20086 Final Grade Soil Assessment Report_Chadbourn Mill 20210917

Via Email
September 17, 2021
NCDEQ – Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, NC 27699-1646
Attention: Mr. Bill Schmithorst
Re: Final Grade Assessment Report
Chadbourn Mill
451 Jordan Place
Charlotte, North Carolina
Brownfields Project No. 20086-16-060
H&H Job No. WPP-005
Dear Bill,
On behalf of Chadbourn Mill Owner, LLC, Hart & Hickman, PC is providing the attached Final
Grade Assessment Report for the Chadbourne Mill Brownfields Site (Brownfields Project
20086-16-060) in Charlotte, Mecklenburg County, North Carolina.
Should you have any questions or need additional information, please do not hesitate to contact
us.
Very truly yours,
Hart & Hickman, PC
John Lopez, PG, RSM Ralph McGee, PG
Project Manager Project Manager
cc: Mr. Justin Trowbridge (White Point Partners)

Attachment: Final Grade Assessment Report
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Final Grade Soil Assessment Report
Chadbourn Mill
451 Jordan Place
Charlotte, North Carolina
Brownfields Project No. 20086-16-060
H&H Job No.WPP-005

Table of Contents
1.0 Introduction ............................................................................................................................ 1
2.0 Final Grade Soil Assessment Activities ................................................................................ 2
2.1 Final Grade Soil Sampling Methodologies .......................................................................... 2
2.2 Final Grade Soil Sample Results .......................................................................................... 4
2.3 Risk Evaluation..................................................................................................................... 5
3.0 Summary .................................................................................................................................. 6

List of Attachments

Table 1 Summary of Soil Analytical Data

Figure 1 Site Location Map
Figure 2 Final Grade Soil Sample Location Map

Appendix A Laboratory Analytical Report
Appendix B DEQ Risk Calculator

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Final Grade Soil Assessment Report
Chadbourn Mill
451 Jordan Place
Charlotte, North Carolina
Brownfields Project No. 20086-16-060
H&H Job No.WPP-005

1.0 Introduction

On behalf of Chadbourn Mill Owner, LLC (Prospective Developer or PD), Hart & Hickman, PC
(H&H) has prepared this Final Grade Soil Assessment Report for a portion of the Chadbourn Mill
Brownfields property (Brownfield Project No. 20086-16-060) located at 451 Jordan Place in
Charlotte, Mecklenburg County, North Carolina (Site). The Chadbourn Mill Brownfields property
has been subdivided into two parcels of land. The Site is comprised of the approximately 2-acre
parcel of land (Parcel ID No. 0836707) located in the western portion of the larger approximately
5.75-acre Chadbourn Mill Brownfields property. A Site location map is provided as Figure 1, and
a Site plan is depicted in Figure 2.

Brownfields redevelopment activities at the Site included upfit and renovations for adaptive reuse
of the existing mill building and boiler building for commercial purposes. A description of the
Brownfields redevelopment activities was provided to the North Carolina Department of
Environmental Control (DEQ) Brownfields Program in the Annual Redevelopment Summary
Report and Final Grade Soil Assessment Work Plan dated January 30, 2021.

A Brownfields Agreement between DEQ and Faison-Chadbourn Mill, LLC was executed for the
Site on September 1, 2017. Land Use Restriction (LUR) No. 11 of the executed Brownfields
Agreement includes a requirement for collection of final grade soil samples in areas at the Site that
are not covered with buildings or concrete or asphaltic paved surfaces. Accordingly, H&H
included a Final Grade Soil Assessment Work Plan (Work Plan) in the January 30, 2021 submittal
to the Brownfields Program referenced above to conduct final grade soil sampling at the Site. The
Work Plan was subsequently approved by DEQ in a letter dated October 27, 2021.

The following report describes final grade soil sampling activities conducted at the Site.
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2.0 Final Grade Soil Assessment Activities

As discussed in the Work Plan, H&H walked the Site on January 24, 2021 to identify areas not
covered by building foundations, sidewalks, or asphaltic or concrete paved (hardscape) surfaces.
The result of the Site walk indicated that the Site is predominately covered with impervious
surfaces with the exception of landscaped and/or grassy areas along the Site boundaries. In
addition, landscaped and/or grassy areas were identified within islands installed in the asphalt
parking area. A figure depicting landscaped areas at the Site along with proposed final grade
sample locations was provided in the approved Work Plan, and is again provided as Figure 2.

On April 22, 2021, final grade soil sampling activities were conducted at the Site to evaluate the
potential for impacts in shallow soil in landscaped areas of the Site that may pose unacceptable
exposure risks to residential occupants. The soil sampling activities were performed in general
accordance with the DEQ IHSB Guidelines for Assessment and Cleanup of Contaminated Sites
(Guidelines) dated January 2020, the DEQ-approved Work Plan, and the most recent versions of
the U.S. Environmental Protection Agency (EPA) Region IV Science and Ecosystem Support
Division (SESD) Field Branches Quality System and Technical Procedures guidance.

2.1 Final Grade Soil Sampling Methodologies

As discussed in the approved Work Plan, landscaped areas at the Site were divided into four final
grade evaluation areas (FG-1 through FG-4). Soil borings were advanced in each final grade
evaluation area for collection of aliquot soil samples. The final grade evaluation areas and aliquot
soil boring locations are shown in Figure 2 and are described further below:

 Final grade evaluation area FG-1 included the landscaped and/or grassy areas located near
the southwestern Site boundary along Jordan Place;
 Final grade evaluation area FG-2 included the landscaped and/or grassy areas located
around the northern corner of the mill building and along N. Brevard Street;
 Final grade evaluation area FG-3 included the landscaped and/or grassy areas in the vicinity
of the boiler building and along Charles Avenue; and
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 Final grade evaluation area FG-4 included the landscaped and/or grassy areas located to
the southeast of the boiler building and the islands in the asphalt parking lot.

To collect representative soil samples, five aliquot soil borings were advanced within each final
grade evaluation area (Figure 2). Each aliquot soil boring was advanced to approximately 2 feet
below ground surface (bgs) utilizing a decontaminated stainless-steel hand auger. Continuous soil
samples were collected from the center of the hand auger bucket at each boring and observed for
lithology , the presence of obvious staining or unusual odors, and field screened for volatile organic
vapors using a calibrated photo-ionization detector (PID). Field personnel did not observe the
presence of staining or odors in the aliquot soil samples and field screening with the PID did not
indicate obvious evidence of impact. Soil lithology at the aliquot locations generally consisted of
moist clayey silt.

Following boring advancement, one representative grab soil sample was collected from an
undisturbed portion of a sample aliquot location in each final grade evaluation area. Soil sample
aliquots from each area were then combined and homogenized to form one composite soil sample
representative of that evaluation area for a total of four (4) composite soil samples (FG-1 through
FG-4). Soil samples selected for laboratory analysis from each evaluation area were collected
directly into dedicated laboratory supplied sample containers, labeled with the sample
identification, date, time, and requested analysis and placed in a laboratory supplied cooler with
ice. The samples were then delivered to Pace Analytical (Pace) under standard chain of custody
protocols for analysis.

Composite soil samples were submitted to Pace for analysis of semi-volatile organic compounds
(SVOCs) by EPA Method 8270 and Resource Conservation and Recovery Act (RCRA) metals
plus hexavalent chromium by EPA Methods 6020/7471/7196. The grab soil samples were
submitted to Pace for analysis of VOCs by EPA Method 8260.

For quality assurance and quality control (QA/QC) purposes, H&H collected a duplicate composite
and grab sample (FG-DUP) from final grade evaluation area FG-3. The duplicate soil sample was
submitted for the same analyses as the parent samples as described above.
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Following sampling activities, the soil borings were properly abandoned and the surfaces were
repaired similar to pre-drilling conditions. Additionally, the soil boring locations were estimated
using a hand-held global positioning system (GPS) unit. Results of the laboratory analysis of the
final grade samples are discussed below.

2.2 Final Grade Soil Sample Results

A tabular summary of final grade soil sample laboratory analytical results is presented in Table 1,
and a copy of the laboratory analytical report and chain of custody record is provided in Appendix
A. The laboratory analytical results were compared to the IHSB Non-Residential PSRGs dated
June 2021. In addition to the PSRGs, metals results were compared to published concentrations
for naturally occurring metals in soil.

VOCs
Trace levels of VOCs were detected in the soil samples collected from final grade areas FG-1, FG-
2, and FG-3. The detected concentrations were below the respective IHSB Non-Residential
PSRGs. Please note, multiple compounds were detected in duplicate sample FG-DUP, including
trichloroethene, which were not detected in the parent sample FG-3. The laboratory reviewed the
data and did not find any errors. The discrepancy is likely due to homogenization of the sample,
however this result suggests that the trace concentrations of VOCs detected are not likely
widespread.

SVOCs
No SVOCs were detected above the laboratory method detection limits in the final grade soil
samples.

Metals
As expected, due to the presence of naturally occurring metals in soil, several metals were detected
at concentrations above laboratory method detection limits in the final grade soil samples collected
at the Site. Arsenic was detected above the IHSB Residential PSRG of 3.0 mg/kg and slightly
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above the upper limit of the range of naturally occurring arsenic in North Carolina soil (18 mg/kg)
in FG-1 at a concentration of 24.7 mg/kg. No other metals were detected above the IHSB Non-
Residential PSRGs.

Because the concentrations of other metals detected in FG-1 are similar to concentrations detected
in other samples and are generally similar to published background concentrations, the
concentration of arsenic detected in FG-1 is likely anomalous and not widespread or representative
of soil conditions at the Site. Although the arsenic detection is likely anomalous, H&H utilized
the arsenic concentration detected in FG-1 in the conservative risk evaluation described below.

2.3 Risk Evaluation

The DEQ IHSB health-based PSRGs are very conservative and based on the lower of a Target
Carcinogenic Risk (TCR) of 1 x 10-6 for potential carcinogenic risks and a Target Hazard Quotient
(THQ) of 0.2 for potential noncarcinogenic risks. The DEQ and EPA acceptable risks for potential
carcinogenic risks is a cumulative lifetime incremental carcinogenic risk (LICR) of 1 x 10-4 and a
cumulative hazard index (HI) of 1 for noncarcinogenic risks. H&H utilized the DEQ Risk
Calculator (June 2021 version) to further evaluate cumulative risks to residential occupants based
on the final grade soil sample analytical results.

The highest concentration of each compound detected in any final grade soil sample (including the
arsenic concentration detected in FG-1 and trace VOC concentrations in FG-DUP) was used to
model a hypothetical worst-case exposure risk under a non-residential use scenario. Please note
that, although other metal concentrations detected were consistent with background, these
concentrations were also included in the risk calculator.

The risk calculator results indicate that the cumulative LICR is 8.5 x 10-6 and the cumulative HI is
0.10. The results of the risk calculations indicate that the calculated cumulative carcinogenic and
noncarcinogenic risks are minimum of one order of magnitude below the DEQ and EPA acceptable
levels for non-residential use. A copy of the completed DEQ Risk Calculator is provided as
Appendix B.
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3.0 Summary

Redevelopment activities at the Chadbourn Mill Brownfields property located at 451 Jordan Place
in Charlotte, Mecklenburg County, North Carolina are complete. Redevelopment activities
included mass grading, upfit of the existing mill building, and construction of new parking areas.

In accordance with the Brownfields Agreement, H&H conducted final grade soil sampling
activities at the Site. The final grade soil sampling activities were conducted in April 2021 and in
accordance with the approved Work Plan dated January 30, 2021. Final grade soil sampling
activities included the collection of soil samples to evaluate the potential for impacts in areas at
the Site that were not covered by building foundations, sidewalks, or asphaltic or concrete parking
areas and driveways following redevelopment.

Laboratory analytical results indicate the presence of arsenic slightly above the DEQ IHSB Non-
Residential PSRG in FG-1. The arsenic detection in FG-1 appears anomalous in comparison to
the other concentrations detected at the Site. However, the arsenic concentration was still utilized
in the risk evaluation for the Site. No other compounds were detected in Site soil at concentrations
exceeding the Non-Residential PSRGs.

To further evaluate cumulative risks to non-residential occupants, H&H utilized the DEQ Risk
Calculator dated June 2021. Results of a hypothetical worst-case risk calculation utilizing the
highest concentrations detected indicate that cumulative carcinogenic and noncarcinogenic risks
are a minimum of one order of magnitude below the DEQ and EPA acceptable levels under a non-
residential use scenario. Accordingly, the Site has been redeveloped for its intended use in
accordance with the DEQ-approved EMP and no further final grade sampling is warranted.

Table
Table 1Summary of Soil Analytical DataChadbourn Mill451 Jordan PlaceCharlotte, North CarolinaH&H Job No. WPP-005Sample IDSample LocationDepth (ft bgs)Sample TypeComposite Grab Composite Grab Composite Grab Composite Grab Composite GrabDateUnitsVOCs (8260B)-- -- --AcetoneNA <0.0524 NA0.147 JNA <0.0663 NA0.0621 JNA <0.0466140,000-- --BenzeneNA <0.0033 NA <0.0034 NA <0.0041 NA0.0083 JNA <0.00295.4-- --EthylbenzeneNA <0.0038 NA <0.0040 NA <0.0048 NA0.0053 JNA <0.003427-- --NapthaleneNA0.0163NA0.0195NA0.0085 JNA0.0140NA <0.00388.8-- --TolueneNA0.0052 JNA <0.0024 NA0.0066 JNA0.0156NA <0.00219,700-- --TrichloroetheneNA <0.0021 NA <0.0022 NA <0.0027 NA1.330NA <0.00194.0-- --1,2,4-TrimethylbenzeneNA0.0047 JNA <0.0023 NA <0.0028 NA0.0043 JNA <0.0020370-- --m&p-XyleneNA <0.0056 NA <0.0059 NA <0.0071 NA0.0230NA <0.0050500-- --o-XyleneNA0.0052 JNA <0.0038 NA <0.0046 NA0.0105NA <0.0032590-- --SVOCs (8270E)ALL BDL NA ALL BDL NA ALL BDL NA ALL BDL NA ALL BDL NA-- -- --Metals (6020B/7471B/7199)Arsenic 24.7NA2.10NA1.69NA1.97NA1.80NA3.0 1.0 - 18 4.8Barium 81.0NA107NA106NA144NA117NA47,000 50 - 1,000 356Cadmium 0.233 JNA0.152 JNA0.124 JNA0.143 JNA <0.111 NA200 1.0 - 10 4.3Chromium (total) 33.8NA51.7NA34.2NA60.0NA43.0NANE 7.0 - 300 65Hexavalent Chromium 0.361 JNA <0.331 NA <0.358 NA <0.327 NA <0.330 NA6.5 NE NETrivalent Chromium 33.8NA51.7NA34.2NA60.0NA43.0NA350,000 NE NELead 48.2NA21.1NA10.3NA11.6NA10.4NA800 0 - 50 16Mercury 0.0603NA0.0305 JNA0.0302 JNA0.0238 JNA <0.0233 NA70 0.03 - 0.52 0.121Selenium 0.747 JNA0.881 JNA0.771 JNA1.17 JNA1.54 JNA1,200 <0.1 - 0.8 0.4Silver<0.111 NA <0.112 NA <0.121 NA <0.111 NA <0.112 NA1,200 0 - 5.0 NENotes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021).2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Background Cd and Ag concentrations were taken from Southeastern and Conterminous US soils.Soil concentrations are reported in milligrams per kilogram (mg/kg). Laboratory analytical methods are shown in parentheses.Compound concentrations are reported to the laboratory method detection limit.Aside from metals, only those compounds detected in at least one sample are shown in the table above.ft bgs = feet below ground surface; VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; NA = not analyzed; NE = not established; -- = not applicable; BDL = below laboratoy method detection limitJ = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in an estimated concentration. 0-2FG-4 Western Site Area and Parking Lot Islands0-24/22/2021Background MetalsNorth Carolina 2Range MeanNon-Residential PSRGs1mg/kgNorthern Corner of Mill Buidling - N. Brevard StreetFG-20-24/22/2021FG-3/FG-DUPNorthern Site Boundary - Charles Avenue0-24/22/2021FG-1 4/22/2021Southwestern Site BoundaryTable 1 (Page 1 of 1)Hart & Hickman, PC
Figures
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE EAST, NORTH CAROLINA 1991
TITLE
PROJECT
SITE LOCATION MAP
CHADBOURN MILL451 JORDAN PLACECHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
1-19-20 0
1WPP-005
SITE
REVISION NO. 0
JOB NO. WPP-005
DATE: 8-13-21
FIGURE NO. 2
CHADBOURN MILL451 JORDAN PLACE
CHARLOTTE, NORTH CAROLINA
FINAL GRADE SOIL SAMPLE
LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
CHADBOURN MILL BROWNFIELDSPROPERTY BOUNDARY
LYNX BLUE LINE LIGHT RAIL
LANDSCAPED AREAS
FG-1 SOIL ALIQUOT SAMPLE LOCATION
FG-2 SOIL ALIQUOT SAMPLE LOCATION
FG-3 SOIL ALIQUOT SAMPLE LOCATION
FG-4 SOIL ALIQUOT SAMPLE LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
N. B
R
E
V
A
R
D
S
T
R
E
E
T
RESIDENTIAL
JORD
A
N

P
L
AC
E
CHARL
E
S

A
V
E
N
U
E
NOTES:
1. REDEVELOPMENT PLANS PROVIDED BY CLINE DESIGN.
CHARL
E
S

A
V
E
N
U
E
FG-1A
FG-1C
FG-1D
FG-1E
FG-2A
FG-2B
FG-2C
FG-2D
FG-3A
FG-3B
FG-3C
FG-3D FG-4A
FG-4B
FG-4C
FG-4E
ADJACENT PORTION OF CHADBOURN
MILL BROWNFIELDS
(CUSA NC HOLDINGS LP)
FORMER BOILER BUILDING
MILL BUILDING
FG-1B
FG-2E FG-3E
FG-4D

