 2.8 J ND 6.8 3.4 J ND 1.9 J 11 ND 5 ND 12 3.0 J 1.5 J 2.6 J ND 13 -- 2.8 J 1.6 J Dry ND 5 ND 11 1.8 J 1.4 J 2.2 J 0.39 J 16 2.8 J ND 1.6 J Dry ND 5 ND 7.0 ND 1.5 J 2.5 J ND 9.1 3.2 J ND 2.0 J Dry ND 5 ND 7.3 ND ND 1.7 J ND 11 1.2 J ND 1.7 J Dry ND 5 ND 4.0 J ND ND 1.2 J ND 5.6 2.7 J ND 1.7 J Dry ND -- 5 ND 6.7 ND ND 1.6 J ND 6.8 1.6 J ND 2.1 J Dry ND 0.15 5 Dry 5.3 0.43 J 0.70 J 1.9 J ND 4.3 J 2.5 J ND 1.2 J Dry ND 0.15 5 ND 3.4 J 3.1 J ND 2.0 J ND 1.6 J 0.47 J ND 0.89 J Dry ND 0.15 5 ND 4.3 J ND ND 1.7 J ND 2.6 J 2.7 J ND 0.69 J 1.5 J ND 0.15 5 ND 3.1 J 1.0 J ND 0.88 J ND 2.0 J 0.49 J 0.50 J 0.85 J 0.42 J ND 0.15 5 ND 3.6 J 0.58 J ND 0.68 J ND 2.0 J 2.1 J 0.52 J 0.63 J 0.53 J ND 0.15 5 ND 3.0 J ND ND 1.9 B ND 2.5 B ND 0.66 B 0.60 B ND ND 0.15 5 ND -- 2.2 J ND 1.1 J 0.81 J ND 0.68 J 1.8 J 2.0 J 0.84 J 1.0 J ND 0.15 5 ND 2.6 J 3.0 J ND 1.6 J ND 1.2 J ND 4.4 J 1.0 J ND 0.54 J 1.9 J ND 0.15 1 -- ND 3.6 3.0 0.80 J 1.8 ND ND ND 3.3 0.64 J ND 1.0 1.6 ND 0.15 1 ND 3.3 2.3 ND 1.1 ND 0.44 J ND 1.3 ND ND 1.3 2.5 ND 0.15 1 ND 2.4 3.9 1.8 ND -- 1.5 1.1 0.72 J 0.84 J ND 1.5 2.0 ND 0.43 J 0.76 J ND 0.15 1 ND ND ND ND ND 3.9 ND ND -- -- 1.9 ND ND ND 2.1 NS 0.15 1 ND 3.0 ND 0.96 J 1.7 ND ND 3.8 ND ND 1.7 ND ND ND 3.1 7.8 0.43 J 0.74 J 1.6 ND 0.15 1 ND 3.0 ND ND ND ND ND 2.9 1.5 1.9 1.2 NS NS NS 1.2 0.61 J 0.71 J 1.2 2.5 NS 0.15 1 ND 3.3 1 ND ND 1.3 ND 1.8 ND ND 1 ND 0.68 J ND 2.2 0.98 J ND J ND 2.4 ND T:-Proj--358-20-043A Moore County R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 Appendix III -R151oMc G-21-10 WQMR Tables Fa App,d - Page 19 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituent/Parameter Lthylbenzene Units ug/L Sample Date 0:3/05/90 MDL PQL SWSL MW-501V MMW 13MSR MW-13DR MW-14 MW-1 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 MW-q�p PN NC 2L = 600 ug/L ug/L 03/21/91 ND EPA MCL = 700 ug/L ug/L 03/10/92 ND ug/L 04/20/95 ND ug/L 06/27/95 ND ND ND ND ND ug/L 09/22/95 ND ND ND ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 ND ND ND ND ND ND 9.4 ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 ND ND ND ND ND ND ND ND ug/L 04/27/99 ND ND ND ND ND ND ND ND ug/L 10/21/99 ND ND ND ND ND ND ND ND ug/L 03/14/00 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 ND ND ND ND ND ND ND ND ug/L 10/11/01 ND ND ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 ND ND ND ND ND ND ND ND ug/L 04/09/03 ND ND ND ND ND ND ND ND ug/L 10/13/03 ND ND ND ND ND ND ND ND ug/L 04/26/04 ND ND ND ND ND ND ND ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND ND ND ND ND ND ug/L 10/04/05 ND ND ND ND ND ND ND ND ug/L 04/28/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/24/07 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/30/07 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/23/08 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/06/08 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/13/09 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/15/09 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/26/10 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/19/10 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/18/11 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/10/11 1 ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/17/12 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/09/12 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/15/13 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 09/30/13 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/16/14 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/15/14 0.13 1 Dry ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/15/15 0.13 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/07/15 0.13 1 ND 0.62 J ND ND ND ND 0.66 J ND ND ND ND ND ug/L 04/11/16 0.13 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/30/16 0.13 1 ND 0.48 J ND ND ND ND ND ND ND ND ND ND ug/L 04/11/17 0.13 1 ND ND ND ND ND ND ND ND ND ND ND ug/L 12/12/17 0.13 1 ND 0.48 J ND ND ND ND ND ND ND ND ND ND ug/L 06/20/18 0.13 1 ND ND 0.41 J ND ND ND ND ND ND ND ND ND ND ND ug/L 11/27/18 0.13 1 -- ND ND 0.46 J ND ND ND ND ND ND ND ND ND ND ND ug/L 04/02/19 0.13 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/19/19 0.13 1 ND ND 0.58 J ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/07/20 0.13 1 ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/13/20 0.13 1 ND ND ND ND 0.67 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/13/21 0.13 1 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/19/21 0.13 1 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS T—Plj--358-20-043A — County R-Im LFG & WQ —1-1,g—, 03 - 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I WQ 2021-2022T,11 2021 App,dl, III - 11— G-21 -10 WQMR Tables F, App,dk— Page 20 of 31 mBLsSA Record mGroundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April no,Monitoring Event Moore County Landfill, woSolid Waste Permit No. o`-0, Aberdeen, Moore County, North Carolina xmmsProject No. *`58-2o-0*`^ ug/L 0310e9 - - - - - - - - - - - - - - - - - - - - - ' wo ug/L 03/21m1 - - - - - ' ' - - - - - - - - - - - - - - - wo ug/L 03m0/92 - - - - - ' ' - - - - - - - - - - - - - - - wo ug/L 04/20m5 - - - - - ' ' - - - - - - - - - - - - - - - wo ug/L worm, - - - - - ' ' - - - - - - - - - - wo wn wo wo - wo ug/L 09/22m5 - - - wo - ' ' - - - - - wo - wo wo wo wo wo wo wo - wo ug/L 03/28m6 - - - wo - ' - - - - - - - - wo wo - wo wn wo wo - wo ug/L 10/29m6 - - - wo - ' - - - - - - - - - - - wo wo wo wo - wo ugu owomo - - - wo - ' - - - - - - - - - - - wo wo wo wo - wo ugu 10/29197 - - - wo - ' '' wo - - - - - - - - - wo wo eo wo wo wo ugu owomo - - - wo - ' - *v - - - - - - - - - wo wo wo wo wo wo ugu 10n4198 - - - wo - ' - 3e - - - - - - - - - wo wo wo wo wo wo ugu oweno - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu 10/e1m9 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu 03/14100 - - - wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu 04m9/00 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu ,unmm - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu wmom, - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu 10n1m1 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu 04m8/02 - - - wo - - - wo - - - - - - - - - wo wo mo wo wo wo ugu ,ommo - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu owomo - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu 10n3/03 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu owemo - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu 10/25m4 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu owowo - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu 10m*m5 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu owemo - - - wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu ,omomo - - - wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu owewo - - - wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu ,omomr - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu ow,mo - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu 10m6m8 - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu 04m3109 - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu 10n5109 - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu owemo - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu ,unono - - , wo - - - wo - - - - wo - wo wo 0.67 J wo wo wo wo wo wo ugu 04m8w1 - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu 10n0n1 - - , wo - - - wo - - - - wo - wo wo wo wo - wo wo m' wo ugu wm,n, - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo m' wo ugu 10m9e - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo mv wo ugu wmnnn - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo m' wo ugu omnmn - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo m' wo ugu wmun* - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo mv wo ugu ,unnn* o.m - , m' - - - wo - - - - wo - wo wo wo wo wo wo wo m' wo ugu wmnnn o.m - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo mv wo ugu 10m7/5 o.m - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu wm,no o.m - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu 11m0o o.m - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu 04m1n7 o.m - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu ,un,nr o.m - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu omemo o.m - , wo wo - - wo - - - - wo wo wo wo wo wo wo wo wo wo wo ugu 11m7/8 o.m ' - wo wo - - wo - - - - wo wo wo wo wo wo wo wo wo wo wo ugu 04/02/19 o.m , - wo wo - - wo - - - - wo wo wo wo wo wo wo wo wo wo wo ugu 11n9n9 o.m ' - wo wo - - wo wo wo - - wo wo wo wo wo wo wo wo wo wo wo ugu 04/07/20 o.m , - wo wo - - wo wo wo wo - wo wo wa wo wo wo wo wo wo wo wo ugu 10n3/20 o.m , - wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo ugu 04m3/e1 o.m ' - wo wo wo wo wo wo wo wo wo wo wo wa wo wa wo wo wo wo wo wo ugu | ,unm,, | o.m | , | - | wo | wo wo wo wo wo wo wo wo | wo wo | wa wo wo wo wo wo wo wo | wo —ty R-Im LFG & WQ -1-1,g—,°- S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11— G—=WQMR �-~Ap�,dk- Page uwo TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituent/Parameter Methylene chloride Units ug/L Sample Date 0:3/05/90 MDL PQL SWSL MW-501V MMW 13MSR MW-13DR MW-14 MW-1 7S MW-17D MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 MW-q�p PN NC 2L = 5 ug/L ug/L 03/21/91 ND EPA MCL = 5 ug/L ug/L 03/10/92 ND ug/L 04/20/95 ND ug/L 06/27/95 ND ND ND ND ND ug/L 09/22/95 ND ND ND ND ND 40 ND ND ND ND ug/L 03/28/96 ND ND ND 15 ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 ND ND ND ND ND ND ND ND ug/L 04/30/98 ND ND ND ND ND ND ND ND ug/L 10/14/98 ND ND ND ND ND ND ND ND ug/L 04/27/99 ND ND ND ND ND ND ND ND ug/L 10/21/99 ND ND ND ND ND ND ND ND ug/L 03/14/00 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/19/00 ND ND ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 ND ND ND ND ND ND ND ND ug/L 10/11/01 ND ND ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 ND ND ND ND ND ND ND ND ug/L 04/09/03 ND ND ND ND ND ND ND ND ug/L 10/13/03 ND ND ND ND ND ND ND ND ug/L 04/26/04 ND ND ND ND ND ND ND ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND ND ND ND ND ND ug/L 10/04/05 ND ND ND ND ND ND ND ND ug/L 04/28/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/24/07 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/30/07 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/23/08 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/06/08 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/13/09 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/15/09 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/26/10 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/19/10 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/18/11 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/10/11 1 ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/17/12 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/09/12 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/15/13 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 09/30/13 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/16/14 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/15/14 0.23 1 Dry ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/15/15 0.23 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/07/15 0.23 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/11/16 0.23 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/30/16 0.23 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/11/17 0.23 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 12/12/17 0.23 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 06/20/18 0.23 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/27/18 0.23 1 -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/02/19 0.23 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/19/19 0.23 1 ND ND ND ND ND ND ND ND ND ND ND 0.64 J ND ND ND ND ug/L 04/07/20 0.23 1 ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/13/20 0.23 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/13/21 0.23 1 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/19/21 0.23 1 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS T—Plj--358-20-043A — County R-Im LFG & WQ —1-1,g—, 03 - S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11— G-21 -10 WQMR Tables F, App,dk— Page 22 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells DetectedActive Constituent/Parameter wig Units D.MW-501VD- MW-11SR MW-1 MW-2 MW-9 MW-15/15R M 2-Butanone ug/L 10/30/07 -- -- 100 ND -- -- -- ND -- -- -- -- ND -- ND ND ND ND ND ND ND ND ND NC 2L = 4000 ug/L ug/L 04/23/08 100 ND ND ND ND ND ND ND 4.8 J 2.8 J ND ND ND ug/L 10/06/08 100 ND ND ND ND ND ND 17 J 14 J ND ND ND ND ug/L 04/13/09 100 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/15/09 100 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/26/10 100 ND ND ND ND ND ND ND ND ND 6.8 J ND ND ug/L 10/19/10 100 ND ND ND ND ND ND 3.8 J ND ND ND ND ND ug/L 04/18/11 100 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/10/11 100 ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/17/12 100 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/09/12 100 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/15/13 100 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 09/30/13 100 ND ND ND ND ND ND 2.6 J ND ND ND Dry ND ug/L 04/16/14 100 ND ND ND ND ND ND 2.4 J 1.3 J ND 13 J Dry ND ug/L 10/15/14 1.3 100 Dry ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/15/15 1.3 100 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/07/15 1.3 100 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/11/16 1.3 100 ND ND ND ND ND ND 28 J 7.0 J ND 4.2 J ND ND ug/L 11/30/16 1.3 100 ND ND ND ND ND ND 1.4 J ND ND ND 6.4 J ND ug/L 04/11/17 1.3 100 ND ND ND ND ND ND ND ND ND ND 24 J ND ug/L 12/12/17 1.3 100 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 06/20/18 1.3 -- 100 ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/27/18 1.3 5 -- ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/02/19 1.3 5 ND ND ND ND ND ND ND ND ND 21 ND ND ND ND ug/L 11/19/19 1.3 5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 5.7 ND ug/L 04/07/20 1.3 5 ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/13/20 1.3 5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/13/21 1.3 5 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10/19/21 1.3 5 ND ND ND ND ND ND ND ND ND ND ND NS NS NS ND 9.3 ND ND ND NS Naphthalene ug/L 03/05/90 -- -- -- ND NC 2L = 6 ug/L ug/L 03/21/91 ND ug/L 03/10/92 ND ug/L 04/20/95 ND ug/L 06/27/95 -- -- -- -- -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND 2.5 ND ND ug/L 09/22/95 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/30/98 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/14/98 ND ND ND ND ND ND ND ND ug/L 04/27/99 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/21/99 ND ND ND ND ND ND ND ND ug/L 03/14/00 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/19/00 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/17/00 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 04/10/01 -- -- -- ND -- -- -- ND -- -- -- -- -- -- -- -- -- ND ND ND ND ND ND ug/L 10/11/01 ND ND ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 ND ND ND ND ND ND ND ND ug/L 04/09/03 ND ND ND ND ND ND ND ND ug/L 10/13/03 ND ND ND ND ND ND ND ND ug/L 04/26/04 ND ND ND ND ND ND ND ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND ND ND ND ND ND ug/L 10/04/05 ND ND ND ND ND ND ND ND ug/L 04/28/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 10/09/06 -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 04/24/07 -- -- -- -- -- -- -- -- -- -- -- -- -- -- ug/L 06/20/18 0.11 -- 10 ND ND -- -- 0.65 J -- -- -- -- ND 0.58 J -- -- -- ND ND -- -- -- -- ug/L 11/27/18 0.11 1 -- ND ND ND ug/L 04/02/19 0.11 1 ND 0.40 J ND ug/L 11/19/19 0.11 1 ND ND ND ug/L 04/07/20 0.11 1 ND 0.42 J ND ug/L 10/13/20 0.11 1 ND ND ND ND 0.49 J ND ND ND ND ND ND ND ANR ug/L 04/13/21 0.11 1 ND ND ND ND ND ND ND ND ND ND NS NS NS ANR ANR ANR ANR ANR NS ug/L 10/19/21 0.11 1 ND ND ND ND ND ND ND ND ND ND NS NS NS ANR ANR ANR ANR ANR NS T:-Proj--358-20-043A Moore County R-Im LFG6 WQ Mon1-1,g-, 03-S--Annual WQ 2021-2022Te112021 AppendixIII- RlsioMc G-21-10 WQMR Tables Fa App,d - Page 23 of 31 mBLsSA Record mGroundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April no,Monitoring Event Moore County Landfill, woSolid Waste Permit No. o`-0, Aberdeen, Moore County, North Carolina xmmsProject No. *`58-2o-0*`^ ~m"g/L ugu nanmo - - - - - - - - - - - - - - - - - - - - - ' wo ug/L 03/21m1 - - - - - ' ' - - - - - - - - - - - - - - - wo ugu 03m0/92 - - - - - ' ' - - - - - - - - - - - - - - - wo ug/L 04/20m5 - - - - - ' ' - - - - - - - - - - - - - - - wo ugu om,no - - - - - ' - - - - - - - - - - - o* 3.2 wo wo - wo ug/L 09/22m5 - - - wo - ' - - - - - - wo - wo wo wo wo wo wo wo - wo ugu oaemo - - - wo - ' - - - - - - - - wo wo - n wo wo wo - wo ug/L 10/29m6 - - - wo - ' - wo - - - - - - - - - wo wn wo wo o wo ugu owomo - - - wo - - - wo - - - - - - - - - wo wo wo wo o wo ug/L 10/29m7 - - - wo - - - wo - - - - - - - - - 9.2 wo wo wo o^ wo ugu ownmo - - - wo - - - wo - - - - - - - - - wo wo wo wo 8.2 wo ug/L 10n4/98 - - - wo - - - wo - - - 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wo wo wo wo wo wo ug/L 04/28m6 - - - wo - - - wo - - - - wo - wo wo wo wo wn wo wo wo mo ugu 10m9m6 - - - wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L 04/24m7 - - - wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu ,omomr - - , wo - - - 0.52 J - - - - 0.35 J - wo wo wo wo wo wo wo 0.38 J wo ug/L 04/23m8 - - , wo - - - mw J - - - - wo - wo wo wo wo wn wo wo wo mo ugu 10m6m8 - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo o/m J wo ug/L wmmw - - , wo - - - mw J - - - - wo - wo wo wo wo wn wo wo v/m J mo ugu 10n5109 - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo 0.50 J wo ug/L 04/26n0 - - ' wo - - - wo - - - - wo - wo wo wo wo wo wo wo v/n J wo ugu 10n9n0 - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo 0.52 J wo ug/L 04m8n1 - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo mo ugu 10n0n1 - - , wo - - - wo - - - - wo - wo wo wo wo - wo wo mv wo ug/L wmrnu - - ' wo - - - wo - - - - wo - wo wo wo wo wo wo wo mv wo ugu ,omo , - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo Dry wo ug/L wm,wo - - , wo - - - wo - - - - wo - wo wo wo wo wn wo wo mv mo ugu omomn - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo mv wo ug/L 04m6w4 - - , wo - - - wo - - - - wo - wo wo wo wo wn wo wo mv mo ugu ,unnn* 0.17 - , o, - - - wo - - - - wo - wo wo wo wo wo wo wo Dry wo ug/L wmono 0.17 - ' wo - - - wo - - - - wo - wo wo wo wo wo wo wo mv wo ugu 10m7/5 0.17 - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L 04m1n6 0.17 - , wo - - - wo - - - - wo - wo wo wo wo wn wo wo wo wo ugu 11m0o 0.17 - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L 04m1n7 0.17 - ' wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu ,un,nr 0.17 - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L womo 0.17 - ` wo wo - - wo - - - - wo wo wo wo wo wo wn wo wo wo wo ugu 11m7/8 0.17 ' - wo wo - - wo - - - - wo wo wo wo wo wo wo wo wo wo wo ug/L ow000 0.17 , - wo wo - - wo - - - - wo wo wo wo wo wo wn wo wo wo wo ugu ,,nono 0.17 , - wo wo - - wo wo wo - - wo wo wo wo wo wo wo wo wo wo wo ug/L owmoo 0.17 , - wo wo - - wo wo wo wo - wo wo wo wu wo wo wo wo wo wo wo ugu 10n3/20 0.17 ' - wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo wo ug/L 04m3o1 0.17 , - wo wo wo wo wo wo wo wo wo wo wo wa wu wo wo wo wo wo wo wo ugu | 10n9m1 | 0.17 | ' | - | wo | wo wo wo wo wo wo wo wo | wo wo | wa wo wu wo wo wo wo wo | wo —ty R-Im LFG & WQ -1-1,g—,°- S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11— G—=WQMR �-~Ap�,dk- Page 24wo TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Sa Active C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituent/Parameter Toluene Units ug/L Amb 03/05/90 PQL SWSL MW-501V MMW 13MSR MW-13DR MW-14 MW-1 7S MW-17D =7���E6" MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 M�= ND NC 2L = 600 ug/L ug/L 03/21/91 ND EPA MCL = 1000 ug/L ug/L 03/10/92 ND ug/L 04/20/95 ND ug/L 06/27195 ND ND ND ND ND ug/L 09/22/95 ND ND ND ND ND ND ND ND ND ND ug/L 03/28/96 ND ND ND ND ND ND ND ND ug/L 10/29/96 ND ND ND ND ND ND ND ND ug/L 04/08/97 ND ND ND ND ND ND ND ND ug/L 10/29/97 ND ND ND ND ND ND ND ND ug/L 04/30198 ND ND ND ND ND ND 15 ND ug/L 10/14/98 ND ND ND ND ND ND ND ND ug/L 04/27/99 ND ND ND ND ND ND ND ND ug/L 10/21/99 ND ND -- ND ND ND ND ND ND ug/L 03/14100 ND ND 2 ND ND ND ND ND ND ND ND ND ug/L 04/19/00 ND ND -- ND ND ND ND ND ND ug/L 10/17/00 ND ND ND ND ND ND ND ND ug/L 04/10/01 ND ND ND ND ND ND ND ND ug/L 10/11/01 ND ND ND ND ND ND ND ND ug/L 04/18/02 ND ND ND ND ND ND ND ND ug/L 10/08/02 ND ND ND ND ND ND ND ND ug/L 04/09/03 ND ND ND ND ND ND ND ND ug/L 10/13/03 ND ND ND ND ND ND ND ND ug/L 04/26/04 ND ND ND ND ND ND ND ND ug/L 10/25/04 ND ND ND ND ND ND ND ND ug/L 04/04/05 ND ND ND ND ND ND ND ND ug/L 10/04/05 ND ND ND ND ND ND ND ND ug/L 04/28/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/09/06 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/24/07 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/30107 1 ND 0.31 J ND ND ND ND ND ND ND ND ND ND ug/L 04/23/08 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/06108 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/13/09 1 ND 0.53 J ND ND ND ND ND ND ND ND ND ND ug/L 10/15109 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/26/10 1 ND 0.47 J ND ND ND ND ND ND ND ND ND ND ug/L 10/19/10 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 04/18/11 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 10/10/11 1 ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/17/12 1 ND 0.47 J ND ND ND ND ND ND ND ND Dry ND ug/L 10/09/12 1 ND 0.43 J ND ND ND ND ND 0.44 J ND ND Dry ND ug/L 04/15/13 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 09/30/13 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 04/16/14 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/15/14 0.14 1 Dry ND ND ND ND ND ND ND 0.59 J ND Dry ND ug/L 04/15/15 0.14 1 ND ND ND ND ND ND ND ND ND ND Dry ND ug/L 10/07/15 0.14 1 ND ND ND ND ND ND ND ND 0.56 J ND ND ND ug/L 04/11/16 0.14 1 ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/30/16 0.14 1 ND ND ND ND ND ND 0.48 J ND 0.60 J ND ND ND ug/L 04/11/17 0.14 1 ND ND ND ND ND ND ND ND 1.0 B ND ND ND ug/L 12/12/17 0.14 1 ND ND ND ND ND ND ND ND 0.64 J ND 0.44 J ND ug/L 06/20/18 0.14 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/27/18 0.14 1 -- ND ND ND ND ND ND ND ND ND ND 0.48 J ND ND ND ug/L 04/02/19 0.14 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/L 11/19/19 0.14 1 ND ND ND ND ND ND ND ND ND ND ND ND 0.48 J ND 0.43 J ND ug/L 04/07/20 0.14 1 ND ND ND ND ND ND ND ND NS NS NS ND ND 0.40 J ND ND NS ug/L 10/13/20 0.14 1 ND ND ND ND 0.48 J ND ND ND ND ND ND ND ND ND 0.40 J ND 0.51 J 0.43 J ND ND ug/L 04/13/21 0.14 1 ND ND ND ND 0.48 J ND ND ND ND ND ND NS NS NS ND ND ND ND ND NS ug/L 10119/21 0.14 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.61 J 1.3 0.67 J 0.52 J ND ND T-Plj--358-20-043A - County R-Im LFG & WQ -1-1,g-, 03 - S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11- G-21 -10 WQMR Tables F, App,dk- Page 25 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituent/Parameter I richloroethene Units ug/L Sample Date 03/05t90 MDL PQL SWSL MW-501V MMW 13MSR MW-13DR MW-14 MW-1 7S MW-17D -- MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 M NC 2L = 3 ug/L ug/L 03/21/91 NO EPA MCL = 5 ug/L ug/L 03/10/92 NO ug/L 04/20/95 -- NO ug/L 06/27/95 3.6 NO NO ND NO ug/L 09/22/95 NO NO NO NO ND NO NO NO ND NO ug/L 03/28/96 NO NO NO 6.4 NO NO ND -- NO ug/L 10/29/96 NO ND NO NO NO ND 5 NO ug/L 04/08/97 NO NO NO NO NO ND NO NO ug/L 10/29/97 NO ND NO NO NO ND 5.9 NO ug/L 04/30198 ND ND ND NO ND ND 5.4 NO ug/L 10/14/98 NO NO ND NO NO ND NO NO ug/L 04/27199 ND ND ND NO ND ND ND NO ug/L 10/21/99 NO NO ND NO NO ND NO NO ug/L 03/14100 ND ND NO NO ND ND ND NO ND ND 3 NO ug/L 04/19/00 NO NO ND NO NO ND NO NO ug/L 10/17/00 NO NO NO NO NO ND ND NO ug/L 04/10/01 NO NO 5.2 NO NO ND NO NO ug/L 10/11/01 NO NO NO NO NO ND NO NO ug/L 04/18/02 ND ND NO NO NO ND NO NO ug/L 10/08/02 NO NO NO NO NO ND NO NO ug/L 04/09/03 ND ND NO NO NO ND NO NO ug/L 10/13/03 ND ND ND NO ND ND ND NO ug/L 04/26/04 NO NO ND NO NO ND NO NO ug/L 10/25104 ND ND ND NO ND ND ND NO ug/L 04/04/05 NO NO ND NO NO ND NO NO ug/L 10/04105 ND ND ND NO ND ND ND NO ug/L 04/28/06 NO NO ND ND ND ND ND NO NO ND NO NO ug/L 10/09106 ND ND ND NO ND ND ND NO ND ND ND NO ug/L 04/24/07 ND ND ND NO ND ND NO NO NO ND NO NO ug/L 10/30/07 1 NO 1.5 J 0.40 J NO 0.30 J ND NO NO 0.31 J ND 0.46 J NO ug/L 04/23/08 1 ND 1.0 ND NO ND ND NO NO NO ND NO NO ug/L 10/06/08 1 NO 0.76 J ND NO NO ND NO NO NO ND 0.46 J NO ug/L 04/13/09 1 NO 1.0 ND ND ND ND NO NO NO ND 0.74 J NO ug/L 10/15/09 1 NO 0.97 J 0.51 J 0.64 J NO ND NO NO 0.44 J ND 0.50 J NO ug/L 04/26/10 1 NO 0.85 J ND ND NO ND NO NO NO ND 0.50 J NO ug/L 10/19/10 1 ND 0.59 J ND ND ND ND ND NO ND ND 0.42 J NO ug/L 04/18/11 1 NO NO ND ND NO ND ND NO NO ND NO NO ug/L 10/10/11 1 ND 0.77 J ND ND ND ND ND ND ND Dry NO ug/L 04/17/12 1 NO 0.50 J ND ND NO ND ND NO NO ND Dry NO ug/L 10/09/12 1 ND 0.54 J ND ND ND ND ND NO ND ND Dry NO ug/L 04/15/13 1 NO ND ND ND ND ND NO NO NO ND Dry NO ug/L 09/30/13 1 NO NO ND ND NO ND NO NO NO ND Dry NO ug/L 04/16/14 1 NO 0.41 J ND NO ND ND NO NO NO ND Dry NO ug/L 10/15/14 0.15 1 Dry NO ND NO NO ND NO NO NO ND Dry NO ug/L 04/15/15 0.15 1 NO 0.50 J ND NO NO ND NO NO NO ND Dry NO ug/L 10/07/15 0.15 1 NO NO ND ND NO ND NO NO NO ND 0.53 J NO ug/L 04/11/16 0.15 1 ND NO ND ND NO ND NO NO NO ND NO NO ug/L 11130/16 0.15 1 ND ND ND ND ND ND ND NO ND ND ND NO ug/L 04/11/17 0.15 1 NO NO ND ND 0.95 J ND ND NO NO ND NO NO ug/L 12112117 0.15 1 ND ND ND ND ND ND ND NO ND ND ND NO ug/L 06/20/18 0.15 1 ND ND NO ND NO ND NO ND ND NO NO ND NO NO ug/L 11127118 0.15 1 -- ND ND ND ND ND ND ND ND ND NO ND ND ND NO ug/L 04/02/19 0.15 1 NO ND NO ND NO ND NO ND NO NO NO ND NO NO ug/L 11/19/19 0.15 1 NO ND NO NO NO ND NO ND NO ND NO NO NO ND NO NO ug/L 04/07/20 0.15 1 NO ND NO NO NO NO ND ND NS NS NS NO NO NO ND NO NS ug/L 10/13/20 0.15 1 NO ND NO ND NO NO NO ND NO ND ND ND NO ND NO NO NO ND NO ND ug/L 04/13/21 0.15 1 NO ND NO ND NO NO NO ND NO ND NO NS NS NS NO NO NO ND ND NS ug/L 10/19/21 0.15 1 NO ND NO ND NO NO NO ND NO ND ND NS NS NS NO NO NO ND NO NS T-Plj--358-20-043A - County R-Im LFG & WQ -1-1,g-, 03 - S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11- G-21 -10 WQMR Tables F, App,dk- Page 26 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Active C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Detected Monitoring Constituent/Parameter Vinyl chloride Units ug/L Sample Date 03/05t90 MDL PQL SWSL MW-501V MMW 13MSR MW-13DR MW-14 MW-1 7S MW-17D =���E6" MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 MW-9�= ND NC 2L = 0.03 ug/L ug/L 03/21/91 NO EPA MCL = 2 ug/L ug/L 03/10/92 NO ug/L 04/20/95 NO ug/L 06/27/95 5.3 9.4 40.3 15.9 NO ug/L 09/22/95 NO NO NO NO ND NO NO 45 20 NO ug/L 03/28/96 NO NO 13 NO NO 12 ND NO ug/L 10/29/96 NO ND -- NO NO NO ND NO NO ug/L 04/08/97 NO NO NO NO NO ND NO NO ug/L 10/29/97 NO ND NO NO NO ND NO NO ug/L 04/30198 ND ND ND 10 ND ND ND NO ug/L 10/14/98 