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HomeMy WebLinkAbout4407_ROSCANS_20144 0 NCDENR eq North Carolina Department of Environment and Natural Resources Pat McCrory Governor April 9, 2014 CERTIFIED MAIL: RETURN RECEIPT REQUESTED #7012 1010 0002 1965 8250 Stephen King Haywood County Solid Waste Department 278 Recycle Drive Clyde, NC 28721 SUBJECT: Notice of Violation Compliance Inspection Report White Oak Landfill 44-07 Haywood County Dear Mr. Dillard, John E. Skvarla, III Secretary # 7012 1010 0002 1965 8267 Matt Dillard Santek Waste Services, Inc. 650 25t" St. NW Suite 100 Cleveland, TN 37311 On March 21, 2014, Andrea Keller, representing the State of North Carolina, Division of Waste Management Solid Waste Section, inspected the above referenced facility for compliance with North Carolina solid waste statues and rules. Mr. John Preston was present on site, and Mr. Stephen King was present off site for a follow-up review, and represented White Oak Landfill during this inspection. The following violations were noted: A. 15A NCAC 13B .1604 (b)(L)(iii) Reporting Requirements: The permittee shall report orally within 24 hours from the time the permittee becomes aware of the circumstances of any release or discharge outside the liner, collection system or other containment component, any fire, or explosion from the permitted landfill facility. Such reports shall be made to the Division representative at the appropriate regional office of the Department of Environment and Natural Resources. B. 15A NCAC 136.1626 (8)(d) Leachate shall be contained within a lined disposal cell or leachate collection and storage system. All leachate shall be treated, as required by the receiving facility, prior to discharge. An NPDES permit may be required prior to the discharge of leachate to surface waters, as provided by 40 CFR Parts 258.26 and 258.27. 2090 US Highway 70, Swannanoa, North Carolina 28778 Phone: 828-296-45001 FAX: 828-299-70431 Internet: http://portal.ncdenr.org/web/wm/sw An Equal Opportunity 1 Affirmative Action Employer — Made in part by recycled paper (Domestic Marl On/y.;, No Insurance Coverage Provide For'deltvery information visit our webs)teat www u.§ps com® Er Postage r ru Postmark E-3 Return Receipt Fee Here O (Endorsement Required) 0 Restricted Delivery Fee 0 (Endorsement Required) ra O Total Postage & Fees r- ru Sent 7o Matt Dillard SLR%. K ru sir"eer,APCrvo:; Santek Waste Services, Inc. �- or PO Box No. 650 25th St. NW Suite 100 �4 -1)L?/j1 city Sfaie,ZiP+a Cleveland. 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Mr. Allen Gaither SOLID WASTE SECTION NCDENR ASHEVILLE REGIONAL OFFICE Division of Waste Management 2090 U.S. 70 Highway Swannanoa, NC 28778 RE: Responses to NCDENR's Comment Letter dated August 14, 2014 Revised Operations Plan Haywood County (White Oak) MSW Landfill Permit Number: 44-07-MSWLF-1993 Dear Mr. Gaither: Santek Waste Services, Inc. (Santek) has prepared the following responses to the North Carolina Department of Environment and Natural Resources (NCDENR) comments contained in the letter dated August 14, 2014. The responses and revisions are intended to make corrections and clarify discrepancies within the current Haywood County (White Oak) MSW Landfill Operations Plan. Please find the NCDENR's comment followed by Santek's response below. NCDENR Comment 1 "The second paragraph on page 6 states the County also operates a 4.8-acre Land Clearing and Inert Debris Landfill (LCID). An LCID has been permitted for construction and operation, however, the unit has not been constructed and the pre- operational conditions in the Permit have not been met." Santek Response 1 The second paragraph on page 6 of the Operations Plan has been revised to clarify the current status of the permitted Land Clearing and Inert Debris Landfill (LCID). NCDENR Comment 2 "The sixth paragraph on page 7 states See Section 2b for requirements of the Alternate Daily Cover tarp and soil/mulch material. However, Section 2 discusses waste filling practices while Section 3 discusses cover material requirements. Santek Response 2 The sixth paragraph on page 7 of the Operations Plan has been revised to reference Section 3 for alternate daily cover (ADC) requirements. NCDENR Comment 3 "The second paragraph on page 8 and Section 8, Erosion and Sedimentation Control Requirements, part c., state Provisions of a vegetative ground cover sufficient to restrain erosion will be accomplished within 15 calendar days upon completion of any phase of landfill development. This is not a Solid Waste requirement, however, since it is stated in the Operations Plan the Field Operations Branch inspector can hold the facility accountable for this requirement." Santek Response 3 The text, within 15 calendar days, has been removed from paragraph 2 on page 8 of the Operations Plan. NCDENR Comment 4 "Section 1, Waste Acceptance and Disposal Requirements, part b., states Typically the landfill is open Monday through Saturday from 7: 30a.m. to 3: 30p. m. However, the landfill may accept waste 24 hours a day, 7 days per week. As a Reminder, an individual certified in landfill operations must be on -site during all cooperating hours of the facility." Santek Response 4 A sentence has been added to Section 1, Waste Acceptance and Disposal Requirements, part b that states a certified landfill operator must be present during operations. NCDENR Comment 5 "Section 1, Waste Acceptance and Disposal Requirements, part c, provides a list of wastes prohibited from disposal at the MSWLF. The list does not include all banned wastes listed in G. S .13 0A-3 09.10(f). " Santek Response 5 Section 1, Waste Acceptance and Disposal Requirements, part c of the Operations Plan has been revised to include the banned wastes listed in G.S. 130A-309. 10(f). NCDENR Comment 6 "Section 1, Waste Acceptance and Disposal Requirements, part g., states Haywood County will continue a program at the Landfill for detecting and preventing the disposal of hazardous and liquid wastes. The detection program should include all prohibited wastes including those banned wastes listed in G.S. 130A-309.10(f)." Santek Response 6 The banned wastes listed in G.S.130A-309.10(f) have been added to Section 1, Waste Acceptance and Disposal Requirements, part g of the Operations Plan. NCDENR Comment 7 "Section 3, Cover Material Requirements, discusses the various types of daily cover used at the facility. Given the different requirements for the different types, the Section recommends the use of daily log to ensure all cover material requirements are being met." Santek Response 7 According to the site manager, a daily log is currently used to document cover matericals. NCDENR Comment 8 "Section 5, Explosive Gases Control, part b., states Haywood County will implement a routine methane monitoring program to ensure that the standards of 4 (a) are met. Section 4 discusses disease vector control." Santek Response 8 Section 5, Explosive Gases Control, part b has been revised to reference the standards of 5(a) instead of 4(a). NCDENR Comment 9 "Section 5, Explosive Gases Control, part c., states If methane gas levels exceeding the limits specified in 4 (a) are detected, the owner or operator will:. Section 4 discusses disease vector control." Santek Response 9 Section 5 (Explosive Gass Control), part c has been revised to reference the limits specified in 5(a) instead of 