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Home My WebLink About5601_ROSCANS_1999Pace Analytical Services, Inc. 54 Ravenscroft Drive Asheville, NC 28801 Tel: 828-254-7176 Fax: 828-252-4618 March 31, 1999 Mr. Mike Gladden McDowell County Landfill 10 East Court St. Marion, NC 28752 RE: Pace Project Number: 934485 Client Project 10: Landfill Dear Mr. Gladden: Enclosed are the results of analyses for sample(s) received by the laboratory on March 16, 1999. If you have any questions concerning this report, please feel free to contact me. Sincerely, Waiter MilLer Project Manager Enclosures Laboratory Certification Us Laboratory Certification IDa NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980 NCDrinkingWater 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. I INVOICE 54 Ravenscroft Dri ve Number- 93033554 Asheville, NC 2880, D I ate I : Phone: (828) 254-7176 03Z31/1999 Fax: (828) 252-4618 Please Remit To: Mr. Mi ke Gl adden Pace Analytical Services, Inc. McDowell County Landfill NW 8922 10 East Court St. P.O. Box 1450 Marion, NC 28752 Minneapolis, MN 55485-8922 701305/MCDOWELL CO. Purchase, Order No Project Marlader Walter Millpr Terms Due Upon Receipt ePa e'Na, - I Client Reference: Landfill Pace Project No: 934485 Quantity U/M Description Method Matrix Price Total ANALYaTICAL 7Charges: 1.00 ea Charge for Field Services Water 192.25 $ 192.25 4.00 ea Monitoring Well Data Water 5.00 $ 20.00 4 1 nn .DO ea Field Grab Data Water 2.50 $ 10.00 4.00 ea Barium EPA 6010 Water 10.00 $ 40.00 4.00 ea Copper EPA 6010 Water 10.00 $ 40.00 4.00 ea Nickel EPA 6010 Water 10.00 $ 40.00 4.00 ea Zinc EPA 6010 Water 10.00 $ 40.00 4.00 ea Antimony, AAS Furnace EPA 7041 Water 10.00 $ 40.00 4.00 ea Arsenic, AAS Furnace EPA 7060 Water 10.00 $ 40.00 4.00 ea Beryllium, AAS Furnace EPA 7091 Water 10.00 $ 40.00 4.00 ea Cadmium, AAS Furnace EPA 7131 Water 10.00 $ 40.00 4.00 ea Chromium Furnace EPA 7191 Water 10.00 $ 40.00 4.00 ea Cobalt, AAS Furnace EPA 7201 Water 10.00 $ 40.00 4.00 ea Lead. AAS Furnace EPA 7421 Water 10.00 $ 40.00 4.00 ea Selenium, AAS Furnace EPA 7740 Water 10.00 $ 40.00 4.00 ea Silver by Furnace EPA 7761 Water 10.00 $ 40.00 4.00 ea Thallium, AAS Furnace EPA 7841 Water 10.00 $ 40.00 4.00 ea Vanadium. AAS Furnace EPA 7911 Water 10.00 $ 40.00 4.00 ea Volatile Organics, EPA 8260 Water 150.00 $ 600.00 ANALYTICAL SUBTOTAL: .............. $ 1422.25 TOTAL INVOICE AMOUNT: .............. $ 1422.25 1.5% MONTHLY FINANCE F qFMn RPMTTTAKIrP 1307 nP P171717P CHARGE ASSESSED AFTER 30 MVnTrF NIIMPFP 01('111r, _10 INVOIC DAYS rA W rM OPWITMr W CLIENT AN EQUAL OPPORTUNITY EMPLOYER E Mr. Mike Gladden McDowell County Landfill 10 East Court St. Marion, NC 28752 54 Ravenscroft Dri%;e Asheville, NC 288( 1 Phone: (828) 254-7176 Fax: (828) 252-4618 INVOICE Number- 93,33,,4 [t'a-te-:- 03/33/1999 Please Remit To: Pace Analytical Services, Inc. NW 8922 P.O. Box 1450 Minneapolis, MN 55485-8922 ClentNq, 701305/MCDOWELL CO. Purchase Order No ',.ProiectManacier Walter Miller iTernn&'-`�";'---,' Due Upon Receipt N ".7 01 2 PLEASE REMIT THIS PAGE WITH PAYMENT TOTAL INVOICE AMOUNT: $ 1422.25 1.5% MONTHLY FINANCE CHARGE ASSESSED AFTER 30 DAYS. RFmTT-rANrr PArr CLIENT AN EQUAL OPPORTUNITY EMPLOYER M 0 1 0 0 ITEM # CL cn to M 0 — 2 E. 0 a 21 LD. Cn 'I z A < (I) , 0 0 0 c, �j N, 1�� 0 0 = A W t I -2. cn tz I I c: . M @ M 0 . - I - z z z a cl) ? a 0 0 Ml— F > z 2 "N >:E 0 M K tl—�fFl0c:N"� MW M �m X4 M x 0 wx 10 Cn M 0 M ATRIX CODE IM 3 3 DATE Ei L, - 3 3 a COLLECTED > J, a 0 �j 3 TIME fD C L ECTED 0 L #containers Unprese d Ne HCI \.P- Na2S203 -a Tl� j 0 0 3 0 -A; cr Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 828-254-7176 Fax: 828-252-4618 McDowel. L County Landf it 1. 10 East Court St. Marion, NC 28752 Attn: Mr. Mike GLadden Phone: (700659-2521 SoLid results are reported on a wet weight basis Pace Sampte No: Ctient Sample ID: Parameters --------------- FieLd Services DATE: 03/31/99 PAGE: 1 Pace Project Number: 934485 Ctient Project ID: LandfiLt 93208940 Date Co(Lected: 03/16/99 Matrix: Water MW#1 Date Received: 03/16/99 Results Units PRL AnaLyzed AnaLyst CAS# Footnotes ---------- ---------- --------- ---------- -------- ----- ---------- ---------- Monitoring Weil. Data Method: Prep Method: FieLd Specific Conductance 61 umhos1cm 03/16/99 MPS Depth of Water 20.74 feet 0 03/16/99 MPS Field Grab Data Method: Prep Method; FieLd pH 6.5 Std. Units 0 03/16/99 MPS FieLd Temperature 14 deg C 0 03/16/99 MPS Metals MetaLs, ICP Method: EPA 6010 Prep Method: EPA 3010 Barium 0.30 mg/l 0.11 03/22/99 KEK 7440-39-3 Copper No mg/L 0.01 03/22/99 KEK 7440-50-8 Nickel No mg/t 0.05 03/22/99 KEK 7440-02-0 Zinc 0.06 mg/L 0.01 03/22/99 KEK 7440-66-6 Date Digested 03/17/99 Antimony, AAS Furnace Method: EPA 7041 Prep Method: EPA 3020 Antimony ND mg/l 0.005 03/19/99 KEK 7440-36-0 Date Digested 03/17/99 Arsenic, AAS Furnace Method; EPA 7060 Prep Method: EPA 3020 Arsenic ND mg/t 0.005 03/18/99 KEK 7440-38-2 Date Digested 03/17/99 BerylLium, AAS Furnace Method: EPA 7091 Prep Method: EPA 3020 Beryl.Hum No mg/L 0.001 03/19/99 KEK 7440-41-7 Laboratory Certification IDS NC Wastewater 40 REPORT OF LABORATORY ANALYSIS NC Drinking Water 37712 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Laboratocy Certification IDS TN Drinking Water 02980 SC Environmental 99030 Pace Sample No: 93208940 Client Sample ID. MW#1 Parameters -------------------------------- Date Digested Cadmium, AAs Furnace cadmium Date Digested Chromium Furnace Chromi um Date Digested Cobalt, AAS Furnace Cobalt Date Digested Lead, AAS Furnace Lead Date Digested Selenium, AAS Furnace Selenium Date Digested Silver by Furnace Silver Date Digested Thallium, AAS Furnace Thattium Date Digested Vanedi um, AAS Furnace Vanadium Date Digested Laboratory Certification IDs NC Wastewater 40 NC Drinking Water 37712 Pace Analytical Services, Inc. 54 Ravenscroft Drive Asheville, NC 28801 Tel: 828-254-7176 Fax: 828-252-4618 DATE: 03/31/99 PAGE: 2 Pace Project Number: 934485 Client Project ID: Landfill Date Collected: 03/16/99 Matrix: Water Date Received: 03/16/99 Results Units PRL Analyzed Analyst CAS# Footnotes ---------- --------- ---------- -------- ----- ---------- ---------- 03/17/99 Method: EPA 7131 Prep Method: EPA 3020 ND mg/l 0.001 03/25/99 KEK 7440-43-9 03/17/99 Method: EPA 7191 Prep Method: EPA 3020 0.011 mg/t 0.002 03/18/99 KEK 7440-47-3 03/17/99 Method: EPA 7201 Prep Method: EPA 3020 0.015 mg/( 0.002 03/23199 KEK 7440-48-4 03/17/99 Method: EPA 7421 Prep Method: EPA 3020 0.027 mg/l 0.005 03/22/99 KEK 7439-92-1 03/17/99 Method: EPA 7740 Prep Method: EPA 3020 ND mg/l 0.005 03/23/99 KEK 7782-49-2 03/17/99 Method: EPA 7761 Prep Method: EPA 3020 ND mg/t 0.002 03/18/99 KEK 7440-22-4 03/17/99 Method: EPA 7841 Prep Method: EPA 3020 ND mg/l 0.002 03/23/99 KEK 7440-28-0 03/17/99 Method: EPA 7911 Prep Method: EPA 3020 0.09 mg/t 0.005 03/31/99 KEK 7440-62-2 03/17/99 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Laboratory Certification IDs TIN Drinking Water 02980 SC Environmental 99030 Pace Analocal Services, Inc. 54 Ravenscroft Drive Pace Analytocal Asheville, NC 28801 Tel: 828-254-7177 Fax: 828-252-4618 DATE: 03/31/99 PAGE: 3 Pace Project Number: 934485 C1. ient Project I D: Landf i L L Pace Sampte No: 93208957 Date ColLected: 03/16/99 Matrix: Water CLient SampLe 10: MW#2 Date Received: 03/16/99 Parameters Resutts Units PRIL AnsLyzed Analyst CAS# Footnotes --------------------------------- ---------- --------- ---------- -------- ----- ---------- ---------- FieLd Services Monitoring Welt Data Method: Prep Method: FIeLd Specific Conductance 460 umhos/cm 03/16/99 MPS Depth of Water 38.50 feet 0 03/16/99 MPS Field Grab Data Method; Prep Method: Field PH 6.4 Std. Units 0 03/16199 MPS Field Temperature 15 deg C 0 03/16/99 MPS Metals MetaLs, ICP Method: EPA 6010 Prep Method: EPA 3010 Barium 0.20 mg/L 0.1 03/22/99 KEK 7440-39-3 Copper No mg/L 0.01 03/22/99 KEK 7440-50-8 Nickel No mg/t 0.05 03/22/99 KEK 7440-02-0 Zinc 0.02 mg/L 0.01 03/22/99 KEK 7440-66-6 Date Digested 03/17/99 Antimony, AAS Furnace Method: EPA 7041 Prep Method: EPA 3020 Antimony No mg/1 0.005 03/19/99 KEK 7440-36-0 Date Digested 03/17/99 Arsenic, AAS Furnace Method: EPA 7060 Prep Method: EPA 3020 Arsenic RD mg/L 0.005 03/18/99 KEK 7440-38-2 Date Digested 03/17/99 BeryLHum, AAS Furnace Method; EPA 7091 Prep Method: EPA 3020 Beryl.Lium ND mg/t 0.001 03/19/99 KEK 7440-41-7 Date Digested 03/17/99 Cadmium, AAS Furnace Method: EPA 7131 Prep Method: EPA 3020 Cadmium ND mg/1 0.001 03/25/99 KEK 7440-43-9 Date Digested 03/17/99 Chromi um Furnace Method: EPA 7191 Prep Method: EPA 3020 Chromi um 0.004 mg/L 0.002 03/18/99 KEK 7440-47-3 Date Digested 03/17/99 Laboratory Certification IDs Laboratory Certification IDS INC Wastewater 40 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analyticill Asheville, NC 28801 Tel: 828-254-7176 Fax: 828-252-4618 Pace Sample No: 93208957 Client Sample ID: MW#2 Parameters -------------------------------- Cobalt, AAS Furnace CobaLt Date Digested Lead, AAS Furnace Lead Date Digested Selenium, AAS Furnace Selenium Date Digested SiLver by Furnace Silver Date Digested ThaLlium, AAS Furnace ThaLtium Date Digested Vanadium, AAS furnace Vanadium Date Digested DATE: 03/31/99 PAGE: 4 Pace Project Number: 934485 CLient Project ID: Landfill. Date Collected: 03/16/99 Matrix; Water Date Received: 03/16/99 Results Units PRL Analyzed Analyst CAS# Footnotes ---------- --------- -------- - -------- ----- ---------- ---------- Method: EPA 7201 Prep Method: EPA 3020 0.029 mg/l 0.002 03/23/99 KEK 7440-48-4 03/17/99 Method: EPA 7421 0.006 mg/l 0.005 Method: EPA 7740 No mg/ L 0.005 Method: EPA 7761 ND mg/1 0.002 Method: EPA 7841 ND mg/1 0.002 Method: EPA 7911 0.014 mg/t 0.005 Prep Method: EPA 3020 03/22/99 KEK 7439-92-1 03/17/99 Prep Method: EPA 3020 03/23/99 KEK 7782-49-2 03/17/99 Prep Method: EPA 3020 03/18/99 KEK 7440-22-4 03/17/99 Prep Method: EPA 3020 03/23/99 KEK 7440-28-0 03/17/99 Prep Method: EPA 3020 03/31/99 KEK 7440-62-2 03/17/99 Laboratory Certification IDs Laboratory Certification 10s NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytocal Asheville, NC 28801 Tel: 828-254-717 Fax:828-252-4618 DATE: 03/31/99 PAGE: 5 Pace Project Number: 934485 Client Project ID: Landfill Pace Sampte No: 93208965 Date Collected: 03/16/99 Matrix: Water Client Sample ID: MWI#3 Date Received: 03/16/99 Parameters Results Units PRIL Analyzed Anatyst CAS# Footnotes ------------------------- ------- ---------- --------- ---------- -------- ----- ---------- ---------- Field Services Monitoring Welt Data Method: Prep Method; Field Specific Conductance 340 umhos/cm 03/16/99 MPS Depth of Water 42.34 feet 0 03/16/99 MPS Field Grab Data Method: Prep Method: Field PH 6.7 Stall. Units 0 03/16/99 MPS Field Temperature 14 deg C 0 03/16/99 MPS Metals Metals, ICP Method: EPA 6010 Prep Method: EPA 3010 Barium 0.20 mg/L 0.1 03/22/99 KEK 7440-39-3 Copper ND mg/L 0.01 03/22/99 KEK 7440-50-8 Nickel NO mg/l 0.05 03/22/99 KEK 7440-02-0 Zinc 0.02 mg/L 0.01 03/22/99 KEK 7440-66-6 Date Digested 03/17/99 Antimony, AAS Furnace Method: EPA 7041 Prep Method; EPA 3020 Antimony ND mg/t 0.005 03/19/99 KEK 7440-36-0 Date Digested 03/17/99 Arsenic, AAS Furnace Method: EPA 7060 Prep Method: EPA 3020 Arsenic ND mg/t 0.005 03/18/99 KEK 7440-38-2 Date Digested 03/17/99 Beryllium, AAS Furnace Method; EPA 7091 Prep Method: EPA 3020 Beryllium ND mg/L 0.001 03/19/99 KEK 7440-41-7 Date Digested 03/17/99 Cadmi um, AAS Furnace Method: EPA 7131 Prep Method: EPA 3020 Cadmium ND mg/t 0.001 03/25/99 KEK 7440-43-9 Date Digested 03/17/99 Chromium Furnace Method: EPA 7191 Prep Method: EPA 3020 Chromium 0.002 mg/t 0.002 03/18/99 KEK 7440-47-3 Date Digested 03/17/99 Laboratory Cart fication IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs NC Wastewater 40 TN Drinking Water 02980 NCDrinkingWater 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytoral Asheville, NC 28801 Tel: 828-254-7176 Fax: 828-252-4618 Pace sample No: Ctient SampLe ID: Parameters ---------------------- Cobalt, AAS Furnace CobaLt Date Digested Lead, AAS Furnace Lead Date Digested Setenium, AAS Furnace Seleni um Date Digested SiLver by Furnace SiLver Date Digested ThatLium, AAS Furnace Tha(Lium Date Digested Vanadium, AAS Furnace Vanadium Date Digested DATE: 03/31/99 PAGE: 6 Pace Project Number: 934485 CHent Project ID: LandfiLl 93208965 Date CoLLected: 03/16/99 Matrix; Water MW#3 Date Received: 03/16/99 ResuLts Units PRL AnaLyzed Analyst CAS# Footnotes ---------- --------- ---------- -------- ----- ---------- ---------- Method: EPA 7201 Prep Method: EPA 3020 0.009 mg/l 0.002 03/23199 KEK 7440-48-4 03/17/99 Method: EPA 7421 ND mg/t 0.005 Method: EPA T740 ND mg/l 0.005 Method: EPA 7761 ND mg/L 0.002 Method: EPA 7841 ND mg/L 0.002 Method: EPA 7911 0.008 mg/L 0.005 Prep Method: EPA 3020 03/22/99 KEK 7439-92-1 03/17/99 Prep Method: EPA 3020 03/23/99 KEK 7782-49-2 03/17/99 Prep Method: EPA 3020 03/18/99 KEK 7440-22-4 03/17/99 Prep Method: EPA 3020 03/23/99 KEK 7440-28-0 03/17/99 Prep Method: EPA 3020 03/31/99 KEK 7440-62-2 03/17/99 Laboratory Certification IDs Laboratory Certification IDS NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TIM Drinking Water 02980 INCDrinkingWater 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytocal Asheville, NC 28801 Tel: 828-254-717 Fax: 828-252-4618 DATE: 03/31/99 PAGE: 7 Pace Project Number: 934485 Client Project ID: Landfil.l. Pace SampLe No: 93208973 Date CoLLected: 03/16/99 Matrix: Water Client SampLe ID: MW#4 Date Received: 03/16/99 Parameters Results Units PRIL AnaLyzed Analyst CAS# Footnotes --------------------------------- ---------- --------- ---------- -------- ----- ---------- ---------- Field Services Monitoring We(L Data Method: Prep Method: Fietc! Specific Conductance 39 umhos/cm 03/16/99 MPS Depth of Water 17.38 feet 0 03/16/99 MPS Field Grab Data Method: Prep Method: FieLd PH 5.0 Std. Units 0 03/16/99 MPS FieLd Temperature 15 deg C 0 03/16/99 MPS MetaLs Metats, 1CP Method: EPA 6010 Prep Method: EPA 3010 Barium 0.10 mg/l 0.1 03/22/99 KEK 7440-39-3 Copper ND mg/L 0.01 03/22/99 KEK 7440-50-8 Nickel. ND mg/L 0.05 03/22/99 KEK 7440-02-0 Zinc 0.09 mg/I. 0.01 03/22/99 KEK 7440-66-6 Date Digested 03/17/99 Antimony, AAS Furnace Method: EPA 7041 Prep Method: EPA 3020 Antimony ND mg/L 0.005 03/19/99 KEK 7440-36-0 Date Digested 03/17/99 Arsenic, AAS Furnace Method: EPA 7060 Prep Method: EPA 3020 Arsenic ND mg/t 0.005 03/18/99 KEK 7440-38-2 Date Digested 03/17/99 Bery(Lium, AAS Furnace Method: EPA 7091 Prep Method: EPA 3020 BerytH um ND mg/L 0.001 03/19/99 KEK 7440-41-7 Date Digested 03/17/99 Cadmium, AAS Furnace Method: EPA 7131 Prep Method: EPA 3020 Cadmium ND mg/L 0.001 03/25/99 KEK 7440-43-9 Date Digested 03/17/99 Chromium Furnace Method: EPA 7191 Prep Method: EPA 3020 Chromium 0.007 mg/l 0.002 03/18/99 KEK 7440-47-3 Date Digested 03/17/99 Laboratory Can fication 10s; Laboratoty Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 ING Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 828-254-7176 Fax: 828-252-4618 Pace sample No: 93208973 Client Sample 11): MW#4 DATE: 03/31/99 PAGE: 8 Pace Project Number: 934485 Client Project ID: Landfill. Date Collected: 03/16/99 Matrix: Water Date Received: 03116/99 Parameters Results Units PRL Analyzed Analyst CAS# Footnotes --------------------------------- ---------- --------- ---------- -------- ----- ---------- ---------- Cobalt, AAS Furnace Method: EPA 7201 Prep Method: EPA 3020 cobalt 0.002 mg/L 0.002 03/23/99 KEK 7440-48-4 Date Digested 03/17/99 Lead, AAS Furnace Lead Date Digested Selenium, AAS Furnace Selenium Date Digested silver by Furnace silver Date Digested ThatLium, AAS Furnace Thaltium Date Digested Vanadium, AAS Furnace Vanadium Date Digested Method: EPA 7421 NO mg/l. 0.005 Method: EPA 7740 No mg/L 0.005 Method: EPA 7761 NO mg/1. 0.002 Method: EPA 7841 No mg/L 0.002 Method: EPA 7911 No mg/l 0.005 Prep Method: EPA 3020 03/22/99 KEK 7439-92-1 03/17/99 Prep Method: EPA 3020 03/31/99 KEK 7782-49-2 03/17/99 Prep Method: EPA 3020 03/18/99 KEK 7440-22-4 03/17/99 Prep Method: EPA 3020 03/23/99 KEK 7440-28-0 03/17/99 Prep Method: EPA 3020 03/31/99 KEK 7440-62-2 03/17/99 Laboratory Certification IDs Laboratory Certificat on IDS NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980 NCDrinkingWater 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc, Pace Analytical Servus, Inc. 54 Ravenscroft Drive Pace Analytmcal Asheville, NC 28801 Tel: 828-254-7176 Fax: 828-252-4618 DATE: 03/31/99 PAGE: 9 Pace Project Number: 934485 Client Project ID: Landfill Pace Sample No: 93208999 Date Collected: 03/16/99 Matrix: Water Client Sample ID: EQUIPMENT SLANK-ASH031699 Date Received: 03/16/99 Parameters --------------------------------- Results Units ---------- --------- PRIL ---------- Analyzed -------- Analyst ----- CAS# ---------- Footnotes ---------- Metals Metals, ICP Method: EPA 6010 Prep Method: EPA 3010 Bari um ND mg/L 0.1 03/22/99 KEK 7440-39-3 Copper ND mg/L 0.01 03/22/99 KEK 7440-50-8 Nickel ND mg/L 0.05 03/22/99 KEK 7440-02-0 Zinc ND mg/t 0.01 03/22/99 KEK 7440-66-6 Date Digested 03/17/99 Antimony, AAS Furnace Method: EPA 7041 Prep Method: EPA 3020 Antimony ND mg/L 0.005 03/19/99 KEK 7440-36-0 Date Digested 03/17/99 Arsenic, AAS Furnace Method; EPA 7060 Prep Method: EPA 3020 Arsenic ND mg/L 0.005 03/18/99 KEK 7440-38-2 Date Digested 03/17/99 Beryllium, AAS Furnace Method: EPA 7091 Prep Method: EPA 3020 Beryllium ND mg/I 0.001 03/19/99 KEK 7440-41-7 Date Digested 03/17/99 Cadmium, AAS Furnace Method: EPA 7131 Prep Method: EPA 3020 Cadmium ND mg/L 0.001 03/25/99 KEK 7440-43-9 Date Digested 03/17/99 Chromium Furnace Method: EPA 7191 Prep Method: EPA 3020 Chromium ND mg/L 0.002 03/18/99 KEK 7440-47-3 Date Digested 03/17/99 Cobalt, AAS Furnace Method: EPA 7201 Prep Method: EPA 3020 cobalt ND mg/t 0.002 03/23/99 KEK 7440-48-4 Date Digested 03/17/99 Lead, AAS Furnace Method: EPA 7421 Prep Method: EPA 3020 Lead ND mg/t 0.005 03/22/99 KEK 7439-92-1 Date Digested 03/17/99 Selenium, AAS Furnace Method: EPA 7740 Prep Method: EPA 3020 Selenium ND mg/L 0.005 03/31/99 KEK 7782-49-2 Laboratory Certification IDS Laboratory Carl fication IDS NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 INC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Servfces, Inc. 54 Ravenscroft Drive Pace Analytical Asheville, NC 28801 Tel: 828-254-7176 Fax: 828-252-4618 DATE: 03/31/99 PAGE: 10 Pace Project Number: 934485 Ctient Project ID: LandfiLL Pace SampLe No: 93208999 Date CotLected: 03/16/99 Matrix: Water CHent sample ID: EQUIPMENT BLANK-ASH031699 Date Received: 03/16/99 Parameters --------------------------------- ResuLts Units ---------- --------- PRL ---------- AnaLyzed Anatyst CAS# Footnotes Date Digested -------- 03/17/99 ----- ---------- ---------- SiLver by Furnace Method: EPA 7761 Prep Method: EPA 3020 Silver ND mg/L 0.002 03/18/99 KEK 7440-22-4 Date Digested 03/17/99 ThaLLium, AAS Furnace Method: EPA 7841 Prep Method: EPA 3020 Thal.Lium ND mg/t 0.002 03/23/99 KEK 7440-28-0 Date Digested 03/17/99 Vanadium, AAS Furnace Method: EPA 7911 Prep Method: EPA 3020 Vanadium ND mg/L 0.005 03/31/99 KEK 7440-62-2 Date Digested 03117/99 Laboratory Certification JDs INC Wastewater 40 REPORT OF LABORATORY ANALYSIS NCDrInkIngWater 37712 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Laboratory Certif cation I Ds TIN Drinking Water 02980 SC Environmental 99030 Pace Analytical Services, Inc. 54 Ravenscroft Drive Pace Analytocal Asheville, NC 28801 Tel: 828-254-71 7F Fax: 828-252-4618 DATE: 03/31/99 PAGE: 11 Pace Project Number: 934485 Ctient Project ID: LandfiLL PARAMETER FOOTNOTES NO Not Detected NC Not Calculable PRIL Pace Reporting Limit Laboratory Certification IDs Laboratory Certification Us NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc- 9800 Kincey Avenue, Suite 100 Pace Analytical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 03/30/99 PAGE: I McDowel I County Landf i I L 10 East Court St. Marion, NC 28752 Attn: Mr. Mike GLadden SoLid results are reported on a dry weight basis Pace Project Number: 925122 CHent Project ID: MCDOWELL - 934485 Pace Sample No: 92370683 Date COLLected: 03/16/99 Matrix: Water CHent Sample ID: MW-1 Date Received: 03/17/99 Parameters Results ------------------ -------------- ------- GC/MS VotatiLes Units PRL AnaLyzed Analyst CAB# Footnotes GC/MS VOCs by 8260 Method: EPA 8260 Prep Method: EPA 8260 ChLoromethane ND ug/t 10 03/25/99 VFT 74-87-3 Vinyl ChLoride NO ug/L 10 03/25/99 VFT 75-01-4 Bromomethane ND ug/L 10 03/25/99 VFT 74-83-9 ChLoroethane ND ug/l 10 03125/99 VFT 75-00-3 TrichLorofluoromethane ND ug/L 10 03/25/99 VFT 75-69-4 Acetone NO ug/L 100 03/25/99 VFT 67-64-1 1,1-Dichtoroethene IND ug/t 5 03/25/99 VFT 75-35-4 lodomethane ND ug/t 5 03/25/99 VFT 74-88-4 Acrylonitrite ND ug/L 100 03/25/99 VFT 107-13-1 Methytene Chloride ND ug/L 5 03/25/99 VFT 75-09-2 Carbon Disutfide ND ug/L 5 03/25/99 VFT 75-15-0 trans- 1 , 2-Dich I oroethene ND ug/L 5 03/25/99 VFT 156-60-5 1,1-DichLoroethane ND ug/t 5 03/25/99 VFT 75-34-3 Vinyl Acetate ND ug/L 50 03/25/99 VFT 108-05-4 2-Butanone ND ug/L 100 03/25/99 VFT 78-93-3 cis-1,2-DichLoroethene ND ug/L 5 03/25/99 VFT 156-59-2 Chtoroform ND ug/L 5 03/25/99 VFT 67-66-3 BromochLoromethare ND ug/L 5 03/25/99 VFT 74-97-5 1,1,1-Trichloroethane ND ug/L 5 03/25/99 VFT 71-55-6 1,2-Dichtoroethane ND ug/1 5 03/25/99 VFT 107-06-2 Carbon Tetrachloride ND ug/t 5 03/25/99 VFT 56-23-5 Benzene MID ug/L 5 03/25/99 VFT 71-43-2 Trichloroethene ND ug/L 5 03/25/99 VFT 79-01-6 1,2-DichLoropropane ND ug/l. 5 03/25/99 VFT 78-87-5 Dibromomethane ND ug/t 5 03/25/99 VFT 74-95-3 BromodichLoromethane ND ug/L 5 03/25/99 VFT 75-27-4 Laboratory Certification IlDs Laboratory Certification IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analytical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 03/30/99 PAGE: 2 Pace Project Number: 925122 CHent Project ID: MCDOWELL - 934485 Pace Sampte No: 92370683 Date CoiLected: 03/16/99 Matrix: Water CLient Sampte ID: MW-1 Date Received: 03/17/99 Parameters --------------------------------- ResuLts .......... Units --------- PRL AnaLyzed AnaLyst CAS# Footnotes 4-MethyL-2-Pentanone NO ug/l. ---------- so -------- 03/25/99 ----- VFT ---------- ---------- 108-10-1 cis-1,3-DichLorapropene NO ug/t 5 03/25/99 VFT 10061-01-5 ToLuene ND ug/L 5 03/25/99 VFT 108-88-3 trans -1 3-DichL or opropene NO ug/L 5 03/25/99 VFT 10061-02-6 1,1,2-Trichlorcethane NO ug/L 5 03/25/99 VFT 79-00-5 2-Hexanone NO ug/L 50 03125/99 VFT 591-78-6 D i bromoch [ orometh one ND ug/L 5 03/25/99 VFT 124-48-1 T at rach I. o root In ene NO ug/1 5 03/25/99 VFT 127-18-4 1,2-Dibromoethane ND ug/1 5 03/25/99 VFT 106-93-4 Chtorobenzene NO Uq/L 5 03/25/99 VFT 108-90-7 1 , I , I , 2 - T at ra ch I. o roet hane ND ug/L 5 03/25/99 VFT 630-20-6 EthyLbenzene NO ug/L 5 03/25/99 VFT 100-41-4 m&p-Xytene NO ug/1 10 03/25/99 VFT 7816-60-0 Styrene No ug/L 5 03/25/99 VFT 100-42-5 o-XyLene (1,2-DimethyLbenzene) ND ug/L 5 03/25/99 VFT 95-47-6 Bromoform NO ug/l. 5 03/25/99 VFT 75-25-2 1,1,2,2-Tetrachtoroethane NO ug/t 5 03/25/99 VFT 79-34-5 1,2,3-Trichtoropropane NO uq/L 5 03/25/99 VFT 96-18-4 trans-1,4-Dichtoro-2-Butene ND ug/L 5 03/25/99 VFT 110-57-6 1,4-Dichtorobenzene NO ug/l. 5 03/25/99 VFT 106-46-7 1,2-DichLorobenzene NO ug/L 5 03/25/99 VFT 95-50-1 1,2-Dibromo-3-Chtoropropane ND ug/L 5 03/25/99 VFT 96-12-8 Dibromofluoromethane (S) 91 % 03/25/99 VFT 1868-53-7 1,2-Dichtoroethane-d4 (S) 82 % 03/25/99 VFT 17060-07-0 Toluene-d8 (S) 100 % 03/25/99 VFT 2037-26-5 4-Bromof Luorobenzene (S) 100 % 03/25/99 VFT 460-00-4 Laboratory Certification IDs Laboratory Certification lDs NC Wastewater 12 KY Drinking Water 90090 INC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LET List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, INC 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 03/30/99 PAGE. 3 Pace Project Number: 925122 Client Project ID: MCDOWELL - 934485 Pace SarnpLe No: 92370691 Date CotLected: 03/16/99 Matrix: Water Ctient Sampte ID: MW-2 Date Received: 03/17/99 Parameters Resutts Units PRL Anatyzed Analyst CAS# Footnotes --------------------------------- ---------- --------- ---------- -------- ----- ------- -- ---------- GC/MS VoLatites GC/MS VOCs by8260 Method: EPA 8260 Prep Method: EPA 8260 ChLoromethane NO ug/l 10 03/25/99 VFT 74-87-3 Vinyl ChLoride NO ug/L 10 03/25/99 VFT 75-01-4 Bromomethane NO ug/L 10 03/25/99 vrT 74-83-9 Chtoroethane NO ug/t 10 03/25/99 VFT 75-00-3 Trichtorof Luoromethane NO ug/L 10 03/25/99 VFT 75-69-4 Acetone NO ug/L 100 03/25/99 VFT 67-64-1 1 1-DichLoroethene IND ug/t 5 03/25/99 VFT 75-35-4 lodomethane ND ug/L 5 03/25/99 VFT 74-88-4 AcryLonitrite NO ug/L 100 03/25/99 VFT 107-13-1 MethyLene Chtoride NO ug/t 5 03/25/99 VFT 75-09-2 Carbon Disuifide NO ug/L 5 03/25/99 VFT 75-15-0 trans- 1, 2-Dich toroethene ND ug/L 5 03/25/99 VFT 156-60-5 1,1-DichLoroethane 15 ug/L 5 03125/99 VFT 75-34-3 Vinyl. Acetate NO ug/L 50 03/25/99 VFT 108-05-4 2-Butanone NO ug/1 100 03/25/99 VFT 78-93-3 cis- 1 2-Dichtoroethene 140 ug/L 5 03/25/99 VFT 156-59-2 Chloroform ND ug/L 5 03/25/99 VFT 67-66-3 Bromochtoromethane NO ug/t 5 03/25/99 VFT 74-97-5 1,1,1-Trichloroethane NO ug/L 5 03/25/99 VFT 71-55-6 1,2-Dichioroethane ND ug/L 5 03/25/99 VFT 107-06-2 Carbon Tetrachloride NO Ug/1 5 03/25/99 VFT 56-23-5 Benzene 13 ug/L 5 03/25/99 VFT 71-43-2 TrichLoroethene ND ug/L 5 03/25/99 VFT 79-01-6 1,2-DichLoropropane NO ug/t 5 03/25/99 VFT 78-87-5 Dibromomethane No ug/L 5 03/25/99 VFT 74-95-3 BromodichLoromethane NO Ug/t 5 03/25/99 VFT 75-27-4 4-MethyL-2-Pentanone NO ug/L 50 03/25/99 VFT 108-10-1 cis-1,3-Dichloropropene ND Uq/t 5 03/25/99 VFT 10061-01-5 ToLuene 26 us/[ 5 03/25/99 VFT 108-88-3 trans-1,3-Dichtoropropene ND ug/L 5 03/25/99 VFT 10061-02-6 1,1,2-TrichLoroethane NO ugit 5 03/25/99 VFT 79-00-5 2-Nexanone NO ug/l 50 03/25/99 VFT 591-78-6 DibromochLoromethane ND ug/L 5 03/25/99 VFT 124-48-1 Tetrachtoroethene NO ug/t 5 03/25/99 VFT 127-18-4 1,2-Dibromoethane NO ug/L 5 03/25/99 VFT 106-93-4 ChLorobenzene NO Uq/t 5 03/25/99 VFT 108-90-7 Laboratory Certifi ation IDs Laboratory Certification IM NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-875-909" Fax: 704-875-9091 DATE: 03/30/99 PAGE: 4 Pace Project Number: 925122 Client Project ID: MCDOWELL - 934485 Pace SampLe No: 92370691 Date ColLected: 03/16/99 Matrix: Water CLient SampLe 10: MW-2 Date Received: 03/17/99 Parameters ------------------ -------------- ResuLts ---------- Units PIRL Analyzed Analyst CAS# 1,1,1,2-Tetrachloroethane ND --------- ug/l ---------- 5 -------- 03/25/99 ----- VFT ---------- 630-20-6 EthyLbenzene ND ug/L 5 03/25/99 VFT 100-41-4 m&p-Xytene 13 ug/t 10 03/25/99 VFT 7816-60-0 Styrene NO ug/t 5 03/25/99 VFT 100-42-5 o-Xytene (1,2-Dim�ethytbenzene) 11 ug/L 5 03/25/99 VFT 95-47-6 Bromform NO ug/t 5 03/25/99 VFT 75-25-2 1,1,2,2-Tetrachtorcethane NO Uq/1. 5 03/25/99 VFT 79-34-5 1,2,3-Trichtoropropane ND ug/L 5 03/25/99 VFT 96-18-4 trans-1,4-Dichloro-2-Butene NO ug/L 5 03/25/99 VFT 110-57-6 1,4-DichLorobenzene 7.1 ug/1. 5 03/25/99 VFT 106-46-7 1,2-Dichtorobenzene ND ug/L 5 03/25/99 VFT 95-50-1 1,2-Dibromo-3-ChLoropropane NO Ug/1 5 03/25/99 VFT 96-12-8 Dibromoftuoromethane (S) 96 % 03/25/99 VFT 1868-53-7 1,2-Dichloroethane-d4 (S) 92 % 03/25/99 VFT 17060-07-0 ToLuene-d8 (S) 102 % 03/25/99 VFT 2037-26-5 4-BromofLuorobenzene (S) 103 % 03/25/99 VFT 460-00-4 Footnotes ---------- Laboratory Certification Laboratory Certification IDS KY Drinking Water 90090 REPORT OF LABORATORY ANALYSIS TIN UST List This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. IDs NC Wastewater 12 INC Drinking Water 37706 SC 99006 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analytical Huntersvilfe, NC 28078 Tel: 704-875-9097 Fax:704-875-9091 DATE: 03/30/99 PAGE: 5 Pace Project Number: 925122 Client Project ID: MCDOWELL - 934485 Pace Sampte No: 92370709 Date CotLected: 03/16/99 Matrix: Water CHent sample ID: mw-3 Date Received: 03/17/99 Parameters ResuLts Units PRL AnaLyzed AnaLyst CAS# Footnotes --------------- ----------------- ---------- --------- ---------- -------- ----- ---------- ---------- GC/MS Votatites GCJMS VOCs by 8260 Method: EPA 8260 Prep Method: EPA 8260 ChLoromethane ND ug/L 10 03/25/99 VFT 74-87-3 Vinyl Chtoride NO ug/1 10 03/25/99 VFT 75-01-4 Bromomethane ND ug/t 10 03/25/99 VFT 74-83-9 Chloroethane ND ug/L 10 03/25/99 VFT 75-00-3 TrichLorofLuoromethane NO ug/L 10 03/25/99 VFT 75-69-4 Acetone NO uq/t 100 03/25/99 VFT 67-64-1 1,1-DichLaroethene ND ug/l. 5 03/25/99 VFT 75-35-4 Iodomethane ND ug/L 5 03/25/99 VFT 74-88-4 AcryLonitrile NO ug/L 100 03/25/99 VFT 107-13-1 Methylene Chloride NO ug/t 5 03/25/99 VFT 75-09-2 Carbon Disu[fide ND us/[ 5 03/25/99 VFT 75-15-0 trans- 1, 2-Dich toroethene NO ug/L 5 03/25/99 VFT 156-60-5 1,1-DichLoroethane NO ug/L 5 03/25/99 VFT 75-34-3 Vinyl Acetate NO ug/l. 50 03/25/99 VFT 108-05-4 2-Butanone ND ug/L 100 03/25/99 VFT 78-93-3 cis- I 2-D ichloroethene NO ug/L 5 03/25/99 VFT 156-59-2 Ch(oroform ND ug/i 5 03/25/99 VFT 67-66-3 Bromochtoromethane NO ug/l 5 03/25/99 VFT 74-97-5 1,1,1-Trichtoroethane NO ug/L 5 03/25/99 VFT 71-55-6 1,2-DichLoroethane NO ug/1 5 03/25/99 VFT 107-06-2 Carbon TetrachLoride ND ug/t 5 03/25/99 VFT 56-23-5 Benzene NO ug/L 5 03/25/99 VFT 71-43-2 Trichtoroethene ND ug/L 5 03/25/99 VFT 79-01-6 1,2-Dichtorapropane ND ug/l. 5 03/25/99 VFT 78-87-5 Dibromomethane ND ug/t 5 03125/99 VFT 74-95-3 BromodichLorom,ethane NO ug/L 5 03/25/99 VFT 75-27-4 4-MethyL-2-Pentanone NO ug/l, 50 03/25/99 VFT 108-10-1 cis- 1,3-Dichloropropene ND ug/l 5 03/25/99 VFT 10061-01-5 Toluene NO ug/L 5 03/25/99 VFT 108-88-3 trans-1,3-Dichtoropropene NO ug/L 5 03/25/99 VFT 10061-02-6 1,1,2-Trichloroethane NO ug/1 5 03/25/99 VFT 79-00-5 2-Hexanone ND ug/t 50 03/25/99 VFT 591-78-6 DibromochLoromethane ND ug/L 5 03/25/99 VFT 124-48-1 Tetrachtoroethene ND ug/L 5 03/25/99 VFT 127-18-4 1,2-Dibromoethane ND ug/t 5 03/25/99 VFT 106-93-4 Chlorobenzene NO ug/L 5 03/25/99 VFT 108-90-7 Laboratory Certification IDs Laboratoty Cerdfication IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 03/30/99 PAGE: 6 Pace Project Number: 925122 Client Project ID: MCDOWELL - 934485 Pace Sample No: 92370709 Date Collected: 03/16199 Matrix: Water Client Sample ID: MW-3 Date Received: 03/17/99 Parameters ------------------------------ Results ---------- Units --------- PRL AnaLyzed AnaLyst CAS# 1, 1 , 1 2-Tetrach I oroethane ND us/[ ---------- 5 -------- 03/25/99 ----- VFT ---------- 630-20-6 Ethyllbenzene ND Ug/t 5 03/25/99 VFT 100-41-4 m&p-Xytene ND ug/L 10 03/25/99 VFT 7816-60-0 Styrene ND ug/L 5 03/25/99 VFT 100-42-5 o-Xylene (1,2-Dimethytbenzene) ND Ug/t 5 03/25/99 VFT 95-47-6 Bromform ND Ug/t 5 03/25/99 VFT 75-25-2 1,1,2,2-TetrachLoroethane ND ug/L 5 03/25/99 VFT 79-34-5 1,2,3-Trichloropropane ND ug/l 5 03/25/99 VFT 96-18-4 trans-1,4-Dichloro-2-Butene ND Uq/L 5 03/25/99 VFT 110-57-6 1,4-Dichlorobenzene ND ug/L 5 03/25/99 VFT 106-46-7 1,2-DichLorobenzene ND ug/l 5 03/25/99 VFT 95-50-1 1, 2-D i bromo-3 - Ch I. oropropane ND ug/l 5 03/25/99 VFT 96-12-8 Dibromofluoromethane (s) 96 % 03/25/99 VFT 1868-53-7 1,2-DichLoroethane-d4 (S) 93 % 03/25/99 VFT 17060-07-0 ToLuene-d8 (S) 101 % 03/25/99 VFT 2G37-26-5 4-Bromoftuorobenzene (S) 105 % 03/25/99 VFT 460-00-4 Footnotes ---------- Laboratory Certification lDs Laboratory Certification IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List SC; 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Ki ncey Aven ue, S u ite 100 Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 03/30/99 PAGE: 7 Pace Project Nurnber: 925122 CHent Project ID: MCDOWELL - 934485 Pace Sampte No: 92370717 Date ColLected: 03/16/99 Matrix: Water CHent SampLe ID: MW-4 Date Received: 03/17/99 Paramters Resutts Units PRL AnaLyzed AnaLyst CAS# Footnotes --------------------------------- ---------- --------- ---------- -------- ----- ---------- --------- GC/MS VoLatiles GC/MS VOCs by 8260 Method: EPA 8260 Prep Method: EPA 8260 Ch Loromethane ND ug/l 10 03/25/99 VFT 74-87-3 Vinyl. ChLoride NO ug/L 10 03/25199 VFT 75-01-4 Bromomethane NO ug/L 10 03/25/99 VFT 74-83-9 ChLoroethane NO ug/L 10 03/25/99 VFT 75-00-3 TrichLorof Luoromethane NO ug/l 10 03/25/99 VFT 75-69-4 Acetone NO ug/L 100 03/25/99 VFT 67-64-1 1 1-DichLoroethene ND ug/L 5 03/25/99 VFT 75-35-4 loclomethane ND ug/t 5 03/25/99 VFT 74-88-4 AcryLonitrile NO ug/1 100 03/25/99 VFT 107-13-1 MethyLene ChLoride NO ug/L 5 03/25/99 VFT 75-09-2 Carbon Disuificle ND ug/l 5 03125/99 VFT 75-15-0 trans- 1 2-Dich Loroethere NO ug/l 5 03/25/99 VFT 156-60-5 1,1-DichLoroethane NO ug/L 5 03/25/99 VFT 75-34-3 Vinyl Acetate ND ug/L 50 03/25/99 VFT 108-05-4 2-Butanone ND ugjt 100 03/25/99 VFT 78-93-3 cis- 1, 2-D ichloroethene NO ug/t 5 03/25/99 VFT 156-59-2 ChLoroform NO ug/L 5 03/25/99 VFT 67-66-3 Bromochioromethane ND ug/L 5 03/25/99 VFT 74-97-5 1,1,1-Trichloroethane NO ug/l. 5 03/25/99 VFT 71-55-6 1,2-DichLoroethane NO ug/L 5 03/25/99 VFT 107-06-2 Carbon Tetrachloride ND ug/L 5 03/25/99 VFT 56-23-5 Benzene ND ug/1 5 03/25/99 VFT 71-43-2 TrichLoroethene NO ug/t 5 03/25/99 VFT 79-01-6 1,2-DichLorapropane ND ug/L 5 03/25/99 VFT 78-87-5 Dibromomethane ND uq/L 5 03/25/99 VFT 74-95-3 Bromodichlormethane NO ug/1 5 03/25/99 VFT 75-27-4 4-MethyL-2-Pentanone NO ug/L 50 03/25/99 VFT 108-10-1 cis-1,3-Dichloropropene ND ug/L 5 03/25/99 VFT 10061-01-5 ToLuene NO uq/L 5 03/25/99 VFT 108-88-3 trans- 1 3-Dich L oropropene NO ug/l 5 03/25/99 VFT 10061-02-6 1,1,2-Trichtoroethene NO ug/L 5 03/25/99 VFT 79-00-5 2-Hexanone NO ug/L 50 03/25/99 VFT 591-78-6 Dibromochloro�thane NO uq/l 5 03/25/99 VFT 124-48-1 Tetrachtoroethene NO ug/t 5 03/25/99 VFT 127-18-4 1,2-Dibromoethane ND ug/L 5 03/25/99 VFT 106-93-4 ChLorobenzene NO ug/l 5 03/25/99 VFT 108-90-7 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc, Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analytocal Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 03/30/99 PAGE: 8 Pace Project Number: 925122 client Project ID: MCDOWELL - 934485 Pace Sample No: 92370717 Date Collected: 03/16/99 Matrix: Water client Sample ID: MW-4 Date Received: 03/17/99 Parameters --------------------------------- Results ---------- Units --------- PRL Analyzed Analyst CAS# 1, 1 , I 2-Tetrachtoroethane ND ug/L ---------- 5 -------- 03/25/99 ----- VFT ---------- 630-20-6 Ethytbenzene ND ug/t 5 03/25/99 VFT 100-41-4 m&p-Xy(ene NO ug/L 10 03/25/99 VFT 7816-60-0 Styrene ND Ug/t 5 03/25/99 VFT 100-42-5 o-XyLene (1,2-Dimthytbenzene) ND ug/L 5 03/25/99 VFT 95-47-6 Bromoform ND ug/L 5 03/25/99 VFT 75-25-2 1, 1 , 2,2-TetrachLoroethane ND u9/1 5 03/25/99 VFT 79-34-5 1,2,3-Trichtoropropane ND ug/L 5 03/25/99 VFT 96-18-4 trans-1,4-Dichtoro-2-Butene ND ug/L 5 03/25/99 VFT 110-57-6 1,4-DichLorobenzene ND US/[ 5 03/25/99 VFT 106-46-7 1,2-DichLorobenzene ND ug/L 5 03/25/99 VFT 95-50-1 1,2-Dibromo-3-ChLoropropane ND ug/t 5 03/25/99 VFT 96-12-8 Dibromofluoromethane (S) 97 % 03/25/99 VFT 1868-53-7 1,2-Dichtoroethane-d4 (S) 95 % 03/25/99 VFT 17060-07-0 Totuene-d8 (S) 102 % 03/25/99 VFT 2037-26-5 4-BromofLuorobenzene (S) 105 % 03/25/99 VFT 460-00-4 Footnotes Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analyt"cal Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 03/30/99 PAGE: 9 Pace Project Number: 925122 CLient Project 10: MCDOWELL - 934485 Pace SampLe No: 92370725 Date Coltected: 03/16/99 Matrix: Water Client SampLe ID: TRAVEL BLANK Date Received: 03/17/99 Parameters ResuLts Units PRL Anatyzed Analyst CA$# --------------------------------- ---------- --------- ---------- -------- ----- ------- GC/MS VoLatiLes Footnotes GC/MS VOCs by 8260 Method: EPA 8260 Prep Method: EPA 8260 Chtoromethane NO ug/L 10 03/25/99 VFT 74-87-3 Vinyl ChLoride NO ug/l. 10 03/25/99 VFT 75-01-4 Bromomethane NO ug/L 10 03/25/99 VFT 74-83-9 Chtoroethane NO ug/L 10 03/25/99 VFT 75-00-3 TrichLorof Luorcmethane NO Ug/1 10 03/25/99 VFT 75-69-4 Acetone NO ug/l 100 03/25/99 VFT 67-64-1 1,1-Dichtorcethene NO ug/L 5 03/25/99 VFT 75-35-4 lodomethane NO Ug/1 5 03/25/99 VFT 74-88-4 Acrylonitrile NO ug/L 100 03/25/99 VFT 107-13-1 Methytene Chloride No ug/L 5 03/25/99 VFT 75-09-2 Carbon DisuLficle NO Ug/1 5 03/25/99 VFT 75-15-0 trans- 1 2-D ich Loroethene NO ug/L 5 03/25/99 VFT 156-60-5 1,1-Dichtoroethane No ug/L 5 03/25/99 VFT 75-34-3 Vinyl Acetate ND ug/1 50 03/25/99 VFT 108-05-4 2-Butanone NO ug/t 100 03/25/99 VFT 78-93-3 cis-1,2-Dichtoroethene NO ug/L 5 03/25/99 VFT 156-59-2 ChLoroform NO Uq/t 5 03/25/99 VFT 67-66-3 BromochLoromethane NO ug/t 5 03/25/99 VFT 74-97-5 1,1,1-Trichtoroethane NO ug/L 5 03/25/99 VFT 71-55-6 1,2-DichLoroethene NO Ug/L 5 03/25/99 VFT 107-06-2 Carbon TetrachLoride NO ug/t 5 03/25/99 VFT 56-23-5 Benzene NO ug/L 5 03/25/99 VFT 71-43-2 TrichLoroethene NO ug/1 5 03/25/99 VFT 79-01-6 1,2-Dichloropropane NO ug/t 5 03/25/99 VFT 78-87-5 D i bromomethane NO ug/L 5 03/25/99 VFT 74-95-3 B romodi ch L oromethane NO ug/t 5 03/25/99 VFT 75-27-4 4 - Methy L - 2- Pentanone NO ug/t 50 03/25/99 VFT 108-10-1 cis-1,3-Dichlorapropene NO ug/L 5 03/25/99 VFT 10061-01-5 ToLuene NO Ug/t 5 03/25/99 VFT 108-88-3 t rans - 1 3 -D i ch L oropropene NO ug/t 5 03/25/99 VFT 10061-02-6 1 , 1 2- T r i ch 1. oroethane NO ug/L 5 03/25/99 VFT 79-00-5 2-Hexanone NO Ug/t 50 03/25/99 VFT 591-78-6 D i bromoch I oromethane NO ug/t 5 03/25/99 VFT 124-48-1 Tat rach t oroethene NO ug/L 5 03/25/99 VFT 127-18-4 1, 2 - D i bromoethane NO ug/t 5 03/25/99 VFT 106-93-4 ChLorobenzene NO ug/t 5 03/25/99 VFT 108-90-7 Laboratory Certification lDs Laboratory Certification IDs INIC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN LIST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Fax: 704-875-9091 DATE: 03/30/99 PAGE: 10 Pace Project Number: 925122 Ctient Project ID: MCDOWELL - 934485 Pace SampLe No: 92370725 Date Cottected: 03/16/99 Matrix: Water Ctient Sampte ID: TRAVEL BLANK Date Received: 03/17/99 Parameters --------------------------------- Resutts ---------- Units --------- PRL AnaLyzed Anatyst CAS# 1, 1 1 2-TetrachLoroethane ND ug/L ---------- 5 -------- 03125/99 ----- VFT ---------- 630-20-6 Ethylbenzene ND ug/L 5 03/25/99 VFT 100-41-4 rdp-Xytene ND ug/1 10 03/25/99 VFT 7816-60-0 Styrene ND uq/L 5 03/25/99 VFT 100-42-5 o-Xylene (1,2-DimthyLbenzene) ND uq/L 5 03/25/99 VFT 95-47-6 Bromoform ND ug/t 5 03/25/99 VFT 75-25-2 1, 1 2,2-Tetrachtoroethane IND ug/t 5 03/25/99 VFT 79-34-5 1,2,3-Trichtoropropane ND ug/L 5 03/25/99 VFT 96-18-4 trans-1,4-DichLoro-2-Butene ND Uq/t 5 03/25/99 VFT 110-57-6 1,4-Dichlorobenzene ND ug/t 5 03/25/99 VFT 106-46-7 1,2-DichLorobenzene ND ug/L 5 03/25/99 VFT 95-50-1 1, 2- D i brow-3- Ch ( oropropane ND ug/t 5 03/25/99 VFT 96-12-8 Dibromoftuoronmethane (S) 97 % 03/25/99 VFT 1868-53-7 1,2-DichLoroethane-d4 (S) 96 % 03/25/99 VFT 17060-07-0 Totuene-d8 (S) 101 % 03/25/99 VFT 2037-26-5 4-Bromoftuorobenzene (S) 103 % 03/25/99 VFT 460-00-4 Footnotes Laboratory Certification IDs Laboratory Certification IDS NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 03/30/99 PAGE: 11 Pace Project Number: 925122 CLient Project ID: MCDOWELL - 934485 Pace Sampte No: 92370733 Date CoLLected: 03/16/99 Matrix: Water Client Sampte ID: EQUIP BLANK A13 Date Received: 03/17/99 Parameters Results Units PRIL Analyzed Analyst CAS# Footnotes -------------- ------------------ ---------- --------- ---------- -------- ----- ---------- ---------- GC/MS VoLatiles GC/MS VOCs by 8260 Method: EPA 8260 Prep Method: EPA 8260 Chloromethame ND ug/L 10 03/25/99 VFT 74-87-3 Vinyl ChLoride NO ug/L 10 03/25/99 VFT 75-01-4 Bromomethane NO ug/t 10 03/25/99 VFT 74-83-9 Chtoroethane NO ug/L 10 03/25/99 VFT 75-00-3 TrichLoroftuoromethane NO ug/1 10 03/25/99 VFT 75-69-4 Acetone NO ug/l 100 03/25/99 VFT 67-64-1 1,1-DichLoroethene ND ug/L 5 03/25/99 VFT 75-35-4 lodomethane NO ug/I. 5 03/25/99 VFT 74-88-4 AcryLonitrile ND ug/L 100 03/25/99 VFT 107-13-1 Methytene ChLoride NO ug/L 5 03/25/99 VFT 75-09-2 Carbon Disulfide ND ug/t 5 03/25/99 VFT 75-15-0 trans- 1 2-Dich Loroethene NO ug/L 5 03/25/99 VFT 156-60-5 1,1-Dichloroethane NO ug/l. 5 03/25/99 VFT 75-34-3 Vinyl Acetate ND ug/L 50 03/25/99 VFT 108-05-4 2-Butanone NO ug/1 100 03/25/99 VFT 78-93-3 cis-1,2-Dichtoroethene ND ug/( 5 03/25/99 VFT 156-59-2 ChLoroform ND ug/L 5 03/25/99 VFT 67-66-3 Bromochtoromethane NO ug/1 5 03/25/99 VFT 74-97-5 1,1,1-Trichtoroethane ND uq/t 5 03/25/99 VFT 71-55-6 1,2-DichLoroethane NO ug/L 5 03/25/99 VFT 107-06-2 Carbon Tetrachtoride ND ug/l 5 03/25/99 VFT 56-23-5 Benzene NO ug/L 5 03/25/99 VFT 71-43-2 TrichLoroethene NO ug/1 5 03/25/99 VFT 79-01-6 1,2-DichLoropropane ND ug/L 5 03/25/99 VFT 78-87-5 Dibrommethane NO ug/L 5 03/25/99 VFT 74-95-3 BromodichLoromethane NO ug/t 5 03/25/99 VFT 75-27-4 4-Methyt-2-Pentanone ND ug/L 50 03/25/99 VFT 108-10-1 cis-1,3-Dichloropropene NO ug/l. 5 03/25/99 VFT 10061-01-5 ToLuene ND ug/L 5 03/25199 VFT 108-88-3 trans- 1 3-Dich Loropropene NO ug/L 5 03/25/99 VFT 10061-02-6 1,1,2-TrichLoroethane NO ug/t 5 03/25/99 VFT 79-00-5 2-Hexanone ND ug/L 50 03/25/99 VFT 591-78-6 DibromochLoromethane NO ug/t 5 03/25/99 VFT 124-48-1 Tetrachloroethene ND ug/L 5 03/25/99 VFT 127-18-4 1,2-Dibromoethane NO ug/t 5 03/25/99 VFT 106-93-4 Ch(crobenzene NO ug/L 5 03/25/99 VFT 108-90-7 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc, Pace Anaiytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analytocal Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 03/30/99 PAGE: 12 Pace Project Number: 925122 CHent Project ID: MCDOWELL - 934485 Pace Sampte No: 92370733 Date CotLected: 03/16/99 Matrix: Water Client Sample ID: EQUIP BLANK A13 Date Received: 03/17/99 Parameters --------------- ----------------- ResuLts -------- Units - --------- PRL AnaLyzed Analyst CA$* 1,1,1,2-Tetrachtoroethane NO ug/t ---------- 5 -------- 03/25/99 ..... VFT ---------- 630-20-6 EthyLbenzene NO ug/L 5 03/25/99 VFT 100-41-4 m&p-XyLene NO ug/L 10 03/25/99 VFT 7816-60-0 Styrene NO ug/I 5 03/25/99 VFT 100-42-5 o-XyLene (1,2-Dimthytbenzene) NO ug/L 5 03/25/99 VFT 95-47-6 Bromoform NO ug/L 5 03/25/99 VFT 75-25-2 1,1,2,2-TetrachLoroethane NO ug/t 5 03/25/99 VFT 79-34-5 1,2,3-Trichloropropane NO ug/l 5 03/25/99 VFT 96-18-4 trans-1,4-Dichtoro-2-Butene NO ug/L 5 03/25/99 VFT 110-57-6 1,4-Dichtorobenzene NO ug/L 5 03/25/99 VFT 106-46-7 1,2-Dichlorobenzene NO ug/t 5 03/25/99 VFT 95-50-1 1,2-Dibromo-3-Chtoropropane NO ug/L 5 03/25/99 VFT 96-12-8 Dibromofluoromethane (S) 97 % 03/25/99 VFT 1868-53-7 1,2-Dichtoroethane-d4 (5) 92 % 03/25/99 VFT 17060-07-0 ToLuene-dB (S) 101 % 03/25/99 VFT 2037-26-5 4-BromofLuorobenzene (S) 102 % 03/25/99 VFT 460-00-4 Footnotes ---------- Laboratory Cerfification IDs Laboratory Certification IDS NC Wastewater 12 KY Drinking Water 90090 ING Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN LIST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analytical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 03/30/99 PAGE: 13 Pace Project Nwber: 925122 CLient Project ID: MCDOWELL - 934485 PARAMETER FOOTNOTES NO Not Detected Nc Not Calculable PRIL Pace Reporting Limit (S) Surrogate Laboratory Certification IDS Laboratory Certification IDS NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analytical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 McD owe 1. 1 County L a ndf i L I 10 East Court St. Marion, NC 28752 Attn: Mr. Mike Gladden OC Batch ID: 10762 AnaLysis Method: EPA 8260 Associated Pace Samples: Associated Pace Samples: Parameter ChLoromethane Vinyl. ChLoride Bromomethane ChLoroethane Trichlorof Luoromethane Acetone 1,1-Dichtoroethene lodomethane Acrylonitrite MethyLene ChLoride Carbon Disutficle trans-1,2-DichLoroethene 1,1-Dichtoroethane Vinyl Acetate 2-Butanone cis-1,2-DichLoroethene Chloroform BromochLoromethane 1,1,1-TrichLoroethane 1,2-DichLoroethane Carbon TetrachLoride Benzene Trichtoroethene 1,2-DichLoropropane 92370683 92370733 92370683 Units Ug/ I Ug/ I uq/ ug/ ug/ L ug/ I ug/ L ug/ L ug/ I Ug/ t ug/ L Ug/ ug/ ug/ ug/L ug/ I ug/ I ug/ I ug/ t ug/ I uq/ I US/ I. ug/ L uq/ L QUALITY CONTROL DATA DATE: 03/30/99 PAGE: 14 Pace Project Number: 925122 CLient Project ID: MCDOWELL - 934485 QC Batch Method: EPA 8260 Analysis Description: GC/MS VOCs by 8260 92370691 92370709 92370717 92370725 92370691 92370709 92370717 Method Btank ResuLt PRIL Footnotes ---------- ---------- ---------- NO 10 NO 10 NO 10 NO 10 NO 10 NO 100 NO 5 NO 5 NO 100 NO 5 NO 5 NO 5 ND 5 NO 50 NO 100 NO 5 NO 5 NO 5 NO 5 NO 5 NO 5 NO 5 NO 5 NO 5 92370725 92370733 Laboratory Certification IDs Laboratory Certification lDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analytical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 METHOD BLANK: 92383322 Associated Pace Samples: Parameter QUALITY CONTROL DATA DATE: 03/30/99 PAGE: 15 Pace Project Number: 925122 CLient Project ID: MCDOWELL - 934485 92370683 92370691 92370709 Method BLank Units ResuLt PRL 92370717 92370725 92370733 Footnotes ------------------------------ Dibromomethane ---------- ug/l ---------- ND ---------- ---------- 5 BrowdichLoromethane ug/L NO 5 4-Methyt-2-Pentanone Ug/L NO 50 cis- I 3-Dich toropropene Ug/l NO 5 Totuene ug/L NO 5 transwl,3-DichLoropropene ug/L NO 5 1,1,2-TrichLorcethane Ug/t ND 5 2-Hexanone ug/t ND 50 Dibromochloromethane ug/L NO 5 Tetrachtoroethene Ug/t ND 5 1,2-Dibromoethane uq/L NO 5 ChLorobenzene ug/L NO 5 1,1,1,2-Tetrachloroethane Ug/l ND 5 Ethytbenzene Uq/t ND 5 m&p-Xylene uq/L NO 10 Styrene Ug/L ND 5 o-XyLene (1,2-Dimethyibenzene) ug/l ND 5 Bromoform ug/L NO 5 1,1,2,2-Tetrachtoroethane Uq/t ND 5 1,2,3-Trichtoropropane ug/t ND 5 trans-1,4-Dichloro-2-Butene ug/L NO 5 1,4-Dichtorobenzene uq/1 ND 5 1,2-Dichtorobenzene ug/L No 5 1,2-Dibromo-3-ChLoropropane ug/L NO 5 Dibromoftuoromethane (S) % 97 1,2-Dichtoroethane-d4 (S) % 95 ToLuene-d8 (S) % 101 4-BromofLuorobenzene (S) % 105 LABORATORY CONTROL SAMPLE. 92383330 Spike LCS Spike Parameter ------------------------------ Units ---------- Conc. Resutt % Rec Footnotes ChLoromethane Ug/L ------- 50 ---------- 42.16 ----- --------- 84.3 Vinyl. Chloride ug/L 50 42.24 84.5 Bromomethane uq/t 50 26.61 53.2 Chtoroethane ug/L 50 43.34 86.7 Laboratory Certification 10s Laboratory Certificaton IDS NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List . Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Fax:704-875-9091 QUALITY CONTROL DATA DATE: 03/30/99 PAGE: 16 Pace Project Number: 925122 CHent Project ID: MCDOWELL - 934485 LABORATORY CONTROL SAMPLE: 92383330 Spike LCS Spike Parameter ---------------- ------------- Units -------- Conc. Result % Rec Footnotes Trichtorofluoropathane ug/L - ------- 50 ---------- 43.92 ----- ---------- 87.8 Acetone ug/1 100 97.94 97.9 1 , 1 -Dich I oroethene ug/L 50 50.41 101 loclomethane ug/t 100 55.70 55.7 Acrytonitrite ug/L 500 538.0 108 MethyLene Chtoride ug/t 50 51.82 104 Carbon Disutfide Ug/t 100 106.6 107 trans- 1 2-D ich toroethere ug/t 50 53.28 107 1,1-Dichloroethane ug/L 50 50.81 102 Vinyl. Acetate ug/L 100 139.2 139 2-Butanone ug/t 100 108.9 109 cis-1,2-Dichloroethene ug/L 50 53.72 107 Chloroform ug/L 50 52.96 106 BromochLormethane uq/1. 50 42.18 84.4 1,1,1-TrichLoroethane ug/L 50 54.49 109 1,2-Dichtoroethane ug/L 50 53.19 106 Carbon Tetrachloride ug/1 50 63.22 126 Benzene ug/1. 50 51.75 104 Trichtoroethene uq/t 50 54.55 109 1,2-DichLoropropane ug/t 50 52.06 104 Dibromomethane ug/t 50 54.48 109 BromodichLoromethane ug/L 50 56.94 114 4-MethyL-2-Pentanone ug/L 100 114.1 114 cis- 1 3-Dichtoropropene UR/I 50 53.44 107 Toluene ug/L 50 53.42 107 trans- I 3-Dichloropropene ug/L 50 57.31 115 1,1,2-TrichLoroethane ug/t 50 52.03 104 2-Hexanone ug/L 100 110.2 110 Dibromochtoromethane ug/L 50 57.67 115 Tetrachtoroethene ug/t 50 56.48 113 1,2-Dibromoethane ug/L 50 55.42 ill ChLorobenzene usull 50 52.59 105 1,1,1,2-Tetrachtoroethane ug/t 50 57.44 115 Ethy(benzene ug/L 50 52.33 105 m&p-XyLene uq/1 100 107.4 107 Styrene ug/t 50 53.31 107 o-Xytene (1, 2-Dimethyt benzene) ug/L 50 53.22 106 Bromoform uq/t 50 62.60 125 1,1,2,2-Tetrachioroethane ug/L 50 55.71 ill 1,2,3-Trichloropropane ug/L 50 55.15 110 trans- 1 4-D i ch Loro- 2-Butene ug/L 50 56.85 114 Laboratory Certification IDs Laboratory Cert fication IDS NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST Ust Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 LABORATORY CONTROL SAMPLE: 92383330 Parameter 1,4-D i ch I orobenzene 1, 2-D ich Lorobenzene 1 , 2 -D i bromo-3- Ch I oropropane Dibromof tuoromethane (S) 1,2-Dichioroethane-d4 (S) ToLuene-d8 (S) 4-Bromof Luorobenzene (S) SAMPLE DUPLICATE: 92383348 Tel: 704-875-9092 Fax: 704-875-9091 QUALITY CONTROL DATA DATE: 03/30/99 PAGE: 17 Pace Project Number: 925122 Client Project ID: MCDOWELL - 934485 Spike LCS Units Conc. Resutt ---------- ug/L ------- 50 ---------- 53.26 ug/l 50 51.51 ug/L 50 55.76 Spike % Rec Footnotes ----- ---------- 107 103 112 98 94 101 104 Dup. Parameter ------------------ ----------- Units ---------- 92370717 ResuLt RPD Footnotes ChLoromethane ug/L ---------- ND ---------- NO ----- ---------- NC Vinyl ChLoride Ug/L NO ND NC Bromomethane ug/t ND NO NC Chloroethane ug/L NO ND NC Trichtorof tuorwethane Uq/L NO ND NC Acetone ug/L ND NO NC 1 1-DichLoroethene ug/L ND ND NC Iodomethane ug/L NO ND Nc AcryLonitriLe ug/L ND NO NC MethyLene Chtoride Ug/l NO ND NC Carbon DisuLfide ug/k NO NO NC trans-1,2-DichLoroethene ug/L ND NO NC 1,1-Dichloroethane Uq/t NO ND NC Vinyl Acetate ug/L ND NO NC 2-Butanone ug/L IND ND NC cis-1,2-DichLoroethene uq/1 NO NO NC ChLoroform ug/L ND NO Nc BromochLoromethane ug/L NO ND NC 1,1,1-TrichLoroethane us/[ NO NO NC 1,2-DichLoroethane ug/L ND NO NC Carbon Tetrachloride Ug/l NO ND NC Benzene ug/t ND NO NC Trichloroethene ug/L NO ND NC 1,2-Dichtoropropane ug/t NO NO NC Dibromomethane ug/L ND NO NC Bromodichtoromethane Uq/t NO ND NC 4-Methyl-2-Pentanone ug/l. ND NO NC cis- 1 3-D ichloropropene ug/L ND ND NC Laboratory Certification IDs Laboratory Certification IDS NG Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-875-9F92 Fax: 704-875-9091 QUALITY CONTROL DATA DATE: 03/30/99 PAGE: 18 Pace Project Nmber: 925122 CLient Project ID: MCDOWELL - 934485 SAMPLE DUPLICATE. 9-2383348 Dup. Parar�eter ------------------------------ Units ---------- 92370717 ---------- Resuit RPD Footnotes ToLuene ug/L ND ---------- NO ----- --------- NC trans-1,3-Dichtoropropene Ug/L NO ND NC 1,1,2-TrichLoroethane ug/L ND NO NC 2-Hexanone ug/t NO No NC Dibromochloromethane Ug/L NO NO NC TetrachLoroethene ug/L ND NO NC 1,2-Dibromoethane Ug/L NO NO NC ChLorobenzene ug/t NO NO NC 1,1,1,2-Tetrachloroethane ug/L NO NO NC EthyLbenzene uq/L NO NO NC m&p-XyLene ug/L IND NO NC Styrene ug/t NO ND NC o-Xytene (1,2-DimethyL benzene) ug/L NO NO NC Bromform ug/L NO NO NC 1,1,2,2-Tetrachlaroethane ug/L NO NO NC 1,2,3-TrichLoropropane ug/L ND NO NC trans- 1 4-Dichtoro-2-Butene ug/t NO ND NC 1,4-DichLorobenzene ug/L NO NO NC 1,2-Dichtorobenzene ug/L NO NO NC 1,2-Dibromo-3-Chtoropropane Ug/L NO NO NC Dibromof Luoromethane (S) % 97 94 0 1,2-Dichtoroethane-d4 (S) % 95 91 0 Totuene-d8 (S) % 102 102 0 4-Bromoftuorobenzene (S) % 105 104 0 Laboratory Certification IDS Laboratory Certification IPq NC Wastewater 12 KY Drinking Water 90090 INC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-875-909, z Fax: 704-875-9091 DATE: 03/30/99 PAGE: 19 Pace Project Number: 925122 CLient Project ID: MCDOWELL - 934485 QUALITY CONTROL DATA PARAMETER FOOTNOTES Consistent with EPA quidetines unrounded concentrations are dispLayed and have been used to calcuLate % Rec and RPD vaLues. NO Not Detected NC Not CaLculable PRL Pace Reporting Limit RPD ReLative Percent Difference (S) Surrogate Labgrat= Certification IDs Laboratory Certification Ds INC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. FROM HC DEHNR SOLID WASTE SECTION 733-4810 07.02. 1999 10100 P. I rwm-ft r-ax 1VQ18 101Z ND. of Pages TOW Date Tirnq ,TO 91 J From cwpany LwiAn 'L t' Depl. Charge Fat TI !$ 1FOX4 Twephone # -'� o) Cownents C)=ill Destroy Retunn Call Ior Wckvp ID Ion. 11 p NORTH CARdLINA DICPARTMKNT Oir ENVIRONMENT AND I NATURAL RICSOURCISS DIVISION OF WASYS MANAORMCINIT I July 2, 1999 MEMORANDUM TO: Tim Jewett, SWS FROM; Ellen Lorschelder, SWS SUBJECT: Review of Site Suitability App Icatlon Proposed McDowell Co. C &,�"D Landfill RECEIVED N.C. Dept. of EHNR JUL - 2 IM Winston-Salem Regional Office A site visit was made of the aforemendoned site on June 3% 1999. In attendance was George Jensen of Jensen Engineering, Mike Gladden McDowell Counry Public Works DIrector, and A[ Hetzell of the Solid Waste Section. A review of the Application was then made according to Rules; I 5A NCAC 13B .0503 (1) and .0504 (1) after my sIte visit. It has become�apparent to me that additional Investigations wIll not ensure that the site will be f�und suitable for waste management activities. There Is not enough detailed lhformadon provided to establish site suitability. Please consider the following: In order to monitor for compliance with groundwater quallo standards, the applicant must be able to reasonably predict groundwater mbvement. The understanding presented In the application relies on too IltdO site Information. Water table elevations have not been established on the site, � The two borIngs which are advanced to wateronly one water level readings, ;;aken at the time of boring. A potendometric map Is not Included with the repoh and cannot be produced without further fieldwork. The bedrock aquifer will need to be thoroughly understood n order to design a monitoring system. In addition, each major Ilthologic unIt n.�eds to be thoroughly understood In order to determine that the site can be monitbred. The soil and saprolite will need to be better understood In order to pred[O the direction of flow from the bottom of the landfill In the event of a release. Because the groundwater flows largely within fractured bedr' ck( and the site has such variable lithologles and structures, a good understandiln'of the hydrogeology will requhre more exploration than Is generally feasible for D landfills. A thorough analysis of fracture densities and dlstdbudons of the varylng lithologles at the site would be a first step. Understanding the hydraulic I terconnection of fractures and the relation to discharge features would require Installation of many more wells. This understanding of the water movement through the soil and saprolite layers, and then through the fractured rock Is essential on this site 40109114LI" 0A11,0U11r*150,ftA&.91QH,NC27000 . MKftrAPXP9 . I FROM NIC DEHNR SOLID WASTE SECTION 733-4810 07.02. 1999 10!02 P. 2 because there are no apparent discharge features (streams, s0rings, etc.) and monitoring would be reliant on monitoring wells In the fracture system where the water movement (and therefore possible contamination) would be most likely. In addition to the Monitoring considerations, additional borings would be necessary to determination If there Is separation of the rock 'from the bottom of proposed waste. Outcropping of weathered and hard rock Is apparent throughout the site. It Is especially of concern along the southwestern ridge (see cross sections 1 and 2). More Information concerning separation from ro9k would be needed In this and other areas. Please note that I Informed Mr. )ensen and Mr. Gladden that additional work would be necessary before monitorablilty could be establls;W. The amount of Reld data needed to approve (or deny) site sultablilty may be prohibitive to a site of this size. Please call me to discuss this project, ***END*** NC DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES Division of Solid waste Management Solid Waste Section SOLID WASTE KUAGENENT FACILITY EVALUATION REPORT Type of Facilit- Permit # county Name of Facility_ Date of Last Evaluation I- Pennit Conditions Followed A- Specific Condition(s) Vi Yes II. Operational RecMirevients Followed Yes 15A N-C. Achnin. Code 13B Section A- Specific Violation(s) by number and Letter. III- Other Violations of Rule or Law IV. Evaluator's Caments No N/A No Location V. Continuatim Page Recpjirec17 Yes No Receiving Signature Evaluation Date Solid Waste Section DEHNR 3793 (Part I White: Facility Part II Canary: Central Office Part III Pink: Regional Office) Solid Waste Section (Review 7/94) 4 Pace Analytical Services, Inc. 54 Ravenscroff Drive Eace alytical Asheville, NG 28801 Tel: 828-254-7176 Fax: 828-252-4618 September 13, 1999 Mr. Mike Gladden McDowett County Landfill 10 East Court St. Marion, NC 28752 RE: Pace Project Number: 937576 Ctient Project ID: Monitoring Welts (LandfiLL) Dear Mr. Gladden: Enctosed Sre the resuLts of anatyses for sample(s) received by the laboratory on August 26, 1999. If you have any questions concerning this report, please feet free to contact me. S i ncere I y, Walter Miller Project Manager Enclosures 4wz Labgralory Certifigation IDS Laboriggry Certification IDs NIC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive In Eace I Asheville, NC 28801 McDowet I County Landf 111 10 East Court St. Marion, NC 28752 Attn: Mr. Mike Gladden Phone: (704)659-2521 SoLid results are reported on a wet weight basis Pace Sample No: 93342277 Client SampLe ID: MW #1 Parameters --------------------------------- I Field Services Monitoring Well Data FieLd Specific Conductance Depth of Water FieLd Grab Data Field pH FieLd Temperature MetaLs Metals, ICP, trace-tevel. Antimony Arsenic Barium Beryllium Cadmium Chromi um CobaLt Copper Lead Nickel. SeLenium SiLver Vanadium Zinc Date Digested Tel: 828-254-7176 Fax: 828-252-4.918 DATE: 09/13/99 PAGE: 1 Pace Project Number: 937576 Ctient Project ID: Monitoring WeLLs (Landfil Date ColLected: 08/26/99 Date Received: 08/26/99 Results Units PRIL AnaLyzed AnaLyst CAS# ---------- --------- ---------- -------- ----- ------ Method: 61 umhos/cm 23.30 feet 0 Method: 5.9 Std. Units 0 15 deg C 0 Method: EPA 6010 IND mg/1 No mg/L 0.31 mg/L IND mg/L 0.0038 mg/L 0.012 mg1L 0.022 mg/L 0.0089 me/[ 0.013 mg/L 0.017 mg/t 0.021 mg/L IND mg/t 0.11 mg/L 0.068 mg/l. 0.01 0.01 0.005 0.002 0.001 0.005 0.005 0.005 0.01 0.005 0.02 0.002 0.005 0.01 Prep Method: 08/26/99 MPS 08/26/99 MPS Prep Method; 08/26/99 MPS 08/26/99 MPS Matrix: Water Footnotes ---------- Prep Method: EPA 3010 09/01/99 WWB 7440-36-0 09/01/99 WWB 7440-38-2 09/01/99 WWB 7440-39-3 09/01/99 WWB 7440-41-7 09/01/99 WWB 7440-43-9 09/01/99 WWB 7440-47-3 09101/99 WWB 7440-48-4 09/01/99 WWB 7440-50-8 09/01/99 WWB 7439-92-1 09/01/99 WWB 7440-02-0 09/01/99 WWB 7782-49-2 09/01/99 WWB 7440-22-4 09/01/99 WWB 7440-62-2 09/01/99 WWB 7440-66-6 08/27/99 LabQ[WOry Certification I IDS INC Wastewater 40 Laboratory Certification IN NC Drinking Water 37712 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Eace Aaa1vtical Asheville, NC 28801 Tel: 828-254-7 776 Fax: 828-252-4�18 Pace Sample No: 93342277 Client Sample ID: MW #1 Parameters ------------------------------- Mercury in Water Mercury Thal.Hcun, AAS Furnace ThaLLium Date Digested DATE: 09/13199 PAGE: 2 Pace Project Number: 937576 Client Project ID: Monitoring Welts (Landfill) Date Collected: 08/26/99 Matrix: Water Date Received: 08/26/99 Results Units PRIL Analyzed Analyst CAS# Footnotes ---------- --------- ---------- -------- ----- ---------- ---------- Method: EPA 7470 Prep Method: EPA 7470 IND mg/L 0.0002 09/13/99 WW8 7439-97-6 Method: EPA 7841 Prep Method: EPA 3020 IND mg/L 0.002 08/30/99 WWI3 7440-28-0 08/27/99 Laboratory Certification Ili Lal;lgrajory Certification IDS NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980 INC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Eau Analytical Asheville, NC 28801 Tel: 828-254-7176 Fax:828-252-41518 Pace Sample No: 93342285 Client Sample ID: MW #2 Parameters Field Services DATE: 09/13/99 PAGE: 3 Pace Project Number: 937576 Client Project ID: Monitoring WeLts (LandfiLL) Date ColLected: 08/26199 Matrix: Water Date Received: 08/26/99 Results Units PRIL Analyzed AnaLyst CAB# Footnotes --------------- ---------- --------- — -------- -------- ----- ---------- ---------- Monitoring WeLL Data Field Specific Conductance Depth of Water Field Grab Data FieLd pH Field Temperature I MetaLs MetaLs, ICP, trace -level. Antimony Arsenic Barium BeryLLium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Si(ver Vanadium Zinc Date Digested Mercury in Water Mercury Thattium, AAS Furnace ThatLim Date Digested Method: 490 umhos/cm 39.65 feet 0 Method: 6.1 Std. Units 0 16 deg C 0 Prep Method: 08/26/99 MPS 08/26/99 MPS Prep Method: 08126/99 MPS 08/26/99 MPS Method: EPA 6010 Prep Method; EPA 3010 ND mg/L 0.01 09/01/99 WWO 7440-36-0 ND mg/1 0.01 09101/99 WWB 7440-38-2 0.35 mg/L 0.005 09/01/99 WWB 7440-39-3 0.0024 mg/L 0.002 09/01/99 WWB 7440-41-7 0.0042 mg/1 0.001 09/01/99 wwa 7440-43-9 0.025 mg/l. 0.005 09/01/99 WWB 7440-47-3 0.038 mg/L 0.005 09/01/99 WWB 7440-48-4 0.016 mg/l. 0.005 09/01/99 WWO 7440-50-8 ND mg/L 0.01 09/01/99 WWB 7439-92-1 0.022 mg/L 0.005 09/01/99 WWB 7440-02-0 ND mg/t 0.02 09/01/99 WWB 7782-49-2 ND mg/L 0.002 09/01/99 WWB 7440-22-4 0.057 mg/L 0.005 09/01/99 WWB 7440-62-2 0.072 mg/l. 0.01 09101/99 WWB 7440-66-6 08/27/99 Method: EPA 7470 ND mg/t 0.0002 Method: EPA 7841 ND mg/L 0.002 Prep Method: EPA 7470 08/31/99 WWB 7439-97-6 Prep Method: EPA 3020 08/30/99 WWB 7440-28-0 08/27/99 Laboratory Certification 1ps Laboratory Certification IDs NO Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NO Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive alylical Asheville, NC 28801 Tel: 828-254-7176 Fax: 828-252-4Q18 DATE: 09/13/99 PAGE: 4 Pace Project Number: 937576 Client Project ID: Monitoring WeLLs (Landfil[L) Pace Sample No: 93342293 Date COLLected: 08/26/99 Matrix: Water Client Sample ID: MW #3 Date Received: 08/26/99 Parameters Results Units PRL Analyzed Analyst CAB# Footnotes --------------------------------- ---------- --------- ---------- -------- ----- ---------- ---------- Hatt! Services Monitoring WelL Data FieLd Specific Conductance Depth of Water Field Grab Data Field PH FieLd Temperature Metals MetaLs, 1CP, trace -Level Antimony Arsenic Barium BeryLtium Cadmium Chromium Cobatt Copper Lead Nickel Selenium Silver Vanadium Zinc Date Digested Mercury in Water Mercury Thattium, AAS Furnace ThaLtium Date Digested Method: 340 umhos/cm 44.00 feet 0 Method: 6.3 Stall. Units 0 16 deg C 0 Prep Method: 08/26/99 MPS 08/26/99 MPS Prep Method: 08/26/99 MPS 08/26/99 MPS Method: EPA 6010 Prep Method: EPA 3010 NO mg/l. 0.01 09/01/99 WW3 7440-36-0 No mg/L 0.01 09/01/99 WWB 7440-38-2 0.17 mg/L 0.005 09/01/99 WW8 7440-39-3 0.002 mg/t 0.002 09/01/99 WWB 7440-41-7 0.0012 mg/L 0.001 09/01/99 WWB 7440-43-9 NO mq/1 0.005 09/01/99 WW3 7440-47-3 0.0078 mg/L 0.005 09/01/99 WWB 7440-48-4 NO mg/L 0.005 09/01/99 WWB 7440-50-8 NO mg/t 0.01 09/01/99 WWB 7439-92-1 0.0058 mg/L 0.005 09/01/99 WWB 7440-02-0 ND mg/l 0.02 09/01/99 WWB 7782-49-2 NO mg/L 0.002 09/01/99 WWB 7440-22-4 0.02 mg/t 0.005 09/01/99 WWB 7440-62-2 0.033 mg/L 0.01 09/01/99 WWB 7440-66-6 08/27/99 Method: EPA 7470 NO mg/t 0.0002 Method: EPA 7841 NO mg/L 0.002 Prep Method: EPA 7470 09/13/99 WWS 7439-97-6 Prep Method: EPA 3020 08/30/99 WWB 7440-28-0 08/27/99 Laboratory Certification lDs Laboratory Certification IDS INC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NIC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Eace Analytical Asheville, NC 28801 Tel: 828-254-7176 Fax: 828-252-4618 Pace SampLe No: 93342301 CLient SampLe ID: MW #4 Parameters ResuLts Units --------------------------------- ---------- ----- Field Services DATE: 09/13/99 PAGE: 5 Pace Project Number: 937576 CHent Project ID: Monitoring Watts (LandfiLt) Date Collected: 08/26/99 Matrix; Water Date Received: 08/26/99 PRL AnaLyzed AnaLyst CAS# Footnotes ---------- -------- ----- ---------- ---------- Monitoring Well. Data Method: Prep Method: Field Specific Conductance 68 umhos/cm 08/26/99 MPS Depth of Water 20.07 feet 0 08/26/99 MPS FieLd Grab Data Method: Prep Method: FieLd PH 4.9 Std. Units 0 08/26/99 MPS FieLd Temperature 18 deg C 0 08/26/99 MPS Metals Metals, 1CP, trace-Levet Method: EPA 6010 Prep Method; EPA 3010 Antimony No mg/L 0.01 09/01/99 WWB 7440-36-0 Arsenic No mg/1 0.01 09/01199 WWB 7440-38-2 Barium 0.27 mg/L 0.005 09/01/99 WWB 7440-39-3 BeryLLium No mg/L 0.002 09/01/99 WWB 7440-41-7 Cadmium No mg/1 0.001 09/01/99 WWB 7440-43-9 Chromium No mg/l 0.005 09/01/99 WWB 7440-47-3 cobaLt No mg/L 0.005 09/01/99 WWS 7440-48-4 Copper No mg/L 0.005 09/01/99 WWB 7440-50-8 Lead ND mg/l 0.01 09/01/99 WWB 7439-92-1 Nickel No mg/L 0.005 09/01/99 WWB 7440-02-0 Seleni um ND mg/t 0.02 09/01/99 WWB T782-49-2 SiLver ND mg/t 0.002 09/01/99 WWB 7440-22-4 Vanadium No mg/L 0.005 09/01/99 WWB 7440-62-2 Zinc 0.027 mg/1 0.01 09/01/99 WWS 7440-66-6 Date Digested 08/27/99 Mercury in Water Mercury ThaLlium, AAS Furnace ThaLHum Date Digested Method; EPA 7470 ND mg/l 0.0002 Method: EPA 7841 No me/[ 0.002 Prep Method: EPA 7470 08/31/99 WWB 7439-97-6 Prep Method: EPA 3020 08/30/99 WWB 7440-28-0 08/27/99 Laboratory Certilication IDS LgIboralory Certification la NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Earae Analytical Asheville, NO 28801 Tel: 828-254-7177 Fax: 828-252-4618 Pace SampLe No: 93342327 Ctient Sampte ID: EQUIPMENT BLANK DATE: 09/13/99 PAGE: 6 Pace Project Number: 937576 Client Project ID: Monitoring WetLs (LandfiLt) Date CotLected: 08/26/99 Matrix: Water Date Received: 08/26/99 Parameters Resutts Units PRL Anatyzed AnaLyst CAB# Footnotes --------------------------------- ---------- --------- ---------- -------- ----- ---------- ---------- MetaLs Metats, ICP, trace -level Method: EPA 6010 Prep Method: EPA 3010 Antimony ND mg/I 0.01 09/01199 WWB 7440-36-0 Arsenic ND mg/L 0.01 09/01/99 WWB 7440-38-2 Barium ND mg/L 0.005 09/01/99 WWB 7440-39-3 Beryl Lim ND mg/L 0.002 09/01/99 WWII 7440-41-7 Cadmium ND mg/L 0.001 09/01/99 WW9 7440-43-9 Chromium ND mg/1 0.005 09/15/99 WWB 7440-47-3 cobaLt ND mg/L 0.005 09/01/99 Wwa 7440-48-4 Copper ND mg/t 0.005 09/01/99 WWB 7440-50-8 Lead ND mg/L 0.01 09/01/99 WWII 7439-92-1 Nickel ND mg/l. 0.005 09/15/99 WWB 7440-02-0 Selenium ND mg/L 0.02 09/01/99 WWB 7782-49-2 SiLver ND mg/L 0.002 09/01/99 WWII 7440-22-4 Vanadium ND mg/I 0.005 09/01/99 WWB 7440-62-2 Zinc ND mg/L 0.01 09/01/99 WWB 7440-66-6 Date Digested 08/27/99 Mercury in Water Mercury ThaLlium, AAS Furnace ThaLliurn Date Digested Method: EPA 7470 NO mg/L 0.0002 Method: EPA 7841 ND mq1L 0.002 Prep Method: EPA 7470 08/31/99 WWS 7439-97-6 Prep Method: EPA 3020 08/30/99 WWB 7440-28-0 08/27/99 Laboratory Certification 1ps Laboratory Certification IDs NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 54 Ravenscroft Drive Eace AnaLylical Asheville, NC 28801 Tel: 828-254-7177 Fax: 828-252-4618 PARAMETER FOOTNOTES NO Not Detected NC Not CatcutabLe PRL Pace Reporting Limit DATE: 09/13/99 PAGE: 7 Pace Project NLxrber: 937576 CHent Project ID: Monitoring Wells (LandfiLt) 11 epq Laboratory Certilkation IDS Laboratory Certification Ds NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kinsey Avenue, Suite 100 Eace Anabilial Huntersville, NC 28078 Tel: 704-875-7092 Fax: 704-875-90�1 McDowel. I County Landf i t L 10 East Court Street Marion, NC 28752 Attn: Mr. Mike Gladden Solid results are reported on a dry weight basis DATE: 09/02/99 PAGE: I Pace Project Number: 928351 Client Project ID: McDowell Landfill-937576 Pace Sampte No: 93342277 Date Collected: 08/26/99 Matrix: Water Client Semple ID: MW#1 Date Received: 08/27/919 Parameters Results Units PRL App. DF Analyzed Analyst CAB# Footnotes ------------------ -------------- ---------- --------- ---------- -------- -------- ----- ---------- --------- GC/MS Votatites GC/MS VOCs by 8260 Method: EPA 8260 Prep Method: EPA 8260 Chtoromthane ND ug/1 10 1.00 08/30/99 RPJ 74-87-3 Vinyl Chloride ND Ug/t 10 1.00 08/30/99 RPJ 75-01-4 Bromomethane ND ug/L 10 1.00 08/30/99 RPJ 74-83-9 Chloroethane ND Ug/t 10 1.00 08/30/99 RPJ 75-00-3 TrichLorofLuormethane ND ug/L 10 1.00 08/30/99 RPJ 75-69-4 Acetone ND ug/L 100 1.00 08/30/99 RPJ 67-64-1 1,1-Dichtoroethene ND ug/t 5 1.00 08/30/99 RPJ 75-35-4 lodomethane ND ug/L 5 1.00 08/30/99 Rod 74-88-4 Acrytonitrite ND ug/t 100 1.00 08/30/99 RPJ 107-13-1 MethyLene Chloride ND ug/L 5 1.00 08/30/99 RPJ 75-09-2 Carbon Disulf ide ND ug/L 5 1.00 08/30/99 RPJ 75-15-0 trans- 1 , 2-Dich Loroethene ND Ug/l 5 1.00 08/30/99 RPJ 156-60-5 1 , 1 - D i ch L a roe t h one ND ug/L 5 1.00 08/30/99 RPJ 75-34-3 Vinyl Acetate ND Ug/1 50 1.00 08/30/99 RPJ 108-05-4 2-Butanone ND ug/L 100 1.00 08130/99 RPJ 78-93-3 cis-1,2-Dichtoroethene ND ug/L 5 1.00 08130199 RPJ 156-59-2 Chloroform ND Ug/t 5 1.00 08/30/99 RPJ 67-66-3 Bromochtoromethane ND ug/L 5 1.00 08/30/99 RPJ 74-97-5 1,1,1-Trichloroethane ND Ug/I. 5 1.00 08/30/99 RPJ 71-55-6 1,2-DichLoroethene ND ug/L 5 1.00 08/30/99 RPJ 107-06-2 Carbon Tetrachloride ND ug/L 5 1.00 08/30/99 RPJ 56-23-5 Benzene ND Ug/l 5 1.00 08/30/99 RPJ 71-43-2 TrichLoroethene ND ug/L 5 1.00 08/30/99 RPJ 79-01-6 1,2-Dichtoropropane ND ug/t 5 1.00 08/30/99 RPJ 78-87-5 Dibromomethane ND ug/L 5 1.00 08/30/99 RPJ 74-95-3 BromodichLoromethane ND ug/1 5 1.00 08/30/99 RPJ 75-27-4 Laboratory Certification IDs Laboratoty Certification lDs INC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kinney Avenue, Suite 100 Pace fillualytical Huntersvii1e, NC 28078 Tel: 704-875-9092 Fax: 704-875-90§1 DATE: 09/02/99 PAGE: 2 Pace Project Number: 928351 CL lent Project I D : McDowel. L Landf i L L-937576 Pace SampLe No: 93342277 Date CotLected: 08/26/99 Matrix; Water CHent Sample ID: MW#1 Date Received: 08/27/99 Parameters Results Units PRL App. DF Analyzed Analyst CAS# Footnotes --------------------------------- 4-Methyl-2-Pentanone ---------- ND --------- ug/l. ---------- 50 -------- 1.00 -------- 08/30/99 ----- RPJ ---------- ---------- 108-10-1 cis-1,3-DichLoropropene ND ug/t 5 1.00 08/30/99 RPJ 10061-01-5 Totuene IND ug/L 5 1.00 08/30199 RPJ 108-88-3 trans-1,3-Dichloropropene ND ug/L 5 1.00 08/30/99 RPJ 10061-02-6 1,1,2-TrichLoroethane ND ug/L 5 1.00 08/30/99 RPJ 79-00-5 2-Nexanone ND ug/t 50 1.00 08/30/99 RPJ 591-78-6 D i bromoch L ormeth ane ND ug/t 5 1.00 08/30/99 RPJ 124-48-1 Tat rach to roethene ND ug/L 5 1.00 08/30/99 RPJ 127-18-4 1,2-Dibromethane ND ug/t 5 1.00 08/30/99 RPJ 106-93-4 Chlorobenzene ND ug/l 5 1.00 08/30/99 RPJ 108-90-7 1,1,1,2-TetrachLoroethane ND ug/L 5 1.00 08/30/99 RPJ 630-20-6 Ethytbenzene ND ug/l 5 1.00 08/30199 RPJ 100-41-4 rn&p-XyLene ND ug/l 10 1.00 08/30/99 RPJ 7816-60-0 Styrene ND ug/L 5 1.00 08/30/99 RPJ 100-42-5 o-XyLene (1,2-Dimethylbenzene) ND ug/L 5 1.00 08/30/99 RPJ 95-47-6 Bromoform ND ug/1 5 1.00 08/30/99 RPJ 75-25-2 1,1,2,2-Tetrachloroethane ND ug/l 5 1.00 08/30/99 RPJ 79-34-5 1,2,3-Trichloropropane IND ug/L 5 1.00 08/30/99 RPJ 96-18-4 trans-1,4-Dichloro-2-Butene ND ug/L 5 1.00 08/30199 RPJ 110-57-6 1,4-Dichiorobenzene ND ug/L 5 1.00 08/30/99 RPJ 106-46-7 1,2-Dichlorobenzene ND ug/t 5 1.00 08/30199 RPJ 95-50-1 1,2-Dibromo-3-ChLoropropane ND ug/L 5 1.00 08/30/99 RPJ 96-12-8 Dibromof luoromethane (S) 102 % 1.00 08/30/99 RPJ 1868-53-7 1,2-Dichloroethane-d4 (S) 102 % 1.00 08/30/99 RPJ 17060-07-0 ToLuene-d8 (S) 88 % 1.00 08/30/99 RPJ 2037-26-5 4-BromofLuorobenzene (S) 90 % 1.00 08/30/99 RPJ 460-00-4 Laboratory Certification IDS Laboratory Certification IDS NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Bace Analytical Huntersville, NG 28078 Tel: 704-875-9092 Fax: 704-875-90�) DATE: 09/02/99 PAGE: 3 Pace Project Nwber: 928351 Client Project ID: McDoweLL Landfill-937576 Pace SampLe No: 93342285 Date CoLLected: 08/26/99 Matrix: Water Client SampLe ID-. MW#2 Date Received: 08/27199 Parameters Results Units PRL App. OF Analyzed Analyst CAS# Footnotes --------------------------------- ---------- --------- .......... -------- -------- ----- ---------- --------- GC/MS VotatiLes GC/MS VOCs by 8260 Method: EPA 8260 Prep Method: EPA 8260 Chtoromethane ND ug/L 10 1.00 08/30/99 RPJ 74-87-3 Vinyl, ChLoricle NO ug/l. 10 1.00 08/30/99 RPJ 75-01-4 Bromomethane NO ug/l 10 1.00 08/30/99 RPJ 74-83-9 Chloroethane NO ug/L 10 1.00 08/30/99 RPJ 75-00-3 Trichlorof tuoromethane ND ug/L 10 1.00 08/30/99 RPJ 75-69-4 Acetone NO ug/l 100 11.00 08/30/99 RPJ 67-64-1 1,1-Dichioroethene NO ug/t 5 1.00 08/30/99 RPJ 75-35-4 Iodomethane NO ug/L 5 1.00 08/30/99 RPJ 74-88-4 Acrytonitrite NO ug/t 100 1.00 08/30/99 RPJ 107-13-1 MethyLene ChLoricle NO ug/t 5 1.00 08/30/99 RPJ 75-09-2 Carbon Disutfide NO ug/L 5 1.00 08/30/99 RPJ 75-15-0 trans-1,2-Dichloroethene ND ug/L 5 1.00 08/30/99 RPJ 156-60-5 1,1-Dichtoroethane 14 ug/l. 5 1.00 08/30/99 RPJ 75-34-3 Vinyl Acetate NO ug/l 50 1.00 08/30/99 RPJ 108-05-4 2-Butanone NO ug/L 100 1.00 08/30/99 RPJ 78-93-3 cis-1,2-DichLoroethene 140 ug/L 5 1.00 08/30/99 RPJ 156-59-2 Chtoroform NO ug/l. 5 1.00 08/30/99 RPJ 67-66-3 Bromochloromethane NO ug/t 5 1.00 08/30/99 RPJ 74-97-5 1,1,1-Trichtoroethane ND ug/L 5 1.00 08/30/99 RPJ 71-55-6 1,2-Dichioroethane ND ug/L 5 1�00 08/30/99 RPJ 107-06-2 Carbon Tetrachloride ND ug/I. 5 1.00 08/30/99 RPJ 56-23-5 Benzene 12 ug/L 5 1.00 08/30/99 RPJ 71-43-2 TrichLoroethene ND ug/L 5 1.00 08/30/99 RPJ 79-01-6 1,2-DichLoropropane NO ug/L 5 1.00 08/30/99 RPJ 78-87-5 Dibromomethane NO ug/l 5 1.00 08/30/99 RPJ 74-95-3 B romod i ch I orometh ane ND ug/L 5 1.00 08/30199 RPJ 75-27-4 4-MethyL-2-Pentanone ND ug/L 50 1.00 08/30/99 RPJ 108-10-1 cis-1,3-Dichtoropropene NO ug/t 5 1.00 08/30/99 RPJ 10061-01-5 ToLuene 24 ug/L 5 1.00 08/30/99 RPJ 108-88-3 trans- 1 3-Dich Loropropene ND ug/L 5 1.00 08/30/99 RPJ 10061-02-6 1,1,2-Trichloroethane IND ug/L 5 1.00 08/30/99 RPJ 79-00-5 2-Hexanone NO ug/l 50 1.00 08/30/99 RPJ 591-78-6 D i br omoch I. orometh ane ND ug/L 5 1.00 08/30/99 RPJ 124-48-1 T et ra ch L o roeth ene ND ug/L 5 1.00 08/30199 RPJ 127-18-4 1 , 2 - D i br owet In ane NO ug/L 5 1.00 08/30/99 RPJ 106-93-4 Chtorobenzene NO Ug/1. 5 1.00 08/30/99 RPJ 108-90-7 Laboratory Cerlificartion IDs Laboratory Certification IDs NC Wastewater 12 KY Drinking Water 90090 INC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace,Analylical Huntersville, NC 28078 Tel: 704-875-9092 Fax:704-875-9091 DATE: 09/02/99 PAGE: 4 Pace Project Number: 928351 Client Project ID: McDowell. LandfiLL-937576 Pace Sample No: 93342285 Date Collected: 08/26/99 Matrix: Water Client Sample ID: MW#2 Date Received: 08/27/99 Parameters --------------------------------- Results ---------- Units --------- PIRL App. DF Analyzed AnaLyst CAS4 Footnotes 1, 1, 1,2-Tetrachtoroethane ND uq/t ---------- 5 -------- 1.00 -------- 08/30/99 ----- RPJ ---------- ---------- 630-20-6 Ethyllbenzene ND ug/l 5 1.00 08/30/99 RPJ 100-41-4 rr&p-Xytene 12 ug/L 10 1.00 08/30/99 RPJ 7816-60-0 Styrene IND ug/L 5 1.00 08/30/99 RPJ 100-42-5 o-Xytene (1, 2 -D i methyl benzene) 14 ug/t 5 1.00 08/30/99 RPJ 95-47-6 Bromoform ND ug/L 5 1.00 08/30/99 RPJ 75-25-2 1,1,2,2-TetrachLoroethane ND uq/1 5 1.00 08/30/99 RPJ 79-34-5 1,2,3-Trichloropropane ND ug/l 5 1.00 08/30/99 RPJ 96-18-4 trans- 1 4-Dich toro-2-Butene MID ug/L 5 1.00 08/30/99 RPJ 110-57-6 1,4-Dichtorobenzene 6.2 ug/L 5 1.0b 08/30/99 RPJ 106-46-7 1,2-DichLorobenzene 5.0 ug/l 5 1.00 08/30/99 RPJ 95-50-1 1,2-Dibroma-3-ChLoropropane ND ug/L 5 1.00 08/30/99 RPJ 96-12-8 Dibromoftuoromethane (S) 101 % 1.00 08/30/99 RPJ 1868-53-7 1,2-DichLoroethane-d4 (s) 100 % 1.00 08/30/99 RPJ 17060-07-0 ToLuene-d8 (S) 99 % 1.00 08/30/99 RPJ 2037-26-5 4-Bromoftuorobenzene (S) 96 % 1.00 08/30/99 RPJ 460-00-4 Laboratory Certification IlDs Laboratory Certification IDs INC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List SIC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Eace Analytical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 09/02/99 PAGE: 5 Pace Project Number: 928351 Client Project ID: McDowett Landfi[L-937576 Pace SampLe No: 93342293 Date CoLtected: 08/26/99 Matrix: Water Client SampLe ID: MW#3 Date Received: 08/27/99 Parameters ResuLts Units PRL App. OF Anatyzed Analyst CAB# Footnotes --------------------------------- ---------- --------- ---------- -------- -------- ----- ---------- --------- GC/MS VoLatiLes GC/MS VOCs by 8260 Method: EPA 8260 Prep Method: EPA 8260 Chtoromethane NO ug/L 10 1.00 08/30/99 RPJ 74-87-3 Vinyt ChLoricle NO ug/L 10 1.00 08/30/99 RPJ 75-01-4 Bromomethane NO ug/t 10 1.00 08/30/99 RPJ 74-83-9 Chtoroethane NO ug/L 10 1.00 08/30/99 RPJ 75-00-3 TrichLorof luoromethane ND ug/L 10 1.00 08/30/99 RPJ 75-69-4 Acetone NO ug/1 100 1.00 08/30/99 RPJ 67-64-1 1,1-Dichtoroethene NO ug/t 5 1.00 08/30/99 RPJ 75-35-4 loclomethane IND ug/L 5 1.00 08/30/99 RPJ 74-88-4 AcrylonitriLe NO ug/L 100 1.00 08/30/99 RPJ 107-13-1 Methylene ChLoride NO ug/t 5 1.00 08/30/99 RPJ 75-09-2 Carbon Disulfide ND Ug/L 5 1.00 08/30/99 RPJ 75-15-0 trans-1,2-Dichtoroethene ND ug/L 5 1.00 08/30/99 RPJ 156-60-5 1,1-Dichtoroethane NO ug/t 5 1.00 08/30/99 RPJ 75-34-3 Vinyl Acetate NO ug/L 50 1.00 08/30/99 RPJ 108-05-4 2-Butanone NO ug/L 100 1.00 08/30/99 RPJ 78-93-3 cis-1,2-DichLoroethene NO ug/t 5 1.00 08/30/99 RPJ 156-59-2 ChLoroform NO ug/l 5 1.00 08/30/99 RPJ 67-66-3 BromochLoromethane NO ug/L 5 1.00 08/30/99 RPJ 74-97-5 1,1,1-Trich[oroethane NO ug/L 5 1.00 08/30/99 RPJ 71-55-6 1,2-Dichtoroethane NO ug/l 5 1.00 08/30/99 RPJ 107-06-2 Carbon Tetrachtoride IND ug/L 5 1.00 08/30/99 RPJ 56-23-5 Benzene NO ug/L 5 1.00 08/30/99 RPJ 71-43-2 TrichLoroethene NO ug/1 5 1.00 08/30/99 RPJ 79-01-6 1,2-DichLorapropane NO Ug/t 5 1.00 08/30/99 RPJ 78-87-5 Dibromomethane NO ug/L 5 1.00 08/30/99 RPJ 74-95-3 BromodichLoromethane NO ug/L 5 1.00 08/30/99 RPJ 75-27-4 4-MethyL-2-Pentanone NO ug/l. 50 1.00 08/30/99 RPJ 108-10-1 cis-1,3-Dichloropropene ND Ug/l 5 1.00 08/30/99 RPJ 10061-01-5 Totuene NO ug/L 5 1.00 08/30/99 RPJ 108-88-3 trans-1,3-Dichloropropene NO ug/L 5 1.00 08/30/99 RPJ 10061-02-6 1,1,2-Trichloroethane NO Ug/l 5 1.00 08/30/99 RPJ 79-00-5 2-Hexanone NO ug/L 50 1.00 08/30/99 RPJ 591-78-6 DibromochLoromethane NO ug/L 5 1.00 08/30/99 RPJ 124-48-1 Tetrachloroethene NO ug/t 5 1.00 08/30/99 RPJ 127-18-4 1,2-Dibromoethane NO ug/L 5 1.00 08/30/99 RPJ 106-93-4 ChLorobenzene NO ug/L 5 1.00 08/30/99 RPJ 108-90-7 Laboratory Certification IDs Laboratory Certification IDs INC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Aaalytig;al Huntersville, NG 28078 Tel: 704-875-9092 Fax: 704-875-90.9,1 DATE: 09/02/99 PAGE: 6 Pace Project Number: 928351 Client Project ID: McDowell LancifiLL-937576 Pace Sample No: 93342293 Date Collected: 08/26/99 Matrix: Water Client Sample ID: MW#3 Date Received: 08/27/99 Parameters --------------------------------- Results ---------- Units PRIL App. DF Analyzed Analyst CAS# Footnotes 1, 1 , 1,2-Tetrach I oroethane ND --------- uq/L ---------- 5 -------- 1.00 -------- 08/30/99 ----- RPJ ---------- ---------- 630-20-6 EthyLbenzene ND ug/l 5 1.00 08/30/99 RPJ 100-41-4 m&p-Xytene ND ug/l 10 1.00 08/30/99 RPJ 7816-60-0 Styrene ND ug/L 5 1.00 08/30/99 RPJ 100-42-5 o-Xylene (1,2-DimethyLbenzene) ND uq/L 5 1.00 08/30/99 RPJ 95-47-6 Bromoform ND ug/I. 5 1.00 08/30/99 RPJ 75-25-2 1,1,2,2-Tetrachloroethane ND ug/L 5 1.00 08/30/99 RPJ 79-34-5 1,2,3-TrichLoropropane ND ug/L 5 1.00 08/30/99 RPJ 96-18-4 trans- 1,4-Dichtoro-2-Butene ND ug/L 5 1.00 08/30/99 RPJ 110-57-6 1,4-Dichtorobenzene ND ug/t 5 1.00 08/30/99 RPJ 106-46-7 1,2-Dichtorobenzene ND ug/l 5 1.00 08/30/99 RPJ 95-50-1 1,2-Dibromo-3-ChLoropropane ND ug/L 5 1.00 08/30/99 RPJ 96-12-8 Dibromofluormethane (S) 102 % 1.00 08/30/99 RPJ 1868-53-7 1,2-Dichtoroethane-d4 (S) 100 % 1.00 08/30/99 RPJ 17060-07-0 ToLuene-d8 (S) 99 % 1.00 08/30/99 RPJ 2037-26-5 4-BromofLuorobenzene (S) 83 % 1.00 08/30/99 RPJ 460-00-4 1 w Laboratory Certlication lDs Laboratoty Certification IDa NC Wastewater 12 KY Drinking Water 90090 INC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kinney Avenue, Suite 100 Eace Analytical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 '-1 DATE: 09/02/99 PAGE: 7 Pace Project Number: 928351 Client Project ID: McDoweLL LandfiLl-937576 Pace SampLe No: 93342301 Date CoLtected; 08/26/99 Matrix: Water CLient Sample ID: MW#4 Date Received: 08/27/99 Parameters Resutts Units PRIL App. OF Analyzed Anatyst CAS# Footnotes --------------------------------- ---------- --------- ---------- -------- -------- ----- ---------- ---------- GC/MS VolatiLes GC/MS VOCs by 8260 Method: EPA 8260 Prep Method: EPA 8260 Chioromethane NO ug/L 10 1.00 08/30/99 RPJ 74-87-3 Vinyl Chloride NO ug/L 10 1.00 08/30/99 RPJ 75-01-4 Bromomethane NO ug/1 10 1.00 08/30/99 RPJ 74-83-9 Chloroethame NO ug/l 10 1.00 08/30/99 RPJ 75-00-3 Trichtorof luoromethane NO ug/L 10 1.00 08/30/99 RPJ 75-69-4 Acetone NO ug/t 100 1.00 08/30/99 RPJ 67-64-1 1,1-DichLoroethene NO ug/t 5 1.00 08/30/99 RPJ 75-35-4 lodomethane NO ug/L 5 1.00 08/30/99 RPJ 74-88-4 AcryLonitrile, NO ug/l. 100 1.00 08/30/99 RPJ 107-13-1 Methylene Chloride NO ug/l 5 1.00 08130/99 RPJ 75-09-2 Carbon Disutfide NO ug/L 5 1.00 08/30/99 RPJ 75-15-0 trans-1,2-Dichtoroethene NO ug/L 5 1.00 08/30/99 RPJ 156-60-5 1, 1 -Dich Loroethane NO ug/l 5 1.00 08/30/99 RPJ 75-34-3 Vinyl Acetate NO ug/L 50 1.00 08/30/99 RPJ 108-05-4 2-Butanone NO ug/L 100 1.00 08/30/99 RPJ 78-93-3 cis-1,2-Dichtoroethene NO ug/t 5 1.00 08/30/99 RPJ 156-59-2 ChLoroform NO ug/l. 5 1.00 08/30/99 RPJ 67-66-3 Bromochtoromethane NO ug/L 5 1.00 08/30/99 RPJ 74-97-5 1,1,1-Trichloroethane NO ug/1 5 1.00 08/30/99 RPJ 71-55-6 1,2-Dichtoroethane NO ug/l 5 1.00 08/30/99 RPJ 107-06-2 Carbon Tetrachloride NO ug/L 5 1.00 08/30/99 RPJ 56-23-5 Benzene NO U911 5 1.00 08/30/99 RPJ 71-43-2 TrichLoroethene NO ug/l. 5 1.00 08/30/99 RPJ 79-01-6 1,2-Dichloropropane NO ug/L 5 1.00 08/30/99 RPJ 78-87-5 Dibromomethane NO ug/L 5 1.00 08/30/99 RPJ 74-95-3 Bromodichtoromethane NO ug/l 5 1.00 08/30/99 RPJ 75-27-4 4-MethyL-2-Pentanone NO ug/L 50 1.00 08/30/99 RPJ 108-10-1 cis-1,3-DichLoropropene NO ug/L 5 1.00 08/30/99 RPJ 10061-01-5 ToLuene NO uq/t 5 1.00 08/30/99 RPJ 108-88-3 trans-1,3-Dichtoropropene ND ug/L 5 1.00 08/30/99 RPJ 10061-02-6 1,1,2-Trichloroethane NO ug/L 5 1.00 08/30/99 RPJ 79-00-5 2-Hexanone NO ug/l. 50 1.00 08/30/99 RPJ 591-78-6 DibromochLoromethane NO ug/L 5 1.00 08/30/99 RPJ 124-48-1 Tetrachloroethere NO ug/L 5 1.00 08/30/99 RPJ 127-18-4 1,2-Dibromoethane NO ug/t 5 1.00 08/30/99 RPJ 106-93-4 ChLorobenzene ND ug/L 5 1.00 08/30/99 RPJ 108-90-7 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Ki ncey Aven u e, S u ite 100 Pace Analvtical Huntersville, NO 28078 Tel: 704-875-9092 Fax: 704-875-9OPI DATE: 09/02/99 PAGE: 8 Pace Project Number; 928351 CHent Project ID: McDoweLL LandfitL-937576 Pace SampLe No: 93342301 Date CotLected: 08/26/99 Matrix: Water Client Sample ID: MW#4 Date Received: 08/27/99 Parameters --------------------------------- Results ---------- Units PRL App. DF AnaLyzed Analyst CAS# Footnotes 1,1,1,2-Tetrachtoroethane ND --------- ug/L ---------- 5 -------- 1.00 -------- 08/30/99 ----- RPJ ---------- ---------- 630-20-6 EthyLbenzene ND ug/L 5 1.00 08/30/99 RPJ 100-41-4 m&p-Xylene ND ug/l. 10 1.00 08/30/99 RPJ 7816-60-0 Styrene ND ug/L 5 1.00 08/30/99 RPJ 100-42-5 o-XyLene (1,2-DimethyLbenzene) ND ug/L 5 1.00 08/30/99 RPJ 95-47-6 gromoform ND ug/1 5 1.00 08/30/99 RPJ 75-25-2 1, 1 2,2-Tetrachloroethane IND ug/L 5 1.00 08/30/99 RPJ 79-34-5 1,2,3-Trichtoropropane ND uq/L 5 1.00 08/30/99 RPJ 96-18-4 trans- 1,4-Dich toro-2-Butene ND ug/1 5 1.00 08/30/99 RPJ 110-57-6 1,4-Dichtorobenzene ND ug/L 5 1.00 08/30/99 RPJ 106-46-7 1 , 2 - D i ch t orobenzene ND ug/L 5 1.00 08/30/99 RPJ 95-50-1 1 , 2 - D i bromo- 3 - Ch E crop ropane ND ug/1 5 1.00 08/30/99 RPJ 96-12-8 Dibromoftuoromethane (S) 102 % 1.00 08/30/99 RPJ 1868-53-7 1,2-DichLocoethane-d4 (S) 102 % 1.00 08/30/99 RPJ 17060-07-0 Totuene-d8 (S) 98 % 1.00 08/30/99 RPJ 2037-26-5 4-Brmoftuorobenzene (S) 84 % 1.00 08130/99 RPJ 460-00-4 2 Laboratory Certification IDS Laboratory Certification IDS NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analyti!Gal Huntersville, NG 28078 Tel: 704-875-9092 Fax: 704-875-9Q�,11 DATE: 09/02/99 PAGE: 9 Pace Project Number: 928351 Client Project ID: McDoweLt LandfiLL-937576 Pace Sampte No: 93342319 Date CoLtected: 08/26/99 Matrix: Water Client SampLe ID: TRAVEL BLANK Date Received: 08/27/99 Parameters Results Units PRL App. DF Analyzed AnaLyst CAS# --------------------------------- ---------- --------- ---------- -------- -------- ----- ------ GC/MS Volatites GC/MS VCCs by 8260 Method: EPA 8260 Prep Method: EPA 8260 Chloromethane ND uq/t 10 1.00 08/30/99 RPJ 74-87-3 VinyL Chloride ND ug/L 10 1.00 08/30/99 RPJ 75-01-4 Bromomethane NO ug/L 10 1.00 08/30/99 RPJ 74-83-9 ChLoroethane ND ug/l. 10 1.00 08/30/99 RPJ 75-00-3 Trichtorof luoromethane ND ug/L 10 1.00 08/30/99 RPJ 75-69-4 Acetone ND ug/L 100 1.00 08/30/99 RPJ 67-64-1 1,1-Dichtoroethene ND ug/t 5 1.00 08/30/99 RPJ 75-35-4 lodomethene ND ug/t 5 1.00 08/30/99 RPJ 74-88-4 AcrytonitriLe ND uq/L 100 1.00 08130/99 RPJ 107-13-1 MethyLene ChLoride ND ug/l. 5 1.00 08/30/99 RPJ 75-09-2 Carbon Disutfide ND ug/l 5 1.00 08/30/99 RPJ 75-15-0 trans-1,2-DichLoroethene ND ug/L 5 1.00 08/30/99 RPJ 156-60-5 1,1-Dichioroethane ND us/[ 5 1.00 08/30/99 RPJ 75-34-3 Vinyl. Acetate ND ug/l. 50 1.00 08/30/99 RPJ 108-05-4 2-Butanone ND ug/L 100 1.00 08/30/99 RPJ 78-93-3 cis-1,2-DichLoroethene ND ug/1 5 1.00 08/30/99 RPJ 156-59-2 ChLoroform ND ug/t 5 1.00 08/30/99 RPJ 67-66-3 Bromochloromethane ND ug/L 5 1.00 08/30/99 RPJ 74-97-5 1,1,1-Trichloroethane ND ug/1 5 1.00 08/30/99 RPJ 71-55-6 1,2-DichLoroethane ND ug/t 5 1.00 08/30/99 RPJ 107-06-2 Carbon TetrachLoride ND uq/L 5 1.00 08/30/99 RPJ 56-23-5 Benzene ND ug/L 5 1.00 08/30/99 RPJ 71-43-2 TrichLoroethene ND ug/l. 5 1.00 08/30/99 RPJ 79-01-6 1,2-Dichloropropane ND ug/l 5 1.00 08/30/99 RPJ 78-87-5 Dibromomethane ND ug/L 5 1.00 08/30/99 RPJ 74-95-3 BromodichLoromethane ND ug/L 5 1.00 08/30/99 RPJ 75-27-4 4-Methyl-2-Pentanone ND uq/( 50 1.00 08/30/99 RPJ 108-10-1 cis-1,3-DichLoropropene ND ug/L 5 1.00 08/30/99 RPJ 10061-01-5 ToLuene ND ug/L 5 1.00 08/30/99 RPJ 108-88-3 trans-1,3-Dichteropropene ND ug/t 5 1.00 08/30/99 RPJ 10061-02-6 1,1,2-Trichtoroethane ND uq/t 5 1.00 08/30/99 RPJ 79-00-5 2-Hexanone ND uqJL 50 1.00 08/30/99 RPJ 591-78-6 Dibromochioromethane ND ug/1 5 1.00 08/30/99 RPJ 124-48-1 TetrachLoroethene ND ug/l 5 1.00 08130/99 RPJ 127-18-4 1,2-Dibromoethane ND uq/L 5 1.00 08/30/99 RPJ 106-93-4 Chlorobenzene ND ug/L 5 1.00 08/30/99 RPJ 108-90-7 Footnotes Laboratory Certification Laboratory Certification I Ds KY Drinking Water 90090 REPORT OF LABORATORY ANALYSIS TN LIST List This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. IDs NC Wastewater 12 INC Drinking Water 37706 SC 99006 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Eace Analytical Huntersville, NG 28078 Tel: 704-875-9092 Fax: 704-875-909,1 DATE: 09/02/99 PAGE: 10 Pace Project Number: 928351 CHent Project ID: McDowell LandfiLt-937576 Pace Sample No: 93342319 Date CoLLected: 08/26/99 Matrix: Water Client Sampte ID: TRAVEL BLANK Date Received: 08/27/99 Parameters Results Units PRIL --------------------------------- 1,1,1,2-Tetrachtoroethane ---------- ND --------- ug/L ---------- 5 Ethytbenzene ND ug/L 5 rn&p-XyLene ND uq/1 10 Styrene No ug/t 5 o-XyLene (1,2-Dimethytbenzene) ND ug/L 5 Bromoform No ug/L 5 1,1,2,2-TetrachLoroethane No ug/1 5 1,2,3-Trichloropropane ND ug/1 5 trans- I 4-Dichtoro-2-Butene ND ug/L 5 1,4-DichLorobenzene ND ug/L 5 1,2-Dichlorobenzene ND ug/L 5 1,2-Dibrow-3-Chloropropane ND ug/t 5 Dibromof Luoromethane (S) 102 % 1,2-DichLoroethane-d4 (S) 101 % ToLuene-d8 (S) 98 % 4-Bromofluorobenzene (S) 97 % App. DF AnaLyzed Analyst CAS# Footnotes -------- -------- ----- ---------- ---------- 1.00 08/30/99 RPJ 630-20-6 1.00 08/30/99 RPJ 100-41-4 1.00 08/30/99 RPJ 7816-60-0 1.00 08/30/99 RPJ 100-42-5 1.00 08/30/99 RPJ 95-47-6 1.00 08/30/99 RPJ 75-25-2 1.00 08/30/99 RPJ 79-34-5 1.00 08/30/99 RPJ 96-18-4 1.00 08/30/99 RPJ 110-57-6 1.00 08/30/99 RPJ 106-46-7 1.00 08/30/99 RPJ 95-50-1 1.00 08/30/99 RPJ 96-12-8 1.00 08/30/99 RPJ 1868-53-7 1.00 08/30/99 RPJ 17060-07-0 1.00 08/30/99 RPJ 2037-26-5 1.00 08/30/99 RPJ 460-00-4 Laboratory Certfication IN Laboratory Certification IDs; NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 KinGey Avenue, Suite 100 EaQe Analytical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9Q�'l DATE: 09/02/99 PAGE: 11 Pace Project Number: 928351 Client Project ID: McDowell. LandfiLL-937576 Pace Sample No: 93342327 Date Cottected: 08/26/99 Matrix: Water Client Sample ID: EQUIP BLANK Date Received: 08/27/99 Parameters Results Units PRIL App. OF Analyzed Analyst CAB# Footnotes --------------------------------- ---------- --------- ---------- -------- -------- ----- ---------- --------- GC/MS VoLatiLes GC/MS VOCs by 8260 Method: EPA 8260 Prep Method: EPA 8260 Chloromethane NO ug/L 10 1.00 08/31/99 RPJ 74-87-3 Vinyl Chloride NO ug/l 10 1.00 08/31/99 RPJ 75-01-4 Bromomethane NO uq/L 10 1.00 08/31/99 RPJ 74-83-9 Chtoroethane NO ug/L 10 1.00 08/31/99 RPJ 75-00-3 Trichtorof luoromethane NO ug/t 10 1.00 08/31/99 RPJ 75-69-4 Acetone NO ug/L 100 1.00 08/31/99 RPJ 67-64-1 1,1-DichtorDethene ND ug/L 5 1.00 08/31/99 RPJ 75-35-4 Iodomethane NO ug/I 5 1.00 08/31/99 RPJ 74-88-4 Acrylonitrile NO ug/L 100 1.00 08/31/99 RPJ 107-13-1 Methytene Chloride NO ug/t 5 1.00 08/31/99 RPJ 75-09-2 Carbon Disutfide NO uq/t 5 1.00 08/31/99 RPJ 75-15-0 trans-1,2-Dichloroethene NO ug/L 5 1.00 08/31/99 RPJ 156-60-5 1,1-Dichtoroethane NO ug/1 5 1.00 08/31/99 RPJ 75-34-3 Vinyl. Acetate NO ug/L 50 1.00 08/31/99 RPJ 108-05-4 2-Butanone NO ug/L 100 1.00 08/31/99 RPJ 78-93-3 cis-1,2-DichLoroethene NO ug/t 5 1.00 08/31/99 RPJ 156-59-2 Chloroform NO ug/L 5 1.00 08/31/99 RPJ 67-66-3 gromochtoromethane NO ug/L 5 1.00 08/31199 RPJ 74-97-5 1,1,1-Trichloroethane NO ug/l 5 1.00 08/31/99 RPJ 71-55-6 1,2-DichLoroethane NO ug/L 5 1.00 08/31/99 RPJ 107-06-2 Carbon Tetrachloride NO ug/L 5 1.00 08/31/99 RPJ 56-23-5 Benzene NO ug/t 5 1.00 08/31/99 RPJ 71-43-2 Trichtoroethene NO ug/L 5 1.00 08/31/99 RPJ 79-01-6 1,2-Dichtoropropane NO ug/L 5 1.00 08/31/99 RPJ 78-87-5 Dibromomethane NO ug/I 5 1.00 08/31/99 RPJ 74-95-3 Bromodichloromethane NO ug/L 5 1.00 08/31/99 RPJ 75-27-4 4-MethyL-2-Pentanone NO ug/L 50 1.00 08/31/99 RPJ 108-10-1 cis-1,3-Dichtoropropene NO ug/t 5 1.00 08/31/99 RPJ 10061-01-5 Toluene NO ug/L 5 1.00 08/31/99 RPJ 108-88-3 trans-1,3-Dichloropropene NO uq/1 5 1.00 08/31/99 RPJ 10061-02-6 1,1,2-Trichtoroethene NO ug/I 5 1.00 08/31199 RPJ 79-00-5 2-Hexanone NO ug/L 50 1.00 08/31/99 RPJ 591-78-6 Dibromochtoromethane NO ug/1 5 1.00 08/31/99 RPJ 124-48-1 Tetrachloroethene NO uq/L 5 1.00 08/31/99 RPJ 127-18-4 1,2-Dibromoethane NO ug/L 5 1.00 08/31/99 RPJ 106-93-4 ChLorobenzene NO ug/I 5 1.00 08/31/99 RPJ 108-90-7 Laboratory Certification IDs Laboratory Certification IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS Thl UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Aaalytical Huntersville, NC 28078 Tel: 704-875-7092 Fax: 704-875-9091 DATE: 09/02/99 PAGE: 12 Pace Project Number: 928351 CLient Project ID: McDowell. LandfiLL-937576 Pace SampLe No: 93342327 Date Cottected: 08/26/99 Matrix: Water CLient SampLe ID: EQUIP BLANK Date Received: 08/27/99 Parameters --------------------------------- Results ---------- Units PRL App. DF 1, 1, 1 2-TetrachLoroethane ND --------- ug/t ---------- 5 -------- 1.00 EthyLbenzene ND ug/L 5 1.00 m&p-Xytene ND ug/t 10 1.00 Styrene ND ug/L 5 1.00 o-Xylene (1,2-Dimethylbenzene) ND ug/t 5 1.00 Bromoform ND ug/t 5 1.00 1,1,2,2-Tetrachioroethane ND ug/L 5 1.00 1,2,3-Trichlorapropane ND ug/I 5 1.00 trans- 1, 4-Dich [Oro-2-Butene ND ug/L 5 1.00 1,4-DichLorobenzene ND uq/1 5 1.00 1,2-Dichlorobenzene ND ug/L 5 1.00 1,2-Dibromo-3-ChLoropropane ND uq/t 5 1.00 Dibromofluoromethane (S) 101 % 1.00 1,2-DichLoroethane-d4 (s) 100 % 1.00 ToLuene-d8 (S) 101 % 1.00 4-Bromof Luorobenzene (S) 95 % 1.00 Analyzed AnaLyst CAB# Footnotes 08/31/99 RPJ 630-20-6 08/31/99 RPJ 100-41-4 08/31/99 RPJ 7816-60-0 08/31/99 RPJ 100-42-5 08/31/99 RPJ 95-47-6 08/31/99 RPJ 75-25-2 08/31199 RPJ 79-34-5 08/31/99 RPJ 96-18-4 08/31/99 RPJ 110-57-6 08/31/99 RPJ 106-46-7 08/31/99 RPJ 95-50-1 08/31/99 RPJ 96-12-8 08/31/99 RPJ 1868-53-7 08/31/99 RPJ 17060-07-0 08/31/99 RPJ 2037-26-5 08/31/99 RPJ 460-00-4 Labgratory Certification IDs Laboratory Certification IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kuncey Avenue, Suite 100 Pace Aualytical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-90p) DATE: 09/02/99 PAGE: 13 Pace Project Number: 928351 Client Project ID: McDowell. LandfiLL-937576 PARAMETER FOOTNOTES NO Not Detected NC Not Calculable PRL Pace Reporting Limit (S) Surrogate App. DF Applied Dilution Factor 0] Surrogate recovery outside of acceptance window confirmed as matrix affect by analysis of MS/MSD on this sample matrix. [21 Low surrogate recovery was confirmed as a matrix effect by a second analysis. Laboratory Certification IDs LaborgaQry CerifiQation IDS NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analytical Huntersviffe, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 QUALITY CONTROL DATA DATE: 09/02/99 PAGE: 14 McDowel L County Landf i I I Pace Project Number: 928351 10 East Court Street Ctient Project ID: McDoweLt LandfiLL-937576 Marion, NC 28752 Attn: Mr. Mike GLadden QC Batch ID: 16722 QC Batch Method: EPA 8260 Analysis Method: EPA 8260 Anatysis Description: GC/MS VOCs by 8260 Associated Pace Samptes: 93342277 93342285 93342293 93342301 93342319 93342327 METHOD BLANK: 92607670 Associated Pace SampLes: 93342277 93342285 93342293 93342301 93342319 93342327 Method Stank Parameter ------------------------------ Units ---------- ResuLt PRL Footnotes Chtoromethane Ug/t ---------- NO ---------- ---------- 10 Vinyl Chtoride ug/L NO 10 Bromomethane ug/I NO 10 ChLoroethane ug/L ND 10 TrichLorofluoromethane Ug/t NO 10 Acetone ug/L ND 100 1,1-Dichloroethene ug/1 NO 5 lodomethane ug/t ND 5 AcrytonitriLe ug/1 ND 100 Methytene Chloride ug/t NO 5 Carbon DisuLfide ug/L IND 5 trans-1,2-Dichlorcethene ug/I NO 5 1,1-DichLoroethane ug/L ND 5 Vinyl. Acetate Uq/t ND 50 2-Butanone ug/L NO 100 cis-1,2-DichLoroethene Ug/l. NO 5 Chloroform ug/t NO 5 Bromochloromethane Ug/1 NO 5 1,1,1-Trichtoroethane ug/L NO 5 1,2-Dichtoroethane ug/L NO 5 Carbon TetrachLoride ug/t NO 5 Benzene ug/t NO 5 Trichloroethene ug/l NO 5 1,2-Dichtoropropane Ug/t NO 5 Laboratory Certification IlDs Laboratory Certification IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analytical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 QUALITY CONTROL DATA DATE: 09/02/99 PAGE: 15 Pace Project Number: 928351 CLient Project ID: McDowett. Landfitt-937576 METHOD BLANK: 92607670 Associated Pace SampLes: 93342277 93342285 93342293 93342301 93342319 93342327 Method BLank Parameter ------------------------ ----- Units Resutt PRL Footnotes Dibromomethane ---------- ug/L ---------- NO ---------- ---------- 5 Bromodi ch Loromethane u9/1 ND 5 4-Methyt -2-Pentanone uq/L NO 50 cis- 1 3-D i ch Loropropene ug/1 NO 5 Toluene uq/1 ND 5 trans -I 3-D i chtoropropene ug/L NO 5 1, 1 2-Tri ch Loroethane uq/I NO 5 2-Hexanone ug/L ND 50 D i bromoch I orometh ane Uq/1 NO 5 TetrachLoroethene ug/1 ND 5 i 2 - D i br omoet h ane ug/L NO 5 ChLorobenzene ug/t NO 5 1 , 1 , 1 , 2 - T et r ach I o roet In ane ug/L ND 5 Ethylbenzene Ug/I NO 5 m&p-Xytene ug/L ND 10 Styrene ug/t NO 5 o-Xytene (1,2-Dimethylbenzene) ug/t No 5 Bromoform ug/t ND 5 1,1,2,2-Tetrachloroethane ug/1 NO 5 1 2, 3 - T r i ch I o ropr opane ug/L No 5 trans-1,4-Dichloro-2-Butene ug/t NO 5 1,4-Dichlorobenzene Ug/L NO 5 1,2-DichLorobenzene ug/1 NO 5 1 , 2 - D i b r omo - 3 - Ch L o rop ropane ug/L He 5 Dibromof Luoromethane (S) % 100 1,2-Dichtoroethane-d4 (s) % 101 Toluene-d8 (S) % 100 4-BromofLuorobenzene (S) % 81 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 92607720 92607738 Matrix Matrix Spike Spike Spike Spike Sp. Dup. Dup Parameter Units 93342293 Conc. - --------------------------- ---------- ---------- ------- Result ---------- % Rec ----- Resutt ---------- % Rec RPD Footnotes ----- ----- ---------- 1,1-Dichtoroethene Uq/1 0 50 49.71 99.4 56.53 Benzene Uq/L 0 50 46.97 93.9 49.43 Trichloroethene us/[ 0 50 47.39 94.8 50.56 ToLuene ug/L 0 50 44.67 89.3 47.99 113 13 98.9 5 101 6 96.0 7 Laboratory Certification IlDs Laboratory Certification IDs KY Drinking Water 90090 TN LIST List VA Drinking Water 213 INC Wastewater 12 REPORT OF LABORATORY ANALYSIS NC Drinking Water 37706 Sc 99006 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Bace Analytical Huntersville, NG 28078 Tel: 704-875-7092 Fax: 704-875-90ql QUALITY CONTROL DATA DATE: 09/02/99 PAGE: 16 Pace Project Number: 928351 Client Project ID: McDowell Landfitt-937576 MATRIX SPIKE MATRIX SPIKE DUPLICAIE: 94007(eU Y260MB Matrix Matrix Spike Spike Spike Spike Sp. Oup. Dup Parameter Units 93342293 Cone. ------------------------------ ---------- ---------- ------- Result ---------- % Rae ----- Result ---------- % Rae RPD Footnotes ----- -- ChLorobenzene ug/L 0 50 45.38 90.8 47.52 95.0 5 Dibromoftuoromethane (S) 104 105 1,2-DichLoroethane-d4 (S) 101 102 Toluene-d8 (S) 98 98 4-Bromoftuorobenzene (S) 98 86 LABORATORY CONTROL SAMPLE: 92607688 Spike LCS Spike Parameter ------------------------------ Units ---------- Cone. Result % Rae Footnotes Chloromethane ug/L ------- 50 ---------- 25.51 ----- ---------- 51.0 Vinyt Chloride ug/t 50 32.85 65.7 Br omt, methane Uq/L 50 36.37 72.7 ChLoroethane ug/l 50 34.28 68.6 Trichlorof tuoromethane ug/L 50 36.71 73.4 Acetone ug/t 100 129.1 129 1, 1-Dichtoroethene ug/L 50 40.49 81.0 lodomethane ug/l 100 76.49 76.5 AcryLonitrite ug/L 500 361.1 72.2 Methylene Chloride US/[ 50 35.95 71.9 Carbon DisuLfide ug/t 100 81.25 81.3 trans- 1 2-D i ch toroethene ug/L 50 40.35 80.7 1,1-DichLoroethane ug/t 50 36.95 73.9 Vinyl Acetate uq/L 100 53.12 53.1 2-Butanone ug/t 100 96.53 96.5 cis- 1 , 2-Dichlaroethene ug/L 50 39.14 78.3 Chloroform ug/t 50 38.98 78.0 Bromochtoromethane ug/L 50 39.35 78.7 1 , 1 , 1 -Trichioroethane ug/t 50 40.40 80.8 1,2-Dichtoroethane ug/L 50 37.97 75.9 Carbon Tetrachloride ug/t 50 42.24 84.5 Benzene ug/L 50 39.24 78.5 Trichtoroethene ug/L 50 40.43 80.9 1,2-Dichloropropane ug/l 50 40.03 80.1 Dibromomethane ug/L 50 37.46 74.9 Bromodichloromethane ug/t 50 38.58 77.2 4-Methyt-2-Pentanone ug/L 100 73.74 73.7 cis-1;3-Dichtoropropene ug/I 50 36.33 72.7 Toluene ug/L 50 40.15 80.3 trans- 1 3-Dichloropropene ug/l 50 37.90 75.8 Laboratory Certification IDS Laboratory Certification IDS NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN LIST List SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Analytical Huntersville, NO 28078 Tel: 704-875-9092 Fax: 704-875-90.ql LABORATORY CONTROL SAMPLE: 92607688 Parameter 1, 1 2-Trichtoroethane 2-Hexanone D i bromoch Loromethare Tat rach I o roe thene 1 2 -D i bromoethane ChLorobenzene 1 , 1 , 1,2-TetrachLoroethane Ethylbenzene m&p-Xylene Styrene o-XyLene (1,2-Dimethylbenzene) Brormoform 1,1,2,2-Tetrachtoroethane 1,2,3-Trichloropropane trans- 1 4-D i chioro-2-Butene 1,4-DichLorobenzene 1,2-Dichlorobenzene 1,2-Dibromo-3-ChLoropropane Dibromofluoromethane (S) 1,2-Dichloroethane-d4 (s) Toluene-d8 (S) 4-Bromofluorobenzene (s) SAMPLE DUPLICAIE: Y40UYZ6e QUALITY CONTROL DATA DATE: 09/02/99 PAGE: 17 Pace Project Number: 928351 CLient Project ID: McDowell LandfiLL-937576 Spike LCS Spike Units ---------- Conc. ------- Result % Rec Footnotes ug/L 50 ---------- 37.29 ----- --------- 74.6 uq/t 100 89.96 90.0 ug/1 50 37.43 74.9 ug/t 50 40.58 81.2 uq/t 50 38.46 76.9 ug/L 50 38.23 76.5 uq/t 50 39.27 78.5 ug/L 50 35.91 71.8 uq/t 100 64.88 64.9 1 ug/L 50 30.09 60.2 1 ug/t 50 29.74 59.5 1 Ug/t 50 36.50 73.0 uq/t 50 38.52 77.0 uq/1 50 37.61 75.2 ug/l 50 39.62 79.2 ug/1 50 38.24 76.5 ug/L 50 37.51 75.0 uq/t 50 37.98 76.0 99 97 102 86 Cup. Parameter ------------------------------ Units ---------- 92608470 Result RPD Footnotes Chloromethane ug/L ---------- NO ---------- NO ----- ---------- NC Vinyl Chloride ug/t NO NO NC Bromomethane ug/L NO NO NC ChLoroethane ug/l NO ND NC TrichLorofLuoromethane uq/t NO ND NC Acetone ug/L 110.0 130.0 16 1,1-DichLoroethene us/[ NO ND NC loclomethane ug/L NO NO NC Acrytonitrite uq/L NO NO NC MethyLene Chloride uq/1 NO NO NC Carbon Disulfide ug/L NO NO NC trans- I 2-D i ch toroethene us/[ NO ND NC 1,1-Dichtoroethane ug/L NO NO NC Laboratory Certiftation IDs NC Wastewater 12 Laboratoty Certification IDs KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN LIST List SID 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 EaGe Analvtical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-909,1 QUALITY CONTROL DATA DATE: 09/02/99 PAGE: 18 Pace Project Number: 928351 Client Project ID: McDowell. Landfiti-93-(576 SAMPLE DUPLICATE: 92609262 CUP. Parameter ------------------------------ Units ---------- 92608470 Resuit RPD Footnotes Vinyl. Acetate ug/l. ---------- ND ---------- NO ----- ---------- NC 2-Butanone ug/L NO ND NC cis-1,2-Dich[oroethene ug/t ND NO NC Chtoroform ug/L NO ND NC Bromochloromethane ug/t ND NO NC 1,1,1-Trichtoroethane uq/L NO NO NC 1,2-Dichtoroethane ug/t 130.0 130.0 2 Carbon Tetrachloride ug/L NO NO NC Benzene ug/1 1700 1700 0 TrichLoroethene ug/L NO NO NC 1,2-Dichtoropropane ug/1 ND ND NC Dibromomethane ug/L NO NO NC Promodichtoromethane ug/L ND NO NC 4-MethyL-2-Pentanone ug/1 NO NO NC cis- 1,3-Dichloropropene ug/k ND NO NC Toluene ug/t 2000 1900 6 trans-1,3-Dichtoropropene ug/t NO NO NC 1,1,2-TrichLoroethane us/[ NO NO NC 2-Hexanone ug/L ND NO NC Dibromochloromethane ug/t NO NO Nc Tetrachloroethene ug/L NO NO NC 1,2-Dibromoethane ug/t 50.00 52.00 4 ChLorobenzene ug/L NO NO NC 1,1,1,2-Tetrachioroethane uq/1 NO NO NC EthyLbenzene ug/L 190.0 220.0 15 m&p-Xylene ug/t 1100 1300 18 Styrene ug/L NO NO NC D-Xytene (1,2-DimethyLbenzene) us/[ 480.0 560.0 14 Bromoform ug/L NO NO NC 1,1,2,2-Tetrachtoroethane ug/t ND ND NC 1,2,3-TrichLoropropane ug/L NO NO NC trans-1,4-Dichloro-2-Butene ug/t ND NO NC 1,4-Dichlorobenzene ug/L NO NO NC 1,2-Dichtorobenzene u9/1 - ND ND NC 1,2-Dibromo-3-Chloropropane ug/t NO NO NC Dibromoftuoromethane (S) % 102 102 0 1,2-Dichtoroethane-d4 (S) % 99 101 0 ToLuene-d8 (S) % 100 99 0 4-Bromofluorobenzene (S) % 96 92 0 1 4�j'7" --�' Laboratory Certification IDS Laboratory Can fication IDs NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Pace Atiabitical Huntersville, NO 28078 Tel: 704-875-9092 Fax: 704-875-9091 DATE: 09/02/99 PAGE: 19 Pace Project Number: 928351 CLient Project ID: McDowel.l. LandfitL-937576 QUALITY CONTROL DATA PARAMETER FOOTNOTES Consistent with EPA guidelines unrouncled concentrations are dispLayed and have been used to caLculate X Rec and RPD VaLues. NO Not Detected NC Not CaLcutable PRL Pace Reporting Limit RPD Retative Percent Difference (S) Surrogate Ell The surrogate and/or spike recovery was outside acceptance limits. Laboratory Certification Laboratory Certification IDS KY Drinking Water 90090 REPORT OF LABORATORY ANALYSIS TN UST List This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. IDs NC Wastewater 12 NC Drinking Water 37706 Sc 99006 N V rr rr x - rr rr (r, TT rr 7M c m 2 (n 0 z cn 0 Sn -n 0 0 C) Go 0 Q� 00 > anon ITEM > 0 Z m ciF 3 U) (D 0 0 0 0 0 5p? la� 3 M co cm m 9 cn OR 0 0 "A IN cm z z z 0 M MY N c Z 0 > m 3 3 0 q,: 'XI 0 MATRIX CODE ca 3 DATE R. COLLECTED 0 0 3 3 a ��t 3 K TIME e 0 C LLECTED e Containers 0 Unpreserved a �1, 0 H,SO, ID 5 HNO, A- HCI Na,S,O, 0 r 31 J N > ILL Ilk, 7 A Tmsp ,x 77,, V 0 IMMMA rA NCDENR NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES ASHEVILLE REGIONAL OFFICE: DIVISION OF WASTE MANAGEMENT SOLID WASTE SECTION JAMES B. HLINTJR. GOVERNOR MEMORANDUM TO: Phil Prete WAYNE McDEvrrr SECRETARY FROM: Al Hetzell SUBJECT: McDowell County C&D Stockpile/Temporary Storage Area Closure DATE: September 16, 1999 After having reviewed the existing records and information in regards to the area used by McDowell County to store their C&D waste, while a permit was in process, Julian Foscue and I after discussing the situation, feel we can best handle this closure in the field. The County is no longer using this site and wants to close it. A new site proposed for their C&D cannot be permitted so McDowell is currently separating and shipping their C&D waste that can't be recycled. A closure date of April 1, 2000 has been discussed with the Solid Waste Director who is in agreement. Enclosure: Records INTERCHANGE BUILDING, 59 WOODFIN PLACE, ASHEVILLE, NORTH CAROLINA 28801 PHONE 828-2SI-6208 FAX828-251-64S2 AN EQUAL OPPORTUNITY /AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER