5601_ROSCANS_1997

Fae/Perm/Co ID # Date ,/j Doc ID#
a ✓ �y l Il DIN
STATE OF NORTH CAROLINA
DEPARTMENT OF T ANSPORTATION
)Am Es B. HUNT JR. DIVISION OF HIGHWAYS GARIAND B. GARRETT JR.
GOVERNOR SECRETARY
January 2, 1997
Mr. Mark Poindexter
Division of Solid Waste
P. 0. Box 27687
Raleigh, NC 27611-0692
RE: McDowell County Landfill
Monitor Well Permit
Dear Mr. Poindexter:
Enclosed a request to install monitor wells at the McDowell
County Landfill. Two of the wells are on county property and
the other 2 are on Department of Transportation property.
The DOT and the McDowell County have an agreement that DOT
will initially pay for the installation of the wells. If the
site investigation determines that the landfill is the source
of. contamination, the County will reimburse DOT and continue
the investigation. This negotiation was the cause of the
delay.
Four wells are to be installed to a depth of SO feet in the
areas discussed on site during the meeting back in September
24, 1996. In the event that the drill rig cannot get to the
proposed location, an alternate location will be selected as
close as possible. These welts will be 2-inch diameter,
Schedule 40, PVC with flush -mounted manways. Installation
should be completed in three weeks.
Please process this request at your earliest convenience. If
you have questions, please call me at 733-2220.
Sincerely,
I=
Eric Motzno, L.G.
Hydrogeologist
encl.
Rol

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*SVCALE 11 SITE LOCATION MAP
0' 1,000, 2.000, 4,000. NCDOT MAINTENANCE YARD
N,c.", MARION, NORTH CAROLINA
2'000' QUADRANGLE LpG1TI0N FRONT ROYAL
ENVIRONMENTAL SERVICES, M.
REF: USCS MARION EAV, NC QUADRANGLE (1982) PROJ. # 0012--96-059 F"1 G U R E 1

p E;dsh►j IJell
. Ppvpnxd We1rs 1
1,5001 RADIUS
N
WOOVELL COUNTY
(175.91A)
6242
McDowell
County
McDowell ► 1
s County—
JL 10 East Court Street • \�� NJ
Marion, North Carolina 28752 \
DOT/\ \ ---
/ ,rift 1.011.Y ` \
/ i KOX eow \
14LI , \
4779 \ McDowell
/ \ County
City
of
Marion _ ;
Post Office Drawer 700
Marion, North Carolina 28752
INDEX ON 1720.01
INDEXED ON 1720.0
McDowell
McDowell County
Agricultural
Center
�1 /7
c14.474,
-- 63CO
r OI
SURROUNDING PROPERTY FIGURE 3
OWNERS MAP FRONT ROYAL SCALE: 1"= 4001
NCDOT MAINTENANCE YARD ENVrRONWENTAL SERVICES, INC.
MARION, NORTH CAROLINA PROJ. 0012-96-059

Jt_ CiEF T OF T KiiN:_ . itL _�1`�?�, 11'� _;rF, U J 1 !"1 ID IiU r ,U^
t11VZXlll L-fll'"A-"IAL
ENTIRc 1Tv EWAL MANAGEMENT COMMISSION
DEPAYCMI ENT OF ENVI120NMENr, HEAL`Ii-1, & NATURAL RESOURCZ
CATION FOR. PERMIT TQ OONS"MUCT A MONTI OR NG WEIL SYSTEM
Date: �` 30 , 19�r County /f4i •D'Pwe I1
In accordance Aith the provisions of Article 7, Chapter 87, General Statutes of North Carolina and req.,iations pursuant
thereto, application is hereby made for a permit to monitoring wells.
1. Name of Appl'Icant %dr / _ (Telephone: 91f. 733 RRO d )
Applicant's Mailing Address:
2. Name of Properly Owner (if different from applicant)
Ownees Mailing Address'
rO
3. Contact Person:- �rl 4 (Telephone: Q 733 ZRAO }
a. Location of Property:--HWi ao�� 50v�[
5, Beason for Monitoring Well(s):
(ex: norxiischarga pewit requirements, s d aorttarm on rn+ironmantal as�rssrna�n, etc-)
6. Type, of facility or site, for which the monitoring well(s) Is needed: 44,n4tT �
(ex: norldi=harge facility, waste dsporsl site, landriil, undergrourd storage tank, ate.)
7. Type of contamination beirg monitored (if applicable): --
(ex: rxmfents, organics, heavy metafe, etc.)
8, Are any existing recovery welts associated with the monitoring wall($)?___yt] -- - if yes, how many?
Recovery Well Construction Permit No.
S. Distance to a known waste or pollution source: aP feet
10. Are arty water supply wells located less than 500 feet from the proposed monitoring wells?.— —
It yes, give distanCe:—._ feet
1 1- Well Driller: b�
12. Registration #:
13, Drillers Address:
R P D MONITORING WFIJ CONST T10N RMATI N
1. Total Number of Wells to be Constructed —._.. i (A) Numt>lr to be completed in bedrock?
(l3) Number to to completed in unconsolidated material? — Q
2, Estimated depth Of wetl(s): ,Z Q— feet
3. Gravel or sand pack interval (if appropriate)
From -30 - feet To SO feet
4. Type of casing used: Pe4L
(ex: PVC, stainless steel, galvanized steel, eta.)
5. Diameter of casing: X- inches
—
FOR 0-M SSE Y
.._ PERMfTTED
ACTtVITY
U.S,T, LEAK
DETECTION
GROUNDWATER QUALITY STANDARDS
VCLATIONS
SUSPECTED FROM UNPERMITTED
ACTIVITIES
_ NOTICE OF
NON-COMPLIANCE AT
UNPERMII"TED FACILITIES
PERMIT NO. ISSUED. 19.�
INCIDENT #
GW.22M (7,'g1) ,ram hn,inr� nn navAr�*L

Nt: DEFT . OF TRA11 T EL 919?33�1192 Sep 30' 6 115 26 No ,010 F .0
6. Th; ss of casing: Sf-h YO -fe+ies
7.. How will the well(s) be secured? 104t 1 Q + Z-re.,,!d teg
8. Estimated beginning construction date: f - Tan oil _ . f7
9. Estimated completion date: /� 1r�r`-�
ADDITIQNAL INFORMATION
1. ATTACH A SITE MAP SHOWING THE LOCATIONS OF THE FCLLOWING:
1.
1 - PROPOSED MONITORING WELL(S)
2 - ALL E=XISTING MONITORING AND RECOVERY WELLS OR 17EST BORINGS WFTH THE PROPER?Y
BOUNDARY
3 • ALL WATER SUPPLY WELLS WITHIN 500 FEET OF THE WASTE SOURCES
4 • AT LEAST TVVO REFERENCE POINTS (NUMBERED ROADS, INTE=RSECT0NS, STREAMS, ETC.)
2. PROVIDE A WELL CONSTRUCTION DIAGRAM OF EACH WELL SHOWING DIAMETER, ESTIMATED DEPTH, SCREEN
INTERVALS, SAND/GRAVEL PACKS, TYPE OF CASING MATERIAL, CASING WALL THICKNESS, WELL HEAD COMPLE-
TION DETAILS, ETC.)
The Applicant hereby agrees the proposed well(s) will be Constructed in accordance with
approved specifications and conditions of the Well Construction Permit as regulated under the Well
Construction Standards (Me 15A North Carolina Administrative Code, Subchapter 20) and accepts
full responsibility for compliance with these rules,
Signature of Applicant or Agent
440 Sea/a j, f
Title (if applicable)) "
If the property is owned by someone other than the applicant, the property owner hereby
consents to allow the applicant to construct monitoring wells as outlined in this application and that
it shall be the responsibility of the applicant to ensure that these monitoring wells confcrm to the We!I
nstructio Standards (True 15A North Carolina Administrative Code, Subchapter 2C).
Sionature of Property Owner (if different m applicant}

STATE OF NORTH CAROLINA
DEPARTMENT OF TRANSPORTATION
J",Es B. HUNT j R.
GoviRNOR
Mr. Chuck Abernathy
10 East Court Street
Marion, NC 28752
DIVISION OF HIGHWAYS
Route 1, Box 169C
Marion, NC 28752
October 22, 1996
Subject: Monitoring Wells to be installed
Property and the McDowell County
to Detect Suspected Contamination
Dear Chuck,
GARiAN o B. GARRETT J R.
SECRETARY
on the DOT
Landfill Property
On September 24, 1996 a meeting was held to discuss the
possibility of placing monitoring wells to determine if
suspected contamination as detected in a monitoring well
located behind the McDowell County School Bus Garage Parking
area on Landfill property is being contaminated from a DOT
source. Present at that meeting were Mr. Jim Parker, Eric
Motzno, Hydro Geologist with the NCDOT, Alan Silvers,
McDowell County Landfill, Al Hetzall and Mr. Poindexter of
DEHNR.
It was determined from this meeting that 4 monitoring
wells would be installed; 2 on DOT property and 2 on the
Landfill property. Before we begin these installations, we
need you to sign an application for a permit to construct a
monitoring well system on the Landfill property which is
attached. Please sign as the property owner on the second
sheet and return this to me.
In my discussions with the Hydro Geologist, it has been
determined that the installation of the well and monitoring
will cost about $3,000 to $4,000 per well. This would cost a
total of $12,000 to $16,000. It should be understood that
should it be determined conclusively that the contamination
source is other than DOT, we would be left with no recourse
but to be reimbursed by the County for these installations.
I trust you understand our position in this regard; as the
potential clean up for this could be very expensive.
247%

Mr. Chuck Abernathy
Page 2
October 22, 1996
Please respond to me in writing if you agree to this and
if you have any questions, as usual please feel free to give
me a call.
Cordially,
Stephen A. (Tony) Moore, P.E.
District Engineer
Dist. 1, Div. 13
SAM:meb
Attachment
cc: Mr. W. D. Smart, P.E.
Mr. Eric Motzno
Mr. Al Hetzall

LA
Front Royal
Environmental Services, Inc.
February 13, 1997
Mr. Eric Motzno
North Carolina Department of Transportation
4809 Beryl Drive
Raleigh, North Carolina 27606
Re: Monitor Well Installation
NCDOT Marion Maintenance Yard
McDowell County Landfill
Front Royal Project No. 0440-96-231
Dear Mr. Motzno:
2200 Gateway Blvd. • Suite 205 • Momss'ille. NC 27560
[phone] • Fax [phone]
Front Royal Environmental Services, Inc. (Front Royal) has completed the installation of four
monitor wells at the NCDOT Marion maintenance yard. Two wells, MW-A and MW-B were
lace on the western border of NCDOT property adjacent to property owned by McDowell
County that is currently being use -as a landflt, This landfill has been operational
approximately 60 years• MW-C was placed on property owned by McDowell County and
cygently used as a school bus garageftnd MW-D was placed in a closed cell of the landfill,
upgradi monitor wells MW-A andTvlW-B. 1 ��z N7 job
Monitor wells MW-A and MW-B were installed by an ATV auger drill rig in weathered soil
from Gneiss bedrock. Monitor wells MW-C and MW-D were installed by a truck -mounted air
rotary drill rig into the bedrock. MW-D was installed through 4 inch PVC casing that was placed
through twenty feet of buried trash and was sealed into the native, partially weathered bedrock at
an approximate depth of 24 feet. This was done to prevent any leachate from entering the well
j� analus and contaminating the well.
c JEach well was developed with a Grundfos submersible pump until a clear water sample was
available. Samples were collected in laboratory supplied bottles, placed on ice and delivered
under chain -of -custody to Tritest, Inc. in Raleigh, North Carolina. The samples were analyzed
by EPA Methods 8240 and 8270.
Enclosed are the completed GW-1 Well Construction Records for each monitor well. Please call
us if you have any questions or comments at [phone].

Sincerely,
FRONT
/ROYAL ENVIRONMENTAL SERVICES, INC.
David E. Meyer
Senior Soil Scientist
Darrell Janezic
Construction Manager
cc: file

NORTH CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT - GROUNDWATER SECTION FOR OFFICE USE ONLY
_ P.O. BOX 27687 - RALEIGH, N.C. 27611, PHONE [phone] Quad. No. Serial No.
Lat. Long. Pc
Minor Basin
Basin Code
Header Ent. GW-1 Ent.
WELL CONSTRUCTION RECORD MW-A
DRILLING CONTRACTOR FRESI STATE WELL CONSTRUCTION
DRILLER REGISTRATION NUMBER 1597 PERMIT NUMBER:
WELL LOCATION:(Show sketch of the location below)
Nearest Town: Marion. North Carolina County: McDowell
NCDOT Maintenance Yard Depth DRILLING LOG
(Road, Community, or Subdivision and Lot No.) From To Formation Description
2. OWNER North Carolina Deoartment of Transportation 0.0' - 2.0'
ADDRESS 4809 Beryl Drive 2.0' - D.U.
Raleigh NC 27606 5.0' - 12.5'
12.5 - 20.0'
City or Town State Zip Code 20.0 - 32.5-
32.5 - 40.0-
3. DATE DRILLED 01-28-97 USE OF WELL Monitoring 40.0 - 45.0-
4. TOTAL DEPTH 46.5' CUTTINGS COLLECTED _Yes _(No
5. DOES WELL REPLACE EXISTING WELL? _Yes 2LNo
6. STATIC WATER LEVEL: 41.37FT. _above TOP OF CASING
below
TOP OF CASING IS +2.5 FT. above LAND SURFACE
7. YIELD (gpm): 2.0 METHOD OF TEST centrifical
8. WATER ZONES (depth): -41.0 to -45.0'
9. CHLORINATION: Type Amount
10.CASING: Wall Thickness
or
Depth Diameter Weight/Ft. Material
From +2.0 To-34.0 Ft. " 0,154-1 PVC
From To_Ft.
From_To_Ft.
11.GROUT:
Depth Material Method
From 0.0 To-30.OFt. cement poured
From -30.OTo -33.OFt. bentonite pellets
12.SCREEN
Depth- Diameter Slot Size Material
From-34.OTo -44.OFt. " in. 0,010 in.PVC
From_To_Ft. in. in.
From_To_Ft. in. in.
13.GRAVEL PACK:
Depth Size Material
From -33.OTo -44.OFt. torpedo sand
14
If additionaL space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least
two State Roads or other map reference points
I DO HEREBY CERTI HAT THIS ELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C. WELL CONSTRUCTION STANDARDS,
AND THAT A COPY �BIEC-0f{I HAS BEEN PROVIDED TO THE WELL OWNER.
� IL 2 I
OF CONTRACTOR OR AGENT
GW-1 Revised 11/84 Submit original to Division of Environmental Management and copy to well owner.l

NORTH CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT - GROUNDWATER SECTION FOR OFFICE USE ONLY
P.O. BOX 27687 - RALEIGH, N.C. 27611, .PHONE [phone] Quad. No. Serial No.
Lat. Long. Pc
Minor Basin
Basin Code
Header Ent. GW-1 Ent. _
WELL CONSTRUCTION RECORD MW-B
DRILLING CONTRACTOR FRE51 STATE WELL CONSTRUCTION
DRILLER REGISTRATION NUMBER 1597 PERMIT NUMBER:
1. WELL LOCATION:(Show sketch of the location below)
Nearest Town: Marion, North Carolina County: McDowell
NCOOT Maintenance Yard Depth DRILLING LOG
(Road, Comminity, or Subdivision and Lot No.) From To Formation Description
2. OWNER North Carolina Department of Transportation 0.01 - 15.0- Light reddish brown clayey fine sandy silt fill (ML)
ADDRESS 4809 Beryl Drive 15.0 - 20.0- Reddish brown clayey micaceous silt (ML)
Raleigh NC 27606 20.0 - 25.O1 Brown clayey fine sandy micaceous sandy silt (ML)
25.0 - 35.0- Rod clayey fine sandy silt (M0
City or Town State Zip Code 35.0 - 45.0- Light brownish gray clayey fine sandy silt (ML)
3. DATE DRILLED 01.28-97 USE OF WELL Monitoring
4. TOTAL DEPTH 46.0- CUTTINGS COLLECTED _Yes _�(No
5. DOES WELL REPLACE EXISTING WELL? _Yes (-No
6. STATIC WATER LEVEL: 3J UFT. _above TOP OF CASING
below
TOP OF CASING IS +2.0 FT. above LAND SURFACE
7. YIELD (gpm): 2.0 METHOD OF TEST centrifical
8. WATER ZONES (depth): -35.0 to -45.0'
9. CHLORINATION: Type Amount
10.CASING:
Depth Diameter
From +2.0 To-34.0 Ft. 211
From_ToFt.
From_To_Ft.
11.GROUT:
Wall Thickness
or If additional space is needed use back of form
Weight/Ft. Material
LOCATION SKETCH
0.150 PVC (Show direction and distance from at least
two State Roads or other map reference points
Depth Material Method
From 0.0 To •30.OFt. cement poured
From -30.0To -33.OFt. bentonite oell ets
12.SCREEN
Depth Diameter Slot Size Material
From -34.OTo •44.OFt. 21, in. 0.010 in. PVC
From To_Ft. in. in.
From_To_Ft. in. in.
13.GRAVEL PACK:
Depth Size Material
From -33.OTo -44.OFt. torpedo sand
14.REMARKS
I DO HEREBY CERTIFY THA THIS WE IL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C. WELL CONSTRUCTION STANDARDS,
AND THAT A COPY OF CORP H S BEEN PROVIDED TO THE WELL OWNER. .
SIGNATURE OF CONTRACTOROR AGENT
Z
DATE
GW-1 Revised 11184 Submit original to Division of Environmental Management and copy to well owner.t

NORTH CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT - GROUNDWATER SECTION FOR OFFICE USE ONLY
P.O. BOX 27687 - RALEIGH, N.C. 27611, PHONE [phone] Quad. No. Serial No.
Let. Long. Pc
Minor Basin
Basin Code
Header Ent. GW-1 Ent.
WELL CONSTRUCTION RECORD MW-C
DRILLING CONTRACTOR FRFSI STATE WELL CONSTRUCTION
DRILLER REGISTRATION NUMBER 1597 - PERMIT NUMBER:
1. WELL LOCATION:(Show sketch of the location below)
Nearest Town: Marion. North Carolina County: McDowe
NcDcT Maintenenpe Yard Depth
(Road, Conmunity, or Subdivision and Lot No.) From To
Formation Description
2. OWNER North Carolina Department of Transportation 0.01 - 20.01 Greenish gray sandy sitt (ML)
ADDRESS 4809 Beryl Drive — 20.0 - 30.01 1 iQht reddish brown Bandy silt (ML)
Raleigh NC 2760E' 30.0 - 44.0- -Greenish gray sandy sitt wl gravel (VL)
City or Town State Zip Code
3. DATE DRILLED 02-11-97 USE OF WELL Monitoring
4. TOTAL DEPTH 65.01 CUTTINGS COLLECTED _Yes _lNo
5. DOES WELL REPLACE EXISTING WELL? _Yes A -No
6. STATIC WATER LEVEL: 49.64FT. _above TOP OF CASING
_jLpelow
TOP OF CASING IS +2.0 FT. above LAND SURFACE
7. YIELD (gpm): +5.0 METHOD OF TEST submersible
8. WATER ZONES (depth): -50n to -63.01
9. CHLORINATION: Type Amount
1O.CASING: Wall Thickness
or
Depth Diameter Weight/Ft.
If additional space is needed use back of form
Material
From +2.0 To-53.0 Ft. '. 0,15411 PVC —
From To,_,Ft.
From_To_Ft.
11. GROUT:
Depth Material Method
From O.0 To -47.OFt. cement poured
From-47.OTo -49.OFt. bentonite pellets
12.SCREEN
Depth Diameter Slot Size Material
From -53.OTo-63.OFt. min. 0.010 in.PVC_
From_To_Ft. in. in.
From_To_Ft. in. in.
13.GRAVEL PACK:
Depth Size Material
From-49.OTo -63.OFt. torpedo sand
LOCATION SKETCH
(Show direction and distance from at least
two State Roads or other map reference points
14.REMARKS:
I DO HEREBY CERTIFY AT THIS ELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C. WELL CONSTRUCTION STANDARDS,
AND THAT A COPY S RE OR HAS BEEN PROVIDED TO THE NELL OWNER.
Z IIN 197
S IGNATUR OF CON ACTOR OR AGENT DATE
GW-1 Revised 11/84 Submit original to Division of Environmental Management and copy to well owner.l

NORTH CAROLINA DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT - GROUNDWATER SECTION FOR OFFICE USE ONLY
P.O. BOX 27687 - RALEIGH, N.C. 27611, PHONE [phone] Quad. No. Serial No.
Let. Long. Pc
Minor Basin
Basin Code
Header Ent. GW-1 Ent.
WELL CONSTRUCTION RECORD MW-D
DRILLING CONTRACTOR FRPSI _ STATE WELL CONSTRUCTION
DRILLER REGISTRATION NUMBER 1597 PERMIT NUMBER:
1. WELL LOCATION:(Show sketch of the location below)
Nearest Town: Marion. North Carolina County: n,,M,cDowe
NcDOT Maintenance Yard i=
(Road, Community, or Subdivision and Lot No.) From To
2. OWNER North Carolina Department of Transportation 0.0- - 20.01
ADDRESS 4809 Beryl Drive 20.0 - 35.0'
Raleigh NC 27606 35.0 - 37.01
37.0 - 40.0-
City or Town State Zip Code 40.0 - 53.5'
53.5 - 81.0�
3. DATE DRILLED 02-12-97 USE OF WELL Monitoring
4. TOTAL DEPTH 84.0- CUTTINGS COLLECTED _Yes _(No
5. DOES WELL REPLACE EXISTING WELL? _Yes ILNO
6. STATIC WATER LEVEL: 71.OSFT. _above TOP OF CASING
_jLbelow
TOP OF CASING IS +3.0 FT. above LAND SURFACE
7. YIELD (gpm): +5.0 METHOD OF TEST submersible
B. WATER ZONES (depth): -69.0 to -81.0'
9. CHLORINATION- Type Amount_
10.CASING: Wall Thickness
or
Depth Diameter Weight/Ft.
From +3.0 To-66.0 Ft. " 0.154--
From ToFt.
From_To_Ft.
11.GROUT:
Depth Material Method
From 0.0 To -57.OFt. cement poured
From jZ&To -59.OFt. bentonite pellets
12.SCREEN
Depth Diameter Slot Size Material
From -66.OTa-81.OFt. " in. 0.010 in., PVC
From_ToFt. in. in.
From., -TO -Ft. in. in.
13.GRAVEL PACK:
Depth Size Material
From -59.OTo-81.OFt. torpedo sand
Formation Description
- - -'-W51[Cx1i1U1ffM4R" M
If additional space is needed use back of form
Material
LOCATION SKETCH
PVC (Show direction and distance from at least
two State Roads or other map reference points
I DO HEREBY CERTIFY THAT THIS LL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C. WELL CONSTRUCTION STANDARDS,
AND THAT A COPY OF"FN1(S,RECQ§DII AS BEEN PROVIDED TO THE WELL OWNER.
21�
SIGNATURE OF CONTRACTOR OR AGENT
GW-1 Revised 11/84 Submit original to Division of Environmental Management and copy to Well ouner.l

TRITEST, INC.
3909 Beryl Road
Raleigh, NC 27607
Telephone: [phone]
Fax: [phone]
NC/WW Cert.#: 067
L a b o r a t Cry Report
--- Prepared for --- Page 1 of 7
Eric Motzno Report Date: 2/18/97
NCDOT Beryl Rd. Office Date Received: 1/31/97
4809 Beryl Rd.
Raleigh, NC 27606 Work Order #: 9701-31002
Cust. Code: NC3532
Project ID: DOT/BERYL RD. Cust. P.O.#:879048
Project Info: MONITORING WELLS/MARION PROJ.# 5.8711215
No.
Sample
ID
Date Sampled
Time Sampled
Matrix
Condition
1
MW-A /
MARION
1/28/97
15:00
GW
4±2'0C
Test Performed
Method
Date
Results Tech Analyzed Qual
Volatiles in Water by GC/MS
EPA
8240
ZW
2/10/97
Acetone
EPA
8240
<50
ug/L
ZW
2/10/97
Acrolein
EPA
8240
<50
ug/L
ZW
2/10/97
Acrylonitrile
EPA
8240
<50
ug/L
ZW
2/10/97
Benzene
EPA
8240
9.4
ug/L
ZW
2/10/97
Bromodichlorcmethane
EPA
8240
<5
ug/L
ZW
2/10/97
Bromoform
EPA
8240
<5
ug/L
ZW
2/10/97
Bromomethane
EPA
8240
<10
ug/L
ZW
2/10/97
Carbon tetrachloride
EPA
8240
<5
ug/L
ZW
2/10/97
Chlorobenzene
EPA
8240
<5
ug/L
ZW
2/10/97
Chloroethane N5
EPA
8240
22.1
ug/L
ZW
2/10/97
2-Chloroethylvinyl ether
EPA
8240
<10
ug/L
ZW
2/10/97
Chloroform
EPA
8240
<5
ug/L
ZW
2/10/97
Chloromethane
EPA.
8240
<10
ug/L
ZW
2/10/97
Dibromochloromethane
EPA
8240
<5
ug/L
ZW
2/10/97
1,2-Dibromo-3-chloropropane
EPA
8240
<25
ug/L
ZW
2/10/97
1,2-Dibromoethane
EPA
8240
<5
ug/L
ZW
2/10/97
Dibromomethane
EPA
8240
<10
ug/L
ZW
2/10/97
Dichlorodifluoromethane
EPA
8240
<5
ug/L
ZW
2/10/97
1,1-Dichloroethane %00
EPA
8240
55.8
ug/L
ZW
2/10/97
1,2-Dichloroethane
EPA
8240
<5
ug/L
ZW
2/10/97
1,1-Dichloroethene
EPA
8240
<5
ug/L
ZW
2/10/97
trans-1,2-Dichloroethene jD
EPA
8240
43.6
ug/L
ZW
2/10/97
1,2-Dichloropropane -
EPA
8240
<5
ug/L
ZW
2/10/97
cis-1,3-Dichloropropene
EPA
8240
<5
ug/L
ZW
2/10/97
trans-1,3-Dichloropropene
EPA
8240
<5
ug/L
ZW
2/10/97
Ethylbenzene
EPA
8240
<5
ug/L
ZW
2/10/97
--- Continued on Next Page ----

TRITEST, INC.
L a b o r a t o r y Report
NCDOT Beryl Rd. Office Report Date
Project No. DOT/BERYL RD. Work Order No
No. Sample ID
1 MW-A / MARION
Test Performed
Method
Page 2 of 7
2/18/97
9701-31002
Date
Results Tech Analyzed Qual
2-Hexanone
EPA
8240
<50
ug/L
ZW
2/10/97
Methylene chloride
EPA
8240
451
ug/L
ZW
2/12/97
Methyl ethyl ketone (MEK)
EPA
8240
<50
ug/L
ZW
2/10/97
MIBK (4-Methyl-2-pentanone)
EPA
8240
<50
ug/L
ZW
2/10/97
Styrene
EPA
8240
<5
ug/L
ZW
2/10/97
1,1,1,2-Tetrachloroethane
EPA
8240
<5
ug/L
ZW
2/10/97
1,1,2,2-Tetrachloroethane
EPA
8240
<5
ug/L
ZW
2/10/97
Tetrachloroethene
EPA
8240
<5
ug/L
ZW
2/10/97
Toluene
EPA
8240
<5
ug/L
ZW
2/10/97
1,1,1-Trichloroethane
EPA
8240
12.7
ug/L
ZW
2/10/97
1,1,2-Trichloroethane
EPA
8240
<5
ug/L
ZW
2/10/97
Trichloroethene
EPA
8240
<5
ug/L
ZW
2/10/97
Trichlorofluoromethane
EPA
8240
<5
ug/L
ZW
2/10/97
1,2,3-Trichloropropane
EPA
8240
<15
ug/L
ZW
2/10/97
Vinyl acetate
EPA
8240
<50
ug/L
ZW
2/10/97
Vinyl chloride
EPA
8240
<10
ug/L
ZW
2/10/97
o-Xylene
EPA
8240
<5
ug/L
ZW
2/10/97
m- & p-Xylene
EPA
8240
5.7
ug/L
ZW
2/10/97
8270 (A&B/N), Waters
EPA
8270B
SRB
2/06/97
Acenaphthene
EPA
8270B
<10
ug/L
SRB
2/06/97
Acenaphthylene
EPA
8270B
<10
ug/L
SRB
2/06/97
Acetophenone
EPA
8270B
<10
ug/L
SRB
2/06/97
2-Acetylaminofluorene
EPA
8270B
<20
ug/L
SRB
2/06/97
4-Aminobiphenyl
EPA
8270B
<20
ug/L
SRB
2/06/97
Aniline
EPA
8270B
<10
ug/L
SRB
2/06/97
Anthracene
EPA
8270B
<10
ug/L
SRB
2/06/97
Benzo(a)anthracene
EPA
8270B
<10
ug/L
SRB
2/06/97
Benzo(b)fluoranthene
EPA
8270B
<10
ug/L
SRB
2/06/97
Benzo(k)fluoranthene
EPA
8270B
<10
ug/L
SRB
2/06/97
Benzo(a)pyrene
EPA
8270B
<10
ug/L
SRB
2/06/97
Benzo(g,h,i)perylene
EPA
8270D
<10
ug/L
SRB
2/06/97
Benzoic acid
EPA
8270B
<50
ug/L
SRB
2/06/97
Benzyl alcohol
EPA
8270B
<10
ug/L
SRB
2/06/97
Benzyl butyl phthalate
EPA
8270E
<10
ug/L
SRB
2/06/97
Bis(2-chloroethyl)ether
EPA
82702
<10
ug/L
SRB
2/06/97
Bis(2-chloroethoxy)methane
EPA
8270B
<10
ug/L
SRB
2/06/97
Bis(2-chloroisopropyl)ether
EPA
8270B
<10
ug/L
SRB
2/06/97
Bis(2-ethylhexyl)phthalate
EPA
8270B
<10
ug/L
SRB
2/06/97
4-Bromophenyl phenyl ether
EPA
8270E
<10
ug/L
SRB
2/06/97
4-Chloroaniline
EPA
8270E
<20
ug/L
SRB
2/06/97
- -- Continued on Next Page ----

TRITEST, INC.
L a b o r a t o r y R e p o r t
NCDOT Beryl Rd. Office Report Date
Project No. DOT/BERYL RD. Work Order No
No. Sample ID
1 MW-A / MARION
Test Performed
Method
Page 3 of 7
2/18/97
9701-31002
Date
Results Tech Analyzed Qual
2-Chloronaphthalene
EPA
8270B
<10
ug/L
SRB
2/06/97
4-Chloro-3-methylphenol
EPA
8270E
<10
ug/L
SRB
2/06/97
2-Chlorophenol
EPA
8270B
<10
ug/L
SRB
2/06/97
4-Chlorophenyl phenyl ether
EPA
8270D
<10
ug/L
SRB
2/06/97
Chrysene
EPA
8270B
<10
ug/L
SRB
2/06/97
Dibenzo(a,h)anthracene
EPA
8270B
<10
ug/L
SRB
2/06/97
Dibenzofuran
EPA
8270B
<10
ug/L
SRB
2/06/97
Di-n-butyl phthalate
EPA
8270D
<10
ug/L
SRB
2/06/97
3,31-Dichlorobenzidine
EPA
8270B
<20
ug/L
SRB
2/06/97
1,2-Dichlorobenzene
EPA
8270D
<10
ug/L
SRB
2/06/97
1,3-Dichlorobenzene
EPA
8270B
<10
ug/L
SRB
2/06/97
1,4-Dichlorobenzene
EPA
8270B
<10
ug/L
SRB
2/06/97
2,4-Dichlorophenol
EPA
8270B
<10
ug/L
SRB
2/06/97
Diethyl phthalate
EPA
8270B
<10
ug/L
SRB
2/06/97
2,4-Dimethylphenol
EPA
8270E
<10
ug/L
SRB
2/06/97
Dimethyl phthalate
EPA
8270B
<10
ug/L
SRB
2/06/97
2,4-Dinitrophenol
EPA
8270B
<50
ug/L
SRB
2/06/97
2,4-Dinitrotoluene
EPA
8270B
<10
ug/L
SRB
2/06/97
2,6-Dinitrotoluene
EPA
8270B
<10
ug/L
SRB
2/06/97
Di-n-octyl phthalate
EPA
8270B
<10
ug/L
SRB
2/06/97
Fluoranthene
EPA
8270B
<10
ug/L
SRB
2/06/97
Fluorene
EPA
8270E
<10
ug/L
SRB
2/06/97
Hexachlorobenzene
EPA
8270B
<10
ug/L
SRB
2/06/97
Hexachlorobutadiene
EPA
8270E
<10
ug/L
SRB
2/06/97
Hexachlorocyclopentadiene
EPA
8270B
<10
ug/L
SRB
2/06/97
Hexachloroethane
EPA
8270B
<10
ug/L
SRB
2/06/97
Indeno(1,2,3-c,dipyrene
EPA
8270B
<10
ug/L
SRB
2/06/97
Isophorone
EPA
8270B
<10
ug/L
SRB
2/06/97
2-Methyl-4,6-dinitrophenol
EPA
8270B
<50
ug/L
SRB
2/06/97
1-Methylnaphthalene
EPA
8270B
<10
ug/L
SRB
2/06/97
2-Methylnaphthalene
EPA
8270B
<10
ug/L
SRB
2/06/97
2-Methylphenol
EPA
8270B
<10
ug/L
SRB
2/06/97
3- & 4-Methylphenol
EPA
8270E
<20
ug/L
SRB
2/06/97
Naphthalene
EPA
8270B
<10
ug/L
SRB
2/06/97
2-Nitroaniline
EPA
8270B
<10
ug/L
SRB
2/06/97
3-Nitroaniline
EPA
8270E
<20
ug/L
SRB
2/06/97
4-Nitroaniline
EPA
82703
<20
ug/L
SRB
2/06/97
Nitrobenzene
EPA
82703
<10
ug/L
SRB
2/06/97
2-Nitrophenol
EPA
8270D
<10
ug/L
SRB
2/06/97
4-Nitrophenol
EPA
8270B
<10
ug/L
SRB
2/06/97
---- Continued on Next Page ----

TRITEST, INC.
Page 4 of 7
L a b o rat cry Report
NCDOT Beryl Rd. Office
Project No. DOT/BERYL RD.
No. Sample ID
1 MW-A / MARION
Test Performed
Method
Report Date
Work Order No
Results Tech
2/18/97
9701-31002
Date
Analyzed Quay
N-Nitrosodimethylamine
EPA
8270B
<10
ug/L
SRB
2/06/97
- N-Nitrosodiphenylamine
EPA
8270B
<20
ug/L
SRB
2/06/97
N-Nitrosodi-n-propylamine
EPA
8270B
<20
ug/L
SRB
2/06/97
Pentachlorophenol
EPA
8270B
<30
ug/L
SRB
2/06/97
Phenanthrene
EPA
8270E
<10
ug/L
SRB
2/06/97
Phenol
EPA
8270B
<10
ug/L
SRB
2/06/97
Pyrene
EPA
8270E
<10
ug/L
SRB
2/06/97
Pyridine
EPA
8270B
<10
ug/L
SRB
2/06/97
1, 1,2,4-Trichlorobenzene
EPA
8270B
<20
ug/L
SRB
2/06/97
2,4,5-Trichlorophenol
EPA
8270E
<20
ug/L
SRB
2/06/97
2,4,6-Trichlorophenol
EPA
8270B
<10
ug/L
SRB
2/06/97
Extraction, 8270 Waters
EPA
3510
done
DJ
2/04/97
No.
Sample
ID
Date Sampled
Time Sampled
Matrix
Condition
2
MW-B /
MARION
1/28/97
17:25
GW
4±2°C
Date
Test Performed Method Results Tech Analyzed Qual
Volatiles in Water by GC/MS EPA 6240
Acetone
EPA
8240
Acrolein
EPA
8240
Acrylonitrile
EPA
8240
Benzene
EPA
8240
Bromodichloromethane
EPA
8240
Bromoform
EPA
8240
Bromomethane
EPA
8240
Carbon tetrachloride
EPA
8240
Chlorobenzene
EPA
8240
Chloroethane
EPA
8240
2-Chloroethylvinyl ether
EPA
8240
Chloroform
EPA
8240
Chloromethane
EPA
8240
Dibromochlorcmethane
EPA
8240
1,2-Dibromo-3-chloropropane
EPA
8240
1,2-Dibromoethane
EPA
8240
Dibromomethane
EPA
8240
Dichlorodifluoromethane
EPA
8240
---- Continued on Next Page ----
ZW
2/10/97
<50
ug/L
ZW
2/10/97
<50
ug/L
ZW
2/10/97
<50
ug/L
ZW
2/10/97
<5
ug/L
ZW
2/10/97
<5
ug/L
ZW
2/10/97
<5
ug/L
ZW
2/10/97
<10
ug/L
ZW
2/10/97
<5
ug/L
ZW
2/10/97
<5
ug/L
ZW
2/10/97
<10
ug/L
ZW
2/10/97
<10
ug/L
ZW
2/10/97
<5
ug/L
ZW
2/10/97
<10
ug/L
ZW
2/10/97
<5
ug/L
ZW
2/10/97
<25
ug/L
ZW
2/10/97
<5
ug/L
ZW
2/10/97
<10
ug/L
ZW
2/10/97
<5
ug/L
ZW
2/10/97

TRITEST, INC.
L a b o r a t o r y R e p o r t
NCDOT Beryl Rd. Office
Project No
No. Sample ID
2 MW-B / MARION
Test Performed
DOT/BERYL RD.
Method
Report Date
Work Order No
Results Tech
Page 5 of 7
2/18/97
9701-31002
Date
Analyzed Qual
1,1-Dichloroethane
EPA
8240
7.8
ug/L
ZW
2/10/97
1,2-Dichloroethane
EPA
8240
<5
ug/L
ZW
2/10/97
1,1-Dichloroethene
EPA
8240
<5
ug/L
ZW
2/10/97
trans-1,2-Dichloroethene
EPA
8240
7.5
ug/L
ZW
2/10/97
1,2-Dichloropropane
EPA
8240
<5
ug/L
ZW
2/10/97
cis-1,3-Dichloropropene
EPA
8240
<5
ug/L
ZW
2/10/97
trans-1, 3-Dichloropropene
EPA
8240
<5
ug/L
ZW
2/10/97
Ethylbenzene
EPA
6240
<5
ug/L
ZW
2/10/97
2-Hexanone
EPA
8240
<50
ug/L
ZW
2/10/97
Methylene chloride
EPA
8240
82.3
ug/L
ZW
2/12/97
Methyl ethyl ketone (MEK)
EPA
8240
<50
ug/L
ZW
2/10/97
MIBK (4-Methyl-2-pentanone)
EPA
6240
<50
ug/L
ZW
2/10/97
Styrene
EPA
8240
<5
ug/L
ZW
2/10/97
1,1,1,2-Tetrachloroethane
EPA
8240
<5
ug/L
ZW
2/10/97
1,1,2,2-Tetrachloroethane
EPA
8240
<5
ug/L
ZW
2/10/97
Tetrachloroethene
EPA
8240
<5
ug/L
ZW
2/10/97
Toluene
EPA
8240
<5
ug/L
ZW
2/10/97
1,1,1-Trichloroethane
EPA
8240
<5
ug/L
ZW
2/10/97
1,1,2-Trichloroethane
EPA
8240
<5
ug/L
ZW
2/10/97
Trichloroethene
EPA
8240
<5
ug/L
ZW
2/10/97
Trichloroflucromethane
EPA
8240
<5
ug/L
ZW
2/10/97
1,2,3-Trichloropropane
EPA
8240
<15
ug/L
ZW
2/10/97
Vinyl acetate
EPA
8240
<50
ug/L
ZW
2/10/97
Vinyl chloride
EPA
8240
<10
ug/L
ZW
2/10/97
o-Xylene
EPA
8240
<5
ug/L
ZW
2/10/97
m- & p-Xylene
EPA
8240
<5
ug/L
ZW
2/10/97
8270 (AWN), Waters
EPA
8270B
SRB
2/06/97
Acenaphthene
EPA
8270B
<10
ug/L
SRB
2/06/97
Acenaphthylene
EPA
8270B
<10
ug/L
SRB
2/06/97
Acetophenone
EPA
8270B
<10
ug/L
SRB
2/06/97
2-Acetylamino£luorene
EPA
827013
<20
ug/L
SRB
2/06/97
4-Aminobiphenyl
EPA
8270E
<20
ug/L
SRB
2/06/97
Aniline
EPA
8270B
<10
ug/L
SRB
2/06/97
Anthracene
EPA
8270B
<10
ug/L
SRB
2/06/97
Benzo(a)anthracene
EPA
8270B
<10
ug/L
SRB
2/06/97
Benzo(b)fluoranthene
EPA
8270D
<10
ug/L
SRB
2/06/97
Benzo(k)fluoranthene
EPA
8270E
<10
ug/L
SRB
2/06/97
Benzo(a)pyrene
EPA
8270B
<10
ug/L
SRB
2/06/97
Benzo(g,h,i)perylene
EPA
8270B
<10
ug/L
SRB
2/06/97
Benzoic acid
EPA
8270B
<50
ug/L
SRB
2/06/97
---- Continued on
Next Page ----

TRITEST, INC.
L a b o r a t o r y R e p o r t
NCDOT Beryl Rd. Office Report Date
Project No. DOT/BERYL RD. Work Order No
No. Sample ID
2 MW-B / MARION
Page 6 of 7
2/18/97
9701-31002
Date
Test Performed Method Results Tech Analyzed Qual
Benzyl alcohol
EPA
8270E
<10
ug/L
SRB
2/06/97
Benzyl butyl phthalate
EPA
8270B
<10
ug/L
SRB
2/06/97
Bis(2-chloroethyl)ether
EPA
8270B
<10
ug/L
SRB
2/06/97
Bis(2-chloroethoxy)methane
EPA
8270E
<10
ug/L
SRB
2/06/97
Bis(2-chloroisopropyl)ether
EPA
8270B
<10
ug/L
SRB
2/06/97
Bis(2-ethylhexyl)phthalate
EPA
8270B
<10
ug/L
SRB
2/06/97
4-Bromophenyl phenyl ether
EPA
8270E
<10
ug/L
SRB
2/06/97
4-Chloroaniline
EPA
8270B
<20
ug/L
SRB
2/06/97
2-Chloronaphthalene
EPA
8270E
<10
ug/L
SRB
2/06/97
4-Chloro-3-methylphenol
EPA
8270B
<10
ug/L
SRB
2/06/97
2-Chlorophenol
EPA
8270B
<10
ug/L
SRB
2/06/97
4-Chlorophenyl phenyl ether
EPA
8270B
<10
ug/L
SRB
2/06/97
Chrysene
EPA
8270E
<10
ug/L
SRB
2/06/97
Dibenzo(a,h)anthracene
EPA
8270B
<10
ug/L
SRB
2/06/97
Dibenzofuran
EPA
8270B
<10
ug/L
SRB
2/06/97
Di-n-butyl phthalate
EPA
8270B
<10
ug/L
SRB
2/06/97
3,31-Dichlorobenzidine
EPA
8270B
<20
ug/L
SRB
2/06/97
1,2-Dichlorobenzene
EPA
8270E
<10
ug/L
SRB
2/06/97
1,3-Dichlorobenzene
EPA
8270E
<10
ug/L
SRB
2/06/97
1,4-Dichlorobenzene
EPA
8270B
<10
ug/L
SRB
2/06/97
2,4-Dichlorophenol
EPA
8270B
<10
ug/L
SRB
2/06/97
Diethyl phthalate
EPA
8270B
<10
ug/L
SRB
2/06/97
2,4-Dimethylphenol
EPA
8270B
<10
ug/L
SRB
2/06/97
Dimethyl phthalate
EPA
8270B
<10
ug/L
SRB
2/06/97
2,4-Dinitrophenol
EPA
8270B
<50
ug/L
SRB
2/06/97
2,4-Dinitrotoluene
EPA
8270E
<10
ug/L
SRB
2/06/97
2,6-Dinitrotoluene
EPA
8270E
<10
ug/L
SRB
2/06/97
Di-n-octyl phthalate
EPA
8270E
<10
ug/L
SRB
2/06/97
Fluoranthene
EPA
8270B
<10
ug/L
SRB
2/06/97
Fluorene
EPA
8270E
<10
ug/L
SRB
2/06/97
Hexachlorobenzene
EPA
8270B
<10
ug/L
SRB
2/06/97
Hexachlorobutadiene
EPA
8270B
<10
ug/L
SRB
2/06/97
Hexachlorocyclopentadiene
EPA
8270B
<10
ug/L
SRB
2/06/97
Hexachloroethane
EPA
8270B
<10
ug/L
SRB
2/06/97
Indeno(1,2,3-c,d)pyrene
EPA
8270B
<10
ug/L
SRB
2/06/97
Isophorone
EPA
8270B
<10
ug/L
SRB
2/06/97
2-Methyl-4,6-dinitrophenol
EPA
8270B
<50
ug/L
SRB
2/06/97
1-Methylnaphthalene
EPA
8270B
<10
ug/L
SRB
2/06/97
2-Methylnaphthalene
EPA
8270B
<10
ug/L
SRB
2/06/97
2-Methylphenol
EPA
8270B
<10
ug/L
SRB
2/06/97
---- Continued on Next Page ----

TRITEST, INC.
Page 7 of 7
L a b o r a t cry Report
NCDOT Beryl Rd. Office Report Date
Project No. DOT/BERYL RD. Work Order No
No. Sample ID
2 MW-B / MARION
2/18/97
9701-31002
Date
Test Performed Method Results Tech Analyzed Qual
3- & 4-Methylphenol
EPA
8270E
<20
ug/L
SRB
2/06/97
- Naphthalene
EPA
8270B
<10
ug/L
SRB
2/06/97
2-Nitroaniline
EPA
8270B
<10
ug/L
SRB
2/06/97
3-Nitroaniline
EPA
8270B
<20
ug/L
SRB
2/06/97
4-Nitroaniline
EPA
8270B
<20
ug/L
SRB
2/06/97
Nitrobenzene
EPA
8270B
<10
ug/L
SRB
2/06/97
{j 2-Nitrophenol
EPA
8270B
<10
ug/L
SRB
2/06/97
4-Nitrophenol
EPA
8270D
<10
ug/L
SRB
2/06/97
N-Nitrosodimethylamine
EPA
8270D
<10
ug/L
SRB
2/06/97
N-Nitrosodiphenylamine
EPA
8270B
<20
ug/L
SRB
2/06/97
N-Nitrosodi-n-propylamine
EPA
827013
<20
ug/L
SRB
2/06/97
Pentachlorophenol
EPA
8270B
<30
ug/L
SRB
2/06/97
Phenanthrene
EPA
82703
<10
ug/L
SRB
2/06/97
Phenol
EPA
8270B
<10
ug/L
SRB
2/06/97
Pyrene
EPA
8270B
<10
ug/L
SRB
2/06/97
Pyridine
EPA
8270B
<10
ug/L
SRB
2/06/97
1,2,4-Trichlorobenzene
EPA
8270B
<20
ug/L
SRB
2/06/97
-. 2,4,5-Trichlorophenol
EPA
8270E
<20
ug/L
SRB
2/06/97
2,4,6-Trichlorophenol
EPA
8270B
<10
ug/L
SRB
2/06/97
Extraction, 8270 Waters
EPA
3510
done
DJ
2/04/97
Report certified by:
for Tritest, Inc.

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TRITEST, INC.
3909 Beryl Road
Raleigh, NC 27607
Telephone: [phone]
Fax: [phone]
NC/WW Cert.#: 067
L a b o r a t o r y R e p o r t
Prepared for ---
Eric Motzno
NCDOT Beryl Rd. Office
4809 Beryl Rd.
Raleigh, NC 27606
Page 1 of 7
Report Date: 2/26/97
Date Received: 2/13/97
Work Order #: 9702-13017
Cust. Code: NC3532
Project ID: DOT/BERYL RD. Cust. P.O.#:879048
Project Info: GROUNDWATER/MARIONPROJ.# 5.8711215
No. Sample ID Date Sampled Time Sampled Matrix Condition
1 MW-C / MARION 2/11 2/11/97 14:15 GW 4±2°C
Test Performed
Method
Date
Results Tech Analyzed Qual
volatiles in Water by GC/MS
EPA
8240
ZW
2/19/97
Acetone
EPA
8240
<50
ug/L
ZW
2/19/97
Acrolein
EPA
8240
<50
ug/L
ZW
2/19/97
Acrylonitrile
EPA
8240
<50
ug/L
ZW
2/19/97
Benzene
EPA
8240
16.8
ug/L
ZW
2/19/97
Bromodichloromethane
EPA
8240
<5
ug/L
ZW
2/19/97
Bromoform
EPA
8240
<5
ug/L
ZW
2/19/97
Bromomethane
EPA
6240
<10
ug/L
ZW
2/19/97
Carbon tetrachloride
EPA
8240
<5
ug/L
ZW
2/19/97
Chlorobenzene
EPA
8240
<5
ug/L
ZW
2/19/97
Chloroethane
EPA
8240
<10
ug/L
ZW
2/19/97
2-Chlorcethylvinyl ether
EPA
8240
<10
ug/L
ZW
2/19/97
Chloroform
EPA
8240
<5
ug/L
ZW
2/19/97
Chloromethane
EPA
8240
<10
ug/L
ZW
2/19/97
Dibromochloromethane
EPA
8240
<5
ug/L
ZW
2/19/97
1,2-Dibromo-3-chloropropane
EPA
8240
<25
ug/L
ZW
2/19/97
1,2-Dibromoethane
EPA
8240
<5
ug/L
ZW
2/19/97
Dibromomethane
EPA
8240
<10
ug/L
ZW
2/19/97
Dichlorodifluoromethane
EPA
8240
<5
ug/L
ZW
2/19/97
1,1-Dichloroethane
EPA
8240
6.8
ug/L
ZW
2/19/97
1,2-Dichloroethane
EPA
8240
<5
ug/L
ZW
2/19/97
1,1-Dichloroethene
EPA
8240
<5
ug/L
ZW
2/19/97
trans-1,2-Dichloroethene
EPA
8240
166
ug/L
ZW
2/19/97
1,2-Dichloropropane
EPA
8240
<5
ug/L
ZW
2/19/97
cis-1,3-Dichloropropene
EPA
8240
<5
ug/L
ZW
2/19/97
trans-1,3-Dichloropropene
EPA
8240
<5
ug/L
ZW
2/19/97
Ethylbenzene
EPA
8240
6.7
ug/L
ZW
2/19/97
-- Continued on
Next Page ----

TRITEST, INC.
Page 2 of 7
L a b o r a t o r y R e p o r t
NCDOT Beryl Rd. Office
Project No. DOT/BERYL RD.
No. Sample ID
1 MW-C / MARION 2/11
Test Performed
Method
Report Date
Work Order No
Results Tech
2/26/97
9702-13017
Date
Analyzed Qual
2-Hexanone
EPA
8240
<50
ug/L
ZW
2/19/97
Methylene chloride
EPA
8240
<5
ug/L
ZW
2/19/97
Methyl ethyl ketone (MEK)
EPA
8240
<50
ug/L
ZW
2/19/97
MIBK (4-Methyl-2-pentanone)
EPA
8240
<50
ug/L
ZW
2/19/97
Styrene
EPA
8240
<5
ug/L
ZW
2/19/97
1,1,1,2-Tetrachloroethane
EPA
8240
<5
ug/L
ZW
2/19/97
1,1,2,2-Tetrachloroethane
EPA
8240
<5
ug/L
ZW
2/19/97
Tetrachloroethene
EPA
8240
<5
ug/L
ZW
2/19/97
Toluene
EPA
8240
21.1
ug/L
ZW
2/19/97
1,1,1-Trichloroethane
EPA
8240
<5
ug/L
ZW
2/19/97
1,1,2-Trichloroethane
EPA
8240
<5
ug/L
ZW
2/19/97
Trichloroethene
EPA
8240
<5
ug/L
ZW
2/19/97
Trichlorofluoromethane
EPA
8240
<5
ug/L
ZW
2/19/97
1,2,3-Trichlorcpropane
EPA
8240
<15
ug/L
ZW
2/19/97
Vinyl acetate
EPA
8240
<50
ug/L
ZW
2/19/97
Vinyl chloride
EPA
8240
13.6
ug/L
ZW
2/19/97
o-Xylene
EPA
8240
46.4
ug/L
ZW
2/19/97
m- & p-Xylene
EPA
8240
19.8
ug/L
ZW
2/19/97
8270 (A&B/N), Waters
EPA
8270B
SRB
2/19/97
Acenaphthene
EPA
8270B
<10
ug/L
SRB
2/19/97
Acenaphthylene
EPA
8270B
<10
ug/L
SRB
2/19/97
Acetophenone
EPA
8270D
<10
ug/L
SRB
2/19/97
2-Acetylaminofluorene
EPA
8270B
<20
ug/L
SRB
2/19/97
4-Aminobiphenyl
EPA
8270E
<20
ug/L
SRB
2/19/97
Aniline
EPA
8270B
<10
ug/L
SRB
2/19/97
Anthracene
EPA
8270E
<10
ug/L
SRB
2/19/97
Benzo(a)anthracene
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzo(b)fluoranthene
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzo(k)fluoranthene
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzo(a)pyrene
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzo(g,h,i)perylene
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzoic acid
EPA
8270E
<50
ug/L
SRB
2/19/97
Benzyl alcohol
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzyl butyl phthalate
EPA
8270B
<10
ug/L
SRB
2/19/97
Bis(2-chloroethyl)ether
EPA
8270B
<10
ug/L
SRB
2/19/97
Bis(2-chloroethoxy)methane
EPA
8270B
<10
ug/L
SRB
2/19/97
Bis(2-chloroisopropyl)ether
EPA
8270B
<10
ug/L
SRB
2/19/97
Bis(2-ethylhexyl)phthalate
EPA
8270B
<10
ug/L
SRB
2/19/97
4-Bromophenyl phenyl ether
EPA
8270B
<10
ug/L
SRB
2/19/97
4-Chloroaniline
EPA
8270B
<20
ug/L
SRB
2/19/97
---- Continued on
Next Page ----