4(a). NCDENR Comment 10 "Section 12, Spreading and Compacting Requirements, part b., states subsequent lifts can be placed up to final grades. However, Section 2, Waste Filling Practices, part b., states To compensate for anticipated settlement the initial placement of waste may exceed the fill grades for the top of waste by up to five feet (S) on the outer slopes and top offill surfaces. Santek Response 10 Section 12 has been revised to reference Section 2(b) for final grade procedures. NCDENR Comment 11 "Appendix 3, Explosive Gas Control Plan, references a Figure 1 and 2. However, "there are no figures presented in the plan. These Figures must be available for review by the Field Operations Branch inspector at any time." Santek Response 11 Figures 1 and 2 have been added to Appendix 3 (Explosive Gas Control Plan). NCDENR Comment 12 "Appendix 3, Explosive Gas Control Plan, states Observations will be recorded on the aforementioned "Landfill Gas Measurements Field Workrheet, White Oak MEW Landfill, Haywood County, North Carolina"form. There is no form provided in the plan. This form must be available for review by the Field Operations Branch inspector at any time." Santek Response 12 The Landfill Gas Monitoring Field Worksheet, White Oak MSW Landfill, Haywood County, North Carolina form has been added to Appendix 3 (Explosive Gas Control Plan). NCDENR Comment 13 "Appendix 3, Explosive Gas Control Plan, states If methane gas is detected above 25% of its lower explosive limit (25% LEL) in any structure, excluding gas control or gas recovery system components, the detection instrument will be recalibrated in accordance with the manufacturer's instructions and the structure resampled. The final paragraph then states If methane gas is detected beyond 25% of its lower explosive limit in any structure, check the calibration of the monitor and resample. The first statement indicates the unit will be recalibrated, the second statement indicates the calibrat-ion will be verified." Santek Response 13 Page 34 of Appendix 3 (Explosive Gas Control Plan) has been updated to clarify that the monitoring technician will verify the field calibration of the methane monitoring instrument in the event methane is detected above 25% of the lower explosive limit (LEL) at any landfill structure. The second and third paragraphs on page 35, Appendix 3 (Explosive Gas Control Plan), appear to be duplicate text regarding methane monitoring at landfill structures. The duplicate text has been removed. NCDENR Comment 14 "Appendix 4, Operations Plan Mulching and Grinding Treatment and Processing discusses the procedures for the stated activity. However, this stated activity is not mentioned anywhere else in the Operations Plan." Santek Response 14 The Introduction section of the Operations Plan, page 6, has been revised to mention that a Mulching and Grinding Treatment and Processing operation is on -site. NCDENR Comment 15 "Appendix 4, Operations Plan Mulching and Grinding Treatment and Processing, Section III, Operations Procedures, part A. Overview, states A description of the procedures used for creating the soil/mulch ADC are included in Section 2(h) of the White Oak MSWLandfill Operations Plan. However, Section 2 discusses waste filling practices while Section 3 discusses cover material requirements." Santek Response 15 Section III, part A of Appendix 4 (Operations Plan - Mulching and Grinding Treatment and Processing) has been revised to reference section 3 (b) instead of 2(b). NCDENR Comment 16 "Appendix 4, Operations Plan Mulching and Grinding Treatment and Processing, Section III, Operations Procedures, part C. Technical Operational Requirements, item 3), states Mulched materials will be removed from the 'site several times a week. However, there is a large stockpile of material on -site and no indication any material has been removed." Santek Response 16 Section III, part C(3) of Appendix 4 (Operations Plan — Mulching and Grinding Treatment and Processing) has been revised stating that mulched material will be removed from the Mulching and Grinding Treatment and Processing area as needed. In addition to the revisions based on the NCDENR comments above, the following two revisions were made to the Operations Plan: 1. Page 5, Introduction: The County Manager was changed to Mr. Ira Dove. 2. Page 36, Appendix 4 (Operations Plan— Mulching and Grinding Treatment and Processing), Introduction, B: Text has been added to allow the mulching and grinding operation to change to another on -site location pending approval from the NCDENR, Division of Waste Management. A redlined copy and an original copy of the revised Operations Plan are provided for your review. If you have any questions or require additional information, please feel free to call at (423) 303- 7101. Sincerely, Ron E. Vail, P.E. V.P. of Engineering Enclosures Will Martin Environmental Compliance Coordinator cc: Andrea Keller, Environmental Senior Specialist, NCDENR Ira Dove, Interim Manager, Haywood County Stephen King, Solid Waste Director, Haywood, County (with enclosure) Cheryl Dunson, Executive V.P. of Marketing, Santek Robert D. Burnette, P.E., Executive V.P. of Engineering, Santek Matt Dillard, Executive V.P. of Operations, Santek John Preston, Landfill Manager, Santek (with enclosure) SANTEK Ir L A& V WasteServices 650 25th Street, N.W., Suite 100 Cleveland, Tennessee 37311 (423) 303.7101 Email: mail@santekenviro.com Internet: www.santekenviro.com May 9, 2014 Ms. Andrea Keller Environmental Senior Specialist NC Department of Environment and Natural Resources Division of Waste Management — Solid Waste Section 2090 US Hwy 70 Swannanoa, NC 28778 Re: Response to Notice of Violation dated April 9, 2014 Haywood County (White Oak) Landfill Permit No. 44-07 Deaf Vs. Keller: Santek Waste Services, Inc. (Santek) is submitting this letter and the enclosed documents in response to the Notice of Violation (NOV) letter dated April 9, 2014 from the North Carolina Department of Environment and Natural Resources (NCDENR), Division of Solid Waste Management — Solid Waste Section. The April 9, 2014 NOV letter was issued to the Haywood County Solid Waste Department and Santek following a compliance inspection conducted at the Haywood County (White Oak) Landfill on March 21, 2014. Please find the NCDENR compliance requests and Santek responses below. NCDENR Compliance Request 1 "To come in compliance with 1 SA NCAC 13B .1604(b)(L)(iii), the permit holder must, within 30 days, submit an update to the operations plan for the facility. The updated operations plan must include, at a minimum, an update to Section 13 — Leachate Management Plan to include leachate response%ontingency plans and notification requirements. " Santek Response As requested, Section 13 (Leachate Management Plan) of the facility's Operations Plan has been updated to include Leachate response/contingency plans and notification requirements in the event of a Leachate release outside the lined disposal area or leachate collection and storage system. The updated Section 13 (Leachate Management Plan) has been sent to Mr. Allen Gaither (NCDENR, Division of Waste Management - Solid Waste Section) for approval. A redline copy of revised page 19 of the Leachate Management Plan is located in Appendix A.