NO 35 NO NO NO ND NO NO ug/L 04/27199 ND 58 18 NO ND ND NO NO ug/L 10/21/99 NO 28 -- 21 NO NO ND 17 NO ug/L 03/14100 ND 16 NO NO 8 ND is 5 4 ND 9 NO ug/L 04/19/00 NO NO -- 25 21 NO ND 11 NO ug/L 10/17/00 NO 40 14 NO 28 13 NO NO ug/L 04/10/01 NO 35 25 16 ND 11 16 NO ug/L 10/11/01 NO 12 15 12 28 ND NO NO ug/L 04/18/02 ND ND 13 10.8 17.7 ND NO NO ug/L 10/08/02 NO NO NO NO ND ND NO NO ug/L 04/09/03 ND 18.5 ND NO NO ND NO NO ug/L 10/13/03 ND 12.5 ND NO ND 11.4 ND NO ug/L 04/26/04 NO 15.9 ND NO 19.4 ND NO NO ug/L 10/25104 ND ND ND NO 13.3 ND ND NO ug/L 04/04/05 NO ND ND NO NO ND NO NO ug/L 10/04105 ND ND 11.7 NO 12.8 ND ND NO ug/L 04/28/06 NO 12.8 ND NO NO ND 14.2 NO NO ND NO NO ug/L 10/09106 ND ND ND NO ND ND NO NO 12.4 ND ND NO ug/L 04/24/07 ND 7.6 ND NO ND ND NO NO NO -- NO NO ug/L 10/30/07 1 NO 2.8 0.30 J NO 2.7 ND 3.6 NO 4.2 1.2 NO NO ug/L 04/23/08 1 ND 5.1 ND NO 1.4 ND NO 3.0 NO 1.8 NO NO ug/L 10/06/08 1 NO 5.8 ND NO 1.2 ND 3.4 J 2.1 ND 1.9 3.9 NO ug/L 04/13/09 1 NO 5.4 ND NO 1.6 ND 1.3 NO 0.67 J 1.7 3.0 NO ug/L 10/15/09 1 NO 3.5 0.62 J 0.92 J 2.1 ND 4.0 NO 5.3 1.1 NO NO ug/L 04/26/10 1 NO 5.4 ND ND 1.9 ND 2.0 2.4 0.81 J 1.6 2.4 NO ug/L 10/19/10 1 ND NO ND ND 1.3 ND NO NO 0.53 J NO 2.1 NO ug/L 04/18/11 1 NO 2.8 ND ND 0.91 J ND 0.78 J 0.90 J 1.0 0.71 J 2.2 NO ug/L 10/10/11 1 ND 3.1 ND ND 0.86 J ND 2.8 -- 3.7 1.2 Dry NO ug/L 04/17/12 1 NO 3.7 ND 0.39 J 0.79 J ND 2.0 1.5 NO 1.1 Dry NO ug/L 10/09/12 1 ND 2.6 ND ND 1.3 ND 2.0 2.0 ND 1.4 Dry NO ug/L 04/15/13 1 NO 3.5 ND ND 0.61 J ND 2.6 1.5 NO 1.1 Dry NO ug/L 09/30/13 1 NO 2.3 ND NO NO ND 3.1 1.4 ND 0.85 J Dry NO ug/L 04/16/14 1 NO 3.1 ND NO ND ND 1.7 1.8 NO 1.3 Dry NO ug/L 10/15/14 0.32 1 Dry 2.3 ND NO 0.62 J ND 2.2 1.5 0.57 J 0.55 J Dry NO ug/L 04/15/15 0.32 1 NO 1.8 ND NO 0.72 J ND 0.78 J NO NO ND Dry NO ug/L 10/07/15 0.32 1 NO 3.4 ND ND 0.61 J ND 2.7 1.5 ND 0.51 J 1.2 NO ug/L 04/11/16 0.32 1 ND 3.3 ND ND NO ND 0.72 J 0.71 J 0.48 J 0.42 1 NO NO ug/L 11130/16 0.32 1 ND 2.5 ND ND ND ND 1.3 1.1 0.64 J ND 0.48 J NO ug/L 04/11/17 0.32 1 NO 1.9 ND ND NO ND 1.4 0.45 J 0.65 J ND NO NO ug/L 12112117 0.32 1 ND -- 2.0 ND -- ND ND ND 1.5 1.1 0.99 J ND 0.47 J NO ug/L 06/20/18 0.32 1 ND 2.2 2.7 ND 1.9 ND NO ND 2.1 2.1 NO ND NO NO ug/L 11/27118 0.32 1 -- ND 1.8 2.3 ND 2.3 ND ND ND 1.9 1.1 ND ND 0.50 J NO ug/L 04/02/19 0.32 1 NO 2.1 1.4 ND 2.1 ND NO ND NO 2.4 NO ND NO NO ug/L 11/19/19 0.32 1 NO 1.3 2.5 ND ND -- ND 2.0 ND NO ND 1.3 1.3 ND ND 0.74 J NO ug/L 04/07/20 0.32 1 NO 1.3 1.3 ND NO 1.8 ND 2.0 NS INS NS NO 0.89 J NO ND ND NS (Verification Event) ug/L 06/05/20 0.32 1 NO ANR ANR ANR ANR ANR ANR 1.1 ANR ANR ANR ANR ANR ANR ANR ANR ANR ANR ANR ug/L 10/13/20 0.32 1 ND 1.8 NO ND 2.3 0.79 J NO 1.9 NO ND 2.4 ND ND ND 1.1 5.4 NO ND 1.1 NO ug/L 04/13/21 0.32 1 NO 2.2 0.86 J ND 0.85 J ND ND 1.6 0.6 J 0.5 J 1.8 NS NS NS 1.2 2.2 ND ND ND NS ug/L 10/19/21 0.32 1 ND NO NO ND 2.6 1.8 NO 1.0 J NO ND J ND ND NS ND 1.2 1.6 NO ND NO NO T-Plj--358-20-043A - County R-Im LFG & WQ -1-1,g-, 03 - S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11- G-21 -10 WQMR Tables F, App,dk- Page 27 of 31 mBLsSA Record mGroundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April no,Monitoring Event Moore County Landfill, woSolid Waste Permit No. o`-0, Aberdeen, Moore County, North Carolina xmmsProject No. *`58-2o-0*`^ ~mmugu ugu omnnmo - - - - - - - - - - - - - - - - - - - - - ' wo ug/L 03/21m1 - - - - - ' ' - - - - - - - - - - - - - - - wo ugu 03/10/92 - - - - - ' ' - - - - - - - - - - - - - - - wo ug/L 04/20m5 - - - - - ' ' - - - - - - - - - - - - - - - wo ugu omeno - - - - - ' - - - - - - - - - - - wo wo ^r *.3 - wo ugu 09/22m5 - - - wo - ' - - - - - - wo - wo wo wo wo wn wo wo - mo ugu oaemo - - - wo - ' - - - - - - - - wo wo - wo wo wo wo - wo ug/L 10/29m6 - - - wo - ' - wo - - - - - - - - - wo wn wo wo wo mo ugu owomo - - - wo - ' - wo - - - - - - - - - wo wo wo wo wo wo ug/L 10/29m7 - - - wo - ' - wo - - - - - - - - - 10.2 wn wo wo wo mo ugu ownmo - - - wo - - - wo - - - - - - - - - wo wo wo wo m wo ug/L 10n4/98 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu ow,no - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L 10o1m9 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu 03/14100 - - - wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L 04m9/00 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu 10n7/00 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L 04m0m1 - - - wo - - - wo - - - - - - - - - wo wn wo wo wo wo ugu 10n1m1 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L 04m8/02 - - - wo - - - wo - - - - - - - - - wo wn wo wo wo wo ugu 10m8/0 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L owomo - - - wo - - - wo - - - - - - - - - wo wn wo wo wo wo ugu 10n3/03 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L 04/26m4 - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu 10/2510* - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L owowo - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ugu ,om*mn - - - wo - - - wo - - - - - - - - - wo wo wo wo wo wo ug/L 04/28m6 - - - wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu ,omomo - - - wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ug/L 04/24m7 - - - wo - - - wo - - - - wo - wo wo wo wo wn wo wo wo mo ugu 10m0m7 - - s wo - - - 0.52 J - - - - wo - wo wo wo 0.34 J wo ^^ J o/w J wo wo ug/L 04/23m8 - - , wo - - - wo - - - - wo - wo wo wo wo wn wo wo wo mo ugu 10m6m8 - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo 5.4 wo ug/L wmmw - - , wo - - - uw J - - - - wo - wo wo wo wo wn wo 0.41 J vya J mo ugu 10n5/09 - - , wo - - - um J - - - - wo - wo wo wo wo wo 0.46 J o/m J wo wo ug/L 04/26n0 - - , wo - - - um J - - - - wo - wo wo wo wo wo wo wo ,.0 J wo ugu ,unono - - , wo - - - mm J - - - - wo - wo wo wo wo wo mn J 0.41 J wo wo ug/L 04m8n1 - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu ,unun, - - s wo - - - wo - - - - wo - wo wo wo wo - wo wo m' wo ug/L wmrnu - - , wo - - - uw J - - - - wo - wo wo wo wo wo wo wo mv wo ugu ,omo , - - , wo - - - mm J - - - - wo - wo wo wo wo wo wo wo Dry wo ug/L wm,wo - - , wo - - - wo - - - - wo - wo wo wo wo wn wo wo mv mo ugu omomn - - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo mv wo ug/L 04m6w4 - - n wo - - - wo - - - - wo - wo wo wo wo wn wo wo mv mo ugu 10n5n* o/m - , Dry - - - wo - - - - wo - wo wo wo wo wo mm J wo mv wo ug/L wm,w, o,m - n wo - - - wo - - - - wo - wo wo wo wo wn wo wo mv mo ugu 10m7/5 o/m - , wo - - - wo - - - - wo - wo wo wo wo wo 0.93 J wo wo wo ug/L 04m1n6 o,m - , wo - - - wo - - - - wo - wo wo wo wo wo wo wo wo wo ugu ,,mo o o/m - s wo - - - wo - - - - wo - wo wo wo wo wo ua, J wo wo wo ugu wm,nr o/m - s wo - - - wo - - - - wo - wo wo wo wo wo ,.o a wo wo wo ugu 1enen7 o/m - s wo - - - wo - - - - wo - wo wo wo wo wo 1.2 J wo wo wo ugu omemo o/m - s wo wo - - wo - - - - wo wo wo wo wo