Appendix A
Laboratory Analytical Report

#=CL#
May 03, 2021
LIMS USE: FR - ALEXIS MCKENZIE
LIMS OBJECT ID: 92534944
92534944
Project:
Pace Project No.:
RE:
Alexis McKenzie
Hart & Hickman
2923 S Tryon Street
Suite 100
Charlotte, NC 28203
WPP-005
Dear Alexis McKenzie:
Enclosed are the analytical results for sample(s) received by the laboratory on April 23, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 55
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92534944
WPP-005
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 55
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92534944
WPP-005
Lab ID Sample ID Matrix Date Collected Date Received
92534944001 FG-1 (0-2)Solid 04/22/21 14:10 04/23/21 09:30
92534944002 FG-2 (0-2)Solid 04/22/21 14:30 04/23/21 09:30
92534944003 FG-3 (0-2)Solid 04/22/21 14:45 04/23/21 09:30
92534944004 FG-4 (0-2)Solid 04/22/21 15:30 04/23/21 09:30
92534944005 FG-DUP Solid 04/22/21 00:00 04/23/21 09:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 55
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92534944
WPP-005
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92534944001 FG-1 (0-2)EPA 6020B 7 PANLD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92534944002 FG-2 (0-2)EPA 6020B 7 PANLD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92534944003 FG-3 (0-2)EPA 6020B 7 PANLD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92534944004 FG-4 (0-2)EPA 6020B 7 PANLD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANMSP
92534944005 FG-DUP EPA 6020B 7 PANLD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CSEM
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANMSP
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-1 (0-2)Lab ID:92534944001 Collected:04/22/21 14:10 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 24.7 mg/kg 04/25/21 21:20 7440-38-204/25/21 12:411.28 0.128 5
Barium 81.0 mg/kg 04/25/21 21:20 7440-39-304/25/21 12:413.21 0.195 5
Cadmium 0.233J mg/kg 04/25/21 21:20 7440-43-9 J04/25/21 12:411.28 0.110 5
Chromium 33.8 mg/kg 04/25/21 21:20 7440-47-304/25/21 12:416.42 0.380 5
Lead 48.2 mg/kg 04/25/21 21:20 7439-92-104/25/21 12:412.57 0.127 5
Selenium 0.747J mg/kg 04/25/21 21:20 7782-49-2 J04/25/21 12:413.21 0.231 5
Silver ND mg/kg 04/25/21 21:20 7440-22-404/25/21 12:410.642 0.111 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0603 mg/kg 04/27/21 13:57 7439-97-604/26/21 14:110.0514 0.0231 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/21 11:07 83-32-904/27/21 09:233971391
Acenaphthylene ND ug/kg 04/27/21 11:07 208-96-804/27/21 09:233971391
Aniline ND ug/kg 04/27/21 11:07 62-53-304/27/21 09:233971551
Anthracene ND ug/kg 04/27/21 11:07 120-12-704/27/21 09:233971301
Benzo(a)anthracene ND ug/kg 04/27/21 11:07 56-55-304/27/21 09:233971321
Benzo(a)pyrene ND ug/kg 04/27/21 11:07 50-32-804/27/21 09:233971371
Benzo(b)fluoranthene ND ug/kg 04/27/21 11:07 205-99-204/27/21 09:233971321
Benzo(g,h,i)perylene ND ug/kg 04/27/21 11:07 191-24-204/27/21 09:233971541
Benzo(k)fluoranthene ND ug/kg 04/27/21 11:07 207-08-904/27/21 09:233971391
Benzoic Acid ND ug/kg 04/27/21 11:07 65-85-004/27/21 09:2319808521
Benzyl alcohol ND ug/kg 04/27/21 11:07 100-51-604/27/21 09:237943011
4-Bromophenylphenyl ether ND ug/kg 04/27/21 11:07 101-55-304/27/21 09:233971531
Butylbenzylphthalate ND ug/kg 04/27/21 11:07 85-68-704/27/21 09:233971671
4-Chloro-3-methylphenol ND ug/kg 04/27/21 11:07 59-50-704/27/21 09:237942791
4-Chloroaniline ND ug/kg 04/27/21 11:07 106-47-804/27/21 09:237943111
bis(2-Chloroethoxy)methane ND ug/kg 04/27/21 11:07 111-91-104/27/21 09:233971651
bis(2-Chloroethyl) ether ND ug/kg 04/27/21 11:07 111-44-404/27/21 09:233971491
2-Chloronaphthalene ND ug/kg 04/27/21 11:07 91-58-704/27/21 09:233971581
2-Chlorophenol ND ug/kg 04/27/21 11:07 95-57-804/27/21 09:233971491
4-Chlorophenylphenyl ether ND ug/kg 04/27/21 11:07 7005-72-304/27/21 09:233971481
Chrysene ND ug/kg 04/27/21 11:07 218-01-904/27/21 09:233971441
Dibenz(a,h)anthracene ND ug/kg 04/27/21 11:07 53-70-304/27/21 09:233971531
Dibenzofuran ND ug/kg 04/27/21 11:07 132-64-904/27/21 09:233971431
1,2-Dichlorobenzene ND ug/kg 04/27/21 11:07 95-50-104/27/21 09:233971431
1,3-Dichlorobenzene ND ug/kg 04/27/21 11:07 541-73-104/27/21 09:233971411
1,4-Dichlorobenzene ND ug/kg 04/27/21 11:07 106-46-704/27/21 09:233971521
3,3'-Dichlorobenzidine ND ug/kg 04/27/21 11:07 91-94-1 IL04/27/21 09:237942681
2,4-Dichlorophenol ND ug/kg 04/27/21 11:07 120-83-204/27/21 09:233971551
Diethylphthalate ND ug/kg 04/27/21 11:07 84-66-204/27/21 09:233971451
2,4-Dimethylphenol ND ug/kg 04/27/21 11:07 105-67-9 v104/27/21 09:233971651
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-1 (0-2)Lab ID:92534944001 Collected:04/22/21 14:10 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 04/27/21 11:07 131-11-304/27/21 09:233971441
Di-n-butylphthalate ND ug/kg 04/27/21 11:07 84-74-204/27/21 09:233971331
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/21 11:07 534-52-104/27/21 09:237943701
2,4-Dinitrophenol ND ug/kg 04/27/21 11:07 51-28-504/27/21 09:23198012301
2,4-Dinitrotoluene ND ug/kg 04/27/21 11:07 121-14-204/27/21 09:233971531
2,6-Dinitrotoluene ND ug/kg 04/27/21 11:07 606-20-204/27/21 09:233971451
Di-n-octylphthalate ND ug/kg 04/27/21 11:07 117-84-004/27/21 09:233971561
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/21 11:07 117-81-704/27/21 09:233971541
Fluoranthene ND ug/kg 04/27/21 11:07 206-44-004/27/21 09:233971361
Fluorene ND ug/kg 04/27/21 11:07 86-73-704/27/21 09:233971391
Hexachloro-1,3-butadiene ND ug/kg 04/27/21 11:07 87-68-3 v104/27/21 09:233971721
Hexachlorobenzene ND ug/kg 04/27/21 11:07 118-74-104/27/21 09:233971551
Hexachlorocyclopentadiene ND ug/kg 04/27/21 11:07 77-47-404/27/21 09:233972271
Hexachloroethane ND ug/kg 04/27/21 11:07 67-72-104/27/21 09:233971521
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/21 11:07 193-39-504/27/21 09:233971561
Isophorone ND ug/kg 04/27/21 11:07 78-59-104/27/21 09:233971771
1-Methylnaphthalene ND ug/kg 04/27/21 11:07 90-12-004/27/21 09:233971391
2-Methylnaphthalene ND ug/kg 04/27/21 11:07 91-57-604/27/21 09:233971591
2-Methylphenol(o-Cresol)ND ug/kg 04/27/21 11:07 95-48-704/27/21 09:233971621
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/21 11:07 15831-10-404/27/21 09:233971601
Naphthalene ND ug/kg 04/27/21 11:07 91-20-304/27/21 09:233971351
2-Nitroaniline ND ug/kg 04/27/21 11:07 88-74-404/27/21 09:2319803251
3-Nitroaniline ND ug/kg 04/27/21 11:07 99-09-204/27/21 09:2319803111
4-Nitroaniline ND ug/kg 04/27/21 11:07 100-01-604/27/21 09:237943021
Nitrobenzene ND ug/kg 04/27/21 11:07 98-95-304/27/21 09:233971841
2-Nitrophenol ND ug/kg 04/27/21 11:07 88-75-504/27/21 09:233971721
4-Nitrophenol ND ug/kg 04/27/21 11:07 100-02-704/27/21 09:2319807671
N-Nitrosodimethylamine ND ug/kg 04/27/21 11:07 62-75-904/27/21 09:233971331
N-Nitroso-di-n-propylamine ND ug/kg 04/27/21 11:07 621-64-704/27/21 09:233971491
N-Nitrosodiphenylamine ND ug/kg 04/27/21 11:07 86-30-604/27/21 09:233971411
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/21 11:07 108-60-104/27/21 09:233971891
Pentachlorophenol ND ug/kg 04/27/21 11:07 87-86-504/27/21 09:237943881
Phenanthrene ND ug/kg 04/27/21 11:07 85-01-804/27/21 09:233971301
Phenol ND ug/kg 04/27/21 11:07 108-95-204/27/21 09:233971771
Pyrene ND ug/kg 04/27/21 11:07 129-00-004/27/21 09:233971611
Pyridine ND ug/kg 04/27/21 11:07 110-86-104/27/21 09:233971251
1,2,4-Trichlorobenzene ND ug/kg 04/27/21 11:07 120-82-104/27/21 09:233971561
2,4,5-Trichlorophenol ND ug/kg 04/27/21 11:07 95-95-404/27/21 09:233971821
2,4,6-Trichlorophenol ND ug/kg 04/27/21 11:07 88-06-204/27/21 09:233971641
Surrogates
Nitrobenzene-d5 (S)79 %04/27/21 11:07 4165-60-004/27/21 09:2321-130 1
2-Fluorobiphenyl (S)69 %04/27/21 11:07 321-60-804/27/21 09:2319-130 1
Terphenyl-d14 (S)68 %04/27/21 11:07 1718-51-004/27/21 09:2315-130 1
Phenol-d6 (S)76 %04/27/21 11:07 13127-88-304/27/21 09:2318-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-1 (0-2)Lab ID:92534944001 Collected:04/22/21 14:10 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)72 %04/27/21 11:07 367-12-404/27/21 09:2318-130 1
2,4,6-Tribromophenol (S)93 %04/27/21 11:07 118-79-604/27/21 09:2318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/27/21 01:52 67-64-104/26/21 16:3416352.4 1
Benzene ND ug/kg 04/27/21 01:52 71-43-204/26/21 16:348.2 3.3 1
Bromobenzene ND ug/kg 04/27/21 01:52 108-86-104/26/21 16:348.2 2.7 1
Bromochloromethane ND ug/kg 04/27/21 01:52 74-97-504/26/21 16:348.2 2.4 1
Bromodichloromethane ND ug/kg 04/27/21 01:52 75-27-404/26/21 16:348.2 3.2 1
Bromoform ND ug/kg 04/27/21 01:52 75-25-204/26/21 16:348.2 2.9 1
Bromomethane ND ug/kg 04/27/21 01:52 74-83-904/26/21 16:3416.3 12.9 1
2-Butanone (MEK)ND ug/kg 04/27/21 01:52 78-93-304/26/21 16:3416339.2 1
n-Butylbenzene ND ug/kg 04/27/21 01:52 104-51-804/26/21 16:348.2 3.9 1
sec-Butylbenzene ND ug/kg 04/27/21 01:52 135-98-804/26/21 16:348.2 3.6 1
tert-Butylbenzene ND ug/kg 04/27/21 01:52 98-06-604/26/21 16:348.2 2.9 1
Carbon tetrachloride ND ug/kg 04/27/21 01:52 56-23-504/26/21 16:348.2 3.1 1
Chlorobenzene ND ug/kg 04/27/21 01:52 108-90-704/26/21 16:348.2 1.6 1
Chloroethane ND ug/kg 04/27/21 01:52 75-00-304/26/21 16:3416.3 6.3 1
Chloroform ND ug/kg 04/27/21 01:52 67-66-304/26/21 16:348.2 5.0 1
Chloromethane ND ug/kg 04/27/21 01:52 74-87-304/26/21 16:3416.3 6.9 1
2-Chlorotoluene ND ug/kg 04/27/21 01:52 95-49-804/26/21 16:348.2 2.9 1
4-Chlorotoluene ND ug/kg 04/27/21 01:52 106-43-404/26/21 16:348.2 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/27/21 01:52 96-12-804/26/21 16:348.2 3.2 1
Dibromochloromethane ND ug/kg 04/27/21 01:52 124-48-104/26/21 16:348.2 4.6 1
1,2-Dibromoethane (EDB)ND ug/kg 04/27/21 01:52 106-93-404/26/21 16:348.2 3.6 1
Dibromomethane ND ug/kg 04/27/21 01:52 74-95-304/26/21 16:348.2 1.7 1
1,2-Dichlorobenzene ND ug/kg 04/27/21 01:52 95-50-104/26/21 16:348.2 2.9 1
1,3-Dichlorobenzene ND ug/kg 04/27/21 01:52 541-73-104/26/21 16:348.2 2.5 1
1,4-Dichlorobenzene ND ug/kg 04/27/21 01:52 106-46-704/26/21 16:348.2 2.1 1
Dichlorodifluoromethane ND ug/kg 04/27/21 01:52 75-71-804/26/21 16:3416.3 3.5 1
1,1-Dichloroethane ND ug/kg 04/27/21 01:52 75-34-304/26/21 16:348.2 3.4 1
1,2-Dichloroethane ND ug/kg 04/27/21 01:52 107-06-204/26/21 16:348.2 5.4 1
1,1-Dichloroethene ND ug/kg 04/27/21 01:52 75-35-404/26/21 16:348.2 3.4 1
cis-1,2-Dichloroethene ND ug/kg 04/27/21 01:52 156-59-204/26/21 16:348.2 2.8 1
trans-1,2-Dichloroethene ND ug/kg 04/27/21 01:52 156-60-504/26/21 16:348.2 2.9 1
1,2-Dichloropropane ND ug/kg 04/27/21 01:52 78-87-504/26/21 16:348.2 2.5 1
1,3-Dichloropropane ND ug/kg 04/27/21 01:52 142-28-904/26/21 16:348.2 2.5 1
2,2-Dichloropropane ND ug/kg 04/27/21 01:52 594-20-704/26/21 16:348.2 2.7 1
1,1-Dichloropropene ND ug/kg 04/27/21 01:52 563-58-604/26/21 16:348.2 3.9 1
cis-1,3-Dichloropropene ND ug/kg 04/27/21 01:52 10061-01-504/26/21 16:348.2 2.2 1
trans-1,3-Dichloropropene ND ug/kg 04/27/21 01:52 10061-02-604/26/21 16:348.2 2.8 1
Diisopropyl ether ND ug/kg 04/27/21 01:52 108-20-304/26/21 16:348.2 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-1 (0-2)Lab ID:92534944001 Collected:04/22/21 14:10 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 04/27/21 01:52 100-41-404/26/21 16:348.2 3.8 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/21 01:52 87-68-304/26/21 16:3416.3 13.4 1
2-Hexanone ND ug/kg 04/27/21 01:52 591-78-604/26/21 16:3481.7 7.9 1
Isopropylbenzene (Cumene)ND ug/kg 04/27/21 01:52 98-82-804/26/21 16:348.2 2.8 1
p-Isopropyltoluene ND ug/kg 04/27/21 01:52 99-87-604/26/21 16:348.2 4.0 1
Methylene Chloride ND ug/kg 04/27/21 01:52 75-09-204/26/21 16:3432.7 22.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/27/21 01:52 108-10-104/26/21 16:3481.7 7.9 1
Methyl-tert-butyl ether ND ug/kg 04/27/21 01:52 1634-04-404/26/21 16:348.2 3.1 1
Naphthalene 16.3 ug/kg 04/27/21 01:52 91-20-304/26/21 16:348.2 4.3 1
n-Propylbenzene ND ug/kg 04/27/21 01:52 103-65-104/26/21 16:348.2 2.9 1
Styrene ND ug/kg 04/27/21 01:52 100-42-504/26/21 16:348.2 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/27/21 01:52 630-20-604/26/21 16:348.2 3.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/27/21 01:52 79-34-504/26/21 16:348.2 2.2 1
Tetrachloroethene ND ug/kg 04/27/21 01:52 127-18-404/26/21 16:348.2 2.6 1
Toluene 5.2J ug/kg 04/27/21 01:52 108-88-304/26/21 16:348.2 2.3 1
1,2,3-Trichlorobenzene ND ug/kg 04/27/21 01:52 87-61-604/26/21 16:348.2 6.6 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/21 01:52 120-82-104/26/21 16:348.2 6.9 1
1,1,1-Trichloroethane ND ug/kg 04/27/21 01:52 71-55-604/26/21 16:348.2 4.2 1
1,1,2-Trichloroethane ND ug/kg 04/27/21 01:52 79-00-504/26/21 16:348.2 2.7 1
Trichloroethene ND ug/kg 04/27/21 01:52 79-01-604/26/21 16:348.2 2.1 1
Trichlorofluoromethane ND ug/kg 04/27/21 01:52 75-69-404/26/21 16:348.2 4.5 1
1,2,3-Trichloropropane ND ug/kg 04/27/21 01:52 96-18-404/26/21 16:348.2 4.1 1
1,2,4-Trimethylbenzene 4.7J ug/kg 04/27/21 01:52 95-63-604/26/21 16:348.2 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 04/27/21 01:52 108-67-804/26/21 16:348.2 2.7 1
Vinyl acetate ND ug/kg 04/27/21 01:52 108-05-404/26/21 16:3481.7 5.9 1
Vinyl chloride ND ug/kg 04/27/21 01:52 75-01-404/26/21 16:3416.3 4.1 1
Xylene (Total)5.2J ug/kg 04/27/21 01:52 1330-20-704/26/21 16:3416.3 4.7 1
m&p-Xylene ND ug/kg 04/27/21 01:52 179601-23-104/26/21 16:3416.3 5.6 1
o-Xylene 5.2J ug/kg 04/27/21 01:52 95-47-604/26/21 16:348.2 3.6 1
Surrogates
Toluene-d8 (S)98 %04/27/21 01:52 2037-26-504/26/21 16:3470-130 1
4-Bromofluorobenzene (S)105 %04/27/21 01:52 460-00-404/26/21 16:3469-134 1
1,2-Dichloroethane-d4 (S)104 %04/27/21 01:52 17060-07-004/26/21 16:3470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.9 %04/23/21 17:27 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 77.9 %04/28/21 17:0104/28/21 16:531
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-1 (0-2)Lab ID:92534944001 Collected:04/22/21 14:10 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.361J mg/kg 05/01/21 19:57 18540-29-9 J05/01/21 11:031.28 0.327 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-2 (0-2)Lab ID:92534944002 Collected:04/22/21 14:30 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.10 mg/kg 04/25/21 21:24 7440-38-204/25/21 12:411.30 0.130 5
Barium 107 mg/kg 04/25/21 21:24 7440-39-304/25/21 12:413.24 0.197 5
Cadmium 0.152J mg/kg 04/25/21 21:24 7440-43-9 J04/25/21 12:411.30 0.111 5
Chromium 51.7 mg/kg 04/25/21 21:24 7440-47-304/25/21 12:416.48 0.384 5
Lead 21.1 mg/kg 04/25/21 21:24 7439-92-104/25/21 12:412.59 0.128 5
Selenium 0.881J mg/kg 04/25/21 21:24 7782-49-2 J04/25/21 12:413.24 0.233 5
Silver ND mg/kg 04/25/21 21:24 7440-22-404/25/21 12:410.648 0.112 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0305J mg/kg 04/27/21 13:59 7439-97-6 J04/26/21 14:110.0519 0.0233 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/21 12:07 83-32-904/27/21 09:234161461
Acenaphthylene ND ug/kg 04/27/21 12:07 208-96-804/27/21 09:234161461
Aniline ND ug/kg 04/27/21 12:07 62-53-304/27/21 09:234161631
Anthracene ND ug/kg 04/27/21 12:07 120-12-704/27/21 09:234161361
Benzo(a)anthracene ND ug/kg 04/27/21 12:07 56-55-304/27/21 09:234161391
Benzo(a)pyrene ND ug/kg 04/27/21 12:07 50-32-804/27/21 09:234161441
Benzo(b)fluoranthene ND ug/kg 04/27/21 12:07 205-99-204/27/21 09:234161391
Benzo(g,h,i)perylene ND ug/kg 04/27/21 12:07 191-24-204/27/21 09:234161611
Benzo(k)fluoranthene ND ug/kg 04/27/21 12:07 207-08-904/27/21 09:234161461
Benzoic Acid ND ug/kg 04/27/21 12:07 65-85-004/27/21 09:2320808941
Benzyl alcohol ND ug/kg 04/27/21 12:07 100-51-604/27/21 09:238323151
4-Bromophenylphenyl ether ND ug/kg 04/27/21 12:07 101-55-304/27/21 09:234161601
Butylbenzylphthalate ND ug/kg 04/27/21 12:07 85-68-704/27/21 09:234161751
4-Chloro-3-methylphenol ND ug/kg 04/27/21 12:07 59-50-704/27/21 09:238322921