�:�9� ate: RECEIVE® R MAY 12 2014 SOLID WASTE SECTION ASHEVILLE REGIONAL OFFICE NCDENR Compliance Request 2 "To come in compliance with 1 SA NCAC 13B .1626(8)(d), the permit holders must investigate and determine the extent of the leachate release, as instructed by the Section compliance hydrogeologist. Further action may be required by the Division. " Santek Response On April 14, 2014, Santek representatives (Mr. Ron Vail and Mr. Will Martin) contacted Mr. Ervin Lane (NCDENR, Compliance Hydrogeologist) to discuss the April 9, 2014 NOV letter and to request instructions for compliance with the NOV. Mr. Lane instructed Santek to submit a leachate outbreak summary including the corrective actions taken by the site and a location map showing where the leachate outbreak occurred. Mr. Lane also requested soil samples be collected in the area where the leachate outbreak occurred and analyzed for Appendix 1 Metals & Volatile Organic Compounds (VOC's), Chemical Oxygen Demand (COD), Phosphorus and Sulfate. A chronological summary of the March 12, 2014 leachate outbreak and corrective actions is provided below: 1:00 p.m. - Santek personnel and Mr. Stephen King (Haywood County Solid Waste & Recycling Director) performed a landfill inspection and observed a small amount of leachate (approximately 5 gallons) pooled behind a check dam in the perimeter ditch on the northeast portion of Phase 1. 1:30 p.m. - Santek personnel notified Mr. John Preston (Landfill Manger) of the leachate outbreak. Mr. Preston gave specific instructions to clean up the leachate and repair the affected area. Santek personnel used a track hoe to remove the small amount of leachate, affected soil and check dam from the perimeter ditch. All affected materials were transported to the landfill working face for proper disposal. Clean, uncontaminated, soil was installed in the area affected by the leachate outbreak. A new check dam was also installed in the perimeter ditch. 3:30 p.m. - All corrective actions were completed. According to Mr. Preston, the area affected by the leachate outbreak was less than 10 ft. wide by 20 ft. long. All contaminated soil in this area was removed and replaced with clean, uncontaminated, soil. There was no indication that any leachate traveled beyond the Phase 1 perimeter ditch check dam. A map showing the location of the March 12, 2014 leachate outbreak is provided in Appendix B. As requested, Santek collected soil samples on April 21, 2014 from the area where the leachate outbreak occurred. The map in Appendix B shows the approximate location of the soil sample collection points (S-1, S-2 and BA). S-1 and S-2 were sample points located in the leachate outbreak area, and sample point BA was collected as a background sample in an area unaffected by leachate. Soil samples were analyzed by Analytical Environmental Services, Inc. (AES) for the constituents requested above. Each constituent detected in the soil sample locations was also detected in the background sample at similar levels. Furthermore, the volatile organic compounds detected in the landfill's leachate were not present in S-1 or S-2. Therefore, Santek believes the areas of S-land S-2 are determined to be uncontaminated and representative of local soil constituents. Analytical results are provided in Appendix C. In order to prevent future leachate outbreaks from occurring in this area, Santek will inspect the leachate cleanout located in the northeast portion of Phase 1. This leachate cleanout was installed by Haywood County in order to promote proper leachate drainage. When leachate is present in the cleanout, Santek will remove the leachate and transport it to the on -site leachate storage lagoon. Implementing this operational procedure should reduce the possibility of another leachate outbreak in this area. If you have any questions or require additional information, please feel free to call at (423) 303- 7101. Sincerely, Will Martin Environmental Compliance Coordinator Enclosures Ron E. Vail, P.E. V.P. of Engineering cc: Ervin Lane, Compliance Hydrogeologist, NCDENR Ira Dove, Interim Manger, Haywood County Stephen King, Solid Waste & Recycling Director, Haywood County Robert D. Burnette, P.E., Executive V.P. of Engineering, Santek Matt Dillard, Executive V.P. of Operations, Santek Cheryl Dunson, Executive V.P. of Marketing, Santek John Preston, Landfill Manager, San RECEI"VED MAY 12 2014 SOLID WASTE SECTION ASHEVILLE REC-IONAL OFFICE will be temporarily stored within the MSWLF units until such a time the flow of leachate can continue to the lagoon. If any rain or other event requires storage of leachate or storm water in the cell, the Division of Waste Management will be notified verbally and immediately followed by written communication. During wet weather, the pump and hauling may have to be performed 24 hours a day for several days until the leachate lagoon levels have been reduced. In the early phases of waste fill operations in MSW Phase 3, the discharge from the stormwater removal pump can be diverted to the leachate gravity system, if necessary during extreme conditions. f. The recirculation of leachate within the landfill is a viable alternative to the present pump and haul leachate management operation and is considered a part of the overall Leachate Management Plan. Prior to actually beginning leachate recirculation, the County will prepare the appropriate leachate recirculation plan for submission to and approval by the North Carolina Department of Environment and Natural Resources (NCDENR), Division of Waste Management. g. Leachate Release Response/Contingency Plan: In the event of a leachate release outside the lined disposal area or leachate collection and storage system Haywood County or Santek will immediately utilize all available resources to contain and minimize the leachate release. Soil berms, ditches and landfill equipment may be used to contain the leachate and repair the affected area. h. Leachate Release Notification Requirements: In the event of a leachate release outside the lined disposal area or leachate collection and storage system Haywood County or Santek will notifX the NCDENR, Division of Waste Management within 24 hours of becoming aware of the leachate release. i. Haywood County installed a leachate cleanout in the northeast portion of Phase I to assist leachate flow through the leachate collection system. Haywood County or Santek will monitor this cleanout for the presence of leachate. If leachate is detected in the cleanout, Haywood County or Santek will pump out the leachate and transport it to the leachate storm lagoon. MAY 1 2 2014 SOLID WASTE SECTION Operations Plan ASHL:VILLE REGIONAL OFFICE White Oak Landfill Revised May 2014 Page 19 Soil Sample Results ANALYTICAL ENVIRONMENTAL SERVICES, INC. AES April 30, 2014 Will Martin Santek Environmental Inc. 650 25th Street NW Cleveland TN 37311 TEL: (423) 476-9160 FAX: (423) 479-1952 RE: Haywood Soil Samples Dear Will Martin: Order No: 1404M59 Analytical Environmental Services, Inc. received 3 samples on 4/23/2014 9:45:00 AM for the analyses presented in following report. No problems were encountered during the analyses. Additionally, all results for the associated Quality Control samples were within EPA and/or AES established limits. Any discrepancies associated with the analyses contained herein will be noted and submitted in the form of a project Case Narrative. AES' certifications are as follows: -NELAC/Florida Certification number E87582 for analysis of Environmental Water, soil/hazardous waste, and Drinking Water Microbiology, effective 07/01/13-06/30/14. -AIHA-LAP, LLC Laboratory ID: 100671 for Industrial Hygiene samples (Organics, Inorganics), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) effective until 09/01/15. These results relate only to the items tested. This report may only be reproduced in full. If you have any questions regarding these test results, please feel free to call. HIM Chantelle Kanhai Project Manager MAY 1 2 2014 SOLID WASTE SECTION ASHEVILLE REGIONAL OF ICE 080 Pre-iJ utial Drive - Atlattl , Georgia 30340 • .i`A 770,45781.7: • Fax: 70A-57.8188 * Toll Frei!: 00.972.4889 'fS'ps'?