5601_ROSCANS_2006

MCDOWELL COUNTY
PUBLIC WORKS
MIKE GLADDEN, DIRECTOR
60 EAST COURT STREET
MARION, NC 28752
January 17, 2006
Mr. Al Hetzell
Division of Waste Management
Solid Waste Section
2090 US Hwy 70
Swannanoa, NC 28778
Dear Al,
I am forwarding you a copy of the "Grey Water Analysis" received from Pace
Analytical. I am also enclosing a copy of a letter received from Larry Carver,
WWTP Superintendent, City of Marion.
As you will note, City of Marion requires a notice of State approval for us to
continue with this project.
Will you please let me hear when this approval is authorized.
Thanks for your help.
MG/grns
cc: Deborah Aja
file
SITE LOCATION:
3849 HWY. 226 SOUT14
MARION, NC 28752
PHONE: [phone]
FAX: [phone]

CITY OF MARION
WASTEWATER TREATMENT PLANT
P. 0. Drawer 700 SUPERINTENDENT
Marion, North Carolina 28752
January, 11, 2006
Mr. Nlike Gladden
McDowell County Landfill
10 East Court St.
Marion, NC 28752
RE: Grey Water at Landfill
Dear Mr. Gladden:
Please be advised that after reviewing the laboratory analysis from Pace Analytical on the
grey water from the landfill, I have determined that nothing was found that would deter
us ftom receiving the liquid in our waste stream. Should this finding change at any time,
You would be notified immediately.
Once you have State approval, we will proceed to set up a file, that will authorize you to
pump and haul the liquid to our Public Works facility.
We will treat this process just like we do our septic haulers. The cost of dumping is
$15.00 per load and $.02 per gallon. Your truck would have to have a gauge to measure
the gallons.
If you have any questions, or need further information please call me at 652-8843.
WWTP Superintendent

'a , Jq
U
P20
Pa��ceAnalyfical"`
www.,uacelabs.com
December 16, 2005
Mr. Mike Gladden
McDowell County Landfill
10 East Court St.
Marion. NC 28752
Pace Analytical Services, Inc.
9800ftceyAvenue, Suite too
HURt6rSville, NC 28078
Phone [phone]
FW 704.875.9091
Pace Analyfical Services, Inc.
2225 Riverside Drive
Asheville, NG28804
Phone, 828.254.7176
rax: 828.252,4618
RE: Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Dear Mr. Gladden:
Enclosed are the analytical results for sample(s) received by the laboratory on December 5. 2005. Results
reported herein conform to the most current NELAC standards, where applicable. unless otherwise narrated in the
body of the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If -you have any questions concerning this report please feel free to contact me
Sincerely,
To lil las
[e-mail]
Project Manager
Encl osures
Asheville Certification IDs
NC Wastewater 40
NG Drinking Water 37712
Sc 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
"'2CS-"
Qhariiifte Certification IDs
NC Wastewater 12
NG Drinking Water 37706
SC 99006
FL NELAP E87627

P
--1--i'diceAnalyticale
www.pacalabs.com
Lab Sample No: 926408667
Client Sample ID: GREY WATER
Pace Analytical Services, Inc.
9800 KIncey Avenue, Suite 100
Huntersville, PIC 28078
Phone: [phone]
Fax [phone]
Pace Aflillica' Ser ce " c
2226 RiverTdosH;lv�,
Asheville, NC 28804
Phone., 828.254.7176
Fax., 828.252.4618
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Project Sample Number: 92108723-001 Date Collected: 12/01/05 09:00
Matrix: Water Date Received: 12105105 10:45
Parameters
Results
Units
Report Limit
Analyzed
By
CAS Non Qual ReqLmt
Metal s
Trace ICP Metals
Prep/Method: / EPA 200.7
Aluminum
5.8
mg/l
0.10
12/14/05
12:38
SAJ
7429-90-5
Antimony
0.012
mg/l
0.0050
12/14/05
12:38
SAJ
7440-36-0
Arsenic
0.070
mg/l
0.0050
12/14/05
12:38
SAJ
7440-38-2
Barium
0.29
mg/l
0.0050
12/14105
12:38
SAJ
7440-39-3
Beryllium
NO
mg/l
0.0010
12/14/05
12:38
SAJ
7440-41-7
Cadmium
0.0090
mg/l
0.0010
12/14/05
12:38
SAJ
7440-43-9
Chromium
0.045
mg/1
0,0020
12/14/05
12:38
SAJ
7440-47-3
Copper
0.013
mg/l,
0.0020
12/14/05
12:38
SAJ
7440-50-8
Lead
0.11
mg/1
0.0050
12/14/05
12:38
SAJ
7439-92-1
Molybdenum
0.12
mg/l
0.0050
12/14/05
12:38
SAJ
7439-98-7
Nickel
O�083
mg/l
0.0050
12/14/05
12:38
SAJ
7440-02-0
Selenium
0.022
mg/l
0.0050
12/14/05
12:38
SAJ
7782-49-2
Silver
NO
mg/l
0.0020
12/14/05
12:38
SAJ
7440-22-4
Thallium
MID
mg/l
0.010
12/14105
12:38
SAJ
7440-28-0
Zinc
4.2
mg/l
0.010
12/14/05
12:38
SAJ
7440-66-6
Date Digested
12/07/05 16:50
12/07105
16:50
Mercury, CVAAS, in Water
Method: EPA
245.1
Mercury
0.0010
mg/l
0.00020
12/06/05
10:39
ALV
7439-97-6
Wet Chemistry
Total Suspended Solids
Method: EPA
160,2
Total Suspended Solids
760
mg/l
33.
12/06/05
21:23
TMR
Chloride (Mercuric Nitrate)
Method: EPA
325.2
Chloride
1100
mg/l
270
12/08/05
21:00
BMF
16887-00.6
Cyanide, Total, Water
Method: EPA
335.2
Cyanide
ND
mg/l
0.0050
12/07/05
11:30
BMF
57-12-5
Fl uori de
Fl uori de
Ammonia
Nitrogen, Ammonia
Chemical Oxygen Demand
Date: 12116/05
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
Method: EPA 340.2
0.22 mg/l
Method: EPA 350.1
0.13 mg/l
Method: EPA 410.4
0.10 12/08/05 11:20 TMR 16984-48-8
0.10 12/07/05 08:00 BMIF 7727-37-9
I IM
REPORT OF LABORATORY ANALIDIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc.
t
z,n hrl�
Page: I of 35
Charlotte Certification iDs
NC Wastewater
12
ING Drinking Water
37706
SC
99006
FIL NELAP
E87627

raceAnalyficale
www.pacelabs.com
Page Analytical Saryices, Jac.
9800 Kincey Avenue, Suite 100
Hunt6rsville, NC 28078
Phone., 704.875.9092
Fax [phone]
Pace Analjdaal Services, Inc.
2225 Riverside Drive
Ast7oville, NC28804
Phone: [phone]
Fax.'828.252,4618
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Lab Sample No: 926408667
Client Sample 10: GREY
Project Sample Number: 92108723-001 Date Collected: 12101105 Og:oo
WATER
Matrix: Water
Date Received- 12/05/05 10:45
Parameters
Results
Units
Report Limit Analyzed By
CAS No. Qual ReqLmt
Chemical Oxygen Demand
810
mg/l
25.
12/09/05 06:30 EWS
GUMS Serilivolatiles
Semivolatile Organics
Prep/Method:
EPA 3510
EPA 8270
Acenaphthene
NO
ug/l
it.
12/08/05 19:56 BET
83-32-9
Acenaphthylene
No
ug/l
it.
12/08/05 19:56 BET
208-96-8
Aniline
ND
ug/l
11,
12/08105 19:56 BET
62-53-3
Anthracene
NO
ug/l
11.
12/08/05 19:56 BET
120-12.7
Benzo(k)fluoranthene
NO
ug/l
11.
12/08/05 19:56 BET
207-08-9
Benzo(b)fluoranthene
NO
ug/l
11.
12/08/05 19:56 BET
205-99.2
Benzo(a)anthracene
ND
ug/I
11.
12/08/05 19:56 BET
56�55-3
Benzoic acid
NO
ug/l
53.
12/08/05 19:56 BET
65-85-0
Benzo(g.h,i)perylene
ND
ug/l
it.
12/08/05 19:56 BET
191-24.2
Benzyl alcohol
ND
ug/l
21,
12108/05 19:66 BET
100-51-6
Benzo(a)pyrene
NO
ug/l
11.
12/08/05 19:56 BET
50-32-8
4-Bromophenylphenyl ether
ND
ug/l
11.
12/08105 19:56 BET
101-55-3
Butylbenzylphthalate
ND
ug/l
11.
12/08/05 19:56 BET
85-68-7
4-Chloro-3-methylphenol
NO
ug/l
21.
12/08/05 19:56 BET
59-50-7
4-Chloroaniline
ND
ug/l
21.
12/08/05 19:56 BET
106-47.8
bis(2-Chloroethoxy)methane
NO
ug/l
11.
12/08/05 19:56 BET
111-91,1
bis(2-Chloroethyl) ether
ND
ug/l
11.
12/08/05 19:56 BET
111-44.4
bis(2-Chloroisopropyl) ether
NO,
ug/l
11,
12108/05 19:56 BET
39638-32-9
2-Chloronaphthalene
ND
ug/l
11.
12/08/05 19:56 BET
91-58-7
2-Chlorophenol
NO
U911
it.
12/08/05 19:56 BET
95-57-8
4-Chlorophenylphenyl ether
NO
ug/l
it.
12/08/05 19:56 BET
7005-72-3
Chrysene
ND
ug/l
11.
12108/05 19:56 BET
218-01-9
Dibenz(a,h)anthracene
NO
ug/1
11.
12/08/05 19:56 BET
53-70-3
Dibenzofuran
ND
ug/l
it.
12/08/05 19:56 BET
132-64,9
1.2-Dicblorobenzene
NO
ug/1
11�
12/08/05 19:56 BET
95-50-1
1.3-Dichlorobenzene
NO
ug/l
11.
12/08/05 19:56 BET
541-73-1
1,4-Dichlorobenzene
ND
ug/l
it.
12/08/05 19:56 BET
106-46-7
3,3' - Di chl orobenzi dine
ND
ug1l
21.
12/08/05 19:56 BET
91-94-1
2.4-Dichlorophenol
NO
ug/l
it.
12/08/05 19:56 BET
120-83-2
Diethylphthalate
47.
ug/l
11.
12108/05 19:56 BET
84-66-2
2,4 - Dimethyl phenol
ND
ug/l
11.
12/08/05 19:56 BET
105-67�9
Dimethylphthalate
NO
ug/l
11.
12/08/05 19:56 BET
131-11-3
Di-n-butylphthalate
15.
ug/l
11.
12/08105 19:56 BET
84-74-2
4.6-Dinitro-2-methylphenol
NO
ugil
53.
12/08/05 19:56 BET
534-52.1
2.4-Dinitrophenol
NO
ug/I
53.
12/08/05 19:56 BET
51-28�5
Date: 12/16105
Page: 2 of 35
A5heville Certification IDs
NC Wastewater 40
REPORT OF LABORATORY ANALYSIS
Chgrlotte Certfication IDs
NC Drinking Water 37719
This report shall not be reproduced,
except in full,
NC Wastewater 12
SC 99030
without the written consent
of Pace Analytical Services, Inc.
NC Drinking Water 37706
FL NELAP E87648
SC 99006
FL NELAP E87627
niphr

