8602_Surry_MtAiry_MSWLF_CDLF_June21GW_FID1619768_20211020

DNLY ❑ Paper Report ❑ Electronic Data - Email CD (data loaded: Yes / No
NC DENR
Division of Waste Management - Solid Waste
Doc/Event #:
Environmental Monitoring
Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
• Prepare one form for each individually monitored unit.
Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
• Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
• Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
• Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646-"flail Service Center, Raleigh, NC 27699-1646.
S�tid Waste:Monitoring Data Submittal Information -.
Name of entity submitting data (laboratory, consultant, facility owner).
Municipal Engineering Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Jonathan Pfohl
E-mail: [e-mail]
Facility name:
Surry County Closed C&� and
Closed MSW Landfill -Mt. Airy
Facility Address:
'237 Landfill Road
�;Mt. �ciry, NC 27030
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring � Detection Monitoring
T e of data submitted: (Check all that apply)
X Groundwater monitoring data from monitoring wells
X Groundwater monitoring data -from private water supply wells
Leachate monitoring data
X Surface water monitoring data
Notification attached?
Phone: [phone]
Facility Permit #
NC Landfill Rule
(.0500 or .1600)
1600
® Assessment Monitoring
Methane gas monitoring data
Corrective action data (specify}
Other(specify)
Actual sampling dates (e.g.,
October 2Q-24, 2006)
I,June 23-25, 2021
Corrective Action
MNA parameters on 7 wells
I_ No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC ZL groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification -
To the best of_my knowledge, the information reported and statements made on this data submittal and attachments aro true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
S.J. Zimmerman, P.G. Project Manager [phone]
Fac�RepresenQ Name (Print) Title (Area Code) Telephorre Number
Signatlur/i
V
P.O. BOX 97, Garner, NC 27529
Facility Representative Address
C-0281
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
o / Z,D �
Date
Affix NC Licensed/ Professional Geologist Seal
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June 2021
L���111L l��o 96 0�,
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Jonathan Pfohl
environmental Specialist
mg,,,mesco. com
MUNICIPAL Ei�1GINEERING
6e SHIPWASH DR ivE, GARKER, NC 27529 - PH❑NE: 91 9.772.5393
P.Q. BOX 349, BOONE. NC 28607 - PHONE@& S2$-262-1 767
LICENSE NUMBER: CM02B1

TABLE OF CONTENTS
SECTION
Introduction....................................................................................................................................................................................................................................................................................................................................Page
1
Background......................................................................................................................................................................................................................................................................................................................................
Page 1
SamplingProcedures........................................................................................................................................................................................................................................................................................................Page
2
FieldParameter Data......................................................................................................................................................................................................................................................................................................._Page
2
LaboratoryResults.............................................................................................................................................................................................................................................................................................................._Page
2
QualityControl Samples..........................................................................................................................................................................................................................................................................................Page
3
Groundwater Samples Detected Above Standards..........................................................................................................................................................................................................Page
3
Surface Water Samples Detected Above Standards......................................................................................................................................................................................................Page
4
CorrectiveAction Update.........................................................................................................................................................................................................................................................................................Page
4
MNA Analysis (AOCs Northern, Southern and MW-11)...................................................................................................................................................................................Page
4
Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern)....................................................................................................Page
4
MW-I I AOC Investigations................................................................................................................................................................................................................................................................................Page
5
Groundwaterand Surface Water Characterization..........................................................................................................................................................................................................Page
5
Findings..................................................................................................................................................................................................................................................................................................................................................Page
5
Closing....................................................................................................................................................................................................................................................................................................................................................Page
6
Topographic Map with Site Location.................................................................
Single Event Potentiometric Map of Uppermost Aquifer
FIGURES
1
2
Total Cumulative VOC Concentrations Pre/Post Injection Comparison..........................................................................................................................Figure 1
Total Cumulative VOC Concentrations Time Series Graphs/Table.........................................................................................................................................Figure 2
TABLES
GroundwaterMonitoring Well Construction Table....................................................................................................................................................................................................Table
1
FieldObservations of Monitoring Locations.........................................................................................................................................................................................................................Table
2
FieldParameter Data Summary ................................................................................................................................................................................................................................................................_Table
3
Samplingand Analysis Summary ............................................................................................................................................................................................................................................................Table
4
Groundwaterand QC Sample Detections..................................................................................................................................................................................................................................Table
5
SurfaceWater Sample Detections............................................................................................................................................................................................................................................................Table
6
Hydrologic Properties at Monitoring Well Locations.............................................................................................................................................................................................Table
7
APPENDICIES
FieldSampling Parameter Data Sheets..........................................................................................................................................................................................................................._Appendix A
Laboratory Analysis Report and Chains of Custody..................................................................................................................................................................................Appendix B

Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Semi -
Annual Water Quality Report with Corrective Action Update for the late Spring 2021 event performed at the Surry
County closed construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount
Airy. NCDEQ Solid Waste Rules 15ANCAC 13B.1632 requires that Surry County provide this report to the NC Solid
Waste Section (SWS) on a semi-annual basis. This report documents the quality of the ground and surface waters
during an event performed on June 23-25, 2021.
During this event laboratory analytical results indicate Appendix I constituents continue to persist in concentrations
above groundwater compliance Standards in samples collected from eight monitoring wells. No constituents were
detected in any surface water sample above established surface water quality standards (NC 2B Standards). Corrective
action to remediate volatile organic compounds (VOCs) in groundwater is ongoing within all three areas of concern
(AOC) as described in the most recent Corrective Action Evaluation Report (CAER) and improvement has been
observed with updated information presented herein.
Background
The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy, North
Carolina. The site location topographic map is depicted in the attached Sheet 1. Prior to becoming a C&D landfill the
site operated as an unlined sanitary landfill that consisted of two units.
The northern unit was closed prior to October 1991. The southern unit is comprised of two contiguous portions. The
first part stopped receiving waste prior to October 1991 and the second part stopped receiving waste prior to January 1,
1999. Both portions of the southern unit were properly closed with a low permeability cohesive cap per the Transition
Plan. The top portion of the southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time
it was properly closed with another cohesive cap in accordance with the Closure Plan. For continuity, both the northern
and the southern units are monitored and reported together.
An Alternative Source Demonstration (ASD), which established Site Maximum Allowable Contaminate (SMAC)
regulatory compliance levels for three metals (cadmium, cobalt, vanadium), was approved by the NCDEQ on April 20,
2020 (FID:1395468).
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since
1994. This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B
and as a condition of the post -closure portion of the permit to operate and memorandums this report contains sampling
procedures, field and laboratory results, groundwater and surface water characterization, and findings. This report also
contains a table of detections compared to Standards, field data results table, groundwater flow directions/rates table,
field observations of the monitoring network table, a potentiometric map of the uppermost aquifer, histograms of
historical detections, statistical trend analysis, laboratory analytical reports with chains -of -custody (C-O-C) and quality
assurance/quality control data.

Sampling Procedures
The water quality monitoring program, current as of this event date, includes sampling locations and parameters as
outlined in the Water Quality Sampling and Analysis Plan (SAP) (DIN:1320110 dated April 2019 and approved by the
SWS (DIN: 1320181) on May 1, 2019. Monitoring locations are shown on the enclosed potentiometric map (Sheet
2). MESCO personnel collected water samples from 16 out of 17 downgradient groundwater monitoring wells (MW-
3R, MW-6, MW-7, MW-9, MW-11, MW-125, MW-13 through MW-17 and MW-19 through MW-23), one background
well (MW-1), one newly installed water supply well (WSW-2), one supply well that no longer serves the scale house
(SCALEHOUSE) and four surface water locations (SW-1, SW-2, SW-3 and SW-4). Data from three surface water
points (SWN-1, SWN-2 and SW-C) designated in the Water Quality Monitoring Plan for the adjacent lined MSWLF
are presented because both permitted landfills share discharge areas. Quality control measures implemented during this
event included the quantification of potential artifact contaminants via equipment (EB) and field (FB) blanks. Samples
were not analyzed from the six injection wells (IW-1), (IW-2/MW-2), (IW-3/MW-3RS), (IW-4/MW-4), (IW-5/MW-5)
and (IW-6/MW-8) since they are exempt due to the presence of injectant residue which would yield water quality results
not representative of actual site contaminant conditions.
A summary of the construction of the monitoring wells is presented on Table 1. The function and integrity of all
monitoring locations were visually evaluated as documented on Table 2. The depth to water in each well was
electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping methodology or
bailing was utilized to adequately purge the wells to a minimum of three times the volume of standing water in the well
or until dry. Surface water samples were collected from the Stoney Creek discharge feature at previously designated
locations. During well purging and surface water sample collection the required field parameters were recorded.
The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene
bailer. Samples were collected, kept on ice, and transported to a NC -certified laboratory under proper C-O-C protocols
within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included depth to water, pH, temperature, specific
conductance, hardness, dissolved oxygen (DO) and turbidity. The field parameter data indicates the monitored
groundwater is slightly acidic with relatively low specific conductance which is generally consistent relative to each
other and congruent with data historically reported. Field parameter data recorded at the surface water locations had
low specific conductance and neutral pH which is consistent with uncontaminated water. A summary of the field
parameter data is presented in Table 3 and the field sampling data sheet is enclosed in Appendix A.
Laboratory Results
Pace Analytical Laboratory (PACE) performed the laboratory analysis of water samples for the total recoverable
constituents listed in 40 CFR Appendix I and 1,4-Dioxane. As part of assessment monitoring cyanide, an Appendix II
parameter, was targeted in two wells (MW-16, MW-22) since it was detected in low levels during the previous event.
A sampling and analysis table summarizing the locations, constituents, and methods is presented on Table
4. Laboratory results and C-O-Cs are contained in Appendix B.
2

Water samples were analyzed to the laboratory -established Method Detection Limits (MDL) and any value between the
MDL and laboratory -established Reporting Limit (RL) is qualified by the laboratory as an estimated concentration
hence qualified with a "J". Estimated concentrations are considered non -quantifiable and discretion should be made
prior to making decisions based solely on an approximate value. Table 5 summarizes constituents detected in
groundwater and QC samples compared to groundwater compliance standards, which include Interim Maximum
Allowable Concentrations (IMAC), North Carolina Groundwater Standards (2L) and Site Maximum Allowable
Concentrations (SMAC). Although not applicable for regulatory compliance purposes detections are also compared to
the Maximum Contaminant Level (MCL) commonly referenced as the Federal "Drinking Water Standard". Table 6
lists the constituents detected in surface water samples compared with the NC Division of Water Resources "Surface
Water Quality Standards, Criteria & Protected Values", modified July 26, 2021.
Quality Control Samples
Methylene chloride and zinc were detected in the quality control blanks (EB, FB). Since these constituents were not
detected in any other samples above allowable levels the identified artifact contaminant is largely inconsequential.
Groundwater Samples Detected Above Standards
Cobalt was detected in samples collected from eight wells [MW-6 (30.6 ug/L), MW-7 (68 ug/L), MW-9 (240 ug/L),
MW-11 (22.1 ug/L), MW-13 (12.9 ug/L), MW-16 (541 ug/L) MW-20 (165 ug/L) and MW-22 (150 ug/L)] above its
SMAC (II ug/L).
VOC(s) were detected in quantifiable concentrations (> RL) above the NC 2L Standard in samples collected from four
wells as shown summarized below.
VOC(s) Detected Above 2L Standards in Groundwater
1,2-DCA
Benzene
1,4-DCB
VC
2L STD.
0.4
1
6
0.03
MW-9
1.8
10
MW-15
3.1
MW-16
1.5
1.4
MW-20
1.3
3.7
Concentrations in ug/L,
The majority of the monitoring locations that were found to contain VOCs included a mixture of dissolved phase
aromatic hydrocarbons and chlorinated aliphatic hydrocarbons. The only constituent which originated from an
anthropogenic source in levels above the EPA established maximum contaminant levels (MCLs) primary "Drinking
Water Standards" was vinyl chloride in samples from MW-9, MW-15 and MW-20. A site map depicting the
concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard during this event is presented
on Sheet 2.
N

Surface Water Samples
Total cobalt was detected in surface water samples SW-2 (28.3 ug/L) and SW-3 (27.5 ug/L) above its NC In -Stream
Target Value (1.6 chronic and 16 acute).
Corrective Action Update
Groundwater remediation continues to be implemented per the approved Corrective Action Plan (CAP) at the three
designated areas of concern (AOC) (Northern, Southern and MW-11). A second Corrective Action Evaluation Report
(CAER) (DIN: 1320112) was submitted on April 30, 2019 which demonstrated that groundwater conditions continue to
improve, except for area near MW-9, which was approved by the SWS on May 1, 2019 (DIN:1320182). A historical
summary of corrective actions performed to date are briefly described in the following sections.
MNA Analysis (AOCs Northern, Southern and MW-11)
Semi-annual MNA monitoring of a subset of 12 wells for the full suite of parameters recommended by the SWS, was
initiated on May 18, 2010 and performed for four consecutive semi-annual events to establish a baseline. A revised SAP
prescribing 7 wells with various targeted MNA constituents was approved by the SWS and initiated during an event
performed in May 2013. MNA monitoring during this event consisted of targeting volatile fatty acids, dissolved
hydrogen, ethene, ethane, methane, dissolved carbon dioxide, alkalinity, sulfate, sulfide, chloride, total organic carbon,
chemical oxygen demand, iron and DO) as presented on Table 5.
Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern)
Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was initiated
in the Southern and NorthernAOCs in accordance with requirements outlined in the Injection Well Permit Application
and Well Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic chlorinated
hydrocarbons in groundwater to below the 2L Standards. An edible oil substate (EOS)-water emulsion with a sodium
bromide tracer was injected into four wells (IW-1, IW-2, IW-3 and IW-5) on November 2-3, 2011. Similar substrates
were injected into monitoring wells MW-4/IW-4 and MW-8/IW-6 on October 24-25, 2012. Details of the injection
events are provided in the Injection Event Record dated November 4, 2011 and January 10, 2013.
As directed in the UIC Injection Well Permit renewed on April 15, 2013, semi-annual post -injection water quality
monitoring of wells located downgradient of viable injection points (MW-3R, MW-7, MW-9, MW-12S, MW-13, MW-
14, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20, MW-21, MW-22, MW-23) and upgradient background well
MW-1 was also performed in conjunction with this semi-annual event. Total aggregate VOC concentrations reported
during this event were lower at all locations and an increasing trend was not evident when compared to the respective
moving averages of the five events preceding injection in the selected wells downgradient of the injection
points (Figure 1).
4

MW-11 AOC Investigations
The CAP designated MW-11 as an area of concern due to detections of VOCs in exceedance of 2L Standards. MW-11
is located within the compliance boundary near the northern property line which is hydraulically upgradient of the
closed northern landfill. The northern landfill closed before October 1991, which was before adoption of NC Section
.1600 rules that address assessment and corrective action. VOCs have historically been detected in excess of the 2L
Standard at MW-11, which includes a mixture of aromatics (fuel hydrocarbons) and chlorinated hydrocarbons
(solvents). VOCs were not detected above allowable Standards in samples collected from MW-11 for the fifth
consecutive event which is an improvement compared to previous events. MNA will continue at MW-I I and substrate
injection is no longer planned nor required as described in the most recent CAER.
Groundwater and Surface Water Characterization
A potentiometric map constructed from water elevations taken from the uppermost aquifer which consists of both
saprolite and the hydraulically connected upper portion of the fractured bedrock system is enclosed as Sheet
2. Groundwater flow directions and velocity rates were calculated through a modified Darcy's equation as shown on
Table 7. Consistent with previous events the groundwater apparently flows in a general southeasterly direction towards
the tributaries of the Ararat River. The calculated average linear velocity of groundwater indicates an approximate
average of 2,029 ft/yr. in the wells screened in regolith and 391 ft/yr. in the wells screened in the bedrock. The consistent
disparity in flow rates between wells is indicative of heterogeneous geologic conditions and/or a product of the
limitations of the linear velocity equation when applied to anisotropic conditions which are characteristic of the geology
of the Piedmont. Streams located within the facility boundaries were observed to be of moderate volume and flow
with low turbidity.
Findings
One or more Appendix I constituent(s) were detected above allowable compliance levels in samples collected from the
uppermost aquifer at nine locations (MW-6, MW-7, MW-9, MW-11, MW-13, MW-15, MW-16, MW-20 and MW-22).
Since the October 2018 event the northern AOC plume has advanced beyond MW-20. All concentrations remain within
their own respective historically identified range except for cobalt and benzene in sample MW-20.
Qualitative evaluation of VOC concentrations indicates a general decreasing trend over time and distance from the
landfill. During this event total cumulative VOC concentrations decreased compared to their respective five event
averages preceding corrective action at most locations (Figure 2). Results of statistical temporal trend analysis, using
Sen's Slope Estimator at a 95% confidence level indicate that none of the individual well's cumulative VOC
concentrations have increased compared to when corrective action began 8 years ago except for MW-9 and MW-20.
The Southern AOC and site -wide cumulative VOC levels continue to exhibit a decreasing trend and VOCs are
increasing in the northern AOC.
The area of the uppermost aquifer beyond the compliance boundary containing quantifiable concentrations of VOCs in
exceedance of the 2L Standard during this event is estimated at 0.0 acres in the Northern AOC, 0.0 acres in the MW- I I
AOC and 4 acres in the Southern AOC for a total facility wide area of approximately 4 acres (Sheet 2). The total area
impacted beyond the compliance boundary has retracted an estimated 50% (from 8 acres to 4 acres) compared to when
corrective action was initiated 10 years ago and remains the same as the previous event.
9

Evaluation of the most current water quality data continues to support assertions drawn in previous reports. A few
VOCs persist in the upper portion of the aquifer but concentrations are decreasing over time and distance away from
the landfill. Samples collected from the local discharge features, which are all located within the property boundaries,
continue to lack contaminates above allowable levels. Data continues to indicate that the plumes within each AOC
have stabilized and/or are decreasing and there is adequate evidence that groundwater is naturally attenuating.
Corrective action will continue per the approved CAP with amendments described in the latest CAER.
Surface water samples SW-2 and SW-3, collected from the south flowing discharge feature located west of the landfill,
continues to contain levels of cobalt above allowable Standards. Cobalt was not detected in samples SW- 4 and SWN-
2 collected further downstream
Closing
Water quality monitoring will continue with the next sampling event scheduled for Fall of 2021.
211

Sheets

Topographic Map with Site Location
Surry County Landfill, Mt. Airy fl
237 Landfill Road
Mount Airy, NC 28621
Lat: 36-26-30.065
Long:-80-34-15.314
Northing:983356.18
Easting:1537885.48
0 Surry Co Property Line
O Closed Unlined C&D Landfill
O Closed Unlined Sanitary Landfill
O Active Lined MSW Landfill
SHEET 1

NOW OR FORMERLY
OWNED BY
JOHNNY COX
v% V 'v
SWN-1 (-350 FT UPSTREAM)
1050 -
1000
1100 1050
------------
INACTIVE LINED 0000
PHASE 1
PTO 12/1 /98
MONITORED SEPERATELY
.0000
ACTIVE LFG EXTRACTION
M W-9
Benzene - 1.8
Vinyl Chloride - 10
M -
Benzene - 1.3
r
Chlorid -
/ IW-3'
GWE=989.4
MW-3R*
MW-16 /GWE=976.82 '
GWE=974.19 A
MW-16
12-Dichloroethane - 1.5
Benzene - 1.4
SW-3
�MW--17
GWE=954.72
0
237 LANDFILL ROAD
MW--11
6WE=1129.60 --
__
SCALEHOUSE
11'o �` X
_ - CLOSED UNLINED MSW (8602-MSWLF-1983)
I - STOPPED RECEIVING WASTE BEFORE OCTOBER 9, 1991
1 �
1 ACTIVE LCID (NO PERMIT) <2 ACRES
IW--6
-MW--9 �WE=1049.00—a'�
GWE=1062.13 IW
�� MW WSW-2
a
M - GWE=1063.58 05� MW-1
SW-2 sw • GWE=1109.32
TIRES BURIED UNDER SOIL AND GRASS
/MW-7
I'
GWE=1062.13 _
CLOSED UNLINED C&D(8602-CDLF-2001)
�I STOPPED RECEIVING C&D BEFORE JUNE 30, 2008
l CLOSURE REQUIREMENTS COMPLETED BEFORE P
MW-6 -
GWE=1045.17
CLOSED C&D OVER CLOSED UNLINED MSW (8602-CDLF ON TOP OF MSW)
/ I STOPPED RECEIVING C&D BEFORE MARCH 3, 2006
STOPPED RECEIVING MSW BY JAN. 1, 1999
°
LFG EXTRACTION SYSTEM
D7U -
_
\ MW-12D* �\
IW-2 �� GWE=>1027.05
GWE= "' MUV--12$
_ �O5O ���� IW i GWE=1012.64
W-13,0007
GWE=983.84
'4
G WE= / 0000 0,
V
MW-14
O GWE=984.45
SW-1
MW-21
GWE=960.23
PROPERTY LINE
MW-15
Vinyl Chloride - 3.
MW-15
GWE=1027.12
NOW OR FORMERLY
OWNED BY
SHAWNA SUMMERS
LEGEND
EXISTING TOPOGRAPHIC CONTOURS
EXISITING ROAD/PATH
EXISTING CHAINLINK FENCE
EXISTING STRUCTURE
PERENNIAL CREEK, STREAM, ETC.
INTERMITTANT CREEK, STREAM, ETC.
PROPERTY LINE
LINED MSWLF PHASE LIMITS
- — — — — — — — — -
UNLINED WASTE LIMITS (APPROXIMATE)
- — -
COMPLIANCE BOUNDARY
1060
POTENTIOMETRIC GROUNDWATER CONTOUR (JUNE 22-23, 2021)
GWE = 2626.85
GROUNDWATER POTENTIOMETRIC ELEVATION
*MW-
ELEVATION NOT USED FOR CONTOURING
ESTIMATED EXTENT OF VOC VIOLATIONS (JUNE 2021
BEYOND COMPLIANCE BOUNDARY (--4 ACRES)
sw
SURFACE WATER SAMPLING LOCATION
":
MONITORING WELL EXISTING
1w
INJECTION WELL EXISTING
WATER SUPPLY WELL EXISTING
(APPROXIMATE LOCATION)
GRAPHIC SCALE
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SHEET 2
1 OF 1

Figures

Total Cumulative VOCs
Figure 1
Total Cumulative VOC Concentrations Pre/Post Injection Comparison
October 22, 2009 - June 25, 2021
Total Cumulative VOCs (Downgradient of IW-2)
DOWNGMDIENT OF IW 2
senpeoere svrgeoep
Total Cumulative VOCs
s.meDa.
Total Cumulative VOCs
s�Dve
Baseline
Period (Oct.
2009-Oct.
2011)
Difference
Difference
Average of
Between
Between
first Five
Corrective
Most
Most
Statistical
Oct
May
Oct
May
Oct
Action
June
Recent &
Recent &
Trend* Between
2009
2010
2010
2011
2011
Events
2021
Baseline
Baseline
Oct. 2009-June
Well ID
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(uq/L)
(uq/L)
N
2021
INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN
INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S & MW-13
MW-12S
0.00
0.00
0.00
0.00
5.40
1.08
0.00
0.00
0
HNo TrendH
MW-13
61.00
50.60
74.20
87.30
72.50
69.12
16.10
-53.02
-77
�Downward�
INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16
MW-3R
0.00
0.00
1 0.00
0.00
0.00
0.00
0.00
0.00
0
HNo TrendH
MW-16
1137.90
113.60
135.70
121.20
116.30
124.94
18.96
-105.98
-85
. Downward
INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23
MW-14
15.20
15.60
15.60
8.20
17.00
14.32
4.90
-9.42
-66
HNo TrendH
MW-21
52.10
50.70
51.38
39.10
32.41
45.14
15.39
-29.75
-66
Downward.
MW-23
4.30
0.00
0.00
0.00
0.00
0.86
1.12
0.26
30
HNo TrendH
INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MW-19
MW-15
96.13
63.89
55.00
78.10
64.06
71.44
32.36
-39.08
-39
Downward.
MW-19
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0
HNo TrendH
INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE
* = Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

Figure 2
Total Cumulative VOC Concentrations Time Series Graphs/Table
October 22, 2009 - June 25, 2021
ENTIRE SITE TOTAL CUMULATIVE VOCs in ALL WELLS (SINCE CA STARTED)
Time -aeries Graph of AIIW"11s
C o C r C M C o C v C m C rn
C C C C C C C C C C C C C
a a a a a a a a a a a a
Sample Uate
Total Cumulative VOCs (SOUTHERN AOC) Total Cumulative VOCs (NORTHERN AOC)
sa
OMN18 OW-13 .MN22 dI.M14-23 IAfiY21 e"VI-14 IAM1Y-15
AOC
Well ID
Oct
2009
May
2010
Oct
2010
May
2011
Oct
2011
Average of
first Five
Corrective
Action
Events
June 2021
Difference
Difference
Statistical Trend
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
N
Oct 2009 dune 2021
Background
MW-1
0.00
0.00
0.00
0.00
0.00
0.00
0
0.00
0
No Trend
IW-2 (MW-2)
105.25
207.00
207.93
159.90
79.10
151.84
79.10 NS
NS
NS
No Trend
IW-3 (MW-3RS)
202.90
127.50
127.50
144.00
127.60
145.90
127.60 NS
NS
NS
No Trend
MW-3R
0.00
0.00
0.00
0.00
0.00
0.00
0
0.00
0
No Trend
IW-4 (MW-4)
27.00
24.20
24.20
27.60
23.50
25.30
18.10 NS
NS
NS
No Trend
IW-5 (MW-5)
35.00
46.50
46.50
47.40
34.80
42.04
34.80 NS
NS
NS
No Trend
MW-12S
0.00
0.00
0.00
0.00
5.40
1.08
0.00
-1.08
-100
No Trend
MW-12D
0.00
0.00
0.00
0.00
0.00
0.00
0 NS
NS
NS
No Trend
MW-13
61.00
50.60
74.20
87.30
72.50
69.12
16.1
-53.02
-77
Downward
Southern
MW-14
15.20
15.60
15.60
8.20
17.00
14.32
4.9
-9.42
-66
Downward
MW-15
96.13
55.00
55.00
78.10
64.06
69.66
32.36
-37.30
-54
Downward
MW-16
137.90
113.60
135.70
121.20
116.30
124.94
18.96
-105.98
-85
Downward
MW-17
20.34
8.40
8.85
0.00
5.77
8.67
0
-8.67
-100
No Trend
MW-18
0.00
0.00
0.00
0.00
0.00
0.00
0 NS
NS
NS
No Trend
MW-19
0.00
0.00
0.00
0.00
0.00
0.00
1.11
1.11
100
No Trend
MW-21
52.10
50.70
51.38
39.10
32.41
45.14
15.39
-29.75
-66
Downward
MW-22
28.90
23.80
23.80
11.66
5.20
18.67
3.96
-14.71
-79
Downward
MW-23
4.30
0.00
0.00
0.00
0.00
0.86
1.12
0.26
-30
No Trend
Combined Total
786.02
722.90
770.66
724.46
583.64
717.54
353.50
-364.04
-51
Downward
MW-6
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
-100
No Trend
MW-7
7.40
9.40
11.20
9.70
8.80
9.30
0.00
-9.30
-100
Downward
Northern
IW-6 (MW-8)
22.00
23.90
16.00
12.30
12.60
17.36
10.20 NS
NS
NS
No Trend
MW-9
23.50
20.40
23.20
25.80
22.90
23.16
33.99
10.83
47
Upward
MW-20
0.00
0.00
0.00
0.00
0.00
0.00
16.31
16.31
100
Upward
Combined Total
52.90
53.70
50.40
47.80
44.30
49.82
60.50
10.68
21
Upward
MW-11
MW-11
10.10
6.00
6.00
5.44
23.20
10.15
0.39
-9.76
-96
No Trend
SITEWIDE
Combined Total
849.02
782.60
827.06
777.70
651.14
777.50
414.39
-363.11
-47
Downward
"s = Not sampled this event. Most recent concentration shown and used in calculations
* = Statistical trend analysis via Sen's Slope Estimator on original and transformed log -normal at a 95% Confidence Level
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

Tables

Table 1
Groundwater Monitoring Well Construction Table
June 22-24, 2021
Monitoring Well
Date
Installed
Well
Diameter
Total Well
Depth
Top of Screen
Depth
Screen
Length
Geology of
Screened
Interval
Top of Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
Latitude
Longitude
(inches)
(ft bgs)
(ft bgs)
(ft)
(ft amsl)
(ft amsl)
(ft amsl)
(ft btoc)
MW-1
11/28/89
2
40
30
10
Clay
1134.35
1133.15
1109.32
25.03
36.439211
-80.568133
0-2 (was MW-2)
11/28/89
2
70
60
10
Clay
1068.86
1068.36
NR
NR
36.435833
-80.568894
MW-3R
9/27/94
2
101
86
15
Rock
1017.50
1015.00
976.82
40.68
36.434725
-80.571989
IW-3 (was MW-3RS)
5/17/01
2
52
37
15
Rock
1020.57
1018.24
989.46
31.11
36.434656
-80.571858
IW-4 (was MW-4)
8/30/94
2
55.4
40.4
15
Rock
1026.26
1025.06
NR
NR
36.434686
-80.569200
0-5 (was MW-5)
8/27/94
2
63
48
15
Rock
1080.18
1077.78
NR
NR
36.434614
-80.570436
MW-6
9/7/94
2
29.7
14.7
15
Rock
1067.67
1065.61
1045.17
22.5
36.437431
-80.571067
MW-7
8/23/94
2
23
8
15
Rock
1073.50
1071.50
1061.85
11.65
36.438439
-80.570722
IW-6 (was MW-8)
8/16/94
2
54
39
15
Rock
1088.45
1086.45
NR
NR
36.439278
-80.570381
MW-9
8/22/94
2
43.8
28.8
15
Rock
1094.07
1092.07
1062.13
31.94
36.439289
-80.571508
MW-11
8/15/94
2
40
25
15
Rock
1151.80
1150.40
1129.60
22.20
36.441589
-80.569558
MW-12S
5/31/01
2
51
11
40
Rock
1025.80
1023.25
1012.64
13.16
36.435942
-80.567972
MW-12D
5/30/01
2
100
90
10
Rock
1027.05
1023.75
1027.05
0.00
36.435964
-80.567994
MW-13
5/30/06
2
35.78
20.78
15
Saprolite
1008.48
1005.75
983.84
24.64
36.435036
-80.568183
MW-14
5/30/06
2
48.03
33.03
15
Rock
1018.80
1016.11
984.45
34.35
36.434267
-80.569239
MW-15
6/22/06
2
57
42
15
Rock
1075.96
1073.23
1027.15
48.81
36.433797
-80.570467
MW-16
6/21/06
2
36.3
21.3
15
Rock
999.54
996.67
974.19
25.35
36.434536
-80.572117
MW-17
6/1/07
2
15.32
5.32
10
Rock
965.43
962.26
954.72
10.71
36.433558
-80.572517
MW-18
6/1/07
2
18.15
8.15
10
Saprolite
983.00
980.00
NR
NR
36.435453
-80.567050
MW-19
6/1/07
2
17.1
7.1
10
PWR
946.27
942.97
936.89
9.38
36.432231
-80.570556
MW-20
6/1/07
2
25.64
10.64
15
Rock
1082.19
1079.12
1063.58
18.61
36.439025
-80.571650
MW-21
6/1/07
2
15.41
5.41
10
Saprolite/PWR
965.36
962.22
960.23
5.13
36.434214
-80.568717
MW-22
6/1/07
2
16.04
6.04
10
Saprolite
953.40
950.23
948.29
5.11
36.432928
-80.571678
MW-23
6/1/07
2
17.1
7.1
10
Sandy Silt
955.31
952.09
947.72
7.59
36.432828
-80.569156
NOTE:
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Slurry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Table 2
Field Observations of Monitoring Locations
June 22-24, 2021
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked on
Arrival &
Departure
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears
Effective
Comments
MW-1
Yes
Yes
Yes
Yes
Yes
Yes
IW-1
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11.
IW-2 (was MW-2)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11. No pad visible
MW-3R
Yes
Yes
Yes
Yes
Yes
Yes
IW-3 (was MW-3RS)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11.
IW-4 (was MW-4)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 10/24/12.
IW-5 (was MW-5)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11. Bailer would not descend
MW-6
Yes
Yes
Yes
Yes
Yes
Yes
Orange purge water
MW-7
Yes
Yes
Yes
Yes
Yes
Yes
IW-6 (was MW-8)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 10/24/12.
MW-9
Yes
Yes
Yes
Yes
Yes
Yes
MW-11
Yes
Yes
Yes
Yes
Yes
Yes
Strong odor
MW-12S
No
Yes
Yes
Yes
Yes
Yes
MW-12D
Yes
Yes
Yes
Yes
Yes
Yes
Flowing artesian which is typical
MW-13
Yes
Yes
Yes
Yes
Yes
Yes
MW-14
Yes
Yes
Yes
Yes
Yes
Yes
MW-15
Yes
Yes
Yes
Yes
Yes
Yes
MW-16
Yes
Yes
Yes
Yes
Yes
Yes
Pad loose
MW-17
Yes
Yes
Yes
Yes
Yes
Yes
MW-18
Yes
Yes
Yes
Yes
Yes
Yes
MW-19
Yes
Yes
Yes
Yes
Yes
Yes
Orange purge water
MW-20
Yes
Yes
Yes
Yes
Yes
Yes
Orange purge water
MW-21
Yes
Yes
Yes
Yes
Yes
Yes
Orange purge water
MW-22
Yes
Yes
Yes
Yes
Yes
Yes
Orange purge water
MW-23
Yes
Yes
Yes
Yes
Yes
Yes
Turbid purge water
sW-1
Yes
SW-2
Yes
Moderate gage height & flow
SW-3
Yes
Moderate gage height & flow
SW-4
Yes
Moderate gage height & flow
sW-c
Yes
Moderate gage height & flow
SW N-1
Yes
Moderate gage height & flow
SWN-2
Yes
Moderate gage height & flow
WSW-2
Yes
Taken from hose bib since well sealed closed
SCALEHOUSE
Yes
Not in use
Any unusual field conditions, observations, or events:
Injection wells (IW-1, IW-2, IW-3, IW4, IW-5 and IW-6) exempt from laboratory analysis as approved by NC SWS on May 10, 2013 (DIN:18938)
Visual markers (10 ft PVC pipes) remain secured to each monitoring well case
Slurry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Table 3
Field Parameter Data Summary
June 22-24, 2021
Parameter
Depth to
Water
Water
Elevation
TOC
Elevation
DO
Temp.
pH
Hardness
Specific
Conductance
Turbidity
Units
ft (btoc)
ft (amsl)
ft (amsl)
mg/L
C
SU
mg/L
umhos/cm
NTU
MW-1
25.03
1109.32
1134.35
3.4
19.3
6.97
NR
949
4.30
IW-2
NR
NR
1068.86
NR
NR
NR
NR
NR
>1000
MW-3R
40.68
976.82
1017.50
NR
15.2
6.81
NR
277
906
IW-3
31.11
989.46
1020.57
NR
NR
NR
NR
NR
>1000
IW-4
NR
NR
1026.26
NR
NR
NR
NR
NR
>1000
IW-5
NR
<1040.18
1080.18
NR
NR
NR
NR
NR
NR
MW-6
22.50
1045.17
1067.67
NR
15.5
6.39
NR
130
4.62
MW-7
11.65
1061.85
1073.50
1.7
NR
NR
NR
NR
2.12
IW-6
NR
NR
1088.45
NR
NR
NR
NR
NR
NR
MW-9
31.94
1062.13
1094.07
0.5
NR
NR
NR
NR
7.65
MW-11
22.20
1129.60
1151.80
4.0
19.1
5.50
NR
854
13.8
MW-12S
13.16
1012.64
1025.80
NR
15.4
6.45
NR
236
29.3
MW-12D
0.00
>1027.05
1027.05
NR
NR
NR
NR
NR
NR
MW-13
24.64
983.84
1008.48
NR
15.1
6.01
NR
145
8.26
MW-14
34.35
984.45
1018.80
4.4
18.7
5.83
NR
204
1.66
MW-15
48.84
1027.12
1075.96
1.3
NR
NR
NR
NR
28.7
MW-16
25.35
974.19
999.54
NR
14.9
5.86
NR
403
14.1
MW-17
10.71
954.72
965.43
NR
14.8
6.21
NR
250
7.07
MW-18
NR
NR
983.00
NR
NR
NR
NR
NR
NR
MW-19
9.38
936.89
946.27
NR
14.9
5.41
NR
36
11.10
MW-20
18.61
1063.58
1082.19
NR
14.7
5.51
NR
148
96.1
MW-21
5.13
960.23
965.36
2.3
18.9
6.33
NR
331
11.0
MW-22
5.11
948.29
953.40
NR
15.6
5.88
NR
337
9.71
MW-23
7.59
947.72
955.31
NR
15.1
5.73
NR
42
6.06
Scalehouse
na
na
na
NR
NR
NR
NR
NR
NR
Minimum
0.00
936.89
946.27
0.5
14.7
5.41
-
36
1.66
Average
20.42
1009.33
1034.58
2.5
16.2
6.06
-
310
68.3
Maximum
48.84
1129.60
1151.80
4.4
19.3
6.97
-
949
>1000
SW-1
-
-
-
NR
NR
NR
34.2
NR
11.4
SW-2
-
-
-
NR
NR
NR
51.3
NR
8.63
SW-3
-
-
-
NR
NR
NR
51.3
NR
12.9
SW-4
-
-
-
NR
NR
NR
NR
NR
NR
SW-C
-
-
-
NR
NR
NR
17.1
NR
4.21
SWN-1
-
-
-
NR
NR
NR
34.2
NR
6.06
SWN-2
-
-
-
NR
NR
NR
34.2
NR
8.13
Minimum
-
-
-
-
-
-
17.1
-
4.21
Average
-
-
-
-
-
-
37.1
-
8.56
Maximum
-
-
-
-
-
-
51.3
-
12.9
btoc = Below top of casing
amsl = Above mean sea level
na = Not available
NR = No reading attempted
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Table 4
Sampling and Analysis Summary
June 23-25, 2021
App. I
Other
App 2
MNA
Field Parameters
a
o:
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co0
0
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a
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W
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0
J
JLL
LL
LL
LL
LL
LL
IW-1
Not sampled since exempt per NC SWS approved WQMP
MW-1
X I X I X I Ix X X X X X X X X XjXj 1XIX I X I I X I X
IW-2
Not sampled since exempt per NC SWS approved WQMP
MW-3R
X I X I X I I I I I I I X I I X I I X I X
IW-3
Not sampled since exempt per NC SWS approved WQMP
IW-4
Not sampled since exempt per NC SWS approved WQMP
IW-5
Not sampled since exempt
per NC SWS approved WQMP
MW-6
X
X
I X
I
I
I
I
I
I
I X
I X
X
X
X
MW-7
X
I X
I X
I
jx
X
XIXIX
X
x
X
X
X
X
I X
I X
X
I X
X
IW-6
Not sampled since exempt
per NC SWS approved WQMP
MW-9
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-11
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-12S
X
X
X
X
X
X
X
MW-12D
Not sampled since exempt
per NC SWS approved WQMP
MW-13
X
X
X
X
X
X
X
MW-14
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-15
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-16
X
X
X
X
X
X
X
X
MW-17
X
X
X
X
X
X
X
MW-18
Not sampled since exempt
per NC SWS approved WQMP
MW-19
X
X
X
X
X
X
X
MW-20
X
X
X
X
X
X
X
MW-21
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-22
X
X
X
X
X
X
X
X
MW-23
X
X
X
X
X
X
X
Scalehouse
X
X
X
X
X
X
WSW-2
X
X
X
X
X
X
sW-1
X
X
X
X
X
X
X
X
SW-2
X
X
X
X
X
X
X
X
SW-3
X
X
X
X
X
X
X
X
SW-4
X
X
X
X
X
X
X
X
SW-C
X
X
X
X
X
X
SWN-1
X
X
X
X
X
X
X
X
SWN-2
X
X
X
X
X
X
X
X
EB
X
X1
X
FB
X1
I X
Hpp i a u Lists = rrom current 4u crrc zba
Eight wells exempt from lab testing per NC SWS approved WQMP [FID:13201811
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Table 5
Groundwater and Quality Control Sample Detections
June 23-25, 2021
Parameter Name
MDL
RL
2L Standard
MCL
MW-1
MW-3R
MW-6
MW-7
MW-9
MW-11
MW-12S
MW-13
MW-14
MW-15
MW-16
MW-17
MW-19
MW-20
MW-21
MW-22
MW-23
SCALEHOUSE
WSW-2
EB
FB
IMAC Value
SMAC Value*
BG
S
S
S
S
I S
S
S
S
S
S
S
S
I S
I S
I S
I S
I WSW
I WSW
QC
QC
Metals
(Targeted
40CFit
258
Appendix
I
Antimony, total
3
5
1
6
4.1J
4.4J
Arsenic, total
4.7
10
10
10
6J
5J
5.8J
6.5J
Barium, total
3.5
5
700
2000
34.9
5.7
73
52.6
55.7
35.7
12.9
66.2
40
21.4
115
9.7
19.4
50.4K55.4
75.2
31.2
13
3.8J
Cadmium, total
0.4
1
8**
5
0.73J
0.72J
0.51J
0.47J
1.8
4.8
2
0.46J
1.92.3
0.85J
Cobalt, total
3.6
5
11*
NE
30.6 (L)
68 (L)
240 (L)
22.1 (L)
12.9 (L)
541 (L)
165 (L)150
(L)
Copper, total
4.3
5
1000
1300
43.5
Nickel, total
3.5
5
100
NE
8.6
24
7.410.7
Selenium, total
4.7
10
20
50
5.4J
5.6J
6.5J
Thallium, total
0.05
1
0.28
2
0.64J
0.14J
0.57J
0.1J
O.OSSJ
0.054J
0.38J
0.81J0.17J
Vanadium, total
3.9
5
27 *
NE
4J
3.9J
5.5
4.2J4.2J
Zinc, total
9.5
10
1000
NE
71.7
15.2
17.8
13.3
45.2
15.4
11.2
VOCs (Targeted 40CFR 258 Appendix I, cyanide
and 1,4-Dioxane
1,1-Dichloroethane
0.37
1
6
NE
0.94J
0.39J
0.86J
1.2
4.4
0.591
0.43J
1.1V12.
0.62J
0.38J
1,2-Dichlorobenzene
0.34
1
20
NE
2.2
0.4J
0.63J
1.80.39J
1,2-Dichloroethane
0.32
1
0.4
5
0.84J
0.53J
1.5(L)
0.49J
1,2-Dichloropropane
0.36
1
0.6
5
0.74J
Benzene
0.34
1
1
5
1.8 (L)
0.43J
1.4 (L)
1.3 (L)0.36J
Chloroethane
0.65
1
3000
NE
0.951
0.81J
cis-1,2-Dichloroethene
0.38
1
70
70
18.1
12.1
3.7
21.9
12.4
0.68J
7.6
2.1
0.74J
Meth lene Chloride
2
5
5
5
2.1 J
2.1 J
Toluene
0.48
1
600
1000
1.9
Trichloroethene
0.38
1
3
5
2
Vinyl chloride
0.39
1
0.03
2
10 (L)
3.1 (L)
1.7
3.7 (L)
MNA
Performance
Parameters
Acetic Acid
120
500
NE
NE
300J
-
-
360J
3000J
310J
-
-
360J
380J
-
-
-
-
670J
-
-
-
-
--
--
Alkalinity
5000
5000
NE
NE
11800
-
-
90800
54800
22800
-
-
41000
29700
-
-
-
-
33000
-
-
-
-
--
--
Chemical Oxvgen
12500
25000
NE
NE
-
-
24600J
24600J
-
-
-
-
-
-
-
-
-
-
--
--
Chloride
500
1000
250000
NE
2580
-
-
25000
28400
10700
-
-
2790
2250
-
-
-
-
29100
-
-
-
-
--
--
Ethane
0.17
1
NE
NE
-
-
0.65J
28
-
-
-
-
-
-
-
-
-
-
--
--
Ethene
0.24
1
NE
NE
-
-
2.6
-
-
-
-
-
-
-
-
-
-
--
--
Formic acid
55
500
NE
NE
5300
-
-
4600
44000
5200
-
-
5800
4900
-
-
-
-
12000
-
-
-
-
--
--
Hydrogen (nM)
0.49
1.9
NE
NE
0.55J
-
-
1J
1.3J
8
-
-
2.8
5.3
-
-
-
-
1J
-
-
-
-
--
--
Lactic Acid
40
1 500
NE
NE
-
-
19100
43J
-
-
40J
44J
-
-
-
-
55J
-
-
-
-
--
--
Methane
53
500
NE
NE
91J
86J
2301
2204
57J
Sulfate
2
5
250000
NE
170
2200
120
1100
Sulfide
1 500
1 10001
NE
I NE
1 4860
1
1
1 6960
1 776J
1 15600
1
1
1 872J
1 1730
1
1
1
1
1 1420
500
1 10001
NE
I NE
I 505J
I
1
1 3680
1 2830
1 947J
I
I
I 799J
I 773J
I
I
I
1
1 1540
Notes:
Units ug/L unless shown otherwise, Blank cells means not detected above MDL, -- means parameter not analyzed, NE means not established.
Bold Above RL and Established 21-/IMAC/SMAC (Regulatory compliance Standard)
Above Established Federal MCL Drinking Water Std. (NOT a regulatory compliance Standard)
BG= Background Well Sample, QC = Quality Control Sample, S = Sentinal Well Sample
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
RL = Reporting Limit defined by Pace laboratory as "The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix."
2L/IMAC/SMAC = NC 2L, IMAC and SMAC values recognized by the NC SWS as regulatory groundater Standards.
2L = NC 2L Groundater Standard 15A NCAC 02L .0202
IMAC = Interim Maximum Allowable Concentration
SMAC = Site Maximum Allwable Concentration. Approved by NC SWS via ASD April 1, 2020.
MCL = Primary Maximum Contaminant Level for drinking water established by the USEPA.
J = "J-qualified". Defined by the lab as "estimated concentration above the adjusted method detection limit and below the adjusted reporting limit".
(N) Preliminary source is believed to be Natural originating from erosion of natural deposits. Source not anthropogenic.
(L) Prelilminary source is believed to be anthropogenic with Landfill Gas Wor leachale as suspected transport mechanism.
A definitive source of the detections was not determined as part of this report.
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Table 6
Surface Water Sample Detections
June 25, 2021
Parameter Name
MDL
RL
NC 2B
STD1
EPA
NRWQCZ
NC ISTVs
MCL"
SWN-2
SW-4
SW-C
SW-1
SW-2
SW-3
Downstream
Downstream
Downstream
Downstream
Downstream
Downstream
Metals (Targeted
40CFR 258 Appendix 1)
Barium, total
3.5
5
NE
NE
21,000
2000
16.2
16.4
21.9
24.8
45.3
Barium, dissolved
3.5
5
NE
NE
NE
2000
39.6
Cobalt, total
3.6
5
NE
NE
1.6c. 16A
NE
28.3
27.5
Cobalt, dissolved
3.6
5
NE
NE
NE
NE
23.5
Thallium, total
0.05
0.1
NE
NE
2
2
0.11
VOCs (Targeted 40CFR 258 Appendix I and 1,4-Dioxane)
1,4-Dichlorobenzene
0.33
1
NE
NE
100
75
0.33 J
cis-1,2-Dichloroethene
0.29
1
NE
NE
720
70
2.9
Vinyl chloride
0.24
1
2.4
NE
NE
2
1
Hardness as CaCo3 (Field Measured)
Hardness (mg/L) 20 20 NE NE NE I NE 34.2 NR 17.1 34.2 51.3 51.3
Turbidity (Field Measured)
Turbidity NTU 0.01 50 NE NE I -- 8.13 1 12.9 4.20 11.4 8.63 12.9
Notes:
Units ug/L unless indicated otherwise, Blank cells means Not Detected, NE means Standard Not Established
J = "J-qualified". Defined by the lab as "Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit".
Red Bold Above RL and Applicable Established 213 Std.
Above Established Federal MCL Primary Drinking Water Std.
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
RL = Reporting Limit defined by Pace laboratory as "The lowest concentration value that meets project requirements for quantitative data with
known precision and bias for a specific analyte in a specific matrix"
Receivina surface waters are Stoney Creek (12-72-12) and Ararat River 02-72-(4.5) Both Class C. 03040101 (8-Diait HUC).
NC 2B STD = North Carolina 15A NCAC 02B Water Quality Standards for Surface Waters. Presumed NC SWS adopted the numerical Standard for regulatory compliance purposes.
2B Standards from All Waters (C & SC) or Class C. 2B Standard for cadmium, cooper, lead, nickel and zinc from calculations for acute exposure based on measured hardness values.
EPA NRWQC= EPA Nationally Recommended Water Quality Criteria for Aquatic Life & Human Health.
Nationally Recommended Water Quality Criteria for which NC does not have a Water Quality Standard for one or more uses
' NC ISTV= North Carolina In -Stream Target Value. Established per language in 15A NCAC 02B .0202 & .0208. Contact DWR staff for further information.
MCL= Maximum Contaminant Level. Federal Primary "Drinking Water Standard". Shown for comparison purposes only. Not applicable for regulatory compliance purposes.
A = Acute
c = Chronic
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Appendix A
Field Sampling Parameter Data Sheet(s)

........ . .
Project: Surry Co Closed C&D and Closed MSWLF-Mt. Airy Samplers: /_,� , y„ �-
Sampling
Parameters
Water
Quality
Parameters (Stabilized)
Depth
to
Depth to
p
Water
Volume
Sample
Goes
Dry
Total
Depth
Total
Depth
Comment
DO
Temp.
Specific
TDS
:B
CH4
Monitoring
Purge
Purge
Collect
Collect
Point
Date
Time
Date
Time
Water
(BTOP)
Purged
Type
Durin
Measured
Expecte
s
(mg/L)
ORP
pH
©
Cond.
(mg/L)
.fl
Gas
(BTOP)
(Gal)
g
as
d
(us/cm
F
Vapors
Static
Collection
Purge
expected
MW-1: _
&/2,3
t' L x
5, (0
IW-2
-
-
-
-
-
-
-
-
68.08
-
-
-
-
-
IW-3
52
-
-
-
-
-
-
IW-4
-
-
-
-
-
-
-
-
57
-
-
-
-
-
-
IW-5
-
-
-
-
-
-
-
-
64
MW-6
31
- 3 q
5
; r
IW-6
-
-
-
-
-
-
-
-
56
-
-
-
-
-
-
MW-9
_
46
�r
MW-11
_
17
40
0 r
i Lill
MW-12D
100
-
-
-
-
-
-
-
MW-12S
61
7C : 3
S "la
13, 1
i
51
_
L,L
. 3
MW-13
&' 12,M
:6L!
9
35.78
Gl
15,
MW-14"�
'.
,� 'r
3 4
48.03
. 3
a:
" 0_
iF
MW-15.:
-
56.98
MW-16
blA
36.28
_
12
t
0
MW-17
6v
j 1
15.32
.,{
ff.'
MW-18
-
-
-
-
-
-
-
18.15
-
-
-
-
-
-
-
MW-20
j `,
' 3.-
25.64
�_
6,1
MW-21
��,
` s'
15.41`'�
MW-22
#:�3
,.
OR
'
16.04
�, �.z,.,s
)5,61
?�
MW-23
p
�;.'
S
13
l
17.1
5,
SCALEHOUSE
-
_
222
-
SS B=Stainless Steel Baler, b B=Disposable Baler, P=Low flow Pump, PD=Purged Dry
VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear
NR=No Reading Attempted, NS=No Sample Obtained

Project: SUrN Co Closed C&D over Closed MSWLF & Active Subtitle D Lined- Mt. AIN (cmarea ,urrace vvaiers) od[flfj=a.
Sampling Parameters ZWater Quality Parameters (Stabilized)
Monitoring
Point
SW-1-
SW-2
SW-3
Collect
Date
Collect
Time
—
Visual
Flow
Rate
Lab
Parameters
to be
analyzed for
--• I
Visual
Gua g
e Ht.
_
Sample
Type
Goes
Dry
Durin
9
Pure
-
Total
Depth
Measured
as
ex ected
-
Comments
DO
(mgl�)
ORP
_
pH
Temp.
©
Specific
Cond.
(us/cm
Hardness
(mglL)
_
:a
.Q
�
�—
�,�
CH4
Gas
Vapors
(ppm)
SW-4
I
SW-5-
SWN-1
I
-
-
6a e
-
SWN-2
SWN-3
I
-
-
SWN-4-
SW-C
't
SS B=Stainless Steel Baler, D B=Disposable Baler, P=Low flow Pump, PD=Purgeo Dry
VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear
NR=No Reading Attempted, NS=No Sample Obtained

Appendix B
Laboratory Analysis Reports
Chains of Custody

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
October 15, 2021
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between June 24, 2021 and June 25, 2021.
The results relate only to the samples included in this report. Results reported herein conform to the applicable
TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the
report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Gulf Coast
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
A revised laboratory report is being submitted on 10/15/21 to revise the sample IDS for samples -015 and -016, per client
request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
O*a- `ry] '
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Accounts Payable, Municipal Engineering Services
Jonathan Pfohl, Municipal Engineering Services
Jay Zimmerman, PG, Municipal Engineering Services Co.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Pace Analytical Gulf Coast
7979 Innovation Park Drive, Baton Rouge, LA 70820
Arkansas Certification #: 88-0655
DoD ELAP Certification #: L18-597
Florida Certification #: E87854
Illinois Certification #: 004585
Kansas Certification #: E-10354
Louisiana/LELAP Certification #: 01955
North Carolina Certification #: 618
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Dakota Certification #: R-195
Oklahoma Certification #: 2019-101
South Carolina Certification #: 73006001
Texas Certification #: T104704178-19-11
USDA Soil Permit # P330-19-00209
Virginia Certification #: 460215
Washington Certification #: C929
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92546336001
MW-3R
Water
06/23/2114:27
06/24/21 07:00
92546336002
MW-6
Water
06/23/21 17:26
06/24/21 07:00
92546336003
MW-12S
Water
06/23/2117:20
06/24/21 07:00
92546336004
MW-19
Water
06/23/2113:46
06/24/21 07:00
92546336005
MW-20
Water
06/23/21 17:23
06/24/21 07:00
92546336006
MW-23
Water
06/23/21 14:35
06/24/21 07:00
92546336007
MW-13
Water
06/23/2117:13
06/24/21 07:00
92546336008
MW-17
Water
06/23/2114:00
06/24/21 07:00
92546336009
MW-16
Water
06/23/2114:22
06/24/21 07:00
92546336010
MW-22
Water
06/23/21 13:56
06/24/21 07:00
92546336011
MW-1
Water
06/24/2115:00
06/25/2116:43
92546336012
MW-7
Water
06/25/2110:00
06/25/2116:43
92546336013
MW-9
Water
06/25/2112:00
06/25/2116:43
92546336014
MW-11
Water
06/24/2116:00
06/25/2116:43
92546336015
MW-15
Water
06/24/2111:30
06/25/2116:43
92546336016
MW-14
Water
06/25/2108:30
06/25/2116:43
92546336017
MW-21
Water
06/25/2114:00
06/25/2116:43
92546336018
SCALEHOUSE
Water
06/25/2112:50
06/25/2116:43
92546336019
WSW-2
Water
06/25/2114:00
06/25/2116:43
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
SURRY CLOSED MT AIRY
92546336
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92546336001
MW-3R
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546336002
MW-6
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546336003
MW-12S
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546336004
MW-19
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546336005
MW-20
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546336006
MW-23
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546336007
MW-13
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546336008
MW-17
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546336009
MW-16
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546336010
MW-22
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546336011
MW-1
AM20GAX
TJT
1
GCLA
AM20GAX
TJT
3
GCLA
RSK-175
BMR
1
GCLA
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
SM 2320B-2011
ECH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 125

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9800 Kincey Ave. Suite 100
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SAMPLE ANALYTE COUNT
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
SM 3500-Fe B-2011
DMN
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
AM23G
MOS
10
GCLA
92546336012
MW-7
AM20GAX
TJT
1
GCLA
AM20GAX
TJT
3
GCLA
RSK-175
BMR
1
GCLA
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 3500-Fe B-2011
DMN
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
AM23G
MOS
10
GCLA
92546336013
MW-9
AM20GAX
TJT
1
GCLA
AM20GAX
TJT
3
GCLA
RSK-175
BMR
1
GCLA
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 3500-Fe B-2011
DMN
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
AM23G
MOS
10
GCLA
92546336014
MW-11
AM20GAX
TJT
1
GCLA
AM20GAX
TJT
3
GCLA
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 5 of 125

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
RSK-175
BMR
1
GCLA
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 3500-Fe B-2011
DMN
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
AM23G
MOS
10
GCLA
92546336015 MW-15 AM20GAX
TJT
1
GCLA
AM20GAX
TJT
3
GCLA
RSK-175
BMR
1
GCLA
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 3500-Fe B-2011
DMN
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
AM23G
MOS
10
GCLA
92546336016 MW-14 AM20GAX
TJT
1
GCLA
AM20GAX
TJT
3
GCLA
RSK-175
BMR
1
GCLA
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 3500-Fe B-2011
DMN
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 125

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
SURRY CLOSED MT AIRY
Pace Project No.:
92546336
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
SM 5220D-2011
JP1
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
AM23G
MOS
10
GCLA
92546336017
MW-21
AM20GAX
TJT
1
GCLA
AM20GAX
TJT
3
GCLA
RSK-175
BMR
1
GCLA
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 3500-Fe B-2011
DMN
1
PASI-A
SM 4500-S2D-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
AM23G
MOS
10
GCLA
92546336018
SCALEHOUSE
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546336019
WSW-2
EPA 601 OD
DS
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
GCLA = Pace Analytical Gulf Coast
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 125

lceAnalyircal
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9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-3R Lab ID: 92546336001 Collected: 06/23/21 14:27 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/06/2116:19
07/07/2112:06
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2112:06
7440-38-2
Barium
5.7
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:06
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/2116:19
07/07/2112:06
7440-41-7
Cadmium
0.73J
ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 12:06
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/2116:19
07/07/2112:06
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/06/2116:19
07/07/2112:06
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/06/2116:19
07/07/2112:06
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/06/2116:19
07/07/2112:06
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:06
7440-02-0
Selenium
5.4J
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2112:06
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/2116:19
07/07/2112:06
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/06/2116:19
07/07/2112:06
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/06/2116:19
07/07/2112:06
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
1.0
0.050
1
06/30/2116:15
07/02/2101:31
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/25/21 13:03
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/25/21 13:03
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/25/21 13:03
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/25/21 13:03
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/25/21 13:03
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/25/21 13:03
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/25/21 13:03
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/25/21 13:03
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/25/21 13:03
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/25/21 13:03
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/25/21 13:03
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/25/21 13:03
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/25/21 13:03
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/25/21 13:03
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/25/21 13:03
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/25/21 13:03
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/25/21 13:03
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/25/21 13:03
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/25/21 13:03
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/25/21 13:03
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/25/21 13:03
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/25/21 13:03
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/25/21 13:03
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/25/21 13:03
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
v2
Page 8 of 125

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-3R Lab ID: 92546336001 Collected: 06/23/21 14:27 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/25/21 13:03
156-59-2
ND
ug/L
1.0
0.40
1
06/25/21 13:03
156-60-5
ND
ug/L
1.0
0.36
1
06/25/21 13:03
78-87-5
ND
ug/L
1.0
0.36
1
06/25/21 13:03
10061-01-5
ND
ug/L
1.0
0.36
1
06/25/21 13:03
10061-02-6
ND
ug/L
150
38.7
1
06/25/21 13:03
123-91-1
ND
ug/L
1.0
0.30
1
06/25/21 13:03
100-41-4
ND
ug/L
5.0
0.48
1
06/25/21 13:03
591-78-6
ND
ug/L
20.0
9.7
1
06/25/21 13:03
74-88-4
ND
ug/L
5.0
2.0
1
06/25/21 13:03
75-09-2
ND
ug/L
5.0
2.7
1
06/25/21 13:03
108-10-1
ND
ug/L
1.0
0.29
1
06/25/21 13:03
100-42-5
ND
ug/L
1.0
0.31
1
06/25/21 13:03
630-20-6
ND
ug/L
1.0
0.22
1
06/25/21 13:03
79-34-5
ND
ug/L
1.0
0.29
1
06/25/21 13:03
127-18-4
ND
ug/L
1.0
0.48
1
06/25/21 13:03
108-88-3
ND
ug/L
1.0
0.33
1
06/25/21 13:03
71-55-6
ND
ug/L
1.0
0.32
1
06/25/21 13:03
79-00-5
ND
ug/L
1.0
0.38
1
06/25/21 13:03
79-01-6
ND
ug/L
1.0
0.30
1
06/25/21 13:03
75-69-4
ND
ug/L
1.0
0.26
1
06/25/21 13:03
96-18-4
ND
ug/L
2.0
1.3
1
06/25/21 13:03
108-05-4
ND
ug/L
1.0
0.39
1
06/25/21 13:03
75-01-4
ND
ug/L
1.0
0.34
1
06/25/21 13:03
1330-20-7
98
%
70-130
1
06/25/21 13:03
460-00-4
90
%
70-130
1
06/25/21 13:03
17060-07-0
104
%
70-130
1
06/25/21 13:03
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 125

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-6 Lab ID: 92546336002 Collected: 06/23/21 17:26 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/06/21 16:19
07/07/21 12:26
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 12:26
7440-38-2
Barium
73.0
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 12:26
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/21 16:19
07/07/21 12:26
7440-41-7
Cadmium
0.72J
ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 12:26
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/21 16:19
07/07/21 12:26
7440-47-3
Cobalt
30.6
ug/L
5.0
3.6
1
07/06/21 16:19
07/07/21 12:26
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/06/21 16:19
07/07/21 12:26
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/06/21 16:19
07/07/21 12:26
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 12:26
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 12:26
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/21 16:19
07/07/21 12:26
7440-22-4
Vanadium
4.0.1
ug/L
5.0
3.9
1
07/06/21 16:19
07/07/21 12:26
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/06/21 16:19
07/07/21 12:26
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
0.64J
ug/L
1.0
0.050
1
06/30/2116:15
07/02/2101:52
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/25/21 13:20
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/25/21 13:20
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/25/21 13:20
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/25/21 13:20
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/25/21 13:20
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/25/21 13:20
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/25/21 13:20
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/25/21 13:20
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/25/21 13:20
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/25/21 13:20
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/25/21 13:20
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/25/21 13:20
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/25/21 13:20
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/25/21 13:20
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/25/21 13:20
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/25/21 13:20
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/25/21 13:20
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/25/21 13:20
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/25/21 13:20
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/25/21 13:20
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/25/21 13:20
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/25/21 13:20
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/25/21 13:20
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/25/21 13:20
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
v2
Page 10 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-6 Lab ID: 92546336002 Collected: 06/23/21 17:26 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/25/21 13:20
156-59-2
ND
ug/L
1.0
0.40
1
06/25/21 13:20
156-60-5
ND
ug/L
1.0
0.36
1
06/25/21 13:20
78-87-5
ND
ug/L
1.0
0.36
1
06/25/21 13:20
10061-01-5
ND
ug/L
1.0
0.36
1
06/25/21 13:20
10061-02-6
ND
ug/L
150
38.7
1
06/25/21 13:20
123-91-1
ND
ug/L
1.0
0.30
1
06/25/21 13:20
100-41-4
ND
ug/L
5.0
0.48
1
06/25/21 13:20
591-78-6
ND
ug/L
20.0
9.7
1
06/25/21 13:20
74-88-4
ND
ug/L
5.0
2.0
1
06/25/21 13:20
75-09-2
ND
ug/L
5.0
2.7
1
06/25/21 13:20
108-10-1
ND
ug/L
1.0
0.29
1
06/25/21 13:20
100-42-5
ND
ug/L
1.0
0.31
1
06/25/21 13:20
630-20-6
ND
ug/L
1.0
0.22
1
06/25/21 13:20
79-34-5
ND
ug/L
1.0
0.29
1
06/25/21 13:20
127-18-4
ND
ug/L
1.0
0.48
1
06/25/21 13:20
108-88-3
ND
ug/L
1.0
0.33
1
06/25/21 13:20
71-55-6
ND
ug/L
1.0
0.32
1
06/25/21 13:20
79-00-5
ND
ug/L
1.0
0.38
1
06/25/21 13:20
79-01-6
ND
ug/L
1.0
0.30
1
06/25/21 13:20
75-69-4
ND
ug/L
1.0
0.26
1
06/25/21 13:20
96-18-4
ND
ug/L
2.0
1.3
1
06/25/21 13:20
108-05-4
ND
ug/L
1.0
0.39
1
06/25/21 13:20
75-01-4
ND
ug/L
1.0
0.34
1
06/25/21 13:20
1330-20-7
97
%
70-130
1
06/25/21 13:20
460-00-4
89
%
70-130
1
06/25/21 13:20
17060-07-0
104
%
70-130
1
06/25/21 13:20
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-12S Lab ID: 92546336003 Collected: 06/23/21 17:20 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/06/2116:19
07/07/2112:29
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2112:29
7440-38-2
Barium
12.9
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:29
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/2116:19
07/07/2112:29
7440-41-7
Cadmium
1.8
ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 12:29
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/2116:19
07/07/2112:29
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/06/2116:19
07/07/2112:29
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/06/2116:19
07/07/2112:29
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/06/2116:19
07/07/2112:29
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:29
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2112:29
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/2116:19
07/07/2112:29
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/06/2116:19
07/07/2112:29
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/06/2116:19
07/07/2112:29
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
1.0
0.050
1
06/30/2116:15
07/02/2101:56
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/25/21 13:38
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/25/21 13:38
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/25/21 13:38
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/25/21 13:38
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/25/21 13:38
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/25/21 13:38
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/25/21 13:38
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/25/21 13:38
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/25/21 13:38
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/25/21 13:38
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/25/21 13:38
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/25/21 13:38
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/25/21 13:38
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/25/21 13:38
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/25/21 13:38
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/25/21 13:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/25/21 13:38
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/25/21 13:38
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/25/21 13:38
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/25/21 13:38
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/25/21 13:38
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/25/21 13:38
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/25/21 13:38
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/25/21 13:38
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
v2
Page 12 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-12S Lab ID: 92546336003 Collected: 06/23/21 17:20 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/25/21 13:38
156-59-2
ND
ug/L
1.0
0.40
1
06/25/21 13:38
156-60-5
ND
ug/L
1.0
0.36
1
06/25/21 13:38
78-87-5
ND
ug/L
1.0
0.36
1
06/25/21 13:38
10061-01-5
ND
ug/L
1.0
0.36
1
06/25/21 13:38
10061-02-6
ND
ug/L
150
38.7
1
06/25/21 13:38
123-91-1
ND
ug/L
1.0
0.30
1
06/25/21 13:38
100-41-4
ND
ug/L
5.0
0.48
1
06/25/21 13:38
591-78-6
ND
ug/L
20.0
9.7
1
06/25/21 13:38
74-88-4
ND
ug/L
5.0
2.0
1
06/25/21 13:38
75-09-2
ND
ug/L
5.0
2.7
1
06/25/21 13:38
108-10-1
ND
ug/L
1.0
0.29
1
06/25/21 13:38
100-42-5
ND
ug/L
1.0
0.31
1
06/25/21 13:38
630-20-6
ND
ug/L
1.0
0.22
1
06/25/21 13:38
79-34-5
ND
ug/L
1.0
0.29
1
06/25/21 13:38
127-18-4
ND
ug/L
1.0
0.48
1
06/25/21 13:38
108-88-3
ND
ug/L
1.0
0.33
1
06/25/21 13:38
71-55-6
ND
ug/L
1.0
0.32
1
06/25/21 13:38
79-00-5
ND
ug/L
1.0
0.38
1
06/25/21 13:38
79-01-6
ND
ug/L
1.0
0.30
1
06/25/21 13:38
75-69-4
ND
ug/L
1.0
0.26
1
06/25/21 13:38
96-18-4
ND
ug/L
2.0
1.3
1
06/25/21 13:38
108-05-4
ND
ug/L
1.0
0.39
1
06/25/21 13:38
75-01-4
ND
ug/L
1.0
0.34
1
06/25/21 13:38
1330-20-7
93
%
70-130
1
06/25/21 13:38
460-00-4
88
%
70-130
1
06/25/21 13:38
17060-07-0
101
%
70-130
1
06/25/21 13:38
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-19 Lab ID: 92546336004 Collected: 06/23/21 13:46 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/06/2116:19
07/07/2112:32
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2112:32
7440-38-2
Barium
19.4
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:32
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/2116:19
07/07/2112:32
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/06/2116:19
07/07/2112:32
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/2116:19
07/07/2112:32
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/06/2116:19
07/07/2112:32
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/06/2116:19
07/07/2112:32
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/06/2116:19
07/07/2112:32
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:32
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2112:32
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/2116:19
07/07/2112:32
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/06/2116:19
07/07/2112:32
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/06/2116:19
07/07/2112:32
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
1.0
0.050
1
06/30/2116:15
07/02/2102:09
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/25/21 13:55
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/25/21 13:55
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/25/21 13:55
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/25/21 13:55
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/25/21 13:55
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/25/21 13:55
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/25/21 13:55
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/25/21 13:55
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/25/21 13:55
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/25/21 13:55
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/25/21 13:55
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/25/21 13:55
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/25/21 13:55
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/25/21 13:55
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/25/21 13:55
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/25/21 13:55
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/25/21 13:55
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/25/21 13:55
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/25/21 13:55
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/25/21 13:55
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/25/21 13:55
110-57-6
1,1-Dichloroethane
0.43J
ug/L
1.0
0.37
1
06/25/21 13:55
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/25/21 13:55
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/25/21 13:55
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
v2
Page 14 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-19 Lab ID: 92546336004 Collected: 06/23/21 13:46 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
0.68J
ug/L
1.0
0.38
1
06/25/21 13:55
156-59-2
ND
ug/L
1.0
0.40
1
06/25/21 13:55
156-60-5
ND
ug/L
1.0
0.36
1
06/25/21 13:55
78-87-5
ND
ug/L
1.0
0.36
1
06/25/21 13:55
10061-01-5
ND
ug/L
1.0
0.36
1
06/25/21 13:55
10061-02-6
ND
ug/L
150
38.7
1
06/25/21 13:55
123-91-1
ND
ug/L
1.0
0.30
1
06/25/21 13:55
100-41-4
ND
ug/L
5.0
0.48
1
06/25/21 13:55
591-78-6
ND
ug/L
20.0
9.7
1
06/25/21 13:55
74-88-4
ND
ug/L
5.0
2.0
1
06/25/21 13:55
75-09-2
ND
ug/L
5.0
2.7
1
06/25/21 13:55
108-10-1
ND
ug/L
1.0
0.29
1
06/25/21 13:55
100-42-5
ND
ug/L
1.0
0.31
1
06/25/21 13:55
630-20-6
ND
ug/L
1.0
0.22
1
06/25/21 13:55
79-34-5
ND
ug/L
1.0
0.29
1
06/25/21 13:55
127-18-4
ND
ug/L
1.0
0.48
1
06/25/21 13:55
108-88-3
ND
ug/L
1.0
0.33
1
06/25/21 13:55
71-55-6
ND
ug/L
1.0
0.32
1
06/25/21 13:55
79-00-5
ND
ug/L
1.0
0.38
1
06/25/21 13:55
79-01-6
ND
ug/L
1.0
0.30
1
06/25/21 13:55
75-69-4
ND
ug/L
1.0
0.26
1
06/25/21 13:55
96-18-4
ND
ug/L
2.0
1.3
1
06/25/21 13:55
108-05-4
ND
ug/L
1.0
0.39
1
06/25/21 13:55
75-01-4
ND
ug/L
1.0
0.34
1
06/25/21 13:55
1330-20-7
95
%
70-130
1
06/25/21 13:55
460-00-4
91
%
70-130
1
06/25/21 13:55
17060-07-0
103
%
70-130
1
06/25/21 13:55
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-20 Lab ID: 92546336005 Collected: 06/23/21 17:23 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/06/21 16:19
07/07/21 12:35
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 12:35
7440-38-2
Barium
50.4
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 12:35
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/21 16:19
07/07/21 12:35
7440-41-7
Cadmium
1.9
ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 12:35
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/21 16:19
07/07/21 12:35
7440-47-3
Cobalt
165
ug/L
5.0
3.6
1
07/06/21 16:19
07/07/21 12:35
7440-48-4
Copper
ND
ug/L
25.0
21.3
5
07/06/21 16:19
07/07/2118:49
7440-50-8 D3
Lead
ND
ug/L
5.0
4.5
1
07/06/21 16:19
07/07/21 12:35
7439-92-1
Nickel
7.4
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 12:35
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 12:35
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/21 16:19
07/07/21 12:35
7440-22-4
Vanadium
4.2J
ug/L
5.0
3.9
1
07/06/21 16:19
07/07/21 12:35
7440-62-2
Zinc
13.3
ug/L
10.0
9.5
1
07/06/21 16:19
07/07/21 12:35
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
0.811
ug/L
1.0
0.050
1
06/30/2116:15 07/02/2102:13
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
06/25/21 14:12
67-64-1
ND
ug/L
10.0
1.8
1
06/25/21 14:12
107-13-1
1.3
ug/L
1.0
0.34
1
06/25/21 14:12
71-43-2
ND
ug/L
1.0
0.47
1
06/25/21 14:12
74-97-5
ND
ug/L
1.0
0.31
1
06/25/21 14:12
75-27-4
ND
ug/L
1.0
0.34
1
06/25/21 14:12
75-25-2
ND
ug/L
2.0
1.7
1
06/25/21 14:12
74-83-9
ND
ug/L
5.0
4.0
1
06/25/21 14:12
78-93-3
ND
ug/L
2.0
0.73
1
06/25/21 14:12
75-15-0
ND
ug/L
1.0
0.33
1
06/25/21 14:12
56-23-5
ND
ug/L
1.0
0.28
1
06/25/21 14:12
108-90-7
0.81J
ug/L
1.0
0.65
1
06/25/21 14:12
75-00-3
ND
ug/L
5.0
1.6
1
06/25/21 14:12
67-66-3
ND
ug/L
1.0
0.54
1
06/25/21 14:12
74-87-3
ND
ug/L
2.0
0.34
1
06/25/21 14:12
96-12-8
ND
ug/L
1.0
0.36
1
06/25/21 14:12
124-48-1
ND
ug/L
1.0
0.27
1
06/25/21 14:12
106-93-4
ND
ug/L
1.0
0.39
1
06/25/21 14:12
74-95-3
1.8
ug/L
1.0
0.34
1
06/25/21 14:12
95-50-1
ND
ug/L
1.0
0.33
1
06/25/21 14:12
106-46-7
ND
ug/L
1.0
0.56
1
06/25/21 14:12
110-57-6
1.1
ug/L
1.0
0.37
1
06/25/21 14:12
75-34-3
ND
ug/L
1.0
0.32
1
06/25/21 14:12
107-06-2
ND
ug/L
1.0
0.35
1
06/25/21 14:12
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
Page 16 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-20 Lab ID: 92546336005 Collected: 06/23/21 17:23 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
7.6
ug/L
1.0
0.38
1
06/25/21 14:12
156-59-2
ND
ug/L
1.0
0.40
1
06/25/21 14:12
156-60-5
ND
ug/L
1.0
0.36
1
06/25/21 14:12
78-87-5
ND
ug/L
1.0
0.36
1
06/25/21 14:12
10061-01-5
ND
ug/L
1.0
0.36
1
06/25/21 14:12
10061-02-6
ND
ug/L
150
38.7
1
06/25/21 14:12
123-91-1
ND
ug/L
1.0
0.30
1
06/25/21 14:12
100-41-4
ND
ug/L
5.0
0.48
1
06/25/21 14:12
591-78-6
ND
ug/L
20.0
9.7
1
06/25/21 14:12
74-88-4
ND
ug/L
5.0
2.0
1
06/25/21 14:12
75-09-2
ND
ug/L
5.0
2.7
1
06/25/21 14:12
108-10-1
ND
ug/L
1.0
0.29
1
06/25/21 14:12
100-42-5
ND
ug/L
1.0
0.31
1
06/25/21 14:12
630-20-6
ND
ug/L
1.0
0.22
1
06/25/21 14:12
79-34-5
ND
ug/L
1.0
0.29
1
06/25/21 14:12
127-18-4
ND
ug/L
1.0
0.48
1
06/25/21 14:12
108-88-3
ND
ug/L
1.0
0.33
1
06/25/21 14:12
71-55-6
ND
ug/L
1.0
0.32
1
06/25/21 14:12
79-00-5
ND
ug/L
1.0
0.38
1
06/25/21 14:12
79-01-6
ND
ug/L
1.0
0.30
1
06/25/21 14:12
75-69-4
ND
ug/L
1.0
0.26
1
06/25/21 14:12
96-18-4
ND
ug/L
2.0
1.3
1
06/25/21 14:12
108-05-4
3.7
ug/L
1.0
0.39
1
06/25/21 14:12
75-01-4
ND
ug/L
1.0
0.34
1
06/25/21 14:12
1330-20-7
99
%
70-130
1
06/25/21 14:12
460-00-4
91
%
70-130
1
06/25/21 14:12
17060-07-0
104
%
70-130
1
06/25/21 14:12
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-23 Lab ID: 92546336006 Collected: 06/23/21 14:35 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/06/2116:19
07/07/2112:39
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2112:39
7440-38-2
Barium
31.2
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:39
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/2116:19
07/07/2112:39
7440-41-7
Cadmium
0.85J
ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 12:39
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/2116:19
07/07/2112:39
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/06/2116:19
07/07/2112:39
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/06/2116:19
07/07/2112:39
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/06/2116:19
07/07/2112:39
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:39
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2112:39
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/2116:19
07/07/2112:39
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/06/2116:19
07/07/2112:39
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/06/2116:19
07/07/2112:39
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
1.0
0.050
1
06/30/2116:15
07/02/2102:17
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/25/21 14:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/25/21 14:30
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/25/21 14:30
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/25/21 14:30
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/25/21 14:30
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/25/21 14:30
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/25/21 14:30
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/25/21 14:30
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/25/21 14:30
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/25/21 14:30
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/25/21 14:30
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/25/21 14:30
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/25/21 14:30
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/25/21 14:30
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/25/21 14:30
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/25/21 14:30
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/25/21 14:30
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/25/21 14:30
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/25/21 14:30
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/25/21 14:30
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/25/21 14:30
110-57-6
1,1-Dichloroethane
0.38J
ug/L
1.0
0.37
1
06/25/21 14:30
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/25/21 14:30
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/25/21 14:30
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
v2
Page 18 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-23 Lab ID: 92546336006 Collected: 06/23/21 14:35 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
0.74J
ug/L
1.0
0.38
1
06/25/21 14:30
156-59-2
ND
ug/L
1.0
0.40
1
06/25/21 14:30
156-60-5
ND
ug/L
1.0
0.36
1
06/25/21 14:30
78-87-5
ND
ug/L
1.0
0.36
1
06/25/21 14:30
10061-01-5
ND
ug/L
1.0
0.36
1
06/25/21 14:30
10061-02-6
ND
ug/L
150
38.7
1
06/25/21 14:30
123-91-1
ND
ug/L
1.0
0.30
1
06/25/21 14:30
100-41-4
ND
ug/L
5.0
0.48
1
06/25/21 14:30
591-78-6
ND
ug/L
20.0
9.7
1
06/25/21 14:30
74-88-4
ND
ug/L
5.0
2.0
1
06/25/21 14:30
75-09-2
ND
ug/L
5.0
2.7
1
06/25/21 14:30
108-10-1
ND
ug/L
1.0
0.29
1
06/25/21 14:30
100-42-5
ND
ug/L
1.0
0.31
1
06/25/21 14:30
630-20-6
ND
ug/L
1.0
0.22
1
06/25/21 14:30
79-34-5
ND
ug/L
1.0
0.29
1
06/25/21 14:30
127-18-4
ND
ug/L
1.0
0.48
1
06/25/21 14:30
108-88-3
ND
ug/L
1.0
0.33
1
06/25/21 14:30
71-55-6
ND
ug/L
1.0
0.32
1
06/25/21 14:30
79-00-5
ND
ug/L
1.0
0.38
1
06/25/21 14:30
79-01-6
ND
ug/L
1.0
0.30
1
06/25/21 14:30
75-69-4
ND
ug/L
1.0
0.26
1
06/25/21 14:30
96-18-4
ND
ug/L
2.0
1.3
1
06/25/21 14:30
108-05-4
ND
ug/L
1.0
0.39
1
06/25/21 14:30
75-01-4
ND
ug/L
1.0
0.34
1
06/25/21 14:30
1330-20-7
97
%
70-130
1
06/25/21 14:30
460-00-4
97
%
70-130
1
06/25/21 14:30
17060-07-0
108
%
70-130
1
06/25/21 14:30
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-13 Lab ID: 92546336007 Collected: 06/23/21 17:13 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/06/21 16:19
07/07/21 12:42
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 12:42
7440-38-2
Barium
66.2
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 12:42
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/21 16:19
07/07/21 12:42
7440-41-7
Cadmium
4.8
ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 12:42
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/21 16:19
07/07/21 12:42
7440-47-3
Cobalt
12.9
ug/L
5.0
3.6
1
07/06/21 16:19
07/07/21 12:42
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/06/21 16:19
07/07/21 12:42
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/06/21 16:19
07/07/21 12:42
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 12:42
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 12:42
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/21 16:19
07/07/21 12:42
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/06/21 16:19
07/07/21 12:42
7440-62-2
Zinc
15.2
ug/L
10.0
9.5
1
07/06/21 16:19
07/07/21 12:42
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
0.088J
ug/L
1.0
0.050
1
06/30/2116:15
07/02/2102:21
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/25/21 14:47
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/25/21 14:47
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/25/21 14:47
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/25/21 14:47
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/25/21 14:47
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/25/21 14:47
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/25/21 14:47
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/25/21 14:47
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/25/21 14:47
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/25/21 14:47
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/25/21 14:47
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/25/21 14:47
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/25/21 14:47
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/25/21 14:47
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/25/21 14:47
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/25/21 14:47
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/25/21 14:47
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/25/21 14:47
74-95-3
1,2-Dichlorobenzene
0.40J
ug/L
1.0
0.34
1
06/25/21 14:47
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/25/21 14:47
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/25/21 14:47
110-57-6
1,1-Dichloroethane
0.86J
ug/L
1.0
0.37
1
06/25/21 14:47
75-34-3
1,2-Dichloroethane
0.84J
ug/L
1.0
0.32
1
06/25/21 14:47
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/25/21 14:47
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
v2
Page 20 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-13 Lab ID: 92546336007 Collected: 06/23/21 17:13 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
12.1
ug/L
1.0
0.38
1
06/25/21 14:47
156-59-2
ND
ug/L
1.0
0.40
1
06/25/21 14:47
156-60-5
ND
ug/L
1.0
0.36
1
06/25/21 14:47
78-87-5
ND
ug/L
1.0
0.36
1
06/25/21 14:47
10061-01-5
ND
ug/L
1.0
0.36
1
06/25/21 14:47
10061-02-6
ND
ug/L
150
38.7
1
06/25/21 14:47
123-91-1
ND
ug/L
1.0
0.30
1
06/25/21 14:47
100-41-4
ND
ug/L
5.0
0.48
1
06/25/21 14:47
591-78-6
ND
ug/L
20.0
9.7
1
06/25/21 14:47
74-88-4
ND
ug/L
5.0
2.0
1
06/25/21 14:47
75-09-2
ND
ug/L
5.0
2.7
1
06/25/21 14:47
108-10-1
ND
ug/L
1.0
0.29
1
06/25/21 14:47
100-42-5
ND
ug/L
1.0
0.31
1
06/25/21 14:47
630-20-6
ND
ug/L
1.0
0.22
1
06/25/21 14:47
79-34-5
ND
ug/L
1.0
0.29
1
06/25/21 14:47
127-18-4
1.9
ug/L
1.0
0.48
1
06/25/21 14:47
108-88-3
ND
ug/L
1.0
0.33
1
06/25/21 14:47
71-55-6
ND
ug/L
1.0
0.32
1
06/25/21 14:47
79-00-5
ND
ug/L
1.0
0.38
1
06/25/21 14:47
79-01-6
ND
ug/L
1.0
0.30
1
06/25/21 14:47
75-69-4
ND
ug/L
1.0
0.26
1
06/25/21 14:47
96-18-4
ND
ug/L
2.0
1.3
1
06/25/21 14:47
108-05-4
ND
ug/L
1.0
0.39
1
06/25/21 14:47
75-01-4
ND
ug/L
1.0
0.34
1
06/25/21 14:47
1330-20-7
98
%
70-130
1
06/25/21 14:47
460-00-4
96
%
70-130
1
06/25/21 14:47
17060-07-0
102
%
70-130
1
06/25/21 14:47
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-17 Lab ID: 92546336008 Collected: 06/23/21 14:00 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/06/2116:19
07/07/2112:45
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2112:45
7440-38-2
Barium
9.7
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:45
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/2116:19
07/07/2112:45
7440-41-7
Cadmium
0.46J
ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 12:45
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/2116:19
07/07/2112:45
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/06/2116:19
07/07/2112:45
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/06/2116:19
07/07/2112:45
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/06/2116:19
07/07/2112:45
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:45
7440-02-0
Selenium
6.5.1
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2112:45
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/2116:19
07/07/2112:45
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/06/2116:19
07/07/2112:45
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/06/2116:19
07/07/2112:45
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
1.0
0.050
1
06/30/2116:15
07/02/2102:25
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/25/21 15:04
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/25/21 15:04
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/25/21 15:04
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/25/21 15:04
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/25/21 15:04
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/25/21 15:04
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/25/21 15:04
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/25/21 15:04
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/25/21 15:04
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/25/21 15:04
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/25/21 15:04
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/25/21 15:04
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/25/21 15:04
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/25/21 15:04
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/25/21 15:04
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/25/21 15:04
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/25/21 15:04
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/25/21 15:04
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/25/21 15:04
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/25/21 15:04
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/25/21 15:04
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/25/21 15:04
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/25/21 15:04
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/25/21 15:04
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
v2
Page 22 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-17 Lab ID: 92546336008 Collected: 06/23/21 14:00 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/25/21 15:04
156-59-2
ND
ug/L
1.0
0.40
1
06/25/21 15:04
156-60-5
ND
ug/L
1.0
0.36
1
06/25/21 15:04
78-87-5
ND
ug/L
1.0
0.36
1
06/25/21 15:04
10061-01-5
ND
ug/L
1.0
0.36
1
06/25/21 15:04
10061-02-6
ND
ug/L
150
38.7
1
06/25/21 15:04
123-91-1
ND
ug/L
1.0
0.30
1
06/25/21 15:04
100-41-4
ND
ug/L
5.0
0.48
1
06/25/21 15:04
591-78-6
ND
ug/L
20.0
9.7
1
06/25/21 15:04
74-88-4
ND
ug/L
5.0
2.0
1
06/25/21 15:04
75-09-2
ND
ug/L
5.0
2.7
1
06/25/21 15:04
108-10-1
ND
ug/L
1.0
0.29
1
06/25/21 15:04
100-42-5
ND
ug/L
1.0
0.31
1
06/25/21 15:04
630-20-6
ND
ug/L
1.0
0.22
1
06/25/21 15:04
79-34-5
ND
ug/L
1.0
0.29
1
06/25/21 15:04
127-18-4
ND
ug/L
1.0
0.48
1
06/25/21 15:04
108-88-3
ND
ug/L
1.0
0.33
1
06/25/21 15:04
71-55-6
ND
ug/L
1.0
0.32
1
06/25/21 15:04
79-00-5
ND
ug/L
1.0
0.38
1
06/25/21 15:04
79-01-6
ND
ug/L
1.0
0.30
1
06/25/21 15:04
75-69-4
ND
ug/L
1.0
0.26
1
06/25/21 15:04
96-18-4
ND
ug/L
2.0
1.3
1
06/25/21 15:04
108-05-4
ND
ug/L
1.0
0.39
1
06/25/21 15:04
75-01-4
ND
ug/L
1.0
0.34
1
06/25/21 15:04
1330-20-7
95
%
70-130
1
06/25/21 15:04
460-00-4
88
%
70-130
1
06/25/21 15:04
17060-07-0
104
%
70-130
1
06/25/21 15:04
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-16 Lab ID: 92546336009 Collected: 06/23/21 14:22 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
4.4J
ug/L
5.0
3.0
1
07/06/21 16:19
07/07/21 12:48
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 12:48
7440-38-2
Barium
115
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 12:48
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/21 16:19
07/07/21 12:48
7440-41-7
Cadmium
2.0
ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 12:48
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/21 16:19
07/07/21 12:48
7440-47-3
Cobalt
541
ug/L
5.0
3.6
1
07/06/21 16:19
07/07/21 12:48
7440-48-4
Copper
ND
ug/L
25.0
21.3
5
07/06/21 16:19
07/07/2118:53
7440-50-8 D3
Lead
ND
ug/L
5.0
4.5
1
07/06/21 16:19
07/07/21 12:48
7439-92-1
Nickel
24.0
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 12:48
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 12:48
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/21 16:19
07/07/21 12:48
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/06/21 16:19
07/07/21 12:48
7440-62-2
Zinc
17.8
ug/L
10.0
9.5
1
07/06/21 16:19
07/07/21 12:48
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
0.38J
ug/L
1.0
0.050
1
06/30/21 16:15 07/02/2102:29
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
06/25/21 15:22
67-64-1
ND
ug/L
10.0
1.8
1
06/25/21 15:22
107-13-1
1.4
ug/L
1.0
0.34
1
06/25/21 15:22
71-43-2
ND
ug/L
1.0
0.47
1
06/25/21 15:22
74-97-5
ND
ug/L
1.0
0.31
1
06/25/21 15:22
75-27-4
ND
ug/L
1.0
0.34
1
06/25/21 15:22
75-25-2
ND
ug/L
2.0
1.7
1
06/25/21 15:22
74-83-9
ND
ug/L
5.0
4.0
1
06/25/21 15:22
78-93-3
ND
ug/L
2.0
0.73
1
06/25/21 15:22
75-15-0
ND
ug/L
1.0
0.33
1
06/25/21 15:22
56-23-5
ND
ug/L
1.0
0.28
1
06/25/21 15:22
108-90-7
ND
ug/L
1.0
0.65
1
06/25/21 15:22
75-00-3
ND
ug/L
5.0
1.6
1
06/25/21 15:22
67-66-3
ND
ug/L
1.0
0.54
1
06/25/21 15:22
74-87-3
ND
ug/L
2.0
0.34
1
06/25/21 15:22
96-12-8
ND
ug/L
1.0
0.36
1
06/25/21 15:22
124-48-1
ND
ug/L
1.0
0.27
1
06/25/21 15:22
106-93-4
ND
ug/L
1.0
0.39
1
06/25/21 15:22
74-95-3
0.63J
ug/L
1.0
0.34
1
06/25/21 15:22
95-50-1
ND
ug/L
1.0
0.33
1
06/25/21 15:22
106-46-7
ND
ug/L
1.0
0.56
1
06/25/21 15:22
110-57-6
0.591
ug/L
1.0
0.37
1
06/25/21 15:22
75-34-3
1.5
ug/L
1.0
0.32
1
06/25/21 15:22
107-06-2
ND
ug/L
1.0
0.35
1
06/25/21 15:22
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
Page 24 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-16 Lab ID: 92546336009 Collected: 06/23/21 14:22 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
12.4
ug/L
1.0
0.38
1
06/25/21 15:22
156-59-2
ND
ug/L
1.0
0.40
1
06/25/21 15:22
156-60-5
0.74J
ug/L
1.0
0.36
1
06/25/21 15:22
78-87-5
ND
ug/L
1.0
0.36
1
06/25/21 15:22
10061-01-5
ND
ug/L
1.0
0.36
1
06/25/21 15:22
10061-02-6
ND
ug/L
150
38.7
1
06/25/21 15:22
123-91-1
ND
ug/L
1.0
0.30
1
06/25/21 15:22
100-41-4
ND
ug/L
5.0
0.48
1
06/25/21 15:22
591-78-6
ND
ug/L
20.0
9.7
1
06/25/21 15:22
74-88-4
ND
ug/L
5.0
2.0
1
06/25/21 15:22
75-09-2
ND
ug/L
5.0
2.7
1
06/25/21 15:22
108-10-1
ND
ug/L
1.0
0.29
1
06/25/21 15:22
100-42-5
ND
ug/L
1.0
0.31
1
06/25/21 15:22
630-20-6
ND
ug/L
1.0
0.22
1
06/25/21 15:22
79-34-5
ND
ug/L
1.0
0.29
1
06/25/21 15:22
127-18-4
ND
ug/L
1.0
0.48
1
06/25/21 15:22
108-88-3
ND
ug/L
1.0
0.33
1
06/25/21 15:22
71-55-6
ND
ug/L
1.0
0.32
1
06/25/21 15:22
79-00-5
ND
ug/L
1.0
0.38
1
06/25/21 15:22
79-01-6
ND
ug/L
1.0
0.30
1
06/25/21 15:22
75-69-4
ND
ug/L
1.0
0.26
1
06/25/21 15:22
96-18-4
ND
ug/L
2.0
1.3
1
06/25/21 15:22
108-05-4
1.7
ug/L
1.0
0.39
1
06/25/21 15:22
75-01-4
ND
ug/L
1.0
0.34
1
06/25/21 15:22
1330-20-7
94
%
70-130
1
06/25/21 15:22
460-00-4
90
%
70-130
1
06/25/21 15:22
17060-07-0
104
%
70-130
1
06/25/21 15:22
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-22 Lab ID: 92546336010 Collected: 06/23/21 13:56 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/06/21 16:19
07/07/21 12:52
7440-36-0
Arsenic
6.5J
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 12:52
7440-38-2
Barium
75.2
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 12:52
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/21 16:19
07/07/21 12:52
7440-41-7
Cadmium
2.3
ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 12:52
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/21 16:19
07/07/21 12:52
7440-47-3
Cobalt
150
ug/L
5.0
3.6
1
07/06/21 16:19
07/07/21 12:52
7440-48-4
Copper
ND
ug/L
25.0
21.3
5
07/06/21 16:19
07/07/2118:56
7440-50-8 D3
Lead
ND
ug/L
5.0
4.5
1
07/06/21 16:19
07/07/21 12:52
7439-92-1
Nickel
10.7
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 12:52
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 12:52
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/21 16:19
07/07/21 12:52
7440-22-4
Vanadium
4.2.1
ug/L
5.0
3.9
1
07/06/21 16:19
07/07/21 12:52
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/06/21 16:19
07/07/21 12:52
7440-66-6
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
0.17J
ug/L
1.0
0.050
1
06/30/21 16:15 07/02/2102:34
7440-28-0
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
06/25/21 15:39
67-64-1
ND
ug/L
10.0
1.8
1
06/25/21 15:39
107-13-1
0.36J
ug/L
1.0
0.34
1
06/25/21 15:39
71-43-2
ND
ug/L
1.0
0.47
1
06/25/21 15:39
74-97-5
ND
ug/L
1.0
0.31
1
06/25/21 15:39
75-27-4
ND
ug/L
1.0
0.34
1
06/25/21 15:39
75-25-2
ND
ug/L
2.0
1.7
1
06/25/21 15:39
74-83-9
ND
ug/L
5.0
4.0
1
06/25/21 15:39
78-93-3
ND
ug/L
2.0
0.73
1
06/25/21 15:39
75-15-0
ND
ug/L
1.0
0.33
1
06/25/21 15:39
56-23-5
ND
ug/L
1.0
0.28
1
06/25/21 15:39
108-90-7
ND
ug/L
1.0
0.65
1
06/25/21 15:39
75-00-3
ND
ug/L
5.0
1.6
1
06/25/21 15:39
67-66-3
ND
ug/L
1.0
0.54
1
06/25/21 15:39
74-87-3
ND
ug/L
2.0
0.34
1
06/25/21 15:39
96-12-8
ND
ug/L
1.0
0.36
1
06/25/21 15:39
124-48-1
ND
ug/L
1.0
0.27
1
06/25/21 15:39
106-93-4
ND
ug/L
1.0
0.39
1
06/25/21 15:39
74-95-3
0.39J
ug/L
1.0
0.34
1
06/25/21 15:39
95-50-1
ND
ug/L
1.0
0.33
1
06/25/21 15:39
106-46-7
ND
ug/L
1.0
0.56
1
06/25/21 15:39
110-57-6
0.62J
ug/L
1.0
0.37
1
06/25/21 15:39
75-34-3
0.49J
ug/L
1.0
0.32
1
06/25/21 15:39
107-06-2
ND
ug/L
1.0
0.35
1
06/25/21 15:39
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
Page 26 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-22 Lab ID: 92546336010 Collected: 06/23/21 13:56 Received: 06/24/21 07:00 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
2.1
ug/L
1.0
0.38
1
06/25/21 15:39
156-59-2
ND
ug/L
1.0
0.40
1
06/25/21 15:39
156-60-5
ND
ug/L
1.0
0.36
1
06/25/21 15:39
78-87-5
ND
ug/L
1.0
0.36
1
06/25/21 15:39
10061-01-5
ND
ug/L
1.0
0.36
1
06/25/21 15:39
10061-02-6
ND
ug/L
150
38.7
1
06/25/21 15:39
123-91-1
ND
ug/L
1.0
0.30
1
06/25/21 15:39
100-41-4
ND
ug/L
5.0
0.48
1
06/25/21 15:39
591-78-6
ND
ug/L
20.0
9.7
1
06/25/21 15:39
74-88-4
ND
ug/L
5.0
2.0
1
06/25/21 15:39
75-09-2
ND
ug/L
5.0
2.7
1
06/25/21 15:39
108-10-1
ND
ug/L
1.0
0.29
1
06/25/21 15:39
100-42-5
ND
ug/L
1.0
0.31
1
06/25/21 15:39
630-20-6
ND
ug/L
1.0
0.22
1
06/25/21 15:39
79-34-5
ND
ug/L
1.0
0.29
1
06/25/21 15:39
127-18-4
ND
ug/L
1.0
0.48
1
06/25/21 15:39
108-88-3
ND
ug/L
1.0
0.33
1
06/25/21 15:39
71-55-6
ND
ug/L
1.0
0.32
1
06/25/21 15:39
79-00-5
ND
ug/L
1.0
0.38
1
06/25/21 15:39
79-01-6
ND
ug/L
1.0
0.30
1
06/25/21 15:39
75-69-4
ND
ug/L
1.0
0.26
1
06/25/21 15:39
96-18-4
ND
ug/L
2.0
1.3
1
06/25/21 15:39
108-05-4
ND
ug/L
1.0
0.39
1
06/25/21 15:39
75-01-4
ND
ug/L
1.0
0.34
1
06/25/21 15:39
1330-20-7
96
%
70-130
1
06/25/21 15:39
460-00-4
95
%
70-130
1
06/25/21 15:39
17060-07-0
103
%
70-130
1
06/25/21 15:39
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MWA Lab ID: 92546336011 Collected: 06/24/21 15:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
0.55J nM
1.9
0.49
1
07/07/2113:19
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Methane
ND ug/L
5.0
2.0
1
07/14/2112:22
74-82-8
Ethane
ND ug/L
1.0
0.17
1
07/14/2112:22
74-84-0
Ethene
ND ug/L
1.0
0.24
1
07/14/2112:22
74-85-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
ND ug/L
900
127
1
07/07/21 12:18
124-38-9
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
3.0
1
07/06/2116:19
07/07/2112:55
7440-36-0
Arsenic
6.OJ ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 12:55
7440-38-2
Barium
34.9 ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:55
7440-39-3
Beryllium
ND ug/L
1.0
0.70
1
07/06/2116:19
07/07/2112:55
7440-41-7
Cadmium
ND ug/L
1.0
0.40
1
07/06/2116:19
07/07/2112:55
7440-43-9
Chromium
ND ug/L
5.0
3.7
1
07/06/2116:19
07/07/2112:55
7440-47-3
Cobalt
ND ug/L
5.0
3.6
1
07/06/2116:19
07/07/2112:55
7440-48-4
Copper
ND ug/L
5.0
4.3
1
07/06/2116:19
07/07/2112:55
7440-50-8
Lead
ND ug/L
5.0
4.5
1
07/06/2116:19
07/07/2112:55
7439-92-1
Nickel
ND ug/L
5.0
3.5
1
07/06/2116:19
07/07/2112:55
7440-02-0
Selenium
ND ug/L
10.0
4.7
1
07/06/2116:19
07/07/2112:55
7782-49-2
Silver
ND ug/L
5.0
2.5
1
07/06/2116:19
07/07/2112:55
7440-22-4
Vanadium
ND ug/L
5.0
3.9
1
07/06/2116:19
07/07/2112:55
7440-62-2
Zinc
ND ug/L
10.0
9.5
1
07/06/2116:19
07/07/2112:55
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Thallium
ND ug/L
1.0
0.050
1
06/30/2116:15
07/02/2102:38
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
5.1
1
06/29/21 14:42
67-64-1
Acrylonitrile
ND ug/L
10.0
1.8
1
06/29/21 14:42
107-13-1
Benzene
ND ug/L
1.0
0.34
1
06/29/21 14:42
71-43-2
Bromochloromethane
ND ug/L
1.0
0.47
1
06/29/21 14:42
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.31
1
06/29/21 14:42
75-27-4
Bromoform
ND ug/L
1.0
0.34
1
06/29/21 14:42
75-25-2
Bromomethane
ND ug/L
2.0
1.7
1
06/29/21 14:42
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
4.0
1
06/29/21 14:42
78-93-3
Carbon disulfide
ND ug/L
2.0
0.73
1
06/29/21 14:42
75-15-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-1 Lab ID: 92546336011 Collected: 06/24/21 15:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 14:42
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 14:42
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 14:42
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 14:42
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 14:42
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 14:42
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 14:42
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 14:42
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 14:42
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/29/21 14:42
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 14:42
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 14:42
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/29/21 14:42
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 14:42
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 14:42
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.38
1
06/29/21 14:42
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
06/29/21 14:42
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 14:42
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 14:42
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 14:42
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
38.7
1
06/29/21 14:42
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.30
1
06/29/21 14:42
100-41-4
2-Hexanone
ND
ug/L
5.0
0.48
1
06/29/21 14:42
591-78-6
lodomethane
ND
ug/L
20.0
9.7
1
06/29/21 14:42
74-88-4
Methylene Chloride
ND
ug/L
5.0
2.0
1
06/29/21 14:42
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
06/29/21 14:42
108-10-1
Styrene
ND
ug/L
1.0
0.29
1
06/29/21 14:42
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
06/29/21 14:42
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
06/29/21 14:42
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
06/29/21 14:42
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
06/29/21 14:42
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
06/29/21 14:42
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 14:42
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
06/29/21 14:42
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
06/29/21 14:42
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
06/29/21 14:42
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/29/21 14:42
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
06/29/21 14:42
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
06/29/21 14:42
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
06/29/21 14:42
460-00-4
1,2-Dichloroethane-d4 (S)
116
%
70-130
1
06/29/21 14:42
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
06/29/21 14:42
2037-26-5
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 10/15/2021 02:14 PM
without the written
consent of Pace
Analytical Services, LLC.
Page 29 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MWA Lab ID: 92546336011 Collected: 06/24/21 15:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2320B Alkalinity
Alkalinity, Total as CaCO3
Iron, Ferrous
Iron, Ferrous
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
4500 Chloride
Chloride
5220D COD
Chemical Oxygen Demand
531013 TOC
Total Organic Carbon
Low Level Volatile Fatty Acids
Lactic Acid
Acetic Acid
Propionic Acid
Formic acid
Butyric Acid
Pyruvic Acid
i-Pentanoic Acid
Pentanoic Acid
i-Hexanoic Acid
Hexanoic Acid
Date: 10/15/2021 02:14 PM
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
11800 ug/L 5000
5000
1
07/01 /21 20:49
Analytical Method: SM 3500-Fe B-2011
Pace Analytical Services -Asheville
ND mg/L 0.50
0.040
1
07/06/2116:27
H3,N2
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100
50.0
1
07/01/2105:05
18496-25-8
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
4860 ug/L 1000
500
1
06/29/2122:05
14808-79-8
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
2580 ug/L 1000
500
1
07/07/2120:07
16887-00-6
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Pace Analytical Services -Asheville
ND ug/L 25000
12500
1
07/07/2102:33 07/07/2106:10
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
5051 ug/L 1000
500
1
06/29/2121:00
7440-44-0
Analytical Method: AM23G
Pace Analytical Gulf Coast
0.0911 mg/L 0.50
0.053
1
07/08/2120:41
50-21-5
0.30J mg/L 0.50
0.12
1
07/08/2120:41
64-19-7
ND mg/L 0.50
0.053
1
07/08/2120:41
79-09-4
5.3 mg/L 0.50
0.055
1
07/08/2120:41
64-18-6
ND mg/L 0.50
0.058
1
07/08/2120:41
107-92-6
ND mg/L 0.50
0.060
1
07/08/2120:41
127-17-3
ND mg/L 0.50
0.061
1
07/08/2120:41
503-74-2
ND mg/L 0.50
0.056
1
07/08/2120:41
109-52-4
ND mg/L 0.50
0.056
1
07/08/2120:41
646-07-1
ND mg/L 0.50
0.058
1
07/08/2120:41
142-62-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 30 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-7 Lab ID: 92546336012 Collected: 06/25/21 10:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
1.0J nM
1.9
0.49
1
07/07/2113:46
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Methane
170 ug/L
5.0
2.0
1
07/14/21 12:37
74-82-8
Ethane
0.65J ug/L
1.0
0.17
1
07/14/21 12:37
74-84-0
Ethene
ND ug/L
1.0
0.24
1
07/14/21 12:37
74-85-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
ND ug/L
900
127
1
07/07/21 12:23
124-38-9
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
3.0
1
07/06/21 16:19
07/07/21 13:05
7440-36-0
Arsenic
5.01 ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 13:05
7440-38-2
Barium
52.6 ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 13:05
7440-39-3
Beryllium
ND ug/L
1.0
0.70
1
07/06/21 16:19
07/07/21 13:05
7440-41-7
Cadmium
0.511 ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 13:05
7440-43-9
Chromium
ND ug/L
5.0
3.7
1
07/06/21 16:19
07/07/21 13:05
7440-47-3
Cobalt
68.0 ug/L
5.0
3.6
1
07/06/21 16:19
07/07/21 13:05
7440-48-4
Copper
ND ug/L
5.0
4.3
1
07/06/21 16:19
07/07/21 13:05
7440-50-8
Lead
ND ug/L
5.0
4.5
1
07/06/21 16:19
07/07/21 13:05
7439-92-1
Nickel
ND ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 13:05
7440-02-0
Selenium
ND ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 13:05
7782-49-2
Silver
ND ug/L
5.0
2.5
1
07/06/21 16:19
07/07/21 13:05
7440-22-4
Vanadium
3.9J ug/L
5.0
3.9
1
07/06/21 16:19
07/07/21 13:05
7440-62-2
Zinc
ND ug/L
10.0
9.5
1
07/06/21 16:19
07/07/21 13:05
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Thallium
0.14J ug/L
1.0
0.050
1
06/30/2116:15
07/02/2102:42
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
5.1
1
06/29/21 15:00
67-64-1
Acrylonitrile
ND ug/L
10.0
1.8
1
06/29/21 15:00
107-13-1
Benzene
ND ug/L
1.0
0.34
1
06/29/21 15:00
71-43-2
Bromochloromethane
ND ug/L
1.0
0.47
1
06/29/21 15:00
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.31
1
06/29/21 15:00
75-27-4
Bromoform
ND ug/L
1.0
0.34
1
06/29/21 15:00
75-25-2
Bromomethane
ND ug/L
2.0
1.7
1
06/29/21 15:00
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
4.0
1
06/29/21 15:00
78-93-3
Carbon disulfide
ND ug/L
2.0
0.73
1
06/29/21 15:00
75-15-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-7 Lab ID: 92546336012 Collected: 06/25/21 10:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 15:00
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 15:00
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 15:00
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 15:00
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 15:00
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 15:00
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 15:00
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 15:00
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 15:00
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/29/21 15:00
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 15:00
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 15:00
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/29/21 15:00
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 15:00
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 15:00
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.38
1
06/29/21 15:00
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
06/29/21 15:00
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 15:00
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 15:00
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 15:00
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
38.7
1
06/29/21 15:00
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.30
1
06/29/21 15:00
100-41-4
2-Hexanone
ND
ug/L
5.0
0.48
1
06/29/21 15:00
591-78-6
lodomethane
ND
ug/L
20.0
9.7
1
06/29/21 15:00
74-88-4
Methylene Chloride
ND
ug/L
5.0
2.0
1
06/29/21 15:00
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
06/29/21 15:00
108-10-1
Styrene
ND
ug/L
1.0
0.29
1
06/29/21 15:00
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
06/29/21 15:00
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
06/29/21 15:00
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
06/29/21 15:00
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
06/29/21 15:00
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
06/29/21 15:00
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 15:00
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
06/29/21 15:00
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
06/29/21 15:00
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
06/29/21 15:00
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/29/21 15:00
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
06/29/21 15:00
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
06/29/21 15:00
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
06/29/21 15:00
460-00-4
1,2-Dichloroethane-d4 (S)
117
%
70-130
1
06/29/21 15:00
17060-07-0
Toluene-d8 (S)
108
%
70-130
1
06/29/21 15:00
2037-26-5
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 10/15/2021 02:14 PM
without the written
consent of Pace
Analytical Services, LLC.
Page 32 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-7 Lab ID: 92546336012 Collected: 06/25/21 10:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2320B Alkalinity
Alkalinity, Total as CaCO3
Iron, Ferrous
Iron, Ferrous
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
4500 Chloride
Chloride
5220D COD
Chemical Oxygen Demand
531013 TOC
Total Organic Carbon
Low Level Volatile Fatty Acids
Lactic Acid
Acetic Acid
Propionic Acid
Formic acid
Butyric Acid
Pyruvic Acid
i-Pentanoic Acid
Pentanoic Acid
i-Hexanoic Acid
Hexanoic Acid
Date: 10/15/2021 02:14 PM
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
90800 ug/L 5000
5000
1
07/02/2116:04
Analytical Method: SM 3500-Fe B-2011
Pace Analytical Services -Asheville
ND mg/L 0.50
0.040
1
07/06/2116:30
H3,N2
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100
50.0
1
07/01/2105:06
18496-25-8
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
6960 ug/L 1000
500
1
06/29/2122:18
14808-79-8
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
25000 ug/L 1000
500
1
07/07/2120:36
16887-00-6
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Pace Analytical Services -Asheville
24600J ug/L 25000
12500
1
07/07/2102:33 07/07/2106:12
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
3680 ug/L 1000
500
1
06/29/2121:15
7440-44-0
Analytical Method: AM23G
Pace Analytical Gulf Coast
0.086J mg/L 0.50
0.053
1
07/08/2121:34
50-21-5
0.36J mg/L 0.50
0.12
1
07/08/2121:34
64-19-7
ND mg/L 0.50
0.053
1
07/08/2121:34
79-09-4
4.6 mg/L 0.50
0.055
1
07/08/2121:34
64-18-6
ND mg/L 0.50
0.058
1
07/08/2121:34
107-92-6
ND mg/L 0.50
0.060
1
07/08/2121:34
127-17-3
ND mg/L 0.50
0.061
1
07/08/2121:34
503-74-2
ND mg/L 0.50
0.056
1
07/08/2121:34
109-52-4
ND mg/L 0.50
0.056
1
07/08/2121:34
646-07-1
ND mg/L 0.50
0.058
1
07/08/2121:34
142-62-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 33 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-9 Lab ID: 92546336013 Collected: 06/25/21 12:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
1.3J nM
1.9
0.49
1
07/07/2114:02
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Methane
2200 ug/L
5.0
2.0
1
07/14/21 12:57
74-82-8
Ethane
28 ug/L
1.0
0.17
1
07/14/21 12:57
74-84-0
Ethene
2.6 ug/L
1.0
0.24
1
07/14/21 12:57
74-85-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
ND ug/L
900
127
1
07/07/21 12:27
124-38-9
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Antimony
4.1J ug/L
5.0
3.0
1
07/06/21 16:19
07/07/21 13:08
7440-36-0
Arsenic
ND ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 13:08
7440-38-2
Barium
55.7 ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 13:08
7440-39-3
Beryllium
ND ug/L
1.0
0.70
1
07/06/21 16:19
07/07/21 13:08
7440-41-7
Cadmium
0.47J ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 13:08
7440-43-9
Chromium
ND ug/L
5.0
3.7
1
07/06/21 16:19
07/07/21 13:08
7440-47-3
Cobalt
240 ug/L
5.0
3.6
1
07/06/21 16:19
07/07/21 13:08
7440-48-4
Copper
ND ug/L
5.0
4.3
1
07/06/21 16:19
07/07/21 13:08
7440-50-8
Lead
ND ug/L
5.0
4.5
1
07/06/21 16:19
07/07/21 13:08
7439-92-1
Nickel
8.6 ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 13:08
7440-02-0
Selenium
5.6J ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 13:08
7782-49-2
Silver
ND ug/L
5.0
2.5
1
07/06/21 16:19
07/07/21 13:08
7440-22-4
Vanadium
5.5 ug/L
5.0
3.9
1
07/06/21 16:19
07/07/21 13:08
7440-62-2
Zinc
71.7 ug/L
10.0
9.5
1
07/06/21 16:19
07/07/21 13:08
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Thallium
0.57J ug/L
1.0
0.050
1
06/30/2116:15
07/02/2102:46
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
5.1
1
06/29/21 17:38
67-64-1
Acrylonitrile
ND ug/L
10.0
1.8
1
06/29/21 17:38
107-13-1
Benzene
1.8 ug/L
1.0
0.34
1
06/29/21 17:38
71-43-2
Bromochloromethane
ND ug/L
1.0
0.47
1
06/29/21 17:38
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.31
1
06/29/21 17:38
75-27-4
Bromoform
ND ug/L
1.0
0.34
1
06/29/21 17:38
75-25-2
Bromomethane
ND ug/L
2.0
1.7
1
06/29/21 17:38
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
4.0
1
06/29/21 17:38
78-93-3
Carbon disulfide
ND ug/L
2.0
0.73
1
06/29/21 17:38
75-15-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 34 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-9 Lab ID: 92546336013 Collected: 06/25/21 12:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 17:38
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 17:38
108-90-7
Chloroethane
0.95J
ug/L
1.0
0.65
1
06/29/21 17:38
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 17:38
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 17:38
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 17:38
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 17:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 17:38
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 17:38
74-95-3
1,2-Dichlorobenzene
2.2
ug/L
1.0
0.34
1
06/29/21 17:38
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 17:38
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 17:38
110-57-6
1,1-Dichloroethane
0.94J
ug/L
1.0
0.37
1
06/29/21 17:38
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 17:38
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 17:38
75-35-4
cis-1,2-Dichloroethene
18.1
ug/L
1.0
0.38
1
06/29/21 17:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
06/29/21 17:38
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 17:38
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 17:38
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 17:38
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
38.7
1
06/29/21 17:38
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.30
1
06/29/21 17:38
100-41-4
2-Hexanone
ND
ug/L
5.0
0.48
1
06/29/21 17:38
591-78-6
lodomethane
ND
ug/L
20.0
9.7
1
06/29/21 17:38
74-88-4
Methylene Chloride
ND
ug/L
5.0
2.0
1
06/29/21 17:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
06/29/21 17:38
108-10-1
Styrene
ND
ug/L
1.0
0.29
1
06/29/21 17:38
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
06/29/21 17:38
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
06/29/21 17:38
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
06/29/21 17:38
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
06/29/21 17:38
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
06/29/21 17:38
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 17:38
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
06/29/21 17:38
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
06/29/21 17:38
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
06/29/21 17:38
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/29/21 17:38
108-05-4
Vinyl chloride
10.0
ug/L
1.0
0.39
1
06/29/21 17:38
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
06/29/21 17:38
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
06/29/21 17:38
460-00-4
1,2-Dichloroethane-d4 (S)
115
%
70-130
1
06/29/21 17:38
17060-07-0
Toluene-d8 (S)
106
%
70-130
1
06/29/21 17:38
2037-26-5
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 10/15/2021 02:14 PM
without the written
consent of Pace
Analytical Services, LLC.
Page 35 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-9 Lab ID: 92546336013 Collected: 06/25/21 12:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2320B Alkalinity
Alkalinity, Total as CaCO3
Iron, Ferrous
Iron, Ferrous
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
4500 Chloride
Chloride
5220D COD
Chemical Oxygen Demand
531013 TOC
Total Organic Carbon
Low Level Volatile Fatty Acids
Lactic Acid
Acetic Acid
Propionic Acid
Formic acid
Butyric Acid
Pyruvic Acid
i-Pentanoic Acid
Pentanoic Acid
i-Hexanoic Acid
Hexanoic Acid
Date: 10/15/2021 02:14 PM
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
54800 ug/L 5000
5000
1
07/02/2116:16
Analytical Method: SM 3500-Fe B-2011
Pace Analytical Services -Asheville
19.1 mg/L 5.0
0.40
10
07/06/2117:07
H3,N2
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100
50.0
1
07/01/2105:07
18496-25-8
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
776J ug/L 1000
500
1
06/29/2122:32
14808-79-8
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
28400 ug/L 1000
500
1
07/07/2120:40
16887-00-6
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Pace Analytical Services -Asheville
24600J ug/L 25000
12500
1
07/07/2102:33 07/07/2106:12
Analytical Method: SM 5310B-2011
Pace Analytical Services -Asheville
2830 ug/L 1000
500
1
06/29/2122:09
7440-44-0
Analytical Method: AM23G
Pace Analytical Gulf Coast
ND mg/L 5.0
0.53
10
07/08/2122:28
50-21-5
3.OJ mg/L 5.0
1.2
10
07/08/2122:28
64-19-7
ND mg/L 5.0
0.53
10
07/08/2122:28
79-09-4
44 mg/L 5.0
0.55
10
07/08/2122:28
64-18-6
ND mg/L 5.0
0.58
10
07/08/2122:28
107-92-6
ND mg/L 5.0
0.60
10
07/08/2122:28
127-17-3
ND mg/L 5.0
0.61
10
07/08/2122:28
503-74-2
ND mg/L 5.0
0.56
10
07/08/2122:28
109-52-4
ND mg/L 5.0
0.56
10
07/08/2122:28
646-07-1
ND mg/L 5.0
0.58
10
07/08/2122:28
142-62-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 36 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-11 Lab ID: 92546336014 Collected: 06/24/21 16:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
8.0 nM
1.9
0.49
1
07/07/2114:16
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Methane
120 ug/L
5.0
2.0
1
07/14/2113:11
74-82-8
Ethane
ND ug/L
1.0
0.17
1
07/14/2113:11
74-84-0
Ethene
ND ug/L
1.0
0.24
1
07/14/2113:11
74-85-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
ND ug/L
900
127
1
07/07/21 12:34
124-38-9
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
3.0
1
07/06/2116:19
07/07/2113:11
7440-36-0
Arsenic
5.8J ug/L
10.0
4.7
1
07/06/2116:19
07/07/2113:11
7440-38-2
Barium
35.7 ug/L
5.0
3.5
1
07/06/2116:19
07/07/2113:11
7440-39-3
Beryllium
ND ug/L
1.0
0.70
1
07/06/2116:19
07/07/2113:11
7440-41-7
Cadmium
ND ug/L
1.0
0.40
1
07/06/2116:19
07/07/2113:11
7440-43-9
Chromium
ND ug/L
5.0
3.7
1
07/06/2116:19
07/07/2113:11
7440-47-3
Cobalt
22.1 ug/L
5.0
3.6
1
07/06/2116:19
07/07/2113:11
7440-48-4
Copper
ND ug/L
5.0
4.3
1
07/06/2116:19
07/07/2113:11
7440-50-8
Lead
ND ug/L
5.0
4.5
1
07/06/2116:19
07/07/2113:11
7439-92-1
Nickel
ND ug/L
5.0
3.5
1
07/06/2116:19
07/07/2113:11
7440-02-0
Selenium
ND ug/L
10.0
4.7
1
07/06/2116:19
07/07/2113:11
7782-49-2
Silver
ND ug/L
5.0
2.5
1
07/06/2116:19
07/07/2113:11
7440-22-4
Vanadium
ND ug/L
5.0
3.9
1
07/06/2116:19
07/07/2113:11
7440-62-2
Zinc
ND ug/L
10.0
9.5
1
07/06/2116:19
07/07/2113:11
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Thallium
0.10J ug/L
1.0
0.050
1
06/30/2116:15
07/02/2102:58
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
5.1
1
06/29/21 17:03
67-64-1
Acrylonitrile
ND ug/L
10.0
1.8
1
06/29/21 17:03
107-13-1
Benzene
ND ug/L
1.0
0.34
1
06/29/21 17:03
71-43-2
Bromochloromethane
ND ug/L
1.0
0.47
1
06/29/21 17:03
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.31
1
06/29/21 17:03
75-27-4
Bromoform
ND ug/L
1.0
0.34
1
06/29/21 17:03
75-25-2
Bromomethane
ND ug/L
2.0
1.7
1
06/29/21 17:03
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
4.0
1
06/29/21 17:03
78-93-3
Carbon disulfide
ND ug/L
2.0
0.73
1
06/29/21 17:03
75-15-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 37 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-11 Lab ID: 92546336014 Collected: 06/24/21 16:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 17:03
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 17:03
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 17:03
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 17:03
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 17:03
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 17:03
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 17:03
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 17:03
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 17:03
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/29/21 17:03
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 17:03
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 17:03
110-57-6
1,1-Dichloroethane
0.39J
ug/L
1.0
0.37
1
06/29/21 17:03
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 17:03
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 17:03
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.38
1
06/29/21 17:03
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
06/29/21 17:03
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 17:03
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 17:03
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 17:03
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
38.7
1
06/29/21 17:03
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.30
1
06/29/21 17:03
100-41-4
2-Hexanone
ND
ug/L
5.0
0.48
1
06/29/21 17:03
591-78-6
lodomethane
ND
ug/L
20.0
9.7
1
06/29/21 17:03
74-88-4
Methylene Chloride
ND
ug/L
5.0
2.0
1
06/29/21 17:03
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
06/29/21 17:03
108-10-1
Styrene
ND
ug/L
1.0
0.29
1
06/29/21 17:03
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
06/29/21 17:03
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
06/29/21 17:03
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
06/29/21 17:03
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
06/29/21 17:03
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
06/29/21 17:03
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 17:03
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
06/29/21 17:03
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
06/29/21 17:03
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
06/29/21 17:03
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/29/21 17:03
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
06/29/21 17:03
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
06/29/21 17:03
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
06/29/21 17:03
460-00-4
1,2-Dichloroethane-d4 (S)
116
%
70-130
1
06/29/21 17:03
17060-07-0
Toluene-d8 (S)
107
%
70-130
1
06/29/21 17:03
2037-26-5
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 10/15/2021 02:14 PM
without the written
consent of Pace
Analytical Services, LLC.
Page 38 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-11 Lab ID: 92546336014 Collected: 06/24/21 16:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2320B Alkalinity
Alkalinity, Total as CaCO3
Iron, Ferrous
Iron, Ferrous
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
4500 Chloride
Chloride
5220D COD
Chemical Oxygen Demand
531013 TOC
Total Organic Carbon
Low Level Volatile Fatty Acids
Lactic Acid
Acetic Acid
Propionic Acid
Formic acid
Butyric Acid
Pyruvic Acid
i-Pentanoic Acid
Pentanoic Acid
i-Hexanoic Acid
Hexanoic Acid
Date: 10/15/2021 02:14 PM
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
22800 ug/L 5000
5000
1
07/01 /21 20:55
Analytical Method: SM 3500-Fe B-2011
Pace Analytical Services -Asheville
0.043J mg/L 0.50
0.040
1
07/06/2116:27
H3,N2
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100
50.0
1
07/01/2105:05
18496-25-8
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
15600 ug/L 1000
500
1
06/29/2122:45
14808-79-8
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
10700 ug/L 1000
500
1
07/07/2120:41
16887-00-6
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Pace Analytical Services -Asheville
ND ug/L 25000
12500
1
07/07/2102:33 07/07/2106:12
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
947J ug/L 1000
500
1
06/29/2123:04
7440-44-0
Analytical Method: AM23G
Pace Analytical Gulf Coast
0.23J mg/L 0.50
0.053
1
07/08/2123:21
50-21-5
0.31J mg/L 0.50
0.12
1
07/08/2123:21
64-19-7
ND mg/L 0.50
0.053
1
07/08/2123:21
79-09-4
5.2 mg/L 0.50
0.055
1
07/08/2123:21
64-18-6
ND mg/L 0.50
0.058
1
07/08/2123:21
107-92-6
ND mg/L 0.50
0.060
1
07/08/2123:21
127-17-3
ND mg/L 0.50
0.061
1
07/08/2123:21
503-74-2
ND mg/L 0.50
0.056
1
07/08/2123:21
109-52-4
ND mg/L 0.50
0.056
1
07/08/2123:21
646-07-1
ND mg/L 0.50
0.058
1
07/08/2123:21
142-62-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 39 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-15 Lab ID: 92546336015 Collected: 06/24/21 11:30 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
2.8 nM
1.9
0.49
1
07/07/2114:31
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Methane
1100 ug/L
5.0
2.0
1
07/14/21 13:26
74-82-8
Ethane
ND ug/L
1.0
0.17
1
07/14/2113:26
74-84-0
Ethene
ND ug/L
1.0
0.24
1
07/14/2113:26
74-85-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
ND ug/L
900
127
1
07/07/21 12:38
124-38-9
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
3.0
1
07/06/2116:19
07/07/2113:15
7440-36-0
Arsenic
ND ug/L
10.0
4.7
1
07/06/2116:19
07/07/2113:15
7440-38-2
Barium
40.0 ug/L
5.0
3.5
1
07/06/2116:19
07/07/2113:15
7440-39-3
Beryllium
ND ug/L
1.0
0.70
1
07/06/2116:19
07/07/2113:15
7440-41-7
Cadmium
ND ug/L
1.0
0.40
1
07/06/2116:19
07/07/2113:15
7440-43-9
Chromium
ND ug/L
5.0
3.7
1
07/06/2116:19
07/07/2113:15
7440-47-3
Cobalt
ND ug/L
5.0
3.6
1
07/06/2116:19
07/07/2113:15
7440-48-4
Copper
ND ug/L
5.0
4.3
1
07/06/2116:19
07/07/2113:15
7440-50-8
Lead
ND ug/L
5.0
4.5
1
07/06/2116:19
07/07/2113:15
7439-92-1
Nickel
ND ug/L
5.0
3.5
1
07/06/2116:19
07/07/2113:15
7440-02-0
Selenium
ND ug/L
10.0
4.7
1
07/06/2116:19
07/07/2113:15
7782-49-2
Silver
ND ug/L
5.0
2.5
1
07/06/2116:19
07/07/2113:15
7440-22-4
Vanadium
ND ug/L
5.0
3.9
1
07/06/2116:19
07/07/2113:15
7440-62-2
Zinc
ND ug/L
10.0
9.5
1
07/06/2116:19
07/07/2113:15
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Thallium
0.054J ug/L
0.47
0.050
1
06/30/2116:15
07/02/2103:03
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
5.1
1
06/29/21 17:20
67-64-1
Acrylonitrile
ND ug/L
10.0
1.8
1
06/29/21 17:20
107-13-1
Benzene
0.43J ug/L
1.0
0.34
1
06/29/21 17:20
71-43-2
Bromochloromethane
ND ug/L
1.0
0.47
1
06/29/21 17:20
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.31
1
06/29/21 17:20
75-27-4
Bromoform
ND ug/L
1.0
0.34
1
06/29/21 17:20
75-25-2
Bromomethane
ND ug/L
2.0
1.7
1
06/29/21 17:20
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
4.0
1
06/29/21 17:20
78-93-3
Carbon disulfide
ND ug/L
2.0
0.73
1
06/29/21 17:20
75-15-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-15 Lab ID: 92546336015 Collected: 06/24/21 11:30 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.33
1
06/29/21 17:20
56-23-5
ND
ug/L
1.0
0.28
1
06/29/21 17:20
108-90-7
ND
ug/L
1.0
0.65
1
06/29/21 17:20
75-00-3
ND
ug/L
5.0
1.6
1
06/29/21 17:20
67-66-3
ND
ug/L
1.0
0.54
1
06/29/21 17:20
74-87-3
ND
ug/L
2.0
0.34
1
06/29/21 17:20
96-12-8
ND
ug/L
1.0
0.36
1
06/29/21 17:20
124-48-1
ND
ug/L
1.0
0.27
1
06/29/21 17:20
106-93-4
ND
ug/L
1.0
0.39
1
06/29/21 17:20
74-95-3
ND
ug/L
1.0
0.34
1
06/29/21 17:20
95-50-1
ND
ug/L
1.0
0.33
1
06/29/21 17:20
106-46-7
ND
ug/L
1.0
0.56
1
06/29/21 17:20
110-57-6
4.4
ug/L
1.0
0.37
1
06/29/21 17:20
75-34-3
0.53J
ug/L
1.0
0.32
1
06/29/21 17:20
107-06-2
ND
ug/L
1.0
0.35
1
06/29/21 17:20
75-35-4
21.9
ug/L
1.0
0.38
1
06/29/21 17:20
156-59-2
ND
ug/L
1.0
0.40
1
06/29/21 17:20
156-60-5
ND
ug/L
1.0
0.36
1
06/29/21 17:20
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 17:20
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/21 17:20
10061-02-6
ND
ug/L
150
38.7
1
06/29/21 17:20
123-91-1
ND
ug/L
1.0
0.30
1
06/29/21 17:20
100-41-4
ND
ug/L
5.0
0.48
1
06/29/21 17:20
591-78-6
ND
ug/L
20.0
9.7
1
06/29/21 17:20
74-88-4
ND
ug/L
5.0
2.0
1
06/29/21 17:20
75-09-2
ND
ug/L
5.0
2.7
1
06/29/21 17:20
108-10-1
ND
ug/L
1.0
0.29
1
06/29/21 17:20
100-42-5
ND
ug/L
1.0
0.31
1
06/29/21 17:20
630-20-6
ND
ug/L
1.0
0.22
1
06/29/21 17:20
79-34-5
ND
ug/L
1.0
0.29
1
06/29/21 17:20
127-18-4
ND
ug/L
1.0
0.48
1
06/29/21 17:20
108-88-3
ND
ug/L
1.0
0.33
1
06/29/21 17:20
71-55-6
ND
ug/L
1.0
0.32
1
06/29/21 17:20
79-00-5
2.0
ug/L
1.0
0.38
1
06/29/21 17:20
79-01-6
ND
ug/L
1.0
0.30
1
06/29/21 17:20
75-69-4
ND
ug/L
1.0
0.26
1
06/29/21 17:20
96-18-4
ND
ug/L
2.0
1.3
1
06/29/21 17:20
108-05-4
3.1
ug/L
1.0
0.39
1
06/29/21 17:20
75-01-4
ND
ug/L
1.0
0.34
1
06/29/21 17:20
1330-20-7
94
%
70-130
1
06/29/21 17:20
460-00-4
115
%
70-130
1
06/29/21 17:20
17060-07-0
107
%
70-130
1
06/29/21 17:20
2037-26-5
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
without the written
consent of Pace
Analytical Services, LLC.
Page 41 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-15 Lab ID: 92546336015 Collected: 06/24/21 11:30 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2320B Alkalinity
Alkalinity, Total as CaCO3
Iron, Ferrous
Iron, Ferrous
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
4500 Chloride
Chloride
5220D COD
Chemical Oxygen Demand
531013 TOC
Total Organic Carbon
Low Level Volatile Fatty Acids
Lactic Acid
Acetic Acid
Propionic Acid
Formic acid
Butyric Acid
Pyruvic Acid
i-Pentanoic Acid
Pentanoic Acid
i-Hexanoic Acid
Hexanoic Acid
Date: 10/15/2021 02:14 PM
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
41000 ug/L 5000
5000
1
07/02/2115:06
Analytical Method: SM 3500-Fe B-2011
Pace Analytical Services -Asheville
0.040J mg/L 0.50
0.040
1
07/06/2116:25
H3,N2
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100
50.0
1
07/01/2105:06
18496-25-8
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
872J ug/L 1000
500
1
06/29/2123:39
14808-79-8
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
2790 ug/L 1000
500
1
07/07/2120:14
16887-00-6
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Pace Analytical Services -Asheville
ND ug/L 25000
12500
1
07/07/2102:33 07/07/2106:12
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
799J ug/L 1000
500
1
06/29/2123:21
7440-44-0
Analytical Method: AM23G
Pace Analytical Gulf Coast
0.22J mg/L 0.50
0.053
1
07/09/2100:15
50-21-5
0.36J mg/L 0.50
0.12
1
07/09/2100:15
64-19-7
ND mg/L 0.50
0.053
1
07/09/2100:15
79-09-4
5.8 mg/L 0.50
0.055
1
07/09/2100:15
64-18-6
ND mg/L 0.50
0.058
1
07/09/2100:15
107-92-6
ND mg/L 0.50
0.060
1
07/09/2100:15
127-17-3
ND mg/L 0.50
0.061
1
07/09/2100:15
503-74-2
ND mg/L 0.50
0.056
1
07/09/2100:15
109-52-4
ND mg/L 0.50
0.056
1
07/09/2100:15
646-07-1
ND mg/L 0.50
0.058
1
07/09/2100:15
142-62-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 42 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-14 Lab ID: 92546336016 Collected: 06/25/21 08:30 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
5.3 nM
1.9
0.49
1
07/07/2114:44
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Methane
ND ug/L
5.0
2.0
1
07/14/2114:17
74-82-8
Ethane
ND ug/L
1.0
0.17
1
07/14/2114:17
74-84-0
Ethene
ND ug/L
1.0
0.24
1
07/14/2114:17
74-85-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
ND ug/L
900
127
1
07/07/21 12:43
124-38-9
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
3.0
1
07/06/2116:19
07/07/2113:18
7440-36-0
Arsenic
ND ug/L
10.0
4.7
1
07/06/2116:19
07/07/2113:18
7440-38-2
Barium
21.4 ug/L
5.0
3.5
1
07/06/2116:19
07/07/2113:18
7440-39-3
Beryllium
ND ug/L
1.0
0.70
1
07/06/2116:19
07/07/2113:18
7440-41-7
Cadmium
ND ug/L
1.0
0.40
1
07/06/2116:19
07/07/2113:18
7440-43-9
Chromium
ND ug/L
5.0
3.7
1
07/06/2116:19
07/07/2113:18
7440-47-3
Cobalt
ND ug/L
5.0
3.6
1
07/06/2116:19
07/07/2113:18
7440-48-4
Copper
ND ug/L
5.0
4.3
1
07/06/2116:19
07/07/2113:18
7440-50-8
Lead
ND ug/L
5.0
4.5
1
07/06/2116:19
07/07/2113:18
7439-92-1
Nickel
ND ug/L
5.0
3.5
1
07/06/2116:19
07/07/2113:18
7440-02-0
Selenium
ND ug/L
10.0
4.7
1
07/06/2116:19
07/07/2113:18
7782-49-2
Silver
ND ug/L
5.0
2.5
1
07/06/2116:19
07/07/2113:18
7440-22-4
Vanadium
ND ug/L
5.0
3.9
1
07/06/2116:19
07/07/2113:18
7440-62-2
Zinc
ND ug/L
10.0
9.5
1
07/06/2116:19
07/07/2113:18
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Thallium
ND ug/L
0.47
0.050
1
06/30/2116:15
07/02/2103:07
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
5.1
1
06/29/21 17:55
67-64-1
Acrylonitrile
ND ug/L
10.0
1.8
1
06/29/21 17:55
107-13-1
Benzene
ND ug/L
1.0
0.34
1
06/29/21 17:55
71-43-2
Bromochloromethane
ND ug/L
1.0
0.47
1
06/29/21 17:55
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.31
1
06/29/21 17:55
75-27-4
Bromoform
ND ug/L
1.0
0.34
1
06/29/21 17:55
75-25-2
Bromomethane
ND ug/L
2.0
1.7
1
06/29/21 17:55
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
4.0
1
06/29/21 17:55
78-93-3
Carbon disulfide
ND ug/L
2.0
0.73
1
06/29/21 17:55
75-15-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 43 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-14 Lab ID: 92546336016 Collected: 06/25/21 08:30 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 17:55
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 17:55
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 17:55
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 17:55
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 17:55
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 17:55
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 17:55
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 17:55
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 17:55
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/29/21 17:55
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 17:55
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 17:55
110-57-6
1,1-Dichloroethane
1.2
ug/L
1.0
0.37
1
06/29/21 17:55
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 17:55
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 17:55
75-35-4
cis-1,2-Dichloroethene
3.7
ug/L
1.0
0.38
1
06/29/21 17:55
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
06/29/21 17:55
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 17:55
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 17:55
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 17:55
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
38.7
1
06/29/21 17:55
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.30
1
06/29/21 17:55
100-41-4
2-Hexanone
ND
ug/L
5.0
0.48
1
06/29/21 17:55
591-78-6
lodomethane
ND
ug/L
20.0
9.7
1
06/29/21 17:55
74-88-4
Methylene Chloride
ND
ug/L
5.0
2.0
1
06/29/21 17:55
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
06/29/21 17:55
108-10-1
Styrene
ND
ug/L
1.0
0.29
1
06/29/21 17:55
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
06/29/21 17:55
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
06/29/21 17:55
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
06/29/21 17:55
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
06/29/21 17:55
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
06/29/21 17:55
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 17:55
79-00-5
Trichloroethene
ND
ug/L
1.0
0.38
1
06/29/21 17:55
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
06/29/21 17:55
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
06/29/21 17:55
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/29/21 17:55
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
06/29/21 17:55
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
06/29/21 17:55
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
06/29/21 17:55
460-00-4
1,2-Dichloroethane-d4 (S)
112
%
70-130
1
06/29/21 17:55
17060-07-0
Toluene-d8 (S)
107
%
70-130
1
06/29/21 17:55
2037-26-5
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 10/15/2021 02:14 PM
without the written
consent of Pace
Analytical Services, LLC.
Page 44 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-14 Lab ID: 92546336016 Collected: 06/25/21 08:30 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2320B Alkalinity
Alkalinity, Total as CaCO3
Iron, Ferrous
Iron, Ferrous
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
4500 Chloride
Chloride
5220D COD
Chemical Oxygen Demand
531013 TOC
Total Organic Carbon
Low Level Volatile Fatty Acids
Lactic Acid
Acetic Acid
Propionic Acid
Formic acid
Butyric Acid
Pyruvic Acid
i-Pentanoic Acid
Pentanoic Acid
i-Hexanoic Acid
Hexanoic Acid
Date: 10/15/2021 02:14 PM
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
29700 ug/L 5000
5000
1
07/02/2116:26
Analytical Method: SM 3500-Fe B-2011
Pace Analytical Services -Asheville
0.044J mg/L 0.50
0.040
1
07/06/2116:29
H3,N2
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100
50.0
1
07/01/2105:07
18496-25-8
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
1730 ug/L 1000
500
1
06/29/2123:52
14808-79-8
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
2250 ug/L 1000
500
1
07/07/2120:17
16887-00-6
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Pace Analytical Services -Asheville
ND ug/L 25000
12500
1
07/07/2102:33 07/07/2106:13
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
773J ug/L 1000
500
1
06/29/2123:43
7440-44-0
Analytical Method: AM23G
Pace Analytical Gulf Coast
0.057J mg/L 0.50
0.053
1
07/09/2101:08
50-21-5
0.38J mg/L 0.50
0.12
1
07/09/2101:08
64-19-7
ND mg/L 0.50
0.053
1
07/09/2101:08
79-09-4
4.9 mg/L 0.50
0.055
1
07/09/2101:08
64-18-6
ND mg/L 0.50
0.058
1
07/09/2101:08
107-92-6
ND mg/L 0.50
0.060
1
07/09/2101:08
127-17-3
ND mg/L 0.50
0.061
1
07/09/2101:08
503-74-2
ND mg/L 0.50
0.056
1
07/09/2101:08
109-52-4
ND mg/L 0.50
0.056
1
07/09/2101:08
646-07-1
ND mg/L 0.50
0.058
1
07/09/2101:08
142-62-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 45 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-21 Lab ID: 92546336017 Collected: 06/25/21 14:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
1.0J nM
1.9
0.49
1
07/07/2114:59
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Methane
ND ug/L
5.0
2.0
1
07/14/2114:35
74-82-8
Ethane
ND ug/L
1.0
0.17
1
07/14/2114:35
74-84-0
Ethene
ND ug/L
1.0
0.24
1
07/14/2114:35
74-85-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
ND ug/L
900
127
1
07/07/21 13:14
124-38-9
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
3.0
1
07/06/2116:19
07/07/2113:21
7440-36-0
Arsenic
ND ug/L
10.0
4.7
1
07/06/2116:19
07/07/2113:21
7440-38-2
Barium
55.4 ug/L
5.0
3.5
1
07/06/2116:19
07/07/2113:21
7440-39-3
Beryllium
ND ug/L
1.0
0.70
1
07/06/2116:19
07/07/2113:21
7440-41-7
Cadmium
ND ug/L
1.0
0.40
1
07/06/2116:19
07/07/2113:21
7440-43-9
Chromium
ND ug/L
5.0
3.7
1
07/06/2116:19
07/07/2113:21
7440-47-3
Cobalt
4.1J ug/L
5.0
3.6
1
07/06/2116:19
07/07/2113:21
7440-48-4
Copper
ND ug/L
5.0
4.3
1
07/06/2116:19
07/07/2113:21
7440-50-8
Lead
ND ug/L
5.0
4.5
1
07/06/2116:19
07/07/2113:21
7439-92-1
Nickel
ND ug/L
5.0
3.5
1
07/06/2116:19
07/07/2113:21
7440-02-0
Selenium
ND ug/L
10.0
4.7
1
07/06/2116:19
07/07/2113:21
7782-49-2
Silver
ND ug/L
5.0
2.5
1
07/06/2116:19
07/07/2113:21
7440-22-4
Vanadium
ND ug/L
5.0
3.9
1
07/06/2116:19
07/07/2113:21
7440-62-2
Zinc
ND ug/L
10.0
9.5
1
07/06/2116:19
07/07/2113:21
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services -Asheville
Thallium
ND ug/L
1.0
0.050
1
06/30/2116:15
07/02/2103:11
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
5.1
1
06/29/21 18:13
67-64-1
Acrylonitrile
ND ug/L
10.0
1.8
1
06/29/21 18:13
107-13-1
Benzene
ND ug/L
1.0
0.34
1
06/29/21 18:13
71-43-2
Bromochloromethane
ND ug/L
1.0
0.47
1
06/29/21 18:13
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.31
1
06/29/21 18:13
75-27-4
Bromoform
ND ug/L
1.0
0.34
1
06/29/21 18:13
75-25-2
Bromomethane
ND ug/L
2.0
1.7
1
06/29/21 18:13
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
4.0
1
06/29/21 18:13
78-93-3
Carbon disulfide
ND ug/L
2.0
0.73
1
06/29/21 18:13
75-15-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 46 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-21 Lab ID: 92546336017 Collected: 06/25/21 14:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 18:13
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 18:13
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 18:13
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 18:13
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 18:13
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 18:13
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 18:13
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 18:13
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 18:13
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/29/21 18:13
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 18:13
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 18:13
110-57-6
1,1-Dichloroethane
1.7
ug/L
1.0
0.37
1
06/29/21 18:13
75-34-3
1,2-Dichloroethane
0.57J
ug/L
1.0
0.32
1
06/29/21 18:13
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 18:13
75-35-4
cis-1,2-Dichloroethene
12.6
ug/L
1.0
0.38
1
06/29/21 18:13
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.40
1
06/29/21 18:13
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 18:13
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 18:13
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.36
1
06/29/21 18:13
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
38.7
1
06/29/21 18:13
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.30
1
06/29/21 18:13
100-41-4
2-Hexanone
ND
ug/L
5.0
0.48
1
06/29/21 18:13
591-78-6
lodomethane
ND
ug/L
20.0
9.7
1
06/29/21 18:13
74-88-4
Methylene Chloride
ND
ug/L
5.0
2.0
1
06/29/21 18:13
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
2.7
1
06/29/21 18:13
108-10-1
Styrene
ND
ug/L
1.0
0.29
1
06/29/21 18:13
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.31
1
06/29/21 18:13
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
06/29/21 18:13
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.29
1
06/29/21 18:13
127-18-4
Toluene
ND
ug/L
1.0
0.48
1
06/29/21 18:13
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.33
1
06/29/21 18:13
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 18:13
79-00-5
Trichloroethene
0.52J
ug/L
1.0
0.38
1
06/29/21 18:13
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
06/29/21 18:13
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.26
1
06/29/21 18:13
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.3
1
06/29/21 18:13
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39
1
06/29/21 18:13
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34
1
06/29/21 18:13
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
06/29/21 18:13
460-00-4
1,2-Dichloroethane-d4 (S)
119
%
70-130
1
06/29/21 18:13
17060-07-0
Toluene-d8 (S)
108
%
70-130
1
06/29/21 18:13
2037-26-5
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 10/15/2021 02:14 PM
without the written
consent of Pace
Analytical Services, LLC.
Page 47 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: MW-21 Lab ID: 92546336017 Collected: 06/25/21 14:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2320B Alkalinity
Alkalinity, Total as CaCO3
Iron, Ferrous
Iron, Ferrous
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
4500 Chloride
Chloride
5220D COD
Chemical Oxygen Demand
531013 TOC
Total Organic Carbon
Low Level Volatile Fatty Acids
Lactic Acid
Acetic Acid
Propionic Acid
Formic acid
Butyric Acid
Pyruvic Acid
i-Pentanoic Acid
Pentanoic Acid
i-Hexanoic Acid
Hexanoic Acid
Date: 10/15/2021 02:14 PM
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
33000 ug/L 5000
5000
1
07/02/2116:33
Analytical Method: SM 3500-Fe B-2011
Pace Analytical Services -Asheville
0.055J mg/L 0.50
0.040
1
07/06/2116:34
H3,N2
Analytical Method: SM 4500-S2D-2011
Pace Analytical Services -Asheville
ND ug/L 100
50.0
1
07/01/2105:08
18496-25-8
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
1420 ug/L 1000
500
1
06/30/2100:06
14808-79-8
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
29100 ug/L 1000
500
1
07/07/2120:18
16887-00-6
Analytical Method: SM 5220D-2011 Preparation
Method: SM 5220D-2011
Pace Analytical Services -Asheville
ND ug/L 25000
12500
1
07/07/2102:33 07/07/2106:13
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
1540 ug/L 1000
500
1
06/30/2100:01
7440-44-0
Analytical Method: AM23G
Pace Analytical Gulf Coast
ND mg/L 1.0
0.11
2
07/09/2102:01
50-21-5
0.67J mg/L 1.0
0.25
2
07/09/2102:01
64-19-7
ND mg/L 1.0
0.11
2
07/09/2102:01
79-09-4
12 mg/L 1.0
0.11
2
07/09/2102:01
64-18-6
ND mg/L 1.0
0.12
2
07/09/2102:01
107-92-6
ND mg/L 1.0
0.12
2
07/09/2102:01
127-17-3
ND mg/L 1.0
0.12
2
07/09/2102:01
503-74-2
ND mg/L 1.0
0.11
2
07/09/2102:01
109-52-4
ND mg/L 1.0
0.11
2
07/09/2102:01
646-07-1
ND mg/L 1.0
0.12
2
07/09/2102:01
142-62-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 48 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: SCALEHOUSE Lab ID: 92546336018 Collected: 06/25/21 12:50 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/06/2116:19
07/07/2113:24
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2113:24
7440-38-2
Barium
13.0
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2113:24
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/2116:19
07/07/2113:24
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/06/2116:19
07/07/2113:24
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/2116:19
07/07/2113:24
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/06/2116:19
07/07/2113:24
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/06/2116:19
07/07/2113:24
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/06/2116:19
07/07/2113:24
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/06/2116:19
07/07/2113:24
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/06/2116:19
07/07/2113:24
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/2116:19
07/07/2113:24
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/06/2116:19
07/07/2113:24
7440-62-2
Zinc
45.2
ug/L
10.0
9.5
1
07/06/21 16:19
07/07/21 13:24
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
1.0
0.050
1
06/30/2116:15
07/02/2103:15
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/29/21 15:17
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/29/21 15:17
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/29/21 15:17
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/29/21 15:17
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/29/21 15:17
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/29/21 15:17
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/29/21 15:17
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/29/21 15:17
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/29/21 15:17
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 15:17
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 15:17
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 15:17
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 15:17
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 15:17
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 15:17
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 15:17
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 15:17
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 15:17
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/29/21 15:17
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 15:17
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 15:17
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/29/21 15:17
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 15:17
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 15:17
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 49 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: SCALEHOUSE Lab ID: 92546336018 Collected: 06/25/21 12:50 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/29/21 15:17
156-59-2
ND
ug/L
1.0
0.40
1
06/29/21 15:17
156-60-5
ND
ug/L
1.0
0.36
1
06/29/21 15:17
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 15:17
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/21 15:17
10061-02-6
ND
ug/L
150
38.7
1
06/29/21 15:17
123-91-1
ND
ug/L
1.0
0.30
1
06/29/21 15:17
100-41-4
ND
ug/L
5.0
0.48
1
06/29/21 15:17
591-78-6
ND
ug/L
20.0
9.7
1
06/29/21 15:17
74-88-4
ND
ug/L
5.0
2.0
1
06/29/21 15:17
75-09-2
ND
ug/L
5.0
2.7
1
06/29/21 15:17
108-10-1
ND
ug/L
1.0
0.29
1
06/29/21 15:17
100-42-5
ND
ug/L
1.0
0.31
1
06/29/21 15:17
630-20-6
ND
ug/L
1.0
0.22
1
06/29/21 15:17
79-34-5
ND
ug/L
1.0
0.29
1
06/29/21 15:17
127-18-4
ND
ug/L
1.0
0.48
1
06/29/21 15:17
108-88-3
ND
ug/L
1.0
0.33
1
06/29/21 15:17
71-55-6
ND
ug/L
1.0
0.32
1
06/29/21 15:17
79-00-5
ND
ug/L
1.0
0.38
1
06/29/21 15:17
79-01-6
ND
ug/L
1.0
0.30
1
06/29/21 15:17
75-69-4
ND
ug/L
1.0
0.26
1
06/29/21 15:17
96-18-4
ND
ug/L
2.0
1.3
1
06/29/21 15:17
108-05-4
ND
ug/L
1.0
0.39
1
06/29/21 15:17
75-01-4
ND
ug/L
1.0
0.34
1
06/29/21 15:17
1330-20-7
98
%
70-130
1
06/29/21 15:17
460-00-4
115
%
70-130
1
06/29/21 15:17
17060-07-0
106
%
70-130
1
06/29/21 15:17
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 50 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: WSW-2 Lab ID: 92546336019 Collected: 06/25/21 14:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/06/21 16:19
07/07/21 13:28
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 13:28
7440-38-2
Barium
3.8J
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 13:28
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/06/21 16:19
07/07/21 13:28
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/06/21 16:19
07/07/21 13:28
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/06/21 16:19
07/07/21 13:28
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/06/21 16:19
07/07/21 13:28
7440-48-4
Copper
43.5
ug/L
5.0
4.3
1
07/06/21 16:19
07/07/21 13:28
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/06/21 16:19
07/07/21 13:28
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/06/21 16:19
07/07/21 13:28
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/06/21 16:19
07/07/21 13:28
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/06/21 16:19
07/07/21 13:28
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/06/21 16:19
07/07/21 13:28
7440-62-2
Zinc
15.4
ug/L
10.0
9.5
1
07/06/21 16:19
07/07/21 13:28
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
1.0
0.050
1
06/30/2116:15
07/02/2103:19
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/29/21 15:35
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/29/21 15:35
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/29/21 15:35
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/29/21 15:35
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/29/21 15:35
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/29/21 15:35
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/29/21 15:35
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/29/21 15:35
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/29/21 15:35
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 15:35
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 15:35
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 15:35
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 15:35
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 15:35
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 15:35
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 15:35
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 15:35
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 15:35
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/29/21 15:35
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 15:35
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 15:35
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/29/21 15:35
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 15:35
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 15:35
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 51 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Sample: WSW-2 Lab ID: 92546336019 Collected: 06/25/21 14:00 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 10/15/2021 02:14 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/29/21 15:35
156-59-2
ND
ug/L
1.0
0.40
1
06/29/21 15:35
156-60-5
ND
ug/L
1.0
0.36
1
06/29/21 15:35
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 15:35
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/21 15:35
10061-02-6
ND
ug/L
150
38.7
1
06/29/21 15:35
123-91-1
ND
ug/L
1.0
0.30
1
06/29/21 15:35
100-41-4
ND
ug/L
5.0
0.48
1
06/29/21 15:35
591-78-6
ND
ug/L
20.0
9.7
1
06/29/21 15:35
74-88-4
ND
ug/L
5.0
2.0
1
06/29/21 15:35
75-09-2
ND
ug/L
5.0
2.7
1
06/29/21 15:35
108-10-1
ND
ug/L
1.0
0.29
1
06/29/21 15:35
100-42-5
ND
ug/L
1.0
0.31
1
06/29/21 15:35
630-20-6
ND
ug/L
1.0
0.22
1
06/29/21 15:35
79-34-5
ND
ug/L
1.0
0.29
1
06/29/21 15:35
127-18-4
ND
ug/L
1.0
0.48
1
06/29/21 15:35
108-88-3
ND
ug/L
1.0
0.33
1
06/29/21 15:35
71-55-6
ND
ug/L
1.0
0.32
1
06/29/21 15:35
79-00-5
ND
ug/L
1.0
0.38
1
06/29/21 15:35
79-01-6
ND
ug/L
1.0
0.30
1
06/29/21 15:35
75-69-4
ND
ug/L
1.0
0.26
1
06/29/21 15:35
96-18-4
ND
ug/L
2.0
1.3
1
06/29/21 15:35
108-05-4
ND
ug/L
1.0
0.39
1
06/29/21 15:35
75-01-4
ND
ug/L
1.0
0.34
1
06/29/21 15:35
1330-20-7
97
%
70-130
1
06/29/21 15:35
460-00-4
113
%
70-130
1
06/29/21 15:35
17060-07-0
110
%
70-130
1
06/29/21 15:35
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 52 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 715604 Analysis Method: AM20GAX
QC Batch Method: AM20GAX Analysis Description: Indicator Gases Bubble Strip H2
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
METHOD BLANK: 2209966 Matrix: Air
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Hydrogen nM ND 1.9 0.49 07/07/2111:39
LABORATORY CONTROL SAMPLE & LCSD: 2209967 2209968
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Hydrogen nM 12 12 13 104 107 70-130 3 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 53 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 715951 Analysis Method: AM20GAX
QC Batch Method: AM20GAX Analysis Description: Indicator Gases Water LHC
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
METHOD BLANK: 2212022
Matrix: Water
Associated Lab Samples:
92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
Blank Reporting
Parameter
Units
Result Limit
MDL Analyzed Qualifiers
Methane
ug/L
ND 5.0
2.0 07/14/2111:57
Ethane
ug/L
ND 1.0
0.17 07/14/2111:57
Ethene
ug/L
ND 1.0
0.24 07/14/2111:57
LABORATORY CONTROL SAMPLE & LCSD:
2212023
2212024
Spike
LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units Conc.
Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
Methane
ug/L 750
720 740
97 99
70-130 2 20
Ethane
ug/L 38
44 44
116 116
70-130 0 20
Ethene
ug/L 35
41 41
116 116
70-130 0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 54 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 715570 Analysis Method: RSK-175
QC Batch Method: RSK-175 Analysis Description: EPA RSK 175 CO2
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92546336011, 92546336012, 92546336013, 92546336014, 92546336015, 92546336016
METHOD BLANK: 2209863 Matrix: Water
Associated Lab Samples: 92546336011, 92546336012, 92546336013, 92546336014, 92546336015, 92546336016
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Carbon dioxide ug/L ND 900 127 07/07/21 09:40
LABORATORY CONTROL SAMPLE & LCSD: 2209864 2209865
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Carbon dioxide ug/L 8700 8220 8480 94 97 38-147 3 40
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 55 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 715618 Analysis Method: RSK-175
QC Batch Method: RSK-175 Analysis Description: EPA RSK 175 CO2
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92546336017
METHOD BLANK: 2210052 Matrix: Water
Associated Lab Samples: 92546336017
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Carbon dioxide ug/L ND 900 127 07/07/21 12:57
LABORATORY CONTROL SAMPLE & LCSD: 2210053 2210054
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Carbon dioxide ug/L 8700 7980 8860 92 102 38-147 10 40
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 56 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 631641 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546336001, 92546336002, 92546336003, 92546336004, 92546336005, 92546336006, 92546336007,
92546336008,92546336009,92546336010,92546336011,92546336012,92546336013,92546336014,
92546336015,92546336016,92546336017,92546336018,92546336019
METHOD BLANK: 3318285 Matrix: Water
Associated Lab Samples: 92546336001, 92546336002, 92546336003, 92546336004, 92546336005, 92546336006, 92546336007,
92546336008,92546336009,92546336010,92546336011,92546336012,92546336013,92546336014,
92546336015,92546336016,92546336017,92546336018,92546336019
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Antimony
ug/L
ND
5.0
3.0
07/07/2111:59
Arsenic
ug/L
ND
10.0
4.7
07/07/2111:59
Barium
ug/L
ND
5.0
3.5
07/07/2111:59
Beryllium
ug/L
ND
1.0
0.70
07/07/2111:59
Cadmium
ug/L
ND
1.0
0.40
07/07/2111:59
Chromium
ug/L
ND
5.0
3.7
07/07/2111:59
Cobalt
ug/L
ND
5.0
3.6
07/07/2111:59
Copper
ug/L
ND
5.0
4.3
07/07/2111:59
Lead
ug/L
ND
5.0
4.5
07/07/2111:59
Nickel
ug/L
ND
5.0
3.5
07/07/2111:59
Selenium
ug/L
ND
10.0
4.7
07/07/2111:59
Silver
ug/L
ND
5.0
2.5
07/07/2111:59
Vanadium
ug/L
ND
5.0
3.9
07/07/2111:59
Zinc
ug/L
ND
10.0
9.5
07/07/2111:59
LABORATORY CONTROL SAMPLE:
Parameter
3318286
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
486
97
80-120
Arsenic
ug/L
500
481
96
80-120
Barium
ug/L
500
488
98
80-120
Beryllium
ug/L
500
500
100
80-120
Cadmium
ug/L
500
490
98
80-120
Chromium
ug/L
500
498
100
80-120
Cobalt
ug/L
500
476
95
80-120
Copper
ug/L
500
506
101
80-120
Lead
ug/L
500
478
96
80-120
Nickel
ug/L
500
491
98
80-120
Selenium
ug/L
500
472
94
80-120
Silver
ug/L
250
246
98
80-120
Vanadium
ug/L
500
496
99
80-120
Zinc
ug/L
500
475
95
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 125

lV11.1 Analytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
SURRY CLOSED
92546336
MT AIRY
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3318287
3318288
MS
MSD
92546336001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
490
488
98
97
75-125
0
20
Arsenic
ug/L
ND
500
500
492
500
98
100
75-125
2
20
Barium
ug/L
5.7
500
500
488
493
96
97
75-125
1
20
Beryllium
ug/L
ND
500
500
500
505
100
101
75-125
1
20
Cadmium
ug/L
0.73J
500
500
500
504
100
101
75-125
1
20
Chromium
ug/L
ND
500
500
502
511
100
102
75-125
2
20
Cobalt
ug/L
ND
500
500
470
474
94
95
75-125
1
20
Copper
ug/L
ND
500
500
499
509
100
102
75-125
2
20
Lead
ug/L
ND
500
500
479
484
96
97
75-125
1
20
Nickel
ug/L
ND
500
500
488
493
98
99
75-125
1
20
Selenium
ug/L
5AJ
500
500
506
507
100
100
75-125
0
20
Silver
ug/L
ND
250
250
248
252
99
101
75-125
1
20
Vanadium
ug/L
ND
500
500
500
509
100
102
75-125
2
20
Zinc
ug/L
ND
500
500
482
486
96
97
75-125
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 58 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 630470 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546336001, 92546336002, 92546336003, 92546336004, 92546336005, 92546336006, 92546336007,
92546336008,92546336009,92546336010,92546336011,92546336012,92546336013,92546336014,
92546336015,92546336016,92546336017,92546336018,92546336019
METHOD BLANK: 3312731 Matrix: Water
Associated Lab Samples: 92546336001, 92546336002, 92546336003, 92546336004, 92546336005, 92546336006, 92546336007,
92546336008,92546336009,92546336010,92546336011,92546336012,92546336013,92546336014,
92546336015,92546336016,92546336017,92546336018,92546336019
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 1.0 0.050 07/02/2101:23
LABORATORY CONTROL SAMPLE: 3312732
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 25 23.9 96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3312733 3312734
MS MSD
92546336001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 25 25 22.2 24.0 89 96 75-125 8 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 59 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 629502 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92546336001, 92546336002, 92546336003, 92546336004, 92546336005, 92546336006, 92546336007,
92546336008,92546336009,92546336010
METHOD BLANK: 3308398 Matrix: Water
Associated Lab Samples: 92546336001, 92546336002, 92546336003, 92546336004, 92546336005, 92546336006, 92546336007,
92546336008,92546336009,92546336010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
06/25/21 11:01
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
06/25/21 11:01
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
06/25/21 11:01
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
06/25/21 11:01
1,1-Dichloroethane
ug/L
ND
1.0
0.37
06/25/21 11:01
1,1-Dichloroethene
ug/L
ND
1.0
0.35
06/25/21 11:01
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
06/25/21 11:01
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
06/25/21 11:01
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
06/25/21 11:01
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
06/25/21 11:01
1,2-Dichloroethane
ug/L
ND
1.0
0.32
06/25/21 11:01
1,2-Dichloropropane
ug/L
ND
1.0
0.36
06/25/21 11:01
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
06/25/21 11:01
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
38.7
06/25/21 11:01
2-Butanone (MEK)
ug/L
ND
5.0
4.0
06/25/21 11:01
2-Hexanone
ug/L
ND
5.0
0.48
06/25/21 11:01
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
06/25/21 11:01
Acetone
ug/L
ND
25.0
5.1
06/25/21 11:01
Acrylonitrile
ug/L
ND
10.0
1.8
06/25/21 11:01
Benzene
ug/L
ND
1.0
0.34
06/25/21 11:01
Bromochloromethane
ug/L
ND
1.0
0.47
06/25/21 11:01
Bromodichloromethane
ug/L
ND
1.0
0.31
06/25/21 11:01
Bromoform
ug/L
ND
1.0
0.34
06/25/21 11:01
Bromomethane
ug/L
ND
2.0
1.7
06/25/21 11:01
Carbon disulfide
ug/L
ND
2.0
0.73
06/25/21 11:01
Carbon tetrachloride
ug/L
ND
1.0
0.33
06/25/21 11:01
Chlorobenzene
ug/L
ND
1.0
0.28
06/25/21 11:01
Chloroethane
ug/L
ND
1.0
0.65
06/25/21 11:01
Chloroform
ug/L
ND
5.0
1.6
06/25/21 11:01
Chloromethane
ug/L
ND
1.0
0.54
06/25/21 11:01 v2
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
06/25/21 11:01
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/25/21 11:01
Dibromochloromethane
ug/L
ND
1.0
0.36
06/25/21 11:01
Dibromomethane
ug/L
ND
1.0
0.39
06/25/21 11:01
Ethylbenzene
ug/L
ND
1.0
0.30
06/25/21 11:01
lodomethane
ug/L
ND
20.0
9.7
06/25/21 11:01
Methylene Chloride
ug/L
ND
5.0
2.0
06/25/21 11:01
Styrene
ug/L
ND
1.0
0.29
06/25/21 11:01
Tetrachloroethene
ug/L
ND
1.0
0.29
06/25/21 11:01
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
METHOD BLANK: 3308398 Matrix: Water
Associated Lab Samples: 92546336001, 92546336002, 92546336003, 92546336004, 92546336005, 92546336006, 92546336007,
92546336008,92546336009,92546336010
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Toluene
ug/L
ND
1.0
0.48
06/25/21 11:01
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
06/25/21 11:01
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/25/21 11:01
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
06/25/21 11:01
Trichloroethene
ug/L
ND
1.0
0.38
06/25/21 11:01
Trichlorofluoromethane
ug/L
ND
1.0
0.30
06/25/21 11:01
Vinyl acetate
ug/L
ND
2.0
1.3
06/25/21 11:01
Vinyl chloride
ug/L
ND
1.0
0.39
06/25/21 11:01
Xylene (Total)
ug/L
ND
1.0
0.34
06/25/21 11:01
1,2-Dichloroethane-d4 (S)
%
92
70-130
06/25/21 11:01
4-Bromofluorobenzene (S)
%
96
70-130
06/25/21 11:01
Toluene-d8 (S)
%
105
70-130
06/25/21 11:01
LABORATORY CONTROL SAMPLE:
Parameter
3308399
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.0
102
70-130
1,1,1-Trichloroethane
ug/L
50
44.4
89
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.0
100
70-130
1,1,2-Trichloroethane
ug/L
50
49.2
98
70-130
1,1-Dichloroethane
ug/L
50
45.0
90
70-130
1,1-Dichloroethene
ug/L
50
47.6
95
70-132
1,2,3-Trichloropropane
ug/L
50
50.0
100
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
52.9
106
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.5
103
70-130
1,2-Dichlorobenzene
ug/L
50
49.3
99
70-130
1,2-Dichloroethane
ug/L
50
42.2
84
70-130
1,2-Dichloropropane
ug/L
50
48.0
96
70-130
1,4-Dichlorobenzene
ug/L
50
49.7
99
70-130
1,4-Dioxane(p-Dioxane)
ug/L
1000
1040
104
70-137
2-Butanone (MEK)
ug/L
100
83.5
83
70-133
2-Hexanone
ug/L
100
93.9
94
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
94.0
94
70-130
Acetone
ug/L
100
88.1
88
70-144
Acrylonitrile
ug/L
250
221
88
70-130
Benzene
ug/L
50
47.7
95
70-130
Bromochloromethane
ug/L
50
43.7
87
70-130
Bromodichloromethane
ug/L
50
48.6
97
70-130
Bromoform
ug/L
50
50.4
101
70-131
Bromomethane
ug/L
50
51.2
102
30-177
Carbon disulfide
ug/L
50
47.3
95
70-133
Carbon tetrachloride
ug/L
50
49.7
99
70-130
Chlorobenzene
ug/L
50
47.8
96
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 61 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
LABORATORY CONTROL SAMPLE:
Parameter
3308399
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloroethane
ug/L
50
58.6
Chloroform
ug/L
50
44.5
Chloromethane
ug/L
50
36.4
cis-1,2-Dichloroethene
ug/L
50
42.6
cis-1,3-Dichloropropene
ug/L
50
50.6
Dibromochloromethane
ug/L
50
49.5
Dibromomethane
ug/L
50
46.8
Ethylbenzene
ug/L
50
47.2
lodomethane
ug/L
100
104
Methylene Chloride
ug/L
50
40.9
Styrene
ug/L
50
48.5
Tetrachloroethene
ug/L
50
48.4
Toluene
ug/L
50
46.3
trans-1,2-Dichloroethene
ug/L
50
47.0
trans- 1,3-Dichloropropene
ug/L
50
50.2
trans-1,4-Dichloro-2-butene
ug/L
50
55.0
Trichloroethene
ug/L
50
48.3
Trichlorofluoromethane
ug/L
50
41.5
Vinyl acetate
ug/L
100
90.8
Vinyl chloride
ug/L
50
43.0
Xylene (Total)
ug/L
150
144
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
117
46-131
89
70-130
73
49-130 v3
85
70-130
101
70-130
99
70-130
94
70-130
94
70-130
104
47-140
82
68-130
97
70-130
97
70-130
93
70-130
94
70-130
100
70-130
110
25-200
97
70-130
83
61-130
91
70-140
86
59-142
96
70-130
85
70-130
97
70-130
98
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3308400
MS
92546350001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3308401
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.0
21.9
110
109
70-135
0
30
1,1,1-Trichloroethane
ug/L
ND
20
20
21.9
23.6
109
118
70-148
8
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.3
21.2
107
106
70-131
1
30
1,1,2-Trichloroethane
ug/L
ND
20
20
21.7
21.3
109
106
70-136
2
30
1,1-Dichloroethane
ug/L
10.1
20
20
32.9
34.1
114
120
70-147
4
30
1,1-Dichloroethene
ug/L
ND
20
20
23.8
24.2
119
121
70-158
1
30
1,2,3-Trichloropropane
ug/L
ND
20
20
21.6
22.2
108
111
67-137
3
30
1,2-Dibromo-3-
ug/L
ND
20
20
21.2
19.7
106
98
69-136
8
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.2
22.5
111
112
70-137
1
30
1,2-Dichlorobenzene
ug/L
0.62J
20
20
22.4
23.4
109
114
70-133
4
30
1,2-Dichloroethane
ug/L
ND
20
20
21.0
20.9
105
104
67-138
1
30
1,2-Dichloropropane
ug/L
ND
20
20
22.4
22.1
112
110
70-138
2
30
1,4-Dichlorobenzene
ug/L
ND
20
20
32.8
34.5
164
172
70-133
5
30 M1
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
400
461
429
115
107
69-146
7
30
2-Butanone (MEK)
ug/L
6.2
40
40
45.2
48.1
97
105
61-147
6
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 62 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3308400
3308401
MS
MSD
92546350001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
2-Hexanone
ug/L
ND
40
40
35.8
36.3
89
91
67-139
2
30
4-Methyl-2-pentanone
ug/L
ND
40
40
39.9
37.3
97
91
67-136
7
30
(MIBK)
Acetone
ug/L
ND
40
40
46.3
50.3
116
126
55-159
8
30
Acrylonitrile
ug/L
ND
100
100
105
104
105
104
68-140
1
30
Benzene
ug/L
3.9
20
20
27.3
27.1
117
116
67-150
1
30
Bromochloromethane
ug/L
ND
20
20
21.0
21.2
105
106
70-146
1
30
Bromodichloromethane
ug/L
ND
20
20
21.7
21.8
108
109
70-138
0
30
Bromoform
ug/L
ND
20
20
20.2
19.7
101
99
57-138
2
30
Bromomethane
ug/L
ND
20
20
23.7
24.2
119
121
10-200
2
30
Carbon disulfide
ug/L
ND
20
20
27.6
24.5
138
122
70-152
12
30
Carbon tetrachloride
ug/L
ND
20
20
24.2
23.4
121
117
70-147
3
30
Chlorobenzene
ug/L
53.6
20
20
77.0
72.6
117
95
70-137
6
30
Chloroethane
ug/L
4.3
20
20
30.7
29.3
132
125
51-166
5
30
Chloroform
ug/L
ND
20
20
23.8
21.9
119
110
70-144
8
30
Chloromethane
ug/L
ND
20
20
17.6
17.9
88
90
24-161
2
30 v3
cis-1,2-Dichloroethene
ug/L
14.8
20
20
36.7
37.2
110
112
67-148
1
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.2
21.0
106
105
70-142
1
30
Dibromochloromethane
ug/L
ND
20
20
20.7
21.1
103
105
68-138
2
30
Dibromomethane
ug/L
ND
20
20
21.4
21.0
107
105
70-134
2
30
Ethylbenzene
ug/L
0.64J
20
20
23.4
22.8
114
111
68-143
2
30
Iodomethane
ug/L
ND
40
40
45.8
52.7
115
132
20-161
14
30
Methylene Chloride
ug/L
ND
20
20
20.6
22.6
95
105
64-148
9
30
Styrene
ug/L
ND
20
20
22.7
22.9
114
114
70-136
1
30
Tetrachloroethene
ug/L
ND
20
20
21.8
22.3
109
112
70-139
2
30
Toluene
ug/L
ND
20
20
22.6
22.0
110
108
47-157
2
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
23.0
23.5
115
117
70-149
2
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
21.0
19.9
105
99
70-138
5
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
18.0
17.4
90
87
31-145
4
30
Trichloroethene
ug/L
ND
20
20
22.3
22.4
112
112
70-149
0
30
Trichlorofluoromethane
ug/L
ND
20
20
21.7
21.8
108
109
61-154
1
30
Vinyl acetate
ug/L
ND
40
40
36.4
34.4
91
86
48-156
6
30
Vinyl chloride
ug/L
ND
20
20
23.3
23.9
117
120
55-172
3
30
Xylene (Total)
ug/L
0.68J
60
60
70.0
69.9
115
115
66-145
0
30
1,2-Dichloroethane-d4 (S)
%
88
93
70-130
4-Bromofluorobenzene (S)
%
97
96
70-130
Toluene-d8 (S)
%
98
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 63 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 630255 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017,
92546336018,92546336019
METHOD BLANK: 3311481
Matrix: Water
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017,
92546336018,92546336019
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
06/29/21 11:30
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
06/29/21 11:30
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
06/29/21 11:30
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
06/29/21 11:30
1,1-Dichloroethane
ug/L
ND
1.0
0.37
06/29/21 11:30
1,1-Dichloroethene
ug/L
ND
1.0
0.35
06/29/21 11:30
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
06/29/21 11:30
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
06/29/21 11:30
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
06/29/21 11:30
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
06/29/21 11:30
1,2-Dichloroethane
ug/L
ND
1.0
0.32
06/29/21 11:30
1,2-Dichloropropane
ug/L
ND
1.0
0.36
06/29/21 11:30
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
06/29/21 11:30
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
38.7
06/29/21 11:30
2-Butanone (MEK)
ug/L
ND
5.0
4.0
06/29/21 11:30
2-Hexanone
ug/L
ND
5.0
0.48
06/29/21 11:30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
06/29/21 11:30
Acetone
ug/L
ND
25.0
5.1
06/29/21 11:30
Acrylonitrile
ug/L
ND
10.0
1.8
06/29/21 11:30
Benzene
ug/L
ND
1.0
0.34
06/29/21 11:30
Bromochloromethane
ug/L
ND
1.0
0.47
06/29/21 11:30
Bromodichloromethane
ug/L
ND
1.0
0.31
06/29/21 11:30
Bromoform
ug/L
ND
1.0
0.34
06/29/21 11:30
Bromomethane
ug/L
ND
2.0
1.7
06/29/21 11:30
Carbon disulfide
ug/L
ND
2.0
0.73
06/29/21 11:30
Carbon tetrachloride
ug/L
ND
1.0
0.33
06/29/21 11:30
Chlorobenzene
ug/L
ND
1.0
0.28
06/29/21 11:30
Chloroethane
ug/L
ND
1.0
0.65
06/29/21 11:30
Chloroform
ug/L
ND
5.0
1.6
06/29/21 11:30
Chloromethane
ug/L
ND
1.0
0.54
06/29/21 11:30
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
06/29/21 11:30
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/29/21 11:30
Dibromochloromethane
ug/L
ND
1.0
0.36
06/29/21 11:30
Dibromomethane
ug/L
ND
1.0
0.39
06/29/21 11:30
Ethylbenzene
ug/L
ND
1.0
0.30
06/29/21 11:30
lodomethane
ug/L
ND
20.0
9.7
06/29/21 11:30
Methylene Chloride
ug/L
ND
5.0
2.0
06/29/21 11:30
Styrene
ug/L
ND
1.0
0.29
06/29/21 11:30
Tetrachloroethene
ug/L
ND
1.0
0.29
06/29/21 11:30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 64 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
METHOD BLANK: 3311481 Matrix: Water
Associated Lab Samples: 92546336011, 92546336012, 92546336013, 92546336014, 92546336015, 92546336016, 92546336017,
92546336018,92546336019
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
0.48
06/29/21 11:30
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
06/29/21 11:30
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/29/21 11:30
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
06/29/21 11:30
Trichloroethene
ug/L
ND
1.0
0.38
06/29/21 11:30
Trichlorofluoromethane
ug/L
ND
1.0
0.30
06/29/21 11:30
Vinyl acetate
ug/L
ND
2.0
1.3
06/29/21 11:30
Vinyl chloride
ug/L
ND
1.0
0.39
06/29/21 11:30
Xylene (Total)
ug/L
ND
1.0
0.34
06/29/21 11:30
1,2-Dichloroethane-d4 (S)
%
111
70-130
06/29/21 11:30
4-Bromofluorobenzene (S)
%
97
70-130
06/29/21 11:30
Toluene-d8 (S)
%
107
70-130
06/29/21 11:30
LABORATORY CONTROL SAMPLE:
Parameter
3311482
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
49.6
99
70-130
1,1,1-Trichloroethane
ug/L
50
47.1
94
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.0
100
70-130
1,1,2-Trichloroethane
ug/L
50
49.4
99
70-130
1,1-Dichloroethane
ug/L
50
48.9
98
70-130
1,1-Dichloroethene
ug/L
50
48.2
96
70-132
1,2,3-Trichloropropane
ug/L
50
48.8
98
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
55.1
110
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.5
103
70-130
1,2-Dichlorobenzene
ug/L
50
52.5
105
70-130
1,2-Dichloroethane
ug/L
50
47.8
96
70-130
1,2-Dichloropropane
ug/L
50
49.1
98
70-130
1,4-Dichlorobenzene
ug/L
50
51.2
102
70-130
1,4-Dioxane (p-Dioxane)
ug/L
1000
1020
102
70-137
2-Butanone (MEK)
ug/L
100
105
105
70-133
2-Hexanone
ug/L
100
100
100
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
99.3
99
70-130
Acetone
ug/L
100
107
107
70-144
Acrylonitrile
ug/L
250
247
99
70-130
Benzene
ug/L
50
47.2
94
70-130
Bromochloromethane
ug/L
50
47.3
95
70-130
Bromodichloromethane
ug/L
50
47.9
96
70-130
Bromoform
ug/L
50
44.0
88
70-131
Bromomethane
ug/L
50
55.2
110
30-177
Carbon disulfide
ug/L
50
50.0
100
70-133
Carbon tetrachloride
ug/L
50
47.2
94
70-130
Chlorobenzene
ug/L
50
46.8
94
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 65 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
LABORATORY CONTROL SAMPLE:
Parameter
3311482
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Chloroethane
ug/L
50
62.8
126
46-131
Chloroform
ug/L
50
46.4
93
70-130
Chloromethane
ug/L
50
46.7
93
49-130
cis-1,2-Dichloroethene
ug/L
50
49.2
98
70-130
cis-1,3-Dichloropropene
ug/L
50
50.2
100
70-130
Dibromochloromethane
ug/L
50
52.3
105
70-130
Dibromomethane
ug/L
50
46.8
94
70-130
Ethylbenzene
ug/L
50
46.1
92
70-130
lodomethane
ug/L
100
104
104
47-140
Methylene Chloride
ug/L
50
47.9
96
68-130
Styrene
ug/L
50
48.5
97
70-130
Tetrachloroethene
ug/L
50
44.8
90
70-130
Toluene
ug/L
50
45.9
92
70-130
trans-1,2-Dichloroethene
ug/L
50
49.9
100
70-130
trans- 1,3-Dichloropropene
ug/L
50
52.0
104
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
63.3
127
25-200
Trichloroethene
ug/L
50
46.6
93
70-130
Trichlorofluoromethane
ug/L
50
43.6
87
61-130
Vinyl acetate
ug/L
100
118
118
70-140
Vinyl chloride
ug/L
50
47.1
94
59-142
Xylene (Total)
ug/L
150
142
95
70-130
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
96
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3311483
MS
92546336011 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3311484
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.1
20.9
106
104
70-135
1
30
1,1,1-Trichloroethane
ug/L
ND
20
20
22.6
22.5
113
112
70-148
1
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.5
23.0
112
115
70-131
2
30
1,1,2-Trichloroethane
ug/L
ND
20
20
21.7
20.9
109
105
70-136
4
30
1,1-Dichloroethane
ug/L
ND
20
20
24.5
23.3
123
116
70-147
5
30
1,1-Dichloroethene
ug/L
ND
20
20
23.5
25.3
117
127
70-158
8
30
1,2,3-Trichloropropane
ug/L
ND
20
20
22.9
23.3
115
116
67-137
1
30
1,2-Dibromo-3-
ug/L
ND
20
20
21.7
20.1
109
100
69-136
8
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.4
22.5
107
112
70-137
5
30
1,2-Dichlorobenzene
ug/L
ND
20
20
21.3
22.1
106
110
70-133
4
30
1,2-Dichloroethane
ug/L
ND
20
20
22.8
22.7
114
113
67-138
0
30
1,2-Dichloropropane
ug/L
ND
20
20
22.7
22.8
113
114
70-138
1
30
1,4-Dichlorobenzene
ug/L
ND
20
20
21.5
21.7
108
109
70-133
1
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
400
409
442
102
110
69-146
8
30
2-Butanone (MEK)
ug/L
ND
40
40
50.9
48.9
127
122
61-147
4
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 66 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3311483
3311484
MS
MSD
92546336011
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
2-Hexanone
ug/L
ND
40
40
42.0
44.0
105
110
67-139
5
30
4-Methyl-2-pentanone
ug/L
ND
40
40
42.7
45.2
107
113
67-136
6
30
(MIBK)
Acetone
ug/L
ND
40
40
49.7
47.7
124
119
55-159
4
30
Acrylonitrile
ug/L
ND
100
100
122
116
122
116
68-140
5
30
Benzene
ug/L
ND
20
20
22.7
22.7
113
114
67-150
0
30
Bromochloromethane
ug/L
ND
20
20
21.5
20.8
107
104
70-146
3
30
Bromodichloromethane
ug/L
ND
20
20
20.8
20.9
104
105
70-138
0
30
Bromoform
ug/L
ND
20
20
17.2
17.6
86
88
57-138
2
30
Bromomethane
ug/L
ND
20
20
28.7
28.1
144
140
10-200
2
30
Carbon disulfide
ug/L
ND
20
20
24.6
24.3
123
122
70-152
1
30
Carbon tetrachloride
ug/L
ND
20
20
21.9
21.0
110
105
70-147
4
30
Chlorobenzene
ug/L
ND
20
20
20.8
22.2
104
111
70-137
6
30
Chloroethane
ug/L
ND
20
20
26.2
25.1
131
125
51-166
4
30
Chloroform
ug/L
ND
20
20
24.6
24.4
123
122
70-144
1
30
Chloromethane
ug/L
ND
20
20
22.9
23.7
114
118
24-161
4
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
23.9
23.2
119
116
67-148
3
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.9
21.4
105
107
70-142
2
30
Dibromochloromethane
ug/L
ND
20
20
20.5
21.3
102
106
68-138
4
30
Dibromomethane
ug/L
ND
20
20
19.9
20.5
99
102
70-134
3
30
Ethylbenzene
ug/L
ND
20
20
21.1
22.4
106
112
68-143
6
30
Iodomethane
ug/L
ND
40
40
37.3
41.3
93
103
20-161
10
30
Methylene Chloride
ug/L
ND
20
20
23.2
22.6
116
113
64-148
2
30
Styrene
ug/L
ND
20
20
21.0
22.0
105
110
70-136
5
30
Tetrachloroethene
ug/L
ND
20
20
20.4
20.3
102
101
70-139
1
30
Toluene
ug/L
ND
20
20
21.8
22.3
109
112
47-157
2
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.6
23.9
123
119
70-149
3
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
21.1
21.8
105
109
70-138
4
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
21.2
22.4
106
112
31-145
5
30
Trichloroethene
ug/L
ND
20
20
20.4
21.8
102
109
70-149
6
30
Trichlorofluoromethane
ug/L
ND
20
20
21.1
22.6
106
113
61-154
7
30
Vinyl acetate
ug/L
ND
40
40
49.8
48.1
125
120
48-156
4
30
Vinyl chloride
ug/L
ND
20
20
24.2
24.0
121
120
55-172
1
30
Xylene (Total)
ug/L
ND
60
60
64.1
67.0
107
112
66-145
4
30
1,2-Dichloroethane-d4 (S)
%
112
106
70-130
4-Bromofluorobenzene (S)
%
97
100
70-130
Toluene-d8 (S)
%
100
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 67 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 630880 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546336011, 92546336014
METHOD BLANK: 3314397 Matrix: Water
Associated Lab Samples: 92546336011, 92546336014
Blank Reporting
Parameter Units Result Limit
Alkalinity, Total as CaCO3 ug/L ND 5000
LABORATORY CONTROL SAMPLE: 3314398
Spike LCS
Parameter Units Conc. Result
Alkalinity, Total as CaCO3 ug/L 50000 53300
MDL Analyzed Qualifiers
5000 07/01 /21 14:47
LCS % Rec
% Rec Limits Qualifiers
107 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3314399 3314400
MS MSD
92545881003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 131 mg/L 50000 50000 180000 182000 97 102 80-120 1 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3314401 3314402
MS MSD
92546764003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 233 mg/L 50000 50000 279000 282000 93 99 80-120 1 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 68 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 631187 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546336012, 92546336013, 92546336015, 92546336016, 92546336017
METHOD BLANK: 3316049 Matrix: Water
Associated Lab Samples: 92546336012, 92546336013, 92546336015, 92546336016, 92546336017
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Alkalinity, Total as CaCO3 ug/L ND 5000 5000 07/02/21 14:20
LABORATORY CONTROL SAMPLE: 3316050
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 ug/L 50000 50200 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3316051 3316052
MS MSD
92547076004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L ND 50000 50000 45600 45900 91 92 80-120 1 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3316053 3316054
MS MSD
92546336017 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 33000 50000 50000 84600 85800 103 106 80-120 1 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 69 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 631200 Analysis Method: SM 3500-Fe B-2011
QC Batch Method: SM 3500-Fe B-2011 Analysis Description: Iron, Ferrous
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
METHOD BLANK: 3316114 Matrix: Water
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Iron, Ferrous mg/L ND 0.50 0.040 07/06/21 16:20 N2
LABORATORY CONTROL SAMPLE: 3316115
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Iron, Ferrous mg/L 1.5 1.5 102 90-110 N2
SAMPLE DUPLICATE: 3316116
92545978001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Iron, Ferrous mg/L ND ND 10 H3,N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 70 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 630815 Analysis Method: SM 4500-S2D-2011
QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
METHOD BLANK: 3314257 Matrix: Water
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Sulfide ug/L ND 100 50.0 07/01/2105:01
LABORATORY CONTROL SAMPLE: 3314258
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfide ug/L 500 515 103 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3314259 3314260
MS MSD
92546439001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfide ug/L 0.23 mg/L 500 500 639 672 81 87 80-120 5 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3314261 3314262
MS MSD
92546336017 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfide ug/L ND 500 500 456 472 88 91 80-120 3 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 71 of 125

lV11.1 Analytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 630278 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
METHOD BLANK: 3311565 Matrix: Water
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Sulfate ug/L ND 1000 500 06/29/2121:25
LABORATORY CONTROL SAMPLE: 3311566
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfate ug/L 50000 50100 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3311567 3311568
MS MSD
92546336017 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfate ug/L 1420 50000 50000 56600 56000 110 109 90-110 1 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 72 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 631938 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
METHOD BLANK: 3319691 Matrix: Water
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chloride ug/L ND 1000 500 07/07/2120:04
LABORATORY CONTROL SAMPLE: 3319692
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chloride ug/L 20000 21000 105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3319693 3319694
MS MSD
92546336011 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chloride ug/L 2580 10000 10000 13400 12800 108 102 90-110 5 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3319695 3319696
MS MSD
92546336012 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chloride ug/L 25000 10000 10000 35000 35000 100 100 90-110 0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 73 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 631747 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
METHOD BLANK: 3318741 Matrix: Water
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chemical Oxygen Demand ug/L ND 25000 12500 07/07/21 06:10
LABORATORY CONTROL SAMPLE: 3318742
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand ug/L 750000 759000 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3318743 3318744
MS MSD
92546336011 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand ug/L ND 100000 100000 104000 102000 104 102 90-110 2 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3318745 3318746
MS MSD
92546889001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand ug/L 412 mg/L 100000 100000 521000 507000 109 95 90-110 3 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 74 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 630380 Analysis Method: SM 531 OB-2011
QC Batch Method: SM 531 OB-2011 Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
METHOD BLANK: 3312161 Matrix: Water
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Organic Carbon ug/L ND 1000 500 06/29/21 16:28
LABORATORY CONTROL SAMPLE: 3312162
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Organic Carbon ug/L 25000 23000 92 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3312163 3312164
MS MSD
92545608001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon ug/L 10.0 mg/L 25000 25000 34600 34800 98 99 90-110 0 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3312165 3312166
MS MSD
92546336012 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon ug/L 3680 25000 25000 28500 28600 99 100 90-110 0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC.
Page 75 of 125

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
QC Batch: 715643 Analysis Method: AM23G
QC Batch Method: AM23G Analysis Description: Low Level Volatile Fatty Acids
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
METHOD BLANK: 2210235 Matrix: Water
Associated Lab Samples: 92546336011,92546336012,92546336013,92546336014,92546336015,92546336016,92546336017
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Lactic Acid
mg/L
ND
0.50
0.053
07/08/2119:48
Acetic Acid
mg/L
ND
0.50
0.12
07/08/2119:48
Propionic Acid
mg/L
ND
0.50
0.053
07/08/2119:48
Formic acid
mg/L
ND
0.50
0.055
07/08/21 19:48
Butyric Acid
mg/L
ND
0.50
0.058
07/08/2119:48
Pyruvic Acid
mg/L
ND
0.50
0.060
07/08/2119:48
i-Pentanoic Acid
mg/L
ND
0.50
0.061
07/08/2119:48
Pentanoic Acid
mg/L
ND
0.50
0.056
07/08/2119:48
i-Hexanoic Acid
mg/L
ND
0.50
0.056
07/08/2119:48
Hexanoic Acid
mg/L
ND
0.50
0.058
07/08/2119:48
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2210236
Units
Spike
Conc.
2210237
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
Lactic Acid
mg/L
2
1.9
1.9
97
96
70-130
2
20
Acetic Acid
mg/L
2
2.0
1.9
98
97
70-130
1
20
Propionic Acid
mg/L
2
2.0
1.9
98
97
70-130
1
20
Formic acid
mg/L
2
2.0
1.9
98
96
70-130
1
20
Butyric Acid
mg/L
2
1.9
1.9
96
94
70-130
1
20
Pyruvic Acid
mg/L
2
2.0
2.0
99
98
70-130
2
20
i-Pentanoic Acid
mg/L
2
1.9
1.9
95
93
70-130
2
20
Pentanoic Acid
mg/L
2
2.0
1.9
99
97
70-130
2
20
i-Hexanoic Acid
mg/L
2
2.0
2.0
101
99
70-130
2
20
Hexanoic Acid
mg/L
2
2.0
2.0
100
98
70-130
2
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 76 of 125

Pace Analytical Services, LLC
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0788
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QUALIFIERS
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
WORKORDER QUALIFIERS
WO: 92546336
[1] This workorder was initially ran within hold time, but due to instrument issues we were unable to pass a closing CCV. It
took several days to successfully complete a calibration, which is why the samples are being analyzed this far out of hold.
[2] Work order 221070231 was received with TSP preservative. CO2 requires non -preserved vials. Data may be affected.
[3] In analytical batch 715592 the closing calibration standard was recovered double the expected concentration.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
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Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 77 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SURRY CLOSED MT AIRY
Pace Project No.: 92546336
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92546336011
MW-1
AM20GAX
715604
92546336012
MW-7
AM20GAX
715604
92546336013
MW-9
AM20GAX
715604
92546336014
MW-11
AM20GAX
715604
92546336015
MW-15
AM20GAX
715604
92546336016
MW-14
AM20GAX
715604
92546336017
MW-21
AM20GAX
715604
92546336011
MW-1
AM20GAX
715951
92546336012
MW-7
AM20GAX
715951
92546336013
MW-9
AM20GAX
715951
92546336014
MW-11
AM20GAX
715951
92546336015
MW-15
AM20GAX
715951
92546336016
MW-14
AM20GAX
715951
92546336017
MW-21
AM20GAX
715951
92546336011
MW-1
RSK-175
715570
92546336012
MW-7
RSK-175
715570
92546336013
MW-9
RSK-175
715570
92546336014
MW-11
RSK-175
715570
92546336015
MW-15
RSK-175
715570
92546336016
MW-14
RSK-175
715570
92546336017
MW-21
RSK-175
715618
92546336001
MW-3R
EPA 3010A
631641
EPA 6010D
631708
92546336002
MW-6
EPA 3010A
631641
EPA 6010D
631708
92546336003
MW-12S
EPA 3010A
631641
EPA 6010D
631708
92546336004
MW-19
EPA 3010A
631641
EPA 6010D
631708
92546336005
MW-20
EPA 3010A
631641
EPA 6010D
631708
92546336006
MW-23
EPA 3010A
631641
EPA 6010D
631708
92546336007
MW-13
EPA 3010A
631641
EPA 6010D
631708
92546336008
MW-17
EPA 3010A
631641
EPA 6010D
631708
92546336009
MW-16
EPA 3010A
631641
EPA 6010D
631708
92546336010
MW-22
EPA 3010A
631641
EPA 6010D
631708
92546336011
MW-1
EPA 3010A
631641
EPA 6010D
631708
92546336012
MW-7
EPA 3010A
631641
EPA 6010D
631708
92546336013
MW-9
EPA 3010A
631641
EPA 6010D
631708
92546336014
MW-11
EPA 3010A
631641
EPA 6010D
631708
92546336015
MW-15
EPA 3010A
631641
EPA 6010D
631708
92546336016
MW-14
EPA 3010A
631641
EPA 6010D
631708
92546336017
MW-21
EPA 3010A
631641
EPA 6010D
631708
92546336018
SCALEHOUSE
EPA 3010A
631641
EPA6010D
631708
92546336019
WSW-2
EPA 3010A
631641
EPA 6010D
631708
92546336001
MW-3R
EPA 3010A
630470
EPA 6020B
630773
92546336002
MW-6
EPA 3010A
630470
EPA 6020B
630773
92546336003
MW-12S
EPA 3010A
630470
EPA 6020B
630773
92546336004
MW-19
EPA 3010A
630470
EPA 6020B
630773
92546336005
MW-20
EPA 3010A
630470
EPA 6020B
630773
92546336006
MW-23
EPA 3010A
630470
EPA 6020B
630773
REPORT OF LABORATORY ANALYSIS
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Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 78 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
SURRY CLOSED MT AIRY
92546336
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92546336007
MW-13
EPA 3010A
630470
EPA 6020B
630773
92546336008
MW-17
EPA 3010A
630470
EPA 6020B
630773
92546336009
MW-16
EPA 3010A
630470
EPA 6020B
630773
92546336010
MW-22
EPA 3010A
630470
EPA 6020B
630773
92546336011
MW-1
EPA 3010A
630470
EPA 6020B
630773
92546336012
MW-7
EPA 3010A
630470
EPA 6020B
630773
92546336013
MW-9
EPA 3010A
630470
EPA 6020B
630773
92546336014
MW-11
EPA 3010A
630470
EPA 6020B
630773
92546336015
MW-15
EPA 3010A
630470
EPA 6020B
630773
92546336016
MW-14
EPA 3010A
630470
EPA 6020B
630773
92546336017
MW-21
EPA 3010A
630470
EPA 6020B
630773
92546336018
SCALEHOUSE
EPA 3010A
630470
EPA 6020B
630773
92546336019
WSW-2
EPA 3010A
630470
EPA 6020B
630773
92546336001
MW-3R
EPA 8260D
629502
92546336002
MW-6
EPA 8260D
629502
92546336003
MW-12S
EPA 8260D
629502
92546336004
MW-19
EPA 8260D
629502
92546336005
MW-20
EPA 8260D
629502
92546336006
MW-23
EPA 8260D
629502
92546336007
MW-13
EPA 8260D
629502
92546336008
MW-17
EPA 8260D
629502
92546336009
MW-16
EPA 8260D
629502
92546336010
MW-22
EPA 8260D
629502
92546336011
MW-1
EPA 8260D
630255
92546336012
MW-7
EPA 8260D
630255
92546336013
MW-9
EPA 8260D
630255
92546336014
MW-11
EPA 8260D
630255
92546336015
MW-15
EPA 8260D
630255
92546336016
MW-14
EPA 8260D
630255
92546336017
MW-21
EPA 8260D
630255
92546336018
SCALEHOUSE
EPA 8260D
630255
92546336019
WSW-2
EPA 8260D
630255
92546336011
MW-1
SM 2320B-2011
630880
92546336012
MW-7
SM 2320B-2011
631187
92546336013
MW-9
SM 2320B-2011
631187
92546336014
MW-11
SM 2320B-2011
630880
92546336015
MW-15
SM 2320B-2011
631187
92546336016
MW-14
SM 2320B-2011
631187
92546336017
MW-21
SM 2320B-2011
631187
92546336011
MW-1
SM 3500-Fe B-2011
631200
92546336012
MW-7
SM 3500-Fe B-2011
631200
92546336013
MW-9
SM 3500-Fe B-2011
631200
92546336014
MW-11
SM 3500-Fe B-2011
631200
92546336015
MW-15
SM 3500-Fe B-2011
631200
92546336016
MW-14
SM 3500-Fe B-2011
631200
REPORT OF LABORATORY ANALYSIS
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Date: 10/15/2021 02:14 PM without the written consent of Pace Analytical Services, LLC. Page 79 of 125

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
SURRY CLOSED MT AIRY
92546336
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92546336017
MW-21
SM 3500-Fe B-2011
631200
92546336011
MW-1
SM 4500-S2D-2011
630815
92546336012
MW-7
SM 4500-S2D-2011
630815
92546336013
MW-9
SM 4500-S2D-2011
630815
92546336014
MW-11
SM 4500-S2D-2011
630815
92546336015
MW-15
SM 4500-S2D-2011
630815
92546336016
MW-14
SM 4500-S2D-2011
630815
92546336017
MW-21
SM 4500-S2D-2011
630815
92546336011
MW-1
EPA 300.0 Rev 2.1 1993
630278
92546336012
MW-7
EPA 300.0 Rev 2.1 1993
630278
92546336013
MW-9
EPA 300.0 Rev 2.1 1993
630278
92546336014
MW-11
EPA 300.0 Rev 2.1 1993
630278
92546336015
MW-15
EPA 300.0 Rev 2.1 1993
630278
92546336016
MW-14
EPA 300.0 Rev 2.1 1993
630278
92546336017
MW-21
EPA 300.0 Rev 2.1 1993
630278
92546336011
MW-1
SM 4500-CI-E-2011
631938
92546336012
MW-7
SM 4500-CI-E-2011
631938
92546336013
MW-9
SM 4500-CI-E-2011
631938
92546336014
MW-11
SM 4500-CI-E-2011
631938
92546336015
MW-15
SM 4500-CI-E-2011
631938
92546336016
MW-14
SM 4500-CI-E-2011
631938
92546336017
MW-21
SM 4500-CI-E-2011
631938
92546336011
MW-1
SM 5220D-2011
631747
SM 5220D-2011
631762
92546336012
MW-7
SM 5220D-2011
631747
SM 5220D-2011
631762
92546336013
MW-9
SM 5220D-2011
631747
SM 5220D-2011
631762
92546336014
MW-11
SM 5220D-2011
631747
SM 5220D-2011
631762
92546336015
MW-15
SM 5220D-2011
631747
SM 5220D-2011
631762
92546336016
MW-14
SM 5220D-2011
631747
SM 5220D-2011
631762
92546336017
MW-21
SM 5220D-2011
631747
SM 5220D-2011
631762
92546336011
MW-1
SM 531OB-2011
630380
92546336012
MW-7
SM 531OB-2011
630380
92546336013
MW-9
SM 531OB-2011
630380
92546336014
MW-11
SM 531OB-2011
630380
92546336015
MW-15
SM 531OB-2011
630380
92546336016
MW-14
SM 531OB-2011
630380
92546336017
MW-21
SM 531OB-2011
630380
92546336011
MW-1
AM23G
715643
92546336012
MW-7
AM23G
715643
92546336013
MW-9
AM23G
715643
92546336014
MW-11
AM23G
715643
92546336015
MW-15
AM23G
715643
92546336016
MW-14
AM23G
715643
92546336017
MW-21
AM23G
715643
Date: 10/15/2021 02:14 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 80 of 125

Document Name:
naSample Condition r;.;
_ fYrrticaf. Documentent Na.:
F-CAR-CS-033-Rev.07
Document Revised: October 28, 2020
Page 1 of 2
Issuing Authority:
Pace Carolinas Qualitv Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville 9 Raleiglt❑ Mechanicsville❑ Atlanta[] Kernersville❑
ConditionSample Client Name:
Upon • . Project ! WO# : g2546336
r I r fi:
i� r �, o YI m -- -
❑ Commercial space I ❑Other: II � Ill III III II I I I II III
92546336
Custody Seal Present? []Yes 'ENO Seals Intact? []Yes 'SNo
Date/Initials.Farsan-examining-GontenE � � � � �
Packing Material: ❑Bubble Wrap [Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: I❑Yes []No UN/A
Wet ❑Bkue []None
{l IR Gun ID: 92TO64 Type of lee:
/� Correction Factor:
Cooler Temp: ' Add/Subtract (°C) _p 1 Temp should be above freezing to VC
[]Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (°Cj: _ '?. has begun
USDA Regulated Soll (JgN/A, water sample)
Old samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source [internationally,
r-lVpc r7Nn including Hawaii and Puertn Airnl? MYes MNo
Comments/Discrepancy:
Chain of Custody Present?
Ayes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
TaYes
❑Na
N/A
2.
Short Hold Time Analysis (<72 hr.l?
[-]Yes
VNo
❑N/A
3.
Rush Turn Around Time Requested?
C]Yes
'ffNa
❑N/A
4.
Sufficient Volume?
j5 Yes
❑No
❑NIA
5.
Correct Containers Used?
-Pace Containers Used?
tjYes
5Yes
❑No
QNo
❑N/A
[—]N/A
6.
Containers Intact?
Yes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
[]Yes
No
❑N/A
a.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Yes
i
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
tNo
[]N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Dyes
'5gNo
(nNo
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes []No
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review:
Lot ID of split containers:
Date:
Project Manager SRF Review: Date;
Page 81 of 125

R
dC8 Andlyrical
Document Name:
Sampfe Condition Upan Receipt[SCURL _
Document Revised: October 2B, 2020
Page 2 of 2
Document No.:
F-CAR-CS-033-Rev.07
issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project #
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bolto.m..half_ctfbox_is_to_list_number_o.f_bottles._____._ .__.__...___... __ __._
WO## : 92546336
PM: AMB Due Dale: 07/09/21
CLIENT: 92—Municipal
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—L�Ls
pH Adjustment Log for Preserved Samples
Sample to
Type of Preservative
pH upon receipt
pate preservation adjusted
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adjusted
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added
lot 4
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 82 of 125

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Document Name:
Document Revised: October 28, 2020
r�
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
c7C13 11?� lCr7�
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.07
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville L] Raleigh[] Mechanicsville[] Atlanta❑ Kernersville❑
ConditionSample Client Name: WO# ' 92546336
PM: AMB Due Date; 07/12/21
❑ Commercial ❑Pace ❑Other: CLIENT: 92—Municipal
Custody Seal Present? Des. ❑No Seals Intact? ❑Yes nNo
Date/InSf+als.Person•bHamining.Ganlen - YJ f
Packing Material: ❑Bubble Wrap ❑gubble Sags []None ❑ Other
Thermometer:
EJ Ili Gun 1D: ❑Wet ❑Blue
92TO64 Type of Ice:
1l; Correction Factor:
Cooler Temp: Add/Subtract ('C) -0.1
Cooler Temp Corrected ('C):
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
11Yps FINn
Biological Tissue frozen?
[]Yes[-]No[]N/A❑ Nane
Temp should be above freezing to 6'C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source linternationally,
inriudinn Hawaii and P,cprtn Rirnl? 71Vp; I-11un
Comments/Discrepancy:
Chain of Custody Present?
13YeS
❑No
❑N/A
I.
Samples Arrived within Hold Time?
00
No
[:]N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
K)NO
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
[Z]No
❑N/A
4_
Sufficient Volume?
(Yes
❑No
❑NIA
S.
Correct Containers Used?
-Pace Containers Used?
ElYes
JAYes
❑No
❑No
❑N/A
[-]N/A
6.
Containers Intact?
t]Yes
[-]No
❑N/A
7.
Dissolved analysis; Samples Field Filtered?
❑Yes
No
❑N/A
8.
Sample Labels Match COC?
-includesDate/Time/ID/Analysis Matrix:
T
^.� I
No
❑N/A
9. iS a-0 -s
ree.aw�ed uh add
ylok- lic4Cd av'7 -1-VU GOG Cor 1fY W-1, YAw`l,
PAW-Ry'AW-%11 �A�Aj"'t4, Yv%w)rt5 s GlvW r
Headspace in VOA Vials (n5-6mm)?
❑Yes
[]No
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
[:]Yes
[]NO
[:]No
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot 1D of split containers:
Field Data Required? ❑Yes ❑Nn
JAI
CLIENT NOTIFICATION/RESOLUTION
Coc - d w l A Nn e- s Q y►n p Le s &AD e-s "o 1 !rl u u -e- :kjn e c�dd i rtaD
L.Q -t tv a -I I'S U) UALde-at as s c-�W t Q-h't �x�t+:t e Ly1 'F0 r m a-t� e-yl • v
Person contacted: [)ate/ -rime --
Project Manager SCURF Review: kAQ;, Date:
Project Manager SRF Review: Date:
Page 86 of 125

Document Name:
Document Revised: October 28, 2020
ace nalynca
Sample Condition Upon ReceiptlSCUR)_
Page 2 of
Document No.:
Issuing Authority:
F-CAR-05-033-Rev.07
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom_half_oLbox-is_to-list_number_o.f_bottles _._...__. __.
Project W0#•92546336
PM: AMB Due Date: 07/12/21
CLIENT: 92—Municipal
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Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of Ms form wild be sent to the North Carolina DEHNR Certification Office (i.e,
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 87 of 125

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Page 88 of 125

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Page 89 of 125

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Page 90 of 125

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Page 91 of 125
W

con-testo
A Pace Analytical® Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
July 8, 2021
Angela Baioni
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: NC
Client Job Number:
Project Number: 92546336
Laboratory Work Order Number: 21F1678
Enclosed are results of analyses for samples received by the laboratory on June 24, 2021. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
�srrs�vnzre.�

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
21F1678-01
21F1678-02
Sample Preparation Information
QC Data
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
B285330
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
5
5
6
7
8
8
8
9
10
11
�ST.M.!YY:StiD1�
�.•; •

Table of Contents
con-testo
A Pace Analytical® Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100 REPORT DATE: 7/8/2021
Huntersville, NC 28078 PURCHASE ORDER NUMBER:
ATTN: Angela Baioni
PROJECT NUMBER: 92546336
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 21F1678
The results of analyses performed on the following samples submitted to CON -TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION: NC
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
MW-16 211`1678-01 Water SM21-22 4500 CN E
MW-22 21171678-02 Water SM21-22 4500 CN E
Page 3 of 13

con-testo
A Pace Analytical® Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
�ST.TS!L'�S�iD1�

Table of Contents
con-testo
A Pace ArkTocalc Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: NC Sample Description: Work Order: 21F1678
Date Received: 6/24/2021
Field Sample #: MW-16 Sampled: 6/23/2021 14:22
Samnle ID: 21F1678-01
Samnle Matrix: Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Cyanide ND 0.010 0.0073 mg/L 1 SM21-22 4500 CN E 7/6/21 7/6/21 21:00 DJM
Page 5 of 13

Table of Contents
con-testo
A Pace ArkTocalc Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: NC Sample Description: Work Order: 21F1678
Date Received: 6/24/2021
Field Sample #: MW-22 Sampled: 6/23/2021 13:56
Samnle ID: 21F1678-02
Samnle Matrix: Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Cyanide ND 0.010 0.0073 mg/L 1 SM21-22 4500 CN E 7/6/21 7/6/21 21:00 DJM
Page 6 of 13

con-testo
A Pace Analytical® Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Sample Extraction Data
SM21-22 4500 CN E
Lab Number [Field ID] Batch Initial [mL] Final [mL] Date
21F1678-01 [MW-16] B285330 50.0 50.0 07/06/21
21F1678-02 [MW-22] B285330 50.0 50.0 07/06/21
�ST.TS!T:�S�iD1�

con-testo
A Pace Analytical® Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B285330 - SM21-22 4500 CN E
Blank (B285330-BLK1)
Prepared & Analyzed: 07/06/21
Cyanide
LCS (B285330-BS1)
ND 0.010
mg/L
Prepared & Analyzed: 07/06/21
Cyanide
LCS Dup (B285330-BSD1)
0.64 0.010
mg/L
0.656 97.2
Prepared & Analyzed: 07/06/21
77.6-115
Cyanide
Matrix Spike (B285330-MSI)
0.63 0.010
Source: 21F1678-02
mg/L
0.656 96.6
Prepared & Analyzed: 07/06/21
77.6-115 0.652 8.69
Cyanide
Matrix Spike Dup (B285330-MSDI)
0.30 0.010
Source: 21F1678-02
mg/L
0.332 ND 89.6
Prepared & Analyzed: 07/06/21
58.3-128
Cyanide
0.29 0.010
mg/L
0.332 ND 87.7
58.3-128 2.11 8.87
Page 8 of 13

con-testo
A Pace Analytical® Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 * FAX [phone] " TEL. [phone]
FLAG/QUALIFIER SUMMARY
*
QC result is outside of established limits.
fi
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
ND
Not Detected
RL
Reporting Limit is at the level of quantitation (LOQ)
DL
Detection Limit is the lower limit of detection determined by the MDL study
MCL
Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
� ST.TSi f �7�Z S t:i V1�

con-testo
A Pace ArkTocalc Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SM21-22 4500 CNE in Water
Cyanide CT,MA,NH,NY,RI,NC,ME,VA
Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditation:
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2017
100033
03/l/2022
MA
Massachusetts DEP
M-MA100
06/30/2022
CT
Connecticut Department of Publilc Health
PH-0165
12/31/2022
NY
New York State Department of Health
10899 NELAP
04/l/2022
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2022
RI
Rhode Island Department of Health
LA000112
12/30/2021
NC
North Carolina Div. of Water Quality
652
12/31/2021
NJ
New Jersey DEP
MA007 NELAP
06/30/2022
FL
Florida Department of Health
E871027 NELAP
06/30/2022
VT
Vermont Department of Health Lead Laboratory
LL720741
07/30/2022
ME
State of Maine
MA00100
06/9/2023
VA
Commonwealth of Virginia
460217
12/14/2021
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2021
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2022
NC-DW
North Carolina Department of Health
25703
07/31/2021
PA
Commonwealth of Pennsylvania DEP
68-05812
06/30/2022
MI
Dept. of Env, Great Lakes, and Energy
9100
09/6/2021
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Page 11 of 13 1

Table of Contents
TRACK ANOTHER SHIPMENT
987548432755
ADD NICKNAME
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Saturday, June 26, 2021 at 10.28 am
FROM
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Travel History
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Local Scan Time
Saturday, June 26, 2021
DELIVERED
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GET STATUS UPDATES
OBTAIN PROOF OF DELIVERY
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TO
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WEIGHT
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Page 12 of 13

Table of Contents
Numbers With Lab Staff Before Relinquishing
Login Sample Receipt Checklist - (Rejection riteria Listing - Using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client
Received By
How were the samples In Cooler Nu�n r On Ice � No Ice
received? Di���mSampling
---- --� �mbiant Melted |�
By Gun Aotuo|Tmm
VVmnasamples vx�hn
Temperature? 3-8'C ByBlank # Actual Temp
Was Custody Seal
'Intact? �% Were Samples Tampered with? -
Was C{}CRelinquished ? -r- D�mnChain Agree VVithSamples? /�____
___---__- ~
Are there bnnkonXmaking/|oonocaps onany samples? i���_
In C{}C in ink/ Legible? Were samples received within holding time?
Did <�{}C include all
Analysis ���Qamp|mr Nome
pertinent Information? Project----- |D'n ��CoUentionOedmn/T|maa___��____
Amy QomcHe labels filled out and legible? -]r___
Are there Lab toFilters? Who was notified?
Are there Rushes? t- Who was notified?
Are there Short Holds?
|uthere enough Volume?
|uthere Hmadapaoewhere applicable?
Proper Media/Containers Used? -7-�___
VVanm trip blanks received?
Doall samples have the proper pH?
Who was notified?
K88XMQO? -
--------- is splitting samples required?
OnCOC? r
Acid Base /
_____

aceAnalyfical
LELAP CERTIFICATE NUMBER: 01955
DOD-ELAP ACCREDITATION NUMBER: 74960
ANALYTICAL RESULTS
•:I
Pace Analytical Gulf Coast
7979 Innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 07/15/2021
Report Y2210J0231
�1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i �1��i III
Project 92546336 Surry Closed
Samples Collected 6/24/21 - 6/25/21
Deliver To Additional Recipients
Angela Baioni Bonnie Vang, Pace Analytical
Pace Analytical Services, Inc. Lindsey Wooten, Pace Analytical Charlotte
9800 Kincey Ave
Suite 100
Huntersville, NC 28078
[phone]
1*6.wk
FJ LA
Testing
tloD FLAP
ccRto
Pala 10ri of 17.ri
Pace Gulf Coast Report#: 221070231 Page 1 of 21

0-1? Report#: 221070231
F'acaAnaJytical
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
" Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis — when appended to Client Sample ID
Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
Pace Gulf Coast Report 221070231
Pages 106 of 17.ri
Pace Gulf Coast Report#: 221070231 Page 2 of 21

Report#: 221070231
- PaceAna&tical
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Certifications
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Pages 107 of 1?5
Pace Gulf Coast Report#: 221070231 Page 3 of 21

0-1? Report#: 221070231
F'acaAnaJytical
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Case Narrative
Client: Pace Analytical Services Report: 221070231
Pace Analytical Gulf Coast received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
VOLATILES GAS CHROMATOGRAPHY
Work order 221070231 was received with TSP preservative. CO2 requires non -preserved vials. Data may be affected.
In analytical batch 715592 the closing calibration standard was recovered double the expected concentration.
The samples in this was initially ran within hold time, but due to instrument issues we were unable to pass a closing CCV. It took
several days to successfully complete a calibration, which is why the samples are being analyzed this far out of hold
Pages 108 of 17.ri
Pace Gulf Coast Report#: 221070231 Page 4 of 21

0-1?
F'acaAnaJytical
Report#: 221070231
Project ID: 92546336 Surry Closed
Report Date:
07/15/2021
Sample Summary
Lab ID
Client ID
Matrix
Collect Date
Receive Date
22107023101
MW-1
Bubble Strip
6/24/21 15:00
7/01/21 10:01
22107023102
MW-7
Bubble Strip
6/25/21 10:00
7/01/21 10:01
22107023103
MW-9
Bubble Strip
6/25/21 12:00
7/01/21 10:01
22107023104
MW-11
Bubble Strip
6/24/21 16:00
7/01/21 10:01
22107023105
MW-14
Bubble Strip
6/24/21 11:30
7/01/21 10:01
22107023106
MW-15
Bubble Strip
6/25/21 08:30
7/01/21 10:01
22107023107
MW-21
Bubble Strip
6/25/21 14:00
7/01/21 10:01
22107023108
MW-1
Water
6/24/21 15:00
7/01/21 10:01
22107023109
MW-7
Water
6/25/21 10:00
7/01/21 10:01
22107023110
MW-9
Water
6/25/21 12:00
7/01/21 10:01
22107023111
MW-11
Water
6/24/21 16:00
7/01/21 10:01
22107023112
MW-14
Water
6/24/21 11:30
7/01/21 10:01
22107023113
MW-15
Water
6/25/21 08:30
7/01/21 10:01
22107023114
MW-21
Water
6/25/21 14:00
7/01/21 10:01
Pages lop of J?ri
Pace Gulf Coast Report#: 221070231 Page 5 of 21

Ar? Report#: 221070231
Facvk?alytu1
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Q Flag Summary
NO Q FLAGS FOR THIS WORKORDER
Pages 11f1 of 1?ri
Pace Gulf Coast Report#: 221070231 Page 6 of 21

0-1?
Report#: 221070231
F'acaAnaJytical
Project ID: 92546336 Surry Closed
Report Date:
07/15/2021
Detect Summary
Results and Detection Limits are adjusted for
dilution and moisture when applicable
AM23G
Lab ID
Client ID
Parameter
Units
Result
Dil.
%Moist
22107023108
MW-1
Acetic Acid
mg/L
0.30J
1
NA
22107023108
MW-1
Formic Acid
mg/L
5.3
1
NA
22107023108
MW-1
Lactic Acid
mg/L
0.0911
1
NA
22107023109
MW-7
Acetic Acid
mg/L
0.36J
1
NA
22107023109
MW-7
Formic Acid
mg/L
4.6
1
NA
22107023109
MW-7
Lactic Acid
mg/L
0.086J
1
NA
22107023110
MW-9
Acetic Acid
mg/L
3.OJ
10
NA
22107023110
MW-9
Formic Acid
mg/L
44
10
NA
22107023111
MW-11
Acetic Acid
mg/L
0.31 J
1
NA
22107023111
MW-11
Formic Acid
mg/L
5.2
1
NA
22107023111
MW-11
Lactic Acid
mg/L
0.23J
1
NA
22107023112
MW-14
Acetic Acid
mg/L
0.36J
1
NA
22107023112
MW-14
Formic Acid
mg/L
5.8
1
NA
22107023112
MW-14
Lactic Acid
mg/L
0.22J
1
NA
22107023113
MW-15
Acetic Acid
mg/L
0.38J
1
NA
22107023113
MW-15
Formic Acid
mg/L
4.9
1
NA
22107023113
MW-15
Lactic Acid
mg/L
0.057J
1
NA
22107023114
MW-21
Acetic Acid
mg/L
0.67J
2
NA
22107023114
MW-21
Formic Acid
mg/L
12
2
NA
AM20GAX
Lab ID
Client ID
Parameter
Units
Result
Dil.
%Moist
22107023101
MW-1
Hydrogen
nM
0.55J
1
NA
22107023102
MW-7
Hydrogen
nM
1.01
1
NA
22107023103
MW-9
Hydrogen
nM
1.3J
1
NA
22107023104
MW-11
Hydrogen
nM
8.0
1
NA
22107023105
MW-14
Hydrogen
nM
2.8
1
NA
22107023106
MW-15
Hydrogen
nM
5.3
1
NA
22107023107
MW-21
Hydrogen
nM
1.01
1
NA
22107023109
MW-7
Ethane
ug/L
0.65J
1
NA
22107023109
MW-7
Methane
ug/L
170
1
NA
22107023110
MW-9
Ethane
ug/L
28
1
NA
22107023110
MW-9
Ethene
ug/L
2.6
1
NA
22107023110
MW-9
Methane
ug/L
2200
1
NA
22107023111
MW-11
Methane
ug/L
120
1
NA
22107023112
MW-14
Methane
ug/L
1100
1
NA
Pages 111 of 1 i.ri
Pace Gulf Coast Report#: 221070231 Page 7 of 21

Ar? Report#: 221070231
Facvk?alytical
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Sample Results
Collect Date 06/24/2021 15:00 Lab ID 22107023101
MW-1 Receive Date 07/01/2021 10:01 Matrix Bubble Strip
GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2113:19 715604 TJT
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
0.55J
0.49
1.9
nM
Collect Date 06/25/2021 10:00 Lab ID 22107023102
MW-7 Receive Date 07/01/2021 10:01 Matrix Bubble Strip
GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2113:46 715604 TJT
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
1.01
0.49
1.9
nM
Collect Date 06/25/2021 12:00 Lab ID 22107023103
MW-9 Receive Date 07/01/2021 10:01 Matrix Bubble Strip
GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2114:02 715604 TJT
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
1.3,1
0.49
1.9
nM
Collect Date 06/24/2021 16:00 Lab ID 22107023104
MW-1 1 Receive Date 07/01/2021 10:01 Matrix Bubble Strip
GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2114:16 715604 TJT
CAS# Parameter
1333-74-0 Hydrogen
Result
DL
LOQ
Units
8.0
0.49
1.9
nM
Pages 112 of 1 i.ri
Pace Gulf Coast Report#: 221070231 Page 8 of 21

.N-? Report#: 221070231
Facvkujytical
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Sample Results
MW-14 Collect Date 06/24/2021 11:30 Lab ID 22107023105
Receive Date 07/01/2021 10:01 Matrix Bubble Strip
GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2114:31 715604 TJT
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
2.8
0.49
1.9
nM
MW-15 Collect Date 06/25/2021 08:30 Lab ID 22107023106
Receive Date 07/01/2021 10:01 Matrix Bubble Strip
GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2114:44 715604 TJT
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
5.3
0.49
1.9
nM
MW-21 Collect Date 06/25/2021 14:00 Lab ID 22107023107
Receive Date 07/01/2021 10:01 Matrix Bubble Strip
GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2114:59 715604 TJT
CAS#
Parameter
Result
DL
LOQ
Units
1333-74-0
Hydrogen
1.01
0.49
1.9
nM
Collect Date 06/24/2021 15:00 Lab ID 22107023108
MW-1 Receive Date 07/01/2021 10:01 Matrix Water
RSK-175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2112:18 715570 BMR
CAS# Parameter
124-38-9 Carbon Dioxide
Result
DL
LOQ
Units
127U
127
900
ug/L
Pages 113 of 1 i.ri
Pace Gulf Coast Report#: 221070231 Page 9 of 21

�J
7�aceArralytical
Report#: 221070231
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Sample Results
Collect Date 06/24/2021 15:00 Lab ID 22107023108
MW-1 Receive Date 07/01/2021 10:01 Matrix Water
?3G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/08/2120:41 715643 MOS
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.30J
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
5.3
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.0911
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/14/2112:22 715951 TJT
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.17U
0.17
1.0
ug/L
74-85-1
Ethene
0.24U
0.24
1.0
ug/L
74-82-8
Methane
2.OU
2.0
5.0
ug/L
Collect Date 06/25/2021 10:00 Lab ID 22107023109
MW�% Receive Date 07/01/2021 10:01 Matrix Water
� RSK-175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2112:23 715570 BMR
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 127U 127 900 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/08/2121:34 715643 MOS
CAS#
Parameter
64-19-7
Acetic Acid
107-92-6
Butyric Acid
64-18-6
Formic Acid
142-62-1
Hexanoic Acid
646-07-1
i-Hexanoic Acid
Result
DL
0.36J
0.12
0.058U
0.058
4.6
0.055
0.058U
0.058
0.056U
0.056
LOQ
Units
0.50
mg/L
0.50
mg/L
0.50
mg/L
0.50
mg/L
0.50
mg/L
Pages 114 of 1?5
Pace Gulf Coast Report#: 221070231 Page 10 of 21

�J
7�aceArralytical
Report#: 221070231
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Sample Results
Collect Date 06/25/2021 10:00 Lab ID 22107023109
MW�7 Receive Date 07/01/2021 10:01 Matrix Water
?3G (Continued)
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/08/2121:34 715643 MOS
CAS#
Parameter
Result
DL
LOQ
Units
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.086J
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060LI
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/14/2112:37 715951 TJT
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.65J
0.17
1.0
ug/L
74-85-1
Ethene
0.24U
0.24
1.0
ug/L
74-82-8
Methane
170
2.0
5.0
ug/L
MW-9 Collect Date 06/25/2021 12:00 Lab ID 22107023110
Receive Date 07/01/2021 10:01 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2112:27 715570 BMR
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 127U 127 900 ug/L
AM23G *Results And limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 10 07/08/2122:28 715643 MOS
CAS#
Parameter
64-19-7
Acetic Acid
107-92-6
Butyric Acid
64-18-6
Formic Acid
142-62-1
Hexanoic Acid
646-07-1
i-Hexanoic Acid
503-74-2
i-Pentanoic Acid
50-21-5
Lactic Acid
109-52-4
Pentanoic Acid
79-09-4
Propionic Acid
Result
DL
LOQ
Units
3.0,1
1.2
5.0
mg/L
0.58U
0.58
5.0
mg/L
44
0.55
5.0
mg/L
0.58U
0.58
5.0
mg/L
0.56U
0.56
5.0
mg/L
0.61 U
0.61
5.0
mg/L
0.53U
0.53
5.0
mg/L
0.56U
0.56
5.0
mg/L
0.53U
0.53
5.0
mg/L
Pala 11.ri of 1 i.ri
Pace Gulf Coast Report#: 221070231 Page 11 of 21

�J
7�aceArralytical
Report#: 221070231
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Sample Results
MW-9 Collect Date 06/25/2021 12:00 Lab ID 22107023110
Receive Date 07/01/2021 10:01 Matrix Water
AM23G (Continued) "Results And limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 10 07/08/2122:28 715643 MOS
CAS# Parameter Result DL LOQ Units
127-17-3 Pyruvic Acid 0.60U 0.60 5.0 mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/14/2112:57 715951 TJT
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
28
0.17
1.0
ug/L
74-85-1
Ethene
2.6
0.24
1.0
ug/L
74-82-8
Methane
2200
2.0
5.0
ug/L
MW-1 1 Collect Date 06/24/2021 16:00 Lab ID 22107023111
Receive Date 07/01/2021 10:01 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2112:34 715570 BMR
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 127U 127 900 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/08/2123:21 715643 MOS
CAS#
Parameter
64-19-7
Acetic Acid
107-92-6
Butyric Acid
64-18-6
Formic Acid
142-62-1
Hexanoic Acid
646-07-1
i-Hexanoic Acid
503-74-2
i-Pentanoic Acid
50-21-5
Lactic Acid
109-52-4
Pentanoic Acid
79-09-4
Propionic Acid
127-17-3
Pyruvic Acid
Result
DL
LOQ
Units
0.31 J
0.12
0.50
mg/L
0.058U
0.058
0.50
mg/L
5.2
0.055
0.50
mg/L
0.058U
0.058
0.50
mg/L
0.056U
0.056
0.50
mg/L
0.061 U
0.061
0.50
mg/L
0.23J
0.053
0.50
mg/L
0.056U
0.056
0.50
mg/L
0.053U
0.053
0.50
mg/L
0.060U
0.060
0.50
mg/L
Pages 116 of 1 i.ri
Pace Gulf Coast Report#: 221070231 Page 12 of 21

..'7
FaceAfulytical
Report#: 221070231
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Sample Results
MW-1 1 Collect Date 06/24/2021 16:00 Lab ID 22107023111
Receive Date 07/01/2021 10:01 Matrix Water
?OGAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/14/2113:11 715951 TJT
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.17U
0.17
1.0
ug/L
74-85-1
Ethene
0.24U
0.24
1.0
ug/L
74-82-8
Methane
120
2.0
5.0
ug/L
Collect Date 06/24/2021 11:30 Lab ID 22107023112
MW�14 Receive Date 07/01/2021 10:01 Matrix Water
EPA RSK-175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2112:38 715570 BMR
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 127U 127 900 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/09/2100:15 715643 MOS
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.36J
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
5.8
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.22J
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/14/2113:26 715951 TJT
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
0.17U
0.17
1.0
ug/L
0.24U
0.24
1.0
ug/L
1100
2.0
5.0
ug/L
Pages 117 of 1?5
Pace Gulf Coast Report#: 221070231 Page 13 of 21

..'7
FaceAfulytical
Report#: 221070231
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Sample Results
MW-1 5 Collect Date 06/25/2021 08:30 Lab ID 22107023113
Receive Date 07/01/2021 10:01 Matrix Water
� RSK-175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2112:43 715570 BMR
CAS# Parameter Result DL LOQ Units
124-38-9 Carbon Dioxide 127U 127 900 ug/L
AM23G
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/09/2101:08 715643 MOS
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.38J
0.12
0.50
mg/L
107-92-6
Butyric Acid
0.058U
0.058
0.50
mg/L
64-18-6
Formic Acid
4.9
0.055
0.50
mg/L
142-62-1
Hexanoic Acid
0.058U
0.058
0.50
mg/L
646-07-1
i-Hexanoic Acid
0.056U
0.056
0.50
mg/L
503-74-2
i-Pentanoic Acid
0.061 U
0.061
0.50
mg/L
50-21-5
Lactic Acid
0.057J
0.053
0.50
mg/L
109-52-4
Pentanoic Acid
0.056U
0.056
0.50
mg/L
79-09-4
Propionic Acid
0.053U
0.053
0.50
mg/L
127-17-3
Pyruvic Acid
0.060U
0.060
0.50
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/14/2114:17 715951 TJT
CAS#
Parameter
Result
DL
LOQ
Units
74-84-0
Ethane
0.17U
0.17
1.0
ug/L
74-85-1
Ethene
0.24U
0.24
1.0
ug/L
74-82-8
Methane
2.OU
2.0
5.0
ug/L
Collect Date 06/25/2021 14:00 Lab ID 22107023114
MW"21 Receive Date 07/01/2021 10:01 Matrix Water
� RSK-175
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/07/2113:14 715618 BMR
CAS# Parameter
124-38-9 Carbon Dioxide
Result
DL
LOQ
Units
127U
127
900
ug/L
Pages 118 of 17.ri
Pace Gulf Coast Report#: 221070231 Page 14 of 21

w'? Report#: 221070231
Facvkujytical
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
Sample Results
MW-21 Collect Date 06/25/2021 14:00 Lab ID 22107023114
Receive Date 07/01/2021 10:01 Matrix Water
AM23G "Results And limits are adjusted for dilution.
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 2 07/09/2102:01 715643 MOS
CAS#
Parameter
Result
DL
LOQ
Units
64-19-7
Acetic Acid
0.67J
0.25
1.0
mg/L
107-92-6
Butyric Acid
0.12U
0.12
1.0
mg/L
64-18-6
Formic Acid
12
0.11
1.0
mg/L
142-62-1
Hexanoic Acid
0.12U
0.12
1.0
mg/L
646-07-1
i-Hexanoic Acid
0.11 U
0.11
1.0
mg/L
503-74-2
i-Pentanoic Acid
0.12U
0.12
1.0
mg/L
50-21-5
Lactic Acid
0.11 U
0.11
1.0
mg/L
109-52-4
Pentanoic Acid
0.11 U
0.11
1.0
mg/L
79-09-4
Propionic Acid
0.11 U
0.11
1.0
mg/L
127-17-3
Pyruvic Acid
0.12U
0.12
1.0
mg/L
AM20GAX
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 07/14/2114:35 715951 TJT
CAS#
Parameter
74-84-0
Ethane
74-85-1
Ethene
74-82-8
Methane
Result
DL
LOQ
Units
0.17U
0.17
1.0
ug/L
0.24U
0.24
1.0
ug/L
2.OU
2.0
5.0
ug/L
Pages 11 q of 1 i.ri
Pace Gulf Coast Report#: 221070231 Page 15 of 21

Ar? Report#: 221070231
Facvk?alytuI
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
GC Volatiles QC Summary
Analytical Batch Client ID
MB715570
LCS715570
LCSD715570
715570 Lab ID
2209863
2209864
2209865
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
07/07/21 09:40
07/07/21 10:06
07/07/21 10:22
Matrix
Water
Water
Water
EPA RSK-175
Units
ug/L
Spike
Result
%R
I
Control
I
Spike
Result
%R
RPD
RPD
Result
DLI
Added
Limits%R
1 Added
Limit
Carbon Dioxide 124-38-9
127U
127
8700
8220
94
38 - 147
8700
8480
97
3
40
Analytical Batch Client ID
MB715618
LCS715618
LCSD715618
715618 Lab ID
2210052
2210053
2210054
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
07/07/21 12:57
07/07/21 13:04
07/07/21 13:08
Matrix
Water
Water
Water
EPA RSK-175
Units
ug/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DLI
Added
Limits%R
Added
Limit
Carbon Dioxide 124-38-9
127U
127
8700
7980
92
38 - 147
8700
886011n9l
10
1 40
Pages 19f1 of 1?ri
Pace Gulf Coast Report#: 221070231 Page 16 of 21

Ar? Report#: 221070231
Facvk?alytuI
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
General Chemistry QC Summary
Analytical Batch Client ID
MB715643
LCS715643
LCSD715643
715643 Lab ID
2210235
2210236
2210237
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
07/08/21 19:48
07/08/21 18:54
07/09/21 05:35
Matrix
Water
Water
Water
AM23G
Units
mg/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Acetic Acid
64-19-7
0.12U
0.12
2.0
2.0
98
70 - 130
2.0
1.9
97
1
20
Butyric Acid
107-92-6
0.058U
0.058
2.0
1.9
96
70 - 130
2.0
1.9
94
1
20
Formic Acid
64-18-6
0.055U
0.055
2.0
2.0
98
70 - 130
2.0
1.9
96
1
20
Hexanoic Acid
142-62-1
0.058U
0.058
2.0
2.0
100
70 - 130
2.0
2.0
98
2
20
i-Hexanoic Acid
646-07-1
0.056U
0.056
2.0
2.0
101
70 - 130
2.0
2.0
99
2
20
i-Pentanoic Acid
503-74-2
0.061 U
0.061
2.0
1.9
95
70 - 130
2.0
1.9
93
2
20
Lactic Acid
50-21-5
0.053U
0.053
2.0
1.9
97
70 - 130
2.0
1.9
96
2
20
Pentanoic Acid
109-52-4
0.056U
0.056
2.0
2.0
99
70 - 130
2.0
1.9
97
2
20
Propionic Acid
79-09-4
0.053U
0.053
2.0
2.0
98
70 - 130
2.0
1.9
97
1
20
Pyruvic Acid
127-17-3
0.060U
0.060
2.0
2.0
99
70 - 130
2.0
2.0
98
2
20
Pages 1 ? 1 of 17.ri
Pace Gulf Coast Report#: 221070231 Page 17 of 21

Ar? Report#: 221070231
Facvk?alytuI
Project ID: 92546336 Surry Closed Report Date: 07/15/2021
General Chromatography QC Summary
Analytical Batch Client ID
MB715604
LCS715604
LCSD715604
715604 Lab ID
2209966
2209967
2209968
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
07/07/21 11:39
07/07/21 11:52
07/07/21 12:05
Matrix
Bubble Strip
Bubble Strip
Bubble Strip
AM20GAX
Units
nM
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Hydrogen 1333-74-0
0.49U
0.49
12
12
104
70 - 130
12
13
107
3
20
Analytical Batch
Client ID
MB715951
LCS715951
LCSD715951
715951
Lab ID
2212022
2212023
2212024
Sample Type
MB
LCS
LCSD
Prep Date
NA
NA
NA
Analysis Date
07/14/21 11:57
07/14/21 11:30
07/14/21 11:43
Matrix
Water
Water
Water
AM20GAX
Units
ug/L
Spike
Result
%R
Control
Spike
Result
%R
RPD
RPD
Result
DL
Added
Limits%R
Added
Limit
Ethane
74-84-0
0.17U
0.17
38
44
116
70 - 130
38
44
116
0
20
Ethene
74-85-1
0.24U
0.24
35
41
116
70 - 130
35
41
116
0
20
Methane
74-82-8
2.OU
2.0
750
720
97
70-130
750
740
99
2
20
Pages 1?? of 17.ri
Pace Gulf Coast Report#: 221070231 Page 18 of 21

Internal Transfer Chain of Custody
111111110111111111IHH11111111111 ❑ Samples Pre -Logged into ecoc.
Workorder: 92546336 Workorder Name: SLURRY CLOSED MT AIRY
"�c `� ace Analytical
State Of Origin: NC { v+i** Ar +Ose w..,ffi�shozom
Cert. Needed. ❑ Yes ❑ No
Owner Received Date: 6f2512021 Results Requested By, 7112f2021
Report To Subcontract To
Requested
Analysis
Angela Baioni Pace Gulf Coast
PaceAnalrytical Gharldtte 7979 Innovation Park Or
9800 Kinc ey Ave. Suite 100 Baton Rouge, LA 70820
Huntersville, NC 28078 Phone [phone]
to
a
Phone {704)875-9092
;�
a
rt
i
a
8
n
D
i
S
a
u51
a
Presarv*d Containers
a
U.
a
o
'p
s
Sample
Collect
Item
Sample ID
Type
DateMme
Lab JD
matrix
LAB USE ONLY
1 1
MW-7
PS
6r242021 15:00
82546336011
Water
3
x
x
X
2
MM7
PS
6125f202110:00
W546336012
Water
3
}4'
x
x
3
MW-9
PS
61251202112:00
92545338013
Walef
3
x
x
x
3 Q
4
M4v-14
PS
612412021 16;00
92546336014
Water
3
x
x
}(
5
MW-1d
PS
612412132111:30
92546336015
Water
3
x
x
X
Cj
6
MW-15
PS
6f2512021 08:30
92546336016
Water
3
X
x
x
ELL
� f 3
7
w-21
PS
&25r102114:00
1 9254633W17
Mler
3
K
x
x
I114
Comments
Transfers
Released By DateMrne
Receirrea By Raterrime
'
1
lam_
Z
3
Cooler Temperature on Receipt °C Custody Seal Y or N deceived on Ice Y or N Samples Intact Y or N
In order to maintain client confidentiality, locationIname of the sampling site, sampler's nan7e and signaturle may not be provided on this COC document.
This chain of custody is considered complete as is since this information is available in the owner laboratory.
Tuesday. Jufm 2% 2021 8:35:08AM
client lD: 4367 - Pace Analytical Services
SDG: 221070231
PM: RVve 1
PaQa 1?3 of 17.r;
Pace Gulf Coast Report#: 221070231 Page 19 of 21

Internal Tradsfe
Workorder: 92546336
Report To -
Angela Baioni
Pace Analyfical. Charl at e
9840ttinoeyAve- Suit 100
Huntersville, NC 2807
Phone (704}&75-9fl92
Item I Sample ID
1 Mw-t
Transfers Released E3y
i
2
3
hain f Custody
r F—] Samples Pre -Logged into eCOC.
r Marne: SLIRRY CLOSED MTAIRY
Pace Gull Coast
7979 Innovation Park Dr
Baton Rouge, LA 70a20
Phone [phone]
sarrrµl� 1collect
Type
❑atefrlme
Lab ID
Matrix
PS
8124=2115:DD
92546336011
Water
PS
6f25r202110=
132546336012
Water
PS
612512112112-00
92546336013
Water
PS
6f2VM2116:DD
925463M14
Water
PS
6124r202111:30
925413336015
Water
PS
6)251202108.30
92546336016
Water
PS
6f25f202114-00
925463360W
Water
DatefTlme
eceived By
P'Jc do-esvl"f aceAr IXica!
State Of Origin: INIC q- (kw-` +Zf iQ(. -I44VSP• wwrr. p.edaGs.eora
Cert. Needed: ❑ Yes El no
Owner Received Date: 812512021 Results fiequested By: 711212021
. Reu ueated Anal4s% -
aalerTirne
-I _/CC?
Cooler Tern Deratu on R ref Pt I C Gustoci Seal Y or N 1 Received on lee Y or N I samples imam. 1
1"fn order to rnainl n them Leo
nklentitmplete
y, locetioWnarne of the sarnp#ng site, sampler's name and signature may Trot be provided on this COC docurne0l.
This charm of cus ody is as is since this information is available in the owner laboratory.
Tuesday, ,tune 29, 2021 8:35,08
LAB USE ONLY
7
CtientlD: 416 -Pace AnalyticaijjSleiviiee1s `
SDG: 221070231 I � ft; i
PM: RVVe
Papa 124 of 1,25
Pace Gulf Coast Report#: 221070231 Page 20 of 21

(��a'ceAnalyfical'SAMPLE RECEIVING CHECKLIST IIIIIIIIIIII III
SAMPLE DELIVERY GROUP
221070231
CHECKLIST
YES
NO
Client PM RIUe
Transport Method
Samples received with proper thermal preservation?
*❑
❑
4367 - Pace Analytical Services
F®DC
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
*❑
*❑
❑
❑
Profile Number
Received By
282148
N/bane, DDdie N
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
*❑
0
❑
❑
Line Item(s)
Receive Date(s)
10 - IVY, 002, VFA
07/01/21
11 - Hydrogen
Preservative added to any containers?
❑
�I❑
If received, was headspace for VOC water containers < 6mm?
*❑
❑
Samples collected in containers provided by Pace Gulf Coast?
0
❑
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Thermometer ID: E34
Temp °C
None
None
NA
0.2
987548433681
NA
NOTES
Revision 1.6
Pace Gulf Coast Report#: 221070231
Page 1 of 1
Papa 125 of 1,25
Page 21 of 21

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
July 12, 2021
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: SURRY BLANKS
Pace Project No.: 92546678
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 25, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Accounts Payable, Municipal Engineering Services
Jay Zimmerman, PG, Municipal Engineering Services Co.
REPORT OF LABORATORY ANALYSIS
r
0
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 21

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SURRY BLANKS
Pace Project No.: 92546678
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 21

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9800 Kincey Ave. Suite 100
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[phone]
SAMPLE SUMMARY
Project: SURRY BLANKS
Pace Project No.: 92546678
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92546678001
EB
Water
06/25/2114:09
06/25/2116:43
92546678002
FB
Water
06/25/2114:12
06/25/2116:43
92546678003
EB-metals
Water
06/25/2114:09
06/25/2116:43
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 3 of 21

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9800 Kincey Ave. Suite 100
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SAMPLE ANALYTE COUNT
Project: SURRY BLANKS
Pace Project No.: 92546678
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92546678001 EB
EPA 8260D
SAS
51
PASI-C
92546678002 FB
EPA 8260D
SAS
51
PASI-C
92546678003 EB-metals
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 21

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY BLANKS
Pace Project No.: 92546678
Sample: EB Lab ID: 92546678001 Collected: 06/25/21 14:09 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Date: 07/12/2021 05:20 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
06/29/2116:10
67-64-1
ND
ug/L
10.0
1.8
1
06/29/2116:10
107-13-1
ND
ug/L
1.0
0.34
1
06/29/2116:10
71-43-2
ND
ug/L
1.0
0.47
1
06/29/2116:10
74-97-5
ND
ug/L
1.0
0.31
1
06/29/2116:10
75-27-4
ND
ug/L
1.0
0.34
1
06/29/2116:10
75-25-2
ND
ug/L
2.0
1.7
1
06/29/2116:10
74-83-9
ND
ug/L
5.0
4.0
1
06/29/2116:10
78-93-3
ND
ug/L
2.0
0.73
1
06/29/2116:10
75-15-0
ND
ug/L
1.0
0.33
1
06/29/2116:10
56-23-5
ND
ug/L
1.0
0.28
1
06/29/2116:10
108-90-7
ND
ug/L
1.0
0.65
1
06/29/2116:10
75-00-3
ND
ug/L
5.0
1.6
1
06/29/2116:10
67-66-3
ND
ug/L
1.0
0.54
1
06/29/2116:10
74-87-3
ND
ug/L
2.0
0.34
1
06/29/2116:10
96-12-8
ND
ug/L
1.0
0.36
1
06/29/2116:10
124-48-1
ND
ug/L
1.0
0.27
1
06/29/2116:10
106-93-4
ND
ug/L
1.0
0.39
1
06/29/2116:10
74-95-3
ND
ug/L
1.0
0.34
1
06/29/2116:10
95-50-1
ND
ug/L
1.0
0.33
1
06/29/2116:10
106-46-7
ND
ug/L
1.0
0.56
1
06/29/2116:10
110-57-6
ND
ug/L
1.0
0.37
1
06/29/2116:10
75-34-3
ND
ug/L
1.0
0.32
1
06/29/2116:10
107-06-2
ND
ug/L
1.0
0.35
1
06/29/2116:10
75-35-4
ND
ug/L
1.0
0.38
1
06/29/2116:10
156-59-2
ND
ug/L
1.0
0.40
1
06/29/2116:10
156-60-5
ND
ug/L
1.0
0.36
1
06/29/2116:10
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 16:10
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/2116:10
10061-02-6
ND
ug/L
150
38.7
1
06/29/2116:10
123-91-1
ND
ug/L
1.0
0.30
1
06/29/2116:10
100-41-4
ND
ug/L
5.0
0.48
1
06/29/2116:10
591-78-6
ND
ug/L
20.0
9.7
1
06/29/2116:10
74-88-4
2.1J
ug/L
5.0
2.0
1
06/29/2116:10
75-09-2
ND
ug/L
5.0
2.7
1
06/29/2116:10
108-10-1
ND
ug/L
1.0
0.29
1
06/29/2116:10
100-42-5
ND
ug/L
1.0
0.31
1
06/29/2116:10
630-20-6
ND
ug/L
1.0
0.22
1
06/29/2116:10
79-34-5
ND
ug/L
1.0
0.29
1
06/29/2116:10
127-18-4
ND
ug/L
1.0
0.48
1
06/29/2116:10
108-88-3
ND
ug/L
1.0
0.33
1
06/29/2116:10
71-55-6
ND
ug/L
1.0
0.32
1
06/29/2116:10
79-00-5
ND
ug/L
1.0
0.38
1
06/29/2116:10
79-01-6
ND
ug/L
1.0
0.30
1
06/29/2116:10
75-69-4
ND
ug/L
1.0
0.26
1
06/29/2116:10
96-18-4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 5 of 21

lceAnalyircal
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9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: SURRY BLANKS
Pace Project No.: 92546678
Sample: EB
Parameters
Lab ID:
Results
92546678001
Units
Collected:
Report
Limit
06/25/21 14:09
MDL DF
Received: 06/25/21 16:43 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Vinyl acetate
ND
ug/L
2.0
1.3 1
06/29/21 16:10
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39 1
06/29/21 16:10
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34 1
06/29/21 16:10
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
93
%
70-130
1
06/29/21 16:10
460-00-4
1,2-Dichloroethane-d4 (S)
116
%
70-130
1
06/29/21 16:10
17060-07-0
Toluene-d8 (S)
109
%
70-130
1
06/29/21 16:10
2037-26-5
Date: 07/12/2021 05:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 21

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY BLANKS
Pace Project No.: 92546678
Sample: FB Lab ID: 92546678002 Collected: 06/25/21 14:12 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Date: 07/12/2021 05:20 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
06/29/2116:28
67-64-1
ND
ug/L
10.0
1.8
1
06/29/2116:28
107-13-1
ND
ug/L
1.0
0.34
1
06/29/2116:28
71-43-2
ND
ug/L
1.0
0.47
1
06/29/2116:28
74-97-5
ND
ug/L
1.0
0.31
1
06/29/2116:28
75-27-4
ND
ug/L
1.0
0.34
1
06/29/2116:28
75-25-2
ND
ug/L
2.0
1.7
1
06/29/2116:28
74-83-9
ND
ug/L
5.0
4.0
1
06/29/2116:28
78-93-3
ND
ug/L
2.0
0.73
1
06/29/2116:28
75-15-0
ND
ug/L
1.0
0.33
1
06/29/2116:28
56-23-5
ND
ug/L
1.0
0.28
1
06/29/2116:28
108-90-7
ND
ug/L
1.0
0.65
1
06/29/2116:28
75-00-3
ND
ug/L
5.0
1.6
1
06/29/2116:28
67-66-3
ND
ug/L
1.0
0.54
1
06/29/2116:28
74-87-3
ND
ug/L
2.0
0.34
1
06/29/2116:28
96-12-8
ND
ug/L
1.0
0.36
1
06/29/2116:28
124-48-1
ND
ug/L
1.0
0.27
1
06/29/2116:28
106-93-4
ND
ug/L
1.0
0.39
1
06/29/2116:28
74-95-3
ND
ug/L
1.0
0.34
1
06/29/2116:28
95-50-1
ND
ug/L
1.0
0.33
1
06/29/2116:28
106-46-7
ND
ug/L
1.0
0.56
1
06/29/2116:28
110-57-6
ND
ug/L
1.0
0.37
1
06/29/2116:28
75-34-3
ND
ug/L
1.0
0.32
1
06/29/2116:28
107-06-2
ND
ug/L
1.0
0.35
1
06/29/2116:28
75-35-4
ND
ug/L
1.0
0.38
1
06/29/2116:28
156-59-2
ND
ug/L
1.0
0.40
1
06/29/2116:28
156-60-5
ND
ug/L
1.0
0.36
1
06/29/2116:28
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 16:28
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/2116:28
10061-02-6
ND
ug/L
150
38.7
1
06/29/2116:28
123-91-1
ND
ug/L
1.0
0.30
1
06/29/2116:28
100-41-4
ND
ug/L
5.0
0.48
1
06/29/2116:28
591-78-6
ND
ug/L
20.0
9.7
1
06/29/2116:28
74-88-4
2.1J
ug/L
5.0
2.0
1
06/29/2116:28
75-09-2
ND
ug/L
5.0
2.7
1
06/29/2116:28
108-10-1
ND
ug/L
1.0
0.29
1
06/29/2116:28
100-42-5
ND
ug/L
1.0
0.31
1
06/29/2116:28
630-20-6
ND
ug/L
1.0
0.22
1
06/29/2116:28
79-34-5
ND
ug/L
1.0
0.29
1
06/29/2116:28
127-18-4
ND
ug/L
1.0
0.48
1
06/29/2116:28
108-88-3
ND
ug/L
1.0
0.33
1
06/29/2116:28
71-55-6
ND
ug/L
1.0
0.32
1
06/29/2116:28
79-00-5
ND
ug/L
1.0
0.38
1
06/29/2116:28
79-01-6
ND
ug/L
1.0
0.30
1
06/29/2116:28
75-69-4
ND
ug/L
1.0
0.26
1
06/29/2116:28
96-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
CO
Page 7 of 21

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: SURRY BLANKS
Pace Project No.: 92546678
Sample: FB
Parameters
Lab ID:
Results
92546678002
Units
Collected:
Report
Limit
06/25/21 14:12
MDL DF
Received: 06/25/21 16:43 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Vinyl acetate
ND
ug/L
2.0
1.3 1
06/29/21 16:28
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39 1
06/29/21 16:28
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34 1
06/29/21 16:28
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
06/29/21 16:28
460-00-4
1,2-Dichloroethane-d4 (S)
118
%
70-130
1
06/29/21 16:28
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
06/29/21 16:28
2037-26-5
Date: 07/12/2021 05:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 21

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY BLANKS
Pace Project No.: 92546678
Sample: EB-metals
Lab ID:
92546678003
Collected:
06/25/21 14:09
Received: 06/25/21 16:43 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical
Method: EPA 6010D
Preparation Method: EPA 3010A
Pace Analytical
Services
-Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/08/2111:00
07/09/2100:01
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:01
7440-38-2
Barium
ND
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:01
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/08/2111:00
07/09/2100:01
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/08/2111:00
07/09/2100:01
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/08/2111:00
07/09/2100:01
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/08/2111:00
07/09/2100:01
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/08/2111:00
07/09/2100:01
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/08/2111:00
07/09/2100:01
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:01
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:01
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/08/2111:00
07/09/2100:01
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/08/2111:00
07/09/2100:01
7440-62-2
Zinc
11.2
ug/L
10.0
9.5
1
07/08/2111:00
07/09/2100:01
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020E
Preparation Method: EPA 3010A
Pace Analytical
Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2103:50
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 21

lV11.1 Analytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
QC Batch: 631987 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546678003
METHOD BLANK: 3320015
Associated Lab Samples: 92546678003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
5.0
3.0
07/08/2123:19
Arsenic
ug/L
ND
10.0
4.7
07/08/2123:19
Barium
ug/L
ND
5.0
3.5
07/08/2123:19
Beryllium
ug/L
ND
1.0
0.70
07/08/2123:19
Cadmium
ug/L
ND
1.0
0.40
07/08/2123:19
Chromium
ug/L
ND
5.0
3.7
07/08/2123:19
Cobalt
ug/L
ND
5.0
3.6
07/08/2123:19
Copper
ug/L
ND
5.0
4.3
07/08/2123:19
Lead
ug/L
ND
5.0
4.5
07/08/2123:19
Nickel
ug/L
ND
5.0
3.5
07/08/2123:19
Selenium
ug/L
ND
10.0
4.7
07/08/2123:19
Silver
ug/L
ND
5.0
2.5
07/08/2123:19
Vanadium
ug/L
ND
5.0
3.9
07/08/2123:19
Zinc
ug/L
ND
10.0
9.5
07/08/2123:19
LABORATORY CONTROL SAMPLE:
Parameter
3320016
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
493
99
80-120
Arsenic
ug/L
500
476
95
80-120
Barium
ug/L
500
487
97
80-120
Beryllium
ug/L
500
492
98
80-120
Cadmium
ug/L
500
490
98
80-120
Chromium
ug/L
500
484
97
80-120
Cobalt
ug/L
500
478
96
80-120
Copper
ug/L
500
497
99
80-120
Lead
ug/L
500
480
96
80-120
Nickel
ug/L
500
487
97
80-120
Selenium
ug/L
500
484
97
80-120
Silver
ug/L
250
246
99
80-120
Vanadium
ug/L
500
485
97
80-120
Zinc
ug/L
500
489
98
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
SURRY BLANKS
92546678
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE: 3320017
3320018
MS
MSD
92546523001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
4.9J
500
500
510
514
101
102
75-125
1
20
Arsenic
ug/L
<4.7
500
500
504
506
101
101
75-125
0
20
Barium
ug/L
474
500
500
970
965
99
98
75-125
1
20
Beryllium
ug/L
<0.70
500
500
506
503
101
101
75-125
0
20
Cadmium
ug/L
<0.40
500
500
507
509
101
102
75-125
0
20
Chromium
ug/L
<3.7
500
500
486
495
97
99
75-125
2
20
Cobalt
ug/L
4.8J
500
500
480
482
95
95
75-125
0
20
Copper
ug/L
500
500
512
517
102
103
75-125
1
20
Lead
ug/L
<4.5
500
500
481
481
96
96
75-125
0
20
Nickel
ug/L
5.3
500
500
485
486
96
96
75-125
0
20
Selenium
ug/L
<4.7
500
500
512
517
102
103
75-125
1
20
Silver
ug/L
<2.5
250
250
254
255
101
102
75-125
1
20
Vanadium
ug/L
<3.9
500
500
501
507
100
101
75-125
1
20
Zinc
ug/L
<9.5
500
500
497
498
99
100
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
QC Batch: 631772 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546678003
METHOD BLANK: 3318797
Matrix:
Water
Associated Lab Samples: 92546678003
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Thallium
ug/L
ND
0.47
0.050 07/08/2103:40
LABORATORY CONTROL SAMPLE:
3318798
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
25.2
101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3318799 3318800
MS MSD
92546678003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 25 25 25.5 25.2 102 101 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
QC Batch: 630255 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92546678001, 92546678002
METHOD BLANK: 3311481
Associated Lab Samples: 92546678001, 92546678002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
06/29/21 11:30
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
06/29/21 11:30
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
06/29/21 11:30
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
06/29/21 11:30
1,1-Dichloroethane
ug/L
ND
1.0
0.37
06/29/21 11:30
1,1-Dichloroethene
ug/L
ND
1.0
0.35
06/29/21 11:30
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
06/29/21 11:30
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
06/29/21 11:30
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
06/29/21 11:30
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
06/29/21 11:30
1,2-Dichloroethane
ug/L
ND
1.0
0.32
06/29/21 11:30
1,2-Dichloropropane
ug/L
ND
1.0
0.36
06/29/21 11:30
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
06/29/21 11:30
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
38.7
06/29/21 11:30
2-Butanone (MEK)
ug/L
ND
5.0
4.0
06/29/21 11:30
2-Hexanone
ug/L
ND
5.0
0.48
06/29/21 11:30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
06/29/21 11:30
Acetone
ug/L
ND
25.0
5.1
06/29/21 11:30
Acrylonitrile
ug/L
ND
10.0
1.8
06/29/21 11:30
Benzene
ug/L
ND
1.0
0.34
06/29/21 11:30
Bromochloromethane
ug/L
ND
1.0
0.47
06/29/21 11:30
Bromodichloromethane
ug/L
ND
1.0
0.31
06/29/21 11:30
Bromoform
ug/L
ND
1.0
0.34
06/29/21 11:30
Bromomethane
ug/L
ND
2.0
1.7
06/29/21 11:30
Carbon disulfide
ug/L
ND
2.0
0.73
06/29/21 11:30
Carbon tetrachloride
ug/L
ND
1.0
0.33
06/29/21 11:30
Chlorobenzene
ug/L
ND
1.0
0.28
06/29/21 11:30
Chloroethane
ug/L
ND
1.0
0.65
06/29/21 11:30
Chloroform
ug/L
ND
5.0
1.6
06/29/21 11:30
Chloromethane
ug/L
ND
1.0
0.54
06/29/21 11:30
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
06/29/21 11:30
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/29/21 11:30
Dibromochloromethane
ug/L
ND
1.0
0.36
06/29/21 11:30
Dibromomethane
ug/L
ND
1.0
0.39
06/29/21 11:30
Ethylbenzene
ug/L
ND
1.0
0.30
06/29/21 11:30
lodomethane
ug/L
ND
20.0
9.7
06/29/21 11:30
Methylene Chloride
ug/L
ND
5.0
2.0
06/29/21 11:30
Styrene
ug/L
ND
1.0
0.29
06/29/21 11:30
Tetrachloroethene
ug/L
ND
1.0
0.29
06/29/21 11:30
Toluene
ug/L
ND
1.0
0.48
06/29/21 11:30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
METHOD BLANK: 3311481
Associated Lab Samples: 92546678001, 92546678002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
06/29/21 11:30
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/29/21 11:30
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
06/29/21 11:30
Trichloroethene
ug/L
ND
1.0
0.38
06/29/21 11:30
Trichlorofluoromethane
ug/L
ND
1.0
0.30
06/29/21 11:30
Vinyl acetate
ug/L
ND
2.0
1.3
06/29/21 11:30
Vinyl chloride
ug/L
ND
1.0
0.39
06/29/21 11:30
Xylene (Total)
ug/L
ND
1.0
0.34
06/29/21 11:30
1,2-Dichloroethane-d4 (S)
%
111
70-130
06/29/21 11:30
4-Bromofluorobenzene (S)
%
97
70-130
06/29/21 11:30
Toluene-d8 (S)
%
107
70-130
06/29/21 11:30
LABORATORY CONTROL SAMPLE:
3311482
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
49.6
99
70-130
1,1,1-Trichloroethane
ug/L
50
47.1
94
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.0
100
70-130
1,1,2-Trichloroethane
ug/L
50
49.4
99
70-130
1,1-Dichloroethane
ug/L
50
48.9
98
70-130
1,1-Dichloroethene
ug/L
50
48.2
96
70-132
1,2,3-Trichloropropane
ug/L
50
48.8
98
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
55.1
110
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.5
103
70-130
1,2-Dichlorobenzene
ug/L
50
52.5
105
70-130
1,2-Dichloroethane
ug/L
50
47.8
96
70-130
1,2-Dichloropropane
ug/L
50
49.1
98
70-130
1,4-Dichlorobenzene
ug/L
50
51.2
102
70-130
1,4-Dioxane (p-Dioxane)
ug/L
1000
1020
102
70-137
2-Butanone (MEK)
ug/L
100
105
105
70-133
2-Hexanone
ug/L
100
100
100
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
99.3
99
70-130
Acetone
ug/L
100
107
107
70-144
Acrylonitrile
ug/L
250
247
99
70-130
Benzene
ug/L
50
47.2
94
70-130
Bromochloromethane
ug/L
50
47.3
95
70-130
Bromodichloromethane
ug/L
50
47.9
96
70-130
Bromoform
ug/L
50
44.0
88
70-131
Bromomethane
ug/L
50
55.2
110
30-177
Carbon disulfide
ug/L
50
50.0
100
70-133
Carbon tetrachloride
ug/L
50
47.2
94
70-130
Chlorobenzene
ug/L
50
46.8
94
70-130
Chloroethane
ug/L
50
62.8
126
46-131
Chloroform
ug/L
50
46.4
93
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
LABORATORY CONTROL SAMPLE:
Parameter
3311482
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
Methylene Chloride
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
46.7
93
49-130
49.2
98
70-130
50.2
100
70-130
52.3
105
70-130
46.8
94
70-130
46.1
92
70-130
104
104
47-140
47.9
96
68-130
48.5
97
70-130
44.8
90
70-130
45.9
92
70-130
49.9
100
70-130
52.0
104
70-130
63.3
127
25-200
46.6
93
70-130
43.6
87
61-130
118
118
70-140
47.1
94
59-142
142
95
70-130
100
70-130
99
70-130
96
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3311483
MS
92546336011 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3311484
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.1
20.9
106
104
70-135
1
30
1,1,1-Trichloroethane
ug/L
ND
20
20
22.6
22.5
113
112
70-148
1
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.5
23.0
112
115
70-131
2
30
1,1,2-Trichloroethane
ug/L
ND
20
20
21.7
20.9
109
105
70-136
4
30
1,1-Dichloroethane
ug/L
ND
20
20
24.5
23.3
123
116
70-147
5
30
1,1-Dichloroethene
ug/L
ND
20
20
23.5
25.3
117
127
70-158
8
30
1,2,3-Trichloropropane
ug/L
ND
20
20
22.9
23.3
115
116
67-137
1
30
1,2-Dibromo-3-
ug/L
ND
20
20
21.7
20.1
109
100
69-136
8
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.4
22.5
107
112
70-137
5
30
1,2-Dichlorobenzene
ug/L
ND
20
20
21.3
22.1
106
110
70-133
4
30
1,2-Dichloroethane
ug/L
ND
20
20
22.8
22.7
114
113
67-138
0
30
1,2-Dichloropropane
ug/L
ND
20
20
22.7
22.8
113
114
70-138
1
30
1,4-Dichlorobenzene
ug/L
ND
20
20
21.5
21.7
108
109
70-133
1
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
400
409
442
102
110
69-146
8
30
2-Butanone (MEK)
ug/L
ND
40
40
50.9
48.9
127
122
61-147
4
30
2-Hexanone
ug/L
ND
40
40
42.0
44.0
105
110
67-139
5
30
4-Methyl-2-pentanone
ug/L
ND
40
40
42.7
45.2
107
113
67-136
6
30
(MIBK)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3311483
3311484
MS
MSD
92546336011
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Acetone
ug/L
ND
40
40
49.7
47.7
124
119
55-159
4
30
Acrylonitrile
ug/L
ND
100
100
122
116
122
116
68-140
5
30
Benzene
ug/L
ND
20
20
22.7
22.7
113
114
67-150
0
30
Bromochloromethane
ug/L
ND
20
20
21.5
20.8
107
104
70-146
3
30
Bromodichloromethane
ug/L
ND
20
20
20.8
20.9
104
105
70-138
0
30
Bromoform
ug/L
ND
20
20
17.2
17.6
86
88
57-138
2
30
Bromomethane
ug/L
ND
20
20
28.7
28.1
144
140
10-200
2
30
Carbon disulfide
ug/L
ND
20
20
24.6
24.3
123
122
70-152
1
30
Carbon tetrachloride
ug/L
ND
20
20
21.9
21.0
110
105
70-147
4
30
Chlorobenzene
ug/L
ND
20
20
20.8
22.2
104
111
70-137
6
30
Chloroethane
ug/L
ND
20
20
26.2
25.1
131
125
51-166
4
30
Chloroform
ug/L
ND
20
20
24.6
24.4
123
122
70-144
1
30
Chloromethane
ug/L
ND
20
20
22.9
23.7
114
118
24-161
4
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
23.9
23.2
119
116
67-148
3
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.9
21.4
105
107
70-142
2
30
Dibromochloromethane
ug/L
ND
20
20
20.5
21.3
102
106
68-138
4
30
Dibromomethane
ug/L
ND
20
20
19.9
20.5
99
102
70-134
3
30
Ethylbenzene
ug/L
ND
20
20
21.1
22.4
106
112
68-143
6
30
lodomethane
ug/L
ND
40
40
37.3
41.3
93
103
20-161
10
30
Methylene Chloride
ug/L
ND
20
20
23.2
22.6
116
113
64-148
2
30
Styrene
ug/L
ND
20
20
21.0
22.0
105
110
70-136
5
30
Tetrachloroethene
ug/L
ND
20
20
20.4
20.3
102
101
70-139
1
30
Toluene
ug/L
ND
20
20
21.8
22.3
109
112
47-157
2
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.6
23.9
123
119
70-149
3
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
21.1
21.8
105
109
70-138
4
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
21.2
22.4
106
112
31-145
5
30
Trichloroethene
ug/L
ND
20
20
20.4
21.8
102
109
70-149
6
30
Trichlorofluoromethane
ug/L
ND
20
20
21.1
22.6
106
113
61-154
7
30
Vinyl acetate
ug/L
ND
40
40
49.8
48.1
125
120
48-156
4
30
Vinyl chloride
ug/L
ND
20
20
24.2
24.0
121
120
55-172
1
30
Xylene (Total)
ug/L
ND
60
60
64.1
67.0
107
112
66-145
4
30
1,2-Dichloroethane-d4 (S)
%
112
106
70-130
4-Bromofluorobenzene (S)
%
97
100
70-130
Toluene-d8 (S)
%
100
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 21

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: SURRY BLANKS
Pace Project No.: 92546678
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
CO Result confirmed by second analysis.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 21

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
SURRY BLANKS
92546678
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92546678003
EB-metals
EPA 3010A
631987 EPA 6010D
632207
92546678003
EB-metals
EPA 3010A
631772 EPA 6020B
631953
92546678001
EB
EPA 8260D
630255
92546678002
FB
EPA 8260D
630255
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 21

Document Name: Document Revised: October 28, 2020
Sample Condition Upon Receipt(SCUR) Page 1 of 2
aci3MafyticatLDocument No.: Issuing Authority
F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ HuntersvilleIr"P11. Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑
Name:
Project #
WO#:92546676
92546678
Custody Seal Present? Dyes 'J;4N0 Seals Intact? ❑Yes [gNo
DateiGnilia Werson-Examining-Gontent
Packing Material: ❑Bubble Wrap [RBubbie Bags [-]None ❑ other Biological Tissue Frozen?
Thermometer:
[-]Yes []No 19N/A
Wet ❑9iue ❑None
IR Gun ID: 921064 Type of ice:
q Correction Factor
Cooler Temp: Add/Subtract (°Ci _0 1 Temp should be above freezing to 6'C
q ❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected ('C): U.8 has begun
USDA Regulated Sail ( ® N/A, water sample}
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {internationally,
l—IYes nNn Includrne Hawaii and Puerto Wcoi? FlYes 11No
Comments/Discrepancy:
Chain of Custody Present?
blYes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
3yes
❑No
❑N/A
2.
Short Hold Tlme Analysis <72 hr.i?
❑Yes
IgNo
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
gNo
❑N/A
4.
Sufficient Volume?
'Yes
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
®Yes
®Yes
[:)No
❑No
[-]N/A
❑N/A
6.
Containers Intact?
®Yes
[]No
[]N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
gNo
[-]NIA
B.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
19Yes
[:]No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
[-]Yes
®No
[I N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
[]Yes
❑No
[]No
5gN/A
N/A
11,
j V �
on IQ ,P�D, _ _ Lot ID of split containers: _
CLIENT NOTIFICATION/RESOLUTION
need -to kia ye- Vla:, a 1p a !M aed _ -ror yne-W c- .
OI +- rnn Go(- �Jo _ �n e� Qs need e d_fo r F:6 - - - - - - --
Person contacted: Fyo_y) La*yj b,e�--t _ Date/Time: U -aq
Project Manager SCURF Review: — f t`" 6
Date: te -';'Cl —a 1
Project Manager SRF Review:
Page 19 of 21

Document Name: Document Revised: October 28, 2020
Samule Condition Uoon ReceiotlISCURi I paEP 7 of 7
(ALjU"""y"°"" Document No.:
F-CAR-CS-033•Rev.07
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
** tom_halUoUbox_istoiist_number_of_botties _
Issuing Authority:
Pace Carolinas quality Office
Project ol# ; 92546678
p14: pM8 Due Date: 07/12A21
CLIENT: 92—Municipal j
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot p
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina OEHNR Certification Office (Le,
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 20 of 21

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Page 21 of 21

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
July 12, 2021
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: Surry MSWLF SWs
Pace Project No.: 92546684
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 25, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Accounts Payable, Municipal Engineering Services
Jay Zimmerman, PG, Municipal Engineering Services Co.
REPORT OF LABORATORY ANALYSIS
r
0
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 33

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92546684001
SW-1
Water
06/25/2108:10
06/25/2116:43
92546684002
SW-2
Water
06/25/2111:50
06/25/2116:43
92546684003
SW-3
Water
06/25/2107:55
06/25/2116:43
92546684004
SW-4
Water
06/25/2107:10
06/25/2116:43
92546684005
SWN-1
Water
06/25/2111:05
06/25/2116:43
92546684006
SWN-2
Water
06/25/2113:15
06/25/2116:43
92546684007
SW-C
Water
06/25/2107:30
06/25/2116:43
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92546684001 SW-1
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546684002 SW-2
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546684003 SW-3
EPA 601OD
SH1
14
PASI-A
EPA 601 OD
RDT
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546684004 SW-4
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546684005 SWN-1
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546684006 SWN-2
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546684007 SW-C
EPA 8260D
NSCQ
51
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 33

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SW-1 Lab ID: 92546684001 Collected: 06/25/21 08:10 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/08/2111:00
07/09/2100:04
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:04
7440-38-2
Barium
21.9
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:04
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/08/2111:00
07/09/2100:04
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/08/2111:00
07/09/2100:04
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/08/2111:00
07/09/2100:04
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/08/2111:00
07/09/2100:04
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/08/2111:00
07/09/2100:04
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/08/2111:00
07/09/2100:04
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:04
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:04
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/08/2111:00
07/09/2100:04
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/08/2111:00
07/09/2100:04
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/08/2111:00
07/09/2100:04
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2104:12
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/28/21 20:40
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/28/21 20:40
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/28/21 20:40
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/28/21 20:40
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/28/21 20:40
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/28/21 20:40
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/28/21 20:40
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/28/21 20:40
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/28/21 20:40
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/28/21 20:40
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/28/21 20:40
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/28/21 20:40
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/28/21 20:40
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/28/21 20:40
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/28/21 20:40
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/28/21 20:40
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/28/21 20:40
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/28/21 20:40
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/28/21 20:40
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/28/21 20:40
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/28/21 20:40
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/28/21 20:40
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/28/21 20:40
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/28/21 20:40
75-35-4
REPORT OF
LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 07/12/2021 11:03 AM
without the written consent of Pace Analytical Services,
LLC.
IK
v1
Page 5 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SW-1 Lab ID: 92546684001 Collected: 06/25/21 08:10 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/12/2021 11:03 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/28/21 20:40
156-59-2
ND
ug/L
1.0
0.40
1
06/28/21 20:40
156-60-5
ND
ug/L
1.0
0.36
1
06/28/21 20:40
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 20:40
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/21 20:40
10061-02-6
ND
ug/L
150
38.7
1
06/28/21 20:40
123-91-1
ND
ug/L
1.0
0.30
1
06/28/21 20:40
100-41-4
ND
ug/L
5.0
0.48
1
06/28/21 20:40
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/28/21 20:40
74-88-4
ND
ug/L
5.0
2.0
1
06/28/21 20:40
75-09-2
ND
ug/L
5.0
2.7
1
06/28/21 20:40
108-10-1
ND
ug/L
1.0
0.29
1
06/28/21 20:40
100-42-5
ND
ug/L
1.0
0.31
1
06/28/21 20:40
630-20-6
ND
ug/L
1.0
0.22
1
06/28/21 20:40
79-34-5
ND
ug/L
1.0
0.29
1
06/28/21 20:40
127-18-4
ND
ug/L
1.0
0.48
1
06/28/21 20:40
108-88-3
ND
ug/L
1.0
0.33
1
06/28/21 20:40
71-55-6
ND
ug/L
1.0
0.32
1
06/28/21 20:40
79-00-5
ND
ug/L
1.0
0.38
1
06/28/21 20:40
79-01-6
ND
ug/L
1.0
0.30
1
06/28/21 20:40
75-69-4
ND
ug/L
1.0
0.26
1
06/28/21 20:40
96-18-4
ND
ug/L
2.0
1.3
1
06/28/21 20:40
108-05-4
ND
ug/L
1.0
0.39
1
06/28/21 20:40
75-01-4
ND
ug/L
1.0
0.34
1
06/28/21 20:40
1330-20-7
100
%
70-130
1
06/28/21 20:40
460-00-4
103
%
70-130
1
06/28/21 20:40
17060-07-0
100
%
70-130
1
06/28/21 20:40
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SW-2 Lab ID: 92546684002 Collected: 06/25/21 11:50 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/08/2111:00
07/09/2100:08
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:08
7440-38-2
Barium
24.8
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:08
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/08/2111:00
07/09/2100:08
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/08/2111:00
07/09/2100:08
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/08/2111:00
07/09/2100:08
7440-47-3
Cobalt
28.3
ug/L
5.0
3.6
1
07/08/21 11:00
07/09/2100:08
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/08/2111:00
07/09/2100:08
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/08/2111:00
07/09/2100:08
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:08
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:08
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/08/2111:00
07/09/2100:08
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/08/2111:00
07/09/2100:08
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/08/2111:00
07/09/2100:08
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2104:17
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/28/21 20:58
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/28/21 20:58
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/28/21 20:58
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/28/21 20:58
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/28/21 20:58
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/28/21 20:58
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/28/21 20:58
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/28/21 20:58
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/28/21 20:58
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/28/21 20:58
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/28/21 20:58
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/28/21 20:58
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/28/21 20:58
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/28/21 20:58
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/28/21 20:58
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/28/21 20:58
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/28/21 20:58
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/28/21 20:58
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/28/21 20:58
95-50-1
1,4-Dichlorobenzene
0.33J
ug/L
1.0
0.33
1
06/28/21 20:58
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/28/21 20:58
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/28/21 20:58
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/28/21 20:58
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/28/21 20:58
75-35-4
REPORT OF
LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 07/12/2021 11:03 AM
without the written consent of Pace Analytical Services,
LLC.
IK
v1
Page 7 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SW-2 Lab ID: 92546684002 Collected: 06/25/21 11:50 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/12/2021 11:03 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
2.9
ug/L
1.0
0.38
1
06/28/21 20:58
156-59-2
ND
ug/L
1.0
0.40
1
06/28/21 20:58
156-60-5
ND
ug/L
1.0
0.36
1
06/28/21 20:58
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 20:58
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/21 20:58
10061-02-6
ND
ug/L
150
38.7
1
06/28/21 20:58
123-91-1
ND
ug/L
1.0
0.30
1
06/28/21 20:58
100-41-4
ND
ug/L
5.0
0.48
1
06/28/21 20:58
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/28/21 20:58
74-88-4
ND
ug/L
5.0
2.0
1
06/28/21 20:58
75-09-2
ND
ug/L
5.0
2.7
1
06/28/21 20:58
108-10-1
ND
ug/L
1.0
0.29
1
06/28/21 20:58
100-42-5
ND
ug/L
1.0
0.31
1
06/28/21 20:58
630-20-6
ND
ug/L
1.0
0.22
1
06/28/21 20:58
79-34-5
ND
ug/L
1.0
0.29
1
06/28/21 20:58
127-18-4
ND
ug/L
1.0
0.48
1
06/28/21 20:58
108-88-3
ND
ug/L
1.0
0.33
1
06/28/21 20:58
71-55-6
ND
ug/L
1.0
0.32
1
06/28/21 20:58
79-00-5
ND
ug/L
1.0
0.38
1
06/28/21 20:58
79-01-6
ND
ug/L
1.0
0.30
1
06/28/21 20:58
75-69-4
ND
ug/L
1.0
0.26
1
06/28/21 20:58
96-18-4
ND
ug/L
2.0
1.3
1
06/28/21 20:58
108-05-4
1.0
ug/L
1.0
0.39
1
06/28/21 20:58
75-01-4
ND
ug/L
1.0
0.34
1
06/28/21 20:58
1330-20-7
99
%
70-130
1
06/28/21 20:58
460-00-4
103
%
70-130
1
06/28/21 20:58
17060-07-0
99
%
70-130
1
06/28/21 20:58
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SW-3 Lab ID: 92546684003 Collected: 06/25/21 07:55 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/08/2111:00
07/09/2100:11
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:11
7440-38-2
Barium
45.3
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:11
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/08/2111:00
07/09/2100:11
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/08/2111:00
07/09/2100:11
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/08/2111:00
07/09/2100:11
7440-47-3
Cobalt
27.5
ug/L
5.0
3.6
1
07/08/2111:00
07/09/2100:11
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/08/2111:00
07/09/2100:11
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/08/2111:00
07/09/2100:11
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:11
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:11
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/08/2111:00
07/09/2100:11
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/08/2111:00
07/09/2100:11
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/08/2111:00
07/09/2100:11
7440-66-6
6010 MET ICP, Lab Filtered
Analytical Method: EPA 6010D Preparation Method:
EPA
3010A
Pace Analytical Services
-Asheville
Antimony, Dissolved
ND
ug/L
5.0
3.0
1
07/09/21 16:45
07/10/21 15:58
7440-36-0
P4
Arsenic, Dissolved
ND
ug/L
10.0
4.7
1
07/09/21 16:45
07/10/21 15:58
7440-38-2
P4
Barium, Dissolved
39.6
ug/L
5.0
3.5
1
07/09/21 16:45
07/10/21 15:58
7440-39-3
P4
Beryllium, Dissolved
ND
ug/L
1.0
0.70
1
07/09/21 16:45
07/10/21 15:58
7440-41-7
P4
Cadmium, Dissolved
ND
ug/L
1.0
0.40
1
07/09/21 16:45
07/10/21 15:58
7440-43-9
P4
Chromium, Dissolved
ND
ug/L
5.0
3.7
1
07/09/21 16:45
07/10/21 15:58
7440-47-3
P4
Cobalt, Dissolved
23.5
ug/L
5.0
3.6
1
07/09/21 16:45
07/10/21 15:58
7440-48-4
P4
Copper, Dissolved
ND
ug/L
5.0
4.3
1
07/09/21 16:45
07/10/21 15:58
7440-50-8
P4
Lead, Dissolved
ND
ug/L
5.0
4.5
1
07/09/21 16:45
07/10/21 15:58
7439-92-1
P4
Nickel, Dissolved
ND
ug/L
5.0
3.5
1
07/09/21 16:45
07/10/21 15:58
7440-02-0
P4
Selenium, Dissolved
ND
ug/L
10.0
4.7
1
07/09/21 16:45
07/10/21 15:58
7782-49-2
P4
Silver, Dissolved
ND
ug/L
5.0
2.5
1
07/09/21 16:45
07/10/21 15:58
7440-22-4
P4
Thallium, Dissolved
ND
ug/L
10.0
8.1
1
07/09/21 16:45
07/10/21 15:58
7440-28-0
P4
Vanadium, Dissolved
ND
ug/L
5.0
3.9
1
07/09/21 16:45
07/10/21 15:58
7440-62-2
P4
Zinc, Dissolved
ND
ug/L
10.0
9.5
1
07/09/21 16:45
07/10/21 15:58
7440-66-6
P4
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Pace Analytical Services -Asheville
Thallium
0.10J
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2104:21
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/28/2121:16
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/28/2121:16
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/28/2121:16
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/28/2121:16
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/28/2121:16
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/28/2121:16
75-25-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SW-3 Lab ID: 92546684003 Collected: 06/25/21 07:55 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/12/2021 11:03 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
2.0
1.7
1
06/28/21 21:16
74-83-9
ND
ug/L
5.0
4.0
1
06/28/21 21:16
78-93-3
ND
ug/L
2.0
0.73
1
06/28/21 21:16
75-15-0
ND
ug/L
1.0
0.33
1
06/28/21 21:16
56-23-5
ND
ug/L
1.0
0.28
1
06/28/21 21:16
108-90-7
ND
ug/L
1.0
0.65
1
06/28/21 21:16
75-00-3 IK
ND
ug/L
5.0
1.6
1
06/28/21 21:16
67-66-3
ND
ug/L
1.0
0.54
1
06/28/21 21:16
74-87-3
ND
ug/L
2.0
0.34
1
06/28/21 21:16
96-12-8
ND
ug/L
1.0
0.36
1
06/28/21 21:16
124-48-1
ND
ug/L
1.0
0.27
1
06/28/21 21:16
106-93-4
ND
ug/L
1.0
0.39
1
06/28/21 21:16
74-95-3
ND
ug/L
1.0
0.34
1
06/28/21 21:16
95-50-1
ND
ug/L
1.0
0.33
1
06/28/21 21:16
106-46-7
ND
ug/L
1.0
0.56
1
06/28/21 21:16
110-57-6 v1
ND
ug/L
1.0
0.37
1
06/28/21 21:16
75-34-3
ND
ug/L
1.0
0.32
1
06/28/21 21:16
107-06-2
ND
ug/L
1.0
0.35
1
06/28/21 21:16
75-35-4
ND
ug/L
1.0
0.38
1
06/28/21 21:16
156-59-2
ND
ug/L
1.0
0.40
1
06/28/21 21:16
156-60-5
ND
ug/L
1.0
0.36
1
06/28/21 21:16
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 21:16
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/21 21:16
10061-02-6
ND
ug/L
150
38.7
1
06/28/21 21:16
123-91-1
ND
ug/L
1.0
0.30
1
06/28/21 21:16
100-41-4
ND
ug/L
5.0
0.48
1
06/28/21 21:16
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/28/21 21:16
74-88-4
ND
ug/L
5.0
2.0
1
06/28/21 21:16
75-09-2
ND
ug/L
5.0
2.7
1
06/28/21 21:16
108-10-1
ND
ug/L
1.0
0.29
1
06/28/21 21:16
100-42-5
ND
ug/L
1.0
0.31
1
06/28/21 21:16
630-20-6
ND
ug/L
1.0
0.22
1
06/28/21 21:16
79-34-5
ND
ug/L
1.0
0.29
1
06/28/21 21:16
127-18-4
ND
ug/L
1.0
0.48
1
06/28/21 21:16
108-88-3
ND
ug/L
1.0
0.33
1
06/28/21 21:16
71-55-6
ND
ug/L
1.0
0.32
1
06/28/21 21:16
79-00-5
ND
ug/L
1.0
0.38
1
06/28/21 21:16
79-01-6
ND
ug/L
1.0
0.30
1
06/28/21 21:16
75-69-4
ND
ug/L
1.0
0.26
1
06/28/21 21:16
96-18-4
ND
ug/L
2.0
1.3
1
06/28/21 21:16
108-05-4
ND
ug/L
1.0
0.39
1
06/28/21 21:16
75-01-4
ND
ug/L
1.0
0.34
1
06/28/21 21:16
1330-20-7
98
%
70-130
1
06/28/21 21:16
460-00-4
100
%
70-130
1
06/28/21 21:16
17060-07-0
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
without the written
consent of Pace
Analytical Services, LLC.
Page 10 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SW-3 Lab ID: 92546684003 Collected: 06/25/21 07:55 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Surrogates
Toluene-d8 (S) 100 % 70-130 1 06/28/21 21:16 2037-26-5
Date: 07/12/2021 11:03 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SW-4 Lab ID: 92546684004 Collected: 06/25/21 07:10 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/08/2111:00
07/09/2100:14
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:14
7440-38-2
Barium
16.4
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:14
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/08/2111:00
07/09/2100:14
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/08/2111:00
07/09/2100:14
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/08/2111:00
07/09/2100:14
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/08/2111:00
07/09/2100:14
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/08/2111:00
07/09/2100:14
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/08/2111:00
07/09/2100:14
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:14
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:14
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/08/2111:00
07/09/2100:14
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/08/2111:00
07/09/2100:14
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/08/2111:00
07/09/2100:14
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2104:35
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/28/21 21:34
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/28/21 21:34
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/28/21 21:34
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/28/21 21:34
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/28/21 21:34
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/28/21 21:34
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/28/21 21:34
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/28/21 21:34
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/28/21 21:34
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/28/21 21:34
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/28/21 21:34
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/28/21 21:34
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/28/21 21:34
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/28/21 21:34
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/28/21 21:34
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/28/21 21:34
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/28/21 21:34
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/28/21 21:34
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/28/21 21:34
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/28/21 21:34
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/28/21 21:34
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/28/21 21:34
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/28/21 21:34
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/28/21 21:34
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC.
IK
v1
Page 12 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SW-4 Lab ID: 92546684004 Collected: 06/25/21 07:10 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/12/2021 11:03 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/28/21 21:34
156-59-2
ND
ug/L
1.0
0.40
1
06/28/21 21:34
156-60-5
ND
ug/L
1.0
0.36
1
06/28/21 21:34
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 21:34
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/21 21:34
10061-02-6
ND
ug/L
150
38.7
1
06/28/21 21:34
123-91-1
ND
ug/L
1.0
0.30
1
06/28/21 21:34
100-41-4
ND
ug/L
5.0
0.48
1
06/28/21 21:34
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/28/21 21:34
74-88-4
ND
ug/L
5.0
2.0
1
06/28/21 21:34
75-09-2
ND
ug/L
5.0
2.7
1
06/28/21 21:34
108-10-1
ND
ug/L
1.0
0.29
1
06/28/21 21:34
100-42-5
ND
ug/L
1.0
0.31
1
06/28/21 21:34
630-20-6
ND
ug/L
1.0
0.22
1
06/28/21 21:34
79-34-5
ND
ug/L
1.0
0.29
1
06/28/21 21:34
127-18-4
ND
ug/L
1.0
0.48
1
06/28/21 21:34
108-88-3
ND
ug/L
1.0
0.33
1
06/28/21 21:34
71-55-6
ND
ug/L
1.0
0.32
1
06/28/21 21:34
79-00-5
ND
ug/L
1.0
0.38
1
06/28/21 21:34
79-01-6
ND
ug/L
1.0
0.30
1
06/28/21 21:34
75-69-4
ND
ug/L
1.0
0.26
1
06/28/21 21:34
96-18-4
ND
ug/L
2.0
1.3
1
06/28/21 21:34
108-05-4
ND
ug/L
1.0
0.39
1
06/28/21 21:34
75-01-4
ND
ug/L
1.0
0.34
1
06/28/21 21:34
1330-20-7
99
%
70-130
1
06/28/21 21:34
460-00-4
102
%
70-130
1
06/28/21 21:34
17060-07-0
99
%
70-130
1
06/28/21 21:34
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SWN-1 Lab ID: 92546684005 Collected: 06/25/21 11:05 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/08/2111:00
07/09/2100:18
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:18
7440-38-2
Barium
17.4
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:18
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/08/2111:00
07/09/2100:18
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/08/2111:00
07/09/2100:18
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/08/2111:00
07/09/2100:18
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/08/2111:00
07/09/2100:18
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/08/2111:00
07/09/2100:18
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/08/2111:00
07/09/2100:18
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:18
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:18
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/08/2111:00
07/09/2100:18
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/08/2111:00
07/09/2100:18
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/08/2111:00
07/09/2100:18
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2104:39
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/28/21 21:52
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/28/21 21:52
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/28/21 21:52
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/28/21 21:52
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/28/21 21:52
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/28/21 21:52
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/28/21 21:52
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/28/21 21:52
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/28/21 21:52
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/28/21 21:52
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/28/21 21:52
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/28/21 21:52
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/28/21 21:52
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/28/21 21:52
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/28/21 21:52
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/28/21 21:52
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/28/21 21:52
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/28/21 21:52
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/28/21 21:52
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/28/21 21:52
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/28/21 21:52
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/28/21 21:52
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/28/21 21:52
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/28/21 21:52
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC.
IK
v1
Page 14 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SWN-1 Lab ID: 92546684005 Collected: 06/25/21 11:05 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/12/2021 11:03 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/28/21 21:52
156-59-2
ND
ug/L
1.0
0.40
1
06/28/21 21:52
156-60-5
ND
ug/L
1.0
0.36
1
06/28/21 21:52
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 21:52
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/21 21:52
10061-02-6
ND
ug/L
150
38.7
1
06/28/21 21:52
123-91-1
ND
ug/L
1.0
0.30
1
06/28/21 21:52
100-41-4
ND
ug/L
5.0
0.48
1
06/28/21 21:52
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/28/21 21:52
74-88-4
ND
ug/L
5.0
2.0
1
06/28/21 21:52
75-09-2
ND
ug/L
5.0
2.7
1
06/28/21 21:52
108-10-1
ND
ug/L
1.0
0.29
1
06/28/21 21:52
100-42-5
ND
ug/L
1.0
0.31
1
06/28/21 21:52
630-20-6
ND
ug/L
1.0
0.22
1
06/28/21 21:52
79-34-5
ND
ug/L
1.0
0.29
1
06/28/21 21:52
127-18-4
ND
ug/L
1.0
0.48
1
06/28/21 21:52
108-88-3
ND
ug/L
1.0
0.33
1
06/28/21 21:52
71-55-6
ND
ug/L
1.0
0.32
1
06/28/21 21:52
79-00-5
ND
ug/L
1.0
0.38
1
06/28/21 21:52
79-01-6
ND
ug/L
1.0
0.30
1
06/28/21 21:52
75-69-4
ND
ug/L
1.0
0.26
1
06/28/21 21:52
96-18-4
ND
ug/L
2.0
1.3
1
06/28/21 21:52
108-05-4
ND
ug/L
1.0
0.39
1
06/28/21 21:52
75-01-4
ND
ug/L
1.0
0.34
1
06/28/21 21:52
1330-20-7
100
%
70-130
1
06/28/21 21:52
460-00-4
101
%
70-130
1
06/28/21 21:52
17060-07-0
99
%
70-130
1
06/28/21 21:52
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SWN-2 Lab ID: 92546684006 Collected: 06/25/21 13:15 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/08/2111:00
07/09/2100:21
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:21
7440-38-2
Barium
16.2
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:21
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/08/2111:00
07/09/2100:21
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/08/2111:00
07/09/2100:21
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/08/2111:00
07/09/2100:21
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/08/2111:00
07/09/2100:21
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/08/2111:00
07/09/2100:21
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/08/2111:00
07/09/2100:21
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:21
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:21
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/08/2111:00
07/09/2100:21
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/08/2111:00
07/09/2100:21
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/08/2111:00
07/09/2100:21
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2104:44
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/28/21 22:10
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/28/21 22:10
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/28/21 22:10
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/28/21 22:10
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/28/21 22:10
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/28/21 22:10
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/28/21 22:10
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/28/21 22:10
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/28/21 22:10
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/28/21 22:10
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/28/21 22:10
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/28/21 22:10
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/28/21 22:10
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/28/21 22:10
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/28/21 22:10
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/28/21 22:10
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/28/21 22:10
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/28/21 22:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/28/21 22:10
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/28/21 22:10
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/28/21 22:10
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/28/21 22:10
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/28/21 22:10
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/28/21 22:10
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC.
IK
v1
Page 16 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SWN-2 Lab ID: 92546684006 Collected: 06/25/21 13:15 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/12/2021 11:03 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/28/21 22:10
156-59-2
ND
ug/L
1.0
0.40
1
06/28/21 22:10
156-60-5
ND
ug/L
1.0
0.36
1
06/28/21 22:10
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 22:10
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/21 22:10
10061-02-6
ND
ug/L
150
38.7
1
06/28/21 22:10
123-91-1
ND
ug/L
1.0
0.30
1
06/28/21 22:10
100-41-4
ND
ug/L
5.0
0.48
1
06/28/21 22:10
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/28/21 22:10
74-88-4
ND
ug/L
5.0
2.0
1
06/28/21 22:10
75-09-2
ND
ug/L
5.0
2.7
1
06/28/21 22:10
108-10-1
ND
ug/L
1.0
0.29
1
06/28/21 22:10
100-42-5
ND
ug/L
1.0
0.31
1
06/28/21 22:10
630-20-6
ND
ug/L
1.0
0.22
1
06/28/21 22:10
79-34-5
ND
ug/L
1.0
0.29
1
06/28/21 22:10
127-18-4
ND
ug/L
1.0
0.48
1
06/28/21 22:10
108-88-3
ND
ug/L
1.0
0.33
1
06/28/21 22:10
71-55-6
ND
ug/L
1.0
0.32
1
06/28/21 22:10
79-00-5
ND
ug/L
1.0
0.38
1
06/28/21 22:10
79-01-6
ND
ug/L
1.0
0.30
1
06/28/21 22:10
75-69-4
ND
ug/L
1.0
0.26
1
06/28/21 22:10
96-18-4
ND
ug/L
2.0
1.3
1
06/28/21 22:10
108-05-4
ND
ug/L
1.0
0.39
1
06/28/21 22:10
75-01-4
ND
ug/L
1.0
0.34
1
06/28/21 22:10
1330-20-7
98
%
70-130
1
06/28/21 22:10
460-00-4
101
%
70-130
1
06/28/21 22:10
17060-07-0
99
%
70-130
1
06/28/21 22:10
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SW-C Lab ID: 92546684007 Collected: 06/25/21 07:30 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Date: 07/12/2021 11:03 AM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
06/28/2122:28
67-64-1
ND
ug/L
10.0
1.8
1
06/28/2122:28
107-13-1
ND
ug/L
1.0
0.34
1
06/28/2122:28
71-43-2
ND
ug/L
1.0
0.47
1
06/28/2122:28
74-97-5
ND
ug/L
1.0
0.31
1
06/28/2122:28
75-27-4
ND
ug/L
1.0
0.34
1
06/28/2122:28
75-25-2
ND
ug/L
2.0
1.7
1
06/28/2122:28
74-83-9
ND
ug/L
5.0
4.0
1
06/28/2122:28
78-93-3
ND
ug/L
2.0
0.73
1
06/28/2122:28
75-15-0
ND
ug/L
1.0
0.33
1
06/28/2122:28
56-23-5
ND
ug/L
1.0
0.28
1
06/28/2122:28
108-90-7
ND
ug/L
1.0
0.65
1
06/28/2122:28
75-00-3
ND
ug/L
5.0
1.6
1
06/28/2122:28
67-66-3
ND
ug/L
1.0
0.54
1
06/28/2122:28
74-87-3
ND
ug/L
2.0
0.34
1
06/28/2122:28
96-12-8
ND
ug/L
1.0
0.36
1
06/28/2122:28
124-48-1
ND
ug/L
1.0
0.27
1
06/28/2122:28
106-93-4
ND
ug/L
1.0
0.39
1
06/28/2122:28
74-95-3
ND
ug/L
1.0
0.34
1
06/28/2122:28
95-50-1
ND
ug/L
1.0
0.33
1
06/28/2122:28
106-46-7
ND
ug/L
1.0
0.56
1
06/28/2122:28
110-57-6
ND
ug/L
1.0
0.37
1
06/28/2122:28
75-34-3
ND
ug/L
1.0
0.32
1
06/28/2122:28
107-06-2
ND
ug/L
1.0
0.35
1
06/28/2122:28
75-35-4
ND
ug/L
1.0
0.38
1
06/28/2122:28
156-59-2
ND
ug/L
1.0
0.40
1
06/28/2122:28
156-60-5
ND
ug/L
1.0
0.36
1
06/28/2122:28
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 22:28
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/2122:28
10061-02-6
ND
ug/L
150
38.7
1
06/28/2122:28
123-91-1
ND
ug/L
1.0
0.30
1
06/28/2122:28
100-41-4
ND
ug/L
5.0
0.48
1
06/28/2122:28
591-78-6
ND
ug/L
20.0
9.7
1
06/28/2122:28
74-88-4
ND
ug/L
5.0
2.0
1
06/28/2122:28
75-09-2
ND
ug/L
5.0
2.7
1
06/28/2122:28
108-10-1
ND
ug/L
1.0
0.29
1
06/28/2122:28
100-42-5
ND
ug/L
1.0
0.31
1
06/28/2122:28
630-20-6
ND
ug/L
1.0
0.22
1
06/28/2122:28
79-34-5
ND
ug/L
1.0
0.29
1
06/28/2122:28
127-18-4
ND
ug/L
1.0
0.48
1
06/28/2122:28
108-88-3
ND
ug/L
1.0
0.33
1
06/28/2122:28
71-55-6
ND
ug/L
1.0
0.32
1
06/28/2122:28
79-00-5
ND
ug/L
1.0
0.38
1
06/28/2122:28
79-01-6
ND
ug/L
1.0
0.30
1
06/28/2122:28
75-69-4
ND
ug/L
1.0
0.26
1
06/28/2122:28
96-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
IN
v1
v1
Page 18 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
Sample: SW-C
Parameters
Lab ID:
Results
92546684007
Units
Collected:
Report
Limit
06/25/21 07:30
MDL DF
Received: 06/25/21 16:43 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Vinyl acetate
ND
ug/L
2.0
1.3 1
06/28/21 22:28
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39 1
06/28/21 22:28
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34 1
06/28/21 22:28
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
06/28/21 22:28
460-00-4
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
06/28/21 22:28
17060-07-0
Toluene-d8 (S)
98
%
70-130
1
06/28/21 22:28
2037-26-5
Date: 07/12/2021 11:03 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 33

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92546684
QC Batch: 631987 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546684001, 92546684002, 92546684003, 92546684004, 92546684005, 92546684006
METHOD BLANK: 3320015 Matrix: Water
Associated Lab Samples: 92546684001, 92546684002, 92546684003, 92546684004, 92546684005, 92546684006
Blank Reporting
Parameter Units Result Limit MDL Analyzed
Antimony
ug/L
ND
5.0
3.0
07/08/2123:19
Arsenic
ug/L
ND
10.0
4.7
07/08/2123:19
Barium
ug/L
ND
5.0
3.5
07/08/2123:19
Beryllium
ug/L
ND
1.0
0.70
07/08/2123:19
Cadmium
ug/L
ND
1.0
0.40
07/08/2123:19
Chromium
ug/L
ND
5.0
3.7
07/08/2123:19
Cobalt
ug/L
ND
5.0
3.6
07/08/2123:19
Copper
ug/L
ND
5.0
4.3
07/08/2123:19
Lead
ug/L
ND
5.0
4.5
07/08/2123:19
Nickel
ug/L
ND
5.0
3.5
07/08/2123:19
Selenium
ug/L
ND
10.0
4.7
07/08/2123:19
Silver
ug/L
ND
5.0
2.5
07/08/2123:19
Vanadium
ug/L
ND
5.0
3.9
07/08/2123:19
Zinc
ug/L
ND
10.0
9.5
07/08/2123:19
LABORATORY CONTROL SAMPLE:
Parameter
3320016
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
493
99
80-120
Arsenic
ug/L
500
476
95
80-120
Barium
ug/L
500
487
97
80-120
Beryllium
ug/L
500
492
98
80-120
Cadmium
ug/L
500
490
98
80-120
Chromium
ug/L
500
484
97
80-120
Cobalt
ug/L
500
478
96
80-120
Copper
ug/L
500
497
99
80-120
Lead
ug/L
500
480
96
80-120
Nickel
ug/L
500
487
97
80-120
Selenium
ug/L
500
484
97
80-120
Silver
ug/L
250
246
99
80-120
Vanadium
ug/L
500
485
97
80-120
Zinc
ug/L
500
489
98
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 33

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Surry MSWLF SWs
92546684
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3320017
3320018
MS
MSD
92546523001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
4.9J
500
500
510
514
101
102
75-125
1
20
Arsenic
ug/L
<4.7
500
500
504
506
101
101
75-125
0
20
Barium
ug/L
474
500
500
970
965
99
98
75-125
1
20
Beryllium
ug/L
<0.70
500
500
506
503
101
101
75-125
0
20
Cadmium
ug/L
<0.40
500
500
507
509
101
102
75-125
0
20
Chromium
ug/L
<3.7
500
500
486
495
97
99
75-125
2
20
Cobalt
ug/L
4.8J
500
500
480
482
95
95
75-125
0
20
Copper
ug/L
500
500
512
517
102
103
75-125
1
20
Lead
ug/L
<4.5
500
500
481
481
96
96
75-125
0
20
Nickel
ug/L
5.3
500
500
485
486
96
96
75-125
0
20
Selenium
ug/L
<4.7
500
500
512
517
102
103
75-125
1
20
Silver
ug/L
<2.5
250
250
254
255
101
102
75-125
1
20
Vanadium
ug/L
<3.9
500
500
501
507
100
101
75-125
1
20
Zinc
ug/L
<9.5
500
500
497
498
99
100
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC.
Page 21 of 33

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92546684
QC Batch: 631994 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET Filtered Diss.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546684003
METHOD BLANK: 3320032
Associated Lab Samples: 92546684003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony, Dissolved
ug/L
ND
5.0
3.0
07/10/21 15:45
Arsenic, Dissolved
ug/L
ND
10.0
4.7
07/10/21 15:45
Barium, Dissolved
ug/L
ND
5.0
3.5
07/10/21 15:45
Beryllium, Dissolved
ug/L
ND
1.0
0.70
07/10/21 15:45
Cadmium, Dissolved
ug/L
ND
1.0
0.40
07/10/21 15:45
Chromium, Dissolved
ug/L
ND
5.0
3.7
07/10/21 15:45
Cobalt, Dissolved
ug/L
ND
5.0
3.6
07/10/21 15:45
Copper, Dissolved
ug/L
ND
5.0
4.3
07/10/21 15:45
Lead, Dissolved
ug/L
ND
5.0
4.5
07/10/21 15:45
Nickel, Dissolved
ug/L
ND
5.0
3.5
07/10/21 15:45
Selenium, Dissolved
ug/L
ND
10.0
4.7
07/10/21 15:45
Silver, Dissolved
ug/L
ND
5.0
2.5
07/10/21 15:45
Thallium, Dissolved
ug/L
ND
10.0
8.1
07/10/21 15:45
Vanadium, Dissolved
ug/L
ND
5.0
3.9
07/10/21 15:45
Zinc, Dissolved
ug/L
ND
10.0
9.5
07/10/21 15:45
LABORATORY CONTROL SAMPLE:
Parameter
3320033
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony, Dissolved
ug/L
500
433
87
80-120
Arsenic, Dissolved
ug/L
500
419
84
80-120
Barium, Dissolved
ug/L
500
436
87
80-120
Beryllium, Dissolved
ug/L
500
434
87
80-120
Cadmium, Dissolved
ug/L
500
440
88
80-120
Chromium, Dissolved
ug/L
500
434
87
80-120
Cobalt, Dissolved
ug/L
500
415
83
80-120
Copper, Dissolved
ug/L
500
423
85
80-120
Lead, Dissolved
ug/L
500
428
86
80-120
Nickel, Dissolved
ug/L
500
436
87
80-120
Selenium, Dissolved
ug/L
500
426
85
80-120
Silver, Dissolved
ug/L
250
216
87
80-120
Thallium, Dissolved
ug/L
500
418
84
80-120
Vanadium, Dissolved
ug/L
500
432
86
80-120
Zinc, Dissolved
ug/L
500
431
86
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC.
Page 22 of 33

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92546684
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3320034
3320035
MS
MSD
92546684003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony, Dissolved
ug/L
ND
500
500
438
427
87
85
75-125
3
20
Arsenic, Dissolved
ug/L
ND
500
500
424
412
84
82
75-125
3
20
Barium, Dissolved
ug/L
39.6
500
500
471
458
86
84
75-125
3
20
Beryllium, Dissolved
ug/L
ND
500
500
433
423
87
85
75-125
2
20
Cadmium, Dissolved
ug/L
ND
500
500
437
422
87
84
75-125
4
20
Chromium, Dissolved
ug/L
ND
500
500
429
420
86
84
75-125
2
20
Cobalt, Dissolved
ug/L
23.5
500
500
435
424
82
80
75-125
3
20
Copper, Dissolved
ug/L
ND
500
500
427
417
85
83
75-125
2
20
Lead, Dissolved
ug/L
ND
500
500
423
410
84
82
75-125
3
20
Nickel, Dissolved
ug/L
ND
500
500
431
418
86
83
75-125
3
20
Selenium, Dissolved
ug/L
ND
500
500
429
417
86
83
75-125
3
20
Silver, Dissolved
ug/L
ND
250
250
218
211
87
84
75-125
3
20
Thallium, Dissolved
ug/L
ND
500
500
402
391
80
78
75-125
3
20
Vanadium, Dissolved
ug/L
ND
500
500
434
421
87
84
75-125
3
20
Zinc, Dissolved
ug/L
ND
500
500
431
418
86
83
75-125
3
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC.
Page 23 of 33

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92546684
QC Batch: 631772 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546684001, 92546684002, 92546684003, 92546684004, 92546684005, 92546684006
METHOD BLANK: 3318797 Matrix: Water
Associated Lab Samples: 92546684001, 92546684002, 92546684003, 92546684004, 92546684005, 92546684006
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 0.47 0.050 07/08/2103:40
LABORATORY CONTROL SAMPLE: 3318798
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 25 25.2 101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3318799 3318800
MS MSD
92546678003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 25 25 25.5 25.2 102 101 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC.
Page 24 of 33

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92546684
QC Batch: 630139 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92546684001, 92546684002, 92546684003, 92546684004, 92546684005, 92546684006, 92546684007
METHOD BLANK: 3311182 Matrix: Water
Associated Lab Samples: 92546684001, 92546684002, 92546684003, 92546684004, 92546684005, 92546684006, 92546684007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
06/28/21 19:27
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
06/28/21 19:27
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
06/28/21 19:27
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
06/28/21 19:27
1,1-Dichloroethane
ug/L
ND
1.0
0.37
06/28/21 19:27
1,1-Dichloroethene
ug/L
ND
1.0
0.35
06/28/21 19:27
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
06/28/21 19:27
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
06/28/21 19:27
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
06/28/21 19:27
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
06/28/21 19:27
1,2-Dichloroethane
ug/L
ND
1.0
0.32
06/28/21 19:27
1,2-Dichloropropane
ug/L
ND
1.0
0.36
06/28/21 19:27
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
06/28/21 19:27
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
38.7
06/28/21 19:27
2-Butanone (MEK)
ug/L
ND
5.0
4.0
06/28/21 19:27
2-Hexanone
ug/L
ND
5.0
0.48
06/28/21 19:27
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
06/28/21 19:27
Acetone
ug/L
ND
25.0
5.1
06/28/21 19:27
Acrylonitrile
ug/L
ND
10.0
1.8
06/28/21 19:27
Benzene
ug/L
ND
1.0
0.34
06/28/21 19:27
Bromochloromethane
ug/L
ND
1.0
0.47
06/28/21 19:27
Bromodichloromethane
ug/L
ND
1.0
0.31
06/28/21 19:27
Bromoform
ug/L
ND
1.0
0.34
06/28/21 19:27
Bromomethane
ug/L
ND
2.0
1.7
06/28/21 19:27
Carbon disulfide
ug/L
ND
2.0
0.73
06/28/21 19:27
Carbon tetrachloride
ug/L
ND
1.0
0.33
06/28/21 19:27
Chlorobenzene
ug/L
ND
1.0
0.28
06/28/21 19:27
Chloroethane
ug/L
ND
1.0
0.65
06/28/21 19:27
Chloroform
ug/L
ND
5.0
1.6
06/28/21 19:27
Chloromethane
ug/L
ND
1.0
0.54
06/28/21 19:27
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
06/28/21 19:27
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/28/21 19:27
Dibromochloromethane
ug/L
ND
1.0
0.36
06/28/21 19:27
Dibromomethane
ug/L
ND
1.0
0.39
06/28/21 19:27
Ethylbenzene
ug/L
ND
1.0
0.30
06/28/21 19:27
lodomethane
ug/L
ND
20.0
9.7
06/28/21 19:27
Methylene Chloride
ug/L
ND
5.0
2.0
06/28/21 19:27
Styrene
ug/L
ND
1.0
0.29
06/28/21 19:27
Tetrachloroethene
ug/L
ND
1.0
0.29
06/28/21 19:27
Toluene
ug/L
ND
1.0
0.48
06/28/21 19:27
v1
I:/
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 33

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92546684
METHOD BLANK: 3311182 Matrix: Water
Associated Lab Samples: 92546684001, 92546684002, 92546684003, 92546684004, 92546684005, 92546684006, 92546684007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
06/28/21 19:27
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/28/21 19:27
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
06/28/21 19:27 v1
Trichloroethene
ug/L
ND
1.0
0.38
06/28/21 19:27
Trichlorofluoromethane
ug/L
ND
1.0
0.30
06/28/21 19:27
Vinyl acetate
ug/L
ND
2.0
1.3
06/28/21 19:27
Vinyl chloride
ug/L
ND
1.0
0.39
06/28/21 19:27
Xylene (Total)
ug/L
ND
1.0
0.34
06/28/21 19:27
1,2-Dichloroethane-d4 (S)
%
103
70-130
06/28/21 19:27
4-Bromofluorobenzene (S)
%
99
70-130
06/28/21 19:27
Toluene-d8 (S)
%
99
70-130
06/28/21 19:27
LABORATORY CONTROL SAMPLE:
Parameter
3311183
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
52.6
105
70-130
1,1,1-Trichloroethane
ug/L
50
51.0
102
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
57.5
115
70-130
1,1,2-Trichloroethane
ug/L
50
53.8
108
70-130
1,1-Dichloroethane
ug/L
50
52.4
105
70-130
1,1-Dichloroethene
ug/L
50
53.2
106
70-132
1,2,3-Trichloropropane
ug/L
50
56.0
112
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
61.8
124
70-132
1,2-Dibromoethane (EDB)
ug/L
50
54.2
108
70-130
1,2-Dichlorobenzene
ug/L
50
54.8
110
70-130
1,2-Dichloroethane
ug/L
50
49.3
99
70-130
1,2-Dichloropropane
ug/L
50
53.2
106
70-130
1,4-Dichlorobenzene
ug/L
50
56.1
112
70-130
1,4-Dioxane (p-Dioxane)
ug/L
1000
1280
128
70-137
2-Butanone (MEK)
ug/L
100
123
123
70-133
2-Hexanone
ug/L
100
125
125
70-130 v1
4-Methyl-2-pentanone (MIBK)
ug/L
100
124
124
70-130
Acetone
ug/L
100
110
110
70-144
Acrylonitrile
ug/L
250
282
113
70-130
Benzene
ug/L
50
51.8
104
70-130
Bromochloromethane
ug/L
50
45.5
91
70-130
Bromodichloromethane
ug/L
50
52.9
106
70-130
Bromoform
ug/L
50
56.8
114
70-131
Bromomethane
ug/L
50
50.5
101
30-177
Carbon disulfide
ug/L
50
54.4
109
70-133
Carbon tetrachloride
ug/L
50
51.5
103
70-130
Chlorobenzene
ug/L
50
53.2
106
70-130
Chloroethane
ug/L
50
37.3
75
46-131 IK
Chloroform
ug/L
50
53.2
106
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 33

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92546684
LABORATORY CONTROL SAMPLE:
Parameter
3311183
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloromethane
ug/L
50
54.0
cis-1,2-Dichloroethene
ug/L
50
52.5
cis-1,3-Dichloropropene
ug/L
50
57.6
Dibromochloromethane
ug/L
50
53.5
Dibromomethane
ug/L
50
53.7
Ethylbenzene
ug/L
50
52.7
lodomethane
ug/L
100
104
Methylene Chloride
ug/L
50
50.4
Styrene
ug/L
50
54.9
Tetrachloroethene
ug/L
50
50.5
Toluene
ug/L
50
52.9
trans-1,2-Dichloroethene
ug/L
50
53.2
trans- 1,3-Dichloropropene
ug/L
50
57.7
trans-1,4-Dichloro-2-butene
ug/L
50
77.9
Trichloroethene
ug/L
50
53.5
Trichlorofluoromethane
ug/L
50
48.3
Vinyl acetate
ug/L
100
126
Vinyl chloride
ug/L
50
52.2
Xylene (Total)
ug/L
150
157
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
108
49-130
105
70-130
115
70-130
107
70-130
107
70-130
105
70-130
104
47-140
101
68-130
110
70-130
101
70-130
106
70-130
106
70-130
115
70-130
156
25-200 v1
107
70-130
97
61-130
126
70-140
104
59-142
105
70-130
93
70-130
99
70-130
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3311184
MS
92546693010 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3311185
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.5
20.5
107
102
70-135
5
30
1,1,1-Trichloroethane
ug/L
ND
20
20
21.3
20.3
107
101
70-148
5
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.1
21.3
110
107
70-131
3
30
1,1,2-Trichloroethane
ug/L
ND
20
20
21.5
20.9
108
104
70-136
3
30
1,1-Dichloroethane
ug/L
ND
20
20
21.6
20.8
108
104
70-147
4
30
1,1-Dichloroethene
ug/L
ND
20
20
22.2
21.6
111
108
70-158
3
30
1,2,3-Trichloropropane
ug/L
ND
20
20
21.7
20.9
108
105
67-137
3
30
1,2-Dibromo-3-
ug/L
ND
20
20
23.0
22.4
115
112
69-136
3
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.4
21.0
107
105
70-137
2
30
1,2-Dichlorobenzene
ug/L
ND
20
20
22.2
21.6
111
108
70-133
3
30
1,2-Dichloroethane
ug/L
ND
20
20
19.9
19.1
99
96
67-138
4
30
1,2-Dichloropropane
ug/L
ND
20
20
21.9
21.2
109
106
70-138
3
30
1,4-Dichlorobenzene
ug/L
ND
20
20
23.2
22.5
116
113
70-133
3
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
400
498
475
124
119
69-146
5
30
2-Butanone (MEK)
ug/L
ND
40
40
42.7
42.5
107
106
61-147
1
30
2-Hexanone
ug/L
ND
40
40
46.2
44.7
115
112
67-139
3
30
4-Methyl-2-pentanone
ug/L
ND
40
40
44.5
44.2
111
110
67-136
1
30
(MIBK)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC.
Page 27 of 33

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92546684
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3311184
3311185
MS
MSD
92546693010
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Acetone
ug/L
ND
40
40
39.5
38.6
99
96
55-159
2
30
Acrylonitrile
ug/L
ND
100
100
107
103
107
103
68-140
4
30
Benzene
ug/L
ND
20
20
21.5
21.3
108
107
67-150
1
30
Bromochloromethane
ug/L
ND
20
20
19.8
19.7
99
98
70-146
1
30
Bromodichloromethane
ug/L
ND
20
20
21.0
20.8
105
104
70-138
1
30
Bromoform
ug/L
ND
20
20
21.4
21.0
107
105
57-138
2
30
Bromomethane
ug/L
ND
20
20
19.7
21.6
99
108
10-200
9
30 IH
Carbon disulfide
ug/L
ND
20
20
22.6
22.1
113
110
70-152
2
30
Carbon tetrachloride
ug/L
ND
20
20
21.8
21.6
109
108
70-147
1
30
Chlorobenzene
ug/L
ND
20
20
22.5
21.8
112
109
70-137
3
30
Chloroethane
ug/L
ND
20
20
24.1
24.5
120
122
51-166
2
30
Chloroform
ug/L
ND
20
20
21.2
20.9
106
105
70-144
1
30
Chloromethane
ug/L
ND
20
20
18.1
18.0
91
90
24-161
1
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
21.4
20.6
107
103
67-148
4
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
23.0
22.3
115
112
70-142
3
30
Dibromochloromethane
ug/L
ND
20
20
21.3
20.4
107
102
68-138
4
30
Dibromomethane
ug/L
ND
20
20
22.0
21.2
110
106
70-134
4
30
Ethylbenzene
ug/L
ND
20
20
22.6
21.7
113
109
68-143
4
30
lodomethane
ug/L
ND
40
40
50.9
53.5
127
134
20-161
5
30
Methylene Chloride
ug/L
ND
20
20
20.4
19.8
102
99
64-148
3
30
Styrene
ug/L
ND
20
20
22.8
22.0
114
110
70-136
4
30
Tetrachloroethene
ug/L
ND
20
20
22.2
21.6
111
108
70-139
3
30
Toluene
ug/L
ND
20
20
21.9
21.5
109
108
47-157
2
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
22.0
21.4
110
107
70-149
3
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.3
22.1
112
111
70-138
1
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
23.3
23.1
116
115
31-145
1
30 IH,v1
Trichloroethene
ug/L
ND
20
20
22.3
22.1
111
111
70-149
1
30
Trichlorofluoromethane
ug/L
ND
20
20
21.1
20.5
106
103
61-154
3
30
Vinyl acetate
ug/L
ND
40
40
46.5
44.7
116
112
48-156
4
30
Vinyl chloride
ug/L
ND
20
20
21.8
21.3
109
107
55-172
2
30
Xylene (Total)
ug/L
ND
60
60
67.9
64.6
113
108
66-145
5
30
1,2-Dichloroethane-d4 (S)
%
96
96
70-130
4-Bromofluorobenzene (S)
%
99
99
70-130
Toluene-d8 (S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC.
Page 28 of 33

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALIFIERS
Project: Surry MSWLF SWs
Pace Project No.: 92546684
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
P4 Sample field preservation does not meet EPA or method recommendations for this analysis.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 11:03 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 33

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Surry MSWLF SWs
92546684
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92546684001
SW-1
EPA 3010A
631987
EPA 6010D
632207
92546684002
SW-2
EPA 3010A
631987
EPA 6010D
632207
92546684003
SW-3
EPA 3010A
631987
EPA 6010D
632207
92546684004
SW-4
EPA 3010A
631987
EPA 6010D
632207
92546684005
SWN-1
EPA 3010A
631987
EPA 6010D
632207
92546684006
SWN-2
EPA 3010A
631987
EPA 6010D
632207
92546684003
SW-3
EPA 3010A
631994
EPA 6010D
632545
92546684001
SW-1
EPA 3010A
631772
EPA 6020B
631953
92546684002
SW-2
EPA 3010A
631772
EPA 6020B
631953
92546684003
SW-3
EPA 3010A
631772
EPA 6020B
631953
92546684004
SW-4
EPA 3010A
631772
EPA 6020B
631953
92546684005
SWN-1
EPA 3010A
631772
EPA 6020B
631953
92546684006
SWN-2
EPA 3010A
631772
EPA 6020B
631953
92546684001
SW-1
EPA 8260D
630139
92546684002
SW-2
EPA 8260D
630139
92546684003
SW-3
EPA 8260D
630139
92546684004
SW-4
EPA 8260D
630139
92546684005
SWN-1
EPA 8260D
630139
92546684006
SWN-2
EPA 8260D
630139
92546684007
SW-C
EPA 8260D
630139
Date: 07/12/2021 11:03 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 30 of 33

Document Name: Document Revised: October 28, 2020
r Sample Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F•CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [`%� Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
Sample • Client Name: l
Upon Receipt , , r , I Pro;ecttt WQ# : 92546684
❑ Commercial [Pace ❑Other:
92545684
Custody Seal Present? ❑Yes �No Seals Intact? [:]Yes PNo a�
Date%lnitials.Rerson-Examining.Gonten
Packing Material: Q13ubble Wrap Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: �t, ❑Yes [-]No ®N/A
IR Gun ID: rJwet ❑Blue ❑None
92TO64 Type of Ice:
Correction Factor:
Cooler Temp: Add/Subtract (•C) _p i Temp should be above freezing to VC
[]Samples out of temp uiteria. Samples on ice, cooling process
Cooler Temp Corrected (•C): �. has begun
USDA Regulated Sail (,g N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source !internationally,
F�Yes MNo including Hawaii and Puerto Ricol? ❑Yes ❑No
Comments/Discrepancy:
Chain of Custody Present?
plyes
❑ND
❑N/A
1.
Samples Arrived within Hold Time?
Yes
QNO
[]N/A
2.
Short Hold Time Analysis (c72 hr.)?
❑Yes
JANo
[]N/A
3,
Rush Turn Around Tlme Requested?
❑Yes
[gNo
❑N/A
4.
Sufficient Volume?
[@Yes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
[BYes
Yes
❑No
(:]No
❑N/A
❑N/A
6.
Containers Intact?
®Yes
[-]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
nNo
❑N/A
8.
Sample Labels Match COC?
-Includes Date/Time/10/Analysis Matr+x:
oyes
YY
❑No
[-]N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
nNo
Cl NIA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
❑No
[]No
JflN/A
ON/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No
Lot ID of solit containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:-�1�Ol�l'±i} p�� I Date/Time: -{� tL� �— � " � _
Project Manager SCURF Review: _ IA:::m �L2 _ _ _ Date: -I — i _,a l
Project Manager SRF Review: Date: Page 31 of 33

Document Name:
Document Revised: October 28, 2020
�acena1—cd7-
Sample Condition Upon Receipt(SCUR _
Pag F
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.07
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dethlorination is Project W�# ■92�����4
verified and within the acceptance range for preservation ■
samples. PM: RMB Due Date: 07/12/21
Exceptions: VOA, Califprm, TOC, Oil and Grease, DRO/BOIS (water) DOC, LLHg CLIENT: 92—Munic ipa 1
**Bottom_half_nfbox_is_to_list_numb.er_o.f-bottles_—_... _____.-___... _. I _
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot N
Nate: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 32 of 33

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Page 33 of 33