5601_ROSCANS_1998

NC DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
Division of Solid Waste Kanagement
Solid Waste Section
SOLID WASTE MUGENENT FACILITY EVALLATION REPORT
Type of facility, Permit county.
Name of FaciLity. Location
Date of Last Evaluation
1. Permit Conditions Followed Yes -No NIA
A. Specific Condition(s) Violated
II. Operational Requirements Followed Yes No
15A N.C. Admin. Code 13B Section
A- Specific Violation(s) by maber and letter.
III. Other Violations of Rule or Law
IV. Evaluator Is Comments
V. Continuation Page Recpire& Yes No Receiving Signature
Evaluatim Date Solid Waste Section
DEHNR 3793 (Part I White: Facility Part II Canary: Central Office Part III Pink: Regional Office)
Solid Waste Section (Review 7/%)

TO. ALBERT A. HETZELL
SOLID WASTE SECTION
NORTH CAROLINA DEPT
OF ENVIRONMENT, HEALTH,
AND NATURAL RESOURCES
FR: MIKE GLADDEN
MCDOWELL COUNTY
PUBLIC WORKS DEPT.
RE: LANDFILL AREA
MONITORING WELLS
Dear Al,
Enclosed are the results of our semi annual monitoring,
of the landfill wells, numbers 1,2,3,& 4.
If you have any questions, please contact me.
S:,L-Pqe V� e
&Gladden
Public Works Director

I
Pace Analytical Services, Inc.
54 havenscroft Drive
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
February 26, 1998
Mr. Mike Gladden
McDowell County Landfill
10 East Court Street
Marion, NC 28752
RE: PACE Project No. A80211.601
Client Reference: Landfill MWIs
Dear Mr. Gladden:
Enclosed is the report of laboratory analyses for samples received
February 11, 1998.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
'--�al-ier L. Mil er
� Project Manager
Enclosures
Labgratory Certification Ips Labqr=jy Certification LDg
No Wastewater 40 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980
NC Drinking Water 37712
SC Environmental 99030 This report shall not be reproduced, except in full, FL Environmental 96317
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analyflical Asheville, NC 28801
Tel: [phone]
Fax: [phone]
McDowell County Landfill
10 East Court Street
Marion, NC 28752
Attn: Mr. Mike Gladden
Client Reference: Landfill MW's
February 26, 1998
PACE Project Number: A80211601
NC Wastewater Lab Cert. #40
NC Drinkingwater Lab Cert. #37712
SC Lab Ceirt,. #99030
PACE Sample Number:
93 0523781
93 0523790
93 0523803
Date Collected:
02/11/98
02/11/98
02/11/98
Date Received:
02/11/98
02/11/98
02/11/98
Client Sample ID:
MW #1
MW #2
MW #3
Parameter
Units PRL
FIELD ANALYSIS
INDIVIDUAL PARAMETERS
Depth to Water
feet
0.01
18.29
40.42
37.00
Specific Conductivity (Field)
umhos/cm2
10
40
280
350
Temperature (Field)
Degrees C
0.5
15
16
16
pH (Field)
Units
0.1
5.0
5.6
5.7
INORGANIC ANALYSIS
APPENDIX I METALS
Silver
mg/L
0.001
0.002
ND
NO
Arsenic
mg/L
0.005
ND
ND
0.006
Barium
mg/L
0.1
1.1
0.2
0.8
Beryllium
mg/L
0.001
0.003
0.002
0.003
Cadmium
mg/L
0.001
ND
0.002
0.002
Cobalt
mg/L
0.001
0.041
0.024
0.019
Chromium
mg/L
0.001
0.024
0.005
0.023
Copper
mg/L
0.01
0.02
0.01
0.03
Nickel
mg/L
0.05
ND
ND
ND
Lead
mg/L
0.005
0.044
0.023
0.071
Antimony
mg/L
0.003
ND
ND
ND
Selenium
mg/L
0.005
ND
ND
ND
Thallium
mg/L
0.001
ND
ND
ND
Vanadium
mg/L
0.005
0.239
0.022
0.085
Zinc
mg/L
0.01
0.16
0.06
0.18
Laboratory Certification 1ps Laboratory Certification A29
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712
SC Environmental 99030 This report shall not be reproduced, except in full, FL Errvironmental 96317
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytmcal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden
Page 2
Client Reference: Landfill MW's
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter Units —PRL
FIELD ANALYSIS
INDIVIDUAL PARAMETERS
February 26, 1998
PACE Project Number: A80211601
93 0523811
02/11/98
02/11/98
MW #4
Depth to Water
feet
0.01
15.84
Specific Conductivity (Field)
umhos/cm2
10
45
Temperature (Field)
Degrees C
0.5
16
pH (Field)
Units
0.1
4.6
INORGANIC ANALYSIS
APPENDIX I METALS
93 0523846
02/11/98
02/11/98
Equip.
Blank
Silver
mg/L
0.001
0.006
NO
Arsenic
mg/L
0.005
0.008
ND
Barium
mg/L
0.1
0.2
IND
Beryllium
mg/L
0.001
NO
ND
Cadmium
mg/L
0.001
NO
NO
Cobalt
mg/L
0.001
ND
NO
Chromium
mg/L
0.001
NO
ND
Copper
mg/L
0.01
ND
NO
Nickel
mg/L
0.05
ND
NO
Lead
mg/L
0.005
NO
IND
Antimony
mg/L
0.003
NO
NO
Selenium
mg/L
0.005
ND
ND
Thallium
mg/L
0.001
ND
NO
Vanadium
mg/L
0.005
0.007
NO
Zinc
mg/L
0.01
0.01
ND
These data have been reviewed and are approved for release.
goo&
Walter L. Miller
Operations Manager
Laboratory Certification IDs Laboratory Certification Qa
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980
NC Drinking Water 37712
SC Environmental 99030 This report shall not be reproduced, except in full, FIL Environmental 96317
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
Pace Analvtical 54 Ravenscroft Drive
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden FOOTNOTES February 26, 1998
Page 3 for pages 1 through 2 PACE Project Number: A80211601
Client Reference: Landfill MW's
ND Not detected at or above the PRL.
PRL PACE Reporting Limit
Labgratory Certification
Lab.Qratory Certification V1
REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
This report shall not be reproduced, except in full, FL Environmental 96317
without the written consent of Pace Analytical Services, Inc.
IN
NC Wastewater
40
NC Drinking Water
37712
SC ErnAronmental
99030

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
McDowell County Landfill
Marion, NC 28752
Attn: Mr. Mike Gladden
Client Reference: McDowell Co.
Tel: [phone]
Fax: [phone]
February 24, 1998
PACE Project Number: A80211601
PACE Sample Number:
93 0523781
Date Collected:
02/11/98
Date Received:
02/12/98
Client Sample ID:
MW#I
Parameter
Units
PRL
DATE & TIME
ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
Methyl Chloride
ug/L
10
ND
02/13/98
16:25
Chloroethene (Vinyl chloride)
ug/L
10
NO
02/13/98
16:25
Bromomethane
ug/L
10
NO
02/13/98
16:25
Chloroethane
ug/L
10
ND
02/13/98
16:25
Trichlorofluoromethane
ug/L
5.0
NO
02/13/98
16:25
Acetone
ug/L
100
NO
02/13/98
16:25
1,1-Dichloroethene
ug/"L
5.0
NO
02/13/98
16:25
Methyl iodide
ug/L
5.0
NO
02/13/98
16:25
Acrylonitrile
ug/L
100
NO
02/13/98
16:25
Dichloromethane
ug/L
5.0
NO
02/13/98
16:25
Carbon disulfide
ug/L
5.0
NO
02/13/98
16:25
trans-1,2-Dichloroethene
ug/L
5.0
ND
02/13/98
16:25
1,1-Dichloroethane
ug/L
5.0
NO
02/13/98
16:25
Vinyl acetate
ug/L
50
ND
02/13/98
16:25
Methyl ethyl ketone
ug/L
100
NO
02/13/98
16:25
cis-1,2-Dichloroethene
ug/L
5.0
NO
02/13/98
16:25
Chloroform
ug/L
5.0
NO
02/13/98
16:25
Bromochloromethane
ug/L
5.0
ND
02/13/98
16:25
1,1,1-Trichloroethane
ug/L
5.0
NO
02/13/98
16:25
1,2-Dichloroethane
ug/L
5.0
ND
02/13/98
16:25
Carbon tetrachloride
ug/L
5.0
NO
02/13/98
16:25
Benzene
ug/L
5.0
NO
02/13/98
16:25
Trichloroethene
ug/L
5.0
ND
02/13/98
16:25
1,2-Dichloropropane
ug/L
5.0
ND
02/13/98
16:25
Dibromomethane
ug/L
5.0
NO
02/13/98
16:25
Bromodichloromethane
ug/L
5.0
ND
02/13/98
16:25
4-Methyl-2-pentanone (MIBK)
ug/L
50
NO
02/13/98
16:25
cis-1,3-Dichloropropene
ug/L
5.0
NO
02/13/98
16:25
Toluene
ug/L
5.0
NO
02/13/98
16:25
Laboratory Certification IN Laboratory Certification IN
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST Ust
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kiflcey Avenue, Suite 100
Huntersville, NC 28078
Mr. Mike Gladden
Page 2
Client Reference: McDowell Co.
Fax: [phone]
February 24, 1998
PACE Project Number: A80211601
PACE Sample Number:
93 0523781
Date Collected:
02/11/98
Date Received:
02/12/98
Client Sample ID:
MW#I
Parameter
Units
—PRL
DATE & TIME
ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
02/13/98
16:25
1,1,2-Trichloroethane
ug/L
5.0
ND
02/13/98
16:25
2-Hexanone
ug/L
50
NO
02/13/98
16:25
Dibromochloromethane
ug/L
5.0
NO
02/13/98
16:25
Tetrachloroethylene
ug/L
5.0
NO
02/13/98
16:25
1,2-Dibromoethane
ug/L
5.0
NO
02/13/98
16:25
Chlorobenzene
ug/L
5,0
NO
02/13/98
16:25
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
02/13/98
16:25
Ethylbenzene
ug/L
5.0
NO
02/13/98
16:25
Xylenes, (total)
ug/L
5.0
NO
02/13/98
16:25
Styrene
ug/L
5.0
NO
02/13/98
16:25
Bromoform
ug/L
5.0
NO
02/13/98
16:25
1,1,2,2-Tetrachloroethane
ug/L
5.0
NO
02/13/98
16:25
1,2,3-Trichloropropane
ug/L
5.0
NO
02/13/98
16:25
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
02/13/98
16:25
1,4-Dichlorobenzene
ug/L
5.0
NO
02/13/98
16:25
1,2-Dichlorobenzene
ug/L
5.0
ND
02/13/98
16:25
1,2-Dibromo-3-chloropropane
ug/L
5.0
NO
02/13/98
16:25
Surrogate - Dibromofluoromethane
%
99
02/13/98
16:25
Surrogate - Toluene-d8
%
106
02/13/98
16:25
Surrogate - 4-Bromofluorobenzene
%
106
02/13/98
16:25
Laboratory Certification Laboratory Certification IN
KY Drinking Water 90090
REPORT OF LABORATORY ANALYSIS TN LIST List
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.
IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite too
Pace Analytocal Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden February 24, 1998
Page 3 PACE Project Number: A80211601
Client Reference: McDowell Co.
PACE Sample Number: 93 0523790
Date Collected: 02/11/98
Date Received: 02/12/98
Client Sample ID: MW#2
Parameter Units PRL DATE & TIME ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
Methyl Chloride
ug/L
10
ND
02/13/98
17: 02
Chloroethene (Vinyl chloride)
ug/L
10
11
02/13/98
17:02
Bromomethane
ug/L
10
ND
02/13/98
17:02
Chloroethane
ug/L
10
ND
02/13/98
17:02
Trichlorofluoromethane
ug/L
5.0
ND
02/13/98
17:02
Acetone
ug/L
100
ND
02/13/98
17:02
1,1-Dichloroetheric.
ug/L
5.0
ND
02/13/98
17:02
Methyl iodide
ug/L
5.0
ND
02/13/98
17:02
Acrylonitrile
ug/L
100
ND
02/13/98
17:02
Dichloromethane
ug/L
5.0
ND
02/13/98
17:02
Carbon disulfide
ug/L
5.0
5.8
02/13/98
17:02
trans-1,2-Dichloroethene
ug/L
5.0
ND
02/13/98
17:02
I,I-Dichloroethane
ug/L
5.0
12
02/13/98
17:02
Vinyl acetate
ug/L
50
ND
02/13/98
17:02
Methyl ethyl ketone
ug/L
100
ND
02/13/98
17:02
cis-1,2-Dichloroethene
ug/L
5.0
91
02/13/98
17:02
Chloroform
ug/L
5.0
ND
02/13/98
17:02
Bromochloromethane
ug/L
5.0
ND
02/13/98
17:02
1,1,1-Trichloroethane
ug/L
5.0
ND
02/13/98
17:02
1,2-Dichloroethane
ug/L
5.0
ND
02/13/98
17:02
Carbon tetrachloride
ug/L
5.0
ND
02/13/98
17:02
Benzene
ug/L
5.0
16
02/13/98
17:02
Trichloroethene
ug/L
5.0
ND
02/13/98
17:02
1,2-Dichloropropane
ug/L
5.0
ND
02/13/98
17:02
Dibromomethane
ug/L
5.0
ND
02/13/98
17:02
Bromodichloromethane
ug/L
5.0
ND
02/13/98
17:02
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
02/13/98
17:02
cis-1,3-Dichloropropene
ug/L
5.0
ND
02/13/98
17:02
Toluene
ug/L
5.0
10
02/13/98
17:02
trans-1,3-Dichloro-l-propene
ug/L
5.0
ND
02/13/98
17:02
1,1,2-Trichloroethane
ug/L
5.0
ND
02/13/98
17:02
Laboratory Certification IDs Laboratory Certification 112s
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST Ust
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services. Inc.
9800 Kincey Avenue. Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden February 24, 1998
Page 4 PACE Project Number: A80211601
Client Reference: McDowell Co.
PACE Sample Number: 93 0523790
Date Collected: 02/11/98
Date Received: 02/12/98
Client Sample ID: MW#2
Parameter Units —PRL DATE & TIME ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
2-Hexanone
ug/L
50
IND
02/13/98
17:02
Dibromochloromethane
ug/L
5.0
NO
02/13/98
17:02
Tetrachloroethylene
ug/L
5.0
ND
02/13/98
17:02
1,2-Dibromoethane
ug/L
5.0
ND
02/13/98
17:02
Chlorobenzene
ug/L
5.0
16
02/13/98
17:02
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
02/13/98
17:02
Ethylbenzene
ug/L
5.0
NU
02/13/98
17:02
Xylenes, (total)
ug/L
5.0
18
02/13/98
17:02
Styrene
ug/L
5.0
IND
02/13/98
17:02
Bromoform
ug/L
5.0
ND
02/13/98
17:02
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
02/13/98
17:02
1,2,3-Trichloropropane
ug/L
5.0
NO
02/13/98
17:02
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
02/13/98
17:02
1,4-Dichlorobenzene
ug/L
5.0
8.7
02/13/98
17:02
1,2-Dichlorobenzene
ug/L
5.0
ND
02/13/98
17:02
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
02/13/98
17:02
Surrogate - Dibromofluoromethane
%
107
02/13/98
17:02
Surrogate - Toluene-d8
%
106
02/13/98
17:02
Surrogate - 4-Bromofluorobenzene
%
103
02/13/98
17:02
Laboratory Certification
IDs
Laboratory Certification lDa
NC Wastewater
NC Drinking Water
12
37706
REPORT OF LABORATORY ANALYSIS
KY Drinking Water 90090
TN UST List
Sc
99006
This report shall not be reproduced, except in full,
VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Mr. Mike Gladden
Page 5
Client Reference: McDowell Co.
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
Methyl Chloride
Chloroethene (Vinyl chloride)
Bromomethane
Chloroethane
Trichlorofluoromethane
Acetone
Tel: [phone]' ,
Fax: [phone]
February 24, 1998
PACE Project Number: A80211601
93 0523803
02/11/98
02/12/98
MW#3
Units —PRL DATE & TIME ANALYZED
ug/L
10
ND
02/13/98
17:39
ug/L
10
ND
02/13/98
17:39
ug/L
10
ND
02/13/98
17:39
ug/L
10
ND
02/13/98
17:39
ug/L
5.0
ND
02/13/98
17:39
ug/L
100
ND
02/13/98
17:39
I,I-Dichloroethene
ug/L
5.0
ND
02/13/98
17 :39
Methyl iodide
ug/L
5.0
ND
02/13/98
17:39
Acrylonitrile
ug/L
100
ND
02/13/98
17:39
Dichloromethane
ug/L
5.0
ND
02/13/98
17:39
Carbon disulfide
ug/L
5.0
ND
02/13/98
17:39
trans-1,2-Dichloroethene
ug/L
5.0
ND
02/13/98
17:39
I,I-Dichloroethane
ug/L
5.0
ND
02/13/98
17:39
Vinyl acetate
ug/L
50
ND
02/13/98
17:39
Methyl ethyl ketone
ug/L
100
ND
02/13/98
17:39
cis-1,2-Dichloroethene
ug/L
5.0
ND
02/13/98
17:39
Chloroform
ug/L
5.0
ND
02/13/98
17:39
Bromochloromethane
ug/L
5.0
ND
02/13/98
17:39
1,1,1-Trichloroethane
ug/L
5.0
ND
02/13/98
17:39
1,2-Dichloroethane
ug/L
5.0
ND
02/13/98
17:39
Carbon tetrachloride
ug/L
5.0
ND
02/13/98
17:39
Benzene
ug/L
5.0
ND
02/13/98
17:39
Trichloroethene
ug/L
5.0
ND
02/13/98
17:39
1,2-Dichloropropane
ug/L
5.0
ND
02/13/98
17:39
Dibromomethane
ug/L
5.0
ND
02/13/98
17:39
Bromodichloromethane
ug/L
5.0
ND
02/13/98
17:39
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
02/13/98
17:39
cis-1,3-Dichloropropene
ug/L
5.0
ND
02/13/98
17:39
Toluene
ug/L
5.0
ND
02/13/98
17:39
trans-1,3-Dichloro-l-propene
ug/L
5.0
ND
02/13/98
17:39
1,1,2-Trichloroethane
ug/L
5.0
ND
02/13/98
17:39
Laboratory Certification IDs Laboratory Certification IN
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST Ust
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Fax: [phone]
Mr. Mike Gladden
Page 6
February
24, 1998
PACE Project Number: A80211601
Client Reference: McDowell Co.
PACE Sample Number:
93 0523803
Date Collected:
02/11/98
Date Received:
02/12/98
Client Sample ID:
MW#3
Parameter
Units
—PRL
DATE & TIME
ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
2-Hexanone
Dibromochloromethane
ug/L
ug/L
50
5.0
ND
02/13/98
17:39
Tetrachloroethylene
ug/L
5.0
ND
ND
02/13/98
17:39
1,2-Dibromoethane
Chlorobenzene
ug/L
5.0
ND
02/13/98
02/13/98
17:39
17:39
1,1,1,2-Tetrachloroethane
ug/L
ug/L
5.0
5.0
ND
ND
02/13/98
17:39
02/13/98
17:39
E thyl benzene
Xylenes, (total)
ug/L
5.0
IND
021/1,3/98
17 :39
Styrene
ug/L
ug/L
5.0
5.0
IND
ND
02/13/98
17:39
Bromoform
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
02/13/98
02/13/98
17:39
17:39
1,2,3-Trichloropropane
ug/L
ug/L
5.0
5.0
ND
ND
02/13/98
17:39
02/13/98
17:39
trans-1,4-Dichloro-2-butene
1,4-Dichlorobenzene
ug/L
5.0
ND
02/13/98
17:39
1,2-Dichlorobenzene
ug/L
ug/L
5.0
5.0
IND
02/13/98
17:39
1,2-Dibromo-3-chloropropane
ug/L
5.0
IND
IND
02/13/98
17:39
Surrogate - Dibromofluoromethane
%
110
02/13/98
17:39
Surrogate - Toluene-dS
%
108
02/13/98
17:39
02/13/98
17:39
Surrogate - 4-Bromofluorobenzene
%
98
02/13/98
17:39
Labgr=ry Certification ios
INC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Ubgratory Certification Ma
KY Drinking Water 90090
TN LIST List
VADrinkingWater 213

Pace Analytical Services, Inc.
9800 Kjflcey Avenue, Suite 100
Huntersville, NC 28078
Mr. Mike Gladden
Page 7
Client Reference: McDowell Co.
Fax: [phone]
February 24, 1998
PACE Project Number: A80211601
PACE Sample Number:
93 0523811
Date Collected:
02/11/98
Date Received:
02/12/98
Client Sample ID:
MW#4
Parameter
Units
PRL
DATE & TIME
ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
Methyl Chloride
Chloroethene (Vinyl chloride)
ug/L
ug/L
10
10
NO
NO
02/13/98
18:16
Bromomethane
ug/L
10
NO
02/13/98
02/13/98
18:16
18:16
Chloroethane
Trichlorofluoromethane
ug/L
ug/L
10
5.0
NO
NO
02/13/98
18:16
Acetone
ug/L
100
ND
02/13/98
02/13/98
18:16
18:16
1, 1 -Di-�chlcroethene
Methyl iodide
ug/L
5.0
ND
01211-5198
18:16
Acrylonitrile
ug/L
ug/L
5.0
100
ND
NO
02/13/98
02/13/98
18:16
18:16
Dichloromethane
Carbon disulfide
ug/L
5.0
NO
02/13/98
18:16
trans-1,2-Dichloroethene
ug/L
ug/L
5.0
5.0
13
NO
02/13/98
02/13/98
18:16
18:16
1,1-Dichloroethane
Vinyl acetate
ug/L
5.0
ND
02/13/98
18:16
Methyl ethyl ketone
ug/L
ug/L
50
100
ND
ND
02/13/98
02/13/98
18:16
18:16
cis-1,2-Dichloroethene
Chloroform
ug/L
5.0
NO
02/13/98
18:16
Bromochloromethane
ug/L
ug/L
5.0
5.0
NO
NO
02/13/98
18:16
02/13/98
18:16
1,1,1-Trichloroethane
1,2-Dichloroethane
ug/L
5.0
ND
02/13/98
18:16
Carbon tetrachloride
ug/L
ug/L
5.0
5.0
NO
NO
02/13/98
02/13/98
18:16
18:16
Benzene
Trichloroethene
ug/L
ug/L
5.0
5.0
NO
IND
02/13/98
18:16
1,2-Dichloropropane
ug/L
5.0
NO
02/13/98
02/13/98
18:16
18:16
Dibromomethane
Bromodichloromethane
ug/L
ug/L
5.0
5.0
NO
02/13/98
18:16
4-Methyl-2-pentanone (MIBK)
ug/L
50
NO
NO
02/13/98
02/13/98
18:16
18:16
cis-1,3-Dichloropropene
Toluene
ug/L
5.0
ND
02/13/98
18:16
trans-1,3-Dichloro-l-propene
ug/L
ug/L
5.0
5.0
NO
NO
02/13/98
02/13/98
18:16
18:16
1,1,2-Trichloroethane
ug/L
5.0
NO
02/13/98
18:16
LabQ=iy certification lips
NC Wastewater 12
NC Drinking Water 37706 REPORT OF
LABORATORY ANALYSIS
Laboratory certification IDs;
KY Drinking Water 90090
sc 99006 This report shall not be reproduced,
except in full,
TN UST List
VA Drinking Water 213
without the written
consent of Pace Analytical Services,
Inc,

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite too
Huntersville, NC 28078
J
Mr. Mike Gladden
Page 8
Client Reference: McDowell Co.
Tel: [phone],
Fax: [phone]
February 24, 1998
PACE Project Number: A80211601
PACE Sample Number:
93 0523811
Date Collected:
02/11/98
Date Received:
02/12/98
Client Sample 10:
MW#4
Parameter
Units
PRL
DATE & TIME
ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
2-Hexanone
ug/L
50
ND
02/13/98
18:16
Dibromochloromethane
ug/L
5.0
ND
02/13/98
18:16
Tetrachloroethylene
ug/L
5.0
ND
02/13/98
18:16
1,2-Dibromoethane
ug/L
5.0
ND
02/13/98
18:16
Chlorobenzene
ug/L
5.0
ND
02/13/98
18:16
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
02/13/98
18:16
Ethylbenzent:
ug/L
5.0
ND
02/31-7/98
-118-16
Xylenes, (total)
ug/L
5.0
ND
02/13/98
18:16
Styrene
Bromoform
ug/L
5.0
ND
02/13/98
18:16
1,1,2,2-Tetrachloroethane
ug/L
ug/L
5.0
5.0
ND
ND
02/13/98
02/13/98
18:16
18:16
1,2,3-Trichloropropane
ug/L
5.0
ND
02/13/93
18:16
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
02/13/98
18:16
1,4-Dichlorobenzene
ug/L
5.0
ND
02/13/98
18:16
1,2-Dichlorobenzene
ug/L
5.0
ND
02/13/98
18:16
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
02/13/98
18:16
Surrogate - Dibromofluoromethane
%
106
02/13/98
18:16
Surrogate - Toluene-d8
%
109
02/13/98
18:16
Surrogate - 4-Bromofluorobenzene
%
99
02/13/98
18:16
Laboratory Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report she[] not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification Ds
KY Drinking Water 90090
TN LIST List
VA Drinking Water 213

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytocal Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden February 24, 1998
Page 9 PACE Project Number: A80211601
Client Reference: McDowell Co.
PACE Sample Number: 93 0523820
Date Collected: 02/11/98
Date Received: 02/12/98
Client Sample ID: Travel
Parameter Units PRL Blank DATE & TIME ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
Methyl Chloride
ug/L
10
IND
02/13/98
18: 08
Chloroethene (Vinyl chloride)
ug/L
10
ND
02/13/98
18:08
Bromomethane
ug/L
10
ND
02/13/98
18:08
Chloroethane
ug/L
10
ND
02/13/98
18:08
Trichlorofluoromethane
ug/L
5.0
ND
02/13/98
18:08
Acetone
ug/L
100
ND
02/13/98
18:08
I,1-Dichloroet'hE:i,L,
ug/L
5.0
ND
02/13/98
18:U�
Methyl iodide
ug/L
5.0
ND
02/13/98
18:08B
Acrylonitrile
ug/L
100
ND
02/13/98
18:08
Dichloromethane
ug/L
5.0
ND
02/13/98
18:08
Carbon disulfide
ug/L
5.0
ND
02/13/98
18:08
trans-1,2-Dichloroethene
ug/L
5.0
ND
02/13/98
18:08
I,I-Dichloroethane
ug/L
5.0
IND
02/13/98
18:08
Vinyl acetate
ug/L
50
ND
02/13/98
18:08
Methyl ethyl ketone
ug/L
100
IND
02/13/98
18:08
cis-1,2-Dichloroethene
ug/L
5.0
ND
02/13/98
18:08
Chloroform
ug/L
5.0
ND
02/13/98
18:08
Bromochloromethane
ug/L
5.0
ND
02/13/98
18:08
1,1,1-Trichloroethane
ug/L
5.0
ND
02/13/98
18:08
1,2-Dichloroethane
ug/L
5.0
ND
02/13/98
18:08
Carbon tetrachloride
ug/L
5.0
ND
02/13/98
18:08
Benzene
ug/L
5.0
ND
02/13/98
18:08
Trichloroethene
ug/L
5.0
ND
02/13/98
18:08
1,2-Dichloropropane
ug/L
5.0
ND
02/13/98
18:08
Dibromomethane
ug/L
5.0
ND
02/13/98
18:08
Bromodichloromethane
ug/L
5.0
ND
02/13/98
18:08
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
02/13/98
18:08
cis-1,3-Dichloropropene
ug/L
5.0
ND
02/13/98
18:08
Toluene
ug/L
5.0
ND
02/13/98
18:08
trans-1,3-Dichloro-l-propene
ug/L
5.0
ND
02/13/98
18:08
1,1,2-Trichloroethane
ug/L
5.0
ND
02/13/98
18:08
Laboratory CertlAcaton IDs Laboratory Certification IlDs
INC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIM UST List
SC 99006 This report shall not be reproduced, except in full, VA Drinkng Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Hufltersville, NC 28078
Mr. Mike Gladden
Page 10
Client Reference: McDowell Co.
Tel: [phone],
1
Fax: [phone]
February 24, 1998
PACE Project Number: A80211601
PACE Sample Number:
93 0523820
Date Collected:
02/11/98
Date Received:
02/12/98
Client Sample ID:
Travel
Parameter
Units
PRL
Blank
DATE & TIME
ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
2-Hexanone
ug/L
50
ND
02/13/98
18:08
Dibromochloromethane
ug/L
5.0
ND
02/13/98
18:08
Tetrachloroethylene
ug/L
5.0
ND
02/13/98
18:08
1,2-Dibromoethane
ug/L
5.0
ND
02/13/98
18:08
Chlorobenzene
ug/L
5.0
ND
02/13/98
18:08
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
02/13/98
18:08
Ethylbenzene ,
ug/L
5.0
ND
02/13/98
18:08
Xylenes, (total)
ug/L
5.0
IND
02/13/98
18:08
Styrene
ug/L
5.0
ND
02/13/98
18:08
Bromoform
ug/L
5.0
IND
02/13/98
18:08
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
02/13/98
18:08
1,2,3-Trichloropropane
ug/L
5.0
ND
02/13/98
18:08
trans--1,4-Dichloro-2-butene
ug/L
5.0
ND
02/13/98
18:08
1,4-Dichlorobenzene
ug/L
5.0
IND
02/13/98
18:08
1,2-Dichlorobenzene
ug/L
5.0
ND
02/13/98
18:08
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
02/13/98
18:08
Surrogate - Dibromofluoromethane
%
108
02/13/98
18:08
Surrogate - Toluene-d8
%
106
02/13/98
18:08
Surrogate - 4-Bromofluorobenzene
%
102
02/13/98
18:08
Laboratory Certification Us Laboratory Certification IN
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

. 1.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Mr. Mike Gladden
Page 11
Client Reference: McDowell Co.
Fax: [phone]
February 24, 1998
PACE Project Number: A80211601
PACE Sample Number:
93 0523846
Date Collected:
02/11/98
Date Received:
02/12/98
Client Sample ID:
Equip.
Parameter
Units
PRL
Blank
DATE & TIME
ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
Methyl Chloride
ug/L
10
ND
02/13/98
20:45
Chloroethene (Vinyl chloride)
ug/L
10
NO
02/13/98
20:45
Bromomethane
Chloroethme
ug/L
10
NO
02/13/98
20:45
Trichlorofluoromethane
ug/L
ug/L
10
5.0
ND
ND
02/13/98
02/13/98
20:45
20:45
Acetone
ug/L
100
NO
02/13/98
20:45
1,1-Dichloroethene
ug/L
5.0
ND
02/13/98
20:45
Methyl iodide
ug/L
5.0
NO
02/13/98
20:45
Acrylonitrile
ug/L
100
NO
02/13/98
20:45
Dichloromethane
ug/L
5.0
ND
02/13/98
20:45
Carbon disulfide
ug/L
5.0
NO
02/13/98
20:45
trans-1,2-Dichloroethene
ug/L
5.0
NO
02/13/98
20:45
I,I-Dichloroethane
ug/L
5.0
NO
02/13/98
20:45
Vinyl acetate
ug/L
50
NO
02/13/98
20:45
Methyl ethyl ketone
ug/L
100
ND
02/13/98
20:45
cis-1,2-Dichloroethene
ug/L
5.0
NO
02/13/98
20:45
Chloroform
ug/L
5.0
NO
02/13/98
20:45
Bromochloromethane
ug/L
5.0
NO
02/13/98
20:45
1,1,1-Trichloroethane
ug/L
5.0
NO
02/13/98
20:45
1,2-Dichloroethane
ug/L
5.0
ND
02/13/98
20:45
Carbon tetrachloride
ug/L
5.0
ND
02/13/98
20:45
Benzene
Trichloroethene
ug/L
ug/L
5.0
5.0
NO
NO
02/13/98
20:45
1,2-Dichlaropropane
ug/L
5.0
ND
02/13/98
02/13/98
20:45
20:45
Dibromomethane
ug/L
5.0
NO
02/13/98
20:45
Bromodichloromethane
ug/L
5.0
NO
02/13/98
20:45
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
02/13/98
20:45
cis-1,3-Dichloropropene
ug/L
5.0
NO
02/13/98
20:45
Toluene
ug/L
5.0
NO
02/13/98
20:45
trans-1,3-Dichloro-l-propene
ug/L
5.0
ND
02/13/98
20:45
1,1,2-Trichloroethane
ug/L
5.0
NO
02/13/98
20:45
Laboratory Certificat on lDs Laboratory Certification 1121
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIM UST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc,
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Mr. Mike Gladden
Page 12
Client Reference: McDowell Co.
Tel: [phone]
Fax: [phone]
February 24, 1998
PACE Project Number: A80211601
PACE Sample Number:
93 0523846
Date Collected:
02/11/98
Date Received:
02/12/98
Client Sample ID:
Equip.
Parameter
Units
PRL
Blank
DATE & TIME
ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
2-Hexanone
Dibromochloromethane
ug/L
ug/L
50
5.0
NO
NO
02/13/98
02/13/98
20:45
20:45
Tetrachloroethylene
ug/L
5.0
NO
02/13/98
20:45
1,2-Dibromoethane
ug/L
5.0
NO
02/13/98
20:45
Chlorobenzene
ug/L
5.0
NO
02/13/98
20:45
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
02/13/98
20:45
Ethylbenzene
Xylenes, (total)
ug/L
ug/L
5.0
5.0
NO
NO
02/13/98
20:45
Styrene
ug/L
5.0
ND
02/13/98
02/13/98
20:45
20:45
Bromoform
1,1,2,2-Tetrachloroethane
ug/L
ug/L
5.0
5.0
ND
NO
02/13/98
02/13/98
20:45
20:45
1,2,3-Trichloropropane
ug/L
5.0
NO
02/13/98
20:45
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
02/13/98
20:45
1,4-Dichlorobenzene
ug/L
5.0
NO
02/13/98
20:45
1,2-Dichlorobenzene
ug/L
5.0
ND
02/13/98
20:45
1,2-Dibromo-3-chloropropane
ug/L
5.0
NO
02/13/98
20:45
Surrogate - Dibromofluoromethane
%
105
02/13/98
20:45
Surrogate - Toluene-d8
%
109
02/13/98
20:45
Surrogate - 4-Bromofluorobenzene
%
100
02/13/98
20:45
Laboratory Cerfificallon IN Labgratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services. Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Mr. Mike Gladden
Page 13
Client Reference: McDowell Co.
FOOTNOTES
for pages 1 through 12
NO Not detected at or above the PRL.
PRL PACE Reporting Limit
Tel: [phone]
Fax:[phone]
February 24, 1998
PACE Project Number: A80211601
Laboratory Certificati n IlDs Laboratory Certification 1121
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Mr. Mike Gladden
Page 14
Client Reference: McDowell Co.
QUALITY CONTROL DATA
Fax: [phone]
February 24, 1998
PACE Project Number: A80211601
APPENDIX 1, LANDFILL VOLATILES
Batch: 92 69623
Samples: 93 0523781, 93 0523790, 93 0523803, 93 0523811, 93 0523820
93 0523846
METHOD BLANK:
Method
Parameter
Units
PRL
Blank
Methyl CHloride
Tg—/L—
To--
No
Chloroethene (Vinyl chloride)
ug/L
10
ND
Bromomethane
ug/L
10
ND
Chloroethane
ug/L
10
NO
Trichlorofluoromethane
ug/L
5.0
ND
Acetone
ug/L
100
NO
1,1-Dichloroethene
ug/L
5.0
ND
Methyl iodide
ug/L
5.0
NO
Acrylonitrile
ug/L
100
NO
Dichloromethane
ug/L
5.0
ND
Carbon disulfide
ug/L
5.0
NO
trans-1,2-Dichloroethene
ug/L
5.0
ND
1,1-Dichloroethane
ug/L
5.0
NO
Vinyl acetate
ug/L
50
ND
Methyl ethyl ketone
ug/L
100
ND
cis-1,2-Dichloroethene
ug/L
5.0
ND
Chloroform
ug/L
5.0
ND
Bromochloromethane
ug/L
5.0
ND
1,1,1-Trichloroethane
ug/L
5.0
ND
1,2-Dichloroethane
ug/L
5.0
ND
Carbon tetrachloride
ug/L
5.0
ND
Benzene
ug/L
5.0
ND
Trichloroethene
ug/L
5.0
ND
1,2-Dichloropropane
ug/L
5.0
ND
Dibromomethane
ug/L
5.0
ND
Bromodichloromethane
ug/L
5.0
ND
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
cis-1,3-Dichloropropene
ug/L
5.0
ND
Toluene
ug/L
5.0
ND
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
1,1,2-Trichloroethane
ug/L
5.0
ND
Laboratory Certification IN Laboratory Certification IN
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST Ust
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Mr. Mike Gladden
Page 15
Client Reference: McDowell Co.
Pace Analytical Services, Inc.
9800 Kjflcey Avenue, Suite 100
Huntersville, NG 28078
Tel: [phone]'
Fax: [phone]
QUALITY CONTROL DATA February 24, 1998
PACE Project Number: A80211601
APPENDIX I, LANDFILL VOLATILES
Batch: 92 69623
Samples: 93 0523781, 93 0523790, 93 0523803, 93 0523811, 93 0523820
93 0523846
METHOD BLANK:
Method
Parameter
Units
PRL
Blank
2-HexanFne
ug/L
50
ND
Dibromochloromethane
ug/L
5.0
IND
Tetrachloroethylene
ug/L
5.0
NO
1,2-Dibromoethane
ug/L
5.0
ND
Chlorobenzene
ug/L
5.0
IND
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
Ethylbenzene
ug/L
5.0
NO
Xylenes, (total)
ug/L
5.0
NO
Styrene
ug/L
5.0
ND
Bromoform
ug/L
5.0
IND
1,1,2,2-Tetrachloroethane
ug/1-
5.0
NO
1,2,3-Trichloropropane
ug/L
5.0
NO
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
1,4-Dichlorobenzene
ug/L
5.0
IND
1,2-Dichlorobenzene
ug/L
5.0
ND
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
Surrogate - Dibromofluoromethane
%
103
Surrogate - 1,2-Dichloroethane-d4
%
103
Surrogate - Toluene-d8 %
Surrogate - 4-Bromofluorobenzene %
SPIKE AND SPIKE DUPLICATE:
106
101
Spi ke
930523811
Spike
Dupl
Parameter
Units
PRL
MW#4
Recv
Recv
RPD
T�,I-Dichloroethene
7—
gJL
5.0
—
ND
50
-985%
MR
4%
Benzene
ug/L
5.0
ND
50
110%
108%
2%
Trichloroethene
ug/L
5.0
ND
50
112%
112%
0%
Toluene
ug/L
5.0
ND
50
104%
104%
0%
Chlorobenzene
ug/L
5.0
ND
50
108%
106%
2%
Laboratory Certfication IDs Laboratocy Certification -ID
NC Wastewater 12 -a
INC Drinking Water KY Drinking Water 90090
37706 REPORT OF LABORATORY ANALYSIS TIN LIST List
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analyfical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA February 24, 1998
Page 16 PACE Project Number: A80211601
Client Reference: McDowell Co.
APPENDIX 1, LANDFILL VOLATILES
Batch: 92 69623
Samples: 93 0523781, 93 0523790, 93 0523803, 93 0523811, 93 0523820
93 0523846
LABORATORY CONTROL SAMPLE:
Parameter
Units
PRL
Reference
Value
Recv
Methyl CTIoride
U-97 —L
-1-0
--2-0--
135%
Chloroethene (Vinyl chloride)
ug/L
10
20
130%
Bromomethane
ug/L
10
20
155%
Chloroethane
ug/L
10
20
130%
Trichlorofluoromethane
ug/L
5.0
20
115%
Acetone
ug/L
100
40
118%
1,1-Dichloroethene
ug/L
5.0
20
95%
Methyl iodide
ug/L
5.0
40
105%
Acrylonitrile
ug/L
100
200
112%
Dichloromethane
ug/L
5.0
20
105%
Carbon disulfide
ug/L
5.0
40
118%
trans-1,2-Dichloroethene
ug/L
5.0
20
105%
I,I-Dichloroethane
ug/L
5.0
20
105%
Vinyl acetate
ug/L
50
40
113%
Methyl ethyl ketone
ug/L
100
40
128%
cis-1,2-Dichloroethene
ug/L
5.0
20
110%
Chloroform
ug/L
5.0
20
105%
Bromochloromethane
ug/L
5.0
20
105%
1,1,1-Trichloroethane
ug/L
5.0
20
105%
1,2-Dichloroethane
ug/L
5.0
20
105%
Carbon tetrachloride
ug/L
5.0
20
100%
Benzene
ug/L
5.0
20
105%
Trichloroethene
ug/L
5.0
20
110%
1,2-Dichloropropane
ug/L
5.0
20
110%
Dibromomethane
ug/L
5.0
20
110%
Bromodichloromethane
ug/L
5.0
20
100%
4-Methyl-2-pentanone (MIBK)
ug/L
so
40
115%
cis-1,3-Dichloropropene
ug/L
5.0
20
100%
Toluene
ug/L
5.0
20
105%
trans-1,3-Dichloro-l-propene
ug/L
5.0
20
100%
1,1,2-Trichloroethane
ug/L
5.0
20
105%
Laboratory Cerfificaton IN Laboratory Certifical on Ds
INC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST Ust
SC 99006 This report she[] not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Anallit"cal Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA February 24, 1998
Page 17 PACE Project Number: A80211601
Client Reference: McDowell Co.
APPENDIX I, LANDFILL VOLATILES
Batch: 92 69623
Samples: 93 0523781, 93 0523790, 93 0523803, 93 0523811, 93 0523820
93 0523846
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
PRL
Value
Recv
2-Hexanone
-(Tg —/L
5-0
TO-
MY%
Dibromochloromethane
ug/L
5.0
20
100%
Tetrachloroethylene
ug/L
5.0
20
110%
1,2-Dibromoethane
ug/L
5.0
20
105%
Chlorobenzene
ug/L
5.0
20
110%
1,1,1,2-Tetrachloroethane
ug/L
5.0
20
100%
Ethylbenzene
ug/L
5.0
20
110%
Xylenes, (total)
ug/L
5.0
60
97%
Styrene
ug/L
5.0
20
115%
Bromoform
ug/L
5.0
20
105%
1,1,2,2-Tetrachloroethane
ug/L
5.0
20
115%
1 , 2, 3 - T r i c h 1 o r o p r o p a n e
ug/L
5.0
20
110%
trans-1,4-Dichloro-2-butene
ug/L
5.0
20
110%
1,4-Dichlorobenzene
ug/L
5.0
20
115%
1,2-Dichlorobenzene
ug/L
5.0
20
110%
1,2-Dibromo-3-chloropropane
ug/L
5.0
20
135%
Laboratory Certification IDs Laborato!y certification IN
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Fax: [phone]
Mr. Mike Gladden FOOTNOTES February 24, 1998
Page 18 for pages 14 through 17 PACE Project Number: A80211601
Client Reference: McDowell Co.
ND Not detected at or above the PRL.
PRL PACE Reporting Limit
RPD Relative Percent Difference
Laboratory Certificaton IDs
NC Wastewater 12 LahQr&ry Certification 10a
KY Drinking Water googo
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

392958
CHAIN -OF -CUSTODY RECORD
Analytical Request
Client f'i / � .
� j
r , " i
Report To:
�C,:
Turn around Time
-7"0 36
Address
24 Houl.
Pace Client No. 5
Bill.To:
El 48 Hours
�7
El 3-5 Days
Pace Project Manager
P.O. #/Billing
Referenc
2 Weeks
Pace Projec No.
Phone
Pro'ect N a
o.
El Normal 14 Days
Sampled By (PRINT):
W
Requested Due Date:
a:
w
PRESERVATIVES
ANALYSES
REQUEST
bampler Sign
e�
ature Date Sampled
z
w
>
CC
0
0
w
w
No. SAMPLE DESCRIPTION TIME
MATRIX
u_
0
ul
0
z
0
z
PACE NO.
—
0
z
wc
0
x >
z
REMARK
z
6,? 379,
2
I'.) cy
3
4
5 fj lo
o
n
>
6
l'o
—
—
—
—
—
—
—
—
—
—
7
—
—
—
—
—
—
—
8
—
—
— — —
— — — — —
— —
NIP
Li t:.
Additional Comments
SAMPLE
�CONDITION�..
SEE REVERSE SIDE FOR INSTRUCTIONS

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analyfical Asheville, NC 28801
Tel: [phone]
Fax: [phone]
September 09, 1998
Mr. Mike Gladden
McDowell County Landfill
10 East Court St.
Marion. NC 28752
RE: Pace Project Number: 93666
CLient Project ID: Landfill. MW's
Dear Mr. Gladden:
Enclosed are the resuLts of analyses for sample(s) received by the Laboratory on August 24, 1998. If you have any
questions concerning this report, pLease feet free to contact me.
S i ncerel. y,
I I e
0 On
WaLterMilLer
Project Manager
EncLosures
Laboratory Certification IDS Laboratory Certification Ds
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980
NC Drinking Water 37712 FL Environmental 96317
SC Environmental 99030 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drve
Pace Analytocal Asheville, NC 28801
McDowell County Landfill
10 East Court St.
Marion, NC 28752
Attn: Mr. Mike Gladden
Phone; [phone]
solid results are reported on a wet weight basis
Tel: [phone]
Fax: [phone]
DATE: 09/09/98
PAGE: 1
Pace Project Number: 93666
Client Project ID: Landfill MW's
Pace Sample No:
9330044
Date
Collected: 08/24/98 Matrix: Water
Client Sample 10:
MW #1
Date
Received: 08/24/98
Parameters
---------------------------------
Results Units
---------- ---------
PRL
----------
Analyzed Analyst CAB# Footnotes
-------- ----- ---------- ----------
Field Services
Monitoring Wet[ Data
Field Specific Conductance
Depth of Water
Field Grab Data
Field PH
Field Temperature
Metals
1CP Metals
Barium
Copper
Nickel
Zinc
Date Digested
Antimony Furnace, Method 204.2
Antimony
Date Digested
Arsenic, Furnace, Method 206.2
Arsenic
Date Digested
Beryllium, Furnace, Mtd. 210.2
Beryllium
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
Method: Prep Method:
42 umhoslcm 08/24/98 MPS
16.77FT feet 0 08/24/98 MPS
Method: Prep Method:
6.6 0 08/24/98 MPS
16 0 08/24/98 MPS
Method: EPA 200.7
0.52
mg1L
0.1
NO
mg/L
0.01
NO
mg/L
0.05
0.03
mg/L
0.01
Method: EPA 204.2
NO mg1L 0.003
Method: EPA 206.2
NO mg/L 0.005
Method: EPA 210.2
0.001 mg/L 0.001
Prep Method: EPA 3010
09/01/98 KEK 7440-39-3
09/01/98 KEK 7440-50-8
09/01/98 KEK 7440-02-0
09/01/98 KEK 7440-66-6
08/27/98
Prep Method: EPA 20OF
08/28/98 KEK 7440-36-0
08/27/98
Prep Method: EPA 20OF
08/29/98 KEK 7440-38-2
08/27/98
Prep Method: EPA 20OF
08/29/98 MLP 7440-41-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification IDs
TIN Drinking Water 02980
FL Environmental 96317

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analvtical Asheville, NC 28801
Tel: [phone]
Fax: [phone]
DATE: 09/09/98
PAGE: 2
Pace Project Number: 93666
Client Project ID: Landfill MW's
Pace Sampte No: 9330044 Date CoLLected: 08/24/98 Matrix: Water
CLient Sample ID: MW #1 Date Received: 08/24/98
Parameters Results Units PRL AnaLyzed Analyst CAS# Footnotes
--------------------------------- ---------- --------- ---------- -------- ----- ---------- ----------
Date Digested 08/27/98
Cadmium by Furnace, Mtcl
213.2
Method: EPA
213.2
Prep
Method; EPA
20OF
Cadmium
NO mg/L
0.001
09/01/98
KEK
7440-43-9
Date Digested
08/27/98
Chromium by Furnace, Mtd
218.2
Method: EPA
218.2
Prep
Method: EPA
20OF
chromium
0.004 mg/L
0.001
09/02/98
KEK
7440-47-3
Date Digested
08/27/98
Cobalt by Furnace, Mtd 219.2
Method: EPA
219.2
Prep
Method: EPA
20OF
Cobalt
0.018 mg/L
0.001
08/31/98
KEK
7440-48-4
Date Digested
08/27/98
Lead by Furnace, Method
239.2
Method: EPA
239.2
Prep
Method: EPA
20OF
Lead
0.014 mg/L
0.005
08/31/98
KEK
7439-92-1
Date Digested
08/27/98
SeLenium by Furnace, Mtd
270.2
Method: EPA
270.2
Prep
Method: EPA
20OF
SeLenium
ND mg/L
0.005
08/28/98
KEK
7782-49-2
Date Digested
08/27/98
Silver by Furnace, Mtd
272.2
Method: EPA
272.2
Prep
Method: EPA
20OF
silver
NO mg/L
0.001
08/28/98
KEK
7440-22-4
Date Digested
08/27/98
Thattium by Furnace, mtd
279.2
Method: EPA
279.2
Prep
Method: EPA
20OF
ThalLium
NO mg/L
0.001
08/28/98
KEK
7440-28-0
Date Digested
08/27/98
Vanadium by Furnace, Mtd
286.2
Method: EPA
286.2
Prep
Method: EPA
20OF
Vanadium
0.051 mg/L
0.005
09/04/98
KEK
7440-62-2
Date Digested
08/27/98
Laboratory Certification IN
NC Wastewater 40
NG Drinking Water 37712
SC Environmental 99030
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,
Laboratory Certification IN
TIN Drinking Water 02980
FL Environmental 96317

Pace AflaWical Services, Inc.
54 Ravenscroft Drive
Pace Analyfical Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Pace Sample No: 9330051
CLient Sample 10: MW #2
DATE: 09/09/98
PAGE: 3
Pace Project Number: 93666
Client Project ID: LandfitL MW's
Date Collected: 08/24/98
Date Received: 08/24/98
Parameters Results Units PRI. AnaLyzed Analyst CAB#
--------------------------------- ---------- --------- ---------- -------- ----- ------
FieLd Services
Monitoring Wait Data
Method:
Prep Method:
FieLd Specific Conductance
460 umhos/cm
08/24/98
MPS
Depth of Water
34.92FT feet 0
08/24/98
MPS
FieLd Grab Data
Method:
Prep Method:
FieLd PH
6.0 0
08/24/98
MPS
Field Temperature
17 0
08/24/98
MPS
MetaLs
Matrix: Water
Footnotes
1CP MetaLs
Method: EPA
200.7
Prep
Method; EPA
3010
Barium
0.15
mg/L
0.1
09/01/98
KEK
7440-39-3
Copper
0.02
mg/L
0.01
09/01/98
KEK
7440-50-8
Nickel,
ND
mg/L
0.05
09/01/98
KEK
7440-02-0
Zinc
0.03
mg/L
0.01
09/01/98
KEK
7440-66-6
Date Digested
08/27/98
Antimony Furnace, Method
204.2
Method: EPA
204.2
Prep
Method: EPA
20OF
Antimony
ND
mg/L
0.003
08/28/98
KEK
7440-36-0
Date Digested
08/27/98
Arsenic, Furnace, Method
206.2
Method: EPA
206.2
Prep
Method: EPA
20OF
Arsenic
ND
mg/L
0.005
08/29/98
KEK
7440-38-2
Date Digested
08/27/98
Beryllium, Furnace, Mtd.
210.2
Method: EPA
210.2
Prep
Method: EPA
20OF
Beryllium
ND
mg/L
0.001
08/29/98
MLP
7440-41-7
Date Digested
08/27/98
Cadmium by Furnace, Mtd 213.2
Method: EPA
213.2
Prep
Method: EPA
20OF
Cadmium
ND
mg/L
0.001
09/01/98
KEK
7440-43-9
Date Digested
08/27/98
Chromium by Furnace, Mtd
218.2
Method: EPA
218.2
Prep
Method: EPA
20OF
Chromium
0.001
mg/L
0.001
09/02/98
KEK
7440-47-3
Date Digested
08/27/98
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NIC Drinking Water 37712 FL Environmental 96317
SC Environmental 99030 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
64 Ravenscroff Drive
Parp- Aanalvtiral Asheville, NC 28801
Tel: [phone]
Fax: [phone]
DATE: 09/09/98
PAGE: 4
Pace Project Number: 93666
CHent Project ID: LandfiLt MW's
Pace SampLe NO: 9330051 Date CoLLected: 08/24/98 Matrix: Water
CLient Sample ID: MW #2 Date Received; 08/24/98
Parameters Results Units PIRL AnaLyzed Analyst CAS# Footnotes
------------------- ------------- ---------- --------- ---------- -------- ----- ---------- ----------
Cobalt by Furnace, Mtcl 219.2 Method: EPA 219.2 Prep Method: EPA 20OF
CobaLt 0.023 mg/L 0.001 08/31/98 KEK 7440-48-4
Date Digested 08/27/98
Lead by Furnace, Method 239.2
Lead
Date Digested
SeLenium by Furnace, Mtd 270.2
Selenium
Date Digested
Silver by Furnace, Mtcl 272.2
SiLver
Date Digested
ThaLLium by Furnace, Mtd 279.2
ThaLLium
Date Digested
Vanadium by Furnace, Mtcl 286.2
Vanadium
Date Digested
Method: EPA 239.2
0.01 mg/L 0.005
Method: EPA 270.2
ND mg/L 0.005
Method: EPA 272.2
ND mg/L 0.001
Method: EPA 279.2
ND mg/L 0.001
Method: EPA 286.2
ND mg/L 0.005
Prep Method: EPA 20OF
08/31/98 KEK 7439-92-1
08/27/98
Prep Method: EPA 20OF
08/28/98 KEK 7782-49-2
08/27/98
Prep Method; EPA 20OF
08/28/98 KEK 7440-22-4
08/27/98
Prep Method: EPA 20OF
08/28/98 KEK 7440-28-0
08/27/98
Prep Method: EPA 20OF
09/04/98 KEK 7440-62-2
08/27/98
Laboratory Certification IDs Laboratory Certification IDS
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NCDrinkingWater 37712 FIL Environmental 96317
SC Environmental 99030 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscreft Drive
Pace Ana1vtical Asheville, NC 28801
Tel: [phone]
Fax: [phone]
DATE: 09/09/98
PAGE: 5
Pace Project Number: 93666
CHent Project ID: Landfil.l. MW's
Pace SampLe No: 9330069 Date CoLLected: 08/24/98
Ctient SampLe ID: MW #3 Date Received: 08/24/98
Parameters ResuLts Units PRL AnaLyzed AnaLyst CAS#
--------------------------------- ---------- --------- ---------- -------- ----- ----------
FieLd Services
Monitoring Well Data
Method:
Prep Method:
FieLd Specific Conductance
270 umhos/cm
08/24/98
MPS
Depth of Water
35.82FT feet 0
08/24/98
MPS
FieLd Grab Data
Method:
Prep Method:
FieLd PH
6.4 0
08/24/98
MPS
FieLd Temperature
18 0
08/24/98
MPS
MetaLs
Matrix: Water
Footnotes
ICP Metals
Method: EPA 200.7
Prep
Method: EPA
3010
Barium
0.22
mg/L 0.1
09/01/98
KEK
7440-39-3
Copper
0.01
mg1L 0.01
09/01/98
KEK
7440-50-8
Nickel.
NO
mg/L 0.05
09/01/98
KEK
7440-02-0
Zinc
0.01
mg/L 0�01
09/01/98
KEK
7440-66-6
Date Digested
08/27/98
Antimony Furnace, Method
204.2
Method; EPA 204.2
Prep
Method: EPA
20OF
Antimony
ND
mg/L 0.003
08/28/98
KEK
7440-36-0
Date Digested
08/27/98
Arsenic, Furnace, Method
206.2
Method: EPA 206.2
Prep
Method: EPA
20OF
Arsenic
ND
mg1L 0.005
08/29/98
KEK
7440-38-2
Date Digested
08/27/98
Beryl.Lium, Furnace, Mtd.
210.2
Method: EPA 210.2
Prep
Method: EPA
20OF
Beryl
ND
mg/L 0.001
08/29/98
MILP
7440-41-7
Date Digested
08/27/98
Cadmium by Furnace, mtd 213.2
Method: EPA 213.2
Prep
Method: EPA
20OF
Cadmium
ND
mg/L 0.001
09/01/98
KEK
7440-43-9
Date Digested
08/27/98
Chromium by Furnace, Mtcl
218.2
Method: EPA 218.2
Prep
Method: EPA
20OF
Chromium
ND
mg/L 0.001
09/02/98
KEK
7440-47-3
Date Digested
08/27/98
Laboratory Ceftification IDS
NC Wastewater 40
REPORT
OF LABORATORY ANALYSIS
INC Drinking Water 37712
SC Errvironmental 99030
This report shall not be reproduced, except in full,
without the written consent of Pace
Analytical Services, Inc.
Laboratory Certification IDs
TIN Drinking Water 02980
FL EnAronmental 96317

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
To[: 704-254-7176
Fax: [phone]
Pace SampLe No: 9330069
CLient SampLe ID: MW #3
DATE: 09/09/98
PAGE: 6
Pace Project Number: 93666
Client Project ID: LandfiLL MW's
Date CoLLected: 08/24/98 Matrix: Water
Date Received: 08/24/98
Parameters Results Units PRIL AnaLyzed AnaLyst CAS# Footnotes
--------------------------------- ---------- --------- ---------- -------- ----- ---------- ----------
CobaLt by Furnace, Mtcl 219.2 Method: EPA 219.2 Prep Method: EPA 20OF
cobalt 0.017 mg/L 0.001 08/31/98 KEK 7440-48-4
Date Digested 08/27/98
Lead by Furnace, Method 239.2
Lead
Date Digested
SeLenium by Furnace, Mtcl 270.2
Selenium
Date Digested
SiLver by Furnace, Mtd 272.2
Si Lver
Date Digested
Thal.Lium by Furnace, Mtd 279.2
ThatHurn
Date Digested
Vanadium by Furnace, Mtcl 286.2
Vanadium
Date Digested
Method: EPA 239.2
0.007 mg/L 0.005
Method: EPA 270.2
ND mg/L 0.005
Method: EPA 272.2
ND mg/L 0.001
Method: EPA 279.2
ND mg/L 0.001
Method: EPA 286.2
0.024 mg/L 0.005
Prep Method: EPA 20OF
08/31/93 KEK 7439-92-1
08/27/98
Prep Method: EPA 20OF
08/28/98 KEK 7782-49-2
08/27/98
Prep Method: EPA 20OF
08/28/98 KEK 7440-22-4
08/27/98
Prep Method: EPA 20OF
08/28/98 KEK 7440-28-0
08/27/98
Prep Method: EPA 20OF
09/04/98 KEK 7440-62-2
08/27/98
Laboratory Certification lDs Laboratory Certification Ma
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TIN Drinking Water 02980
NC Drinking Water 37712 FL Environmental 96317
SC Environmental 99030 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytical Asheville, NC 28801
Tel: [phone]
Fax: [phone]
DATE: 09/09/98
PAGE: 7
Pace Project Number: 93666
Client Project ID: LandfiLL MW's
Pace Sample No: 9330077 Date Collected: 08/24/98 Matrix: Water
Ctient Sampte ID: MW #4 Date Received: 08/24/98
Parameters ResuLts Units PRL AnaLyzed Analyst CAS# Footnotes
--------------------------------- ---------- --------- ---------- -------- ----- ---------- ----------
Field Services
Monitoring Well Data
Method:
Prep
Method:
Field Specific Conductance
58
umhos/cm
08/24/98
MPS
Depth of Water
29.30FT
feet
0
08/24/98
MPS
Field Grab Data
Method:
Prep
Method:
Field pH
5.4
0
08/24/98
MPS
Field Temperature
16
0
08/24/98
MPS
Metals
ICP MetaLs
Method: EPA 200.7
Prep
Method: EPA 3010
Barium
0.25
mg/L
0.1
09/01198
KEK
7440-39-3
Copper
ND
mg/L
0.01
09/01/98
KEK
7440-50-8
Nickel
ND
mg/L
0.05
09/01/98
KEK
7440-02-0
Zinc
0.02
mg/L
0.01
09/01/98
KEK
7440-66-6
Date Digested
08/27/98
Antimony Furnace, Method 204.2
Method: EPA 204.2
Prep
Method: EPA 20OF
Antimony
MID
mg/L
0.003
08/28/98
KEK
7440-36-0
Date Digested
08/27/98
Arsenic, Furnace, Method 206.2
Arsenic
Date Digested
BeryL(ium, Furnace, mtd. 210.2
BeryLLium
Date Digested
Cadmium by Furnace, Mtd 213.2
Cadmium
Date Digested
Chromium by Furnace, Mtd 218.2
Chromium
Date Digested
Method: EPA 206.2
ND mg/L 0.005
Method: EPA 210.2
ND mg/L 0.001
Method: EPA 213.2
MID mg/L 0.001
Method: EPA 218.2
MID mg/L 0.001
Prep Method: EPA 20OF
08/29/98 KEK 7440-38-2
08/27/98
Prep Method: EPA 20OF
08/29/98 MLP 7440-41-7
08/27/98
Prep Method: EPA 20OF
09101/98 KEK 7440-43-9
08/27/98
Prep Method: EPA 20OF
09/02/98 KEK 7440-47-3
08/27/98
Laboratory Certification Laboratory Certification IDS
REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
FL EnAronmental 96317
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
IDS
NC Wastewater
40
NC Drinking Water
37712
SC Enwonmental
99030

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Pace sample NO: 9330077
Client sample ID: MW #4
Parameters
----------------------------
Cobalt by Furnace, Mtd 219.2
Cobalt
Date Digested
Lead by Furnace, Method 239.2
Lead
Date Digested
selenium by Furnace, Mtcl 270.2
selenium
Date Digested
Silver by Furnace, Mtd 272.2
Si Lver
Date Digested
ThaLtium by Furnace, Mtd 279.2
Tha(tium
Date Digested
Vanadium by Furnace, Mtd 286.2
Vanadium
Date Digested
DATE: 09/09/98
PAGE: 8
Pace Project Number: 93666
Client Project ID: Landfill MW's
Date CoLtected: 08/24/98 Matrix: Water
Date Received: 08/24/98
Results Units PRL AnaLyzed Analyst CAS# Footnotes
---------- --------- ---------- -------- ----- ---------- ----------
Method: EPA 219.2 Prep Method: EPA 20OF
ND mg/L 0.001 08/31/98 KEK 7440-48-4
08/27/98
Method: EPA 239.2
ND mg/L 0.005
Method: EPA 270.2
ND mg/L 0.005
Method: EPA 272.2
ND mg/L 0.001
Method; EPA 279.2
ND mg/L 0.001
Method: EPA 286.2
ND mg/L 0.005
Prep Method: EPA 20OF
08/31/98 KEK 7439-92-1
08/27/98
Prep Method: EPA 20OF
08/28/98 KEK 7782-49-2
08/27/98
Prep Method; EPA 20OF
08/28/98 KEK 7440-22-4
08/27/98
Prep method: EPA 20OF
08/28/98 KEK 7440-28-0
08/27/98
Prep Method: EPA 20OF
09/04/98 KEK 7440-62-2
08/27/98
Laboratory Certfication IlDs Laboratory Certification IDs
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712 FL Environmental 96317
SC Environmental 99030 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Favenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Pace SampLe No: 9330085
Client SampLe ID: EQUIPMENT BLANK
DATE: 09/09/98
PAGE: 9
Pace Project Number: 93666
CLient Project ID: LandfitL MW's
Date CoLLected: 08/24/98 Matrix: Water
Date Received: 08/24/98
Parameters ResuLts Units FRI. AnaLyzed Analyst CAB# Footnotes
--------------------------------- ---------- --------- ---------- -------- ----- ---------- ----------
MetaLs
ICP Metals
Method: EPA
200.7
Prep
Method: EPA 3010
Barium
ND
mg/L
0.1
09/01/98
KEK
7440-39-3
copper
ND
mg/L
0.01
09/01/98
KEK
7440-50-8
Nickel
ND
mg/L
0.05
09/01/98
KEK
7440-02-0
Zinc
ND
mg/L
0.01
09/01/98
KEK
7440-66-6
Date Digested
08/27/98
Antimony Furnace, Method 204.2
Method: EPA
204.2
Prep
Method: EPA 20OF
Antimony
ND
mg/L
0.003
08/28/98
KEK
7440-36-0
Date Digested
08/27/98
Arsenic, Furnace, Method 206.2
Arsenic
Date Digested
Bery(Lium, Furnace, Mtd. 210.2
Beryl.Lium
Date Digested
Cadmium by Furnace, Mtd 213.2
Cadmium
Date Digested
Chromium by Furnace, Mtcl 218.2
Chromium
Date Digested
CobaLt by Furnace, Mtcl 219.2
CobaLt
Date Digested
Lead by Furnace, Method 239.2
Lead
Date Digested
Method: EPA 206.2
ND mg/L 0.005
Method: EPA 210.2
NO mg/L 0.001
Method: EPA 213.2
ND mg/L 0.001
Method: EPA 218.2
ND mg1L 0.001
Method: EPA 219.2
ND mg/L 0.001
Method; EPA 239.2
ND mg/L 0.005
Prep Method: EPA 20OF
08/29/98 KEK 7440-38-2
08/27/98
Prep Method: EPA 20OF
08/29/98 MLP 7440-41-7
08/27/98
Prep Method: EPA 20OF
09/01/98 KEK 7440-43-9
08/27/98
Prep Method: EPA 20OF
09/02/98 KEK 7440-47-3
08/27/98
Prep Method: EPA 20OF
08/31/98 KEK 7440-48-4
06/27/98
Prep Method: EPA 20OF
08/31/98 KEK 7439-92-1
08/27/98
Selenium by Furnace, Mtd 270.2 Method: EPA 270.2 Prep Method: EPA 20OF
SeLenium ND mg/L 0.005 08/28/98 KEK 7782-49-2
Laboratory Certification Ds
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS
NC Drinking Water 37712
SC Environmental 99030 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification Ds
TN Drinking Water 02980
FL Environmental 96317

Pace Analytical Services, Inc.
54 Favenscroft Drive
Pni-P Dinniv,tie-ni Asheville, NC 28801
Pace SampLe No: 9330085
CLient SarnpLe ID: EQUIPMENT BLANK
Tel: [phone]
Fax: [phone]
DATE: 09/09/98
PAGE: 10
Pace project Number: 93666
CLient Project ID: LandfitL MW's
Date CoLLected: 08/24/93 Matrix: Water
Date Received: Ca/24/98
Parameters ResuLts Units PRL Anatyzed Anatyst CAS# Footnotes
--------------------------------- ---------- --------- ---------- -------- ----- ---------- ----------
Date Digested 08127/98
SiLver by Furnace, Mtd 272.2 Method: EPA 272.2 Prep Method: EPA 20OF
SiLver ND mg/L 0.001 08/28/98 KEK 7440-22-4
Date Digested 08/27/98
ThaLHum by Furnace, Mtd 279.2
Thal.Hum
Date Digested
Vanadium by Furnace, Mtd 286.2
Vanadium
Date Digested
Method: EPA 279.2
ND mg/L 0.001
Method: EPA 286.2
ND mg1L 0.005
Prep Method; EPA 20OF
08/28/98 KEK 7440-28-0
08/27/98
Prep Method: EPA 20OF
09/04/98 KEK 7440-62-2
08/27/98
Laboratoiy Certification IDs Laboratory Certification lDs
INC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712 FL Environmental 96317
SC Environmental 99030 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytical Asheville, NC 28SC1
Tel: [phone]
Fax: [phone]
DATE: 09/09/98
PAGE: 11
Pace Project Number: 93666
Client Project ID: LandfiLL MWIS
PARAMETER FOOTNOTES
ND Not Detected
NO Not CalcuLabte
PRL Pace Reporting Limit
Laboratory Certification Laboratory Certification IDS
REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
FL Enwonmental 96317
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Sewices, Inc.
IDs
NC Wastewater
40
NCDdnkingWater
37712
SC Environmental
99030

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
To]: 704-875-9092
Fax: [phone]
McD owe t I County Landfi I I
10 East Court Street
Marion, NC 28752
Attn: Mr. Mike G[adden
Solid results are reported on a dry weight basis
DATE: 09/02/98
PAGE: 1
Pace Project Number: 921263
Client Project ID: McDowell Landfitt-93666
Pace Sample No: 9282179 Date Collected: 08/24/98 Matrix: Water
Client Sampte ID: mw-1 - 9330044 Date Received: 08/25/98
Parameters ResuLts Units PRL Analyzed Analyst CAS# Footnotes
--------------------------------- ---------- --------- ---------- -------- ----- ---------- ---------
GC/MS -- VOA
GC/MS vocs by 8260
Method; EPA 8260
Prep
Method: EPA 8260
DichLorodif tuoromethane
ND
ug/L
10
08/25/98
JAC
75-71-8
Chloromethane
ND
ug/L
10
08/25/98
JAC
74-87-3
Vinyl Chloride
ND
ug/L
10
08/25/98
JAC
75-01-4
Bromomethane
ND
ug/L
10
08/25/98
JAC
74-83-9
ChLoroethane
ND
ug/L
10
08/25/98
JAC
75-00-3
T rich Lorof Luoromethane
ND
ug/L
10
08/25/98
JAC
75-69-4
I,I-Dichtoroethene
ND
ug/L
5
08125/98
JAC
75-35-4
MethyLene chicride
No
ug/L
5
08/25/98
JAC
75-09-2
trans- 1 2-Dich Loroethene
ND
ug/L
5
08/25/98
JAC
156-60-5
1,1-Dichloroethane
NO
uq/L
5
08/25/98
JAC
75-34-3
cis- 1 2-Dichlorcethene
ND
ug/L
5
08/25/98
JAC
156-59-2
2,2-Dichloropropane
ND
ug/L
5
08/25/98
JAC
594-20-7
Chloroform
ND
ug/L
5
08/25/98
JAC
67-66-3
BromochLoromethane
ND
ug/L
5
08/25/98
JAC
74-97-5
1,1,1-TrichLoroethane
ND
ug/L
5
08/25/98
JAC
71-55-6
1,1-Dichloropropene
ND
ug/L
5
08/25/98
JAC
563-58-6
1,2-Dichloroethane
ND
ug/L
5
08/25/98
JAC
107-06-2
Carbon Tetrachloride
ND
ug/L
5
08/25/98
JAC
56-23-5
Benzene
ND
ug/L
5
08/25/98
JAC
71-43-2
TrichLoroethene
ND
ug/L
5
08/25/98
JAC
79-01-6
1,2-DichLoropropane
ND
ug/L
5
08/25/98
JAC
78-87-5
Dibromomethane
ND
ug/L
5
08/25/98
JAC
74-95-3
Bromodichloromethane
No
ug/L
5
08/25/98
JAC
75-27-4
Toluene
ND
ug/L
5
08/25/98
JAC
108-88-3
1,1,2-Trichtoroethene
ND
ug/L
5
08/25/98
JAC
79-00-5
1,3-Dichloropropane
ND
ug/L
5
08/25/98
JAC
142-28-9
Laboratory Certification IDS Laboratory Certification Ds
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytocal Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 09/02/98
PAGE: 2
Pace Project Number: 921263
CHent Project ID: McDoweLL Landfilt-93666
Pace Sample No: 9282179 Date Collected: 08/24/98 Matrix: Water
CHent Sample 10: MW-1 - 9330044 Date Received: 08/25/98
Parameters
Resutts
Units
PRL
Analyzed
--------
AnaLyst CAS# Footnotes
----- ---------- ----------
---------------------------------
D i bromoch I a romethane
----------
NO
---------
ug/L
----------
5
08/25/98
JAC
124-48-1
Tetrach I oroethene
NO
ug/L
5
08/25/98
JAC
127-18-4
1,2-Dibromoethane
NO
ug/L
5
08/25/98
JAC
106-93-4
ChLorobenzene
NO
ug/L
5
08/25/98
JAC
108-90-7
1, 1 , 1 , 2-Tetrach I or oethane
ND
uq/L
5
08/25/98
JAC
630-20-6
Ethy(benzene
ND
ug/L
5
08/25/98
JAC
100-41-4
m&p-XyLene
NO
ug/L
10
08/25/98
JAC
7816-60-0
Styrene
NO
ug/L
5
08/25/98
JAC
100-42-5
o-XyLene (1,2-DimethyLbenzene)
NO
ug/L
5
08/25/98
JAC
95-47-.6
Bromoform
NO
ug/L
5
08/25/98
JAC
75-25-2
1,1,2,2-Tetrachlaroethane
ND
uq/L
5
08/25/98
JAC
79-34-5
1 sopropyt benzene (Cumene)
ND
ug/L
5
08/25/98
JAC
98-82-8
1,2,3-Trichtoropropane
ND
ug/L
5
08/25/98
JAC
96-18-4
Bromobenzene
NO
ug/L
5
08/25/98
JAC
108-86-1
n-PropyLbenzene
NO
ug/L
5
08/25198
JAC
103-65-1
2-ChLorotoLuene
NO
ug/L
5
08/25/98
JAC
95-49-8
4-ChtorotoLuene
NO
uq/L
5
08/25/98
JAC
106-43-4
1,3,5-TrimethyLbenzene
ND
ug/L
5
08/25/98
JAC
108-67-8
tert-Butyt benzene
ND
ug/L
5
08/25/98
JAC
98-06-6
1,2,4-TrimethyLbenzene
ND
ug/L
5
08/25/98
JAC
95-63-6
sec-autylbenzene
NO
ug/L
5
08/25/98
JAC
135-98-8
1,3-Dichlorobenzene
NO
ug/L
5
08/25/98
JAC
541-73-1
p-isopropyttoLuene
NO
ug/L
5
08/25/98
JAC
99-87-6
1,4-Dichtorobenzene
ND
uq/L
5
08/25/98
JAC
106-46-7
1,2-DichLorobenzene
ND
ug/L
5
08/25/98
JAC
95-50-1
n-Butytbenzene
NO
ug/L
5
08/25/98
JAC
104-51-8
1,2-Dibromo-3-ChLoropropane
NO
ug/L
5
08/25/98
JAC
96-12-8
1,2,4-Trichlorobenzene
NO
uq/L
5
08/25/98
JAC
120-82-1
NaphthaLene
ND
ug/L
5
08/25/98
JAC
91-20-3
Hexachtorobutadiene
ND
uq/L
5
08/25198
JAC
87-68-3
1,2,3-Trichlorobenzene
ND
ug/L
5
08/25/98
JAC
87-61-6
DibromofLuoromethane (S)
95
%
08/25/98
JAC
1868-53-7
1,2-DichLoroethane-d4 (S)
93
%
08/25/98
JAC
17060-07-0
ToLuene-d8 (S)
106
%
08/25/98
JAC
2037-26-5
4-Bromofluorobenzene (S)
105
%
08/25/98
JAC
460-00-4
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pa e Analytocal Huntersville, NC 28078
Tel: [phone]
Fax [phone]
DATE: 09/02/98
PAGE: 3
Pace Project Number: 921263
CLient Project ID: McDowell. Landfitt-93666
Pace SampLe No: 9282187 Date CoLLected: 08/24/98 Matrix: Water
CHent SampLe ID: mw-2 - 9330051 Date Received: 08/25/98
Parameters Results Units PRL Analyzed Analyst CAS# Footnotes
--------------------------------- ---------- --------- ---------- -------- ----- ---------- ---------
GC/MS -- VOA
GC/MS VOCs by 8260
Method: EPA 8260
Prep
Method: EPA 8260
Dichtorodif luoromethane
ND
ug/L
10
08/25/98
JAC
75-71-8
Chloromethane
ND
ug/L
10
08/25/98
JAC
74-87-3
Vinyl. ChLoride
NO
ug/L
10
08/25/98
JAC
75-01-4
Bromomethane
NO
ug/L
10
08/25/98
JAC
74-83-9
ChLoroethane
ND
ug/L
10
08/25/98
JAC
75-00-3
TrichLoroftuoromethane
ND
ug/L
10
08/25/98
JAC
75-69-4
1,1-DichLoroethene
NO
ug/L
5
08/25/98
JAC
75-35-4
MethyLene Chloride
ND
ug/L
5
08/25/98
JAC
75-09-2
trans- 1 , 2-Dich L oroethene
NO
ug/L
5
08/25/98
JAC
156-60-5
1,1-Dichtoroethane
6.6
ug/L
5
08/25/98
JAC
75-34-3
cis-1,2-Dichloroethene
73
u9/1-
5
08/25/98
JAC
156-59-2
2,2-DichLoropropane
NO
ug/L
5
08/25/98
JAC
594-20-7
ChLoroform
NO
ug/L
5
08/25/98
JAC
67-66-3
Bromochloromethane
NO
ug/L
5
08/25/98
JAC
74-97-5
1,1,1-Trichtoroethane
ND
ug/L
5
08/25/98
JAC
71-55-6
1,1-DichLoropropene
NO
ug/L
5
08/25/98
JAC
563-58-6
1,2-DichLoroethane
NO
ug/L
5
08/25/98
JAC
107-06-2
carbon Tetrachloride
ND
ug/L
5
08/25/98
JAC
56-23-5
Benzene
13
ug/L
5
08/25/98
JAC
71-43-2
Trichtoroethene
ND
ug/L
5
08/25/98
JAC
79-01-6
1,2-Dichloropropane
ND
ug/L
5
08/25/98
JAC
78-87-5
Dilbromomethane
ND
ug/L
5
08/25/98
JAC
74-95-3
BromodichLoromethane
ND
ug/L
5
08/25/98
JAC
75-27-4
ToLuene
23
ug/L
5
08/25/98
JAC
108-88-3
1,1,2-Trichloroethane
NO
ug/L
5
08/25/98
JAC
79-00-5
1,3-Dichloropropane
NO
ug/L
5
08/25/98
JAC
142-28-9
DibromochLoromethane
ND
ug/L
5
08/25/98
JAC
124-48-1
TetrachLoroethene
ND
ug/L
5
08/25/98
JAC
127-18-4
1,2-Dibromoethane
NO
ug/L
5
08/25/98
JAC
106-93-4
Chlorobenzene
22
ug/L
5
08/25/98
JAC
108-90-7
1,1,1,2-TetrachLoroethane
ND
ug/L
5
08/25/98
JAC
630-20-6
EthyLbenzene
ND
ug/L
5
08/25/98
JAC
100-41-4
m&p-Xytene
16
ug/L
10
08/25/98
JAC
7816-60-0
Styrene
NO
ug/L
5
08/25/98
JAC
100-42-5
o-XyLene (1,2-Dimethytbenzene)
8.9
ug/L
5
08/25/98
JAC
95-47-6
Bromoform
ND
ug/L
5
08/25/98
JAC
75-25-2
Laboratory Certification Laboratory Certification IDS
KY Drinking Water 90090
REPORT OF LABORATORY ANALYSIS TIN UST List
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.
IDS
NC Wastewater
12
INC Drinking Water
37706
Sc
99006

Pace Analytical Services, Inc.
9800 Kinney Avenue, Suite 100
Pace Analyfical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 09102/98
PAGE: 4
Pace Project Number: 921263
CLient Project ID: McDoweLt LandfiLL-93666
Pace Sampke No: 9282187 Date CoLLected; 08/24/98 Matrix: Water
CHent Sampte ID: MW-2 - 9330051 Date Received: 08/25/98
Parameters
ResuLts
Units
PRL
----------
AnaLyzed
--------
AnaLyst CAS# Footnotes
----- ---------- ---------
---------------------------------
1,1,2,2-Tetrachloroethane
----------
ND
---------
ug/L
5
08/25/98
JAC
79-34-5
1 sopropy I benzene (Cumene)
ND
ug/L
5
08/25/98
JAC
98-82-8
1,2,3-Trichloropropane
NO
ug/L
5
08125/98
JAC
96-18-4
Bromobenzene
NO
ug/L
5
08/25/98
JAC
108-86-1
n-PropyLbenzene
ND
ug/L
5
08125/98
JAC
103-65-1
2-ChLorotoLuene
ND
ug/L
5
08/25/98
JAC
95-49-8
4-ChLorotoLuene
NO
ug/L
5
08/25/98
JAC
106-43-4
1 , 3,5 -Trimethy t benzene
ND
ug/L
5
08/25/98
JAC
108-67-8
tert-ButyLbenzene
No
ug/L
5
08/25/98
JAC
98-06-6
1,2,4-TrimethyLbenzene
NO
ug/L
5
08/25/98
JAC
95-63-6
sec-Butytbenzene
ND
ug/L
5
08/25/98
JAC
135-98-8
1,3-DichLorobenzene
ND
ug/L
5
08/25/98
JAC
541-73-1
p- I sopropy I to L uene
NO
ug/L
5
08/25/98
JAC
99-87-6
1,4-Dichlorobenzone
7.7
ug/L
5
08/25/98
JAC
106-46-7
1,2-Dichtorobenzene
NO
ug/L
5
08/25/98
JAC
95-50-1
n-ButyLbenzene
No
ug/L
5
08/25/98
JAC
104-51-8
1,2-Dibromo-3-ChLoropropane
ND
ug/L
5
08/25/98
JAC
96-12-8
1 , 2, 4 - T r i ch I o roben z ene
NO
ug/L
5
08/25/98
JAC
120-82-1
NaphthaLene
9.2
ug/L
5
08/25/98
JAC
91-20-3
H exe ch I o r obut ad i ene
ND
ug/L
5
08/25/98
JAC
87-68-3
1,2,3-Trichiorobenzene
HD
ug/L
5
08/25/98
JAC
87-61-6
Dibromoftuoromethane (S)
98
%
08/25/98
JAC
1868-53-7
1,2-Dichioroethane-d4 (S)
96
%
08/25/98
JAC
17060-07-0
Totuene-d8 (S)
105
%
08/25/98
JAC
2037-26-5
4-Bromof Luorobenzene (S)
105
%
08/25/98
JAC
460-00-4
Laboratory Certification
IDs
Laboratory Certification IDs
NC Wastewater
12
REPORT OF LABORATORY ANALYSIS
KY Drinking Water 90090
NC Drinking Water
37706
TIN UST List
Sc
99006
This report shall not be reproduced, except in full,
VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 09/02/98
PAGE: 5
Pace Project Number: 921263
Ctient Project 10: McDoweLL Landfitt-93666
Pace Sample No: 9282195 Date CoLlected: 08/24/98 Matrix: Water
CLient Sample ID: MW-3 - 9330069 Date Received: 08/25/98
Parameters ResuLts Units PRL Analyzed Analyst CAS# Footnotes
--------------------------------- ---------- --------- ---------- -------- ----- ---------- ---------
GC/MS -- VOA
GC/MS VCCs by 8260
Method: EPA 8260
Prep
Method: EPA 8260
Dichtorodif Luoromethane
NO
uq1L
10
08/25/98
JAC
75-71-8
ChLoromethane
NO
uq/L
10
08/25/98
JAC
74-87-3
vinyl Chloride
ND
uq/L
10
08/25/98
JAC
75-01-4
Bromomethane
NO
ug/L
10
08/25/98
JAC
74-83-9
ChLoroethane
NO
us/L
10
08/25/98
JAC
75-0073
Trichtorof Luoromethane
NO
ug/L
10
08/25/98
JAC
75-69-4
1,1-Dichioroethene
ND
ug/L
5
08/25/98
JAC
75-35-4
MethyLene Chloride
NO
ug/L
5
08/25/98
JAC
75-09-2
trans- 1 2-Dich toroethene
NO
ug/L
5
08/25/98
JAC
156-60-5
1,1-DichLoroethane
NO
ug/L
5
08/25/98
JAC
75-34-3
cis- 1 2-Dichtoroethene
NO
ug/L
5
08/25/98
JAC
156-59-2
2,2-Dichtoropropane
NO
ug/L
5
08/25198
JAC
594-20-7
Chtoroform
NO
ug/L
5
08/25/98
JAC
67-66-3
Bromochloromethane
NO
ug/L
5
08/25/98
JAC
74-97-5
1,1,1-Trichtoroethane
NO
ug/L
5
08/25/98
JAC
71-55-6
1,1-DichLoropropene
ND
ug/L
5
08125/98
JAC
563-58-6
1,2-DichLoroethane
NO
ug/L
5
08/25/98
JAC
107-06-2
Carbon TetrachLoride
NO
ug/L
5
08/25/98
JAC
56-23-5
Benzene
NO
ug/L
5
08/25/98
JAC
71-43-2
TrichLoroethene
ND
ug/L
5
08/25/98
JAC
79-01-6
1,2-DichLoropropane
NO
ug/L
5
08/25/98
JAC
78-87-5
Dibromomethame
NO
ug/L
5
08/25/98
JAC
74-95-3
Bromodichtoromethane
ND
ug/L
5
08/25/98
JAC
75-27-4
ToLuene
NO
ug/L
5
08/25/98
JAC
108-88-3
1,1,2-Trichtorcethane
NO
ug/L
5
08/25/98
JAC
79-00-5
1,3-DichLoropropane
NO
ug/L
5
08/25/98
JAC
142-28-9
DibromochLoromethane
NO
ug/L
5
08/25/98
JAC
124-48-1
Tetrachtoroethene
NO
ug/L
5
08/25/98
JAC
127-18-4
1,2-Dibromoethane
NO
ug/L
5
08/25/98
JAC
106-93-4
ChLorobenzene
NO
ug/L
5
08/25/98
JAC
108-90-7
1,1,1,2-Tetrachtoroethane
NO
ug/L
5
08/25/98
JAC
630-20-6
Ethy(benzene
NO
ug/L
5
08/25/98
JAC
100-41-4
m&p-Xylene
NO
ug/L
10
08/25/98
JAC
7816-60-0
Styrene
NO
ug/L
5
08/25/98
JAC
100-42-5
o-Xylene (1,2-Dimethytbenzene)
ND
ug/L
5
08/25/98
JAC
95-47-6
Bromoform
NO
ug/L
5
08/25/98
JAC
75-25-2
Laboratory Certification IDs Laboratory Certification IN
NC Wastewater 12 KY Drinking Water 90090
INC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analyt"cal Huntersvifle, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 09/02/98
PAGE: 6
Pace Project Number: 921263
Client Project ID: McDoweLt Landfill-93666
Pace SampLe No: 9282195 Date Collected: 08/24/98 Matrix: Water
Client SampLe ID: MW-3 - 9330069 Date Received: 08/25/98
Parameters
Results
Units
FRI.
Analyzed
Analyst CAS#
---------------------------------
1, 1 2, 2-Tetrach I oroethane
----------
NO
---------
ug/L
----------
5
--------
08/25/98
-----
JAC
----------
79-34-5
1 sopropyt benzene (Cmene)
NO
ug/L
5
08/25/98
JAC
98-82-8
1,2,3-Trichtoropropane
ND
ug/L
5
08/25/98
JAC
96-18-4
Bromobenzene
NO
ug/L
5
08/25/98
JAC
108-86-1
n-Propylbenzene
NO
ug/L
5
08/25/98
JAC
103-65-1
2-chtorototuene
ND
ug/L
5
08/25/98
JAC
95-49-8
4-ChLorotoLuene
NO
uq/L
5
08/25/98
JAC
106-43-4
1,3,5-Trimethytbenzene
NO
ug/L
5
08/25/98
JAC
108-67-8
tert-ButyLbenzene
ND
ug/L
5
08/25/98
JAC
98-06-6
1,2,4-TrimethyLbenzene
NO
ug/L
5
08/25/98
JAC
95-63-6
sec-Butylbenzene
NO
ug/L
5
08/25/98
JAC
135-98-8
1,3-DichLarobenzene
ND
ug/L
5
08/25/98
JAC
541-73-1
p-isopropyttotuene
ND
ug/L
5
08/25/98
JAC
99-87-6
1,4-Dichlorobenzene
NO
ug/L
5
08/25/98
JAC
106-46-7
1,2-Dichierobenzene
NO
ug/L
5
08/25/98
JAC
95-50-1
n-ButyLbenzene
NO
ug/L
5
08/25/98
JAC
104-51-8
1,2-Dibromo-3-Chloropropane
ND
ug/L
5
08/25198
JAC
96-12-8
1,2,4-Trichlorobenzene
NO
ug/L
5
08/25/98
JAC
120-82-1
Naphthalene
ND
ug/L
5
08/25/98
JAC
91-20-3
Hexachlorobutadiene
NO
uq/L
5
08/25/98
JAC
87-68-3
1,2,3-Trichlorobenzene
ND
ug/L
5
08/25/98
JAC
87-61-6
Dibromof I uoromethane (S)
97
%
08/25/98
JAC
1868-53-7
1,2-Dichloroethane-d4 (S)
100
%
08/25/98
JAC
17060-07-0
ToLuene-d8 (S)
104
%
08/25/98
JAC
2037-26-5
4-13romof Luorobenzene (S)
106
%
08/25/98
JAC
460-00-4
Footnotes
Laboratory Certification Ds Laborato1y Certification IDS
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN LIST List
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytocal Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 09/02/98
PAGE: 7
Pace Project Number: 921263
Client Project ID: McDowel.l. LandfiH-93666
Pace Sampte No: 9282203 Date Cottected: 08/24/98 Matrix: Water
CHent SampLe ID: MW-4 - 9330077 Date Received: 08/25/98
Parameters ResuLts Units PRL Analyzed AnaLyst CAS# Footnotes
---------------- ---------------- ---------- --------- ---------- -------- ----- ---------- ----------
GC/MS -- VOA
GC/MS VOCs by 8260
Method: EPA 8260
Prep
Method: EPA 8260
DichLorodifluoromethane
NO
uq/L
10
08/25198
JAC
75-71-8
ChLoromethane
NO
ug/L
10
08/25/98
JAC
74-87-3
VinyL ChLoride
NO
ug/L
10
08/25/98
JAC
75-01-4
Bromomethane
ND
ug/L
10
08/25/98
JAC
74-83-9
ChLoroethane
NO
ug/L
10
08/25/98
JAC
75-0073
TrichLorofluoromethane
NO
ug/L
10
08/25/98
JAC
75-69-4
1 , 1 -DichLoroethene
NO
ug/L
5
08/25/93
JAC
75-35-4
Methylene Chloride
NO
ug/L
5
08/25/98
JAC
75-09-2
trans - 1 , 2-Dich Loroethene
ND
ug/L
5
08/25/98
JAC
156-60-5
1 , 1 -D i ch Lorcethene
NO
ug/L
5
08/25/98
JAC
75-34-3
cis-1,2-Dichloroethene
NO
ug/L
5
08/25/98
JAC
156-59-2
2, 2-D i ch I. oropropane
ND
ug/L
5
08/25/98
JAC
594-20-7
ChLoroform
ND
ug/L
5
08/25/98
JAC
67-66-3
Bromoch I. or omethane
ND
ug/L
5
08/25/98
JAC
74-97-5
1,1,1-TrichLoroethane
NO
ug/L
5
08/25/98
JAC
71-55-6
I,I-Dichloropropene
NO
ug/L
5
08/25/98
JAC
563-58-6
1 , 2-D i ch L oroethane
ND
ug/L
5
08/25198
JAC
107-06-2
Carbon TetrachLoride
NO
ug/L
5
08/25/98
JAC
56-23-5
Benzene
NO
ug/L
5
08/25/98
JAC
71-43-2
Trich(oroethene
NO
uq/L
5
08/25/98
JAC
79-01-6
1,2-DichLoropropane
ND
ug/L
5
08/25/98
JAC
78-87-5
Dibromomethane
ND
ug/L
5
08/25/98
JAC
74-95-3
BromodichLoromethane
ND
ug/L
5
08/25/98
JAC
75-27-4
Toluene
NO
ug/L
5
08/25/98
JAC
108-88-3
1,1,2-TrichLoroethane
NO
ug/L
5
08/25/98
JAC
79-00-5
1,3-DichLoropropene
NO
ug/L
5
08/25/98
JAC
142-28-9
Dibromochtormethane
ND
ug/L
5
08/25/98
JAC
124-48-1
Tetrachtoroethene
ND
ug/L
5
08/25/98
JAC
127-18-4
1,2-Dibromoethane
ND
ug/L
5
08/25/98
JAC
106-93-4
Chlorobenzene
ND
ug/L
5
08/25/98
JAC
108-90-7
1,1,1,2-TetrachLoroethane
NO
ug/L
5
08/25/98
JAC
630-20-6
EthyLbenzene
NO
ug/L
5
08/25/98
JAC
100-41-4
m&p-XyLene
NO
ug/L
10
08/25/98
JAC
7816-60-0
Styrene
ND
ug/L
5
08/25/98
JAC
100-42-5
o-Xytene (1,2-DimethyLbenzene)
NO
ug/L
5
08/25/98
JAC
95-47-6
Bromoform
NO
ug/L
5
08/25/98
JAC
75-25-2
Laborato1y Certification IDS Laboratory Certification IN
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List
SIC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Pace Sample No: 9282203
Client Sample ID: MW-4 - 9330077
Parameters
1, 1 2,2-Tetrach I oroethane
I sopropy L benzene (Cumene)
1,2,3-Trichloropropane
Bromobenzene
n-Propylbenzene
2-Chtorototuene
4-ChLorotoLuene
1,3,5-TrimethyLbenzene
tert-ButyLbenzene
1 , 2, 4 - T r i methy L benzene
sec -Butyl benzene
1 , 3 - D i ch I. o robenzene
p - I a opropy I to I. uene
1 , 4 - D i c h L o r oben zone
1 , 2 - D i ch L o rcben zene
n- Buty I benzene
I , 2 - D i lor omo - 3 - Ch I o rop ropane
1 , 2, 4 - T r i c h L o r obenzene
Naphthalene
H ex a c h L o r obutad i ene
1 , 2, 3 - T r i c h L or o benz ene
Dilbromof I uoromethane (S)
1,2-Dichtoroethane-d4 (S)
ToLuene-d8 (S)
4-Bromof luorobenzene (S)
Resutts Units
ND
ND
ND
MD
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
93
89
107
103
ug/L
ug/L
uq/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
uq/L
ug/L
ug/L
ug/L
ug/L
uq/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
DATE: 09/02/98
PAGE: 8
Pace Project Number: 921263
CLient Project ID: McDowel.l. LandfiLL-93666
Date ColLected: 08/24/98
Date Received: 08/25/98
PRL AnaLyzed Analyst CAS9
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
08/25/98
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
JAC
79-34-5
98-82-8
96-18-4
108-86-1
103-65-1
95-49-8
106-43-4
108-67-8
98-06i6
95-63-6
135-98-8
541-73-1
99-87-6
106-46-7
95-50-1
104-51-8
96-12-8
120-82-1
91-20-3
87-68-3
87-61-6
1868-53-7
17060-07-0
2037-26-5
460-00-4
Water
Footnotes
Laboratory Certification IN Laboratory Certification IDS
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analyt"cal Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 09/02/98
PAGE: 9
Pace Project Number: 921263
CHent Project ID: McDoweLL LandfiLL-93666
Pace SampLe No: 9282211 Date CoLLected: 08/24/98 Matrix: Water
Ctient SampLe ID: EQUIPMENT BLANK-9330085 Date Received: 08/25/98
Parameters Results Units FRI. AnaLyzed Analyst CAS# Footnotes
---------------- ---------------- ---------- --------- ---------- -------- ----- ---------- ----------
GC/MS -- VOA
CC/MS VoCs by 8260
Method: EPA 8260
Prep
Method: EPA 8260
Dichtorodifluoromethane
ND
uq1L
10
08/25/98
JAC
75-71-8
ChLoromethane
ND
ug/L
10
08/25/98
JAC
74-87-3
Vinyt Chtoride
ND
ug/L
10
08/25/98
JAC
75-01-4
Bromomethane
ND
ug/L
10
08/25/98
JAC
74-83-9
ChLoroethane
ND
ug/L
10
08/25/98
JAC
75-00-3
Trichlorofluoromethane
ND
ug/L
10
08/25/93
JAC
75-69-4
1 , 1-DichLoroethene
ND
ug/L
5
08/25/98
JAC
75-35-4
MethyLene Chtoride
ND
ug/L
5
08/25/98
JAC
75-09-2
trans-1 2-Dich Loroethene
ND
ug/L
5
08/25/98
JAC
156-60-5
1 , I-DichLoroethane
ND
ug/L
5
08/25/98
JAC
75-34-3
cis-1,2-Dichloroethene
ND
ug/L
5
08/25/98
JAC
156-59-2
2,2-DichLoropropane
ND
ug/L
5
08/25/98
JAC
594-20-7
Chtoroform
ND
ug/L
5
08/25/98
JAC
67-66-3
BromochLoromethane
ND
ug/L
5
08/25/98
JAC
74-97-5
1,1,1-Trichloroethane
ND
ug/L
5
08/25/98
JAC
71-55-6
1 , 1-DichLoropropene
ND
ug/L
5
08/25/98
JAC
563-58-6
1,2-DichLoroethane
ND
ug/L
5
08/25/98
JAC
107-06-2
Carbon TetrachLoride
ND
ug/L
5
08/25/98
JAC
56-23-5
Benzene
ND
ug/L
5
08/25/98
JAC
71-43-2
Trichloroethene
ND
ug/L
5
08/25/98
JAC
79-01-6
1,2-DichLoropropene
ND
ug/L
5
08/25/98
JAC
78-87-5
Dibromomethane
ND
ug/L
5
08/25/98
JAC
74-95-3
BromodichLoromethane
ND
ug/L
5
08/25/98
JAC
75-27-4
Toluene
ND
ug/L
5
08/25198
JAC
108-88-3
1,1,2-Trichloroethane
ND
ug/L
5
08/25198
JAC
79-00-5
1,3-DichLoropropane
ND
uq/L
5
08/25/98
JAC
142-28-9
DibromochLoromethane
ND
ug/L
5
08/25/98
JAC
124-48-1
TetrachLoroethene
ND
ug/L
5
08/25/98
JAC
127-18-4
1,2-Dibromoethane
ND
ug/L
5
08/25/98
JAC
106-93-4
ChLorobenzene
ND
ug/L
5
08/25/98
JAC
108-90-7
1,1,1,2-Tetrachtoroethane
ND
ug/L
5
08/25/98
JAC
630-20-6
Ethyl.benzene
ND
ug/L
5
08/25/98
JAC
100-41-4
m&p-Xytene
ND
ug/L
10
08/25/98
JAC
7816-60-0
Styrene
ND
uq/L
5
08/25/98
JAC
100-42-5
o-Xylene (1,2-DimethyLbenzene)
ND
uq/L
5
08/25/98
JAC
95-47-6
Bromoform
ND
ug/L
5
08/25/98
JAC
75-25-2
Laboratory Certification Laboratory Certification IDS
KY Drinking Water 90090
REPORT OF LABORATORY ANALYSIS TN UST List
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.
IDS
INC Wastewater
12
NC Drinking Water
37706
Sc
99006

Pace Analytical Services, Inc.
9800 Kinney Avenue, Suite 100
Pace Analytical Huntersville, NG 28078
Tel: [phone]
Fax: [phone]
DATE: 09/02/98
PAGE: 10
Pace Project Number: 921263
Client Project ID: McDowell LandfiLL-93666
Pace sample No: 9282211 Date Collected: 08/24/98 Matrix: Water
Client sample ID: EQUIPMENT BLANK-9330085 Date Received: 08/25/98
Parameters
Results
Units
PRL
Analyzed
--------
Analyst CAS# Footnotes
----- ---------- ---------
---------------------------------
1, 1 2, 2-Tetrach Loroethane
----- ----
NO
---------
uq/L
----------
5
08/25/98
JAC
79-34-5
1 sopropy I benzene (Cumene)
NO
ug/L
5
08/25/98
JAC
98-82-3
1,2,3-Trichlaropropane
NO
ug/L
5
08/25198
JAC
96-18-4
Bromobenzene
NO
ug/L
5
08/25/98
JAC
108-86-1
n-PropyLbenzene
NO
ug/L
5
08/25/98
JAC
103-65-1
2-ChLorotoluene
ND
ug/L
5
08/25/98
JAC
95-49-8
4-Chtorototuene
NO
ug/L
5
08/25/98
JAC
106-43-4
1,3,5-TrimethyLbenzene
NO
ug/L
5
08/25/98
JAC
108-67-8
tert-ButyLbenzene
NO
ug/L
5
08/25/98
JAC
98-06-6
1,2,4-TrimethyL benzene
ND
Uq/L
5
08/25/98
JAC
95-63-6
sec- Butyl. benzene
ND
ug/L
5
08/25/98
JAC
135-98-8
1,3-Dichiorobenzene
NO
uq/L
5
08/25/98
JAC
541-73-1
p-IsopropyLtoLuene
NO
ug/L
5
08/25/98
JAC
99-87-6
1,4-DichLorobenzene
ND
ug/L
5
08/25/98
JAC
106-46-7
1,2-Dichlorobenzene
ND
ug/L
5
08/25/98
JAC
95-50-1
n-Butylbenzene
NO
ug/L
5
08/25/98
JAC
104-51-8
1,2-Dibromo-3-Chioropropane
NO
ug/L
5
08/25/98
JAC
96-12-8
1,2,4-Trichlorobenzene
ND
ug/L
5
08/25/98
JAC
120-82-1
Naphthalene
ND
ug/L
5
08/25/98
JAC
91-20-3
HexachLorobutacliene
ND
ug/L
5
08/25/98
JAC
87-68-3
1,2,3-TrichLorobenzene
NO
ug/L
5
08/25/98
JAC
87-61-6
DibromofLuoromethane (S)
97
%
08/25/98
JAC
1868-53-7
1,2-DichLoroethane-d4 (S)
98
%
08/25/98
JAC
17060-07-0
ToLuene-d8 (S)
106
%
08/25/98
JAC
2037-26-5
4-Bromofluorobenzene (S)
105
%
08/25/98
JAC
460-00-4
Laboratory Cedification IDs Laboratocy Certification Us
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN LIST List
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 09/02/98
PAGE: 11
Pace Project Number: 921263
CLient Project ID; McDoweLt LandfiLL-93666
Pace SampLe No: 9282229 Date Collected: 08/24/98 Matrix: Water
Client SampLe ID: TRAVEL BLANK-9330101 Date Received: 08/25/98
Parameters
GC/MS -- VOA
ResuLts Units
PRL AnaLyzed Analyst CAS# Footnotes
---------- -------- ----- ---------- ----------
GC/MS VoCs by 8260
Method: EPA 8260
Prep
Method: EPA 8260
DichLorodifluoromethane
ND
ug/L
10
08/25/98
JAC
75-71-8
ChLoromethane
NO
ug/L
10
08/25/98
JAC
74-87-3
VinyL Chtoride
NO
uq1L
10
08/25/98
JAC
75-01-4
Bromomethane
NO
ug/L
10
08/25/98
JAC
74-83-9
Chloroethane
NO
ug/L
10
08/25/98
JAC
75-00-3
TrichlorofLuoromethane
NO
ug/L
10
08/25/98
JAC
75-69-4
1 I-DichLoroethene
NO
uq/L
5
08/25/98
JAC
75-35-4
MethyLene Chloride
NO
ug/L
5
08/25/98
JAC
75-09-2
trans-1 2-Dich Loroethene
NO
ug/L
5
08/25/98
JAC
156-60-5
1,1-Dichtoroethane
NO
ug/L
5
08/25/98
JAC
75-34-3
cis-1,2-Dichtoroethene
NO
ug/L
5
08/25/98
JAC
156-59-2
2,2-DichLoropropane
NO
ug/L
5
08/25/98
JAC
594-20-7
Chtoroform
ND
ug/L
5
08/25/98
JAC
67-66-3
BromochLoromethane
NO
ug/L
5
08/25/98
JAC
74-97-5
1,1,1-Trichloroethane
NO
uq/L
5
08/25/98
JAC
71-55-6
1 , 1-DichLoropropene
NO
ug/L
5
08/25/98
JAC
563-58-6
1,2-DichLoroethane
NO
ug/L
5
08/25/98
JAC
107-06-2
Carbon TetrachLoride
NO
ug/L
5
08/25/98
JAC
56-23-5
Benzene
ND
ug/L
5
08/25/98
JAC
71-43-2
Trichtoroethene
ND
ug/L
5
08/25/98
JAC
79-01-6
1,2-DichLoropropane
NO
ug/L
5
08/25/98
JAC
78-87-5
Dibromomethane
NO
ug/L
5
08/25/98
JAC
74-95-3
Bromodichtoromethane
NO
ug/L
5
08/25/98
JAC
75-27-4
Toluene
ND
ug/L
5
08/25/98
JAC
108-88-3
1,1,2-TrichLoroethane
NO
ug/L
5
08/25/98
JAC
79-00-5
1,3-DichLoropropane
NO
ug/L
5
08/25/98
JAC
142-28-9
Dibromochtoromethane
NO
ug/L
5
08/25/98
JAC
124-48-1
Tetrachtoroethene
NO
ug/L
5
08/25/98
JAC
127-18-4
1,2-Dibromoethane
ND
ug/L
5
08/25/98
JAC
106-93-4
Chlorobenzene
NO
u9/1-
5
08/25/98
JAC
108-90-7
1,1,1,2-TetrachLoroethane
NO
ug/L
5
08/25/98
JAC
630-20-6
EthyLbenzene
NO
uq/L
5
08/25/98
JAC
100-41-4
m&p-XyLene
NO
ug/L
10
08/25/98
JAC
7816-60-0
Styrene
NO
ug/L
5
08/25/98
JAC
100-42-5
o-Xytene (1,2-DimethyLbenzene)
NO
ug/L
5
08/25/98
JAC
95-47-6
Bromoform
ND
ug/L
5
08/25/98
JAC
75-25-2
Laboratory Certification IDs Laboratory Certificat an IDs
INC Wastewater 12 KY Drinking Water 90090
INC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analyt"cal Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
DATE: 09/02/98
PAGE: 12
Pace Project Number: 921263
CLient Project ID: McDowell Landfitt-93666
Pace SampLe No: 9282229 Date Collected: 08/24/98 Matrix: Water
Client Sample ID: TRAVEL BLANK-9330101 Date Received: 08/25/98
Parameters
ResuLts
Units
PRIL
AnaLyzed
Analyst CAS# Footnotes
---------- ----------
---------------------------------
1 , 1 2, 2-TetrachLoroethane
----------
ND
---------
ug/L
----------
5
--------
08/25/98
-----
JAC
79-34-5
1 sopropy t benzene (Cumene)
ND
ug/L
5
08/25/98
JAC
98-82-8
1,2,3-Trich[oropropane
ND
ug/L
5
08/25/98
JAC
96-18-4
Bromobenzene
ND
ug/L
5
08/25/98
JAC
108-86-1
n-Propytbenzene
ND
ug/L
5
08/25/98
JAC
103-65-1
2-chtorotoLuene
ND
uq/1-
5
08/25/98
JAC
95-49-8
4-Chiorototuene
ND
ug/L
5
08/25/98
JAC
106-43-4
1,3,5-Trimethytbenzene
ND
ug/L
5
08/25/98
JAC
108-67-8
tert-Butytbenzene
ND
ug/L
5
08/25/98
JAC
98-0676
1,2,4-TrimethyLbenzene
ND
ug/L
5
08/25/98
JAC
95-63-6
sec-Butytbenzene
ND
ug/L
5
08/25/98
JAC
135-98-8
1,3-DichLorobenzene
ND
ug/L
5
08/25/98
JAC
541-73-1
p-isopropyttoLuene
ND
uq/L
5
08/25/98
JAC
99-87-6
1,4-DichLorobenzene
ND
ug/L
5
08/25/98
JAC
106-46-7
1,2-Dichlorobenzene
ND
ug/L
5
08/25/98
JAC
95-50-1
n-ButyLbenzene
ND
ug/L
5
08/25/98
JAC
104-51-8
1,2-Dibromo-3-Chloropropane
ND
ug/L
5
08/25/98
JAC
96-12-8
1,2,4-Trichtorobenzene
ND
ug/L
5
03/25/98
JAC
120-82-1
NaphthaLene
ND
ug/L
5
08/25/98
JAC
91-20-3
HexachLorobutadiene
ND
ug/L
5
08/25/98
JAC
87-68-3
1,2,3-Trichtorobenzene
NO
ug/L
5
08/25/98
JAC
87-61-6
D i bromof I uoromethane (S)
97
%
08/25/98
JAC
1868-53-7
1,2-Dichtoroethane-64 (S)
94
%
08/25/98
JAC
17060-07-0
ToLuene-d8 (S)
106
%
08/25/98
JAC
2037-26-5
4-Bromof Luorobenzene (S)
106
%
08/25/98
JAC
460-00-4
Laboratory Certification Laboratory Cart fication IDs
KY Drinking Water 90090
REPORT OF LABORATORY ANALYSIS TN UST List
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.
IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006

ND
NC
PRL
(S)
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytocal Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Not Detected
Not CaLcuLabLe
Pace Reporting Limit
Surrogate
DATE: 09/02/98
PAGE: 13
Pace Project Number: 921263
CHent Project 10: McDowetL Landfitt-93666
Laboratory Certification Laboratory Certification VDS
KY Drinking Water 90090
REPORT OF LABORATORY ANALYSIS TN LIST List
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.
IDS
NC Wastewater
12
INC Drinking Water
37706
SC
99006

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
QUALITY CONTROL DATA DATE: 09/02/98
PAGE: 14
McDowel. I County Landf i I I Pace Project Number: 921263
10 East Court Street CL i ent Project ID: McDowel. I Landf i I t -93666
Marion, NC 28752
Attn: Mr. Mike Gladden
QC Batch 10: 2173 QC Batch Method: EPA 8260
AnaLysis Method; EPA 8260 AnaLysis Description: GCIMS VOCs by 8260
Associated Pace Samptes: 9282179 9282187 9282195 9282211
METHOD BLANK: 9285735
Associated Pace Samples:
9282179 9282187 9282195 9282211
Method
Stank
Parameter Units ResuLt PRL Footnotes
-------------------- ---------
Dichlorodif Luoromethane
----------
ug/L
----------
ND
- -
10
ChLoromethane
ug/L
NO
10
Vinyl. Chtoride
ug/L
NO
10
Bromomethane
ug/L
ND
10
Chlorcethane
ug/L
NO
10
Trichlorof tuoromethane
uq/L
NO
10
1 , 1-DichLoroethene
ug/L
ND
5
MethyLene Chloride
ug/L
ND
5
trans-1,2-DichLaroethene
ug/L
NO
5
1,1-DichLoroethane
ug/L
ND
5
cis-1,2-Dichtoroethene
ug/L
ND
5
2,2-DichLoropropane
ug/L
NO
5
ChLoroform
ug/L
NO
5
Bromochloromethare
ug/L
ND
5
1,1,1-Trichloroethane
ug/L
NO
5
1,1-DichLoropropene
ug/L
NO
5
1,2-DichLoroethane
ug/L
NO
5
Carbon Tetrachloride
ug/L
NO
5
Benzene
ug/L
NO
5
Trichtoroethene
ug/L
NO
5
1,2-Dichloropropane
ug/L
ND
5
Dibromomethane
ug/L
ND
5
grcmodichtoromethane
ug/L
NO
5
ToLuene
ug/L
NO
5
1,1,2-Trichtoroethane
ug/L
ND
5
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST List
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytocal Huntersvide, NC 28078
Tel: [phone]
Fax: [phone]
QUALITY CONTROL DATA DATE: 09/02/98
PAGE: 15
Pace Project Number: 921263
CLient Project ID: McDowett Landfitt-93666
METHOD BLANK: 9285735
Associated Pace SampLes:
9282179
9282187
9282195 9282211
Method
BLank
Parameter
Units
Resutt
FRI. Footnotes
------------------------------
1 , 3 -D i ch 1. oropropane
----------
ug/L
----------
NO
---------- ----------
5
D i bromoch L orometh a ne
ug/L
NO
5
TetrachLoroethene
ug/L
NO
5
1,2-Dibromoethane
ug/L
NO
5
Chtorobenzene
uq/L
NO
5
1,1,1,2-Tetrachloroethane
ug/L
NO
5
Ethy[benzene
ug/L
NO
5
m&p-Xytene
ug/L
NO
10
Styrene
ug/L
ND
5
o-Xytene (1,2-Dimethylbenzene)
ug/L
NO
5
Bromoform
ug/L
NO
5
1, 1,2,2-Tetrach I oroethane
ug/L
ND
5
lsopropyLbenzene (Cumene)
ug/L
NO
5
1,2,3-TrichLoropropane
ug/L
NO
5
Bromobenzene
ug/L
NO
5
n-Propytbenzene
ug/L
NO
5
2-ChLorotoLuene
uq/L
NO
5
4-ChLorototuene
ug/L
ND
5
1,3,5-Trimethylbenzene
ug/L
NO
5
tert-Butylbenzene
ug/L
NO
5
1,2,4-TrimethyLbenzene
ug/1-
NO
5
sec-Buty(benzene
ug/L
ND
5
1,3-Dichlorobenzene
ug/L
NO
5
p-IsopropyttoLuene
ug/1-
NO
5
1 , 4 -0 i ch Lorobenzene
uq/1-
NO
5
1,2-Dichlorobenzene
uq/L
NO
5
n-ButyLbenzene
ug/L
NO
5
1,2-Dibromo-3-Chloropropane
ug/L
NO
5
1 , 2, 4- Tri ch L orobenzene
ug/L
NO
5
NaphthaLene
ug/L
ND
5
Hexachlorobutadiene
ug/L
NO
5
1,2,3-Trichtorobenzene
ug/L
ND
5
Dibromof tuoromethane (S)
%
92
1,2-Dichloroethane-d4 (S)
%
89
Toluene-d8 (S)
%
101
4-Bromofluarobenzene (S)
%
100
Laboratory Certification Laboratory Certification IDs
KY Drinking Water 90090
REPORT OF LABORATORY ANALYSIS TN UST List
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.
IDs
NC Wastewater
12
INC Drinking Water
37706
SC
99006

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NG 28078
Tel: [phone]
Fax: [phone]
QUALITY CONTROL DATA DATE: 09/02/98
PAGE: 16
Pace Project Number: 921263
CLient Project ID: McDoweLt Landfill-93666
LABORATORY CONTROL SAMPLE: 9285743
Spike
LCS
Spike
Parameter
------------------------------
Units
----------
Conc.
ResuLt
% Rec Footnotes
Dich(orodif Luoromethane
ug/L
-------
50
----------
37.00
----- ---------
74.0
Chloromethane
ug/L
50
50.00
100
Vinyl ChLoride
ug/L
50
48.00
96.0
Bromomethane
ug/L
50
44.00
88.0
ChLoroethane
uq/L
50
55.00
110
Trichtorof tuoromethane
ug/L
50
50.00
100
1,1-DichLoroethene
ug/L
50
60.00
120
Methylene ChLoride
ug/L
50
47.00
94.0
trans- 1 , 2-D ich loroethene
ug/L
50
50.00
100
1,1-Dichloroethane
ug/L
50
48.00
96.0
cis- 1 , 2-Dich(oroethene
ug/L
50
50.00
100
2,2-DichLoropropane
ug/L
50
49.00
98.0
Chtoroform
ug/L
50
47.00
94.0
Bromochtoromethane
ug/L
50
48.00
96.0
1,1,1-TrichLoroethane
ug/L
50
47.00
94.0
1,1-DichLoropropene
ug/L
50
51.00
102
1,2-Dichtoroethane
uq/L
50
48.00
96.0
Carbon Tetrachloride
ug/1-
50
52.00
104
Benzene
ug/L
50
49.00
98.0
Trichtoroethene
uq/L
50
51.00
102
1,2-Dichloropropane
ug/L
50
55.00
110
Dibromomethane
ug/1-
50
55.00
110
gromodichLoromethane
ug/L
50
49.00
98.0
ToLuene
ug/L
50
51.00
102
1,1,2-TrichLoroethane
ug/L
50
52.00
104
1,3-DichLoropropane
ug/L
50
51.00
102
Dibromochloromethane
ug/L
50
50.00
100
Tetrachtoroethene
ug/L
50
53.00
106
1,2-Dibromoethane
ug/L
50
51.00
102
Chlorobenzene
ug/L
50
49.00
98.0
1,1,1,2-Tetrach(oroethane
ug/L
50
51.00
102
Ethytbenzene
ug/L
50
48.00
96.0
m&p-Xytene
uq/L
100
95�00
95.0
Styrene
ug/L
50
48.00
96.0
o-Xytene (1,2-Dimethylbenzene)
u9/1-
50
48.00
96.0
Bromofarm
ug/L
50
56.00
112
1,1,2,2-Tetrachloroethane
ug/L
50
57.00
114
1 sopropy I benzene (Cumene)
ug/L
50
4MO
96.0
1,2,3-TrichLoropropane
ug/L
50
52.00
104
Bromobenzene
ug/L
50
49.00
98.0
n-PropyLbenzene
ug/L
50
48.00
96.0
Laboratory Certification IDs Laboratory Certification IDS
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE:
9285743
Spike
LCS
Spike
Parameter
------------------------------
Units
----------
Conc.
-------
Result
% Rec
2-ChLoratoluene
ug/L
50
----------
46.00
-----
92.0
4-ChtorotoLuene
ug/L
50
48.00
96.0
1,3,5-Trimethylbenzene
ug/L
50
46.00
92.0
tert-ButyLbenzene
ug/L
50
48.00
96.0
1,2,4-Trimethytbenzene
ug/L
50
46.00
92.0
sec-ButyLbenzene
ug/L
50
46.00
92.0
1,3-DichLorobenzene
ug/L
50
48.00
96.0
p-isopropyttoLuene
ug/L
50
48.00
96.0
1,4-Dichtorobenzene
uq/L
50
49.00
98.0
1,2-DichLorobenzene
ug/L
50
48.00
96.0
n-Butytbenzene
ug/L
50
49.00
98.0
1,2-Dibromo-3-Chloropropane
ug/L
50
54.00
108
1,2,4-Trichtorobenzene
ug/L
50
52.00
104
NaphthaLene
ug/L
50
56.00
112
flexachLorobutacliene
ug/1-
50
46.00
92.0
1,2,3-TrichIcrobenzene
ug/L
50
52.00
104
Dilbromof luoromethane (S)
100
1,2-DichLoroethane-d4 (S)
99
Toluene-d8 (S)
105
4-BromofLuorobenzene (S)
107
DATE: 09/02/98
PAGE: 17
Pace Project Number: 921263
CLient Project ID: McDowel.l. LandfitL-93666
Footnotes
Laboratory Certification IDs Laboratory Certification Ds
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List
SC 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Jnc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
QUALITY CONTROL DATA DATE: 09/02/98
PACE: 18
McDowel. I County Landf i it Pace Project Number: 921263
10 East Court Street CHent Project ID: McDoweLt Landfitt-93666
Marion, NO 28752
Attn: Mr. Mike Gladden
QC Batch ID: 2174 OC Batch Method: EPA 8260
AnaLysis Method: EPA 8260 AnaLysis Description: CC/MS VOCs by 8260
Associated Pace Samples: 9282203 9282229
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
9285776 9285784
Matrix
Matrix
Spike
Spike
Spike
Spike
Sp. Dup.
Cup
Parameter
------------------------------
Units
----------
9282203
Conc.
ResuLt
% ReC
ResuLt
% Rec
RPD Footnotes
1,1-DichLaroethene
uq/L
----------
0
-------
50
----------
52.00
-----
104
----------
48.00
-----
96.0
----- ----------
8
Benzene
ug/L
0
50
53.00
106
51.00
102
4
TrichLoroethene
ug/L
0
50
55.00
110
51.00
102
8
ToLuene
ug/L
0
50
55.00
110
52.00
104
6
ChLorobenzene
ug/L
0
50
52.00
104
50.00
100
4
DibromofLuoromethane (S)
100
99
1,2-Dichloroethane-d4 (S)
102
99
ToLuene-d8 (S)
107
107
4-Bromof Luorobenzene (S)
110
108
LABORATORY CONTROL SAMPLE:
9285768
spike
LCS
Spike
Parameter
------------------------------
Units
Conc.
ResuLt
% Rec Footnotes
DichLorodiftuaromethane
----------
ug/L
-------
50
----------
38.46
----- ----------
76.9
Chtoromethane
ug/L
50
54.14
108
Vinyl. Chtoride
ug/L
50
50.39
101
Bromomethane
ug/L
50
54.59
109
Chloroethane
ug/L
50
58.08
116
Trichloroftuoromethane
ug/L
50
51.17
102
1,1-Dichtoroethene
ug/L
50
51.01
102
Methylene Chtoride
ug/L
50
49.50
99.0
trans- 1 , 2-D ich(orcethene
ug/L
50
52.27
105
1,1-DichLoroethane
ug/L
50
50.11
100
cis-1,2-DichLoroethene
ug/L
50
51.76
104
2,2-DichLoropropane
ug/L
50
46.96
93.9
Laboratory Certification IDs Laboratory Certification la
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN UST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Anal-ytocal Huntersville, NC 28078
Tel: [phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/02/98
PAGE: 19
Pace Project Number: 921263
CLient Project ID: McDoweL[ LandfiLL-93666
LABORATORY CONTROL SAMPLE: 9285768
Spike
LCS
Spike
Parameter
------------------------------
Units
------
Conc.
ResuLt
----------
% Rec Footnotes
Chloroform
---
ug/L
-------
50
48.96
----- ----------
97.9
Bromochloromethane
ug/L
50
45.96
91.9
1 1 , 1 -Trich toroethane
uq/L
50
48.32
96.6
1 1 -Di ch Loropropene
ug/L
50
52.89
106
1 2-D ich loroethane
ug/L
50
49.57
99.1
Carbon Tetrachloride
ug/L
50
52.99
106
Benzene
ug/L
50
52.03
104
Trichloroethene
ug/L
50
53.75
108
1, 2-D i ch Loropropane
ug/L
50
56.17
112
Dibromomethane
ug/L
50
56.63
113
Bromodich Loromethane
ug/L
50
51.24
102
ToLuene
uq/L
50
53.58
107
1, 1, 2-Trich Loroethane
ug/L
50
55.88
112
1,3-Dichloropropane
ug/L
50
52.96
106
Dibromochloromethane
ug/L
50
51.94
104
Tetrachloroethene
ug/L
50
54.23
108
1,2-Dibromoethane
ug/L
50
53.80
108
Chlorobenzene
ug/L
50
51.35
103
1, 1 , 1 2-Tetrach loroethane
ug/L
50
53.39
107
Ethy[loenzene
ug/L
50
49.99
100
m&p-XyLene
ug/L
100
97.69
97.7
Styrene
ug/L
50
51.34
103
o-Xylene ( 1 , 2-D imethyl. benzene)
U9/L
50
49.91
99.8
Bromoform
ug/L
50
58.71
117
1,1,2,2-Tetrachtoroethane
ug/L
50
58.18
116
1 sopropyt benzene (Cumene)
uq/L
50
48.20
96.4
1,2,3-TrichLoropropane
ug/L
50
54.10
108
Bromobenzene
ug/L
50
51�60
103
n-PropyLbenzene
ug/L
50
50.09
100
2-ChtorotoLuene
ug/L
50
49.17
98.3
4-ChLorotoLuene
ug/L
50
49.11
98.2
1 3,5 - Tr imethyt benzene
ug/L
50
47.80
95.6
tert-ButyLbenzene
ug/L
50
51.03
102
1 , 2,4 -Tr imethyl benzene
ug/L
50
48.50
97.0
sec-ButyLbenzene
ug/L
50
47.93
95.9
1,3-Dichtorobenzene
ug/L
50
49.71
99.4
p-Isopropyttoluene
ug/L
50
50.55
101
1,4-Dichtorobenzene
ug/L
50
51.05
102
1,2-DichLorobenzene
uq/L
50
50.45
101
n-Butylbenzene
ug/L
50
51.63
103
1,2-Dibromo-3-Chloropropane
ug/L
50
57.63
115
Laboratory Certification Ds Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TIN LIST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytocal Huntersville, NO 28078
Tel: [phone]
Fax: [phone]
QUALITY CONTROL DATA DATE: 09/02198
PAGE: 20
Pace Project Number: 921263
Client Project To: McDowell LandfiLL-93666
LABORATORY CONTROL SAMPLE: 9285768
Spike
LCS
Spike
Parameter
------------------------------
Units
----------
Conc.
Result
% Rec Footnotes
1 , 2, 4- Tri ch I orobenzene
ug/L
-------
50
----------
54.32
----- ----------
109
Naphthalene
ug/L
50
59.31
119
Hexachtorobutadiene
ug/L
50
49.75
99.5
1 , 2,3-Tri ch I. orobenzene
ug/L
50
54.64
109
Dibromof Luoromethane (S)
100
1,2-Dichtoroethane-d4 (S)
101
ToLuene-d8 (S)
107
4-Bromof Luorobenzene (S)
109
Laboratory Certification lDs Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN LIST List
Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Anallytocal Huntersville, NC 28078
Tel: [phone]
Fax:[phone]
DATE: 09/02/98
PAGE: 21
Pace Project Number: 921263
Client Project ID: McDowell LandfitL-93666
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA quideLines unrounded concentrations are displayed and have been used to catcuLate % Rec and RPD vaLues
ND
Not Detected
NO
Not CatculabLe
PRL
Pace Reporting Limit
RPD
Relative Percent Difference
(S)
Surrogate
Laboratory Cerfification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification IDS
KY Drinking Water 90090
TN LIST List
VA Drinking Water 213