wo wo mm J wo wo wo ugu 11m7/8 o/m 3 - wo wo - - wo - - - - wo wo wo wo wo wo wo wo wo wo wo ugu 04/02/19 o/m 3 - wo wo - - wo - - - - wo wo wo wo wo wo wo wo o/m J wo wo ugu 11n9n9 o/m 3 - wo wo - - wo wo wo - - wo wo wo wo wo wo wo 2.2 J wo wo wo ugu 04/07/20 o/m 3 - wo wo - - o/m J wo wo wo - wo wo wa wo wa wo wo ur J wo wo wo ugu 10n3/20 o/m ` - wo wo wo wo mm J wo wo wo wo wo wo wo wo wo wo 2.2 o^o J wo wo ugu wmam, o/m ` - wo wo wo wo wo wo wo wo wo wo wo wa wo wo wo wo wo wo wo ws ugu | ,unm,, | o/m | ` | - | wo | wo wo wo wo wo wo wo wo | wo wo | wa wo wo wo wo wo wo wo | ws —ty R-Im LFG & WQ -1-1,g—,°- S-- ... I WQ 2021-2022T,11 2021 App,dl, III - 11— G—=WQMR �-~Ap�,dk- Page m*n TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A DetectedActive C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells MDL Constituent/Parameter Units D. 1,4-Dioxane ug/L 11/27/18 1.2 •e 2.0 -- ND �• 5.6 -- D•MW-q'MF -- 15 -- -- -- -- 2.8 7.3 ND 7.8 ND 2.9 4.6 6.3 39 ND N ND NC 2L= 3.0 ug/L ug/L 04/02/19 1.2 2.0 ND 4.8 11 -- -- 2.0 8.4 ND 7.5 ND 1.6 J 4.0 7.2 23 ND ND ug/L 11/19/19 0.8 2.0 ND 3.9 15 1.6 J 5.2 -- 2.0 4.8 2.3 14 1.1 J 1.4 J 10 39 22 ND ND ug/L 04/07/20 0.8 2.0 ND 5.9 -- -- 15 3.0 8.5 11 -- 2.2 4.3 NS NS NS 2.5 1 J 16 29 ND NS ug/L 10/13/20 0.8 2.0 ND 4.4 3.4 2.5 14 2.3 6.8 10 2.8 1.3 5.4 ND 9.7 1.0 J 2.0 6.9 29 25 ND ND ug/L 04/13/21 0.8 2.0 ND 5.3 3.8 3.4 5 0.9 J 10.0 15 7.9 5.3 7.0 NS NS NS 1.7 3.9 22 30 2.2 NS ug/L 10/19/21 0.8 2.0 ND 3.9 9.2 3.3 17 3.4 7.1 13 2.9 1.6 J 5.1 ND 25 1.6 J 1.8 J 6.3 48 34 ND ND Tetrahydrofuran ug/L 06/20/18 0.53 1.0 ND 2.6 -- -- 1.8 -- -- -- -- ND 5.5 -- -- -- -- -- -- ug/L 11/27/18 0.53 1.0 ND ND ND ND ND ug/L 04/02/19 0.53 1.0 ND ND ND ND 15 ug/L 11/19/19 0.53 1.0 ND ND ND ND ND ND ND ug/L 10/13/20 0.53 1.0 ND 2.4 ND ND 3.3 ND ND -- 6 ANR ANR ANR ANR ANR ANR ANR ANR ANR ug/L 04/13/21 0.53 1.0 ND ND ND ND ND ND ND ND ND 8.6 7.5 NS NS NS ANR ANR ANR ANR ANR NS ug/L 10/19/21 0.53 1.0 ND 3.4 ND ND ND ND ND ND ND ND 6.3 ANR ANR ANR ANR ANR ANR ANR ANR ANR T:-Proj--358-20-043A Moore Cowry R-Im LFG 6 WQ 03 - Seml-Annual WQ Mon-I.g 2021-2023Te11202-ppendix III- 1I51oMc G-21-10 WQMR Tables Fa Appendix- Page 29 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A DetectedActive Constituent/Parameter Date C&D Monitoring Wells Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Sulfide Units mg/L 04/11/17 MW-50FF"TMWM-13SF ND MW-13DR MW-14 MW-1 7S MW-17D MW-18 ND WL 0.35 J MW-11SR MW-1 ND MW-2 ND MW-3 ND MW-6 0.89 J 0.82 J MW-8 MW-9 0.77 MW-15/15R J 1.00 -M mg/L 12/12/17 ND -- 0.54 J 0.16 J ND ND ND 0.11 J 1.30 J 2.70 J 0.66 J mg/L 06/20/18 0.01 0.1 ND 0.38 J 0.50 J ND ND ND ND 0.13 J NO 2.70 J ND mg/L 11/27/18 0.01 0.1 ND 0.17 J 0.62 J ND ND ND ND 0.97 J 3.20 1.40 ND mg/L 04/02/19 0.01 0.1 ND 1.50 0.46 J ND ND ND ND 0.65 J 0.57 J 1.70 0.21 J mg/L 04/07/20 0.01 0.1 ND 0.83 J 0.42 J 0.16 J 0.28 J 0.16 2.70 1.00 0.58 J mg/L 10/13/20 0.01 0.1 ND 0.22 J ND NO 0.12 ND ND 0.42 J ND ND 0.17 J NO ND ND 0.16 NO 0.78 J 1.40 0.27 J mg/L 04/13/21 0.01 0.1 ND 0.49 J ND NO 0.37 ND ND 0.30 J ND ND 1.10 NS NS NS 0.19 NO 1.10 1.60 0.35 J NS ug/L 10/19/21 0.01 0.1 ND 0.04 J 0.02 J ND 0.16 ND ND 0.06 J ND 0.07 J 0.05 J NS ND ND 0.19 0.46 0.14 0.30 0.29 J ANR Chloride mg/L 04/11/17 ND -- -- -- 42 43 -- ND 40 3.7 J 16 2.9 J 95 ND mg/L 12/12/17 2 J -- 47 31 9.9 54 4.1 J 20 14 92 ND mg/L 06/20/18 2.2 5.0 ND 6.9 44 34 ND 63 2.8 J 15 7.1 110 3.1 J mg/L 11/27/18 2.2 5.0 ND 3.9 J 42 20 ND 30 2.7 J 16 6.3 120 ND mg/L 04/02/19 2.2 5.0 ND 3.5 J 39 20 -- NO 29 3.8 J 13 5.0 94 ND mg/L 04/07/20 2.2 5 ND 8.4 -- -- 33 -- -- 56 -- -- 3.2 J -- -- -- 14 4.0 J 100 3.1 J mg/L 10/13/20 2.2 5 2.5 J 21 7.7 5.8 52 22 3.0 41 14 8.9 27 2.3 J 38 5.5 13 20 69 100 D 2.9 J mg/L 04/13/21 2.2 5 2.9 J 22 8.4 6.8 15 8.2 2.9 51 36 30 34 NS NS NS 13 10 50 99 D 3.1 J NS ug/L 10/19/21 2.2 5 3.5 J 18.00 1.6 7 61.00 27 3 J 44.00 13 10.00 26.00 2.7 J 93 7.8 13.00 25.00 110.00 D 120.00 D 3.30 J ANR Nitrate as N mg/L 04/11/17 0.240 J -- -- -- -- -- -- 0.100 J -- 14 -- 0.950 J 0.180 J ND 0.077 J 0 J 0.140 J 0.180 J mg/L 12/12/17 0.550 J 0.130 J 0.280 J 0.600 J 1.100 J ND 0.140 J 0 J 0.120 J 0.160 J mg/L 06/20/18 0.025 1.000 0.450 J 0.120 J 6.000 J 0.840 J 1.700 J ND 0.140 J 0 J 0.170 J 0.140 J mg/L 11/27/18 0.025 1 0.410 0.170 4.400 1.200 0.050 J ND 0.130 0 0.200 0.240 mg/L 04/07/20 0.025 1 0.320 -- -- -- -- 0.089 J 0 J 0.090 J 0.076 J mg/L 10/13/20 0.41 1 0.380 J ANR ANR ANR ANR ANR ANR ANR ANR 2.300 J 90 J 0.850 0.130 ND 0.110 0 0.120 0.100 0.510 mg/L 04/13/21 0.41 1 1.400 ANR ANR ANR ANR ANR ANR ANR ANR 0.220 ND NS NS NS ND 1 ND ND ND NS ug/L 10/19/21 0.41 1 0.940 ANR ANR ANR ANR ANR ANR ANR ANR 0.11 0.15 760 4.6 D 0.35 0.12 0.14 0.09 J 0.10 0.11 ANR Nitrite as N mg/L 04/11/17 ND 19 J 0.030 J -- ND ND NO 0.033 J NO ND ND mg/L 12/12/17 ND ND ND ND ND NO ND NO ND ND mg/L 06/20/18 0.017 0.1 ND ND ND ND ND NO ND NO ND ND mg/L 11/27/18 0.017 0.1 ND ND ND ND ND ND 0.017 J ND ND ND mg/L 04/02/19 0.017 0.1 ND 27 J ND ND ND ND 0.098 J ND ND ND mg/L 04/07/20 0.017 0.1 ND -- ND ND ND 0.038 J mg/L 10/13/20 0.017 0.1 ND ANR ANR ANR ANR ANR ANR ANR ANR ND ND ND ND ND ND ND ND ND ND mg/L 04/13/21 0.017 0.1 ND ANR ANR ANR ANR ANR ANR ANR ANR ND ND NS NS NS ND ND ND ND ND NS ug/L 10/19/21 0.017 0.1 ND ANR ANR ANR ANR ANR ANR ANR ANR 0.021 ND ND ND ND ND ND ND ND ND ANR Total Dissolved Solids mg/L 06/20/18 50 50 ND ND 180 200 mg/L 11/27/18 50 50 ND ND 160 110 mg/L 04/02/19 50 50 ND ND -- 270 220 -- mg/L 04/07/20 10 10 ND 66 -- -- 420 -- -- 280 -- -- 290 mg/L 10/13/20 10 10 ND 250 96 50 240 350 200 430 160 150 550 mg/I 04/13/21 10 10 ND 270 82 30 74 240 250 470 350 520 680 NS NS NS ANR ANR ANR ANR ANR NS ug/L 10/19/21 10 10 ND 200 78 ND 250 380 150 410 8 130 540 ANR ANR ANR ANR ANR ANR ANR ANR ANR Sulfate as SO4 mg/L 04/11/17 ND -- -- -- -- -- 14 J -- 98 J -- 9.3 J 10 J 8.7 J 14 J ND 3.5 J ND mg/L 12/12/17 ND 11 J 38 J 10.0 J 16 J 10 J 8.9 J ND ND 1.8 J mg/L 06/20/18 2.9 5.0 ND ND 9.8 J 22 J 8.6 J 13 J 9.1 J 7.3 J ND ND 3.1 J mg/L 11/27/18 2.9 5.0 ND ND 8.1 29 7.6 5.2 7.6 9.2 ND ND 1.1 mg/L 04/02/19 2.9 5.0 ND ND -- 9.2 61 8.2 4.5 J 7.9 1.6 ND ND 8.7 mg/L 04/07/20 2.9 5 ND ND -- -- 35 -- -- ND -- 38 -- -- -- 10 ND ND 9.7 mg/L 10/13/20 2.9 5 ND 13 16 9.1 7.1 99 35 7 12 32 ND 8.0 5.5 8.4 7.2 ND ND ND 7.2 mg/L 04/13/21 2.9 5 2.9 12 18 10 19 20 33 45 23 110 14 NS NS NS 11 ND ND ND 6.8 NS ug/L 10/19/21 2.9 5 2.9 J 11 18 8 7 95 30 42 10 35 ND 9 17 11 7 ND ND ND 9.6 ANR Total Alkalinity as CaCO3 mg/L 04/11/17 ND -- -- -- -- -- -- 150 -- 470 ND 230 ND 200 110 920 110 mg/L 12/12/17 ND -- 170 350 49 290 D ND 260 110 1,000 130 mg/L 06/20/18 14 15 ND 87 170 94 ND 310 ND 250 150 1,100 85 mg/L 11/27/18 14 15 ND 81 130 41 ND 180 ND 240 160 890 90 mg/L 04/02/19 14 15 ND ND -- 120 20 -- ND 170 ND ND ND 710 40 mg/L 04/07/20 14 15 ND 51 -- 190 -- -- 140 -- -- 170 -- 210 110 740 83 mg/L 10/13/20 14 15 ND 220 49 ND 190 140 120 290 95 39 620 ND 180 ND 190 120 240 D 830 96 mg/I 04/13/21 14 15 ND 260 34 21 42 24 160 320 D 200 D 260 730 D NS NS NS 240 300 230 D 760 110 NS ug/L 10/19/21 14 15 ND 210 D 43 3 220 190 97 31 D 45 D 60 470 D ND 320 D ND 21 D 89 D 310 D 900 D 40 ANR Total Organic Carbon mg/L 04/11/17 ND -- -- -- -- -- -- 9.2 -- 43 -- 1 9.1 0.780 J 26 13 59 37 mg/L 12/12/17 ND 13 27 5 8.7 9.2 15 7.1 40 14 mg/L 06/20/18 0.34 1.0 ND 12 11 1.7 12 1.1 19 6.5 66 4.8 mg/L 11/27/18 0.34 1.0 470 J 15 9.3 2 7.8 1.0 25 6.0 68 3.3 mg/L 04/02/19 0.34 1.0 ND 12 11 1.1 6.2 0.95 J 56 9.4 42 43 mg/L 04/07/20 0.54 1.0 ND -- -- -- -- -- -- 26 17 32 1.7 mg/L 10/13/20 0.54 1.0 ND ANR ANR ANR ANR ANR ANR ANR ANR 11 22 0.9 J 30 21 21 37 2.6 mg/L 04/13/21 0.54 1.0 1.0 ANR ANR ANR ANR ANR ANR ANR ANR 42 34 NS NS NS 57 26 18 34 2.5 NS ug/L 10/19/21 0.54 1.0 ND ANR ANR ANR ANR ANR ANR ANR ANR 14 21 1 13 2 18 28 26 39 2.2 ANR T:-Proj--358-20-043A Moore County R-Im LFG 6 WQ 03 - Seml-Annual WQ Mon-I.g 2021-2023Te11202-ppendix III- RlsioMc G-21-10 WQMR Tables Fa Appendix- Page 30 of 31 TABLESA Record of Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, April 2021 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Constituent/Parameter Active C&D Monitoring Wells "116" Closed MSW Monitoring Wells & MNA Performance Monitoring Wells k�hi Nitrate/Nitrite as N Units mg/L �- 04/11/17 0.24 �- 0.120 14.0 0.950 0.180 NO 0.110 0.160 0.140 0.180 AM mg/L 12/12/17 0.55 0.130 2.8 0.600 1.100 NO 0.140 0.140 0.120 0.160 mg/L 06/20/18 0.041 0.1 0.45 0.120 6.0 0.840 1.700 NO 0.140 0.110 0.170 0.140 mg/L 11/27/18 0.041 0.1 0.41 0.170 4.4 1.200 0.050 J NO 0.150 0.200 0.200 0.240 mg/L 04/02/19 0.041 0.1 0.32 0.110 3.6 1.000 0.048 J NO 0.150 0.080 J 0.100 0.120 mg/L 04/07/20 0.041 0.1 0.32 0.089 J 0.095 J 0.099 J 0.110 mg/L 10/13/20 0.041 0.1 0.38 J ANR ANR ANR ANR ANR ANR ANR ANR 2.3 J 0.090 J 0.85 0.130 0.110 0.200 0.120 0.100 0.510 mg/L 04/13/21 0.041 0.1 1.40 ANR ANR ANR ANR ANR ANR ANR ANR 0 NO NS NS NS NO 0.650 NO NO NO NS ug/L 10/19/21 0.041 0.1 0.94 ANR ANR ANR ANR ANR ANR ANR ANR 0 150 760 5 D 350 0 140.000 94 J 100 110 ANR Ethane mg/L 04/11/17 NO NO NO NO NO NO NO NO NO NO mg/L 12/12/17 NO NO NO NO NO NO NO ND NO NO mg/L 06/20/18 0.0013 0.002 NO NO NO NO NO NO NO ND NO NO mg/L 11/27/18 0.0013 0.002 NO NO NO NO NO NO NO ND NO NO mg/L 04/02/19 0.0013 0.002 NO NO NO NO NO NO NO ND NO NO mg/L 04/07/20 0.0051 0.006 NO NO ND NO ND mg/L 10/13/20 0.0051 0.006 NO ANR ANR ANR ANR ANR ANR ANR ANR NO ND NO NO ND ND NO NO mg/L 04/13/21 0.0051 0.006 NO ANR ANR ANR ANR ANR ANR ANR ANR NO ND NS NS NS NO ND ND NO NO NS ug/L 10/19/21 0.0051 0.006 NO ANR ANR ANR ANR ANR ANR ANR ANR ANR ND NO NO NO NO ND ND NO NO ANR Ethene mg/L 04/11/17 NO NO NO NO ND NO NO ND NO NO mg/L 12/12/17 ND NO NO NO ND NO NO ND NO NO mg/L 06/20/18 0.0015 0.003 ND NO NO NO ND NO NO ND NO ND mg/L 11/27/18 0.0015 0.003 ND NO NO NO ND NO NO ND NO NO mg/L 04/02/19 0.0051 0.006 ND NO NO NO ND NO NO ND NO NO mg/L 04/07/20 0.0051 0.006 NO NO ND NO NO mg/L 10/13/20 0.0051 0.006 NO ANR ANR ANR ANR ANR ANR ANR ANR NO ND NO NO NO ND ND NO NO mg/L 04/13/21 0.0051 0.006 NO ANR ANR ANR ANR ANR ANR ANR ANR NO ND NS NS NS NO ND ND NO NO NS ug/L 10/19/21 0.0051 0.006 NO ANR ANR ANR ANR ANR ANR ANR ANR ANR ND NO NO NO NO NO ND NO NO ANR Methane mg/L 04/11/17 496 J 5.06 0.372 0.636 J 0.099 NO 6.05 1.56 5.90 5.10 mg/L 12/12/17 567 J 1.67 0.879 0.264 0.012 NO 1.79 1.62 2.34 3.58 mg/L 06/20/18 0.45 1.00 NO 3.10 0.154 NO 0.041 NO 1.45 2.97 2.35 0.40 mg/L 11/27/18 0.45 1.00 NO 1.06 0.948 NO 0.019 NO 3.84 4.02 5.64 0.96 mg/L 04/02/19 0.45 1.00 NO 3.60 0.039 0.566 J 0.055 NO 4.06 5.93 5.04 2.08 mg/L 04/07/20 0.0051 0.006 NO 2.16 1.94 0.67 1.36 mg/L 10/13/20 0.0051 0.006 NO ANR ANR ANR ANR ANR ANR ANR ANR NO 4.46 NO NO 3.68 6.150 5.68 D 3.20 mg/L 04/13/21 0.0051 0.006 ND ANR ANR ANR ANR ANR ANR ANR ANR 0.323 3.28 NS NS NS 12.4 5.91 D 6.370 D NO 1.64 NS ug/L 10/19/21 0.0051 0.006 NO ANR ANR ANR ANR ANR ANR ANR ANR 0.480 D 2.44 NO 0.824 NO 2.8 D 2.78 D 3.930 D 1 1.52 ANR Carbon dioxide mg/L 04/07/20 17.2 51 55.7 499 288 451 365 mg/L 10/13/20 21.6 ANR ANR ANR ANR ANR ANR ANR ANR 573 55.7 5.24 47.5 429 D 406 D 462 J 729 D 425 mg/L 04/13/21 62.1 75.0 28.1 ANR ANR ANR ANR ANR ANR ANR ANR 217 D 423 NS NS NS NO 373 D 126 NO 242 NS ug/L 10/19/21 2.07 2.5 22.5 ANR ANR ANR ANR ANR ANR ANR ANR 73 D 448 D 60.2 259 D 81.8 239 D 243 D 314 D 179 216 ANR 2,4-D [2C] ug/L 06/20/18 0.27 NO NO NO ND NO NO NO Dinoseb [2C] ug/L 06/20/18 0.32 NO NO ND NO ND NO NO 2,4,5-TP (Silvex) ug/L 06/20/18 0.44 NO 0.49 J ND NO ND NO NO Notes: 1.) ug/L = Micrograms per liter 2.) NO = Not detected at the stated reporting limit 3.) NM = Not measured 4.) J = Estimated concentration reported below Solid Waste Section Limit 5.) -- = No data available 6.) Blanks = Field, trip, and method blanks 7.) Reanalysis = Reanalysis result in parenthesis next to the original result (e.g., reanalysis was performed for arsenic in January 2017) 8.) Dissolved = Dissolved sample in brackets [e.g. a dissolved sample was analyzed for MW-9 for the Febuary 2017 verification event] 9.) Bold = Concentration above the current NC 2L Groundwater Standard or NC 2L IMAC Groundwater Standard 10.) Shaded and Bold = Concentration above the current NC 2L Groundwater Standard or NC 2L IMAC Groundwater Standard and EPA MCL 11.) EPA MCL = US Environmental Protection Agency Maximum Contaminant Level 12.) SWS GSP = Solid Waste Section Groundwater Protection Standard 13.) SWS Reporting Limit = NCPQL or lab -specific reporting limit prior to October 2007 and NCSWSL starting in October 2007 and ending June 1, 2018 14.) = EPA MCL is an action level 15.) = EPA MCL is a secondary standard 16.) Historical data prior to 10/30/07 provided by HDR Engineering of the Carolinas, Inc. Data 10/30/07 to 6/30/2020 Provided by Golder 17.) Samples collected using low -flow purge and sample techniques. 18.) The following dilutions were noted for the April 2020 event: Chloride & Sulfate 2x @ MW-17S, 4x @ MW-18, 5x @ MW-5, 10x @ MW-14, 50x @ MW-9; Nitrate as N, Nitrate/Nitrite as N 10x @ MW-4; Total Alkalinity as CaCO3 2x @ MW-6, MW-7, MW-8, MW-14, 5x @ MW-11 SR, MW-11 DR, MW-18, 10x @ MW-9; Antimony, Selenium, Thallium 2x @ MW-4, MW-5, MW-11SR, MW-11 DR, MW-13S, MW-13D, MW-14, W 19.) PQL = Practical quantitation limit - lab specific limit 20.) MDL = Method Detection Limit 21.) SWSL = Solid Waste Section Reporting Limits (historic) 22.) The Blake Well not sampled in June 2018 and April 2020 as the power was out at the residence and no sample could be obtained. TP1j2 35 20-043A Moore County R-Im LFG6 WQ Mon1-Ii 03- Seml-AnnueI WQ Monll 1i 2021-2022Te112021 AppendixIII- HlsioMc G-21-10 WQMR Tables Fa Appendix Msx Page 31 of 31 Appendix IV - Time vs Concentration Charts 12.0 11.5 11.0 10.5 10.0 9.5 9.0 8.5 8.0 7.5 J 00 7.0 7 c 6.5 0 +� 6.0 L v 5.5 U 0 5.0 v 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 Benzene Concentrations Over Time - MSW Landfill Wells tD I� n X W M M O . 