-v,at}{Ad TClta.x-ogT7 Page 1 of 9 siauieluoz)jo 1014 M /^1 r'd rvwi V V rgpx . -IN w h W Q N 1w � C _y n t �3 C. .�. ri � 4 O ,'.a .� -- I � 60 N Z N O i^ w a $0000ul n � 6 I'i.'- IF > 'C F � Q h a a � C� w a �p o a a a a ° w 7 F � U a> � v7 U V a .J002 F { 7 Fa+ q �0717 (sapoo aas) cx� a xine� < f � atisodwo0 Zp OU v o ° H W M x O p-'` AO o MAW Z w w Nz o OF �a O � M o- 20 W Page 2 of 9 a n Analytical Environmental Services, Inc Date: 30-Apr-14 Client: Santek Environmental Inc. Client Sample ID: S-1 Project Name: Haywood Soil Samples Collection Date: 4/21/2014 11:35:00 AM Lab ID: 1404M59-001 Matrix: Soil Analyses Result Reporting Limit Qual Units BatchID Dilution Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260B (SW5035) Chloromethane BRL 13 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Vinyl chloride BRL 13 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Bromomethane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Chloroethane BRL 13 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Trichlorofluoromethane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD 1,1-Dichloroethene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Acetone BRL 130 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Iodomethane BRL 13 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Carbon disulfide BRL 13 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Vinyl acetate BRL 13 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Methylene chloride BRL 25 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Acrylonitrile BRL 63 ug/Kg-dry 190198 1 04/26/2014 16:28 MD trans-1,2-Dichloroethene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD 1,1-Dichloroethane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD cis-1,2-Dichloroethene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD 2-Butanone BRL 63 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Bromochloromethane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Chloroform BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD 1, 1, 1 -Trichloroethane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Carbon tetrachloride BRL 6.3 ug/Kg-dxy 190198 1 04/26/2014 16:28 MD Benzene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD 1,2-Dichloroethane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Trichloroethene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD 1,2-Dichloropropane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Dibromomethane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Bromodichloromethane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD cis-1,3-Dichloropropene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD 4-Methyl-2-pentanone BRL 13 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Toluene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD trans-1,3-Dichloropropene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD 1,1,2-Trichloroethane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD 2-Hexanone BRL 13 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Tetrachloroethene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Dibromochloromethane BRL 6.3 ug(Kg-dry 190198 1 04/26/2014 16:28 MD 1,2-Dibromoethane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Chlorobenzene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD 1, 1, 1,2-Tetrachloroethane BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Ethylbenzene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD m,p-Xylene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD o-Xylene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Styrene BRL 6.3 ug/Kg-dry 190198 1 04/26/2014 16:28 MD Qualifiers: ' Value exceeds maximum contaminant level E Estimated (value above quantitation range) F"'g r 1 BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Narr See case narrative N Analyte not NELAC certified NC Not confirmed MAY 1 2 2014 B Analyte detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit ?dV ,%TE SECTION ASHEVILLE REGIONAL OFFICE Analytical Environmental Services, Inc Date: 30-Apr-14 Client: Santek Environmental Inc. Client Sample ID: S-1 Project Name: Haywood Soil Samples Collection Date: 4/21/2014 11:35:00 AM Lab ID: 1404M59-001 Matrix: Soil Reporting Dilution Analyses Result Qual Units BatchID Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260B Bromoform BRL 1,1,2,2-Tetrachloroethane BRL 1,2,3-Trichloropropane BRL trans-1,4-Dichloro-2-butene BRL 1,4-Dichlorobenzene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL Xylenes, Total BRL Surr: 4-Bromofluorobenzene 90.8 Surr: Dibromofluoromethane 102 Surr: Toluene-d8 102 Total Phosphorus, soils E365.1 Phosphorus, Total (As P) 604 ION SCAN SW9056A Sulfate 63 Chemical Oxygen Demand (COD) E410.4 Chemical Oxygen Demand 22.2 METALS, TOTAL SW6010C Antimony BRL Arsenic BRL Barium 377 Beryllium BRL Cadmium BRL Chromium 36.1 Cobalt 18.7 Copper 29.3 Lead 14.3 Nickel 17.8 Selenium BRL Silver BRL Thallium 8.07 Vanadium 67.8 Zinc 73.1 PERCENT MOISTURE D2216 Percent Moisture 28.6 (SW5035) 6.3 ug/Kg-dry 190198 1 04/26/201416:28 MD 6.3 ug/Kg-dry 190198 1 04/26/201416:28 MD 6.3 ug/Kg-dry 190198 1 04/26/201416:28 MD 13 ug/Kg-dry 190198 1 04/26/201416:28 MD 6.3 ug/Kg-dry 190198 1 04/26/201416:28 MD 6.3 ug/Kg-dry 190198 1 04/26/201416:28 MD 6.3 ug/Kg-dry 190198 1 04/26/201416:28 MD 6.3 ug/Kg-dry 190198 1 04/26/201416:28 MD 70-128 %REC 190198 1 04/26/201416:28 MD 78.2-128 %REC 190198 1 04/26/201416:28 MD 76.5-116 %REC 190198 1 04/26/201416:28 MD (E365.1) 13.7 mg/Kg-dry 190262 1 04/29/201414:35 LV (SW9056A) 14 mg/Kg-dry 190184 1 04/24/201419:00 GR 10.0 mg/Kg R266353 1 04/25/201412:00 MG (SW3050B) 6.96 mg/Kg-dry 190227 1 04/28/201418:20 JL 6.96 mg/Kg-dry 190227 1 04/28/201418:20 JL 6.96 mg/Kg-dry 190227 1 04/28/201418:20 JL 3.48 mg/Kg-dry 190227 1 04/28/201418:20 JL 3.48 mg/Kg-dry 190227 1 04/28/201418:20 JL 3.48 mg/Kg-dry 190227 1 04/28/201418:20 JL 3.48 mg(Kg-dry 190227 1 04/28/201418:20 JL 3.48 mg(Kg-dry 190227 1 04/28/201418:20 JL 6.96 mg/Kg-drY 190227 1 04/28/201418:20 JL 6.96 mg/K9-dry 190227 1 04/28/201418:20 JL 6.96 m9(Kg-dry 190227 1 04/28/201418:20 JL 3.48 mg/Kg-drY 190227 1 04/28/201418:20 JL 6.96 mgfKg-dry 190227 1 04/28/201418:20 JL 6.96 mg(Kg-dry 190227 1 04/28/201418:20 JL 6.96 mg(Kg-dry 190227 1 04/28/201418:20 JL 0 Wt% R266368 1 04/25/2014 09:30 SG �rr� Rass Qualifiers: ' Value exceeds maximum contaminant level E Estimated (value above quantization range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Nart See case narrative N Analyte not NELAC certified NC Not communed MAY 1 2 2014 B Analyte detected in the associated method blank a Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit SOLID WASTE SECTION ggyL%2ek9t&ZONAL OFFICE Analytical Environmental Services, Inc Date: 30-Apr-14 Client: Santek Environmental Inc. Client Sample ID: S-2 Project Name: Haywood Soil Samples Collection Date: 4/21/2014 11:35:00 AM Lab ID: 1404M59-002 Matrix: Soil Reporting Dilution Analyses Result Qual Units BatchID Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260B (SWM35) Chloromethane BRL 11 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Vinyl chloride BRL 11 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Bromomethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Chloroethane BRL 11 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Trichlorofluoromethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 1,1-Dichloroethene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Acetone BRL 110 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Iodomethane BRL 11 ug(Kg-dry 190198 1 04/26/2014 16:58 MD Carbon disulfide BRL 11 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Vinyl acetate BRL 11 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Methylene chloride BRL 22 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Acrylonitrile BRL 56 ug/Kg-dry 190198 1 04/26/2014 16:58 MD trans-1,2-Dichloroethene BRL 5.6 ug/Kg-dry 190198 1 04/261201416:58 MD 1,1-Dichloroethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD cis-1,2-Dichloroethene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 2-Butanone BRL 56 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Bromochloromethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Chloroform BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 1, 1, 1 -Trichloroethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Carbon tetrachloride BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Benzene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 1,2-Dichloroethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Trichloroethene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 1,2-Dichloropropane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Dibromomethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Bromodichloromethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD cis-1,3-Dichloropropene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 4-Methyl-2-pentanone BRL 11 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Toluene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD trans-1,3-Dichloropropene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 1,1,2-Trichloroethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 2-Hexanone BRL 11 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Tetrachloroethene BRL 5.6 ug(Kg-dry 190198 1 04/26/2014 16:58 MD Dibromochloromethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 1,2-Dibromoethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Chlorobenzene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 1, 1, 1,2-Tetrachloroethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Ethylbenzene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD m,p-Xylene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD o-Xylene BRL 5.6 ug(Kg-dry 190198 1 04/26/2014 16:58 MD Styrene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Qualifiers: * Value exceeds maximum contaminant level E Estimated (value above quantitation range)�r5' BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Narr See case narrative M AY 1 2 2014 N Analyte not NELAC certified NC Not confirmed B Analyte detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit SOLID WASTE SECTION ASHE\ilkgge IaDINAL OFFICE Analytical Environmental Services, Inc Date: 30-Apr-14 Client: Santek Environmental Inc. Client Sample ID: S-2 Project Name: Haywood Soil Samples Collection Date: 4/21/2014 11:35:00 AM Lab ID: 1404M59-002 Matrix: Soil Analyses Result Reporting Limit Qual Units BatchID Dilution Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW826013 (SW5035) Bromoform BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 1,1,2,2-Tetrachloroethane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 1,2,3-Trichloropropane BRL 5.6 uB/Kg-dry 190198 1 04/26/2014 16:58 MD trans-1,4-Dichloro-2-butene BRL 11 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 1,4-Dichlorobenzene BRL 5.6 ugfKg-dry 190198 1 04/26/2014 16:58 MD 1,2-Dichlorobenzene BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD 1,2-Dibromo-3-chloropropane BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Xylenes, Total BRL 5.6 ug/Kg-dry 190198 1 04/26/2014 16:58 MD Sum 4-Bromofluorobenzene 91.2 70-128 %REC 190198 1 04/26/2014 16:58 MD Surr: Dibromofluoromethane 104 78.2-128 %REC 190198 1 04/26/2014 16:58 MD Surr: Toluene-d8 101 76.5-116 %REC 190198 1 04/26/2014 16:58 MD Total Phosphorus, soils E365.1 (E365.1) Phosphorus, Total (As P) 4090 45.9 mg/Kg-dry 190262 4 04/29/2014 14:42 I,V ION SCAN SW9056A (SW9056A) Sulfate 27 11 rng/Kg-dry 190184 1 04/24/201419:15 GR Chemical Oxygen Demand (COD) E410.4 Chemical Oxygen Demand 200 10.0 mg/Kg R266353 1 04/25/2014 12:00 MG METALS, TOTAL SW6010C (SW3050B) Antimony BRL 5.33 mg/Kg-dry 190227 1 04/28/201418:24 JL Arsenic BRL 5.33 mg/Kg-dry 190227 1 04/28/201418:24 JL Barium 506 5.33 mg/Kg-dry 190227 1 04/28/201418:24 JL Beryllium BRL 2.67 mg/Kg-dry 190227 1 04/28/201418:24 JL Cadmium BRL 2.67 mg/Kg-dry 190227 1 04/28/201418:24 JL Chromium 39.3 2.67 -g/Kg-dry 190227 1 04/28/201418:24 JL Cobalt 26.7 2.67 mg/Kg-dry 190227 1 04/28/201418:24 JL Copper 16.5 2.67 mg/Kg-dry 190227 1 04/28/201418:24 JL Lead 8.00 5.33 mg/Kg-dry 190227 1 04/28/201418:24 JL Nickel 16.1 5.33 mg/Kg-dry 190227 1 04/28/201418:24 JL Selenium BRL 5.33 mg/Kg-dry 190227 1 04/28/201418:24 JL Silver BRL 2.67 mg/Kg-dry 190227 1 04/28/201418:24 JL Thallium 12.1 5.33 mg/Kg-dry 190227 1 04/28/201418:24 JL Vanadium 82.9 5.33 mg/Kg-dry 190227 1 04/28/201418:24 JL Zinc 96.8 5.33 mg/Kg-dry 190227 1 04/28/201418:24 JL PERCENT MOISTURE D2216 Percent Moisture 13.8 0 wt% R266368 1 04/25/2014 09:30 SG Qualifiers: ' Value exceeds maximum contaminant level E Estimated (value above quantitation range) 4e��a�F -z- BRL Below reporting limit S Spike Recovery outside limits due to matrix ■ E1. H Holding times for preparation or analysis exceeded Narr See case narrative N Analyte not NELAC certified NC Not confirmed MAY 1 2 2014 B Analyte detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit ZQW! 6f,16,71] SECTION ASKVILLE REGIONAL OFFICE Analytical Environmental Services, Inc Date: 30-Apr-14 Client: Santek Environmental Inc. Client Sample ID: BA Project Name: Haywood Soil Samples Collection Date: 4/21/2014 12:05:00 PM Lab ID: 1404M59-003 Matrix: Soil Analyses Result Reporting Limit Qual Units BatchID Dilution Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260B (SW5035) Chloromethane BRL 12 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Vinyl chloride BRL 12 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Bromomethane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Chloroethane BRL 12 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Trichlorofluoromethane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD 1,1-Dichloroethene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Acetone BRL 120 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Iodomethane BRL 12 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Carbon disulfide BRL 12 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Vinyl acetate BRL 12 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Methylene