4-Chloroaniline ND ug/kg 04/27/21 12:07 106-47-804/27/21 09:238323261
bis(2-Chloroethoxy)methane ND ug/kg 04/27/21 12:07 111-91-104/27/21 09:234161731
bis(2-Chloroethyl) ether ND ug/kg 04/27/21 12:07 111-44-404/27/21 09:234161561
2-Chloronaphthalene ND ug/kg 04/27/21 12:07 91-58-704/27/21 09:234161651
2-Chlorophenol ND ug/kg 04/27/21 12:07 95-57-804/27/21 09:234161561
4-Chlorophenylphenyl ether ND ug/kg 04/27/21 12:07 7005-72-304/27/21 09:234161551
Chrysene ND ug/kg 04/27/21 12:07 218-01-904/27/21 09:234161511
Dibenz(a,h)anthracene ND ug/kg 04/27/21 12:07 53-70-304/27/21 09:234161601
Dibenzofuran ND ug/kg 04/27/21 12:07 132-64-904/27/21 09:234161501
1,2-Dichlorobenzene ND ug/kg 04/27/21 12:07 95-50-104/27/21 09:234161501
1,3-Dichlorobenzene ND ug/kg 04/27/21 12:07 541-73-104/27/21 09:234161471
1,4-Dichlorobenzene ND ug/kg 04/27/21 12:07 106-46-704/27/21 09:234161591
3,3'-Dichlorobenzidine ND ug/kg 04/27/21 12:07 91-94-1 IL04/27/21 09:238322811
2,4-Dichlorophenol ND ug/kg 04/27/21 12:07 120-83-204/27/21 09:234161631
Diethylphthalate ND ug/kg 04/27/21 12:07 84-66-204/27/21 09:234161521
2,4-Dimethylphenol ND ug/kg 04/27/21 12:07 105-67-9 v104/27/21 09:234161731
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-2 (0-2)Lab ID:92534944002 Collected:04/22/21 14:30 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 04/27/21 12:07 131-11-304/27/21 09:234161511
Di-n-butylphthalate ND ug/kg 04/27/21 12:07 84-74-204/27/21 09:234161401
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/21 12:07 534-52-104/27/21 09:238323881
2,4-Dinitrophenol ND ug/kg 04/27/21 12:07 51-28-504/27/21 09:23208012901
2,4-Dinitrotoluene ND ug/kg 04/27/21 12:07 121-14-204/27/21 09:234161601
2,6-Dinitrotoluene ND ug/kg 04/27/21 12:07 606-20-204/27/21 09:234161521
Di-n-octylphthalate ND ug/kg 04/27/21 12:07 117-84-004/27/21 09:234161641
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/21 12:07 117-81-704/27/21 09:234161611
Fluoranthene ND ug/kg 04/27/21 12:07 206-44-004/27/21 09:234161421
Fluorene ND ug/kg 04/27/21 12:07 86-73-704/27/21 09:234161461
Hexachloro-1,3-butadiene ND ug/kg 04/27/21 12:07 87-68-3 v104/27/21 09:234161801
Hexachlorobenzene ND ug/kg 04/27/21 12:07 118-74-104/27/21 09:234161631
Hexachlorocyclopentadiene ND ug/kg 04/27/21 12:07 77-47-404/27/21 09:234162381
Hexachloroethane ND ug/kg 04/27/21 12:07 67-72-104/27/21 09:234161591
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/21 12:07 193-39-504/27/21 09:234161641
Isophorone ND ug/kg 04/27/21 12:07 78-59-104/27/21 09:234161851
1-Methylnaphthalene ND ug/kg 04/27/21 12:07 90-12-004/27/21 09:234161461
2-Methylnaphthalene ND ug/kg 04/27/21 12:07 91-57-604/27/21 09:234161661
2-Methylphenol(o-Cresol)ND ug/kg 04/27/21 12:07 95-48-704/27/21 09:234161701
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/21 12:07 15831-10-404/27/21 09:234161681
Naphthalene ND ug/kg 04/27/21 12:07 91-20-304/27/21 09:234161411
2-Nitroaniline ND ug/kg 04/27/21 12:07 88-74-404/27/21 09:2320803401
3-Nitroaniline ND ug/kg 04/27/21 12:07 99-09-204/27/21 09:2320803261
4-Nitroaniline ND ug/kg 04/27/21 12:07 100-01-604/27/21 09:238323161
Nitrobenzene ND ug/kg 04/27/21 12:07 98-95-304/27/21 09:234161931
2-Nitrophenol ND ug/kg 04/27/21 12:07 88-75-504/27/21 09:234161801
4-Nitrophenol ND ug/kg 04/27/21 12:07 100-02-704/27/21 09:2320808041
N-Nitrosodimethylamine ND ug/kg 04/27/21 12:07 62-75-904/27/21 09:234161401
N-Nitroso-di-n-propylamine ND ug/kg 04/27/21 12:07 621-64-704/27/21 09:234161561
N-Nitrosodiphenylamine ND ug/kg 04/27/21 12:07 86-30-604/27/21 09:234161471
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/21 12:07 108-60-104/27/21 09:234161981
Pentachlorophenol ND ug/kg 04/27/21 12:07 87-86-504/27/21 09:238324071
Phenanthrene ND ug/kg 04/27/21 12:07 85-01-804/27/21 09:234161361
Phenol ND ug/kg 04/27/21 12:07 108-95-204/27/21 09:234161851
Pyrene ND ug/kg 04/27/21 12:07 129-00-004/27/21 09:234161691
Pyridine ND ug/kg 04/27/21 12:07 110-86-104/27/21 09:234161311
1,2,4-Trichlorobenzene ND ug/kg 04/27/21 12:07 120-82-104/27/21 09:234161641
2,4,5-Trichlorophenol ND ug/kg 04/27/21 12:07 95-95-404/27/21 09:234161901
2,4,6-Trichlorophenol ND ug/kg 04/27/21 12:07 88-06-204/27/21 09:234161711
Surrogates
Nitrobenzene-d5 (S)50 %04/27/21 12:07 4165-60-004/27/21 09:2321-130 1
2-Fluorobiphenyl (S)31 %04/27/21 12:07 321-60-804/27/21 09:2319-130 1
Terphenyl-d14 (S)36 %04/27/21 12:07 1718-51-004/27/21 09:2315-130 1
Phenol-d6 (S)53 %04/27/21 12:07 13127-88-304/27/21 09:2318-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-2 (0-2)Lab ID:92534944002 Collected:04/22/21 14:30 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)52 %04/27/21 12:07 367-12-404/27/21 09:2318-130 1
2,4,6-Tribromophenol (S)57 %04/27/21 12:07 118-79-604/27/21 09:2318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 147J ug/kg 04/27/21 02:10 67-64-104/26/21 16:3417155.0 1
Benzene ND ug/kg 04/27/21 02:10 71-43-204/26/21 16:348.6 3.4 1
Bromobenzene ND ug/kg 04/27/21 02:10 108-86-104/26/21 16:348.6 2.8 1
Bromochloromethane ND ug/kg 04/27/21 02:10 74-97-504/26/21 16:348.6 2.5 1
Bromodichloromethane ND ug/kg 04/27/21 02:10 75-27-404/26/21 16:348.6 3.3 1
Bromoform ND ug/kg 04/27/21 02:10 75-25-204/26/21 16:348.6 3.0 1
Bromomethane ND ug/kg 04/27/21 02:10 74-83-904/26/21 16:3417.1 13.5 1
2-Butanone (MEK)ND ug/kg 04/27/21 02:10 78-93-304/26/21 16:3417141.1 1
n-Butylbenzene ND ug/kg 04/27/21 02:10 104-51-804/26/21 16:348.6 4.0 1
sec-Butylbenzene ND ug/kg 04/27/21 02:10 135-98-804/26/21 16:348.6 3.8 1
tert-Butylbenzene ND ug/kg 04/27/21 02:10 98-06-604/26/21 16:348.6 3.0 1
Carbon tetrachloride ND ug/kg 04/27/21 02:10 56-23-504/26/21 16:348.6 3.2 1
Chlorobenzene ND ug/kg 04/27/21 02:10 108-90-704/26/21 16:348.6 1.6 1
Chloroethane ND ug/kg 04/27/21 02:10 75-00-304/26/21 16:3417.1 6.6 1
Chloroform ND ug/kg 04/27/21 02:10 67-66-304/26/21 16:348.6 5.2 1
Chloromethane ND ug/kg 04/27/21 02:10 74-87-304/26/21 16:3417.1 7.2 1
2-Chlorotoluene ND ug/kg 04/27/21 02:10 95-49-804/26/21 16:348.6 3.0 1
4-Chlorotoluene ND ug/kg 04/27/21 02:10 106-43-404/26/21 16:348.6 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/27/21 02:10 96-12-804/26/21 16:348.6 3.3 1
Dibromochloromethane ND ug/kg 04/27/21 02:10 124-48-104/26/21 16:348.6 4.8 1
1,2-Dibromoethane (EDB)ND ug/kg 04/27/21 02:10 106-93-404/26/21 16:348.6 3.8 1
Dibromomethane ND ug/kg 04/27/21 02:10 74-95-304/26/21 16:348.6 1.8 1
1,2-Dichlorobenzene ND ug/kg 04/27/21 02:10 95-50-104/26/21 16:348.6 3.1 1
1,3-Dichlorobenzene ND ug/kg 04/27/21 02:10 541-73-104/26/21 16:348.6 2.7 1
1,4-Dichlorobenzene ND ug/kg 04/27/21 02:10 106-46-704/26/21 16:348.6 2.2 1
Dichlorodifluoromethane ND ug/kg 04/27/21 02:10 75-71-804/26/21 16:3417.1 3.7 1
1,1-Dichloroethane ND ug/kg 04/27/21 02:10 75-34-304/26/21 16:348.6 3.5 1
1,2-Dichloroethane ND ug/kg 04/27/21 02:10 107-06-204/26/21 16:348.6 5.7 1
1,1-Dichloroethene ND ug/kg 04/27/21 02:10 75-35-404/26/21 16:348.6 3.5 1
cis-1,2-Dichloroethene ND ug/kg 04/27/21 02:10 156-59-204/26/21 16:348.6 2.9 1
trans-1,2-Dichloroethene ND ug/kg 04/27/21 02:10 156-60-504/26/21 16:348.6 3.0 1
1,2-Dichloropropane ND ug/kg 04/27/21 02:10 78-87-504/26/21 16:348.6 2.6 1
1,3-Dichloropropane ND ug/kg 04/27/21 02:10 142-28-904/26/21 16:348.6 2.7 1
2,2-Dichloropropane ND ug/kg 04/27/21 02:10 594-20-704/26/21 16:348.6 2.8 1
1,1-Dichloropropene ND ug/kg 04/27/21 02:10 563-58-604/26/21 16:348.6 4.1 1
cis-1,3-Dichloropropene ND ug/kg 04/27/21 02:10 10061-01-504/26/21 16:348.6 2.3 1
trans-1,3-Dichloropropene ND ug/kg 04/27/21 02:10 10061-02-604/26/21 16:348.6 2.9 1
Diisopropyl ether ND ug/kg 04/27/21 02:10 108-20-304/26/21 16:348.6 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-2 (0-2)Lab ID:92534944002 Collected:04/22/21 14:30 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 04/27/21 02:10 100-41-404/26/21 16:348.6 4.0 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/21 02:10 87-68-304/26/21 16:3417.1 14.0 1
2-Hexanone ND ug/kg 04/27/21 02:10 591-78-604/26/21 16:3485.6 8.3 1
Isopropylbenzene (Cumene)ND ug/kg 04/27/21 02:10 98-82-804/26/21 16:348.6 2.9 1
p-Isopropyltoluene ND ug/kg 04/27/21 02:10 99-87-604/26/21 16:348.6 4.2 1
Methylene Chloride ND ug/kg 04/27/21 02:10 75-09-204/26/21 16:3434.3 23.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/27/21 02:10 108-10-104/26/21 16:3485.6 8.3 1
Methyl-tert-butyl ether ND ug/kg 04/27/21 02:10 1634-04-404/26/21 16:348.6 3.2 1
Naphthalene 19.5 ug/kg 04/27/21 02:10 91-20-304/26/21 16:348.6 4.5 1
n-Propylbenzene ND ug/kg 04/27/21 02:10 103-65-104/26/21 16:348.6 3.0 1
Styrene ND ug/kg 04/27/21 02:10 100-42-504/26/21 16:348.6 2.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/27/21 02:10 630-20-604/26/21 16:348.6 3.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/27/21 02:10 79-34-504/26/21 16:348.6 2.3 1
Tetrachloroethene ND ug/kg 04/27/21 02:10 127-18-404/26/21 16:348.6 2.7 1
Toluene ND ug/kg 04/27/21 02:10 108-88-304/26/21 16:348.6 2.4 1
1,2,3-Trichlorobenzene ND ug/kg 04/27/21 02:10 87-61-604/26/21 16:348.6 6.9 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/21 02:10 120-82-104/26/21 16:348.6 7.2 1
1,1,1-Trichloroethane ND ug/kg 04/27/21 02:10 71-55-604/26/21 16:348.6 4.5 1
1,1,2-Trichloroethane ND ug/kg 04/27/21 02:10 79-00-504/26/21 16:348.6 2.8 1
Trichloroethene ND ug/kg 04/27/21 02:10 79-01-604/26/21 16:348.6 2.2 1
Trichlorofluoromethane ND ug/kg 04/27/21 02:10 75-69-404/26/21 16:348.6 4.7 1
1,2,3-Trichloropropane ND ug/kg 04/27/21 02:10 96-18-404/26/21 16:348.6 4.3 1
1,2,4-Trimethylbenzene ND ug/kg 04/27/21 02:10 95-63-604/26/21 16:348.6 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 04/27/21 02:10 108-67-804/26/21 16:348.6 2.9 1
Vinyl acetate ND ug/kg 04/27/21 02:10 108-05-404/26/21 16:3485.6 6.2 1
Vinyl chloride ND ug/kg 04/27/21 02:10 75-01-404/26/21 16:3417.1 4.3 1
Xylene (Total)ND ug/kg 04/27/21 02:10 1330-20-704/26/21 16:3417.1 4.9 1
m&p-Xylene ND ug/kg 04/27/21 02:10 179601-23-104/26/21 16:3417.1 5.9 1
o-Xylene ND ug/kg 04/27/21 02:10 95-47-604/26/21 16:348.6 3.8 1
Surrogates
Toluene-d8 (S)99 %04/27/21 02:10 2037-26-504/26/21 16:3470-130 1
4-Bromofluorobenzene (S)106 %04/27/21 02:10 460-00-404/26/21 16:3469-134 1
1,2-Dichloroethane-d4 (S)106 %04/27/21 02:10 17060-07-004/26/21 16:3470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.1 %04/23/21 17:27 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 77.1 %04/28/21 17:0104/28/21 16:531
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-2 (0-2)Lab ID:92534944002 Collected:04/22/21 14:30 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 05/01/21 20:02 18540-29-905/01/21 11:031.30 0.331 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-3 (0-2)Lab ID:92534944003 Collected:04/22/21 14:45 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 1.69 mg/kg 04/25/21 21:27 7440-38-204/25/21 12:411.40 0.140 5
Barium 106 mg/kg 04/25/21 21:27 7440-39-304/25/21 12:413.51 0.213 5
Cadmium 0.124J mg/kg 04/25/21 21:27 7440-43-9 J04/25/21 12:411.40 0.120 5
Chromium 34.2 mg/kg 04/25/21 21:27 7440-47-304/25/21 12:417.01 0.415 5
Lead 10.3 mg/kg 04/25/21 21:27 7439-92-104/25/21 12:412.80 0.139 5
Selenium 0.771J mg/kg 04/25/21 21:27 7782-49-2 J04/25/21 12:413.51 0.252 5
Silver ND mg/kg 04/25/21 21:27 7440-22-404/25/21 12:410.701 0.121 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0302J mg/kg 04/27/21 14:01 7439-97-6 J04/26/21 14:110.0561 0.0252 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/21 12:33 83-32-904/27/21 09:234101441
Acenaphthylene ND ug/kg 04/27/21 12:33 208-96-804/27/21 09:234101441
Aniline ND ug/kg 04/27/21 12:33 62-53-304/27/21 09:234101601
Anthracene ND ug/kg 04/27/21 12:33 120-12-704/27/21 09:234101341
Benzo(a)anthracene ND ug/kg 04/27/21 12:33 56-55-304/27/21 09:234101371
Benzo(a)pyrene ND ug/kg 04/27/21 12:33 50-32-804/27/21 09:234101421
Benzo(b)fluoranthene ND ug/kg 04/27/21 12:33 205-99-204/27/21 09:234101371
Benzo(g,h,i)perylene ND ug/kg 04/27/21 12:33 191-24-204/27/21 09:234101591
Benzo(k)fluoranthene ND ug/kg 04/27/21 12:33 207-08-904/27/21 09:234101441
Benzoic Acid ND ug/kg 04/27/21 12:33 65-85-004/27/21 09:2320508811
Benzyl alcohol ND ug/kg 04/27/21 12:33 100-51-604/27/21 09:238203111
4-Bromophenylphenyl ether ND ug/kg 04/27/21 12:33 101-55-304/27/21 09:234101581
Butylbenzylphthalate ND ug/kg 04/27/21 12:33 85-68-704/27/21 09:234101731
4-Chloro-3-methylphenol ND ug/kg 04/27/21 12:33 59-50-704/27/21 09:238202881
4-Chloroaniline ND ug/kg 04/27/21 12:33 106-47-804/27/21 09:238203221
bis(2-Chloroethoxy)methane ND ug/kg 04/27/21 12:33 111-91-104/27/21 09:234101701
bis(2-Chloroethyl) ether ND ug/kg 04/27/21 12:33 111-44-404/27/21 09:234101541
2-Chloronaphthalene ND ug/kg 04/27/21 12:33 91-58-704/27/21 09:234101631
2-Chlorophenol ND ug/kg 04/27/21 12:33 95-57-804/27/21 09:234101541
4-Chlorophenylphenyl ether ND ug/kg 04/27/21 12:33 7005-72-304/27/21 09:234101531
Chrysene ND ug/kg 04/27/21 12:33 218-01-904/27/21 09:234101491
Dibenz(a,h)anthracene ND ug/kg 04/27/21 12:33 53-70-304/27/21 09:234101581
Dibenzofuran ND ug/kg 04/27/21 12:33 132-64-904/27/21 09:234101481
1,2-Dichlorobenzene ND ug/kg 04/27/21 12:33 95-50-104/27/21 09:234101481
1,3-Dichlorobenzene ND ug/kg 04/27/21 12:33 541-73-104/27/21 09:234101451
1,4-Dichlorobenzene ND ug/kg 04/27/21 12:33 106-46-704/27/21 09:234101571
3,3'-Dichlorobenzidine ND ug/kg 04/27/21 12:33 91-94-1 IL04/27/21 09:238202771
2,4-Dichlorophenol ND ug/kg 04/27/21 12:33 120-83-204/27/21 09:234101601
Diethylphthalate ND ug/kg 04/27/21 12:33 84-66-204/27/21 09:234101501
2,4-Dimethylphenol ND ug/kg 04/27/21 12:33 105-67-904/27/21 09:234101701
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-3 (0-2)Lab ID:92534944003 Collected:04/22/21 14:45 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 04/27/21 12:33 131-11-304/27/21 09:234101491
Di-n-butylphthalate ND ug/kg 04/27/21 12:33 84-74-204/27/21 09:234101381
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/21 12:33 534-52-104/27/21 09:238203831
2,4-Dinitrophenol ND ug/kg 04/27/21 12:33 51-28-5 v104/27/21 09:23205012701
2,4-Dinitrotoluene ND ug/kg 04/27/21 12:33 121-14-204/27/21 09:234101581
2,6-Dinitrotoluene ND ug/kg 04/27/21 12:33 606-20-204/27/21 09:234101501
Di-n-octylphthalate ND ug/kg 04/27/21 12:33 117-84-004/27/21 09:234101621
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/21 12:33 117-81-704/27/21 09:234101591
Fluoranthene ND ug/kg 04/27/21 12:33 206-44-004/27/21 09:234101401
Fluorene ND ug/kg 04/27/21 12:33 86-73-704/27/21 09:234101441
Hexachloro-1,3-butadiene ND ug/kg 04/27/21 12:33 87-68-304/27/21 09:234101781
Hexachlorobenzene ND ug/kg 04/27/21 12:33 118-74-104/27/21 09:234101601
Hexachlorocyclopentadiene ND ug/kg 04/27/21 12:33 77-47-404/27/21 09:234102351
Hexachloroethane ND ug/kg 04/27/21 12:33 67-72-104/27/21 09:234101571
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/21 12:33 193-39-504/27/21 09:234101621
Isophorone ND ug/kg 04/27/21 12:33 78-59-104/27/21 09:234101831
1-Methylnaphthalene ND ug/kg 04/27/21 12:33 90-12-004/27/21 09:234101441
2-Methylnaphthalene ND ug/kg 04/27/21 12:33 91-57-604/27/21 09:234101641
2-Methylphenol(o-Cresol)ND ug/kg 04/27/21 12:33 95-48-704/27/21 09:234101681
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/21 12:33 15831-10-404/27/21 09:234101651
Naphthalene ND ug/kg 04/27/21 12:33 91-20-304/27/21 09:234101391
2-Nitroaniline ND ug/kg 04/27/21 12:33 88-74-404/27/21 09:2320503361
3-Nitroaniline ND ug/kg 04/27/21 12:33 99-09-204/27/21 09:2320503221
4-Nitroaniline ND ug/kg 04/27/21 12:33 100-01-604/27/21 09:238203121
Nitrobenzene ND ug/kg 04/27/21 12:33 98-95-304/27/21 09:234101901
2-Nitrophenol ND ug/kg 04/27/21 12:33 88-75-504/27/21 09:234101781
4-Nitrophenol ND ug/kg 04/27/21 12:33 100-02-704/27/21 09:2320507931
N-Nitrosodimethylamine ND ug/kg 04/27/21 12:33 62-75-904/27/21 09:234101381
N-Nitroso-di-n-propylamine ND ug/kg 04/27/21 12:33 621-64-704/27/21 09:234101541