1 c 1 N N M V �* M M tD LD I� W 00 M O O . 1 c 1 N N M M V M M tD LD I� 00 W O M O O -i N M M M M M M M O O O O O O O O O O O O O O O O O -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 N C4 N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ c-I ci ci ci ci ci ci ci ci ci ci ci c-I ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O LD c\-I 00 f\11 O L) N n N M KT -1 LD -1 00 M O l 1 N n N M 'ZT\-I tD .\-I 0000 c\ O Lr N n N a) KT\-I t\D\-I 0000 !\ O l! N n N O O O O r-I O -4 O O O O -4 O O O O c-I O c-I O O O O C-I O O O O -4 O -4 O O O O -4 O O O O c-I O c-I O O Sampling Dates MW-6 MW-7 MW-8 MW-9 MW-15R T:\ENV\Proj.ta'202014358-20-043A Moore County Routine LFG & W Q MoniWingThase 03 - Semi -Annual W Q Monitoring 2021-2022\FaII 2021 Wppendix IV - ChanaM20-10 Table fa 2L Exoeedanoe Cha0s.Aax 5.0 4.5 4.0 3.5 - 3.0 c c 0 + 2.5 c v U C 2.0 1.5 1.0 0.5 0.0 Benzene Concentrations Over Time - C&D Landfill Wells lD I� n 00 Q1 O O O -1 N N M M �* �* M LD LD I, n W O O O O -i -i N M m �* �* M lD lD I� n 00 W Ol O O c-I O O O O Q1 O O O O O O O O O O O O O O O O O O -1 -1 -1 -1 -1 -1 -1 -1 -1 c-I ci ci ci c-I c-I ci ci N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ c-I ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci a-i ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O l! N n N M .\-t L\D -1 W !\ O l! N n N M\-I l\D -1 W !\ O l! N n N M .\-I L\D rt O c-t O O O O a--t O O O O c-t O c-t O O O O c-t O O O O c-t O c-t O O O O c-t O Sampling Dates MW-11DR MW-13D MW-13SR MW-14 T:\ENV\Proj.ta'202014358-20-043A Moore County Routine LFG & W Q MoniWingThase 03 - Semi -Annual W Q Monitoring 2021-2022\FaII 2021 Wppendix IV - ChanaM20-10 Table fa 2L Exoeedanoe Cha0s.Aax 30.0 25.0 20.0 C C 0 -P 15.0 L a) U C 0 U 10.0 5.0 0.0 Vinyl Chloride Concentrations Over Time - MSW Landfill Wells lD I� n W M M O O -1 N N m M V V M LD LD I, n W O M O O -1 -1 N m M �* V M LD LD Ol O O Ql M M O O O O O O O O O O O O O O O O O -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 a --I a --I a --I ci ci ci N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci a-i a --I ci ci ci ci ci ci ci \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ O C) N I) N 0 (D c-I LD ci QO m O C) N a N Ol a .--I LD Cr-ID 0 C3 O a N a N Ol a .--I LD ci 0 m O Lf1 N I� N 0 � c-t O i--t O O O O c-t O O O O c-t O i--t O O O O i--t O O O O c-t O c-t O O O O i--t O O O O c-t O i--t O O O O Sampling Dates MW-6 MW-7 MW-8 MW-9 MW-15R T:\ENV\Proj.ts'202014358-20-043A Moore County Routine LFG & W Q MoniWingThase 03 - Semi -Annual W Q Monitoring 2021-2022\FaII 2021 Wppendix IV - ChanaM20-10 Table fa 2L Exoeedanoe Cha0s.Aax C 60.0 50.0 40.0 20.0 10.0 0.0 Vinyl Chloride Concentrations Over Time - C&D Landfill Wells l0 n n QO Q1 M O O -1 N N M M �* V Ln LD LD I, n w M M O O r-I r-I N M M V V M LD LD I, n M w M O O r-I Ol Ol Ol M Ql M O O O O O O O O O O O O O O O O O ri rH r-I r-I ri ri ri r-I r-I ri ri ri ri ri ri ri ri N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ c-I c-I ri c-I c-I c-I ri c-I c-I c-I c-I c-I c-I ri c-I c-I c-I c-I c-I ri c-I c-I c-I c-I a --I c-I a --I c-I c-I c-I c-I c-I ri c-I c-I c-I ri c-I c-I c-I c-I c-I ri O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O Ln N n N O\l �* r-I LLDD r-I W !\ O Lr N n N a) �* -i L\D -1 W !\ O Ln N n N O\l �* r-I tDD r-I W M O Ln N n N M �* -4 O r-I O O O O r-I O O O O r-I O r 4 O O O O r 4 O O O O r-I O r-I O O O O r-I O O O O "I O "I O O O O Sampling Dates MW-11DR MW-13D MW-13SR MW-14 T:\ENV\Proj.ta'202014358-20-043A Moore County Routine LFG & W Q MoniWingThase 03 - Semi -Annual W Q Monitoring 2021-2022\FaII 2021 Wppendix IV - ChanaM20-10 Table fa 2L Exoeedanoe Cha0s.Aax C 30.0 25.0 20.0 10.0 5.0 0.0 tD O O O O \ ci \ ci \ ci \ ci O O O O \ C) \ O \ a \ O cis-1,2-Dichlloroethene Concentrations Over Time - MSW Landfill Wells 00 00 0) M O O N N M m to Ln l0 LD I, n 00 00 0) 01 O O -1 a1 O O O O ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci c-I c-I N N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ c-I c-I ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci O O O O O O O O O O O O O O O O O O O O O O O O O O O O O V O V O V O V O O O O O O zT O V O V O zT O O c-t O -4 O -4 O -4 O -4 O -4 O I--t O c-t O c-t O c-t O c-t O c-t O c-t O r- Sampling Dates MW-6 MW-7 MW-8 MW-9 MW-15R T:\ENV\Proj.ta'202014358-20-043A Moore County Routine LFG & W Q MoniWingThase 03 - Semi -Annual W Q Monitoring 2021-2022\FaII 2021 Wppendix IV - ChanaM20-10 Table fa 2L Exoeedanoe Cha0s.Aax 60.0 50.0 40.0 C C 0 +� 30.0 c U U C 0 U 20.0 10.0 cis 1,2-Dichloroethene Concentrations Over Time - C&D Landfill Wells 0.0 — Sr v� l0 9.0 I, n 00 00 Ql 0) -1 N N M M Ln Ln l0 w I, n 00 00 01 of O O O O O O O O O O .--t .--t .-i .--t .-i .--t .--t .-i .--t .--t .--t .-i .-i .--i -1 N (N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ C) 0 C) 0 C) C) 0 C) CD CD CD CD 0 CD 0 0 CD 0 C) C) C) C) C) 0 0 C) 0 C) C) C) C) C) O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O a O a O a O ItT O ItT O Rt O Rt O Rt O a O a O a O a O ItT O ItT O ItT O Rt O O -1 O -1 O -1 O -i O -i O -i O -i O -1 O -1 O -1 O -1 O -1 O -i O -i O -1 O -1 Sampling Dates MW-11DR MW-13D MW-13SR MW-14 T:\ENV\Proj.ts'202014358-20-043A Moore County Routine LFG & W Q MoniWingThase 03 - Semi -Annual W Q Monitoring 2021-2022\FaII 2021 Wppendix IV - ChanaM20-10 Table fa 2L Exoeedanoe Cha0s.Aax c 1,4-Dioxane Concentrations Over Time - MSW Landfill Wells 39.0 34.0 29.0 24.0 14.0 9.0 4.0 -1.0 00 Q) rn rn m m 0, O O O O O O ci ci ci c-I ci ci ci N N N N N N \ \ \ \ \ \ \ \ \ \ \ \ \ O O O O O O O O O O O O O \ \ \ \ \ \ \ \ \ \ \ \ \ -1 0 M 0 n 01 -1 ci M 0 n 01 -1 O O O CD CDO O O Sampling Dates -i -i -i ci ci ci \ \ \ ci M Lf1 O O O MW-6 MW-7 MW-8 MW-9 MW-15R MW-2 T:\ENV\Proj.ts'202014358-20-043A Moore County Routine LFG & W Q MoniWingThase 03 - Semi -Annual W Q Monitoring 2021-2022\FaII 2021 Wppendix IV - ChanaM20-10 Table fa 2L Exoeedanoe Cha0s.Aax 16.0 15.0 14.0 13.0 12.0 11.0 10.0 J OA 9.0 0 +� 8.0 L Y u 7.0 c 0 v 6.0 5.0 4.0 3.0 2.0 1.0 0.0 1,4-Dioxane Concentrations Over Time - C&D Landfill Wells 00 00 O O O 0) O 0) O O O O ci ci ci ci ci ci ci ci N N N N \ \ \ \ \ \ \ \ \ \ \ \ ci ci ci ci ci ci ci ci ci ci ci ci O O O O O O O O O O O O O N N to 00 O N N L\D 0000 rt c-t O O O O r-t c-t O O O O Sampling Dates MW-11DR MW-13D MW-13SR MW-14 O o -1 rt -1 \ \ \ \ \ ci ci ci ci ci \ \ \ \ \ 1 -4 O O O T:\ENV\Proj.ta'202014358-20-043A Moore County Routine LFG & W Q MoniWingThase 03 - Semi -Annual W Q Monitoring 2021-2022\FaII 2021 Wppendix IV - ChanaM20-10 Table fa 2L Exoeedanoe Cha0s.Aax