TRITEST, INC.
Page 3 of 7
L a b o r a t o r y R e p o r t
NCDOT Beryl Rd. Office
Project No. DOT/BERYL RD.
No. Sample ID
1 MW-C / MARION 2/11
Test Performed
Method
Report Date
Work Order No
Results Tech
2/26/97
9702-13017
Date
Analyzed Qual
2-Chloronaphthalene
EPA
8270B
<10
ug/L
SRB
2/19/97
4-Chloro-3-methylphenol
EPA
8270B
<10
ug/L
SRB
2/19/97
2-Chlorophenol
EPA
8270B
<10
ug/L
SRB
2/19/97
4-Chlorophenyl phenyl ether
EPA
8270B
<10
ug/L
SRB
2/19/97
Chrysene
EPA
8270B
<10
ug/L
SRB
2/19/97
Dibenzo(a,h)anthracene
EPA
8270D
<10
ug/L
SRB
2/19/97
Dibenzofuran
EPA
8270B
<10
ug/L
SRB
2/19/97
Di-n-butyl phthalate
EPA
8270B
<10
ug/L
SRB
2/19/97
3,31-Dichlorobenzidine
EPA
8270B
<20
ug/L
SRB
2/19/97
1,2-Dichlorobenzene
EPA
8270B
<10
ug/L
SRB
2/19/97
1,3-Dichlorobenzene
EPA
8270B
<10
ug/L
SRB
2/19/97
1,4-Dichlorobenzene
EPA
8270B
11.9
ug/L
SRB
2/19/97
2,4-Dichlorophenol
EPA
8270B
<10
ug/L
SRB
2/19/97
Diethyl phthalate
EPA
8270B
<10
ug/L
SRB
2/19/97
2,4-Dimethylphenol
EPA
8270D
<10
ug/L
SRB
2/19/97
Dimethyl phthalate
EPA
8270B
<10
ug/L
SRB
2/19/97
2,4-Dinitrophenol
EPA
8270B
<50
ug/L
SRB
2/19/97
2,4-Dinitrotoluene
EPA
8270B
<10
ug/L
SRB
2/19/97
2,6-Dinitrotoluene
EPA
8270B
<10
ug/L
SRB
2/19/97
Di-n-octyl phthalate
EPA
8270B
<10
ug/L
SRB
2/19/97
Fluoranthene
EPA
8270B
<10
ug/L
SRB
2/19/97
Fluorene
EPA
8270B
<10
ug/L
SRB
2/19/97
Hexachlorobenzene
EPA
8270B
<10
ug/L
SRB
2/19/97
Hexachlorobutadiene
EPA
8270B
<10
ug/L
SRB
2/19/97
Hexachlorocyclopentadiene
EPA
6270B
<10
ug/L
SRB
2/19/97
Hexachloroethane
EPA
8270B
<10
ug/L
SRB
2/19/97
Indeno(1,2,3-c,d)pyrene
EPA
8270B
<10
ug/L
SRB
2/19/97
Isophorone
EPA
8270B
<10
ug/L
SRB
2/19/97
2-Methyl-4,6-dinitrophenol
EPA
8270E
<50
ug/L
SRB
2/19/97
1-Methylnaphthalene
EPA
8270E
<10
ug/L
SRB
2/19/97
2-Methylnaphthalene
EPA
8270B
<10
ug/L
SRB
2/19/97
2-Methylphenol
EPA
8270B
<10
ug/L
SRB
2/19/97
3- & 4-Methylphenol
EPA
8270B
<20
ug/L
SRB
2/19/97
Naphthalene
EPA
8270B
<10
ug/L
SRB
2/19/97
2-Nitroaniline
EPA
8270B
<10
ug/L
SRB
2/19/97
3-Nitroaniline
EPA
8270B
<20
ug/L
SRB
2/19/97
4-Nitroaniline
EPA
8270B
<20
ug/L
SRB
2/19/97
Nitrobenzene
EPA
8270B
<10
ug/L
SRB
2/19/97
2-Nitrophenol
EPA
8270E
<10
ug/L
SRB
2/19/97
4-Nitrophenol
EPA
8270B
<10
ug/L
SRB
2/19/97
- - Continued on Next Page ----

TRITEST, INC.
Page 4 of 7
L a b o r a t o r y R e p o r t
NCDOT Beryl Rd. Office Report Date
Project No. DOT/BERYL RD. Work Order No
No. Sample ID
1 MW-C / MARION 2/11
2/26/97
9702-13017
Date
Test Performed Method Results Tech Analyzed Qual
N-Nitrosodimethylamine
EPA
8270B
<10
ug/L
SRB
2/19/97
N-Nitrosodiphenylamine
EPA
6270B
<20
ug/L
SRB
2/19/97
N-Nitrosodi-n-propylamine
EPA
8270B
<20
ug/L
SRB
2/19/97
Pentachlorophenol
EPA
8270B
<30
ug/L
SRB
2/19/97
Phenanthrene
EPA
8270B
<10
ug/L
SRB
2/19/97
Phenol
EPA
8270B
<10
ug/L
SRB
2/19/97
Pyrene
EPA
8270B
<10
ug/L
SRB
2/19/97
Pyridine
EPA
8270B
<10
ug/L
SRB
2/19/97
1,2,4-Trichlorobenzene
EPA
8270B
<20
ug/L
SRB
2/19/97
2,4,5-Trichlorophenol
EPA
8270B
<20
ug/L
SRB
2/19/97
2,4,6-Trichlorophenol
EPA
8270B
<10
ug/L
SRB
2/19/97
Extraction, 8270 Waters
EPA
3510
done
DJ
2/18/97
No. Sample ID Date Sampled Time Sampled Matrix Condition
2 MW-D / MARION 2/12 2/11/97 14:15 GW 4±2°C
Date
Test Performed Method Results Tech Analyzed Qual
Volatiles in Water by GC/MS
EPA
8240
ZW
2/19/97
Acetone
EPA
8240
80.7
ug/L
ZW
2/19/97
Acrolein
EPA
8240
<50
ug/L
ZW
2/19/97
Acrylonitrile
EPA
8240
<50
ug/L
ZW
2/19/97
Benzene
EPA
8240
14.9
ug/L
ZW
2/19/97
Bromodichloromethane
EPA
8240
<5
ug/L
ZW
2/19/97
Bromoform
EPA
8240
<5
ug/L
ZW
2/19/97
Bromomethane
EPA
8240
<10
ug/L
ZW
2/19/97
Carbon tetrachloride
EPA
8240
<5
ug/L
ZW
2/19/97
Chlorobenzene
EPA
8240
<5
ug/L
ZW
2/19/97
Chloroethane
EPA
8240
<10
ug/L
ZW
2/19/97
2-Chloroethylvinyl ether
EPA
8240
<10
ug/L
ZW
2/19/97
Chloroform
EPA
8240
<5
ug/L
ZW
2/19/97
Chloromethane
EPA
8240
<10
ug/L
ZW
2/19/97
Dibromochloromethane
EPA
8240
<5
ug/L
ZW
2/19/97
1,2-Dibromo-3-chloropropane
EPA
8240
<25
ug/L
ZW
2/19/97
1,2-Dibromoethane
EPA
8240
<5
ug/L
ZW
2/19/97
Dibromomethane
EPA
8240
<10
ug/L
ZW
2/19/97
Dichlorodifluoromethane
EPA
8240
<5
ug/L
ZW
2/19/97
---- Continued on Next Page ----

TRITEST, INC.
Page 5 of 7
L a b o r a t o r y Report
NCDOT Beryl Rd. Office
Project No. DOT/BERYL RD.
No. Sample ID
2 MW-D / MARION 2/12
Test Performed
Method
Report Date
Work Order No
Results Tech
2/26/97
9702-13017
Date
Analyzed Qual
1,1-Dichloroethane
EPA
8240
12.2
ug/L
ZW
2/19/97
1,2-Dichloroethane
EPA
8240
<5
ug/L
ZW
2/19/97
1,1-Dichloroethene
EPA
8240
<5
ug/L
ZW
2/19/97
trans-1,2-Dichloroethene
EPA
8240
138
ug/L
ZW
2/19/97
1,2-Dichloropropene
EPA
8240
<5
ug/L
ZW
2/19/97
cis-1,3-Dichloropropene
EPA
8240
<5
ug/L
ZW
2/19/97
trans-1,3-Dichloropropene
EPA
8240
<5
ug/L
ZW
2/19/97
Ethylbenzene
EPA
8240
<5
ug/L
ZW
2/19/97
2-Hexanone
EPA
8240
<50
ug/L
ZW
2/19/97
Methylene chloride
EPA
8240
<5
ug/L
ZW
2/19/97
Methyl ethyl ketone (MEK)
EPA
8240
150
ug/L
ZW
2/19/97
MIBK (4-Methyl-2-pentanone)
EPA
8240
<50
ug/L
ZW
2/19/97
Styrene
EPA
8240
<5
ug/L
ZW
2/19/97
1,1,1,2-Tetrachloroethane
EPA
8240
<5
ug/L
ZW
2/19/97
1,1,2,2-Tetrachloroethane
EPA
8240
<5
ug/L
ZW
2/19/97
Tetrachloroethene
EPA
8240
<5
ug/L
ZW
2/19/97
Toluene
EPA
8240
12.2
ug/L
ZW
2/19/97
1,1,1-Trichloroethane
EPA
8240
<5
ug/L
ZW
2/19/97
1,1,2-Trichloroethane
EPA
8240
<5
ug/L
ZW
2/19/97
Trichloroethene
EPA
8240
<5
ug/L
ZW
2/19/97
Trichlorofluoromethane
EPA
8240
<5
ug/L
ZW
2/19/97
1,2,3-Trichloropropane
EPA
8240
<15
ug/L
ZW
2/19/97
Vinyl acetate
EPA
8240
<50
ug/L
ZW
2/19/97
Vinyl chloride
EPA
8240
10.4
ug/L
ZW
2/19/97
o-Xylene
EPA
8240
18.8
ug/L
ZW
2/19/97
m- & p-Xylene
EPA
8240
7.0
ug/11
ZW
2/19/97
8270 (A&B/N), Waters
EPA
8270B
SRB
2/19/97
Acenaphthene
EPA
8270B
<10
ug/L
SRB
2/19/97
Acenaphthylene
EPA
8270D
<10
ug/L
SRB
2/19/97
Acetophenone
EPA
8270D
<10
ug/L
SRB
2/19/97
2-Acetylaminof luorene
EPA
6270B
<20
ug/L
SRB
2/19/97
4-Aminobiphenyl
EPA
8270B
<20
ug/L
SRB
2/19/97
Aniline
EPA
8270B
<10
ug/L
SRB
2/19/97
Anthracene
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzo(a)anthracene
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzo(b)fluoranthene
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzo(k)fluoranthene
EPA
8270E
<10
ug/L
SRB
2/19/97
Benzo(a)pyrene
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzo(g,h,i)perylene
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzoic acid
EPA
8270B
<50
ug/L
SRB
2/19/97
--- Continued on Next Page ----

TRITEST, INC.
L a b o r a t o r y R e p o r t
NCDOT Beryl Rd. Office
Project No. DOT/BERYL RD.
No. Sample ID
2 MW-D / MARION 2/12
Test Performed
Method
Report Date
Work Order No
Results Tech
Page 6 of 7
2/26/97
9702-13017
Date
Analyzed Qual
Benzyl alcohol
EPA
8270B
<10
ug/L
SRB
2/19/97
Benzyl butyl phthalate
EPA
8270B
<10
ug/L
SRB
2/19/97
Bis(2-chloroethyl)ether
EPA
8270B
<10
ug/L
SRB
2/19/97
Bis(2-chloroethoxy)methane
EPA
8270B
<10
ug/L
SRB
2/19/97
Bis(2-chloroisopropyl)ether
EPA
8270B
<10
ug/L
SRB
2/19/97
Bis(2-ethylhexyl)phthalate
EPA
8270B
<10
ug/L
SRB
2/19/97
4-Bromophenyl phenyl ether
EPA
8270B
<10
ug/L
SRB
2/19/97
4-Chloroaniline
EPA
8270B
<20
ug/L
SRB
2/19/97
2-Chloronaphthalene
EPA
8270B
<10
ug/L
SRB
2/19/97
4-Chloro-3-methylphenol
EPA
8270E
<10
ug/L
SRB
2/19/97
2-Chlorophenol
EPA
8270B
<10
ug/L
SRB
2/19/97
4-Chlorophenyl phenyl ether
EPA
8270B
<10
ug/L
SRB
2/19/97
Chrysene
EPA
8270B
<10
ug/L
SRB
2/19/97
Dibenzo(a,h)anthracene
EPA
8270E
<10
ug/L
SRB
2/19/97
Dibenzofuran
EPA
8270B
<10
ug/L
SRB
2/19/97
Di-n-butyl phthalate
EPA
8270B
<10
ug/L
SRB
2/19/97
3,31-Dichlorobenzidine
EPA
8270B
<20
ug/L
SRB
2/19/97
1,2-Dichlorobenzene
EPA
8270B
<10
ug/L
SRB
2/19/97
1,3-Dichlorobenzene
EPA
8270B
<10
ug/L
SRB
2/19/97
1,4-Dichlorobenzene
EPA
8270B
<10
ug/L
SRB
2/19/97
2,4-Dichlorophenol
EPA
8270B
<10
ug/L
SRB
2/19/97
Diethyl phthalate
EPA
8270E
<10
ug/L
SRB
2/19/97
2,4-Dimethylphenol
EPA
8270B
<10
ug/L
SRB
2/19/97
Dimethyl phthalate
EPA
8270B
<10
ug/L
SRB
2/19/97
2,4-Dinitrophenol
EPA
8270B
<50
ug/L
SRB
2/19/97
2,4-Dinitrotoluene
EPA
8270B
<10
ug/I:
SRB
2/19/97
2,6-Dinitrotoluene
EPA
8270B
<10
ug/L
SRB
2/19/97
Di-n-octyl phthalate
EPA
8270B
<10
ug/L
SRB
2/19/97
Fluoranthene
EPA
8270B
<10
ug/L
SRB
2/19/97
Fluorene
EPA
8270B
<10
ug/L
SRB
2/19/97
Hexachlorobenzene
EPA
8270B
<10
ug/L
SRB
2/19/97
Hexachlorobutadiene
EPA
8270B
<10
ug/L
SRB
2/19/97
Hexachlorocyclopentadiene
EPA
8270B
<10
ug/L
SRB
2/19/97
Hexachloroethane
EPA
8270B
<10
ug/L
SRB
2/19/97
Indeno(1,2,3-c,d)pyrene
EPA
8270B
<10
ug/L
SRB
2/19/97
Isophorone
EPA
8270B
<10
ug/L
SRB
2/19/97
2-Methyl-4,6-dinitrophenol
EPA
8270B
<50
ug/L
SRB
2/19/97
1-Methylnaphthalene
EPA
8270B
<10
ug/L
SRB
2/19/97
2-Methylnaphthalene
EPA
8270B
<10
ug/L
SRB
2/19/97
2-Methylphenol
EPA
8270B
<10
ug/L
SRB
2/19/97
---- Continued on Next Page ----

TRITEST, INC.
L a b o r a t o r y R e p o r t
NCDOT Beryl Rd. Office
Project No. DOT/BERYL RD.
No. Sample ID
2 MW-D / MARION 2/12
Report Date
Work Order No
Page 7 of 7
2/26/97
9702-13017
Date
Test Performed Method Results Tech Analyzed Qual
3- & 4-Methylphenol
EPA
8270B
<20
ug/L
SRB
2/19/97
Naphthalene
EPA
8270B
<10
ug/L
SRB
2/19/97
2-Nitroaniline
EPA
8270B
<10
ug/L
SRB
2/19/97
3-Nitroaniline
EPA
8270B
<20
ug/L
SRB
2/19/97
4-Nitroaniline
EPA
6270B
<20
ug/L
SRB
2/19/97
Nitrobenzene
EPA
8270B
<10
ug/L
SRB
2/19/97
2-Nitrophenol
EPA
8270B
<10
ug/L
SRB
2/19/97
4-Nitrophenol
EPA
8270B
<10
ug/L
SRB
2/19/97
N-Nitrosodimethylamine
EPA
8270B
<10
ug/L
SRB
2/19/97
N-Nitrosodiphenylamine
EPA
8270B
<20
ug/L
SRB
2/19/97
N-Nitrosodi-n-propylamine
EPA
8270B
<20
ug/L
SRB
2/19/97
Pentachlorophenol
EPA
8270E
<30
ug/L
SRB
2/19/97
Phenanthrene
EPA
8270B
<10
ug/L
SRB
2/19/97
Phenol
EPA
8270E
<10
ug/L
SRB
2/19/97
Pyrene
EPA
8270B
<10
ug/L
SRB
2/19/97
Pyridine
EPA
8270B
<10
ug/L
SRB
2/19/97
1,2,4-Trichlorobenzene
EPA
8270B
<20
ug/L
SRB
2/19/97
2,4,5-Trichlorophenol
EPA
8270B
<20
ug/L
SRB
2/19/97
2,4,6-Trichlorophenol
EPA
82703
<10
ug/L
SRB
2/19/97
Extraction, 8270 Waters
EPA
3510
done
DJ
2/18/97
Report certifier. by:
(Z
for Tritest, Inc.

T'x test Inc.
3909 Beryl Road, 11aleigh, NC 27607
ph: [phone] Faaic [phone]
NCWW Cert#67, NCDW cent
Report Results To:
Company: rYool-nAXI-,J l vt/'Jtr )
Address: %09 kgyb� oRtqG
eAt6lbt} W- n'Jwo
Attn: ERw .nod
Phone: ?31-L1-Lv
Sampled by (signature):
Cr-(A.ss
Bill To:
SAwrZ
Project Reference:
P roject N u mber:
Purchase Order #:
Tritest W.0 #�
tk-Doi 5•�-7//-Z/5
❑ Standard Report Delivery
❑ Fush Report Delivery (w/ surcharge)
-usn are seoieot m v#or avere m by the iabmmory
Fequested Due Date:
Sample Description
C.','N ,r
G.e
_ Start _Date _
Start Time
End Date
_ End Time
Matrix
ow.'a':m
Analyses Requested
it
Togs
satac'e#
MN -C
(1
Iylj
i•(I
(qtr
`41V 1
1 (`t1r
&
9W , 91,70
Relinqui hed b sign re)
Rece d by (signature) -
aL�-(-G(, �-�—
Data
211�Il7
Time
�2i2�
Receipt Conditions (Lab Use Only),
9 4t2°C ❑ Temp: "C
Res. Chlorine E Absent ❑Present ❑n/a
Acid preserv. Q? ❑Yes ❑No ❑n/a
Base preserv. >12? []Yes ❑No ❑n/a
Relinquished by (signaure)
Received by (signature)
pate
I me
Relinquished by (signature)
'
Received by(signature)
-
pate
Time

a
A:po�'A Wm/ s vJ S
STATE OF NORTH CAROLINA
DEPARTMENT OF TRANSPORTATION
JAMH B. HUNT JR. DIVISION OF HIGHWAYS GARLAND B. GARRETT JR.
GOVERNOR SECRETARY
March 17, 1997
Mr. Mark Poindexter
Division of Solid Waste
P.O. Box 27687
Raleigh, NC 27611-0692
RE: McDowell County Landfill, Marion
Dear Mark:
As requested, the Department of Transportation installed 4
monitor wells in and arAund the McDowell County landfill to
determine the source oTS BTEX contamination in MW-2. On
January 28, 1997, monitor wells A and B were installed on DOT
property by Front Royal Environmental Services. These wells
were drilled by an auger drill rig.(PWhen attempts were made
to drill the wells on county property, auger refusal was
encountered above the water table. Therefore, Front Royal
mobilized a second time on February 11 and 12, with an air -
rotary drill rig to install wells C and D. The well
locations are indicated in Figure 1. The well construction
records are in Appendix A. Table 1 is a summary of well
construction data.
On February 19, Front Royal measured the water levels in all
4 wells. The relative wellhead elevations were surveyed
based on the existing MW-2 (100.00'). Table 2 provides data
on wellhead and water table elevation. No data was available
on MW-2. Based on the water table elevations in well A, B,
and C, the ground water flow direction is to the west (Figure
2). Since the water level in well D represents the bedrock
aquifer rather than the surficial aquifer in wells A, B and
C, it was not appropriate to include well D data in
calculating the poteniometric surface.n
On January 28, wells A and B were sampled by Front $oyal and
the samples were submitted on January 31 to Tritest`l Inc, for
analyses by Methods 8240 and 8270B. Wells C and D were
sampled on February 11 by Front Royal and the samples were
submitted to Tritest on Feb. 13 for analyses by the same
methods above. The two laboratory reports dated February 18
and 26 are in Appendix B.
LeaN

Mr. Mark Poindexter
March 17, 1997
Page 2.
The laboratory analyses show ground water contamination by
various volatiles and semi-volatiles. Table 3 lists these
compounds along with the 2L standard if established.
Separate plume maps for benzene, toluene, ethylbenzene and
total xylenes are included in this report as Figures 3 thru
6. Since the source of BTEX contamination in the county's
MW-2 is suspected to be from the DOT, plume maps for other
compounds were not generated.
Based on the combination of ground water flow direction and
the concentrations of BTEX in wells A thru D, the source of
the BTEX in MW-2 seems to be the landfill. If you have
questions, please call me at [phone].
Sincerely,
Eric Motzno, L.G.
Hydrogeologist
CC; Tony Moore, F.E.
District Engineer
Chuck Abernathy
County Manager

Table 1.
Well Construction Details
A
1/28/97
46.5'
34' - 44'
41.37
B
1/28/97
46.0'
34' - 44'
35.10
C
2/11/97
65.0'
53' - 63'
49.64
D
2/12/97
84.0'
66' - 81'
71.05

Table 2.
Wellhead and Water Table Elevations
A
tl�g
110.83 -
41.37
= 69.46
B
94.88 -
35.10
= 59.78
C
97.03 -
49.64
= 47.39
*D
117.34 -
71.05
= 46.29
* Well D is bedrock aquifer

Table 3.
Laboratory Analyses
Methods 8240 and 8270B
Acetone
700
80.7
Benzene
1
9.4
16.8
14.9
Chloroethane
22.1
1,1-Dichloroethane
700
55.8
7.8
6.8
12.2
trans- 1, 2-Dichloroethene
70
43.6
7.5
166
138
Ethylbenzene
29
6.7
Methylene chloride
5
451
82.3
Methyl ethyl ketone (MEK)
170
150
Toluene
1000
21.1
12.2
1,1,1-Trichloroethane
200
12.7
Vinyl chloride
0.015
13.6
10.4
Xylenes
530
5.7
66.2
25.8
1,4-Dichlorobenzene
75
1
1
11.9
MW-A and MW-B sampled 1-28-97
MW-C and MW-D sampled 2-11.97

WELL t7
EL. 97.03
(D WELL V
1:0 EL. 117.34
WELL,;,
EL. 100.00
_-WELL46 O WELL,4
rT A EL 110
i— --3
Figure /,
L on W-Fi 1(
i "x m 0,

Li
p Q
icl' C' .p o• T � iT
-F T
5c-hoo 1 }

I L
W E
E 2 WELL,� 3dr,,k
,/E 910 S/
97 't�
V7.3q/ EL. 117.34 C7- rOq A W k1a 7� r
F(owl Direcftom
WELLe
EL. 100.00
t
LL WELLA
94.88 EL. I 10 83
�21 6,
oll
0""., 01.
lb I
A
.0�
0

1)
5cho6
Q,a D�—
Li
-44

WELL 2
EL. 97.Oj
0 WELL 5
iz) EL. 117.34
1#11
.13
--/ ----------
OD BI)L.--- � 32
u
Z-
C�
Benene
Al;v- a
WELL I
0 EL. 100.00
@ WET T
EL. 94.88 EL. I LO. 8
WELT I
z
per n

1�
c
WE
EL. LL 2 WELL 5
97.03 EL. 117.34
Aa6 /-n.3 ��A
WELL I
E) EL. 100.00
-1
a&_
fi �/l
- �R� 1�
0
I WELL 1 0 WELL 4 1-- a; ?
EL 94 88
EL. 110.83
a -o
a 104.11
'o
—1c / t( e n e- 60
Fig, � *:

WELL 2
EL. 97.01
r,7 �
0 WELL 5
EL. 117.34
WELL I
0 EL. 100.00
WELL 3 WELL 4
EL. 94.88 EL. 110.8-
q) BD L apl-
ZZ,
10
e-o I.,
1.0 f,o
IS
F 0
EMylhe4z(f�&-

WELL 2 WELL 5 Xylene5
EL. 97.03 0 EL. 117.34
WhLL I
0 EL. 100.00
01
WELL 3 WELL 4 0
EL. 110.83
EL. 94.8�
0504
3j
ZA
+
2
0
c 0'
4,,
0
TA X y /04(f 5 (pp,6)

NC DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
Division of Solid waste Kanagement
Solid Waste Section
SOLID WASTE MAGEMENT FACILITY EVALUATION REPORT
Type of Facility
Permit # County
Name of Facility Locati
Date of Last Evaluation
I. Permit Conditions Followed Yes No N/A
A. Specific Condition(s) Violated
II. Operational Requiremients FolLowed Yes No
15A N-C. Admin. code 13B section
A. Specific VioLation(s) by number and Letter.
III- Other Violations of Rule or Law
IV. Evaluator's Coffnents
V. Continuation Page Required7 Yes No Receiving Signature
,,,, , / 4
Evaluation Date Solid Waste Section
DEHNR 3793 (Part I White: Facility Part II Canary: Central Office Part III Pink: Regional Office)
Solid Waste Section (Review 7/94)

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pade Analytocal
Asheville, NC 28801
Tel: [phone]
McDowell County Landfill
Fax: [phone]
June 12, 1997
10 East Court Street
PACE Project Number: A70529601
Marion, NC 28752
Attn:
Client Reference: Monitoring Wells
PACE Sample Number:
93 0399177 93 0399185 93 0399193
Date Collected:
05/29/97 05/29/97 05/29/97
Date Received:
05/29/97 05/29/97 05/29/97
DOT MW #A DOT MW #B DOT MW #C
Parameter
Units
PRL
FIELD ANALYSIS
INDIVIDUAL PARAMETERS
Depth to Water
feet
0.01
38.90 33.92 48.14
Specific Conductivity (Field)
umhos/cm2
10
150 - -
Specific Conductivity (Field)
umhos/cm2
100
- 1500 600
Temperature (Field)
Degrees C
0.5
15 15 16
pH (Field)
Units
0.1
4.0 3.7 5.1
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Antimony
mg/L
0.004
ND
ND
ND
Arsenic
mg/L
0.005
ND
ND
ND
Barium
mg/L
0.10
0.99
3.7
0.61
Beryllium
mg/L
0.002
NO
0.005
ND
Cadmium
mg/L
0.001
ND
0.001
0.001
Chromium
mg/L
0.001
0.005
0.007
0.005
Cobalt
mg/L
0.010
0.013
0.033
0.015
Copper
mg/L
0.01
0.02
0.03
0.03
Lead
mg/L
0.005
0.012
0.034
0.013
Nickel
mg/L
0.05
ND
ND
NO
Selenium
mg/L
0.005
IND
ND
ND
Silver
mg/L
0.001
ND
ND
ND
Thallium
mg/L
0.002
ND
0.002
ND
Vanadium
mg/L
0.040
ND
ND
ND
Zinc
mg/L
0.01
0.07
0.07
0.08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal
Asheville, NG 28801
Tel: [phone]
Fax: [phone]
age
June
12, 1997
PACE
Project Number: A70529601
Client Reference: Monitoring Wells
PACE Sample Number:
Date Collected:
93 0399207 93 0399223
Date Received:
05/29/97
05/29/97
Client Sample ID:
05/29/97 05/29/97
DOT MW #D
Equipment
Parameter
Units
PRL
Blank
Bailer A
FIELD ANALYSIS
INDIVIDUAL PARAMETERS
Depth to Water
feet
0.01
69.00
-
Specific Conductivity (Field)
umhos/cm2
100
1200
-
Temperature (Field)
Degrees C
0.5
18
-
PH (Field)
Units
0.1
4.5
-
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Antimony
mg/L
0.004
NO
ND
Arsenic
mg/L
0.005
NO
NO
Barium
mg/L
0.10
0.49
NO
Beryllium
mg/L
0.002
ND
NO
Cadmium
mg/L
0.001
ND
NO
Chromium
mg/L
0.001
0.004
ND
Cobalt
Copper
mg/L
0.010
0.052
NO .
Lead
mg/L
0.01
0.01
NO
Nickel
mg/L
0.005
0.009
ND
Selenium
mg/L
0.05
NO
ND
Silver
mg/L
0.005
NO
ND
mg/L
0.001
NO
ND
Thallium
mg/L
0.002
ND
NO
Vanadium
mg/L
0.040
NO
ND
Zinc
mg/L
0.01
0.07
0.01
These data have been reviewed and are approved for release.
m -jL
Walter L. Miller
Operations Manager
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
E!ac,e Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Page 3 FOOTNOTES June 12, 1997
for pages I through 2 PACE Project Number: A70529601
Client Reference: Monitoring Wells
NO Not detected at or above the PRIL.
PRL PACE Reporting Limit
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Eace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
McDowell County Landfill June 11, 1997
10 East Court Street PACE Project Number: A70529601
Marion, NC 28752
Attn:
Client Reference: McDowell Co. Landfill
PACE Sample Number:
93 0399177
Date Collected:
05/29/97
Date Received:
05/29/97
DOT MW#A
Parameter
Units
PRL
METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
NO
06/09/97
Chloroethene (Vinyl chloride)
ug/L
10
NO
06/09/97
Bromomethane
ug/L
10
NO
06/09/97
Chloroethane
ug/L
10
13
06/09/97
Trichlorofluoromethane
ug/L
5.0
NO
06/09/97
Acetone
ug/L
100
NO
06/09/97
1,1-Dichloroethene
ug/L
5.0
NO
06/09/97
Methyl iodide
ug/L
5.0
NO
06/09/97
Acrylonitrile
ug/L
100
NO
06/09/97
Dichloromethane
ug/L
25
360
06/09/97
Carbon disulfide
ug/L
5.0
ND
06/09/97
trans-1,2-Dichloroethene
ug/L
5.0
NO
06109/97
1,1-Dichloroethane
ug/L
5.0
35
06/09/97
Vinyl acetate
ug/L
50
ND
06/09/97
Methyl ethyl ketone
ug/L
100
NO
06/09/97
cis-1,2-Dichloroethene
ug/L
5.0
50
06/09/97
Chloroform
ug/L
5.0
NO
06/09/97
Bromochloromethane
ug/L
5.0
NO
06/09/97
1,1,1-Trichloroethane
ug/L
5.0
8.5
06/09/97
1,2-Dichloroethane
ug/L
5.0
NO
06/09/97
Carbon tetrachloride
ug/L
5.0
NO
06/09/97
Benzene
ug/L
5.0
8.5
06/09/97
Trichloroethene
ug/L
5.0
5.4
06/09/97
1,2-Dichloropropane
ug/L
5.0
ND
06/09/97
Dibromomethane
ug/L
5.0
ND
06/09/97
Bromodichloromethane
ug/L
5.0
NO
06/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
NO
06/09/97
cis-1,3-Dichloropropene
ug/L
5.0
NO
06/09/97
Toluene
ug/L
5.0
NO
06/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NG 28801
Pag 2
Client Reference: McDowell Co. Landfill
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter Units PRL
ORGANIC ANALYSIS
Tel: [phone]
Fax: [phone]
June 11, 1997
PACE Project Number: A70529601
93 0399177
05/29/97
05/29/97
DOT MW#A
METHOD DATE ANALYZED
APPENDIX 1, LANDFILL VOLATILES
8260
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
06/09/97
1,1,2-Trichloroethane
ug/L
5.0
NO
06/09/97
2-Hexanone
ug/L
50
NO
06/09/97
Dibromochloromethane
ug/L
5.0
NO
06/09/97
Tetrachloroethylene
ug/L
5.0
7.1
06/09/97
1,2-Dibromoethane
ug/L
5.0
NO
06/09/97
Chlorobenzene
ug/L
5.0
NO
06/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
06/09/97
Ethylbenzene
ug/L
5.0
NO
06/09/97
Xylenes, (total)
ug/L
5.0
25
06/09/97
Styrene
ug/L
5.0
NO
06/09/97
Bromoform
ug/L
5.0
NO
06/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
06/09/97
1,2,3-Trichloropropane
ug/L
5.0
NO
06/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
06/09/97
1,4-Dichlorobenzene
ug/L
5.0
NO
06/09/97
1,2-Dichlorobenzene
ug/L
5.0
NO
06/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
IND
06/09/97
Surrogate - Dibromofluoromethane
%
107
06/09/97
Surrogate - Toluene-d8
%
101
06/09/97
Surrogate - 4-Bromofluorobenzene
%
99
06/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
June 11, 1997
Page 3 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
PACE Sample Number: 93 0399185
Date Collected: 05/29/97
Date Received: 05/29/97
Client Sample ID: DOT MW#B
Parameter Units PRL METHOD DATE ANALYZED
AW10.11 a 111F.11 I! F-11 W&I &4
APPENDIX 1, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
ND
06/09/97
Chloroethene (Vinyl chloride)
ug/L
10
ND
06/09/97
Bromomethane
ug/L
10
NO
06/09/97
Chloroethane
ug/L
10
NO
06/09/97
Trichlorofluoromethane
ug/L
5.0
NO
06/09/97
Acetone
ug/L
100
ND
06/09/97
1,1-Dichloroethene
ug/L
5.0
NO
06/09/97
Methyl iodide
ug/L
5.0
NO
06/09/97
Acrylonitrile
ug/L
100
NO
06/09/97
Dichloromethane
ug/L
5.0
54
06/09/97
Carbon disulfide
ug/L
5.0
ND
06/09/97
trans-1,2-Dichloroethene
ug/L
5.0
NO
06/09/97
1,1-Dichloroethane
ug/L
5.0
6.1
06/09/97
Vinyl acetate
ug/L
50
ND
06/09/97
Methyl ethyl ketone
ug/L
100
NO
06/09/97
cis-1,2-Dichloroethene
ug/L
5.0
5.3
06/09/97
Chloroform
ug/L
5.0
NO
06/09/97
Bromochloromethane
ug/L
5.0
ND
06/09/97
1,1,1-Trichloroethane
ug/L
5.0
NO
06/09/97
1,2-Dichloroethane
ug/L
5.0
NO
06/09/97
Carbon tetrachloride
ug/L
5.0
ND
06/09/97
Benzene
ug/L
5.0
NO
06/09/97
Trichloroethene
ug/L
5.0
NO
06/09/97
1,2-Dichloropropane
ug/L
5.0
ND
06/09/97
Dibromomethane
ug/L
5.0
NO
06/09/97
Bromodichloromethane
ug/L
5.0
NO
06/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
NO
06/09/97
cis-1,3-Dichloropropene
ug/L
5.0
ND
06/09/97
Toluene
ug/L
5.0
ND
06/09/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
06/09/97
1,1,2-Trichloroethane
ug/L
5.0
ND
06/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Raveflscroft Drive
Race Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
June 11, 1997
Page 4 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
PACE Sample Number: 93 0399185
Date Collected: 05/29/97
Date Received: 05/29/97
Client Sample ID: DOT MW#B
Parameter Units PRL METHOD DATE ANALYZED
APPENDIX I, LANDFILL VOLATILES
8260
2-Hexanone
ug/L
50
ND
06/09/97
Dibromochloromethane
ug/L
5.0
ND
06/09/97
Tetrachloroethylene
ug/L
5.0
ND
06/09/97
1,2-Dibromoethane
ug/L
5.0
ND
06/09/97
Chlorobenzene
ug/L
5.0
ND
06/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
06/09/97
Ethylbenzene
ug/L
5.0
ND
06/09/97
Xylenes, (total)
ug/L
5.0
NO
06/09/97
Styrene
ug/L
5.0
ND
06/09/97
Bromoform
ug/L
5.0
ND
06/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
06/09/97
1,2,3-Trichloropropane
ug/L
5.0
NO
06/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
06�09/97
1,4-Dichlorobenzene
ug/L
5.0
ND
06/09/97
1,2-Dichlorobenzene
ug/L
5.0
ND
06/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
NO
06/09/97
Surrogate - Dibromofluoromethane
%
96
06/09/97
Surrogate - Toluene-d8
%
102
06/09/97
Surrogate - 4-Bromofluorobenzene
%
102
06/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Favenscroft Drive
Pace AnalyUcal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
age 5
Client Reference: McDowell Co. Landfill
June 11, 1997
PACE Project Number: A70529601
PACE Sample Number: 93 0399193
Date Collected: 05/29/97
Date Received: 05/29/97
Client Sample ID: DOT MW#C
Parameter Units PRL METHOD DATE ANALYZED
A,
I Jefifflifliff.11kirAW3160
APPENDIX I, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
IND
06/09/97
Chloroethene (Vinyl chloride)
ug/L
10
14
06/09/97
Bromomethane
ug/L
10
NO
06/09/97
Chloroethane
ug/L
10
NO
06/09/97
Trichlorofluoromethane
ug/L
5.0
ND
06/09/97
Acetone
ug/L
100
ND
06/09/97
1,1-Dichloroethene
ug/L
5.0
NO
06/09/97
Methyl iodide
ug/L
5.0
ND
06/09/97
Acrylonitrile
ug/L
100
ND
06/09/97
Dichloromethane
ug/L
5.0
11
06/09/97
Carbon disulfide
ug/L
5.0
ND
06/09/97
trans-1,2-Dichloroethene
ug/L
5.0
NO
06/09/97
1,1-Dichloroethane
ug/L
5.0
ND
06/09/97
Vinyl acetate
ug/L
50
IND
06/09/97
Methyl ethyl ketone
ug/L
100
130
06/09/97
cis-1,2-Dichloroethene
ug/L
5.0
170
06/09/97
Chloroform
ug/L
5.0
ND
06/09/97
Bromochloromethane
ug/L
5.0
ND
06/09/97
1,1,1-Trichloroethane
ug/L
5.0
ND
06/09/97
1,2-Dichloroethane
ug/L
5.0
ND
06/09/97
Carbon tetrachloride
ug/L
5.0
ND
06/09/97
Benzene
ug/L
5.0
16
06/09/97
Trichloroethene
ug/L
5.0
5.0
06/09/97
1,2-Dichloropropane
ug/L
5.0
ND
06/09/97
Dibromomethane
ug/L
5.0
ND
06/09/97
Bromodichloromethane
ug/L
5.0
ND
06/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
81
06/09/97
cis-1,3-Dichloropropene
ug/L
5.0
ND
06/09/97
Toluene
ug/L
5.0
110
06/09/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
ND
06/09/97
1,1,2-Trichloroethane
ug/L
5.0
ND
06/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Anaixtical Asheville, NG 28801
Tel: [phone]
Fax: [phone]
June 11, 1997
Pag 6 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
PACE Sample Number:
93 0399193
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
DOT MW#C
Parameter
Units
PRL
METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
2-Hexanone
ug/L
50
NO
06/09/97
Dibromochloromethane
ug/L
5.0
NO
06/09/97
Tetrachlorioethylene
ug/L
5.0
7.6
06/09/97
1,2-Dibromoethane
ug/L
5.0
NO
06/09/97
Chlorobenzene
ug/L
5.0
NO
06/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
06/09/97
Ethylbenzene
ug/L
5.0
33
06/09/97
Xylenes, (total)
ug/L
5.0
230
06/09/97
Styrene
ug/L
5.0
NO
06/09/97
Bromoform
ug/L
5.0
NO
06/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
NO
06/09/97
1,2,3-Trichloropropane
ug/L
5.0
NO
06/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
06/09/97
1,4-Dichlorobenzene
ug/L
5.0
34
06/09/97
1,2-Dichlorobenzene
ug/L
5.0
6.6
06/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
06/09/97
Surrogate - Dibromofluoromethane
%
100
06/09/97
Surrogate - Toluene-d8
%
107
06/09/97
Surrogate - 4-Bromofluorobenzene
%
104
06/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Anay-tical Services, I nc.
54 Ravenscroft Drive
Pace Analytocal
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
June
11, 1997
Pag 7
PACE
Project Number: A70529601
Client Reference: McDowell Co. Landfill
PACE Sample Number:
93 0399207
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
DOT MW#D
Parameter
Units
PRL
METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
NO
06/09/97
Chloroethene (Vinyl chloride)
ug/L
10
NO
06/09/97
Bromomethane
ug/L
10
NO
06/09/97
Chloroethane
ug/L
10
NO
06/09/97
Trichlorofluoromethane
ug/L
5.0
NO
06/09/97
Acetone
ug/L
500
1700
06/09/97
1,1-Dichloroethene
ug/L
5.0
NO
06/09/97
Methyl iodide
ug/L
5.0
NO
06/09/97
Acrylonitrile
ug/L
100
NO
06/09/97
Dichloromethane
ug/L
5.0
8.6
06/09/97
Carbon disulfide
ug/L
5.0
6.0
06/09/97
trans-1,2-Dichloroethene
ug/L
5.0
NO
06/09/97
1,1-Dichloroethane
ug/L
5.0
7.4
06/09/97
Vinyl acetate
ug/L
50
NO
06/09/97
Methyl ethyl ketone
ug/L
500
2400
06/09/97
cis-1,2-Dichloroethene
ug/L
5.0
170
06/09/97
Chloroform
ug/L
5.0
NO
06/09/97
Bromochloromethane
ug/L
5.0
NO
06/09/97
1,1,1-Trichloroethane
ug/L
5.0
ND
06/09/97
1,2-Dichloroethane
ug/L
5.0
NO
06/09/97
Carbon tetrachloride
ug/L
5.0
NO
06/09/97
Benzene
ug/L
5.0
15
06/09/97
Trichloroethene
ug/L
5.0
ND
06/09/97
1,2-Dichloropropane
ug/L
5.0
NO
06/09/97
Dibromomethane
ug/L
5.0
NO
06/09/97
Bromodichloromethane
ug/L
5.0
NO
06/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
160
06/09/97
cis-1,3-Dichloropropene
ug/L
5.0
ND
06/09/97
Toluene
ug/L
5.0
66
06/09/97
trans-1,3-Dichlora-l-propene
ug/L
5.0
ND
06/09/97
1,1,2-Trichloroethane
ug/L
5.0
ND
06/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Favenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
June 11, 1997
Page 8 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
PACE Sample Number: 93 0399207
Date Collected: 05/29/97
Date Received: 05/29/97
Client Sample ID: DOT MW#D
Parameter Units PRL METHOD DATE ANALYZED
WIT0.1 WIRIV:
APPENDIX I, LANDFILL VOLATILES
8260
2-Hexanone
ug/L
50
NO
06/09/97
Dibromochloromethane
ug/L
5.0
ND
06/09/97
Tetrachloroethylene
ug/L
5.0
NO
06/09/97
1,2-Dibromoethane
ug/L
5.0
ND
06/09/97
Chlorobenzene
ug/L
5.0
ND
06/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
06/09/97
Ethylbenzene
ug/L
5.0
18
06/09/97
Xylenes, (total)
ug/L
5.0
110
06/09/97
Styrene
ug/L
5.0
NO
06/09/97
Bromoform
ug/L
5.0
NO
06/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
06/09/97
1,2,3-Trichloropropane
ug/L
5.0
ND
06/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
06/09/97
1,4-Dichlorobenzene
ug/L
5.0
19
06/09/97
1,2-Dichlorobenzene
ug/L
5.0
ND
06/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
06/09/97
Surrogate - Dibromofluoromethane
%
99
06/09/97
Surrogate - Toluene-d8
%
102
06/09/97
Surrogate - 4-Bromofluorobenzene
%
98
06/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC �8801
Tel: [phone]F
Fax: [phone]
June 11, 1997
Page 9 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
PACE Sample Number:
93 0399215
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
Travel
Parameter
Units
PRL
Blank METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
NO
06/09/97
Chloroethene (Vinyl chloride)
ug/L
10
NO
06/09/97
Bromomethane
ug/L
10
NO
06/09/97
Chloroethane
ug/L
10
NO
06/09/97
Trichlorofluoromethane
ug/L
5.0
NO
06/09/97
Acetone
ug/L
100
NO
06/09/97
1,1-Dichloroethene
ug/L
5.0
NO
06/09/97
Methyl iodide
ug/L
5.0
NO
06/09/97
Acrylonitrile
ug/L
100
NO
06/09/97
Dichloromethane
ug/L
5.0
NO
06/09/97
Carbon disulfide
ug/L
5.0
NO
06/09/97
trans-1,2-Dichloroethene
ug/L
5.0
NO
06/09/97
1,1-Dichloroethane
ug/L
5.0
NO
06/09/97
Vinyl acetate
ug/L
50
NO
06/09/97
Methyl ethyl ketone
ug/L
100
NO
06/09/97
cis-1,2-Dichloroethene
ug/L
5.0
NO
06/09/97
Chloroform
ug/L
5.0
NO
06/09/97
Bromochloromethane
ug/L
5.0
NO
06/09/97
1,1,1-Trichloroethane
ug/L
5.0
ND
06/09/97
1,2-Dichloroethane
ug/L
5.0
NO
06/09/97
Carbon tetrachloride
ug/L
5.0
NO
06/09/97
Benzene
ug/L
5.0
NO
06/09/97
Trichloroethene
ug/L
5.0
ND
06/09/97
1,2-Dichloropropane
ug/L
5.0
NO
06/09/97
Dibromomethane
ug/L
5.0
NO
06/09/97
Bromodichloromethane
ug/L
5.0
NO
06/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
06/09/97
cis-1,3-Dichloropropene
ug/L
5.0
NO
06/09/97
Toluene
ug/L
5.0
ND
06/09/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
06/09/97
1,1,2-Trichlaroethane
ug/L
5.0
ND
06/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wriften consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal
Asheville, NC 28801
Tel: [phone]F
Fax: [phone]
June
11, 1997
Page 10
PACE
Project Number: A70529601
Client Reference: McDowell Co. Landfill
PACE Sample Number:
93 0399215
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
Travel
Parameter
Units
PRL
Blank
METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
2-Hexanone
ug/L
50
ND
06/09/97
Dibromochloromethane
ug/L
5.0
ND
06/09/97
Tetrachloroethylene
ug/L
5.0
ND
06/09/97
1,2-Dibromoethane
ug/L
5.0
ND
06/09/97
Chlorobenzene
ug/L
5.0
ND
06/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
06/09/97
Ethylbenzene
ug/L
5.0
ND
06/09/97
Xylenes, (total)
ug/L
5.0
ND
06/09/97
Styrene
ug/L
5.0
ND
06/09/97
Bromoform
ug/L
5.0
ND
06/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
06/09/97
1,2,3-Trichloropropane
ug/L
5.0
ND
06/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
06/09/97
1,4-Dichlorobenzene
ug/L
5.0
ND
06/09/97
1,2-Dichlorobenzene
ug/L
5.0
ND
06/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
06/09/97
Surrogate - Dibromofluoromethane
%
101
06/09/97
Surrogate - Toluene-d8
%
102
06/09/97
Surrogate - 4-Bromofluorobenzene
%
100
06/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
June 11, 1997
Page I I PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
PACE Sample Number: 93 0399223
Date Collected: 05/29/97
Date Received: 05/29/97
Client Sample ID: Equipment
Blank
Parameter Units PRL Bailer A METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
NO
06/09/97
Chloroethene (Vinyl chloride)
ug/L
10
NO
06/09/97
Bromomethane
ug/L
10
NO
06/09/97
Chloroethane
ug/L
10
NO
06/09/97
Trichlorofluoromethane
ug/L
5.0
NO
06/09/97
Acetone
ug/L
100
NO
06/09/97
1,1-Dichloroethene
ug/L
5.0
NO
06/09/97
Methyl iodide
ug/L
5.0
NO
06/09/97
Acrylonitrile
ug/L
100
NO
06/09/97
Dichloromethane
ug/L
5.0
ND
06/09/97
Carbon disulfide
ug/L
5.0
NO
06/09/97
trans-1,2-Dichloroethene
ug/L
5.0
NO
06/09/97
1,1-Dichloroethane
ug/L
5.0
ND
06/09/97
Vinyl acetate
ug/L
50
NO
06/09/97
Methyl ethyl ketone
ug/L
100
NO
06/09/97
cis-1,2-Dichloroethene
ug/L
5.0
NO
06/09/97
Chloroform
ug/L
5.0
NO
06/09/97
Bromochloromethane
ug/L
5.0
IND
06/09/97
1,1,1-Trichloroethane
ug/L
5.0
NO
06/09/97
1,2-Dichloroethane
ug/L
5.0
ND
06/09/97
Carbon tetrachloride
ug/L
5.0
ND
06/09/97
Benzene
ug/L
5.0
NO
06/09/97
Trichloroethene
ug/L
5.0
NO
06/09/97
1,2-Dichloropropane
ug/L
5.0
NO
06/09/97
Dibromomethane
ug/L
5.0
NO
06/09/97
Bromodichloromethane
ug/L
5.0
NO
06/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
IND
06/09/97
cis-1,3-Dichloropropene
ug/L
5.0
NO
06/09/97
Toluene
ug/L
5.0
NO
06/09/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
06/09/97
1,1,2-Trichloroethane
ug/L
5.0
ND
06/09/97
REPORT OF
LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written
consent of Pace Analytical Services,
Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
June 11, 1997
ag PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
PACE Sample Number: 93 0399223
Date Collected: 05/29/97
Date Received: 05/29/97
Client Sample ID: Equipment
Blank
Parameter Units PRL Bailer A METHOD DATE ANALYZED
A r
'114.11 � 110.111! fil wills&,
APPENDIX I, LANDFILL VOLATILES
8260
2-Hexanone
ug/L
50
NO
06/09/97
Dibromochloromethane
ug/L
5.0
NO
06/09/97
Tetrachloroethylene
ug/L
5.0
NO
06/09/97
1,2-Dibromoethane
ug/L
5.0
NO
06/09/97
Chlorobenzene
ug/L
5.0
ND
06/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
06/09/97
Ethylbenzene
ug/L
5.0
NO
06/09/97
Xylenes, (total)
ug/L
5.0
NO
06/09/97
Styrene
ug/L
5.0
ND
06/09/97
Bromoform
ug/L
5.0
NO
06/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
NO
06/09/97
1,2,3-Trichloropropane
ug/L
5.0
NO
06/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
06/09/97
1,4-Dichlorobenzene
ug/L
5.0
NO
06/09/97
1,2-Dichlorobenzene
ug/L
5.0
NO
06/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
06/09/97
Surrogate - Dibromofluoromethane
%
98
06/09/97
Surrogate - Toluene-d8
%
100
06/09/97
Surrogate - 4-Bromofluorobenzene
%
106
06/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NG 28801
Tel: [phone]
Fax: [phone]
FOOTNOTES June 11, 1997
Page 13 for pages I through 12 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
NO Not detected at or above the PRL.
PRL PACE Reporting Limit
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
QUALITY CONTROL DATA June 11, 1997
Page 14 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
APPENDIX I, LANDFILL VOLATILES
Batch: 92 60345
Samples: 93 0399177, 93 0399185, 93 0399193, 93 0399207, 93 0399215
93 0399223
METHOD BLANK:
Method
Parameter
Units
PRL
Blank
Methyl Chloride
Ug—/L—
T-O
NO
Chloroethene (Vinyl chloride)
ug/L
10
ND
Bromomethane
ug/L
10
NO
Chloroethane
ug/L
10
NO
Trichlorofluoromethane
ug/L
5.0
NO
Acetone
ug/L
100
ND
I,I-Dichloroethene
ug/L
5.0
ND
Methyl iodide
ug/L
5.0
NO
Acrylonitrile
ug/L
100
NO
Dichloromethane
ug/L
5.0
NO
Carbon disulfide
ug/L
5.0
ND
trans-1,2-Dichloroethene
ug/L
5.0
NO
I,I-Dichloroethane
ug/L
5.0
NO
Vinyl acetate
ug/L
50
ND
Methyl ethyl ketone
ug/L
100
NO
cis-1,2-Dichloroethene
ug/L
5.0
NO
Chloroform
ug/L
5.0
NO
Bromochloromethane
ug/L
5.0
NO
1,1,1-Trichloroethane
ug/L
5.0
NO
1,2-Dichloroethane
ug/L
5.0
NO
Carbon tetrachloride
ug/L
5.0
NO
Benzene
ug/L
5.0
NO
Trichloroethene
ug/L
5.0
NO
1,2-Dichloropropane
ug/L
5.0
NO
Dibromomethane
ug/L
5.0
NO
Bromodichloromethane
ug/L
5.0
NO
4-Methyl-2-pentanone (MIBK)
ug/L
50
NO
cis-1,3-Dichloropropene
ug/L
5.0
NO
Toluene
ug/L
5.0
ND
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
1,1,2-Trichloroethane
ug/L
5.0
ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Fax: [phone]
QUALITY CONTROL DATA June 11, 1997
Page 15 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
APPENDIX I, LANDFILL VOLATILES
Batch: 92 60345
Samples: 93 0399177, 93 0399185, 93 0399193, 93 0399207, 93 0399215
93 0399223
METHOD BLANK:
Method
Parameter
Units
PRL
Blank
2-Hexanone
Ug—/L—
5-0—
NO
Dibromochloromethane
ug/L
5.0
NO
Tetrachloroethylene
ug/L
5.0
NO
1,2-Dibromoethane
ug/L
5.0
NO
Chlorobenzene
ug/L
5.0
NO
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
Ethylbenzene
ug/L
5.0
NO
Xylenes, (total)
ug/L
5.0
NO
Styrene
ug/L
5.0
NO
Bromoform
ug/L
5.0
NO
1,1,2,2-Tetrachloroethane
ug/L
5.0
NO
1,2,3-Trichloropropane
ug/L
5.0
NO
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
1,4-Dichlorobenzene
ug/L
5.0
NO
1,2-Dichlorobenzene
ug/L
5.0
NO
1,2-Dibromo-3-chloropropane
ug/L
5.0
NO
Surrogate - Dibromofluoromethane
%
104
Surrogate - Toluene-d8
%
105
Surrogate - 4-Bromofluorobenzene
%
99
SPIKE AND SPIKE DUPLICATE:
Spi ke
Spike
Dupl
Parameter
Units
PRL
920104234
Spike
Recv
Recv
RPD
APPENDIX I, LANDFILL VOLATILES
(1)
Methyl Chloride
ug/L
10
ND
50
90%
94%
4%
Chloroethene (Vinyl chloride)
ug/L
10
NO
50
94%
98%
4%
Bromomethane
ug/L
10
NO
50
94%
94%
0%
Chloroethane
ug/L
10
ND
50
96%
96%
0%
Trichlorofluoromethane
ug/L
5.0
ND
50
102%
98%
4%
Acetone
ug/L
100
NO
100
90%
93%
3%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NG 28801
Tel: [phone]
Fax: [phone]
QUALITY CONTROL DATA June 11, 1997
Page 16 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
APPENDIX 1, LANDFILL VOLATILES
Batch: 92 60345
Samples: 93 0399177, 93 0399185, 93 0399193, 93 0399207, 93 0399215
93 0399223
SPIKE AND SPIKE DUPLICATE:
Spike
Spike
Dupl
Parameter
Units
PRL
920104234
Recv
Recv
RPD
APPENDIX I, LANDFILL VOLATILES
(1)
I,I-Dichloroethene
ug/L
5.0
NO
50
102%
100%
2%
Methyl iodide
ug/L
5.0
NO
100
96%
99%
3%
Acrylonitrile
ug/L
100
NO
500
85%
85%
0%
Dichloromethane
ug/L
5.0
ND
50
88%
86%
2%
Carbon disulfide
ug/L
5.0
NO
100
101%
100%
1%
trans-1,2-Dichloroethene
ug/L
5.0
NO
50
96%
94%
2%
1,1-Dichloroethane
ug/L
5.0
ND
50
102%
104%
2%
Vinyl acetate
ug/L
50
NO
100
54%
54%
0%
Methyl ethyl ketone
ug/L
100
NO
100
72%
92%
24%
cis-1,2-Dichloroethene
ug/L
5.0
NO
50
106%
102%
4%
Chloroform
ug/L
5.0
NO
50
104%
108%
4%
Bromochloromethane
ug/L
5.0
NO
50
102%
102%
0%
1,1,1-Trichloroethane
ug/L
5.0
NO
50
106%
102%
4%
1,2-Dichloroethane
ug/L
5.0
NO
50
108%
108%
0%
Carbon tetrachloride
ug/L
5.0
ND
50
104%
110%
6%
Benzene
ug/L
5.0
ND
50
106%
112%
6%
Trichloroethene
ug/L
5.0
NO
50
110%
114%
4%
1,2-Dichloropropane
ug/L
5.0
NO
50
114%
116%
2%
Dibromomethane
ug/L
5.0
NO
50
96%
100%
4%
Bromodichloromethane
ug/L
5.0
NO
50
96%
100%
4%
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
100
91%
98%
7%
cis-1,3-Dichloropropene
ug/L
5.0
ND
50
96%
98%
2%
Toluene
ug/L
5.0
ND
50
104%
108%
4%
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
50
92%
98%
6%
1,1,2-Trichloroethane
ug/L
5.0
ND
50
102%
104%
2%
2-Hexanone
ug/L
50
NO
100
86%
95%
10%
Dibromochloromethane
ug/L
5.0
ND
50
96%
100%
4%
Tetrachloroethylene
ug/L
5.0
ND
50
100%
108%
8%
1,2-Dibromoethane
ug/L
5.0
ND
50
96%
100%
4%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
ToL 704-254-7176
Fax: [phone]
QUALITY CONTROL DATA June 11, 1997
Page 17 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
APPENDIX 1, LANDFILL VOLATILES
Batch: 92 60345
Samples: 93 0399177, 93 0399185, 93 0399193, 93 0399207, 93 0399215
93 0399223
SPIKE AND SPIKE DUPLICATE:
Spike
Spike
Dupl
Parameter
Units
PRL
920104234
Recy
Recv
RPD
APPENDIX 1, LANDFILL VOLATILES
(1)
Chlorobenzene
ug/L
5.0
NO
50
104%
108%
4%
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
50
108%
108%
0%
Ethylbenzene
ug/L
5.0
NO
50
106%
114%
7%
Xylenes, (total)
ug/L
5.0
NO
150
107%
113%
5%
Styrene
ug/L
5.0
NO
50
104%
104%
0%
Bromoform
ug/L
5.0
NO
50
80%
84%
5%
1,1,2,2-Tetrachloroethane
ug/L
5.0
NO
50
88%
100%
13%
1,2,3-Trichloropropane
ug/L
5.0
NO
50
92%
104%
12%
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
50
68%
72%
6%
1,4-Dichlorobenzene
ug/L
5.0
NO
50
102%
100%
2%
1,2-Dichlorobenzene
ug/L
5.0
NO
50
100%
100%
0%
1,2-Dibromo-3-chloropropane
ug/L
5.0
NO
50
84%
86%
2%
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
PRL
Value
Recv
Methyl Chloride
iig—/ L—
Tro
20
95%
Chloroethene (Vinyl chloride)
ug/L
10
20
90%
Bromomethane
ug/L
10
20
110%
Chl oroethane
ug/L
10
20
105%
Trichlorofluoromethane
ug/L
5.0
20
100%
Acetone
ug/L
100
40
110%
I,I-Dichloroethene
ug/L
5.0
20
105%
Methyl iodide
ug/L
5.0
40
93%
Acrylonitrile
ug/L
100
200
110%
Dichloromethane
ug/L
5.0
20
95%
Carbon disulfide
ug/L
5.0
40
105%
trans-1,2-Dichloroethene
ug/L
5.0
20
100%
I,I-Dichloroethane
ug/L
5.0
20
105%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical SeNices, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
QUALITY CONTROL DATA June 11, 1997
e 18 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
APPENDIX I, LANDFILL VOLATILES
Batch: 92 60345
Samples: 93 0399177, 93 0399185, 93 0399193, 93 0399207, 93 0399215
93 0399223
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
PRL
Value
Recv
Vinyl ac�tate
u—g/—L
wo
40
60%
Methyl ethyl ketone
ug/L
100
40
105%
cis-1,2-Dichloroethene
ug/L
5.0
20
105%
Chloroform
ug/L
5.0
20
105%
Bromochloromethane
ug/L
5.0
20
100%
1,1,1-Trichloroethane
ug/L
5.0
20
105%
1,2-Dichloroethane
ug/L
5.0
20
110%
Carbon tetrachloride
ug/L
5.0
20
95%
Benzene
ug/L
5.0
20
105%
Trichloroethene
ug/L
5.0
20
105%
1,2-Dichloropropane
ug/L
5.0
20
110%
Dibromomethane
ug/L
5.0
20
95%
Bromodichloromethane
ug/L
5.0
20
95%
4-Methyl-2-pentanone (MIBK)
ug/L
50
40
105%
cis-1,3-Dichloropropene
ug/L
5.0
20
95%
Toluene
ug/L
5.0
20
100%
trans-1,3-Dichloro-l-propene
ug/L
5.0
20
95%
1,1,2-Trichloroethane
ug/L
5.0
20
100%
2-Hexanone
ug/L
50
40
103%
Dibromochloromethane
ug/L
5.0
20
90%
Tetrachloroethylene
ug/L
5.0
20
100%
1,2-Dibromoethane
ug/L
5.0
20
95%
Chlorobenzene
ug/L
5.0
20
100%
1,1,1,2-Tetrachloroethane
ug/L
5.0
20
100%
Ethylbenzene
ug/L
5.0
20
100%
Xylenes, (total)
ug/L
5.0
60
103%
Styrene
ug/L
5.0
20
100%
Bromoform
ug/L
5.0
20
85%
1,1,2,2-Tetrachloroethane
ug/L
5.0
20
95%
1,2,3-Trichloropropane
ug/L
5.0
20
100%
trans-1,4-Dichloro-2-butene
ug/L
5.0
20
80%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NG 28801
Fax: [phone]
QUALITY CONTROL DATA June 11, 1997
ge 19 PACE Project Number: A70529601
Client Reference: McDowell Co. Landfill
APPENDIX I, LANDFILL VOLATILES
Batch: 92 60345
Samples: 93 0399177, 93 0399185, 93 0399193, 93 0399207, 93 0399215
93 0399223
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
PRL
Value
Recv
1,4-Dichlorobenzene
U-971
570-
20
105%
1,2-Dichlorobenzene
ug/L
5.0
20
105%
1,2-Dibromo-3-chloropropane
ug/L
5.0
20
85%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
FOOTNOTES
Page 20 for pages 14 through 19
Client Reference: McDowell Co. Landfill
NO Not detected at or above the PRL.
PRL PACE Reporting Limit
RPD Relative Percent Difference
(1) Analyzed 10 minutes outside tune time.
Tel: [phone]
Fax: [phone]
June 11, 1997
PACE Project Number: A70529601
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

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Pace Analytical Services, Inc.
54 Savenscroft Drive
Asheville, NC 28801
June 12, 1997
McDowell County Landfill
10 East Court Street
Marion, NC 28752
RE: PACE Project No. A70529.600
Client Reference: Landfill Monitoring Wells
Dear Mr. Silver:
Enclosed is the report of laboratory analyses for samples received
May 29, 1997.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
Walter L. Miller
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Tel: [phone]
Fax: [phone]

41 1
Pace Analytical Services, Inc
54 Ravenscroft Drive
Pace Analytical Asheville, NC 28801
Tel: [phone]F
Fax: [phone]
McDowell County Landfill
June
12, 1997
10 East Court Street
PACE
Project Number: A70529600
Marion, NC 28752
Attn: 49010sm
Client Reference: Landfill Monitoring Wells
PACE Sample NUmber:
93 0399118
93 0399126
93 0399134
Date Collected:
05/29/97
05/29/97
05/29/97
Date Received:
05/29/97
05/29/97
05/29/97
Client Sample ID:
Landfill
Landfill
Landfill
Parameter Units
PRL MW I
MW 2
MW 3
FIELD ANALYSIS
INDIVIDUAL PARAMETERS
Depth to Water
feet
0.01
15.62
34.95
35.48
Specific Conductivity (Field)
uti
10
31
410
240
Temperature (Field)
Degrees C
0.5
15
16
16
pH (Field)
Units
0.1
5.3
4.2
5.2
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Antimony
mg/L
0.004
ND
ND
ND
Arsenic
mg/L
0.005
ND
ND
ND
Barium
mg/L
0.10
0.21
0.16
0.29
Beryllium
mg/L
0.002
ND
ND
ND
Cadmium
mg/L
0.001
ND
ND
ND
Chromium
mg/L
0.001
0.003
0.002
0.001
Cobalt
mg/L
0.010
ND
0.022
0.014
Copper
mg/L
0.01
0.02
0.03
0.03
Lead
mg/L
0.005
0.010
0.006
ND
Nickel
mg/L
0.05
ND
ND
ND
Selenium
mg/L
0.005
ND
ND
ND
Silver
mg/L
0.001
ND
ND
ND
Thallium
mg/L
0.002
ND
ND
ND
Vanadium
mg/L
0.040
ND
ND
ND
Zinc
mg/L
0.01
0.05
0.03
0.03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Page 2
Client Reference: Landfill Monitoring Wells
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
D--+—
FIELD ANALYSIS
INDIVIDUAL PARAMETERS
Units PRL
Fax: [phone]
June 12, 1997
PACE Project Number: A70529600
93 0399142 93 0399169
05/29/97 05/29/97
05/29/97 05/29/97
Landfill Equipment
MW 4 Blank
Bailer Al
Depth to Water
feet
0.01
17.13
-
Specific Conductivity (Field)
umhos/cm2
10
60
-
Temperature (Field)
Degrees C
0.5
15
-
PH (Field)
Units
0.1
4.1
-
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Antimony
mg/L
0.004
NO
NO
Arsenic
mg/L
0.005
NO
ND
Barium
mg/L
0.10
0.31
NO
Beryllium
mg/L
0.002
ND
ND
Cadmium
mg/L
0.001
NO
NO
Chromium
mg/L
0.001
ND
ND
Cobalt
mg/L
0.010
NO
NO
Copper
mg/L
0.01
0.02
ND
Lead
mg/L
0.005
NO
NO
Nickel
mg/L
0.05
NO
ND
Selenium
mg/L
0.005
NO
NO
Silver
mg/L
0.001
ND
NO
Thallium
mg/L
0.002
ND
NO
Vanadium
mg/L
0.040
NO
ND
Zinc
mg/L
0.01
0.02
NO
These data have been reviewed and are approved for release.
Walter L. Miller
Operations Manager
14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
FOOTNOTES
Page 3 for pages I through 2
Client Reference: Landfill Monitoring Wells
NO Not detected at or above the PRL.
PRL PACE Reporting Limit
Tel: [phone]
Fax: [phone]
June 12, 1997
PACE Project Number: A70529600
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NG 28801
Tel: [phone]
Fax: [phone]
McDowell County Landfill June 11, 1997
10 East Court Street PACE Project Number: A70529600
Marion, NC 28752
Attn:
Client Reference: McDowell Co. Landfill
PACE Sample Number:
93 0399118
Date Collected:
05/29/97
Date Received:
05/29/97
Landfill
Parameter
Units
PRL
MW1 METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
ND
06/08/97
Chloroethene (Vinyl chloride)
ug/L
10
ND
06/08/97
Bromomethane
ug/L
10
IND
06/08/97
Chloroethane
ug/L
10
ND
06/08/97
Trichlorofluoromethane
ug/L
5.0
ND
06/08/97
Acetone
ug/L
100
ND
06/08/97
1,1-Dichloroethene
ug/L
5.0
ND
06/08/97
Methyl iodide
ug/L
5.0
ND
06/08/97
Acrylonitrile
ug/L
100
ND
06/08/97
Dichloromethane
ug/L
5.0
ND
06/08/97
Carbon disulfide
ug/L
5.0
ND
06/08/97
trans-1,2-Dichloroethene
ug/L
5.0
ND
06/08/97
I,I-Dichloroethane
ug/L
5.0
ND
06/08/97
Vinyl acetate
ug/L
50
ND
06/08/97
Methyl ethyl ketone
ug/L
100
ND
06/08/97
cis-1,2-Dichloroethene
ug/L
5.0
IND
06/08/97
Chloroform
ug/L
5.0
ND
06/08/97
Bromochloromethane
ug/L
5.0
ND
06/08/97
1,1,1-Trichloroethane
1
5.0
ND
06/08/97
1,2-Dichloroethane
ug/L
5.0
ND
06/08/97
Carbon tetrachloride
ug/L
5.0
ND
06/08/97
Benzene
ug/L
5.0
ND
06/08/97
Trichloroethene
ug/L
5.0
ND
06/08/97
1,2-Dichloropropane
ug/L
5.0
ND
06/08/97
Dibromomethane
ug/L
5.0
ND
06/08/97
Bromodichloromethane
ug/L
5.0
ND
06/08/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
IND
06/08/97
cis-1,3-Dichloropropene
ug/L
5.0
ND
06/08/97
Toluene
ug/L
5.0
ND
06/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
June
11, 1997
Page 12
PACE
Project Number: A70529600
Client Reference: McDowell Co. Landfill
PACE Sample Number:
93 0399118
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
Landfill
Parameter
Units
PRL
MW1
METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
trans-1,3-Dichloro-l-propene
ug/L
5.0
ND
06/08/97
1,1,2-Trichloroethane
ug/L
5.0
ND
06/08/97
2-Hexanone
ug/L
50
ND
06/08/97
Dibromochloromethane
ug/L
5.0
ND
06/08/97
Tetrachloroethylene
ug/L
5.0
ND
06/08/97
1,2-Dibromoethane
ug/L
5.0
ND
06/08/97
Chlorobenzene
ug/L
5.0
ND
06/08/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
06/08/97
Ethylbenzene
ug/L
5.0
ND
06/08/97
Xylenes, (total)
ug/L
5.0
ND
06/08/97
Styrene
ug/L
5.0
ND
06/08/97
Bromoform
ug/L
5.0
ND
06/08/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
06/�08/97
1,2,3-Trichloropropane
ug/L
5.0
ND
06/08/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
06/08/97
1,4-Dichlorobenzene
ug/L
5.0
ND
06/08/97
1,2-Dichlorobenzene
ug/L
5.0
ND
06/08/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
06/08/97
Surrogate - Dibromofluoromethane
%
96
06/08/97
Surrogate - Toluene-d8
%
104
06/08/97
Surrogate - 4-Bromofluorobenzene
%
100
06/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
June
11, 1997
Page 3
PACE
Project Number: A70529600
Client Reference: McDowell Co.
Landfill
PACE Sample Number:
93 0399126
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
Landfill
Parameter
Units
PRL
MW2
METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
ND
06/08/97
Chloroethene (Vinyl chloride)
ug/L
10
ND
06/08/97
Bromomethane
ug/L
10
ND
06/08/97
Chloroethane
ug/L
10
ND
06/08/97
Trichlorofluoromethane
ug/L
5.0
ND
06/08/97
Acetone
ug/L
100
ND
06/08/97
1,1-Dichloroethene
ug/L
5.0
ND
06/08/97
Methyl iodide
ug/L
5.0
ND
06/08/97
Acrylonitrile
ug/L
100
ND
06/08/97
Dichloromethane
ug/L
5.0
ND
06/08/97
Carbon disulfide
ug/L
5.0
8.6
06/08/97
trans-1,2-Dichloroethene
ug/L
5.0
ND
06/08/97
1,1-Dichloroethane
ug/L
5.0
9.8
06/'08/97
Vinyl acetate
ug/L
50
ND
06/08/97
Methyl ethyl ketone
ug/L
100
ND
06/08/97
cis-1,2-Dichloroethene
ug/L
5.0
83
06/08/97
Chloroform
ug/L
5.0
ND
06/08/97
Bromochloromethane
ug/L
5.0
ND
06/08/97
1,1,1-Trichloroethane
ug/L
5.0
ND
06/08/97
1,2-Dichloroethane
ug/L
5.0
ND
06/08/97
Carbon tetrachloride
ug/L
5.0
ND
06/08/97
Benzene
ug/L
5.0
16
06/08/97
Trichloroethene
ug/L
5.0
ND
06/08/97
1,2-Dichloropropane
ug/L
5.0
ND
06/08/97
Dibromomethane
ug/L
5.0
ND
06/08/97
Bromodichloromethane
ug/L
5.0
ND
06/08/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
06/08/97
cis-1,3-Dichloropropene
ug/L
5.0
ND
06/08/97
Toluene
ug/L
5.0
11
06/08/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
ND
06/08/97
1,1,2-Trichloroethane
ug/L
5.0
ND
06/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
June
11, 1997
Page 4
PACE
Project Number: A70529600
Client Reference: McDowell Co. Landfill
PACE Sample Number:
93 0399126
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
Landfill
Parameter
Units
PRL
MW2
METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
2-Hexanone
ug/L
50
ND
06/08/97
Dibromochloromethane
ug/L
5.0
ND
06/08/97
Tetrachloroethylene
ug/L
5.0
ND
06/08/97
1,2-Dibromoethane
ug/L
5.0
ND
06/08/97
Chlorobenzene
ug/L
5.0
24
06/08/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
06/08/97
Ethylbenzene
ug/L
5.0
ND
06/08/97
Xylenes, (total)
ug/L
5.0
31
06/08/97
Styrene
ug/L
5.0
ND
06/08/97
Bromoform
ug/L
5.0
ND
06/08/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
06/08/97
1,2,3-Trichloropropane
ug/L
5.0
IND
06/08/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
06/*08/97
1,4-Dichlorobenzene
ug/L
5.0
8.3
06/08/97
1,2-Dichlorobenzene
ug/L
5.0
IND
06/08/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
06/08/97
Surrogate - Dibromofluoromethane
%
99
06/08/97
Surrogate - Toluene-d8
%
103
06/08/97
Surrogate - 4-Bromofluorobenzene
%
98
06/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytical
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
June
11, 1997
age
PACE
Project Number: A70529600
Client Reference: McDowell Co.
Landfill
PACE Sample Number:
93 0399134
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
Landfill
Parameter
Units
PRL
MW3
METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
ND
06/08/97
Chloroethene (Vinyl chloride)
ug/L
10
ND
06/08/97
Bromomethane
ug/L
10
ND
06/08/97
Chloroethane
ug/L
10
ND
06/08/97
Trichlorofluoromethane
ug/L
5.0
ND
06/08/97
Acetone
ug/L
100
ND
06/08/97
1,1-Dichloroethene
ug/L
5.0
ND
06/08/97
Methyl iodide
ug/L
5.0
ND
06/08/97
Acrylonitrile
ug/L
100
ND
06/08/97
Dichloromethane
ug/L
5.0
ND
06/08/97
Carbon disulfide
ug/L
5.0
ND
06/08/97
trans-1,2-Dichloroethene
ug/L
5.0
ND
06/08/97
1,1-Dichloroethane
ug/L
5.0
ND
06/08/97
Vinyl acetate
ug/L
50
ND
06/08/97
Methyl ethyl ketone
ug/L
100
ND
06/08/97
cis-1,2-Dichloroethene
ug/L
5.0
ND
06/08/97
Chloroform
ug/L
5.0
ND
06/08/97
Bromochloromethane
ug/L
5.0
ND
06/08/97
1,1,1-Trichloroethane
ug/L
5.0
ND
06/08/97
1,2-Dichloroethane
ug/L
5.0
ND
06/08/97
Carbon tetrachloride
ug/L
5.0
ND
06/08/97
Benzene
ug/L
5.0
ND
06/08/97
Trichloroethene
ug/L
5.0
ND
06/08/97
1,2-Dichloropropane
ug/L
5.0
ND
06/08/97
Dibromomethane
ug/L
5.0
ND
06/08/97
Bromodichloromethane
ug/L
5.0
ND
06/08/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
06/08/97
cis-1,3-Dichloropropene
ug/L
5.0
ND
06/08/97
Toluene
ug/L
5.0
ND
06/08/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
ND
06/08/97
1,1,2-Trichloroethane
ug/L
5.0
ND
06/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical SeNices, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Fax: [phone]
age 6
June
11, 1997
PACE
Project Number: A70529600
Client Reference: McDowell Co. Landfill
PACE Sample Number:
93 0399134
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
Landfill
Parameter
Units
PRL
MW3
METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
2-Hexanone
Dibromochloromethane
ug/L
ug/L
50
5.0
ND
ND
06/08/97
Tetrachloroethylene
ug/L
5.0
ND
06/08/97
06 08/97
1,2-Dibromoethane
Chlorobenzene
ug/L
5.0
ND
06/08/97
1,1,1,2-Tetrachloroethane
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
06/08/97
Ethylbenzene
Xylenes, (total)
ug/L
5.0
ND
06/08/97
Styrene
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
Bromoform
ug/L
5.0
ND
06/08/97
06 08/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
06/08/97
1,2,3-Trichloropropane
ug/L
5.0
ND
06/08/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
06/08/97
1,4-Dichlorobenzene
1,2-Dichlorobenzene
ug/L
5.0
ND
06/08/97
1,2-Dibromo-3-chlaropropane
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
Surrogate - Dibromofluoromethane
%
101
06/08/97
06/08/97
Surrogate - Toluene-d8
%
105
06/08/97
Surrogate - 4-Bromofluorobenzene
%
100
06/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville. NC 28801
Tel: [phone]
Fax: [phone]
June 11, 1997
Page 7 PACE Project Number: A70529600
Client Reference: McDowell Co. Landfill
PACE Sample Number:
93 0399142
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
Landfill
Parameter
Units
PRL
MW4 METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
NO
06/08/97
Chloroethene (Vinyl chloride)
ug/L
10
NO
06/08/97
Bromomethane
ug/L
10
NO
06/08/97
Chloroethane
ug/L
10
NO
06/08/97
Trichlorofluoromethane
ug/L
5.0
NO
06/08/97
Acetone
ug/L
100
NO
06/08/97
1,1-Dichloroethene
ug/L
5.0
NO
06/08/97
Methyl iodide
ug/L
5.0
NO
06/08/97
Acrylonitrile
ug/L
100
NO
06/08/97
Dichloromethane
ug/L
5.0
NO
06/08/97
Carbon disulfide
ug/L
5.0
NO
06/08/97
trans-1,2-Dichloroethene
ug/L
5.0
ND
06/08/97
1,1-Dichloroethane
ug/L
5.0
NO
06�08/97
Vinyl acetate
ug/L
50
NO
06/08/97
Methyl ethyl ketone
ug/L
100
ND
06/08/97
cis-1,2-Dichloroethene
ug/L
5.0
NO
06/08/97
Chloroform
ug/L
5.0
NO
06/08/97
Bromochloromethane
ug/L
5.0
NO
06/08/97
1,1,1-Trichloroethane
ug/L
5.0
NO
06/08/97
1,2-Dichloroethane
ug/L
5.0
NO
06/08/97
Carbon tetrachloride
ug/L
5.0
NO
06/08/97
Benzene
ug/L
5.0
ND
06/08/97
Trichloroethene
ug/L
5.0
NO
06/08/97
1,2-Dichloropropane
ug/L
5.0
NO
06/08/97
Dibromomethane
ug/L
5.0
NO
06/08/97
Bromodichloromethane
ug/L
5.0
ND
06/08/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
06/08/97
cis-1,3-Dichloropropene
ug/L
5.0
NO
06/08/97
Toluene
ug/L
5.0
ND
06/08/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
06/08/97
1,1,2-Trichloroethane
ug/L
5.0
NO
06/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Fax: [phone]
Page 8
June 11, 1997
PACE Project Number: A70529600
Client Reference: McDowell Co.
Landfill
PACE Sample Number:
Date Collected:
93 0399142
Date Received:
05/29/97
Client Sample ID:
05/29/97
Parameter
Units
PRL
Landfill
MW4 METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
2-Hexanone
Dibromochloromethane
ug/L
50
IND
06/08/97
Tetrachloroethylene
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
1,2-Dibromoethane
ug/L
5.0
ND
06/08/97
Chlorobenzene
ug/L
5.0
ND
06/08/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
06/08/97
06/08/97
Ethylbenzene
Xylenes, (total)
ug/L
5.0
ND
06/08/97
Styrene
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
Bromoform
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
06/08/97
06/08/97
1,2,3-Trichloropropane
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
06/08/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
IND
1,4-Dichlorobenzene
ug/L
5.0
ND
06�08/97
1,2-Dichlorobenzene
ug/L
5.0
IND
06/08/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
06/08/97
Surrogate - Dibromofluoromethane
%
101
06/08/97
Surrogate - Toluene-d8
%
104
06/08/97
06/08/97
Surrogate - 4-Bromofluorobenzene
%
104
06/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
Pace Analytocal
54 Ravenscroft Drive
Asheville, NO 28801
Tel: [phone]
Fax: [phone]
Page 9
June
11, 1997
PACE
Project Number: A70529600
Client Reference: McDowell Co.
Landfill
PACE Sample Number:
93 0399150
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
Travel
Parameter
Units
PRL
Blank
METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
Methyl Chloride
Chloroethene (Vinyl chloride)
ug/L
ug/L
10
10
ND
ND
06/08/97
Bromomethane
ug/L
10
ND
06/08/97
06/08/97
Chloroethane
Trichlorofluoromethane
ug/L
ug/L
10
5.0
ND
ND
06/08/97
Acetone
ug/L
100
ND
06/08/97
06/08/97
I,I-Dichloroethene
Methyl iodide
ug/L
5.0
ND
06/08/97
Acrylonitrile
ug/L
ug/L
5.0
100
ND
ND
06/08/97
06/08/97
Dichloromethane
Carbon disulfide
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
trans-1,2-Dichloroethene
ug/L
5.0
ND
06/08/97
06/08/97
I,I-Dichloroethane
Vinyl acetate
ug/L
5.0
ND
06/08/97
Methyl ethyl ketone
ug/L
ug/L
50
100
ND
ND
06/08/97
06/08/97
cis-1,2-Dichloroethene
ug/L
5.0
ND
06/08/97
Chloroform
Bromochloromethane
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
06/08/97
1,1,1-Trichloroethane
ug/L
5.0
ND
06/08/97
1,2-Dichloroethane
ug/L
5.0
ND
06/08/97
Carbon tetrachloride
Benzene
ug/L
5.0
ND
06/08/97
Trichloroethene
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
06/08/97
1,2-Dichloropropane
ug/L
5.0
ND
06/08/97
Dibromomethane
Bromodichloromethane
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
06/08/97
06/08/97
cis-1,3-Dichloropropene
ug/L
5.0
ND
06/08/97
Toluene
trans-1,3-Dichloro-l-propene
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
06/08/97
1,1,2-Trichloroethane
ug/L
5.0
ND
06/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Fax: [phone]
Page 0
June
11, 1997
PACE
Project Number: A70529600
Client Reference: McDowell Co.
Landfill
PACE Sample Number:
Date Collected:
93 0399150
Date Received:
05/29/97
Client Sample ID:
05/29/97
Parameter
Units
PRL
Travel
Blank
METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
2-Hexanone
Dibromochloromethane
ug/L
50
ND
06/08/97
Tetrachloroethylene
ug/L
ug/L
5.0
5.0
NO
ND
06/08/97
1,2-Dibromoethane
ug/L
5.0
NO
06/08/97
Chlorobenzene
ug/L
5.0
NO
06/08/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
06/08/97
06/08/97
Ethylbenzene
Xylenes, (total)
ug/L
5.0
NO
06/08/97
Styrene
ug/L
ug/L
5.0
5.0
NO
NO
06/08/97
Bromoform
ug/L
5.0
NO
06/08/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
NO
06/08/97
1,2,3-Trichloropropane
ug/L
5.0
ND
06/08/97
06/08/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
1,4-Dichlorobenzene
ug/L
5.0
NO
06/08/97
1,2-Dichlorobenzene
ug/L
5.0
ND
06/08/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
NO
06/08/97
Surrogate - Dibromofluoromethane
%
100
06/08/97
Surrogate - Toluene-d8
%
101
06/08/97
06/08/97
Surrogate - 4-Bromofluorobenzene
%
98
06/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Nce Anal tocal
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NG 28801
To]: 704-254-7176
Fax: [phone]
Page 11
June 11,
1997
PACE Project
Number: A70529600
Client Reference: McDowell Co. Landfill
PACE Sample Number:
93 0399169
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
Equipment
Parameter
Units
PRL
Blank
Bailer Al
METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
Methyl Chloride
Chloroethene (Vinyl chloride)
ug/L
ug/L
10
10
ND
ND
06/08/97
Bromomethane
ug/L
10
ND
06/08/97
06/08/97
Chloroethane
Trichlorofluoromethane
ug/L
ug/L
10
5.0
ND
ND
06/08/97
Acetone
ug/L
100
ND
06 08/97
06/08/97
1,1-Dichloroethene
Methyl iodide
ug/L
5.0
ND
06/08/97
Acrylonitrile
ug/L
ug/L
5.0
100
IND
ND
06/08/97
Dichloromethane
ug/L
5.0
ND
06/08/97
06/08/97
Carbon disulfide
trans-1,2-Dichloroethene
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
06/08/97
1,1-Dichloroethane
Vinyl acetate
ug/L
5.0
ND
06/08/97
Methyl ethyl ketone
ug/L
ug/L
50
100
ND
ND
06/08/97
cis-1,2-Dichloroethene
ug/L
5.0
ND
06/08/97
06/08/97
Chloroform
Bromochloromethane
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
06/08/97
1,1,1-Trichloroethane
1,2-Dichloroethane
ug/L
5.0
ND
06/08/97
Carbon tetrachloride
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
Benzene
Trichloroethene
ug/L
5.0
ND
06/08/97
06/08/97
1,2-Dichloropropane
ug/L
ug/L
5.0
5.0
IND
IND
06/08/97
06/08/97
Dibromomethane
Bromodichloromethane
ug/L
5.0
ND
06/08/97
4-Methyl-2-pentanone (MIBK)
ug/L
ug/L
5.0
50
ND
ND
06/08/97
cis-1,3-Dichloropropene
ug/L
5.0
ND
06/08/97
06/08/97
Toluene
trans-1,3-Dichloro-l-propene
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
06/08/97
1,1,2-Trichloroethane
ug/L
5.0
ND
06/08/97
REPORT OF
LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written
consent of Pace Analytical Services,
Inc.

Pace Analytocal
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Tel: [phone]'
Fax: [phone]
Page 12
June 11,
1997
PACE Project
Number: A70529600
Client Reference: McDowell Co.
Landfill
PACE Sample Number:
93 0399169
Date Collected:
05/29/97
Date Received:
05/29/97
Client Sample ID:
Equipment
Parameter
Units
PRL
Blank
Bailer Al
METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
2-Hexanone
Dibromochloromethane
ug/L
ug/L
50
5.0
IND
ND
06/08/97
Tetrachloroethylene
ug/L
5.0
ND
06 08/97
06 08/97
1,2-Dibromoethane
Chlorobenzene
ug/L
5.0
ND
06 08/97
1,1,1,2-Tetrachloroethane
ug/L
ug/L
5.0
5.0
IND
ND
06 08/97
06/08/97
Ethylbenzene
Xylenes, (total)
ug/L
5.0
ND
06/08/97
Styrene
ug/L
ug/L
5.0
5.0
IND
IND
06/08/97
Bromoform
1,1,2,2-Tetrachloroethane
ug/L
ug/L
5.0
5.0
ND
06/08/97
06 08/97
1,2,3-Trichloropropane
ug/L
5.0
ND
ND
06/08/97
06/08/97
trans-1,4-Dichloro-2-butene
1,4-Dichlorobenzene
ug/L
5.0
IND
06/08/97
1,2-Dichlorobenzene
ug/L
ug/L
5.0
5.0
ND
ND
06/08/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
06/08/97
06/08/97
Surrogate - Dibromofluoromethane
%
100
06/08/97
Surrogate - Toluene-d8
%
107
06/08/97
Surrogate - 4-Bromofluorobenzene
%
103
06/08/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Page 13
FOOTNOTES
for pages I through 12
Client Reference: McDowell Co. Landfill
ND Not detected at or above the PRL.
PRL PACE Reporting Limit
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Tel: [phone]
Fax: [phone]
June 11, 1997
PACE Project Number: A70529600

Pace Analytical Services, Inc.
54 Savenscroft Drive
Asheville, NC 28801
Page 14
QUALITY CONTROL DATA
Client Reference: McDowell Co. Landfill
Tel: [phone]
Fax: [phone]
June 11, 1997
PACE Project Number: A70529600
APPENDIX 1, LANDFILL VOLATILES
Batch: 92 60294
Samples: 93 0399118, 93 0399126, 93 0399134, 93 0399142, 93 0399150
93 0399169
METHOD BLANK:
Parameter
Units
PRL
Method
Blank
Methyl CFloride
I OF
WD--
Chloroethene (Vinyl chloride)
ug/L
10
NO
Bromomethane
ug/L
10
NO
Chloroethane
ug/L
10
NO
Trichlorofluoromethane
ug/L
5.0
NO
Acetone
ug/L
100
NO
1,1-Dichloroethene
ug/L
5.0
NO
Methyl iodide
ug/L
5.0
NO
Acrylonitrile
ug/L
100
NO
Dichloromethane
ug/L
5.0
NO
Carbon disulfide
ug/L
5.0
NO
trans-1,2-Dichloroethene
ug/L
5.0
NO
I,I-Dichloroethane
ug/L
5.0
ND
Vinyl acetate
ug/L
50
ND
Methyl ethyl ketone
ug/L
100
NO
cis-1,2-Dichloroethene
ug/L
5.0
NO
Chloroform
ug/L
5.0
NO
Bromochloromethane
ug/L
5.0
NO
1,1,1-Trichloroethane
ug/L
5.0
NO
1,2-Dichloroethane
ug/L
5.0
ND
Carbon tetrachloride
ug/L
5.0
ND
Benzene
ug/L
5.0
ND
Trichloroethene
ug/L
5.0
ND
1,2-Dichloropropane
ug/L
5.0
NO
Dibromomethane
ug/L
5.0
ND
Bromodichloromethane
ug/L
5.0
ND
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
cis-1,3-Dichloropropene
ug/L
5.0
NO
Toluene
ug/L
5.0
NO
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
1,1,2-Trichloroethane
ug/L
5.0
ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Page 15
QUALITY CONTROL DATA
Client Reference: McDowell Co. Landfill
Tel: [phone]
Fax: [phone]
June 11, 1997
PACE Project Number: A70529600
APPENDIX 1, LANDFILL VOLATILES
Batch: 92 60294
Samples: 93 0399118, 93 0399126, 93 0399134, 93 0399142, 93 0399150
93 0399169
METHOD BLANK:
Parameter
Units
PRL
Method
Blank
2-Hexanone
tTg —/L
TOT
N-D—
Dibromochloromethane
ug/L
5.0
NO
Tetrachloroethylene
ug/L
5.0
ND
1,2-Dibromoethane
ug/L
5.0
ND
Chlorobenzene
ug/L
5.0
NO
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
Ethylbenzene
ug/L
5.0
NO
Xylenes, (total)
ug/L
5.0
ND
Styrene
ug/L
5.0
ND
Bromoform
ug/L
5.0
NO
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
1,2,3-Trichloropropane
ug/L
5.0
ND
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
1,4-Dichlorobenzene
ug/L
5.0
ND
1,2-Dichlorobenzene
ug/L
5.0
ND
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
Surrogate - Dibromofluoromethane
%
102
Surrogate - Toluene-d8
%
95
Surrogate - 4-Bromofluorobenzene
%
101
SPIKE AND SPIKE DUPLICATE:
930399118
Spike
Parameter
---T-T —Moride
Units
PRL
Landfill
MW1
ke
Spike
Recv
Dupl
Recv
RPD
M et y
Chloroethene (Vinyl chloride)
ug/L
ug/L
10-
10
WD—
NO
5 OP
1-080%
—8 -471.
25%
Bromomethane
ug/L
10
NO
50
50
100%
94%
82%
88%
20%
7%
Chloroethane
Trichlorofluoromethane
ug/L
ug/L
10
5.0
NO
NO
50
100%
90%
11%
Acetone
ug/L
100
NO
50
100
102%
99%
94%
97%
8%
2%
I,I-Dichloroethene
ug/L
5.0
NO
50
98%
96%
2%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
Pace Analytocal
54 Ravenscroft
Drive
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Page 16
QUALITY CONTROL DATA
June 11, 1997
PACE Project
Number: A70529600
Client Reference: McDowell Co. Landfill
APPENDIX 1, LANDFILL VOLATILES
Batch: 92 60294
Samples: 93 0399118, 93 0399126,
93 0399134, 93
0399142,
93 0399150
93 0399169
SPIKE AND SPIKE DUPLICATE:
930399118
Spike
Parameter
Met 'iodide
Units
PRL
Landfill
MWI pi e
Spike
Recv
Dupl
Recv
RPD
YT
Acrylonitrile
ug/L
ug/L
T.—O
100
TD—
NO
100
500
—92P7.
104%
-9-61r.
100%
97.
Dichloromethane
ug/L
5.0
NO
50
88%
82%
4%
7%
Carbon disulfide
trans-1,2-Dichloroethene
ug/L
ug/L
5.0
5.0
ND
100
104%
99%
5%
1,1-Dichloroethane
ug/L
5.0
ND
NO
50
50
96%
104%
88%
96%
9%
8%
Vinyl acetate
Methyl ethyl ketone
ug/L
ug/L
50
100
NO
NO
100
58%
54%
7%
cis-1,2-Dichloroethene
ug/L
5.0
ND
100
50
112%
106%
103%
96%
8%
10%
Chloroform
Bromochloromethane
ug/L
5.0
NO
50
110%
102%
8%
1,1,1-Trichloroethane
ug/L
ug/L
5.0
5.0
NO
NO
50
50
108%
96%
12%
104%
96%
8%
1,2-Dichloroethane
Carbon tetrachloride
ug/L
5.0
ND
50
112%
100%
11%
Benzene
ug/L
5.0
ND
50
104%
96%
8%
Trichloroethene
ug/L
ug/L
5.0
5.0
NO
NO
50
50
108%
98%
10%
1,2-Dichloropropane
ug/L
5.0
NO
50
112%
118%
100%
104%
11%
13%
Dibromomethane
ug/L
5.0
ND
50
108%
96%
12%
Bromodichloromethane
4-Methyl-2-pentanone (MIBK)
ug/L
5.0
ND
50
104%
92%
12%
cis-1,3-Dichloropropene
ug/L
ug/L
50
5.0
ND
ND
100
50
115%
104%
10%
Toluene
ug/L
5.0,
ND
50
104%
108%
90%
100%
14%
8%
trans-1,3-Dichloro-l-propene
ug/L
5.0
ND
50
106%
92%
14%
1,1,2-Trichloroethane
ug/L
5.0
NO
50
114%
102%
11%
2-Hexanone
Dibromochloromethane
ug/L
50
ND
100
111%
103%
7%
Tetrachloroethylene
ug/L
ug/L
5.0
5.0
ND
ND
50
50
102%
94%
8%
1,2-Dibromoethane
ug/L
5.0
ND
50
110%
110%
98%
100%
12%
10%
Chlorobenzene
ug/L
5.0
NO
50
106%
96%
10%
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
50
108%
100%
8%
Ethylbenzene
ug/L
5.0
ND
50
104%
98%
6%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical
Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Page 17
QUALITY CONTROL DATA
Client Reference: McDowell Co. Landfill
Tel: [phone]
Fax: [phone]
June 11, 1997
PACE Project Number: A70529600
APPENDIX I, LANDFILL VOLATILES
Batch: 92 60294
Samples: 93 0399118, 93 0399126, 93 0399134, 93 0399142, 93 0399150
93 0399169
SPIKE AND SPIKE DUPLICATE:
930399118
Spike
Parameter
XyTe—nes, (total)
Units
PRL
Landfill
MWI
Spike
Spike
Recv
Dupi
Recv
RPD
Styrene
ug/L
.0
5.0
D
NO
150
50
10-87-
TOM%
5%
Bromoform
ug/L
5.0
NO
50
104%
92%
100%
84%
4%
9%
1,1,2,2-Tetrachloroethane
ug/L
5.0
NO
50
110%
100%
10%
1,2,3-Trichloropropane
ug/L
5.0
NO
50
110%
102%
8%
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
50
80%
72%
11%
1,4-Dichlorobenzene
ug/L
5.0
NO
50
96%
92%
4%
1,2-Dichlorobenzene
ug/L
5.0
NO
50
98%
94%
4%
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
50
98%
96%
2%
LABORATORY CONTROL -SAMPLE:
Parameter
M ---F
et YT—Moride
Units
—9/ —L
PRL
Reference
Value
—20—
Recv
Chloroethene (Vinyl chloride)
U
ug/L
i-0
10
20
85%
85%
Bromomethane
ug/L
10
20
105%
Chloroethane
ug/L
10
20
95%
Trichlorofluoromethane
ug/L
5.0
20
100%
Acetone
ug/L
100
40
98%
1,1-Dichloroethene
ug/L
5.0
20
100%
Methyl iodide
Acrylonitrile
ug/L
5.0
40
90%
Dichloromethane
ug/L
ug/L
100
5.0
200
104%
Carbon disulfide
ug/L
5.0
20
40
90%
103%
trans-1,2-Dichloroethene
ug/L
5.0
20
95%
1,1-Dichloroethane
ug/-L
5.0
20
95%
Vinyl acetate
ug/L
50
40
60%
Methyl ethyl ketone
cis-1,2-Dichloroethene
ug/L
100
40
108%
Chloroform
ug/L
ug/L
5.0
5.0
20
20
100%
110%
Bromochloromethane
ug/L
5.0
20
100%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Analytical Asheville, NC 28801
Tel: [phone]
Fax: [phone]
QUALITY CONTROL DATA June 11, 1997
Page 18 PACE Project Number: A70529600
Client Reference: McDowell Co. Landfill
APPENDIX I, LANDFILL VOLATILES
Batch: 92 60294
Samples: 93 0399118, 93 0399126, 93 0399134, 93 0399142, 93 0399150
93 0399169
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
PRL
Value
Recv
1,1,1-Trichloroethane
U9 —/L
5-.-0
2F—
--9 N
1,2-Dichloroethane
ug/L
5.0
20
100%
Carbon tetrachloride
ug/L
5.0
20
105%
Benzene
ug/L
5.0
20
95%
Trichloroethene
ug/L
5.0
20
105%
1,2-Dichloropropane
ug/L
5.0
20
100%
Dibromomethane
ug/L
5.0
20
100%
Bromodichloromethane
ug/L
5.0
20
95%
4-Methyl-2-pentanone (MIBK)
ug/L
50
40
105%
cis-1,3-Dichloropropene
ug/L
5.0
20
100%
Toluene
ug/L
5.0
20
100%
trans-1,3-Dichloro-l-propene
ug/L
5.0
20
100%
1,1,2-Trichloroethane
ug/L
5.0
20
100%
2-Hexanone
ug/L
50
40
108%
Dibromochloromethare
ug/L
5.0
20
100%
Tetrachloroethylene
ug/L
5.0
20
105%
1,2-Dibromoethane
ug/L
5.0
20
105%
Chlorobenzene
ug/L
5.0
20
100%
1,1,1,2-Tetrachloroethane
ug/L
5.0
20
105%
Ethylbenzene
ug/L
5.0
20
100%
Xylenes, (total)
ug/L
5.0
60
107%
Styrene
ug/L
5.0
20
105%
Bromoform
ug/L
5.0
20
105%
1,1,2,2-Tetrachloroethane
ug/L
5.0
20
105%
1,2,3-Trichloropropane
ug/L
5.0
20
105%
trans-1,4-Dichloro-2-butene
ug/L
5.0
20
95%
1,4-Dichlorobenzene
ug/L
5.0
20
100%
1,2-Dichlorobenzene
ug/L
5.0
20
100%
1,2-Dibromo-3-chloropropane
ug/L
5.0
20
95%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Page 19
FOOTNOTES
for pages 14 through 18
Client Reference: McDowell Co. Landfill
ND Not detected at or above the PRL.
PRL PACE Reporting Limit
RPD Relative Percent Difference
Fax: [phone]
June 11, 1997
PACE Project Number: A70529600
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
LAND QUALITY SECTION: Interchange Bldg., 59 Woodfin Place, AshevilleNC 28801 [phone]
County-11 6, Pen, -
Person Financially
Addre.-m 10 V
Case #
1. Project Location o f A 44-S -2 2 Pictures: Yes No Ej'� Ffints 0 Slides [] Video
2. Weather and Soil Conditions 'K4 r 4 L
3. Is site currently under notice of violation9 Yes No 0
4. Is the site in compliance with the S.P.C.A. and rules? Yes 0 No If no, check violations below:
5. Violations:
11 a. No approved plan, G.S. 113A-57 (4) and 15A N.C.A.0 4B.0007(c) g. Inadequate buffer zone, G.S. 113A-57(l)
0"'b. Failure to follow approved plan, G.S. 113A-61.1 h. Graded slopes and fills too steep,
c. F ailure to submit revised plan, G.S. I I 3A-54. I (b) and G.S. 113A-57(2) or 15A N.C.A.C. 4B.0024(d)
15A N.C.A.C. 4B.001 8(a) i. Unprotected exposed slopes, G.S. 113A-57(2)
d. Failure to provide adequate groundcover, G.S. 113A-57(3) and J. Failure to maintain erosion control measures,
15A N.C.A.C. 4B.0007(b) or 15A N.C.A.0 4B.0024(e) 15A N.C.A.C. 413.0013
Insufficient measures to retain sediment on site, G.S. 113A-57(3) k. Other(describe)
Failure to take all reasonable measures, 15A N.C.A.C.411.0005
6. Has sedimentation damage occurred since last inspection? Yes [2"' If Yes, where? all that apply): No
,'>heck
Lake/natural watercourse on the tract 0 Lake/natural watercourse off the tractEl' Other property
Description 'L,, .�r.
_ ,,at r e, ee V4. 12 6 e e",
Degree of damage: Slight El Moderate 0' Severe 0
7. Contact made with (Nanne) �� , 11 �� -c Title
Inspection Report given El or sent [3" to Person Financially Responsible. Date given/sent
8. Corrective actions needed:
e, 4 Ir 4opc� 4 "Pe"eA, 0
Conunents:-4�' P 13 Ae44 ea
-r t i -, 4' Iq
&14? 41� cl� ell Ce 4"4.
��Atedl eece,-#,-e--4
Report by: P Oz&,� �e kv Others Present
Date of Inspection 12 7 Time arriving on site Time leaving site' 11J v AA
cc:

NC DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
Division of Solid waste Kanagement
Solid Waste Section
SOLID WASTE KUYUNEWNT FACILITY EVALUATION REPORT
Type of Facility. Permi t # County.
Name of Fac i t i ty Location /44'�"
Date of Last Evaluation /
I- Permit Conditions Followed Yes No 117 '4',�"4j
N/A
A- Specific Condition(s) Viol
11. Operational Requirements Followed Yes No
15A N-C. Admin. Code 13B Section
A- Specific VioLation(s) by number and Letter.
III. Other Violations of Rule or Law
IV. Evaluator's Comments
V. Continuation Page Required? Yes _�,�No Receiving Signature_
Evaluation Date Solid Waste Section—
DEHUR 3793 (Part I Uhite. Facility Part 11 Canary: Central Office Part III Pink: Regional office)
Solid Waste Section (Review 7/94)

r Fac/Perm/Co 10 # Date Doc ID#
h/ I bq DIN
V
cc) pq
From:
North Carolina Department of Environment,
Health, and Natural Resources eq

WELL t WELL P
E) EL. 97.03 . 0
TIP EL. 117-34 L
WELLI
EL. 100-00
ZP
z 0
LLa WPLL4
i _NE EL. 110-83
gr
EL. 94.98
f7 a 0
cL
ZZ
X"
Or
".0 1-0 -1-0
JA
5Cqle 6
Fisvre /.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NG 28801
Tel: [phone]
Fax: [phone]
September 16, 1997
Mr. Mike Gladden
McDowell County Landfill
10 East Court Street
Marion, NC 28752
RE: PACE Project No. A70828.600
Client Reference: Monitoring Wells (Landfille)
Dear Mr. Gladden:
Enclosed is the report of laboratory analyses for samples received
August 29, 1997.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
-o 166z� -�
Walter L. Miller
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytacal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
McDowell County Landfill September 16, 1997
10 East Court Street PACE Project Number: A70828600
Marion, NC 28752 NC Wastewater Lab Cert. #40
NC Drinkingwater Lab Cert. #37712
SIC Lab Cert. #99030
Attn: Mr. Mike Gladden
Client Reference: Monitoring Wells (Landfill)
PACE Sample Number: 93 0451187
Date Collected: 08/28/97
Date Received: 08/29/97
Client Sample ID: MW #1
Parameter Units PRL DATE ANALYZED
FIELD ANALYSIS
INDIVIDUAL PARAMETERS
Depth to Water feet 0.01 17.38 08/28/97
Specific Conductivity (Field) umhos/cm2 10 40 08/28/97
Temperature (Field) Degrees C 0.5 17 08/28/97
PH (Field) Units 0.1 5.5 08/28/97
INORGANIC ANALYSIS
APPENDIX I METALS
Silver
mg/L
0.001
ND
09/08/97
Arsenic
mg/L
0.005
NO
09/09/97
Bari um
mg/L
0.10
0.4
09/09/97
Beryllium
mg/L
0.001
ND
09/10/97
Cadmium
mg/L
0.001
0.002
09/08/97
Cobalt
mg/L
0.001
0.010
09/05/97
Chromium
mg/L
0.001
0.002
09/05/97
Copper
mg/L
0.01
ND
09/09/97
Nickel
mg/L
0.05
ND
09/09/97
Lead
mg/L
0.005
0.014
09/08/97
Antimony
mg/L
0.003
ND
09/10/97
Selenium
mg/L
0.005
ND
09/08/97
Thallium
mg/L
0.001
NO
09/10/97
Vanadium
mg/L
0.005
0.012
09/05/97
Zinc
mg/L
0.01
0.04
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analvtocal Asheville, NG 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden September 16, 1997
Page 2 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfill)
PACE Sample Number: 93 0451195
Date Collected: 08/28/97
Date Received: 08/29/97
Client Sample ID: MW #2
Parameter Units PRL DATE ANALYZED
FIELD ANALYSIS
INDIVIDUAL PARAMETERS
Depth to Water
feet 0.01
35.95
08/28/97
Specific Conductivity (Field)
umhos/cm2 10
420
08/28/97
Temperature (Field)
Degrees C 0.5
17
08/28/97
pH (Field)
Units 0.1
5.6
08/28/97
INORGANIC ANALYSIS
APPENDIX I METALS
Silver
mg/L
0.001
ND
09/08/97
Arsenic
mg/L
0.005
NO
09/09/97
Barium
mg/L
0.10
0.2
09/09/97
Beryllium
mg/L
0.001
0.001
09/10/97
Cadmium
mg/L
0.001
ND
09/08/97
Cobalt
mg/L
0.001
0.023
09/05/97
Chromium
mg/L
0.001
ND
09/05/97
Copper
mg/L
0.01
ND
09/09/97
Nickel
mg/L
0.05
ND
09/09/97
Lead
mg/L
0.005
0.012
09/08/97
Antimony
mg/L
0.003
ND
09/10/97
Selenium
mg/L
0.005
NO
09/08/97
Thallium
mg/L
0.001
ND
09/10/97
Vanadium
mg/L
0.005
0.036
09/05/97
Zinc
mg/L
0.01
0.05
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Favenscroft Drive
Pace Analyfical Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden September 16, 1997
Page 3 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfill)
PACE Sample Number: 93 0451209
Date Collected: 08/28/97
Date Received: 08/29/97
Client Sample ID: MW #3
Parameter Units PRL DATE ANALYZED
FIELD ANALYSIS
INDIVIDUAL PARAMETERS
Depth to Water feet 0.01 37.46 08/28/97
Specific Conductivity (Field) umhos/cm2 10 310 08/28/97
Temperature (Field) Degrees C 0.5 19 08/28/97
pH (Field) Units 0.1 6.1 08/28/97
fiffl M110140H.1111FIRI&I
APPENDIX I METALS
Silver
mg/L
0.001
ND
09/08/97
Arsenic
mg/L
0.005
ND
09/09/97
Barium
mg/L
0.10
0.3
09/09/97
Beryllium
mg/L
0.001
0.001
09/10/97
Cadmium
mg/L
0.001
ND
09/08/97
Cobalt
mg/L
0.001
0.012
09/05/97
Chromium
mg/L
0.001
0.001
09/05/97
Copper
mg/L
0.01
ND
09/09/97
Nickel
mg/L
0.05
ND
09/09/97
Lead
mg/L
0.005
0.013
09/08/97
Antimony
mg/L
0.003
IND
09/10/97
Selenium
mg/L
0.005
ND
09/08/97
Thallium
mg/L
0.001
0.001
09/10/97
Vanadium
mg/L
0.005
0.015
09/05/97
Zinc
mg/L
0.01
0.02
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden
Page 4
Client Reference: Monitoring Wells (Landfill)
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Pararnptpr
FIELD ANALYSIS
INDIVIDUAL PARAMETERS
Units PRL
September 16, 1997
PACE Project Number: A70828600
93 0451217
08/28/97
08/29/97
MW #4
Depth to Water feet 0.01 18.48 08/28/97
Specific Conductivity (Field) umhos/cm2 10 62 08/28/97
Temperature (Field) Degrees C 0.5 18 08/28/97
PH (Field) Units 0.1 4.9 08/28/97
INORGANIC ANALYSIS
APPENDIX I METALS
Silver
mg/L
0.001
ND
09/08/97
Arsenic
mg/L
0.005
ND
09/09/97
Barium
mg/L
0.10
0.3
09/09/97
Beryllium
mg/L
0.001
ND
09/10/97
Cadmium
mg/L
0.001
ND
09/08/97
Cobalt
mg/L
0.001
ND
09/05/97
Chromium
mg/L
0.001
ND
09/05/97
Copper
mg/L
0.01
ND
09/09/97
Nickel
mg/L
0.05
ND
09/09/97
Lead
mg/L
0.005
ND
09/08/97
Antimony
mg/L
0.003
ND
09/10/97
Selenium
mg/L
0.005
ND
09/08/97
Thallium
mg/L
0.001
ND
09/10/97
Vanadium
mg/L
0.005
ND
09/05/97
Zinc
mg/L
0.01
0.03
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analyfleal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden
Page 5
Client Reference: Monitoring Wells (Landfill)
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Pararnptpr
INORGANIC ANALYSIS
F.119 29 ki I a Kea 0111.11 I&i
Units
September 16, 1997
PACE Project Number: A70828600
93 0451233
08/28/97
08/29/97
Equpip
Blank A13
PRL Ash032597 DATE ANALYZED
Silver
mg/L
0.001
NO
09/08/97
Arsenic
mg/L
0.005
ND
09/09/97
Barium
mg/L
0.10
ND
09/09/97
Beryllium
mg/L
0.001
NO
09/10/97
Cadmium
mg/L
0.001
NO
09/08/97
Cobalt
mg/L
0.001
ND
09/05/97
Chromium
mg/L
0.001
ND
09/05/97
Copper
mg/L
0.01
NO
09/09/97
Nickel
mg/L
0.05
ND
09/09/97
Lead
mg/L
0.005
ND
09/08/97
Antimony
mg/L
0.003
ND
09/10/97
Selenium
mg/L
0.005
ND
09/08/97
Thallium
mg/L
0.001
ND
09/10/97
Vanadium
mg/L
0.005
ND
09/05/97
Zinc
mg/L
0.01
ND
09/09/97
These data have been reviewed
and are approved
for release.
�Jxi� N&
Walter L. Miller
Operations Manager
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NG 28801
Td: 704-254-717;
Fax: [phone]
Mr. Mike Gladden FOOTNOTES September 16, 1997
Page 6 for pages 1 through 5 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfill)
NO Not detected at or above the PRL.
PRL PACE Reporting Limit
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Havenscroft Drive
Pace Analytwcal Asheville, NC 28801
Tel: [phone];
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 4 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Antimony
Batch: 93 46881
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Antimony
SPIKE:
Parameter
Antimony
LABORATORY CONTROL SAMPLE:
Parameter
Antimony
Units
il�g AL
Units
iF9 / —L
Units
mg/L
Duplicate
Method of
PRL Blank 930453287 93 0453287 RPD
U—.O 0 3 WD— N D NO NC
Spi ke
PRL 930453287 §SR� Recv
07003 170 — 0.025 104%
Reference
PRL Value Recv
-6—.003 0.035 94%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytmeal
Pace Analyfical Services, Ifle.
54 Raveflscroft Drive
Asheville, NC 28801,
To]: 704-254-7176
Fax: [phone]
Mr. Mike Gladden QUALITY
CONTROL DATA
September 16, 1997
Page 5
PACE Project Number: A70828600
Client Reference: Monitoring Wells
(Landfille)
Arsenic
Batch: 93 46837
Samples: 93 0451187, 93 0451195, 93
0451209, 93
0451217,
93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter
Units
PRL
Blank 930452175 93 0452175 RPD
Arsenic
F9—/ —L
D—.O-05
ND NO NO — N—c—
SPIKE:
Spike
Parameter
Units
PRL
930452175 Recv
ing AL
0700 5
ND 0.025 96%
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
PRL
Value Recv
Arsenic
F9—/L
-a—.005
0.035 103%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 6 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Barium
Batch: 93 46854
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Barium
SPIKE:
Parameter
Barium
LABORATORY CONTROL SAMPLE:
Parameter
Barium
Units
Fg—/ —L
Units
i�g—/ —L
Units
mg/L
Duplicate
Method
930451187
of
PRL
Blank
MW #1
93 0451187 RPD
b—.10
NO
0.4
0.4 0%
930451187
Spike
PRL
MW #1
S
§J?j�
Recv
0—.10
T.-4
1.00
110%
Reference
PRL Value Recv
OA 0 1—.00 --997%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NG 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 7 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Beryl I i um
Batch: 93 46880
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Beryllium
SPIKE:
Parameter
Berylliu�
LABORATORY CONTROL SAMPLE:
Parameter
Beryllium
Units
� —9/ —L
Units
i5-9/ —L
Units
mg/L
Duplicate
Method of
PRL Blank 930453287 93 0453287 RPD
U—.O 0 1 N-D— N—D— ND NC
Spike
PRL 930453287 Recv
U—.001 NO 0.002 100%
Reference
PRL Value Recv
U-.-001 0.0-03-5 10—H
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NG 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 8 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Cadmi um
Batch: 93 46832
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter Units
Cadmium F97 —L
LABORATORY CONTROL SAMPLE:
Parameter Units
Cadmium i�g —/L
Duplicate
Method 930451217 of
PRL Blank MW #4 93 0451217 RPD
U-001 N—D— ND--- ND— N-C—
Reference
PRL Value Recv
o—.0-01 0.0035 97%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 9 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Chromium
Batch: 93 46779
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Chromium
SPIKE:
Parameter
Chromium
LABORATORY CONTROL SAMPLE:
Parameter
Mrom �Ium
Duplicate
Method of
Units PRL Blank 930447988 93 0447988 RPD
Fg—/L 070-01 NO NO NO NC
Units
Fg-/ —L
Units
iFg-/-L-
Spi ke
PRL 930447988 Sk� Recv
0-.0-01 ND — 0.006 100%
Reference
PRL Value Recv
U—.001 0.010 100%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone];
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 10 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Cobal t
Batch: 93 46781
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Cobalt
SPIKE:
Parameter
Cobalt
LABORATORY CONTROL SAMPLE:
Parameter
Cobalt
Units
T�9—/ —L
Units
59 —/L—
Units
mg/L
Duplicate
Method of
PRL Blank 930447996 93 0447996 RPD
0—.0 0 1 WD— N—D NO NC
Spi ke
PRL 930447996 S like Recv
-a—. I ffD PT 7
00 0.02 272%
Reference
PRL Value Recv
U—.001 0.035 91%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytmeal Asheville, NC 28801
Tel: [phone];
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 11 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Copper
Batch: 93 46859
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
FAFTHH,
Parameter
Copper
SPIKE:
Parameter
Copper
LABORATORY CONTROL SAMPLE:
Parameter
Copper
Units
PRL
iFg —/L
U—.O I
Units
PRL
F9 —/L
-a—.01
Units PRL
F97 —L 0—.0 1
Duplicate
Method 930451187 of
Blank MW #1 93 0451187 RPD
ND ND ND N—C
930451187 Spike
MW #1 Sk� Recv
Z 1.00 105%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Reference
Value Recv
--T.00 99%

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analyt"cal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 12 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Lead
Batch: 93 46829
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method 930451187 of
Parameter Units PRL Blank MW #1 93 0451187 RPD
Lead r�-91 —L -6-005 90— T-O 1 —4 -6-0-1-3— —71.
SPIKE:
Parameter Units
Lead rn-9/ —L
LABORATORY CONTROL SAMPLE:
Parameter Units
Lead M-9-1 —L
930451187 Spike
PRL MW #1 Recv
D—.O 0 5 T.-014 0.030 70%
Reference
PRL Value Recv
U—.005 0.035 106%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone];
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 13 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Nickel
Batch: 93 46866
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Nickel
SPIKE:
Parameter
Nickel
LABORATORY CONTROL SAMPLE:
Parameter
Nickel
Units
i�g-/ —L
Units
i5i/ —L
Units
mg/L
Duplicate
Method
930451187
of
PRL
Blank
MW #1
93 0451187 RPD
U-0-5
N—D—
N—D—
RD--- R—C
930451187
Spike
PRL
MW #1
Recv
�--.05
NO
1.00
102%
Reference
PRL Value Recv
'6—.0 5 —1.00 96%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analyfical Asheville, NC 28801
Tel: [phone];
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 14 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Selenium
Batch: 93 46835
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Selenium
SPIKE:
Parameter
Selenium
LABORATORY CONTROL SAMPLE:
Parameter
Selenium
Duplicate
Method of
Units PRL Blank 930452175 93 0452175 RPD
iRg-/ —L U-0-05 N—D— ITD-- N`D-- N-C
Units
Fg-/-L-
Units
Fg- —/L
Sp i ke
PRL 930452175 Recv
0-.0-05 ND 0.025 --8-807.
Reference
PRL Value Recv
U—.005 0.035 97%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 15 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Silver
Batch: 93 46834
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
Parameter
Silver
SPIKE:
Parameter
Silver
Parameter
Silver
V4
M11 111W.'rur"
Units
ra-97L
Units
F9 —/L
Units
TK9-1 F
Duplicate
Method 930451217 of
PRL Blank MW #4 93 0451217 RPD
'670 0 1 WD-- ND-- N-D--- N—C
930451217
PRL MW #4
070-0 1 RD— 0.005
Reference
PRL Value
U—.001 0.005
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Sp i ke
Recv
80%
Recv
100%

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 16 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Thal 1 i um
Batch: 93 46882
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Thallium
SPIKE:
Parameter
LABORATORY CONTROL SAMPLE:
Parameter
Thallium
Units
F9-/ —L
Units
M-9 —/L-
Units
mg/L
Duplicate
Method of
PRL Blank 930453287 93 0453287 RPD
U-.O 0 1 NO NO NO ffc--
Spi ke
PRL 930453287 Recv
070-01 TO — 0.025 108%
Reference
PRL Value Recv
U70-01 --E-0-3-5— 1-0907.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analltocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA
September 16, 1997
Page 17
PACE Project Number:
A70828600
Client Reference: Monitoring Wells
(Landfille)
Vanadium
Batch: 93 46783
Samples: 93 0451187, 93 0451195, 93
0451209, 93
0451217,
93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method
of
Parameter
Units
PRL
Blank 930447996
93 0447996 RPD
VanaTiFum
Mg/L
0.005
NO N—D
ND wc—
SPIKE:
Spike
Parameter
Units
PRL
930447996 S
Recv
Vanadium
F9 —/L
U—.O 0 5
TD— 0.050
60%
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
PRL
Value
Recv
Vanadium
r�9-1 —L
T.—O 0 5
0.100
100%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NG 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 18 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
Zinc
Batch: 93 46871
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451233
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Zinc
SPIKE:
Parameter
Zinc
LABORATORY CONTROL SAMPLE:
Parameter
Ti—nc
Units
Fg-/ —L
Units
� Fg/ —L
Units
T5-9/ —L
Duplicate
Method 930451187 of
PRL Blank MW #1 93 0451187 RPD
U-.O-1 NO 0.04 0.03 29%
930451187
PRL MW #1 LI!Le
U —.0 1 -O-.T4— 2 . 0 0
Reference
PRL Value
U—.01 2.00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Spi ke
Recv
105%
Recv
9961.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace AnaLytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden FOOTNOTES September 16, 1997
Page 19 for pages 4 through 18 PACE Project Number: A70828600
Client Reference: Monitoring Wells (Landfille)
NC No calculation due to value below detection limit.
NO Not detected at or above the PRL.
PRL PACE Reporting Limit
RPD Relative Percent Difference
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
McDowell County Landfill September 16, 1997
10 East Court Street PACE Project Number: A70828600
Marion, NC 28752 NC Wastewater Lab Cert. #12
NC Drinkingwater Lab Cert. #37706
SC Lab Cert. #99006
Attn: Mr. Mike Gladden
Client Reference: McDowell Co.
PACE Sample Number:
93 0451187
Date Collected:
08/28/97
Date Received:
09/03/97
Client Sample ID:
MW #1
Parameter
Units
PRL
METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
NO
09/09/97
Chloroethene (Vinyl chloride)
ug/L
10
NO
09/09/97
Bromomethane
ug/L
10
NO
09/09/97
Chloroethane
ug/L
10
NO
09/09/97
Trichlorofluoromethane
ug/L
5.0
ND
09/09/97
Acetone
ug/L
100
NO
09/09/97
1,1-Dichloroethene
ug/L
5.0
NO
09/09/97
Methyl iodide
ug/L
5.0
NO
09/09/97
Acrylonitrile
ug/L
100
ND
09/09/97
Dichloromethane
ug/L
5.0
NO
09/09/97
Carbon disulfide
ug/L
5.0
ND
09/09/97
trans-1,2-Dichloroethene
ug/L
5.0
NO
09/09/97
I,I-Dichloroethane
ug/L
5.0
NO
09/09/97
Vinyl acetate
ug/L
50
NO
09/09/97
Methyl ethyl ketone
ug/L
100
ND
09/09/97
cis-1,2-Dichloroethene
ug/L
5.0
NO
09/09/97
Chloroform
ug/L
5.0
NO
09/09/97
Bromochloromethane
ug/L
5.0
IND
09/09/97
1,1,1-Trichloroethane
ug/L
5.0
ND
09/09/97
1,2-Dichloroethane
ug/L
5.0
NO
09/09/97
Carbon tetrachloride
ug/L
5.0
NO
09/09/97
Benzene
ug/L
5.0
IND
09/09/97
Trichloroethene
ug/L
5.0
NO
09/09/97
1,2-Dichloropropane
ug/L
5.0
ND
09/09/97
Dibromomethane
ug/L
5.0
NO
09/09/97
Bromodichloromethane
ug/L
5.0
NO
09/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
NO
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden September 16, 1997
Page 2 PACE Project Number: A70828600
Client Reference: McDowell Co.
PACE Sample Number:
93 0451187
Date Collected:
08/28/97
Date Received:
09/03/97
Client Sample ID:
Mid #1
Parameter
Units
PRL
METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
cis-1,3-Dichloropropene
ug/L
5.0
NO
09/09/97
Toluene
ug/L
5.0
NO
09/09/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
09/09/97
1,1,2-Trichloroethane
ug/L
5.0
NO
09/09/97
2-Hexanone
ug/L
50
NO
09/09/97
Dibromochloromethane
ug/L
5.0
NO
09/09/97
Tetrachloroethylene
ug/L
5.0
NO
09/09/97
1,2-Dibromoethane
ug/L
5.0
NO
09/09/97
Chlorobenzene
ug/L
5.0
NO
09/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
09/09/97
Ethylbenzene
ug/L
5.0
NO
09/09/97
Xylenes, (total)
ug/L
5.0
NO
09/09/97
Styrene
ug/L
5.0
NO
09/09/97
Bromoform
ug/L
5.0
NO
09/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
NO
09/09/97
1,2,3-Trichloropropane
ug/L
5.0
NO
09/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
09/09/97
1,4-Dichlorobenzene
ug/L
5.0
NO
09/09/97
1,2-Dichlorobenzene
ug/L
5.0
NO
09/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
NO
09/09/97
Surrogate - Dibromofluoromethane
%
100
09/09/97
Surrogate - Toluene-d8
%
98
09/09/97
Surrogate - 4-Bromofluorobenzene
%
98
09/09/97
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801 '
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden September 16, 1997
Page 3 PACE Project Number: A70828600
Client Reference: McDowell Co.
PACE Sample Number:
93 0451195
Date Collected:
08/28/97
Date Received:
09/03/97
Client Sample ID:
MW #2
Parameter
Units
PRL
METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
NO
09/09/97
Chloroethene (Vinyl chloride)
ug/L
10
NO
09/09/97
Bromomethane
ug/L
10
NO
09/09/97
Chloroethane
ug/L
10
NO
09/09/97
Trichlorofluoromethane
ug/L
5.0
NO
09/09/97
Acetone
ug/L
100
NO
09/09/97
I,I-Dichloroethene
ug/L
5.0
NO
09/09/97
Methyl iodide
ug/L
5.0
NO
09/09/97
Acrylonitrile
ug/L
100
NO
09/09/97
Dichloromethane
ug/L
5.0
NO
09/09/97
Carbon disulfide
ug/L
5.0
NO
09/09/97
trans-1,2-Dichloroethene
ug/L
5.0
NO
09/09/97
1,1-Dichloroethane
ug/L
5.0
9.4
09/09/97
Vinyl acetate
ug/L
50
NO
09/09/97
Methyl ethyl ketone
ug/L
100
NO
09/09/97
cis-1,2-Dichloroethene
ug/L
5.0
87
09/09/97
Chloroform
ug/L
5.0
NO
09/09/97
Bromochloromethane
ug/L
5.0
NO
09/09/97
1,1,1-Trichloroethane
ug/L
5.0
NO
09/09/97
1,2-Dichloroethane
ug/L
5.0
NO
09/09/97
Carbon tetrachloride
ug/L
5.0
NO
09/09/97
Benzene
ug/L
5.0
is
09/09/97
Trichloroethene
ug/L
5.0
NO
09/09/97
1,2-Dichloropropane
ug/L
5.0
NO
09/09/97
Dibromomethane
ug/L
5.0
NO
09/09/97
Bromodichloromethane
ug/L
5.0
NO
09/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
NO
09/09/97
cis-1,3-Dichloropropene
ug/L
5.0
NO
09/09/97
Toluene
ug/L
5.0
35
09/09/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
09/09/97
1,1,2-Trichloroethane
ug/L
5.0
NO
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wriften consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden
Page 4
Client Reference: McDowell Co.
September 16, 1997
PACE Project Number: A70828600
PACE Sample Number:
93 0451195
Date Collected:
08/28/97
Date Received:
09/03/97
Client Sample ID:
MW #2
Parameter
Units
PRL
METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
2-Hexanone
ug/L
50
ND
09/09/97
Dibromochloromethane
ug/L
5.0
ND
09/09/97
Tetrachloroethylene
ug/L
5.0
ND
09/09/97
1,2-Dibromoethane
ug/L
5.0
ND
09/09/97
Chlorobenzene
ug/L
5.0
18
09/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
09/09/97
Ethylbenzene
ug/L
5.0
ND
09/09/97
Xylenes, (total)
ug/L
5.0
35
09/09/97
Styrene
ug/L
5.0
ND
09/09/97
Bromoform
ug/L
5.0
ND
09/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
09/09/97
1,2,3-Trichloropropane
ug/L
5.0
ND
09/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
09/09/97
1,4-Dichlorobenzene
ug/L
5.0
7.7
09/09/97
1,2-Dichlorobenzene
ug/L
5.0
ND
09/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
09/09/97
Surrogate - Dibromofluoromethane
%
110
09/09/97
Surrogate - Toluene-d8
%
95
09/09/97
Surrogate - 4-Bromofluorobenzene
%
102
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
Pace Anal 54 Ravenscroft Drive
.ytmj;a1 Asheville, NC 28801
Tel: [phone];
Fax: [phone]
Mr. Mike Gladden
Page 5
Client Reference: McDowell Co.
September 16, 1997
PACE Project Number: A70828600
PACE Sample Number:
93 0451209
Date Collected:
08/28/97
Date Received:
09/03/97
Client Sample ID:
MW #3
Parameter
Units
PRL
METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
NO
09/09/97
Chloroethene (Vinyl chloride)
ug/L
10
ND
09/09/97
Bromomethane
ug/L
10
NO
09/09/97
Chloroethane
ug/L
10
ND
09/09/97
Trichlorofluoromethane
ug/L
5.0
NO
09/09/97
Acetone
ug/L
100
NO
09/09/97
1,1-Dichloroethene
ug/L
5.0
NO
09/09/97
Methyl iodide
ug/L
5.0
NO
09/09/97
Acrylonitrile
ug/L
100
NO
09/09/97
Dichloromethane
ug/L
5.0
NO
09/09/97
Carbon disulfide
ug/L
5.0
NO
09/09/97
trans-1,2-Dichloroethene
ug/L
5.0
ND
09/09/97
1,1-Dichloroethane
ug/L
5.0
ND
09/09/97
Vinyl acetate
ug/L
50
NO
09/09/97
Methyl ethyl ketone
ug/L
100
ND
09/09/97
cis-1,2-Dichloroethene
ug/L
5.0
NO
09/09/97
Chloroform
ug/L
5.0
ND
09/09/97
Bromochloromethane
ug/L
5.0
NO
09/09/97
1,1,1-Trichloroethane
ug/L
5.0
ND
09/09/97
1,2-Dichloroethane
ug/L
5.0
NO
09/09/97
Carbon tetrachloride
ug/L
5.0
NO
09/09/97
Benzene
ug/L
5.0
NO
09/09/97
Trichloroethene
ug/L
5.0
ND
09/09/97
1,2-Dichloropropane
ug/L
5.0
NO
09/09/97
Dibromomethane
ug/L
5.0
ND
09/09/97
Bromodichloromethane
ug/L
5.0
NO
09/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
09/09/97
cis-1,3-Dichloropropene
ug/L
5.0
NO
09/09/97
Toluene
ug/L
5.0
ND
09/09/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
ND
09/09/97
1,1,2-Trichloroethane
ug/L
5.0
NO
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analyfical Asheville, NC 28801
Tel: [phone];
Fax: [phone]
Mr. Mike Gladden September 16, 1997
Page 6 PACE Project Number: A70828600
Client Reference: McDowell Co.
PACE Sample Number:
93 0451209
Date Collected:
08/28/97
Date Received:
09/03/97
Client Sample ID:
MW #3
Parameter
Units
PRL
METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
2-Hexanone
ug/L
50
NO
09/09/97
Dibromochloromethane
ug/L
5.0
NO
09/09/97
Tetrachloroethylene
ug/L
5.0
NO
09/09/97
1,2-Dibromoethane
ug/L
5.0
NO
09/09/97
Chlorobenzene
ug/L
5.0
NO
09/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
09/09/97
Ethylbenzene
ug/L
5.0
NO
09/09/97
Xylenes, (total)
ug/L
5.0
NO
09/09/97
Styrene
ug/L
5.0
NO
09/09/97
Bromoform
ug/L
5.0
ND
09/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
NO
09/09/97
1,2,3-Trichloropropane
ug/L
5.0
ND
09/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
09/09/97
1,4-Dichlorobenzene
ug/L
5.0
ND
09/09/97
1,2-Dichlorobenzene
ug/L
5.0
NO
09/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
NO
09/09/97
Surrogate - Dibromofluoromethane
%
106
09/09/97
Surrogate - Toluene-d8
%
101
09/09/97
Surrogate - 4-Bromofluorobenzene
%
103
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Raveflscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone];
Fax: [phone]
Mr. Mike Gladden September 16, 1997
Page 7 PACE Project Number: A70828600
Client Reference: McDowell Co.
PACE Sample Number: 93 0451217
Date Collected: 08/28/97
Date Received: 09/03/97
Client Sample ID: MW #4
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
ND
09/09/97
Chloroethene (Vinyl chloride)
ug/L
10
NO
09/09/97
Bromomethane
ug/L
10
NO
09/09/97
Chloroethane
ug/L
10
NO
09/09/97
Trichlorofluoromethane
ug/L
5.0
NO
09/09/97
Acetone
ug/L
100
ND
09/09/97
1,1-Dichloroethene
ug/L
5.0
NO
09/09/97
Methyl iodide
ug/L
5.0
ND
09/09/97
Acrylonitrile
ug/L
100
NO
09/09/97
Dichloromethane
ug/L
5.0
NO
09/09/97
Carbon disulfide
ug/L
5.0
NO
09/09/97
trans-1,2-Dichloroethene
ug/L
5.0
NO
09/09/97
1,1-Dichloroethane
ug/L
5.0
NO
09/09/97
Vinyl acetate
ug/L
50
NO
09/09/97
Methyl ethyl ketone
ug/L
100
ND
09/09/97
cis-1,2-Dichloroethene
ug/L
5.0
NO
09/09/97
Chloroform
ug/L
5.0
ND
09/09/97
Bromochloromethane
ug/L
5.0
ND
09/09/97
1,1,1-Trichloroethane
ug/L
5.0
ND
09/09/97
1,2-Dichloroethane
ug/L
5.0
NO
09/09/97
Carbon tetrachloride
ug/L
5.0
NO
09/09/97
Benzene
ug/L
5.0
ND
09/09/97
Trichloroethene
ug/L
5.0
NO
09/09/97
1,2-Dichloropropane
ug/L
5.0
NO
09/09/97
Dibromomethane
ug/L
5.0
ND
09/09/97
Bromodichloromethane
ug/L
5.0
ND
09/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
NO
09/09/97
cis-1,3-Dichloropropene
ug/L
5.0
ND
09/09/97
Toluene
ug/L
5.0
NO
09/09/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
09/09/97
1,1,2-Trichloroethane
ug/L
5.0
NO
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analyfical Asheville, NC 28801
Tel: [phone];
Fax: [phone]
Mr. Mike Gladden September 16, 1997
Page 8 PACE Project Number: A70828600
Client Reference: McDowell Co.
PACE Sample Number: 93 0451217
Date Collected: 08/28/97
Date Received: 09/03/97
Client Sample ID: MW #4
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX 1, LANDFILL VOLATILES
8260
2-Hexanone
ug/L
50
NO
09/09/97
Dibromochloromethane
ug/L
5.0
NO
09/09/97
Tetrachloroethylene
ug/L
5.0
NO
09/09/97
1,2-Dibromoethane
ug/L
5.0
ND
09/09/97
Chlorobenzene
ug/L
5.0
NO
09/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
09/09/97
Ethylbenzene
ug/L
5.0
ND
09/09/97
Xylenes, (total)
ug/L
5.0
ND
09/09/97
Styrene
ug/L
5.0
NO
09/09/97
Bromoform
ug/L
5.0
ND
09/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
NO
09/09/97
1,2,3-Trichloropropane
ug/L
5.0
NO
09/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
09/09/97
1,4-Dichlarobenzene
ug/L
5.0
ND
09/09/97
1,2-Dichlorobenzene
ug/L
5.0
NO
09/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
09/09/97
Surrogate - Dibromofluoromethane
%
102
09/09/97
Surrogate - Toluene-d8
%
94
09/09/97
Surrogate - 4-Bromofluorobenzene
%
96
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Anal4mcal Asheville, NC 28801
Tel: [phone];
Fax: [phone]
Mr. Mike Gladden September 16, 1997
Page 9 PACE Project Number: A70828600
Client Reference: McDowell Co.
PACE Sample Number: 93 0451225
Date Collected: 08/28/97
Date Received: 09/03/97
Client Sample ID: Travel
Parameter Units PRL Blank METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
NO
09/09/97
Chloroethene (Vinyl chloride)
ug/L
10
ND
09/09/97
Bromomethane
ug/L
10
NO
09/09/97
Chloroethane
ug/L
10
NO
09/09/97
Trichlorofluoromethane
ug/L
5.0
ND
09/09/97
Acetone
ug/L
100
NO
09/09/97
I,I-Dichloroethene
ug/L
5.0
ND
09/09/97
Methyl iodide
ug/L
5.0
NO
09/09/97
Acrylonitrile
ug/L
100
ND
09/09/97
Dichloromethane
ug/L
5.0
NO
09/09/97
Carbon disulfide
ug/L
5.0
ND
09/09/97
trans-1,2-Dichloroethene
ug/L
5.0
NO
09/09/97
I,I-Dichloroethane
ug/L
5.0
ND
09/09/97
Vinyl acetate
ug/L
50
NO
09/09/97
Methyl ethyl ketone
ug/L
100
ND
09/09/97
cis-1,2-Dichloroethene
ug/L
5.0
NO
09/09/97
Chloroform
ug/L
5.0
NO
09/09/97
Bromochloromethane
ug/L
5.0
ND
09/09/97
1,1,1-Trichloroethane
ug/L
5.0
ND
09/09/97
1,2-Dichloroethane
ug/L
5.0
NO
09/09/97
Carbon tetrachloride
ug/L
5.0
ND
09/09/97
Benzene
ug/L
5.0
NO
09/09/97
Trichloroethene
ug/L
5.0
NO
09/09/97
1,2-Dichloropropane
ug/L
5.0
ND
09/09/97
Dibromomethane
ug/L
5.0
ND
09/09/97
Bromodichloromethane
ug/L
5.0
NO
09/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
NO
09/09/97
cis-1,3-Dichloropropene
ug/L
5.0
ND
09/09/97
Toluene
ug/L
5.0
NO
09/09/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
ND
09/09/97
1,1,2-Trichloroethane
ug/L
5.0
ND
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, lflc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden
Page 10
Client Reference: McDowell Co.
September 16, 1997
PACE Project Number: A70828600
PACE Sample Number:
93 0451225
Date Collected:
08/28/97
Date Received:
09/03/97
Client Sample ID:
Travel
Parameter
Units
PRL
Blank METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
2-Hexanone
ug/L
50
ND
09/09/97
Dibromochloromethane
ug/L
5.0
ND
09/09/97
Tetrachloroethylene
ug/L
5.0
ND
09/09/97
1,2-Dibromoethane
ug/L
5.0
ND
09/09/97
Chlorobenzene
ug/L
5.0
ND
09/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
09/09/97
Ethylbenzene
ug/L
5.0
ND
09/09/97
Xylenes, (total)
ug/L
5.0
ND
09/09/97
Styrene
ug/L
5.0
ND
09/09/97
Bromoform
ug/L
5.0
ND
09/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
09/09/97
1,2,3-Trichloropropane
ug/L
5.0
ND
09/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
09/09/97
1,4-Dichlorobenzene
ug/L
5.0
ND
09/09/97
1,2-Dichlorobenzene
ug/L
5.0
ND
09/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
09/09/97
Surrogate - Dibromofluoromethane
%
94
09/09/97
Surrogate - Toluene-d8
%
96
09/09/97
Surrogate - 4-Bromofluorobenzene
%
100
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden September 16, 1997
Page 11 PACE Project Number: A70828600
Client Reference: McDowell Co.
PACE Sample Number: 93 0451233
Date Collected: 08/28/97
Date Received: 09/03/97
Client Sample ID: Equipment
Parameter Units PRL Blank METHOD DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
Methyl Chloride
ug/L
10
NO
09/09/97
Chloroethene (Vinyl chloride)
ug/L
10
NO
09/09/97
Bromomethane
ug/L
10
NO
09/09/97
Chloroethane
ug/L
10
ND
09/09/97
Trichlorofluoromethane
ug/L
5.0
NO
09/09/97
Acetone
ug/L
100
NO
09/09/97
I,I-Dichloroethene
ug/L
5.0
NO
09/09/97
Methyl iodide
ug/L
5.0
NO
09/09/97
Acrylonitrile
ug/L
100
NO
09/09/97
Dichloromethane
ug/L
5.0
ND
09/09/97
Carbon disulfide
ug/L
5.0
NO
09/09/97
trans-1,2-Dichloroethene
ug/L
5.0
NO
09/09/97
I,I-Dichloroethane
ug/L
5.0
NO
09/09/97
Vinyl acetate
ug/L
50
ND
09/09/97
Methyl ethyl ketone
ug/L
100
NO
09/09/97
cis-1,2-Dichloroethene
ug/L
5.0
ND
09/09/97
Chloroform
ug/L
5.0
NO
09/09/97
Bromochloromethane
ug/L
5.0
NO
09/09/97
1,1,1-Trichloroethane
ug/L
5.0
NO
09/09/97
1,2-Dichloroethane
ug/L
5.0
ND
09/09/97
Carbon tetrachloride
ug/L
5.0
NO
09/09/97
Benzene
ug/L
5.0
ND
09/09/97
Trichloroethene
ug/L
5.0
NO
09/09/97
1,2-Dichloropropane
ug/L
5.0
NO
09/09/97
Dibromomethane
ug/L
5.0
NO
09/09/97
Bromodichloromethane
ug/L
5.0
ND
09/09/97
4-Methyl-2-pentanone (MIBK)
ug/L
50
ND
09/09/97
cis-1,3-Dichloropropene
ug/L
5.0
NO
09/09/97
Toluene
ug/L
5.0
ND
09/09/97
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
09/09/97
1,1,2-Trichloroethane
ug/L
5.0
ND
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace AnaLytscal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden
Page 12
Client Reference: McDowell Co.
September 16, 1997
PACE Project Number: A70828600
PACE Sample Number:
93 0451233
Date Collected:
08/28/97
Date Received:
09/03/97
Client Sample ID:
Equipment
Parameter
Units
PRL
Blank METHOD
DATE ANALYZED
ORGANIC ANALYSIS
APPENDIX I, LANDFILL VOLATILES
8260
2-Hexanone
ug/L
50
ND
09/09/97
Dibromochloromethane
ug/L
5.0
ND
09/09/97
Tetrachloroethylene
ug/L
5.0
ND
09/09/97
1,2-Dibromoethane
ug/L
5.0
ND
09/09/97
Chlorobenzene
ug/L
5.0
ND
09/09/97
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
09/09/97
Ethylbenzene
ug/L
5.0
ND
09/09/97
Xylenes, (total)
ug/L
5.0
ND
09/09/97
Styrene
ug/L
5.0
ND
09/09/97
Bromoform
ug/L
5.0
ND
09/09/97
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
09/09/97
1,2,3-Trichloropropane
ug/L
5.0
ND
09/09/97
trans-1,4-Dichloro-2-butene
ug/L
5.0
ND
09/09/97
1,4-Dichlorobenzene
ug/L
5.0
ND
09/09/97
1,2-Dichlorobenzene
ug/L
5.0
ND
09/09/97
1,2-Dibromo-3-chloropropane
ug/L
5.0
ND
09/09/97
Surrogate - Dibromofluoromethane
%
99
09/09/97
Surrogate - Toluene-d8
%
100
09/09/97
Surrogate - 4-Bromofluorobenzene
%
99
09/09/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden FOOTNOTES September 16, 1997
Page 13 for pages I through 12 PACE Project Number: A70828600
Client Reference: McDowell Co.
NO Not detected at or above the PRL.
PRIL PACE Reporting Limit
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Uce Analytocal Asheville, NC 28801
Tel: [phone];
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 14 PACE Project Number: A70828600
Client Reference: McDowell Co.
APPENDIX I, LANDFILL VOLATILES
Batch: 92 63609
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451225
93 0451233
METHOD BLANK:
Method
Parameter
Units
PRL
Blank
Methyl Moride
W9—/L
10--
N-D—
Chloroethene (Vinyl chloride)
ug/L
10
NO
Bromomethane
ug/L
10
NO
Chloroethane
ug/L
10
ND
Trichlorofluoromethane
ug/L
5.0
NO
Acetone
ug/L
100
NO
1,1-Dichloroethene
ug/L
5.0
NO
Methyl iodide
ug/L
5.0
NO
Acrylonitrile
ug/L
100
NO
Dichloromethane
ug/L
5.0
NO
Carbon disulfide
ug/L
5.0
NO
trans-1,2-Dichloroethene
ug/L
5.0
NO
1,1-Dichloroethane
ug/L
5.0
NO
Vinyl acetate
ug/L
50
ND
Methyl ethyl ketone
ug/L
100
ND
cis-1,2-Dichloroethene
ug/L
5.0
NO
Chloroform
ug/L
5.0
ND
Bromochloromethane
ug/L
5.0
ND
1,1,1-Trichloroethane
ug/L
5.0
NO
1,2-Dichloroethane
ug/L
5.0
ND
Carbon tetrachloride
ug/L
5.0
NO
Benzene
ug/L
5.0
ND
Trichloroethene
ug/L
5.0
ND
1,2-Dichloropropane
ug/L
5.0
NO
Dibromomethane
ug/L
5.0
ND
Bromodichloromethane
ug/L
5.0
ND
4-Methyl-2-pentanone (MIBK)
ug/L
50
NO
cis-1,3-Dichloropropene
ug/L
5.0
ND
Toluene
ug/L
5.0
ND
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
1,1,2-Trichloroethane
ug/L
5.0
NO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Mr. Mike Gladden
Page 15
Client Reference: McDowell Co.
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
QUALITY CONTROL DATA September 16, 1997
PACE Project Number: A70828600
APPENDIX 1, LANDFILL VOLATILES
Batch: 92 63609
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451225
93 0451233
METHOD BLANK:
Parameter
Units
PRL
Method
Blank
2-HexanoFe
T9-1L
5-0
ffD—
Dibromochloromethane
ug/L
5.0
ND
Tetrachloroethylene
ug/L
5.0
NO
1,2-Dibromoethane
ug/L
5.0
NO
Chlorobenzene
ug/L
5.0
NO
1,1,1,2-Tetrachloroethane
ug/L
5.0
ND
Ethylbenzene
ug/L
5.0
NO
Xylenes, (total)
ug/L
5.0
NO
Styrene
ug/L
5.0
NO
Bromoform
ug/L
5.0
ND
1,1,2,2-Tetrachloroethane
ug/L
5.0
ND
1,2,3-Trichloropropane
ug/L
5.0
NO
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
1,4-Dichlorobenzene
ug/L
5.0
ND
1,2-Dichlorobenzene
ug/L
5.0
NO
1,2-Dibromo-3-chloropropane
ug/L
5.0
NO
Surrogate - Dibromofluoromethane
%
102
Surrogate - Toluene-d8
%
98
Surrogate - 4-Bromofluorobenzene
%
98
SPIKE AND SPIKE DUPLICATE:
Spike
Parameter
Units
PRL
930451217
MW #4
S ike
10—
Spike
Recv
Dupl
Recv
RPD
Metli-YT--Moride
ug-/-U-
10—
RD---
�
—9-6-/r.
TOM%
6%
Chloroethene (Vinyl chloride)
ug/L
10
NO
50
98%
106%
8%
Bromomethane
ug/L
10
NO
50
104%
108%
4%
Chloroethane
ug/L
10
NO
50
94%
102%
8%
Trichlorofluoromethane
ug/L
5.0
ND
50
94%
90%
4%
Acetone
ug/L
100
NO
100
133%
120%
10%
1,1-Dichloroethene
ug/L
5.0
ND
50
92%
100%
8%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc,
54 Ravenscroft Drive
Pace Analytogal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 16 PACE Project Number: A70828600
Client Reference: McDowell Co.
APPENDIX 1, LANDFILL VOLATILES
Batch: 92 63609
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451225
93 0451233
SPIKE AND SPIKE DUPLICATE:
Spi ke
930451217
Spi ke
Dupl
Parameter
Units
PRL
MW #4
SPI e
Recv
Recv
RPD
Methyl iodide
Ug­/ —L
570-
9D--
100
—8 -0 6/."
_775
11%
Acrylonitrile
ug/L
100
ND
500
101%
96%
5%
Dichloromethane
ug/L
5.0
NO
50
88%
94%
7%
Carbon disulfide
ug/L
5.0
ND
100
89%
93%
4%
trans-1,2-Dichloroethene
ug/L
5.0
NO
50
92%
94%
2%
I,I-Dichloroethane
ug/L
5.0
NO
50
98%
98%
0%
Vinyl acetate
ug/L
50
NO
100
47%
37%
24%
Methyl ethyl ketone
ug/L
100
NO
100
104%
112%
7%
cis-1,2-Dichloroethene
ug/L
5.0
NO
50
94%
100%
6%
Chloroform
ug/L
5.0
NO
50
104%
100%
4%
Bromochloromethane
ug/L
5.0
NO
50
102%
100%
2%
1,1,1-Trichloroethane
ug/L
5.0
ND
50
106%
98%
8%
1,2-Dichloroethane
ug/L
5.0
NO
50
108%
102%
6%
Carbon tetrachloride
ug/L
5.0
NO
50
112%
108%
4%
Benzene
ug/L
5.0
NO
50
100%
102%
2%
Trichloroethene
ug/L
5.0
NO
50
102%
102%
0%
1,2-Dichloropropane
ug/L
5.0
NO
50
104%
106%
2%
Dibromomethane
ug/L
5.0
NO
50
102%
100%
2%
Bromodichloromethane
ug/L
5.0
NO
50
104%
96%
8%
4-Methyl-2-pentanone (MIBK)
ug/L
50
NO
100
116%
96%
19%
cis-1,3-Dichloropropene
ug/L
5.0
NO
50
102%
88%
15%
Toluene
ug/L
5.0
ND
50
102%
98%
4%
trans-1,3-Dichloro-l-propene
ug/L
5.0
NO
50
104%
86%
19%
1,1,2-Trichloroethane
ug/L
5.0
NO
50
106%
100%
6%
2-Hexanone
ug/L
50
NO
100
114%
104%
9%
Dibromochloromethane
ug/L
5.0
ND
50
116%
108%
7%
Tetrachloroethylene
ug/L
5.0
NO
50
102%
106%
4%
1,2-Dibromoethane
ug/L
5.0
NO
50
112%
102%
9%
Chlorobenzene
ug/L
5.0
ND
50
98%
104%
6%
1,1,1,2-Tetrachloroethane
ug/L
5.0
NO
50
112%
108%
4%
Ethylbenzene
ug/L
5.0
ND
50
100%
104%
4%
REPORT OF
LABORATORY ANALYSIS
This report shall not be reproduced,
except in
full,
without the written
consent of Pace Analytical Services,
Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 17 PACE Project Number: A70828600
Client Reference: McDowell Co.
APPENDIX I, LANDFILL VOLATILES
Batch: 92 63609
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451225
93 0451233
SPIKE AND SPIKE DUPLICATE:
Spike
930451217
Spike
Dupl
Parameter
Xylenes, (total)
Units
ug/—L
PRL
-670-
MW #4
WD—
Spike
Recv
Recv
1
RPD
—7Y.
150
OUR
Styrene
ug/L
5.0
NO
50
96%
102%
6%
Bromoform
ug/L
5.0
ND
50
114%
112%
2%
1,1,2,2-Tetrachloroethane
ug/L
5.0
NO
50
110%
106%
4%
1,2,3-Trichloropropane
ug/L
5.0
ND
50
110%
108%
2%
trans-1,4-Dichloro-2-butene
ug/L
5.0
NO
50
102%
78%
27%
1,4-Dichlorobenzene
ug/L
5.0
NO
50
100%
100%
0%
1,2-Dichlorobenzene
ug/L
5.0
NO
50
98%
100%
2%
1,2-Dibromo-3-chloropropane
ug/L
5.0
IND
so
108%
98%
10%
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
PRL
Value
Recv
MetFY-T-CTIoride
T9 —7L
10--
20
120%
Chloroethene (Vinyl chloride)
ug/L
10
20
115%
Bromomethane
ug/L
10
20
130%
Chloroethane
ug/L
10
20
110%
Trichlorofluoromethane
ug/L
5.0
20
95%
Acetone
ug/L
100
40
150%
1,1-Dichloroethene
ug/L
5.0
20
105%
Methyl iodide
ug/L
5.0
40
80%
Acrylonitrile
ug/L
100
200
104%
Dichloromethane
ug/L
5.0
20
110%
Carbon disulfide
ug/L
5.0
40
100%
trans-1,2-Dichloroethene
ug/L
5.0
20
100%
1,1-Dichloroethane
ug/L
5.0
20
105%
Vinyl acetate
ug/L
50
40
55%
Methyl ethyl ketone
ug/L
100
40
145%
cis-1,2-Dichloroethene
ug/L
5.0
20
115%
Chloroform
ug/L
5.0
20
110%
Bromochloromethane
ug/L
5.0
20
105%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc,
54 Ravenscroft Drive
Pace Analytocal Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden QUALITY CONTROL DATA September 16, 1997
Page 18 PACE Project Number: A70828600
Client Reference: McDowell Co.
APPENDIX I, LANDFILL VOLATILES
Batch: 92 63609
Samples: 93 0451187, 93 0451195, 93 0451209, 93 0451217, 93 0451225
93 0451233
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
PRL
Value
Recv
1,1,1-Trichloroethane
—U9—/ 1-
5-.-0
—1-0—
-1 —107'.
1,2-Dichloroethane
ug/L
5.0
20
110%
Carbon tetrachloride
ug/L
5.0
20
110%
Benzene
ug/L
5.0
20
105%
Trichloroethene
ug/L
5.0
20
105%
1,2-Dichloropropane
ug/L
5.0
20
110%
Dibromomethane
ug/L
5.0
20
100%
Bromodichloromethane
ug/L
5.0
20
95%
4-Methyl-2-pentanone (MIBK)
ug/L
50
40
118%
cis-1,3-Dichloropropene
ug/L
5.0
20
105%
Toluene
ug/L
5.0
20
105%
trans-1,3-Dichloro-l-propene
ug/L
5.0
20
105%
1,1,2-Trichloroethane
ug/L
5.0
20
100%
2-Hexanone
ug/L
50
40
108%
Dibromochloromethane
ug/L
5.0
20
95%
Tetrachloroethylene
ug/L
5.0
20
90%
1,2-Dibromoethane
ug/L
5.0
20
90%
Chlorobenzene
ug/L
5.0
20
95%
1,1,1,2-Tetrachloroethane
ug/L
5.0
20
100%
Ethylbenzene
ug/L
5.0
20
95%
Xylenes, (total)
ug/L
5.0
60
90%
Styrene
ug/L
5.0
20
95%
Bromoform
ug/L
5.0
20
95%
1,1,2,2-Tetrachloroethane
ug/L
5.0
20
100%
1,2,3-Trichloropropane
ug/L
5.0
20
95%
trans-1,4-Dichloro-2-butene
ug/L
5.0
20
90%
1,4-Dichlorobenzene
ug/L
5.0
20
110%
1,2-Dichlorobenzene
ug/L
5.0
20
105%
1,2-Dibromo-3-chloropropane
ug/L
5.0
20
110%
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscraft Drive
Pace Analytical Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Mr. Mike Gladden FOOTNOTES September 16, 1997
Page 19 for pages 14 through 18 PACE Project Number: A70828600
Client Reference: McDowell Co.
NO Not detected at or above the PRL.
PRL PACE Reporting Limit
RPD Relative Percent Difference
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

CHAIN -OF -CUSTODY RECORD
Analutirnt
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Turn around Time
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Sampled By (PRINT):
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Ir PRESERVATIVES
— — — —
ANALYSES
REQUEST
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TIME MATRIX PACE NO.
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REMARKS
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TIME ACCEPTED
BY/AFFILIATI N
Additional Comments
SAMPLE CONDITION
Temp: - _-C
Received on Ice: Y / N
I SealedCooler: Y/N
Samplesintact:
Y/N
pH
2 SEE REVERSE SIDE FOR INSTRUCTIONS

NC DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
Division of Solid waste Kanagement
Solid Waste Section
SOLID WASTE K&KAGENENT FACILITY EVALLATION REPORT
Type of Facility.
ame of Facility
ate of Last Evaluation
I- Permit Conditions Followed
A- Specific Condition(s) Violated.
Permit #
Yes -RO N/A
II. Operational Requirements Followed Yes No
15A N-C. Admin. Code 138 Section
A- Specific VioLation(s) by number and letter.
III- Other Violations of Rule or Law
IV. Evaluator's Comments
county.
Location
V. Continuation Page Required? Yes No Receiving Signature
Evaluation Date
Solid Waste Section
DEHUR 3793 (Part I White: Facility Part II Canary: Central Office Part III Pink: RegionaL Office)
Solid Waste Section (Review 71%)