N-Nitrosodiphenylamine ND ug/kg 04/27/21 12:33 86-30-604/27/21 09:234101451
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/21 12:33 108-60-104/27/21 09:234101951
Pentachlorophenol ND ug/kg 04/27/21 12:33 87-86-504/27/21 09:238204011
Phenanthrene ND ug/kg 04/27/21 12:33 85-01-804/27/21 09:234101341
Phenol ND ug/kg 04/27/21 12:33 108-95-204/27/21 09:234101831
Pyrene ND ug/kg 04/27/21 12:33 129-00-004/27/21 09:234101671
Pyridine ND ug/kg 04/27/21 12:33 110-86-104/27/21 09:234101291
1,2,4-Trichlorobenzene ND ug/kg 04/27/21 12:33 120-82-104/27/21 09:234101621
2,4,5-Trichlorophenol ND ug/kg 04/27/21 12:33 95-95-404/27/21 09:234101881
2,4,6-Trichlorophenol ND ug/kg 04/27/21 12:33 88-06-204/27/21 09:234101691
Surrogates
Nitrobenzene-d5 (S)48 %04/27/21 12:33 4165-60-004/27/21 09:2321-130 1
2-Fluorobiphenyl (S)26 %04/27/21 12:33 321-60-804/27/21 09:2319-130 1
Terphenyl-d14 (S)25 %04/27/21 12:33 1718-51-004/27/21 09:2315-130 1
Phenol-d6 (S)51 %04/27/21 12:33 13127-88-304/27/21 09:2318-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-3 (0-2)Lab ID:92534944003 Collected:04/22/21 14:45 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)49 %04/27/21 12:33 367-12-404/27/21 09:2318-130 1
2,4,6-Tribromophenol (S)48 %04/27/21 12:33 118-79-604/27/21 09:2318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/27/21 02:28 67-64-104/26/21 16:3420766.3 1
Benzene ND ug/kg 04/27/21 02:28 71-43-204/26/21 16:3410.3 4.1 1
Bromobenzene ND ug/kg 04/27/21 02:28 108-86-104/26/21 16:3410.3 3.4 1
Bromochloromethane ND ug/kg 04/27/21 02:28 74-97-504/26/21 16:3410.3 3.1 1
Bromodichloromethane ND ug/kg 04/27/21 02:28 75-27-404/26/21 16:3410.3 4.0 1
Bromoform ND ug/kg 04/27/21 02:28 75-25-204/26/21 16:3410.3 3.6 1
Bromomethane ND ug/kg 04/27/21 02:28 74-83-904/26/21 16:3420.7 16.3 1
2-Butanone (MEK)ND ug/kg 04/27/21 02:28 78-93-304/26/21 16:3420749.6 1
n-Butylbenzene ND ug/kg 04/27/21 02:28 104-51-804/26/21 16:3410.3 4.9 1
sec-Butylbenzene ND ug/kg 04/27/21 02:28 135-98-804/26/21 16:3410.3 4.5 1
tert-Butylbenzene ND ug/kg 04/27/21 02:28 98-06-604/26/21 16:3410.3 3.7 1
Carbon tetrachloride ND ug/kg 04/27/21 02:28 56-23-504/26/21 16:3410.3 3.9 1
Chlorobenzene ND ug/kg 04/27/21 02:28 108-90-704/26/21 16:3410.3 2.0 1
Chloroethane ND ug/kg 04/27/21 02:28 75-00-304/26/21 16:3420.7 8.0 1
Chloroform ND ug/kg 04/27/21 02:28 67-66-304/26/21 16:3410.3 6.3 1
Chloromethane ND ug/kg 04/27/21 02:28 74-87-304/26/21 16:3420.7 8.7 1
2-Chlorotoluene ND ug/kg 04/27/21 02:28 95-49-804/26/21 16:3410.3 3.7 1
4-Chlorotoluene ND ug/kg 04/27/21 02:28 106-43-404/26/21 16:3410.3 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/27/21 02:28 96-12-804/26/21 16:3410.3 4.0 1
Dibromochloromethane ND ug/kg 04/27/21 02:28 124-48-104/26/21 16:3410.3 5.8 1
1,2-Dibromoethane (EDB)ND ug/kg 04/27/21 02:28 106-93-404/26/21 16:3410.3 4.5 1
Dibromomethane ND ug/kg 04/27/21 02:28 74-95-304/26/21 16:3410.3 2.2 1
1,2-Dichlorobenzene ND ug/kg 04/27/21 02:28 95-50-104/26/21 16:3410.3 3.7 1
1,3-Dichlorobenzene ND ug/kg 04/27/21 02:28 541-73-104/26/21 16:3410.3 3.2 1
1,4-Dichlorobenzene ND ug/kg 04/27/21 02:28 106-46-704/26/21 16:3410.3 2.7 1
Dichlorodifluoromethane ND ug/kg 04/27/21 02:28 75-71-804/26/21 16:3420.7 4.5 1
1,1-Dichloroethane ND ug/kg 04/27/21 02:28 75-34-304/26/21 16:3410.3 4.3 1
1,2-Dichloroethane ND ug/kg 04/27/21 02:28 107-06-204/26/21 16:3410.3 6.8 1
1,1-Dichloroethene ND ug/kg 04/27/21 02:28 75-35-404/26/21 16:3410.3 4.3 1
cis-1,2-Dichloroethene ND ug/kg 04/27/21 02:28 156-59-204/26/21 16:3410.3 3.5 1
trans-1,2-Dichloroethene ND ug/kg 04/27/21 02:28 156-60-504/26/21 16:3410.3 3.6 1
1,2-Dichloropropane ND ug/kg 04/27/21 02:28 78-87-504/26/21 16:3410.3 3.1 1
1,3-Dichloropropane ND ug/kg 04/27/21 02:28 142-28-904/26/21 16:3410.3 3.2 1
2,2-Dichloropropane ND ug/kg 04/27/21 02:28 594-20-704/26/21 16:3410.3 3.4 1
1,1-Dichloropropene ND ug/kg 04/27/21 02:28 563-58-604/26/21 16:3410.3 5.0 1
cis-1,3-Dichloropropene ND ug/kg 04/27/21 02:28 10061-01-504/26/21 16:3410.3 2.8 1
trans-1,3-Dichloropropene ND ug/kg 04/27/21 02:28 10061-02-604/26/21 16:3410.3 3.6 1
Diisopropyl ether ND ug/kg 04/27/21 02:28 108-20-304/26/21 16:3410.3 2.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-3 (0-2)Lab ID:92534944003 Collected:04/22/21 14:45 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 04/27/21 02:28 100-41-404/26/21 16:3410.3 4.8 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/21 02:28 87-68-304/26/21 16:3420.7 16.9 1
2-Hexanone ND ug/kg 04/27/21 02:28 591-78-604/26/21 16:34103101
Isopropylbenzene (Cumene)ND ug/kg 04/27/21 02:28 98-82-804/26/21 16:3410.3 3.5 1
p-Isopropyltoluene ND ug/kg 04/27/21 02:28 99-87-604/26/21 16:3410.3 5.1 1
Methylene Chloride ND ug/kg 04/27/21 02:28 75-09-204/26/21 16:3441.3 28.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/27/21 02:28 108-10-104/26/21 16:34103101
Methyl-tert-butyl ether ND ug/kg 04/27/21 02:28 1634-04-404/26/21 16:3410.3 3.9 1
Naphthalene 8.5J ug/kg 04/27/21 02:28 91-20-304/26/21 16:3410.3 5.4 1
n-Propylbenzene ND ug/kg 04/27/21 02:28 103-65-104/26/21 16:3410.3 3.7 1
Styrene ND ug/kg 04/27/21 02:28 100-42-504/26/21 16:3410.3 2.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/27/21 02:28 630-20-604/26/21 16:3410.3 4.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/27/21 02:28 79-34-504/26/21 16:3410.3 2.7 1
Tetrachloroethene ND ug/kg 04/27/21 02:28 127-18-404/26/21 16:3410.3 3.3 1
Toluene 6.6J ug/kg 04/27/21 02:28 108-88-304/26/21 16:3410.3 2.9 1
1,2,3-Trichlorobenzene ND ug/kg 04/27/21 02:28 87-61-604/26/21 16:3410.3 8.3 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/21 02:28 120-82-104/26/21 16:3410.3 8.7 1
1,1,1-Trichloroethane ND ug/kg 04/27/21 02:28 71-55-604/26/21 16:3410.3 5.4 1
1,1,2-Trichloroethane ND ug/kg 04/27/21 02:28 79-00-504/26/21 16:3410.3 3.4 1
Trichloroethene ND ug/kg 04/27/21 02:28 79-01-604/26/21 16:3410.3 2.7 1
Trichlorofluoromethane ND ug/kg 04/27/21 02:28 75-69-404/26/21 16:3410.3 5.7 1
1,2,3-Trichloropropane ND ug/kg 04/27/21 02:28 96-18-404/26/21 16:3410.3 5.2 1
1,2,4-Trimethylbenzene ND ug/kg 04/27/21 02:28 95-63-604/26/21 16:3410.3 2.8 1
1,3,5-Trimethylbenzene ND ug/kg 04/27/21 02:28 108-67-804/26/21 16:3410.3 3.5 1
Vinyl acetate ND ug/kg 04/27/21 02:28 108-05-404/26/21 16:341037.5 1
Vinyl chloride ND ug/kg 04/27/21 02:28 75-01-404/26/21 16:3420.7 5.2 1
Xylene (Total)ND ug/kg 04/27/21 02:28 1330-20-704/26/21 16:3420.7 5.9 1
m&p-Xylene ND ug/kg 04/27/21 02:28 179601-23-104/26/21 16:3420.7 7.1 1
o-Xylene ND ug/kg 04/27/21 02:28 95-47-604/26/21 16:3410.3 4.6 1
Surrogates
Toluene-d8 (S)98 %04/27/21 02:28 2037-26-504/26/21 16:3470-130 1
4-Bromofluorobenzene (S)106 %04/27/21 02:28 460-00-404/26/21 16:3469-134 1
1,2-Dichloroethane-d4 (S)106 %04/27/21 02:28 17060-07-004/26/21 16:3470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.8 %04/23/21 17:27 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 71.3 %04/28/21 17:0104/28/21 16:531
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-3 (0-2)Lab ID:92534944003 Collected:04/22/21 14:45 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 05/01/21 20:07 18540-29-905/01/21 11:031.40 0.358 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-4 (0-2)Lab ID:92534944004 Collected:04/22/21 15:30 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 1.80 mg/kg 04/25/21 21:30 7440-38-204/25/21 12:411.30 0.130 5
Barium 117 mg/kg 04/25/21 21:30 7440-39-304/25/21 12:413.24 0.197 5
Cadmium ND mg/kg 04/25/21 21:30 7440-43-904/25/21 12:411.30 0.111 5
Chromium 43.0 mg/kg 04/25/21 21:30 7440-47-304/25/21 12:416.48 0.383 5
Lead 10.4 mg/kg 04/25/21 21:30 7439-92-104/25/21 12:412.59 0.128 5
Selenium 1.54J mg/kg 04/25/21 21:30 7782-49-2 J04/25/21 12:413.24 0.233 5
Silver ND mg/kg 04/25/21 21:30 7440-22-404/25/21 12:410.648 0.112 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 04/27/21 09:49 7439-97-604/26/21 10:360.0518 0.0233 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/21 13:01 83-32-904/27/21 09:234121451
Acenaphthylene ND ug/kg 04/27/21 13:01 208-96-804/27/21 09:234121451
Aniline ND ug/kg 04/27/21 13:01 62-53-304/27/21 09:234121611
Anthracene ND ug/kg 04/27/21 13:01 120-12-704/27/21 09:234121351
Benzo(a)anthracene ND ug/kg 04/27/21 13:01 56-55-304/27/21 09:234121371
Benzo(a)pyrene ND ug/kg 04/27/21 13:01 50-32-804/27/21 09:234121421
Benzo(b)fluoranthene ND ug/kg 04/27/21 13:01 205-99-204/27/21 09:234121371
Benzo(g,h,i)perylene ND ug/kg 04/27/21 13:01 191-24-204/27/21 09:234121601
Benzo(k)fluoranthene ND ug/kg 04/27/21 13:01 207-08-904/27/21 09:234121451
Benzoic Acid ND ug/kg 04/27/21 13:01 65-85-004/27/21 09:2320608861
Benzyl alcohol ND ug/kg 04/27/21 13:01 100-51-604/27/21 09:238253121
4-Bromophenylphenyl ether ND ug/kg 04/27/21 13:01 101-55-304/27/21 09:234121591
Butylbenzylphthalate ND ug/kg 04/27/21 13:01 85-68-704/27/21 09:234121741
4-Chloro-3-methylphenol ND ug/kg 04/27/21 13:01 59-50-704/27/21 09:238252901
4-Chloroaniline ND ug/kg 04/27/21 13:01 106-47-804/27/21 09:238253241
bis(2-Chloroethoxy)methane ND ug/kg 04/27/21 13:01 111-91-104/27/21 09:234121711
bis(2-Chloroethyl) ether ND ug/kg 04/27/21 13:01 111-44-404/27/21 09:234121551
2-Chloronaphthalene ND ug/kg 04/27/21 13:01 91-58-704/27/21 09:234121641
2-Chlorophenol ND ug/kg 04/27/21 13:01 95-57-804/27/21 09:234121551
4-Chlorophenylphenyl ether ND ug/kg 04/27/21 13:01 7005-72-304/27/21 09:234121541
Chrysene ND ug/kg 04/27/21 13:01 218-01-904/27/21 09:234121501
Dibenz(a,h)anthracene ND ug/kg 04/27/21 13:01 53-70-304/27/21 09:234121591
Dibenzofuran ND ug/kg 04/27/21 13:01 132-64-904/27/21 09:234121491
1,2-Dichlorobenzene ND ug/kg 04/27/21 13:01 95-50-104/27/21 09:234121491
1,3-Dichlorobenzene ND ug/kg 04/27/21 13:01 541-73-104/27/21 09:234121461
1,4-Dichlorobenzene ND ug/kg 04/27/21 13:01 106-46-704/27/21 09:234121571
3,3'-Dichlorobenzidine ND ug/kg 04/27/21 13:01 91-94-1 IL04/27/21 09:238252791
2,4-Dichlorophenol ND ug/kg 04/27/21 13:01 120-83-204/27/21 09:234121611
Diethylphthalate ND ug/kg 04/27/21 13:01 84-66-204/27/21 09:234121511
2,4-Dimethylphenol ND ug/kg 04/27/21 13:01 105-67-904/27/21 09:234121711
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-4 (0-2)Lab ID:92534944004 Collected:04/22/21 15:30 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 04/27/21 13:01 131-11-304/27/21 09:234121501
Di-n-butylphthalate ND ug/kg 04/27/21 13:01 84-74-204/27/21 09:234121391
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/21 13:01 534-52-104/27/21 09:238253851
2,4-Dinitrophenol ND ug/kg 04/27/21 13:01 51-28-5 v104/27/21 09:23206012701
2,4-Dinitrotoluene ND ug/kg 04/27/21 13:01 121-14-204/27/21 09:234121591
2,6-Dinitrotoluene ND ug/kg 04/27/21 13:01 606-20-204/27/21 09:234121511
Di-n-octylphthalate ND ug/kg 04/27/21 13:01 117-84-004/27/21 09:234121621
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/21 13:01 117-81-704/27/21 09:234121601
Fluoranthene ND ug/kg 04/27/21 13:01 206-44-004/27/21 09:234121411
Fluorene ND ug/kg 04/27/21 13:01 86-73-704/27/21 09:234121451
Hexachloro-1,3-butadiene ND ug/kg 04/27/21 13:01 87-68-304/27/21 09:234121791
Hexachlorobenzene ND ug/kg 04/27/21 13:01 118-74-104/27/21 09:234121611
Hexachlorocyclopentadiene ND ug/kg 04/27/21 13:01 77-47-404/27/21 09:234122361
Hexachloroethane ND ug/kg 04/27/21 13:01 67-72-104/27/21 09:234121571
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/21 13:01 193-39-504/27/21 09:234121621
Isophorone ND ug/kg 04/27/21 13:01 78-59-104/27/21 09:234121841
1-Methylnaphthalene ND ug/kg 04/27/21 13:01 90-12-004/27/21 09:234121451
2-Methylnaphthalene ND ug/kg 04/27/21 13:01 91-57-604/27/21 09:234121651
2-Methylphenol(o-Cresol)ND ug/kg 04/27/21 13:01 95-48-704/27/21 09:234121691
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/21 13:01 15831-10-404/27/21 09:234121661
Naphthalene ND ug/kg 04/27/21 13:01 91-20-304/27/21 09:234121401
2-Nitroaniline ND ug/kg 04/27/21 13:01 88-74-404/27/21 09:2320603371
3-Nitroaniline ND ug/kg 04/27/21 13:01 99-09-204/27/21 09:2320603241
4-Nitroaniline ND ug/kg 04/27/21 13:01 100-01-604/27/21 09:238253141
Nitrobenzene ND ug/kg 04/27/21 13:01 98-95-304/27/21 09:234121911
2-Nitrophenol ND ug/kg 04/27/21 13:01 88-75-504/27/21 09:234121791
4-Nitrophenol ND ug/kg 04/27/21 13:01 100-02-704/27/21 09:2320607971
N-Nitrosodimethylamine ND ug/kg 04/27/21 13:01 62-75-904/27/21 09:234121391
N-Nitroso-di-n-propylamine ND ug/kg 04/27/21 13:01 621-64-704/27/21 09:234121551
N-Nitrosodiphenylamine ND ug/kg 04/27/21 13:01 86-30-604/27/21 09:234121461
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/21 13:01 108-60-104/27/21 09:234121961
Pentachlorophenol ND ug/kg 04/27/21 13:01 87-86-504/27/21 09:238254041
Phenanthrene ND ug/kg 04/27/21 13:01 85-01-804/27/21 09:234121351
Phenol ND ug/kg 04/27/21 13:01 108-95-204/27/21 09:234121841
Pyrene ND ug/kg 04/27/21 13:01 129-00-004/27/21 09:234121671
Pyridine ND ug/kg 04/27/21 13:01 110-86-104/27/21 09:234121301
1,2,4-Trichlorobenzene ND ug/kg 04/27/21 13:01 120-82-104/27/21 09:234121621
2,4,5-Trichlorophenol ND ug/kg 04/27/21 13:01 95-95-404/27/21 09:234121891
2,4,6-Trichlorophenol ND ug/kg 04/27/21 13:01 88-06-204/27/21 09:234121701
Surrogates
Nitrobenzene-d5 (S)43 %04/27/21 13:01 4165-60-004/27/21 09:2321-130 1
2-Fluorobiphenyl (S)42 %04/27/21 13:01 321-60-804/27/21 09:2319-130 1
Terphenyl-d14 (S)56 %04/27/21 13:01 1718-51-004/27/21 09:2315-130 1
Phenol-d6 (S)40 %04/27/21 13:01 13127-88-304/27/21 09:2318-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-4 (0-2)Lab ID:92534944004 Collected:04/22/21 15:30 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)39 %04/27/21 13:01 367-12-404/27/21 09:2318-130 1
2,4,6-Tribromophenol (S)62 %04/27/21 13:01 118-79-604/27/21 09:2318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/27/21 02:46 67-64-104/26/21 16:3414546.6 1
Benzene ND ug/kg 04/27/21 02:46 71-43-204/26/21 16:347.3 2.9 1
Bromobenzene ND ug/kg 04/27/21 02:46 108-86-104/26/21 16:347.3 2.4 1
Bromochloromethane ND ug/kg 04/27/21 02:46 74-97-504/26/21 16:347.3 2.1 1
Bromodichloromethane ND ug/kg 04/27/21 02:46 75-27-404/26/21 16:347.3 2.8 1
Bromoform ND ug/kg 04/27/21 02:46 75-25-204/26/21 16:347.3 2.6 1
Bromomethane ND ug/kg 04/27/21 02:46 74-83-904/26/21 16:3414.5 11.5 1
2-Butanone (MEK)ND ug/kg 04/27/21 02:46 78-93-304/26/21 16:3414534.9 1
n-Butylbenzene ND ug/kg 04/27/21 02:46 104-51-804/26/21 16:347.3 3.4 1
sec-Butylbenzene ND ug/kg 04/27/21 02:46 135-98-804/26/21 16:347.3 3.2 1
tert-Butylbenzene ND ug/kg 04/27/21 02:46 98-06-604/26/21 16:347.3 2.6 1
Carbon tetrachloride ND ug/kg 04/27/21 02:46 56-23-504/26/21 16:347.3 2.7 1
Chlorobenzene ND ug/kg 04/27/21 02:46 108-90-704/26/21 16:347.3 1.4 1
Chloroethane ND ug/kg 04/27/21 02:46 75-00-304/26/21 16:3414.5 5.6 1
Chloroform ND ug/kg 04/27/21 02:46 67-66-304/26/21 16:347.3 4.4 1
Chloromethane ND ug/kg 04/27/21 02:46 74-87-304/26/21 16:3414.5 6.1 1
2-Chlorotoluene ND ug/kg 04/27/21 02:46 95-49-804/26/21 16:347.3 2.6 1
4-Chlorotoluene ND ug/kg 04/27/21 02:46 106-43-404/26/21 16:347.3 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/27/21 02:46 96-12-804/26/21 16:347.3 2.8 1
Dibromochloromethane ND ug/kg 04/27/21 02:46 124-48-104/26/21 16:347.3 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 04/27/21 02:46 106-93-404/26/21 16:347.3 3.2 1
Dibromomethane ND ug/kg 04/27/21 02:46 74-95-304/26/21 16:347.3 1.6 1
1,2-Dichlorobenzene ND ug/kg 04/27/21 02:46 95-50-104/26/21 16:347.3 2.6 1
1,3-Dichlorobenzene ND ug/kg 04/27/21 02:46 541-73-104/26/21 16:347.3 2.3 1
1,4-Dichlorobenzene ND ug/kg 04/27/21 02:46 106-46-704/26/21 16:347.3 1.9 1
Dichlorodifluoromethane ND ug/kg 04/27/21 02:46 75-71-804/26/21 16:3414.5 3.2 1
1,1-Dichloroethane ND ug/kg 04/27/21 02:46 75-34-304/26/21 16:347.3 3.0 1
1,2-Dichloroethane ND ug/kg 04/27/21 02:46 107-06-204/26/21 16:347.3 4.8 1
1,1-Dichloroethene ND ug/kg 04/27/21 02:46 75-35-404/26/21 16:347.3 3.0 1