ke Analytical
www.,Uacelalis.com
Lab Sample No: 926408667
Client Sample ID: GREY WATER
Paco Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
Pace Analyfi:jl Serrices, Inc.
2225Riverstide Mrive,
Asheville, AIC28804
Phooe., B28.254.7176
Fa.x- 828.252.4618
Lab Project Number: 92108723
Client Project 10: Grey Water Analysis
Project Sample Number: 92108723-001 Date Collected: 12/01/05 09:00
Matrix: Water Date Received: 12/05/05 10:45
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual Recil-art
2,4-Dinitrotoluene
ND
ug/l
11.
12/08/05
19:56
BET
121-14-2
2,6-Dinitrotoluene
ND
ug/I
11�
12/08/05
19:56
BET
606-20-2
Di-n-octylphthalate
ND
ug/l
11.
12/08/05
19:56
BET
117-84-0
1.2-Diphenylhydrazine
NO
ug/l
21.
12108106
19:56
BET
122-66-7
bis(2-Ethylhexyl)phthalate
16.
ug/l
11.
12/08/05
19:56
BET
117-81-7
Fluoranthene
NO
ug/l
11.
12/08/05
19:56
BET
206-44-0
Fluorene
ND
ug/l
11.
12/08/05
19:56
BET
86-73-7
Hexachloro-1,3-butadiene
NO
ug/l
11.
12/08/05
19:56
BET
87-68-3
Hexachlorobenzene
NO
ug/l
11.
12/08/05
19:56
BET
118-74-1
Nexachlorocyclopentadiene
ND
ug/1
11.
12/08/05
19:56
BET
77-47-4
Hexachloroethane
ND
ug/1
11.
12/08/05
19:56
BET
67-72-1
Indeno(l.2.3-cd)pyrene
ND
ug/l
11.
12/08/05
19:56
BET
193-39-5
Isophorone
ND
ug/l
11.
12/06/05
19:56
BET
78-59-1
2-Methylnaphthalene
ND
ug/l
11,
12108/05
19:56
BET
91-57-6
2-Methylphenol (o-Cresol)
ND
ug/1
11.
12/08/05
19:56
BET
95-48-7
3&4-Methylphenol
ND
ug/l
11.
12/08/05
19:56
BET
Naphthalene
ND
ug/l
11.
12/08/05
19:56
BET
91-20-3
2-Nitroaniline
ND
ug/l
53.
12/08/05
19:56
BET
88-74-4
3-Nitroaniline
NO
ug/l
53�
12108/05
19:56
BET
99-09-2
4-Nitroaniline
ND
ug/l
53.
12/08105
19:56
BET
100-01-6
Nitrobenzene
NO
ug/1
11.
12/08105
19:56
BET
98-95-3
2-Nitrophenal
ND
ug/1
11.
12/08/05
19:56
BET
88-75-5
4-Nitrophenal
ND
ug/l
53.
12/08/05
19:56
BET
100-02-7
N-Nitrosodimethylamine
NO
ug/l
11.
12/08/05
19:56
BET
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/1
11.
12/08/05
19:56
BET
621-64-7
N-Nitrosodiphenylamine
ND
ug/l
11.
12/08105
19:56
BET
86-30-6
Pentachlorophenol
NO
ug/l
53.
12/08/05
19:56
BET
87-86-5
Phenanthrene
ND
ug/l
11.
12/08105
19:56
BET
85-01-8
Phenol
ND
ug/1
11.
12/08/05
19:56
BET
108-95-2
Pyrene
NO
ug/l
11.
12/08/05
19:56
BET
129-00-0
1,2,4-Trichlorobenzene
ND
ug/l
11.
12/08/05
19:56
BET
120-82-1
2,4.5-Trichlorophenol
NO
ug/1
53.
12/08/05
19:56
BET
95-95-4
2.4,6-Trichlorophenol
ND
ug/1
11.
12/08105
19:56
BET
88-06-2
Nitrobenzene-d5 (S)
77
%
12/08/05
19:56
BET
4165-60-0
2-Fluorobiphenyl (S)
89
%
12/08/05
19:56
BET
321-60-8
Terphenyl-d14 (S)
172
9
12/08/05
19:56
BET
1718-51-0 1
Phenol-d5 (S)
47
%
12/08105
19:56
BET
4165-62-2
2-Fluorophenol (S)
55
%
12108/05
19:56
BET
367-12-4
2,4,6-Tribromophenol (S)
93
%
12/08/05
19:56
BET
118-79-6
Date: 12116/05
Page: 3 of 35
Asheville Certification II)s
REPORT OF LABORATORY ANALYSIS
Charlotte Certification
IN
NC Wastewater
40
NC Wastewater
12
NC Drinking Water
37712
This report shall riot be reproduced, except in full,
NC Drinking Water
37706
Sc
99030
without the written consent of Pace Analytical Services, Inc.
Sc
99006
FL NELAP
E87648
FL NELAP
E87627

011 /
AaceAnalyticala
www.pagaiabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Hunters ville, NC 28078
Phone: [phone]
Fax: 704,875.9091
Pace Analytical Services, Inc,
22257 Riverside Drive
Asheville, NC 28804
Phone., 828.254.7176
fax., 826.252.4618
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Lab Sample No: 926408667
Project Sample Number: 92108723-001 Date Collected: 12/01/05 09:00
Client Sample ID: GREY WATER
Matrix: Water
Date Received: 12/05105 10:45
Parameters
Results
Units Report Limit Analyzed By
CAS No, Qua] ReqLmt
Date Extracted
12/07105
12/07/05
GUMS Volatiles
GUMS VOCs by 8260
Method: EPA
8260
Acetone
86.
ug/l
25.
12/13/05 11:40 MSF
67-64-1
Benzene
NO
ug/l
5.0
12/13105 11:40 MSF
71-43-2
Bromobenzene
NO
ug/l
5.0
12/13/05 11:40 MSF
108-86.1
Bromochloromethane
NO
ug/l
5.0
12/13/05 11:40 MSF
74-97.5
Bromodichloromethane
NO
ug/l
5.0
12/13/05 11:40 14SF
75-27-4
Bromoform
NO
ug/l
5.0
12/13/05 11:40 MSF
75-25-2
Bromomethane
NO
ug/l
5.0
12/13/05 11:40 MSF
74-83-9
2-Butanone (MEK)
14.
ug/l
10.
12/13/05 11:40 MSF
78-93-3
n-Butylbenzene
NO
ug/l
5.0
12/13/05 11:40 MSF
104-51.8
sec- Butyl benzene
NO
ug/l
5.0
12/13/05 11:40 MSF
135-98.8
tert-Butylbenzene
NO
ug/l
5.0
12113/05 11:40 MSF
98-06-6
Carbon tetrachloride
NO
ug/l
5.0
12/13/05 11:40 MSF
56-23-5
Chlorobenzene
NO
ug/l
5.0
12/13105 11:40 MSF
108-90-7
Chloroethane
NO
ug/l
10.
12/13/05 11:40 MSF
75-00-3
Chloroform
NO
ug/l
5.0
12/13105 11:40 MSF
67-66-3
Chloromethane
NO
ug/l
5.0
12/13/05 11:40 MSF
74-87-3
2-Chlorotoluene
NO
ug/l
5,0
12/13/05 11:40 MSF
95-49-8
4-Chlorotoluene
NO
ug/l
5.0
12/13/05 11:40 MSF
106-43-4
1.2-Dibromo-3-chlorapropane
NO
ug/l
5.0
12/13/05 11:40 MSF
96-12-8
Dibromachloromethane
NO
ug/l
5.0
12/13/05 11:40 MSF
12448-1
1.2-Bibromoethane (EDB)
ND
ug/l
5.0
12/13/05 11:40 MSF
106,93-4
Dibromomethane
NO
ug/l
5.0
12/13/05 11:40 MSF
74-95.3
1,2-Dichlorobenzene
NO
ug/l
5.0
12/13/05 11:40 MSF
95-50-1
1.3-Dichlorobenzene
NO
ug/I
5.0
12/13105 11:40 MSF
541-73-1
1.4-Dichlorobenzene
NO
ug/l
5.0
12113/05 11:40 MSF
106-46-7
Di chl orodi fl uoromethane
NO
ug/l
5,0
12/13/05 11:40 MSF
75-71.8
1.1-Dichlaroethane
NO
ug/l
5.0
12/13/05 11:40 MSF
75-34-3
1.2-Dichloroethane
NO
ug/l
5.0
12/13105 11:40 MSF
107-06.2
1.1-Dichloroethene
NO
ug/l
5.0
12/13/05 11:40 MSF
75-35-4
ci s - 1, 2 - Di chl oroethene
ND
ug/l
5,0
12/13/05 11:40 MSF
15&59-2
trans - 1. 2 - Di chl oroethene
NO
ug/l
5.0
12/13/05 11:40 MSF
15&60-5
1.2-Dichloropropane
NO
ug/l
5.0
12/13/05 11:40 MSF
78-87-5
1,3-Dichloropropane
NO
u9/1
5.0
12/13/05 11:40 MSF
142-28-9
2.2-Dichloropropane
NO
ug/l
5.0
12/13/05 11:40 MSF
594-20-7
1.1-Dichloropropene
NO
ug/I
5.0
12/13/05 11:40 MSF
563-5&6
Date: 12/16/05
Page: 4 of 35
Agboville Certification II)s
NG Wastewater
REPORT
OF LABORATORY
ANALYSIS
Charlatt Certification IDs
40
NG Drinking Water 37719
This report shall not be reproduced,
except in full,
NC Wastewater 12
Sc 99030
without the written consent of Pace Analytical Services, Inc.
NG Drinking Water 37706
FL NELAP E87648
Sc 99006
FL NELAP E87627

-----�,rdceAnalyticalo
www.pacefabs.com
Lab Sample No: 926408667
Client Sample ID: GREY WATER
Pace Anaiytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntorsville, AtC28078
Phone: 704,875.9092
Fax. [phone]
Pace AnalytiCif Services, Inc.
2225 Pive D a
LZ4
rs] .
Asheville, NC 28 0
Phone.- 828.254.7176
Fax. [phone]
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Project Sample Number: 92108723-001 Date Collected: 12/01/05 09:OU
Matrix: Water Date Received: 12/05/05 10:45
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLmt
cis-1,3-Dichloropropene
ND
ug/l
5.0
12113/05
11:40
MSF
10061-01-5
trans-1.3-Dichloropropene
ND
ug/l
5.0
12/13/05
11:40
MSF
10061-02-6
Diisopropyl ether
NO
ug/1
5.0
12/13/05
11:40
MSF
108-20-3
Ethylbenzene
ND
ug/l
5.0
12/13/05
11:40
MSF
100-41-4
Hexachloro-1.3-butadiene
NO
ug/1
5.0
12/13/05
11:40
MSF
87-68-3
2-Hexanone
NO
ug/l
10.
12/13/05
11:40
MSF
591-78.6
isopropylbenzene (Cumene)
NO
ug/l
5.0
12/13/05
11:40
MSF
98-82-8
p-Isopropyltoluene
6.8
ug/l
5.0
12113/05
11:40
MSF
99-87-6
Methylene chloride
NO
ug/l
5.0
12113/05
11:40
MSF
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/l
10.
12/13105
11:40
MSF
108-10-1
Methyl-tert-butyl ether
NO
ug/1
5.0
12113/05
11:40
MSIF
1634-04-4
Naphthalene
NO
ug/l
5.0
12/13105
11:40
MSF
91-20-3
n-Propylbenzene
ND
ug/l
5.0
12/13/05
11:40
MSF
103-65-1
Styrene
NO
ug/1
5.0
12/13/05
11:40
MSF
100-42-5
1.1.1,2-Tetrachloroethane
ND
ug/1
5.0
112113/05
11:40
MSF
630-20-6
1,1,2.2-Tetrachloroethane
ND
ug/1
5.0
12/13/05
11:40
MSF
79-34-5
Tetrachlorcethene
ND
ug/l
5.0
12/13/05
11:40
MSF
127-18-4
Toluene
NO
ug/l
5.0
12/13/05
11:40
MSF
108-88-3
1.2,3-Trichlorobenzene
IND
ug/l
5.0
12/13/05
11:40
MSF
87-61-6
1.2,4-Trichlorobenzene
NO
ug/1
5.0
12/13/05
11:40
MSF
120-82-1
1,1.1-Trichloroethane
ND
ug/l
5.0
12/13/05
11:40
MSF
71-55-6
1.1.2-Trichloroethane
NO
ug/1
5.0
12/13/05
11:40
MSF
79-00-5
Trichloroethene
NO
ug/1
5.0
12/13/05
11:40
MSF
79-01-6
Trichlorofluoromethane
NO
ug/l
10.
12/13/05
11:40
MSF
75-69-4
1.2,3-Trichloropropane
ND
ug/l
5.0
12/13/05
11:40
MSF
96-18-4
1,2.4-Trimethylbenzene
ND
ug/1
5.0
12113/05
11:40
MSF
95-63-6
1.3.5-Trimethylbenzene
ND
ug/l
5.0
12/13/05
11:40
MSF
108-67-8
Vinyl acetate
ND
ug/1
10.
12113/05
11:40
MSF
108-05-4
Vinyl chloride
ND
ug/l
5.0
12/13/05
11:40
MSF
75-01-4
Xylene (Total)
ND
ugil
5.0
12/13/05
11:40
MSF
1330-20-7
m&p-Xylene
NO
ug/1
10.
12/13/05
11:40
MSF
o-Xylene
ND
ug/1
5.0
12/13/05
11:40
MSF
95-47-6
Toluene-d8 (S)
96
%
12/13/05
11:40
MSF
2037-26-5
4-Bromofluorobenzene (S)
104
%
12/13/05
11:40
MSF
460-00-4
Dibromofluoromethane (S)
90
%
12/13/05
11:40
MSF
1868-53-7
1.2-Dichloroethane-d4 (S)
85
%
12/13/05
11:40
MSF
17060-07-0
Date: 12/16/05
Asheville Certification ID
NC Wastewater
40
NC Drinking Water
37712
SIC
99030
Fl- NELAP
E87648
REPORT OF LABORATOR. Y ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,np
Page: 5 of 35
Charlotte CeEtificatign IN
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

ap
P 'aceAnalyticale
www.pacelabs.com
PARMETER FOOTNOTES
Method 9071B modified to use ASE.
Pace Analytical Services, Ine.
9800 Kincey Avenue, Suite 100
Huntersville, NC 26078
Phone: [phone]
Fax., 704.875-9091
Pace Analytical Services, Inc.
2226 Riverside Drive
Asheville, NC 28804
Phor7e, 828,254.7176
Fax [phone]
Lab Project Number: 92108723
Client Project 10: Grey Water Analysis
All pfl, Free Chlorine. Total Chlorine and Ferrous Iron analyses conducted Outside of EPA recommended immediate
hold time.
Depending on the moisture content the PRLs can be elevated for all sail samples reported on a dry weight basis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) Surrogate
[I] Base/neutral surrogate recovery outside of control limits. The data was accepted based on valid recovery of
remaining two base/neutral surrogates.
Date: 12/16105
Meville Certification los
NG Wastewater
40
NG Drinking Water
37712
SC
99030
FL NELAP
E87648
REPORT OF LABORATORY AN A LYS IS
VR%
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, InG.
Page: 6 of 35
CharlQlLe Certification lDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

/Ow -MR,
a ceAnalyticale
WWW.Parcelahs.cam
OC Batch: 143857
QC Batch Method; EPA 3610
Associated Lab Samples: 926408667
METHOD BLANK: 926419458
Associated Lab Samples: 926408667
Pace Analytical Services, Inc. Pace Analyfait Serv�Fas, Inc.
9800 Kincey Avenue, Suite 100 2226 Riverside Nrive -
Huntersville, NC28078 Ast7evillo, NC 28804
Phone: [phone] Phone: [phone]
Fax., 704.875.9091 Fax, 828.252.4618
QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Analysis Method: EPA 8270
Analysis Description: Semivolatile Organics
Blank
Reporting
Parameter -
Units
Result
Limit Footnotes-
Acenaphthene
ug/l
NO
10.
Acenaphthylene
ug/I
NO
10.
Aniline
ug/l
ND
10.
Anthracene
ug/l
NO
10.
Benzo(k)fl uoranthene
ug/l
NO
10.
Benzo(b)fluoranthene
ug/l
NO
10.
Benzo(a)anthracene
ug/I
NO
10.
Benzoic acid
ug/l
NO
50.
Benzo(g,h.i)perylene
ug/l
NO
10.
Benzyl alcohol
ug/l
NO
20.
Benzo(a)pyrene
ug/1
NO
10.
4-Bromophenylphenyl ether
ug/l
NO
10.
Butylbenzylphthalate
Ug/I
NO
10.
4-Chloro-3-methylphenal
ug/l
NO
20.
4-Chloroaniline
ug/l
NO
20.
bis(2-Chloroethoxy)methane
ug/l
NO
10.
bis(2-Chloroethyl) ether
ug/l
NO
10.
bis(2-Chlorolsopropyl) ether
ug/l
NO
10.
2-Chloronaphthalene
ug/1
NO
10.
2-Chlorophenol
ug/l
NO
10.
4-Chlorophenylphenyl ether
Ug/l
NO
10.
Chrysene
ug/l
ND
10.
Dibenz(a.h)anthracene
ug/l
NO
10.
Dibenzofuran
ug/1
NO
10,
1.2-Dichlorobenzene
ug/l
NO
10.
1,3-Dichlorobenzene
ug/l
NO
10.
1.4-Dichlorobenzene
ug/l
NO
10.
3.3'-Dichlorobenzidine
ug/1
ND
20.
2,4-Dichlorophenol
ug/I
NO
10.
Diethylphthalate
ug/I
NO
10.
2,4-Dimethylphenol
ug/l
NO
10.
Date: 12/16/05
A-sheville Certification 10s
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYT S IS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc.
Page: 7 of 35
Charlotte Certification 1Ds
NG Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Services, Inc. Pace Analyfical Services, Inc.
9800 Kincey Avenue, Suite 100 2226 Riverside Drive
Huntersville, NC 28078 Astieville, IVC 28804
Phone: [phone] Phooe., 828.254.7176
Analvticalo Fax., 704.875.9091 Fax., 828,252.4618
www.pacelahs.canr QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project M Grey Water Analysis
ML[HUO BLANK: 926419458
Associated Lab Samples: 926408667
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Dimethylphthalate
ug/l
ND
10.
Di-n-butylphthalate
ug/1
ND
10.
4,6-13initro�2-methylphenol
ug/l
ND
50.
2.4-Dinitrophenol
ug/l
ND
50.
2.4-Dinitrotoluene
ug/l
ND
10.
2.6-Dinitrotoluene
ug/l
ND
10.
01 - n - octyl phthal ate
ug/l
ND
10.
1. 2 - Di phenyl hydrazi ne
ug/l
ND
20.
bi s (2 - Ethyl hexyl ) phthal ate
ug/l
ND
10.
Fluoranthene
ug/l
ND
10.
Fluorene
ug/1
ND
10.
Hexachl oro - 1. 3 - but adi ene
ug/l
ND
10.
Hexachl orobenzene
U911
ND
10,
Hexachlorocyclopentadiene
ug/l
ND
10.
Hexachloroethane
ug/l
ND
10.
Indeno(l.2,3-cd)pyrene
ug/l
ND
10.
Isophorone
ug/l
ND
10.
2-Methylnaphthalene
ug/1
ND
10.
2-Methylphenol (o-Cresol)
ug/l
ND
10.
3&4-Methyl phenol
ug/l
ND
10.
Naphthalene
ug/l
ND
10.
2-Nitroaniline
ug/l
ND
50.
3-Nitroaniline
ug/l
ND
50.
4-Nitroaniline
ug/l
ND
50.
Nitrobenzene
ug/1
ND
10.
2-Nitrophenol
ug/l
ND
10.
4-Nitrophenol
ug/l
ND
50.
N-Nitrosodimethylamine
ug/l
ND
10.
N-nitroso-di-n-propylamine
ug/l
ND
10.
N-Nitrosodiphenylamine
ug/l
ND
10.
Pentachlorophenol
ug/l
ND
so.
Phenanthrene
ug/l
ND
10.
Phenol
ug/l
ND
10.
Pyrene
ug/1
ND
10.
1. 2,4 -Tri chl orobenzene
ug/l
ND
10.
2.4. 5 - Tri chi orophenol
ug/l
ND
50.
Date: 12/16/05
Asheville C rtification ID
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FIL NELAP E87648
I W&
REPORT OF LABORATORY ANALTOIS
This report shall not be reproduced, except in full,
without the written consent of Pace AnaMical Services, Inc.
Page: 8 of 35
Karlotte Certification lDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

