8603_Surry_Elkin_MSWLF_CDLF_June21GW_20211018

Electronic Data - Email CD (data loaded: Yes / No
NC DENR
Division of Waste Management - Solid Waste
Doc/Event #:
Environmental Monitoring
Renortina Form
Notice: This
form and
any
information attached
to it are "Public Records"
as defined in NC
General Statute 132-1. As such, these documents are
available for
inspection
and
examination by any
person upon request (NC
General Statute 132-6),
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Municipal Engineering Services Co., PA
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Jonathan Pfohl Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit* (.0500 or .1600) October 20-24, 2006)
Surry County Closed C&D and Landfill Road off Joe Mill Lane (SR 1121) g6 03 .1600 FJune, 2021
Closed MSW Landfill -Elkin Elkin, NC 28621
Environmental Status: (Check all that apply)
Initial/Background Monitoring �X Detection Monitoring ❑X Assessment Monitoring � Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells
Leachate monitoring data ❑
Surface water monitorina data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were Exceeded.
X Yes, a notification of values exceeding -a groundwater o,r surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
FJ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements -made on this data submittal and attachments are trua and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis -of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making -any false statement, representation, or certification including the possibility of a fine and imprisonment.
S.J. Zimmerman, P.G. Project Manager [phone]
P.O. Box 97. Garner. NC 27529
Facility Representative Address
C-0281
NC PE Firm License Number (if applicable effective May 1, 2009)
a Code) Telephone Numb ers�, ,"
Affix NC License, P�ofession��'C7eologist Seal
Q.'�� fin•.
111,
011.
rlA
111,
1172
e45,4r I M �« �
Revised 6/2009

Semi -Annual Water Quality Monitoring Report
June 2021
Prepared for
Surry County Closed C&D and Closed Landfill
Elkin, North Carolina
Permit No. 86-03
Prepared by
Municipal Engineering Services Company, P.A.
P.O. BOX 97
S. J. �aihi e man, P.G.
Senior Project Manager
j [e-mail]
Garner, North Carolina
MESCO Project Number: G21031.0
MUNICIPAL ENGINEERING
�E SERVICES COMPANY P.A.
f� 68 SHIPWASH DRIVE, GARNER, NC 27529 - PHONE: [phone]
P.D. Box 349, BODNE. NC 28607 - PHONE: [phone]
LICENSE NUMBER: 0-O281
Jonathan Pfohl
Environmental Specialist
infohl a,mesco.com

Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to
present this Semi -Annual Water Quality Monitoring Report for an event performed at the Surry County
closed construction and demolition (C&D) and closed unlined municipal solid waste landfill (MSWLF)
located in Elkin NC (SWS Permit No. 86-03) on June 24-25, 2021. The site is located at the end of
Landfill Road off Joe Mill Lane (SR 1121), Elkin, Surry County, North Carolina. The site location
topographic map is depicted as Sheet 1.
NCDEQ Solid Waste Rules 15ANCAC1313.1630 through .1637 require that Surry County provide this
monitoring report to the SWS on a semi-annual basis. In general accordance with 15A NCAC
13B.16320), the SWS Environmental Monitoring Report Form and SWS memorandums, this report
contains sampling procedures, field and laboratory results, groundwater characterization and a brief
discussion of the findings. Detection tables, a potentiometric map, field parameters and the laboratory
analytical reports with quality assurance/quality control data and chains -of -custody (COC) are also
included in this report.
Laboratory analytical results indicate that between one and four constituents were detected above their
reporting limit and respective North Carolina Groundwater Standard in groundwater samples collected
from 4 wells. No parameters were detected above allowable standards in samples collected from either
surface water point.
Background
Prior to operating as a C&D landfill the site operated as an unlined sanitary MSWLF that consisted of two
units. The first area was closed prior to October 1991 with a 24 inch final soil cover. The second area was
closed with a cohesive cap of 18 inches of soil with a minimum permeability of less than 1 x 10-5 cm/sec,
and 18 inches of erosive layer prior to December 31, 1998 in accordance with the Transition Plan. C&D
waste was placed on top of the cohesive capped MSW unit until 2008. The transfer station that operated
at the landfill closed around June 2010 and the site has remained vacant since.
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data
available since 1994. The landfill has been in assessment monitoring since 1997 in response to
detections of VOCs. The SWS approved a modification to the assessment monitoring program on
October 15, 2014 (DIN:21983) which entails a subset of wells to be sampled for Appendix II parameters
once every three years which was last performed in December 2020.
Sampling Locations
The monitoring network includes 12 locations; nine downgradient monitoring wells (MW-2, MW-3,
MW-3A, MW-4, MW-5, MW-6, MW-7S, MW-713 and MW-8), a background monitoring well (MW-1)
and two downstream surface water points (SW-1, SW-2). All locations were sampled during this event.
Water monitoring locations are depicted on Sheet 2. A summary detailing the construction of the water
monitoring wells is presented on Table 1.

Sampling Procedures
Sampling was conducted utilizing portable methodologies outlined in the NCDENR SWS guidance
document Solid Waste Section Guidelines for Groundwater, Soil, and Surface Water Sampling revised
April 2008. The function and integrity of all monitoring locations were visually evaluated as documented
on Table 2. The depth to water in each well was electronically gaged prior to purging to quantify the
static water level elevation. Bailing or submersible pumping was utilized to purge the wells a minimum
of three times the volume of standing water in the well or until dry. Surface water samples were dipped
from the surface of Snow Creek at previously designated locations. Stabilized field parameters were
recorded during purging. Samples were then placed into laboratory -prepared, pre -preserved containers.
Samples were kept on ice and transported to a NC -certified laboratory under proper chain of custody (C-
O-C) protocol within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters recorded during purging included pH, specific conductance, temperature,
hardness and turbidity. A summary of the field parameter data is presented in Table 3 and field data
sheets are in Appendix A. In general field parameter results remain consistent with previously reported
events.
Laboratory Results
Pace Analytical Laboratories (PACE) (NC Cert. #12 & 40) performed the laboratory analysis. Pace
reported that their procedures conformed to the most current, applicable TNI/NELAC standards and their
Quality Assurance Manual, where applicable, unless otherwise noted in the body of the laboratory report.
Water samples were tested for constituents listed in 40 CFR 258 Appendix I and 1,4-dioxane. A
sampling and analysis table summarizing the locations, targeted constituents and methods is presented as
Table 4. Laboratory results and C-O-Cs are presented in Appendix B.
Water samples were analyzed to the laboratory -established Method Detection Limits (MDL) and any
value between the MDL and laboratory -established Reporting Limit (RL) is qualified by the laboratory as
with a "J" which indicates an estimated concentration. "J-qualified" concentrations are considered non -
quantifiable and discretion should be made prior to making decisions based on a value that the laboratory
considers an estimate. Table 5 summarizes constituents detected in groundwater samples compared to
Interim Maximum Allowable Concentrations (IMAC) and North Carolina Groundwater Standards (2L)
which are recognized by the NC SWS as groundwater compliance Standards. Although not applicable for
regulatory compliance purposes the detections are also compared to the Maximum Contaminant Level
(MCL) commonly referenced as the Federal Primary "Drinking Water Standard". Table 6 lists the
constituents detected in surface water samples compared with the NC Division of Water Resources
"Surface Water Quality Standards, Criteria & Protected Values", modified July 26, 2021.
Groundwater Samples Above Standards
Metals
One or two total recoverable metals were detected above their respective NC 2L/IMAC value in samples
collected from three wells as summarized below.
Metals Detected Above NC 2L/IMAC
Arsenic
Cadmium
Cobalt
2L/IMAC
10
2
1
MW-2
29
MW-3A
36.6
MW-6
3
27
ug/L
2

VOCs
One to three VOCs were also detected above the RL and NC 2L Standard in samples collected from 3
wells as summarized below.
VOCs Detected in Groundwater Samples Above RL and NC 2L Standard
1,4-DCB
Benzene
1,4-Dioxane
2L
6
1
3
MW-2
14.9
3.7
153
MW-3
1.6
MW-3A
10.5
ug/L
Surface Water Samples Above Standards
No constituents were detected above those allowed per NC 2B Rules in either surface water sample (SW-
1, SW-2) collected downstream of the facility.
Groundwater Characterization
A single -day potentiometric map constructed from groundwater levels collected during this event is
presented as Sheet 2. Groundwater flow rates and directions were calculated and are included in Table 7.
Groundwater flows generally southwest, towards the Snow Creek discharge feature. Groundwater average
linear velocity rates calculated from modified Darcy's equation indicate flow rates ranged from
approximately 22 ft/yr (MW-7S) to 295 ft/yr (MW-4).
Findings
Parameters attributed to a release of leachate and/or landfill gas continue to be detected above compliance
Standards in groundwater samples collected downgradient of the landfill. Concentrations for all of the
constituents remain within their respective historically identified range. The reduction in VOC
concentrations over time and distance from the landfill and the prevalence of biodegradation byproducts
indicate natural attenuation is occurring and groundwater quality is expected to continue to improve.
No constituents were detected in either surface water sample.
Closing
Semi-annual water quality assessment monitoring is planned to be performed again in the Fall of 2021.
Notwithstanding any changes samples will be tested for Appendix II parameters in the winter of 2023.
3

Sheets

Topographic Map with Site Location
Surry County Closed MSW/C&D Landfill - Elkin
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ROAD CLASSIFICATION
QUADRANGLE LEGEND Primary highway, Light -duty road, hard or
hard Surface... _-.. improved surface........__ --- _
Secondary highway,
�� hard surface... Unimproved road.. ---------
1" — 2000Interstate Route rj U. S Route 0 State Route
Landfill Road (Off Joe Mill Ln SR 1121)
Elkin, NC 28621
Lat:36-17-49.4007
Long:-80-46-20.6499
Northing:931704.33
Easting:1477683.95
SHEET 1

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PIN: 497300725490 I
OWNER: SURRY COUNTY �� \
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PIN: 497300914703
OWNER: HERRERA VINEYARDS LLC
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OWNER: FINNEY _
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NOTES:
1. TOPOGRAPHIC CONTOURS FROM NC ONEMAP (11-2013)
2. WELL LOCATIONS PLOTTED WITH ELEVATIONS EXTRAPOLATED
FROM AERIAL PHOTOGPAHY INSPECTION
3. PARCEL BOUNDARY FROM NC ONEMAP (10/2018)
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TOPOGRAPHIC CONTOURS
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SURFACE WATER MONITORING POINT
UPPERMOST GROUNDWATER CONTOUR (INFERRED)
Lu
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GWE: GROUNDWATER ELEVATION (APPROXIMATE)
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GRAPHIC SCALE
200 0 100 200 400
( IN FEET )
SHEET L
m
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SCALE: AS SHOWN
DATE: 1017121
DRWN. BY: J. PFOHL
CHKD. BY: J. PFOHL
PROJECT NUMBER
G21031.0
DRAWING NO.
SHEET NO.

Tables

Table 1
Groundwater Monitoring Well Construction Table
June 24, 2021
Monitoring
Well
Date
Installed
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length
Geology of Screened
Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
Latitude
Longitude
(inches)
(ft bgs)
(ft bgs)
(ft)
(ft amsl)
(ft amsl)
(ft amsl)
(ft btoc)
MW-1
11/28/89
4
80
70
10
Soil
1042
1041
994
48.11
36.29711
-80.77236
MW-2
11/08/89
4
79
69
10
Soil
948
947
894
54.46
36.29572
-80.77620
MW-3
11/28/89
4
63
53
10
Soil
932
931
883
48.91
36.29362
-80.77646
MW-3A
09/16/94
2
40
24
16
Fractured Rock
927
924
896
30.81
36.29457
-80.77675
MW-4
09/15/94
2
29
13
16
Fractured Rock
933
929
922
10.78
36.29379
-80.77528
MW-5
09/15/94
2
31
16
15
Fractured Rock
949
845
938
10.80
36.29450
-80.77456
MW-6
09/15/94
2
66
51
15
Fractured Rock
1005
1002
958
46.65
36.29780
-80.77270
MW-7S
06/05/01
2
24
9
15
Fractured Rock
901
889
890
11.15
36.29407
-80.77730
MW-7D
06/05/01
2
90
80
10
Fractured Rock
901
889
889
11.74
36.29407
-80.77730
MW-8
1 06/04/01
1 2
1 67
52
15
Fractured Rock
1015
1013
979
35.59
36.29739
-80.77246
NOTE:
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Slurry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 1
Groundwater Monitoring Well Construction Table
June 24, 2021
Monitoring
Well
Date
Installed
Well
Diameter
Total
Well
Depth
Top of
Screen
Depth
Screen
Length
Geology of Screened
Interval
Top of
Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
Latitude
Longitude
(inches)
(ft bgs)
(ft bgs)
(ft)
(ft amsl)
(ft amsl)
(ft amsl)
(ft btoc)
MW-1
11/28/89
4
80
70
10
Soil
1042
1041
994
48.11
36.29711
-80.77236
MW-2
11/08/89
4
79
69
10
Soil
948
947
894
54.46
36.29572
-80.77620
MW-3
11/28/89
4
63
53
10
Soil
932
931
883
48.91
36.29362
-80.77646
MW-3A
09/16/94
2
40
24
16
Fractured Rock
927
924
896
30.81
36.29457
-80.77675
MW-4
09/15/94
2
29
13
16
Fractured Rock
933
929
922
10.78
36.29379
-80.77528
MW-5
09/15/94
2
31
16
15
Fractured Rock
949
845
938
10.80
36.29450
-80.77456
MW-6
09/15/94
2
66
51
15
Fractured Rock
1005
1002
958
46.65
36.29780
-80.77270
MW-7S
06/05/01
2
24
9
15
Fractured Rock
901
889
890
11.15
36.29407
-80.77730
MW-7D
06/05/01
2
90
80
10
Fractured Rock
901
889
889
11.74
36.29407
-80.77730
MW-8
1 06/04/01
1 2
1 67
52
15
Fractured Rock
1015
1013
979
35.59
36.29739
-80.77246
NOTE:
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Slurry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 3
Field Parameter Data Summary
June 24-25, 2021
Parameter
Depth to
Water
ft (btoc)
Water
Elevation*
ft (amsl)
TOC
Elevation*
ft (amsl)
Temp.
C
pH
SU
Specific
Conductance
umhos/cm
Hardness
mg/L
Turbidity of
Metals Sample
NTU
MW-1
52.65
989
1042.00
16.9
6.87
71
1660
-
4.36
MW-2
55.91
892
948.00
17.1
6.21
--
51.1
MW-3
48.79
883
932.00
17.3
6.35
204
--
2.33
MW-3A
30.68
896
926.50
16.5
6.36
890
--
4.95
MW-4
10.90
922
932.50
15.9
6.09
28
--
12.3
MW-5
10.63
938
948.50
16.1
6.15
54
--
6.45
MW-6
46.00
959
1004.50
15.8
6.33
374
--
48.3
MW-7S
10.57
890
901.01
15.7
6.75
206
--
2.11
MW-7D
2.75
898
900.95
15.4
7.84
103
--
7.36
MW-8
38.52
976
1014.87
15.9
6.89
150
--
14.3
Minimum
2.75
883
900.95
15.4
6.09
28
--
2.11
Average
30.74
924
955.08
16.3
6.58
374
--
15.4
Maximum
55.91
989
1042.00
17.3
7.84
1660
--
51.1
SW-1
-
-
-
19.4
7.31
103
17.1
8.36
SW-2
-
-
-
19.1
7.26
94
17.1
9.04
Minimum
-
-
-
19.1
7.26
94
17.1
8.36
Average
-
-
-
-
19.3
7.29
99
17.1
8.70
Maximum
-
-
19.4
7.31
103
17.1
9.04
NOTES:
* = Elevation extrapolated from photo inspected LIDAR released in 2007 by NCDOT (Not Surveyed).
btoc = below top of casing
amsl = above mean sea level
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 4
Sampling and Analysis Summary
June 25, 2021
App.
I
Other
Field
Parameters
ro
T
-2:1
co
IZ
X
M
N
>
U
J
U
0
O
>
H
H
2
U
a
H
0
0
0
t:
0
0
M
CD
<°
CDN
0
cc
00
00
d
<
w
Y
w
w
a
N
J
N
J
N
J
LL
LL
LL
LL
LL
MW-1
x
x
x
x
x
x
x
MW-2
x
x
x
x
x
x
x
MW-3
x
x
x
x
x
x
x
MW-3A
x
x
x
x
x
x
x
MW-4
x
x
x
x
x
x
x
MW-5
x
x
x
x
x
x
x
MW-6
x
x
x
x
x
x
x
MW-7S
x
x
x
x
x
x
x
MW-7D
x
x
x
x
x
x
x
MW-8
x
x
x
x
x
x
x
SW-1
x
x
x
x
x
x
x
x
SW-2
x
x
x
x
x
x
x
x
EB
x
x
x
FB
x
x
App I & II = Lists from current 40 CFR 258
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 5
Groundwater Sample Detections
June 25, 2021
Parameter Name
MDL
RL
2L Standard
MCL
MW-1
MW-2
MW-3
MW-3A
MW-4
MW-5
MW-6
MW-7D
MW-7S
MW-8
EB
FB
IMAC Value
BG
S
S
S
S
S
S
S
S
S
QC
QC
Metal(Tarcieted 40CFR 258 ADDendix
I
Antimony, total
3
5
1
6
Arsenic, total
4.7
10
10
10
29 (U
Barium, total
3.5
1
700
2000
27.6
295
66.8
398
23.3
21.4
94.4
11.3
116
Cadmium, total
0.4
1
2
5
1
0.92 J
0.83 J
0.5 J
1.4
3 (U
0.93 J
1.6
Cobalt, total
3.6
5
1
NE
36.6 (U
27 (L)
Nickel, total
3.5
1
100
NE
4.4 J
30.1
30.9
8.2
Lead, total
4.5
5
15
15
9.4
Selenium, total
4.7
10
20
50
7 J
Zinc, total
9.5
10
1000
NE
L
11.2
VOCs (Tarneted
40CFR 258 Appendix
I & 1, 4-Dioxane
1,1-Dichloroethane
0.37
1
6
NE
0.48 J
0.54 J
0.57 J
0.73 J
1,2-Dichlorobenzene
0.34
1
20
NE
8.2
3.4
1.9
0.37J
1,2-Dichloroethane
0.32
1
0.4
5
0.56J
1,2-Dichloropropane
0.36
1
0.6
5
0.51 J
1,4-Dichlorobenzene
0.33
1
6
75
14.9 (L)
3.1
10.5 (U
2.8
1,4-Dioxane
38.7
150
3
NE
153 (U
Benzene
0.34
1
1
5
1.9 (L)
1.6 (U
0.76 J
0.71 J
0.35 J
Chlorobenzene
0.28
1
50
100
13.1
0.54 J
4.7
6.6
0.29 J
cis-1,2-Dichloroethene
0.38
1
70
70
0.44 J
6.1
8.6
2.5
1.8
4.2
2.3
Methylene Chloride
2
5
5
5
2.1 J
2.1 J
Toluene
0.48
1
600
1000
0.7 J
Trichloroethene
0.38
1
3
5
0.63 J
Vinyl chloride
1 0.39
1 1
1 0.03
1 2
Notes:
Units ug/L unless shown otherwise, Blank cells means not detected above MDL, NE means not established.
BG= Background Well Sample, S = Sentinel Well Sample, QC = Quality Control Sample
Bold Above RL and Established 2L/IMAC
Above Established Federal MCL Drinking Water Std. (NOT a regulatory compliance Standard)
U= Well Upgradient, D = Well Downgradient
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
matrix."
2L Standard and IMAC Values recognized by the NC SWS as regulatory groundater Standards.
2L = NC 2L Groundater Standard 15A NCAC 02L .0202
IMAC = Interim Maximum Allowable Concentration
MCL = Maximum Contaminant Level for drinking water established by the USEPA.
J = "J-qualified". Defined by the lab as "estimated concentration above the adjusted method detection limit and below the adjusted reporting limit".
(L) Prelilminary source is believed to be anthropogenic with Landfill Gas Wor leachate as suspected transport mechanism.
A definitive source of the detections was not determined as part of this report.
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 6
Surface Water Sample Detections
June 25, 2021
Parameter Name
MDL
RL
B
STD17T
NRWQC2
isTV3
MCC
SW-2
Do nst ream
Downstream
Targeted 40CFR 258 Appendix I & 1 4-Dioxane
Barium, total 0.28 11 NE
NE 1200,000 1 2000 19.5
19.4
Hardness
Hardness 117,1001 NE I NE
NE I NE I NE 17100
17,100
Notes:
Units ug/L unless indicated otherwise, Blank cells means Not Detected, NE means Not Established
Bold Above Applicable Established 2B Std.
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
analyte
in a specific matrix."
Receiving surface water is Snow Creek (12-62-15) Class C
' NC 2B STD = North Carolina 15A NCAC 02B Water Quality Standards for Surface Waters. Presumed NC SWS adopted the numerical Standard for regulatory compliance purposes.
'EPA NRWQC = EPA Nationally Recommended Water Quality Criteria for Aquatic Life & Human Health.
Nationally Recommended Water Quality Criteria for which NC does not have a Water Quality Standard for one or more uses.
s NC ISTV= North Carolina In -Stream Target Value. Established per language in 15A NCAC 02B .0202 & .0208. Contact DWR staff for further information.
NC PV for barium from fresh and salt water All waters (Class C & SC) for fish consumption.
4 MCL= Maximum Contaminant Level. Federal 'Primary Drinking Water Standard". Shown for comparison purposes only. Not applicable for regulatory compliance purposes.
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Table 7
Hydrologic Properties at Monitoring Locations
June 24, 2021
Monitoring
Well
Hydraulic
Conductivity
(cm/second)
Effective
Porosity
N
Hydraulic
Gradient
(feet/feet)
Groundwater
Average Linear
Velocity Rate
(feet/year)
Flow
Direction
Depth to
Groundwater
(ft btoc)
Groundwater
Potentiometric
Elevation*
(ft amsl)
Screened Interval
Lithology
MW-1
9.90E-05
5
0.143
293
N39W
50.63
994
Clay
MW-2
2.00E-05
5
na
na
na
53.45
894**
Clay
MW-3
5.00E-05
5
na
na
na
48.27
883**
Clay
Minimum
2.00E-05
5
0.143
293
-
48.27
884
-
Average
5.63E-05
5
0.143
293
-
50.78
923
-
Maximum
9.90E-05
5
0.143
293
-
53.45
991
-
MW-3A
2.50E-05
5
0.316
163
S61 W
30.38
896
Fractured Rock
MW-4
4.20E-04
5
0.034
295
S70W
10.23
922
Fractured Rock
MW-5
2.70E-04
5
0.033
186
N74W
9.72
938
Fractured Rock
MW-6
1.20E-04
5
0.025
61
N08W
44.51
958
Fractured Rock
MW-7S
2.30E-04
5
0.005
22
S79W
10.47
890
Fractured Rock
MW-7D
na
na
na
na
na
14.17
889**
Fractured Rock
MW-8
2.40E-05
5
0.281
140
N23W
37.18
979
Fractured Rock
Minimum
2.40E-05
5
0.005
22
-
9.72
896
-
Average
1.82E-04
5
0.116
144
-
22.38
925
-
Maximum
4.20E-04
1 5
1 0.316
295
1-
44.51
1 939
1-
NOTE: Effective porosity data obtained from GAI Consultants' January 1995 Groundwater Sampling Report.
Hydraulic conductivity values from MW-7S and MW-8 derived from slug tests performed by Joyce Engineering on July 25, 2001.
Values for MW-1 through MW-6 obtained from GAI consultants' January 1995 Groundwater Sampling Report.
Hydrologic gradient calculated from groundwater elevations recorded June 24, 2021.
Wells screened in both the upper bedrock & unconfined aquifer utilized for flow directions/gradients.
= Datum used to determine elevation extrapolated from photo inspected LIDAR released 2007 by NCDOT (Not Surveyed).
* = Denotes wells with depressed potentiometric head. Therefore, flow directions and rates not calculable.
Average Linear Velocity Rate (Q) is defined by modified Darcy's equation:
where K A
Q _ne dl
K = hydraulic conductivity
ne = effective porosity
dh = head difference
dl = horizontal distance
Surry County Closed C&D and Closed MSWLF, Elkin Page 1 of 1