cis-1,2-Dichloroethene ND ug/kg 04/27/21 02:46 156-59-204/26/21 16:347.3 2.5 1
trans-1,2-Dichloroethene ND ug/kg 04/27/21 02:46 156-60-504/26/21 16:347.3 2.5 1
1,2-Dichloropropane ND ug/kg 04/27/21 02:46 78-87-504/26/21 16:347.3 2.2 1
1,3-Dichloropropane ND ug/kg 04/27/21 02:46 142-28-904/26/21 16:347.3 2.3 1
2,2-Dichloropropane ND ug/kg 04/27/21 02:46 594-20-704/26/21 16:347.3 2.4 1
1,1-Dichloropropene ND ug/kg 04/27/21 02:46 563-58-604/26/21 16:347.3 3.5 1
cis-1,3-Dichloropropene ND ug/kg 04/27/21 02:46 10061-01-504/26/21 16:347.3 2.0 1
trans-1,3-Dichloropropene ND ug/kg 04/27/21 02:46 10061-02-604/26/21 16:347.3 2.5 1
Diisopropyl ether ND ug/kg 04/27/21 02:46 108-20-304/26/21 16:347.3 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-4 (0-2)Lab ID:92534944004 Collected:04/22/21 15:30 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 04/27/21 02:46 100-41-404/26/21 16:347.3 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/21 02:46 87-68-304/26/21 16:3414.5 11.9 1
2-Hexanone ND ug/kg 04/27/21 02:46 591-78-604/26/21 16:3472.6 7.0 1
Isopropylbenzene (Cumene)ND ug/kg 04/27/21 02:46 98-82-804/26/21 16:347.3 2.5 1
p-Isopropyltoluene ND ug/kg 04/27/21 02:46 99-87-604/26/21 16:347.3 3.6 1
Methylene Chloride ND ug/kg 04/27/21 02:46 75-09-204/26/21 16:3429.1 19.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/27/21 02:46 108-10-104/26/21 16:3472.6 7.0 1
Methyl-tert-butyl ether ND ug/kg 04/27/21 02:46 1634-04-404/26/21 16:347.3 2.7 1
Naphthalene ND ug/kg 04/27/21 02:46 91-20-304/26/21 16:347.3 3.8 1
n-Propylbenzene ND ug/kg 04/27/21 02:46 103-65-104/26/21 16:347.3 2.6 1
Styrene ND ug/kg 04/27/21 02:46 100-42-504/26/21 16:347.3 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/27/21 02:46 630-20-604/26/21 16:347.3 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/27/21 02:46 79-34-504/26/21 16:347.3 1.9 1
Tetrachloroethene ND ug/kg 04/27/21 02:46 127-18-404/26/21 16:347.3 2.3 1
Toluene ND ug/kg 04/27/21 02:46 108-88-304/26/21 16:347.3 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 04/27/21 02:46 87-61-604/26/21 16:347.3 5.9 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/21 02:46 120-82-104/26/21 16:347.3 6.1 1
1,1,1-Trichloroethane ND ug/kg 04/27/21 02:46 71-55-604/26/21 16:347.3 3.8 1
1,1,2-Trichloroethane ND ug/kg 04/27/21 02:46 79-00-504/26/21 16:347.3 2.4 1
Trichloroethene ND ug/kg 04/27/21 02:46 79-01-604/26/21 16:347.3 1.9 1
Trichlorofluoromethane ND ug/kg 04/27/21 02:46 75-69-404/26/21 16:347.3 4.0 1
1,2,3-Trichloropropane ND ug/kg 04/27/21 02:46 96-18-404/26/21 16:347.3 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 04/27/21 02:46 95-63-604/26/21 16:347.3 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/27/21 02:46 108-67-804/26/21 16:347.3 2.4 1
Vinyl acetate ND ug/kg 04/27/21 02:46 108-05-404/26/21 16:3472.6 5.3 1
Vinyl chloride ND ug/kg 04/27/21 02:46 75-01-404/26/21 16:3414.5 3.7 1
Xylene (Total)ND ug/kg 04/27/21 02:46 1330-20-704/26/21 16:3414.5 4.1 1
m&p-Xylene ND ug/kg 04/27/21 02:46 179601-23-104/26/21 16:3414.5 5.0 1
o-Xylene ND ug/kg 04/27/21 02:46 95-47-604/26/21 16:347.3 3.2 1
Surrogates
Toluene-d8 (S)99 %04/27/21 02:46 2037-26-504/26/21 16:3470-130 1
4-Bromofluorobenzene (S)103 %04/27/21 02:46 460-00-404/26/21 16:3469-134 1
1,2-Dichloroethane-d4 (S)104 %04/27/21 02:46 17060-07-004/26/21 16:3470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.9 %04/23/21 17:27 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 77.2 %04/28/21 17:0104/28/21 16:531
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-4 (0-2)Lab ID:92534944004 Collected:04/22/21 15:30 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 04/29/21 15:33 18540-29-904/27/21 17:381.30 0.330 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-DUP Lab ID:92534944005 Collected:04/22/21 00:00 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 1.97 mg/kg 04/25/21 21:33 7440-38-204/25/21 12:411.28 0.128 5
Barium 144 mg/kg 04/25/21 21:33 7440-39-304/25/21 12:413.21 0.195 5
Cadmium 0.143J mg/kg 04/25/21 21:33 7440-43-9 J04/25/21 12:411.28 0.110 5
Chromium 60.0 mg/kg 04/25/21 21:33 7440-47-304/25/21 12:416.42 0.380 5
Lead 11.6 mg/kg 04/25/21 21:33 7439-92-104/25/21 12:412.57 0.127 5
Selenium 1.17J mg/kg 04/25/21 21:33 7782-49-2 J04/25/21 12:413.21 0.231 5
Silver ND mg/kg 04/25/21 21:33 7440-22-404/25/21 12:410.642 0.111 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0238J mg/kg 04/27/21 09:51 7439-97-6 J04/26/21 10:360.0513 0.0231 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/21 13:29 83-32-904/27/21 09:234261501
Acenaphthylene ND ug/kg 04/27/21 13:29 208-96-804/27/21 09:234261501
Aniline ND ug/kg 04/27/21 13:29 62-53-304/27/21 09:234261671
Anthracene ND ug/kg 04/27/21 13:29 120-12-704/27/21 09:234261401
Benzo(a)anthracene ND ug/kg 04/27/21 13:29 56-55-304/27/21 09:234261421
Benzo(a)pyrene ND ug/kg 04/27/21 13:29 50-32-804/27/21 09:234261471
Benzo(b)fluoranthene ND ug/kg 04/27/21 13:29 205-99-204/27/21 09:234261421
Benzo(g,h,i)perylene ND ug/kg 04/27/21 13:29 191-24-204/27/21 09:234261651
Benzo(k)fluoranthene ND ug/kg 04/27/21 13:29 207-08-904/27/21 09:234261501
Benzoic Acid ND ug/kg 04/27/21 13:29 65-85-004/27/21 09:2321309161
Benzyl alcohol ND ug/kg 04/27/21 13:29 100-51-604/27/21 09:238533231
4-Bromophenylphenyl ether ND ug/kg 04/27/21 13:29 101-55-304/27/21 09:234261641
Butylbenzylphthalate ND ug/kg 04/27/21 13:29 85-68-704/27/21 09:234261801
4-Chloro-3-methylphenol ND ug/kg 04/27/21 13:29 59-50-704/27/21 09:238533001
4-Chloroaniline ND ug/kg 04/27/21 13:29 106-47-804/27/21 09:238533351
bis(2-Chloroethoxy)methane ND ug/kg 04/27/21 13:29 111-91-104/27/21 09:234261771
bis(2-Chloroethyl) ether ND ug/kg 04/27/21 13:29 111-44-404/27/21 09:234261601
2-Chloronaphthalene ND ug/kg 04/27/21 13:29 91-58-704/27/21 09:234261691
2-Chlorophenol ND ug/kg 04/27/21 13:29 95-57-804/27/21 09:234261601
4-Chlorophenylphenyl ether ND ug/kg 04/27/21 13:29 7005-72-304/27/21 09:234261591
Chrysene ND ug/kg 04/27/21 13:29 218-01-904/27/21 09:234261551
Dibenz(a,h)anthracene ND ug/kg 04/27/21 13:29 53-70-304/27/21 09:234261641
Dibenzofuran ND ug/kg 04/27/21 13:29 132-64-904/27/21 09:234261541
1,2-Dichlorobenzene ND ug/kg 04/27/21 13:29 95-50-104/27/21 09:234261541
1,3-Dichlorobenzene ND ug/kg 04/27/21 13:29 541-73-104/27/21 09:234261511
1,4-Dichlorobenzene ND ug/kg 04/27/21 13:29 106-46-704/27/21 09:234261631
3,3'-Dichlorobenzidine ND ug/kg 04/27/21 13:29 91-94-1 IL04/27/21 09:238532881
2,4-Dichlorophenol ND ug/kg 04/27/21 13:29 120-83-204/27/21 09:234261671
Diethylphthalate ND ug/kg 04/27/21 13:29 84-66-204/27/21 09:234261561
2,4-Dimethylphenol ND ug/kg 04/27/21 13:29 105-67-904/27/21 09:234261771
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-DUP Lab ID:92534944005 Collected:04/22/21 00:00 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 04/27/21 13:29 131-11-304/27/21 09:234261551
Di-n-butylphthalate ND ug/kg 04/27/21 13:29 84-74-204/27/21 09:234261431
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/21 13:29 534-52-104/27/21 09:238533981
2,4-Dinitrophenol ND ug/kg 04/27/21 13:29 51-28-5 v104/27/21 09:23213013201
2,4-Dinitrotoluene ND ug/kg 04/27/21 13:29 121-14-204/27/21 09:234261641
2,6-Dinitrotoluene ND ug/kg 04/27/21 13:29 606-20-204/27/21 09:234261561
Di-n-octylphthalate ND ug/kg 04/27/21 13:29 117-84-004/27/21 09:234261681
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/21 13:29 117-81-704/27/21 09:234261651
Fluoranthene ND ug/kg 04/27/21 13:29 206-44-004/27/21 09:234261461
Fluorene ND ug/kg 04/27/21 13:29 86-73-704/27/21 09:234261501
Hexachloro-1,3-butadiene ND ug/kg 04/27/21 13:29 87-68-304/27/21 09:234261851
Hexachlorobenzene ND ug/kg 04/27/21 13:29 118-74-104/27/21 09:234261671
Hexachlorocyclopentadiene ND ug/kg 04/27/21 13:29 77-47-404/27/21 09:234262441
Hexachloroethane ND ug/kg 04/27/21 13:29 67-72-104/27/21 09:234261631
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/21 13:29 193-39-504/27/21 09:234261681
Isophorone ND ug/kg 04/27/21 13:29 78-59-104/27/21 09:234261901
1-Methylnaphthalene ND ug/kg 04/27/21 13:29 90-12-004/27/21 09:234261501
2-Methylnaphthalene ND ug/kg 04/27/21 13:29 91-57-604/27/21 09:234261711
2-Methylphenol(o-Cresol)ND ug/kg 04/27/21 13:29 95-48-704/27/21 09:234261741
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/21 13:29 15831-10-404/27/21 09:234261721
Naphthalene ND ug/kg 04/27/21 13:29 91-20-304/27/21 09:234261451
2-Nitroaniline ND ug/kg 04/27/21 13:29 88-74-404/27/21 09:2321303491
3-Nitroaniline ND ug/kg 04/27/21 13:29 99-09-204/27/21 09:2321303351
4-Nitroaniline ND ug/kg 04/27/21 13:29 100-01-604/27/21 09:238533241
Nitrobenzene ND ug/kg 04/27/21 13:29 98-95-304/27/21 09:234261981
2-Nitrophenol ND ug/kg 04/27/21 13:29 88-75-504/27/21 09:234261851
4-Nitrophenol ND ug/kg 04/27/21 13:29 100-02-704/27/21 09:2321308241
N-Nitrosodimethylamine ND ug/kg 04/27/21 13:29 62-75-904/27/21 09:234261431
N-Nitroso-di-n-propylamine ND ug/kg 04/27/21 13:29 621-64-704/27/21 09:234261601
N-Nitrosodiphenylamine ND ug/kg 04/27/21 13:29 86-30-604/27/21 09:234261511
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/21 13:29 108-60-104/27/21 09:234262031
Pentachlorophenol ND ug/kg 04/27/21 13:29 87-86-504/27/21 09:238534171
Phenanthrene ND ug/kg 04/27/21 13:29 85-01-804/27/21 09:234261401
Phenol ND ug/kg 04/27/21 13:29 108-95-204/27/21 09:234261901
Pyrene ND ug/kg 04/27/21 13:29 129-00-004/27/21 09:234261731
Pyridine ND ug/kg 04/27/21 13:29 110-86-104/27/21 09:234261341
1,2,4-Trichlorobenzene ND ug/kg 04/27/21 13:29 120-82-104/27/21 09:234261681
2,4,5-Trichlorophenol ND ug/kg 04/27/21 13:29 95-95-404/27/21 09:234261951
2,4,6-Trichlorophenol ND ug/kg 04/27/21 13:29 88-06-204/27/21 09:234261761
Surrogates
Nitrobenzene-d5 (S)48 %04/27/21 13:29 4165-60-004/27/21 09:2321-130 1
2-Fluorobiphenyl (S)28 %04/27/21 13:29 321-60-804/27/21 09:2319-130 1
Terphenyl-d14 (S)34 %04/27/21 13:29 1718-51-004/27/21 09:2315-130 1
Phenol-d6 (S)59 %04/27/21 13:29 13127-88-304/27/21 09:2318-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-DUP Lab ID:92534944005 Collected:04/22/21 00:00 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)55 %04/27/21 13:29 367-12-404/27/21 09:2318-130 1
2,4,6-Tribromophenol (S)59 %04/27/21 13:29 118-79-604/27/21 09:2318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 62.1J ug/kg 04/27/21 03:04 67-64-104/26/21 16:3416653.3 1
Benzene 8.3J ug/kg 04/27/21 03:04 71-43-204/26/21 16:348.3 3.3 1
Bromobenzene ND ug/kg 04/27/21 03:04 108-86-104/26/21 16:348.3 2.7 1
Bromochloromethane ND ug/kg 04/27/21 03:04 74-97-504/26/21 16:348.3 2.5 1
Bromodichloromethane ND ug/kg 04/27/21 03:04 75-27-404/26/21 16:348.3 3.2 1
Bromoform ND ug/kg 04/27/21 03:04 75-25-204/26/21 16:348.3 2.9 1
Bromomethane ND ug/kg 04/27/21 03:04 74-83-904/26/21 16:3416.6 13.1 1
2-Butanone (MEK)ND ug/kg 04/27/21 03:04 78-93-304/26/21 16:3416639.9 1
n-Butylbenzene ND ug/kg 04/27/21 03:04 104-51-804/26/21 16:348.3 3.9 1
sec-Butylbenzene ND ug/kg 04/27/21 03:04 135-98-804/26/21 16:348.3 3.7 1
tert-Butylbenzene ND ug/kg 04/27/21 03:04 98-06-604/26/21 16:348.3 3.0 1
Carbon tetrachloride ND ug/kg 04/27/21 03:04 56-23-504/26/21 16:348.3 3.1 1
Chlorobenzene ND ug/kg 04/27/21 03:04 108-90-704/26/21 16:348.3 1.6 1
Chloroethane ND ug/kg 04/27/21 03:04 75-00-304/26/21 16:3416.6 6.4 1
Chloroform ND ug/kg 04/27/21 03:04 67-66-304/26/21 16:348.3 5.1 1
Chloromethane ND ug/kg 04/27/21 03:04 74-87-304/26/21 16:3416.6 7.0 1
2-Chlorotoluene ND ug/kg 04/27/21 03:04 95-49-804/26/21 16:348.3 2.9 1
4-Chlorotoluene ND ug/kg 04/27/21 03:04 106-43-404/26/21 16:348.3 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/27/21 03:04 96-12-804/26/21 16:348.3 3.2 1
Dibromochloromethane ND ug/kg 04/27/21 03:04 124-48-104/26/21 16:348.3 4.7 1
1,2-Dibromoethane (EDB)ND ug/kg 04/27/21 03:04 106-93-404/26/21 16:348.3 3.7 1
Dibromomethane ND ug/kg 04/27/21 03:04 74-95-304/26/21 16:348.3 1.8 1
1,2-Dichlorobenzene ND ug/kg 04/27/21 03:04 95-50-104/26/21 16:348.3 3.0 1
1,3-Dichlorobenzene ND ug/kg 04/27/21 03:04 541-73-104/26/21 16:348.3 2.6 1
1,4-Dichlorobenzene ND ug/kg 04/27/21 03:04 106-46-704/26/21 16:348.3 2.2 1
Dichlorodifluoromethane ND ug/kg 04/27/21 03:04 75-71-804/26/21 16:3416.6 3.6 1
1,1-Dichloroethane ND ug/kg 04/27/21 03:04 75-34-304/26/21 16:348.3 3.4 1
1,2-Dichloroethane ND ug/kg 04/27/21 03:04 107-06-204/26/21 16:348.3 5.5 1
1,1-Dichloroethene ND ug/kg 04/27/21 03:04 75-35-404/26/21 16:348.3 3.4 1
cis-1,2-Dichloroethene ND ug/kg 04/27/21 03:04 156-59-204/26/21 16:348.3 2.8 1
trans-1,2-Dichloroethene ND ug/kg 04/27/21 03:04 156-60-504/26/21 16:348.3 2.9 1
1,2-Dichloropropane ND ug/kg 04/27/21 03:04 78-87-504/26/21 16:348.3 2.5 1
1,3-Dichloropropane ND ug/kg 04/27/21 03:04 142-28-904/26/21 16:348.3 2.6 1
2,2-Dichloropropane ND ug/kg 04/27/21 03:04 594-20-704/26/21 16:348.3 2.7 1
1,1-Dichloropropene ND ug/kg 04/27/21 03:04 563-58-604/26/21 16:348.3 4.0 1
cis-1,3-Dichloropropene ND ug/kg 04/27/21 03:04 10061-01-504/26/21 16:348.3 2.3 1
trans-1,3-Dichloropropene ND ug/kg 04/27/21 03:04 10061-02-604/26/21 16:348.3 2.9 1
Diisopropyl ether ND ug/kg 04/27/21 03:04 108-20-304/26/21 16:348.3 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-DUP Lab ID:92534944005 Collected:04/22/21 00:00 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene 5.3J ug/kg 04/27/21 03:04 100-41-404/26/21 16:348.3 3.9 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/21 03:04 87-68-304/26/21 16:3416.6 13.6 1
2-Hexanone ND ug/kg 04/27/21 03:04 591-78-604/26/21 16:3483.1 8.0 1
Isopropylbenzene (Cumene)ND ug/kg 04/27/21 03:04 98-82-804/26/21 16:348.3 2.8 1
p-Isopropyltoluene ND ug/kg 04/27/21 03:04 99-87-604/26/21 16:348.3 4.1 1
Methylene Chloride ND ug/kg 04/27/21 03:04 75-09-204/26/21 16:3433.2 22.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/27/21 03:04 108-10-104/26/21 16:3483.1 8.0 1
Methyl-tert-butyl ether ND ug/kg 04/27/21 03:04 1634-04-404/26/21 16:348.3 3.1 1
Naphthalene 14.0 ug/kg 04/27/21 03:04 91-20-304/26/21 16:348.3 4.4 1
n-Propylbenzene ND ug/kg 04/27/21 03:04 103-65-104/26/21 16:348.3 3.0 1
Styrene ND ug/kg 04/27/21 03:04 100-42-504/26/21 16:348.3 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/27/21 03:04 630-20-604/26/21 16:348.3 3.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/27/21 03:04 79-34-504/26/21 16:348.3 2.2 1
Tetrachloroethene ND ug/kg 04/27/21 03:04 127-18-404/26/21 16:348.3 2.6 1
Toluene 15.6 ug/kg 04/27/21 03:04 108-88-304/26/21 16:348.3 2.4 1
1,2,3-Trichlorobenzene ND ug/kg 04/27/21 03:04 87-61-604/26/21 16:348.3 6.7 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/21 03:04 120-82-104/26/21 16:348.3 7.0 1
1,1,1-Trichloroethane ND ug/kg 04/27/21 03:04 71-55-604/26/21 16:348.3 4.3 1
1,1,2-Trichloroethane ND ug/kg 04/27/21 03:04 79-00-504/26/21 16:348.3 2.8 1
Trichloroethene 1330 ug/kg 04/27/21 03:04 79-01-604/26/21 16:348.3 2.1 1
Trichlorofluoromethane ND ug/kg 04/27/21 03:04 75-69-404/26/21 16:348.3 4.6 1
1,2,3-Trichloropropane ND ug/kg 04/27/21 03:04 96-18-404/26/21 16:348.3 4.2 1
1,2,4-Trimethylbenzene 4.3J ug/kg 04/27/21 03:04 95-63-604/26/21 16:348.3 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 04/27/21 03:04 108-67-804/26/21 16:348.3 2.8 1
Vinyl acetate ND ug/kg 04/27/21 03:04 108-05-404/26/21 16:3483.1 6.0 1
Vinyl chloride ND ug/kg 04/27/21 03:04 75-01-404/26/21 16:3416.6 4.2 1
Xylene (Total)33.4 ug/kg 04/27/21 03:04 1330-20-704/26/21 16:3416.6 4.7 1
m&p-Xylene 23.0 ug/kg 04/27/21 03:04 179601-23-104/26/21 16:3416.6 5.7 1
o-Xylene 10.5 ug/kg 04/27/21 03:04 95-47-604/26/21 16:348.3 3.7 1
Surrogates
Toluene-d8 (S)99 %04/27/21 03:04 2037-26-504/26/21 16:3470-130 1
4-Bromofluorobenzene (S)106 %04/27/21 03:04 460-00-404/26/21 16:3469-134 1
1,2-Dichloroethane-d4 (S)107 %04/27/21 03:04 17060-07-004/26/21 16:3470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.6 %04/23/21 17:27 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 77.9 %04/28/21 17:0104/28/21 16:531