chloride BRL 25 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Acrylonitrile BRL 61 ug/Kg-dry 190198 1 04/26/2014 17:27 MD trans-1,2-Dichloroethene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD 1,1-Dichloroethane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD cis-1,2-Dichloroethene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD 2-Butanone BRL 61 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Bromochloromethane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Chloroform BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD 1, 1, 1 -Trichloroethane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Carbon tetrachloride BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Benzene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD 1,2-Dichloroethane BRL 6.1 ug/Kg-dry 190198 1 04126/201417:27 MD Trichloroethene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD 1,2-Dichloropropane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Dibromomethane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Bromodichloromethane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD cis-1,3-Dichloropropene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD 4-Methyl-2-pentanone BRL 12 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Toluene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD trans-1,3-Dichloropropene BRL 6.1 ug/Kg-dry 190198 1 04126/201417:27 MD 1,1,2-Trichloroethane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD 2-Hexanone BRL 12 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Tetrachloroethene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Dibromochloromethane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD 1,2-Dibromoethane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Chlorobenzene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD 1, 1, 1,2-Tetrachloroethane BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Ethylbenzene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD m,p-Xylene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD o-Xylene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Styrene BRL 6.1 ug/Kg-dry 190198 1 04/26/2014 17:27 MD Qualifiers: • Value exceeds maximum contaminant level E Estimated (value above quantitation range) $sue rn� V�'`� 5 D BRL Below reporting limit S Spike Recovery outside limits due to matrix r H Holding times for preparation or analysis exceeded Narr See case narrative N Analyte not NELAC certified NC Not confirmed M AY .1 2 2014 B Analyte detected in the associated method blank < Less than Result value > Greater than Result value ] Estimated value detected below Reporting Limit Shp Y f,' E SECTION ASNEVIL E R"-.GIONAL OFFICE Analytical Environmental Services, Inc Date: 30-Apr-14 Client: Santek Environmental Inc. Client Sample ID: BA Project Name: Haywood Soil Samples Collection Date: 4/21/2014 12:05:00 PM Lab ID: 1404M59-003 Matrix: Soil Reporting Dilution Analyses Result Qual Units BatchID Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260B Bromoform BRL 1,1,2,2-Tetrachloroethane BRL 1,2,3-Trichloropropane BRL trans-1,4-Dichloro-2-butene BRL 1,4-Dichlorobenzene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL Xylenes, Total BRL Surr: 4-Bromofluorobenzene 94 Surr: Dibromofluoromethane 102 Surr: Toluene-d8 101 Total Phosphorus, soils E365.1 Phosphorus, Total (As P) 405 ION SCAN SW9056A Sulfate 340 Chemical Oxygen Demand (COD) E410.4 Chemical Oxygen Demand 13.3 METALS, TOTAL SW6010C Antimony BRL Arsenic BRL Barium 289 Beryllium BRL Cadmium BRL Chromium 61.1 Cobalt 21.2 Copper 26.8 Lead 8.26 Nickel 36.9 Selenium BRL Silver BRL Thallium 8•20 Vanadium 73.9 Zinc 80.5 PERCENT MOISTURE D2216 Percent Moisture 17.9 Qualifiers: • Value exceeds maximum contaminant level BRL Below reporting limit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank > Greater than Result value 6.1 6.1 6.1 12 6.1 6.1 6.1 6.1 70-128 78.2-128 76.5-116 11.8 12 10.0 5.77 5.77 5.77 2.89 2.89 2.89 2.89 2.89 5.77 5.77 5.77 2.89 5.77 5.77 5.77 (SW5035) ug/Kg-dry 190198 ug/Kg-dry 190198 ug/Kg-dry 190198 ug/Kg-dry 190198 ug/Kg-dry 190198 ug/Kg-dry 190198 ug/Kg-dry 190198 ug/Kg-dry 190198 %REC 190198 %REC 190198 o/uREC 190198 (E365.1) mg/Kg-dry 190262 (SW9056A) mg/Kg-dry 190184 mg/Kg R266353 (SW3050B) mg/Kg-dry 190227 mg/Kg-dry 190227 mg/Kg-dry 190227 mg/Kg-dry 190227 mg/Kg-dry 190227 mg/Kg-dty 190227 mg/Kg-dry 190227 mg/Kg-dry 190227 mg/Kg-dry 190227 mg/Kg-dry 190227 mg/Kg-dry 190227 mg/Kg-dry 190227 mg/Kg-dry 190227 mg/Kg-dry 190227 mg/Kg-dry 190227 1 04/26/201417:27 MD 1 04/26/201417:27 MD 1 04/26/201417:27 MD 1 04/26/201417:27 MD 1 04/26/201417:27 MD 1 04/26/201417:27 MD 1 04/26/201417:27 MD 1 04/26/201417:27 MD 1 04/26/201417:27 MD 1 04/26/201417:27 MD 1 04/26/2014 17:27 MD 1 04/29/201414:51 LV 1 04/24/201419:30 GR 1 04/25/2014 12:00 MG 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 1 04/28/2014 18:28 JL JL JL JL JL JL JL JL JL JL JL JL JL JL JL 0 wt% R266368 1 04/25/2014 09:30 SG E Estimated (value above quantitation range) S Spike Recovery outside limits due to matrix Narr See case narrative NC Not confirmed MAY 1 2 2014 < Less than Result value J Estimated value detected below Reporting Limit SOCTION A%11=V1LL6 r-:C,1t.0'rAL OFFICE Analytical Environmental Services, Inc. Sample/Cooler Receipt Checklist Client,Yl-� 2 it . Work Order Number Checklist completed by Signature Date Carrier name: FedEx ✓UPS , Courier — Client ^ US Mail Other Shipping container/cooler in good condition? Yes Custody seals intact on shipping container/cooler? Yes Custody seals intact on sample bottles? Yes Container/Temp Blank temperature in compliance?' (4°C-h2)* Yes . Cooler #1' 3 '3 Cooler #2 CooIer #3 Cooler #4 Chain of custody present? Yes / Chain of custody signed when relinquished and received? Yes Chain of custody agrees with sample labels? Yes Samples in proper container/bottle? Yes Sample containers intact? Yes Sufficient sample volume for indicated test? Yes -- All samples received within holding time? Yes j Was TAT marked on the COC? Yes Proceed with Standard TAT as per project history? Yes Water - VOA vials have zero headspace? No VOA vials submitted i W No. Not Present No _ Not Present ,_✓ No Not Present No Cooler#5 Cooler #6 No No No No No No No No No Yes ater - pH acceptable upon receipt? Yes _ _ No Adjusted? Checked by Sample Condition: Good _ Other(Explain) (For diffusive samples or A1HA lead) Is a known blank included? Yes See Case Narrative for resolution of the Non -Conformance. No Not Applicable! No Not Applicable t MAY 1 2 2014 : * Samples do not have to comply with the given range for certain parameters. SOLID W,A,ST= SECTION MHEVILLE R€CIONAL OFFICE \L\Quality Assurance\Checklists Procedures Sign -Off Templates\Checklists\Sample Receipt Checklists\Sample Cooler Receipt_Checklist Page 9 of 9 Leachate Results 11�;aceAnalytical ..pacelabs.com r' I ANALYTICAL RESULTS Project: Leachate White Oak LF Pace Project No.: 92198748 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: Leachate Lab ID: 92198748001 Collected: 04/24/14 13:10 Received: 04/24/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua] 180.1 Turbidity Analytical Method: EPA 180.1 Turbidity 74.5 NTU 1.0 0.50 1 04/25/14 12:00 5210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 53.3 mg/L 2.0 2.0 1 04/25/14 16:07 04/30/14 10:20 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 4450 mg/L 500 500 250 05/01/14 16:31 14808-79-8 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 0.84 mg/L 0.020 0.020 1 04/24/14 22:31 Nitrogen, Nitrite 0.43 mg/L 0.020 0.020 1 04/24/14 22:31 Nitrogen, NO2 plus NO3 1.3 mg/L 0.020 0.020 1 04/24/14 22:31 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 1.7 mg/L 0.050 0.050 1 05/04/1414:21 7723-14-0 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E Cyanide ND mg/L 0.0050 0.0050 1 05/06/14 14:20 57-12-5 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 964 mg/L 25.0 25.0 1 05/05/14 15:53 Date: 05/06/2014 04:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. s RE M AY 1 2 2014 SOLID 1,vm'(E sEC"rjON ASHEVILLE REG:1LX',XL OFFICE Page 5 of 23 Pace Analytical Services, Inc. 2225 Riverside Dr. ;a'ceAna1y4ica1' Asheville, NC 28804 1!' www.pacelabs.com (828)254-7176 ANALYTICAL RESULTS MAY 1 2 2014 Project: Leachate White Oak LF Pace Project No.: 92198748 SOLID WASTE SECTION Sample: Leachate Lab ID: 92198748002 Collected: 04/24/1413:10 Rec�rve `." 042 `TWat,9 Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Monitoring Well Data Analytical Method Collected By MPS 1 04/25/14 11:38 Collected Date 04/24/14 1 04/25/14 11:38 Collected Time 13:10 1 04/25/14 11:38 Field pH 7.3 Std. Units 0.10 0.10 1 04/25/14 11:38 Field Temperature 16.9 deg C 0.50 0.50 1 04/25/14 11:38 Field Specific Conductance 9040 umhos/cm 1.0 1.0 1 04/25/14 11:38 Turbidity 36.3 NTU 1.0 1.0 1 04/25/14 11:38 60101CP Groundwater Analytical Method: EPA6010 Preparation Method: EPA3010 Antimony ND ug/L 5.0 5.0 1 05/02/14 11:00 05/05/14 17:21 7440-36-0 Arsenic 14.3 ug/L 10.0 5.0 1 05/02/14 11:00 05/05/14 17:21 7440-38-2 Barium 376 ug/L 5.0 5.0 1 05/02/14 11:00 05/05/14 17:21 7440-39-3 Beryllium 1.8 ug/L 1.0 1.0 1 05/02/14 11:00 05/05/14 17:21 7440-41-7 Cadmium ND ug/L 1.0 1.0 1 05/02/14 11:00 05/05/14 17:21 7440-43-9 Chromium 14.6 ug/L 5.0 5.0 1 05/02/14 11:00 05/05/14 17:21 7440-47-3 Cobalt 24.8 ug/L 5.0 5.0 1 05/02/14 11:00 05/05/14 17:21 7440-48-4 Copper ND ug/L 5.0 5.0 1 05/02/14 11:00 05/05/14 17:21 7440-50-8 Lead ND ug/L 5.0 5.0 1 05/02/14 11:00 05/05/14 17:21 7439-92-1 Nickel 157 ug/L 5.0 5.0 1 05/02/14 11:00 05/05/14 17:21 7440-02-0 Selenium ND ug/L 10.0 10.0 1 05/02/14 11:00 05/05/14 17:21 7782-49-2 M1 Silver ND ug/L 5.0 5.0 1 05/02/14 11:00 05/05/14 17:21 7440-22-4 Thallium ND ug/L 5.4 5.4 1 05/02/14 11:00 05/05/14 17:21 7440-28-0 M1 Vanadium 15.9 ug/L 5.0 5.0 1 05/02/14 11:00 05/05/14 17:21 7440-62-2 Zinc ND ug/L 10.0 10.0 1 05/02/14 11:00 05/05/14 17:21 7440-66-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 04/26/14 00:40 67-64-1 Acrylonitrile ND ug/L 10.0 1.9 1 04/26/14 00:40 107-13-1 Benzene 2.0 ug/L 1.0 0.25 1 04/26/14 00:40 71-43-2 Bromochloromethane ND ug/L 1.0 0.17 1 04/26/14 00:40 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 04/26/14 00:40 75-27-4 Bromoform ND ug/L 1.0 0.26 1 04/26/14 00:40 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 04/26/14 00:40 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 04/26/14 00:40 78-93-3 Carbon disulfide ND ug/L 2.0 1.2 1 04/26/14 00:40 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.25 1 04/26/14 00:40 56-23-5 Chlorobenzene 3.1 ug/L 1.0 0.23 1 04/26/14 00:40 108-90-7 Chloroethane 5.9 ug/L 1.0 0.54 1 04/26/14 00:40 75-00-3 Chloroform ND ug/L 1.0 0.14 1 04/26/14 00:40 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 04/26/14 00:40 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 04/26/14 00:40 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 04/26/14 00:40 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 04/26/14 00:40 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 04/26/14 00:40 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 04/26/14 00:40 95-50-1 1,4-Dichlorobenzene 3.6 ug/L 1.0 0.33 1 04/26/14 00:40 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/06/2014 04:23 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 23 aceAnalytical www.pacelabs.com r I ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Leachate White Oak LF Pace Project No.: 92198748 Sample: Leachate Lab ID: 92198748002 Collected: 04/24/14 13:10 Received: 04/24/14 17:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1.0 1 04/26/14 00:40 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.32 1 04/26/14 00:40 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 04/26/14 00:40 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 04/26/14 00:40 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 04/26/14 00:40 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 04/26/14 00:40 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 04/26/14 00:40 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 04/26/14 00:40 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 0.26 1 04/26/14 00:40 10061-02-6 Ethylbenzene 15.6 ug/L 1.0 0.30 1 04/26/14 00:40 100-41-4 2-Hexanone 34.8 ug/L 5.0 0.46 1 04/26/14 00:40 591-78-6 lodomethane ND ug/L 5.0 0.32 1 04/26/14 00:40 74-88-4 Methylene Chloride ND ug/L 2.0 0.97 1 04/26/14 00:40 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 04/26/14 00:40 108-10-1 Styrene ND ug/L 1.0 0.26 1 04/26/14 00:40 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 04/26/14 00:40 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 04/26/14 00:40 79-34-5 Tetrachloroethene ND ug/L 1.0 0.46 1 04/26/14 00:40 127-18-4 Toluene 2.6 ug/L 1.0 0.26 1 04/26/14 00:40 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 04/26/14 00:40 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 04/26/14 00:40 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 04/26/14 00:40 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 04/26/14 00:40 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 04/26/14 00:40 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 04/26/14 00:40 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 04/26/14 00:40 75-01-4 Xylene (Total) 41.4 ug/L 2.0 0.66 1 04/26/14 00:40 1330-20-7 m&p-Xylene 29.7 ug/L 2.0 0.66 1 04/26/14 00:40 179601-23-1 o-Xylene 11.7 ug/L 1.0 0.23 1 04/26/14 00:40 95-47-6 Surrogates 4-Bromofluorobenzene (S) 105 % 70-130 1 04/26/14 00:40 460-00-4 1,2-Dichloroethane-d4(S) 100 % 70-130 1 04/26/14 00:40 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 04/26/14 00:40 2037-26-5 Date: 05/06/2014 04:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. W, rem MAY 1 2 2014 AS HL-V,LL CFHCF Page 7 of 23 ZaceAnalytical www.pacelabs.com i I QUALITY CONTROL DATA Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Leachate White Oak LF Pace Project No.: 92198748 QC Batch: MPRP/15832 Analysis Method: EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater Associated Lab Samples: 92198748002 METHOD BLANK: 1189464 Matrix: Water Associated Lab Samples: 92198748002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Antimony ug/L ND 5.0 05/05/1417:14 Arsenic ug/L ND 10.0 05/05/1417:14 Barium ug/L ND 5.0 05/05/1417:14 Beryllium ug/L ND 1.0 05/05/1417:14 Cadmium ug/L ND 1.0 05/05/1417:14 Chromium ug/L ND 5.0 05/05/1417:14 Cobalt ug/L ND 5.0 05/05/1417:14 Copper ug/L ND 5.0 05/05/1417:14 Lead ug/L ND 5.0 05/05/1417:14 Nickel ug/L ND 5.0 05/05/1417:14 Selenium ug/L ND 10.0 05/05/1417:14 Silver ug/L ND 5.0 05/05/1417:14 Thallium ug/L ND 5.4 05/05/1417:14 Vanadium ug/L ND 5.0 05/05/1417:14 Zinc ug/L ND 10.0 05/05/1417:14 LABORATORY CONTROL SAMPLE: 1189465 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 500 491 98 80-120 Arsenic ug/L 500 468 94 80-120 Barium ug/L 500 490 98 80-120 Beryllium ug/L 500 466 93 80-120 Cadmium ug/L 500 450 90 80-120 Chromium u /L 500 458 92 80-120� Cobalt ug/L 500 472 94 80-120 Copper ug/L 500 492 98 80-120 Lead ug/L 500 478 96 80-120 MAY 1 2 2014 Nickel ug/L 500 474 95 80-120 Selenium ug/L 500 470 94 80-120 Silver ug/L 250 234 94 80-120 Thallium ug/L 500 475 95 80-120 SC?LID e'/i�:;TE St_CTIC)N Vanadium ug/L 500 476 95 80-120 AS! EMLLE ;:E(C {JiJAL OFFICE Zinc ug/L 500 450 90 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1189466 1189467 MS MSD 92198748002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 539 552 107 110 75-125 2 25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/06/2014 04:23 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 23 SOLID WASTE MANAGEMENT FACILITY FIRE OCCURRENCE NOTIFICATION NC DENR Division of Waste Management Solid Waste Section ern NCDENR Notify the Section verbally within 24 hours and submit written notification within 15 days of the Occurrence. (If additional space is needed, use back of this form.) NAME OF FACILITY: Haywood County (White Oak) Landfill PERMIT # 44-07 DATE AND TIME OF FIRE: 8/218/14 a unknown - found/reported a 6:30 am HOW WAS THE FIRE REPORTED AND BY WHOM: At approximately 6:00 aro, Thursday rooming, the early crew arrived at the landfill and smelled smoke. Ricky Kirkpatrick and crew members drove around the intdfill and found it on fire. LIST ACTIONS TAKEN: At 6:30 am, 911 and management were informed. At or around 8:15 anu, NCDENR was informed. 'file fire department was on site at 6:18 am and fought the fire with a combination of water and dirt. The fire was extinguished around 8:30 am. Landfill was closed for 24 hours and set a 48 hour fire watch. WHAT WAS THE CAUSE OF THE FIRE: The cause is unknown. heavy thunderstorms were in the area, so their is a possibility that the cause was lightening. No true hot spot was identified. DESCRIBE AREA TYPE, AND AMOUNT OF WASTE INVOLVED: the area was on approximately 100 ft x 50 ft of household waste. The average depth appeared to be around 4 ft deep. WHAT COULD HAVE BEEN DONE TO FREVENT 7'HIS FIRE: The exact cause is unknown. Therefore, preventative measures for this particular fire can not be developed. Landfill personnel plan to continue following the landfill's operations plan and rely on their landfill's operator training. DESCRIBE PLAN OF ACTIONS TO PREVENT FUTURE INCIDENTS: The exact cause is unknown. However, we noticed the material (white plastic sheeting) used for storm water diversion was a fire accelerant which appeared to increase the fire's intensity. Landfill personnel plan to avoid storing and disposing of this material near (lie top of the active working face in the future. NAME:John Preston TITLE: Landfill Operator DATE: 8/26/14 THIS SECTION TO BE COMPLETED BY SOLID WASTE SECTION REGIONAL STAFF DATE RECEIVED � 2 -T 12,a q List any factors not listed that might have contributed to the ?tire or that might prevent occurrence of future fires: FOLL W-UP REQUIRED: NO PHONE CALL ❑ SUBMITTAL MEETING RETURN VISIT BY: (DATE) AC IONS TAKEN OR REQUIRED: ^� Revised 618109 SANTEK I® WasteServices 650 25th Street, N.W., Suite 100 Cleveland, Tennessee 37311 (423) 303-7101 Email: mail@santekenvifo.com Internet: www.santekenviro.com May 9, 2014 Mr. Allen Gaither North Carolina Dept. of Environment and Natural Resources Division of Waste Management 2090 U.S. 70 Highway Swannanoa, NC 28778 RE: Updated Operations Plan — Section 13 (Leachate Management Plan) Haywood County (White Oak) Solid Waste Landfill Haywood County, North Carolina Permit Number: 44-07 Dear Mr. Gaither: In accordance with the Notice of Violation (NOV) letter dated April 9, 2014 from the North Carolina Department of Environment and Natural Resources (NCDENR), Division of Solid Waste Management — Solid Waste Section, Santek Waste Services, Inc. (Santek) is submitting an updated Operations Plan for the Haywood County (White Oak) Landfill. As requested by the April 9, 2014 NOV letter, Section 13 (Leachate Management Plan) has been updated to include leachate release response/contingency plans and notification requirements. A redlined copy of revised page 19 and an original copy of the updated Operations Plan are enclosed for your review. If you have any questions or require additional information, please feel free to call me at (423) 303-7101. Sincerely, Ron E. Vail, P.E. V.P. of Engineering Enclosures RECEIVED MAY 15 2014 SOLID WASTE SECTION ASHEVILLE REGIONAL OFFICE cc: Andrea Keller, Environmental Senior Specialist, NCDENR Ervin Lane, Compliance Hydrogeologist, NCDENR Ira Dove, Interim Manager, Haywood County Stephen King, Solid Waste Director, Haywood, County (with enclosure) Cheryl Dunson, Executive V.P. of Marketing, Santek Robert D. Burnette, P.E., Executive V.P. of Engineering, Santek Matt Dillard, Executive V.P. of Operations, Santek John Preston, Landfill Manager, Santek (with enclosure) Updated Redline Copy Page 19 (Leachate Management Plan) will be temporarily stored within the MSWLF units until such a time the flow of leachate can continue to the lagoon. If any rain or other event requires storage of leachate or storm water in the cell, the Division of Waste Management will be notified verbally and immediately followed by written communication. During wet weather, the pump and hauling may have to be performed 24 hours a day for several days until the leachate lagoon levels have been reduced. In the early phases of waste fill operations in MSW Phase 3, the discharge from the stormwater removal pump can be diverted to the leachate gravity system, if necessary during extreme conditions. f. The recirculation of leachate within the landfill is a viable alternative to the present pump and haul leachate management operation and is considered a part of the overall Leachate Management Plan. Prior to actually beginning leachate recirculation, the County will prepare the appropriate leachate recirculation plan for submission to and approval by the North Carolina Department of Environment and Natural Resources (NCDENR), Division of Waste Management. g. Leachate Release Response/Contingency Plan: In the event of a leachate release outside the lined disposal area or leachate collection and storage system, Haywood County or Santek will immediately utilize all available resources to contain and minimize the leachate release. Soil berms, ditches and landfill equipment may be used to contain the leachate and repair the affected area. h. Leachate Release Notification Requirements: In the event of a leachate release outside the lined disposal area or leachate collection and storage system, Haywood County or Santek will notify the NCDENR, Division of Waste Management within 24 hours of becoming aware of the leachate release. Haywood County installed a leachate cleanout in the northeast portion of Phase I to assist leachate flow through the leachate collection system. Haywood County or Santek will monitor this cleanout for the presence of leachate. If leachate is detected in the cleanout, Hay_ood County or Santek will pump out the leachate and transport it to the leachate storage lagoon. Operations Plan White Oak Landfill Revised May 2014 Page 19 EXISTING SEDIMENT \�\`\ BASIN 5 >> MW-4A e LFG-4r MW `3R \1 MW-3r EXISTING''�J LEACHATE LAGOON MVY-8 J{ N PHASE 30000 PHASE 1 SOIL SAMPLE COLLECTION POINT LOCATIONS ■ ■ ■ ■ ■ �� Lo • •• DATE