0�weAnalytical
_-'-V a
www.pacelabs.com
METHOD BLANK: 926419458
Associated Lab Samples: 926408667
Pace Analyticai Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
QUALITY CONTROL DATA
Pace Analytical Servifes, Inc.
2225 Rivers7 , de Nve -
Ashevi/16, NC28804
Phoue: 828.254- 7176
Fax., 828.252.4618
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Blank Reporting
Parameter
Units
Result Limit Footnotes
2,4.6-Trichlorophenol
ug/l
ND 10.
Nitrobenzene-d5 (S)
65
2-Fluorobiphenyl (S)
%
62
Terphenyl-c[14 (S)
%
76
Phenol-d5 (S)
%
29
2-Fluorophenol (S)
%
43
2.4.6-Tribromophenol (S)
1
63
LABORATORY CONTROL SAMPLE: 926390915
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Acenaphthene
ug/l
50.00
34.37
69
Acenaphthylene
ug/l
50.00
35.28
71
Aniline
ug/l
50.00
56.79
114
Anthracene
ug/l
50.00
37.83
76
Benzo(k) fluoranthene
ug/l
50.00
39.95
80
Benzo(b)fluoranthene
ug/l
50.00
39.35
79
Benzo(a)anthracene
ug/l
50.00
36.67
73
Benzoic acid
ug/l
50.00
10.94
22
Senzo(g.h,i)perylene
ug/l
50.00
18.10
36
Benzyl alcohol
ug/l
50.00
46.96
94
Benzo(a)pyrene
ug/l
50.00
39.07
78
4-Bromophenylphenyl ether
ug/l
50.00
35.37
71
Butylbenzylphthalate
ug/l
50.00
35.43
71
4-Chloro-3-methylphenol
ug/l
50.00
34.61
69
4-Chloroaniline
ug/l
50.00
31.10
62
bis(2-Chloroethoxy)methane
ug/l
50.00
32.84
66
bis(2-Chloroethyl) ether
ug/l
50.00
44.29
89
bis(2-Chloroisopropyl) ether
ug/l
50.00
40.88
82
2-Chloronaphthalene
ug/l
50.00
32.90
66
2-Chlorophenol
ug/l
50.00
36.57
73
4-Chlorophenylphenyl ether
ug/l
50.00
34.99
70
Chrysene
ug/l
50.00
36.34
73
Dibenz(a,h)anthracene
ug/l
50.00
27.28
55
Date: 12/16105
shaville Certification Ills
NC Wastewater
40
NG Drinking Water
37712
SC
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALY, SIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 9 of 35
Charlotte Certification IDs
NG Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Services, Jac, Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersvil/6, NC 28078 Asheville, NC 28804
Phone: [phone] Phviie: 828.254.7176
Analvficalo Fax., 704.875. 9091 fax.' 828.252,4618
www,pacalabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 926390915
Spike
LCS
LCS
Parameter
Units
Cone,
Result
% Rec
Dibenzofuran
ug/l
50.00
34.69
69
1.2-Dichlorobenzene
ug/l
50.00
27.73
56
1.3-Dichlorobenzene
uq/l
50.00
19.91
40
1,4-Dichlorobenzene
ug/l
50.00
22.89
46
3,3' - Of chl orobenzi dine
ug/l
100.00
28.56
29
2.4-Dichlarophenol
ug/l
50.00
32.77
66
Diethylphthalate
ug/l
50.00
34.86
70
2.4 - Di methyl phenol
ug/l
50.00
32.22
64
Dimethylphthalate
ug/l
50.00
34.77
70
Di - n - butyl phthal ate
ug/l
50�00
39.40
79
4.6 - Of n! tro - 2 - methyl phenol
ug/l
50.00
37.84
76
2.4-Dinitrophenol
ug/l
50.00
37.19
74
2.4-Dinitrotoluene
ug/l
50�00
35.43
71
2,6-Dinitrotoluene
ug/l
50.00
36.46
73
Di-n-octylphthalate
ug/l
50.00
35.34
71
1,2-Diphenylhydrazine
ug/l
50.00
32.48
65
bis(2-Ethylhexyl)phthalate
ug/l
50.00
38.20
76
Fluoranthene
ug/l
50.00
37.42
75
Fluorene
ug/l
50.00
34.73
70
Hexachl o ro - 1, 3 - but adi ene
ug/l
50.00
22.38
45
Hexachlorobenzene
ug/l
50�00
35.57
71
Hexachl orocycl opentadi ene
ug/l
50.00
23.84
48
Hexachloroethane
ug/l
50.00
23.33
47
Indeno(I.2,3-cd)pyrene
ug/l
50.00
27.61
55
Isophorone
ug/l
50.00
33.88
68
2-Methyl naphthalene
ug/l
50.00
30.29
61
2-Methylphenol (o-Cresol)
ug/l
50.00
47�89
96
3&4-Methyl phenol
ug/l
50.00
43.07
86
Naphthalene
ug/l
50.00
30.41
61
2-Nitroaniline
ug/l
50.00
32.58
65
3-Nitroaniline
ug/l
50.00
33.35
67
4-Nitroaniline
ug/l
50.00
37.46
75
Nitrobenzene
ug/l
50.00
32.82
66
2-Nitrophenol
ug/l
50.00
32.93
66
4-Nitrophenol
ug/l
50.00
13.82
28
N-Nitrosodimethylamine
ug/l
50.00
8.321
17
N-Nitroso-di-n-propylamine
ug/l
50.00
42.42
85
Date: 12/16/05
Asheville Certification 10s
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Footnotes
REPORT
III OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, InG.
Page: 10 of 35
Charlotte Certification ID
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ceAnalytical@
www.pacelabs.com
LABORATORY CONTROL SAMPLE: 926390915
Parameter
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1.2.4-Trichlorobenzene
2,4,5-Trichlorophenol
2.4.6-TrichlorDphenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d5 (S)
2-Fluorophenol (S)
2.4.6-Tribromophenol (S)
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, PIC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Spike
LCS
LCS
Units
Conc.
Result
%1 Rec
ug/I
50.00
37.18
74
ug/l
50.00
39.95
80
ug/I
50.00
37.61
75
ug/1
50.00
28.00
56
ug/l
50.00
37,48
75
ug/l
50.00
25.62
51
ug/I
50.00
36.58
73
ug/l
50.00
35.31
71
68
74
81
38
65
78
LABORATORY CONTROL SAMPLE: 926398090
Parameter
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(k)fl uoranthene
Benzo(b) fluoranthene
Benzo(a)anthracene
Benzoic acid
Benzo(g.h.i)perylene
Benzyl alcohol
Benzo(a)pyrene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
Date 12/16/05
Asheville Certification IDS
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
Spike
LCS
LCS
Units
Conc.
Result
% Rec
ug/l
50.00
36.44
73
ug/l
50.00
37.01
74
ug/l
50.00
36.29
73
ug/l
50.00
38.89
78
ug/l
50.00
41.05
82
ug/l
50.00
33.61
67
ug/l
50.00
39.69
79
ug/1
50.00
11.58
23
ug/l
50.00
33.53
67
ug/l
50.00
25.51
51
ug/l
50.00
41.15
82
ug/l
50.00
34.90
70
ug/l
50.00
39.00
78
ug/l
50.00
35.47
71
ug/l
50.00
40.07
80
ug/l
50.00
32.61
65
ug/I
50.00
31.31
63
Pace Analyflual Services, Inc.
2225 Rivers7de &ive
Asheville, NC28804
Phone: 828,254- 7176
fax. [phone]
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Footnotes
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 11 of 35
Charlotte Certification IDS
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

,.�7�eAnalytical
www.pac.-Iabs.com
I
LAUUKAIURY CONTROL SAMPLE: 926398090
Pace Analytical Services, Inc,
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: 704.875,9092
Fax: [phone]
QUALITY CONTROL DATA
Spike
LCS
LCS
Parameter _
Units
Conc.
Result
% Rec
bis(2-Chloroisopropyl) ether
ug/l
50.00
29.89
60
2-Chloronaphthalene
ug/l
50-00
35.65
71
2-Chlorophenol
ug/l
50.00
29.34
59
4-Chlorophenylphenyl ether
ug/l
50.00
36.83
74
Chrysene
ug/l
50.00
38.88
78
Dibenz(a,h)anthracene
ug/l
50.00
38.03
76
Dibenzofuran
ug/l
50.00
35.63
71
1.2-Dichlorobenzene
ug/l
50.00
25.46
51
1.3-Dichlorobenzene
ug/l
50.00
24.26
48
1,4-Dichlorobenzene
ug/l
50.00
24.70
49
3.3'-Dichlorobenzidine
ug/l
100.00
31.93
32
2,4-Dichlorophenol
ug/l
50.00
33.78
68
Diethylphthalate
ug/l
50�00
38.21
76
2.4-Dimethylphenol
ug/l
50.00
34.55
69
Dimethylphthalate
ug/l
50.00
35.88
72
Di-n-butylphthalate
ug/l
50.00
44.67
89
4,6-Dinitro-2-methylphenol
ug/l
50.00
37.53
75
2.4-Dinitrophenol
ug/l
50.00
35.87
72
2.4-Dinitrotoluene
ug/l
50.00
37.17
74
2.6-Dinitrotoluene
ug/l
50.00
36.43
73
Di-n-octylphthalate
ug/l
50.00
39.30
79
1.2-Diphenylhydrazine
ug/l
50.00
33.14
66
bis(2-Ethylhexyl)phthalate
ug/l
50.00
41�46
83
Fluoranthene
ug/l
50.00
38,93
78
Fluorene
ug/l
50.00
37.21
74
Hexachloro-1,3-butadiene
ug/l
50.00
23.45
47
Hexachlorobenzene
ug/l
50-00
34.43
69
Hexachlorocyclopentadiene
ug/l
50.00
24.55
49
Hexachloroethane
ug/l
50-00
22.59
45
Indeno(I.2.3-cd)pyrene
ug/l
50.00
36.90
74
Isophorone
ug/l
50.00
39,40
79
2-Methylnaphthalene
ug/l
50.00
33.76
68
2-Methylphenol (o-Cresol)
ug/l
50.00
27.74
56
3&4-Methylphenol
ug/l
50.00
24.22
48
Naphthalene
ug/l
50.00
30.51
61
2-Nitroaniline
ug/l
50�00
34.88
70
3-Nitroaniline
ug/l
50.00
39.58
79
Date: 12/16J05
Asheville Certification IDS
NG Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NO 28804
Phooe., 828.254.7176
Fm: 828.252.4618
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Footnotes
REPORT OF LABORATORY ANALY, SIS
This report shall not be reproduced, except in full,
without the written consent of Paco AnalOcal Services, Inc.
O!i� -
Page: 12 of 35
Chario Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
I'L NELAP
E87627

1g, I
/ '�,�eAnalytical@
WWW.Pacelabs�com
LABORATORY CONTROL SAMPLE: 926398090
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: 704- 875,9092
Fax. [phone]
QUALITY CONTROL DATA
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec
4-Nitroaniline
ug/l
50.00
41.70
83
Nitrobenzene
ug/l
50.00
31.90
64
2-Nitrophenol
ug/l
50.00
30.99
62
4-Nitrophenol
ug/l
50.00
12�33
25
N-Nitrosodimethylamine
ug/I
50.00
19.85
40
N-Nitroso-di-n-propylamine
ug/l
50.00
31.58
63
N-Nitrosodiphenylamine
ug/l
50.00
38.38
77
Pentachlorophenol
ug/1
50.00
36.66
73
Phenanthrene
ugll
50.00
37.60
75
Phenol
ug/l
50.00
12,52
25
Pyrene
ug/l
50.00
40.82
82
1,2.4-Trichlorobenzene
DO
50.00
27.03
54
2.4,5-Trichlorophenol
ug/l
50.00
37.60
75
2,4,6-Trichlorophenol
uq/l
50.GG
36.35
73
Nitrobenzene-d5 (S)
70
2-Fluorobiphenyl (S)
82
Terphenyl-d14 (S)
86
Phenol-d5 (S)
27
2-Fluorophenol (S)
41
2,4,6-Tribromophenol (S)
74
LABORATORY CONTROL SAMPLE: 926419466
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Rec
Acenaphthene
ug/l
50.00
34.41
69
Acenaphthylene
ug/l
50.00
35.43
71
Aniline
ug/l
50.00
35.64
71
Anthracene
ug/l
50.00
37.43
75
Benzo(k)fluoranthene
ug/l
50.00
36.07
72
Benzo(b)fluorantherie
ug/l
50.00
34.14
68
Benzo(a)anthracene
ug/l
50.00
37.50
75
Benzoic acid
ug/l
50.00
14.50
29
Benzo(g,h,i)perylene
ug/l
50.00
30.82
62
Benzyl alcohol
ug/l
50.00
27.24
54
Benzo(a)pyrene
ug/l
50.00
38.27
76
Date: 12/16/05
Asheville Certification IDS
NC Wastewater 40
NC Drinking Water 37712
so 99030
FIL NELAP E87648
Pace Analytical Servipas, Inc.
2225 Riverside &rive
Asheville, NC28804
Phooe., 828.254.7176
Fa.x, 828.252.4618
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Footnotes
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shelf not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 13 of 35
Charlotte Certification IDS
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FIL NELAP E87627