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92534944
WPP-005
Sample:FG-DUP Lab ID:92534944005 Collected:04/22/21 00:00 Received:04/23/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 04/29/21 15:38 18540-29-904/27/21 17:381.28 0.327 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1658291
3050B
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92534944001, 92534944002, 92534944003, 92534944004, 92534944005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3646316-1
Associated Lab Samples:92534944001, 92534944002, 92534944003, 92534944004, 92534944005
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 1.00 04/25/21 21:470.100
Barium mg/kg ND 2.50 04/25/21 21:470.152
Cadmium mg/kg ND 1.00 04/25/21 21:470.0855
Chromium mg/kg ND 5.00 04/25/21 21:470.297
Lead mg/kg ND 2.00 04/25/21 21:470.0990
Selenium mg/kg ND 2.50 04/25/21 21:470.180
Silver mg/kg ND 0.500 04/25/21 21:470.0865
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3646316-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 94.4100 94.4 80.0-120
Barium mg/kg 99.2100 99.2 80.0-120
Cadmium mg/kg 96.0100 96.0 80.0-120
Chromium mg/kg 94.7100 94.7 80.0-120
Lead mg/kg 96.4100 96.4 80.0-120
Selenium mg/kg 98.9100 98.9 80.0-120
Silver mg/kg 19.820.0 99.1 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3646316-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1343116-01
R3646316-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 121 85.2 75.0-12585.7 0.588 201217.69 111 112
Barium mg/kg ML12141.9 75.0-12548.8 2.88 20121237287296
Cadmium mg/kg 121 93.2 75.0-12594.3 1.23 201210.218 113 115
Chromium mg/kg 121 85.5 75.0-12585.2 0.230 2012121.7 125 125
Lead mg/kg 121 103 75.0-12589.1 12.3 2012116.6 141 125
Selenium mg/kg 121 95.1 75.0-12598.1 3.03 201211.33 117 120
Silver mg/kg 24.3 95.4 75.0-12598.2 2.94 2024.3ND 23.1 23.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1658868
7471A
EPA 7471B
Mercury 7471B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92534944004, 92534944005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3647039-1
Associated Lab Samples:92534944004, 92534944005
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0400 04/27/21 08:490.0180
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3647039-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.5030.500 101 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3647039-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1343475-06
R3647039-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.500 102 75.0-12596.1 5.53 200.5000.0306 0.540 0.511
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1658884
7471A
EPA 7471B
Mercury 7471B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92534944001, 92534944002, 92534944003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3647195-1
Associated Lab Samples:92534944001, 92534944002, 92534944003
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0400 04/27/21 12:560.0180
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3647195-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.5150.500 103 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3647195-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1343455-05
R3647195-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.500 92.0 75.0-12596.6 4.64 200.5000.0203 0.480 0.503
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
616268
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92534944001, 92534944002, 92534944003, 92534944004, 92534944005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3243348
Associated Lab Samples:92534944001, 92534944002, 92534944003, 92534944004, 92534944005
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/27/21 01:341.9
1,1,1-Trichloroethane ug/kg ND 5.0 04/27/21 01:342.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/27/21 01:341.3
1,1,2-Trichloroethane ug/kg ND 5.0 04/27/21 01:341.7
1,1-Dichloroethane ug/kg ND 5.0 04/27/21 01:342.1
1,1-Dichloroethene ug/kg ND 5.0 04/27/21 01:342.1
1,1-Dichloropropene ug/kg ND 5.0 04/27/21 01:342.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 04/27/21 01:344.0
1,2,3-Trichloropropane ug/kg ND 5.0 04/27/21 01:342.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 04/27/21 01:344.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 04/27/21 01:341.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/27/21 01:341.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/27/21 01:342.2
1,2-Dichlorobenzene ug/kg ND 5.0 04/27/21 01:341.8
1,2-Dichloroethane ug/kg ND 5.0 04/27/21 01:343.3
1,2-Dichloropropane ug/kg ND 5.0 04/27/21 01:341.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 04/27/21 01:341.7
1,3-Dichlorobenzene ug/kg ND 5.0 04/27/21 01:341.6
1,3-Dichloropropane ug/kg ND 5.0 04/27/21 01:341.6
1,4-Dichlorobenzene ug/kg ND 5.0 04/27/21 01:341.3
2,2-Dichloropropane ug/kg ND 5.0 04/27/21 01:341.6
2-Butanone (MEK)ug/kg ND 100 04/27/21 01:3424.0
2-Chlorotoluene ug/kg ND 5.0 04/27/21 01:341.8
2-Hexanone ug/kg ND 50.0 04/27/21 01:344.8
4-Chlorotoluene ug/kg ND 5.0 04/27/21 01:340.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/27/21 01:344.8
Acetone ug/kg ND 100 04/27/21 01:3432.1
Benzene ug/kg ND 5.0 04/27/21 01:342.0
Bromobenzene ug/kg ND 5.0 04/27/21 01:341.6
Bromochloromethane ug/kg ND 5.0 04/27/21 01:341.5
Bromodichloromethane ug/kg ND 5.0 04/27/21 01:341.9
Bromoform ug/kg ND 5.0 04/27/21 01:341.8
Bromomethane ug/kg ND 10.0 04/27/21 01:347.9
Carbon tetrachloride ug/kg ND 5.0 04/27/21 01:341.9
Chlorobenzene ug/kg ND 5.0 04/27/21 01:340.96
Chloroethane ug/kg ND 10.0 04/27/21 01:343.9
Chloroform ug/kg ND 5.0 04/27/21 01:343.0
Chloromethane ug/kg ND 10.0 04/27/21 01:344.2
cis-1,2-Dichloroethene ug/kg ND 5.0 04/27/21 01:341.7
cis-1,3-Dichloropropene ug/kg ND 5.0 04/27/21 01:341.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3243348
Associated Lab Samples:92534944001, 92534944002, 92534944003, 92534944004, 92534944005
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 04/27/21 01:342.8
Dibromomethane ug/kg ND 5.0 04/27/21 01:341.1
Dichlorodifluoromethane ug/kg ND 10.0 04/27/21 01:342.2
Diisopropyl ether ug/kg ND 5.0 04/27/21 01:341.4
Ethylbenzene ug/kg ND 5.0 04/27/21 01:342.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 04/27/21 01:348.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 04/27/21 01:341.7
m&p-Xylene ug/kg ND 10.0 04/27/21 01:343.4
Methyl-tert-butyl ether ug/kg ND 5.0 04/27/21 01:341.9
Methylene Chloride ug/kg ND 20.0 04/27/21 01:3413.7
n-Butylbenzene ug/kg ND 5.0 04/27/21 01:342.4
n-Propylbenzene ug/kg ND 5.0 04/27/21 01:341.8
Naphthalene ug/kg ND 5.0 04/27/21 01:342.6
o-Xylene ug/kg ND 5.0 04/27/21 01:342.2
p-Isopropyltoluene ug/kg ND 5.0 04/27/21 01:342.5
sec-Butylbenzene ug/kg ND 5.0 04/27/21 01:342.2
Styrene ug/kg ND 5.0 04/27/21 01:341.3
tert-Butylbenzene ug/kg ND 5.0 04/27/21 01:341.8
Tetrachloroethene ug/kg ND 5.0 04/27/21 01:341.6
Toluene ug/kg ND 5.0 04/27/21 01:341.4
trans-1,2-Dichloroethene ug/kg ND 5.0 04/27/21 01:341.8
trans-1,3-Dichloropropene ug/kg ND 5.0 04/27/21 01:341.7
Trichloroethene ug/kg ND 5.0 04/27/21 01:341.3
Trichlorofluoromethane ug/kg ND 5.0 04/27/21 01:342.8
Vinyl acetate ug/kg ND 50.0 04/27/21 01:343.6
Vinyl chloride ug/kg ND 10.0 04/27/21 01:342.5
Xylene (Total)ug/kg ND 10.0 04/27/21 01:342.8
1,2-Dichloroethane-d4 (S)%107 70-130 04/27/21 01:34
4-Bromofluorobenzene (S)%104 69-134 04/27/21 01:34
Toluene-d8 (S)%98 70-130 04/27/21 01:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3243349LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11701250 94 70-130
1,1,1-Trichloroethane ug/kg 11201250 89 70-130
1,1,2,2-Tetrachloroethane ug/kg 11401250 91 70-130
1,1,2-Trichloroethane ug/kg 11501250 92 70-130
1,1-Dichloroethane ug/kg 11301250 91 70-130
1,1-Dichloroethene ug/kg 11801250 94 70-130
1,1-Dichloropropene ug/kg 11001250 88 70-130
1,2,3-Trichlorobenzene ug/kg 11001250 88 65-130
1,2,3-Trichloropropane ug/kg 11601250 93 70-130
1,2,4-Trichlorobenzene ug/kg 10701250 86 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3243349LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 11301250 90 70-130
1,2-Dibromo-3-chloropropane ug/kg 11401250 91 70-130
1,2-Dibromoethane (EDB)ug/kg 12101250 97 70-130
1,2-Dichlorobenzene ug/kg 11201250 90 70-130
1,2-Dichloroethane ug/kg 11601250 93 63-130
1,2-Dichloropropane ug/kg 11601250 92 70-130
1,3,5-Trimethylbenzene ug/kg 11301250 91 70-130
1,3-Dichlorobenzene ug/kg 11001250 88 70-130
1,3-Dichloropropane ug/kg 12301250 98 70-130
1,4-Dichlorobenzene ug/kg 10901250 87 70-130
2,2-Dichloropropane ug/kg 10401250 83 66-130
2-Butanone (MEK)ug/kg 23602500 94 70-130
2-Chlorotoluene ug/kg 11601250 93 70-130
2-Hexanone ug/kg 25002500 100 70-130
4-Chlorotoluene ug/kg 11301250 90 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 23902500 95 70-130
Acetone ug/kg 24802500 99 69-130
Benzene ug/kg 11601250 93 70-130
Bromobenzene ug/kg 11401250 91 70-130
Bromochloromethane ug/kg 11701250 94 70-130
Bromodichloromethane ug/kg 10701250 86 69-130
Bromoform ug/kg 11901250 95 70-130
Bromomethane ug/kg 10301250 83 52-130
Carbon tetrachloride ug/kg 11301250 90 70-130
Chlorobenzene ug/kg 11301250 90 70-130
Chloroethane ug/kg 10501250 84 65-130
Chloroform ug/kg 10401250 83 70-130
Chloromethane ug/kg 10601250 85 55-130
cis-1,2-Dichloroethene ug/kg 11401250 91 70-130
cis-1,3-Dichloropropene ug/kg 11801250 94 70-130
Dibromochloromethane ug/kg 12401250 99 70-130
Dibromomethane ug/kg 11801250 94 70-130
Dichlorodifluoromethane ug/kg 12201250 98 45-156
Diisopropyl ether ug/kg 10801250 87 70-130
Ethylbenzene ug/kg 10601250 85 70-130
Hexachloro-1,3-butadiene ug/kg 10701250 86 66-130
Isopropylbenzene (Cumene)ug/kg 11001250 88 70-130
m&p-Xylene ug/kg 22702500 91 70-130
Methyl-tert-butyl ether ug/kg 11201250 89 70-130
Methylene Chloride ug/kg 11901250 96 65-130
n-Butylbenzene ug/kg 10701250 86 67-130
n-Propylbenzene ug/kg 10801250 86 70-130
Naphthalene ug/kg 11401250 91 70-130
o-Xylene ug/kg 11301250 90 70-130
p-Isopropyltoluene ug/kg 11201250 90 67-130
sec-Butylbenzene ug/kg 10901250 87 69-130
Styrene ug/kg 11801250 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3243349LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 10901250 88 67-130
Tetrachloroethene ug/kg 11201250 90 70-130
Toluene ug/kg 11301250 90 70-130
trans-1,2-Dichloroethene ug/kg 11401250 91 70-130
trans-1,3-Dichloropropene ug/kg 11601250 93 68-130
Trichloroethene ug/kg 11101250 88 70-130
Trichlorofluoromethane ug/kg 10501250 84 70-130
Vinyl acetate ug/kg 26102500 105 70-130
Vinyl chloride ug/kg 10401250 83 61-130
Xylene (Total)ug/kg 34003750 91 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%103 69-134
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3243351MATRIX SPIKE SAMPLE:
MSSpike
Result
92534944002
1,1,1,2-Tetrachloroethane ug/kg 833856 97 70-131ND
1,1,1-Trichloroethane ug/kg 771856 90 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 781856 91 66-130ND
1,1,2-Trichloroethane ug/kg 813856 95 66-133ND
1,1-Dichloroethane ug/kg 752856 88 65-130ND
1,1-Dichloroethene ug/kg 744856 87 10-158ND
1,1-Dichloropropene ug/kg 713856 83 68-133ND
1,2,3-Trichlorobenzene ug/kg 762856 89 27-138ND
1,2,3-Trichloropropane ug/kg 758856 89 67-130ND
1,2,4-Trichlorobenzene ug/kg 694856 81 51-134ND
1,2,4-Trimethylbenzene ug/kg 742856 87 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 681856 79 32-130ND
1,2-Dibromoethane (EDB)ug/kg 837856 98 70-130ND
1,2-Dichlorobenzene ug/kg 756856 88 69-130ND
1,2-Dichloroethane ug/kg 817856 95 59-130ND
1,2-Dichloropropane ug/kg 834856 97 70-130ND
1,3,5-Trimethylbenzene ug/kg 745856 87 65-137ND
1,3-Dichlorobenzene ug/kg 707856 83 70-130ND
1,3-Dichloropropane ug/kg 865856 101 70-130ND
1,4-Dichlorobenzene ug/kg 714856 83 68-130ND
2,2-Dichloropropane ug/kg 614856 72 32-130ND
2-Butanone (MEK)ug/kg 14801720 86 10-136ND
2-Chlorotoluene ug/kg 769856 90 69-141ND
2-Hexanone ug/kg 15101720 88 10-144ND
4-Chlorotoluene ug/kg 739856 86 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 15101720 88 25-143ND
Acetone ug/kg 14001720 73 10-130147J
Benzene ug/kg 831856 97 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3243351MATRIX SPIKE SAMPLE:
MSSpike
Result
92534944002
Bromobenzene ug/kg 788856 92 70-130ND
Bromochloromethane ug/kg 744856 87 69-134ND
Bromodichloromethane ug/kg 737856 86 64-130ND
Bromoform ug/kg 778856 91 62-130ND
Bromomethane ug/kg 567856 66 20-176ND
Carbon tetrachloride ug/kg 757856 88 65-140ND
Chlorobenzene ug/kg 775856 91 70-130ND
Chloroethane ug/kg 351856 41 10-130ND
Chloroform ug/kg 704856 82 63-130ND
Chloromethane ug/kg 842856 98 58-130ND
cis-1,2-Dichloroethene ug/kg 755856 88 66-130ND
cis-1,3-Dichloropropene ug/kg 775856 91 67-130ND
Dibromochloromethane ug/kg 846856 99 67-130ND
Dibromomethane ug/kg 799856 93 63-131ND
Dichlorodifluoromethane ug/kg 792856 93 44-180ND
Diisopropyl ether ug/kg 712856 83 63-130ND
Ethylbenzene ug/kg 740856 86 66-130ND
Hexachloro-1,3-butadiene ug/kg 725856 85 64-150ND
Isopropylbenzene (Cumene)ug/kg 785856 92 69-135ND
m&p-Xylene ug/kg 15501720 91 60-133ND
Methyl-tert-butyl ether ug/kg 729856 85 65-130ND
Methylene Chloride ug/kg 790856 92 61-130ND
n-Butylbenzene ug/kg 673856 79 65-140ND
n-Propylbenzene ug/kg 729856 85 67-140ND
Naphthalene ug/kg 778856 89 15-14519.5
o-Xylene ug/kg 778856 91 66-133ND
p-Isopropyltoluene ug/kg 733856 86 56-147ND
sec-Butylbenzene ug/kg 740856 86 65-139ND
Styrene ug/kg 795856 93 70-132ND
tert-Butylbenzene ug/kg 755856 88 62-135ND
Tetrachloroethene ug/kg 680856 79 70-135ND
Toluene ug/kg 785856 92 67-130ND
trans-1,2-Dichloroethene ug/kg 694856 81 69-130ND
trans-1,3-Dichloropropene ug/kg 756856 88 62-130ND
Trichloroethene ug/kg 751856 88 70-135ND
Trichlorofluoromethane ug/kg 317856 37 10-130ND
Vinyl acetate ug/kg 16701720 97 53-130ND
Vinyl chloride ug/kg 734856 86 61-148ND
Xylene (Total)ug/kg 23302570 91 63-132ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%105 69-134
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92534944001
3243350SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg 4.5J 304.7J
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92534944001
3243350SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg 16.4 1 3016.3
o-Xylene ug/kg 5.0J 305.2J
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg 5.4J 305.2J
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 305.2J
1,2-Dichloroethane-d4 (S)%101104
4-Bromofluorobenzene (S)%104105
Toluene-d8 (S)%9998
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
616413
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92534944001, 92534944002, 92534944003, 92534944004, 92534944005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3243700
Associated Lab Samples:92534944001, 92534944002, 92534944003, 92534944004, 92534944005
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 327 04/27/21 10:42129
1,2-Dichlorobenzene ug/kg ND 327 04/27/21 10:42118
1,3-Dichlorobenzene ug/kg ND 327 04/27/21 10:42116
1,4-Dichlorobenzene ug/kg ND 327 04/27/21 10:42125
1-Methylnaphthalene ug/kg ND 327 04/27/21 10:42115
2,2'-Oxybis(1-chloropropane)ug/kg ND 327 04/27/21 10:42155
2,4,5-Trichlorophenol ug/kg ND 327 04/27/21 10:42150
2,4,6-Trichlorophenol ug/kg ND 327 04/27/21 10:42135
2,4-Dichlorophenol ug/kg ND 327 04/27/21 10:42128
2,4-Dimethylphenol ug/kg ND 327 04/27/21 10:42136
2,4-Dinitrophenol ug/kg ND 1630 v104/27/21 10:421010
2,4-Dinitrotoluene ug/kg ND 327 04/27/21 10:42126
2,6-Dinitrotoluene ug/kg ND 327 04/27/21 10:42120
2-Chloronaphthalene ug/kg ND 327 04/27/21 10:42130
2-Chlorophenol ug/kg ND 327 04/27/21 10:42123
2-Methylnaphthalene ug/kg ND 327 04/27/21 10:42131
2-Methylphenol(o-Cresol)ug/kg ND 327 04/27/21 10:42134
2-Nitroaniline ug/kg ND 1630 04/27/21 10:42267
2-Nitrophenol ug/kg ND 327 04/27/21 10:42142
3&4-Methylphenol(m&p Cresol)ug/kg ND 327 04/27/21 10:42132
3,3'-Dichlorobenzidine ug/kg ND 653 IL04/27/21 10:42221
3-Nitroaniline ug/kg ND 1630 04/27/21 10:42256
4,6-Dinitro-2-methylphenol ug/kg ND 653 04/27/21 10:42305
4-Bromophenylphenyl ether ug/kg ND 327 04/27/21 10:42126
4-Chloro-3-methylphenol ug/kg ND 653 04/27/21 10:42230
4-Chloroaniline ug/kg ND 653 04/27/21 10:42256
4-Chlorophenylphenyl ether ug/kg ND 327 04/27/21 10:42122
4-Nitroaniline ug/kg ND 653 04/27/21 10:42249
4-Nitrophenol ug/kg ND 1630 04/27/21 10:42632
Acenaphthene ug/kg ND 327 04/27/21 10:42115
Acenaphthylene ug/kg ND 327 04/27/21 10:42115
Aniline ug/kg ND 327 04/27/21 10:42128
Anthracene ug/kg ND 327 04/27/21 10:42107
Benzo(a)anthracene ug/kg ND 327 04/27/21 10:42109
Benzo(a)pyrene ug/kg ND 327 04/27/21 10:42113
Benzo(b)fluoranthene ug/kg ND 327 04/27/21 10:42109
Benzo(g,h,i)perylene ug/kg ND 327 04/27/21 10:42127
Benzo(k)fluoranthene ug/kg ND 327 04/27/21 10:42115
Benzoic Acid ug/kg ND 1630 04/27/21 10:42702
Benzyl alcohol ug/kg ND 653 04/27/21 10:42248
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3243700
Associated Lab Samples:92534944001, 92534944002, 92534944003, 92534944004, 92534944005
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 327 04/27/21 10:42136
bis(2-Chloroethyl) ether ug/kg ND 327 04/27/21 10:42123
bis(2-Ethylhexyl)phthalate ug/kg ND 327 04/27/21 10:42127
Butylbenzylphthalate ug/kg ND 327 04/27/21 10:42138
Chrysene ug/kg ND 327 04/27/21 10:42119
Di-n-butylphthalate ug/kg ND 327 04/27/21 10:42110
Di-n-octylphthalate ug/kg ND 327 04/27/21 10:42129
Dibenz(a,h)anthracene ug/kg ND 327 04/27/21 10:42126
Dibenzofuran ug/kg ND 327 04/27/21 10:42118
Diethylphthalate ug/kg ND 327 04/27/21 10:42120
Dimethylphthalate ug/kg ND 327 04/27/21 10:42119
Fluoranthene ug/kg ND 327 04/27/21 10:42112
Fluorene ug/kg ND 327 04/27/21 10:42115
Hexachloro-1,3-butadiene ug/kg ND 327 04/27/21 10:42142
Hexachlorobenzene ug/kg ND 327 04/27/21 10:42128
Hexachlorocyclopentadiene ug/kg ND 327 04/27/21 10:42187
Hexachloroethane ug/kg ND 327 04/27/21 10:42125
Indeno(1,2,3-cd)pyrene ug/kg ND 327 04/27/21 10:42129
Isophorone ug/kg ND 327 04/27/21 10:42146
N-Nitroso-di-n-propylamine ug/kg ND 327 04/27/21 10:42123
N-Nitrosodimethylamine ug/kg ND 327 04/27/21 10:42110
N-Nitrosodiphenylamine ug/kg ND 327 04/27/21 10:42116
Naphthalene ug/kg ND 327 04/27/21 10:42111
Nitrobenzene ug/kg ND 327 04/27/21 10:42151
Pentachlorophenol ug/kg ND 653 04/27/21 10:42320
Phenanthrene ug/kg ND 327 04/27/21 10:42107
Phenol ug/kg ND 327 04/27/21 10:42146
Pyrene ug/kg ND 327 04/27/21 10:42133
Pyridine ug/kg ND 327 04/27/21 10:42103
2,4,6-Tribromophenol (S)%77 18-130 04/27/21 10:42
2-Fluorobiphenyl (S)%71 19-130 04/27/21 10:42
2-Fluorophenol (S)%66 18-130 04/27/21 10:42
Nitrobenzene-d5 (S)%71 21-130 04/27/21 10:42
Phenol-d6 (S)%68 18-130 04/27/21 10:42
Terphenyl-d14 (S)%77 15-130 04/27/21 10:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3243701LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13201690 78 47-130
1,2-Dichlorobenzene ug/kg 12501690 74 49-130
1,3-Dichlorobenzene ug/kg 12501690 74 48-130
1,4-Dichlorobenzene ug/kg 12701690 75 49-130
1-Methylnaphthalene ug/kg 13801690 81 54-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3243701LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 13401690 79 38-130
2,4,5-Trichlorophenol ug/kg 14201690 84 49-130
2,4,6-Trichlorophenol ug/kg 13601690 81 50-130
2,4-Dichlorophenol ug/kg 13801690 82 51-130
2,4-Dimethylphenol ug/kg 14201690 84 53-130
2,4-Dinitrophenol ug/kg 7380 v184508739-130
2,4-Dinitrotoluene ug/kg 13401690 79 53-130
2,6-Dinitrotoluene ug/kg 13401690 79 55-130
2-Chloronaphthalene ug/kg 13301690 79 48-130
2-Chlorophenol ug/kg 13001690 77 54-130
2-Methylnaphthalene ug/kg 13801690 81 57-130
2-Methylphenol(o-Cresol)ug/kg 13401690 79 50-130
2-Nitroaniline ug/kg 29203380 86 49-130
2-Nitrophenol ug/kg 14001690 83 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 13401690 79 50-130
3,3'-Dichlorobenzidine ug/kg 2440 IL33807247-130
3-Nitroaniline ug/kg 27903380 83 45-130
4,6-Dinitro-2-methylphenol ug/kg 32903380 97 50-142
4-Bromophenylphenyl ether ug/kg 15201690 90 55-130
4-Chloro-3-methylphenol ug/kg 28303380 84 52-130
4-Chloroaniline ug/kg 24703380 73 49-130
4-Chlorophenylphenyl ether ug/kg 13801690 82 53-130
4-Nitroaniline ug/kg 24303380 72 51-130
4-Nitrophenol ug/kg 70808450 84 40-130
Acenaphthene ug/kg 13801690 82 56-130
Acenaphthylene ug/kg 14201690 84 58-130
Aniline ug/kg 12201690 72 44-130
Anthracene ug/kg 14201690 84 60-130
Benzo(a)anthracene ug/kg 14801690 88 59-130
Benzo(a)pyrene ug/kg 14601690 86 57-130
Benzo(b)fluoranthene ug/kg 14901690 88 54-130
Benzo(g,h,i)perylene ug/kg 16001690 95 59-130
Benzo(k)fluoranthene ug/kg 14701690 87 54-130
Benzoic Acid ug/kg 59908450 71 19-130
Benzyl alcohol ug/kg 25803380 76 50-130
bis(2-Chloroethoxy)methane ug/kg 13701690 81 55-130
bis(2-Chloroethyl) ether ug/kg 14001690 83 53-130
bis(2-Ethylhexyl)phthalate ug/kg 15601690 92 58-130
Butylbenzylphthalate ug/kg 16001690 95 46-138
Chrysene ug/kg 14601690 87 57-130
Di-n-butylphthalate ug/kg 14301690 85 57-130
Di-n-octylphthalate ug/kg 14501690 86 57-130
Dibenz(a,h)anthracene ug/kg 15101690 89 60-130
Dibenzofuran ug/kg 13401690 80 54-130
Diethylphthalate ug/kg 13901690 82 55-130
Dimethylphthalate ug/kg 13801690 82 57-130
Fluoranthene ug/kg 13501690 80 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3243701LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 14001690 83 56-130
Hexachloro-1,3-butadiene ug/kg 13701690 81 41-130
Hexachlorobenzene ug/kg 14301690 85 53-130
Hexachlorocyclopentadiene ug/kg 11701690 69 23-130
Hexachloroethane ug/kg 12801690 76 48-130
Indeno(1,2,3-cd)pyrene ug/kg 15801690 94 61-130
Isophorone ug/kg 13801690 82 49-130
N-Nitroso-di-n-propylamine ug/kg 13201690 78 52-130
N-Nitrosodimethylamine ug/kg 13701690 81 45-130
N-Nitrosodiphenylamine ug/kg 15101690 89 56-130
Naphthalene ug/kg 13701690 81 56-130
Nitrobenzene ug/kg 13401690 80 50-130
Pentachlorophenol ug/kg 30503380 90 33-130
Phenanthrene ug/kg 14701690 87 60-130
Phenol ug/kg 13201690 78 54-130
Pyrene ug/kg 17001690 100 61-130
Pyridine ug/kg 11001690 65 35-130
2,4,6-Tribromophenol (S)%98 18-130
2-Fluorobiphenyl (S)%85 19-130
2-Fluorophenol (S)%79 18-130
Nitrobenzene-d5 (S)%84 21-130
Phenol-d6 (S)%80 18-130
Terphenyl-d14 (S)%89 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3243702MATRIX SPIKE SAMPLE:
MSSpike
Result
92534944001
1,2,4-Trichlorobenzene ug/kg 14602030 72 22-130ND
1,2-Dichlorobenzene ug/kg 14002030 69 23-130ND
1,3-Dichlorobenzene ug/kg 13702030 67 26-130ND
1,4-Dichlorobenzene ug/kg 13802030 68 27-130ND
1-Methylnaphthalene ug/kg 14702030 72 30-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 12502030 61 30-130ND
2,4,5-Trichlorophenol ug/kg 15102030 74 26-130ND
2,4,6-Trichlorophenol ug/kg 14702030 72 23-130ND
2,4-Dichlorophenol ug/kg 15402030 76 29-130ND
2,4-Dimethylphenol ug/kg 1620 v120308013-130ND
2,4-Dinitrophenol ug/kg 617010200 61 10-131ND
2,4-Dinitrotoluene ug/kg 15402030 76 28-130ND
2,6-Dinitrotoluene ug/kg 14302030 70 36-130ND
2-Chloronaphthalene ug/kg 14002030 69 27-130ND
2-Chlorophenol ug/kg 14102030 69 29-130ND
2-Methylnaphthalene ug/kg 14502030 71 29-130ND
2-Methylphenol(o-Cresol)ug/kg 15002030 73 20-130ND
2-Nitroaniline ug/kg 27304070 67 29-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3243702MATRIX SPIKE SAMPLE:
MSSpike
Result
92534944001
2-Nitrophenol ug/kg 14202030 70 26-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 15202030 75 10-176ND
3,3'-Dichlorobenzidine ug/kg 3060 IL40707515-130ND
3-Nitroaniline ug/kg 25604070 63 28-130ND
4,6-Dinitro-2-methylphenol ug/kg 30204070 74 15-132ND
4-Bromophenylphenyl ether ug/kg 16102030 75 35-130ND
4-Chloro-3-methylphenol ug/kg 30904070 76 30-130ND
4-Chloroaniline ug/kg 28504070 70 28-130ND
4-Chlorophenylphenyl ether ug/kg 16102030 79 32-130ND
4-Nitroaniline ug/kg 26604070 65 30-130ND
4-Nitrophenol ug/kg 790010200 78 17-130ND
Acenaphthene ug/kg 14702030 72 29-130ND
Acenaphthylene ug/kg 14702030 72 31-130ND
Aniline ug/kg 13502030 66 10-130ND
Anthracene ug/kg 15902030 75 33-130ND
Benzo(a)anthracene ug/kg 15902030 76 32-130ND
Benzo(a)pyrene ug/kg 16502030 81 32-130ND
Benzo(b)fluoranthene ug/kg 16502030 81 33-130ND
Benzo(g,h,i)perylene ug/kg 15502030 76 28-130ND
Benzo(k)fluoranthene ug/kg 16602030 82 31-130ND
Benzoic Acid ug/kg 418010200 41 10-130ND
Benzyl alcohol ug/kg 28404070 70 31-130ND
bis(2-Chloroethoxy)methane ug/kg 14602030 72 30-130ND
bis(2-Chloroethyl) ether ug/kg 15102030 74 68-130ND
bis(2-Ethylhexyl)phthalate ug/kg 15302030 75 40-130ND
Butylbenzylphthalate ug/kg 14802030 73 40-130ND
Chrysene ug/kg 15902030 76 30-130ND
Di-n-butylphthalate ug/kg 15502030 76 41-130ND
Di-n-octylphthalate ug/kg 15402030 75 42-130ND
Dibenz(a,h)anthracene ug/kg 15702030 77 27-130ND
Dibenzofuran ug/kg 15102030 74 32-130ND
Diethylphthalate ug/kg 15202030 75 40-130ND
Dimethylphthalate ug/kg 14902030 73 37-130ND
Fluoranthene ug/kg 17602030 82 26-130ND
Fluorene ug/kg 15402030 75 31-130ND
Hexachloro-1,3-butadiene ug/kg 1550 v120307620-130ND
Hexachlorobenzene ug/kg 16702030 82 29-130ND
Hexachlorocyclopentadiene ug/kg 10902030 53 10-130ND
Hexachloroethane ug/kg 14302030 70 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 15702030 77 28-130ND
Isophorone ug/kg 14502030 71 32-130ND
N-Nitroso-di-n-propylamine ug/kg 14602030 72 31-130ND
N-Nitrosodimethylamine ug/kg 12402030 61 20-130ND
N-Nitrosodiphenylamine ug/kg 15502030 76 32-130ND
Naphthalene ug/kg 14202030 70 30-130ND
Nitrobenzene ug/kg 13802030 68 25-130ND
Pentachlorophenol ug/kg 30504070 75 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3243702MATRIX SPIKE SAMPLE:
MSSpike
Result
92534944001
Phenanthrene ug/kg 16702030 78 34-130ND
Phenol ug/kg 15802030 78 14-130ND
Pyrene ug/kg 15802030 74 31-130ND
Pyridine ug/kg 10702030 52 10-130ND
2,4,6-Tribromophenol (S)%83 18-130
2-Fluorobiphenyl (S)%70 19-130
2-Fluorophenol (S)%72 18-130
Nitrobenzene-d5 (S)%70 21-130
Phenol-d6 (S)%72 18-130
Terphenyl-d14 (S)%66 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92534944002
3243703SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND v130ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND IL30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92534944002
3243703SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND v130ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%5857
2-Fluorobiphenyl (S)%3231
2-Fluorophenol (S)%5152
Nitrobenzene-d5 (S)%5050
Phenol-d6 (S)%5253
Terphenyl-d14 (S)%3736
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
615949
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92534944001, 92534944002, 92534944003, 92534944004, 92534944005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92534890001
3241611SAMPLE DUPLICATE:
Percent Moisture %8.3 N24257.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92534963001
3241612SAMPLE DUPLICATE:
Percent Moisture %25.9 N2102523.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1660447
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92534944001, 92534944002, 92534944003, 92534944004, 92534944005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3648142-1
Associated Lab Samples:92534944001, 92534944002, 92534944003, 92534944004, 92534944005
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 04/28/21 17:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3648142-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1343653-01
R3648142-3SAMPLE DUPLICATE:
Total Solids %99.8 0.0169 1099.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1659474
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92534944004, 92534944005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3648392-1
Associated Lab Samples:92534944004, 92534944005
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 04/29/21 13:030.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3648392-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.710.0 107 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3648392-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1338739-01
R3648392-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 22.7 103 75.0-125105 1.25 2022.7ND 23.4 23.7
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3648392-5MATRIX SPIKE SAMPLE:
MSSpike
Result
L1338739-01
Chromium, Hexavalent mg/kg 760724 105 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1338739-02
R3648392-7SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1338739-11
R3648392-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92534944
WPP-005
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1659898
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92534944001, 92534944002, 92534944003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3649288-1
Associated Lab Samples:92534944001, 92534944002, 92534944003
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 05/01/21 17:020.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3649288-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.410.0 104 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3649288-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1343689-04
R3649288-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 26.4 98.2 75.0-12597.9 0.289 2026.40.727 26.7 26.6
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3649288-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1343689-04
Chromium, Hexavalent mg/kg 830849 97.7 75.0-1250.727
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1342745-01
R3649288-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1343754-43
R3649288-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 55
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92534944
WPP-005
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 55
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92534944
WPP-005
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92534944001 1658291 1658291FG-1 (0-2)3050B EPA 6020B
92534944002 1658291 1658291FG-2 (0-2)3050B EPA 6020B
92534944003 1658291 1658291FG-3 (0-2)3050B EPA 6020B
92534944004 1658291 1658291FG-4 (0-2)3050B EPA 6020B
92534944005 1658291 1658291FG-DUP 3050B EPA 6020B
92534944001 1658884 1658884FG-1 (0-2)7471A EPA 7471B
92534944002 1658884 1658884FG-2 (0-2)7471A EPA 7471B
92534944003 1658884 1658884FG-3 (0-2)7471A EPA 7471B
92534944004 1658868 1658868FG-4 (0-2)7471A EPA 7471B
92534944005 1658868 1658868FG-DUP 7471A EPA 7471B
92534944001 616413 616460FG-1 (0-2)EPA 3546 EPA 8270E
92534944002 616413 616460FG-2 (0-2)EPA 3546 EPA 8270E
92534944003 616413 616460FG-3 (0-2)EPA 3546 EPA 8270E
92534944004 616413 616460FG-4 (0-2)EPA 3546 EPA 8270E
92534944005 616413 616460FG-DUP EPA 3546 EPA 8270E
92534944001 616268 616421FG-1 (0-2)EPA 5035A/5030B EPA 8260D
92534944002 616268 616421FG-2 (0-2)EPA 5035A/5030B EPA 8260D
92534944003 616268 616421FG-3 (0-2)EPA 5035A/5030B EPA 8260D
92534944004 616268 616421FG-4 (0-2)EPA 5035A/5030B EPA 8260D
92534944005 616268 616421FG-DUP EPA 5035A/5030B EPA 8260D
92534944001 615949FG-1 (0-2)SW-846
92534944002 615949FG-2 (0-2)SW-846
92534944003 615949FG-3 (0-2)SW-846
92534944004 615949FG-4 (0-2)SW-846
92534944005 615949FG-DUP SW-846
92534944001 1660447 1660447FG-1 (0-2)SM 2540 G SM 2540G
92534944002 1660447 1660447FG-2 (0-2)SM 2540 G SM 2540G
92534944003 1660447 1660447FG-3 (0-2)SM 2540 G SM 2540G
92534944004 1660447 1660447FG-4 (0-2)SM 2540 G SM 2540G
92534944005 1660447 1660447FG-DUP SM 2540 G SM 2540G
92534944001 1659898 1659898FG-1 (0-2)3060A EPA 7199
92534944002 1659898 1659898FG-2 (0-2)3060A EPA 7199
92534944003 1659898 1659898FG-3 (0-2)3060A EPA 7199
92534944004 1659474 1659474FG-4 (0-2)3060A EPA 7199
92534944005 1659474 1659474FG-DUP 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/03/2021 12:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 55
Page 53 of 55
Page 54 of 55
Page 55 of 55

