6002_Mecklenburg_HolbrooksRoad_MSWLF_Sept2021GW_FID1624138_20211109

DENR USE ONLY: I I Liraper Report LJUlectronic
NC DENR
Division of Waste Management - Solid Waste
Email Cu (data loaded: Yes / No
Notice: This
form and
any
information attached
to it are "Public Records"
as defined in NC
Gene
available for
inspection
and
examination by any
person upon request (NC
General Statute 132-6).
Doc/Event #:
Environmental Monitoring
Reporting Form
such, these documents are
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646,
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owne
Mecklenburg County Solid Waste Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Amber R. Grzymski, P.G. Phone: [phone]
E-mail: [e-mail]
Facility name:
Holbrooks Road Landfill
Facility Address:
15401 Holbrooks Road
NC Landfill Rule:
Facility Permit # (.0500 or .1600)
60-02 .0500
Actual sampling dates (e.g.,
October 20-24, 2006)
ber 28-29, 2021,
Environmental Status: (Check all that apply)
Initial/Background Monitoring ❑X Detection Monitoring � Assessment Monitoring � Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data El
water monitoring data
Notification attached?
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
No. No groundwater or surface water standards were exceeded.
)( Yes, a nocation of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levelsand a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
,
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
mber R. Grzymski, P.G. Project Manager 980-314-3855
A
tHrea koael i eiepnone ivumoer
Affix NC Licensed/ Professional Geologist Seal
2145 Suttle Ave, Charlotte, NC 28208
Facility Representative Address
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009

1EUKUE1Nt5U1 U COUNTY
Land Use and Environmental Services Agency
Solid Waste Services
November 9, 2021
Jacl07 Drummond
North Carolina Department of Environment
and Natural Resources
Division of Waste Management
2090 US Highway 70
Swannanoa, NC 28778
Subject: Holbrooks Road Landfill Permit 60-02
Semi-annual Monitoring Results
Dear Ms. Drummond:
Mecklenburg County conducted semi-annual water quality monitoring at the closed
Holbrooks Road Landfill in September 28-29, 2021 in accordance with the approved
sample and analysis plan dated March 27, 2003. This report details the results of that
monitoring event. Laboratory analytical data, field -measured data table of values
exceeding 2L standards and landfill gas monitoring data is contained on the electronic
data deliverable submittal.
Samples were collected from fourteen (14) monitoring wells (HRW-7, HRW-8, HRW-
9R, HRW-10, HRW-11 R, HRW-12, HRW-13, HRW-14, HRW-15, HRW-16, HRW-17,
HRW-18, HRW-19, HRW-20, and HRW-21) and three (3) surface -water sampling
locations (HRSW-2, HRSW-3 and HRSW4). Samples were analyzed for metals and
volatile organic compounds ("VOCs") listed in Appendix I of 40 CFR Part
258.54 "Detection monitoring program". Samples were also analyzed for 1,4-Dioxane
as required as of July 1, 2018. Field measurements of temperature, pH, and specific
conductivity were made at each sampling location using a calibrated instrument.
Additionally, measurements of dissolved oxygen were made at each surface -water
sampling location.
The electronic data deliverable package containing the monitoring data is labeled to
reflect the units used for reporting. Surface water standards listed are the water quality
standards established for freshwater classification for aquatic life as outlined in 15A
NCAC 2B "Classification and Water Quality Standards Applicable to Surface Waters of
North Carolina". Groundwater standards listed are the standards outlined in 15A NCAC
2L "Classification of Water Quality Standards applicable to the Groundwaters of North
Carolina". If the sample is reported in parts per billion, then the standard is also reported
in parts per billion.
PEOPLE •PRIDE PROGRESS •PARTNERSHIP
2145 Suttle Ave •Charlotte, North Carolina 28208 • [phone]
www.wi peouhvaste0 com

Page 2
Surface -water samples.
No VOCs were detected in any of the samples collected fiom the three surface -water
sampling locations (HRSW-2, HRSW-4 and HRSW-3). Barium was detected in all three
sampling locations below the 2B standards at 3 8.0, 3 8.4 and 40.1 ug/l, respectively. All
field -measured parameters were within the established regulatory limits. The following
table summarizes field -measured parameters for surface water samples.
Sample Location
Temp.
°C
pH
S.U.
Specific Conductivity
ms/cm
Dissolved Oxygen
mg/1
HRSW-2 upstream
17.7
7.1
0.270
6.50
HRSW-4 mid -stream
17.7
7.1
0.269
7.31
HRSW-3 downstream
17.2
6.9
0.283
T06
Groundwater samples:
Metals were detected in various wells above the 21 standard. The following table
summarizes metals detection for groundwater samples.
Wel1ID
As
ug/l
Ba
ug/l
Cd
ug/l
Cr
ug/l
Co
ug/1
Cu
ug/l
Pb
ug/l
Ni
ug/1
Sb
ug/1
Se
ug/l
Vn
ug/1
Zn
ug/1
HRW-7
-----
204
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-8
-----
260
-----
5.7
39.1
10.3
-----
8.0
-----
-----
49.2
21.8
HRW-9R
-----
344
-----
-----
8.8
8.5
5.4
-----
-----
-----
77.1
-----
HRW-10
-----
210
-----
-----
-----
-----
-----
11.8
-----
-----
-----
-----
HRW41R-----
385
-----
-----
29.7
-----
-----
81.2
-----
-----
-----
-----
HRW42
-----
875
1.1
-----
58.9
38.8
7.2
183
-----
----
5.2
-----
HRW43-----
190
-----
-----
-----
7.7
----
-----
-----
-----
6.1
-----
HRW44-----
38.1
-----
-----
-----
-----
-----
-----
-----
-----
9.8
-----
HRW45
-----
140
-----
13.0
7.7
90.3
8.1
5.8
-----
-----
73A
44.3
HRW-16
-----
156
-----
6.2
-----
16.7
-----
-----
-----
-----
25.4
14.6
HRW47-----
62.8
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-18
-----
321
-----
-----
7.1
-----
-----
6.2
-----
-----
-----
-----
HRW49
-----
92.5
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-20
-----
110
-----
-----
-----
-----
-----
-----
-----
-----
6.0
-----
HRW-21
-----
76.3
-----
-----
-----
-----
-----
-----
-----
-----
5.5
-----
21, Std.
10
700
2
10
1
100
15
100
1
20
0.3
1,000
Note: Results shown in bold exceed the 21, standard.

Page 3
VOCs were detected in twelve monitoring wells; HRW-7, HRW-8, HRW-9R, HRW-10,
HRW-11R, HRW42, HRW44, HRW45, HRW46, HRW-17, HRW-18 and HRW-20.
1,4-Dioxane was detected above the 21 standard in six monitoring wells.
The fnllnwina table snmmari7es V(�C; detections.
Well ID
Volatile Constituent
Concentration
2L Standard
u/1
u/1
HRW-7
Benzene
1.7
1
cis-1,2-Dichloroethene
8.04
70
Trichloroethene
1.61
3
Vinyl Chloride
09716
0.03
HRW-8
1,1-Dichloroethane
2040
6
HRW-9R
Benzene
0.667
1
Carbon disulfide
0.846
700
Chlorobenzene
1.96
50
1,2-Dichorobenzene
2.76
20
1,4-Dichlorobenzene
3.44
6
1,1-Dichloroethane
37.0
6
1,2-Dichloroethane
2.71
0.4
cis- 1,2-Dichloroethene
65.3
70
trans4,2-Dichloroethene
0.978
100
1,2-Dichloropropane
199
096
Trichloroethene
1.64
3
Vinyl chloride
9924
0.03
1,4=Dioxane
1009
3
HRW40
Chlorobenzene
1.69
50
1,4=Dioxane
8.06
3
HRW-l1R
Benzene
0.848
1
Chlorobenzene
12.5
50
1,2-Dichlorobenzene
0.697
20
1,4-Dichlorobezene
2.40
6
1,1-Dichloroethane
0.907
6
1,4-Dioxane
196
3
HRW42
Benzene
0.846
1
Chlorobenzene
9.63
50
1,2-Dichlorobenzene
0.524
20
1,4-Dichlorobenzene
2.59
6
1,1-Dichloroethane
9979
6
1,4-Dioxane
180
3
HRW44
Tetrachloroethene
1921
0.7
HRW-15
1,1-Dichloroethane
0.883
6
Tetrachloroethene
0.959
0.7
HRW46
1,1-Dichloroethane
2.95
6
Vinyl Chloride
0.611
0.03
194-Dioxane
8994
3
HRW-17
1,1-Dichloroethane
1.42
6

Well ID
Volatile Constituent
Concentration
u/1
2L Standard
u/1
HRW4 8
Benzene
1.34
1
Carbon disulfide
0.826
700
Chlorobenzene
4.97
50
IA-Dichlorobenzene
4.92
6
1,1-Dichloroethane
28.4
6
cis-1, 2-Dichloroethene
1.75
70
1,2-Dichloropropane
4.31
0.6
Vinyl Chloride
12.5
0.03
1,4-Dioxane
5.92
3
FIR)-20
1,1-Dichloroethane
4.86
6
Note: Results shown in bold exceed the 2L standard.
Measurements of pH were more acidic than the 2L standard range of 6.5 to 8.5 standard
units at locations HRW-7, HRW4, HRW-9R, HRW-11R, HRW43, HRW-15, HRW-
16, HRW-19, HRW-20 and HRW-21. Field- measured parameters for groundwater
samples are summarized in the following table.
Sample Location
Tem . °C
PH
Specific Conductivity ms/cm
HRW-7
20.7
6.4
0.620
HRW4
16.3
6.0
0.284
HRW-91Z
16.2
6.3
1.212
HRW40
18.3
6.6
0.887
HRW-11R
17.7
6.3
2.360
HRW42
15.8
6.5
2.236
HRW-13
17.7
5.9
0.436
HRW44
17.3
6.1
0.221
HRW4 5
17.5
6.3
0.244
HRW4 6
18.4
6.2
0.264
HRW-17
17.6
6.8
0.183
HRW4 8
20.1
6.5
1.243
HRW4 9
17.7
6.4
0.343
HRW-20
16.8
6.1
0.369
HRW-21
17.7
5.9
0.533
Note: Results shown in bold are outside of the 2L standard range of 6.5 - 8.5 S.U.
Please contact me at amber.grz�(e,meciclenbur countyno,gov or [phone] if
you have any questions regarding this report.
sincerely_
Project Manager
Solid Waste Services

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leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
October 18, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 28, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 25

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21LA 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92563725001 6002-HRW10
EPA 6010D
IDS
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92563725002 6002-HRW11R
EPA 6010D
DS
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92563725003 6002-HRW12
EPA 6010D
IDS
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92563725004 6002-HRW13
EPA 6010D
IDS
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92563725005 6002-HRW17
EPA 6010D
IDS
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Sample: 6002-HRW10
Lab ID: 92563725001 Collected:
09/28/21 14:30
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:33
7440-36-0 BC
Arsenic
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:33
7440-38-2
Barium
210
ug/L
5.0
1
09/29/2102:00
10/01/2123:33
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:33
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:33
7440-43-9
Chromium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:33
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:33
7440-48-4
Copper
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:33
7440-50-8
Lead
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:33
7439-92-1
Nickel
11.8
ug/L
5.0
1
09/29/2102:00
10/01/2123:33
7440-02-0
Selenium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:33
7782-49-2
Silver
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:33
7440-22-4
Thallium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:33
7440-28-0
Vanadium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:33
7440-62-2
Zinc
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:33
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/29/21 10:37
09/29/21 18:37
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation Method:
8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/09/21 00:52
10/09/21 00:52
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/09/21 00:52
10/09/21 00:52
107-13-1
Benzene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
74-97-5
Bromoform
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/09/21 00:52
10/09/21 00:52
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
56-23-5 LO
Chlorobenzene
1.69
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/09/21 00:52
10/09/21 00:52
75-00-3
Chloroform
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/09/21 00:52
10/09/21 00:52
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/09/21 00:52
10/09/21 00:52
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/09/21 00:52
10/09/21 00:52
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
106-46-7
1,1-Dichloroethane
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Sample: 6002-HRW10
Lab ID: 92563725001
Collected: 09/28/21
14:30
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/09/21 00:52
10/09/21 00:52
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/09/21 00:52
10/09/21 00:52
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/09/21 00:52
10/09/21 00:52
591-78-6
lodomethane
ND
ug/L
5.00
1
10/09/21 00:52
10/09/21 00:52
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/09/21 00:52
10/09/21 00:52
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/09/21 00:52
10/09/21 00:52
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/09/21 00:52
10/09/21 00:52
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/09/21 00:52
10/09/21 00:52
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
127-18-4
Toluene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/09/21 00:52
10/09/21 00:52
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/09/21 00:52
10/09/21 00:52
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/09/21 00:52
10/09/21 00:52
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/09/21 00:52
10/09/21 00:52
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/09/21 00:52
10/09/21 00:52
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/09/21 00:52
10/09/21 00:52
179601-23-1
Surrogates
Toluene-d8 (S)
96.1
%
80.0-120
1
10/09/21 00:52
10/09/21 00:52
2037-26-5
4-Bromofluorobenzene (S)
90.4
%
77.0-126
1
10/09/21 00:52
10/09/21 00:52
460-00-4
1,2-Dichloroethane-d4 (S)
126
%
70.0-130
1
10/09/21 00:52
10/09/21 00:52
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method: EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
8.06
ug/L
3.00
1
10/12/21 18:59
10/12/21 18:59
123-91-1
Surrogates
Toluene-d8 (S)
100
%
77.0-127
1
10/12/21 18:59
10/12/21 18:59
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in
full,
Date: 10/18/2021 11:04 AM
without
the written
consent of Pace Analytical
Services, LLC.
Page 5 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Sample: 6002-HRW11R
Lab ID: 92563725002 Collected:
09/28/21 13:15
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:37
7440-36-0 BC
Arsenic
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:37
7440-38-2
Barium
477
ug/L
5.0
1
09/29/2102:00
10/01/2123:37
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:37
7440-41-7
Cadmium
1.0
ug/L
1.0
1
09/29/2102:00
10/01/2123:37
7440-43-9
Chromium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:37
7440-47-3
Cobalt
29.7
ug/L
5.0
1
09/29/2102:00
10/01/2123:37
7440-48-4
Copper
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:37
7440-50-8
Lead
7.0
ug/L
5.0
1
09/29/2102:00
10/01/2123:37
7439-92-1
Nickel
81.2
ug/L
5.0
1
09/29/2102:00
10/01/2123:37
7440-02-0
Selenium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:37
7782-49-2
Silver
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:37
7440-22-4
Thallium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:37
7440-28-0
Vanadium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:37
7440-62-2
Zinc
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:37
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/29/21 10:37
09/29/21 18:55
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation Method:
8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/09/21 01:12
10/09/21 01:12
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/09/21 01:12
10/09/21 01:12
107-13-1
Benzene
0.848
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
74-97-5
Bromoform
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/09/21 01:12
10/09/21 01:12
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
56-23-5 LO
Chlorobenzene
12.5
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/09/21 01:12
10/09/21 01:12
75-00-3
Chloroform
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/09/21 01:12
10/09/21 01:12
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/09/21 01:12
10/09/21 01:12
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/09/21 01:12
10/09/21 01:12
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
74-95-3
1,2-Dichlorobenzene
0.697
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
541-73-1
1,4-Dichlorobenzene
2.40
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
106-46-7
1,1-Dichloroethane
0.907
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Sample: 6002-HRW11R
Lab ID: 92563725002
Collected: 09/28/21
13:15
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/09/21 01:12
10/09/21 01:12
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/09/21 01:12
10/09/21 01:12
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/09/21 01:12
10/09/21 01:12
591-78-6
lodomethane
ND
ug/L
5.00
1
10/09/21 01:12
10/09/21 01:12
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/09/21 01:12
10/09/21 01:12
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/09/21 01:12
10/09/21 01:12
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/09/21 01:12
10/09/21 01:12
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/09/21 01:12
10/09/21 01:12
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
127-18-4
Toluene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/09/21 01:12
10/09/21 01:12
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/09/21 01:12
10/09/21 01:12
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/09/21 01:12
10/09/21 01:12
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/09/21 01:12
10/09/21 01:12
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/09/21 01:12
10/09/21 01:12
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/09/21 01:12
10/09/21 01:12
179601-23-1
Surrogates
Toluene-d8 (S)
96.7
%
80.0-120
1
10/09/21 01:12
10/09/21 01:12
2037-26-5
4-Bromofluorobenzene (S)
88.4
%
77.0-126
1
10/09/21 01:12
10/09/21 01:12
460-00-4
1,2-Dichloroethane-d4 (S)
123
%
70.0-130
1
10/09/21 01:12
10/09/21 01:12
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method: EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
196
ug/L
3.00
1
10/12/21 19:19
10/12/21 19:19
123-91-1
Surrogates
Toluene-d8 (S)
103
%
77.0-127
1
10/12/21 19:19
10/12/21 19:19
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in
full,
Date: 10/18/2021 11:04 AM
without
the written
consent of Pace Analytical
Services, LLC.
Page 7 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Sample: 6002-HRW12
Lab ID: 92563725003 Collected:
09/28/21 13:25
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:40
7440-36-0 BC
Arsenic
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:40
7440-38-2
Barium
875
ug/L
5.0
1
09/29/2102:00
10/01/2123:40
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:40
7440-41-7
Cadmium
1.1
ug/L
1.0
1
09/29/2102:00
10/01/2123:40
7440-43-9
Chromium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:40
7440-47-3
Cobalt
58.9
ug/L
5.0
1
09/29/2102:00
10/01/2123:40
7440-48-4
Copper
38.8
ug/L
5.0
1
09/29/2102:00
10/01/2123:40
7440-50-8
Lead
7.2
ug/L
5.0
1
09/29/2102:00
10/01/2123:40
7439-92-1
Nickel
183
ug/L
5.0
1
09/29/2102:00
10/01/2123:40
7440-02-0
Selenium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:40
7782-49-2
Silver
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:40
7440-22-4
Thallium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:40
7440-28-0
Vanadium
5.2
ug/L
5.0
1
09/29/2102:00
10/01/2123:40
7440-62-2
Zinc
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:40
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/29/21 10:37
09/29/21 18:59
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation Method:
8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/09/21 01:32
10/09/21 01:32
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/09/21 01:32
10/09/21 01:32
107-13-1
Benzene
0.846
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
74-97-5
Bromoform
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/09/21 01:32
10/09/21 01:32
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
56-23-5 LO
Chlorobenzene
9.63
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/09/21 01:32
10/09/21 01:32
75-00-3
Chloroform
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/09/21 01:32
10/09/21 01:32
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/09/21 01:32
10/09/21 01:32
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/09/21 01:32
10/09/21 01:32
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
74-95-3
1,2-Dichlorobenzene
0.524
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
541-73-1
1,4-Dichlorobenzene
2.59
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
106-46-7
1,1-Dichloroethane
9.79
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Sample: 6002-HRW12
Lab ID: 92563725003
Collected: 09/28/21
13:25
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/09/21 01:32
10/09/21 01:32
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/09/21 01:32
10/09/21 01:32
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/09/21 01:32
10/09/21 01:32
591-78-6
lodomethane
ND
ug/L
5.00
1
10/09/21 01:32
10/09/21 01:32
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/09/21 01:32
10/09/21 01:32
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/09/21 01:32
10/09/21 01:32
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/09/21 01:32
10/09/21 01:32
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/09/21 01:32
10/09/21 01:32
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
127-18-4
Toluene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/09/21 01:32
10/09/21 01:32
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/09/21 01:32
10/09/21 01:32
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/09/21 01:32
10/09/21 01:32
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/09/21 01:32
10/09/21 01:32
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/09/21 01:32
10/09/21 01:32
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/09/21 01:32
10/09/21 01:32
179601-23-1
Surrogates
Toluene-d8 (S)
96.4
%
80.0-120
1
10/09/21 01:32
10/09/21 01:32
2037-26-5
4-Bromofluorobenzene (S)
91.3
%
77.0-126
1
10/09/21 01:32
10/09/21 01:32
460-00-4
1,2-Dichloroethane-d4 (S)
128
%
70.0-130
1
10/09/21 01:32
10/09/21 01:32
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method: EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
180
ug/L
3.00
1
10/12/21 19:39
10/12/21 19:39
123-91-1
Surrogates
Toluene-d8 (S)
102
%
77.0-127
1
10/12/21 19:39
10/12/21 19:39
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in
full,
Date: 10/18/2021 11:04 AM
without
the written
consent of Pace Analytical
Services, LLC.
Page 9 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Sample: 6002-HRW13
Lab ID: 92563725004 Collected:
09/28/21 13:45
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:43
7440-36-0 BC
Arsenic
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:43
7440-38-2
Barium
190
ug/L
5.0
1
09/29/2102:00
10/01/2123:43
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:43
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:43
7440-43-9
Chromium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:43
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:43
7440-48-4
Copper
7.7
ug/L
5.0
1
09/29/2102:00
10/01/2123:43
7440-50-8
Lead
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:43
7439-92-1
Nickel
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:43
7440-02-0
Selenium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:43
7782-49-2
Silver
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:43
7440-22-4
Thallium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:43
7440-28-0
Vanadium
6.1
ug/L
5.0
1
09/29/2102:00
10/01/2123:43
7440-62-2
Zinc
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:43
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/29/21 10:37
09/29/21 19:02
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation Method:
8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/09/21 01:53
10/09/21 01:53
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/09/21 01:53
10/09/21 01:53
107-13-1
Benzene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
74-97-5
Bromoform
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/09/21 01:53
10/09/21 01:53
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
56-23-5 LO
Chlorobenzene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/09/21 01:53
10/09/21 01:53
75-00-3
Chloroform
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/09/21 01:53
10/09/21 01:53
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/09/21 01:53
10/09/21 01:53
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/09/21 01:53
10/09/21 01:53
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
106-46-7
1,1-Dichloroethane
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Sample: 6002-HRW13
Lab ID: 92563725004
Collected: 09/28/21
13:45
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/09/21 01:53
10/09/21 01:53
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/09/21 01:53
10/09/21 01:53
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/09/21 01:53
10/09/21 01:53
591-78-6
lodomethane
ND
ug/L
5.00
1
10/09/21 01:53
10/09/21 01:53
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/09/21 01:53
10/09/21 01:53
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/09/21 01:53
10/09/21 01:53
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/09/21 01:53
10/09/21 01:53
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/09/21 01:53
10/09/21 01:53
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
127-18-4
Toluene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/09/21 01:53
10/09/21 01:53
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/09/21 01:53
10/09/21 01:53
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/09/21 01:53
10/09/21 01:53
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/09/21 01:53
10/09/21 01:53
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/09/21 01:53
10/09/21 01:53
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/09/21 01:53
10/09/21 01:53
179601-23-1
Surrogates
Toluene-d8 (S)
93.1
%
80.0-120
1
10/09/21 01:53
10/09/21 01:53
2037-26-5
4-Bromofluorobenzene (S)
90.0
%
77.0-126
1
10/09/21 01:53
10/09/21 01:53
460-00-4
1,2-Dichloroethane-d4 (S)
126
%
70.0-130
1
10/09/21 01:53
10/09/21 01:53
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method:
EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane) ND ug/L 3.00 1 10/12/21 12:35 10/12/21 12:35 123-91-1
Surrogates
Toluene-d8 (S) 99.1 % 77.0-127 1 10/12/21 12:35 10/12/21 12:35 2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Sample: 6002-HRW17
Lab ID: 92563725005 Collected:
09/28/21 14:05
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:47
7440-36-0 BC
Arsenic
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:47
7440-38-2
Barium
62.8
ug/L
5.0
1
09/29/2102:00
10/01/2123:47
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:47
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:47
7440-43-9
Chromium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:47
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:47
7440-48-4
Copper
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:47
7440-50-8
Lead
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:47
7439-92-1
Nickel
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:47
7440-02-0
Selenium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:47
7782-49-2
Silver
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:47
7440-22-4
Thallium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:47
7440-28-0
Vanadium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:47
7440-62-2
Zinc
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:47
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/29/21 10:37
09/29/21 19:13
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation Method:
8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/09/21 02:13
10/09/21 02:13
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/09/21 02:13
10/09/21 02:13
107-13-1
Benzene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
74-97-5
Bromoform
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/09/21 02:13
10/09/21 02:13
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
56-23-5 LO
Chlorobenzene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/09/21 02:13
10/09/21 02:13
75-00-3
Chloroform
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/09/21 02:13
10/09/21 02:13
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/09/21 02:13
10/09/21 02:13
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/09/21 02:13
10/09/21 02:13
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
106-46-7
1,1-Dichloroethane
1.42
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
Sample: 6002-HRW17
Lab ID: 92563725005
Collected: 09/28/21
14:05
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/09/21 02:13
10/09/21 02:13
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/09/21 02:13
10/09/21 02:13
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/09/21 02:13
10/09/21 02:13
591-78-6
lodomethane
ND
ug/L
5.00
1
10/09/21 02:13
10/09/21 02:13
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/09/21 02:13
10/09/21 02:13
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/09/21 02:13
10/09/21 02:13
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/09/21 02:13
10/09/21 02:13
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/09/21 02:13
10/09/21 02:13
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
127-18-4
Toluene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/09/21 02:13
10/09/21 02:13
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/09/21 02:13
10/09/21 02:13
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/09/21 02:13
10/09/21 02:13
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/09/21 02:13
10/09/21 02:13
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/09/21 02:13
10/09/21 02:13
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/09/21 02:13
10/09/21 02:13
179601-23-1
Surrogates
Toluene-d8 (S)
98.1
%
80.0-120
1
10/09/21 02:13
10/09/21 02:13
2037-26-5
4-Bromofluorobenzene (S)
90.1
%
77.0-126
1
10/09/21 02:13
10/09/21 02:13
460-00-4
1,2-Dichloroethane-d4 (S)
131
%
70.0-130
1
10/09/21 02:13
10/09/21 02:13
17060-07-0 ST
VOA (GC/MS) 8260D-SIM
Analytical Method: EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
ND
ug/L
3.00
1
10/12/21 12:55
10/12/21 12:55
123-91-1
Surrogates
Toluene-d8 (S)
99.9
%
77.0-127
1
10/12/21 12:55
10/12/21 12:55
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in
full,
Date: 10/18/2021 11:04 AM
without
the written
consent of Pace Analytical
Services, LLC.
Page 13 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
QC Batch: 649812 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92563725001, 92563725002, 92563725003, 92563725004, 92563725005
METHOD BLANK: 3408194 Matrix: Water
Associated Lab Samples: 92563725001, 92563725002, 92563725003, 92563725004, 92563725005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony
ug/L
ND
5.0
10/02/2104:28
Arsenic
ug/L
ND
10.0
10/02/2104:28
Barium
ug/L
ND
5.0
10/02/2104:28
Beryllium
ug/L
ND
1.0
10/02/2104:28
Cadmium
ug/L
ND
1.0
10/02/2104:28
Chromium
ug/L
ND
5.0
10/02/2104:28
Cobalt
ug/L
ND
5.0
10/02/2104:28
Copper
ug/L
ND
5.0
10/02/2104:28
Lead
ug/L
ND
5.0
10/02/2104:28
Nickel
ug/L
ND
5.0
10/02/2104:28
Selenium
ug/L
ND
10.0
10/02/2104:28
Silver
ug/L
ND
5.0
10/02/2104:28
Thallium
ug/L
ND
10.0
10/02/2104:28
Vanadium
ug/L
ND
5.0
10/02/2104:28
Zinc
ug/L
ND
10.0
10/02/2104:28
LABORATORY CONTROL SAMPLE:
Parameter
3408195
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
492
98
80-120
Arsenic
ug/L
500
502
100
80-120
Barium
ug/L
500
496
99
80-120
Beryllium
ug/L
500
488
98
80-120
Cadmium
ug/L
500
497
99
80-120
Chromium
ug/L
500
483
97
80-120
Cobalt
ug/L
500
459
92
80-120
Copper
ug/L
500
485
97
80-120
Lead
ug/L
500
495
99
80-120
Nickel
ug/L
500
478
96
80-120
Selenium
ug/L
500
498
100
80-120
Silver
ug/L
250
241
96
80-120
Thallium
ug/L
500
489
98
80-120
Vanadium
ug/L
500
484
97
80-120
Zinc
ug/L
500
502
100
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
60-02 Holbrooks Rd Landfill
92563725
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3408196
3408197
MS
MSD
92563460001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
518
504
103
101
75-125
3
Arsenic
ug/L
ND
500
500
525
508
105
101
75-125
3
Barium
ug/L
12.9
500
500
524
510
102
99
75-125
3
Beryllium
ug/L
ND
500
500
507
492
101
98
75-125
3
Cadmium
ug/L
ND
500
500
508
495
102
99
75-125
3
Chromium
ug/L
ND
500
500
494
479
99
96
75-125
3
Cobalt
ug/L
8.8
500
500
486
472
95
93
75-125
3
Copper
ug/L
113
500
500
603
583
98
94
75-125
3
Lead
ug/L
ND
500
500
506
493
101
98
75-125
3
Nickel
ug/L
5.7
500
500
494
480
98
95
75-125
3
Selenium
ug/L
ND
500
500
534
519
106
103
75-125
3
Silver
ug/L
ND
250
250
247
242
99
97
75-125
2
Thallium
ug/L
ND
500
500
504
490
101
98
75-125
3
Vanadium
ug/L
ND
500
500
503
489
101
98
75-125
3
Zinc
ug/L
ND
500
500
523
508
103
100
75-125
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
QC Batch: 649884 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92563725001, 92563725002, 92563725003, 92563725004, 92563725005
METHOD BLANK: 3408337
Matrix:
Water
Associated Lab Samples: 92563725001, 92563725002, 92563725003, 92563725004, 92563725005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.47
09/29/2118:30
LABORATORY CONTROL SAMPLE:
3408338
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
26.3
105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3408339 3408340
MS MSD
92563725001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 25.1 25.9 100 103 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC.
Page 16 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
QC Batch: 1753823 Analysis Method: EPA 8260D
QC Batch Method: 8260B Analysis Description: VOA (GC/MS) 8260D
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92563725001, 92563725002, 92563725003, 92563725004, 92563725005
METHOD BLANK: R3714680-3 Matrix: Water
Associated Lab Samples: 92563725001, 92563725002, 92563725003, 92563725004, 92563725005
Blank Reporting
Parameter Units Result Limit Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1,1-Trichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1,2,2-Tetrachloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1,2-Trichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1-Dichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1-Dichloroethene
ug/L
ND
0.500
10/08/21 20:27
1,1-Dichloropropene
ug/L
ND
0.500
10/08/21 20:27
1,2,3-Trichloropropane
ug/L
ND
2.50
10/08/21 20:27
1,2-Dibromo-3-chloropropane
ug/L
ND
2.50
10/08/21 20:27
1,2-Dibromoethane (EDB)
ug/L
ND
0.500
10/08/21 20:27
1,2-Dichlorobenzene
ug/L
ND
0.500
10/08/21 20:27
1,2-Dichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,2-Dichloropropane
ug/L
ND
0.500
10/08/21 20:27
1,3-Dichlorobenzene
ug/L
ND
0.500
10/08/21 20:27
1,3-Dichloropropane
ug/L
ND
1.00
10/08/21 20:27
1,4-Dichlorobenzene
ug/L
ND
0.500
10/08/21 20:27
2-Butanone (MEK)
ug/L
ND
5.00
10/08/21 20:27
2-Hexanone
ug/L
ND
5.00
10/08/21 20:27
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.00
10/08/21 20:27
Acetone
ug/L
ND
25.0
10/08/21 20:27
Acrylonitrile
ug/L
ND
5.00
10/08/21 20:27
Benzene
ug/L
ND
0.500
10/08/21 20:27
Bromochloromethane
ug/L
ND
0.500
10/08/21 20:27
Bromodichloromethane
ug/L
ND
0.500
10/08/21 20:27
Bromoform
ug/L
ND
0.500
10/08/21 20:27
Bromomethane
ug/L
ND
2.50
10/08/21 20:27
Carbon disulfide
ug/L
ND
0.500
10/08/21 20:27
Carbon tetrachloride
ug/L
ND
0.500
10/08/21 20:27
Chlorobenzene
ug/L
ND
0.500
10/08/21 20:27
Dibromochloromethane
ug/L
ND
0.500
10/08/21 20:27
Chloroethane
ug/L
ND
2.50
10/08/21 20:27
Chloroform
ug/L
ND
0.500
10/08/21 20:27
Chloromethane
ug/L
ND
1.25
10/08/21 20:27
Chloroprene
ug/L
ND
50.0
10/08/21 20:27
cis-1,2-Dichloroethene
ug/L
ND
0.500
10/08/21 20:27
cis-1,3-Dichloropropene
ug/L
ND
0.500
10/08/21 20:27
Dibromomethane
ug/L
ND
0.500
10/08/21 20:27
Ethylbenzene
ug/L
ND
0.500
10/08/21 20:27
lodomethane
ug/L
ND
5.00
10/08/21 20:27
m&p-Xylene
ug/L
ND
1.00
10/08/21 20:27
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 25

leAnalyiical
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Huntersville, NC 28078
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QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
METHOD BLANK: R3714680-3 Matrix: Water
Associated Lab Samples: 92563725001, 92563725002, 92563725003, 92563725004, 92563725005
Blank Reporting
Parameter Units Result Limit Analyzed
Methylene Chloride
ug/L
ND
2.50
10/08/21 20:27
Naphthalene
ug/L
ND
2.50
10/08/21 20:27
o-Xylene
ug/L
ND
0.500
10/08/21 20:27
Styrene
ug/L
ND
0.500
10/08/21 20:27
Tetrachloroethene
ug/L
ND
0.500
10/08/21 20:27
Toluene
ug/L
ND
0.500
10/08/21 20:27
trans-1,2-Dichloroethene
ug/L
ND
0.500
10/08/21 20:27
trans- 1,3-Dichloropropene
ug/L
ND
0.500
10/08/21 20:27
trans-1,4-Dichloro-2-butene
ug/L
ND
5.00
10/08/21 20:27
Trichloroethene
ug/L
ND
0.500
10/08/21 20:27
Trichlorofluoromethane
ug/L
ND
2.50
10/08/21 20:27
Vinyl acetate
ug/L
ND
5.00
10/08/21 20:27
Vinyl chloride
ug/L
ND
0.500
10/08/21 20:27
Xylene (Total)
ug/L
ND
1.50
10/08/21 20:27
1,2-Dichloroethane-d4 (S)
%
129
70.0-130
10/08/21 20:27
Toluene-d8 (S)
%
94.9
80.0-120
10/08/21 20:27
4-Bromofluorobenzene (S)
%
91.6
77.0-126
10/08/21 20:27
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
R3714680-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
5.00
5.06
101
75.0-125
1,1,1-Trichloroethane
ug/L
5.00
6.13
123
73.0-124
1,1,2,2-Tetrachloroethane
ug/L
5.00
4.29
85.8
65.0-130
1,1,2-Trichloroethane
ug/L
5.00
5.00
100
80.0-120
1,1-Dichloroethane
ug/L
5.00
5.61
112
70.0-126
1,1-Dichloroethene
ug/L
5.00
5.05
101
71.0-124
1,1-Dichloropropene
ug/L
5.00
5.86
117
74.0-126
1,2,3-Trichloropropane
ug/L
5.00
5.04
101
73.0-130
1,2-Dibromo-3-chloropropane
ug/L
5.00
4.08
81.6
58.0-134
1,2-Dibromoethane (EDB)
ug/L
5.00
5.18
104
80.0-122
1,2-Dichlorobenzene
ug/L
5.00
5.10
102
79.0-121
1,2-Dichloroethane
ug/L
5.00
6.05
121
70.0-128
1,2-Dichloropropane
ug/L
5.00
5.28
106
77.0-125
1,3-Dichlorobenzene
ug/L
5.00
4.79
95.8
79.0-120
1,3-Dichloropropane
ug/L
5.00
5.97
119
80.0-120
1,4-Dichlorobenzene
ug/L
5.00
4.91
98.2
79.0-120
2-Butanone (MEK)
ug/L
25.0
27.2
109
44.0-160
2-Hexanone
ug/L
25.0
23.7
94.8
67.0-149
4-Methyl-2-pentanone (MIBK)
ug/L
25.0
27.8
111
68.0-142
Acetone
ug/L
25.0
29.7
119
19.0-160
Acrylonitrile
ug/L
25.0
26.0
104
55.0-149
Benzene
ug/L
5.00
5.37
107
70.0-123
Bromochloromethane
ug/L
5.00
5.08
102
76.0-122
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 25

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
LABORATORY CONTROL SAMPLE:
Parameter
R3714680-1
Units
Spike LCS
Conc. Result
Bromodichloromethane
ug/L
5.00
Bromoform
ug/L
5.00
Bromomethane
ug/L
5.00
Carbon disulfide
ug/L
5.00
Carbon tetrachloride
ug/L
5.00
Chlorobenzene
ug/L
5.00
Dibromochloromethane
ug/L
5.00
Chloroethane
ug/L
5.00
Chloroform
ug/L
5.00
Chloromethane
ug/L
5.00
cis-1,2-Dichloroethene
ug/L
5.00
cis-1,3-Dichloropropene
ug/L
5.00
Dibromomethane
ug/L
5.00
Ethylbenzene
ug/L
5.00
lodomethane
ug/L
25.0
m&p-Xylene
ug/L
10.0
Methylene Chloride
ug/L
5.00
Naphthalene
ug/L
5.00
o-Xylene
ug/L
5.00
Styrene
ug/L
5.00
Tetrachloroethene
ug/L
5.00
Toluene
ug/L
5.00
trans-1,2-Dichloroethene
ug/L
5.00
trans- 1,3-Dichloropropene
ug/L
5.00
trans-1,4-Dichloro-2-butene
ug/L
5.00
Trichloroethene
ug/L
5.00
Trichlorofluoromethane
ug/L
5.00
Vinyl acetate
ug/L
25.0
Vinyl chloride
ug/L
5.00
Xylene (Total)
ug/L
15.0
1,2-Dichloroethane-d4 (S)
%
Toluene-d8 (S)
%
4-Bromofluorobenzene (S)
%
LCS
% Rec
% Rec
Limits Qualifiers
5.55
111
75.0-120
5.31
106
68.0-132
4.30
86.0
10.0-160
5.89
118
61.0-128
6.33
127
68.0-126 LO
4.92
98.4
80.0-121
5.29
106
77.0-125
4.02
80.4
47.0-150
5.80
116
73.0-120
5.08
102
41.0-142
4.81
96.2
73.0-120
5.47
109
80.0-123
5.48
110
80.0-120
5.04
101
79.0-123
27.2
109
33.0-147
9.96
99.6
80.0-122
5.18
104
67.0-120
3.06
61.2
54.0-135
4.79
95.8
80.0-122
4.92
98.4
73.0-130
5.56
111
72.0-132
5.08
102
79.0-120
5.40
108
73.0-120
5.62
112
78.0-124
4.25
85.0
33.0-144
5.48
110
78.0-124
6.00
120
59.0-147
23.9
95.6
11.0-160
4.69
93.8
67.0-131
14.7
98.0
79.0-123
125
70.0-130
96.2
80.0-120
92.0
77.0-126
LABORATORY CONTROL SAMPLE:
R3714680-2
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Chloroprene
ug/L
50.0 45.1 90.2
60.0-143
1,2-Dichloroethane-d4 (S)
%
128
70.0-130
Toluene-d8 (S)
%
95.4
80.0-120
4-Bromofluorobenzene (S)
%
90.9
77.0-126
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
QC Batch: 1755301
Analysis Method: EPA 8260D by SIM
QC Batch Method: 8260B-SIM
Analysis Description: VOA (GC/MS) 8260D-SIM
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92563725001, 92563725002,
92563725003, 92563725004, 92563725005
METHOD BLANK: R3715967-3
Matrix: Water
Associated Lab Samples: 92563725001, 92563725002,
92563725003, 92563725004, 92563725005
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
1,4-Dioxane (p-Dioxane) ug/L
ND 3.00 10/12/21 12:00
Toluene-d8 (S) %
100 77.0-127 10/12/21 12:00
LABORATORY CONTROL SAMPLE & LCSD: R3715967-1 R3715967-2
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units
Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
1,4-Dioxane (p-Dioxane) ug/L
50.0 57.0 49.6 114 99.2 55.0-138 13.9 24
Toluene-d8 (S) %
100 100 77.0-127
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3715967-4 R3715967-5
MS MSD
L1414799-01
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
1,4-Dioxane (p-Dioxane) ug/L 39.2
50.0 50.0 93.3 91.8 108 105 13.0-160 1.62
Toluene-d8 (S) %
99.8 99.7 77.0-127
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92563725
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
ST Surrogate recovery was above laboratory control limits. Results may be biased high.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 25

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
60-02 Holbrooks Rd Landfill
92563725
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92563725001
6002-HRW10
EPA 3010A
649812
EPA6010D
649827
92563725002
6002-HRW11 R
EPA 3010A
649812
EPA6010D
649827
92563725003
6002-HRW12
EPA 3010A
649812
EPA6010D
649827
92563725004
6002-HRW13
EPA 3010A
649812
EPA6010D
649827
92563725005
6002-HRW17
EPA 3010A
649812
EPA6010D
649827
92563725001
6002-HRW10
EPA 3010A
649884
EPA6020B
649963
92563725002
6002-HRW11 R
EPA 3010A
649884
EPA 6020B
649963
92563725003
6002-HRW12
EPA 3010A
649884
EPA6020B
649963
92563725004
6002-HRW13
EPA 3010A
649884
EPA6020B
649963
92563725005
6002-HRW17
EPA 3010A
649884
EPA6020B
649963
92563725001
6002-HRW10
8260D
1753823
EPA 8260D
1753823
92563725002
6002-HRW11R
8260D
1753823
EPA 8260D
1753823
92563725003
6002-HRW12
8260D
1753823
EPA 8260D
1753823
92563725004
6002-HRW13
8260D
1753823
EPA 8260D
1753823
92563725005
6002-HRW17
8260D
1753823
EPA 8260D
1753823
92563725001
6002-HRW10
8260D-SIM
1755301
EPA 8260D by
SIM
1755301
92563725002
6002-HRW11R
8260D-SIM
1755301
EPA 8260D by
SIM
1755301
92563725003
6002-HRW12
8260D-SIM
1755301
EPA 8260D by
SIM
1755301
92563725004
6002-HRW13
8260D-SIM
1755301
EPA 8260D by
SIM
1755301
92563725005
6002-HRW17
8260D-SIM
1755301
EPA 8260D by
SIM
1755301
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/18/2021 11:04 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 25

Document Name: Document Revised: October 28, 2020
Analytical' Sample Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: issuing Authority:
F-CAR-CS-033•Rev.41 Pace Carolinas Quality office
Laboratory receiving samples;
Asheville ❑ Eden❑ Greenwood ❑ Huntersville K� Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑
Courier:
❑ Commercial
Custody Seal Present? []Yes Otto Seals Intact? []Yes QN0
proj�Ltect' 40# : 9256372F
ent
III111111111
92563125
__.., .,-uais rersan Examining Contents: L. c/9- 8 r
Packing Material: ❑Bubble Wrap 0(ubble Bags []None ❑ other Biological Tissue Fryzen? 1 l
Thermorneter� /� []Yes []NO QJ/A
L Q7Jet ❑blue []None
ype or ice:
� ��JJ Correction Factor:
Cooler Temp: Z�_ Add/Subtract (°C) y Temp should be above freezing to VC
❑5amplesout of temp criteria. Samples on ice, coaling process
Cooler Temp Corrected {'C}r has begun
USDA Regulated Sail ( 2N/A, water sample)
Did Sample$ originate in a quarantine Zone within the United 5tates: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationally,
Des ❑No including ilawauand Pue"licopEyes ❑No
Comm en is/oiscreoa n cv:
Chain of Custody Present?
Sam !es Arrived within Hold Time?
Short Hold Time Analysis (<72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers intact?
Llissolved analysis: Samples Field Filtered?
Sample Labels Match CDC?
-Includes Date/TimeilD/Analys
Headspace in VOA Vials (;,5-6mm;
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
LiYes
UNa
LJN/A
1 d.
Os
❑fVo
❑N/A
S.
❑No
❑N/A
6.
L�Y4s
(-]No
❑N/a
es
❑No
7.
[]Yes,
[]NoD} No
,❑,i
N/A
8.
Egy'e's
QNo
❑N/A
9,
❑Yeso
[]NIA
10.
❑Yes MPKO ❑N/A 1 11.
Person contacted: Daterfime
Project Manager SCURF Review:
Project Manager SRF Review:
ID of split containers:
Date:
Field Data Required? ❑Ye5 ENO
Page 23 of 25

Oocument Name:
Sample Condition Upon Rea
Analytical Ootument No.:
F-CAR-CS-033-kev.0
*Check mark top half of box if pH andlor dechiorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/SM (water) DOC, LLHg
—Bottom half of box is to list number of bottles
0acument Reprised: October 28, 2020
lt(SCUR) Page 2 of 2
Issuing Authority:
Pace Carolinas Ounflh, nu.-
Proje 92,5637145
Cue Cate: 10/12/21
CLIEN-r: 92-MECK Co
it
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Page 24 of 25

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Page 25 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
October 19, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 28, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 31

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21LA 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
60-02 HOLBROOKS LANDFILL
92563729
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92563729001
6002-HRW7
EPA 601 OD
DS
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92563729002
6002-HRW18
EPA 601 OD
DS
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92563729003
6002-HRW19
EPA 601 OD
DS
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92563729004
6002-HRW20
EPA 601 OD
DS
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
JAH,JCP
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92563729005
6002-HRW21
EPA 601 OD
DS
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
JAH,JCP
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92563729006
TRIP BLANK
EPA 8260D
JAH,JCP
57
PAN
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: 6002-HRW7
Lab ID: 92563729001 Collected:
09/28/21 14:55
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:50
7440-36-0 BC
Arsenic
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:50
7440-38-2
Barium
204
ug/L
5.0
1
09/29/2102:00
10/01/2123:50
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:50
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:50
7440-43-9
Chromium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:50
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:50
7440-48-4
Copper
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:50
7440-50-8
Lead
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:50
7439-92-1
Nickel
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:50
7440-02-0
Selenium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:50
7782-49-2
Silver
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:50
7440-22-4
Thallium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:50
7440-28-0
Vanadium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:50
7440-62-2
Zinc
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:50
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/29/21 10:37
09/29/21 19:16
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation Method:
8260D
Pace National -
Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/09/21 02:34
10/09/21 02:34
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/09/21 02:34
10/09/21 02:34
107-13-1
Benzene
1.78
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
74-97-5
Bromoform
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/09/21 02:34
10/09/21 02:34
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
56-23-5 LO
Chlorobenzene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/09/21 02:34
10/09/21 02:34
75-00-3
Chloroform
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/09/21 02:34
10/09/21 02:34
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/09/21 02:34
10/09/21 02:34
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/09/21 02:34
10/09/21 02:34
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
106-46-7
1,1-Dichloroethane
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: 6002-HRW7
Lab ID: 92563729001
Collected: 09/28/21
14:55
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D
Preparation Method: 8260D
Pace National -
Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
75-35-4
cis-1,2-Dichloroethene
8.04
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/09/21 02:34
10/09/21 02:34
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/09/21 02:34
10/09/21 02:34
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/09/21 02:34
10/09/21 02:34
591-78-6
lodomethane
ND
ug/L
5.00
1
10/09/21 02:34
10/09/21 02:34
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/09/21 02:34
10/09/21 02:34
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/09/21 02:34
10/09/21 02:34
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/09/21 02:34
10/09/21 02:34
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/09/21 02:34
10/09/21 02:34
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
127-18-4
Toluene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
79-00-5
Trichloroethene
1.61
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/09/21 02:34
10/09/21 02:34
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/09/21 02:34
10/09/21 02:34
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/09/21 02:34
10/09/21 02:34
108-05-4
Vinyl chloride
0.716
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/09/21 02:34
10/09/21 02:34
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/09/21 02:34
10/09/21 02:34
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/09/21 02:34
10/09/21 02:34
179601-23-1
Surrogates
Toluene-d8 (S)
98.7
%
80.0-120
1
10/09/21 02:34
10/09/21 02:34
2037-26-5
4-Bromofluorobenzene (S)
90.3
%
77.0-126
1
10/09/21 02:34
10/09/21 02:34
460-00-4
1,2-Dichloroethane-d4 (S)
128
%
70.0-130
1
10/09/21 02:34
10/09/21 02:34
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method:
EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National -
Mt. Juliet
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
ND ug/L 3.00 1 10/12/21 13:15 10/12/21 13:15 123-91-1
99.6 % 77.0-127 1 10/12/21 13:15 10/12/21 13:15 2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: 6002-HRW18
Lab ID: 92563729002 Collected:
09/28/21 11:40
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:53
7440-36-0 BC
Arsenic
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:53
7440-38-2
Barium
321
ug/L
5.0
1
09/29/2102:00
10/01/2123:53
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:53
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:53
7440-43-9
Chromium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:53
7440-47-3
Cobalt
7.1
ug/L
5.0
1
09/29/2102:00
10/01/2123:53
7440-48-4
Copper
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:53
7440-50-8
Lead
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:53
7439-92-1
Nickel
6.2
ug/L
5.0
1
09/29/2102:00
10/01/2123:53
7440-02-0
Selenium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:53
7782-49-2
Silver
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:53
7440-22-4
Thallium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:53
7440-28-0
Vanadium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:53
7440-62-2
Zinc
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:53
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/29/21 10:37
09/29/21 19:20
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation Method:
8260D
Pace National -
Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/09/21 02:54
10/09/21 02:54
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/09/21 02:54
10/09/21 02:54
107-13-1
Benzene
1.34
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
74-97-5
Bromoform
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/09/21 02:54
10/09/21 02:54
74-83-9
Carbon disulfide
0.826
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
56-23-5 LO
Chlorobenzene
4.97
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/09/21 02:54
10/09/21 02:54
75-00-3
Chloroform
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/09/21 02:54
10/09/21 02:54
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/09/21 02:54
10/09/21 02:54
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/09/21 02:54
10/09/21 02:54
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
541-73-1
1,4-Dichlorobenzene
4.92
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
106-46-7
1,1-Dichloroethane
28.4
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: 6002-HRW18
Lab ID: 92563729002
Collected: 09/28/21
11:40
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D
Preparation Method: 8260D
Pace National -
Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
75-35-4
cis-1,2-Dichloroethene
1.75
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
156-60-5
1,2-Dichloropropane
4.31
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/09/21 02:54
10/09/21 02:54
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/09/21 02:54
10/09/21 02:54
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/09/21 02:54
10/09/21 02:54
591-78-6
lodomethane
ND
ug/L
5.00
1
10/09/21 02:54
10/09/21 02:54
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/09/21 02:54
10/09/21 02:54
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/09/21 02:54
10/09/21 02:54
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/09/21 02:54
10/09/21 02:54
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/09/21 02:54
10/09/21 02:54
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
127-18-4
Toluene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/09/21 02:54
10/09/21 02:54
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/09/21 02:54
10/09/21 02:54
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/09/21 02:54
10/09/21 02:54
108-05-4
Vinyl chloride
12.5
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/09/21 02:54
10/09/21 02:54
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/09/21 02:54
10/09/21 02:54
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/09/21 02:54
10/09/21 02:54
179601-23-1
Surrogates
Toluene-d8 (S)
95.9
%
80.0-120
1
10/09/21 02:54
10/09/21 02:54
2037-26-5
4-Bromofluorobenzene (S)
90.7
%
77.0-126
1
10/09/21 02:54
10/09/21 02:54
460-00-4
1,2-Dichloroethane-d4 (S)
129
%
70.0-130
1
10/09/21 02:54
10/09/21 02:54
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method:
EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National -
Mt. Juliet
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
Date: 10/19/2021 06:47 PM
5.92 ug/L 3.00 1 10/12/21 13:34 10/12/21 13:34 123-91-1
101 % 77.0-127 1 10/12/21 13:34 10/12/21 13:34 2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: 6002-HRW19
Lab ID: 92563729003 Collected:
09/28/21 11:10
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:57
7440-36-0 BC
Arsenic
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:57
7440-38-2
Barium
92.5
ug/L
5.0
1
09/29/2102:00
10/01/2123:57
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:57
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/29/2102:00
10/01/2123:57
7440-43-9
Chromium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:57
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:57
7440-48-4
Copper
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:57
7440-50-8
Lead
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:57
7439-92-1
Nickel
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:57
7440-02-0
Selenium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:57
7782-49-2
Silver
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:57
7440-22-4
Thallium
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:57
7440-28-0
Vanadium
ND
ug/L
5.0
1
09/29/2102:00
10/01/2123:57
7440-62-2
Zinc
ND
ug/L
10.0
1
09/29/2102:00
10/01/2123:57
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/29/21 10:37
09/29/21 19:23
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation Method:
8260D
Pace National -
Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/09/21 03:14
10/09/21 03:14
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/09/21 03:14
10/09/21 03:14
107-13-1
Benzene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
74-97-5
Bromoform
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/09/21 03:14
10/09/21 03:14
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
56-23-5 LO
Chlorobenzene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/09/21 03:14
10/09/21 03:14
75-00-3
Chloroform
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/09/21 03:14
10/09/21 03:14
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/09/21 03:14
10/09/21 03:14
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/09/21 03:14
10/09/21 03:14
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
106-46-7
1,1-Dichloroethane
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: 6002-HRW19
Lab ID: 92563729003
Collected: 09/28/21
11:10
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D
Preparation Method: 8260D
Pace National
- Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/09/21 03:14
10/09/21 03:14
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/09/21 03:14
10/09/21 03:14
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/09/21 03:14
10/09/21 03:14
591-78-6
lodomethane
ND
ug/L
5.00
1
10/09/21 03:14
10/09/21 03:14
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/09/21 03:14
10/09/21 03:14
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/09/21 03:14
10/09/21 03:14
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/09/21 03:14
10/09/21 03:14
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/09/21 03:14
10/09/21 03:14
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
127-18-4
Toluene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/09/21 03:14
10/09/21 03:14
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/09/21 03:14
10/09/21 03:14
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/09/21 03:14
10/09/21 03:14
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/09/21 03:14
10/09/21 03:14
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/09/21 03:14
10/09/21 03:14
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/09/21 03:14
10/09/21 03:14
179601-23-1
Surrogates
Toluene-d8 (S)
95.5
%
80.0-120
1
10/09/21 03:14
10/09/21 03:14
2037-26-5
4-Bromofluorobenzene (S)
87.8
%
77.0-126
1
10/09/21 03:14
10/09/21 03:14
460-00-4
1,2-Dichloroethane-d4 (S)
130
%
70.0-130
1
10/09/21 03:14
10/09/21 03:14
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method:
EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National
- Mt. Juliet
1,4-Dioxane (p-Dioxane)
ND
ug/L
3.00
1
10/12/21 13:55
10/12/21 13:55
123-91-1
Surrogates
Toluene-d8 (S)
100
%
77.0-127
1
10/12/21 13:55
10/12/21 13:55
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in
full,
Date: 10/19/2021 06:47 PM
without
the written
consent of Pace Analytical
Services, LLC.
Page 9 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: 6002-HRW20
Lab ID: 92563729004 Collected:
09/28/21 11:30
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:13
7440-36-0
BC
Arsenic
ND
ug/L
10.0
1
09/29/2102:00
10/02/2100:13
7440-38-2
Barium
110
ug/L
5.0
1
09/29/2102:00
10/02/2100:13
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/29/2102:00
10/02/2100:13
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/29/2102:00
10/02/2100:13
7440-43-9
Chromium
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:13
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:13
7440-48-4
Copper
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:13
7440-50-8
Lead
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:13
7439-92-1
Nickel
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:13
7440-02-0
Selenium
ND
ug/L
10.0
1
09/29/2102:00
10/02/2100:13
7782-49-2
Silver
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:13
7440-22-4
Thallium
ND
ug/L
10.0
1
09/29/2102:00
10/02/2100:13
7440-28-0
Vanadium
6.0
ug/L
5.0
1
09/29/21 02:00
10/02/2100:13
7440-62-2
Zinc
ND
ug/L
10.0
1
09/29/2102:00
10/02/2100:13
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/29/21 10:37
09/29/21 19:27
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation Method:
8260D
Pace National -
Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/10/21 10:47
10/10/21 10:47
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/10/21 10:47
10/10/21 10:47
107-13-1
Benzene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
74-97-5
Bromoform
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/10/21 10:47
10/10/21 10:47
74-83-9
C3
Carbon disulfide
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
56-23-5
Chlorobenzene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/10/21 10:47
10/10/21 10:47
75-00-3
Chloroform
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/10/21 10:47
10/10/21 10:47
74-87-3
C3
Chloroprene
ND
ug/L
50.0
1
10/14/2121:04
10/14/2121:04
126-99-8
H1
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/10/21 10:47
10/10/21 10:47
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
106-46-7
1,1-Dichloroethane
4.86
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: 6002-HRW20
Lab ID: 92563729004
Collected: 09/28/21
11:30
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D
Preparation Method: 8260D
Pace National -
Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/10/21 10:47
10/10/21 10:47
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/10/21 10:47
10/10/21 10:47
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/10/21 10:47
10/10/21 10:47
591-78-6
lodomethane
ND
ug/L
5.00
1
10/10/21 10:47
10/10/21 10:47
74-88-4 C3
2-Butanone (MEK)
ND
ug/L
5.00
1
10/10/21 10:47
10/10/21 10:47
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/10/21 10:47
10/10/21 10:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/10/21 10:47
10/10/21 10:47
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/10/21 10:47
10/10/21 10:47
91-20-3
Styrene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
127-18-4
Toluene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/10/21 10:47
10/10/21 10:47
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/10/21 10:47
10/10/21 10:47
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/10/21 10:47
10/10/21 10:47
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/10/21 10:47
10/10/21 10:47
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/10/21 10:47
10/10/21 10:47
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/10/21 10:47
10/10/21 10:47
179601-23-1
Surrogates
Toluene-d8 (S)
106
%
80.0-120
1
10/10/21 10:47
10/10/21 10:47
2037-26-5
Toluene-d8 (S)
101
%
80.0-120
1
10/14/21 21:04
10/14/21 21:04
2037-26-5
4-Bromofluorobenzene (S)
96.6
%
77.0-126
1
10/10/21 10:47
10/10/21 10:47
460-00-4
4-Bromofluorobenzene (S)
90.8
%
77.0-126
1
10/14/21 21:04
10/14/21 21:04
460-00-4
1,2-Dichloroethane-d4 (S)
112
%
70.0-130
1
10/10/21 10:47
10/10/21 10:47
17060-07-0
1,2-Dichloroethane-d4 (S)
111
%
70.0-130
1
10/14/21 21:04
10/14/21 21:04
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method:
EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National -
Mt. Juliet
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
ND ug/L 3.00 1 10/12/21 14:14 10/12/21 14:14 123-91-1
100 % 77.0-127 1 10/12/21 14:14 10/12/21 14:14 2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: 6002-HRW21
Lab ID: 92563729005 Collected:
09/28/21 10:45
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:17
7440-36-0
BC
Arsenic
ND
ug/L
10.0
1
09/29/2102:00
10/02/2100:17
7440-38-2
Barium
76.3
ug/L
5.0
1
09/29/2102:00
10/02/2100:17
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/29/2102:00
10/02/2100:17
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/29/2102:00
10/02/2100:17
7440-43-9
Chromium
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:17
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:17
7440-48-4
Copper
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:17
7440-50-8
Lead
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:17
7439-92-1
Nickel
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:17
7440-02-0
Selenium
ND
ug/L
10.0
1
09/29/2102:00
10/02/2100:17
7782-49-2
Silver
ND
ug/L
5.0
1
09/29/2102:00
10/02/2100:17
7440-22-4
Thallium
ND
ug/L
10.0
1
09/29/2102:00
10/02/2100:17
7440-28-0
Vanadium
5.5
ug/L
5.0
1
09/29/21 02:00
10/02/2100:17
7440-62-2
Zinc
ND
ug/L
10.0
1
09/29/2102:00
10/02/2100:17
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/29/21 10:37
09/29/21 19:30
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation Method:
8260D
Pace National -
Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/10/21 11:08
10/10/21 11:08
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/10/21 11:08
10/10/21 11:08
107-13-1
Benzene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
74-97-5
Bromoform
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/10/21 11:08
10/10/21 11:08
74-83-9
C3
Carbon disulfide
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
56-23-5
Chlorobenzene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/10/21 11:08
10/10/21 11:08
75-00-3
Chloroform
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/10/21 11:08
10/10/21 11:08
74-87-3
C3
Chloroprene
ND
ug/L
50.0
1
10/14/2121:25
10/14/2121:25
126-99-8
H1
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/10/21 11:08
10/10/21 11:08
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
106-46-7
1,1-Dichloroethane
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: 6002-HRW21
Lab ID: 92563729005
Collected: 09/28/21
10:45
Received: 09/28/21 15:33 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D
Preparation Method: 8260D
Pace National -
Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/10/21 11:08
10/10/21 11:08
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/10/21 11:08
10/10/21 11:08
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/10/21 11:08
10/10/21 11:08
591-78-6
lodomethane
ND
ug/L
5.00
1
10/10/21 11:08
10/10/21 11:08
74-88-4 C3
2-Butanone (MEK)
ND
ug/L
5.00
1
10/10/21 11:08
10/10/21 11:08
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/10/21 11:08
10/10/21 11:08
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/10/21 11:08
10/10/21 11:08
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/10/21 11:08
10/10/21 11:08
91-20-3
Styrene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
127-18-4
Toluene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/10/21 11:08
10/10/21 11:08
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/10/21 11:08
10/10/21 11:08
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/10/21 11:08
10/10/21 11:08
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/10/21 11:08
10/10/21 11:08
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/10/21 11:08
10/10/21 11:08
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/10/21 11:08
10/10/21 11:08
179601-23-1
Surrogates
Toluene-d8 (S)
104
%
80.0-120
1
10/10/21 11:08
10/10/21 11:08
2037-26-5
Toluene-d8 (S)
101
%
80.0-120
1
10/14/21 21:25
10/14/21 21:25
2037-26-5
4-Bromofluorobenzene (S)
96.3
%
77.0-126
1
10/10/21 11:08
10/10/21 11:08
460-00-4
4-Bromofluorobenzene (S)
89.4
%
77.0-126
1
10/14/21 21:25
10/14/21 21:25
460-00-4
1,2-Dichloroethane-d4 (S)
110
%
70.0-130
1
10/10/21 11:08
10/10/21 11:08
17060-07-0
1,2-Dichloroethane-d4 (S)
109
%
70.0-130
1
10/14/21 21:25
10/14/21 21:25
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method:
EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National -
Mt. Juliet
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
ND ug/L 3.00 1 10/12/21 14:34 10/12/21 14:34 123-91-1
100 % 77.0-127 1 10/12/21 14:34 10/12/21 14:34 2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: TRIP BLANK Lab ID: 92563729006 Collected: 09/28/21 09:40 Received: 09/28/21 15:33 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/10/21 06:34
10/10/21 06:34
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/10/21 06:34
10/10/21 06:34
107-13-1
Benzene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
74-97-5
Bromoform
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/10/21 06:34
10/10/21 06:34
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
56-23-5
Chlorobenzene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/10/21 06:34
10/10/21 06:34
75-00-3
Chloroform
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/10/21 06:34
10/10/21 06:34
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/14/2121:46
10/14/2121:46
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/10/21 06:34
10/10/21 06:34
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
106-46-7
1,1-Dichloroethane
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
107-06-2
1,1-Dichloroethene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/10/21 06:34
10/10/21 06:34
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/10/21 06:34
10/10/21 06:34
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/10/21 06:34
10/10/21 06:34
591-78-6
lodomethane
ND
ug/L
5.00
1
10/10/21 06:34
10/10/21 06:34
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/10/21 06:34
10/10/21 06:34
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/10/21 06:34
10/10/21 06:34
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/10/21 06:34
10/10/21 06:34
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/10/21 06:34
10/10/21 06:34
91-20-3
Styrene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
127-18-4
Toluene
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
79-00-5
REPORT OF LABORATORY ANALYSIS
Qual
C3
C3
H1
C3
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
Sample: TRIP BLANK Lab ID: 92563729006 Collected: 09/28/21 09:40 Received: 09/28/21 15:33 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
o-Xylene
m&p-Xylene
Surrogates
Toluene-d8 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
1,2-Dichloroethane-d4 (S)
Date: 10/19/2021 06:47 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
Pace National - Mt. Juliet
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
79-01-6
ND
ug/L
2.50
1
10/10/21 06:34
10/10/21 06:34
75-69-4
ND
ug/L
2.50
1
10/10/21 06:34
10/10/21 06:34
96-18-4
ND
ug/L
5.00
1
10/10/21 06:34
10/10/21 06:34
108-05-4
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
75-01-4
ND
ug/L
1.50
1
10/10/21 06:34
10/10/21 06:34
1330-20-7
ND
ug/L
0.500
1
10/10/21 06:34
10/10/21 06:34
95-47-6
ND
ug/L
1.00
1
10/10/21 06:34
10/10/21 06:34
179601-23-1
103
%
80.0-120
1
10/10/21 06:34
10/10/21 06:34
2037-26-5
98.1
%
80.0-120
1
10/14/21 21:46
10/14/21 21:46
2037-26-5
94.6
%
77.0-126
1
10/10/21 06:34
10/10/21 06:34
460-00-4
92.6
%
77.0-126
1
10/14/21 21:46
10/14/21 21:46
460-00-4
105
%
70.0-130
1
10/10/21 06:34
10/10/21 06:34
17060-07-0
114
%
70.0-130
1
10/14/21 21:46
10/14/21 21:46
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
QC Batch: 649812 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92563729001, 92563729002, 92563729003, 92563729004, 92563729005
METHOD BLANK: 3408194 Matrix: Water
Associated Lab Samples: 92563729001, 92563729002, 92563729003, 92563729004, 92563729005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony
ug/L
ND
5.0
10/02/2104:28
Arsenic
ug/L
ND
10.0
10/02/2104:28
Barium
ug/L
ND
5.0
10/02/2104:28
Beryllium
ug/L
ND
1.0
10/02/2104:28
Cadmium
ug/L
ND
1.0
10/02/2104:28
Chromium
ug/L
ND
5.0
10/02/2104:28
Cobalt
ug/L
ND
5.0
10/02/2104:28
Copper
ug/L
ND
5.0
10/02/2104:28
Lead
ug/L
ND
5.0
10/02/2104:28
Nickel
ug/L
ND
5.0
10/02/2104:28
Selenium
ug/L
ND
10.0
10/02/2104:28
Silver
ug/L
ND
5.0
10/02/2104:28
Thallium
ug/L
ND
10.0
10/02/2104:28
Vanadium
ug/L
ND
5.0
10/02/2104:28
Zinc
ug/L
ND
10.0
10/02/2104:28
LABORATORY CONTROL SAMPLE:
Parameter
3408195
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
492
98
80-120
Arsenic
ug/L
500
502
100
80-120
Barium
ug/L
500
496
99
80-120
Beryllium
ug/L
500
488
98
80-120
Cadmium
ug/L
500
497
99
80-120
Chromium
ug/L
500
483
97
80-120
Cobalt
ug/L
500
459
92
80-120
Copper
ug/L
500
485
97
80-120
Lead
ug/L
500
495
99
80-120
Nickel
ug/L
500
478
96
80-120
Selenium
ug/L
500
498
100
80-120
Silver
ug/L
250
241
96
80-120
Thallium
ug/L
500
489
98
80-120
Vanadium
ug/L
500
484
97
80-120
Zinc
ug/L
500
502
100
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
60-02 HOLBROOKS LANDFILL
92563729
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3408196
3408197
MS
MSD
92563460001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
518
504
103
101
75-125
3
Arsenic
ug/L
ND
500
500
525
508
105
101
75-125
3
Barium
ug/L
12.9
500
500
524
510
102
99
75-125
3
Beryllium
ug/L
ND
500
500
507
492
101
98
75-125
3
Cadmium
ug/L
ND
500
500
508
495
102
99
75-125
3
Chromium
ug/L
ND
500
500
494
479
99
96
75-125
3
Cobalt
ug/L
8.8
500
500
486
472
95
93
75-125
3
Copper
ug/L
113
500
500
603
583
98
94
75-125
3
Lead
ug/L
ND
500
500
506
493
101
98
75-125
3
Nickel
ug/L
5.7
500
500
494
480
98
95
75-125
3
Selenium
ug/L
ND
500
500
534
519
106
103
75-125
3
Silver
ug/L
ND
250
250
247
242
99
97
75-125
2
Thallium
ug/L
ND
500
500
504
490
101
98
75-125
3
Vanadium
ug/L
ND
500
500
503
489
101
98
75-125
3
Zinc
ug/L
ND
500
500
523
508
103
100
75-125
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
QC Batch: 649884 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92563729001, 92563729002, 92563729003, 92563729004, 92563729005
METHOD BLANK: 3408337
Matrix:
Water
Associated Lab Samples: 92563729001, 92563729002, 92563729003, 92563729004, 92563729005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.47
09/29/2118:30
LABORATORY CONTROL SAMPLE:
3408338
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
26.3
105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3408339 3408340
MS MSD
92563725001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 25.1 25.9 100 103 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
QC Batch: 1753823 Analysis Method: EPA 8260D
QC Batch Method: 8260B Analysis Description: VOA (GC/MS) 8260D
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92563729001, 92563729002, 92563729003
METHOD BLANK: R3714680-3 Matrix:
Associated Lab Samples: 92563729001, 92563729002, 92563729003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1,1-Trichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1,2,2-Tetrachloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1,2-Trichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1-Dichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1-Dichloroethene
ug/L
ND
0.500
10/08/21 20:27
1,1-Dichloropropene
ug/L
ND
0.500
10/08/21 20:27
1,2,3-Trichloropropane
ug/L
ND
2.50
10/08/21 20:27
1,2-Dibromo-3-chloropropane
ug/L
ND
2.50
10/08/21 20:27
1,2-Dibromoethane (EDB)
ug/L
ND
0.500
10/08/21 20:27
1,2-Dichlorobenzene
ug/L
ND
0.500
10/08/21 20:27
1,2-Dichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,2-Dichloropropane
ug/L
ND
0.500
10/08/21 20:27
1,3-Dichlorobenzene
ug/L
ND
0.500
10/08/21 20:27
1,3-Dichloropropane
ug/L
ND
1.00
10/08/21 20:27
1,4-Dichlorobenzene
ug/L
ND
0.500
10/08/21 20:27
2-Butanone (MEK)
ug/L
ND
5.00
10/08/21 20:27
2-Hexanone
ug/L
ND
5.00
10/08/21 20:27
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.00
10/08/21 20:27
Acetone
ug/L
ND
25.0
10/08/21 20:27
Acrylonitrile
ug/L
ND
5.00
10/08/21 20:27
Benzene
ug/L
ND
0.500
10/08/21 20:27
Bromochloromethane
ug/L
ND
0.500
10/08/21 20:27
Bromodichloromethane
ug/L
ND
0.500
10/08/21 20:27
Bromoform
ug/L
ND
0.500
10/08/21 20:27
Bromomethane
ug/L
ND
2.50
10/08/21 20:27
Carbon disulfide
ug/L
ND
0.500
10/08/21 20:27
Carbon tetrachloride
ug/L
ND
0.500
10/08/21 20:27
Chlorobenzene
ug/L
ND
0.500
10/08/21 20:27
Dibromochloromethane
ug/L
ND
0.500
10/08/21 20:27
Chloroethane
ug/L
ND
2.50
10/08/21 20:27
Chloroform
ug/L
ND
0.500
10/08/21 20:27
Chloromethane
ug/L
ND
1.25
10/08/21 20:27
Chloroprene
ug/L
ND
50.0
10/08/21 20:27
cis-1,2-Dichloroethene
ug/L
ND
0.500
10/08/21 20:27
cis-1,3-Dichloropropene
ug/L
ND
0.500
10/08/21 20:27
Dibromomethane
ug/L
ND
0.500
10/08/21 20:27
Ethylbenzene
ug/L
ND
0.500
10/08/21 20:27
lodomethane
ug/L
ND
5.00
10/08/21 20:27
m&p-Xylene
ug/L
ND
1.00
10/08/21 20:27
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
METHOD BLANK: R3714680-3 Matrix:
Associated Lab Samples: 92563729001, 92563729002, 92563729003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Methylene Chloride
ug/L
ND
2.50
10/08/21 20:27
Naphthalene
ug/L
ND
2.50
10/08/21 20:27
o-Xylene
ug/L
ND
0.500
10/08/21 20:27
Styrene
ug/L
ND
0.500
10/08/21 20:27
Tetrachloroethene
ug/L
ND
0.500
10/08/21 20:27
Toluene
ug/L
ND
0.500
10/08/21 20:27
trans-1,2-Dichloroethene
ug/L
ND
0.500
10/08/21 20:27
trans- 1,3-Dichloropropene
ug/L
ND
0.500
10/08/21 20:27
trans-1,4-Dichloro-2-butene
ug/L
ND
5.00
10/08/21 20:27
Trichloroethene
ug/L
ND
0.500
10/08/21 20:27
Trichlorofluoromethane
ug/L
ND
2.50
10/08/21 20:27
Vinyl acetate
ug/L
ND
5.00
10/08/21 20:27
Vinyl chloride
ug/L
ND
0.500
10/08/21 20:27
Xylene (Total)
ug/L
ND
1.50
10/08/21 20:27
1,2-Dichloroethane-d4 (S)
%
129
70.0-130
10/08/21 20:27
Toluene-d8 (S)
%
94.9
80.0-120
10/08/21 20:27
4-Bromofluorobenzene (S)
%
91.6
77.0-126
10/08/21 20:27
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
R3714680-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
5.00
5.06
101
75.0-125
1,1,1-Trichloroethane
ug/L
5.00
6.13
123
73.0-124
1,1,2,2-Tetrachloroethane
ug/L
5.00
4.29
85.8
65.0-130
1,1,2-Trichloroethane
ug/L
5.00
5.00
100
80.0-120
1,1-Dichloroethane
ug/L
5.00
5.61
112
70.0-126
1,1-Dichloroethene
ug/L
5.00
5.05
101
71.0-124
1,1-Dichloropropene
ug/L
5.00
5.86
117
74.0-126
1,2,3-Trichloropropane
ug/L
5.00
5.04
101
73.0-130
1,2-Dibromo-3-chloropropane
ug/L
5.00
4.08
81.6
58.0-134
1,2-Dibromoethane (EDB)
ug/L
5.00
5.18
104
80.0-122
1,2-Dichlorobenzene
ug/L
5.00
5.10
102
79.0-121
1,2-Dichloroethane
ug/L
5.00
6.05
121
70.0-128
1,2-Dichloropropane
ug/L
5.00
5.28
106
77.0-125
1,3-Dichlorobenzene
ug/L
5.00
4.79
95.8
79.0-120
1,3-Dichloropropane
ug/L
5.00
5.97
119
80.0-120
1,4-Dichlorobenzene
ug/L
5.00
4.91
98.2
79.0-120
2-Butanone (MEK)
ug/L
25.0
27.2
109
44.0-160
2-Hexanone
ug/L
25.0
23.7
94.8
67.0-149
4-Methyl-2-pentanone (MIBK)
ug/L
25.0
27.8
111
68.0-142
Acetone
ug/L
25.0
29.7
119
19.0-160
Acrylonitrile
ug/L
25.0
26.0
104
55.0-149
Benzene
ug/L
5.00
5.37
107
70.0-123
Bromochloromethane
ug/L
5.00
5.08
102
76.0-122
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
LABORATORY CONTROL SAMPLE:
Parameter
R3714680-1
Units
Spike LCS
Conc. Result
Bromodichloromethane
ug/L
5.00
Bromoform
ug/L
5.00
Bromomethane
ug/L
5.00
Carbon disulfide
ug/L
5.00
Carbon tetrachloride
ug/L
5.00
Chlorobenzene
ug/L
5.00
Dibromochloromethane
ug/L
5.00
Chloroethane
ug/L
5.00
Chloroform
ug/L
5.00
Chloromethane
ug/L
5.00
cis-1,2-Dichloroethene
ug/L
5.00
cis-1,3-Dichloropropene
ug/L
5.00
Dibromomethane
ug/L
5.00
Ethylbenzene
ug/L
5.00
lodomethane
ug/L
25.0
m&p-Xylene
ug/L
10.0
Methylene Chloride
ug/L
5.00
Naphthalene
ug/L
5.00
o-Xylene
ug/L
5.00
Styrene
ug/L
5.00
Tetrachloroethene
ug/L
5.00
Toluene
ug/L
5.00
trans-1,2-Dichloroethene
ug/L
5.00
trans- 1,3-Dichloropropene
ug/L
5.00
trans-1,4-Dichloro-2-butene
ug/L
5.00
Trichloroethene
ug/L
5.00
Trichlorofluoromethane
ug/L
5.00
Vinyl acetate
ug/L
25.0
Vinyl chloride
ug/L
5.00
Xylene (Total)
ug/L
15.0
1,2-Dichloroethane-d4 (S)
%
Toluene-d8 (S)
%
4-Bromofluorobenzene (S)
%
LCS
% Rec
% Rec
Limits Qualifiers
5.55
111
75.0-120
5.31
106
68.0-132
4.30
86.0
10.0-160
5.89
118
61.0-128
6.33
127
68.0-126 LO
4.92
98.4
80.0-121
5.29
106
77.0-125
4.02
80.4
47.0-150
5.80
116
73.0-120
5.08
102
41.0-142
4.81
96.2
73.0-120
5.47
109
80.0-123
5.48
110
80.0-120
5.04
101
79.0-123
27.2
109
33.0-147
9.96
99.6
80.0-122
5.18
104
67.0-120
3.06
61.2
54.0-135
4.79
95.8
80.0-122
4.92
98.4
73.0-130
5.56
111
72.0-132
5.08
102
79.0-120
5.40
108
73.0-120
5.62
112
78.0-124
4.25
85.0
33.0-144
5.48
110
78.0-124
6.00
120
59.0-147
23.9
95.6
11.0-160
4.69
93.8
67.0-131
14.7
98.0
79.0-123
125
70.0-130
96.2
80.0-120
92.0
77.0-126
LABORATORY CONTROL SAMPLE:
R3714680-2
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Chloroprene
ug/L
50.0 45.1 90.2
60.0-143
1,2-Dichloroethane-d4 (S)
%
128
70.0-130
Toluene-d8 (S)
%
95.4
80.0-120
4-Bromofluorobenzene (S)
%
90.9
77.0-126
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
QC Batch: 1754158 Analysis Method: EPA 8260D
QC Batch Method: 8260B Analysis Description: VOA (GC/MS) 8260D
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92563729004, 92563729005, 92563729006
METHOD BLANK: R3716623-2 Matrix:
Associated Lab Samples: 92563729004, 92563729005, 92563729006
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.500
10/10/21 05:51
1,1,1-Trichloroethane
ug/L
ND
0.500
10/10/21 05:51
1,1,2,2-Tetrachloroethane
ug/L
ND
0.500
10/10/21 05:51
1,1,2-Trichloroethane
ug/L
ND
0.500
10/10/21 05:51
1,1-Dichloroethane
ug/L
ND
0.500
10/10/21 05:51
1,1-Dichloroethene
ug/L
ND
0.500
10/10/21 05:51
1,1-Dichloropropene
ug/L
ND
0.500
10/10/21 05:51
1,2,3-Trichloropropane
ug/L
ND
2.50
10/10/21 05:51
1,2-Dibromo-3-chloropropane
ug/L
ND
2.50
10/10/21 05:51
1,2-Dibromoethane (EDB)
ug/L
ND
0.500
10/10/21 05:51
1,2-Dichlorobenzene
ug/L
ND
0.500
10/10/21 05:51
1,2-Dichloroethane
ug/L
ND
0.500
10/10/21 05:51
1,2-Dichloropropane
ug/L
ND
0.500
10/10/21 05:51
1,3-Dichlorobenzene
ug/L
ND
0.500
10/10/21 05:51
1,3-Dichloropropane
ug/L
ND
1.00
10/10/21 05:51
1,4-Dichlorobenzene
ug/L
ND
0.500
10/10/21 05:51
2-Butanone (MEK)
ug/L
ND
5.00
10/10/21 05:51
2-Hexanone
ug/L
ND
5.00
10/10/21 05:51
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.00
10/10/21 05:51
Acetone
ug/L
ND
25.0
10/10/21 05:51
Acrylonitrile
ug/L
ND
5.00
10/10/21 05:51
Benzene
ug/L
ND
0.500
10/10/21 05:51
Bromochloromethane
ug/L
ND
0.500
10/10/21 05:51
Bromodichloromethane
ug/L
ND
0.500
10/10/21 05:51
Bromoform
ug/L
ND
0.500
10/10/21 05:51
Bromomethane
ug/L
ND
2.50
10/10/21 05:51
Carbon disulfide
ug/L
ND
0.500
10/10/21 05:51
Carbon tetrachloride
ug/L
ND
0.500
10/10/21 05:51
Chlorobenzene
ug/L
ND
0.500
10/10/21 05:51
Dibromochloromethane
ug/L
ND
0.500
10/10/21 05:51
Chloroethane
ug/L
ND
2.50
10/10/21 05:51
Chloroform
ug/L
ND
0.500
10/10/21 05:51
Chloromethane
ug/L
ND
1.25
10/10/21 05:51
cis-1,2-Dichloroethene
ug/L
ND
0.500
10/10/21 05:51
cis-1,3-Dichloropropene
ug/L
ND
0.500
10/10/21 05:51
Dibromomethane
ug/L
ND
0.500
10/10/21 05:51
Ethylbenzene
ug/L
ND
0.500
10/10/21 05:51
lodomethane
ug/L
ND
5.00
10/10/21 05:51
m&p-Xylene
ug/L
ND
1.00
10/10/21 05:51
Methylene Chloride
ug/L
ND
2.50
10/10/21 05:51
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
METHOD BLANK: R3716623-2 Matrix:
Associated Lab Samples: 92563729004, 92563729005, 92563729006
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Naphthalene
ug/L
ND
2.50
10/10/21 05:51
o-Xylene
ug/L
ND
0.500
10/10/21 05:51
Styrene
ug/L
ND
0.500
10/10/21 05:51
Tetrachloroethene
ug/L
ND
0.500
10/10/21 05:51
Toluene
ug/L
ND
0.500
10/10/21 05:51
trans-1,2-Dichloroethene
ug/L
ND
0.500
10/10/21 05:51
trans- 1,3-Dichloropropene
ug/L
ND
0.500
10/10/21 05:51
trans-1,4-Dichloro-2-butene
ug/L
ND
5.00
10/10/21 05:51
Trichloroethene
ug/L
ND
0.500
10/10/21 05:51
Trichlorofluoromethane
ug/L
ND
2.50
10/10/21 05:51
Vinyl acetate
ug/L
ND
5.00
10/10/21 05:51
Vinyl chloride
ug/L
ND
0.500
10/10/21 05:51
Xylene (Total)
ug/L
ND
1.50
10/10/21 05:51
1,2-Dichloroethane-d4 (S)
%
106
70.0-130
10/10/21 05:51
Toluene-d8 (S)
%
106
80.0-120
10/10/21 05:51
4-Bromofluorobenzene (S)
%
95.9
77.0-126
10/10/21 05:51
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
R3716623-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
5.00
4.70
94.0
75.0-125
1,1,1-Trichloroethane
ug/L
5.00
4.99
99.8
73.0-124
1,1,2,2-Tetrachloroethane
ug/L
5.00
5.52
110
65.0-130
1,1,2-Trichloroethane
ug/L
5.00
4.78
95.6
80.0-120
1,1-Dichloroethane
ug/L
5.00
4.85
97.0
70.0-126
1,1-Dichloroethene
ug/L
5.00
4.85
97.0
71.0-124
1,1-Dichloropropene
ug/L
5.00
4.57
91.4
74.0-126
1,2,3-Trichloropropane
ug/L
5.00
5.10
102
73.0-130
1,2-Dibromo-3-chloropropane
ug/L
5.00
4.39
87.8
58.0-134
1,2-Dibromoethane (EDB)
ug/L
5.00
4.97
99.4
80.0-122
1,2-Dichlorobenzene
ug/L
5.00
4.99
99.8
79.0-121
1,2-Dichloroethane
ug/L
5.00
5.06
101
70.0-128
1,2-Dichloropropane
ug/L
5.00
4.96
99.2
77.0-125
1,3-Dichlorobenzene
ug/L
5.00
4.77
95.4
79.0-120
1,3-Dichloropropane
ug/L
5.00
5.04
101
80.0-120
1,4-Dichlorobenzene
ug/L
5.00
4.94
98.8
79.0-120
2-Butanone (MEK)
ug/L
25.0
23.4
93.6
44.0-160
2-Hexanone
ug/L
25.0
23.9
95.6
67.0-149
4-Methyl-2-pentanone (MIBK)
ug/L
25.0
25.4
102
68.0-142
Acetone
ug/L
25.0
22.4
89.6
19.0-160
Acrylonitrile
ug/L
25.0
25.4
102
55.0-149
Benzene
ug/L
5.00
4.79
95.8
70.0-123
Bromochloromethane
ug/L
5.00
5.20
104
76.0-122
Bromodichloromethane
ug/L
5.00
5.11
102
75.0-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
LABORATORY CONTROL SAMPLE:
Parameter
R3716623-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Bromoform
ug/L
5.00
4.76
95.2
68.0-132
Bromomethane
ug/L
5.00
1.23
24.6
10.0-160
Carbon disulfide
ug/L
5.00
4.72
94.4
61.0-128
Carbon tetrachloride
ug/L
5.00
4.52
90.4
68.0-126
Chlorobenzene
ug/L
5.00
4.59
91.8
80.0-121
Dibromochloromethane
ug/L
5.00
5.02
100
77.0-125
Chloroethane
ug/L
5.00
4.43
88.6
47.0-150
Chloroform
ug/L
5.00
4.83
96.6
73.0-120
Chloromethane
ug/L
5.00
3.20
64.0
41.0-142
cis-1,2-Dichloroethene
ug/L
5.00
4.63
92.6
73.0-120
cis-1,3-Dichloropropene
ug/L
5.00
4.78
95.6
80.0-123
Dibromomethane
ug/L
5.00
4.70
94.0
80.0-120
Ethylbenzene
ug/L
5.00
4.87
97.4
79.0-123
lodomethane
ug/L
25.0
10.1
40.4
33.0-147
m&p-Xylene
ug/L
10.0
9.35
93.5
80.0-122
Methylene Chloride
ug/L
5.00
5.17
103
67.0-120
Naphthalene
ug/L
5.00
4.27
85.4
54.0-135
o-Xylene
ug/L
5.00
4.35
87.0
80.0-122
Styrene
ug/L
5.00
4.56
91.2
73.0-130
Tetrachloroethene
ug/L
5.00
4.73
94.6
72.0-132
Toluene
ug/L
5.00
4.74
94.8
79.0-120
trans-1,2-Dichloroethene
ug/L
5.00
4.58
91.6
73.0-120
trans- 1,3-Dichloropropene
ug/L
5.00
4.80
96.0
78.0-124
trans-1,4-Dichloro-2-butene
ug/L
5.00
3.77
75.4
33.0-144
Trichloroethene
ug/L
5.00
4.79
95.8
78.0-124
Trichlorofluoromethane
ug/L
5.00
4.97
99.4
59.0-147
Vinyl acetate
ug/L
25.0
29.4
118
11.0-160
Vinyl chloride
ug/L
5.00
4.22
84.4
67.0-131
Xylene (Total)
ug/L
15.0
13.7
91.3
79.0-123
1,2-Dichloroethane-d4 (S)
%
108
70.0-130
Toluene-d8 (S)
%
103
80.0-120
4-Bromofluorobenzene (S)
%
99.1
77.0-126
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
QC Batch: 1757506 Analysis Method: EPA 8260D
QC Batch Method: 8260B Analysis Description: VOA (GC/MS) 8260D
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92563729004, 92563729005, 92563729006
METHOD BLANK: R3716959-3
Matrix:
Water
Associated Lab Samples:
92563729004, 92563729005, 92563729006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chloroprene
ug/L
ND
50.0
10/14/21 20:23
1,2-Dichloroethane-d4 (S)
%
111
70.0-130
10/14/21 20:23
Toluene-d8 (S)
%
102
80.0-120
10/14/21 20:23
4-Bromofluorobenzene (S)
%
91.9
77.0-126
10/14/21 20:23
LABORATORY CONTROL SAMPLE:
R3716959-2
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Chloroprene
ug/L
50.0 44.8 89.6
60.0-143
1,2-Dichloroethane-d4 (S)
%
109
70.0-130
Toluene-d8 (S)
%
99.2
80.0-120
4-Bromofluorobenzene (S)
%
93.3
77.0-126
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
QC Batch: 1755301
Analysis Method: EPA 8260D by SIM
QC Batch Method: 8260B-SIM
Analysis Description: VOA (GC/MS) 8260D-SIM
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92563729001, 92563729002,
92563729003, 92563729004, 92563729005
METHOD BLANK: R3715967-3
Matrix: Water
Associated Lab Samples: 92563729001, 92563729002,
92563729003, 92563729004, 92563729005
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
1,4-Dioxane (p-Dioxane) ug/L
ND 3.00 10/12/21 12:00
Toluene-d8 (S) %
100 77.0-127 10/12/21 12:00
LABORATORY CONTROL SAMPLE & LCSD: R3715967-1 R3715967-2
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units
Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
1,4-Dioxane (p-Dioxane) ug/L
50.0 57.0 49.6 114 99.2 55.0-138 13.9 24
Toluene-d8 (S) %
100 100 77.0-127
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3715967-4 R3715967-5
MS MSD
L1414799-01
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
1,4-Dioxane (p-Dioxane) ug/L 39.2
50.0 50.0 93.3 91.8 108 105 13.0-160 1.62
Toluene-d8 (S) %
99.8 99.7 77.0-127
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 60-02 HOLBROOKS LANDFILL
Pace Project No.: 92563729
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
H1 Analysis conducted outside the recognized method holding time.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
60-02 HOLBROOKS LANDFILL
92563729
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92563729001
6002-HRW7
EPA 3010A
649812
EPA6010D
649827
92563729002
6002-HRW18
EPA 3010A
649812
EPA6010D
649827
92563729003
6002-HRW19
EPA 3010A
649812
EPA6010D
649827
92563729004
6002-HRW20
EPA 3010A
649812
EPA6010D
649827
92563729005
6002-HRW21
EPA 3010A
649812
EPA6010D
649827
92563729001
6002-HRW7
EPA 3010A
649884
EPA 6020B
649963
92563729002
6002-HRW18
EPA 3010A
649884
EPA 6020B
649963
92563729003
6002-HRW19
EPA 3010A
649884
EPA 6020B
649963
92563729004
6002-HRW20
EPA 3010A
649884
EPA 6020B
649963
92563729005
6002-HRW21
EPA 3010A
649884
EPA 6020B
649963
92563729001
6002-HRW7
8260D
1753823
EPA 8260D
1753823
92563729002
6002-HRW18
8260D
1753823
EPA 8260D
1753823
92563729003
6002-HRW19
8260D
1753823
EPA 8260D
1753823
92563729004
6002-HRW20
8260D
1754158
EPA 8260D
1754158
92563729004
6002-HRW20
8260D
1757506
EPA 8260D
1757506
92563729005
6002-HRW21
8260D
1754158
EPA 8260D
1754158
92563729005
6002-HRW21
8260D
1757506
EPA 8260D
1757506
92563729006
TRIP BLANK
8260D
1754158
EPA 8260D
1754158
92563729006
TRIP BLANK
8260D
1757506
EPA 8260D
1757506
92563729001
6002-HRW7
8260D-SIM
1755301
EPA 8260D by
SIM
1755301
92563729002
6002-HRW18
8260D-SIM
1755301
EPA 8260D by
SIM
1755301
92563729003
6002-HRW19
8260D-SIM
1755301
EPA 8260D by
SIM
1755301
92563729004
6002-HRW20
8260D-SIM
1755301
EPA 8260D by
SIM
1755301
92563729005
6002-HRW21
8260D-SIM
1755301
EPA 8260D by
SIM
1755301
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 06:47 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 31

Document Name: Document Revised: October 28, 2020
a Sample Condition Upon Receipt(SCUR) Page 1 of 2
�ceAnalytical Document No.: Issuing Authority:
F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville [/ Raleigh[] Mechanicsville❑ Atlanta[] Kernersville❑
ConditionSample Client Name: WD# 92563729
• Projec #:
Courier: ❑Fed Ex ❑UP5 0QC4ien
Commercial ti 1111111111111111111111
❑ []Pace 0ther: Othe� 82563729
Custody Seal Present? ❑Yes ENO Seals intact? ❑Yes l o
Date/Inftlals Person Examining Contents; =ls
Packing Material- ❑Bubble Wrap [j]Bubble Sags ❑None ❑ Other BlaIogicaI Tissue Fr zen?
Thermometer:' Des ❑iUo f/A
❑Wet ❑Blue []None
ype o ce:
y Correction Factor:
Cooler Temp; 'J Add/Subtract (°C) C! Temp should be above freezing to 6'C
Cooler Temp Corrected ('Ci; 05amQles out of temp criteria. Samples on ite, cooling process
Lru,/ has begun
USDA Regulated Soil ( N/A, water sample)
Did samples oriDinate in a ouarantine 7onp witfsin the I lnit.H rA ndv .,, cr r.�„-I,
Yes LJNo
111-11•uy,
'including Hawa+i and Puerto RRtel? ❑Yes ENO
Corn ments/Disc►epancy:
Chain of Custody Present?
U ees
❑No
❑N/A
1.
Samples Arrived within Hold Time?
iDres
[]No
❑N/A
2.
Short Hold Time Analysis <72 hr.j7
[]Yes.
I]No ,
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
❑ a
❑N/a
4.
Sufficient Volume?
Yes
(:]No
❑H/A
5.
Correct Containers Used?
Des
❑No
❑N/A
6.
-Pace Containers Used?
❑Yes
❑No
❑N/A
Containers Intact?
[]Yes
❑No
❑NIA
7-
Dissolved analysis: SamDles Field Filtered?
❑Yes
❑No
❑N/A
d.
Sample Labels Match COC?
❑Yes
[]NO
❑N/A
9.
Includes Date/Time/ID/Analysis Matrix:
v
Headspace in VOVi A al5 (>cr6mei
❑Ye
/
fQo
❑NIA
10.
Trip Blank Present?
e$
❑No
❑N/A
11.
Trip Blank Custody Seals Present?
es
❑No
❑N/A
COMMENTS/SAMPLE DISCREPANCY
CLIENT 10TIFIC4TI0NIBESOLUTION
-Person-contacted,
Project Manager SCURF Review:
Project Manager SRF Review:
Lot ID of split containers:
Date:
Dale;
Field Data Required? ❑Yes ❑No
Page 29 of 31

Document Name: Document Revised: October 28, 2020
C8MaVlCala Sample Condition Upon Recelpt(SCUR) Page 2 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.a7 Pace Carolinas Quality Office
"Check marls top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Caliform, TOC, Oil and Grease, 0RO/R015 (water) ❑OC, LLHg
**Bottom half of box is to list number of bottles
Project P , ro# ' 92663729
PM: MWB Due Dale: 10/12/21
CLIENT: 92—MECK CO
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pH Adjustment Lag for Preserved Samples - -
Sampie Id
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:ot I
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Note:�/Jheneverthere-is-3- disc repancyaffecting-Vorth-Gamlinit-comp lianEesamples-,-3tapy-oi4his feFm will he cant-_o h�voFFh aralina iJfi�iNi2 ectiflca[ioap[iitz-ll.a.
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Page 30 of 31

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leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
October 14, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 29, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 27

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21LA 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
60-02 Holbrooks Rd Landfill
92564053
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92564053001
6002-HRW8
EPA 601 OD
CBV
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92564053002
6002-HRW9R
EPA 601 OD
CBV
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92564053003
6002-HRW14
EPA 601 OD
CBV
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92564053004
6002-HRW15
EPA 601 OD
CBV
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92564053005
6002-HRW16
EPA 601 OD
CBV
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
JAH
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92564053006
TRIP BLANK
EPA 8260D
JAH
57
PAN
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: 6002-HRW8 Lab ID: 92564053001 Collected: 09/29/21 12:20 Received: 09/29/21 13:19 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2121:45
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2121:45
7440-38-2
Barium
260
ug/L
5.0
1
09/30/21 14:12
10/12/2121:45
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/30/21 14:12
10/12/2121:45
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/30/21 14:12
10/12/2121:45
7440-43-9
Chromium
5.7
ug/L
5.0
1
09/30/21 14:12
10/12/2121:45
7440-47-3
Cobalt
39.1
ug/L
5.0
1
09/30/21 14:12
10/12/2121:45
7440-48-4
Copper
10.3
ug/L
5.0
1
09/30/21 14:12
10/12/2121:45
7440-50-8
Lead
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2121:45
7439-92-1
Nickel
8.0
ug/L
5.0
1
09/30/21 14:12
10/12/2121:45
7440-02-0
Selenium
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2121:45
7782-49-2
Silver
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2121:45
7440-22-4
Thallium
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2121:45
7440-28-0
Vanadium
49.2
ug/L
5.0
1
09/30/21 14:12
10/12/2121:45
7440-62-2
Zinc
21.8
ug/L
10.0
1
09/30/21 14:12
10/12/2121:45
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation
Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/30/2113:22
10/01/2100:56
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation
Method: 8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/08/21 23:10
10/08/21 23:10
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/08/21 23:10
10/08/21 23:10
107-13-1
Benzene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
74-97-5
Bromoform
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/08/21 23:10
10/08/21 23:10
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
56-23-5 LO
Chlorobenzene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/08/21 23:10
10/08/21 23:10
75-00-3
Chloroform
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/08/21 23:10
10/08/21 23:10
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/08/21 23:10
10/08/21 23:10
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/08/21 23:10
10/08/21 23:10
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
106-46-7
1,1-Dichloroethane
2.40
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: 6002-HRW8
Lab ID: 92564053001
Collected: 09/29/21
12:20
Received: 09/29/21 13:19 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/08/21 23:10
10/08/21 23:10
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/08/21 23:10
10/08/21 23:10
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/08/21 23:10
10/08/21 23:10
591-78-6
lodomethane
ND
ug/L
5.00
1
10/08/21 23:10
10/08/21 23:10
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/08/21 23:10
10/08/21 23:10
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/08/21 23:10
10/08/21 23:10
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/08/21 23:10
10/08/21 23:10
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/08/21 23:10
10/08/21 23:10
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
127-18-4
Toluene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/08/21 23:10
10/08/21 23:10
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/08/21 23:10
10/08/21 23:10
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/08/21 23:10
10/08/21 23:10
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/08/21 23:10
10/08/21 23:10
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/08/21 23:10
10/08/21 23:10
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/08/21 23:10
10/08/21 23:10
179601-23-1
Surrogates
Toluene-d8 (S)
97.2
%
80.0-120
1
10/08/21 23:10
10/08/21 23:10
2037-26-5
4-Bromofluorobenzene (S)
88.8
%
77.0-126
1
10/08/21 23:10
10/08/21 23:10
460-00-4
1,2-Dichloroethane-d4 (S)
129
%
70.0-130
1
10/08/21 23:10
10/08/21 23:10
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method: EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
ND
ug/L
3.00
1
10/13/21 02:16
10/13/21 02:16
123-91-1
Surrogates
Toluene-d8 (S)
100
%
77.0-127
1
10/13/21 02:16
10/13/21 02:16
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in
full,
Date: 10/14/2021 09:14 AM
without
the written
consent of Pace Analytical
Services, LLC.
Page 5 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: 6002-HRW9R Lab ID: 92564053002 Collected: 09/29/21 12:00 Received: 09/29/21 13:19 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2122:10
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2122:10
7440-38-2
Barium
344
ug/L
5.0
1
09/30/21 14:12
10/12/2122:10
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/30/21 14:12
10/12/2122:10
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/30/21 14:12
10/12/2122:10
7440-43-9
Chromium
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2122:10
7440-47-3
Cobalt
8.8
ug/L
5.0
1
09/30/21 14:12
10/12/2122:10
7440-48-4
Copper
8.5
ug/L
5.0
1
09/30/21 14:12
10/12/2122:10
7440-50-8
Lead
5.4
ug/L
5.0
1
09/30/21 14:12
10/12/2122:10
7439-92-1
Nickel
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2122:10
7440-02-0
Selenium
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2122:10
7782-49-2
Silver
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2122:10
7440-22-4
Thallium
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2122:10
7440-28-0
Vanadium
77.1
ug/L
5.0
1
09/30/21 14:12
10/12/2122:10
7440-62-2
Zinc
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2122:10
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation
Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/30/2113:22
10/01/2101:06
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation
Method: 8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/08/21 23:30
10/08/21 23:30
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/08/21 23:30
10/08/21 23:30
107-13-1
Benzene
0.667
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
74-97-5
Bromoform
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/08/21 23:30
10/08/21 23:30
74-83-9
Carbon disulfide
0.846
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
56-23-5 LO
Chlorobenzene
1.96
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/08/21 23:30
10/08/21 23:30
75-00-3
Chloroform
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/08/21 23:30
10/08/21 23:30
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/08/21 23:30
10/08/21 23:30
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/08/21 23:30
10/08/21 23:30
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
74-95-3
1,2-Dichlorobenzene
2.76
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
541-73-1
1,4-Dichlorobenzene
3.44
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
106-46-7
1,1-Dichloroethane
37.0
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
75-34-3
1,2-Dichloroethane
2.71
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
107-06-2 C5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: 6002-HRW9R
Lab ID: 92564053002
Collected: 09/29/21
12:00
Received: 09/29/21 13:19 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
75-35-4
cis-1,2-Dichloroethene
65.3
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
156-59-2
trans-1,2-Dichloroethene
0.978
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
156-60-5
1,2-Dichloropropane
2.99
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/08/21 23:30
10/08/21 23:30
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/08/21 23:30
10/08/21 23:30
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/08/21 23:30
10/08/21 23:30
591-78-6
lodomethane
ND
ug/L
5.00
1
10/08/21 23:30
10/08/21 23:30
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/08/21 23:30
10/08/21 23:30
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/08/21 23:30
10/08/21 23:30
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/08/21 23:30
10/08/21 23:30
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/08/21 23:30
10/08/21 23:30
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
127-18-4
Toluene
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
79-00-5
Trichloroethene
1.64
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/08/21 23:30
10/08/21 23:30
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/08/21 23:30
10/08/21 23:30
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/08/21 23:30
10/08/21 23:30
108-05-4
Vinyl chloride
9.24
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/08/21 23:30
10/08/21 23:30
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/08/21 23:30
10/08/21 23:30
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/08/21 23:30
10/08/21 23:30
179601-23-1
Surrogates
Toluene-d8 (S)
98.4
%
80.0-120
1
10/08/21 23:30
10/08/21 23:30
2037-26-5
4-Bromofluorobenzene (S)
88.3
%
77.0-126
1
10/08/21 23:30
10/08/21 23:30
460-00-4
1,2-Dichloroethane-d4 (S)
126
%
70.0-130
1
10/08/21 23:30
10/08/21 23:30
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method:
EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
10.9 ug/L 3.00 1 10/13/2102:36 10/13/2102:36 123-91-1
100 % 77.0-127 1 10/13/21 02:36 10/13/2102:36 2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: 6002-HRW14 Lab ID: 92564053003 Collected: 09/29/21 11:50 Received: 09/29/21 13:19 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:13
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:13
7440-38-2
Barium
38.1
ug/L
5.0
1
09/30/2114:12
10/12/2122:13
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/30/2114:12
10/12/2122:13
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/30/2114:12
10/12/2122:13
7440-43-9
Chromium
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:13
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:13
7440-48-4
Copper
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:13
7440-50-8
Lead
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:13
7439-92-1
Nickel
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:13
7440-02-0
Selenium
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:13
7782-49-2
Silver
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:13
7440-22-4
Thallium
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:13
7440-28-0
Vanadium
9.8
ug/L
5.0
1
09/30/21 14:12
10/12/2122:13
7440-62-2
Zinc
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:13
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation
Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/30/2113:22
10/01/2101:10
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation
Method: 8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/08/21 23:51
10/08/21 23:51
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/08/21 23:51
10/08/21 23:51
107-13-1
Benzene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
74-97-5
Bromoform
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/08/21 23:51
10/08/21 23:51
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
56-23-5 LO
Chlorobenzene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/08/21 23:51
10/08/21 23:51
75-00-3
Chloroform
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/08/21 23:51
10/08/21 23:51
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/08/21 23:51
10/08/21 23:51
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/08/21 23:51
10/08/21 23:51
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
106-46-7
1,1-Dichloroethane
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: 6002-HRW14
Lab ID: 92564053003
Collected: 09/29/21
11:50
Received: 09/29/21 13:19 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/08/21 23:51
10/08/21 23:51
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/08/21 23:51
10/08/21 23:51
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/08/21 23:51
10/08/21 23:51
591-78-6
lodomethane
ND
ug/L
5.00
1
10/08/21 23:51
10/08/21 23:51
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/08/21 23:51
10/08/21 23:51
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/08/21 23:51
10/08/21 23:51
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/08/21 23:51
10/08/21 23:51
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/08/21 23:51
10/08/21 23:51
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
79-34-5
Tetrachloroethene
1.21
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
127-18-4
Toluene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/08/21 23:51
10/08/21 23:51
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/08/21 23:51
10/08/21 23:51
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/08/21 23:51
10/08/21 23:51
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/08/21 23:51
10/08/21 23:51
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/08/21 23:51
10/08/21 23:51
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/08/21 23:51
10/08/21 23:51
179601-23-1
Surrogates
Toluene-d8 (S)
98.4
%
80.0-120
1
10/08/21 23:51
10/08/21 23:51
2037-26-5
4-Bromofluorobenzene (S)
89.4
%
77.0-126
1
10/08/21 23:51
10/08/21 23:51
460-00-4
1,2-Dichloroethane-d4 (S)
130
%
70.0-130
1
10/08/21 23:51
10/08/21 23:51
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method:
EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
ND ug/L 3.00 1 10/13/2102:56 10/13/2102:56 123-91-1
99.9 % 77.0-127 1 10/13/21 02:56 10/13/2102:56 2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: 6002-HRW15 Lab ID: 92564053004 Collected: 09/29/21 11:40 Received: 09/29/21 13:19 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2122:16
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2122:16
7440-38-2
Barium
140
ug/L
5.0
1
09/30/21 14:12
10/12/2122:16
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/30/21 14:12
10/12/2122:16
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/30/21 14:12
10/12/2122:16
7440-43-9
Chromium
13.0
ug/L
5.0
1
09/30/21 14:12
10/12/2122:16
7440-47-3
Cobalt
7.7
ug/L
5.0
1
09/30/21 14:12
10/12/2122:16
7440-48-4
Copper
90.3
ug/L
5.0
1
09/30/21 14:12
10/12/2122:16
7440-50-8
Lead
8.1
ug/L
5.0
1
09/30/21 14:12
10/12/2122:16
7439-92-1
Nickel
5.8
ug/L
5.0
1
09/30/21 14:12
10/12/2122:16
7440-02-0
Selenium
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2122:16
7782-49-2
Silver
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2122:16
7440-22-4
Thallium
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2122:16
7440-28-0
Vanadium
73.4
ug/L
5.0
1
09/30/21 14:12
10/12/2122:16
7440-62-2
Zinc
44.3
ug/L
10.0
1
09/30/21 14:12
10/12/2122:16
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation
Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/30/2113:22
10/01/2101:13
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation
Method: 8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/09/21 00:11
10/09/21 00:11
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/09/21 00:11
10/09/21 00:11
107-13-1
Benzene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
74-97-5
Bromoform
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/09/21 00:11
10/09/21 00:11
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
56-23-5 LO
Chlorobenzene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/09/21 00:11
10/09/21 00:11
75-00-3
Chloroform
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/09/21 00:11
10/09/21 00:11
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/09/21 00:11
10/09/21 00:11
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/09/21 00:11
10/09/21 00:11
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
106-46-7
1,1-Dichloroethane
0.883
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: 6002-HRW15 Lab ID: 92564053004 Collected: 09/29/21 11:40 Received: 09/29/21 13:19 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/09/21 00:11
10/09/21 00:11
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/09/21 00:11
10/09/21 00:11
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/09/21 00:11
10/09/21 00:11
591-78-6
lodomethane
ND
ug/L
5.00
1
10/09/21 00:11
10/09/21 00:11
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/09/21 00:11
10/09/21 00:11
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/09/21 00:11
10/09/21 00:11
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/09/21 00:11
10/09/21 00:11
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/09/21 00:11
10/09/21 00:11
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
79-34-5
Tetrachloroethene
0.959
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
127-18-4
Toluene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/09/21 00:11
10/09/21 00:11
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/09/21 00:11
10/09/21 00:11
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/09/21 00:11
10/09/21 00:11
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/09/21 00:11
10/09/21 00:11
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/09/21 00:11
10/09/21 00:11
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/09/21 00:11
10/09/21 00:11
179601-23-1
Surrogates
Toluene-d8 (S)
93.6
%
80.0-120
1
10/09/21 00:11
10/09/21 00:11
2037-26-5
4-Bromofluorobenzene (S)
86.1
%
77.0-126
1
10/09/21 00:11
10/09/21 00:11
460-00-4
1,2-Dichloroethane-d4 (S)
132
%
70.0-130
1
10/09/21 00:11
10/09/21 00:11
17060-07-0 ST
VOA (GC/MS) 8260D-SIM
Analytical Method: EPA 8260D
by SIM Preparation
Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
ND
ug/L
3.00
1
10/13/21 03:16
10/13/21 03:16
123-91-1
Surrogates
Toluene-d8 (S)
99.9
%
77.0-127
1
10/13/21 03:16
10/13/21 03:16
2037-26-5
REPORT OF LABORATORY
ANALYSIS
This report shall not
be reproduced, except
in full,
Date: 10/14/2021 09:14 AM
without
the written consent
of Pace Analytical Services,
LLC.
Page 11 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: 6002-HRW16 Lab ID: 92564053005 Collected: 09/29/21 11:25 Received: 09/29/21 13:19 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2122:20
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2122:20
7440-38-2
Barium
156
ug/L
5.0
1
09/30/21 14:12
10/12/2122:20
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/30/21 14:12
10/12/2122:20
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/30/21 14:12
10/12/2122:20
7440-43-9
Chromium
6.2
ug/L
5.0
1
09/30/21 14:12
10/12/2122:20
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2122:20
7440-48-4
Copper
16.7
ug/L
5.0
1
09/30/21 14:12
10/12/2122:20
7440-50-8
Lead
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2122:20
7439-92-1
Nickel
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2122:20
7440-02-0
Selenium
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2122:20
7782-49-2
Silver
ND
ug/L
5.0
1
09/30/21 14:12
10/12/2122:20
7440-22-4
Thallium
ND
ug/L
10.0
1
09/30/21 14:12
10/12/2122:20
7440-28-0
Vanadium
25.4
ug/L
5.0
1
09/30/21 14:12
10/12/2122:20
7440-62-2
Zinc
14.6
ug/L
10.0
1
09/30/21 14:12
10/12/2122:20
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation
Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/30/2113:22
10/01/2101:17
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation
Method: 8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/09/21 00:31
10/09/21 00:31
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/09/21 00:31
10/09/21 00:31
107-13-1
Benzene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
74-97-5
Bromoform
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/09/21 00:31
10/09/21 00:31
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
56-23-5 LO
Chlorobenzene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/09/21 00:31
10/09/21 00:31
75-00-3
Chloroform
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/09/21 00:31
10/09/21 00:31
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/09/21 00:31
10/09/21 00:31
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/09/21 00:31
10/09/21 00:31
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
106-46-7
1,1-Dichloroethane
2.95
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: 6002-HRW16
Lab ID: 92564053005
Collected: 09/29/21
11:25
Received: 09/29/21 13:19 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/09/21 00:31
10/09/21 00:31
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/09/21 00:31
10/09/21 00:31
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/09/21 00:31
10/09/21 00:31
591-78-6
lodomethane
ND
ug/L
5.00
1
10/09/21 00:31
10/09/21 00:31
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/09/21 00:31
10/09/21 00:31
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/09/21 00:31
10/09/21 00:31
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/09/21 00:31
10/09/21 00:31
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/09/21 00:31
10/09/21 00:31
91-20-3 C3
Styrene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
127-18-4
Toluene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/09/21 00:31
10/09/21 00:31
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/09/21 00:31
10/09/21 00:31
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/09/21 00:31
10/09/21 00:31
108-05-4
Vinyl chloride
0.611
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/09/21 00:31
10/09/21 00:31
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/09/21 00:31
10/09/21 00:31
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/09/21 00:31
10/09/21 00:31
179601-23-1
Surrogates
Toluene-d8 (S)
97.9
%
80.0-120
1
10/09/21 00:31
10/09/21 00:31
2037-26-5
4-Bromofluorobenzene (S)
91.1
%
77.0-126
1
10/09/21 00:31
10/09/21 00:31
460-00-4
1,2-Dichloroethane-d4 (S)
127
%
70.0-130
1
10/09/21 00:31
10/09/21 00:31
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method:
EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
8.94 ug/L 3.00 1 10/13/2103:36 10/13/2103:36 123-91-1
99.8 % 77.0-127 1 10/13/21 03:36 10/13/2103:36 2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 27

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: TRIP BLANK Lab ID: 92564053006 Collected: 09/29/21 09:30 Received: 09/29/21 13:19 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/08/21 20:47
10/08/21 20:47
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/08/21 20:47
10/08/21 20:47
107-13-1
Benzene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
74-97-5
Bromoform
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/08/21 20:47
10/08/21 20:47
74-83-9
Carbon disulfide
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
56-23-5
Chlorobenzene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/08/21 20:47
10/08/21 20:47
75-00-3
Chloroform
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/08/21 20:47
10/08/21 20:47
74-87-3
Chloroprene
ND
ug/L
50.0
1
10/08/21 20:47
10/08/21 20:47
126-99-8
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/08/21 20:47
10/08/21 20:47
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
106-46-7
1,1-Dichloroethane
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
107-06-2
1,1-Dichloroethene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/08/21 20:47
10/08/21 20:47
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/08/21 20:47
10/08/21 20:47
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/08/21 20:47
10/08/21 20:47
591-78-6
lodomethane
ND
ug/L
5.00
1
10/08/21 20:47
10/08/21 20:47
74-88-4
2-Butanone (MEK)
ND
ug/L
5.00
1
10/08/21 20:47
10/08/21 20:47
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/08/21 20:47
10/08/21 20:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/08/21 20:47
10/08/21 20:47
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/08/21 20:47
10/08/21 20:47
91-20-3
Styrene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
127-18-4
Toluene
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
79-00-5
REPORT OF LABORATORY ANALYSIS
Qual
LO
C3
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 27

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
Sample: TRIP BLANK Lab ID: 92564053006 Collected: 09/29/21 09:30 Received: 09/29/21 13:19 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
o-Xylene
m&p-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 10/14/2021 09:14 AM
Analytical Method: EPA 8260D Preparation Method: 8260D
Pace National - Mt. Juliet
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
79-01-6
ND
ug/L
2.50
1
10/08/21 20:47
10/08/21 20:47
75-69-4
ND
ug/L
2.50
1
10/08/21 20:47
10/08/21 20:47
96-18-4
ND
ug/L
5.00
1
10/08/21 20:47
10/08/21 20:47
108-05-4
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
75-01-4
ND
ug/L
1.50
1
10/08/21 20:47
10/08/21 20:47
1330-20-7
ND
ug/L
0.500
1
10/08/21 20:47
10/08/21 20:47
95-47-6
ND
ug/L
1.00
1
10/08/21 20:47
10/08/21 20:47
179601-23-1
97.6
%
80.0-120
1
10/08/21 20:47
10/08/21 20:47
2037-26-5
89.1
%
77.0-126
1
10/08/21 20:47
10/08/21 20:47
460-00-4
125
%
70.0-130
1
10/08/21 20:47
10/08/21 20:47
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 27

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
QC Batch: 650175 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564053001, 92564053002, 92564053003, 92564053004, 92564053005
METHOD BLANK: 3410019 Matrix: Water
Associated Lab Samples: 92564053001, 92564053002, 92564053003, 92564053004, 92564053005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony
ug/L
ND
5.0
10/12/2121:38
Arsenic
ug/L
ND
10.0
10/12/2121:38
Barium
ug/L
ND
5.0
10/12/2121:38
Beryllium
ug/L
ND
1.0
10/12/2121:38
Cadmium
ug/L
ND
1.0
10/12/2121:38
Chromium
ug/L
ND
5.0
10/12/2121:38
Cobalt
ug/L
ND
5.0
10/12/2121:38
Copper
ug/L
ND
5.0
10/12/2121:38
Lead
ug/L
ND
5.0
10/12/2121:38
Nickel
ug/L
ND
5.0
10/12/2121:38
Selenium
ug/L
ND
10.0
10/12/2121:38
Silver
ug/L
ND
5.0
10/12/2121:38
Thallium
ug/L
ND
10.0
10/12/2121:38
Vanadium
ug/L
ND
5.0
10/12/2121:38
Zinc
ug/L
ND
10.0
10/12/2121:38
LABORATORY CONTROL SAMPLE:
Parameter
3410020
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
485
97
80-120
Arsenic
ug/L
500
476
95
80-120
Barium
ug/L
500
505
101
80-120
Beryllium
ug/L
500
489
98
80-120
Cadmium
ug/L
500
482
96
80-120
Chromium
ug/L
500
491
98
80-120
Cobalt
ug/L
500
469
94
80-120
Copper
ug/L
500
512
102
80-120
Lead
ug/L
500
483
97
80-120
Nickel
ug/L
500
484
97
80-120
Selenium
ug/L
500
461
92
80-120
Silver
ug/L
250
243
97
80-120
Thallium
ug/L
500
481
96
80-120
Vanadium
ug/L
500
492
98
80-120
Zinc
ug/L
500
480
96
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 27

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
60-02 Holbrooks Rd Landfill
92564053
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3410021
3410022
MS
MSD
92564053001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
490
496
98
99
75-125
1
Arsenic
ug/L
ND
500
500
500
494
99
98
75-125
1
Barium
ug/L
260
500
500
769
757
102
100
75-125
2
Beryllium
ug/L
ND
500
500
496
496
99
99
75-125
0
Cadmium
ug/L
ND
500
500
501
498
100
100
75-125
0
Chromium
ug/L
5.7
500
500
506
501
100
99
75-125
1
Cobalt
ug/L
39.1
500
500
518
515
96
95
75-125
0
Copper
ug/L
10.3
500
500
534
525
105
103
75-125
2
Lead
ug/L
ND
500
500
500
496
99
98
75-125
1
Nickel
ug/L
8.0
500
500
499
497
98
98
75-125
0
Selenium
ug/L
ND
500
500
512
515
102
103
75-125
1
Silver
ug/L
ND
250
250
255
253
101
100
75-125
1
Thallium
ug/L
ND
500
500
489
491
97
98
75-125
0
Vanadium
ug/L
49.2
500
500
553
545
101
99
75-125
1
Zinc
ug/L
21.8
500
500
513
508
98
97
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 27

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
QC Batch: 650167 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564053001, 92564053002, 92564053003, 92564053004, 92564053005
METHOD BLANK: 3409966
Matrix:
Water
Associated Lab Samples: 92564053001, 92564053002, 92564053003, 92564053004, 92564053005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.47
10/01/2100:13
LABORATORY CONTROL SAMPLE:
3409967
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
24.8
99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3409968 3409969
MS MSD
92564021001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 24.5 24.6 98 98 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 27

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
QC Batch: 1753823 Analysis Method: EPA 8260D
QC Batch Method: 8260B Analysis Description: VOA (GC/MS) 8260D
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92564053001, 92564053002, 92564053003, 92564053004, 92564053005, 92564053006
METHOD BLANK: R3714680-3 Matrix: Water
Associated Lab Samples: 92564053001, 92564053002, 92564053003, 92564053004, 92564053005, 92564053006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1,1-Trichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1,2,2-Tetrachloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1,2-Trichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1-Dichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,1-Dichloroethene
ug/L
ND
0.500
10/08/21 20:27
1,1-Dichloropropene
ug/L
ND
0.500
10/08/21 20:27
1,2,3-Trichloropropane
ug/L
ND
2.50
10/08/21 20:27
1,2-Dibromo-3-chloropropane
ug/L
ND
2.50
10/08/21 20:27
1,2-Dibromoethane (EDB)
ug/L
ND
0.500
10/08/21 20:27
1,2-Dichlorobenzene
ug/L
ND
0.500
10/08/21 20:27
1,2-Dichloroethane
ug/L
ND
0.500
10/08/21 20:27
1,2-Dichloropropane
ug/L
ND
0.500
10/08/21 20:27
1,3-Dichlorobenzene
ug/L
ND
0.500
10/08/21 20:27
1,3-Dichloropropane
ug/L
ND
1.00
10/08/21 20:27
1,4-Dichlorobenzene
ug/L
ND
0.500
10/08/21 20:27
2-Butanone (MEK)
ug/L
ND
5.00
10/08/21 20:27
2-Hexanone
ug/L
ND
5.00
10/08/21 20:27
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.00
10/08/21 20:27
Acetone
ug/L
ND
25.0
10/08/21 20:27
Acrylonitrile
ug/L
ND
5.00
10/08/21 20:27
Benzene
ug/L
ND
0.500
10/08/21 20:27
Bromochloromethane
ug/L
ND
0.500
10/08/21 20:27
Bromodichloromethane
ug/L
ND
0.500
10/08/21 20:27
Bromoform
ug/L
ND
0.500
10/08/21 20:27
Bromomethane
ug/L
ND
2.50
10/08/21 20:27
Carbon disulfide
ug/L
ND
0.500
10/08/21 20:27
Carbon tetrachloride
ug/L
ND
0.500
10/08/21 20:27
Chlorobenzene
ug/L
ND
0.500
10/08/21 20:27
Dibromochloromethane
ug/L
ND
0.500
10/08/21 20:27
Chloroethane
ug/L
ND
2.50
10/08/21 20:27
Chloroform
ug/L
ND
0.500
10/08/21 20:27
Chloromethane
ug/L
ND
1.25
10/08/21 20:27
Chloroprene
ug/L
ND
50.0
10/08/21 20:27
cis-1,2-Dichloroethene
ug/L
ND
0.500
10/08/21 20:27
cis-1,3-Dichloropropene
ug/L
ND
0.500
10/08/21 20:27
Dibromomethane
ug/L
ND
0.500
10/08/21 20:27
Ethylbenzene
ug/L
ND
0.500
10/08/21 20:27
lodomethane
ug/L
ND
5.00
10/08/21 20:27
m&p-Xylene
ug/L
ND
1.00
10/08/21 20:27
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 27

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
METHOD BLANK: R3714680-3 Matrix: Water
Associated Lab Samples: 92564053001, 92564053002, 92564053003, 92564053004, 92564053005, 92564053006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Methylene Chloride
ug/L
ND
2.50
10/08/21 20:27
Naphthalene
ug/L
ND
2.50
10/08/21 20:27
o-Xylene
ug/L
ND
0.500
10/08/21 20:27
Styrene
ug/L
ND
0.500
10/08/21 20:27
Tetrachloroethene
ug/L
ND
0.500
10/08/21 20:27
Toluene
ug/L
ND
0.500
10/08/21 20:27
trans-1,2-Dichloroethene
ug/L
ND
0.500
10/08/21 20:27
trans- 1,3-Dichloropropene
ug/L
ND
0.500
10/08/21 20:27
trans-1,4-Dichloro-2-butene
ug/L
ND
5.00
10/08/21 20:27
Trichloroethene
ug/L
ND
0.500
10/08/21 20:27
Trichlorofluoromethane
ug/L
ND
2.50
10/08/21 20:27
Vinyl acetate
ug/L
ND
5.00
10/08/21 20:27
Vinyl chloride
ug/L
ND
0.500
10/08/21 20:27
Xylene (Total)
ug/L
ND
1.50
10/08/21 20:27
1,2-Dichloroethane-d4 (S)
%
129
70.0-130
10/08/21 20:27
Toluene-d8 (S)
%
94.9
80.0-120
10/08/21 20:27
4-Bromofluorobenzene (S)
%
91.6
77.0-126
10/08/21 20:27
LABORATORY CONTROL SAMPLE:
Parameter
R3714680-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
5.00
5.06
101
75.0-125
1,1,1-Trichloroethane
ug/L
5.00
6.13
123
73.0-124
1,1,2,2-Tetrachloroethane
ug/L
5.00
4.29
85.8
65.0-130
1,1,2-Trichloroethane
ug/L
5.00
5.00
100
80.0-120
1,1-Dichloroethane
ug/L
5.00
5.61
112
70.0-126
1,1-Dichloroethene
ug/L
5.00
5.05
101
71.0-124
1,1-Dichloropropene
ug/L
5.00
5.86
117
74.0-126
1,2,3-Trichloropropane
ug/L
5.00
5.04
101
73.0-130
1,2-Dibromo-3-chloropropane
ug/L
5.00
4.08
81.6
58.0-134
1,2-Dibromoethane (EDB)
ug/L
5.00
5.18
104
80.0-122
1,2-Dichlorobenzene
ug/L
5.00
5.10
102
79.0-121
1,2-Dichloroethane
ug/L
5.00
6.05
121
70.0-128
1,2-Dichloropropane
ug/L
5.00
5.28
106
77.0-125
1,3-Dichlorobenzene
ug/L
5.00
4.79
95.8
79.0-120
1,3-Dichloropropane
ug/L
5.00
5.97
119
80.0-120
1,4-Dichlorobenzene
ug/L
5.00
4.91
98.2
79.0-120
2-Butanone (MEK)
ug/L
25.0
27.2
109
44.0-160
2-Hexanone
ug/L
25.0
23.7
94.8
67.0-149
4-Methyl-2-pentanone (MIBK)
ug/L
25.0
27.8
111
68.0-142
Acetone
ug/L
25.0
29.7
119
19.0-160
Acrylonitrile
ug/L
25.0
26.0
104
55.0-149
Benzene
ug/L
5.00
5.37
107
70.0-123
Bromochloromethane
ug/L
5.00
5.08
102
76.0-122
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 27

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
LABORATORY CONTROL SAMPLE:
Parameter
R3714680-1
Units
Spike LCS
Conc. Result
Bromodichloromethane
ug/L
5.00
Bromoform
ug/L
5.00
Bromomethane
ug/L
5.00
Carbon disulfide
ug/L
5.00
Carbon tetrachloride
ug/L
5.00
Chlorobenzene
ug/L
5.00
Dibromochloromethane
ug/L
5.00
Chloroethane
ug/L
5.00
Chloroform
ug/L
5.00
Chloromethane
ug/L
5.00
cis-1,2-Dichloroethene
ug/L
5.00
cis-1,3-Dichloropropene
ug/L
5.00
Dibromomethane
ug/L
5.00
Ethylbenzene
ug/L
5.00
lodomethane
ug/L
25.0
m&p-Xylene
ug/L
10.0
Methylene Chloride
ug/L
5.00
Naphthalene
ug/L
5.00
o-Xylene
ug/L
5.00
Styrene
ug/L
5.00
Tetrachloroethene
ug/L
5.00
Toluene
ug/L
5.00
trans-1,2-Dichloroethene
ug/L
5.00
trans- 1,3-Dichloropropene
ug/L
5.00
trans-1,4-Dichloro-2-butene
ug/L
5.00
Trichloroethene
ug/L
5.00
Trichlorofluoromethane
ug/L
5.00
Vinyl acetate
ug/L
25.0
Vinyl chloride
ug/L
5.00
Xylene (Total)
ug/L
15.0
1,2-Dichloroethane-d4 (S)
%
Toluene-d8 (S)
%
4-Bromofluorobenzene (S)
%
LCS
% Rec
% Rec
Limits Qualifiers
5.55
111
75.0-120
5.31
106
68.0-132
4.30
86.0
10.0-160
5.89
118
61.0-128
6.33
127
68.0-126 LO
4.92
98.4
80.0-121
5.29
106
77.0-125
4.02
80.4
47.0-150
5.80
116
73.0-120
5.08
102
41.0-142
4.81
96.2
73.0-120
5.47
109
80.0-123
5.48
110
80.0-120
5.04
101
79.0-123
27.2
109
33.0-147
9.96
99.6
80.0-122
5.18
104
67.0-120
3.06
61.2
54.0-135
4.79
95.8
80.0-122
4.92
98.4
73.0-130
5.56
111
72.0-132
5.08
102
79.0-120
5.40
108
73.0-120
5.62
112
78.0-124
4.25
85.0
33.0-144
5.48
110
78.0-124
6.00
120
59.0-147
23.9
95.6
11.0-160
4.69
93.8
67.0-131
14.7
98.0
79.0-123
125
70.0-130
96.2
80.0-120
92.0
77.0-126
LABORATORY CONTROL SAMPLE:
R3714680-2
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Chloroprene
ug/L
50.0 45.1 90.2
60.0-143
1,2-Dichloroethane-d4 (S)
%
128
70.0-130
Toluene-d8 (S)
%
95.4
80.0-120
4-Bromofluorobenzene (S)
%
90.9
77.0-126
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
QC Batch: 1751497 Analysis Method: EPA 8260D by SIM
QC Batch Method: 8260B-SIM Analysis Description: VOA (GC/MS) 8260D-SIM
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92564053001, 92564053002, 92564053003, 92564053004, 92564053005
METHOD BLANK: R3715966-3 Matrix: Water
Associated Lab Samples: 92564053001, 92564053002, 92564053003, 92564053004, 92564053005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,4-Dioxane (p-Dioxane) ug/L ND 3.00 10/12/21 23:18
Toluene-d8 (S) % 99.7 77.0-127 10/12/21 23:18
LABORATORY CONTROL SAMPLE & LCSD: R3715966-1
R3715966-2
Spike
LCS LCSD
LCS LCSD
% Rec Max
Parameter Units Conc.
Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 50.0
52.9 51.9
106 104
55.0-138 1.91 24
Toluene-d8 (S) %
99.9 100
77.0-127
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC.
Page 22 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 60-02 Holbrooks Rd Landfill
Pace Project No.: 92564053
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
C5 The reported concentration is an estimate. The continuing calibration standard associated with this data responded high.
Data is likely to show a high bias concerning the result.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
ST Surrogate recovery was above laboratory control limits. Results may be biased high.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
60-02 Holbrooks Rd Landfill
92564053
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92564053001
6002-HRW8
EPA 3010A
650175
EPA6010D
650225
92564053002
6002-HRW9R
EPA 3010A
650175
EPA6010D
650225
92564053003
6002-HRW14
EPA 3010A
650175
EPA6010D
650225
92564053004
6002-HRW15
EPA 3010A
650175
EPA6010D
650225
92564053005
6002-HRW16
EPA 3010A
650175
EPA6010D
650225
92564053001
6002-HRW8
EPA 3010A
650167
EPA 6020B
650222
92564053002
6002-HRW9R
EPA 3010A
650167
EPA 6020B
650222
92564053003
6002-HRW14
EPA 3010A
650167
EPA 6020B
650222
92564053004
6002-HRW15
EPA 3010A
650167
EPA 6020B
650222
92564053005
6002-HRW16
EPA 3010A
650167
EPA 6020B
650222
92564053001
6002-HRW8
8260D
1753823
EPA 8260D
1753823
92564053002
6002-HRW9R
8260D
1753823
EPA 8260D
1753823
92564053003
6002-HRW14
8260D
1753823
EPA 8260D
1753823
92564053004
6002-HRW15
8260D
1753823
EPA 8260D
1753823
92564053005
6002-HRW16
8260D
1753823
EPA 8260D
1753823
92564053006
TRIP BLANK
8260D
1753823
EPA 8260D
1753823
92564053001
6002-HRW8
8260D-SIM
1751497
EPA 8260D by
SIM
1751497
92564053002
6002-HRW9R
8260D-SIM
1751497
EPA 8260D by
SIM
1751497
92564053003
6002-HRW14
8260D-SIM
1751497
EPA 8260D by
SIM
1751497
92564053004
6002-HRW15
8260D-SIM
1751497
EPA 8260D by
SIM
1751497
92564053005
6002-HRW16
8260D-SIM
1751497
EPA 8260D by
SIM
1751497
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/14/2021 09:14 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 27

Document Name: Document Revised: October 28, 2020
. acrYAnalytrcal a Sample Condition Upon Recelpt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev,07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑
Sample Condition Client Name: A#: 92564053
1 /// 77 Project
Cou►fer: ❑Fed_Ex ❑UPS ❑LISPS ❑Client 1111111111111
111111111111111
❑ Commercial 4Pace ❑Other:
/ 92564053
i�
Custody SeaiPresent? ❑Yes QNo Seals Intact? ❑Yes QNo
Date/Initlals Person Examining Contents:`//31
Packing Material: ❑Bubble Wrap M8ubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes ❑No CN/A
QWet ❑Blue ❑None
+ --Type OF ce:
Correction Factor:
Gaoler Temp: Add/Subtract ('C) (� Temp shaufd be above freezing to VC
❑Sampies out of temp criteria. 5amples on ice, cooling process
Cooler Temp Corrected (C): _ ) �� has begun
USDA Regulated Soil ( [tJI/A, water sample)
Did samples originate in a quarantine tone within the United States: CA, NY, or SC (check maps)? Did samples originate From a Foreign source (Internationally,
Yes ❑No includingdawau and Puerto Ricol? PYes FNo
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold lime Analysis (02 li
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match COC?
-includes Datefrime/It7/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
Trip Blank Present?
Trip Blank Custody Seals present?
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
IJNO
UIN/A
1.
[]NO❑N/A
2.
@No_
❑N/A
1
® o
❑N/A
4.
[:],'do
QN/A
5.
©No
❑N/A
6.
❑No
❑N/A
LVYes UN/o [--]N/A 7.
❑Yes Q o ❑N/A 8.
EgYes ❑No ❑N/A 9.
.1
LJN/A 1 10.
❑N/A 1 11.
Lot ID of splitcontainers:
Person -cant -acted: DatefTime:
Project Manager SCURF Review: Date:
Protect Manager SRF Review: Dales•
Field Data Required? ❑Yes ❑No
Page 25 of 27

Document Name:
Condition Upon Recei
Document No.;
F CAR-05-033-Aev.07
"Check mark top half of box if pH and f or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Cchform, TCC, OR and Grease, DRO/9025 {water) DOC, LLHg
**Bottom half of box is to list number of bottles
Document Revised! October 28, 2020
Page 2 of 2
issuing Authority:
Project iWO# : 92564Q53
PM: MWB Due Date: 10/13/21
CLIENT: 92—MECK CO
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Sample ID
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Date preservation adjusted
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tat O
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added
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Page 26 of 27

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m
v 0
C
Q"
w
{ � n
z v c
m
m m
ro
d m
TEMP in C
N m A
y
o
Residual Chlorine (Y!N)
c
m m n
_ o
0 p
D
c
' n
Received on
Ice
(YIN)
ustc y
Sealed
Cooler
o
o
O
YIN
z
w
Q
Samples
Intact
(YIN)
Page 27 of 27

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
October 19, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on September 29, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21-A 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92564056001 6002-HRSW2
EPA 601 OD
CBV
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
JAH,JCP
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92564056002 6002-HRSW3
EPA 601 OD
CBV
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
JAH,JCP
57
PAN
EPA 8260D by SIM
BMB
2
PAN
92564056003 6002-HRSW4
EPA 601 OD
CBV
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
JAH,JCP
57
PAN
EPA 8260D by SIM
BMB
2
PAN
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
Sample: 6002-HRSW2 Lab ID: 92564056001 Collected: 09/29/21 11:00 Received: 09/29/21 13:19 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:23
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:23
7440-38-2
Barium
38.0
ug/L
5.0
1
09/30/2114:12
10/12/2122:23
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/30/2114:12
10/12/2122:23
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/30/2114:12
10/12/2122:23
7440-43-9
Chromium
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:23
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:23
7440-48-4
Copper
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:23
7440-50-8
Lead
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:23
7439-92-1
Nickel
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:23
7440-02-0
Selenium
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:23
7782-49-2
Silver
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:23
7440-22-4
Thallium
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:23
7440-28-0
Vanadium
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:23
7440-62-2
Zinc
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:23
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation
Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/30/2113:22
10/01/2101:20
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation
Method: 8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/10/21 11:29
10/10/21 11:29
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/10/21 11:29
10/10/21 11:29
107-13-1
Benzene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
74-97-5
Bromoform
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/10/21 11:29
10/10/21 11:29
74-83-9 C3
Carbon disulfide
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
56-23-5
Chlorobenzene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/10/21 11:29
10/10/21 11:29
75-00-3
Chloroform
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/10/21 11:29
10/10/21 11:29
74-87-3 C3
Chloroprene
ND
ug/L
50.0
1
10/14/2122:07
10/14/2122:07
126-99-8 H1
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/10/21 11:29
10/10/21 11:29
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
106-46-7
1,1-Dichloroethane
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
Sample: 6002-HRSW2
Lab ID: 92564056001
Collected: 09/29/21
11:00
Received: 09/29/21 13:19 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/10/21 11:29
10/10/21 11:29
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/10/21 11:29
10/10/21 11:29
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/10/21 11:29
10/10/21 11:29
591-78-6
lodomethane
ND
ug/L
5.00
1
10/10/21 11:29
10/10/21 11:29
74-88-4 C3
2-Butanone (MEK)
ND
ug/L
5.00
1
10/10/21 11:29
10/10/21 11:29
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/10/21 11:29
10/10/21 11:29
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/10/21 11:29
10/10/21 11:29
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/10/21 11:29
10/10/21 11:29
91-20-3
Styrene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
127-18-4
Toluene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/10/21 11:29
10/10/21 11:29
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/10/21 11:29
10/10/21 11:29
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/10/21 11:29
10/10/21 11:29
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/10/21 11:29
10/10/21 11:29
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/10/21 11:29
10/10/21 11:29
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/10/21 11:29
10/10/21 11:29
179601-23-1
Surrogates
Toluene-d8 (S)
106
%
80.0-120
1
10/10/21 11:29
10/10/21 11:29
2037-26-5
Toluene-d8 (S)
93.5
%
80.0-120
1
10/14/21 22:07
10/14/21 22:07
2037-26-5
4-Bromofluorobenzene (S)
99.7
%
77.0-126
1
10/10/21 11:29
10/10/21 11:29
460-00-4
4-Bromofluorobenzene (S)
93.7
%
77.0-126
1
10/14/21 22:07
10/14/21 22:07
460-00-4
1,2-Dichloroethane-d4 (S)
109
%
70.0-130
1
10/10/21 11:29
10/10/21 11:29
17060-07-0
1,2-Dichloroethane-d4 (S)
112
%
70.0-130
1
10/14/21 22:07
10/14/21 22:07
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method: EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
ND ug/L 3.00 1 10/13/2103:55 10/13/2103:55 123-91-1
100 % 77.0-127 1 10/13/21 03:55 10/13/2103:55 2037-26-5
REPORT OF LABORATORY ANALYSIS
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Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
Sample: 6002-HRSW3 Lab ID: 92564056002 Collected: 09/29/21 10:10 Received: 09/29/21 13:19 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:26
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:26
7440-38-2
Barium
40.1
ug/L
5.0
1
09/30/2114:12
10/12/2122:26
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/30/2114:12
10/12/2122:26
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/30/2114:12
10/12/2122:26
7440-43-9
Chromium
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:26
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:26
7440-48-4
Copper
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:26
7440-50-8
Lead
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:26
7439-92-1
Nickel
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:26
7440-02-0
Selenium
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:26
7782-49-2
Silver
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:26
7440-22-4
Thallium
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:26
7440-28-0
Vanadium
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:26
7440-62-2
Zinc
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:26
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation
Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/30/2113:22
10/01/2101:24
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation
Method: 8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/10/21 11:51
10/10/21 11:51
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/10/21 11:51
10/10/21 11:51
107-13-1
Benzene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
74-97-5
Bromoform
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/10/21 11:51
10/10/21 11:51
74-83-9 C3
Carbon disulfide
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
56-23-5
Chlorobenzene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/10/21 11:51
10/10/21 11:51
75-00-3
Chloroform
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/10/21 11:51
10/10/21 11:51
74-87-3 C3
Chloroprene
ND
ug/L
50.0
1
10/14/2122:27
10/14/2122:27
126-99-8 H1
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/10/21 11:51
10/10/21 11:51
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
106-46-7
1,1-Dichloroethane
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
Sample: 6002-HRSW3
Lab ID: 92564056002
Collected: 09/29/21
10:10
Received: 09/29/21 13:19 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/10/21 11:51
10/10/21 11:51
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/10/21 11:51
10/10/21 11:51
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/10/21 11:51
10/10/21 11:51
591-78-6
lodomethane
ND
ug/L
5.00
1
10/10/21 11:51
10/10/21 11:51
74-88-4 C3
2-Butanone (MEK)
ND
ug/L
5.00
1
10/10/21 11:51
10/10/21 11:51
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/10/21 11:51
10/10/21 11:51
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/10/21 11:51
10/10/21 11:51
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/10/21 11:51
10/10/21 11:51
91-20-3
Styrene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
127-18-4
Toluene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/10/21 11:51
10/10/21 11:51
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/10/21 11:51
10/10/21 11:51
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/10/21 11:51
10/10/21 11:51
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/10/21 11:51
10/10/21 11:51
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/10/21 11:51
10/10/21 11:51
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/10/21 11:51
10/10/21 11:51
179601-23-1
Surrogates
Toluene-d8 (S)
105
%
80.0-120
1
10/10/21 11:51
10/10/21 11:51
2037-26-5
Toluene-d8 (S)
103
%
80.0-120
1
10/14/21 22:27
10/14/21 22:27
2037-26-5
4-Bromofluorobenzene (S)
94.7
%
77.0-126
1
10/10/21 11:51
10/10/21 11:51
460-00-4
4-Bromofluorobenzene (S)
93.3
%
77.0-126
1
10/14/21 22:27
10/14/21 22:27
460-00-4
1,2-Dichloroethane-d4 (S)
109
%
70.0-130
1
10/10/21 11:51
10/10/21 11:51
17060-07-0
1,2-Dichloroethane-d4 (S)
110
%
70.0-130
1
10/14/21 22:27
10/14/21 22:27
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method: EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
ND ug/L 3.00 1 10/13/2104:15 10/13/2104:15 123-91-1
100 % 77.0-127 1 10/13/21 04:15 10/13/2104:15 2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
Sample: 6002-HRSW4 Lab ID: 92564056003 Collected: 09/29/21 10:45 Received: 09/29/21 13:19 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:29
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:29
7440-38-2
Barium
38.4
ug/L
5.0
1
09/30/2114:12
10/12/2122:29
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/30/2114:12
10/12/2122:29
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/30/2114:12
10/12/2122:29
7440-43-9
Chromium
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:29
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:29
7440-48-4
Copper
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:29
7440-50-8
Lead
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:29
7439-92-1
Nickel
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:29
7440-02-0
Selenium
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:29
7782-49-2
Silver
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:29
7440-22-4
Thallium
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:29
7440-28-0
Vanadium
ND
ug/L
5.0
1
09/30/2114:12
10/12/2122:29
7440-62-2
Zinc
ND
ug/L
10.0
1
09/30/2114:12
10/12/2122:29
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation
Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
10/01/2109:20
10/01/2117:15
7440-28-0
VOA (GC/MS) 8260D
Analytical Method:
EPA 8260D Preparation
Method: 8260D
Pace National - Mt. Juliet
Acetone
ND
ug/L
25.0
1
10/10/21 12:12
10/10/21 12:12
67-64-1
Acrylonitrile
ND
ug/L
5.00
1
10/10/21 12:12
10/10/21 12:12
107-13-1
Benzene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
71-43-2
Bromodichloromethane
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
75-27-4
Bromochloromethane
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
74-97-5
Bromoform
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
75-25-2
Bromomethane
ND
ug/L
2.50
1
10/10/21 12:12
10/10/21 12:12
74-83-9 C3
Carbon disulfide
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
75-15-0
Carbon tetrachloride
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
56-23-5
Chlorobenzene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
108-90-7
Dibromochloromethane
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
124-48-1
Chloroethane
ND
ug/L
2.50
1
10/10/21 12:12
10/10/21 12:12
75-00-3
Chloroform
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
67-66-3
Chloromethane
ND
ug/L
1.25
1
10/10/21 12:12
10/10/21 12:12
74-87-3 C3
Chloroprene
ND
ug/L
50.0
1
10/14/2122:48
10/14/2122:48
126-99-8 H1
1,2-Dibromo-3-chloropropane
ND
ug/L
2.50
1
10/10/21 12:12
10/10/21 12:12
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
106-93-4
Dibromomethane
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
106-46-7
1,1-Dichloroethane
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
75-34-3
1,2-Dichloroethane
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
Sample: 6002-HRSW4
Lab ID: 92564056003
Collected: 09/29/21
10:45
Received: 09/29/21 13:19 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D
Preparation Method: 8260D
Pace National - Mt. Juliet
1,1-Dichloroethene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
156-60-5
1,2-Dichloropropane
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
78-87-5
1,1-Dichloropropene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
563-58-6
1,3-Dichloropropane
ND
ug/L
1.00
1
10/10/21 12:12
10/10/21 12:12
142-28-9
cis-1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
10061-02-6
trans-1,4-Dichloro-2-butene
ND
ug/L
5.00
1
10/10/21 12:12
10/10/21 12:12
110-57-6
Ethylbenzene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
100-41-4
2-Hexanone
ND
ug/L
5.00
1
10/10/21 12:12
10/10/21 12:12
591-78-6
lodomethane
ND
ug/L
5.00
1
10/10/21 12:12
10/10/21 12:12
74-88-4 C3
2-Butanone (MEK)
ND
ug/L
5.00
1
10/10/21 12:12
10/10/21 12:12
78-93-3
Methylene Chloride
ND
ug/L
2.50
1
10/10/21 12:12
10/10/21 12:12
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.00
1
10/10/21 12:12
10/10/21 12:12
108-10-1
Naphthalene
ND
ug/L
2.50
1
10/10/21 12:12
10/10/21 12:12
91-20-3
Styrene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
79-34-5
Tetrachloroethene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
127-18-4
Toluene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
108-88-3
1,1,1-Trichloroethane
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
79-00-5
Trichloroethene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
79-01-6
Trichlorofluoromethane
ND
ug/L
2.50
1
10/10/21 12:12
10/10/21 12:12
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.50
1
10/10/21 12:12
10/10/21 12:12
96-18-4
Vinyl acetate
ND
ug/L
5.00
1
10/10/21 12:12
10/10/21 12:12
108-05-4
Vinyl chloride
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
75-01-4
Xylene (Total)
ND
ug/L
1.50
1
10/10/21 12:12
10/10/21 12:12
1330-20-7
o-Xylene
ND
ug/L
0.500
1
10/10/21 12:12
10/10/21 12:12
95-47-6
m&p-Xylene
ND
ug/L
1.00
1
10/10/21 12:12
10/10/21 12:12
179601-23-1
Surrogates
Toluene-d8 (S)
107
%
80.0-120
1
10/10/21 12:12
10/10/21 12:12
2037-26-5
Toluene-d8 (S)
103
%
80.0-120
1
10/14/21 22:48
10/14/21 22:48
2037-26-5
4-Bromofluorobenzene (S)
94.8
%
77.0-126
1
10/10/21 12:12
10/10/21 12:12
460-00-4
4-Bromofluorobenzene (S)
90.4
%
77.0-126
1
10/14/21 22:48
10/14/21 22:48
460-00-4
1,2-Dichloroethane-d4 (S)
107
%
70.0-130
1
10/10/21 12:12
10/10/21 12:12
17060-07-0
1,2-Dichloroethane-d4 (S)
109
%
70.0-130
1
10/14/21 22:48
10/14/21 22:48
17060-07-0
VOA (GC/MS) 8260D-SIM
Analytical Method: EPA 8260D
by SIM Preparation Method: 8260D-SIM
Pace National - Mt. Juliet
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
ND ug/L 3.00 1 10/13/2104:35 10/13/2104:35 123-91-1
99.7 % 77.0-127 1 10/13/21 04:35 10/13/2104:35 2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
QC Batch: 650175 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564056001, 92564056002, 92564056003
METHOD BLANK: 3410019 Matrix: Water
Associated Lab Samples: 92564056001, 92564056002, 92564056003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
10/12/21 21:38
10.0
10/12/21 21:38
5.0
10/12/21 21:38
1.0
10/12/21 21:38
1.0
10/12/21 21:38
5.0
10/12/21 21:38
5.0
10/12/21 21:38
5.0
10/12/21 21:38
5.0
10/12/21 21:38
5.0
10/12/21 21:38
10.0
10/12/21 21:38
5.0
10/12/21 21:38
10.0
10/12/21 21:38
5.0
10/12/21 21:38
10.0
10/12/21 21:38
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3410020
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
485
97
80-120
Arsenic
ug/L
500
476
95
80-120
Barium
ug/L
500
505
101
80-120
Beryllium
ug/L
500
489
98
80-120
Cadmium
ug/L
500
482
96
80-120
Chromium
ug/L
500
491
98
80-120
Cobalt
ug/L
500
469
94
80-120
Copper
ug/L
500
512
102
80-120
Lead
ug/L
500
483
97
80-120
Nickel
ug/L
500
484
97
80-120
Selenium
ug/L
500
461
92
80-120
Silver
ug/L
250
243
97
80-120
Thallium
ug/L
500
481
96
80-120
Vanadium
ug/L
500
492
98
80-120
Zinc
ug/L
500
480
96
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
60-02 HOLBROOKS RD LANDFILL
92564056
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3410021
3410022
MS
MSD
92564053001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
490
496
98
99
75-125
1
Arsenic
ug/L
ND
500
500
500
494
99
98
75-125
1
Barium
ug/L
260
500
500
769
757
102
100
75-125
2
Beryllium
ug/L
ND
500
500
496
496
99
99
75-125
0
Cadmium
ug/L
ND
500
500
501
498
100
100
75-125
0
Chromium
ug/L
5.7
500
500
506
501
100
99
75-125
1
Cobalt
ug/L
39.1
500
500
518
515
96
95
75-125
0
Copper
ug/L
10.3
500
500
534
525
105
103
75-125
2
Lead
ug/L
ND
500
500
500
496
99
98
75-125
1
Nickel
ug/L
8.0
500
500
499
497
98
98
75-125
0
Selenium
ug/L
ND
500
500
512
515
102
103
75-125
1
Silver
ug/L
ND
250
250
255
253
101
100
75-125
1
Thallium
ug/L
ND
500
500
489
491
97
98
75-125
0
Vanadium
ug/L
49.2
500
500
553
545
101
99
75-125
1
Zinc
ug/L
21.8
500
500
513
508
98
97
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
QC Batch: 650167 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564056001, 92564056002
METHOD BLANK: 3409966
Matrix:
Water
Associated Lab Samples: 92564056001, 92564056002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.47
10/01/2100:13
LABORATORY CONTROL SAMPLE:
3409967
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
24.8
99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3409968 3409969
MS MSD
92564021001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 24.5 24.6 98 98 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
QC Batch: 650333 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92564056003
METHOD BLANK: 3410888
Associated Lab Samples: 92564056003
Parameter Units
Thallium ug/L
LABORATORY CONTROL SAMPLE: 3410889
Parameter Units
Thallium ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.47 10/01 /21 16:46
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
25 24.0 96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3410890 3410891
MS MSD
92563951001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 23.4 23.6 93 94 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
QC Batch: 1754158 Analysis Method: EPA 8260D
QC Batch Method: 8260B Analysis Description: VOA (GC/MS) 8260D
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92564056001, 92564056002, 92564056003
METHOD BLANK: R3716623-2 Matrix:
Associated Lab Samples: 92564056001, 92564056002, 92564056003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.500
10/10/21 05:51
1,1,1-Trichloroethane
ug/L
ND
0.500
10/10/21 05:51
1,1,2,2-Tetrachloroethane
ug/L
ND
0.500
10/10/21 05:51
1,1,2-Trichloroethane
ug/L
ND
0.500
10/10/21 05:51
1,1-Dichloroethane
ug/L
ND
0.500
10/10/21 05:51
1,1-Dichloroethene
ug/L
ND
0.500
10/10/21 05:51
1,1-Dichloropropene
ug/L
ND
0.500
10/10/21 05:51
1,2,3-Trichloropropane
ug/L
ND
2.50
10/10/21 05:51
1,2-Dibromo-3-chloropropane
ug/L
ND
2.50
10/10/21 05:51
1,2-Dibromoethane (EDB)
ug/L
ND
0.500
10/10/21 05:51
1,2-Dichlorobenzene
ug/L
ND
0.500
10/10/21 05:51
1,2-Dichloroethane
ug/L
ND
0.500
10/10/21 05:51
1,2-Dichloropropane
ug/L
ND
0.500
10/10/21 05:51
1,3-Dichlorobenzene
ug/L
ND
0.500
10/10/21 05:51
1,3-Dichloropropane
ug/L
ND
1.00
10/10/21 05:51
1,4-Dichlorobenzene
ug/L
ND
0.500
10/10/21 05:51
2-Butanone (MEK)
ug/L
ND
5.00
10/10/21 05:51
2-Hexanone
ug/L
ND
5.00
10/10/21 05:51
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.00
10/10/21 05:51
Acetone
ug/L
ND
25.0
10/10/21 05:51
Acrylonitrile
ug/L
ND
5.00
10/10/21 05:51
Benzene
ug/L
ND
0.500
10/10/21 05:51
Bromochloromethane
ug/L
ND
0.500
10/10/21 05:51
Bromodichloromethane
ug/L
ND
0.500
10/10/21 05:51
Bromoform
ug/L
ND
0.500
10/10/21 05:51
Bromomethane
ug/L
ND
2.50
10/10/21 05:51
Carbon disulfide
ug/L
ND
0.500
10/10/21 05:51
Carbon tetrachloride
ug/L
ND
0.500
10/10/21 05:51
Chlorobenzene
ug/L
ND
0.500
10/10/21 05:51
Dibromochloromethane
ug/L
ND
0.500
10/10/21 05:51
Chloroethane
ug/L
ND
2.50
10/10/21 05:51
Chloroform
ug/L
ND
0.500
10/10/21 05:51
Chloromethane
ug/L
ND
1.25
10/10/21 05:51
cis-1,2-Dichloroethene
ug/L
ND
0.500
10/10/21 05:51
cis-1,3-Dichloropropene
ug/L
ND
0.500
10/10/21 05:51
Dibromomethane
ug/L
ND
0.500
10/10/21 05:51
Ethylbenzene
ug/L
ND
0.500
10/10/21 05:51
lodomethane
ug/L
ND
5.00
10/10/21 05:51
m&p-Xylene
ug/L
ND
1.00
10/10/21 05:51
Methylene Chloride
ug/L
ND
2.50
10/10/21 05:51
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
METHOD BLANK: R3716623-2 Matrix:
Associated Lab Samples: 92564056001, 92564056002, 92564056003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Naphthalene
ug/L
ND
2.50
10/10/21 05:51
o-Xylene
ug/L
ND
0.500
10/10/21 05:51
Styrene
ug/L
ND
0.500
10/10/21 05:51
Tetrachloroethene
ug/L
ND
0.500
10/10/21 05:51
Toluene
ug/L
ND
0.500
10/10/21 05:51
trans-1,2-Dichloroethene
ug/L
ND
0.500
10/10/21 05:51
trans- 1,3-Dichloropropene
ug/L
ND
0.500
10/10/21 05:51
trans-1,4-Dichloro-2-butene
ug/L
ND
5.00
10/10/21 05:51
Trichloroethene
ug/L
ND
0.500
10/10/21 05:51
Trichlorofluoromethane
ug/L
ND
2.50
10/10/21 05:51
Vinyl acetate
ug/L
ND
5.00
10/10/21 05:51
Vinyl chloride
ug/L
ND
0.500
10/10/21 05:51
Xylene (Total)
ug/L
ND
1.50
10/10/21 05:51
1,2-Dichloroethane-d4 (S)
%
106
70.0-130
10/10/21 05:51
Toluene-d8 (S)
%
106
80.0-120
10/10/21 05:51
4-Bromofluorobenzene (S)
%
95.9
77.0-126
10/10/21 05:51
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
R3716623-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
5.00
4.70
94.0
75.0-125
1,1,1-Trichloroethane
ug/L
5.00
4.99
99.8
73.0-124
1,1,2,2-Tetrachloroethane
ug/L
5.00
5.52
110
65.0-130
1,1,2-Trichloroethane
ug/L
5.00
4.78
95.6
80.0-120
1,1-Dichloroethane
ug/L
5.00
4.85
97.0
70.0-126
1,1-Dichloroethene
ug/L
5.00
4.85
97.0
71.0-124
1,1-Dichloropropene
ug/L
5.00
4.57
91.4
74.0-126
1,2,3-Trichloropropane
ug/L
5.00
5.10
102
73.0-130
1,2-Dibromo-3-chloropropane
ug/L
5.00
4.39
87.8
58.0-134
1,2-Dibromoethane (EDB)
ug/L
5.00
4.97
99.4
80.0-122
1,2-Dichlorobenzene
ug/L
5.00
4.99
99.8
79.0-121
1,2-Dichloroethane
ug/L
5.00
5.06
101
70.0-128
1,2-Dichloropropane
ug/L
5.00
4.96
99.2
77.0-125
1,3-Dichlorobenzene
ug/L
5.00
4.77
95.4
79.0-120
1,3-Dichloropropane
ug/L
5.00
5.04
101
80.0-120
1,4-Dichlorobenzene
ug/L
5.00
4.94
98.8
79.0-120
2-Butanone (MEK)
ug/L
25.0
23.4
93.6
44.0-160
2-Hexanone
ug/L
25.0
23.9
95.6
67.0-149
4-Methyl-2-pentanone (MIBK)
ug/L
25.0
25.4
102
68.0-142
Acetone
ug/L
25.0
22.4
89.6
19.0-160
Acrylonitrile
ug/L
25.0
25.4
102
55.0-149
Benzene
ug/L
5.00
4.79
95.8
70.0-123
Bromochloromethane
ug/L
5.00
5.20
104
76.0-122
Bromodichloromethane
ug/L
5.00
5.11
102
75.0-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
LABORATORY CONTROL SAMPLE:
Parameter
R3716623-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Bromoform
ug/L
5.00
4.76
95.2
68.0-132
Bromomethane
ug/L
5.00
1.23
24.6
10.0-160
Carbon disulfide
ug/L
5.00
4.72
94.4
61.0-128
Carbon tetrachloride
ug/L
5.00
4.52
90.4
68.0-126
Chlorobenzene
ug/L
5.00
4.59
91.8
80.0-121
Dibromochloromethane
ug/L
5.00
5.02
100
77.0-125
Chloroethane
ug/L
5.00
4.43
88.6
47.0-150
Chloroform
ug/L
5.00
4.83
96.6
73.0-120
Chloromethane
ug/L
5.00
3.20
64.0
41.0-142
cis-1,2-Dichloroethene
ug/L
5.00
4.63
92.6
73.0-120
cis-1,3-Dichloropropene
ug/L
5.00
4.78
95.6
80.0-123
Dibromomethane
ug/L
5.00
4.70
94.0
80.0-120
Ethylbenzene
ug/L
5.00
4.87
97.4
79.0-123
lodomethane
ug/L
25.0
10.1
40.4
33.0-147
m&p-Xylene
ug/L
10.0
9.35
93.5
80.0-122
Methylene Chloride
ug/L
5.00
5.17
103
67.0-120
Naphthalene
ug/L
5.00
4.27
85.4
54.0-135
o-Xylene
ug/L
5.00
4.35
87.0
80.0-122
Styrene
ug/L
5.00
4.56
91.2
73.0-130
Tetrachloroethene
ug/L
5.00
4.73
94.6
72.0-132
Toluene
ug/L
5.00
4.74
94.8
79.0-120
trans-1,2-Dichloroethene
ug/L
5.00
4.58
91.6
73.0-120
trans- 1,3-Dichloropropene
ug/L
5.00
4.80
96.0
78.0-124
trans-1,4-Dichloro-2-butene
ug/L
5.00
3.77
75.4
33.0-144
Trichloroethene
ug/L
5.00
4.79
95.8
78.0-124
Trichlorofluoromethane
ug/L
5.00
4.97
99.4
59.0-147
Vinyl acetate
ug/L
25.0
29.4
118
11.0-160
Vinyl chloride
ug/L
5.00
4.22
84.4
67.0-131
Xylene (Total)
ug/L
15.0
13.7
91.3
79.0-123
1,2-Dichloroethane-d4 (S)
%
108
70.0-130
Toluene-d8 (S)
%
103
80.0-120
4-Bromofluorobenzene (S)
%
99.1
77.0-126
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
QC Batch: 1757506 Analysis Method: EPA 8260D
QC Batch Method: 8260B Analysis Description: VOA (GC/MS) 8260D
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92564056001, 92564056002, 92564056003
METHOD BLANK: R3716959-3
Matrix:
Water
Associated Lab Samples:
92564056001, 92564056002, 92564056003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chloroprene
ug/L
ND
50.0
10/14/21 20:23
1,2-Dichloroethane-d4 (S)
%
111
70.0-130
10/14/21 20:23
Toluene-d8 (S)
%
102
80.0-120
10/14/21 20:23
4-Bromofluorobenzene (S)
%
91.9
77.0-126
10/14/21 20:23
LABORATORY CONTROL SAMPLE:
R3716959-2
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Chloroprene
ug/L
50.0 44.8 89.6
60.0-143
1,2-Dichloroethane-d4 (S)
%
109
70.0-130
Toluene-d8 (S)
%
99.2
80.0-120
4-Bromofluorobenzene (S)
%
93.3
77.0-126
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
QC Batch: 1751497 Analysis Method: EPA 8260D by SIM
QC Batch Method: 8260B-SIM Analysis Description: VOA (GC/MS) 8260D-SIM
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92564056001, 92564056002, 92564056003
METHOD BLANK: R3715966-3 Matrix: Water
Associated Lab Samples: 92564056001, 92564056002, 92564056003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,4-Dioxane (p-Dioxane) ug/L ND 3.00 10/12/21 23:18
Toluene-d8 (S) % 99.7 77.0-127 10/12/21 23:18
LABORATORY CONTROL SAMPLE & LCSD: R3715966-1
R3715966-2
Spike
LCS LCSD
LCS LCSD
% Rec Max
Parameter Units Conc.
Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 50.0
52.9 51.9
106 104
55.0-138 1.91 24
Toluene-d8 (S) %
99.9 100
77.0-127
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 23

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: 60-02 HOLBROOKS RD LANDFILL
Pace Project No.: 92564056
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
H1 Analysis conducted outside the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
60-02 HOLBROOKS RD LANDFILL
92564056
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92564056001
6002-HRSW2
EPA 3010A
650175
EPA 6010D
650225
92564056002
6002-HRSW3
EPA 3010A
650175
EPA 6010D
650225
92564056003
6002-HRSW4
EPA 3010A
650175
EPA 6010D
650225
92564056001
6002-HRSW2
EPA 3010A
650167
EPA 6020B
650222
92564056002
6002-HRSW3
EPA 3010A
650167
EPA 6020B
650222
92564056003
6002-HRSW4
EPA 3010A
650333
EPA 6020B
650402
92564056001
6002-HRSW2
8260D
1754158
EPA 8260D
1754158
92564056001
6002-HRSW2
8260D
1757506
EPA 8260D
1757506
92564056002
6002-HRSW3
8260D
1754158
EPA 8260D
1754158
92564056002
6002-HRSW3
8260D
1757506
EPA 8260D
1757506
92564056003
6002-HRSW4
8260D
1754158
EPA 8260D
1754158
92564056003
6002-HRSW4
8260D
1757506
EPA 8260D
1757506
92564056001
6002-HRSW2
8260D-SIM
1751497
EPA 8260D by SIM
1751497
92564056002
6002-HRSW3
8260D-SIM
1751497
EPA 8260D by SIM
1751497
92564056003
6002-HRSW4
8260D-SIM
1751497
EPA 8260D by SIM
1751497
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2021 04:49 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 23

Document Name: Document Revised: October 28, 2o2o
Sample Condition Upon Receipt(SCUR) Page 1 of 2
i�r7aiyflC81 Document No.: Issuing Authority:
F-CAR-CS.033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
'
Asheville ❑ Eden[:) Greenwood ❑
Huntersville ❑
Raleigh[]
Mechanicsville[] Atlanta❑ Kernersville❑
Client Name:
Sample Condition 1 i Receipt
..
Project
# Wp# : 92564Q56
�---
}
Caur[er, ❑Fed Ex ❑UPS
❑LISPS
❑Client
f
❑ Commercial ©Pace
[]Other:
II II�
!II
II
Jell
I �AI
I I
I I
I I
j
Custody Seal Present? []Yes ❑No Seats Intact?
[]Yes
,-
ONO
92564OSS
Date/Initials Person Examining Contents: f f 3 i"rZ�
Packing Material: ❑Bubble Wrap Dubble
Bags []None
❑ Cther
Biological Tissue Frozen?
Thermometer:
E}Noel
❑Blue
❑Yes [:]No ON/A
[]None
Ype or ice:
Correction Factor:
Cooler Temp: —4. Add/Subtract (°C)
;j
Temp should be above freezing to VC
Cooler Temp Corrected (°C):
❑5, les Out of temp Criteria. Samples on ice, cooling process
/
USDA Regulated Soil ( !P-N/A, water sample)
has begun
Did samples originate in a quarantine zone within the United States: CA, NY, or SC {check maps}7
Yes ❑No
Did samples orlginate from a foreiu source pnte(nationally,
including4awaii and?uerto RicOl? ❑Yes ❑No
Chain of Custody Present?
Ds
❑NO
❑N/A
1.
Samples Arrived within Hold Time?
©Fes
❑No
❑N/A
2.
Short Hold Time Analysis 1<72 hr.)?
❑Yes
[DNo
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
[2 ,
❑N/A
4.
Sufficient Volume?
&�s
LINO
2N/A
S.
COrTert Containers Used?
[}Yes
❑Na
❑N/A
6.
-Pace Containers Used?
QYes
[-]No
❑N/A
Containers intact?
Q'yeS
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
Dyes
ONO'
❑N/A
S.
Sample Labels Match COC7
Dyes
[]NO
[—]N/A
9.
-includes I7ate/Time/ID/Analysis Matrix: t'
�—
Headspace in VOA Vials (>5-6l
❑yes
L9NO_
❑N/A
10.
Trip Blank Present?
Oyes
Otto
El NIA
11,
Trip Blank Custody Seals PTeSenC?
❑Yes
❑No
QN/A
COMMENTS/SAMPLE DISCREPANCY
Field Data Requlred? Des ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person-cflntacted: DatetTme:
Project Manager SCURF Review: date:
Project Manager SRF Review: Date.
Page 21 of 23

Document Name:
le Condition upon Recel
Document No.:
F-CAR-CS-033-Rev.07
*Check mark top half of box if pH and/or dechiorination is
verified and within the acceptance range for preservation
samples.
Exceptians: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Oacument Revised: October 28, 2020
Page _2of 2
Issuing Authority:
Pace Carolinas Quality Office
Project WO# ; 92564Q56
PM: MWB Due Date: 10/13/21
CLIENT: 52-MECK CO
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pH Adjustment Log for Preserved Samples
Sample V
Type of Preservative
i
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
amount of Preservative Lot q
added i
I
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Note:�Nheneverthere-is-a-discreganey-3f�ectin; yarth-C-ar.�}ina-c-Qmaiiance-;amplesa ;apyaF-shis-form-willFda;enFta�ite-�voFEhfaroiina-EJfiidNR.��ifSratiocr-0flice {I.a,
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Samples
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(YIN)
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SAMPLE TEMP AT COLLECTION
# OF CONTAINERS
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H2SO4
HNO3
HCI
y
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Na2S203
c"
m
N
Melhanal
Other
Analyses Test
YIN
601016420
VOC 8260
V0C 6260 SIM (1,4"1
Trip SLAW
Residual Chlorine (YIN)
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Page 23 of 23