Appendix A
Field Sampling Parameter Data Sheet(s)

\lurvlrlpul ���-� t.nulua<rinC
f I
Project: Surry Co Closed MSWLF & Closed C&D LF, Elkin Samplers: age_ _o
E , i- !2 ,-r, . e d
Sampling
Parameters
Water
Quality
Parameters
Depth to
Water
1Nater
Lab
Parameters
Volume
Sampl
oes
Dry
Total
Depth
Total
CO2
DO
Temp.
Specific
Cond.
TDS
o
Hard-
ness
Monitoring
Purge
Purge
Sample
Sample
Point
Date
Time
Date
Time
(BT
to be
Purged
(Gal)
e Type
Durin
Measured
as
Depth
Expected
(mg/1)
m /L
( g )
ORP
pH
©
(us/Cm
(mg/L)
�
(mg/L)
�j
Static
analyzed for
9
expected
MW-1
R
. (
I(7)
Q
�J
V
80
�'
MW-2
-�;, �,
I(5)
v t
;t I-_ -j,.
79
� �
1 7: S
;
1 60
MW-3
9
l
I(I)
C
� r
80
17.E
e 4
�.
MW-3A
j
o' 0
Im2)
1i
40
�/ , 5-
8.1()
MW-4
1 �`,, C
, $
j t� 20
1 I(0)
29
fit.
1 -S ,
0
3
MW-5
`r _
ss_ 6 ("
I(0)
i
31
!
i d , !
iS"t 5
MW-6
I(3)
,0
MW-7S
Irv',
1
I(6)
C) C 1,ti
24
/7
MW-7D
� �
°-��.—
/. �
In
C
�d-�'i
90
I . `f
1 t)
3b
MW-8
tJ
5,
I(4)
j {�-
�� ��
67
SW-1
I(0)
_zla2
--
2
-
9,01
L
qe
SS B=Stainless Steel Baler, D B=Disposable Baler, P=Low flow Pump, PD=Purged Dry
VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear
NR=No Reading Attempted, NS=No Sample Obtained

Appendix B
Laboratory Analysis Reports
Chains of Custody

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
July 14, 2021
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between June 25, 2021 and July 01, 2021. The
results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC
Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Accounts Payable, Municipal Engineering Services
Jay Zimmerman, PG, Municipal Engineering Services Co.
REPORT OF LABORATORY ANALYSIS
r
0
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92546693001
MW-1
Water
06/25/2109:35
06/25/2116:43
92546693002
MW-2
Water
06/25/2108:13
06/25/2116:43
92546693003
MW-3
Water
06/25/2108:31
06/25/2116:43
92546693004
MW-3A
Water
06/25/2108:18
06/25/2116:43
92546693005
MW-4
Water
06/25/2109:10
06/25/2116:43
92546693006
MW-5
Water
06/25/2109:15
06/25/2116:43
92546693007
MW-7S
Water
06/25/2108:05
06/25/2116:43
92546693008
MW-7D
Water
06/25/2108:09
06/25/2116:43
92546693009
MW-8
Water
06/25/2109:40
06/25/2116:43
92546693010
SW-1
Water
06/25/2108:24
06/25/2116:43
92546693011
SW-2
Water
06/25/2108:45
06/25/2116:43
92546693012
MW-6
Water
06/25/2109:45
07/01/2110:56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Surry Closed LF-Elkin
92546693
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92546693001
MW-1
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546693002
MW-2
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546693003
MW-3
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546693004
MW-3A
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546693005
MW-4
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546693006
MW-5
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
51
PASI-C
92546693007
MW-7S
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546693008
MW-7D
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546693009
MW-8
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546693010
SW-1
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546693011
SW-2
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
92546693012
MW-6
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MWA Lab ID: 92546693001 Collected: 06/25/21 09:35 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/2111:50
07/13/2120:35
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2120:35
7440-38-2
Barium
27.6
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2120:35
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/2111:50
07/13/2120:35
7440-41-7
Cadmium
1.0
ug/L
1.0
0.40
1
07/13/21 11:50
07/13/2120:35
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/2111:50
07/13/2120:35
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/13/2111:50
07/13/2120:35
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/2111:50
07/13/2120:35
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/13/2111:50
07/13/2120:35
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2120:35
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2120:35
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/2111:50
07/13/2120:35
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/2111:50
07/13/2120:35
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/2111:50
07/13/2120:35
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2104:49
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/28/21 22:47
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/28/21 22:47
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/28/21 22:47
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/28/21 22:47
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/28/21 22:47
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/28/21 22:47
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/28/21 22:47
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/28/21 22:47
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/28/21 22:47
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/28/21 22:47
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/28/21 22:47
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/28/21 22:47
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/28/21 22:47
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/28/21 22:47
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/28/21 22:47
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/28/21 22:47
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/28/21 22:47
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/28/21 22:47
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/28/21 22:47
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/28/21 22:47
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/28/21 22:47
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/28/21 22:47
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/28/21 22:47
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/28/21 22:47
75-35-4
REPORT OF
LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 07/14/2021 04:06 PM
without the written consent of Pace Analytical Services,
LLC.
IK
v1
Page 6 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-1 Lab ID: 92546693001 Collected: 06/25/21 09:35 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/28/21 22:47
156-59-2
ND
ug/L
1.0
0.40
1
06/28/21 22:47
156-60-5
ND
ug/L
1.0
0.36
1
06/28/21 22:47
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 22:47
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/21 22:47
10061-02-6
ND
ug/L
150
38.7
1
06/28/21 22:47
123-91-1
ND
ug/L
1.0
0.30
1
06/28/21 22:47
100-41-4
ND
ug/L
5.0
0.48
1
06/28/21 22:47
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/28/21 22:47
74-88-4
ND
ug/L
5.0
2.0
1
06/28/21 22:47
75-09-2
ND
ug/L
5.0
2.7
1
06/28/21 22:47
108-10-1
ND
ug/L
1.0
0.29
1
06/28/21 22:47
100-42-5
ND
ug/L
1.0
0.31
1
06/28/21 22:47
630-20-6
ND
ug/L
1.0
0.22
1
06/28/21 22:47
79-34-5
ND
ug/L
1.0
0.29
1
06/28/21 22:47
127-18-4
ND
ug/L
1.0
0.48
1
06/28/21 22:47
108-88-3
ND
ug/L
1.0
0.33
1
06/28/21 22:47
71-55-6
ND
ug/L
1.0
0.32
1
06/28/21 22:47
79-00-5
ND
ug/L
1.0
0.38
1
06/28/21 22:47
79-01-6
ND
ug/L
1.0
0.30
1
06/28/21 22:47
75-69-4
ND
ug/L
1.0
0.26
1
06/28/21 22:47
96-18-4
ND
ug/L
2.0
1.3
1
06/28/21 22:47
108-05-4
ND
ug/L
1.0
0.39
1
06/28/21 22:47
75-01-4
ND
ug/L
1.0
0.34
1
06/28/21 22:47
1330-20-7
101
%
70-130
1
06/28/21 22:47
460-00-4
100
%
70-130
1
06/28/21 22:47
17060-07-0
99
%
70-130
1
06/28/21 22:47
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-2 Lab ID: 92546693002 Collected: 06/25/21 08:13 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/21 11:50
07/13/2120:48
7440-36-0
Arsenic
29.0
ug/L
10.0
4.7
1
07/13/21 11:50
07/13/2120:48
7440-38-2
Barium
295
ug/L
5.0
3.5
1
07/13/21 11:50
07/13/2120:48
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/21 11:50
07/13/2120:48
7440-41-7
Cadmium
0.92J
ug/L
1.0
0.40
1
07/13/21 11:50
07/13/2120:48
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/21 11:50
07/13/2120:48
7440-47-3
Cobalt
6.6
ug/L
5.0
3.6
1
07/13/21 11:50
07/13/2120:48
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/21 11:50
07/13/2120:48
7440-50-8
Lead
9.4
ug/L
5.0
4.5
1
07/13/21 11:50
07/13/2120:48
7439-92-1
Nickel
4.4J
ug/L
5.0
3.5
1
07/13/21 11:50
07/13/2120:48
7440-02-0
Selenium
7.OJ
ug/L
10.0
4.7
1
07/13/21 11:50
07/13/2120:48
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/21 11:50
07/13/2120:48
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/21 11:50
07/13/2120:48
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/21 11:50
07/13/2120:48
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2104:53
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/28/21 23:05
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/28/21 23:05
107-13-1
Benzene
1.9
ug/L
1.0
0.34
1
06/28/21 23:05
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/28/21 23:05
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/28/21 23:05
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/28/21 23:05
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/28/21 23:05
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/28/21 23:05
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/28/21 23:05
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/28/21 23:05
56-23-5
Chlorobenzene
13.1
ug/L
1.0
0.28
1
06/28/21 23:05
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/28/21 23:05
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/28/21 23:05
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/28/21 23:05
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/28/21 23:05
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/28/21 23:05
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/28/21 23:05
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/28/21 23:05
74-95-3
1,2-Dichlorobenzene
8.2
ug/L
1.0
0.34
1
06/28/21 23:05
95-50-1
1,4-Dichlorobenzene
14.9
ug/L
1.0
0.33
1
06/28/21 23:05
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/28/21 23:05
110-57-6
1,1-Dichloroethane
0.48J
ug/L
1.0
0.37
1
06/28/21 23:05
75-34-3
1,2-Dichloroethane
0.56J
ug/L
1.0
0.32
1
06/28/21 23:05
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/28/21 23:05
75-35-4
REPORT OF
LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 07/14/2021 04:06 PM
without the written consent of Pace Analytical Services,
LLC.
IK
v1
Page 8 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-2 Lab ID: 92546693002 Collected: 06/25/21 08:13 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
0.44J
ug/L
1.0
0.38
1
06/28/21 23:05
156-59-2
ND
ug/L
1.0
0.40
1
06/28/21 23:05
156-60-5
0.511
ug/L
1.0
0.36
1
06/28/21 23:05
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 23:05
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/21 23:05
10061-02-6
153
ug/L
150
38.7
1
06/28/21 23:05
123-91-1
ND
ug/L
1.0
0.30
1
06/28/21 23:05
100-41-4
ND
ug/L
5.0
0.48
1
06/28/21 23:05
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/28/21 23:05
74-88-4
ND
ug/L
5.0
2.0
1
06/28/21 23:05
75-09-2
ND
ug/L
5.0
2.7
1
06/28/21 23:05
108-10-1
ND
ug/L
1.0
0.29
1
06/28/21 23:05
100-42-5
ND
ug/L
1.0
0.31
1
06/28/21 23:05
630-20-6
ND
ug/L
1.0
0.22
1
06/28/21 23:05
79-34-5
ND
ug/L
1.0
0.29
1
06/28/21 23:05
127-18-4
0.70J
ug/L
1.0
0.48
1
06/28/21 23:05
108-88-3
ND
ug/L
1.0
0.33
1
06/28/21 23:05
71-55-6
ND
ug/L
1.0
0.32
1
06/28/21 23:05
79-00-5
ND
ug/L
1.0
0.38
1
06/28/21 23:05
79-01-6
ND
ug/L
1.0
0.30
1
06/28/21 23:05
75-69-4
ND
ug/L
1.0
0.26
1
06/28/21 23:05
96-18-4
ND
ug/L
2.0
1.3
1
06/28/21 23:05
108-05-4
ND
ug/L
1.0
0.39
1
06/28/21 23:05
75-01-4
ND
ug/L
1.0
0.34
1
06/28/21 23:05
1330-20-7
100
%
70-130
1
06/28/21 23:05
460-00-4
102
%
70-130
1
06/28/21 23:05
17060-07-0
99
%
70-130
1
06/28/21 23:05
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-3 Lab ID: 92546693003 Collected: 06/25/21 08:31 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/2111:50
07/13/2120:51
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2120:51
7440-38-2
Barium
66.8
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2120:51
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/2111:50
07/13/2120:51
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/13/2111:50
07/13/2120:51
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/2111:50
07/13/2120:51
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/13/2111:50
07/13/2120:51
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/2111:50
07/13/2120:51
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/13/2111:50
07/13/2120:51
7439-92-1
Nickel
30.1
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2120:51
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2120:51
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/2111:50
07/13/2120:51
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/2111:50
07/13/2120:51
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/2111:50
07/13/2120:51
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2104:58
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/28/21 23:23
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/28/21 23:23
107-13-1
Benzene
1.6
ug/L
1.0
0.34
1
06/28/21 23:23
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/28/21 23:23
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/28/21 23:23
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/28/21 23:23
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/28/21 23:23
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/28/21 23:23
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/28/21 23:23
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/28/21 23:23
56-23-5
Chlorobenzene
0.54J
ug/L
1.0
0.28
1
06/28/21 23:23
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/28/21 23:23
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/28/21 23:23
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/28/21 23:23
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/28/21 23:23
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/28/21 23:23
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/28/21 23:23
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/28/21 23:23
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/28/21 23:23
95-50-1
1,4-Dichlorobenzene
3.1
ug/L
1.0
0.33
1
06/28/21 23:23
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/28/21 23:23
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/28/21 23:23
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/28/21 23:23
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/28/21 23:23
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
IK
v1
Page 10 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-3 Lab ID: 92546693003 Collected: 06/25/21 08:31 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
6.1
ug/L
1.0
0.38
1
06/28/21 23:23
156-59-2
ND
ug/L
1.0
0.40
1
06/28/21 23:23
156-60-5
ND
ug/L
1.0
0.36
1
06/28/21 23:23
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 23:23
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/21 23:23
10061-02-6
ND
ug/L
150
38.7
1
06/28/21 23:23
123-91-1
ND
ug/L
1.0
0.30
1
06/28/21 23:23
100-41-4
ND
ug/L
5.0
0.48
1
06/28/21 23:23
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/28/21 23:23
74-88-4
ND
ug/L
5.0
2.0
1
06/28/21 23:23
75-09-2
ND
ug/L
5.0
2.7
1
06/28/21 23:23
108-10-1
ND
ug/L
1.0
0.29
1
06/28/21 23:23
100-42-5
ND
ug/L
1.0
0.31
1
06/28/21 23:23
630-20-6
ND
ug/L
1.0
0.22
1
06/28/21 23:23
79-34-5
ND
ug/L
1.0
0.29
1
06/28/21 23:23
127-18-4
ND
ug/L
1.0
0.48
1
06/28/21 23:23
108-88-3
ND
ug/L
1.0
0.33
1
06/28/21 23:23
71-55-6
ND
ug/L
1.0
0.32
1
06/28/21 23:23
79-00-5
0.63J
ug/L
1.0
0.38
1
06/28/21 23:23
79-01-6
ND
ug/L
1.0
0.30
1
06/28/21 23:23
75-69-4
ND
ug/L
1.0
0.26
1
06/28/21 23:23
96-18-4
ND
ug/L
2.0
1.3
1
06/28/21 23:23
108-05-4
ND
ug/L
1.0
0.39
1
06/28/21 23:23
75-01-4
ND
ug/L
1.0
0.34
1
06/28/21 23:23
1330-20-7
100
%
70-130
1
06/28/21 23:23
460-00-4
99
%
70-130
1
06/28/21 23:23
17060-07-0
99
%
70-130
1
06/28/21 23:23
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-3A Lab ID: 92546693004 Collected: 06/25/21 08:18 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/21 11:50
07/13/2120:55
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/13/21 11:50
07/13/2120:55
7440-38-2
Barium
398
ug/L
5.0
3.5
1
07/13/21 11:50
07/13/2120:55
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/21 11:50
07/13/2120:55
7440-41-7
Cadmium
0.83J
ug/L
1.0
0.40
1
07/13/21 11:50
07/13/2120:55
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/21 11:50
07/13/2120:55
7440-47-3
Cobalt
36.6
ug/L
5.0
3.6
1
07/13/21 11:50
07/13/2120:55
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/21 11:50
07/13/2120:55
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/13/21 11:50
07/13/2120:55
7439-92-1
Nickel
30.9
ug/L
5.0
3.5
1
07/13/21 11:50
07/13/2120:55
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/13/21 11:50
07/13/2120:55
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/21 11:50
07/13/2120:55
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/21 11:50
07/13/2120:55
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/21 11:50
07/13/2120:55
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2105:02
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/28/21 23:41
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/28/21 23:41
107-13-1
Benzene
0.76J
ug/L
1.0
0.34
1
06/28/21 23:41
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/28/21 23:41
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/28/21 23:41
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/28/21 23:41
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/28/21 23:41
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/28/21 23:41
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/28/21 23:41
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/28/21 23:41
56-23-5
Chlorobenzene
4.7
ug/L
1.0
0.28
1
06/28/21 23:41
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/28/21 23:41
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/28/21 23:41
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/28/21 23:41
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/28/21 23:41
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/28/21 23:41
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/28/21 23:41
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/28/21 23:41
74-95-3
1,2-Dichlorobenzene
3.4
ug/L
1.0
0.34
1
06/28/21 23:41
95-50-1
1,4-Dichlorobenzene
10.5
ug/L
1.0
0.33
1
06/28/21 23:41
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/28/21 23:41
110-57-6
1,1-Dichloroethane
0.54J
ug/L
1.0
0.37
1
06/28/21 23:41
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/28/21 23:41
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/28/21 23:41
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
IK
v1
Page 12 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-3A Lab ID: 92546693004 Collected: 06/25/21 08:18 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8.6
ug/L
1.0
0.38
1
06/28/2123:41
156-59-2
ND
ug/L
1.0
0.40
1
06/28/2123:41
156-60-5
ND
ug/L
1.0
0.36
1
06/28/2123:41
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 23:41
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/2123:41
10061-02-6
ND
ug/L
150
38.7
1
06/28/2123:41
123-91-1
ND
ug/L
1.0
0.30
1
06/28/2123:41
100-41-4
ND
ug/L
5.0
0.48
1
06/28/2123:41
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/28/2123:41
74-88-4
ND
ug/L
5.0
2.0
1
06/28/2123:41
75-09-2
ND
ug/L
5.0
2.7
1
06/28/2123:41
108-10-1
ND
ug/L
1.0
0.29
1
06/28/2123:41
100-42-5
ND
ug/L
1.0
0.31
1
06/28/2123:41
630-20-6
ND
ug/L
1.0
0.22
1
06/28/2123:41
79-34-5
ND
ug/L
1.0
0.29
1
06/28/2123:41
127-18-4
ND
ug/L
1.0
0.48
1
06/28/2123:41
108-88-3
ND
ug/L
1.0
0.33
1
06/28/2123:41
71-55-6
ND
ug/L
1.0
0.32
1
06/28/2123:41
79-00-5
ND
ug/L
1.0
0.38
1
06/28/2123:41
79-01-6
ND
ug/L
1.0
0.30
1
06/28/2123:41
75-69-4
ND
ug/L
1.0
0.26
1
06/28/2123:41
96-18-4
ND
ug/L
2.0
1.3
1
06/28/2123:41
108-05-4
0.56J
ug/L
1.0
0.39
1
06/28/2123:41
75-01-4
ND
ug/L
1.0
0.34
1
06/28/2123:41
1330-20-7
100
%
70-130
1
06/28/2123:41
460-00-4
99
%
70-130
1
06/28/2123:41
17060-07-0
99
%
70-130
1
06/28/2123:41
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-4 Lab ID: 92546693005 Collected: 06/25/21 09:10 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/2111:50
07/13/2120:58
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2120:58
7440-38-2
Barium
23.3
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2120:58
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/2111:50
07/13/2120:58
7440-41-7
Cadmium
0.501
ug/L
1.0
0.40
1
07/13/21 11:50
07/13/2120:58
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/2111:50
07/13/2120:58
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/13/2111:50
07/13/2120:58
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/2111:50
07/13/2120:58
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/13/2111:50
07/13/2120:58
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2120:58
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2120:58
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/2111:50
07/13/2120:58
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/2111:50
07/13/2120:58
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/2111:50
07/13/2120:58
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2105:07
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/28/21 23:59
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/28/21 23:59
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/28/21 23:59
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/28/21 23:59
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/28/21 23:59
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/28/21 23:59
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/28/21 23:59
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/28/21 23:59
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/28/21 23:59
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/28/21 23:59
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/28/21 23:59
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/28/21 23:59
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/28/21 23:59
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/28/21 23:59
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/28/21 23:59
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/28/21 23:59
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/28/21 23:59
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/28/21 23:59
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/28/21 23:59
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/28/21 23:59
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/28/21 23:59
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/28/21 23:59
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/28/21 23:59
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/28/21 23:59
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
IK
v1
Page 14 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-4 Lab ID: 92546693005 Collected: 06/25/21 09:10 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/28/21 23:59
156-59-2
ND
ug/L
1.0
0.40
1
06/28/21 23:59
156-60-5
ND
ug/L
1.0
0.36
1
06/28/21 23:59
78-87-5
ND
ug/L
1.0
0.36
1
06/28/21 23:59
10061-01-5
ND
ug/L
1.0
0.36
1
06/28/21 23:59
10061-02-6
ND
ug/L
150
38.7
1
06/28/21 23:59
123-91-1
ND
ug/L
1.0
0.30
1
06/28/21 23:59
100-41-4
ND
ug/L
5.0
0.48
1
06/28/21 23:59
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/28/21 23:59
74-88-4
ND
ug/L
5.0
2.0
1
06/28/21 23:59
75-09-2
ND
ug/L
5.0
2.7
1
06/28/21 23:59
108-10-1
ND
ug/L
1.0
0.29
1
06/28/21 23:59
100-42-5
ND
ug/L
1.0
0.31
1
06/28/21 23:59
630-20-6
ND
ug/L
1.0
0.22
1
06/28/21 23:59
79-34-5
ND
ug/L
1.0
0.29
1
06/28/21 23:59
127-18-4
ND
ug/L
1.0
0.48
1
06/28/21 23:59
108-88-3
ND
ug/L
1.0
0.33
1
06/28/21 23:59
71-55-6
ND
ug/L
1.0
0.32
1
06/28/21 23:59
79-00-5
ND
ug/L
1.0
0.38
1
06/28/21 23:59
79-01-6
ND
ug/L
1.0
0.30
1
06/28/21 23:59
75-69-4
ND
ug/L
1.0
0.26
1
06/28/21 23:59
96-18-4
ND
ug/L
2.0
1.3
1
06/28/21 23:59
108-05-4
ND
ug/L
1.0
0.39
1
06/28/21 23:59
75-01-4
ND
ug/L
1.0
0.34
1
06/28/21 23:59
1330-20-7
99
%
70-130
1
06/28/21 23:59
460-00-4
100
%
70-130
1
06/28/21 23:59
17060-07-0
99
%
70-130
1
06/28/21 23:59
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-5 Lab ID: 92546693006 Collected: 06/25/21 09:15 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/2111:50
07/13/2121:15
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:15
7440-38-2
Barium
21.4
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:15
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/2111:50
07/13/2121:15
7440-41-7
Cadmium
1.4
ug/L
1.0
0.40
1
07/13/21 11:50
07/13/2121:15
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/2111:50
07/13/2121:15
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/13/2111:50
07/13/2121:15
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/2111:50
07/13/2121:15
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/13/2111:50
07/13/2121:15
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:15
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:15
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/2111:50
07/13/2121:15
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/2111:50
07/13/2121:15
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/2111:50
07/13/2121:15
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2105:11
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/29/21 16:45
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/29/21 16:45
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/29/21 16:45
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/29/21 16:45
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/29/21 16:45
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/29/21 16:45
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/29/21 16:45
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/29/21 16:45
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/29/21 16:45
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 16:45
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 16:45
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 16:45
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 16:45
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 16:45
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 16:45
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 16:45
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 16:45
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 16:45
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/29/21 16:45
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 16:45
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 16:45
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/29/21 16:45
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 16:45
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 16:45
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-5 Lab ID: 92546693006 Collected: 06/25/21 09:15 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/29/21 16:45
156-59-2
ND
ug/L
1.0
0.40
1
06/29/21 16:45
156-60-5
ND
ug/L
1.0
0.36
1
06/29/21 16:45
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 16:45
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/21 16:45
10061-02-6
ND
ug/L
150
38.7
1
06/29/21 16:45
123-91-1
ND
ug/L
1.0
0.30
1
06/29/21 16:45
100-41-4
ND
ug/L
5.0
0.48
1
06/29/21 16:45
591-78-6
ND
ug/L
20.0
9.7
1
06/29/21 16:45
74-88-4
ND
ug/L
5.0
2.0
1
06/29/21 16:45
75-09-2
ND
ug/L
5.0
2.7
1
06/29/21 16:45
108-10-1
ND
ug/L
1.0
0.29
1
06/29/21 16:45
100-42-5
ND
ug/L
1.0
0.31
1
06/29/21 16:45
630-20-6
ND
ug/L
1.0
0.22
1
06/29/21 16:45
79-34-5
ND
ug/L
1.0
0.29
1
06/29/21 16:45
127-18-4
ND
ug/L
1.0
0.48
1
06/29/21 16:45
108-88-3
ND
ug/L
1.0
0.33
1
06/29/21 16:45
71-55-6
ND
ug/L
1.0
0.32
1
06/29/21 16:45
79-00-5
ND
ug/L
1.0
0.38
1
06/29/21 16:45
79-01-6
ND
ug/L
1.0
0.30
1
06/29/21 16:45
75-69-4
ND
ug/L
1.0
0.26
1
06/29/21 16:45
96-18-4
ND
ug/L
2.0
1.3
1
06/29/21 16:45
108-05-4
ND
ug/L
1.0
0.39
1
06/29/21 16:45
75-01-4
ND
ug/L
1.0
0.34
1
06/29/21 16:45
1330-20-7
100
%
70-130
1
06/29/21 16:45
460-00-4
120
%
70-130
1
06/29/21 16:45
17060-07-0
105
%
70-130
1
06/29/21 16:45
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-7S Lab ID: 92546693007 Collected: 06/25/21 08:05 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/2111:50
07/13/2121:18
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:18
7440-38-2
Barium
116
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:18
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/2111:50
07/13/2121:18
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/13/2111:50
07/13/2121:18
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/2111:50
07/13/2121:18
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/13/2111:50
07/13/2121:18
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/2111:50
07/13/2121:18
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/13/2111:50
07/13/2121:18
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:18
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:18
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/2111:50
07/13/2121:18
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/2111:50
07/13/2121:18
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/2111:50
07/13/2121:18
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2105:16
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/29/21 00:35
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/29/21 00:35
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/29/21 00:35
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/29/21 00:35
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/29/21 00:35
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/29/21 00:35
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/29/21 00:35
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/29/21 00:35
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/29/21 00:35
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 00:35
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 00:35
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 00:35
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 00:35
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 00:35
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 00:35
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 00:35
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 00:35
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 00:35
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/29/21 00:35
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 00:35
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 00:35
110-57-6
1,1-Dichloroethane
0.73J
ug/L
1.0
0.37
1
06/29/21 00:35
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 00:35
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 00:35
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
IK
v1
Page 18 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-7S Lab ID: 92546693007 Collected: 06/25/21 08:05 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
4.2
ug/L
1.0
0.38
1
06/29/21 00:35
156-59-2
ND
ug/L
1.0
0.40
1
06/29/21 00:35
156-60-5
ND
ug/L
1.0
0.36
1
06/29/21 00:35
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 00:35
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/21 00:35
10061-02-6
ND
ug/L
150
38.7
1
06/29/21 00:35
123-91-1
ND
ug/L
1.0
0.30
1
06/29/21 00:35
100-41-4
ND
ug/L
5.0
0.48
1
06/29/21 00:35
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/29/21 00:35
74-88-4
ND
ug/L
5.0
2.0
1
06/29/21 00:35
75-09-2
ND
ug/L
5.0
2.7
1
06/29/21 00:35
108-10-1
ND
ug/L
1.0
0.29
1
06/29/21 00:35
100-42-5
ND
ug/L
1.0
0.31
1
06/29/21 00:35
630-20-6
ND
ug/L
1.0
0.22
1
06/29/21 00:35
79-34-5
ND
ug/L
1.0
0.29
1
06/29/21 00:35
127-18-4
ND
ug/L
1.0
0.48
1
06/29/21 00:35
108-88-3
ND
ug/L
1.0
0.33
1
06/29/21 00:35
71-55-6
ND
ug/L
1.0
0.32
1
06/29/21 00:35
79-00-5
ND
ug/L
1.0
0.38
1
06/29/21 00:35
79-01-6
ND
ug/L
1.0
0.30
1
06/29/21 00:35
75-69-4
ND
ug/L
1.0
0.26
1
06/29/21 00:35
96-18-4
ND
ug/L
2.0
1.3
1
06/29/21 00:35
108-05-4
ND
ug/L
1.0
0.39
1
06/29/21 00:35
75-01-4
ND
ug/L
1.0
0.34
1
06/29/21 00:35
1330-20-7
99
%
70-130
1
06/29/21 00:35
460-00-4
98
%
70-130
1
06/29/21 00:35
17060-07-0
99
%
70-130
1
06/29/21 00:35
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-7D Lab ID: 92546693008 Collected: 06/25/21 08:09 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/2111:50
07/13/2121:22
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:22
7440-38-2
Barium
11.3
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:22
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/2111:50
07/13/2121:22
7440-41-7
Cadmium
0.93J
ug/L
1.0
0.40
1
07/13/21 11:50
07/13/2121:22
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/2111:50
07/13/2121:22
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/13/2111:50
07/13/2121:22
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/2111:50
07/13/2121:22
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/13/2111:50
07/13/2121:22
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:22
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:22
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/2111:50
07/13/2121:22
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/2111:50
07/13/2121:22
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/2111:50
07/13/2121:22
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2105:29
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/29/21 00:53
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/29/21 00:53
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/29/21 00:53
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/29/21 00:53
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/29/21 00:53
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/29/21 00:53
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/29/21 00:53
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/29/21 00:53
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/29/21 00:53
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 00:53
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 00:53
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 00:53
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 00:53
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 00:53
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 00:53
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 00:53
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 00:53
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 00:53
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/29/21 00:53
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 00:53
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 00:53
110-57-6
1,1-Dichloroethane
0.57J
ug/L
1.0
0.37
1
06/29/21 00:53
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 00:53
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 00:53
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
IK
v1
Page 20 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-7D Lab ID: 92546693008 Collected: 06/25/21 08:09 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
1.8
ug/L
1.0
0.38
1
06/29/21 00:53
156-59-2
ND
ug/L
1.0
0.40
1
06/29/21 00:53
156-60-5
ND
ug/L
1.0
0.36
1
06/29/21 00:53
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 00:53
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/21 00:53
10061-02-6
ND
ug/L
150
38.7
1
06/29/21 00:53
123-91-1
ND
ug/L
1.0
0.30
1
06/29/21 00:53
100-41-4
ND
ug/L
5.0
0.48
1
06/29/21 00:53
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/29/21 00:53
74-88-4
ND
ug/L
5.0
2.0
1
06/29/21 00:53
75-09-2
ND
ug/L
5.0
2.7
1
06/29/21 00:53
108-10-1
ND
ug/L
1.0
0.29
1
06/29/21 00:53
100-42-5
ND
ug/L
1.0
0.31
1
06/29/21 00:53
630-20-6
ND
ug/L
1.0
0.22
1
06/29/21 00:53
79-34-5
ND
ug/L
1.0
0.29
1
06/29/21 00:53
127-18-4
ND
ug/L
1.0
0.48
1
06/29/21 00:53
108-88-3
ND
ug/L
1.0
0.33
1
06/29/21 00:53
71-55-6
ND
ug/L
1.0
0.32
1
06/29/21 00:53
79-00-5
ND
ug/L
1.0
0.38
1
06/29/21 00:53
79-01-6
ND
ug/L
1.0
0.30
1
06/29/21 00:53
75-69-4
ND
ug/L
1.0
0.26
1
06/29/21 00:53
96-18-4
ND
ug/L
2.0
1.3
1
06/29/21 00:53
108-05-4
ND
ug/L
1.0
0.39
1
06/29/21 00:53
75-01-4
ND
ug/L
1.0
0.34
1
06/29/21 00:53
1330-20-7
99
%
70-130
1
06/29/21 00:53
460-00-4
100
%
70-130
1
06/29/21 00:53
17060-07-0
99
%
70-130
1
06/29/21 00:53
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-8 Lab ID: 92546693009 Collected: 06/25/21 09:40 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/2111:50
07/13/2121:25
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:25
7440-38-2
Barium
45.0
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:25
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/2111:50
07/13/2121:25
7440-41-7
Cadmium
1.6
ug/L
1.0
0.40
1
07/13/21 11:50
07/13/2121:25
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/2111:50
07/13/2121:25
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/13/2111:50
07/13/2121:25
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/2111:50
07/13/2121:25
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/13/2111:50
07/13/2121:25
7439-92-1
Nickel
8.2
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:25
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:25
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/2111:50
07/13/2121:25
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/2111:50
07/13/2121:25
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/2111:50
07/13/2121:25
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2105:34
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/29/21 01:11
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/29/21 01:11
107-13-1
Benzene
0.35J
ug/L
1.0
0.34
1
06/29/21 01:11
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/29/21 01:11
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/29/21 01:11
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/29/21 01:11
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/29/21 01:11
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/29/21 01:11
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/29/21 01:11
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 01:11
56-23-5
Chlorobenzene
0.29J
ug/L
1.0
0.28
1
06/29/21 01:11
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 01:11
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 01:11
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 01:11
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 01:11
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 01:11
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 01:11
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 01:11
74-95-3
1,2-Dichlorobenzene
0.37J
ug/L
1.0
0.34
1
06/29/21 01:11
95-50-1
1,4-Dichlorobenzene
0.61J
ug/L
1.0
0.33
1
06/29/21 01:11
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 01:11
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/29/21 01:11
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 01:11
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 01:11
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
IK
v1
Page 22 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-8 Lab ID: 92546693009 Collected: 06/25/21 09:40 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
2.3
ug/L
1.0
0.38
1
06/29/2101:11
156-59-2
ND
ug/L
1.0
0.40
1
06/29/2101:11
156-60-5
ND
ug/L
1.0
0.36
1
06/29/2101:11
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 01:11
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/2101:11
10061-02-6
ND
ug/L
150
38.7
1
06/29/2101:11
123-91-1
ND
ug/L
1.0
0.30
1
06/29/2101:11
100-41-4
ND
ug/L
5.0
0.48
1
06/29/2101:11
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/29/2101:11
74-88-4
ND
ug/L
5.0
2.0
1
06/29/2101:11
75-09-2
ND
ug/L
5.0
2.7
1
06/29/2101:11
108-10-1
ND
ug/L
1.0
0.29
1
06/29/2101:11
100-42-5
ND
ug/L
1.0
0.31
1
06/29/2101:11
630-20-6
ND
ug/L
1.0
0.22
1
06/29/2101:11
79-34-5
ND
ug/L
1.0
0.29
1
06/29/2101:11
127-18-4
ND
ug/L
1.0
0.48
1
06/29/2101:11
108-88-3
ND
ug/L
1.0
0.33
1
06/29/2101:11
71-55-6
ND
ug/L
1.0
0.32
1
06/29/2101:11
79-00-5
ND
ug/L
1.0
0.38
1
06/29/2101:11
79-01-6
ND
ug/L
1.0
0.30
1
06/29/2101:11
75-69-4
ND
ug/L
1.0
0.26
1
06/29/2101:11
96-18-4
ND
ug/L
2.0
1.3
1
06/29/2101:11
108-05-4
ND
ug/L
1.0
0.39
1
06/29/2101:11
75-01-4
ND
ug/L
1.0
0.34
1
06/29/2101:11
1330-20-7
100
%
70-130
1
06/29/2101:11
460-00-4
99
%
70-130
1
06/29/2101:11
17060-07-0
99
%
70-130
1
06/29/2101:11
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: SW-1 Lab ID: 92546693010 Collected: 06/25/21 08:24 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/2111:50
07/13/2121:28
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:28
7440-38-2
Barium
19.5
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:28
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/2111:50
07/13/2121:28
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/13/2111:50
07/13/2121:28
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/2111:50
07/13/2121:28
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/13/2111:50
07/13/2121:28
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/2111:50
07/13/2121:28
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/13/2111:50
07/13/2121:28
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:28
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:28
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/2111:50
07/13/2121:28
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/2111:50
07/13/2121:28
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/2111:50
07/13/2121:28
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2105:38
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
06/29/21 01:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
06/29/21 01:30
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
06/29/21 01:30
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
06/29/21 01:30
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
06/29/21 01:30
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
06/29/21 01:30
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
06/29/21 01:30
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
06/29/21 01:30
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
06/29/21 01:30
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
06/29/21 01:30
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
06/29/21 01:30
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
06/29/21 01:30
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
06/29/21 01:30
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
06/29/21 01:30
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
06/29/21 01:30
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
06/29/21 01:30
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
06/29/21 01:30
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
06/29/21 01:30
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
06/29/21 01:30
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
06/29/21 01:30
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
06/29/21 01:30
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
06/29/21 01:30
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
06/29/21 01:30
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
06/29/21 01:30
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
IH
IK
IH,v1
Page 24 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: SW-1 Lab ID: 92546693010 Collected: 06/25/21 08:24 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
06/29/21 01:30
156-59-2
ND
ug/L
1.0
0.40
1
06/29/21 01:30
156-60-5
ND
ug/L
1.0
0.36
1
06/29/21 01:30
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 01:30
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/21 01:30
10061-02-6
ND
ug/L
150
38.7
1
06/29/21 01:30
123-91-1
ND
ug/L
1.0
0.30
1
06/29/21 01:30
100-41-4
ND
ug/L
5.0
0.48
1
06/29/21 01:30
591-78-6 v1
ND
ug/L
20.0
9.7
1
06/29/21 01:30
74-88-4
ND
ug/L
5.0
2.0
1
06/29/21 01:30
75-09-2
ND
ug/L
5.0
2.7
1
06/29/21 01:30
108-10-1
ND
ug/L
1.0
0.29
1
06/29/21 01:30
100-42-5
ND
ug/L
1.0
0.31
1
06/29/21 01:30
630-20-6
ND
ug/L
1.0
0.22
1
06/29/21 01:30
79-34-5
ND
ug/L
1.0
0.29
1
06/29/21 01:30
127-18-4
ND
ug/L
1.0
0.48
1
06/29/21 01:30
108-88-3
ND
ug/L
1.0
0.33
1
06/29/21 01:30
71-55-6
ND
ug/L
1.0
0.32
1
06/29/21 01:30
79-00-5
ND
ug/L
1.0
0.38
1
06/29/21 01:30
79-01-6
ND
ug/L
1.0
0.30
1
06/29/21 01:30
75-69-4
ND
ug/L
1.0
0.26
1
06/29/21 01:30
96-18-4
ND
ug/L
2.0
1.3
1
06/29/21 01:30
108-05-4
ND
ug/L
1.0
0.39
1
06/29/21 01:30
75-01-4
ND
ug/L
1.0
0.34
1
06/29/21 01:30
1330-20-7
99
%
70-130
1
06/29/21 01:30
460-00-4
99
%
70-130
1
06/29/21 01:30
17060-07-0
99
%
70-130
1
06/29/21 01:30
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: SW-2 Lab ID: 92546693011 Collected: 06/25/21 08:45 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/2111:50
07/13/2121:32
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:32
7440-38-2
Barium
19.4
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:32
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/2111:50
07/13/2121:32
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/13/2111:50
07/13/2121:32
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/2111:50
07/13/2121:32
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/13/2111:50
07/13/2121:32
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/2111:50
07/13/2121:32
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/13/2111:50
07/13/2121:32
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/13/2111:50
07/13/2121:32
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/13/2111:50
07/13/2121:32
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/2111:50
07/13/2121:32
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/2111:50
07/13/2121:32
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/2111:50
07/13/2121:32
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2105:43
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
07/01/21 00:31
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
07/01/21 00:31
107-13-1
Benzene
ND
ug/L
1.0
0.34
1
07/01/21 00:31
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
07/01/21 00:31
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
07/01/21 00:31
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
07/01/21 00:31
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
07/01/21 00:31
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
07/01/21 00:31
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
07/01/21 00:31
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
07/01/21 00:31
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.28
1
07/01/21 00:31
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
07/01/21 00:31
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
07/01/21 00:31
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
07/01/21 00:31
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
07/01/21 00:31
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
07/01/21 00:31
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
07/01/21 00:31
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
07/01/21 00:31
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
07/01/21 00:31
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
07/01/21 00:31
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
07/01/21 00:31
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
07/01/21 00:31
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
07/01/21 00:31
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
07/01/21 00:31
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
IK
v1
Page 26 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: SW-2 Lab ID: 92546693011 Collected: 06/25/21 08:45 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
1.0
0.38
1
07/01/2100:31
156-59-2
ND
ug/L
1.0
0.40
1
07/01/2100:31
156-60-5
ND
ug/L
1.0
0.36
1
07/01/2100:31
78-87-5
ND
ug/L
1.0
0.36
1
07/01 /21 00:31
10061-01-5
ND
ug/L
1.0
0.36
1
07/01 /21 00:31
10061-02-6
ND
ug/L
150
38.7
1
07/01/2100:31
123-91-1
ND
ug/L
1.0
0.30
1
07/01 /21 00:31
100-41-4
ND
ug/L
5.0
0.48
1
07/01 /21 00:31
591-78-6
ND
ug/L
20.0
9.7
1
07/01/2100:31
74-88-4
ND
ug/L
5.0
2.0
1
07/01/2100:31
75-09-2
ND
ug/L
5.0
2.7
1
07/01/2100:31
108-10-1
ND
ug/L
1.0
0.29
1
07/01/2100:31
100-42-5
ND
ug/L
1.0
0.31
1
07/01/2100:31
630-20-6
ND
ug/L
1.0
0.22
1
07/01/2100:31
79-34-5
ND
ug/L
1.0
0.29
1
07/01/2100:31
127-18-4
ND
ug/L
1.0
0.48
1
07/01/2100:31
108-88-3
ND
ug/L
1.0
0.33
1
07/01 /21 00:31
71-55-6
ND
ug/L
1.0
0.32
1
07/01/2100:31
79-00-5
ND
ug/L
1.0
0.38
1
07/01 /21 00:31
79-01-6
ND
ug/L
1.0
0.30
1
07/01/2100:31
75-69-4
ND
ug/L
1.0
0.26
1
07/01/2100:31
96-18-4
ND
ug/L
2.0
1.3
1
07/01/2100:31
108-05-4
ND
ug/L
1.0
0.39
1
07/01 /21 00:31
75-01-4
ND
ug/L
1.0
0.34
1
07/01/2100:31
1330-20-7
99
%
70-130
1
07/01 /21 00:31
460-00-4
97
%
70-130
1
07/01 /21 00:31
17060-07-0
99
%
70-130
1
07/01 /21 00:31
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-6 Lab ID: 92546693012 Collected: 06/25/21 09:45 Received: 07/01/21 10:56 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/13/21 11:50
07/13/2121:35
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/13/21 11:50
07/13/2121:35
7440-38-2
Barium
94.4
ug/L
5.0
3.5
1
07/13/21 11:50
07/13/2121:35
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/13/21 11:50
07/13/2121:35
7440-41-7
Cadmium
3.0
ug/L
1.0
0.40
1
07/13/21 11:50
07/13/2121:35
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/13/21 11:50
07/13/2121:35
7440-47-3
Cobalt
27.0
ug/L
5.0
3.6
1
07/13/21 11:50
07/13/2121:35
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/13/21 11:50
07/13/2121:35
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/13/21 11:50
07/13/2121:35
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/13/21 11:50
07/13/2121:35
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/13/21 11:50
07/13/2121:35
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/13/21 11:50
07/13/2121:35
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/13/21 11:50
07/13/2121:35
7440-62-2
Zinc
ND
ug/L
10.0
9.5
1
07/13/21 11:50
07/13/2121:35
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Pace Analytical Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2105:57
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
5.1
1
07/03/21 07:53
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.8
1
07/03/21 07:53
107-13-1
Benzene
0.71J
ug/L
1.0
0.34
1
07/03/21 07:53
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.47
1
07/03/21 07:53
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.31
1
07/03/21 07:53
75-27-4
Bromoform
ND
ug/L
1.0
0.34
1
07/03/21 07:53
75-25-2
Bromomethane
ND
ug/L
2.0
1.7
1
07/03/21 07:53
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
4.0
1
07/03/21 07:53
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.73
1
07/03/21 07:53
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.33
1
07/03/21 07:53
56-23-5
Chlorobenzene
6.6
ug/L
1.0
0.28
1
07/03/21 07:53
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
07/03/21 07:53
75-00-3
Chloroform
ND
ug/L
5.0
1.6
1
07/03/21 07:53
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
07/03/21 07:53
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
0.34
1
07/03/21 07:53
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.36
1
07/03/21 07:53
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
07/03/21 07:53
106-93-4
Dibromomethane
ND
ug/L
1.0
0.39
1
07/03/21 07:53
74-95-3
1,2-Dichlorobenzene
1.9
ug/L
1.0
0.34
1
07/03/21 07:53
95-50-1
1,4-Dichlorobenzene
2.8
ug/L
1.0
0.33
1
07/03/21 07:53
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.56
1
07/03/21 07:53
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.37
1
07/03/21 07:53
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.32
1
07/03/21 07:53
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.35
1
07/03/21 07:53
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
Sample: MW-6 Lab ID: 92546693012 Collected: 06/25/21 09:45 Received: 07/01/21 10:56 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 07/14/2021 04:06 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
2.5
ug/L
1.0
0.38
1
07/03/21 07:53
156-59-2
ND
ug/L
1.0
0.40
1
07/03/21 07:53
156-60-5
ND
ug/L
1.0
0.36
1
07/03/21 07:53
78-87-5
ND
ug/L
1.0
0.36
1
07/03/21 07:53
10061-01-5
ND
ug/L
1.0
0.36
1
07/03/21 07:53
10061-02-6
ND
ug/L
150
38.7
1
07/03/21 07:53
123-91-1
ND
ug/L
1.0
0.30
1
07/03/21 07:53
100-41-4
ND
ug/L
5.0
0.48
1
07/03/21 07:53
591-78-6
ND
ug/L
20.0
9.7
1
07/03/21 07:53
74-88-4
ND
ug/L
5.0
2.0
1
07/03/21 07:53
75-09-2
ND
ug/L
5.0
2.7
1
07/03/21 07:53
108-10-1
ND
ug/L
1.0
0.29
1
07/03/21 07:53
100-42-5
ND
ug/L
1.0
0.31
1
07/03/21 07:53
630-20-6
ND
ug/L
1.0
0.22
1
07/03/21 07:53
79-34-5
ND
ug/L
1.0
0.29
1
07/03/21 07:53
127-18-4
ND
ug/L
1.0
0.48
1
07/03/21 07:53
108-88-3
ND
ug/L
1.0
0.33
1
07/03/21 07:53
71-55-6
ND
ug/L
1.0
0.32
1
07/03/21 07:53
79-00-5
ND
ug/L
1.0
0.38
1
07/03/21 07:53
79-01-6
ND
ug/L
1.0
0.30
1
07/03/21 07:53
75-69-4
ND
ug/L
1.0
0.26
1
07/03/21 07:53
96-18-4
ND
ug/L
2.0
1.3
1
07/03/21 07:53
108-05-4
0.96J
ug/L
1.0
0.39
1
07/03/21 07:53
75-01-4
ND
ug/L
1.0
0.34
1
07/03/21 07:53
1330-20-7
95
%
70-130
1
07/03/21 07:53
460-00-4
93
%
70-130
1
07/03/21 07:53
17060-07-0
101
%
70-130
1
07/03/21 07:53
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 29 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
QC Batch: 632976 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546693001, 92546693002, 92546693003, 92546693004, 92546693005, 92546693006, 92546693007,
92546693008,92546693009,92546693010,92546693011,92546693012
METHOD BLANK: 3324745 Matrix: Water
Associated Lab Samples: 92546693001, 92546693002, 92546693003, 92546693004, 92546693005, 92546693006, 92546693007,
92546693008,92546693009,92546693010,92546693011,92546693012
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Antimony
ug/L
ND
5.0
3.0
07/13/2120:28
Arsenic
ug/L
ND
10.0
4.7
07/13/2120:28
Barium
ug/L
ND
5.0
3.5
07/13/2120:28
Beryllium
ug/L
ND
1.0
0.70
07/13/2120:28
Cadmium
ug/L
ND
1.0
0.40
07/13/2120:28
Chromium
ug/L
ND
5.0
3.7
07/13/2120:28
Cobalt
ug/L
ND
5.0
3.6
07/13/2120:28
Copper
ug/L
ND
5.0
4.3
07/13/2120:28
Lead
ug/L
ND
5.0
4.5
07/13/2120:28
Nickel
ug/L
ND
5.0
3.5
07/13/2120:28
Selenium
ug/L
ND
10.0
4.7
07/13/2120:28
Silver
ug/L
ND
5.0
2.5
07/13/2120:28
Vanadium
ug/L
ND
5.0
3.9
07/13/2120:28
Zinc
ug/L
ND
10.0
9.5
07/13/2120:28
LABORATORY CONTROL SAMPLE:
3324746
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Antimony
ug/L
500
510
102
80-120
Arsenic
ug/L
500
487
97
80-120
Barium
ug/L
500
506
101
80-120
Beryllium
ug/L
500
497
99
80-120
Cadmium
ug/L
500
493
99
80-120
Chromium
ug/L
500
500
100
80-120
Cobalt
ug/L
500
480
96
80-120
Copper
ug/L
500
516
103
80-120
Lead
ug/L
500
495
99
80-120
Nickel
ug/L
500
494
99
80-120
Selenium
ug/L
500
489
98
80-120
Silver
ug/L
250
251
100
80-120
Vanadium
ug/L
500
503
101
80-120
Zinc
ug/L
500
479
96
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Surry Closed LF-Elkin
92546693
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3324747
3324748
MS
MSD
92546693001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
512
514
102
103
75-125
0
20
Arsenic
ug/L
ND
500
500
484
497
96
99
75-125
3
20
Barium
ug/L
27.6
500
500
523
531
99
101
75-125
2
20
Beryllium
ug/L
ND
500
500
503
509
101
102
75-125
1
20
Cadmium
ug/L
1.0
500
500
487
494
97
99
75-125
2
20
Chromium
ug/L
ND
500
500
492
498
98
100
75-125
1
20
Cobalt
ug/L
ND
500
500
471
477
94
95
75-125
1
20
Copper
ug/L
ND
500
500
500
512
100
102
75-125
2
20
Lead
ug/L
ND
500
500
483
490
97
98
75-125
2
20
Nickel
ug/L
ND
500
500
486
493
97
98
75-125
1
20
Selenium
ug/L
ND
500
500
514
516
102
103
75-125
0
20
Silver
ug/L
ND
250
250
248
252
99
101
75-125
2
20
Vanadium
ug/L
ND
500
500
496
503
99
101
75-125
1
20
Zinc
ug/L
ND
500
500
477
483
95
96
75-125
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
QC Batch: 631772 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546693001, 92546693002, 92546693003, 92546693004, 92546693005, 92546693006, 92546693007,
92546693008,92546693009,92546693010,92546693011
METHOD BLANK: 3318797 Matrix: Water
Associated Lab Samples: 92546693001, 92546693002, 92546693003, 92546693004, 92546693005, 92546693006, 92546693007,
92546693008,92546693009,92546693010,92546693011
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 0.47 0.050 07/08/2103:40
LABORATORY CONTROL SAMPLE: 3318798
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 25 25.2 101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3318799 3318800
MS MSD
92546678003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 25 25 25.5 25.2 102 101 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
QC Batch: 631778 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546693012
METHOD BLANK: 3318823
Matrix:
Water
Associated Lab Samples: 92546693012
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Thallium
ug/L
ND
0.47
0.050 07/08/2105:47
LABORATORY CONTROL SAMPLE:
3318824
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
25.0
100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3318825 3318826
MS MSD
92546693012 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 25 25 25.4 24.8 102 99 75-125 2 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
QC Batch: 630139 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92546693001, 92546693002, 92546693003, 92546693004, 92546693005, 92546693007, 92546693008,
92546693009,92546693010
METHOD BLANK: 3311182
Matrix: Water
Associated Lab Samples: 92546693001, 92546693002, 92546693003, 92546693004, 92546693005, 92546693007, 92546693008,
92546693009,92546693010
Parameter
Units
Blank
Result
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
06/28/21 19:27
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
06/28/21 19:27
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
06/28/21 19:27
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
06/28/21 19:27
1,1-Dichloroethane
ug/L
ND
1.0
0.37
06/28/21 19:27
1,1-Dichloroethene
ug/L
ND
1.0
0.35
06/28/21 19:27
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
06/28/21 19:27
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
06/28/21 19:27
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
06/28/21 19:27
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
06/28/21 19:27
1,2-Dichloroethane
ug/L
ND
1.0
0.32
06/28/21 19:27
1,2-Dichloropropane
ug/L
ND
1.0
0.36
06/28/21 19:27
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
06/28/21 19:27
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
38.7
06/28/21 19:27
2-Butanone (MEK)
ug/L
ND
5.0
4.0
06/28/21 19:27
2-Hexanone
ug/L
ND
5.0
0.48
06/28/21 19:27
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
06/28/21 19:27
Acetone
ug/L
ND
25.0
5.1
06/28/21 19:27
Acrylonitrile
ug/L
ND
10.0
1.8
06/28/21 19:27
Benzene
ug/L
ND
1.0
0.34
06/28/21 19:27
Bromochloromethane
ug/L
ND
1.0
0.47
06/28/21 19:27
Bromodichloromethane
ug/L
ND
1.0
0.31
06/28/21 19:27
Bromoform
ug/L
ND
1.0
0.34
06/28/21 19:27
Bromomethane
ug/L
ND
2.0
1.7
06/28/21 19:27
Carbon disulfide
ug/L
ND
2.0
0.73
06/28/21 19:27
Carbon tetrachloride
ug/L
ND
1.0
0.33
06/28/21 19:27
Chlorobenzene
ug/L
ND
1.0
0.28
06/28/21 19:27
Chloroethane
ug/L
ND
1.0
0.65
06/28/21 19:27
Chloroform
ug/L
ND
5.0
1.6
06/28/21 19:27
Chloromethane
ug/L
ND
1.0
0.54
06/28/21 19:27
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
06/28/21 19:27
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/28/21 19:27
Dibromochloromethane
ug/L
ND
1.0
0.36
06/28/21 19:27
Dibromomethane
ug/L
ND
1.0
0.39
06/28/21 19:27
Ethylbenzene
ug/L
ND
1.0
0.30
06/28/21 19:27
lodomethane
ug/L
ND
20.0
9.7
06/28/21 19:27
Methylene Chloride
ug/L
ND
5.0
2.0
06/28/21 19:27
Styrene
ug/L
ND
1.0
0.29
06/28/21 19:27
Tetrachloroethene
ug/L
ND
1.0
0.29
06/28/21 19:27
v1
IN
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
METHOD BLANK: 3311182 Matrix: Water
Associated Lab Samples: 92546693001, 92546693002, 92546693003, 92546693004, 92546693005, 92546693007, 92546693008,
92546693009,92546693010
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
0.48
06/28/21 19:27
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
06/28/21 19:27
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/28/21 19:27
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
06/28/21 19:27 v1
Trichloroethene
ug/L
ND
1.0
0.38
06/28/21 19:27
Trichlorofluoromethane
ug/L
ND
1.0
0.30
06/28/21 19:27
Vinyl acetate
ug/L
ND
2.0
1.3
06/28/21 19:27
Vinyl chloride
ug/L
ND
1.0
0.39
06/28/21 19:27
Xylene (Total)
ug/L
ND
1.0
0.34
06/28/21 19:27
1,2-Dichloroethane-d4 (S)
%
103
70-130
06/28/21 19:27
4-Bromofluorobenzene (S)
%
99
70-130
06/28/21 19:27
Toluene-d8 (S)
%
99
70-130
06/28/21 19:27
LABORATORY CONTROL SAMPLE:
Parameter
3311183
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
52.6
105
70-130
1,1,1-Trichloroethane
ug/L
50
51.0
102
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
57.5
115
70-130
1,1,2-Trichloroethane
ug/L
50
53.8
108
70-130
1,1-Dichloroethane
ug/L
50
52.4
105
70-130
1,1-Dichloroethene
ug/L
50
53.2
106
70-132
1,2,3-Trichloropropane
ug/L
50
56.0
112
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
61.8
124
70-132
1,2-Dibromoethane (EDB)
ug/L
50
54.2
108
70-130
1,2-Dichlorobenzene
ug/L
50
54.8
110
70-130
1,2-Dichloroethane
ug/L
50
49.3
99
70-130
1,2-Dichloropropane
ug/L
50
53.2
106
70-130
1,4-Dichlorobenzene
ug/L
50
56.1
112
70-130
1,4-Dioxane (p-Dioxane)
ug/L
1000
1280
128
70-137
2-Butanone (MEK)
ug/L
100
123
123
70-133
2-Hexanone
ug/L
100
125
125
70-130 v1
4-Methyl-2-pentanone (MIBK)
ug/L
100
124
124
70-130
Acetone
ug/L
100
110
110
70-144
Acrylonitrile
ug/L
250
282
113
70-130
Benzene
ug/L
50
51.8
104
70-130
Bromochloromethane
ug/L
50
45.5
91
70-130
Bromodichloromethane
ug/L
50
52.9
106
70-130
Bromoform
ug/L
50
56.8
114
70-131
Bromomethane
ug/L
50
50.5
101
30-177
Carbon disulfide
ug/L
50
54.4
109
70-133
Carbon tetrachloride
ug/L
50
51.5
103
70-130
Chlorobenzene
ug/L
50
53.2
106
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
LABORATORY CONTROL SAMPLE:
Parameter
3311183
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloroethane
ug/L
50
37.3
Chloroform
ug/L
50
53.2
Chloromethane
ug/L
50
54.0
cis-1,2-Dichloroethene
ug/L
50
52.5
cis-1,3-Dichloropropene
ug/L
50
57.6
Dibromochloromethane
ug/L
50
53.5
Dibromomethane
ug/L
50
53.7
Ethylbenzene
ug/L
50
52.7
lodomethane
ug/L
100
104
Methylene Chloride
ug/L
50
50.4
Styrene
ug/L
50
54.9
Tetrachloroethene
ug/L
50
50.5
Toluene
ug/L
50
52.9
trans-1,2-Dichloroethene
ug/L
50
53.2
trans- 1,3-Dichloropropene
ug/L
50
57.7
trans-1,4-Dichloro-2-butene
ug/L
50
77.9
Trichloroethene
ug/L
50
53.5
Trichlorofluoromethane
ug/L
50
48.3
Vinyl acetate
ug/L
100
126
Vinyl chloride
ug/L
50
52.2
Xylene (Total)
ug/L
150
157
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
75
46-131 IK
106
70-130
108
49-130
105
70-130
115
70-130
107
70-130
107
70-130
105
70-130
104
47-140
101
68-130
110
70-130
101
70-130
106
70-130
106
70-130
115
70-130
156
25-200 v1
107
70-130
97
61-130
126
70-140
104
59-142
105
70-130
93
70-130
99
70-130
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3311184
MS
92546693010 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3311185
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.5
20.5
107
102
70-135
5
30
1,1,1-Trichloroethane
ug/L
ND
20
20
21.3
20.3
107
101
70-148
5
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.1
21.3
110
107
70-131
3
30
1,1,2-Trichloroethane
ug/L
ND
20
20
21.5
20.9
108
104
70-136
3
30
1,1-Dichloroethane
ug/L
ND
20
20
21.6
20.8
108
104
70-147
4
30
1,1-Dichloroethene
ug/L
ND
20
20
22.2
21.6
111
108
70-158
3
30
1,2,3-Trichloropropane
ug/L
ND
20
20
21.7
20.9
108
105
67-137
3
30
1,2-Dibromo-3-
ug/L
ND
20
20
23.0
22.4
115
112
69-136
3
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.4
21.0
107
105
70-137
2
30
1,2-Dichlorobenzene
ug/L
ND
20
20
22.2
21.6
111
108
70-133
3
30
1,2-Dichloroethane
ug/L
ND
20
20
19.9
19.1
99
96
67-138
4
30
1,2-Dichloropropane
ug/L
ND
20
20
21.9
21.2
109
106
70-138
3
30
1,4-Dichlorobenzene
ug/L
ND
20
20
23.2
22.5
116
113
70-133
3
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
400
498
475
124
119
69-146
5
30
2-Butanone (MEK)
ug/L
ND
40
40
42.7
42.5
107
106
61-147
1
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 36 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3311184
3311185
MS
MSD
92546693010
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
2-Hexanone
ug/L
ND
40
40
46.2
44.7
115
112
67-139
3
30
4-Methyl-2-pentanone
ug/L
ND
40
40
44.5
44.2
111
110
67-136
1
30
(MIBK)
Acetone
ug/L
ND
40
40
39.5
38.6
99
96
55-159
2
30
Acrylonitrile
ug/L
ND
100
100
107
103
107
103
68-140
4
30
Benzene
ug/L
ND
20
20
21.5
21.3
108
107
67-150
1
30
Bromochloromethane
ug/L
ND
20
20
19.8
19.7
99
98
70-146
1
30
Bromodichloromethane
ug/L
ND
20
20
21.0
20.8
105
104
70-138
1
30
Bromoform
ug/L
ND
20
20
21.4
21.0
107
105
57-138
2
30
Bromomethane
ug/L
ND
20
20
19.7
21.6
99
108
10-200
9
30 IH
Carbon disulfide
ug/L
ND
20
20
22.6
22.1
113
110
70-152
2
30
Carbon tetrachloride
ug/L
ND
20
20
21.8
21.6
109
108
70-147
1
30
Chlorobenzene
ug/L
ND
20
20
22.5
21.8
112
109
70-137
3
30
Chloroethane
ug/L
ND
20
20
24.1
24.5
120
122
51-166
2
30
Chloroform
ug/L
ND
20
20
21.2
20.9
106
105
70-144
1
30
Chloromethane
ug/L
ND
20
20
18.1
18.0
91
90
24-161
1
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
21.4
20.6
107
103
67-148
4
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
23.0
22.3
115
112
70-142
3
30
Dibromochloromethane
ug/L
ND
20
20
21.3
20.4
107
102
68-138
4
30
Dibromomethane
ug/L
ND
20
20
22.0
21.2
110
106
70-134
4
30
Ethylbenzene
ug/L
ND
20
20
22.6
21.7
113
109
68-143
4
30
lodomethane
ug/L
ND
40
40
50.9
53.5
127
134
20-161
5
30
Methylene Chloride
ug/L
ND
20
20
20.4
19.8
102
99
64-148
3
30
Styrene
ug/L
ND
20
20
22.8
22.0
114
110
70-136
4
30
Tetrachloroethene
ug/L
ND
20
20
22.2
21.6
111
108
70-139
3
30
Toluene
ug/L
ND
20
20
21.9
21.5
109
108
47-157
2
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
22.0
21.4
110
107
70-149
3
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.3
22.1
112
111
70-138
1
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
23.3
23.1
116
115
31-145
1
30 IH,v1
Trichloroethene
ug/L
ND
20
20
22.3
22.1
111
111
70-149
1
30
Trichlorofluoromethane
ug/L
ND
20
20
21.1
20.5
106
103
61-154
3
30
Vinyl acetate
ug/L
ND
40
40
46.5
44.7
116
112
48-156
4
30
Vinyl chloride
ug/L
ND
20
20
21.8
21.3
109
107
55-172
2
30
Xylene (Total)
ug/L
ND
60
60
67.9
64.6
113
108
66-145
5
30
1,2-Dichloroethane-d4 (S)
%
96
96
70-130
4-Bromofluorobenzene (S)
%
99
99
70-130
Toluene-d8 (S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 37 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
QC Batch: 630255 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92546693006
METHOD BLANK: 3311481
Associated Lab Samples: 92546693006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
06/29/21 11:30
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
06/29/21 11:30
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
06/29/21 11:30
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
06/29/21 11:30
1,1-Dichloroethane
ug/L
ND
1.0
0.37
06/29/21 11:30
1,1-Dichloroethene
ug/L
ND
1.0
0.35
06/29/21 11:30
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
06/29/21 11:30
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
06/29/21 11:30
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
06/29/21 11:30
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
06/29/21 11:30
1,2-Dichloroethane
ug/L
ND
1.0
0.32
06/29/21 11:30
1,2-Dichloropropane
ug/L
ND
1.0
0.36
06/29/21 11:30
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
06/29/21 11:30
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
38.7
06/29/21 11:30
2-Butanone (MEK)
ug/L
ND
5.0
4.0
06/29/21 11:30
2-Hexanone
ug/L
ND
5.0
0.48
06/29/21 11:30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
06/29/21 11:30
Acetone
ug/L
ND
25.0
5.1
06/29/21 11:30
Acrylonitrile
ug/L
ND
10.0
1.8
06/29/21 11:30
Benzene
ug/L
ND
1.0
0.34
06/29/21 11:30
Bromochloromethane
ug/L
ND
1.0
0.47
06/29/21 11:30
Bromodichloromethane
ug/L
ND
1.0
0.31
06/29/21 11:30
Bromoform
ug/L
ND
1.0
0.34
06/29/21 11:30
Bromomethane
ug/L
ND
2.0
1.7
06/29/21 11:30
Carbon disulfide
ug/L
ND
2.0
0.73
06/29/21 11:30
Carbon tetrachloride
ug/L
ND
1.0
0.33
06/29/21 11:30
Chlorobenzene
ug/L
ND
1.0
0.28
06/29/21 11:30
Chloroethane
ug/L
ND
1.0
0.65
06/29/21 11:30
Chloroform
ug/L
ND
5.0
1.6
06/29/21 11:30
Chloromethane
ug/L
ND
1.0
0.54
06/29/21 11:30
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
06/29/21 11:30
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/29/21 11:30
Dibromochloromethane
ug/L
ND
1.0
0.36
06/29/21 11:30
Dibromomethane
ug/L
ND
1.0
0.39
06/29/21 11:30
Ethylbenzene
ug/L
ND
1.0
0.30
06/29/21 11:30
lodomethane
ug/L
ND
20.0
9.7
06/29/21 11:30
Methylene Chloride
ug/L
ND
5.0
2.0
06/29/21 11:30
Styrene
ug/L
ND
1.0
0.29
06/29/21 11:30
Tetrachloroethene
ug/L
ND
1.0
0.29
06/29/21 11:30
Toluene
ug/L
ND
1.0
0.48
06/29/21 11:30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 38 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
METHOD BLANK: 3311481
Associated Lab Samples: 92546693006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
06/29/21 11:30
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/29/21 11:30
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
06/29/21 11:30
Trichloroethene
ug/L
ND
1.0
0.38
06/29/21 11:30
Trichlorofluoromethane
ug/L
ND
1.0
0.30
06/29/21 11:30
Vinyl acetate
ug/L
ND
2.0
1.3
06/29/21 11:30
Vinyl chloride
ug/L
ND
1.0
0.39
06/29/21 11:30
Xylene (Total)
ug/L
ND
1.0
0.34
06/29/21 11:30
1,2-Dichloroethane-d4 (S)
%
111
70-130
06/29/21 11:30
4-Bromofluorobenzene (S)
%
97
70-130
06/29/21 11:30
Toluene-d8 (S)
%
107
70-130
06/29/21 11:30
LABORATORY CONTROL SAMPLE:
3311482
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
49.6
99
70-130
1,1,1-Trichloroethane
ug/L
50
47.1
94
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.0
100
70-130
1,1,2-Trichloroethane
ug/L
50
49.4
99
70-130
1,1-Dichloroethane
ug/L
50
48.9
98
70-130
1,1-Dichloroethene
ug/L
50
48.2
96
70-132
1,2,3-Trichloropropane
ug/L
50
48.8
98
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
55.1
110
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.5
103
70-130
1,2-Dichlorobenzene
ug/L
50
52.5
105
70-130
1,2-Dichloroethane
ug/L
50
47.8
96
70-130
1,2-Dichloropropane
ug/L
50
49.1
98
70-130
1,4-Dichlorobenzene
ug/L
50
51.2
102
70-130
1,4-Dioxane (p-Dioxane)
ug/L
1000
1020
102
70-137
2-Butanone (MEK)
ug/L
100
105
105
70-133
2-Hexanone
ug/L
100
100
100
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
99.3
99
70-130
Acetone
ug/L
100
107
107
70-144
Acrylonitrile
ug/L
250
247
99
70-130
Benzene
ug/L
50
47.2
94
70-130
Bromochloromethane
ug/L
50
47.3
95
70-130
Bromodichloromethane
ug/L
50
47.9
96
70-130
Bromoform
ug/L
50
44.0
88
70-131
Bromomethane
ug/L
50
55.2
110
30-177
Carbon disulfide
ug/L
50
50.0
100
70-133
Carbon tetrachloride
ug/L
50
47.2
94
70-130
Chlorobenzene
ug/L
50
46.8
94
70-130
Chloroethane
ug/L
50
62.8
126
46-131
Chloroform
ug/L
50
46.4
93
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
LABORATORY CONTROL SAMPLE:
Parameter
3311482
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
Methylene Chloride
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
46.7
93
49-130
49.2
98
70-130
50.2
100
70-130
52.3
105
70-130
46.8
94
70-130
46.1
92
70-130
104
104
47-140
47.9
96
68-130
48.5
97
70-130
44.8
90
70-130
45.9
92
70-130
49.9
100
70-130
52.0
104
70-130
63.3
127
25-200
46.6
93
70-130
43.6
87
61-130
118
118
70-140
47.1
94
59-142
142
95
70-130
100
70-130
99
70-130
96
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3311483
MS
92546336011 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3311484
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.1
20.9
106
104
70-135
1
30
1,1,1-Trichloroethane
ug/L
ND
20
20
22.6
22.5
113
112
70-148
1
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.5
23.0
112
115
70-131
2
30
1,1,2-Trichloroethane
ug/L
ND
20
20
21.7
20.9
109
105
70-136
4
30
1,1-Dichloroethane
ug/L
ND
20
20
24.5
23.3
123
116
70-147
5
30
1,1-Dichloroethene
ug/L
ND
20
20
23.5
25.3
117
127
70-158
8
30
1,2,3-Trichloropropane
ug/L
ND
20
20
22.9
23.3
115
116
67-137
1
30
1,2-Dibromo-3-
ug/L
ND
20
20
21.7
20.1
109
100
69-136
8
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.4
22.5
107
112
70-137
5
30
1,2-Dichlorobenzene
ug/L
ND
20
20
21.3
22.1
106
110
70-133
4
30
1,2-Dichloroethane
ug/L
ND
20
20
22.8
22.7
114
113
67-138
0
30
1,2-Dichloropropane
ug/L
ND
20
20
22.7
22.8
113
114
70-138
1
30
1,4-Dichlorobenzene
ug/L
ND
20
20
21.5
21.7
108
109
70-133
1
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
400
409
442
102
110
69-146
8
30
2-Butanone (MEK)
ug/L
ND
40
40
50.9
48.9
127
122
61-147
4
30
2-Hexanone
ug/L
ND
40
40
42.0
44.0
105
110
67-139
5
30
4-Methyl-2-pentanone
ug/L
ND
40
40
42.7
45.2
107
113
67-136
6
30
(MIBK)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3311483
3311484
MS
MSD
92546336011
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Acetone
ug/L
ND
40
40
49.7
47.7
124
119
55-159
4
30
Acrylonitrile
ug/L
ND
100
100
122
116
122
116
68-140
5
30
Benzene
ug/L
ND
20
20
22.7
22.7
113
114
67-150
0
30
Bromochloromethane
ug/L
ND
20
20
21.5
20.8
107
104
70-146
3
30
Bromodichloromethane
ug/L
ND
20
20
20.8
20.9
104
105
70-138
0
30
Bromoform
ug/L
ND
20
20
17.2
17.6
86
88
57-138
2
30
Bromomethane
ug/L
ND
20
20
28.7
28.1
144
140
10-200
2
30
Carbon disulfide
ug/L
ND
20
20
24.6
24.3
123
122
70-152
1
30
Carbon tetrachloride
ug/L
ND
20
20
21.9
21.0
110
105
70-147
4
30
Chlorobenzene
ug/L
ND
20
20
20.8
22.2
104
111
70-137
6
30
Chloroethane
ug/L
ND
20
20
26.2
25.1
131
125
51-166
4
30
Chloroform
ug/L
ND
20
20
24.6
24.4
123
122
70-144
1
30
Chloromethane
ug/L
ND
20
20
22.9
23.7
114
118
24-161
4
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
23.9
23.2
119
116
67-148
3
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.9
21.4
105
107
70-142
2
30
Dibromochloromethane
ug/L
ND
20
20
20.5
21.3
102
106
68-138
4
30
Dibromomethane
ug/L
ND
20
20
19.9
20.5
99
102
70-134
3
30
Ethylbenzene
ug/L
ND
20
20
21.1
22.4
106
112
68-143
6
30
lodomethane
ug/L
ND
40
40
37.3
41.3
93
103
20-161
10
30
Methylene Chloride
ug/L
ND
20
20
23.2
22.6
116
113
64-148
2
30
Styrene
ug/L
ND
20
20
21.0
22.0
105
110
70-136
5
30
Tetrachloroethene
ug/L
ND
20
20
20.4
20.3
102
101
70-139
1
30
Toluene
ug/L
ND
20
20
21.8
22.3
109
112
47-157
2
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.6
23.9
123
119
70-149
3
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
21.1
21.8
105
109
70-138
4
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
21.2
22.4
106
112
31-145
5
30
Trichloroethene
ug/L
ND
20
20
20.4
21.8
102
109
70-149
6
30
Trichlorofluoromethane
ug/L
ND
20
20
21.1
22.6
106
113
61-154
7
30
Vinyl acetate
ug/L
ND
40
40
49.8
48.1
125
120
48-156
4
30
Vinyl chloride
ug/L
ND
20
20
24.2
24.0
121
120
55-172
1
30
Xylene (Total)
ug/L
ND
60
60
64.1
67.0
107
112
66-145
4
30
1,2-Dichloroethane-d4 (S)
%
112
106
70-130
4-Bromofluorobenzene (S)
%
97
100
70-130
Toluene-d8 (S)
%
100
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 41 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
QC Batch: 630635 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92546693011
METHOD BLANK: 3313424
Associated Lab Samples: 92546693011
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
06/30/21 18:10
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
06/30/21 18:10
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
06/30/21 18:10
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
06/30/21 18:10
1,1-Dichloroethane
ug/L
ND
1.0
0.37
06/30/21 18:10
1,1-Dichloroethene
ug/L
ND
1.0
0.35
06/30/21 18:10
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
06/30/21 18:10
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
06/30/21 18:10
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
06/30/21 18:10
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
06/30/21 18:10
1,2-Dichloroethane
ug/L
ND
1.0
0.32
06/30/21 18:10
1,2-Dichloropropane
ug/L
ND
1.0
0.36
06/30/21 18:10
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
06/30/21 18:10
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
38.7
06/30/21 18:10
2-Butanone (MEK)
ug/L
ND
5.0
4.0
06/30/21 18:10
2-Hexanone
ug/L
ND
5.0
0.48
06/30/21 18:10
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
06/30/21 18:10
Acetone
ug/L
ND
25.0
5.1
06/30/21 18:10
Acrylonitrile
ug/L
ND
10.0
1.8
06/30/21 18:10
Benzene
ug/L
ND
1.0
0.34
06/30/21 18:10
Bromochloromethane
ug/L
ND
1.0
0.47
06/30/21 18:10
Bromodichloromethane
ug/L
ND
1.0
0.31
06/30/21 18:10
Bromoform
ug/L
ND
1.0
0.34
06/30/21 18:10
Bromomethane
ug/L
ND
2.0
1.7
06/30/21 18:10
Carbon disulfide
ug/L
ND
2.0
0.73
06/30/21 18:10
Carbon tetrachloride
ug/L
ND
1.0
0.33
06/30/21 18:10
Chlorobenzene
ug/L
ND
1.0
0.28
06/30/21 18:10
Chloroethane
ug/L
ND
1.0
0.65
06/30/21 18:10
Chloroform
ug/L
ND
5.0
1.6
06/30/21 18:10
Chloromethane
ug/L
ND
1.0
0.54
06/30/21 18:10
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
06/30/21 18:10
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/30/21 18:10
Dibromochloromethane
ug/L
ND
1.0
0.36
06/30/21 18:10
Dibromomethane
ug/L
ND
1.0
0.39
06/30/21 18:10
Ethylbenzene
ug/L
ND
1.0
0.30
06/30/21 18:10
lodomethane
ug/L
ND
20.0
9.7
06/30/21 18:10
Methylene Chloride
ug/L
ND
5.0
2.0
06/30/21 18:10
Styrene
ug/L
ND
1.0
0.29
06/30/21 18:10
Tetrachloroethene
ug/L
ND
1.0
0.29
06/30/21 18:10
Toluene
ug/L
ND
1.0
0.48
06/30/21 18:10
I:/
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 42 of 55

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
METHOD BLANK: 3313424
Matrix:
Water
Associated Lab Samples: 92546693011
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
06/30/21 18:10
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/30/21 18:10
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
06/30/21 18:10 v1
Trichloroethene
ug/L
ND
1.0
0.38
06/30/21 18:10
Trichlorofluoromethane
ug/L
ND
1.0
0.30
06/30/21 18:10
Vinyl acetate
ug/L
ND
2.0
1.3
06/30/21 18:10
Vinyl chloride
ug/L
ND
1.0
0.39
06/30/21 18:10
Xylene (Total)
ug/L
ND
1.0
0.34
06/30/21 18:10
1,2-Dichloroethane-d4 (S)
%
98
70-130
06/30/21 18:10
4-Bromofluorobenzene (S)
%
99
70-130
06/30/21 18:10
Toluene-d8 (S)
%
99
70-130
06/30/21 18:10
LABORATORY CONTROL SAMPLE: 3313425
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
52.2
104
70-130
1,1,1-Trichloroethane
ug/L
50
48.8
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
55.3
111
70-130
1,1,2-Trichloroethane
ug/L
50
53.0
106
70-130
1,1-Dichloroethane
ug/L
50
49.8
100
70-130
1,1-Dichloroethene
ug/L
50
51.1
102
70-132
1,2,3-Trichloropropane
ug/L
50
53.3
107
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
58.0
116
70-132
1,2-Dibromoethane (EDB)
ug/L
50
52.5
105
70-130
1,2-Dichlorobenzene
ug/L
50
53.7
107
70-130
1,2-Dichloroethane
ug/L
50
45.7
91
70-130
1,2-Dichloropropane
ug/L
50
51.9
104
70-130
1,4-Dichlorobenzene
ug/L
50
55.6
111
70-130
1,4-Dioxane(p-Dioxane)
ug/L
1000
1170
117
70-137
2-Butanone (MEK)
ug/L
100
108
108
70-133
2-Hexanone
ug/L
100
119
119
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
114
114
70-130
Acetone
ug/L
100
108
108
70-144
Acrylonitrile
ug/L
250
258
103
70-130
Benzene
ug/L
50
51.2
102
70-130
Bromochloromethane
ug/L
50
44.9
90
70-130
Bromodichloromethane
ug/L
50
51.3
103
70-130
Bromoform
ug/L
50
54.4
109
70-131
Bromomethane
ug/L
50
44.5
89
30-177
Carbon disulfide
ug/L
50
53.1
106
70-133
Carbon tetrachloride
ug/L
50
51.4
103
70-130
Chlorobenzene
ug/L
50
52.8
106
70-130
Chloroethane
ug/L
50
35.6
71
46-131 IK
Chloroform
ug/L
50
49.2
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
LABORATORY CONTROL SAMPLE:
Parameter
3313425
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
Methylene Chloride
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits Qualifiers
47.8
96
49-130
49.8
100
70-130
56.9
114
70-130
52.3
105
70-130
52.7
105
70-130
52.6
105
70-130
113
113
47-140
47.4
95
68-130
53.0
106
70-130
51.7
103
70-130
51.8
104
70-130
51.1
102
70-130
56.2
112
70-130
73.7
147
25-200 v1
52.8
106
70-130
47.0
94
61-130
115
115
70-140
51.5
103
59-142
157
105
70-130
89
70-130
98
70-130
100
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3313426
MS
92545303035 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3313427
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.7
21.0
108
105
70-135
3
30
1,1,1-Trichloroethane
ug/L
ND
20
20
22.8
22.0
114
110
70-148
4
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.4
20.4
102
102
70-131
0
30
1,1,2-Trichloroethane
ug/L
ND
20
20
22.5
21.6
112
108
70-136
4
30
1,1-Dichloroethane
ug/L
ND
20
20
22.1
22.0
110
110
70-147
1
30
1,1-Dichloroethene
ug/L
ND
20
20
22.8
22.4
114
112
70-158
2
30
1,2,3-Trichloropropane
ug/L
ND
20
20
21.9
20.0
110
100
67-137
9
30
1,2-Dibromo-3-
ug/L
ND
20
20
20.4
20.6
102
103
69-136
1
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.2
20.8
106
104
70-137
2
30
1,2-Dichlorobenzene
ug/L
ND
20
20
20.6
20.6
103
103
70-133
0
30
1,2-Dichloroethane
ug/L
ND
20
20
21.0
20.6
105
103
67-138
2
30
1,2-Dichloropropane
ug/L
ND
20
20
22.0
21.9
110
110
70-138
0
30
1,4-Dichlorobenzene
ug/L
ND
20
20
21.1
20.9
105
105
70-133
1
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
400
498
451
124
113
69-146
10
30
2-Butanone (MEK)
ug/L
ND
40
40
45.6
43.4
114
108
61-147
5
30
2-Hexanone
ug/L
ND
40
40
43.7
40.5
109
101
67-139
8
30
4-Methyl-2-pentanone
ug/L
ND
40
40
43.8
41.3
110
103
67-136
6
30
(MIBK)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 44 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3313426
3313427
MS
MSD
92545303035
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Acetone
ug/L
ND
40
40
43.4
40.8
109
102
55-159
6
30
Acrylonitrile
ug/L
ND
100
100
111
107
111
107
68-140
4
30
Benzene
ug/L
ND
20
20
22.6
21.9
113
110
67-150
3
30
Bromochloromethane
ug/L
ND
20
20
23.0
23.3
115
116
70-146
1
30
Bromodichloromethane
ug/L
ND
20
20
22.0
21.3
110
107
70-138
3
30
Bromoform
ug/L
ND
20
20
21.8
22.4
109
112
57-138
3
30
Bromomethane
ug/L
ND
20
20
30.2
30.6
151
153
10-200
1
30 IH
Carbon disulfide
ug/L
ND
20
20
23.4
23.2
117
116
70-152
1
30
Carbon tetrachloride
ug/L
ND
20
20
23.0
22.0
115
110
70-147
4
30
Chlorobenzene
ug/L
ND
20
20
21.4
21.3
107
107
70-137
0
30
Chloroethane
ug/L
ND
20
20
25.4
24.6
127
123
51-166
3
30
Chloroform
ug/L
ND
20
20
22.6
21.9
113
110
70-144
3
30
Chloromethane
ug/L
ND
20
20
26.0
24.0
130
120
24-161
8
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.1
22.0
111
110
67-148
1
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.6
21.6
113
108
70-142
5
30
Dibromochloromethane
ug/L
ND
20
20
22.3
22.1
112
110
68-138
1
30
Dibromomethane
ug/L
ND
20
20
21.8
20.6
109
103
70-134
6
30
Ethylbenzene
ug/L
ND
20
20
21.8
21.2
109
106
68-143
3
30
lodomethane
ug/L
ND
40
40
37.6
37.3
94
93
20-161
1
30
Methylene Chloride
ug/L
ND
20
20
20.8
20.6
104
103
64-148
1
30
Styrene
ug/L
ND
20
20
21.6
21.1
108
105
70-136
3
30
Tetrachloroethene
ug/L
ND
20
20
22.4
20.8
112
104
70-139
7
30
Toluene
ug/L
ND
20
20
22.2
21.4
111
107
47-157
4
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
23.2
22.6
116
113
70-149
3
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.7
21.8
113
109
70-138
4
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
25.3
24.1
127
121
31-145
5
30 IH,v1
Trichloroethene
ug/L
ND
20
20
21.9
21.4
110
107
70-149
2
30
Trichlorofluoromethane
ug/L
ND
20
20
21.9
21.7
109
108
61-154
1
30
Vinyl acetate
ug/L
ND
40
40
47.7
46.1
119
115
48-156
3
30
Vinyl chloride
ug/L
ND
20
20
23.6
22.9
118
115
55-172
3
30
Xylene (Total)
ug/L
ND
60
60
64.9
64.2
108
107
66-145
1
30
1,2-Dichloroethane-d4 (S)
%
99
97
70-130
4-Bromofluorobenzene (S)
%
100
101
70-130
Toluene-d8 (S)
%
100
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 45 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
QC Batch: 631343 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92546693012
METHOD BLANK: 3317058
Associated Lab Samples: 92546693012
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
07/03/21 02:27
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
07/03/21 02:27
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
07/03/21 02:27
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
07/03/21 02:27
1,1-Dichloroethane
ug/L
ND
1.0
0.37
07/03/21 02:27
1,1-Dichloroethene
ug/L
ND
1.0
0.35
07/03/21 02:27
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
07/03/21 02:27
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
07/03/21 02:27
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
07/03/21 02:27
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
07/03/21 02:27
1,2-Dichloroethane
ug/L
ND
1.0
0.32
07/03/21 02:27
1,2-Dichloropropane
ug/L
ND
1.0
0.36
07/03/21 02:27
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
07/03/21 02:27
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
38.7
07/03/21 02:27
2-Butanone (MEK)
ug/L
ND
5.0
4.0
07/03/21 02:27
2-Hexanone
ug/L
ND
5.0
0.48
07/03/21 02:27
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
07/03/21 02:27
Acetone
ug/L
ND
25.0
5.1
07/03/21 02:27
Acrylonitrile
ug/L
ND
10.0
1.8
07/03/21 02:27
Benzene
ug/L
ND
1.0
0.34
07/03/21 02:27
Bromochloromethane
ug/L
ND
1.0
0.47
07/03/21 02:27
Bromodichloromethane
ug/L
ND
1.0
0.31
07/03/21 02:27
Bromoform
ug/L
ND
1.0
0.34
07/03/21 02:27
Bromomethane
ug/L
ND
2.0
1.7
07/03/21 02:27
Carbon disulfide
ug/L
ND
2.0
0.73
07/03/21 02:27
Carbon tetrachloride
ug/L
ND
1.0
0.33
07/03/21 02:27
Chlorobenzene
ug/L
ND
1.0
0.28
07/03/21 02:27
Chloroethane
ug/L
ND
1.0
0.65
07/03/21 02:27
Chloroform
ug/L
ND
5.0
1.6
07/03/21 02:27
Chloromethane
ug/L
ND
1.0
0.54
07/03/21 02:27
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
07/03/21 02:27
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
07/03/21 02:27
Dibromochloromethane
ug/L
ND
1.0
0.36
07/03/21 02:27
Dibromomethane
ug/L
ND
1.0
0.39
07/03/21 02:27
Ethylbenzene
ug/L
ND
1.0
0.30
07/03/21 02:27
lodomethane
ug/L
ND
20.0
9.7
07/03/21 02:27
Methylene Chloride
ug/L
ND
5.0
2.0
07/03/21 02:27
Styrene
ug/L
ND
1.0
0.29
07/03/21 02:27
Tetrachloroethene
ug/L
ND
1.0
0.29
07/03/21 02:27
Toluene
ug/L
ND
1.0
0.48
07/03/21 02:27
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 46 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
METHOD BLANK: 3317058
Associated Lab Samples: 92546693012
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
07/03/21 02:27
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
07/03/21 02:27
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
07/03/21 02:27
Trichloroethene
ug/L
ND
1.0
0.38
07/03/21 02:27
Trichlorofluoromethane
ug/L
ND
1.0
0.30
07/03/21 02:27
Vinyl acetate
ug/L
ND
2.0
1.3
07/03/21 02:27
Vinyl chloride
ug/L
ND
1.0
0.39
07/03/21 02:27
Xylene (Total)
ug/L
ND
1.0
0.34
07/03/21 02:27
1,2-Dichloroethane-d4 (S)
%
91
70-130
07/03/21 02:27
4-Bromofluorobenzene (S)
%
96
70-130
07/03/21 02:27
Toluene-d8 (S)
%
101
70-130
07/03/21 02:27
LABORATORY CONTROL SAMPLE:
3317059
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
52.5
105
70-130
1,1,1-Trichloroethane
ug/L
50
52.4
105
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
51.2
102
70-130
1,1,2-Trichloroethane
ug/L
50
48.9
98
70-130
1,1-Dichloroethane
ug/L
50
51.2
102
70-130
1,1-Dichloroethene
ug/L
50
51.0
102
70-132
1,2,3-Trichloropropane
ug/L
50
52.3
105
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
56.4
113
70-132
1,2-Dibromoethane (EDB)
ug/L
50
52.9
106
70-130
1,2-Dichlorobenzene
ug/L
50
48.7
97
70-130
1,2-Dichloroethane
ug/L
50
50.8
102
70-130
1,2-Dichloropropane
ug/L
50
49.4
99
70-130
1,4-Dichlorobenzene
ug/L
50
49.3
99
70-130
1,4-Dioxane (p-Dioxane)
ug/L
1000
978
98
70-137
2-Butanone (MEK)
ug/L
100
97.6
98
70-133
2-Hexanone
ug/L
100
101
101
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
98.1
98
70-130
Acetone
ug/L
100
104
104
70-144
Acrylonitrile
ug/L
250
266
106
70-130
Benzene
ug/L
50
48.3
97
70-130
Bromochloromethane
ug/L
50
53.9
108
70-130
Bromodichloromethane
ug/L
50
52.3
105
70-130
Bromoform
ug/L
50
54.8
110
70-131
Bromomethane
ug/L
50
44.1
88
30-177
Carbon disulfide
ug/L
50
50.5
101
70-133
Carbon tetrachloride
ug/L
50
51.1
102
70-130
Chlorobenzene
ug/L
50
49.6
99
70-130
Chloroethane
ug/L
50
48.1
96
46-131
Chloroform
ug/L
50
54.0
108
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
LABORATORY CONTROL SAMPLE:
Parameter
3317059
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Chloromethane
ug/L
50
53.8
108
49-130
cis-1,2-Dichloroethene
ug/L
50
52.7
105
70-130
cis-1,3-Dichloropropene
ug/L
50
51.7
103
70-130
Dibromochloromethane
ug/L
50
54.7
109
70-130
Dibromomethane
ug/L
50
49.4
99
70-130
Ethylbenzene
ug/L
50
50.2
100
70-130
lodomethane
ug/L
100
97.9
98
47-140
Methylene Chloride
ug/L
50
50.6
101
68-130
Styrene
ug/L
50
53.2
106
70-130
Tetrachloroethene
ug/L
50
47.8
96
70-130
Toluene
ug/L
50
48.0
96
70-130
trans-1,2-Dichloroethene
ug/L
50
53.0
106
70-130
trans- 1,3-Dichloropropene
ug/L
50
52.4
105
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
63.2
126
25-200
Trichloroethene
ug/L
50
46.9
94
70-130
Trichlorofluoromethane
ug/L
50
47.6
95
61-130
Vinyl acetate
ug/L
100
112
112
70-140
Vinyl chloride
ug/L
50
53.8
108
59-142
Xylene (Total)
ug/L
150
153
102
70-130
1,2-Dichloroethane-d4 (S)
%
108
70-130
4-Bromofluorobenzene (S)
%
106
70-130
Toluene-d8 (S)
%
100
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3317060
MS
92546693012 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3317061
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.8
24.5
114
123
70-135
7
30
1,1,1-Trichloroethane
ug/L
ND
20
20
24.9
25.3
124
127
70-148
2
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.9
24.4
114
122
70-131
7
30
1,1,2-Trichloroethane
ug/L
ND
20
20
21.8
23.4
109
117
70-136
7
30
1,1-Dichloroethane
ug/L
ND
20
20
24.4
24.8
122
124
70-147
2
30
1,1-Dichloroethene
ug/L
ND
20
20
24.7
25.5
123
128
70-158
3
30
1,2,3-Trichloropropane
ug/L
ND
20
20
23.8
25.4
119
127
67-137
6
30
1,2-Dibromo-3-
ug/L
ND
20
20
23.6
25.9
118
129
69-136
9
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.1
24.2
110
121
70-137
9
30
1,2-Dichlorobenzene
ug/L
1.9
20
20
22.0
23.0
101
106
70-133
4
30
1,2-Dichloroethane
ug/L
ND
20
20
23.3
24.1
116
120
67-138
3
30
1,2-Dichloropropane
ug/L
ND
20
20
22.3
23.9
111
120
70-138
7
30
1,4-Dichlorobenzene
ug/L
2.8
20
20
22.2
23.0
97
101
70-133
4
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
400
431
453
108
113
69-146
5
30
2-Butanone (MEK)
ug/L
ND
40
40
46.5
48.7
116
122
61-147
5
30
2-Hexanone
ug/L
ND
40
40
44.2
46.9
111
117
67-139
6
30
4-Methyl-2-pentanone
ug/L
ND
40
40
44.0
46.8
110
117
67-136
6
30
(MIBK)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 48 of 55

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3317060
3317061
MS
MSD
92546693012
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Acetone
ug/L
ND
40
40
43.9
45.9
110
115
55-159
4
30
Acrylonitrile
ug/L
ND
100
100
114
120
114
120
68-140
4
30
Benzene
ug/L
0.71J
20
20
22.1
23.2
107
112
67-150
5
30
Bromochloromethane
ug/L
ND
20
20
24.6
25.9
123
129
70-146
5
30
Bromodichloromethane
ug/L
ND
20
20
22.9
24.0
115
120
70-138
4
30
Bromoform
ug/L
ND
20
20
22.6
23.8
113
119
57-138
5
30 v1
Bromomethane
ug/L
ND
20
20
20.9
21.5
104
108
10-200
3
30
Carbon disulfide
ug/L
ND
20
20
23.4
23.9
117
120
70-152
2
30
Carbon tetrachloride
ug/L
ND
20
20
24.6
25.4
123
127
70-147
3
30
Chlorobenzene
ug/L
6.6
20
20
22.3
23.3
78
83
70-137
4
30
Chloroethane
ug/L
ND
20
20
26.9
27.7
134
138
51-166
3
30 v1
Chloroform
ug/L
ND
20
20
24.7
25.4
124
127
70-144
3
30
Chloromethane
ug/L
ND
20
20
24.7
25.1
124
125
24-161
2
30
cis-1,2-Dichloroethene
ug/L
2.5
20
20
24.6
25.0
111
113
67-148
1
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.3
23.7
111
118
70-142
6
30
Dibromochloromethane
ug/L
ND
20
20
22.8
24.3
114
121
68-138
6
30
Dibromomethane
ug/L
ND
20
20
21.7
23.0
108
115
70-134
6
30
Ethylbenzene
ug/L
ND
20
20
22.9
23.9
115
120
68-143
4
30
lodomethane
ug/L
ND
40
40
41.5
40.1
104
100
20-161
3
30
Methylene Chloride
ug/L
ND
20
20
23.1
23.6
115
118
64-148
2
30
Styrene
ug/L
ND
20
20
23.0
24.6
115
123
70-136
7
30
Tetrachloroethene
ug/L
ND
20
20
21.4
22.3
107
111
70-139
4
30
Toluene
ug/L
ND
20
20
22.4
23.5
112
117
47-157
5
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
23.9
25.2
119
126
70-149
5
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
23.1
24.4
116
122
70-138
5
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
24.5
25.0
123
125
31-145
2
30 v1
Trichloroethene
ug/L
ND
20
20
22.7
22.8
113
114
70-149
1
30
Trichlorofluoromethane
ug/L
ND
20
20
23.9
24.8
119
124
61-154
4
30
Vinyl acetate
ug/L
ND
40
40
47.2
49.4
118
124
48-156
5
30
Vinyl chloride
ug/L
0.96J
20
20
25.3
25.6
122
123
55-172
1
30
Xylene (Total)
ug/L
ND
60
60
69.4
72.7
116
121
66-145
5
30
1,2-Dichloroethane-d4 (S)
%
113
109
70-130
4-Bromofluorobenzene (S)
%
103
105
70-130
Toluene-d8 (S)
%
100
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC.
Page 49 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Surry Closed LF-Elkin
Pace Project No.: 92546693
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/14/2021 04:06 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Surry Closed LF-Elkin
Pace Project No.:
92546693
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92546693001
MW-1
EPA 3010A
632976
EPA 6010D
633151
92546693002
MW-2
EPA 3010A
632976
EPA 6010D
633151
92546693003
MW-3
EPA 3010A
632976
EPA 6010D
633151
92546693004
MW-3A
EPA 3010A
632976
EPA 6010D
633151
92546693005
MW-4
EPA 3010A
632976
EPA 6010D
633151
92546693006
MW-5
EPA 3010A
632976
EPA 6010D
633151
92546693007
MW-7S
EPA 3010A
632976
EPA 6010D
633151
92546693008
MW-7D
EPA 3010A
632976
EPA 6010D
633151
92546693009
MW-8
EPA 3010A
632976
EPA 6010D
633151
92546693010
SW-1
EPA 3010A
632976
EPA 6010D
633151
92546693011
SW-2
EPA 3010A
632976
EPA 6010D
633151
92546693012
MW-6
EPA 3010A
632976
EPA 6010D
633151
92546693001
MW-1
EPA 3010A
631772
EPA 6020B
631953
92546693002
MW-2
EPA 3010A
631772
EPA 6020B
631953
92546693003
MW-3
EPA 3010A
631772
EPA 6020B
631953
92546693004
MW-3A
EPA 3010A
631772
EPA 6020B
631953
92546693005
MW-4
EPA 3010A
631772
EPA 6020B
631953
92546693006
MW-5
EPA 3010A
631772
EPA 6020B
631953
92546693007
MW-7S
EPA 3010A
631772
EPA 6020B
631953
92546693008
MW-7D
EPA 3010A
631772
EPA 6020B
631953
92546693009
MW-8
EPA 3010A
631772
EPA 6020B
631953
92546693010
SW-1
EPA 3010A
631772
EPA 6020B
631953
92546693011
SW-2
EPA 3010A
631772
EPA 6020B
631953
92546693012
MW-6
EPA 3010A
631778
EPA 6020B
631952
92546693001
MW-1
EPA 8260D
630139
92546693002
MW-2
EPA 8260D
630139
92546693003
MW-3
EPA 8260D
630139
92546693004
MW-3A
EPA 8260D
630139
92546693005
MW-4
EPA 8260D
630139
92546693006
MW-5
EPA 8260D
630255
92546693007
MW-7S
EPA 8260D
630139
92546693008
MW-7D
EPA 8260D
630139
92546693009
MW-8
EPA 8260D
630139
92546693010
SW-1
EPA 8260D
630139
92546693011
SW-2
EPA 8260D
630635
92546693012
MW-6
EPA 8260D
631343
Date: 07/14/2021 04:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 51 of 55

Document Name: Document Revised: October 28, 2020
Sample Condition Upon Recei t(SCUR) Page 1 of 2
dCMnaly cat — Document No.: Issuing Authority:
F•CAR-CS-033-Rev,07 Pace Carolinas Quality office
Laboratory receiving Samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville4 Raleigh[] Mechanicsville❑ Atlanta❑ Kernersville❑
Saniple Condition Client Name:Upon Receipt r Project WOE# : 92546693
r r �: _
- -
Other:
❑ Commercial Pace ❑ 92545693
Custody Seal Present? ❑Yes ®No Seals Intact? []Yes o _
Bate/anitials-Aerson•6xartining.Gontent
Packing Material: ❑Bubble Wrap Zoubble Bags ❑None ❑ other Biological Tissue Frozen?
[]Yes ❑Na MN/A
Thermometer: 19Wet ❑Btue [:]None
,fg IR Gun ro: 92TO64 Type of tce:
��]
Correction Factor:
Cooler Temp: O----- Add/5Ubtract (°Cl Temp should be above freezing to 5°C
❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected ('Cl- r'� has begun
USDA Regulated Soil 0 N/A, water sample)
Did samples originate in a quarantine zone within the United states: CA, NY, or Sc (check maps)? Did samples originate from a foreign source ('snternationaily,
FlYes nNo including Hawaii and Puerto Rico)? ❑yes []No
Chain of Custody Present?
rgYes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
09Yes
❑No
❑N/A
2.
Short Hold Tlme Analysis e72 hr.)?
❑Yes
ONO
[]N/A
3.
Rush Turn Around Time Requested?
[]Yes
tZNo
❑N/A
4.
Sufficient Volume?
J2JYes
[]No
❑N/A
5.
Correct Containers Used?
MyeS
❑No
[-]N/A
6.
-Pace Containers Used?
Yes
No
❑N/A
Containers Intact?
®Yes
No
El N/A
7.
Dissolved analysis: Samples field Filtered?
❑Yes
NNo
❑N/A
S.
sample Labels Match COC?
MYes
❑No
❑NIA
9.
-Includes Date/Time/ID/Analysis Matrix: V 1
Headspace in VOA Vials (>5-6mm)? ❑Yes ZNo ❑N/A 10.
Trip Blank Present? ❑Yes [)NO ®N/A 11.
Trip Blank Custody Seals Present? Yes []No N/A
COMMENTS/SAMPLE DISCREPANCY
,r f t ,I 1 i1 +
Lot ID of split containers:
CL1E T NOTIFICATION/RESGILUTION '
Person contacted: ,
KI r �I"-12 { 1 I' Date/Time:
Data Required? l❑Yes ❑No
Project Manager SCURF Review: Date:
Project Manager SRF Revie : Date- age 52 of 55
- Yvl w Lo

Document Name:
Document Revised: October 28, 2020
Sample Condition Upon Receipt aCU _
Page 2 of 2
CO AnalyflGal
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev,07
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechiorination is Project # WO# ; 92546693
verified and within the acceptance range for preservation
samples.
PM: AMB Due Date: 07/12/21
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg CLIENT: 92—Municipal
**Bo-ttom-half_of_b_ox_is_to_list_numb.er-o.f_bottles—_._. .____. ____... __ ----- _ _
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pH Adjustment Log for Preserved Samples
Sample 1D
Type of Preservative
pH upon receipt
late preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
lot 4
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 53 of 55

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Page 54 of 55

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Page 55 of 55

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
July 12, 2021
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: SURRY BLANKS
Pace Project No.: 92546678
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on June 25, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Accounts Payable, Municipal Engineering Services
Jay Zimmerman, PG, Municipal Engineering Services Co.
REPORT OF LABORATORY ANALYSIS
r
0
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 21

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SURRY BLANKS
Pace Project No.: 92546678
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 21

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: SURRY BLANKS
Pace Project No.: 92546678
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92546678001
EB
Water
06/25/2114:09
06/25/2116:43
92546678002
FB
Water
06/25/2114:12
06/25/2116:43
92546678003
EB-metals
Water
06/25/2114:09
06/25/2116:43
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 3 of 21

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: SURRY BLANKS
Pace Project No.: 92546678
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92546678001 EB
EPA 8260D
SAS
51
PASI-C
92546678002 FB
EPA 8260D
SAS
51
PASI-C
92546678003 EB-metals
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 21

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY BLANKS
Pace Project No.: 92546678
Sample: EB Lab ID: 92546678001 Collected: 06/25/21 14:09 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Date: 07/12/2021 05:20 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
06/29/2116:10
67-64-1
ND
ug/L
10.0
1.8
1
06/29/2116:10
107-13-1
ND
ug/L
1.0
0.34
1
06/29/2116:10
71-43-2
ND
ug/L
1.0
0.47
1
06/29/2116:10
74-97-5
ND
ug/L
1.0
0.31
1
06/29/2116:10
75-27-4
ND
ug/L
1.0
0.34
1
06/29/2116:10
75-25-2
ND
ug/L
2.0
1.7
1
06/29/2116:10
74-83-9
ND
ug/L
5.0
4.0
1
06/29/2116:10
78-93-3
ND
ug/L
2.0
0.73
1
06/29/2116:10
75-15-0
ND
ug/L
1.0
0.33
1
06/29/2116:10
56-23-5
ND
ug/L
1.0
0.28
1
06/29/2116:10
108-90-7
ND
ug/L
1.0
0.65
1
06/29/2116:10
75-00-3
ND
ug/L
5.0
1.6
1
06/29/2116:10
67-66-3
ND
ug/L
1.0
0.54
1
06/29/2116:10
74-87-3
ND
ug/L
2.0
0.34
1
06/29/2116:10
96-12-8
ND
ug/L
1.0
0.36
1
06/29/2116:10
124-48-1
ND
ug/L
1.0
0.27
1
06/29/2116:10
106-93-4
ND
ug/L
1.0
0.39
1
06/29/2116:10
74-95-3
ND
ug/L
1.0
0.34
1
06/29/2116:10
95-50-1
ND
ug/L
1.0
0.33
1
06/29/2116:10
106-46-7
ND
ug/L
1.0
0.56
1
06/29/2116:10
110-57-6
ND
ug/L
1.0
0.37
1
06/29/2116:10
75-34-3
ND
ug/L
1.0
0.32
1
06/29/2116:10
107-06-2
ND
ug/L
1.0
0.35
1
06/29/2116:10
75-35-4
ND
ug/L
1.0
0.38
1
06/29/2116:10
156-59-2
ND
ug/L
1.0
0.40
1
06/29/2116:10
156-60-5
ND
ug/L
1.0
0.36
1
06/29/2116:10
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 16:10
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/2116:10
10061-02-6
ND
ug/L
150
38.7
1
06/29/2116:10
123-91-1
ND
ug/L
1.0
0.30
1
06/29/2116:10
100-41-4
ND
ug/L
5.0
0.48
1
06/29/2116:10
591-78-6
ND
ug/L
20.0
9.7
1
06/29/2116:10
74-88-4
2.1J
ug/L
5.0
2.0
1
06/29/2116:10
75-09-2
ND
ug/L
5.0
2.7
1
06/29/2116:10
108-10-1
ND
ug/L
1.0
0.29
1
06/29/2116:10
100-42-5
ND
ug/L
1.0
0.31
1
06/29/2116:10
630-20-6
ND
ug/L
1.0
0.22
1
06/29/2116:10
79-34-5
ND
ug/L
1.0
0.29
1
06/29/2116:10
127-18-4
ND
ug/L
1.0
0.48
1
06/29/2116:10
108-88-3
ND
ug/L
1.0
0.33
1
06/29/2116:10
71-55-6
ND
ug/L
1.0
0.32
1
06/29/2116:10
79-00-5
ND
ug/L
1.0
0.38
1
06/29/2116:10
79-01-6
ND
ug/L
1.0
0.30
1
06/29/2116:10
75-69-4
ND
ug/L
1.0
0.26
1
06/29/2116:10
96-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
CO
Page 5 of 21

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY BLANKS
Pace Project No.: 92546678
Sample: EB
Parameters
Lab ID:
Results
92546678001
Units
Collected:
Report
Limit
06/25/21 14:09
MDL DF
Received: 06/25/21 16:43 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Vinyl acetate
ND
ug/L
2.0
1.3 1
06/29/21 16:10
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39 1
06/29/21 16:10
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34 1
06/29/21 16:10
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
93
%
70-130
1
06/29/21 16:10
460-00-4
1,2-Dichloroethane-d4 (S)
116
%
70-130
1
06/29/21 16:10
17060-07-0
Toluene-d8 (S)
109
%
70-130
1
06/29/21 16:10
2037-26-5
Date: 07/12/2021 05:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 21

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY BLANKS
Pace Project No.: 92546678
Sample: FB Lab ID: 92546678002 Collected: 06/25/21 14:12 Received: 06/25/21 16:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
1,4-Dioxane (p-Dioxane)
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Date: 07/12/2021 05:20 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
25.0
5.1
1
06/29/2116:28
67-64-1
ND
ug/L
10.0
1.8
1
06/29/2116:28
107-13-1
ND
ug/L
1.0
0.34
1
06/29/2116:28
71-43-2
ND
ug/L
1.0
0.47
1
06/29/2116:28
74-97-5
ND
ug/L
1.0
0.31
1
06/29/2116:28
75-27-4
ND
ug/L
1.0
0.34
1
06/29/2116:28
75-25-2
ND
ug/L
2.0
1.7
1
06/29/2116:28
74-83-9
ND
ug/L
5.0
4.0
1
06/29/2116:28
78-93-3
ND
ug/L
2.0
0.73
1
06/29/2116:28
75-15-0
ND
ug/L
1.0
0.33
1
06/29/2116:28
56-23-5
ND
ug/L
1.0
0.28
1
06/29/2116:28
108-90-7
ND
ug/L
1.0
0.65
1
06/29/2116:28
75-00-3
ND
ug/L
5.0
1.6
1
06/29/2116:28
67-66-3
ND
ug/L
1.0
0.54
1
06/29/2116:28
74-87-3
ND
ug/L
2.0
0.34
1
06/29/2116:28
96-12-8
ND
ug/L
1.0
0.36
1
06/29/2116:28
124-48-1
ND
ug/L
1.0
0.27
1
06/29/2116:28
106-93-4
ND
ug/L
1.0
0.39
1
06/29/2116:28
74-95-3
ND
ug/L
1.0
0.34
1
06/29/2116:28
95-50-1
ND
ug/L
1.0
0.33
1
06/29/2116:28
106-46-7
ND
ug/L
1.0
0.56
1
06/29/2116:28
110-57-6
ND
ug/L
1.0
0.37
1
06/29/2116:28
75-34-3
ND
ug/L
1.0
0.32
1
06/29/2116:28
107-06-2
ND
ug/L
1.0
0.35
1
06/29/2116:28
75-35-4
ND
ug/L
1.0
0.38
1
06/29/2116:28
156-59-2
ND
ug/L
1.0
0.40
1
06/29/2116:28
156-60-5
ND
ug/L
1.0
0.36
1
06/29/2116:28
78-87-5
ND
ug/L
1.0
0.36
1
06/29/21 16:28
10061-01-5
ND
ug/L
1.0
0.36
1
06/29/2116:28
10061-02-6
ND
ug/L
150
38.7
1
06/29/2116:28
123-91-1
ND
ug/L
1.0
0.30
1
06/29/2116:28
100-41-4
ND
ug/L
5.0
0.48
1
06/29/2116:28
591-78-6
ND
ug/L
20.0
9.7
1
06/29/2116:28
74-88-4
2.1J
ug/L
5.0
2.0
1
06/29/2116:28
75-09-2
ND
ug/L
5.0
2.7
1
06/29/2116:28
108-10-1
ND
ug/L
1.0
0.29
1
06/29/2116:28
100-42-5
ND
ug/L
1.0
0.31
1
06/29/2116:28
630-20-6
ND
ug/L
1.0
0.22
1
06/29/2116:28
79-34-5
ND
ug/L
1.0
0.29
1
06/29/2116:28
127-18-4
ND
ug/L
1.0
0.48
1
06/29/2116:28
108-88-3
ND
ug/L
1.0
0.33
1
06/29/2116:28
71-55-6
ND
ug/L
1.0
0.32
1
06/29/2116:28
79-00-5
ND
ug/L
1.0
0.38
1
06/29/2116:28
79-01-6
ND
ug/L
1.0
0.30
1
06/29/2116:28
75-69-4
ND
ug/L
1.0
0.26
1
06/29/2116:28
96-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
CO
Page 7 of 21

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY BLANKS
Pace Project No.: 92546678
Sample: FB
Parameters
Lab ID:
Results
92546678002
Units
Collected:
Report
Limit
06/25/21 14:12
MDL DF
Received: 06/25/21 16:43 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
Pace Analytical
Services
- Charlotte
Vinyl acetate
ND
ug/L
2.0
1.3 1
06/29/21 16:28
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.39 1
06/29/21 16:28
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.34 1
06/29/21 16:28
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
06/29/21 16:28
460-00-4
1,2-Dichloroethane-d4 (S)
118
%
70-130
1
06/29/21 16:28
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
06/29/21 16:28
2037-26-5
Date: 07/12/2021 05:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 21

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY BLANKS
Pace Project No.: 92546678
Sample: EB-metals
Lab ID:
92546678003
Collected:
06/25/21 14:09
Received: 06/25/21 16:43 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical
Method: EPA 6010D
Preparation Method: EPA 3010A
Pace Analytical
Services
-Asheville
Antimony
ND
ug/L
5.0
3.0
1
07/08/2111:00
07/09/2100:01
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:01
7440-38-2
Barium
ND
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:01
7440-39-3
Beryllium
ND
ug/L
1.0
0.70
1
07/08/2111:00
07/09/2100:01
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
07/08/2111:00
07/09/2100:01
7440-43-9
Chromium
ND
ug/L
5.0
3.7
1
07/08/2111:00
07/09/2100:01
7440-47-3
Cobalt
ND
ug/L
5.0
3.6
1
07/08/2111:00
07/09/2100:01
7440-48-4
Copper
ND
ug/L
5.0
4.3
1
07/08/2111:00
07/09/2100:01
7440-50-8
Lead
ND
ug/L
5.0
4.5
1
07/08/2111:00
07/09/2100:01
7439-92-1
Nickel
ND
ug/L
5.0
3.5
1
07/08/2111:00
07/09/2100:01
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
07/08/2111:00
07/09/2100:01
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
07/08/2111:00
07/09/2100:01
7440-22-4
Vanadium
ND
ug/L
5.0
3.9
1
07/08/2111:00
07/09/2100:01
7440-62-2
Zinc
11.2
ug/L
10.0
9.5
1
07/08/2111:00
07/09/2100:01
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020E
Preparation Method: EPA 3010A
Pace Analytical
Services
-Asheville
Thallium
ND
ug/L
0.47
0.050
1
07/07/2113:27
07/08/2103:50
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
QC Batch: 631987 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546678003
METHOD BLANK: 3320015
Associated Lab Samples: 92546678003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
5.0
3.0
07/08/2123:19
Arsenic
ug/L
ND
10.0
4.7
07/08/2123:19
Barium
ug/L
ND
5.0
3.5
07/08/2123:19
Beryllium
ug/L
ND
1.0
0.70
07/08/2123:19
Cadmium
ug/L
ND
1.0
0.40
07/08/2123:19
Chromium
ug/L
ND
5.0
3.7
07/08/2123:19
Cobalt
ug/L
ND
5.0
3.6
07/08/2123:19
Copper
ug/L
ND
5.0
4.3
07/08/2123:19
Lead
ug/L
ND
5.0
4.5
07/08/2123:19
Nickel
ug/L
ND
5.0
3.5
07/08/2123:19
Selenium
ug/L
ND
10.0
4.7
07/08/2123:19
Silver
ug/L
ND
5.0
2.5
07/08/2123:19
Vanadium
ug/L
ND
5.0
3.9
07/08/2123:19
Zinc
ug/L
ND
10.0
9.5
07/08/2123:19
LABORATORY CONTROL SAMPLE:
Parameter
3320016
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
493
99
80-120
Arsenic
ug/L
500
476
95
80-120
Barium
ug/L
500
487
97
80-120
Beryllium
ug/L
500
492
98
80-120
Cadmium
ug/L
500
490
98
80-120
Chromium
ug/L
500
484
97
80-120
Cobalt
ug/L
500
478
96
80-120
Copper
ug/L
500
497
99
80-120
Lead
ug/L
500
480
96
80-120
Nickel
ug/L
500
487
97
80-120
Selenium
ug/L
500
484
97
80-120
Silver
ug/L
250
246
99
80-120
Vanadium
ug/L
500
485
97
80-120
Zinc
ug/L
500
489
98
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
SURRY BLANKS
92546678
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE: 3320017
3320018
MS
MSD
92546523001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
4.9J
500
500
510
514
101
102
75-125
1
20
Arsenic
ug/L
<4.7
500
500
504
506
101
101
75-125
0
20
Barium
ug/L
474
500
500
970
965
99
98
75-125
1
20
Beryllium
ug/L
<0.70
500
500
506
503
101
101
75-125
0
20
Cadmium
ug/L
<0.40
500
500
507
509
101
102
75-125
0
20
Chromium
ug/L
<3.7
500
500
486
495
97
99
75-125
2
20
Cobalt
ug/L
4.8J
500
500
480
482
95
95
75-125
0
20
Copper
ug/L
500
500
512
517
102
103
75-125
1
20
Lead
ug/L
<4.5
500
500
481
481
96
96
75-125
0
20
Nickel
ug/L
5.3
500
500
485
486
96
96
75-125
0
20
Selenium
ug/L
<4.7
500
500
512
517
102
103
75-125
1
20
Silver
ug/L
<2.5
250
250
254
255
101
102
75-125
1
20
Vanadium
ug/L
<3.9
500
500
501
507
100
101
75-125
1
20
Zinc
ug/L
<9.5
500
500
497
498
99
100
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
QC Batch: 631772 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546678003
METHOD BLANK: 3318797
Matrix:
Water
Associated Lab Samples: 92546678003
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Thallium
ug/L
ND
0.47
0.050 07/08/2103:40
LABORATORY CONTROL SAMPLE:
3318798
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
25.2
101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3318799 3318800
MS MSD
92546678003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 25 25 25.5 25.2 102 101 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
QC Batch: 630255 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92546678001, 92546678002
METHOD BLANK: 3311481
Associated Lab Samples: 92546678001, 92546678002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.31
06/29/21 11:30
1,1,1-Trichloroethane
ug/L
ND
1.0
0.33
06/29/21 11:30
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
06/29/21 11:30
1,1,2-Trichloroethane
ug/L
ND
1.0
0.32
06/29/21 11:30
1,1-Dichloroethane
ug/L
ND
1.0
0.37
06/29/21 11:30
1,1-Dichloroethene
ug/L
ND
1.0
0.35
06/29/21 11:30
1,2,3-Trichloropropane
ug/L
ND
1.0
0.26
06/29/21 11:30
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
0.34
06/29/21 11:30
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
06/29/21 11:30
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
06/29/21 11:30
1,2-Dichloroethane
ug/L
ND
1.0
0.32
06/29/21 11:30
1,2-Dichloropropane
ug/L
ND
1.0
0.36
06/29/21 11:30
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
06/29/21 11:30
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
38.7
06/29/21 11:30
2-Butanone (MEK)
ug/L
ND
5.0
4.0
06/29/21 11:30
2-Hexanone
ug/L
ND
5.0
0.48
06/29/21 11:30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
2.7
06/29/21 11:30
Acetone
ug/L
ND
25.0
5.1
06/29/21 11:30
Acrylonitrile
ug/L
ND
10.0
1.8
06/29/21 11:30
Benzene
ug/L
ND
1.0
0.34
06/29/21 11:30
Bromochloromethane
ug/L
ND
1.0
0.47
06/29/21 11:30
Bromodichloromethane
ug/L
ND
1.0
0.31
06/29/21 11:30
Bromoform
ug/L
ND
1.0
0.34
06/29/21 11:30
Bromomethane
ug/L
ND
2.0
1.7
06/29/21 11:30
Carbon disulfide
ug/L
ND
2.0
0.73
06/29/21 11:30
Carbon tetrachloride
ug/L
ND
1.0
0.33
06/29/21 11:30
Chlorobenzene
ug/L
ND
1.0
0.28
06/29/21 11:30
Chloroethane
ug/L
ND
1.0
0.65
06/29/21 11:30
Chloroform
ug/L
ND
5.0
1.6
06/29/21 11:30
Chloromethane
ug/L
ND
1.0
0.54
06/29/21 11:30
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.38
06/29/21 11:30
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/29/21 11:30
Dibromochloromethane
ug/L
ND
1.0
0.36
06/29/21 11:30
Dibromomethane
ug/L
ND
1.0
0.39
06/29/21 11:30
Ethylbenzene
ug/L
ND
1.0
0.30
06/29/21 11:30
lodomethane
ug/L
ND
20.0
9.7
06/29/21 11:30
Methylene Chloride
ug/L
ND
5.0
2.0
06/29/21 11:30
Styrene
ug/L
ND
1.0
0.29
06/29/21 11:30
Tetrachloroethene
ug/L
ND
1.0
0.29
06/29/21 11:30
Toluene
ug/L
ND
1.0
0.48
06/29/21 11:30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
METHOD BLANK: 3311481
Associated Lab Samples: 92546678001, 92546678002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.40
06/29/21 11:30
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.36
06/29/21 11:30
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.56
06/29/21 11:30
Trichloroethene
ug/L
ND
1.0
0.38
06/29/21 11:30
Trichlorofluoromethane
ug/L
ND
1.0
0.30
06/29/21 11:30
Vinyl acetate
ug/L
ND
2.0
1.3
06/29/21 11:30
Vinyl chloride
ug/L
ND
1.0
0.39
06/29/21 11:30
Xylene (Total)
ug/L
ND
1.0
0.34
06/29/21 11:30
1,2-Dichloroethane-d4 (S)
%
111
70-130
06/29/21 11:30
4-Bromofluorobenzene (S)
%
97
70-130
06/29/21 11:30
Toluene-d8 (S)
%
107
70-130
06/29/21 11:30
LABORATORY CONTROL SAMPLE:
3311482
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
49.6
99
70-130
1,1,1-Trichloroethane
ug/L
50
47.1
94
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.0
100
70-130
1,1,2-Trichloroethane
ug/L
50
49.4
99
70-130
1,1-Dichloroethane
ug/L
50
48.9
98
70-130
1,1-Dichloroethene
ug/L
50
48.2
96
70-132
1,2,3-Trichloropropane
ug/L
50
48.8
98
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
55.1
110
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.5
103
70-130
1,2-Dichlorobenzene
ug/L
50
52.5
105
70-130
1,2-Dichloroethane
ug/L
50
47.8
96
70-130
1,2-Dichloropropane
ug/L
50
49.1
98
70-130
1,4-Dichlorobenzene
ug/L
50
51.2
102
70-130
1,4-Dioxane (p-Dioxane)
ug/L
1000
1020
102
70-137
2-Butanone (MEK)
ug/L
100
105
105
70-133
2-Hexanone
ug/L
100
100
100
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
99.3
99
70-130
Acetone
ug/L
100
107
107
70-144
Acrylonitrile
ug/L
250
247
99
70-130
Benzene
ug/L
50
47.2
94
70-130
Bromochloromethane
ug/L
50
47.3
95
70-130
Bromodichloromethane
ug/L
50
47.9
96
70-130
Bromoform
ug/L
50
44.0
88
70-131
Bromomethane
ug/L
50
55.2
110
30-177
Carbon disulfide
ug/L
50
50.0
100
70-133
Carbon tetrachloride
ug/L
50
47.2
94
70-130
Chlorobenzene
ug/L
50
46.8
94
70-130
Chloroethane
ug/L
50
62.8
126
46-131
Chloroform
ug/L
50
46.4
93
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
LABORATORY CONTROL SAMPLE:
Parameter
3311482
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
Methylene Chloride
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
46.7
93
49-130
49.2
98
70-130
50.2
100
70-130
52.3
105
70-130
46.8
94
70-130
46.1
92
70-130
104
104
47-140
47.9
96
68-130
48.5
97
70-130
44.8
90
70-130
45.9
92
70-130
49.9
100
70-130
52.0
104
70-130
63.3
127
25-200
46.6
93
70-130
43.6
87
61-130
118
118
70-140
47.1
94
59-142
142
95
70-130
100
70-130
99
70-130
96
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3311483
MS
92546336011 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3311484
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.1
20.9
106
104
70-135
1
30
1,1,1-Trichloroethane
ug/L
ND
20
20
22.6
22.5
113
112
70-148
1
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.5
23.0
112
115
70-131
2
30
1,1,2-Trichloroethane
ug/L
ND
20
20
21.7
20.9
109
105
70-136
4
30
1,1-Dichloroethane
ug/L
ND
20
20
24.5
23.3
123
116
70-147
5
30
1,1-Dichloroethene
ug/L
ND
20
20
23.5
25.3
117
127
70-158
8
30
1,2,3-Trichloropropane
ug/L
ND
20
20
22.9
23.3
115
116
67-137
1
30
1,2-Dibromo-3-
ug/L
ND
20
20
21.7
20.1
109
100
69-136
8
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.4
22.5
107
112
70-137
5
30
1,2-Dichlorobenzene
ug/L
ND
20
20
21.3
22.1
106
110
70-133
4
30
1,2-Dichloroethane
ug/L
ND
20
20
22.8
22.7
114
113
67-138
0
30
1,2-Dichloropropane
ug/L
ND
20
20
22.7
22.8
113
114
70-138
1
30
1,4-Dichlorobenzene
ug/L
ND
20
20
21.5
21.7
108
109
70-133
1
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
400
409
442
102
110
69-146
8
30
2-Butanone (MEK)
ug/L
ND
40
40
50.9
48.9
127
122
61-147
4
30
2-Hexanone
ug/L
ND
40
40
42.0
44.0
105
110
67-139
5
30
4-Methyl-2-pentanone
ug/L
ND
40
40
42.7
45.2
107
113
67-136
6
30
(MIBK)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 21

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY BLANKS
Pace Project No.: 92546678
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3311483
3311484
MS
MSD
92546336011
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Acetone
ug/L
ND
40
40
49.7
47.7
124
119
55-159
4
30
Acrylonitrile
ug/L
ND
100
100
122
116
122
116
68-140
5
30
Benzene
ug/L
ND
20
20
22.7
22.7
113
114
67-150
0
30
Bromochloromethane
ug/L
ND
20
20
21.5
20.8
107
104
70-146
3
30
Bromodichloromethane
ug/L
ND
20
20
20.8
20.9
104
105
70-138
0
30
Bromoform
ug/L
ND
20
20
17.2
17.6
86
88
57-138
2
30
Bromomethane
ug/L
ND
20
20
28.7
28.1
144
140
10-200
2
30
Carbon disulfide
ug/L
ND
20
20
24.6
24.3
123
122
70-152
1
30
Carbon tetrachloride
ug/L
ND
20
20
21.9
21.0
110
105
70-147
4
30
Chlorobenzene
ug/L
ND
20
20
20.8
22.2
104
111
70-137
6
30
Chloroethane
ug/L
ND
20
20
26.2
25.1
131
125
51-166
4
30
Chloroform
ug/L
ND
20
20
24.6
24.4
123
122
70-144
1
30
Chloromethane
ug/L
ND
20
20
22.9
23.7
114
118
24-161
4
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
23.9
23.2
119
116
67-148
3
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.9
21.4
105
107
70-142
2
30
Dibromochloromethane
ug/L
ND
20
20
20.5
21.3
102
106
68-138
4
30
Dibromomethane
ug/L
ND
20
20
19.9
20.5
99
102
70-134
3
30
Ethylbenzene
ug/L
ND
20
20
21.1
22.4
106
112
68-143
6
30
lodomethane
ug/L
ND
40
40
37.3
41.3
93
103
20-161
10
30
Methylene Chloride
ug/L
ND
20
20
23.2
22.6
116
113
64-148
2
30
Styrene
ug/L
ND
20
20
21.0
22.0
105
110
70-136
5
30
Tetrachloroethene
ug/L
ND
20
20
20.4
20.3
102
101
70-139
1
30
Toluene
ug/L
ND
20
20
21.8
22.3
109
112
47-157
2
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.6
23.9
123
119
70-149
3
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
21.1
21.8
105
109
70-138
4
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
21.2
22.4
106
112
31-145
5
30
Trichloroethene
ug/L
ND
20
20
20.4
21.8
102
109
70-149
6
30
Trichlorofluoromethane
ug/L
ND
20
20
21.1
22.6
106
113
61-154
7
30
Vinyl acetate
ug/L
ND
40
40
49.8
48.1
125
120
48-156
4
30
Vinyl chloride
ug/L
ND
20
20
24.2
24.0
121
120
55-172
1
30
Xylene (Total)
ug/L
ND
60
60
64.1
67.0
107
112
66-145
4
30
1,2-Dichloroethane-d4 (S)
%
112
106
70-130
4-Bromofluorobenzene (S)
%
97
100
70-130
Toluene-d8 (S)
%
100
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 21

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: SURRY BLANKS
Pace Project No.: 92546678
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
CO Result confirmed by second analysis.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 21

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
SURRY BLANKS
92546678
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92546678003
EB-metals
EPA 3010A
631987 EPA 6010D
632207
92546678003
EB-metals
EPA 3010A
631772 EPA 6020B
631953
92546678001
EB
EPA 8260D
630255
92546678002
FB
EPA 8260D
630255
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/12/2021 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 21

Document Name: Document Revised: October 28, 2020
Sample Condition Upon Receipt(SCUR) Page 1 of 2
aci3MafyticatLDocument No.: Issuing Authority
F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ HuntersvilleIr"P11. Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑
Name:
Project #
WO#:92546676
92546678
Custody Seal Present? Dyes 'J;4N0 Seals Intact? ❑Yes [gNo
DateiGnilia Werson-Examining-Gontent
Packing Material: ❑Bubble Wrap [RBubbie Bags [-]None ❑ other Biological Tissue Frozen?
Thermometer:
[-]Yes []No 19N/A
Wet ❑9iue ❑None
IR Gun ID: 921064 Type of ice:
q Correction Factor
Cooler Temp: Add/Subtract (°Ci _0 1 Temp should be above freezing to 6'C
q ❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected ('C): U.8 has begun
USDA Regulated Sail ( ® N/A, water sample}
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {internationally,
l—IYes nNn Includrne Hawaii and Puerto Wcoi? FlYes 11No
Comments/Discrepancy:
Chain of Custody Present?
blYes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
3yes
❑No
❑N/A
2.
Short Hold Tlme Analysis <72 hr.i?
❑Yes
IgNo
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
gNo
❑N/A
4.
Sufficient Volume?
'Yes
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
®Yes
®Yes
[:)No
❑No
[-]N/A
❑N/A
6.
Containers Intact?
®Yes
[]No
[]N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
gNo
[-]NIA
B.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
19Yes
[:]No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
[-]Yes
®No
[I N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
[]Yes
❑No
[]No
5gN/A
N/A
11,
j V �
on IQ ,P�D, _ _ Lot ID of split containers: _
CLIENT NOTIFICATION/RESOLUTION
need -to kia ye- Vla:, a 1p a !M aed _ -ror yne-W c- .
OI +- rnn Go(- �Jo _ �n e� Qs need e d_fo r F:6 - - - - - - --
Person contacted: Fyo_y) La*yj b,e�--t _ Date/Time: U -aq
Project Manager SCURF Review: — f t`" 6
Date: te -';'Cl —a 1
Project Manager SRF Review:
Page 19 of 21

Document Name: Document Revised: October 28, 2020
Samule Condition Uoon ReceiotlISCURi I paEP 7 of 7
(ALjU"""y"°"" Document No.:
F-CAR-CS-033•Rev.07
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
** tom_halUoUbox_istoiist_number_of_botties _
Issuing Authority:
Pace Carolinas quality Office
Project ol# ; 92546678
p14: pM8 Due Date: 07/12A21
CLIENT: 92—Municipal j
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot p
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina OEHNR Certification Office (Le,
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 20 of 21

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Page 21 of 21