Appendix B
DEQ Risk Calculator

Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
8/13/2021
Prepared By:H&H
Worst-Case
North Carolina Department of Environmental Quality
Risk Calculator
Chadbourn Mill
451 Jordan Place
DEQ Brownfields
20086-16-060
June 2021
May 2021 EPA RSL Table
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 20086-16-060
Exposure Unit ID: Worst-Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 20086-16-060
Exposure Unit ID: Worst-Case
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(mg/kg)
Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
0.147 67-64-1 Acetone mg/kg
24.7 7440-38-2 Arsenic, Inorganic mg/kg
144 7440-39-3 Barium mg/kg
0.0083 71-43-2 Benzene mg/kg
0.233 7440-43-9 Cadmium (Diet)mg/kg
60 16065-83-1 Chromium(III), Insoluble Salts mg/kg
0.361 18540-29-9 Chromium(VI)mg/kg
0.0053 100-41-4 Ethylbenzene mg/kg
48.2 7439-92-1 ~Lead and Compounds mg/kg
0.0603 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
0.0195 91-20-3 ~Naphthalene mg/kg
1.54 7782-49-2 Selenium mg/kg
0.0156 108-88-3 Toluene mg/kg
1.33 79-01-6 Trichloroethylene mg/kg
0.0047 95-63-6 Trimethylbenzene, 1,2,4-mg/kg
0.023 108-38-3 Xylene, m-mg/kg
0.0105 95-47-6 Xylene, o-mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 20086-16-060
Exposure Unit ID: Worst-Case
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil 8.5E-06 1.0E-01 NO
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 20086-16-060
Exposure Unit ID: Worst-Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.147 0.147 0.147 1.4E-07 7.4E-08 2.1E-07
7440-38-2 Arsenic, Inorganic 24.7 24.7 24.7 6.8E-06 1.4E-06 1.5E-10 8.2E-06 4.2E-02 9.0E-03 6.3E-06 5.1E-02
7440-39-3 Barium 144 144 144 6.2E-04 1.1E-06 6.2E-04
71-43-2 Benzene 0.0083 0.0083 0.0083 1.4E-10 1.4E-09 1.5E-09 1.8E-06 1.7E-05 1.9E-05
7440-43-9 Cadmium (Diet) 0.233 0.233 0.233 5.8E-13 5.8E-13 2.0E-04 3.4E-05 9.0E-08 2.3E-04
16065-83-1 Chromium(III), Insoluble Salts 60 60 60 3.4E-05 3.4E-05
18540-29-9 Chromium(VI) 0.361 0.361 0.361 5.5E-08 4.2E-11 5.5E-08 1.0E-04 1.4E-08 1.0E-04
100-41-4 Ethylbenzene 0.0053 0.0053 0.0053 1.8E-11 1.8E-10 2.0E-10 4.5E-08 2.0E-07 2.5E-07
7439-92-1 ~Lead and Compounds 48.2 48.2 48.2 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.0603 0.0603 0.0603 1.7E-04 7.7E-10 1.7E-04
91-20-3 ~Naphthalene 0.0195 0.0195 0.0195 7.2E-10 3.9E-10 1.1E-09 2.2E-09 8.3E-07 4.6E-07 3.0E-05 3.1E-05
7782-49-2 Selenium 1.54 1.54 1.54 2.6E-04 3.0E-10 2.6E-04
108-88-3 Toluene 0.0156 0.0156 0.0156 1.7E-07 1.6E-07 3.2E-07
79-01-6 Trichloroethylene 1.33 1.33 1.33 1.9E-08 1.4E-07 1.6E-07 2.3E-03 4.8E-02 5.1E-02
95-63-6 Trimethylbenzene, 1,2,4- 0.0047 0.0047 0.0047 4.0E-07 2.1E-06 2.5E-06
1330-20-7 Xylenes 0.0335 0.0335 0.0335 1.4E-07 1.3E-05 1.3E-05
Cumulative: 8.5E-06 1.0E-01
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator