24056 Brayton International BAR (Rev 1) 2021.10.13

BROWNFIELDS ASSESSMENT REPORT & RECEPTOR SURVEY, REV 1.0

BRAYTON INTERNATIONAL FURNISHINGS
257, 263, & 265 SWATHMORE AVENUE
HIGH POINT, GUILFORD COUNTY, NORTH CAROLINA
BROWNFIELDS PROJECT ID. 24056-20-041

ECS PROJECT NO. 49:11046-A
PREPARED FOR
TUGGLE DUGGINS, P.A.
400 BELLEMEADE, SUITE 800
GREENSBORO, NORTH CAROLINA 27401

October 13, 2021
Brownfields Assessment Report & Receptor Survey, Rev. 1.0
Brayton International Furnishings
High Point, Guilford County, North Carolina
Brownfields Project Number 24056-20-041
ECS Project No. 49:8056-C
October 13, 2021

1

TABLE OF CONTENTS
1.0 PROJECT INFORMATION........................................................................................................................ 2
2.0 PREVIOUS INVESTIGATIONS .................................................................................................................. 2
3.0 OBJECTIVE OF THE ASSESSMENT .......................................................................................................... 3
4.0 FIELD ACTIVITIES.................................................................................................................................... 3
4.1 Monitoring Well Permit ....................................................................................................................... 3
4.2 Utility Locate ........................................................................................................................................ 3
4.3 Soil Samples ......................................................................................................................................... 4
4.3 Groundwater Samples ......................................................................................................................... 4
5.0 RESULTS ................................................................................................................................................. 5
5.1 Soil Boring Soil Analysis ....................................................................................................................... 5
5.2 Groundwater Analysis .......................................................................................................................... 6
5.3 Brownfields Receptor Survey............................................................................................................... 7
6.0 CONCLUSIONS ....................................................................................................................................... 7

FIGURES

Figure 1 USGS Topographic Map
Figure 2 Site Aerial Map
Figure 3 Sample Locations Map
Figure 4 Groundwater Contour Map

TABLES

Table 1 Summary of Sample Point Coordinates
Table 2 Monitoring Well Construction Details and Groundwater Elevation Data
Table 3 Summary of Soil Sample Analytical Results
Table 4 Summary of Groundwater Sample Analytical Results

APPENDICES

Appendix A NCDEQ Monitoring Well Permit
Appendix B Boring Logs
Appendix C Groundwater Field Sampling Sheets
Appendix D Laboratory Analytical Reports and Chain-of-Custody Forms
Appendix E NCDEQ Risk Calculator Output
Appendix F Brownfields Receptor Survey Form and Figure
Brownfields Assessment Report & Receptor Survey, Rev. 1.0
Brayton International Furnishings
High Point, Guilford County, North Carolina
Brownfields Project Number 24056-20-041
ECS Project No. 49:8056-C
October 13, 2021

2

1.0 PROJECT INFORMATION

The subject site is located in Guilford and Randolph Counties identified by the Guilford County GIS as
Parcel Identification Numbers (PINs) 7709702670 and 7709609681 and the Randolph County GIS as PIN
7709700498. The site is further listed as being owned by High Point University in both counties. The
approximately 3.84-acre subject property is occupied by one approximate 76,000-square foot industrial
building which was constructed in 1985. The site also includes paved areas and grass covered/landscaped
areas. Municipal water and sewer are provided to the subject property by the City of High Point. The
building contains office space and warehouse space. The building is heated with natural gas and electric
heat pumps. Figure 1 is a site topographic map. Figure 2 is a site aerial photograph.

Due to the previous identification of groundwater impacts on the property, the site is currently in the
North Carolina Department of Environmental Quality (NCDEQ), Inactive Hazardous Site Branch (IHSB) and
given the Identification Number NCD981862121. In addition, the site is listed with the NCDEQ,
Brownfields Program as the Quality Packaging Expansion site (Brownfields Project No. 24056-20-041) and
the current status is “active eligible”.

2.0 PREVIOUS INVESTIGATIONS

Trigon Environmental Management, Inc. previously completed the following reports for the subject site:

• Lacquer Spill Cleanup; dated April 24, 1998
• Additional Lacquer Spill Cleanup; dated May 22, 1998

ECS previously completed the following reports for the subject site:

• Phase I Environmental Site Assessment; ECS Project No.: 09:15566; dated February 27, 2008
• Report of Environmental Services; ECS Project No.: 09:15566A; dated March 25, 2008
• Phase I Environmental Site Assessment; ECS Project No.: 49:7469; September 13, 2018
• Groundwater Assessment Report; ECS Project No.: 49:8056; November 8, 2018
• Groundwater Assessment Report (Revised); ECS Project No.: 49:8056-A; April 26, 2019

According to the 2008 Phase I Environmental Site Assessment, the site contained undeveloped, wooded
land and an agricultural field from at least 1937 until 1985. The site was occupied by Brayton International
from 1985 until 2002 and by Primo Designs from 2004 until 2007. Brayton International manufactured
office furniture at the site. Primo Design used the site as a warehousing and distribution center for
imported furniture. In March 1998, a fifty-five-gallon drum of precatalyzed lacquer was spilled inside the
building in the hazardous materials storage room. Approximately 40 gallons leaked through the concrete
floor and outside wall into the gravel fill beneath the concrete floor.

As part of the activities associated with the ECS reports, a total of five groundwater monitoring wells (MW-
1 through MW-5) were previously installed to investigate the precatalyzed lacquer spill. Monitoring well
MW-1 was installed in the approximate location of the precatalyzed lacquer spill. Results of groundwater
samples collected from these monitoring wells indicated 1,1-dichloroethene (1,1-DCE) in a sample
collected from monitoring well MW-2 (located near the southeast corner of the site building) on October
Brownfields Assessment Report & Receptor Survey, Rev. 1.0
Brayton International Furnishings
High Point, Guilford County, North Carolina
Brownfields Project Number 24056-20-041
ECS Project No. 49:8056-C
October 13, 2021

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23, 2018, at a concentration greater than its North Carolina 2L Groundwater Quality Standard
(NC2LGWQS).
3.0 OBJECTIVE OF THE ASSESSMENT

The objective of the assessment was to create a baseline of site conditions for the Brownfields
redevelopment as discussed during the March 15, 2021, project kickoff meeting with NCDEQ Brownfields,
by conducting the following sampling activities:

• The advancement of two borings to allow the construction of temporary monitoring wells and
collection of groundwater samples.
• Collection of soil samples during temporary monitoring well installation activities.
• Completion of a Brownfields Receptor Survey.

The groundwater samples were submitted for laboratory analysis of volatile organic compounds (VOCs)
by EPA Method 8260, semi-volatile organic compounds (SVOCs) by EPA Method 8270, Total RCRA Metals
by EPA Method 6020/7471, and hexavalent chromium by EPA Method 7199.

The soil samples collected were submitted for laboratory analysis of VOCs by EPA Method 8260, SVOCs
by EPA Method 8270, Total RCRA Metals by EPA Method 6020/7471, and hexavalent chromium by EPA
Method 7199 and were selected from the interval exhibiting the highest flame ionization detector (FID)
reading.

The sampling activities were conducted in general accordance with the Brownfields Assessment Work
Plan (Work Plan) prepared by ECS dated June 11, 2021 and approved by the NCDEQ Brownfields Program
on June 11, 2021. This assessment was also conducted in general accordance with the North Carolina
Division of Waste Management’s (NCDWM) Inactive Hazardous Site Program’s Guidelines for Assessment
and Cleanup (Revised October 2015).

4.0 FIELD ACTIVITIES

4.1 Monitoring Well Permit

Prior to conducting drilling activities, ECS obtained a monitoring well permit from the NCDEQ. The NCDEQ
well permit is included as Appendix A.

4.2 Utility Locate

Prior to commencing with field activities, ECS contacted North Carolina One-Call to locate/mark public
utilities at the site. Required separation distances between subsurface activities and marked utilities
(typically 30-inches) were maintained during the field activities. In addition, ECS contracted with Superior
Locate to clear the boring areas of private utilities.

Brownfields Assessment Report & Receptor Survey, Rev. 1.0
Brayton International Furnishings
High Point, Guilford County, North Carolina
Brownfields Project Number 24056-20-041
ECS Project No. 49:8056-C
October 13, 2021

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4.3 Soil Samples

Number and Sample Location

In general accordance with the Work Plan, on July 2, 2021, ECS collected soil samples from each boring
advanced for the installation of the temporary monitoring wells at the locations shown on Figure 3. The
borings were advanced by a North Carolina licensed driller with 3D Environmental Investigations, LLC (3D)
using a direct push technology (DPT) type drilling rig. Following the advancement of the borings, the
vertical position of each boring was surveyed by Tidemark Land Services (Tidemark). The coordinates for
the sample locations are provided in Table 1.

Soil Sample Collection

ECS collected two aliquots over each sample interval from each boring. Each aliquot was placed in a re-
sealable plastic bag which was promptly sealed after soil was placed within. ECS used a flame ionization
device (FID) to screen for volatile vapors in one of the aliquots associated with each interval for each
boring. ECS identified the aliquot associated with the highest FID readings and collected a sample for
analysis from the other associated aliquot not used for FID screening. Based on the results of the field
screening, the TW-1 soil sample was collected over the zero to two feet below ground surface (bgs)
interval, and the TW-2 soil sample was collected over the 10 to 15 feet bgs interval and were submitted
for laboratory analysis.

Boring logs for each soil boring are located in Appendix B.
Soil Sample Analysis
Following sample collection, the sample containers were placed on ice in a cooler and maintained under
chain-of-custody until delivered to Pace. Chain-of-custody protocol was utilized throughout the collection
and transport of the samples. As previously stated, the soil samples collected were submitted for
laboratory analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, RCRA Metals by EPA
Method 6010/7471, and hexavalent chromium by EPA Method 7199. The laboratory reporting limits were
reported at or below the applicable NCDEQ Preliminary Soil Remediation Goals (PSRGs) for residential soil,
industrial/commercial soil, and protection of groundwater. Additionally, concentrations detected below
the laboratory reporting limit (RL) and above the laboratory method detection limit were reported by the
laboratory were flagged with a J-flag qualifier, indicating the reported concentrations were estimates.

For quality assurance/quality control (QA/QC) purposes, one duplicate soil sample (SS-DUP) was collected
from the same location as the TW-2 soil sample and analyzed for the same compounds as the record
sample.
4.3 Groundwater Samples

Number and Sample Location

In general accordance with the Work Plan, ECS requested that the drilling contractor construct two
temporary monitoring wells at the site. Temporary monitoring wells TW-1 and TW-2 were installed on
Brownfields Assessment Report & Receptor Survey, Rev. 1.0
Brayton International Furnishings
High Point, Guilford County, North Carolina
Brownfields Project Number 24056-20-041
ECS Project No. 49:8056-C
October 13, 2021

5

July 2, 2021. The temporary monitoring wells were installed within borings conducted by direct push
technology drilling rig. The temporary monitoring well locations are shown on Figure 3. Following the
installation of the temporary monitoring wells, the horizontal and vertical position of each temporary
monitoring well was surveyed by Sacks Surveying & Mapping, on July 23, 2021. The coordinates are
provided in Table 1. The elevations and construction details of each temporary monitoring well are
provided in Table 2. Based upon the surveyed elevations of the top-of-casing of each temporary
monitoring well and the depth to water measurements measured on July 7, 2021, groundwater beneath
the site flowed predominantly to the northwest, west, and southwest as shown on Figure 4.

Boring logs for each temporary monitoring well, including well construction details, are included in
Appendix B. Well construction and abandonment forms were not available at the time of submittal of
this report; however, they can be submitted under separate cover if requested.

Sample Collection

The temporary monitoring wells were developed until the water produced was visibly free of sediment.
Following development, the wells were allowed to stabilize for approximately 96 hours prior to sample
collection and measurement of stabilized depth to water.

Samples were collected on July 7, 2021, with a peristaltic pump and new dedicated tubing. Field sampling
sheets are included in Appendix C.

Sample Analysis

Following sample collection, the sample containers were placed on ice in a cooler and maintained under
chain-of-custody until delivered to Pace Analytical Services, LLC (Pace), a North Carolina certified
laboratory located in Huntersville, North Carolina. Chain-of-custody protocol was utilized throughout the
collection and transport of the samples. As previously stated, the groundwater samples were submitted
for laboratory analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, RCRA Metals by EPA
Method 6010/7471, and hexavalent chromium by EPA Method 7199. The laboratory reporting limits were
reported at or below the applicable North Carolina 2L Groundwater Quality Standards (NC2LGWQS).

For QA/QC purposes, one duplicate groundwater sample (TW-DUP) was collected from monitoring well
MW-1 and analyzed for the same compounds as the record sample. In addition, a trip blank was provided
by the laboratory and analyzed for volatile organic compounds (VOCs).

5.0 RESULTS

5.1 Soil Boring Soil Analysis

Several metals were indicated at concentrations greater than the laboratory method detection limit in soil
samples TW-1 and TW-2 collected from the soil borings advanced during the temporary monitoring well
installation activities. A concentration of hexavalent chromium was detected in the TW-1 soil sample
greater than its Residential PSRG, while selenium was detected at a concentration greater than its
Brownfields Assessment Report & Receptor Survey, Rev. 1.0
Brayton International Furnishings
High Point, Guilford County, North Carolina
Brownfields Project Number 24056-20-041
ECS Project No. 49:8056-C
October 13, 2021

6

Protection of Groundwater PSRG in the TW-1 soil sample. The remaining concentrations of metals
detected in the TW-1 and TW-2 soil samples did not exceed their respective PSRGs.

Acetone was detected in the TW-1 soil sample at a concentration greater than the laboratory method
reporting limits, but less than its PSRGs. Additional VOCs and SVOCs were not indicated in either of the
soil samples at concentrations greater than the laboratory method reporting limits.

A summary of the soil sample analytical results is included as Table 3 and the laboratory report is included
as Appendix D.

Quality Control

One duplicate soil sample (DUP) was collected as a duplicate of soil sample TW-2 and analyzed for VOCs,
SVOCs, and RCRA metals plus hexavalent chromium using EPA Method 8260, 8270, 6020/7471, and 7199,
respectively. The compounds detected in the duplicate sample were similar to those detected in TW-2. A
Level II QA/QC package was requested from the laboratory.

The results are summarized in Table 3 and the laboratory report is included as Appendix D.

5.2 Groundwater Analysis

Review of the groundwater analytical results for the VOC analysis indicated 1,1-dichloroethane (1,1-DCA)
and 1,1-DCE at concentrations greater than the laboratory method detection limits in the MW-2 sample,
with the 1,1-DCA concentration greater than its NC2LGWQS. Additional VOCs were not indicated at
concentrations greater than the laboratory reporting limits in any of the remaining groundwater samples
collected as part of this sampling event. Also, concentrations of SVOCs were not detected at
concentrations greater than the laboratory reporting limits in either of the samples collected as part of
this sampling event.

Concentrations of barium, chromium, lead, and mercury in the metals analysis were detected in one or
more of the groundwater samples collected greater than the laboratory method reporting limits. The
following metals concentrations were also detected greater than their respective NC2LGWQS:

Total Chromium (MW-4 and MW-5)
Trivalent Chromium (MW-5)
Hexavalent Chromium (MW-4)
Lead (MW-5)
Mercury (MW-1)

Although the various metals were detected at concentrations greater than their respective NC2LGWQS,
based upon the turbidity of the samples, it is believed that the concentrations are likely due to the leaching
of natural metals from sediment within the sample, and not indicative of a release.

In addition, the concentrations of mercury detected in the MW-1 and MW-2 samples were greater than
its Residential Groundwater Vapor Intrusion Screening Level (VISL), with the concentration detected in
the MW-1 sample also greater than its Non-Residential VISL. In light of the groundwater sample results,
ECS input the laboratory analytical results of the MW-1 and MW-2 samples in to the NCDEQ Risk
Brownfields Assessment Report & Receptor Survey, Rev. 1.0
Brayton International Furnishings
High Point, Guilford County, North Carolina
Brownfields Project Number 24056-20-041
ECS Project No. 49:8056-C
October 13, 2021

7

Calculator. Based on the results of the NCDEQ Risk Calculator, the concentrations in the MW-2 sample
did not exceed the risk thresholds; however, the concentrations in the MW-1 sample did exceed the
hazard index for residential usage. Output from the results of the NCDEQ Risk Calculator are presented
in Appendix E. As mentioned above, it is believed that the elevated metals concentrations are the results
of the turbidity of the samples and not indicative of a release.

A summary of the groundwater analytical results is included as Table 4 and the laboratory report is
included as Appendix D.

Quality Control

One duplicate groundwater sample (DUP-1) was collected as a duplicate of groundwater sample MW-1,
and analyzed for VOCs, SVOCs, and RCRA metals using EPA Method 8260, 8270, and 6010/7470. The
compounds detected in the duplicate sample were similar to those detected in the record sample. A Level
II QA/QC package was requested from the laboratory.

The results are summarized in Table 4 and the laboratory report is included as Appendix D.

5.3 Brownfields Receptor Survey

ECS performed a Brownfields Receptor Survey. The results of the Brownfields Receptor Survey identified
five water supply wells located between 530 feet and 1,450 feet from the source area. The addresses of
the water supply wells are included with the receptor survey form. Underground utilities were noted in
the vicinity of the site at the locations identified on receptor survey form. Unnamed tributaries of Muddy
Creek are located approximately 1,000 and 2,700 feet west, 2,500 feet south, 5,000 feet southeast and
1,900 feet northeast of the site as seen on Figure 1. The Brownfields Receptor Survey form is included as
Appendix F.

6.0 CONCLUSIONS

Based on the results of the sampling presented above, as well as the receptor survey conducted for the
site, ECS has the following conclusions:

• Hexavalent chromium was detected in soil sample TW-1 at a concentration greater than its
Residential PSRG. Selenium was detected in soil sample TW-1 at a concentration greater than
its Protection of Groundwater PSRG. Acetone was detected in the TW-1 soil sample at a
concentration greater than the laboratory method reporting limits, but less than its PSRGs.
Additional VOCs and SVOCs were not detected at concentrations greater than the laboratory
method reporting limits.
• Laboratory results of the VOC analysis for the groundwater samples indicated 1,1-DCA and 1,1-
DCE at concentrations greater than the laboratory method detection limits in the MW-2
sample, with the 1,1-DCA concentration than its NC2LGWQS. Several metals were also
detected in one or more of the MW-1, MW-4, and MW-5 groundwater samples at
concentrations greater than their respective NC2LGWQS. In addition, the concentration of
mercury detected in the MW-1 and MW-2 groundwater samples were greater than its
Brownfields Assessment Report & Receptor Survey, Rev. 1.0
Brayton International Furnishings
High Point, Guilford County, North Carolina
Brownfields Project Number 24056-20-041
ECS Project No. 49:8056-C
October 13, 2021

8

Residential Groundwater Vapor Intrusion Screening Level (VISL), with the concentration
detected in the MW-1 sample greater than its Non-Residential Groundwater VISL.
• It is ECS’ opinion that the elevated metals concentrations are predominantly the result of the
turbidity of the groundwater samples and not indicated of a release.
• The MW-1 and MW-2 groundwater samples detected concentrations were input into the
NCDEQ Risk Calculator. Based on the results of the NCDEQ Risk Calculator, the concentrations
in the MW-2 sample did not exceed the risk thresholds; however, the concentrations in the
MW-1 sample did exceed the hazard index for residential usage.
• Based on the results of the Brownfields Receptor Survey sensitive receptors were not
identified in the vicinity of the site. The Brownfields Receptor Survey form is included as
Appendix E.

FIGURES

FIGURE 1
USGS TOPOGRAPHIC MAP
BRAYTON INTERNATIONAL FURNISHINGS
257, 263, & 265 SWATHMORE AVENUE
HIGH POINT, NORTH CAROLINA
ECS PROJECT NO.: 49:8056-C
SOURCE:
USGS 7.5’ TOPOGRAPHIC MAP
HIGH POINT EAST, NC 2019
SCALE:
AS SHOWN
SITE
FIGURE 2
SITE AERIAL PHOTOGRAPH
BRAYTON INTERNATIONAL FURNISHINGS
257, 263, & 265 SWATHMORE AVENUE
HIGH POINT, NORTH CAROLINA
ECS PROJECT NO.: 49:8056-C
SOURCE:
GUILFORD COUNTY GIS WEBSITE
ACCESSED JULY 8, 2020
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
GUILFORD COUNTY
RANDOLPH COUNTY
FIGURE 3
SAMPLE LOCATION MAP
BRAYTON INTERNATIONAL FURNISHINGS
257, 263, & 265 SWATHMORE AVENUE
HIGH POINT, NORTH CAROLINA
ECS PROJECT NO.: 49:8056-C
SOURCE:
GUILFORD COUNTY GIS WEBSITE
ACCESSED JULY 8, 2020
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
TEMPORARY MONITORING WELL/SOIL SAMPLE LOCATION
MW-1
MW-3
MW-4
MW-2
MW-5
MONITORING WELL LOCATION
TW-1
TW-2
FIGURE 4
GROUNDWATER CONTOUR MAP
BRAYTON INTERNATIONAL FURNISHINGS
257, 263, & 265 SWATHMORE AVENUE
HIGH POINT, NORTH CAROLINA
ECS PROJECT NO.: 49:8056-C
SOURCE:
GUILFORD COUNTY GIS WEBSITE
ACCESSED JULY 8, 2020
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
GROUNDWATER MEASURING POINT
MW-1
(856.55)
MW-3
(862.05)
MW-4
(862.05)
MW-2
(861.95)
MW-5
(866.43)
GROUNDWATER FLOW DIRECTION
TW-1
(864.96)TW-2
(862.98)
GROUNDWATER CONTOUR
858
860 862
864
GROUNDWATER ELEVATION(866.43)

TABLES

Table 1
Summary of Sample Point Coordinates
Brayton International Furnishings
257, 263, & 265 Swathmore Avenue
High Point, Guilford County, North Carolina
NCDEQ Brownfields Project No.: 24056-20-041
ECS Project No.: 49:8056-C
Sample Point Latitude Longitude Northing*Easting*
TW-1 35º55'06.9954"-79º59'24.3665"790,732.93 1,706,837.71
TW-2 35º55'08.2425"-79º59'23.2559"790,858.11 1,706,930.31
MW-1 35º55'04.5301"-79º59'23.8751"790,483.26 1,706,875.64
MW-2 35º55'04.1668"-79º59'21.5953"790,444.66 1,707,062.78
MW-3 35º55'05.3541"-79º59'20.7586"790,564.02 1,707,132.79
MW-4 35º55'03.8360"-79º59'20.7633"790,410.53 1,707,130.88
MW-5 35º55'03.3468"-79º59'21.5009"790,361.67 1,707,069.72
Notes:
* = Coordinate Values are North Carolina State Plane Coordinates (NAD83)
Table 2
Monitoring Well Construction Details and Groundwater Elevation Data
Brayton International Furnishings
257, 263, & 265 Swathmore Avenue
High Point, Guilford County, North Carolina
NCDEQ Brownfields Project No.: 24056-20-041
ECS Project No.: 49:8056-C
Well ID Installation
Date
Well
Diameter (in)
Casing Depth
(ft bgs)
Total Depth
(ft bgs)
Top-of-Casing
Elevation
(ft AMSL)
Date of
Measurement
Depth to
Water
(ft BTOC)
Groundwater
Elevation
(ft AMSL)
03/22/21 21.36 858.41
07/07/21 23.22 856.55
03/22/21 14.43 864.01
07/07/21 16.49 861.95
03/22/21 16.84 864.12
07/07/21 18.91 862.05
03/22/21 8.83 869.55
07/07/21 16.33 862.05
03/22/21 14.22 864.15
07/07/21 11.94 866.43
TW-1 07/02/21 1.0 5.0 5.0 to 20.0 20.0 880.97 07/07/21 16.11 864.86
TW-2 07/02/21 1.0 5.0 5.0 to 20.0 20.0 881.30 07/07/21 18.32 862.98
Notes:
Top-of-casing elevations surveyed by Tidemark Land Services on 11/02/20
Monitoring well MW-7 installed by others previously. Complete construction details are unknown.
in = inches
ft bgs = feet below ground surface
ft AMSL = feet above mean sea level
ft BTOC = feet below top-of-casing
Screen Interval
(x to y ft bgs)
03/27/19
03/27/19
10/22/18
10/22/18
10/22/18 20.02.0
2.0 19.0 19.0 to 34.0
2.0 20.0 20.0
MW-5
MW-4
MW-3
MW-2
MW-1 879.7735.035.0to20.0
34.0 878.44
2.0 19.0 19.0 to 34.0 34.0 880.96
to 35.0 35.0 878.38
35.0 878.372.0 20.0 20.0 to 35.0
Table 3
Summary of Soil Sample Analytical Results
Brayton International Furnishings
257, 263, & 265 Swathmore Avenue
High Point, Guilford County, North Carolina
NCDEQ Brownfields Project No.: 24056-20-041
ECS Project No.: 49:8056-C
VOCs by EPA
Method 8260
SVOCs by EPA
Method 8270 RCRA Metals by EPA Methods 6010D, 7471B, and 7199
AcetoneAll CompoundsArsenicBariumCadmiumTotal ChromiumTrivalent ChromiumHexavalent ChromiumLeadMercurySeleniumSilverProtection of Groundwater PSRG 25 Various 5.8 580 3.0 NE 360,000 3.8 270 1.0 2.1 3.4
Residential PSRG 12,000 Various 0.68 3,100 14 NE 23,000 0.310 NE 2.3 78 78
Industrial/Commercial PSRG 140,000 Various 3.0 47,000 200 NE 350,000 6.5 NE 9.7 1,200 1,200
TW-1 07/02/21 0 - 2 0.15 J BRL <2.3 39.5 <0.092 30.9 30.37 0.527 J 8.4 0.013 3.3 <2.3
TW-2 07/02/21 10 - 15 <0.13 BRL <2.0 21.1 <0.078 7.8 7.8 <1.20 2.9 0.0035 0.72 J <0.39
DUP*07/02/21 10 - 15 0.071 J BRL <1.9 21.3 <0.078 9.6 9.6 <1.16 2.7 0.0038 0.67 J <0.39
Notes:
All results presented in milligrams per kilogram (mg/kg)
Compounds not shown were not detected
ft bgs = feet below ground surface
VOCs = Volatile Organic Compounds
SVOCs = Semi-volatile Organic Compounds
PSRG = Preliminary Soil Remediation Goal (June 2021)
BRL = Below laboratory reporting level
NE = Not established
Trivalent Chromium Concentration = Total Chromium Concentration - Hexavalent Chromium Concentration
J = Estimated concentration detected between laboratory method reporting limit and detection limit
* = DUP is a duplicate of soil sample TW-2
VALUE = concentration greater than the laboratory method reporting limit
VALUE = concentration greater than the Protection of Groundwater PSRG
VALUE = concentration greater than the Residential PSRG
VALUE = concentration greater than Industrial/Commerical PSRG
Sample ID Sample
Date
Sample Depth
(x to y ft bgs)
Table 4Summary of Groundwater Sample Analytical Results
Brayton International Furnishings257, 263, & 265 Swathmore Avenue
High Point, Guilford County, North CarolinaNCDEQ Brownfields Project No.: 24056-20-041
ECS Project No.: 49:8056-C
VOCs by EPA Method
8260
SVOCs by EPA
Method 8270 Total RCRA Metals by EPA Method 6010 and 7470
1,1-Dichloroethane1,1-DichloroetheneAll CompoundsArsenicBariumCadmiumTotal ChromiumTrivalent ChromiumHexavalent ChromiumLeadMercurySeleniumSilverNC2LGWQS 6 350 Various 10 700 2 10 10 10 15 1 20 20
Residential VISLs 7.6 390 Various *******0.18 *NE
Non-Residential VISLs 33 160 Various *******0.75 *NE
MW-1 07/07/21 <1.0 <1.0 BRL <10.0 23.8 <1.0 <5.0 <2.49 2.51 <5.0 1.0 <10.0 <5.0
DUP-1**07/07/21 <1.0 <1.0 BRL <10.0 22.2 <1.0 <5.0 <2.51 2.49 <5.0 0.92 <10.0 <5.0
MW-2 07/07/21 7.4 30.7 BRL <10.0 34.1 <1.0 <5.0 <4.37 0.632 <5.0 0.67 <10.0 <5.0
MW-3 07/07/21 <1.0 <1.0 BRL <10.0 52.2 <1.0 5.9 5.9 <0.5 <5.0 <0.20 <10.0 <5.0
MW-4 07/07/21 <1.0 <1.0 BRL <10.0 45.7 <1.0 16.3 1.9 14.4 <5.0 <0.20 <10.0 <5.0
MW-5 07/07/21 <1.0 <1.0 BRL <10.0 177 <1.0 47.9 47.23 0.673 20.5 <0.20 <10.0 <5.0
TW-1 07/07/21 <1.0 <1.0 BRL <10.0 37.4 <1.0 <5.0 <4.44 0.559 <5.0 <0.20 <10.0 <5.0
TW-2 07/07/21 <1.0 <1.0 BRL <10.0 19.6 <1.0 <5.0 <4.42 0.583 <5.0 <0.20 <10.0 <5.0
Notes:
All results presented in micrograms per liter (µg/L)
Compounds not shown were not detected
VOCs = Volatile Organic Compounds
SVOCs = Semi-volatile Organic Compounds
NC2LGWQS = North Carolina 2L Groundwater Quality Standards
VISL = Vapor Intrusion Screening Level
* = Not Volatile
** =
BRL = Below reporting limit
Trivalent Chromium concentration = Total Chromium concentration - Hexavalent Chromium concentration
VALUE = concentration greater than laboratory method reporting limit
VALUE = concentration greater than NC2LGWQS
VALUE = concentration greater than Residential VISL
VALUE = concentration greater than Non-Residential VISL
Sample
DateSample ID

APPENDIX A

March 26, 2021

Jason Sparrow
Tuggle Duggins, P.A,
400 Bellemeade Street, Suite 800
Greensboro, North Carolina 27401

S0UBJECT: MONITORING WELL CONSTRUCTION
PERMIT NO. WM0401285
COUNTY: Guilford
FILE NAME: Brayton International Furnishings

Dear Mr. Sparrow:

In accordance with your application received on March 24, 2021, we are forwarding herewith:

1. Monitoring Well Construction Permit No. WM0401285 for the construction of two (2)
temporary monitoring wells at 265 Swathmore Avenue in Greensboro in Guilford County.