Pace Analytical Services, Inc, Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, IVC 28804
Phone: 704,875.9692 Phone: [phone]
Analvtical" Fax., 704.875.9091 Fay., B28.252.4618
www.pacelahs.com QUALITY CONTROL DATA
LAtSURAJURY CONTROL SAMPLE: 926419466
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Rec
4-Bromophenylphenyl ether
ug/l
50.00
32.87
66
Butylbenzylphthalate
ug/l
50.00
36.53
73
4-Chloro-3-methylphenol
ug/1
50.00
34.32
69
4-Chloroaniline
ug/l
50-00
40.47
81
bis(2-Chloroethoxy)methane
ug/l
50-00
30.51
61
bis(2-Chloroethyl) ether
ug/l
50.00
29.50
59
bis(2-Chloroisopropyl) ether
ug/l
50.00
27.66
55
2-Chloronaphthalene
ug/l
50.00
32.67
65
2-Chlorophenol
ugll
50.00
27.19
54
4-Chlorophenylphenyl ether
ug/l
50.00
35�47
71
Chrysene
ug/l
50.00
35.82
72
Dibenz(a,h)anthracene
ug/l
50.00
34.34
69
Dibenzofuran
ug/l
50.00
34.18
68
1,2-Dichlorobenzene
ug/l
50.00
23.23
46
1.3-Dichlorobenzene
ug/l
50.00
21.97
44
1.4-Dichlorobenzene
ug/l
50.00
22.80
46
3,3'-Dichlorobenzidine
ugll
100.00
33.76
34
2.4-Dichlorophenol
ug/1
50.00
31.37
63
Diethylphthalate
ug/1
50.00
36.76
74
2.4-Dimethylphenol
ug/l
50.00
31.63
63
Dimethylphthalate
ug/l
50.00
34.25
68
Di-n-butylphthalate
ug/l
50,00
39.29
79
4,6-Dinitro-2-methylphenol
ug/l
50.00
36.51
73
2,4-Dinitrophenol
ug/l
50.00
34.92
70
2.4-Dinitrotaluene
ug/l
50.00
36.29
73
2.6-Dinitrotoluene
ug/l
50.00
35.41
71
Di-n-octylphthalate
ug/l
50.00
37.67
75
1.2-Diphenylhydrazine
ug/l
50,00
32.99
66
bis(2-Ethylhexyl)phthalate
ug/l
50.00
38.09
76
Fluoranthene
ug/1
50.00
37.05
74
Fluorene
ug/l
50.00
35.58
71
Hexachloro-1,3-butadiene
ug/l
50.00
20.55
41
Hexachlorobenzene
ug/l
50.00
32.89
66
Hexachlorocyclopentadiene
ug/l
50.00
21.65
43
Hexachloroethane
ug/l
50.00
21.17
42
Indeno(1,2,3-cd)pyrene
ug/l
50.00
33.95
68
Isophorone
ugll
50.00
36.72
73
Date: 12/16/05
Asheville Certificatinn IN
NC Wastewater
40
NC Drinking Water
37712
3C
99030
FIL NELAP
E87648
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 14 of 35
Charlotte Certification ID
NC Wastewater 12
NG Drinking Water 37706
SC 99006
FL NELAP E87627

051",
"I"WeAnalytical
www.pacelabs.com
LABORATORY CONTROL SAMPLE: 926419466
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, PIC 28078
Phone: [phone]
Fax., 704 875� 9091
QUALITY CONTROL DATA
Spike
LOS
LOS
Parameter
Units
Conc.
Result
Rec
2-Methylnaphthalene
ug/l
50.00
30.85
62
2-Methylphenol (o-Cresol)
Ug/l
50.00
25.60
51
3&4-Methylphenol
ug/l
50.00
23.87
48
Naphthalene
ug/l
50.00
27.01
54
2-Nitroaniline
Ug/l
50.00
33.52
67
3-Nitroaniline
Ug/l
50.00
39.65
79
4-Nitroaniline
Ug/l
50.00
41.58
83
Nitrobenzene
ug/l
50.00
29.26
58
2-Nitrophenol
ug/l
50.00
28.02
56
4-Nitrophenol
Ug/l
50.00
14.33
29
N-Nitrosodimethylamine
Ug/l
50.00
20.34
41
N-Nitroso-di-n-propylamine
Ug/l
50.00
30.56
61
N-Nitrosodiphenylamine
Ug/l
50.00
38.08
76
Pentachloropherol
ug/l
50.00
35.97
72
Phenanthrene
ug/l
50.00
36.36
73
Phenol
ug/l
50.00
12.99
26
Pyrene
ug/l
50.00
37.67
75
1.2.4-Trichlorobenzene
ug/l
50.00
23.12
46
2.4,6-Trichlorophenol
ug/l
50�00
35.46
71
2,4.6-Trichlorophenol
ug/l
50.00
35.29
71
Nitrobenzene-d5 (S)
61
2-Fluorobiphenyl (5)
73
Terphenyl-d14 (S)
77
Phenol-d5 (S)
27
2-Fluorophenol (S)
43
2.4.6-Tribromophenol (S)
69
14ATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926390923 926390931
Parameter
Acenaphthene
4-Chloro-3-methylphenol
2-Chlorophenol
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Date: 12/16/05
Asheville Certification IDs
NC Wastewater
40
NG Drinking Water
37712
Sc
99030
FL NELAP
E87648
926387739
Units
Result
ug/l
1.778
ug/l
0
ug/l
0
Uq/l
0
ug/l
0
Pace Analytical Services, Inc.
2225 Riverside 130ve
Asheville, NC28804
Phone: [phone]
Fax., 828.252.46 18
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Footnotes
Spike
MS
MSO
Ms
MSO
Conc.
Result
Result
% Rec %
Rec
100.00
68.41
69.81
67
68
100.00
67.04
67.92
67
68
100.00
64.41
65.78
64
66
100.00
43.04
41-68
43
42
100.00
69.46
71.47
70
72
REPORT OF LABORATORY ANALY SIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
RPD Footnotes
2
1
2
3
3
Page: 15 of 35
Charlotte Certificat-lonlD
NC Wastewater
12
NC Drinking Water
37706
SO
99006
FL NELAP
E87627

Pace Analytical Services, Inc. Pace Analyfical Services, Inc.
9800 Kincey Avenue, Suite 100 222Y Riverside Drive
Huntersville, NC 28078 Asheville, NC28804
Phone., 704.875.9092 Phofle., 828.254.7176
Analocal" Fax.'704.875.9091 fx* 828152.4618
www.pacelabs.com QUALITY CONTROL DATA
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926390923 926390931
Parameter
4-Nitrophenol
N-Nitroso-di-n-propylamine
Pentachlorophenol
Phenol
Pyrene
1.2,4-Trichlorobenzene
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d5 (S)
2-Fluorophenol (S)
2,4.6-TribroTnophenol (S)
SAMPLE DUPLICATE: 926419490
926387739
Units
Result
ug/1
0
ug/1
0
ug/l
0
ug/1
0
ug/l
0
ug/I
0
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Spike
MS
MSD
MS
MSD
Conc,
Result
Result
% Rec Rec
100.00
25.50
27.48
26
28
100.00
68.17
68.34
68
68
100.00
86.42
88.37
86
88
100.00
34.61
36.47
35
36
100.00
77.13
78.90
77
79
100.00
50.41
49.16
50
49
62
66
72
71
81
84
30
31
39
43
79
83
926411224
DUP
Parameter
Units
Result
Result
RPD Footnotes
Acenaphthene
ug/l
NO
ND
NC
Acenaphthylene
ug/l
ND
ND
NC
Aniline
ug/l
ND
ND
NC
Anthracene
ug/l
ND
ND
NC
Senzo(k)fluoranthene
ug/l
ND
ND
NC
Benzo(b)fluoranthene
ug/I
NO
No
NC
Benzo(a)anthracene
ug/l
NO
ND
NC
Benzoic acid
ug/l
ND
ND
NC
Benzo(g,h,i)perylene
ug/l
ND
ND
NC
Benzyl alcohol
ug/l
ND
NO
NC
Benzo(a)pyrene
ug/I
NO
ND
NC
4-Bromophenylphenyl ether
ug/l
ND
ND
NC
Butylbenzylphthalate
ug/l
ND
NO
NC
4-Chloro-3�methylphenol
ug/l
NO
ND
NC
4-Chloroaniline
ug/l
NO
NO
NC
bis(2-Chloroethoxy)methane
ug/l
NO
NO
NC
bis(2-Chloroethyl) ether
ug/I
NO
NO
NC
bis(2-Chlaroisopropyl) ether
ug/l
ND
ND
NC
2-Chloronaphthalene
ug/l
ND
ND
NC
Date: 12/16/05
A89ville Certification IDs
NG Wastewater 40
NC Drinking Water 37712
Sc 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, excep; in7ll,
without the written consent of Pace Analytical Services, Inc.
RPD Footnotes
7
0
2
5
2
3
Page: 16 of 35
Gbarigite Certification IDs
NG Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

Pace Analytical Services, Inc. Pace Analytical Services, h7c.
9800 Kincey Avenue, Suite 100 222.5 Riversfdo Drive ,
Huntersville, NC 28078 Asheville, NC28804
Phone: [phone] Phofle: 828.254.7176
Analytical' Fax., 704.875.9091 Fax., 828.252.4618
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
SAMPLE DUPLICATE: 926419490
926411224
CUP
Parameter
Units
Result
Result
RPD
2-Chlorophencil
ug/l
NO
NO
NC
4-Chlorophenylphenyl ether
ug/l
NO
NO
NC
Chrysene
ug/l
NO
ND
NC
Dibenz(a,h)anthracene
ug/l
NO
NO
NC
Dibenzofuran
ug/l
NO
NO
NC
1,2-Dichlorobenzene
ug/l
NO
NO
NC
1,3-Dichlorobenzene
ug/l
NO
NO
NC
1,4-Dichlorobenzene
ug/l
NO
RD
NC
3,3'-Dichlorobenzidine
ug/I
NO
NO
NC
2,4-Dichlarophenol
ug/l
NO
NO
NC
Diethylphthalate
ug/1
No
NO
NC
2,4.Dimethylphenol
ug/l
NO
NO
NC
Dimethylphthalate
ug/1
NO
NO
NC
Di-n-butylphthalate
ug/1
NO
ND
NC
4,6-Dinitro-2-methylphenol
ug/l
NO
NO
NC
2,4-Dinitrophenol
ug/1
NO
NO
NC
2,4-Dinitrotoluene
ug/l
No
ND
NC
2,6-Dinitrotoluene
ug/l
ND
NO
NC
Di-n-octylphthalate
ug/l
ND
NO
NC
1,2-Diphenylhydrazine
ug/l
NO
NO
NC
bis(2-Ethylhexyl)phthalate
ug/l
NO
NO
NC
Fluoranthene
ug/l
NO
NO
NC
Fluorene
ug/l
NO
NO
NC
Hexachloro-1.3-butadiene
ug/l
NO
NO
NC
Hexachlorobenzene
ug/l
NO
NO
NC
Hexachlorocyclopentadiene
ug/l
NO
NO
NC
Hexachloroethane
ug/l
NO
NO
NC
Indeno(1,2,3-cd)pyrene
ug/l
NO
NO
NC
Isophorone
ug/l
ND
NO
NC
2-Methylnaphthalene
ug/l
NO
NO
NC
2-Methylphenol (o-Cresol)
ug/l
NO
NO
NC
384-Methylphenol
ug/l
NO
NO
Nc
Naphthalene
ug/l
NO
NO
NC
2-Nitroaniline
ug/l
NO
NO
NC
3-Nitroaniline
ug/l
NO
NO
NC
4-Nitroariline
ug/l
NO
NO
NC
Nitrobenzene
ug/l
NO
NO
NC
Date: 12/16105
Asheville Certification IDs
NG Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 17 of 35
Charlotte CertificaticII10s
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

AP
ace Analytical"
www'Paceiabs,com
SAMPLE DUPLICATE: 926419490
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite too
Huntersville, NC 28078
Phone: [phone]
Fax [phone]
QUALITY CONTROL DATA
9264112?4
DUP
Parameter
Units
Result
Result
2-Nitrophenol
ug/l
ND
NO
4-Nitrophenol
ug/l
ND
NO
N-Nitrosodimethylamine
ug/l
NO
NO
N-NitroSG-di-n-propylamine
ug/l
ND
NO
N-Nitr'osodiphenylamine
ug/l
NO
ND
Pentachlorophenol
ug/l
ND
NO
Phenanthrene
ug/l
NO
ND
Phenol
ug/I
NO
NO
Pyrene
ug/I
NO
NO
1.2.4-Trichlorobenzene
ug/l
ND
NO
2.4.5-Trichlorophenol
ug/l
NO
NO
2,4,6-Trichlorophenol
ug/l
ND
ND
Nitrobenzene-d5 (S)
%
54
59
2-Fluorobiphenyl (S)
z
52
60
Terphenyl-d14 (S)
%
79
77
Phenol-cI5 (S)
%
28
27
2-Fluorophenol (S)
%
39
41
2,4,6-Tribromophenol (S)
60
63
Date: 12/16/05
Ashaville Certification ID
NC Wastewater
40
NC Drinking Water
37712
Sc
99030
FL NELAP
E87648
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, IVC 28804
Phone., 828.254.7176
Fax., 828.252.4618
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
RPD Footnotes
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
a WO
REPORT OF RABORATORY ANALTOIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 18 of 35
Charlotte Certification ID
NG Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

Pace Analytical Services, Inc. Pace Analytical Services, h7c.
9800 Kincey Averrue, Suite 100 2225 RiverOde Drive,
Huntersville, IVC 28078 Mevi]16, NC 28804
Phone: [phone] Phone: 828,254.7176
Analyficale Fax: [phone] Fiex, 828152.4618
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
QC Batch: 144878 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: GC/MS VOCs by 8260
Associated Lab Samples: 926408667
METHOD BLANK: 926437849
Associated Lab Samples: 926408667
Blank
Reporting
Parameter
Units
Result
Limit Footnotes -
Acetone
ug/l
No
25.
Benzene
ug/l
NO
5.0
Bromobenzene
Ug/l
NO
5.0
Bromochloromethane
ug/l
NO
5.0
Bromodichloromethane
ug/l
ND
5.0
Bromoform
ug/1
ND
5.0
Bromomethane
ug/1
ND
5.0
2-Butanone (MEK)
ug/1
ND
10.
n-Butylbenzene
ug/l
ND
5.0
sec-Butylbenzerte
ug/1
NO
5.0
tert-Butylbenzene
ug/l
ND
5.0
Carbon tetrachloride
ug/l
ND
5.0
Chlorobenzene
ug/l
ND
5.0
Chloroethane
ug/1
ND
10.
Chloroform
ugll
ND
5.0
Chloromethane
ug/l
ND
5.0
2-Chlorotoluene
ug/l
ND
5.0
4-Chlorotoluene
ugll
NO
5.0
1,2-Dibromo-3-chloropropane
ugll
ND
5.0
Dibromochloromethane
ug/1
ND
5.0
1,2-Dibromoethane (EDB)
ug/l
ND
5.0
Dibromomethane
ugll
ND
5.0
1.2-Dichlorobenzene
ug/l
ND
5.0
1,3-Dichlorobenzene
ug/l
NO
5.0
1,4-Dichlorobenzene
ug/l
ND
5.0
Dichlorodifluoromethane
ug/l
ND
5.0
1,1-Dichloroethane
ug/l
NO
5.0
1.2-Dichloroethane
ug/l
ND
5.0
1.1-Dichloroethene
ugll
ND
5.0
cis-1,2-Dichloroethene
ug/1
NO
5.0
trans-1,2-Dichloroethene
ug/l
NO
5�O
Date: 12/16/05
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC
99030
Fl- NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Cf"�
I oir t,
Page: 19 of 35
Charlotte CertificadfimMs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
I'L NELAP
E87627

Pace Analytical Services, Inc.
Pace Analytical Services, inc.
9600 Kincey Avenue, Suite 100
2225 Riversice Drive
Hunt6rsville, NC 28078
Asheville, NC 28804
Phone: 704.875.902
Phone: [phone]
4n.qh1tir;?1'
Fax: [phone]
Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
METHOD BLANK: 926437849
Associated Lab Samples: 926408667
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
1,2-Dichloropropane
ug/l
NO
5.0
1.3-Dichloropropane
ug/l
ND
5.0
2,2-Dichloropropane
ug/l
NO
5.0
1,1-Dichlorapropene
ug/1
ND
5.0
ci s- 1, 3 -Di chl oropropene
ugll
ND
5.0
trans-1.3-Dichlaropropene
ug/l
NO
5.0
Diisopropyl ether
ug/l
NO
5.0
Ethylbenzene
ug/l
ND
5'0
Hexachloro-1.3-butadiene
ug/l
ND
5.0
2-Hexanone
ug/l
ND
10.
lsopropyl benzene (Cumene)
ug/l
ND
5.0
p-Isopropyltoluene
ug/l
ND
5.0
Methylene chloride
ug/l
ND
5.0
4-Methyl-2-pentanone (MlBK)
ug/l
ND
10.
Methyl-tert-butyl ether
ug/1
NO
5.0
Naphthalene
ug/l
NO
5.0
n-Propylbenzene
ug/l
ND
5.0
Styrene
ug/1
ND
5.0
1.1.1.2-Tetrachloroethane
ug/l
NO
5.0
1,1,2.2-Tetrachloroethane
ug/l
ND
5.0
Tetrachloroethene
ug/l
ND
5.0
Toluene
ug/1
ND
5.0
1,2,3-Trichlorobenzene
ug/l
NO
5.0
1.2.4-Trichlorobenzene
ug/l
ND
5.0
1. 1. 1 - Tri chi oroethane
ug/l
NO
5.0
1, 1. 2 - Tri chl oroethane
ug/l
ND
5.0
Trichloroethene
ug/l
ND
5�0
Tr i chl o rofl uoromethane
ug/l
NO
10.
1. 2. 3 - Tri chl oropropane
ug/l
ND
5.0
1, 2.4 - Tri methyl benzene
ug/l
NO
5.0
1. 3. 5 - Tri methyl benzene
ug/l
NO
5.0
Vinyl acetate
ug/l
ND
10.
Vinyl chloride
ug/l
ND
5.0
Xylene (Total)
ug/l
NO
5.0
m&p-Xylene
ug/l
NO
10.
o-Xylene
ug/l
NO
5.0
Date: 12116/05
Asheville Certification IDs
NC Wastewater
40
NG Drinking Water
37712
SC
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 20 of 35
Charlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FIL NELAP
E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 2225 Riverside 54ive
Huntersville, NC 28078 Asheville, NC28804
Phone: [phone] Phene.- 828.254.7176
An-qhlfii,�il' Fax., 704.875.9091 Fax: [phone]
www.paceiabs.com QUALITY CONTROL DATA
METHOD BLANK: 926437849
Associated Lab Samples: 926408667
Blank
Parameter Units Result
Toluene-d8 (S3 % 98
4-Bromofluorobenzene (S) % 103
Dibromofluoromethane (S) % 89
1.2-Dichloroethane-d4 (S) % 81
LABORATORY CONTROL SAMPLE: 926437856
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Reporting
Limit Footnotes
Spike
LCS
LCS
Parameter -
Units
Conc.
Result
% Rec
Acetone
ug/l
100.00
76.98
77
Benzene
ug/l
50.00
52�69
105
Bromobenzene
ug/l
50.00
45.36
91
Bromochloromethane
ug/l
50.00
49.84
100
Bromodichloromethane
ug/l
50.00
46.96
94
Bromoform
ug/l
50.00
44.45
89
Bromomethane
ug/l
50.00
51.56
103
2-Butanone (MEK)
ug/l
100.00
75.88
76
n-Butylbenzene
ug/l
50.00
43.14
86
sec-Butylbenzene
ug/l
50.00
49.21
98
tert-Butylbenzene
ug/l
50.00
49.30
99
Carbon tetrachloride
ug/l
50�00
52.95
106
Chlorobenzene
ug/l
50.00
51.47
103
Chloroethane
ug/1
50.00
54.90
110
Chloroform
ug/I
50.00
48.66
97
Chloromethane
ug/I
50.00
47.85
96
2-Chlorotoluene
ug/1
50.00
47.38
95
4-Chlorotoluene
ug/l
50.00
47.16
94
1,2-Dibromo-3-chloropropane
ug/l
5D.00
43.68
87
Dibromochloromethane
ug/1
50.00
48.19
96
1.2-Dibromoethane (EDB)
ug/1
50.00
47.52
95
Dibromomethane
ug/1
50�00
50.19
100
1.2-Dichlorobenzene
ug/1
50.00
48.73
98
1,3-Dichlorobenzene
ug/1
50.00
48.55
97
1,4-Dichlorobenzene
ug/l
50.00
48.30
97
Dichlorodifluoromethare
ug/l
50.00
50.68
101
Date: 12/16/05
Asheville Certification IDs
NG Wastewater 40
NG Drinking Water 37712
SC 99030
FL NELAP E87648
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 21 of 35
Charlotte Certification ID
NC Wastewater
12
NG Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Hunters vfile, NC 28078
Phone: [phone]
AnaIMC81 Fax., 704.875.9091
www.pacelahs.com QUALITY CONTROL DATA
LABURAIURY CONTROL SAMPLE: 926437856
Spike
LCS
LCS
Parameter -
Units
Conc.
Result
Rec
1.1-Dichlaroethane
ug/l
50.00
50.18
100
1.2-Dichloroethane
ug/l
50.00
41.98
84
1,1-Dichloroethene
ug/l
50.00
61.65
123
cis-1.2-Dichloroethene
ug/l
50�00
47.59
95
trans- 1, 2-Dichl oroethene
ug/l
50.00
56�99
114
1.2-Dichloropropane
ug/l
50.00
49.10
98
1.3-Dichloropropane
ug/l
50.00
48.76
98
2.2-Dichloropropane
ug/l
50.00
46.15
92
1. 1 - Di chl oropropene
ug/l
50.00
50.26
101
ci s - 1, 3 - Di chl oropropene
ug/1
50.00
49.04
98
t rans - 1. 3 - Di ch I oropropene
ug/l
50.00
48.42
97
Diisopropyl ether
ug/l
50.00
49.07
98
Ethylbenzene
ug/1
50.00
50.82
102
Hexachl oro - 1, 3 - butadi ene
ug/l
50.00
51.12
102
2-Hexanone
ug/l
100-00
90.96
91
Isopropyl benzene (Cumene)
ug/l
50.00
56.12
112
p-Isopropyltoluene
ug1l
50.00
43.97
88
Methylene chloride
ug/l
50.00
50.37
117
4-Methyl-2-pentanone (MlBK)
ug/1
100.00
87.25
87
Methyl-tert-butyl ether
ug/l
50.00
48.58
97
Naphthalene
ug/l
50.00
44.44
89
n-Propyllbenzene
ug/l
50.00
48.01
96
Styrene
ug/1
50.00
50,41
101
1.1.1.2-Tetrachloroethane
ug/l
50.00
50.32
101
1.1,2,2-Tetrachloroethane
ug/l
50.00
45.07
90
Tetrachloroethene
ug/l
50.00
53�41
107
Toluene
ug/1
50.00
51.28
103
1.2.3-Trichlorobenzene
ug/l
50.00
51.54
103
1,2.4-Trichlorobenzene
ug/l
50.00
49.50
99
1.1.1-Trichlor-oethane
ug/1
50.00
47.38
95
1.1.2-Trichloroethane
ug/l
50.00
48.14
96
Tri chl oroethene
ug/l
50.00
52.22
104
Tri chl orofl uoromethane
ug/l
50.00
48.19
96
1, 2. 3 - Tri chl oropropane
ug/1
50.00
46.24
92
1. 2. 4 - Tri methyl benzene
ug/l
50.00
43.64
87
1,3,5-Trimethylbenzene
ug/l
50.00
43.64
87
Vinyl acetate
ug/l
100.00
94.71
95
Date: 12/16/05
Asheville Certification IDs
NC Wastewater 40
NG Drinking Water 37712
SC 99030
FL NELAP E87648
Pace Analyfleal Services, Inc.
222Y Riverside Drive
Ashevifle, NC 28804
Phone: [phone]
fax., 628.252.4618
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Footnotes
REPORT OF 1ABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 22 of 35
Charlotte Certification ID
NG Wastewater
12
NG Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Services, Inc,
9800 Kincey Avenue, Suits 100
Huntersvi#6, NC28078
Phone: [phone]
AnalXicala Fax: [phone]
www.pacelahs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 926437856
Parameter
Vinyl chloride
Xylene (Total)
m&p-Xylene
a-Xylene
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
MATRIX SPIKE: 926438078
Parameter
Benzene
Chlorobenzene
IJ-Dichloroethene
Toluene
Trichloroethene
Toluene -dB (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
SAMPLE DUPLICATE: 926438094
Spike
LCS
LCS
Units
Conc.
Result
Rec
ug/I
50.00
51.02
102
ug/l
150.00
151,9
101
ug/I
100.00
102.5
103
Ug1l
50.00
49.35
99
926402678
Spike
Units
Result
Conc.
ug/I
0
50.00
ug/l
0
50.00
ug/l
0
50.00
ug/l
0
50.00
ug/I
0
50.00
98
103
88
80
Pace Analylival Services, Inc.
2225 RiversWe Orive
Asheville, NC28804
Phone, 828.254.7176
fe.x, 828.252.4618
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Footnotes
MS
MS
Result
Rec Footnotes
50.57
101
54.02
108
60.45
121
49.15
98
50.98
102
95
105
89
76 1
926423047
DUP
Parameter —
Units
Result
Result RPD Footnotes
Benzene
ug/I
13.00
13.00 1
1.2-Dichloroethane
ug/l
NO
ND NC
Ethylbenzene
ug/l
720�O
720.0 0
Methyl-tert-butyl ether
ug/I
NO
NO NC
Naphthalene
ug/I
320.0
320.0 1
Toluene
ug/l
460.0
450.0 1
Xylene (Total)
ug/I
3700
3700 1
m&p-Xylene
ug/l
2600
2600 1
Date: 12116105
Asheville Certification IDs
REPORT
OF LABORATORY
ANALYSIS
NC Wastewater 40
man
This report shall not be reproduced, except in full,
NC Drinking Water 37712
without
the written consent of Pace Analytical Services, Inc.
Sc 99030
FL NELAP E87648
Page: 23 of 35
Charlotte Cad—iftcaf—lonlDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pecs Analytical Services, Inc, Pace Aiialyfical Services, Inc.
9800 Kincey Avenue, Suite 100 225 Riverside Drive
Huntersv#16, NC 26078 Asheville, NC 28804
Phone., 704.875.9092 Phone., 828.254.7176
AnalMal Fax [phone] far 828.252.4618
www.paceiabs.com QUALITY CONTROL DATA
bAMPLL UUPLICATE: 926438094
Parameter
o-Xylene
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1.2-Dichloroethane-d4 (S)
Date: 12116/05
AsINville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
926423047
DUP
Units
Result
Result
ug/l
1100
1100
%
99
98
%
112
111
%
89
88
%
77
78
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
RPD Footnotes
1
2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 24 of 35
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
sc 99006
FIL NELAP E87627

Pace Analytical Services, inc. Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100 22?5 Rivergide i9rive,
Huntorsville, NC 28078 Ast7eville, NC 28804
Phone: [phone] Phone., 828.254.7176
AnalXical" Fax. [phone] Fax., 828.252.4618
www.paceiabs.com QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
QC Batch: 144229 Analysis Method: EPA 245.1
QC Batch Method: EPA 245.1 Analysis Description: Mercury, CVAAS, in Water
Associated Lab Samples: 926408667
METHOD BLANK: 926407271
Associated Lab Samples: 926408667
Blank Reporting
Parameter Units Result Limit Footnotes
Mercury mg/l NO 0.0002
LABORATORY CONTROL SAMPLE: 926407289
Spike LCS LCS
Parameter Units Conc. Result Rec Footnotes
Mercury mg/l 0.0025 0.0027 108
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926407297 926407305
926399460 Spike Ms MSD MS MSD
Parameter Units Result Conc. Result Result Z Rec Y Rec RPO Footnotes
Mercury mg/l 0.00066 0.0025 0.0034 0.0028 108 86 18
Date: 12/16105
Asheville Certification lDs
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
REPORT OF LABORATORY ANA16Y.SIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 25 of 35
Charlotte Certification IDs
NC Wastewater
12
MC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace AnaJirtical Services, Inc. Paco Analyfical Services, Zac.
9800 Kincey Avenue, Suite IGO 2225 Riverside Drive
Huntersville, NC28078 Asheville, NC28604
Phone: [phone] Phone., 828,254.7176
Analvtical" Fax: [phone] fax.[phone]
www.pavelabs.com QUALITY CONTROL DATA
QL Batch: 144495
QC Batch Method:
Associated Lab Samples: 926408667
METHOD BLANK: 926419169
Associated Lab Samples: 926408667
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
Analysis Method: EPA 200.7
Analysis Description: Trace ICP Metals
Blank
Reporting
Parameter
- Units
Result
Limit Footnotes
Aluminum
mg/l
ND
0.10
Antimony
mg/l
NO
0.0050
Arsenic
mg/l
NO
0.0050
Barium
mg/l
NO
0.0050
Beryllium
mg/l
NO
0.0010
Cadmium
mg/l
NO
0.0010
Chromium
mg/l
NO
0.0020
Copper
mg/l
NO
0.0020
Lead
mg/l
NO
0.0050
Molybdenum
mg/l
NO
0,005D
Nickel
mg/l
NO
0.0050
Selenium
mg/l
NO
0.0050
Silver
mg/1
NO
0.0020
Thallium
mg/1
NO
0.010
Zinc
mg/l
NO
0.010
LABUKAIURY CUNTROL SAMPLE: 926419177
Spike
LCS
LCS
Parameter
_ Units
Conc.
Result
% Rec Footnotes
Aluminum
m9l]
5.000
5.100
102
Antimony
mg/l
0.5000
0.5190
104
Arsenic
mg/l
0.5000
0.5180
104
Barium
mg/l
0,5000
0.4980
100
Beryllium
mg/l
0.5000
0.5170
103
Cadmium
mg/l
0.5000
0.5280
106
Chromium
mg/l
0.5000
0.5290
106
Copper
mg/l
0.5000
0.5020
100
Lead
mg/l
0.5000
0.5230
105
Molybdenum
mg/l
0.5000
0.5220
104
Date: 12116105
Astieville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
Sc
99030
FL NELAP
E87648
I Arekis
REPORT OF LABORATORY ANALTO
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
� �_ A�1%
J n
Page: 26 of 35
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E97627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey/lvenue, Sulte 100 2225 Piversicfp Drive
Huntersville, NC 28078 Asheville, Nd 2884 -
Phone: [phone] Phone: [phone]
Anafyticale Fax., 704.875.9091 rg: 826.252.4618
www,pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
LABORATORY CONTROL SAMPLE: 926419177
Parameter Units
Nickel mg/l
Selenium mg/l
Silver mg/l
Thallium mg/l
Zinc mg/l
Spike LCS LCS
Conc. Result % Rec Footnotes
0.5000 O�5210 104
0.5000 0.5170 103
0.2500 0.2410 96
0.5000 0.4960 99
0.5000 0.5220 104
MATRIX SPIKE MATRIX SPIKE
DUPLICATE:
926419755 926419763
926409178 Spike MS
MSD
MS
MSD
Parameter
Units
Result Cone. Result
Result %
Rec
Rec
RPD Footnotes
Aluminum
mg/l
0.1830 5.000 4.920
5.260
95
102
7
Antimony
mg/l
0 0.5000 0.4830
0.5200
97
104
7
Arsenic
mg/1
0.00438 0.5000 0.5010
0.5450
99
108
8
Barium
mg/l
0.00178 0.5000 0.4510
0.4860
90
97
7
Beryllium
mg/1
0.00013 0.5000 0.4810
0.5190
96
104
8
Cadmium
mg/1
0 0.5000 0.4840
0.5210
97
104
7
Chromium
mg/I
0.00084 0.5000 0.4810
0.5190
96
104
8
Copper
mg/l
0.01300 0.5000 0.4730
0.5080
92
99
7
Lead
mg/l
0.00480 0.5000 0.4870
0.5280
96
105
8
Molybdenum
mg/l
0.1660 0.5000 0.6380
0.6800
94
103
6
Nickel
mg/l
0.04310 0,5000 0.5030
0.5410
92
100
7
Selenium
mg/l
0.00713 0.5000 0.5030
0.5450
99
108
8
Silver
mg/l
0.00055 0.2500 0.2290
0.2470
91
99
8
Thallium
mg/l
0 0.5000 0.4880
0.5180
98
104
6
Zinc
mg/1
0.06610 0.5000 0.5690
0.6020
101
107
6
SAMPLE DUPLICATE: 926419771
926409186 DUP
Parameter
Units
Result Result RPD
Footnotes
Aluminum
mg/l
0.2100 0.2000 7
Antimony
mg/l
NO ND NC
Arsenic
mg/l
ND 0.00580 0
Barium
mg/l
ND NO NC
Beryllium
mg/l
NO NO NC
Date: 12/16/05
Page:
27 of 35
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Celliflegbon IDa
NC Wastewater 40
This report shall not be reproduce'da except in full,
NG Wastewater
NG Drinking Water
12
37706
NC Drinking Water 37712
without
the written consent of Pace Analytical Services, Inc.
Sc
99006
SC 99030
FL NELAP E87648
1. ac
FL NELAP
E87627

Pace AlizalyticjI Services, /,7c. Pace Analytical Services, Inc.
.9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NG28078 Asheville, NC 28804
Phone: 704,675.9092 Phoria. 828.254.7176
Analytical Fax., 704.675.9091 Fax[phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
a�rLt UUFLA(Alt: �IZM19//l
926409186
DUP
Parameter
Units
Result
Result
RPD
Cadmium
mg/l
ND
ND
NC
Chromium
mg/l
ND
ND
NC
Copper
mg/l
0.00530
0.00500
6
Lead
mg/l
ND
ND
NC
Molybdenum
mg/l
0.07100
0.07000
1
Nickel
mg/l
0.01900
0 ' 01800
7
Selenium
mg/l
ND
0.00720
0
Silver
mg/l
ND
0.00740
0
Thallium
mg/l
ND
ND
NC
Zinc
mg/l
0.04100
0.03900
4
Date: 12/16/05
A5heville Certification IDs
NC Wastewater
40
NG Drinking Water
37712
Sc
99030
FIL NELAP
E87648
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 28 of 35
Charlotte ertitication ID
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Anall4lual Services, Inc.
9800 Kincey Avenue, SuI16 100 2226 Rivers06 Plive
Huntersvillo, NC 28078 Asheville, PIC 28804
Phone., 704.875.9092 Phone: 828.254,7176
Analytical" Fax., 704.875.9091 Fax- 828.252.4618
www.paceiabs.com QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
QC Batch: 144389
Analysis Method: EPA 160.2
OC Batch Method: EPA 160.2
Analysis
Description: Total Suspended Solids
Associated Lab Samples:
926408667
METHOD BLANK: 926412917
Associated Lab Samples:
926408667
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Total Suspended Solids
mg/l
NO
1.0
LABORATORY CONTROL SAMPLE:
926412925
Spike
LCS LCS
Parameter
Units
Conc.
Result Rec Footnotes
Total Suspended Solids
mg/l
250.00
224.0 90
SAMPLE DUPLICATE: 926412933
Parameter Units
Total Suspended Solids mg/l
Date: 12/16/05
Asheville Certification IN
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
926400011 OUP
Result Result RPD Footnotes
NO NO NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
ne
Page: 29 of 35
Chariots Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC26078
Phone: [phone]
Anakical Fax. [phone]
www.pacelabs.com QUALITY CONTROL DATA
Pace Analytical Services, Inc.
22?5 Riverside Drive
Asheville, NC28804
Phona, 828,254.7176
Fax: [phone]
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
QC Batch: 144521 Analysis Method: EPA 340.2
QC Batch Method: EPA 340�2 Analysis Description: Fluoride
Associated Lab Samples: 926408667
METHOD BLANK: 926421439
Associated Lab Samples: 926408667
Blank Reporting
Pargmeter Units Result Limit Footnotes
Fluoride mg/l ND 0.10
LABORATORY CONTROL SAMPLE: 926421447
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Fluoride mg/l 2.500 2.660 106
14ATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926421454 926421462
926408527 Spike MS MSD MS MSD
Parameter - Units Result Conc. Result Result % Rec % Rec RPD Footnotes
Fluoride mg/1 0,1920 2.500 2.240 2.240 82 82 0
Lt DUPLICAIL: 926421470
Parameter - Units
Fluoride mg/l
Date: 12/16/05
A51leville Certification Jos
NC Wastewater 40
NG Drinking Water 37712
SC 99030
Fl- NELAP E87648
926408535 DUP
Result Result RPO Footnotes
0.4100 0.3600 12 3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace AnalYtical Services, Inc.
Page: 30 of 35
Lharlottg Cedfication fps
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 10D 222S Rivenioide4rive
Huntersville, NC 28078 Ashevil/q, NC288d
Phone: [phone] Phone: 826,254.7176
An.,,7h1fir;71' Fax [phone] Fax., 828.252.4618
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
QC Batch: 144419
Analysis Method: EPA 350.1
QC Batch Method: EPA 350.1
Analysis
Description: Ammonia
Associated Lab Samples;
926408667
METHOD BLANK: 926414632
Associated Lab Samples:
926408667
Blank
Reporting
Parameter
Units
Result
, Limit Footnotes
Nitrogen, Ammonia
mg/l
ND
0.10
LABORATORY CONTROL SAMPLE:
926414640
Spike
LCS LCS
Parameter
Units
Conc.
Result % Rec Footnotes
Nitrogen, Ammonia
mg/l
1.000
1.019 102
MATRIX SPIKE: 926414657
926412701 Spike MS MS
Parameter - Units Result Conc. Result % Rec Footnotes
Nitrogen, Ammonia mg/l 0.7580 1.000 1.171 41 4
SAMPLE DUPLICATE: 926414665
926408675 DUP
Parameter - Units Result Result RPO Footnotes
Nitrogen, Ammonia mg/l 15.00 16.00 2
Date: 12/16/05
A*hgyille Certification
IDs
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NG Drinking Water
37712
This report shall not be reproduced, except in full,
SC
99030
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
n act
Page. 31 of 35
Charlotte Certification IDs
NO Wastewater
12
NO Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical services, Inc. Pace Analytical Services, Inc,
9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NO 28078 Asheville, NC 28804
Phone: [phone] Phone- 828.254� 7176
Analvhc,n, I Fix., 704.875.9091 FaA., 828.252.4618
www.pacelahs.com QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
QC Batch: 144447 Analysis Method: EPA 335.2
QC Batch Method: EPA 335.2 Analysis Description; Cyanide, Total, Water
Associated Lab Samples: 926408667
ML I HUI) BLANK: 926415084
Associated Lab Samples: 926408667
Blank Reporting
Parameter Units Result Limit Footnotes
Cyanide mg/l ND 0.0050
LABURAIURY CONTROL SAMPLE: 926415092
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec Footnotes
Cyanide
mg/l
0.1000
0.0990
99
MATRIX SPIKE: 926415100
926409913
Spike
MS Ms
Parameter -
Units
Result
Conc.
Result % Rec Footnotes
Cyanide
mg/l
0
0.1000
0.0840 84
�)AMPLE DUPLICATE: 926415118
Parameter - Units
Cyanide mg/1
Date; 12/16/05
Ashevilig Qertification los
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
926408170 CUP
Result Result RPD Footnotes
ND ND NC
REPORT OF LABORATORY ANALLINSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
nelar- t
Page: 32 of 35
Charlotte Certification IDs
NG Wastewater
12
NG Drinking Water
37706
Sc
99006
FL NELAP
E87627

Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suits 100
2225 Rivers4ge Drive
Asheville, NC2JW
Huntersville, NC 28078
Phone: [phone]
Phone: [phone]
aceAnalytical
Fax., 704,875.90,91
Fax: [phone]
www.pacelabs.com
QUALITY CONTROL DATA
Lab Project Number:
92108723
Client Project ID:
Grey Water Analysis
OC Batch; 144624 Analysis Method: EPA 325.2
QC Batch Method: EPA 325.2 Analysis Description: Chloride (Mercuric Nitrate)
Associated Lab Samples: 926408667
METHOD BLANK: 926426883
Associated Lab Samples:
926408667
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Chloride
mg/l
NO
5.0
LABORATORY CONTROL SAMPLE:
926426891
Spike
LCS LCS
Parameter
Units
Conc.
Result % Rec Footnotes
Chloride
mg/l
20.00
20.99 105
MATRIX SPIKE: 926426909
926408527
Spike MS MS
Parameter
Units
Result
Conc. Result X Rec Footnotes
Chloride
mg/l
22�80
20.00 38.54 79
SAMPLE DUPLICATE: 926426917
Parameter Units
Chloride mg/l
Date: 12/16105
Asheville Certification 1Ds
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
926408535 DUP
Result Result RPD Footnotes
20.00 21.00 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
J�!%
Page: 33 of 35
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey/lvenue, Suite 100 2225 Riverside Drive
Huntersville, NC28078 Asheville, NC 28804
Phone: [phone] Phone., 828.254.7176
Anapical' Far 704.875.9091 Fax,'828.252.4618
www.pacelalis.com QUALITY CONTROL DATA
Lab Project Number: 92108723
Client Project ID: Grey Water Analysis
LIL baT:Cn: 14463�! Analysis Method: EPA 410.4 -
QC Batch Method: EPA 410.4 Analysis Description: Chemical Oxygen Demand
Associated Lab Samples: 926408667
mtlhUU MANK: VZb427162
Associated Lab Samples: 926408667
Parameter Units Blank Reporting
Result Limit Footnotes
Chemical Oxygen Demand mg/l NO 25.
LABORATORY CONTROL SAMPLE: 926427170
Parameter Spike LCS LCS
Units Conc. Result Rec Footnotes
Chemical Oxygen Demand mg/l 750-00 775.0 103
Mt: 9Z04Z/188
Parameter 926426156 Spike MS HS
Units Result Conc. .... Result X Rec Footnotes
Chemical Oxygen Demand —
mg/l 59.00 750.00 920.0 115
]RULAIL: 926427196
Parameter Units
Chemical Oxygen Demand mgJl
Date: 12/16/05
Ashgvlllg Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
926412719 DUP
Result Result R—PD Footnotes
730.0 730.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
nelacl,�
Page: 34 of 35
Charlqtte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

Pace Analytical Services, Inc.
Pace AnalyfivBl Services, Inc.
9800 Kincey Avenue, Suite 100
2225 Rivers4le Prive
A6� "
Huntersville, NC 28078
Asheville, 1VV
Phone: [phone]
Phone: [phone]
Analytical" Fax., 704.875.9091
Fax [phone]
www.pacelabs.com
Lab Project Number:
92108723
Client Project ID:
Grey Water Analysis
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
(S) Surrogate
Ell The surrogate and/or spike recovery was outside acceptance limits.
[21 Low surrogate recovery was confirmed as a matrix effect by a second analysis.
[31 The calculated RPD was outside QC acceptance limits.
[41 The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
Date: 12/16/05
Asheville Certification IDs
NG Wastewater 40 REPORT OF LABORATORY ANALYSIS
NG Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
ne
Page: 35 of 35
Charlotte Cartificatim-0s;
NC Wastewater
12
NG Drinking Water
37706
Sc
99006
FL NELAP
E87627

'11��6ceAnalj4icale
4Section
A
Required Client information:
Company D01, �67 COUAA
Address SaLi,�R
6 0 5 e- 0 uef 5 T Aj IV c
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Requested Due jaterw,
Section D Required Client Information
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One Character per box.
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CHAIN -OF -CUSTODY /Analytical Request Document
The Chaln-of-Cus I tody, is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section B Secti-on C Page: 0!4
Required Project Information: Invoice Information: -79-E��2 4 17
Report To: Attention,
Copy To:
C07 ny Name', 11 GROUNDWATER 0 DRINKING
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Purchas
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Project Name: Pao 1101-1 OSC WI OOTHER
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