Henceforth, correspondence and data relating to this well shall be designated as specified in the
subject heading above. This Permit will be effective from the date of issuance and shall be subject
to the conditions and limitations as specified therein. If you have any questions regarding this
permit, please contact me or Jim Gonsiewski at [phone].

Sincerely,

Lon T. Snider
Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NCDEQ – WSRO

cc: Gene Mao – Guilford County Environmental Health (Electronic Copy)
Deborah S. Butt – High Point University (Electronic Copy)
Scott Young – ECS Southeast, LLP (Electronic Copy)
WSRO Electronic Files
Laserfiche Files

NORTH CAROLINA
DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES – WATER QUALITY REGIONAL OPERATIONS
SECTION

PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL

In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and
other applicable Laws, Rules and Regulations.

PERMISSION IS HEREBY GRANTED TO

Tuggle Duggins, P.A.

FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of two temporary
monitoring wells owned by Tuggle Duggins, P.A. The wells will be located at 265 Swathmore
Avenue in High Point, North Carolina, in Guilford County. This Permit is issued in accordance
with the application received on March 24, 2021 in conformity with specifications and supporting
data, all of which are filed with the Department of Environmental Quality and are considered
integral parts of this Permit.

This Permit is for well construction only, and does not waive any provision or requirement of any
other applicable law or regulation. Construction of any well under this Permit shall be in strict
compliance with the North Carolina Well Construction Regulations and Standards (15A NCAC
02C .0100), and other State and Local Laws and regulations pertaining to well construction.

If any requirements or limitations specified in this Permit are unacceptable, you have a right to an
adjudicatory hearing upon written request within 30 days of receipt of this Permit. The request
must be in the form of a written petition conforming to Chapter 150B of the North Carolina General
Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service Center, Raleigh,
North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding.

This Permit will be effective for one year from the date of its issuance and shall be subject to other
specified conditions, limitations, or exceptions as follows:

1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these
wells are being installed as part of an investigation for contamination from an underground
storage tank or dry cleaner incident.
2. Issuance of this Permit does not supersede any other agreement, permit, or requirement
issued by another agency.
3. The well(s) shall be located and constructed as shown on the attachments submitted as part
of the Permit application.
4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC
02C .0108(o).
5. Well construction records (GW-1) for each well shall be submitted to the Division of Water
Resources’ Information Processing Unit within 30 days of the well completion.
6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A
NCAC 02C .0113 and a well abandonment record (GW-30) shall be submitted to the
Division of Water Resources’ Information Processing Unit within 30 days of the well
abandonment.
7. The County Health Department may require a county monitoring well construction permit.
Please contact the health department for their requirements.

Permit issued the 26th day of March, 2021

FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION

_______________________________________________
Lon T Snider, Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NCDEQ - WSRO

By Authority of the Environmental Management Commission

Permit No. # WM0401285

APPENDIX B

Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading10.4
10.0
10.3
10.2 Sample NumberTW-1 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
ML
ML
ML
ML
DescripƟon
Red/Brown Clayey Silt
Red/Brown Silt
Brown Silt
Brown Silt; moist
Brown Silt, saturated
END OF DRILLING AT 20.0 FT
WELL CONSTRUCTION
Schedule 40 PVC
Casing
Bentonite Seal
#2 Filter Sand
Schedule 40 0.010"
PVC Screen
Project Name:Brayton InternaƟonal Furnishings
Client:Tuggle Duggins
Site LocaƟon:257, 263, & 265 Swathmore Avenue, High
Point, North Carolina 27263
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:TW-1
Project No.:49:8056-C
Driller:3D Enviro Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Jul 02 2021
WL (CompleƟon)17.94 Boring Completed:Jul 02 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy Cavallier
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading9.2
8.4
8.7
9.7 Sample NumberTW-2 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML
ML
ML
ML
ML
DescripƟon
Red/Brown Silt
Tan Silt
Tan Silt
Brown Silt; moist
Brown Silt; saturated
END OF DRILLING AT 20.0 FT
WELL CONSTRUCTION
Schedule 40 PVC
Casing
Bentonite
Sand Pack
Schedule 40 0.010"
SloƩed PVC Screen
Project Name:Brayton InternaƟonal Furnishings
Client:Tuggle Duggins
Site LocaƟon:257, 263, & 265 Swathmore Avenue, High
Point, North Carolina 27263
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:TW-2
Project No.:49:8056-C
Driller:3D Enviro Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Jul 02 2021
WL (CompleƟon)16.12 Boring Completed:Jul 02 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy Cavallier
Roger Smith

APPENDIX C

APPENDIX D

#=CL#
July 19, 2021
LIMS USE: FR - SCOTT YOUNG
LIMS OBJECT ID: 92547722
92547722
Project:
Pace Project No.:
RE:
Scott YoungECS Southeast, LLP1812 Center Park DriveSuite DCharlotte, NC 28217
Brayton BF
Dear Scott Young:
Enclosed are the analytical results for sample(s) received by the laboratory on July 06, 2021. The results relate only to thesamples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and thelaboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:• Pace National - Mt. Juliet• Pace Analytical Services - Asheville• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang for
[e-mail]
Project Manager
Angela Baioni
[phone]
Enclosures
cc: ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 49
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92547722
Brayton BF
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 49
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92547722
Brayton BF
Lab ID Sample ID Matrix Date Collected Date Received
92547722001 TW-1 Solid 07/02/21 10:40 07/06/21 11:40
92547722002 TW-2 Solid 07/02/21 12:10 07/06/21 11:40
92547722003 DUP Solid 07/02/21 12:10 07/06/21 11:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 49
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92547722
Brayton BF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92547722001 TW-1 EPA 6010D 7 PASI-ACBV, RDT
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92547722002 TW-2 EPA 6010D 7 PASI-ACBV
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92547722003 DUP EPA 6010D 7 PASI-ACBV
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 49
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92547722
Brayton BF
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92547722001 TW-1
Barium 39.5 mg/kg 07/12/21 15:080.92EPA 6010D
Chromium 30.9 mg/kg 07/12/21 15:080.46EPA 6010D
Lead 8.4 mg/kg 07/12/21 15:080.92EPA 6010D
Selenium 3.3 mg/kg 07/12/21 15:080.92EPA 6010D
Mercury 0.013 mg/kg 07/12/21 14:310.0039EPA 7471B
Acetone 0.15J mg/kg 07/12/21 13:030.20EPA 8260D
Percent Moisture 20.8 %07/06/21 17:11 N20.10SW-846
Total Solids 78.6 %07/09/21 11:54SM 2540G
Chromium, Hexavalent 0.527J mg/kg 07/16/21 14:35 J1.27EPA 7199
92547722002 TW-2
Barium 21.1 mg/kg 07/12/21 15:110.78EPA 6010D
Chromium 7.8 mg/kg 07/12/21 15:110.39EPA 6010D
Lead 2.9 mg/kg 07/12/21 15:110.78EPA 6010D
Selenium 0.72J mg/kg 07/12/21 15:110.78EPA 6010D
Mercury 0.0035 mg/kg 07/12/21 14:330.0023EPA 7471B
Percent Moisture 12.6 %07/06/21 17:12 N20.10SW-846
Total Solids 83.2 %07/09/21 11:54SM 2540G
92547722003 DUP
Barium 21.3 mg/kg 07/12/21 15:140.78EPA 6010D
Chromium 9.6 mg/kg 07/12/21 15:140.39EPA 6010D
Lead 2.7 mg/kg 07/12/21 15:140.78EPA 6010D
Selenium 0.67J mg/kg 07/12/21 15:140.78EPA 6010D
Mercury 0.0038 mg/kg 07/12/21 14:360.0026EPA 7471B
Acetone 0.071J mg/kg 07/09/21 19:400.13EPA 8260D
Percent Moisture 13.3 %07/19/21 11:27 N20.10SW-846
Total Solids 86.1 %07/09/21 11:54SM 2540G
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: TW-1 Lab ID: 92547722001 Collected: 07/02/21 10:40 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND mg/kg 07/12/21 15:08 7440-38-207/11/21 15:512.3 0.46 1
Barium 39.5 mg/kg 07/12/21 15:08 7440-39-307/11/21 15:510.92 0.23 1
Cadmium ND mg/kg 07/12/21 15:08 7440-43-907/11/21 15:510.092 0.046 1
Chromium 30.9 mg/kg 07/12/21 15:08 7440-47-307/11/21 15:510.46 0.23 1
Lead 8.4 mg/kg 07/12/21 15:08 7439-92-107/11/21 15:510.92 0.23 1
Selenium 3.3 mg/kg 07/12/21 15:08 7782-49-207/11/21 15:510.92 0.46 1
Silver ND mg/kg 07/12/21 22:30 7440-22-407/11/21 15:512.3 1.1 5
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.013 mg/kg 07/12/21 14:31 7439-97-607/08/21 16:430.0039 0.0030 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 07/07/21 12:07 83-32-907/06/21 14:120.42 0.15 1
Acenaphthylene ND mg/kg 07/07/21 12:07 208-96-807/06/21 14:120.42 0.15 1
Aniline ND mg/kg 07/07/21 12:07 62-53-307/06/21 14:120.42 0.16 1
Anthracene ND mg/kg 07/07/21 12:07 120-12-707/06/21 14:120.42 0.14 1
Benzo(a)anthracene ND mg/kg 07/07/21 12:07 56-55-307/06/21 14:120.42 0.14 1
Benzo(a)pyrene ND mg/kg 07/07/21 12:07 50-32-807/06/21 14:120.42 0.14 1
Benzo(b)fluoranthene ND mg/kg 07/07/21 12:07 205-99-207/06/21 14:120.42 0.14 1
Benzo(g,h,i)perylene ND mg/kg 07/07/21 12:07 191-24-207/06/21 14:120.42 0.16 1
Benzo(k)fluoranthene ND mg/kg 07/07/21 12:07 207-08-907/06/21 14:120.42 0.15 1
Benzoic Acid ND mg/kg 07/07/21 12:07 65-85-007/06/21 14:122.1 0.90 1
Benzyl alcohol ND mg/kg 07/07/21 12:07 100-51-607/06/21 14:120.84 0.32 1
4-Bromophenylphenyl ether ND mg/kg 07/07/21 12:07 101-55-307/06/21 14:120.42 0.16 1
Butylbenzylphthalate ND mg/kg 07/07/21 12:07 85-68-707/06/21 14:120.42 0.18 1
4-Chloro-3-methylphenol ND mg/kg 07/07/21 12:07 59-50-707/06/21 14:120.84 0.29 1
4-Chloroaniline ND mg/kg 07/07/21 12:07 106-47-807/06/21 14:120.84 0.33 1
bis(2-Chloroethoxy)methane ND mg/kg 07/07/21 12:07 111-91-107/06/21 14:120.42 0.17 1
bis(2-Chloroethyl) ether ND mg/kg 07/07/21 12:07 111-44-407/06/21 14:120.42 0.16 1
2-Chloronaphthalene ND mg/kg 07/07/21 12:07 91-58-707/06/21 14:120.42 0.17 1
2-Chlorophenol ND mg/kg 07/07/21 12:07 95-57-807/06/21 14:120.42 0.16 1
4-Chlorophenylphenyl ether ND mg/kg 07/07/21 12:07 7005-72-307/06/21 14:120.42 0.16 1
Chrysene ND mg/kg 07/07/21 12:07 218-01-907/06/21 14:120.42 0.15 1
Dibenz(a,h)anthracene ND mg/kg 07/07/21 12:07 53-70-307/06/21 14:120.42 0.16 1
Dibenzofuran ND mg/kg 07/07/21 12:07 132-64-907/06/21 14:120.42 0.15 1
1,2-Dichlorobenzene ND mg/kg 07/07/21 12:07 95-50-107/06/21 14:120.42 0.15 1
1,3-Dichlorobenzene ND mg/kg 07/07/21 12:07 541-73-107/06/21 14:120.42 0.15 1
1,4-Dichlorobenzene ND mg/kg 07/07/21 12:07 106-46-707/06/21 14:120.42 0.16 1
3,3'-Dichlorobenzidine ND mg/kg 07/07/21 12:07 91-94-1 IL07/06/21 14:120.84 0.28 1
2,4-Dichlorophenol ND mg/kg 07/07/21 12:07 120-83-207/06/21 14:120.42 0.16 1
Diethylphthalate ND mg/kg 07/07/21 12:07 84-66-207/06/21 14:120.42 0.15 1
2,4-Dimethylphenol ND mg/kg 07/07/21 12:07 105-67-907/06/21 14:120.42 0.17 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: TW-1 Lab ID: 92547722001 Collected: 07/02/21 10:40 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 07/07/21 12:07 131-11-307/06/21 14:120.42 0.15 1
Di-n-butylphthalate ND mg/kg 07/07/21 12:07 84-74-207/06/21 14:120.42 0.14 1
4,6-Dinitro-2-methylphenol ND mg/kg 07/07/21 12:07 534-52-107/06/21 14:120.84 0.39 1
2,4-Dinitrophenol ND mg/kg 07/07/21 12:07 51-28-507/06/21 14:122.1 1.3 1
2,4-Dinitrotoluene ND mg/kg 07/07/21 12:07 121-14-207/06/21 14:120.42 0.16 1
2,6-Dinitrotoluene ND mg/kg 07/07/21 12:07 606-20-207/06/21 14:120.42 0.15 1
Di-n-octylphthalate ND mg/kg 07/07/21 12:07 117-84-007/06/21 14:120.42 0.17 1
bis(2-Ethylhexyl)phthalate ND mg/kg 07/07/21 12:07 117-81-707/06/21 14:120.42 0.16 1
Fluoranthene ND mg/kg 07/07/21 12:07 206-44-007/06/21 14:120.42 0.14 1
Fluorene ND mg/kg 07/07/21 12:07 86-73-707/06/21 14:120.42 0.15 1
Hexachloro-1,3-butadiene ND mg/kg 07/07/21 12:07 87-68-307/06/21 14:120.42 0.18 1
Hexachlorobenzene ND mg/kg 07/07/21 12:07 118-74-107/06/21 14:120.42 0.16 1
Hexachlorocyclopentadiene ND mg/kg 07/07/21 12:07 77-47-4 v207/06/21 14:120.42 0.24 1
Hexachloroethane ND mg/kg 07/07/21 12:07 67-72-107/06/21 14:120.42 0.16 1
Indeno(1,2,3-cd)pyrene ND mg/kg 07/07/21 12:07 193-39-507/06/21 14:120.42 0.17 1
Isophorone ND mg/kg 07/07/21 12:07 78-59-107/06/21 14:120.42 0.19 1
1-Methylnaphthalene ND mg/kg 07/07/21 12:07 90-12-007/06/21 14:120.42 0.15 1
2-Methylnaphthalene ND mg/kg 07/07/21 12:07 91-57-607/06/21 14:120.42 0.17 1
2-Methylphenol(o-Cresol)ND mg/kg 07/07/21 12:07 95-48-707/06/21 14:120.42 0.17 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 07/07/21 12:07 15831-10-407/06/21 14:120.42 0.17 1
Naphthalene ND mg/kg 07/07/21 12:07 91-20-307/06/21 14:120.42 0.14 1
2-Nitroaniline ND mg/kg 07/07/21 12:07 88-74-407/06/21 14:122.1 0.34 1
3-Nitroaniline ND mg/kg 07/07/21 12:07 99-09-2 IL07/06/21 14:122.1 0.33 1
4-Nitroaniline ND mg/kg 07/07/21 12:07 100-01-607/06/21 14:120.84 0.32 1
Nitrobenzene ND mg/kg 07/07/21 12:07 98-95-307/06/21 14:120.42 0.19 1
2-Nitrophenol ND mg/kg 07/07/21 12:07 88-75-507/06/21 14:120.42 0.18 1
4-Nitrophenol ND mg/kg 07/07/21 12:07 100-02-707/06/21 14:122.1 0.81 1
N-Nitrosodimethylamine ND mg/kg 07/07/21 12:07 62-75-907/06/21 14:120.42 0.14 1
N-Nitroso-di-n-propylamine ND mg/kg 07/07/21 12:07 621-64-707/06/21 14:120.42 0.16 1
N-Nitrosodiphenylamine ND mg/kg 07/07/21 12:07 86-30-607/06/21 14:120.42 0.15 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 07/07/21 12:07 108-60-107/06/21 14:120.42 0.20 1
Pentachlorophenol ND mg/kg 07/07/21 12:07 87-86-507/06/21 14:120.84 0.41 1
Phenanthrene ND mg/kg 07/07/21 12:07 85-01-807/06/21 14:120.42 0.14 1
Phenol ND mg/kg 07/07/21 12:07 108-95-207/06/21 14:120.42 0.19 1
Pyrene ND mg/kg 07/07/21 12:07 129-00-007/06/21 14:120.42 0.17 1
Pyridine ND mg/kg 07/07/21 12:07 110-86-107/06/21 14:120.42 0.13 1
1,2,4-Trichlorobenzene ND mg/kg 07/07/21 12:07 120-82-107/06/21 14:120.42 0.17 1
2,4,5-Trichlorophenol ND mg/kg 07/07/21 12:07 95-95-407/06/21 14:120.42 0.19 1
2,4,6-Trichlorophenol ND mg/kg 07/07/21 12:07 88-06-207/06/21 14:120.42 0.17 1
Surrogates
Nitrobenzene-d5 (S)41 %07/07/21 12:07 4165-60-007/06/21 14:1221-130 1
2-Fluorobiphenyl (S)46 %07/07/21 12:07 321-60-807/06/21 14:1219-130 1
Terphenyl-d14 (S)49 %07/07/21 12:07 1718-51-007/06/21 14:1215-130 1
Phenol-d6 (S)42 %07/07/21 12:07 13127-88-307/06/21 14:1218-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: TW-1 Lab ID: 92547722001 Collected: 07/02/21 10:40 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)44 %07/07/21 12:07 367-12-407/06/21 14:1218-130 1
2,4,6-Tribromophenol (S)70 %07/07/21 12:07 118-79-607/06/21 14:1218-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 0.15J mg/kg 07/12/21 13:03 67-64-107/12/21 12:150.20 0.064 1
Benzene ND mg/kg 07/12/21 13:03 71-43-207/12/21 12:150.010 0.0040 1
Bromobenzene ND mg/kg 07/12/21 13:03 108-86-107/12/21 12:150.010 0.0033 1
Bromochloromethane ND mg/kg 07/12/21 13:03 74-97-507/12/21 12:150.010 0.0030 1
Bromodichloromethane ND mg/kg 07/12/21 13:03 75-27-407/12/21 12:150.010 0.0039 1
Bromoform ND mg/kg 07/12/21 13:03 75-25-207/12/21 12:150.010 0.0035 1
Bromomethane ND mg/kg 07/12/21 13:03 74-83-9 IK07/12/21 12:150.020 0.016 1
2-Butanone (MEK)ND mg/kg 07/12/21 13:03 78-93-307/12/21 12:150.20 0.048 1
n-Butylbenzene ND mg/kg 07/12/21 13:03 104-51-807/12/21 12:150.010 0.0047 1
sec-Butylbenzene ND mg/kg 07/12/21 13:03 135-98-807/12/21 12:150.010 0.0044 1
tert-Butylbenzene ND mg/kg 07/12/21 13:03 98-06-607/12/21 12:150.010 0.0036 1
Carbon tetrachloride ND mg/kg 07/12/21 13:03 56-23-507/12/21 12:150.010 0.0037 1
Chlorobenzene ND mg/kg 07/12/21 13:03 108-90-707/12/21 12:150.010 0.0019 1
Chloroethane ND mg/kg 07/12/21 13:03 75-00-307/12/21 12:150.020 0.0077 1
Chloroform ND mg/kg 07/12/21 13:03 67-66-307/12/21 12:150.010 0.0061 1
Chloromethane ND mg/kg 07/12/21 13:03 74-87-307/12/21 12:150.020 0.0084 1
2-Chlorotoluene ND mg/kg 07/12/21 13:03 95-49-807/12/21 12:150.010 0.0035 1
4-Chlorotoluene ND mg/kg 07/12/21 13:03 106-43-407/12/21 12:150.010 0.0018 1
1,2-Dibromo-3-chloropropane ND mg/kg 07/12/21 13:03 96-12-807/12/21 12:150.010 0.0039 1
Dibromochloromethane ND mg/kg 07/12/21 13:03 124-48-107/12/21 12:150.010 0.0056 1
1,2-Dibromoethane (EDB)ND mg/kg 07/12/21 13:03 106-93-407/12/21 12:150.010 0.0044 1
Dibromomethane ND mg/kg 07/12/21 13:03 74-95-307/12/21 12:150.010 0.0021 1
1,2-Dichlorobenzene ND mg/kg 07/12/21 13:03 95-50-107/12/21 12:150.010 0.0036 1
1,3-Dichlorobenzene ND mg/kg 07/12/21 13:03 541-73-107/12/21 12:150.010 0.0031 1
1,4-Dichlorobenzene ND mg/kg 07/12/21 13:03 106-46-707/12/21 12:150.010 0.0026 1
Dichlorodifluoromethane ND mg/kg 07/12/21 13:03 75-71-807/12/21 12:150.020 0.0043 1
1,1-Dichloroethane ND mg/kg 07/12/21 13:03 75-34-307/12/21 12:150.010 0.0041 1
1,2-Dichloroethane ND mg/kg 07/12/21 13:03 107-06-207/12/21 12:150.010 0.0066 1
1,1-Dichloroethene ND mg/kg 07/12/21 13:03 75-35-407/12/21 12:150.010 0.0041 1
cis-1,2-Dichloroethene ND mg/kg 07/12/21 13:03 156-59-207/12/21 12:150.010 0.0034 1
trans-1,2-Dichloroethene ND mg/kg 07/12/21 13:03 156-60-507/12/21 12:150.010 0.0035 1
1,2-Dichloropropane ND mg/kg 07/12/21 13:03 78-87-507/12/21 12:150.010 0.0030 1
1,3-Dichloropropane ND mg/kg 07/12/21 13:03 142-28-907/12/21 12:150.010 0.0031 1
2,2-Dichloropropane ND mg/kg 07/12/21 13:03 594-20-707/12/21 12:150.010 0.0033 1
1,1-Dichloropropene ND mg/kg 07/12/21 13:03 563-58-607/12/21 12:150.010 0.0048 1
cis-1,3-Dichloropropene ND mg/kg 07/12/21 13:03 10061-01-507/12/21 12:150.010 0.0027 1
trans-1,3-Dichloropropene ND mg/kg 07/12/21 13:03 10061-02-607/12/21 12:150.010 0.0034 1
Diisopropyl ether ND mg/kg 07/12/21 13:03 108-20-307/12/21 12:150.010 0.0027 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: TW-1 Lab ID: 92547722001 Collected: 07/02/21 10:40 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 07/12/21 13:03 100-41-407/12/21 12:150.010 0.0046 1
Hexachloro-1,3-butadiene ND mg/kg 07/12/21 13:03 87-68-307/12/21 12:150.020 0.016 1
2-Hexanone ND mg/kg 07/12/21 13:03 591-78-607/12/21 12:150.10 0.0096 1
Isopropylbenzene (Cumene)ND mg/kg 07/12/21 13:03 98-82-807/12/21 12:150.010 0.0034 1
p-Isopropyltoluene ND mg/kg 07/12/21 13:03 99-87-607/12/21 12:150.010 0.0049 1
Methylene Chloride ND mg/kg 07/12/21 13:03 75-09-207/12/21 12:150.040 0.027 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 07/12/21 13:03 108-10-107/12/21 12:150.10 0.0096 1
Methyl-tert-butyl ether ND mg/kg 07/12/21 13:03 1634-04-407/12/21 12:150.010 0.0037 1
Naphthalene ND mg/kg 07/12/21 13:03 91-20-307/12/21 12:150.010 0.0052 1
n-Propylbenzene ND mg/kg 07/12/21 13:03 103-65-107/12/21 12:150.010 0.0036 1
Styrene ND mg/kg 07/12/21 13:03 100-42-507/12/21 12:150.010 0.0026 1
1,1,1,2-Tetrachloroethane ND mg/kg 07/12/21 13:03 630-20-607/12/21 12:150.010 0.0038 1
1,1,2,2-Tetrachloroethane ND mg/kg 07/12/21 13:03 79-34-507/12/21 12:150.010 0.0026 1
Tetrachloroethene ND mg/kg 07/12/21 13:03 127-18-407/12/21 12:150.010 0.0032 1
Toluene ND mg/kg 07/12/21 13:03 108-88-307/12/21 12:150.010 0.0028 1
1,2,3-Trichlorobenzene ND mg/kg 07/12/21 13:03 87-61-607/12/21 12:150.010 0.0081 1
1,2,4-Trichlorobenzene ND mg/kg 07/12/21 13:03 120-82-107/12/21 12:150.010 0.0084 1
1,1,1-Trichloroethane ND mg/kg 07/12/21 13:03 71-55-607/12/21 12:150.010 0.0052 1
1,1,2-Trichloroethane ND mg/kg 07/12/21 13:03 79-00-507/12/21 12:150.010 0.0033 1
Trichloroethene ND mg/kg 07/12/21 13:03 79-01-607/12/21 12:150.010 0.0026 1
Trichlorofluoromethane ND mg/kg 07/12/21 13:03 75-69-407/12/21 12:150.010 0.0055 1
1,2,3-Trichloropropane ND mg/kg 07/12/21 13:03 96-18-407/12/21 12:150.010 0.0050 1
1,2,4-Trimethylbenzene ND mg/kg 07/12/21 13:03 95-63-607/12/21 12:150.010 0.0027 1
1,3,5-Trimethylbenzene ND mg/kg 07/12/21 13:03 108-67-807/12/21 12:150.010 0.0034 1
Vinyl acetate ND mg/kg 07/12/21 13:03 108-05-407/12/21 12:150.10 0.0073 1
Vinyl chloride ND mg/kg 07/12/21 13:03 75-01-407/12/21 12:150.020 0.0051 1
Xylene (Total)ND mg/kg 07/12/21 13:03 1330-20-707/12/21 12:150.020 0.0057 1
m&p-Xylene ND mg/kg 07/12/21 13:03 179601-23-107/12/21 12:150.020 0.0068 1
o-Xylene ND mg/kg 07/12/21 13:03 95-47-607/12/21 12:150.010 0.0044 1
Surrogates
Toluene-d8 (S)103 %07/12/21 13:03 2037-26-507/12/21 12:1570-130 1
4-Bromofluorobenzene (S)99 %07/12/21 13:03 460-00-407/12/21 12:1569-134 1
1,2-Dichloroethane-d4 (S)110 %07/12/21 13:03 17060-07-007/12/21 12:1570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.8 %07/06/21 17:11 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 78.6 %07/09/21 11:5407/09/21 11:451
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: TW-1 Lab ID: 92547722001 Collected: 07/02/21 10:40 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.527J mg/kg 07/16/21 14:35 18540-29-9 J07/14/21 16:591.27 0.325 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: TW-2 Lab ID: 92547722002 Collected: 07/02/21 12:10 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND mg/kg 07/12/21 15:11 7440-38-207/11/21 15:512.0 0.39 1
Barium 21.1 mg/kg 07/12/21 15:11 7440-39-307/11/21 15:510.78 0.20 1
Cadmium ND mg/kg 07/12/21 15:11 7440-43-907/11/21 15:510.078 0.039 1
Chromium 7.8 mg/kg 07/12/21 15:11 7440-47-307/11/21 15:510.39 0.20 1
Lead 2.9 mg/kg 07/12/21 15:11 7439-92-107/11/21 15:510.78 0.20 1
Selenium 0.72J mg/kg 07/12/21 15:11 7782-49-207/11/21 15:510.78 0.39 1
Silver ND mg/kg 07/12/21 15:11 7440-22-407/11/21 15:510.39 0.20 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.0035 mg/kg 07/12/21 14:33 7439-97-607/08/21 16:430.0023 0.0017 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 07/07/21 12:35 83-32-907/06/21 14:120.38 0.13 1
Acenaphthylene ND mg/kg 07/07/21 12:35 208-96-807/06/21 14:120.38 0.13 1
Aniline ND mg/kg 07/07/21 12:35 62-53-307/06/21 14:120.38 0.15 1
Anthracene ND mg/kg 07/07/21 12:35 120-12-707/06/21 14:120.38 0.12 1
Benzo(a)anthracene ND mg/kg 07/07/21 12:35 56-55-307/06/21 14:120.38 0.13 1
Benzo(a)pyrene ND mg/kg 07/07/21 12:35 50-32-807/06/21 14:120.38 0.13 1
Benzo(b)fluoranthene ND mg/kg 07/07/21 12:35 205-99-207/06/21 14:120.38 0.13 1
Benzo(g,h,i)perylene ND mg/kg 07/07/21 12:35 191-24-207/06/21 14:120.38 0.15 1
Benzo(k)fluoranthene ND mg/kg 07/07/21 12:35 207-08-907/06/21 14:120.38 0.13 1
Benzoic Acid ND mg/kg 07/07/21 12:35 65-85-007/06/21 14:121.9 0.82 1
Benzyl alcohol ND mg/kg 07/07/21 12:35 100-51-607/06/21 14:120.76 0.29 1
4-Bromophenylphenyl ether ND mg/kg 07/07/21 12:35 101-55-307/06/21 14:120.38 0.15 1
Butylbenzylphthalate ND mg/kg 07/07/21 12:35 85-68-707/06/21 14:120.38 0.16 1
4-Chloro-3-methylphenol ND mg/kg 07/07/21 12:35 59-50-707/06/21 14:120.76 0.27 1
4-Chloroaniline ND mg/kg 07/07/21 12:35 106-47-807/06/21 14:120.76 0.30 1
bis(2-Chloroethoxy)methane ND mg/kg 07/07/21 12:35 111-91-107/06/21 14:120.38 0.16 1
bis(2-Chloroethyl) ether ND mg/kg 07/07/21 12:35 111-44-407/06/21 14:120.38 0.14 1
2-Chloronaphthalene ND mg/kg 07/07/21 12:35 91-58-707/06/21 14:120.38 0.15 1
2-Chlorophenol ND mg/kg 07/07/21 12:35 95-57-807/06/21 14:120.38 0.14 1
4-Chlorophenylphenyl ether ND mg/kg 07/07/21 12:35 7005-72-307/06/21 14:120.38 0.14 1
Chrysene ND mg/kg 07/07/21 12:35 218-01-907/06/21 14:120.38 0.14 1
Dibenz(a,h)anthracene ND mg/kg 07/07/21 12:35 53-70-307/06/21 14:120.38 0.15 1
Dibenzofuran ND mg/kg 07/07/21 12:35 132-64-907/06/21 14:120.38 0.14 1
1,2-Dichlorobenzene ND mg/kg 07/07/21 12:35 95-50-107/06/21 14:120.38 0.14 1
1,3-Dichlorobenzene ND mg/kg 07/07/21 12:35 541-73-107/06/21 14:120.38 0.13 1
1,4-Dichlorobenzene ND mg/kg 07/07/21 12:35 106-46-707/06/21 14:120.38 0.15 1
3,3'-Dichlorobenzidine ND mg/kg 07/07/21 12:35 91-94-1 IL07/06/21 14:120.76 0.26 1
2,4-Dichlorophenol ND mg/kg 07/07/21 12:35 120-83-207/06/21 14:120.38 0.15 1
Diethylphthalate ND mg/kg 07/07/21 12:35 84-66-207/06/21 14:120.38 0.14 1
2,4-Dimethylphenol ND mg/kg 07/07/21 12:35 105-67-907/06/21 14:120.38 0.16 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: TW-2 Lab ID: 92547722002 Collected: 07/02/21 12:10 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 07/07/21 12:35 131-11-307/06/21 14:120.38 0.14 1
Di-n-butylphthalate ND mg/kg 07/07/21 12:35 84-74-207/06/21 14:120.38 0.13 1
4,6-Dinitro-2-methylphenol ND mg/kg 07/07/21 12:35 534-52-107/06/21 14:120.76 0.35 1
2,4-Dinitrophenol ND mg/kg 07/07/21 12:35 51-28-507/06/21 14:121.9 1.2 1
2,4-Dinitrotoluene ND mg/kg 07/07/21 12:35 121-14-207/06/21 14:120.38 0.15 1
2,6-Dinitrotoluene ND mg/kg 07/07/21 12:35 606-20-207/06/21 14:120.38 0.14 1
Di-n-octylphthalate ND mg/kg 07/07/21 12:35 117-84-007/06/21 14:120.38 0.15 1
bis(2-Ethylhexyl)phthalate ND mg/kg 07/07/21 12:35 117-81-707/06/21 14:120.38 0.15 1
Fluoranthene ND mg/kg 07/07/21 12:35 206-44-007/06/21 14:120.38 0.13 1
Fluorene ND mg/kg 07/07/21 12:35 86-73-707/06/21 14:120.38 0.13 1
Hexachloro-1,3-butadiene ND mg/kg 07/07/21 12:35 87-68-307/06/21 14:120.38 0.16 1
Hexachlorobenzene ND mg/kg 07/07/21 12:35 118-74-107/06/21 14:120.38 0.15 1
Hexachlorocyclopentadiene ND mg/kg 07/07/21 12:35 77-47-4 v207/06/21 14:120.38 0.22 1
Hexachloroethane ND mg/kg 07/07/21 12:35 67-72-107/06/21 14:120.38 0.15 1
Indeno(1,2,3-cd)pyrene ND mg/kg 07/07/21 12:35 193-39-507/06/21 14:120.38 0.15 1
Isophorone ND mg/kg 07/07/21 12:35 78-59-107/06/21 14:120.38 0.17 1
1-Methylnaphthalene ND mg/kg 07/07/21 12:35 90-12-007/06/21 14:120.38 0.13 1
2-Methylnaphthalene ND mg/kg 07/07/21 12:35 91-57-607/06/21 14:120.38 0.15 1
2-Methylphenol(o-Cresol)ND mg/kg 07/07/21 12:35 95-48-707/06/21 14:120.38 0.16 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 07/07/21 12:35 15831-10-407/06/21 14:120.38 0.15 1
Naphthalene ND mg/kg 07/07/21 12:35 91-20-307/06/21 14:120.38 0.13 1
2-Nitroaniline ND mg/kg 07/07/21 12:35 88-74-407/06/21 14:121.9 0.31 1
3-Nitroaniline ND mg/kg 07/07/21 12:35 99-09-2 IL07/06/21 14:121.9 0.30 1
4-Nitroaniline ND mg/kg 07/07/21 12:35 100-01-607/06/21 14:120.76 0.29 1
Nitrobenzene ND mg/kg 07/07/21 12:35 98-95-307/06/21 14:120.38 0.18 1
2-Nitrophenol ND mg/kg 07/07/21 12:35 88-75-507/06/21 14:120.38 0.16 1
4-Nitrophenol ND mg/kg 07/07/21 12:35 100-02-707/06/21 14:121.9 0.74 1
N-Nitrosodimethylamine ND mg/kg 07/07/21 12:35 62-75-907/06/21 14:120.38 0.13 1
N-Nitroso-di-n-propylamine ND mg/kg 07/07/21 12:35 621-64-707/06/21 14:120.38 0.14 1
N-Nitrosodiphenylamine ND mg/kg 07/07/21 12:35 86-30-607/06/21 14:120.38 0.13 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 07/07/21 12:35 108-60-107/06/21 14:120.38 0.18 1
Pentachlorophenol ND mg/kg 07/07/21 12:35 87-86-507/06/21 14:120.76 0.37 1
Phenanthrene ND mg/kg 07/07/21 12:35 85-01-807/06/21 14:120.38 0.12 1
Phenol ND mg/kg 07/07/21 12:35 108-95-207/06/21 14:120.38 0.17 1
Pyrene ND mg/kg 07/07/21 12:35 129-00-007/06/21 14:120.38 0.15 1
Pyridine ND mg/kg 07/07/21 12:35 110-86-107/06/21 14:120.38 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 07/07/21 12:35 120-82-107/06/21 14:120.38 0.15 1
2,4,5-Trichlorophenol ND mg/kg 07/07/21 12:35 95-95-407/06/21 14:120.38 0.17 1
2,4,6-Trichlorophenol ND mg/kg 07/07/21 12:35 88-06-207/06/21 14:120.38 0.16 1
Surrogates
Nitrobenzene-d5 (S)29 %07/07/21 12:35 4165-60-007/06/21 14:1221-130 1
2-Fluorobiphenyl (S)32 %07/07/21 12:35 321-60-807/06/21 14:1219-130 1
Terphenyl-d14 (S)36 %07/07/21 12:35 1718-51-007/06/21 14:1215-130 1
Phenol-d6 (S)30 %07/07/21 12:35 13127-88-307/06/21 14:1218-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: TW-2 Lab ID: 92547722002 Collected: 07/02/21 12:10 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)31 %07/07/21 12:35 367-12-407/06/21 14:1218-130 1
2,4,6-Tribromophenol (S)47 %07/07/21 12:35 118-79-607/06/21 14:1218-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 07/09/21 19:22 67-64-107/09/21 10:480.13 0.041 1
Benzene ND mg/kg 07/09/21 19:22 71-43-207/09/21 10:480.0064 0.0025 1
Bromobenzene ND mg/kg 07/09/21 19:22 108-86-107/09/21 10:480.0064 0.0021 1
Bromochloromethane ND mg/kg 07/09/21 19:22 74-97-507/09/21 10:480.0064 0.0019 1
Bromodichloromethane ND mg/kg 07/09/21 19:22 75-27-407/09/21 10:480.0064 0.0025 1
Bromoform ND mg/kg 07/09/21 19:22 75-25-207/09/21 10:480.0064 0.0022 1
Bromomethane ND mg/kg 07/09/21 19:22 74-83-9 IK07/09/21 10:480.013 0.010 1
2-Butanone (MEK)ND mg/kg 07/09/21 19:22 78-93-307/09/21 10:480.13 0.031 1
n-Butylbenzene ND mg/kg 07/09/21 19:22 104-51-807/09/21 10:480.0064 0.0030 1
sec-Butylbenzene ND mg/kg 07/09/21 19:22 135-98-807/09/21 10:480.0064 0.0028 1
tert-Butylbenzene ND mg/kg 07/09/21 19:22 98-06-607/09/21 10:480.0064 0.0023 1
Carbon tetrachloride ND mg/kg 07/09/21 19:22 56-23-507/09/21 10:480.0064 0.0024 1
Chlorobenzene ND mg/kg 07/09/21 19:22 108-90-707/09/21 10:480.0064 0.0012 1
Chloroethane ND mg/kg 07/09/21 19:22 75-00-307/09/21 10:480.013 0.0049 1
Chloroform ND mg/kg 07/09/21 19:22 67-66-307/09/21 10:480.0064 0.0039 1
Chloromethane ND mg/kg 07/09/21 19:22 74-87-307/09/21 10:480.013 0.0053 1
2-Chlorotoluene ND mg/kg 07/09/21 19:22 95-49-807/09/21 10:480.0064 0.0023 1
4-Chlorotoluene ND mg/kg 07/09/21 19:22 106-43-407/09/21 10:480.0064 0.0011 1
1,2-Dibromo-3-chloropropane ND mg/kg 07/09/21 19:22 96-12-807/09/21 10:480.0064 0.0025 1
Dibromochloromethane ND mg/kg 07/09/21 19:22 124-48-107/09/21 10:480.0064 0.0036 1
1,2-Dibromoethane (EDB)ND mg/kg 07/09/21 19:22 106-93-407/09/21 10:480.0064 0.0028 1
Dibromomethane ND mg/kg 07/09/21 19:22 74-95-307/09/21 10:480.0064 0.0014 1
1,2-Dichlorobenzene ND mg/kg 07/09/21 19:22 95-50-107/09/21 10:480.0064 0.0023 1
1,3-Dichlorobenzene ND mg/kg 07/09/21 19:22 541-73-107/09/21 10:480.0064 0.0020 1
1,4-Dichlorobenzene ND mg/kg 07/09/21 19:22 106-46-707/09/21 10:480.0064 0.0017 1
Dichlorodifluoromethane ND mg/kg 07/09/21 19:22 75-71-807/09/21 10:480.013 0.0028 1
1,1-Dichloroethane ND mg/kg 07/09/21 19:22 75-34-307/09/21 10:480.0064 0.0026 1
1,2-Dichloroethane ND mg/kg 07/09/21 19:22 107-06-207/09/21 10:480.0064 0.0042 1
1,1-Dichloroethene ND mg/kg 07/09/21 19:22 75-35-407/09/21 10:480.0064 0.0026 1
cis-1,2-Dichloroethene ND mg/kg 07/09/21 19:22 156-59-207/09/21 10:480.0064 0.0022 1
trans-1,2-Dichloroethene ND mg/kg 07/09/21 19:22 156-60-507/09/21 10:480.0064 0.0022 1
1,2-Dichloropropane ND mg/kg 07/09/21 19:22 78-87-507/09/21 10:480.0064 0.0019 1
1,3-Dichloropropane ND mg/kg 07/09/21 19:22 142-28-907/09/21 10:480.0064 0.0020 1
2,2-Dichloropropane ND mg/kg 07/09/21 19:22 594-20-707/09/21 10:480.0064 0.0021 1
1,1-Dichloropropene ND mg/kg 07/09/21 19:22 563-58-607/09/21 10:480.0064 0.0031 1
cis-1,3-Dichloropropene ND mg/kg 07/09/21 19:22 10061-01-507/09/21 10:480.0064 0.0017 1
trans-1,3-Dichloropropene ND mg/kg 07/09/21 19:22 10061-02-607/09/21 10:480.0064 0.0022 1
Diisopropyl ether ND mg/kg 07/09/21 19:22 108-20-307/09/21 10:480.0064 0.0017 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: TW-2 Lab ID: 92547722002 Collected: 07/02/21 12:10 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 07/09/21 19:22 100-41-407/09/21 10:480.0064 0.0030 1
Hexachloro-1,3-butadiene ND mg/kg 07/09/21 19:22 87-68-307/09/21 10:480.013 0.010 1
2-Hexanone ND mg/kg 07/09/21 19:22 591-78-607/09/21 10:480.064 0.0061 1
Isopropylbenzene (Cumene)ND mg/kg 07/09/21 19:22 98-82-807/09/21 10:480.0064 0.0022 1
p-Isopropyltoluene ND mg/kg 07/09/21 19:22 99-87-607/09/21 10:480.0064 0.0031 1
Methylene Chloride ND mg/kg 07/09/21 19:22 75-09-207/09/21 10:480.025 0.017 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 07/09/21 19:22 108-10-107/09/21 10:480.064 0.0061 1
Methyl-tert-butyl ether ND mg/kg 07/09/21 19:22 1634-04-407/09/21 10:480.0064 0.0024 1
Naphthalene ND mg/kg 07/09/21 19:22 91-20-307/09/21 10:480.0064 0.0033 1
n-Propylbenzene ND mg/kg 07/09/21 19:22 103-65-107/09/21 10:480.0064 0.0023 1
Styrene ND mg/kg 07/09/21 19:22 100-42-507/09/21 10:480.0064 0.0017 1
1,1,1,2-Tetrachloroethane ND mg/kg 07/09/21 19:22 630-20-607/09/21 10:480.0064 0.0024 1
1,1,2,2-Tetrachloroethane ND mg/kg 07/09/21 19:22 79-34-507/09/21 10:480.0064 0.0017 1
Tetrachloroethene ND mg/kg 07/09/21 19:22 127-18-407/09/21 10:480.0064 0.0020 1
Toluene ND mg/kg 07/09/21 19:22 108-88-307/09/21 10:480.0064 0.0018 1
1,2,3-Trichlorobenzene ND mg/kg 07/09/21 19:22 87-61-607/09/21 10:480.0064 0.0051 1
1,2,4-Trichlorobenzene ND mg/kg 07/09/21 19:22 120-82-107/09/21 10:480.0064 0.0053 1
1,1,1-Trichloroethane ND mg/kg 07/09/21 19:22 71-55-607/09/21 10:480.0064 0.0033 1
1,1,2-Trichloroethane ND mg/kg 07/09/21 19:22 79-00-507/09/21 10:480.0064 0.0021 1
Trichloroethene ND mg/kg 07/09/21 19:22 79-01-607/09/21 10:480.0064 0.0016 1
Trichlorofluoromethane ND mg/kg 07/09/21 19:22 75-69-407/09/21 10:480.0064 0.0035 1
1,2,3-Trichloropropane ND mg/kg 07/09/21 19:22 96-18-407/09/21 10:480.0064 0.0032 1
1,2,4-Trimethylbenzene ND mg/kg 07/09/21 19:22 95-63-607/09/21 10:480.0064 0.0017 1
1,3,5-Trimethylbenzene ND mg/kg 07/09/21 19:22 108-67-807/09/21 10:480.0064 0.0021 1
Vinyl acetate ND mg/kg 07/09/21 19:22 108-05-407/09/21 10:480.064 0.0046 1
Vinyl chloride ND mg/kg 07/09/21 19:22 75-01-407/09/21 10:480.013 0.0032 1
Xylene (Total)ND mg/kg 07/09/21 19:22 1330-20-707/09/21 10:480.013 0.0036 1
m&p-Xylene ND mg/kg 07/09/21 19:22 179601-23-107/09/21 10:480.013 0.0044 1
o-Xylene ND mg/kg 07/09/21 19:22 95-47-607/09/21 10:480.0064 0.0028 1
Surrogates
Toluene-d8 (S)103 %07/09/21 19:22 2037-26-507/09/21 10:4870-130 1
4-Bromofluorobenzene (S)98 %07/09/21 19:22 460-00-407/09/21 10:4869-134 1
1,2-Dichloroethane-d4 (S)109 %07/09/21 19:22 17060-07-007/09/21 10:4870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.6 %07/06/21 17:12 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 83.2 %07/09/21 11:5407/09/21 11:451
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: TW-2 Lab ID: 92547722002 Collected: 07/02/21 12:10 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 07/16/21 15:12 18540-29-907/14/21 16:591.20 0.307 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: DUP Lab ID: 92547722003 Collected: 07/02/21 12:10 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND mg/kg 07/12/21 15:14 7440-38-207/11/21 15:511.9 0.39 1
Barium 21.3 mg/kg 07/12/21 15:14 7440-39-307/11/21 15:510.78 0.19 1
Cadmium ND mg/kg 07/12/21 15:14 7440-43-907/11/21 15:510.078 0.039 1
Chromium 9.6 mg/kg 07/12/21 15:14 7440-47-307/11/21 15:510.39 0.19 1
Lead 2.7 mg/kg 07/12/21 15:14 7439-92-107/11/21 15:510.78 0.19 1
Selenium 0.67J mg/kg 07/12/21 15:14 7782-49-207/11/21 15:510.78 0.39 1
Silver ND mg/kg 07/12/21 15:14 7440-22-407/11/21 15:510.39 0.19 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.0038 mg/kg 07/12/21 14:36 7439-97-607/08/21 16:430.0026 0.0020 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 07/07/21 13:02 83-32-907/06/21 14:120.39 0.14 1
Acenaphthylene ND mg/kg 07/07/21 13:02 208-96-807/06/21 14:120.39 0.14 1
Aniline ND mg/kg 07/07/21 13:02 62-53-307/06/21 14:120.39 0.15 1
Anthracene ND mg/kg 07/07/21 13:02 120-12-707/06/21 14:120.39 0.13 1
Benzo(a)anthracene ND mg/kg 07/07/21 13:02 56-55-307/06/21 14:120.39 0.13 1
Benzo(a)pyrene ND mg/kg 07/07/21 13:02 50-32-807/06/21 14:120.39 0.13 1
Benzo(b)fluoranthene ND mg/kg 07/07/21 13:02 205-99-207/06/21 14:120.39 0.13 1
Benzo(g,h,i)perylene ND mg/kg 07/07/21 13:02 191-24-207/06/21 14:120.39 0.15 1
Benzo(k)fluoranthene ND mg/kg 07/07/21 13:02 207-08-907/06/21 14:120.39 0.14 1
Benzoic Acid ND mg/kg 07/07/21 13:02 65-85-007/06/21 14:121.9 0.83 1
Benzyl alcohol ND mg/kg 07/07/21 13:02 100-51-607/06/21 14:120.77 0.29 1
4-Bromophenylphenyl ether ND mg/kg 07/07/21 13:02 101-55-307/06/21 14:120.39 0.15 1
Butylbenzylphthalate ND mg/kg 07/07/21 13:02 85-68-707/06/21 14:120.39 0.16 1
4-Chloro-3-methylphenol ND mg/kg 07/07/21 13:02 59-50-707/06/21 14:120.77 0.27 1
4-Chloroaniline ND mg/kg 07/07/21 13:02 106-47-807/06/21 14:120.77 0.30 1
bis(2-Chloroethoxy)methane ND mg/kg 07/07/21 13:02 111-91-107/06/21 14:120.39 0.16 1
bis(2-Chloroethyl) ether ND mg/kg 07/07/21 13:02 111-44-407/06/21 14:120.39 0.14 1
2-Chloronaphthalene ND mg/kg 07/07/21 13:02 91-58-707/06/21 14:120.39 0.15 1
2-Chlorophenol ND mg/kg 07/07/21 13:02 95-57-807/06/21 14:120.39 0.14 1
4-Chlorophenylphenyl ether ND mg/kg 07/07/21 13:02 7005-72-307/06/21 14:120.39 0.14 1
Chrysene ND mg/kg 07/07/21 13:02 218-01-907/06/21 14:120.39 0.14 1
Dibenz(a,h)anthracene ND mg/kg 07/07/21 13:02 53-70-307/06/21 14:120.39 0.15 1
Dibenzofuran ND mg/kg 07/07/21 13:02 132-64-907/06/21 14:120.39 0.14 1
1,2-Dichlorobenzene ND mg/kg 07/07/21 13:02 95-50-107/06/21 14:120.39 0.14 1
1,3-Dichlorobenzene ND mg/kg 07/07/21 13:02 541-73-107/06/21 14:120.39 0.14 1
1,4-Dichlorobenzene ND mg/kg 07/07/21 13:02 106-46-707/06/21 14:120.39 0.15 1
3,3'-Dichlorobenzidine ND mg/kg 07/07/21 13:02 91-94-1 IL07/06/21 14:120.77 0.26 1
2,4-Dichlorophenol ND mg/kg 07/07/21 13:02 120-83-207/06/21 14:120.39 0.15 1
Diethylphthalate ND mg/kg 07/07/21 13:02 84-66-207/06/21 14:120.39 0.14 1
2,4-Dimethylphenol ND mg/kg 07/07/21 13:02 105-67-907/06/21 14:120.39 0.16 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: DUP Lab ID: 92547722003 Collected: 07/02/21 12:10 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 07/07/21 13:02 131-11-307/06/21 14:120.39 0.14 1
Di-n-butylphthalate ND mg/kg 07/07/21 13:02 84-74-207/06/21 14:120.39 0.13 1
4,6-Dinitro-2-methylphenol ND mg/kg 07/07/21 13:02 534-52-107/06/21 14:120.77 0.36 1
2,4-Dinitrophenol ND mg/kg 07/07/21 13:02 51-28-507/06/21 14:121.9 1.2 1
2,4-Dinitrotoluene ND mg/kg 07/07/21 13:02 121-14-207/06/21 14:120.39 0.15 1
2,6-Dinitrotoluene ND mg/kg 07/07/21 13:02 606-20-207/06/21 14:120.39 0.14 1
Di-n-octylphthalate ND mg/kg 07/07/21 13:02 117-84-007/06/21 14:120.39 0.15 1
bis(2-Ethylhexyl)phthalate ND mg/kg 07/07/21 13:02 117-81-707/06/21 14:120.39 0.15 1
Fluoranthene ND mg/kg 07/07/21 13:02 206-44-007/06/21 14:120.39 0.13 1
Fluorene ND mg/kg 07/07/21 13:02 86-73-707/06/21 14:120.39 0.14 1
Hexachloro-1,3-butadiene ND mg/kg 07/07/21 13:02 87-68-307/06/21 14:120.39 0.17 1
Hexachlorobenzene ND mg/kg 07/07/21 13:02 118-74-107/06/21 14:120.39 0.15 1
Hexachlorocyclopentadiene ND mg/kg 07/07/21 13:02 77-47-4 v207/06/21 14:120.39 0.22 1
Hexachloroethane ND mg/kg 07/07/21 13:02 67-72-107/06/21 14:120.39 0.15 1
Indeno(1,2,3-cd)pyrene ND mg/kg 07/07/21 13:02 193-39-507/06/21 14:120.39 0.15 1
Isophorone ND mg/kg 07/07/21 13:02 78-59-107/06/21 14:120.39 0.17 1
1-Methylnaphthalene ND mg/kg 07/07/21 13:02 90-12-007/06/21 14:120.39 0.14 1
2-Methylnaphthalene ND mg/kg 07/07/21 13:02 91-57-607/06/21 14:120.39 0.15 1
2-Methylphenol(o-Cresol)ND mg/kg 07/07/21 13:02 95-48-707/06/21 14:120.39 0.16 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 07/07/21 13:02 15831-10-407/06/21 14:120.39 0.16 1
Naphthalene ND mg/kg 07/07/21 13:02 91-20-307/06/21 14:120.39 0.13 1
2-Nitroaniline ND mg/kg 07/07/21 13:02 88-74-407/06/21 14:121.9 0.32 1
3-Nitroaniline ND mg/kg 07/07/21 13:02 99-09-2 IL07/06/21 14:121.9 0.30 1
4-Nitroaniline ND mg/kg 07/07/21 13:02 100-01-607/06/21 14:120.77 0.29 1
Nitrobenzene ND mg/kg 07/07/21 13:02 98-95-307/06/21 14:120.39 0.18 1
2-Nitrophenol ND mg/kg 07/07/21 13:02 88-75-507/06/21 14:120.39 0.17 1
4-Nitrophenol ND mg/kg 07/07/21 13:02 100-02-707/06/21 14:121.9 0.75 1
N-Nitrosodimethylamine ND mg/kg 07/07/21 13:02 62-75-907/06/21 14:120.39 0.13 1
N-Nitroso-di-n-propylamine ND mg/kg 07/07/21 13:02 621-64-707/06/21 14:120.39 0.14 1
N-Nitrosodiphenylamine ND mg/kg 07/07/21 13:02 86-30-607/06/21 14:120.39 0.14 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 07/07/21 13:02 108-60-107/06/21 14:120.39 0.18 1
Pentachlorophenol ND mg/kg 07/07/21 13:02 87-86-507/06/21 14:120.77 0.38 1
Phenanthrene ND mg/kg 07/07/21 13:02 85-01-807/06/21 14:120.39 0.13 1
Phenol ND mg/kg 07/07/21 13:02 108-95-207/06/21 14:120.39 0.17 1
Pyrene ND mg/kg 07/07/21 13:02 129-00-007/06/21 14:120.39 0.16 1
Pyridine ND mg/kg 07/07/21 13:02 110-86-107/06/21 14:120.39 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 07/07/21 13:02 120-82-107/06/21 14:120.39 0.15 1
2,4,5-Trichlorophenol ND mg/kg 07/07/21 13:02 95-95-407/06/21 14:120.39 0.18 1
2,4,6-Trichlorophenol ND mg/kg 07/07/21 13:02 88-06-207/06/21 14:120.39 0.16 1
Surrogates
Nitrobenzene-d5 (S)30 %07/07/21 13:02 4165-60-007/06/21 14:1221-130 1
2-Fluorobiphenyl (S)34 %07/07/21 13:02 321-60-807/06/21 14:1219-130 1
Terphenyl-d14 (S)36 %07/07/21 13:02 1718-51-007/06/21 14:1215-130 1
Phenol-d6 (S)31 %07/07/21 13:02 13127-88-307/06/21 14:1218-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: DUP Lab ID: 92547722003 Collected: 07/02/21 12:10 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)32 %07/07/21 13:02 367-12-407/06/21 14:1218-130 1
2,4,6-Tribromophenol (S)51 %07/07/21 13:02 118-79-607/06/21 14:1218-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 0.071J mg/kg 07/09/21 19:40 67-64-107/09/21 10:480.13 0.041 1
Benzene ND mg/kg 07/09/21 19:40 71-43-207/09/21 10:480.0063 0.0025 1
Bromobenzene ND mg/kg 07/09/21 19:40 108-86-107/09/21 10:480.0063 0.0021 1
Bromochloromethane ND mg/kg 07/09/21 19:40 74-97-507/09/21 10:480.0063 0.0019 1
Bromodichloromethane ND mg/kg 07/09/21 19:40 75-27-407/09/21 10:480.0063 0.0024 1
Bromoform ND mg/kg 07/09/21 19:40 75-25-207/09/21 10:480.0063 0.0022 1
Bromomethane ND mg/kg 07/09/21 19:40 74-83-9 IK07/09/21 10:480.013 0.010 1
2-Butanone (MEK)ND mg/kg 07/09/21 19:40 78-93-307/09/21 10:480.13 0.030 1
n-Butylbenzene ND mg/kg 07/09/21 19:40 104-51-807/09/21 10:480.0063 0.0030 1
sec-Butylbenzene ND mg/kg 07/09/21 19:40 135-98-807/09/21 10:480.0063 0.0028 1
tert-Butylbenzene ND mg/kg 07/09/21 19:40 98-06-607/09/21 10:480.0063 0.0023 1
Carbon tetrachloride ND mg/kg 07/09/21 19:40 56-23-507/09/21 10:480.0063 0.0024 1
Chlorobenzene ND mg/kg 07/09/21 19:40 108-90-707/09/21 10:480.0063 0.0012 1
Chloroethane ND mg/kg 07/09/21 19:40 75-00-307/09/21 10:480.013 0.0049 1
Chloroform ND mg/kg 07/09/21 19:40 67-66-307/09/21 10:480.0063 0.0039 1
Chloromethane ND mg/kg 07/09/21 19:40 74-87-307/09/21 10:480.013 0.0053 1
2-Chlorotoluene ND mg/kg 07/09/21 19:40 95-49-807/09/21 10:480.0063 0.0022 1
4-Chlorotoluene ND mg/kg 07/09/21 19:40 106-43-407/09/21 10:480.0063 0.0011 1
1,2-Dibromo-3-chloropropane ND mg/kg 07/09/21 19:40 96-12-807/09/21 10:480.0063 0.0025 1
Dibromochloromethane ND mg/kg 07/09/21 19:40 124-48-107/09/21 10:480.0063 0.0036 1
1,2-Dibromoethane (EDB)ND mg/kg 07/09/21 19:40 106-93-407/09/21 10:480.0063 0.0028 1
Dibromomethane ND mg/kg 07/09/21 19:40 74-95-307/09/21 10:480.0063 0.0014 1
1,2-Dichlorobenzene ND mg/kg 07/09/21 19:40 95-50-107/09/21 10:480.0063 0.0023 1
1,3-Dichlorobenzene ND mg/kg 07/09/21 19:40 541-73-107/09/21 10:480.0063 0.0020 1
1,4-Dichlorobenzene ND mg/kg 07/09/21 19:40 106-46-707/09/21 10:480.0063 0.0016 1
Dichlorodifluoromethane ND mg/kg 07/09/21 19:40 75-71-807/09/21 10:480.013 0.0027 1
1,1-Dichloroethane ND mg/kg 07/09/21 19:40 75-34-307/09/21 10:480.0063 0.0026 1
1,2-Dichloroethane ND mg/kg 07/09/21 19:40 107-06-207/09/21 10:480.0063 0.0042 1
1,1-Dichloroethene ND mg/kg 07/09/21 19:40 75-35-407/09/21 10:480.0063 0.0026 1
cis-1,2-Dichloroethene ND mg/kg 07/09/21 19:40 156-59-207/09/21 10:480.0063 0.0022 1
trans-1,2-Dichloroethene ND mg/kg 07/09/21 19:40 156-60-507/09/21 10:480.0063 0.0022 1
1,2-Dichloropropane ND mg/kg 07/09/21 19:40 78-87-507/09/21 10:480.0063 0.0019 1
1,3-Dichloropropane ND mg/kg 07/09/21 19:40 142-28-907/09/21 10:480.0063 0.0020 1
2,2-Dichloropropane ND mg/kg 07/09/21 19:40 594-20-707/09/21 10:480.0063 0.0021 1
1,1-Dichloropropene ND mg/kg 07/09/21 19:40 563-58-607/09/21 10:480.0063 0.0030 1
cis-1,3-Dichloropropene ND mg/kg 07/09/21 19:40 10061-01-507/09/21 10:480.0063 0.0017 1
trans-1,3-Dichloropropene ND mg/kg 07/09/21 19:40 10061-02-607/09/21 10:480.0063 0.0022 1
Diisopropyl ether ND mg/kg 07/09/21 19:40 108-20-307/09/21 10:480.0063 0.0017 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: DUP Lab ID: 92547722003 Collected: 07/02/21 12:10 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 07/09/21 19:40 100-41-407/09/21 10:480.0063 0.0030 1
Hexachloro-1,3-butadiene ND mg/kg 07/09/21 19:40 87-68-307/09/21 10:480.013 0.010 1
2-Hexanone ND mg/kg 07/09/21 19:40 591-78-607/09/21 10:480.063 0.0061 1
Isopropylbenzene (Cumene)ND mg/kg 07/09/21 19:40 98-82-807/09/21 10:480.0063 0.0022 1
p-Isopropyltoluene ND mg/kg 07/09/21 19:40 99-87-607/09/21 10:480.0063 0.0031 1
Methylene Chloride ND mg/kg 07/09/21 19:40 75-09-207/09/21 10:480.025 0.017 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 07/09/21 19:40 108-10-107/09/21 10:480.063 0.0061 1
Methyl-tert-butyl ether ND mg/kg 07/09/21 19:40 1634-04-407/09/21 10:480.0063 0.0024 1
Naphthalene ND mg/kg 07/09/21 19:40 91-20-307/09/21 10:480.0063 0.0033 1
n-Propylbenzene ND mg/kg 07/09/21 19:40 103-65-107/09/21 10:480.0063 0.0023 1
Styrene ND mg/kg 07/09/21 19:40 100-42-507/09/21 10:480.0063 0.0017 1
1,1,1,2-Tetrachloroethane ND mg/kg 07/09/21 19:40 630-20-607/09/21 10:480.0063 0.0024 1
1,1,2,2-Tetrachloroethane ND mg/kg 07/09/21 19:40 79-34-507/09/21 10:480.0063 0.0017 1
Tetrachloroethene ND mg/kg 07/09/21 19:40 127-18-407/09/21 10:480.0063 0.0020 1
Toluene ND mg/kg 07/09/21 19:40 108-88-307/09/21 10:480.0063 0.0018 1
1,2,3-Trichlorobenzene ND mg/kg 07/09/21 19:40 87-61-607/09/21 10:480.0063 0.0051 1
1,2,4-Trichlorobenzene ND mg/kg 07/09/21 19:40 120-82-107/09/21 10:480.0063 0.0053 1
1,1,1-Trichloroethane ND mg/kg 07/09/21 19:40 71-55-607/09/21 10:480.0063 0.0033 1
1,1,2-Trichloroethane ND mg/kg 07/09/21 19:40 79-00-507/09/21 10:480.0063 0.0021 1
Trichloroethene ND mg/kg 07/09/21 19:40 79-01-607/09/21 10:480.0063 0.0016 1
Trichlorofluoromethane ND mg/kg 07/09/21 19:40 75-69-407/09/21 10:480.0063 0.0035 1
1,2,3-Trichloropropane ND mg/kg 07/09/21 19:40 96-18-407/09/21 10:480.0063 0.0032 1
1,2,4-Trimethylbenzene ND mg/kg 07/09/21 19:40 95-63-607/09/21 10:480.0063 0.0017 1
1,3,5-Trimethylbenzene ND mg/kg 07/09/21 19:40 108-67-807/09/21 10:480.0063 0.0021 1
Vinyl acetate ND mg/kg 07/09/21 19:40 108-05-407/09/21 10:480.063 0.0046 1
Vinyl chloride ND mg/kg 07/09/21 19:40 75-01-407/09/21 10:480.013 0.0032 1
Xylene (Total)ND mg/kg 07/09/21 19:40 1330-20-707/09/21 10:480.013 0.0036 1
m&p-Xylene ND mg/kg 07/09/21 19:40 179601-23-107/09/21 10:480.013 0.0043 1
o-Xylene ND mg/kg 07/09/21 19:40 95-47-607/09/21 10:480.0063 0.0028 1
Surrogates
Toluene-d8 (S)102 %07/09/21 19:40 2037-26-507/09/21 10:4870-130 1
4-Bromofluorobenzene (S)99 %07/09/21 19:40 460-00-407/09/21 10:4869-134 1
1,2-Dichloroethane-d4 (S)110 %07/09/21 19:40 17060-07-007/09/21 10:4870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.3 %07/19/21 11:27 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 86.1 %07/09/21 11:5407/09/21 11:451
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92547722
Brayton BF
Sample: DUP Lab ID: 92547722003 Collected: 07/02/21 12:10 Received: 07/06/21 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 07/16/21 15:17 18540-29-907/14/21 16:591.16 0.296 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
632238
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92547722001, 92547722002, 92547722003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3321155
Associated Lab Samples:92547722001, 92547722002, 92547722003
Matrix: Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 07/12/21 13:430.0046
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3321156LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0850.083 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3321157MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92547049001
3321158
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg M10.053 74 75-125127 15 200.0540.14 0.18 0.21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
632634
EPA 3050B
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92547722001, 92547722002, 92547722003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3323286
Associated Lab Samples:92547722001, 92547722002, 92547722003
Matrix: Solid
AnalyzedMDL
Arsenic mg/kg ND 2.5 07/12/21 14:170.50
Barium mg/kg ND 1.0 07/12/21 14:170.25
Cadmium mg/kg ND 0.10 07/12/21 14:170.050
Chromium mg/kg ND 0.50 07/12/21 14:170.25
Lead mg/kg ND 1.0 07/12/21 14:170.25
Selenium mg/kg ND 1.0 07/12/21 14:170.50
Silver mg/kg ND 0.50 07/12/21 14:170.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3323287LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 46.250 92 80-120
Barium mg/kg 48.750 97 80-120
Cadmium mg/kg 46.850 94 80-120
Chromium mg/kg 47.650 95 80-120
Lead mg/kg 47.650 95 80-120
Selenium mg/kg 43.650 87 80-120
Silver mg/kg 24.025 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3323288MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92545566001
3323289
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 52.3 96 75-12593 1 2054.2ND 50.2 50.7
Barium mg/kg M1,R152.3 77 75-125181 35 2054.296.7 137 195
Cadmium mg/kg 52.3 95 75-12594 3 2054.20.16 49.9 51.2
Chromium mg/kg 52.3 92 75-12592 3 2054.21.6 50.0 51.3
Lead mg/kg 52.3 98 75-12591 3 2054.21.4 52.5 51.0
Selenium mg/kg 52.3 93 75-12591 1 2054.21.4 49.9 50.6
Silver mg/kg 26.2 95 75-12595 3 2027.1ND 25.0 25.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
632400
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92547722002, 92547722003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3321972
Associated Lab Samples:92547722002, 92547722003
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 07/09/21 13:120.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 07/09/21 13:120.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 07/09/21 13:120.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 07/09/21 13:120.0017
1,1-Dichloroethane mg/kg ND 0.0050 07/09/21 13:120.0021
1,1-Dichloroethene mg/kg ND 0.0050 07/09/21 13:120.0021
1,1-Dichloropropene mg/kg ND 0.0050 07/09/21 13:120.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 07/09/21 13:120.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 07/09/21 13:120.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 07/09/21 13:120.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 07/09/21 13:120.0014
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 07/09/21 13:120.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 07/09/21 13:120.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 07/09/21 13:120.0018
1,2-Dichloroethane mg/kg ND 0.0050 07/09/21 13:120.0033
1,2-Dichloropropane mg/kg ND 0.0050 07/09/21 13:120.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 07/09/21 13:120.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 07/09/21 13:120.0016
1,3-Dichloropropane mg/kg ND 0.0050 07/09/21 13:120.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 07/09/21 13:120.0013
2,2-Dichloropropane mg/kg ND 0.0050 07/09/21 13:120.0016
2-Butanone (MEK)mg/kg ND 0.10 07/09/21 13:120.024
2-Chlorotoluene mg/kg ND 0.0050 07/09/21 13:120.0018
2-Hexanone mg/kg ND 0.050 07/09/21 13:120.0048
4-Chlorotoluene mg/kg ND 0.0050 07/09/21 13:120.00088
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 07/09/21 13:120.0048
Acetone mg/kg ND 0.10 07/09/21 13:120.032
Benzene mg/kg ND 0.0050 07/09/21 13:120.0020
Bromobenzene mg/kg ND 0.0050 07/09/21 13:120.0016
Bromochloromethane mg/kg ND 0.0050 07/09/21 13:120.0015
Bromodichloromethane mg/kg ND 0.0050 07/09/21 13:120.0019
Bromoform mg/kg ND 0.0050 07/09/21 13:120.0018
Bromomethane mg/kg ND 0.010 IK07/09/21 13:120.0079
Carbon tetrachloride mg/kg ND 0.0050 07/09/21 13:120.0019
Chlorobenzene mg/kg ND 0.0050 07/09/21 13:120.00096
Chloroethane mg/kg ND 0.010 07/09/21 13:120.0039
Chloroform mg/kg ND 0.0050 07/09/21 13:120.0030
Chloromethane mg/kg ND 0.010 07/09/21 13:120.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 07/09/21 13:120.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 07/09/21 13:120.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3321972
Associated Lab Samples:92547722002, 92547722003
Matrix: Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 07/09/21 13:120.0028
Dibromomethane mg/kg ND 0.0050 07/09/21 13:120.0011
Dichlorodifluoromethane mg/kg ND 0.010 07/09/21 13:120.0022
Diisopropyl ether mg/kg ND 0.0050 07/09/21 13:120.0014
Ethylbenzene mg/kg ND 0.0050 07/09/21 13:120.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 07/09/21 13:120.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 07/09/21 13:120.0017
m&p-Xylene mg/kg ND 0.010 07/09/21 13:120.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 07/09/21 13:120.0019
Methylene Chloride mg/kg ND 0.020 07/09/21 13:120.014
n-Butylbenzene mg/kg ND 0.0050 07/09/21 13:120.0024
n-Propylbenzene mg/kg ND 0.0050 07/09/21 13:120.0018
Naphthalene mg/kg ND 0.0050 07/09/21 13:120.0026
o-Xylene mg/kg ND 0.0050 07/09/21 13:120.0022
p-Isopropyltoluene mg/kg ND 0.0050 07/09/21 13:120.0025
sec-Butylbenzene mg/kg ND 0.0050 07/09/21 13:120.0022
Styrene mg/kg ND 0.0050 07/09/21 13:120.0013
tert-Butylbenzene mg/kg ND 0.0050 07/09/21 13:120.0018
Tetrachloroethene mg/kg ND 0.0050 07/09/21 13:120.0016
Toluene mg/kg ND 0.0050 07/09/21 13:120.0014
trans-1,2-Dichloroethene mg/kg ND 0.0050 07/09/21 13:120.0018
trans-1,3-Dichloropropene mg/kg ND 0.0050 07/09/21 13:120.0017
Trichloroethene mg/kg ND 0.0050 07/09/21 13:120.0013
Trichlorofluoromethane mg/kg ND 0.0050 07/09/21 13:120.0028
Vinyl acetate mg/kg ND 0.050 07/09/21 13:120.0036
Vinyl chloride mg/kg ND 0.010 07/09/21 13:120.0025
Xylene (Total)mg/kg ND 0.010 07/09/21 13:120.0028
1,2-Dichloroethane-d4 (S)%112 70-130 07/09/21 13:12
4-Bromofluorobenzene (S)%97 69-134 07/09/21 13:12
Toluene-d8 (S)%101 70-130 07/09/21 13:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3321973LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.21.2 92 70-130
1,1,1-Trichloroethane mg/kg 1.11.2 87 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.11.2 88 70-130
1,1,2-Trichloroethane mg/kg 1.11.2 87 70-130
1,1-Dichloroethane mg/kg 1.21.2 100 70-130
1,1-Dichloroethene mg/kg 1.31.2 101 70-130
1,1-Dichloropropene mg/kg 1.21.2 96 70-130
1,2,3-Trichlorobenzene mg/kg 1.21.2 95 65-130
1,2,3-Trichloropropane mg/kg 1.21.2 93 70-130
1,2,4-Trichlorobenzene mg/kg 1.21.2 97 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3321973LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.21.2 93 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.11.2 86 70-130
1,2-Dibromoethane (EDB)mg/kg 1.21.2 94 70-130
1,2-Dichlorobenzene mg/kg 1.11.2 91 70-130
1,2-Dichloroethane mg/kg 1.11.2 90 63-130
1,2-Dichloropropane mg/kg 1.21.2 96 70-130
1,3,5-Trimethylbenzene mg/kg 1.21.2 94 70-130
1,3-Dichlorobenzene mg/kg 1.11.2 92 70-130
1,3-Dichloropropane mg/kg 1.21.2 95 70-130
1,4-Dichlorobenzene mg/kg 1.11.2 91 70-130
2,2-Dichloropropane mg/kg 1.11.2 91 66-130
2-Butanone (MEK)mg/kg 2.42.5 97 70-130
2-Chlorotoluene mg/kg 1.21.2 97 70-130
2-Hexanone mg/kg 2.42.5 96 70-130
4-Chlorotoluene mg/kg 1.11.2 92 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.42.5 95 70-130
Acetone mg/kg 2.52.5 101 69-130
Benzene mg/kg 1.21.2 95 70-130
Bromobenzene mg/kg 1.21.2 95 70-130
Bromochloromethane mg/kg 1.21.2 96 70-130
Bromodichloromethane mg/kg 1.11.2 84 69-130
Bromoform mg/kg 1.11.2 86 70-130
Bromomethane mg/kg 1.4 IK1.2 110 52-130
Carbon tetrachloride mg/kg 1.21.2 95 70-130
Chlorobenzene mg/kg 1.21.2 95 70-130
Chloroethane mg/kg 1.31.2 105 65-130
Chloroform mg/kg 1.31.2 101 70-130
Chloromethane mg/kg 1.21.2 93 55-130
cis-1,2-Dichloroethene mg/kg 1.21.2 96 70-130
cis-1,3-Dichloropropene mg/kg 1.21.2 95 70-130
Dibromochloromethane mg/kg 1.11.2 90 70-130
Dibromomethane mg/kg 1.21.2 92 70-130
Dichlorodifluoromethane mg/kg 1.21.2 100 45-156
Diisopropyl ether mg/kg 1.11.2 90 70-130
Ethylbenzene mg/kg 1.31.2 104 70-130
Hexachloro-1,3-butadiene mg/kg 1.31.2 101 66-130
Isopropylbenzene (Cumene)mg/kg 1.21.2 98 70-130
m&p-Xylene mg/kg 2.42.5 96 70-130
Methyl-tert-butyl ether mg/kg 1.11.2 91 70-130
Methylene Chloride mg/kg 1.31.2 101 65-130
n-Butylbenzene mg/kg 1.31.2 103 67-130
n-Propylbenzene mg/kg 1.21.2 99 70-130
Naphthalene mg/kg 1.11.2 90 70-130
o-Xylene mg/kg 1.21.2 96 70-130
p-Isopropyltoluene mg/kg 1.21.2 96 67-130
sec-Butylbenzene mg/kg 1.21.2 98 69-130
Styrene mg/kg 1.21.2 94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3321973LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.21.2 93 67-130
Tetrachloroethene mg/kg 1.11.2 89 70-130
Toluene mg/kg 1.11.2 91 70-130
trans-1,2-Dichloroethene mg/kg 1.31.2 100 70-130
trans-1,3-Dichloropropene mg/kg 1.21.2 95 68-130
Trichloroethene mg/kg 1.21.2 96 70-130
Trichlorofluoromethane mg/kg 1.21.2 93 70-130
Vinyl acetate mg/kg 2.72.5 106 70-130
Vinyl chloride mg/kg 1.31.2 100 61-130
Xylene (Total)mg/kg 3.63.8 96 70-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%98 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3321974MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92547533001
3321975
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane mg/kg 3.7 88 70-13195 8 303.736.0 Uug/kg 3.2 3.4
1,1,1-Trichloroethane mg/kg 3.7 88 65-13389 1 303.736.0 Uug/kg 3.2 3.2
1,1,2,2-Tetrachloroethane mg/kg 3.7 86 66-13089 3 303.736.0 Uug/kg 3.1 3.2
1,1,2-Trichloroethane mg/kg 3.7 84 66-13388 4 303.736.0 Uug/kg 3.0 3.2
1,1-Dichloroethane mg/kg 3.7 99 65-13099 0 303.736.0 Uug/kg 3.6 3.6
1,1-Dichloroethene mg/kg 3.7 99 10-15899 0 303.736.0 Uug/kg 3.6 3.6
1,1-Dichloropropene mg/kg 3.7 96 68-13395 1 303.736.0 Uug/kg 3.5 3.4
1,2,3-Trichlorobenzene mg/kg 3.7 89 27-13891 2 303.736.0 Uug/kg 3.2 3.3
1,2,3-Trichloropropane mg/kg 3.7 89 67-13092 3 303.736.0 Uug/kg 3.2 3.3
1,2,4-Trichlorobenzene mg/kg 3.7 89 51-13490 1 303.736.0 Uug/kg 3.2 3.2
1,2,4-Trimethylbenzene mg/kg 3.7 89 63-13692 3 303.736.0 Uug/kg 3.2 3.3
1,2-Dibromo-3-chloropropane mg/kg 3.7 77 32-13085 9 303.736.0 Uug/kg 2.8 3.1
1,2-Dibromoethane (EDB) mg/kg 3.7 91 70-13094 4 303.736.0 Uug/kg 3.3 3.4
1,2-Dichlorobenzene mg/kg 3.7 88 69-13090 2 303.736.0 Uug/kg 3.2 3.3
1,2-Dichloroethane mg/kg 3.7 90 59-13091 2 303.736.0 Uug/kg 3.2 3.3
1,2-Dichloropropane mg/kg 3.7 95 70-13097 2 303.736.0 Uug/kg 3.4 3.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3321974MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92547533001
3321975
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,3,5-Trimethylbenzene mg/kg 3.7 89 65-13793 5 303.736.0 Uug/kg 3.2 3.4
1,3-Dichlorobenzene mg/kg 3.7 86 70-13089 4 303.736.0 Uug/kg 3.1 3.2
1,3-Dichloropropane mg/kg 3.7 98 70-130100 2 303.736.0 Uug/kg 3.5 3.6
1,4-Dichlorobenzene mg/kg 3.7 86 68-13089 4 303.736.0 Uug/kg 3.1 3.2
2,2-Dichloropropane mg/kg 3.7 79 32-13078 1 303.736.0 Uug/kg 2.8 2.8
2-Butanone (MEK)mg/kg 7.2 89 10-13691 3 307.2721 Uug/kg 6.4 6.6
2-Chlorotoluene mg/kg 3.7 93 69-14196 3 303.736.0 Uug/kg 3.4 3.5
2-Hexanone mg/kg 7.2 89 10-14492 3 307.2360 Uug/kg 6.4 6.6
4-Chlorotoluene mg/kg 3.7 91 70-13293 2 303.736.0 Uug/kg 3.3 3.3
4-Methyl-2-pentanone(MIBK)mg/kg 7.2 87 25-14390 3 307.2360 Uug/kg 6.3 6.5
Acetone mg/kg 7.2 94 10-13090 5 307.2721 Uug/kg 6.8 6.5
Benzene mg/kg 3.7 93 67-13096 3 303.736.0 Uug/kg 3.4 3.5
Bromobenzene mg/kg 3.7 90 70-13094 4 303.736.0 Uug/kg 3.2 3.4
Bromochloromethane mg/kg 3.7 94 69-13493 1 303.736.0 Uug/kg 3.4 3.3
Bromodichloromethane mg/kg 3.7 79 64-13082 4 303.736.0 Uug/kg 2.8 3.0
Bromoform mg/kg 3.7 78 62-13083 6 303.736.0 Uug/kg 2.8 3.0
Bromomethane mg/kg IK3.7 75 20-17667 12 303.772.1 Uug/kg 2.7 2.4
Carbon tetrachloride mg/kg 3.7 90 65-14092 2 303.736.0 Uug/kg 3.2 3.3
Chlorobenzene mg/kg 3.7 96 70-130100 3 303.736.0 Uug/kg 3.5 3.6
Chloroethane mg/kg 3.7 45 10-13050 11 303.772.1 Uug/kg 1.6 1.8
Chloroform mg/kg 3.7 101 63-130101 1 303.736.0 Uug/kg 3.6 3.6
Chloromethane mg/kg 3.7 94 58-13099 5 303.772.1 Uug/kg 3.4 3.6
cis-1,2-Dichloroethene mg/kg 3.7 95 66-13095 0 303.71420ug/kg 4.8 4.8
cis-1,3-Dichloropropene mg/kg 3.7 92 67-13091 1 303.736.0 Uug/kg 3.3 3.3
Dibromochloromethane mg/kg 3.7 100 67-13090 10 303.736.0 Uug/kg 3.6 3.3
Dibromomethane mg/kg 3.7 89 63-13194 5 303.736.0 Uug/kg 3.2 3.4
Dichlorodifluoromethane mg/kg 3.7 93 44-18099 6 303.772.1 Uug/kg 3.4 3.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3321974MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92547533001
3321975
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Diisopropyl ether mg/kg 3.7 88 63-13089 1 303.736.0 Uug/kg 3.2 3.2
Ethylbenzene mg/kg 3.7 105 66-130107 2 303.736.0 Uug/kg 3.8 3.9
Hexachloro-1,3-butadiene mg/kg 3.7 91 64-15092 1 303.772.1 Uug/kg 3.3 3.3
Isopropylbenzene(Cumene)mg/kg 3.7 100 69-135101 1 303.736.0 Uug/kg 3.6 3.6
m&p-Xylene mg/kg 7.2 98 60-133100 2 307.272.1 Uug/kg 7.1 7.2
Methyl-tert-butyl ether mg/kg 3.7 86 65-13088 2 303.736.0 Uug/kg 3.1 3.2
Methylene Chloride mg/kg 3.7 102 61-130104 2 303.7137Jug/kg 3.8 3.9
n-Butylbenzene mg/kg 3.7 93 65-14095 2 303.736.0 Uug/kg 3.4 3.4
n-Propylbenzene mg/kg 3.7 93 67-14095 2 303.736.0 Uug/kg 3.4 3.4
Naphthalene mg/kg 3.7 86 15-14587 2 303.736.0 Uug/kg 3.1 3.2
o-Xylene mg/kg 3.7 100 66-133100 0 303.736.0 Uug/kg 3.6 3.6
p-Isopropyltoluene mg/kg 3.7 91 56-14794 3 303.736.0 Uug/kg 3.3 3.4
sec-Butylbenzene mg/kg 3.7 93 65-13997 4 303.736.0 Uug/kg 3.4 3.5
Styrene mg/kg 3.7 95 70-13296 1 303.736.0 Uug/kg 3.4 3.5
tert-Butylbenzene mg/kg 3.7 89 62-13593 4 303.736.0 Uug/kg 3.2 3.4
Tetrachloroethene mg/kg 3.7 90 70-13590 0 303.736.0 Uug/kg 3.2 3.2
Toluene mg/kg 3.7 89 67-13092 4 303.736.0 Uug/kg 3.2 3.3
trans-1,2-Dichloroethene mg/kg 3.7 98 69-13098 1 303.736.0 Uug/kg 3.5 3.5
trans-1,3-Dichloropropene mg/kg 3.7 89 62-13089 0 303.736.0 Uug/kg 3.2 3.2
Trichloroethene mg/kg 3.7 97 70-135124 4 303.721200ug/kg 24.7 25.6
Trichlorofluoromethane mg/kg 3.7 71 10-13072 2 303.736.0 Uug/kg 2.5 2.6
Vinyl acetate mg/kg 7.2 96 53-13099 2 307.2360 Uug/kg 6.9 7.1
Vinyl chloride mg/kg 3.7 97 61-148101 4 303.772.1 Uug/kg 3.5 3.7
Xylene (Total)mg/kg 10.8 99 63-132100 1 3010.872.1 Uug/kg 10.7 10.8
1,2-Dichloroethane-d4 (S) %109 70-130103
4-Bromofluorobenzene (S) %103 69-134100
Toluene-d8 (S)%101 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
632736
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92547722001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3323768
Associated Lab Samples:92547722001
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 07/12/21 12:440.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 07/12/21 12:440.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 07/12/21 12:440.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 07/12/21 12:440.0017
1,1-Dichloroethane mg/kg ND 0.0050 07/12/21 12:440.0021
1,1-Dichloroethene mg/kg ND 0.0050 07/12/21 12:440.0021
1,1-Dichloropropene mg/kg ND 0.0050 07/12/21 12:440.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 07/12/21 12:440.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 07/12/21 12:440.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 07/12/21 12:440.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 07/12/21 12:440.0014
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 07/12/21 12:440.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 07/12/21 12:440.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 07/12/21 12:440.0018
1,2-Dichloroethane mg/kg ND 0.0050 07/12/21 12:440.0033
1,2-Dichloropropane mg/kg ND 0.0050 07/12/21 12:440.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 07/12/21 12:440.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 07/12/21 12:440.0016
1,3-Dichloropropane mg/kg ND 0.0050 07/12/21 12:440.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 07/12/21 12:440.0013
2,2-Dichloropropane mg/kg ND 0.0050 07/12/21 12:440.0016
2-Butanone (MEK)mg/kg ND 0.10 07/12/21 12:440.024
2-Chlorotoluene mg/kg ND 0.0050 07/12/21 12:440.0018
2-Hexanone mg/kg ND 0.050 07/12/21 12:440.0048
4-Chlorotoluene mg/kg ND 0.0050 07/12/21 12:440.00088
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 07/12/21 12:440.0048
Acetone mg/kg ND 0.10 07/12/21 12:440.032
Benzene mg/kg ND 0.0050 07/12/21 12:440.0020
Bromobenzene mg/kg ND 0.0050 07/12/21 12:440.0016
Bromochloromethane mg/kg ND 0.0050 07/12/21 12:440.0015
Bromodichloromethane mg/kg ND 0.0050 07/12/21 12:440.0019
Bromoform mg/kg ND 0.0050 07/12/21 12:440.0018
Bromomethane mg/kg ND 0.010 IK07/12/21 12:440.0079
Carbon tetrachloride mg/kg ND 0.0050 07/12/21 12:440.0019
Chlorobenzene mg/kg ND 0.0050 07/12/21 12:440.00096
Chloroethane mg/kg ND 0.010 07/12/21 12:440.0039
Chloroform mg/kg ND 0.0050 07/12/21 12:440.0030
Chloromethane mg/kg ND 0.010 07/12/21 12:440.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 07/12/21 12:440.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 07/12/21 12:440.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3323768
Associated Lab Samples:92547722001
Matrix: Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 07/12/21 12:440.0028
Dibromomethane mg/kg ND 0.0050 07/12/21 12:440.0011
Dichlorodifluoromethane mg/kg ND 0.010 07/12/21 12:440.0022
Diisopropyl ether mg/kg ND 0.0050 07/12/21 12:440.0014
Ethylbenzene mg/kg ND 0.0050 07/12/21 12:440.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 07/12/21 12:440.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 07/12/21 12:440.0017
m&p-Xylene mg/kg ND 0.010 07/12/21 12:440.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 07/12/21 12:440.0019
Methylene Chloride mg/kg ND 0.020 07/12/21 12:440.014
n-Butylbenzene mg/kg ND 0.0050 07/12/21 12:440.0024
n-Propylbenzene mg/kg ND 0.0050 07/12/21 12:440.0018
Naphthalene mg/kg ND 0.0050 07/12/21 12:440.0026
o-Xylene mg/kg ND 0.0050 07/12/21 12:440.0022
p-Isopropyltoluene mg/kg ND 0.0050 07/12/21 12:440.0025
sec-Butylbenzene mg/kg ND 0.0050 07/12/21 12:440.0022
Styrene mg/kg ND 0.0050 07/12/21 12:440.0013
tert-Butylbenzene mg/kg ND 0.0050 07/12/21 12:440.0018
Tetrachloroethene mg/kg ND 0.0050 07/12/21 12:440.0016
Toluene mg/kg ND 0.0050 07/12/21 12:440.0014
trans-1,2-Dichloroethene mg/kg ND 0.0050 07/12/21 12:440.0018
trans-1,3-Dichloropropene mg/kg ND 0.0050 07/12/21 12:440.0017
Trichloroethene mg/kg ND 0.0050 07/12/21 12:440.0013
Trichlorofluoromethane mg/kg ND 0.0050 07/12/21 12:440.0028
Vinyl acetate mg/kg ND 0.050 07/12/21 12:440.0036
Vinyl chloride mg/kg ND 0.010 07/12/21 12:440.0025
Xylene (Total)mg/kg ND 0.010 07/12/21 12:440.0028
1,2-Dichloroethane-d4 (S)%114 70-130 07/12/21 12:44
4-Bromofluorobenzene (S)%98 69-134 07/12/21 12:44
Toluene-d8 (S)%101 70-130 07/12/21 12:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3323769LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.11.2 89 70-130
1,1,1-Trichloroethane mg/kg 1.01.2 81 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.01.2 81 70-130
1,1,2-Trichloroethane mg/kg 1.01.2 82 70-130
1,1-Dichloroethane mg/kg 1.11.2 90 70-130
1,1-Dichloroethene mg/kg 1.11.2 89 70-130
1,1-Dichloropropene mg/kg 1.11.2 88 70-130
1,2,3-Trichlorobenzene mg/kg 1.11.2 91 65-130
1,2,3-Trichloropropane mg/kg 1.11.2 85 70-130
1,2,4-Trichlorobenzene mg/kg 1.11.2 91 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3323769LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.11.2 88 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.01.2 83 70-130
1,2-Dibromoethane (EDB)mg/kg 1.11.2 88 70-130
1,2-Dichlorobenzene mg/kg 1.11.2 87 70-130
1,2-Dichloroethane mg/kg 1.01.2 83 63-130
1,2-Dichloropropane mg/kg 1.11.2 88 70-130
1,3,5-Trimethylbenzene mg/kg 1.11.2 89 70-130
1,3-Dichlorobenzene mg/kg 1.11.2 86 70-130
1,3-Dichloropropane mg/kg 1.11.2 89 70-130
1,4-Dichlorobenzene mg/kg 1.11.2 88 70-130
2,2-Dichloropropane mg/kg 1.01.2 83 66-130
2-Butanone (MEK)mg/kg 2.12.5 85 70-130
2-Chlorotoluene mg/kg 1.11.2 92 70-130
2-Hexanone mg/kg 2.12.5 85 70-130
4-Chlorotoluene mg/kg 1.11.2 86 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.12.5 85 70-130
Acetone mg/kg 2.22.5 87 69-130
Benzene mg/kg 1.11.2 88 70-130
Bromobenzene mg/kg 1.21.2 93 70-130
Bromochloromethane mg/kg 1.21.2 92 70-130
Bromodichloromethane mg/kg 1.01.2 80 69-130
Bromoform mg/kg 1.11.2 87 70-130
Bromomethane mg/kg 1.2 IK1.2 99 52-130
Carbon tetrachloride mg/kg 1.11.2 91 70-130
Chlorobenzene mg/kg 1.11.2 90 70-130
Chloroethane mg/kg 1.21.2 93 65-130
Chloroform mg/kg 1.21.2 95 70-130
Chloromethane mg/kg 1.01.2 84 55-130
cis-1,2-Dichloroethene mg/kg 1.11.2 87 70-130
cis-1,3-Dichloropropene mg/kg 1.11.2 89 70-130
Dibromochloromethane mg/kg 1.11.2 89 70-130
Dibromomethane mg/kg 1.11.2 92 70-130
Dichlorodifluoromethane mg/kg 1.11.2 89 45-156
Diisopropyl ether mg/kg 1.01.2 81 70-130
Ethylbenzene mg/kg 1.21.2 96 70-130
Hexachloro-1,3-butadiene mg/kg 1.21.2 95 66-130
Isopropylbenzene (Cumene)mg/kg 1.11.2 91 70-130
m&p-Xylene mg/kg 2.22.5 89 70-130
Methyl-tert-butyl ether mg/kg 1.11.2 85 70-130
Methylene Chloride mg/kg 1.11.2 92 65-130
n-Butylbenzene mg/kg 1.21.2 93 67-130
n-Propylbenzene mg/kg 1.21.2 92 70-130
Naphthalene mg/kg 1.11.2 86 70-130
o-Xylene mg/kg 1.11.2 90 70-130
p-Isopropyltoluene mg/kg 1.11.2 91 67-130
sec-Butylbenzene mg/kg 1.11.2 90 69-130
Styrene mg/kg 1.11.2 89 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3323769LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.11.2 86 67-130
Tetrachloroethene mg/kg 1.11.2 84 70-130
Toluene mg/kg 1.11.2 85 70-130
trans-1,2-Dichloroethene mg/kg 1.11.2 90 70-130
trans-1,3-Dichloropropene mg/kg 1.11.2 89 68-130
Trichloroethene mg/kg 1.11.2 90 70-130
Trichlorofluoromethane mg/kg 1.11.2 85 70-130
Vinyl acetate mg/kg 2.42.5 96 70-130
Vinyl chloride mg/kg 1.11.2 89 61-130
Xylene (Total)mg/kg 3.43.8 89 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%95 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3323770MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92547652003
3323771
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane mg/kg 6.9 103 70-13189 15 306.9ND 7.1 6.1
1,1,1-Trichloroethane mg/kg 6.9 103 65-13389 14 306.9ND 7.1 6.1
1,1,2,2-Tetrachloroethane mg/kg 6.9 96 66-13083 14 306.9ND 6.6 5.8
1,1,2-Trichloroethane mg/kg 6.9 93 66-13381 14 306.9ND 6.4 5.6
1,1-Dichloroethane mg/kg 6.9 113 65-13096 16 306.9ND 7.8 6.7
1,1-Dichloroethene mg/kg 6.9 116 10-15899 16 306.9ND 8.0 6.8
1,1-Dichloropropene mg/kg 6.9 113 68-13397 16 306.9ND 7.8 6.7
1,2,3-Trichlorobenzene mg/kg 6.9 97 27-13884 14 306.9ND 6.7 5.8
1,2,3-Trichloropropane mg/kg 6.9 100 67-13085 16 306.9ND 6.9 5.9
1,2,4-Trichlorobenzene mg/kg 6.9 99 51-13483 17 306.9ND 6.8 5.8
1,2,4-Trimethylbenzene mg/kg 6.9 100 63-13685 15 306.90.13 7.0 6.0
1,2-Dibromo-3-chloropropane mg/kg 6.9 89 32-13078 13 306.9ND 6.2 5.4
1,2-Dibromoethane (EDB) mg/kg 6.9 102 70-13087 15 306.9ND 7.0 6.0
1,2-Dichlorobenzene mg/kg 6.9 99 69-13086 14 306.9ND 6.8 5.9
1,2-Dichloroethane mg/kg 6.9 105 59-13089 17 306.9ND 7.2 6.1
1,2-Dichloropropane mg/kg 6.9 106 70-13091 15 306.9ND 7.3 6.3
1,3,5-Trimethylbenzene mg/kg 6.9 102 65-13785 18 306.9ND 7.0 5.9
1,3-Dichlorobenzene mg/kg 6.9 101 70-13083 19 306.9ND 6.9 5.8
1,3-Dichloropropane mg/kg 6.9 106 70-13090 17 306.9ND 7.3 6.2
1,4-Dichlorobenzene mg/kg 6.9 100 68-13085 16 306.9ND 6.9 5.8
2,2-Dichloropropane mg/kg 6.9 94 32-13080 16 306.9ND 6.5 5.5
2-Butanone (MEK)mg/kg 13.8 103 10-13690 14 3013.8ND 14.2 12.4
2-Chlorotoluene mg/kg 6.9 106 69-14189 17 306.9ND 7.3 6.2
2-Hexanone mg/kg 13.8 101 10-14487 15 3013.8ND 14.0 12.1
4-Chlorotoluene mg/kg 6.9 100 70-13285 17 306.9ND 6.9 5.84-Methyl-2-pentanone(MIBK)mg/kg 13.8 99 25-14386 14 3013.8ND 13.6 11.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3323770MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92547652003
3323771
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acetone mg/kg 13.8 113 10-13094 18 3013.8ND 15.6 13.0
Benzene mg/kg 6.9 107 67-13091 16 306.90.11 7.5 6.4
Bromobenzene mg/kg 6.9 105 70-13088 18 306.9ND 7.3 6.1
Bromochloromethane mg/kg 6.9 112 69-13494 17 306.9ND 7.7 6.5
Bromodichloromethane mg/kg 6.9 91 64-13079 15 306.9ND 6.3 5.4
Bromoform mg/kg 6.9 91 62-13079 14 306.9ND 6.3 5.5
Bromomethane mg/kg IK,R16.9 114 20-17683 31 306.9ND 7.9 5.7
Carbon tetrachloride mg/kg 6.9 105 65-14091 15 306.9ND 7.2 6.3
Chlorobenzene mg/kg 6.9 109 70-13092 17 306.9ND 7.5 6.3
Chloroethane mg/kg M16.9 131 10-130109 19 306.9ND 9.1 7.5
Chloroform mg/kg 6.9 117 63-130101 15 306.9ND 8.1 6.9
Chloromethane mg/kg 6.9 113 58-13096 17 306.9ND 7.8 6.6
cis-1,2-Dichloroethene mg/kg 6.9 110 66-13093 17 306.9ND 7.6 6.4
cis-1,3-Dichloropropene mg/kg 6.9 99 67-13086 14 306.9ND 6.8 5.9
Dibromochloromethane mg/kg 6.9 96 67-13083 14 306.9ND 6.6 5.7
Dibromomethane mg/kg 6.9 103 63-13190 13 306.9ND 7.1 6.2
Dichlorodifluoromethane mg/kg 6.9 119 44-18098 19 306.9ND 8.2 6.8
Diisopropyl ether mg/kg 6.9 101 63-13084 18 306.90.040J 7.0 5.9
Ethylbenzene mg/kg 6.9 118 66-130101 16 306.9ND 8.1 6.9
Hexachloro-1,3-butadiene mg/kg 6.9 101 64-15087 14 306.9ND 7.0 6.0
Isopropylbenzene(Cumene)mg/kg 6.9 110 69-13594 16 306.9ND 7.6 6.5
m&p-Xylene mg/kg 13.8 109 60-13392 16 3013.80.18 15.2 12.9
Methyl-tert-butyl ether mg/kg 6.9 111 65-13079 6 306.929.3 37.0 34.7
Methylene Chloride mg/kg 6.9 116 61-13095 18 306.90.56 8.6 7.1
n-Butylbenzene mg/kg 6.9 104 65-14089 16 306.9ND 7.2 6.1
n-Propylbenzene mg/kg 6.9 108 67-14090 18 306.9ND 7.4 6.2
Naphthalene mg/kg 6.9 94 15-14581 15 306.9ND 6.5 5.6
o-Xylene mg/kg 6.9 108 66-13393 15 306.90.035J 7.5 6.5
p-Isopropyltoluene mg/kg 6.9 102 56-14787 16 306.9ND 7.1 6.0
sec-Butylbenzene mg/kg 6.9 104 65-13989 16 306.9ND 7.2 6.1
Styrene mg/kg 6.9 104 70-13288 17 306.9ND 7.2 6.1
tert-Butylbenzene mg/kg 6.9 102 62-13587 16 306.9ND 7.0 6.0
Tetrachloroethene mg/kg 6.9 102 70-13586 17 306.9ND 7.0 5.9
Toluene mg/kg 6.9 103 67-13088 16 306.90.042J 7.2 6.1
trans-1,2-Dichloroethene mg/kg 6.9 115 69-13096 18 306.9ND 8.0 6.6
trans-1,3-Dichloropropene mg/kg 6.9 98 62-13085 15 306.9ND 6.8 5.9
Trichloroethene mg/kg 6.9 109 70-13594 15 306.9ND 7.5 6.5
Trichlorofluoromethane mg/kg 6.9 112 10-13095 16 306.9ND 7.7 6.6
Vinyl acetate mg/kg 13.8 112 53-13095 17 3013.8ND 15.5 13.1
Vinyl chloride mg/kg 6.9 116 61-14899 16 306.9ND 8.0 6.8
Xylene (Total)mg/kg 20.7 109 63-13293 16 3020.70.21 22.8 19.4
1,2-Dichloroethane-d4 (S) %108 70-130110
4-Bromofluorobenzene (S) %99 69-134100
Toluene-d8 (S)%101 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
631600
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92547722001, 92547722002, 92547722003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3318114
Associated Lab Samples:92547722001, 92547722002, 92547722003
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.33 07/07/21 07:100.13
1,2-Dichlorobenzene mg/kg ND 0.33 07/07/21 07:100.12
1,3-Dichlorobenzene mg/kg ND 0.33 07/07/21 07:100.12
1,4-Dichlorobenzene mg/kg ND 0.33 07/07/21 07:100.13
1-Methylnaphthalene mg/kg ND 0.33 07/07/21 07:100.12
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 07/07/21 07:100.16
2,4,5-Trichlorophenol mg/kg ND 0.33 07/07/21 07:100.15
2,4,6-Trichlorophenol mg/kg ND 0.33 07/07/21 07:100.14
2,4-Dichlorophenol mg/kg ND 0.33 07/07/21 07:100.13
2,4-Dimethylphenol mg/kg ND 0.33 07/07/21 07:100.14
2,4-Dinitrophenol mg/kg ND 1.7 07/07/21 07:101.0
2,4-Dinitrotoluene mg/kg ND 0.33 07/07/21 07:100.13
2,6-Dinitrotoluene mg/kg ND 0.33 07/07/21 07:100.12
2-Chloronaphthalene mg/kg ND 0.33 07/07/21 07:100.13
2-Chlorophenol mg/kg ND 0.33 07/07/21 07:100.12
2-Methylnaphthalene mg/kg ND 0.33 07/07/21 07:100.13
2-Methylphenol(o-Cresol)mg/kg ND 0.33 07/07/21 07:100.14
2-Nitroaniline mg/kg ND 1.7 07/07/21 07:100.27
2-Nitrophenol mg/kg ND 0.33 07/07/21 07:100.14
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 07/07/21 07:100.13
3,3'-Dichlorobenzidine mg/kg ND 0.66 IL07/07/21 07:100.22
3-Nitroaniline mg/kg ND 1.7 IL07/07/21 07:100.26
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 07/07/21 07:100.31
4-Bromophenylphenyl ether mg/kg ND 0.33 07/07/21 07:100.13
4-Chloro-3-methylphenol mg/kg ND 0.66 07/07/21 07:100.23
4-Chloroaniline mg/kg ND 0.66 07/07/21 07:100.26
4-Chlorophenylphenyl ether mg/kg ND 0.33 07/07/21 07:100.12
4-Nitroaniline mg/kg ND 0.66 07/07/21 07:100.25
4-Nitrophenol mg/kg ND 1.7 07/07/21 07:100.64
Acenaphthene mg/kg ND 0.33 07/07/21 07:100.12
Acenaphthylene mg/kg ND 0.33 07/07/21 07:100.12
Aniline mg/kg ND 0.33 07/07/21 07:100.13
Anthracene mg/kg ND 0.33 07/07/21 07:100.11
Benzo(a)anthracene mg/kg ND 0.33 07/07/21 07:100.11
Benzo(a)pyrene mg/kg ND 0.33 07/07/21 07:100.11
Benzo(b)fluoranthene mg/kg ND 0.33 07/07/21 07:100.11
Benzo(g,h,i)perylene mg/kg ND 0.33 07/07/21 07:100.13
Benzo(k)fluoranthene mg/kg ND 0.33 07/07/21 07:100.12
Benzoic Acid mg/kg ND 1.7 07/07/21 07:100.71
Benzyl alcohol mg/kg ND 0.66 07/07/21 07:100.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3318114
Associated Lab Samples:92547722001, 92547722002, 92547722003
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane mg/kg ND 0.33 07/07/21 07:100.14
bis(2-Chloroethyl) ether mg/kg ND 0.33 07/07/21 07:100.12
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 07/07/21 07:100.13
Butylbenzylphthalate mg/kg ND 0.33 07/07/21 07:100.14
Chrysene mg/kg ND 0.33 07/07/21 07:100.12
Di-n-butylphthalate mg/kg ND 0.33 07/07/21 07:100.11
Di-n-octylphthalate mg/kg ND 0.33 07/07/21 07:100.13
Dibenz(a,h)anthracene mg/kg ND 0.33 07/07/21 07:100.13
Dibenzofuran mg/kg ND 0.33 07/07/21 07:100.12
Diethylphthalate mg/kg ND 0.33 07/07/21 07:100.12
Dimethylphthalate mg/kg ND 0.33 07/07/21 07:100.12
Fluoranthene mg/kg ND 0.33 07/07/21 07:100.11
Fluorene mg/kg ND 0.33 07/07/21 07:100.12
Hexachloro-1,3-butadiene mg/kg ND 0.33 07/07/21 07:100.14
Hexachlorobenzene mg/kg ND 0.33 07/07/21 07:100.13
Hexachlorocyclopentadiene mg/kg ND 0.33 v207/07/21 07:100.19
Hexachloroethane mg/kg ND 0.33 07/07/21 07:100.13
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 07/07/21 07:100.13
Isophorone mg/kg ND 0.33 07/07/21 07:100.15
N-Nitroso-di-n-propylamine mg/kg ND 0.33 07/07/21 07:100.12
N-Nitrosodimethylamine mg/kg ND 0.33 07/07/21 07:100.11
N-Nitrosodiphenylamine mg/kg ND 0.33 07/07/21 07:100.12
Naphthalene mg/kg ND 0.33 07/07/21 07:100.11
Nitrobenzene mg/kg ND 0.33 07/07/21 07:100.15
Pentachlorophenol mg/kg ND 0.66 07/07/21 07:100.32
Phenanthrene mg/kg ND 0.33 07/07/21 07:100.11
Phenol mg/kg ND 0.33 07/07/21 07:100.15
Pyrene mg/kg ND 0.33 07/07/21 07:100.13
Pyridine mg/kg ND 0.33 07/07/21 07:100.10
2,4,6-Tribromophenol (S)%81 18-130 07/07/21 07:10
2-Fluorobiphenyl (S)%57 19-130 07/07/21 07:10
2-Fluorophenol (S)%61 18-130 07/07/21 07:10
Nitrobenzene-d5 (S)%53 21-130 07/07/21 07:10
Phenol-d6 (S)%57 18-130 07/07/21 07:10
Terphenyl-d14 (S)%73 15-130 07/07/21 07:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3318115LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.11.7 67 47-130
1,2-Dichlorobenzene mg/kg 1.11.7 65 49-130
1,3-Dichlorobenzene mg/kg 1.11.7 65 48-130
1,4-Dichlorobenzene mg/kg 1.11.7 67 49-130
1-Methylnaphthalene mg/kg 1.11.7 69 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3318115LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 0.971.7 59 38-130
2,4,5-Trichlorophenol mg/kg 1.21.7 72 49-130
2,4,6-Trichlorophenol mg/kg 1.21.7 72 50-130
2,4-Dichlorophenol mg/kg 1.21.7 73 51-130
2,4-Dimethylphenol mg/kg 1.11.7 68 53-130
2,4-Dinitrophenol mg/kg 6.78.3 80 39-130
2,4-Dinitrotoluene mg/kg 1.21.7 73 53-130
2,6-Dinitrotoluene mg/kg 1.21.7 74 55-130
2-Chloronaphthalene mg/kg 1.11.7 67 48-130
2-Chlorophenol mg/kg 1.11.7 69 54-130
2-Methylnaphthalene mg/kg 1.21.7 71 57-130
2-Methylphenol(o-Cresol)mg/kg 1.11.7 66 50-130
2-Nitroaniline mg/kg 1.83.3 56 49-130
2-Nitrophenol mg/kg 1.31.7 78 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.01.7 63 50-130
3,3'-Dichlorobenzidine mg/kg 2.3 IL3.3 70 47-130
3-Nitroaniline mg/kg 2.2 IL3.3 66 45-130
4,6-Dinitro-2-methylphenol mg/kg 2.83.3 85 50-142
4-Bromophenylphenyl ether mg/kg 1.31.7 78 55-130
4-Chloro-3-methylphenol mg/kg 2.23.3 66 52-130
4-Chloroaniline mg/kg 2.23.3 65 49-130
4-Chlorophenylphenyl ether mg/kg 1.21.7 72 53-130
4-Nitroaniline mg/kg 2.23.3 65 51-130
4-Nitrophenol mg/kg 5.98.3 71 40-130
Acenaphthene mg/kg 1.21.7 72 56-130
Acenaphthylene mg/kg 1.21.7 71 58-130
Aniline mg/kg 1.01.7 61 44-130
Anthracene mg/kg 1.21.7 71 60-130
Benzo(a)anthracene mg/kg 1.21.7 71 59-130
Benzo(a)pyrene mg/kg 1.21.7 74 57-130
Benzo(b)fluoranthene mg/kg 1.21.7 73 54-130
Benzo(g,h,i)perylene mg/kg 1.31.7 77 59-130
Benzo(k)fluoranthene mg/kg 1.31.7 76 54-130
Benzoic Acid mg/kg 5.48.3 65 19-130
Benzyl alcohol mg/kg 2.13.3 63 50-130
bis(2-Chloroethoxy)methane mg/kg 1.11.7 65 55-130
bis(2-Chloroethyl) ether mg/kg 1.11.7 67 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.11.7 68 58-130
Butylbenzylphthalate mg/kg 1.21.7 70 46-138
Chrysene mg/kg 1.21.7 72 57-130
Di-n-butylphthalate mg/kg 1.21.7 73 57-130
Di-n-octylphthalate mg/kg 1.21.7 71 57-130
Dibenz(a,h)anthracene mg/kg 1.31.7 81 60-130
Dibenzofuran mg/kg 1.21.7 70 54-130
Diethylphthalate mg/kg 1.21.7 72 55-130
Dimethylphthalate mg/kg 1.21.7 72 57-130
Fluoranthene mg/kg 1.21.7 73 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3318115LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.21.7 72 56-130
Hexachloro-1,3-butadiene mg/kg 1.11.7 69 41-130
Hexachlorobenzene mg/kg 1.41.7 84 53-130
Hexachlorocyclopentadiene mg/kg 0.84 v31.7 51 23-130
Hexachloroethane mg/kg 1.01.7 63 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.31.7 81 61-130
Isophorone mg/kg 1.01.7 61 49-130
N-Nitroso-di-n-propylamine mg/kg 0.971.7 58 52-130
N-Nitrosodimethylamine mg/kg 1.21.7 73 45-130
N-Nitrosodiphenylamine mg/kg 1.21.7 73 56-130
Naphthalene mg/kg 1.21.7 70 56-130
Nitrobenzene mg/kg 0.981.7 59 50-130
Pentachlorophenol mg/kg 2.93.3 87 33-130
Phenanthrene mg/kg 1.21.7 72 60-130
Phenol mg/kg 1.11.7 69 54-130
Pyrene mg/kg 1.11.7 69 61-130
Pyridine mg/kg 0.961.7 58 35-130
2,4,6-Tribromophenol (S)%97 18-130
2-Fluorobiphenyl (S)%66 19-130
2-Fluorophenol (S)%66 18-130
Nitrobenzene-d5 (S)%59 21-130
Phenol-d6 (S)%63 18-130
Terphenyl-d14 (S)%73 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3318116MATRIX SPIKE SAMPLE:
MSSpike
Result
92547630007
1,2,4-Trichlorobenzene mg/kg 1.32.1 62 22-130ND
1,2-Dichlorobenzene mg/kg 1.32.1 61 23-130ND
1,3-Dichlorobenzene mg/kg 1.32.1 62 26-130ND
1,4-Dichlorobenzene mg/kg 1.32.1 63 27-130ND
1-Methylnaphthalene mg/kg 1.32.1 66 30-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.12.1 55 30-130ND
2,4,5-Trichlorophenol mg/kg 1.42.1 70 26-130ND
2,4,6-Trichlorophenol mg/kg 1.42.1 70 23-130ND
2,4-Dichlorophenol mg/kg 1.52.1 71 29-130ND
2,4-Dimethylphenol mg/kg 1.32.1 65 13-130ND
2,4-Dinitrophenol mg/kg 8.010.2 78 10-131ND
2,4-Dinitrotoluene mg/kg 1.42.1 70 28-130ND
2,6-Dinitrotoluene mg/kg 1.42.1 71 36-130ND
2-Chloronaphthalene mg/kg 1.32.1 64 27-130ND
2-Chlorophenol mg/kg 1.42.1 67 29-130ND
2-Methylnaphthalene mg/kg 1.32.1 66 29-130ND
2-Methylphenol(o-Cresol)mg/kg 1.32.1 63 20-130ND
2-Nitroaniline mg/kg 2.24.1 54 29-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
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Page 37 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3318116MATRIX SPIKE SAMPLE:
MSSpike
Result
92547630007
2-Nitrophenol mg/kg 1.52.1 74 26-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.22.1 59 10-176ND
3,3'-Dichlorobenzidine mg/kg 2.8 IL4.1 68 15-130ND
3-Nitroaniline mg/kg 2.6 IL4.1 64 28-130ND
4,6-Dinitro-2-methylphenol mg/kg 3.44.1 82 15-132ND
4-Bromophenylphenyl ether mg/kg 1.52.1 75 35-130ND
4-Chloro-3-methylphenol mg/kg 2.64.1 63 30-130ND
4-Chloroaniline mg/kg 2.54.1 61 28-130ND
4-Chlorophenylphenyl ether mg/kg 1.42.1 68 32-130ND
4-Nitroaniline mg/kg 2.64.1 64 30-130ND
4-Nitrophenol mg/kg 7.210.2 71 17-130ND
Acenaphthene mg/kg 1.42.1 68 29-130ND
Acenaphthylene mg/kg 1.42.1 68 31-130ND
Aniline mg/kg 1.22.1 57 10-130ND
Anthracene mg/kg 1.42.1 67 33-130ND
Benzo(a)anthracene mg/kg 1.42.1 67 32-130ND
Benzo(a)pyrene mg/kg 1.42.1 71 32-130ND
Benzo(b)fluoranthene mg/kg 1.42.1 69 33-130ND
Benzo(g,h,i)perylene mg/kg 1.62.1 76 28-130ND
Benzo(k)fluoranthene mg/kg 1.42.1 70 31-130ND
Benzoic Acid mg/kg 6.110.2 60 10-130ND
Benzyl alcohol mg/kg 2.54.1 62 31-130ND
bis(2-Chloroethoxy)methane mg/kg 1.22.1 59 30-130ND
bis(2-Chloroethyl) ether mg/kg 1.3 M12.1 63 68-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.22.1 59 40-130ND
Butylbenzylphthalate mg/kg 1.32.1 63 40-130ND
Chrysene mg/kg 1.32.1 65 30-130ND
Di-n-butylphthalate mg/kg 1.42.1 68 41-130ND
Di-n-octylphthalate mg/kg 1.42.1 67 42-130ND
Dibenz(a,h)anthracene mg/kg 1.62.1 77 27-130ND
Dibenzofuran mg/kg 1.32.1 66 32-130ND
Diethylphthalate mg/kg 1.42.1 68 40-130ND
Dimethylphthalate mg/kg 1.42.1 69 37-130ND
Fluoranthene mg/kg 1.42.1 70 26-130ND
Fluorene mg/kg 1.42.1 68 31-130ND
Hexachloro-1,3-butadiene mg/kg 1.42.1 66 20-130ND
Hexachlorobenzene mg/kg 1.72.1 82 29-130ND
Hexachlorocyclopentadiene mg/kg 1.0 v32.1 51 10-130ND
Hexachloroethane mg/kg 1.22.1 59 21-130ND
Indeno(1,2,3-cd)pyrene mg/kg 1.62.1 78 28-130ND
Isophorone mg/kg 1.22.1 57 32-130ND
N-Nitroso-di-n-propylamine mg/kg 1.12.1 54 31-130ND
N-Nitrosodimethylamine mg/kg 1.32.1 62 20-130ND
N-Nitrosodiphenylamine mg/kg 1.42.1 69 32-130ND
Naphthalene mg/kg 1.32.1 65 30-130ND
Nitrobenzene mg/kg 1.12.1 55 25-130ND
Pentachlorophenol mg/kg 3.54.1 85 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
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Page 38 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3318116MATRIX SPIKE SAMPLE:
MSSpike
Result
92547630007
Phenanthrene mg/kg 1.42.1 68 34-130ND
Phenol mg/kg 1.42.1 68 14-130ND
Pyrene mg/kg 1.32.1 63 31-130ND
Pyridine mg/kg 0.872.1 43 10-130ND
2,4,6-Tribromophenol (S)%80 18-130
2-Fluorobiphenyl (S)%53 19-130
2-Fluorophenol (S)%60 18-130
Nitrobenzene-d5 (S)%50 21-130
Phenol-d6 (S)%58 18-130
Terphenyl-d14 (S)%51 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92547648001
3318117SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
1-Methylnaphthalene mg/kg ND 30ND
2,2'-Oxybis(1-chloropropane)mg/kg ND 30ND
2,4,5-Trichlorophenol mg/kg ND 30ND
2,4,6-Trichlorophenol mg/kg ND 30ND
2,4-Dichlorophenol mg/kg ND 30ND
2,4-Dimethylphenol mg/kg ND 30ND
2,4-Dinitrophenol mg/kg ND 30ND
2,4-Dinitrotoluene mg/kg ND 30ND
2,6-Dinitrotoluene mg/kg ND 30ND
2-Chloronaphthalene mg/kg ND 30ND
2-Chlorophenol mg/kg ND 30ND
2-Methylnaphthalene mg/kg ND 30ND
2-Methylphenol(o-Cresol)mg/kg ND 30ND
2-Nitroaniline mg/kg ND 30ND
2-Nitrophenol mg/kg ND 30ND
3&4-Methylphenol(m&p Cresol)mg/kg ND 30ND
3,3'-Dichlorobenzidine mg/kg ND IL30ND
3-Nitroaniline mg/kg ND IL30ND
4,6-Dinitro-2-methylphenol mg/kg ND 30ND
4-Bromophenylphenyl ether mg/kg ND 30ND
4-Chloro-3-methylphenol mg/kg ND 30ND
4-Chloroaniline mg/kg ND 30ND
4-Chlorophenylphenyl ether mg/kg ND 30ND
4-Nitroaniline mg/kg ND 30ND
4-Nitrophenol mg/kg ND 30ND
Acenaphthene mg/kg ND 30ND
Acenaphthylene mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 39 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92547648001
3318117SAMPLE DUPLICATE:
Aniline mg/kg ND 30ND
Anthracene mg/kg ND 30ND
Benzo(a)anthracene mg/kg ND 30ND
Benzo(a)pyrene mg/kg ND 30ND
Benzo(b)fluoranthene mg/kg ND 30ND
Benzo(g,h,i)perylene mg/kg ND 30ND
Benzo(k)fluoranthene mg/kg ND 30ND
Benzoic Acid mg/kg ND 30ND
Benzyl alcohol mg/kg ND 30ND
bis(2-Chloroethoxy)methane mg/kg ND 30ND
bis(2-Chloroethyl) ether mg/kg ND 30ND
bis(2-Ethylhexyl)phthalate mg/kg ND 30ND
Butylbenzylphthalate mg/kg ND 30ND
Chrysene mg/kg ND 30ND
Di-n-butylphthalate mg/kg ND 30ND
Di-n-octylphthalate mg/kg ND 30ND
Dibenz(a,h)anthracene mg/kg ND 30ND
Dibenzofuran mg/kg ND 30ND
Diethylphthalate mg/kg ND 30ND
Dimethylphthalate mg/kg ND 30ND
Fluoranthene mg/kg ND 30ND
Fluorene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Hexachlorobenzene mg/kg ND 30ND
Hexachlorocyclopentadiene mg/kg ND v230ND
Hexachloroethane mg/kg ND 30ND
Indeno(1,2,3-cd)pyrene mg/kg ND 30ND
Isophorone mg/kg ND 30ND
N-Nitroso-di-n-propylamine mg/kg ND 30ND
N-Nitrosodimethylamine mg/kg ND 30ND
N-Nitrosodiphenylamine mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
Nitrobenzene mg/kg ND 30ND
Pentachlorophenol mg/kg ND 30ND
Phenanthrene mg/kg ND 30ND
Phenol mg/kg ND 30ND
Pyrene mg/kg ND 30ND
Pyridine mg/kg ND 30ND
2,4,6-Tribromophenol (S)%8581
2-Fluorobiphenyl (S)%5348
2-Fluorophenol (S)%5553
Nitrobenzene-d5 (S)%5250
Phenol-d6 (S)%5150
Terphenyl-d14 (S)%5357
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 40 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
631715
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92547722001, 92547722002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92547665007
3318639SAMPLE DUPLICATE:
Percent Moisture %33.1 N232534.0
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
634247
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92547722003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92547722003
3331053SAMPLE DUPLICATE:
Percent Moisture %13.4 N212513.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 42 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1702137
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92547722001, 92547722002, 92547722003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3677787-1
Associated Lab Samples:92547722001, 92547722002, 92547722003
Matrix: Solid
AnalyzedMDL
Total Solids %ND 07/09/21 11:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3677787-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1374901-01
R3677787-3SAMPLE DUPLICATE:
Total Solids %92.3 6.20 1098.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92547722
Brayton BF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1704206
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92547722001, 92547722002, 92547722003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3680544-1
Associated Lab Samples:92547722001, 92547722002, 92547722003
Matrix: Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 07/16/21 13:470.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3680544-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.210.0 102 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3680544-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92547722001
R3680544-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 25.5 97.1 75.0-12596.5 0.579 2025.50.527 25.2 25.1
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3680544-6MATRIX SPIKE SAMPLE:
MSSpike
Result
92547722001
Chromium, Hexavalent mg/kg 891868 103 75.0-1250.527
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1374289-04
R3680544-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.792J J0.363 200.795
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1376291-07
R3680544-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 49
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92547722
Brayton BF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision andbias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result shouldbe considered an estimated value.IK
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should beconsidered an estimated value.IL
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. Acomplete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in theassociated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in theassociated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/19/2021 05:08 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 45 of 49
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92547722
Brayton BF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92547722001 632634 632652TW-1 EPA 3050B EPA 6010D
92547722002 632634 632652TW-2 EPA 3050B EPA 6010D
92547722003 632634 632652DUPEPA 3050B EPA 6010D
92547722001 632238 632261TW-1 EPA 7471B EPA 7471B
92547722002 632238 632261TW-2 EPA 7471B EPA 7471B
92547722003 632238 632261DUPEPA 7471B EPA 7471B
92547722001 631600 631780TW-1 EPA 3546 EPA 8270E
92547722002 631600 631780TW-2 EPA 3546 EPA 8270E
92547722003 631600 631780DUPEPA 3546 EPA 8270E
92547722001 632736 632753TW-1 EPA 5035A/5030B EPA 8260D
92547722002 632400 632418TW-2 EPA 5035A/5030B EPA 8260D
92547722003 632400 632418DUPEPA 5035A/5030B EPA 8260D
92547722001 631715TW-1 SW-846
92547722002 631715TW-2 SW-846
92547722003 634247DUPSW-846
92547722001 1702137 1702137TW-1 SM 2540 G SM 2540G
92547722002 1702137 1702137TW-2 SM 2540 G SM 2540G
92547722003 1702137 1702137DUPSM 2540 G SM 2540G
92547722001 1704206 1704206TW-1 3060A EPA 7199
92547722002 1704206 1704206TW-2 3060A EPA 7199
92547722003 1704206 1704206DUP3060AEPA 7199
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 46 of 49
Page 47 of 49
Page 48 of 49
Page 49 of 49
#=CL#
July 21, 2021
LIMS USE: FR - SAMANTHA
LIMS OBJECT ID: 92548712
92548712
Project:
Pace Project No.:
RE:
Samantha M. Szakasits, G.I.T.ECS Southeast, LLP5260 Greens Dary RoadRaleigh, NC 27616
Brayton Intl 49-8056C
Dear Samantha Szakasits, G.I.T.:
Enclosed are the analytical results for sample(s) received by the laboratory on July 08, 2021. The results relate only to thesamples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and thelaboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc: ECS Southeast Reporting, ECS Southeast
Scott Werley, ECS Southeast, LLP
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 1 of 57
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92548712001 TW-2 EPA 6010D 7 PASI-ACBV
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANMCG
92548712002 MW-1 EPA 6010D 7 PASI-ACBV
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANMCG
92548712003 DUP-1 EPA 6010D 7 PASI-ACBV
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANMCG
92548712004 MW-5 EPA 6010D 7 PASI-ACBV
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANMCG
92548712005 MW-2 EPA 6010D 7 PASI-ACBV
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANDGR
92548712006 MW-4 EPA 6010D 7 PASI-ACBV
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANDGR
92548712007 MW-3 EPA 6010D 7 PASI-ACBV
EPA 7470A 1 PASI-ASOO
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANDGR
92548712008 TW-1 EPA 6010D 7 PASI-ACBV
EPA 7470A 1 PASI-ASOO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 57
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
EPA 7199 1 PANDGR
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: TW-2 Lab ID: 92548712001 Collected: 07/07/21 12:00 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND ug/L 07/19/21 20:01 7440-38-207/16/21 12:2010.0 1
Barium 19.6 ug/L 07/19/21 20:01 7440-39-307/16/21 12:205.0 1
Cadmium ND ug/L 07/19/21 20:01 7440-43-907/16/21 12:201.0 1
Chromium ND ug/L 07/19/21 20:01 7440-47-307/16/21 12:205.0 1
Lead ND ug/L 07/19/21 20:01 7439-92-107/16/21 12:205.0 1
Selenium ND ug/L 07/19/21 20:01 7782-49-2 BC07/16/21 12:2010.0 1
Silver ND ug/L 07/19/21 20:01 7440-22-407/16/21 12:205.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 07/13/21 12:57 7439-97-607/12/21 14:590.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/12/21 18:58 83-32-907/10/21 16:399.1 1
Acenaphthylene ND ug/L 07/12/21 18:58 208-96-807/10/21 16:399.1 1
Aniline ND ug/L 07/12/21 18:58 62-53-307/10/21 16:399.1 1
Anthracene ND ug/L 07/12/21 18:58 120-12-707/10/21 16:399.1 1
Benzo(a)anthracene ND ug/L 07/12/21 18:58 56-55-307/10/21 16:399.1 1
Benzo(a)pyrene ND ug/L 07/12/21 18:58 50-32-807/10/21 16:399.1 1
Benzo(b)fluoranthene ND ug/L 07/12/21 18:58 205-99-207/10/21 16:399.1 1
Benzo(g,h,i)perylene ND ug/L 07/12/21 18:58 191-24-207/10/21 16:399.1 1
Benzo(k)fluoranthene ND ug/L 07/12/21 18:58 207-08-907/10/21 16:399.1 1
Benzoic Acid ND ug/L 07/12/21 18:58 65-85-007/10/21 16:3945.5 1
Benzyl alcohol ND ug/L 07/12/21 18:58 100-51-607/10/21 16:3918.2 1
4-Bromophenylphenyl ether ND ug/L 07/12/21 18:58 101-55-307/10/21 16:399.1 1
Butylbenzylphthalate ND ug/L 07/12/21 18:58 85-68-707/10/21 16:399.1 1
4-Chloro-3-methylphenol ND ug/L 07/12/21 18:58 59-50-707/10/21 16:399.1 1
4-Chloroaniline ND ug/L 07/12/21 18:58 106-47-807/10/21 16:3918.2 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/21 18:58 111-91-107/10/21 16:399.1 1
bis(2-Chloroethyl) ether ND ug/L 07/12/21 18:58 111-44-407/10/21 16:399.1 1
2-Chloronaphthalene ND ug/L 07/12/21 18:58 91-58-707/10/21 16:399.1 1
2-Chlorophenol ND ug/L 07/12/21 18:58 95-57-807/10/21 16:399.1 1
4-Chlorophenylphenyl ether ND ug/L 07/12/21 18:58 7005-72-307/10/21 16:399.1 1
Chrysene ND ug/L 07/12/21 18:58 218-01-907/10/21 16:399.1 1
Dibenz(a,h)anthracene ND ug/L 07/12/21 18:58 53-70-307/10/21 16:399.1 1
Dibenzofuran ND ug/L 07/12/21 18:58 132-64-907/10/21 16:399.1 1
1,2-Dichlorobenzene ND ug/L 07/12/21 18:58 95-50-107/10/21 16:399.1 1
1,3-Dichlorobenzene ND ug/L 07/12/21 18:58 541-73-107/10/21 16:399.1 1
1,4-Dichlorobenzene ND ug/L 07/12/21 18:58 106-46-707/10/21 16:399.1 1
3,3'-Dichlorobenzidine ND ug/L 07/12/21 18:58 91-94-107/10/21 16:3918.2 1
2,4-Dichlorophenol ND ug/L 07/12/21 18:58 120-83-207/10/21 16:399.1 1
Diethylphthalate ND ug/L 07/12/21 18:58 84-66-207/10/21 16:399.1 1
2,4-Dimethylphenol ND ug/L 07/12/21 18:58 105-67-907/10/21 16:399.1 1
Dimethylphthalate ND ug/L 07/12/21 18:58 131-11-307/10/21 16:399.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: TW-2 Lab ID: 92548712001 Collected: 07/07/21 12:00 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 07/12/21 18:58 84-74-207/10/21 16:399.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/21 18:58 534-52-107/10/21 16:3918.2 1
2,4-Dinitrophenol ND ug/L 07/12/21 18:58 51-28-507/10/21 16:3945.5 1
2,4-Dinitrotoluene ND ug/L 07/12/21 18:58 121-14-207/10/21 16:399.1 1
2,6-Dinitrotoluene ND ug/L 07/12/21 18:58 606-20-207/10/21 16:399.1 1
Di-n-octylphthalate ND ug/L 07/12/21 18:58 117-84-007/10/21 16:399.1 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/21 18:58 117-81-707/10/21 16:395.5 1
Fluoranthene ND ug/L 07/12/21 18:58 206-44-007/10/21 16:399.1 1
Fluorene ND ug/L 07/12/21 18:58 86-73-707/10/21 16:399.1 1
Hexachloro-1,3-butadiene ND ug/L 07/12/21 18:58 87-68-307/10/21 16:399.1 1
Hexachlorobenzene ND ug/L 07/12/21 18:58 118-74-107/10/21 16:399.1 1
Hexachlorocyclopentadiene ND ug/L 07/12/21 18:58 77-47-407/10/21 16:399.1 1
Hexachloroethane ND ug/L 07/12/21 18:58 67-72-1 R107/10/21 16:399.1 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/21 18:58 193-39-507/10/21 16:399.1 1
Isophorone ND ug/L 07/12/21 18:58 78-59-107/10/21 16:399.1 1
1-Methylnaphthalene ND ug/L 07/12/21 18:58 90-12-007/10/21 16:399.1 1
2-Methylnaphthalene ND ug/L 07/12/21 18:58 91-57-607/10/21 16:399.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/21 18:58 95-48-707/10/21 16:399.1 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/21 18:58 15831-10-407/10/21 16:399.1 1
Naphthalene ND ug/L 07/12/21 18:58 91-20-307/10/21 16:399.1 1
2-Nitroaniline ND ug/L 07/12/21 18:58 88-74-407/10/21 16:3918.2 1
3-Nitroaniline ND ug/L 07/12/21 18:58 99-09-207/10/21 16:3918.2 1
4-Nitroaniline ND ug/L 07/12/21 18:58 100-01-607/10/21 16:3918.2 1
Nitrobenzene ND ug/L 07/12/21 18:58 98-95-307/10/21 16:399.1 1
2-Nitrophenol ND ug/L 07/12/21 18:58 88-75-5 v107/10/21 16:399.1 1
4-Nitrophenol ND ug/L 07/12/21 18:58 100-02-707/10/21 16:3945.5 1
N-Nitrosodimethylamine ND ug/L 07/12/21 18:58 62-75-907/10/21 16:399.1 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/21 18:58 621-64-707/10/21 16:399.1 1
N-Nitrosodiphenylamine ND ug/L 07/12/21 18:58 86-30-607/10/21 16:399.1 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/21 18:58 108-60-107/10/21 16:399.1 1
Pentachlorophenol ND ug/L 07/12/21 18:58 87-86-507/10/21 16:3918.2 1
Phenanthrene ND ug/L 07/12/21 18:58 85-01-807/10/21 16:399.1 1
Phenol ND ug/L 07/12/21 18:58 108-95-207/10/21 16:399.1 1
Pyrene ND ug/L 07/12/21 18:58 129-00-007/10/21 16:399.1 1
1,2,4-Trichlorobenzene ND ug/L 07/12/21 18:58 120-82-107/10/21 16:399.1 1
2,4,5-Trichlorophenol ND ug/L 07/12/21 18:58 95-95-407/10/21 16:399.1 1
2,4,6-Trichlorophenol ND ug/L 07/12/21 18:58 88-06-207/10/21 16:399.1 1
Surrogates
Nitrobenzene-d5 (S)87 %07/12/21 18:58 4165-60-007/10/21 16:3910-144 1
2-Fluorobiphenyl (S)72 %07/12/21 18:58 321-60-807/10/21 16:3910-130 1
Terphenyl-d14 (S)96 %07/12/21 18:58 1718-51-007/10/21 16:3934-163 1
Phenol-d6 (S)37 %07/12/21 18:58 13127-88-307/10/21 16:3910-130 1
2-Fluorophenol (S)56 %07/12/21 18:58 367-12-407/10/21 16:3910-130 1
2,4,6-Tribromophenol (S)96 %07/12/21 18:58 118-79-607/10/21 16:3910-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: TW-2 Lab ID: 92548712001 Collected: 07/07/21 12:00 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 07/13/21 19:28 67-64-125.0 1
Benzene ND ug/L 07/13/21 19:28 71-43-21.0 1
Bromobenzene ND ug/L 07/13/21 19:28 108-86-11.0 1
Bromochloromethane ND ug/L 07/13/21 19:28 74-97-51.0 1
Bromodichloromethane ND ug/L 07/13/21 19:28 75-27-41.0 1
Bromoform ND ug/L 07/13/21 19:28 75-25-21.0 1
Bromomethane ND ug/L 07/13/21 19:28 74-83-92.0 1
2-Butanone (MEK)ND ug/L 07/13/21 19:28 78-93-35.0 1
Carbon tetrachloride ND ug/L 07/13/21 19:28 56-23-51.0 1
Chlorobenzene ND ug/L 07/13/21 19:28 108-90-71.0 1
Chloroethane ND ug/L 07/13/21 19:28 75-00-31.0 1
Chloroform ND ug/L 07/13/21 19:28 67-66-31.0 1
Chloromethane ND ug/L 07/13/21 19:28 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/13/21 19:28 95-49-81.0 1
4-Chlorotoluene ND ug/L 07/13/21 19:28 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 07/13/21 19:28 96-12-82.0 1
Dibromochloromethane ND ug/L 07/13/21 19:28 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 07/13/21 19:28 106-93-41.0 1
Dibromomethane ND ug/L 07/13/21 19:28 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 07/13/21 19:28 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 07/13/21 19:28 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 07/13/21 19:28 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 07/13/21 19:28 75-71-8 v11.0 1
1,1-Dichloroethane ND ug/L 07/13/21 19:28 75-34-31.0 1
1,2-Dichloroethane ND ug/L 07/13/21 19:28 107-06-21.0 1
1,1-Dichloroethene ND ug/L 07/13/21 19:28 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 07/13/21 19:28 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 07/13/21 19:28 156-60-51.0 1
1,2-Dichloropropane ND ug/L 07/13/21 19:28 78-87-51.0 1
1,3-Dichloropropane ND ug/L 07/13/21 19:28 142-28-91.0 1
2,2-Dichloropropane ND ug/L 07/13/21 19:28 594-20-71.0 1
1,1-Dichloropropene ND ug/L 07/13/21 19:28 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 07/13/21 19:28 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 07/13/21 19:28 10061-02-61.0 1
Diisopropyl ether ND ug/L 07/13/21 19:28 108-20-31.0 1
Ethylbenzene ND ug/L 07/13/21 19:28 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 07/13/21 19:28 87-68-32.0 1
2-Hexanone ND ug/L 07/13/21 19:28 591-78-65.0 1
p-Isopropyltoluene ND ug/L 07/13/21 19:28 99-87-61.0 1
Methylene Chloride ND ug/L 07/13/21 19:28 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/13/21 19:28 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 07/13/21 19:28 1634-04-41.0 1
Naphthalene ND ug/L 07/13/21 19:28 91-20-31.0 1
Styrene ND ug/L 07/13/21 19:28 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 07/13/21 19:28 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 07/13/21 19:28 79-34-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: TW-2 Lab ID: 92548712001 Collected: 07/07/21 12:00 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Tetrachloroethene ND ug/L 07/13/21 19:28 127-18-41.0 1
Toluene ND ug/L 07/13/21 19:28 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 07/13/21 19:28 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 07/13/21 19:28 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 07/13/21 19:28 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 07/13/21 19:28 79-00-51.0 1
Trichloroethene ND ug/L 07/13/21 19:28 79-01-61.0 1
Trichlorofluoromethane ND ug/L 07/13/21 19:28 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/13/21 19:28 96-18-41.0 1
Vinyl acetate ND ug/L 07/13/21 19:28 108-05-42.0 1
Vinyl chloride ND ug/L 07/13/21 19:28 75-01-41.0 1
Xylene (Total)ND ug/L 07/13/21 19:28 1330-20-71.0 1
m&p-Xylene ND ug/L 07/13/21 19:28 179601-23-12.0 1
o-Xylene ND ug/L 07/13/21 19:28 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)97 %07/13/21 19:28 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %07/13/21 19:28 17060-07-070-130 1
Toluene-d8 (S)101 %07/13/21 19:28 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.583 ug/L 07/19/21 17:53 18540-29-907/19/21 17:530.500 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-1 Lab ID: 92548712002 Collected: 07/07/21 13:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND ug/L 07/19/21 20:05 7440-38-207/16/21 12:2010.0 1
Barium 23.8 ug/L 07/19/21 20:05 7440-39-307/16/21 12:205.0 1
Cadmium ND ug/L 07/19/21 20:05 7440-43-907/16/21 12:201.0 1
Chromium ND ug/L 07/19/21 20:05 7440-47-307/16/21 12:205.0 1
Lead ND ug/L 07/19/21 20:05 7439-92-107/16/21 12:205.0 1
Selenium ND ug/L 07/19/21 20:05 7782-49-2 BC07/16/21 12:2010.0 1
Silver ND ug/L 07/19/21 20:05 7440-22-407/16/21 12:205.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury 1.0 ug/L 07/13/21 13:00 7439-97-607/12/21 14:590.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/12/21 20:26 83-32-907/10/21 16:399.1 1
Acenaphthylene ND ug/L 07/12/21 20:26 208-96-807/10/21 16:399.1 1
Aniline ND ug/L 07/12/21 20:26 62-53-307/10/21 16:399.1 1
Anthracene ND ug/L 07/12/21 20:26 120-12-707/10/21 16:399.1 1
Benzo(a)anthracene ND ug/L 07/12/21 20:26 56-55-307/10/21 16:399.1 1
Benzo(a)pyrene ND ug/L 07/12/21 20:26 50-32-807/10/21 16:399.1 1
Benzo(b)fluoranthene ND ug/L 07/12/21 20:26 205-99-207/10/21 16:399.1 1
Benzo(g,h,i)perylene ND ug/L 07/12/21 20:26 191-24-207/10/21 16:399.1 1
Benzo(k)fluoranthene ND ug/L 07/12/21 20:26 207-08-907/10/21 16:399.1 1
Benzoic Acid ND ug/L 07/12/21 20:26 65-85-007/10/21 16:3945.5 1
Benzyl alcohol ND ug/L 07/12/21 20:26 100-51-607/10/21 16:3918.2 1
4-Bromophenylphenyl ether ND ug/L 07/12/21 20:26 101-55-307/10/21 16:399.1 1
Butylbenzylphthalate ND ug/L 07/12/21 20:26 85-68-707/10/21 16:399.1 1
4-Chloro-3-methylphenol ND ug/L 07/12/21 20:26 59-50-707/10/21 16:399.1 1
4-Chloroaniline ND ug/L 07/12/21 20:26 106-47-807/10/21 16:3918.2 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/21 20:26 111-91-107/10/21 16:399.1 1
bis(2-Chloroethyl) ether ND ug/L 07/12/21 20:26 111-44-407/10/21 16:399.1 1
2-Chloronaphthalene ND ug/L 07/12/21 20:26 91-58-707/10/21 16:399.1 1
2-Chlorophenol ND ug/L 07/12/21 20:26 95-57-807/10/21 16:399.1 1
4-Chlorophenylphenyl ether ND ug/L 07/12/21 20:26 7005-72-307/10/21 16:399.1 1
Chrysene ND ug/L 07/12/21 20:26 218-01-907/10/21 16:399.1 1
Dibenz(a,h)anthracene ND ug/L 07/12/21 20:26 53-70-307/10/21 16:399.1 1
Dibenzofuran ND ug/L 07/12/21 20:26 132-64-907/10/21 16:399.1 1
1,2-Dichlorobenzene ND ug/L 07/12/21 20:26 95-50-107/10/21 16:399.1 1
1,3-Dichlorobenzene ND ug/L 07/12/21 20:26 541-73-107/10/21 16:399.1 1
1,4-Dichlorobenzene ND ug/L 07/12/21 20:26 106-46-707/10/21 16:399.1 1
3,3'-Dichlorobenzidine ND ug/L 07/12/21 20:26 91-94-107/10/21 16:3918.2 1
2,4-Dichlorophenol ND ug/L 07/12/21 20:26 120-83-207/10/21 16:399.1 1
Diethylphthalate ND ug/L 07/12/21 20:26 84-66-207/10/21 16:399.1 1
2,4-Dimethylphenol ND ug/L 07/12/21 20:26 105-67-907/10/21 16:399.1 1
Dimethylphthalate ND ug/L 07/12/21 20:26 131-11-307/10/21 16:399.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-1 Lab ID: 92548712002 Collected: 07/07/21 13:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 07/12/21 20:26 84-74-207/10/21 16:399.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/21 20:26 534-52-107/10/21 16:3918.2 1
2,4-Dinitrophenol ND ug/L 07/12/21 20:26 51-28-507/10/21 16:3945.5 1
2,4-Dinitrotoluene ND ug/L 07/12/21 20:26 121-14-207/10/21 16:399.1 1
2,6-Dinitrotoluene ND ug/L 07/12/21 20:26 606-20-207/10/21 16:399.1 1
Di-n-octylphthalate ND ug/L 07/12/21 20:26 117-84-007/10/21 16:399.1 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/21 20:26 117-81-707/10/21 16:395.5 1
Fluoranthene ND ug/L 07/12/21 20:26 206-44-007/10/21 16:399.1 1
Fluorene ND ug/L 07/12/21 20:26 86-73-707/10/21 16:399.1 1
Hexachloro-1,3-butadiene ND ug/L 07/12/21 20:26 87-68-307/10/21 16:399.1 1
Hexachlorobenzene ND ug/L 07/12/21 20:26 118-74-107/10/21 16:399.1 1
Hexachlorocyclopentadiene ND ug/L 07/12/21 20:26 77-47-407/10/21 16:399.1 1
Hexachloroethane ND ug/L 07/12/21 20:26 67-72-107/10/21 16:399.1 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/21 20:26 193-39-507/10/21 16:399.1 1
Isophorone ND ug/L 07/12/21 20:26 78-59-107/10/21 16:399.1 1
1-Methylnaphthalene ND ug/L 07/12/21 20:26 90-12-007/10/21 16:399.1 1
2-Methylnaphthalene ND ug/L 07/12/21 20:26 91-57-607/10/21 16:399.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/21 20:26 95-48-707/10/21 16:399.1 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/21 20:26 15831-10-407/10/21 16:399.1 1
Naphthalene ND ug/L 07/12/21 20:26 91-20-307/10/21 16:399.1 1
2-Nitroaniline ND ug/L 07/12/21 20:26 88-74-407/10/21 16:3918.2 1
3-Nitroaniline ND ug/L 07/12/21 20:26 99-09-207/10/21 16:3918.2 1
4-Nitroaniline ND ug/L 07/12/21 20:26 100-01-607/10/21 16:3918.2 1
Nitrobenzene ND ug/L 07/12/21 20:26 98-95-307/10/21 16:399.1 1
2-Nitrophenol ND ug/L 07/12/21 20:26 88-75-5 v107/10/21 16:399.1 1
4-Nitrophenol ND ug/L 07/12/21 20:26 100-02-707/10/21 16:3945.5 1
N-Nitrosodimethylamine ND ug/L 07/12/21 20:26 62-75-907/10/21 16:399.1 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/21 20:26 621-64-707/10/21 16:399.1 1
N-Nitrosodiphenylamine ND ug/L 07/12/21 20:26 86-30-607/10/21 16:399.1 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/21 20:26 108-60-107/10/21 16:399.1 1
Pentachlorophenol ND ug/L 07/12/21 20:26 87-86-507/10/21 16:3918.2 1
Phenanthrene ND ug/L 07/12/21 20:26 85-01-807/10/21 16:399.1 1
Phenol ND ug/L 07/12/21 20:26 108-95-207/10/21 16:399.1 1
Pyrene ND ug/L 07/12/21 20:26 129-00-007/10/21 16:399.1 1
1,2,4-Trichlorobenzene ND ug/L 07/12/21 20:26 120-82-107/10/21 16:399.1 1
2,4,5-Trichlorophenol ND ug/L 07/12/21 20:26 95-95-407/10/21 16:399.1 1
2,4,6-Trichlorophenol ND ug/L 07/12/21 20:26 88-06-207/10/21 16:399.1 1
Surrogates
Nitrobenzene-d5 (S)37 %07/12/21 20:26 4165-60-007/10/21 16:3910-144 1
2-Fluorobiphenyl (S)30 %07/12/21 20:26 321-60-807/10/21 16:3910-130 1
Terphenyl-d14 (S)81 %07/12/21 20:26 1718-51-007/10/21 16:3934-163 1
Phenol-d6 (S)16 %07/12/21 20:26 13127-88-307/10/21 16:3910-130 1
2-Fluorophenol (S)23 %07/12/21 20:26 367-12-407/10/21 16:3910-130 1
2,4,6-Tribromophenol (S)54 %07/12/21 20:26 118-79-607/10/21 16:3910-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-1 Lab ID: 92548712002 Collected: 07/07/21 13:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 07/13/21 19:46 67-64-125.0 1
Benzene ND ug/L 07/13/21 19:46 71-43-21.0 1
Bromobenzene ND ug/L 07/13/21 19:46 108-86-11.0 1
Bromochloromethane ND ug/L 07/13/21 19:46 74-97-51.0 1
Bromodichloromethane ND ug/L 07/13/21 19:46 75-27-41.0 1
Bromoform ND ug/L 07/13/21 19:46 75-25-21.0 1
Bromomethane ND ug/L 07/13/21 19:46 74-83-92.0 1
2-Butanone (MEK)ND ug/L 07/13/21 19:46 78-93-35.0 1
Carbon tetrachloride ND ug/L 07/13/21 19:46 56-23-51.0 1
Chlorobenzene ND ug/L 07/13/21 19:46 108-90-71.0 1
Chloroethane ND ug/L 07/13/21 19:46 75-00-31.0 1
Chloroform ND ug/L 07/13/21 19:46 67-66-31.0 1
Chloromethane ND ug/L 07/13/21 19:46 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/13/21 19:46 95-49-81.0 1
4-Chlorotoluene ND ug/L 07/13/21 19:46 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 07/13/21 19:46 96-12-82.0 1
Dibromochloromethane ND ug/L 07/13/21 19:46 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 07/13/21 19:46 106-93-41.0 1
Dibromomethane ND ug/L 07/13/21 19:46 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 07/13/21 19:46 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 07/13/21 19:46 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 07/13/21 19:46 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 07/13/21 19:46 75-71-8 v11.0 1
1,1-Dichloroethane ND ug/L 07/13/21 19:46 75-34-31.0 1
1,2-Dichloroethane ND ug/L 07/13/21 19:46 107-06-21.0 1
1,1-Dichloroethene ND ug/L 07/13/21 19:46 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 07/13/21 19:46 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 07/13/21 19:46 156-60-51.0 1
1,2-Dichloropropane ND ug/L 07/13/21 19:46 78-87-51.0 1
1,3-Dichloropropane ND ug/L 07/13/21 19:46 142-28-91.0 1
2,2-Dichloropropane ND ug/L 07/13/21 19:46 594-20-71.0 1
1,1-Dichloropropene ND ug/L 07/13/21 19:46 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 07/13/21 19:46 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 07/13/21 19:46 10061-02-61.0 1
Diisopropyl ether ND ug/L 07/13/21 19:46 108-20-31.0 1
Ethylbenzene ND ug/L 07/13/21 19:46 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 07/13/21 19:46 87-68-32.0 1
2-Hexanone ND ug/L 07/13/21 19:46 591-78-65.0 1
p-Isopropyltoluene ND ug/L 07/13/21 19:46 99-87-61.0 1
Methylene Chloride ND ug/L 07/13/21 19:46 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/13/21 19:46 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 07/13/21 19:46 1634-04-41.0 1
Naphthalene ND ug/L 07/13/21 19:46 91-20-31.0 1
Styrene ND ug/L 07/13/21 19:46 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 07/13/21 19:46 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 07/13/21 19:46 79-34-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-1 Lab ID: 92548712002 Collected: 07/07/21 13:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Tetrachloroethene ND ug/L 07/13/21 19:46 127-18-41.0 1
Toluene ND ug/L 07/13/21 19:46 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 07/13/21 19:46 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 07/13/21 19:46 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 07/13/21 19:46 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 07/13/21 19:46 79-00-51.0 1
Trichloroethene ND ug/L 07/13/21 19:46 79-01-61.0 1
Trichlorofluoromethane ND ug/L 07/13/21 19:46 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/13/21 19:46 96-18-41.0 1
Vinyl acetate ND ug/L 07/13/21 19:46 108-05-42.0 1
Vinyl chloride ND ug/L 07/13/21 19:46 75-01-41.0 1
Xylene (Total)ND ug/L 07/13/21 19:46 1330-20-71.0 1
m&p-Xylene ND ug/L 07/13/21 19:46 179601-23-12.0 1
o-Xylene ND ug/L 07/13/21 19:46 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)97 %07/13/21 19:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %07/13/21 19:46 17060-07-070-130 1
Toluene-d8 (S)101 %07/13/21 19:46 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 2.51 ug/L 07/19/21 18:00 18540-29-907/19/21 18:000.500 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: DUP-1 Lab ID: 92548712003 Collected: 07/07/21 13:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND ug/L 07/19/21 20:08 7440-38-207/16/21 12:2010.0 1
Barium 22.2 ug/L 07/19/21 20:08 7440-39-307/16/21 12:205.0 1
Cadmium ND ug/L 07/19/21 20:08 7440-43-907/16/21 12:201.0 1
Chromium ND ug/L 07/19/21 20:08 7440-47-307/16/21 12:205.0 1
Lead ND ug/L 07/19/21 20:08 7439-92-107/16/21 12:205.0 1
Selenium ND ug/L 07/19/21 20:08 7782-49-2 BC07/16/21 12:2010.0 1
Silver ND ug/L 07/19/21 20:08 7440-22-407/16/21 12:205.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury 0.92 ug/L 07/13/21 13:02 7439-97-607/12/21 14:590.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/12/21 20:56 83-32-907/10/21 16:3910.5 1
Acenaphthylene ND ug/L 07/12/21 20:56 208-96-807/10/21 16:3910.5 1
Aniline ND ug/L 07/12/21 20:56 62-53-307/10/21 16:3910.5 1
Anthracene ND ug/L 07/12/21 20:56 120-12-707/10/21 16:3910.5 1
Benzo(a)anthracene ND ug/L 07/12/21 20:56 56-55-307/10/21 16:3910.5 1
Benzo(a)pyrene ND ug/L 07/12/21 20:56 50-32-807/10/21 16:3910.5 1
Benzo(b)fluoranthene ND ug/L 07/12/21 20:56 205-99-207/10/21 16:3910.5 1
Benzo(g,h,i)perylene ND ug/L 07/12/21 20:56 191-24-207/10/21 16:3910.5 1
Benzo(k)fluoranthene ND ug/L 07/12/21 20:56 207-08-907/10/21 16:3910.5 1
Benzoic Acid ND ug/L 07/12/21 20:56 65-85-007/10/21 16:3952.6 1
Benzyl alcohol ND ug/L 07/12/21 20:56 100-51-607/10/21 16:3921.1 1
4-Bromophenylphenyl ether ND ug/L 07/12/21 20:56 101-55-307/10/21 16:3910.5 1
Butylbenzylphthalate ND ug/L 07/12/21 20:56 85-68-707/10/21 16:3910.5 1
4-Chloro-3-methylphenol ND ug/L 07/12/21 20:56 59-50-707/10/21 16:3910.5 1
4-Chloroaniline ND ug/L 07/12/21 20:56 106-47-807/10/21 16:3921.1 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/21 20:56 111-91-107/10/21 16:3910.5 1
bis(2-Chloroethyl) ether ND ug/L 07/12/21 20:56 111-44-407/10/21 16:3910.5 1
2-Chloronaphthalene ND ug/L 07/12/21 20:56 91-58-707/10/21 16:3910.5 1
2-Chlorophenol ND ug/L 07/12/21 20:56 95-57-807/10/21 16:3910.5 1
4-Chlorophenylphenyl ether ND ug/L 07/12/21 20:56 7005-72-307/10/21 16:3910.5 1
Chrysene ND ug/L 07/12/21 20:56 218-01-907/10/21 16:3910.5 1
Dibenz(a,h)anthracene ND ug/L 07/12/21 20:56 53-70-307/10/21 16:3910.5 1
Dibenzofuran ND ug/L 07/12/21 20:56 132-64-907/10/21 16:3910.5 1
1,2-Dichlorobenzene ND ug/L 07/12/21 20:56 95-50-107/10/21 16:3910.5 1
1,3-Dichlorobenzene ND ug/L 07/12/21 20:56 541-73-107/10/21 16:3910.5 1
1,4-Dichlorobenzene ND ug/L 07/12/21 20:56 106-46-707/10/21 16:3910.5 1
3,3'-Dichlorobenzidine ND ug/L 07/12/21 20:56 91-94-107/10/21 16:3921.1 1
2,4-Dichlorophenol ND ug/L 07/12/21 20:56 120-83-207/10/21 16:3910.5 1
Diethylphthalate ND ug/L 07/12/21 20:56 84-66-207/10/21 16:3910.5 1
2,4-Dimethylphenol ND ug/L 07/12/21 20:56 105-67-907/10/21 16:3910.5 1
Dimethylphthalate ND ug/L 07/12/21 20:56 131-11-307/10/21 16:3910.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: DUP-1 Lab ID: 92548712003 Collected: 07/07/21 13:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 07/12/21 20:56 84-74-207/10/21 16:3910.5 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/21 20:56 534-52-107/10/21 16:3921.1 1
2,4-Dinitrophenol ND ug/L 07/12/21 20:56 51-28-507/10/21 16:3952.6 1
2,4-Dinitrotoluene ND ug/L 07/12/21 20:56 121-14-207/10/21 16:3910.5 1
2,6-Dinitrotoluene ND ug/L 07/12/21 20:56 606-20-207/10/21 16:3910.5 1
Di-n-octylphthalate ND ug/L 07/12/21 20:56 117-84-007/10/21 16:3910.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/21 20:56 117-81-707/10/21 16:396.3 1
Fluoranthene ND ug/L 07/12/21 20:56 206-44-007/10/21 16:3910.5 1
Fluorene ND ug/L 07/12/21 20:56 86-73-707/10/21 16:3910.5 1
Hexachloro-1,3-butadiene ND ug/L 07/12/21 20:56 87-68-307/10/21 16:3910.5 1
Hexachlorobenzene ND ug/L 07/12/21 20:56 118-74-107/10/21 16:3910.5 1
Hexachlorocyclopentadiene ND ug/L 07/12/21 20:56 77-47-407/10/21 16:3910.5 1
Hexachloroethane ND ug/L 07/12/21 20:56 67-72-107/10/21 16:3910.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/21 20:56 193-39-507/10/21 16:3910.5 1
Isophorone ND ug/L 07/12/21 20:56 78-59-107/10/21 16:3910.5 1
1-Methylnaphthalene ND ug/L 07/12/21 20:56 90-12-007/10/21 16:3910.5 1
2-Methylnaphthalene ND ug/L 07/12/21 20:56 91-57-607/10/21 16:3910.5 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/21 20:56 95-48-707/10/21 16:3910.5 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/21 20:56 15831-10-407/10/21 16:3910.5 1
Naphthalene ND ug/L 07/12/21 20:56 91-20-307/10/21 16:3910.5 1
2-Nitroaniline ND ug/L 07/12/21 20:56 88-74-407/10/21 16:3921.1 1
3-Nitroaniline ND ug/L 07/12/21 20:56 99-09-207/10/21 16:3921.1 1
4-Nitroaniline ND ug/L 07/12/21 20:56 100-01-607/10/21 16:3921.1 1
Nitrobenzene ND ug/L 07/12/21 20:56 98-95-307/10/21 16:3910.5 1
2-Nitrophenol ND ug/L 07/12/21 20:56 88-75-5 v107/10/21 16:3910.5 1
4-Nitrophenol ND ug/L 07/12/21 20:56 100-02-707/10/21 16:3952.6 1
N-Nitrosodimethylamine ND ug/L 07/12/21 20:56 62-75-907/10/21 16:3910.5 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/21 20:56 621-64-707/10/21 16:3910.5 1
N-Nitrosodiphenylamine ND ug/L 07/12/21 20:56 86-30-607/10/21 16:3910.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/21 20:56 108-60-107/10/21 16:3910.5 1
Pentachlorophenol ND ug/L 07/12/21 20:56 87-86-507/10/21 16:3921.1 1
Phenanthrene ND ug/L 07/12/21 20:56 85-01-807/10/21 16:3910.5 1
Phenol ND ug/L 07/12/21 20:56 108-95-207/10/21 16:3910.5 1
Pyrene ND ug/L 07/12/21 20:56 129-00-007/10/21 16:3910.5 1
1,2,4-Trichlorobenzene ND ug/L 07/12/21 20:56 120-82-107/10/21 16:3910.5 1
2,4,5-Trichlorophenol ND ug/L 07/12/21 20:56 95-95-407/10/21 16:3910.5 1
2,4,6-Trichlorophenol ND ug/L 07/12/21 20:56 88-06-207/10/21 16:3910.5 1
Surrogates
Nitrobenzene-d5 (S)37 %07/12/21 20:56 4165-60-007/10/21 16:3910-144 1
2-Fluorobiphenyl (S)34 %07/12/21 20:56 321-60-807/10/21 16:3910-130 1
Terphenyl-d14 (S)101 %07/12/21 20:56 1718-51-007/10/21 16:3934-163 1
Phenol-d6 (S)16 %07/12/21 20:56 13127-88-307/10/21 16:3910-130 1
2-Fluorophenol (S)23 %07/12/21 20:56 367-12-407/10/21 16:3910-130 1
2,4,6-Tribromophenol (S)64 %07/12/21 20:56 118-79-607/10/21 16:3910-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: DUP-1 Lab ID: 92548712003 Collected: 07/07/21 13:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 07/13/21 20:04 67-64-125.0 1
Benzene ND ug/L 07/13/21 20:04 71-43-21.0 1
Bromobenzene ND ug/L 07/13/21 20:04 108-86-11.0 1
Bromochloromethane ND ug/L 07/13/21 20:04 74-97-51.0 1
Bromodichloromethane ND ug/L 07/13/21 20:04 75-27-41.0 1
Bromoform ND ug/L 07/13/21 20:04 75-25-21.0 1
Bromomethane ND ug/L 07/13/21 20:04 74-83-92.0 1
2-Butanone (MEK)ND ug/L 07/13/21 20:04 78-93-35.0 1
Carbon tetrachloride ND ug/L 07/13/21 20:04 56-23-51.0 1
Chlorobenzene ND ug/L 07/13/21 20:04 108-90-71.0 1
Chloroethane ND ug/L 07/13/21 20:04 75-00-31.0 1
Chloroform ND ug/L 07/13/21 20:04 67-66-31.0 1
Chloromethane ND ug/L 07/13/21 20:04 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/13/21 20:04 95-49-81.0 1
4-Chlorotoluene ND ug/L 07/13/21 20:04 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 07/13/21 20:04 96-12-82.0 1
Dibromochloromethane ND ug/L 07/13/21 20:04 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 07/13/21 20:04 106-93-41.0 1
Dibromomethane ND ug/L 07/13/21 20:04 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 07/13/21 20:04 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 07/13/21 20:04 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 07/13/21 20:04 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 07/13/21 20:04 75-71-8 v11.0 1
1,1-Dichloroethane ND ug/L 07/13/21 20:04 75-34-31.0 1
1,2-Dichloroethane ND ug/L 07/13/21 20:04 107-06-21.0 1
1,1-Dichloroethene ND ug/L 07/13/21 20:04 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 07/13/21 20:04 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 07/13/21 20:04 156-60-51.0 1
1,2-Dichloropropane ND ug/L 07/13/21 20:04 78-87-51.0 1
1,3-Dichloropropane ND ug/L 07/13/21 20:04 142-28-91.0 1
2,2-Dichloropropane ND ug/L 07/13/21 20:04 594-20-71.0 1
1,1-Dichloropropene ND ug/L 07/13/21 20:04 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 07/13/21 20:04 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 07/13/21 20:04 10061-02-61.0 1
Diisopropyl ether ND ug/L 07/13/21 20:04 108-20-31.0 1
Ethylbenzene ND ug/L 07/13/21 20:04 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 07/13/21 20:04 87-68-32.0 1
2-Hexanone ND ug/L 07/13/21 20:04 591-78-65.0 1
p-Isopropyltoluene ND ug/L 07/13/21 20:04 99-87-61.0 1
Methylene Chloride ND ug/L 07/13/21 20:04 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/13/21 20:04 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 07/13/21 20:04 1634-04-41.0 1
Naphthalene ND ug/L 07/13/21 20:04 91-20-31.0 1
Styrene ND ug/L 07/13/21 20:04 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 07/13/21 20:04 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 07/13/21 20:04 79-34-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: DUP-1 Lab ID: 92548712003 Collected: 07/07/21 13:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Tetrachloroethene ND ug/L 07/13/21 20:04 127-18-41.0 1
Toluene ND ug/L 07/13/21 20:04 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 07/13/21 20:04 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 07/13/21 20:04 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 07/13/21 20:04 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 07/13/21 20:04 79-00-51.0 1
Trichloroethene ND ug/L 07/13/21 20:04 79-01-61.0 1
Trichlorofluoromethane ND ug/L 07/13/21 20:04 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/13/21 20:04 96-18-41.0 1
Vinyl acetate ND ug/L 07/13/21 20:04 108-05-42.0 1
Vinyl chloride ND ug/L 07/13/21 20:04 75-01-41.0 1
Xylene (Total)ND ug/L 07/13/21 20:04 1330-20-71.0 1
m&p-Xylene ND ug/L 07/13/21 20:04 179601-23-12.0 1
o-Xylene ND ug/L 07/13/21 20:04 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)97 %07/13/21 20:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %07/13/21 20:04 17060-07-070-130 1
Toluene-d8 (S)101 %07/13/21 20:04 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 2.49 ug/L 07/19/21 18:07 18540-29-907/19/21 18:070.500 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-5 Lab ID: 92548712004 Collected: 07/07/21 15:30 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND ug/L 07/19/21 20:11 7440-38-207/16/21 12:2010.0 1
Barium 177 ug/L 07/19/21 20:11 7440-39-307/16/21 12:205.0 1
Cadmium ND ug/L 07/19/21 20:11 7440-43-907/16/21 12:201.0 1
Chromium 47.9 ug/L 07/19/21 20:11 7440-47-307/16/21 12:205.0 1
Lead 20.5 ug/L 07/19/21 20:11 7439-92-107/16/21 12:205.0 1
Selenium ND ug/L 07/19/21 20:11 7782-49-2 BC07/16/21 12:2010.0 1
Silver ND ug/L 07/19/21 20:11 7440-22-407/16/21 12:205.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 07/13/21 13:38 7439-97-6 M1,R107/12/21 14:590.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/12/21 21:26 83-32-907/10/21 16:398.3 1
Acenaphthylene ND ug/L 07/12/21 21:26 208-96-807/10/21 16:398.3 1
Aniline ND ug/L 07/12/21 21:26 62-53-307/10/21 16:398.3 1
Anthracene ND ug/L 07/12/21 21:26 120-12-707/10/21 16:398.3 1
Benzo(a)anthracene ND ug/L 07/12/21 21:26 56-55-307/10/21 16:398.3 1
Benzo(a)pyrene ND ug/L 07/12/21 21:26 50-32-807/10/21 16:398.3 1
Benzo(b)fluoranthene ND ug/L 07/12/21 21:26 205-99-207/10/21 16:398.3 1
Benzo(g,h,i)perylene ND ug/L 07/12/21 21:26 191-24-207/10/21 16:398.3 1
Benzo(k)fluoranthene ND ug/L 07/12/21 21:26 207-08-907/10/21 16:398.3 1
Benzoic Acid ND ug/L 07/12/21 21:26 65-85-007/10/21 16:3941.7 1
Benzyl alcohol ND ug/L 07/12/21 21:26 100-51-607/10/21 16:3916.7 1
4-Bromophenylphenyl ether ND ug/L 07/12/21 21:26 101-55-307/10/21 16:398.3 1
Butylbenzylphthalate ND ug/L 07/12/21 21:26 85-68-707/10/21 16:398.3 1
4-Chloro-3-methylphenol ND ug/L 07/12/21 21:26 59-50-707/10/21 16:398.3 1
4-Chloroaniline ND ug/L 07/12/21 21:26 106-47-807/10/21 16:3916.7 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/21 21:26 111-91-107/10/21 16:398.3 1
bis(2-Chloroethyl) ether ND ug/L 07/12/21 21:26 111-44-407/10/21 16:398.3 1
2-Chloronaphthalene ND ug/L 07/12/21 21:26 91-58-707/10/21 16:398.3 1
2-Chlorophenol ND ug/L 07/12/21 21:26 95-57-807/10/21 16:398.3 1
4-Chlorophenylphenyl ether ND ug/L 07/12/21 21:26 7005-72-307/10/21 16:398.3 1
Chrysene ND ug/L 07/12/21 21:26 218-01-907/10/21 16:398.3 1
Dibenz(a,h)anthracene ND ug/L 07/12/21 21:26 53-70-307/10/21 16:398.3 1
Dibenzofuran ND ug/L 07/12/21 21:26 132-64-907/10/21 16:398.3 1
1,2-Dichlorobenzene ND ug/L 07/12/21 21:26 95-50-107/10/21 16:398.3 1
1,3-Dichlorobenzene ND ug/L 07/12/21 21:26 541-73-107/10/21 16:398.3 1
1,4-Dichlorobenzene ND ug/L 07/12/21 21:26 106-46-707/10/21 16:398.3 1
3,3'-Dichlorobenzidine ND ug/L 07/12/21 21:26 91-94-107/10/21 16:3916.7 1
2,4-Dichlorophenol ND ug/L 07/12/21 21:26 120-83-207/10/21 16:398.3 1
Diethylphthalate ND ug/L 07/12/21 21:26 84-66-207/10/21 16:398.3 1
2,4-Dimethylphenol ND ug/L 07/12/21 21:26 105-67-907/10/21 16:398.3 1
Dimethylphthalate ND ug/L 07/12/21 21:26 131-11-307/10/21 16:398.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-5 Lab ID: 92548712004 Collected: 07/07/21 15:30 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 07/12/21 21:26 84-74-207/10/21 16:398.3 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/21 21:26 534-52-107/10/21 16:3916.7 1
2,4-Dinitrophenol ND ug/L 07/12/21 21:26 51-28-507/10/21 16:3941.7 1
2,4-Dinitrotoluene ND ug/L 07/12/21 21:26 121-14-207/10/21 16:398.3 1
2,6-Dinitrotoluene ND ug/L 07/12/21 21:26 606-20-207/10/21 16:398.3 1
Di-n-octylphthalate ND ug/L 07/12/21 21:26 117-84-007/10/21 16:398.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/21 21:26 117-81-707/10/21 16:395.0 1
Fluoranthene ND ug/L 07/12/21 21:26 206-44-007/10/21 16:398.3 1
Fluorene ND ug/L 07/12/21 21:26 86-73-707/10/21 16:398.3 1
Hexachloro-1,3-butadiene ND ug/L 07/12/21 21:26 87-68-307/10/21 16:398.3 1
Hexachlorobenzene ND ug/L 07/12/21 21:26 118-74-107/10/21 16:398.3 1
Hexachlorocyclopentadiene ND ug/L 07/12/21 21:26 77-47-407/10/21 16:398.3 1
Hexachloroethane ND ug/L 07/12/21 21:26 67-72-107/10/21 16:398.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/21 21:26 193-39-507/10/21 16:398.3 1
Isophorone ND ug/L 07/12/21 21:26 78-59-107/10/21 16:398.3 1
1-Methylnaphthalene ND ug/L 07/12/21 21:26 90-12-007/10/21 16:398.3 1
2-Methylnaphthalene ND ug/L 07/12/21 21:26 91-57-607/10/21 16:398.3 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/21 21:26 95-48-707/10/21 16:398.3 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/21 21:26 15831-10-407/10/21 16:398.3 1
Naphthalene ND ug/L 07/12/21 21:26 91-20-307/10/21 16:398.3 1
2-Nitroaniline ND ug/L 07/12/21 21:26 88-74-407/10/21 16:3916.7 1
3-Nitroaniline ND ug/L 07/12/21 21:26 99-09-207/10/21 16:3916.7 1
4-Nitroaniline ND ug/L 07/12/21 21:26 100-01-607/10/21 16:3916.7 1
Nitrobenzene ND ug/L 07/12/21 21:26 98-95-307/10/21 16:398.3 1
2-Nitrophenol ND ug/L 07/12/21 21:26 88-75-5 v107/10/21 16:398.3 1
4-Nitrophenol ND ug/L 07/12/21 21:26 100-02-707/10/21 16:3941.7 1
N-Nitrosodimethylamine ND ug/L 07/12/21 21:26 62-75-907/10/21 16:398.3 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/21 21:26 621-64-707/10/21 16:398.3 1
N-Nitrosodiphenylamine ND ug/L 07/12/21 21:26 86-30-607/10/21 16:398.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/21 21:26 108-60-107/10/21 16:398.3 1
Pentachlorophenol ND ug/L 07/12/21 21:26 87-86-507/10/21 16:3916.7 1
Phenanthrene ND ug/L 07/12/21 21:26 85-01-807/10/21 16:398.3 1
Phenol ND ug/L 07/12/21 21:26 108-95-207/10/21 16:398.3 1
Pyrene ND ug/L 07/12/21 21:26 129-00-007/10/21 16:398.3 1
1,2,4-Trichlorobenzene ND ug/L 07/12/21 21:26 120-82-107/10/21 16:398.3 1
2,4,5-Trichlorophenol ND ug/L 07/12/21 21:26 95-95-407/10/21 16:398.3 1
2,4,6-Trichlorophenol ND ug/L 07/12/21 21:26 88-06-207/10/21 16:398.3 1
Surrogates
Nitrobenzene-d5 (S)79 %07/12/21 21:26 4165-60-007/10/21 16:3910-144 1
2-Fluorobiphenyl (S)70 %07/12/21 21:26 321-60-807/10/21 16:3910-130 1
Terphenyl-d14 (S)87 %07/12/21 21:26 1718-51-007/10/21 16:3934-163 1
Phenol-d6 (S)40 %07/12/21 21:26 13127-88-307/10/21 16:3910-130 1
2-Fluorophenol (S)58 %07/12/21 21:26 367-12-407/10/21 16:3910-130 1
2,4,6-Tribromophenol (S)86 %07/12/21 21:26 118-79-607/10/21 16:3910-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-5 Lab ID: 92548712004 Collected: 07/07/21 15:30 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 07/13/21 20:22 67-64-125.0 1
Benzene ND ug/L 07/13/21 20:22 71-43-21.0 1
Bromobenzene ND ug/L 07/13/21 20:22 108-86-11.0 1
Bromochloromethane ND ug/L 07/13/21 20:22 74-97-51.0 1
Bromodichloromethane ND ug/L 07/13/21 20:22 75-27-41.0 1
Bromoform ND ug/L 07/13/21 20:22 75-25-21.0 1
Bromomethane ND ug/L 07/13/21 20:22 74-83-92.0 1
2-Butanone (MEK)ND ug/L 07/13/21 20:22 78-93-35.0 1
Carbon tetrachloride ND ug/L 07/13/21 20:22 56-23-51.0 1
Chlorobenzene ND ug/L 07/13/21 20:22 108-90-71.0 1
Chloroethane ND ug/L 07/13/21 20:22 75-00-31.0 1
Chloroform ND ug/L 07/13/21 20:22 67-66-31.0 1
Chloromethane ND ug/L 07/13/21 20:22 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/13/21 20:22 95-49-81.0 1
4-Chlorotoluene ND ug/L 07/13/21 20:22 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 07/13/21 20:22 96-12-82.0 1
Dibromochloromethane ND ug/L 07/13/21 20:22 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 07/13/21 20:22 106-93-41.0 1
Dibromomethane ND ug/L 07/13/21 20:22 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 07/13/21 20:22 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 07/13/21 20:22 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 07/13/21 20:22 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 07/13/21 20:22 75-71-8 v11.0 1
1,1-Dichloroethane ND ug/L 07/13/21 20:22 75-34-31.0 1
1,2-Dichloroethane ND ug/L 07/13/21 20:22 107-06-21.0 1
1,1-Dichloroethene ND ug/L 07/13/21 20:22 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 07/13/21 20:22 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 07/13/21 20:22 156-60-51.0 1
1,2-Dichloropropane ND ug/L 07/13/21 20:22 78-87-51.0 1
1,3-Dichloropropane ND ug/L 07/13/21 20:22 142-28-91.0 1
2,2-Dichloropropane ND ug/L 07/13/21 20:22 594-20-71.0 1
1,1-Dichloropropene ND ug/L 07/13/21 20:22 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 07/13/21 20:22 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 07/13/21 20:22 10061-02-61.0 1
Diisopropyl ether ND ug/L 07/13/21 20:22 108-20-31.0 1
Ethylbenzene ND ug/L 07/13/21 20:22 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 07/13/21 20:22 87-68-32.0 1
2-Hexanone ND ug/L 07/13/21 20:22 591-78-65.0 1
p-Isopropyltoluene ND ug/L 07/13/21 20:22 99-87-61.0 1
Methylene Chloride ND ug/L 07/13/21 20:22 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/13/21 20:22 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 07/13/21 20:22 1634-04-41.0 1
Naphthalene ND ug/L 07/13/21 20:22 91-20-31.0 1
Styrene ND ug/L 07/13/21 20:22 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 07/13/21 20:22 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 07/13/21 20:22 79-34-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-5 Lab ID: 92548712004 Collected: 07/07/21 15:30 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Tetrachloroethene ND ug/L 07/13/21 20:22 127-18-41.0 1
Toluene ND ug/L 07/13/21 20:22 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 07/13/21 20:22 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 07/13/21 20:22 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 07/13/21 20:22 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 07/13/21 20:22 79-00-51.0 1
Trichloroethene ND ug/L 07/13/21 20:22 79-01-61.0 1
Trichlorofluoromethane ND ug/L 07/13/21 20:22 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/13/21 20:22 96-18-41.0 1
Vinyl acetate ND ug/L 07/13/21 20:22 108-05-42.0 1
Vinyl chloride ND ug/L 07/13/21 20:22 75-01-41.0 1
Xylene (Total)ND ug/L 07/13/21 20:22 1330-20-71.0 1
m&p-Xylene ND ug/L 07/13/21 20:22 179601-23-12.0 1
o-Xylene ND ug/L 07/13/21 20:22 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)96 %07/13/21 20:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %07/13/21 20:22 17060-07-070-130 1
Toluene-d8 (S)102 %07/13/21 20:22 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.673 ug/L 07/19/21 18:15 18540-29-907/19/21 18:150.500 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-2 Lab ID: 92548712005 Collected: 07/07/21 16:20 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND ug/L 07/19/21 20:14 7440-38-207/16/21 12:2010.0 1
Barium 34.1 ug/L 07/19/21 20:14 7440-39-307/16/21 12:205.0 1
Cadmium ND ug/L 07/19/21 20:14 7440-43-907/16/21 12:201.0 1
Chromium ND ug/L 07/19/21 20:14 7440-47-307/16/21 12:205.0 1
Lead ND ug/L 07/19/21 20:14 7439-92-107/16/21 12:205.0 1
Selenium ND ug/L 07/19/21 20:14 7782-49-2 BC07/16/21 12:2010.0 1
Silver ND ug/L 07/19/21 20:14 7440-22-407/16/21 12:205.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury 0.67 ug/L 07/13/21 13:49 7439-97-607/12/21 14:590.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/12/21 21:56 83-32-907/10/21 16:399.1 1
Acenaphthylene ND ug/L 07/12/21 21:56 208-96-807/10/21 16:399.1 1
Aniline ND ug/L 07/12/21 21:56 62-53-307/10/21 16:399.1 1
Anthracene ND ug/L 07/12/21 21:56 120-12-707/10/21 16:399.1 1
Benzo(a)anthracene ND ug/L 07/12/21 21:56 56-55-307/10/21 16:399.1 1
Benzo(a)pyrene ND ug/L 07/12/21 21:56 50-32-807/10/21 16:399.1 1
Benzo(b)fluoranthene ND ug/L 07/12/21 21:56 205-99-207/10/21 16:399.1 1
Benzo(g,h,i)perylene ND ug/L 07/12/21 21:56 191-24-207/10/21 16:399.1 1
Benzo(k)fluoranthene ND ug/L 07/12/21 21:56 207-08-907/10/21 16:399.1 1
Benzoic Acid ND ug/L 07/12/21 21:56 65-85-007/10/21 16:3945.5 1
Benzyl alcohol ND ug/L 07/12/21 21:56 100-51-607/10/21 16:3918.2 1
4-Bromophenylphenyl ether ND ug/L 07/12/21 21:56 101-55-307/10/21 16:399.1 1
Butylbenzylphthalate ND ug/L 07/12/21 21:56 85-68-707/10/21 16:399.1 1
4-Chloro-3-methylphenol ND ug/L 07/12/21 21:56 59-50-707/10/21 16:399.1 1
4-Chloroaniline ND ug/L 07/12/21 21:56 106-47-807/10/21 16:3918.2 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/21 21:56 111-91-107/10/21 16:399.1 1
bis(2-Chloroethyl) ether ND ug/L 07/12/21 21:56 111-44-407/10/21 16:399.1 1
2-Chloronaphthalene ND ug/L 07/12/21 21:56 91-58-707/10/21 16:399.1 1
2-Chlorophenol ND ug/L 07/12/21 21:56 95-57-807/10/21 16:399.1 1
4-Chlorophenylphenyl ether ND ug/L 07/12/21 21:56 7005-72-307/10/21 16:399.1 1
Chrysene ND ug/L 07/12/21 21:56 218-01-907/10/21 16:399.1 1
Dibenz(a,h)anthracene ND ug/L 07/12/21 21:56 53-70-307/10/21 16:399.1 1
Dibenzofuran ND ug/L 07/12/21 21:56 132-64-907/10/21 16:399.1 1
1,2-Dichlorobenzene ND ug/L 07/12/21 21:56 95-50-107/10/21 16:399.1 1
1,3-Dichlorobenzene ND ug/L 07/12/21 21:56 541-73-107/10/21 16:399.1 1
1,4-Dichlorobenzene ND ug/L 07/12/21 21:56 106-46-707/10/21 16:399.1 1
3,3'-Dichlorobenzidine ND ug/L 07/12/21 21:56 91-94-107/10/21 16:3918.2 1
2,4-Dichlorophenol ND ug/L 07/12/21 21:56 120-83-207/10/21 16:399.1 1
Diethylphthalate ND ug/L 07/12/21 21:56 84-66-207/10/21 16:399.1 1
2,4-Dimethylphenol ND ug/L 07/12/21 21:56 105-67-907/10/21 16:399.1 1
Dimethylphthalate ND ug/L 07/12/21 21:56 131-11-307/10/21 16:399.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-2 Lab ID: 92548712005 Collected: 07/07/21 16:20 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 07/12/21 21:56 84-74-207/10/21 16:399.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/21 21:56 534-52-107/10/21 16:3918.2 1
2,4-Dinitrophenol ND ug/L 07/12/21 21:56 51-28-507/10/21 16:3945.5 1
2,4-Dinitrotoluene ND ug/L 07/12/21 21:56 121-14-207/10/21 16:399.1 1
2,6-Dinitrotoluene ND ug/L 07/12/21 21:56 606-20-207/10/21 16:399.1 1
Di-n-octylphthalate ND ug/L 07/12/21 21:56 117-84-007/10/21 16:399.1 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/21 21:56 117-81-707/10/21 16:395.5 1
Fluoranthene ND ug/L 07/12/21 21:56 206-44-007/10/21 16:399.1 1
Fluorene ND ug/L 07/12/21 21:56 86-73-707/10/21 16:399.1 1
Hexachloro-1,3-butadiene ND ug/L 07/12/21 21:56 87-68-307/10/21 16:399.1 1
Hexachlorobenzene ND ug/L 07/12/21 21:56 118-74-107/10/21 16:399.1 1
Hexachlorocyclopentadiene ND ug/L 07/12/21 21:56 77-47-407/10/21 16:399.1 1
Hexachloroethane ND ug/L 07/12/21 21:56 67-72-107/10/21 16:399.1 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/21 21:56 193-39-507/10/21 16:399.1 1
Isophorone ND ug/L 07/12/21 21:56 78-59-107/10/21 16:399.1 1
1-Methylnaphthalene ND ug/L 07/12/21 21:56 90-12-007/10/21 16:399.1 1
2-Methylnaphthalene ND ug/L 07/12/21 21:56 91-57-607/10/21 16:399.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/21 21:56 95-48-707/10/21 16:399.1 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/21 21:56 15831-10-407/10/21 16:399.1 1
Naphthalene ND ug/L 07/12/21 21:56 91-20-307/10/21 16:399.1 1
2-Nitroaniline ND ug/L 07/12/21 21:56 88-74-407/10/21 16:3918.2 1
3-Nitroaniline ND ug/L 07/12/21 21:56 99-09-207/10/21 16:3918.2 1
4-Nitroaniline ND ug/L 07/12/21 21:56 100-01-607/10/21 16:3918.2 1
Nitrobenzene ND ug/L 07/12/21 21:56 98-95-307/10/21 16:399.1 1
2-Nitrophenol ND ug/L 07/12/21 21:56 88-75-5 v107/10/21 16:399.1 1
4-Nitrophenol ND ug/L 07/12/21 21:56 100-02-707/10/21 16:3945.5 1
N-Nitrosodimethylamine ND ug/L 07/12/21 21:56 62-75-907/10/21 16:399.1 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/21 21:56 621-64-707/10/21 16:399.1 1
N-Nitrosodiphenylamine ND ug/L 07/12/21 21:56 86-30-607/10/21 16:399.1 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/21 21:56 108-60-107/10/21 16:399.1 1
Pentachlorophenol ND ug/L 07/12/21 21:56 87-86-507/10/21 16:3918.2 1
Phenanthrene ND ug/L 07/12/21 21:56 85-01-807/10/21 16:399.1 1
Phenol ND ug/L 07/12/21 21:56 108-95-207/10/21 16:399.1 1
Pyrene ND ug/L 07/12/21 21:56 129-00-007/10/21 16:399.1 1
1,2,4-Trichlorobenzene ND ug/L 07/12/21 21:56 120-82-107/10/21 16:399.1 1
2,4,5-Trichlorophenol ND ug/L 07/12/21 21:56 95-95-407/10/21 16:399.1 1
2,4,6-Trichlorophenol ND ug/L 07/12/21 21:56 88-06-207/10/21 16:399.1 1
Surrogates
Nitrobenzene-d5 (S)74 %07/12/21 21:56 4165-60-007/10/21 16:3910-144 1
2-Fluorobiphenyl (S)66 %07/12/21 21:56 321-60-807/10/21 16:3910-130 1
Terphenyl-d14 (S)116 %07/12/21 21:56 1718-51-007/10/21 16:3934-163 1
Phenol-d6 (S)40 %07/12/21 21:56 13127-88-307/10/21 16:3910-130 1
2-Fluorophenol (S)47 %07/12/21 21:56 367-12-407/10/21 16:3910-130 1
2,4,6-Tribromophenol (S)87 %07/12/21 21:56 118-79-607/10/21 16:3910-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-2 Lab ID: 92548712005 Collected: 07/07/21 16:20 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 07/13/21 20:40 67-64-125.0 1
Benzene ND ug/L 07/13/21 20:40 71-43-21.0 1
Bromobenzene ND ug/L 07/13/21 20:40 108-86-11.0 1
Bromochloromethane ND ug/L 07/13/21 20:40 74-97-51.0 1
Bromodichloromethane ND ug/L 07/13/21 20:40 75-27-41.0 1
Bromoform ND ug/L 07/13/21 20:40 75-25-21.0 1
Bromomethane ND ug/L 07/13/21 20:40 74-83-92.0 1
2-Butanone (MEK)ND ug/L 07/13/21 20:40 78-93-35.0 1
Carbon tetrachloride ND ug/L 07/13/21 20:40 56-23-51.0 1
Chlorobenzene ND ug/L 07/13/21 20:40 108-90-71.0 1
Chloroethane ND ug/L 07/13/21 20:40 75-00-31.0 1
Chloroform ND ug/L 07/13/21 20:40 67-66-31.0 1
Chloromethane ND ug/L 07/13/21 20:40 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/13/21 20:40 95-49-81.0 1
4-Chlorotoluene ND ug/L 07/13/21 20:40 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 07/13/21 20:40 96-12-82.0 1
Dibromochloromethane ND ug/L 07/13/21 20:40 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 07/13/21 20:40 106-93-41.0 1
Dibromomethane ND ug/L 07/13/21 20:40 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 07/13/21 20:40 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 07/13/21 20:40 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 07/13/21 20:40 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 07/13/21 20:40 75-71-8 v11.0 1
1,1-Dichloroethane 7.4 ug/L 07/13/21 20:40 75-34-31.0 1
1,2-Dichloroethane ND ug/L 07/13/21 20:40 107-06-21.0 1
1,1-Dichloroethene 30.7 ug/L 07/13/21 20:40 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 07/13/21 20:40 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 07/13/21 20:40 156-60-51.0 1
1,2-Dichloropropane ND ug/L 07/13/21 20:40 78-87-51.0 1
1,3-Dichloropropane ND ug/L 07/13/21 20:40 142-28-91.0 1
2,2-Dichloropropane ND ug/L 07/13/21 20:40 594-20-71.0 1
1,1-Dichloropropene ND ug/L 07/13/21 20:40 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 07/13/21 20:40 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 07/13/21 20:40 10061-02-61.0 1
Diisopropyl ether ND ug/L 07/13/21 20:40 108-20-31.0 1
Ethylbenzene ND ug/L 07/13/21 20:40 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 07/13/21 20:40 87-68-32.0 1
2-Hexanone ND ug/L 07/13/21 20:40 591-78-65.0 1
p-Isopropyltoluene ND ug/L 07/13/21 20:40 99-87-61.0 1
Methylene Chloride ND ug/L 07/13/21 20:40 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/13/21 20:40 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 07/13/21 20:40 1634-04-41.0 1
Naphthalene ND ug/L 07/13/21 20:40 91-20-31.0 1
Styrene ND ug/L 07/13/21 20:40 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 07/13/21 20:40 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 07/13/21 20:40 79-34-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-2 Lab ID: 92548712005 Collected: 07/07/21 16:20 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Tetrachloroethene ND ug/L 07/13/21 20:40 127-18-41.0 1
Toluene ND ug/L 07/13/21 20:40 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 07/13/21 20:40 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 07/13/21 20:40 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 07/13/21 20:40 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 07/13/21 20:40 79-00-51.0 1
Trichloroethene ND ug/L 07/13/21 20:40 79-01-61.0 1
Trichlorofluoromethane ND ug/L 07/13/21 20:40 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/13/21 20:40 96-18-41.0 1
Vinyl acetate ND ug/L 07/13/21 20:40 108-05-42.0 1
Vinyl chloride ND ug/L 07/13/21 20:40 75-01-41.0 1
Xylene (Total)ND ug/L 07/13/21 20:40 1330-20-71.0 1
m&p-Xylene ND ug/L 07/13/21 20:40 179601-23-12.0 1
o-Xylene ND ug/L 07/13/21 20:40 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)95 %07/13/21 20:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %07/13/21 20:40 17060-07-070-130 1
Toluene-d8 (S)101 %07/13/21 20:40 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.632 ug/L 07/20/21 14:32 18540-29-907/20/21 14:320.500 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-4 Lab ID: 92548712006 Collected: 07/07/21 17:30 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND ug/L 07/19/21 20:24 7440-38-207/16/21 12:2010.0 1
Barium 45.7 ug/L 07/19/21 20:24 7440-39-307/16/21 12:205.0 1
Cadmium ND ug/L 07/19/21 20:24 7440-43-907/16/21 12:201.0 1
Chromium 16.3 ug/L 07/19/21 20:24 7440-47-307/16/21 12:205.0 1
Lead ND ug/L 07/19/21 20:24 7439-92-107/16/21 12:205.0 1
Selenium ND ug/L 07/19/21 20:24 7782-49-2 BC07/16/21 12:2010.0 1
Silver ND ug/L 07/19/21 20:24 7440-22-407/16/21 12:205.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 07/13/21 13:52 7439-97-607/12/21 14:590.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/12/21 22:25 83-32-907/10/21 16:3910.0 1
Acenaphthylene ND ug/L 07/12/21 22:25 208-96-807/10/21 16:3910.0 1
Aniline ND ug/L 07/12/21 22:25 62-53-307/10/21 16:3910.0 1
Anthracene ND ug/L 07/12/21 22:25 120-12-707/10/21 16:3910.0 1
Benzo(a)anthracene ND ug/L 07/12/21 22:25 56-55-307/10/21 16:3910.0 1
Benzo(a)pyrene ND ug/L 07/12/21 22:25 50-32-807/10/21 16:3910.0 1
Benzo(b)fluoranthene ND ug/L 07/12/21 22:25 205-99-207/10/21 16:3910.0 1
Benzo(g,h,i)perylene ND ug/L 07/12/21 22:25 191-24-207/10/21 16:3910.0 1
Benzo(k)fluoranthene ND ug/L 07/12/21 22:25 207-08-907/10/21 16:3910.0 1
Benzoic Acid ND ug/L 07/12/21 22:25 65-85-007/10/21 16:3950.0 1
Benzyl alcohol ND ug/L 07/12/21 22:25 100-51-607/10/21 16:3920.0 1
4-Bromophenylphenyl ether ND ug/L 07/12/21 22:25 101-55-307/10/21 16:3910.0 1
Butylbenzylphthalate ND ug/L 07/12/21 22:25 85-68-707/10/21 16:3910.0 1
4-Chloro-3-methylphenol ND ug/L 07/12/21 22:25 59-50-707/10/21 16:3910.0 1
4-Chloroaniline ND ug/L 07/12/21 22:25 106-47-807/10/21 16:3920.0 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/21 22:25 111-91-107/10/21 16:3910.0 1
bis(2-Chloroethyl) ether ND ug/L 07/12/21 22:25 111-44-407/10/21 16:3910.0 1
2-Chloronaphthalene ND ug/L 07/12/21 22:25 91-58-707/10/21 16:3910.0 1
2-Chlorophenol ND ug/L 07/12/21 22:25 95-57-807/10/21 16:3910.0 1
4-Chlorophenylphenyl ether ND ug/L 07/12/21 22:25 7005-72-307/10/21 16:3910.0 1
Chrysene ND ug/L 07/12/21 22:25 218-01-907/10/21 16:3910.0 1
Dibenz(a,h)anthracene ND ug/L 07/12/21 22:25 53-70-307/10/21 16:3910.0 1
Dibenzofuran ND ug/L 07/12/21 22:25 132-64-907/10/21 16:3910.0 1
1,2-Dichlorobenzene ND ug/L 07/12/21 22:25 95-50-107/10/21 16:3910.0 1
1,3-Dichlorobenzene ND ug/L 07/12/21 22:25 541-73-107/10/21 16:3910.0 1
1,4-Dichlorobenzene ND ug/L 07/12/21 22:25 106-46-707/10/21 16:3910.0 1
3,3'-Dichlorobenzidine ND ug/L 07/12/21 22:25 91-94-107/10/21 16:3920.0 1
2,4-Dichlorophenol ND ug/L 07/12/21 22:25 120-83-207/10/21 16:3910.0 1
Diethylphthalate ND ug/L 07/12/21 22:25 84-66-207/10/21 16:3910.0 1
2,4-Dimethylphenol ND ug/L 07/12/21 22:25 105-67-907/10/21 16:3910.0 1
Dimethylphthalate ND ug/L 07/12/21 22:25 131-11-307/10/21 16:3910.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-4 Lab ID: 92548712006 Collected: 07/07/21 17:30 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 07/12/21 22:25 84-74-207/10/21 16:3910.0 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/21 22:25 534-52-107/10/21 16:3920.0 1
2,4-Dinitrophenol ND ug/L 07/12/21 22:25 51-28-507/10/21 16:3950.0 1
2,4-Dinitrotoluene ND ug/L 07/12/21 22:25 121-14-207/10/21 16:3910.0 1
2,6-Dinitrotoluene ND ug/L 07/12/21 22:25 606-20-207/10/21 16:3910.0 1
Di-n-octylphthalate ND ug/L 07/12/21 22:25 117-84-007/10/21 16:3910.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/21 22:25 117-81-707/10/21 16:396.0 1
Fluoranthene ND ug/L 07/12/21 22:25 206-44-007/10/21 16:3910.0 1
Fluorene ND ug/L 07/12/21 22:25 86-73-707/10/21 16:3910.0 1
Hexachloro-1,3-butadiene ND ug/L 07/12/21 22:25 87-68-307/10/21 16:3910.0 1
Hexachlorobenzene ND ug/L 07/12/21 22:25 118-74-107/10/21 16:3910.0 1
Hexachlorocyclopentadiene ND ug/L 07/12/21 22:25 77-47-407/10/21 16:3910.0 1
Hexachloroethane ND ug/L 07/12/21 22:25 67-72-107/10/21 16:3910.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/21 22:25 193-39-507/10/21 16:3910.0 1
Isophorone ND ug/L 07/12/21 22:25 78-59-107/10/21 16:3910.0 1
1-Methylnaphthalene ND ug/L 07/12/21 22:25 90-12-007/10/21 16:3910.0 1
2-Methylnaphthalene ND ug/L 07/12/21 22:25 91-57-607/10/21 16:3910.0 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/21 22:25 95-48-707/10/21 16:3910.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/21 22:25 15831-10-407/10/21 16:3910.0 1
Naphthalene ND ug/L 07/12/21 22:25 91-20-307/10/21 16:3910.0 1
2-Nitroaniline ND ug/L 07/12/21 22:25 88-74-407/10/21 16:3920.0 1
3-Nitroaniline ND ug/L 07/12/21 22:25 99-09-207/10/21 16:3920.0 1
4-Nitroaniline ND ug/L 07/12/21 22:25 100-01-607/10/21 16:3920.0 1
Nitrobenzene ND ug/L 07/12/21 22:25 98-95-307/10/21 16:3910.0 1
2-Nitrophenol ND ug/L 07/12/21 22:25 88-75-5 v107/10/21 16:3910.0 1
4-Nitrophenol ND ug/L 07/12/21 22:25 100-02-707/10/21 16:3950.0 1
N-Nitrosodimethylamine ND ug/L 07/12/21 22:25 62-75-907/10/21 16:3910.0 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/21 22:25 621-64-707/10/21 16:3910.0 1
N-Nitrosodiphenylamine ND ug/L 07/12/21 22:25 86-30-607/10/21 16:3910.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/21 22:25 108-60-107/10/21 16:3910.0 1
Pentachlorophenol ND ug/L 07/12/21 22:25 87-86-507/10/21 16:3920.0 1
Phenanthrene ND ug/L 07/12/21 22:25 85-01-807/10/21 16:3910.0 1
Phenol ND ug/L 07/12/21 22:25 108-95-207/10/21 16:3910.0 1
Pyrene ND ug/L 07/12/21 22:25 129-00-007/10/21 16:3910.0 1
1,2,4-Trichlorobenzene ND ug/L 07/12/21 22:25 120-82-107/10/21 16:3910.0 1
2,4,5-Trichlorophenol ND ug/L 07/12/21 22:25 95-95-407/10/21 16:3910.0 1
2,4,6-Trichlorophenol ND ug/L 07/12/21 22:25 88-06-207/10/21 16:3910.0 1
Surrogates
Nitrobenzene-d5 (S)83 %07/12/21 22:25 4165-60-007/10/21 16:3910-144 1
2-Fluorobiphenyl (S)80 %07/12/21 22:25 321-60-807/10/21 16:3910-130 1
Terphenyl-d14 (S)98 %07/12/21 22:25 1718-51-007/10/21 16:3934-163 1
Phenol-d6 (S)43 %07/12/21 22:25 13127-88-307/10/21 16:3910-130 1
2-Fluorophenol (S)58 %07/12/21 22:25 367-12-407/10/21 16:3910-130 1
2,4,6-Tribromophenol (S)97 %07/12/21 22:25 118-79-607/10/21 16:3910-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-4 Lab ID: 92548712006 Collected: 07/07/21 17:30 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 07/13/21 20:58 67-64-125.0 1
Benzene ND ug/L 07/13/21 20:58 71-43-21.0 1
Bromobenzene ND ug/L 07/13/21 20:58 108-86-11.0 1
Bromochloromethane ND ug/L 07/13/21 20:58 74-97-51.0 1
Bromodichloromethane ND ug/L 07/13/21 20:58 75-27-41.0 1
Bromoform ND ug/L 07/13/21 20:58 75-25-21.0 1
Bromomethane ND ug/L 07/13/21 20:58 74-83-92.0 1
2-Butanone (MEK)ND ug/L 07/13/21 20:58 78-93-35.0 1
Carbon tetrachloride ND ug/L 07/13/21 20:58 56-23-51.0 1
Chlorobenzene ND ug/L 07/13/21 20:58 108-90-71.0 1
Chloroethane ND ug/L 07/13/21 20:58 75-00-31.0 1
Chloroform ND ug/L 07/13/21 20:58 67-66-31.0 1
Chloromethane ND ug/L 07/13/21 20:58 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/13/21 20:58 95-49-81.0 1
4-Chlorotoluene ND ug/L 07/13/21 20:58 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 07/13/21 20:58 96-12-82.0 1
Dibromochloromethane ND ug/L 07/13/21 20:58 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 07/13/21 20:58 106-93-41.0 1
Dibromomethane ND ug/L 07/13/21 20:58 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 07/13/21 20:58 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 07/13/21 20:58 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 07/13/21 20:58 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 07/13/21 20:58 75-71-8 v11.0 1
1,1-Dichloroethane ND ug/L 07/13/21 20:58 75-34-31.0 1
1,2-Dichloroethane ND ug/L 07/13/21 20:58 107-06-21.0 1
1,1-Dichloroethene ND ug/L 07/13/21 20:58 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 07/13/21 20:58 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 07/13/21 20:58 156-60-51.0 1
1,2-Dichloropropane ND ug/L 07/13/21 20:58 78-87-51.0 1
1,3-Dichloropropane ND ug/L 07/13/21 20:58 142-28-91.0 1
2,2-Dichloropropane ND ug/L 07/13/21 20:58 594-20-71.0 1
1,1-Dichloropropene ND ug/L 07/13/21 20:58 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 07/13/21 20:58 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 07/13/21 20:58 10061-02-61.0 1
Diisopropyl ether ND ug/L 07/13/21 20:58 108-20-31.0 1
Ethylbenzene ND ug/L 07/13/21 20:58 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 07/13/21 20:58 87-68-32.0 1
2-Hexanone ND ug/L 07/13/21 20:58 591-78-65.0 1
p-Isopropyltoluene ND ug/L 07/13/21 20:58 99-87-61.0 1
Methylene Chloride ND ug/L 07/13/21 20:58 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/13/21 20:58 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 07/13/21 20:58 1634-04-41.0 1
Naphthalene ND ug/L 07/13/21 20:58 91-20-31.0 1
Styrene ND ug/L 07/13/21 20:58 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 07/13/21 20:58 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 07/13/21 20:58 79-34-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-4 Lab ID: 92548712006 Collected: 07/07/21 17:30 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Tetrachloroethene ND ug/L 07/13/21 20:58 127-18-41.0 1
Toluene ND ug/L 07/13/21 20:58 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 07/13/21 20:58 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 07/13/21 20:58 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 07/13/21 20:58 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 07/13/21 20:58 79-00-51.0 1
Trichloroethene ND ug/L 07/13/21 20:58 79-01-61.0 1
Trichlorofluoromethane ND ug/L 07/13/21 20:58 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/13/21 20:58 96-18-41.0 1
Vinyl acetate ND ug/L 07/13/21 20:58 108-05-42.0 1
Vinyl chloride ND ug/L 07/13/21 20:58 75-01-41.0 1
Xylene (Total)ND ug/L 07/13/21 20:58 1330-20-71.0 1
m&p-Xylene ND ug/L 07/13/21 20:58 179601-23-12.0 1
o-Xylene ND ug/L 07/13/21 20:58 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)97 %07/13/21 20:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %07/13/21 20:58 17060-07-070-130 1
Toluene-d8 (S)101 %07/13/21 20:58 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 14.4 ug/L 07/20/21 14:39 18540-29-907/20/21 14:390.500 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-3 Lab ID: 92548712007 Collected: 07/07/21 18:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND ug/L 07/19/21 20:27 7440-38-207/16/21 12:2010.0 1
Barium 52.2 ug/L 07/19/21 20:27 7440-39-307/16/21 12:205.0 1
Cadmium ND ug/L 07/19/21 20:27 7440-43-907/16/21 12:201.0 1
Chromium 5.9 ug/L 07/19/21 20:27 7440-47-307/16/21 12:205.0 1
Lead ND ug/L 07/19/21 20:27 7439-92-107/16/21 12:205.0 1
Selenium ND ug/L 07/19/21 20:27 7782-49-2 BC07/16/21 12:2010.0 1
Silver ND ug/L 07/19/21 20:27 7440-22-407/16/21 12:205.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 07/13/21 13:59 7439-97-607/12/21 14:590.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/12/21 22:55 83-32-907/10/21 16:399.1 1
Acenaphthylene ND ug/L 07/12/21 22:55 208-96-807/10/21 16:399.1 1
Aniline ND ug/L 07/12/21 22:55 62-53-307/10/21 16:399.1 1
Anthracene ND ug/L 07/12/21 22:55 120-12-707/10/21 16:399.1 1
Benzo(a)anthracene ND ug/L 07/12/21 22:55 56-55-307/10/21 16:399.1 1
Benzo(a)pyrene ND ug/L 07/12/21 22:55 50-32-807/10/21 16:399.1 1
Benzo(b)fluoranthene ND ug/L 07/12/21 22:55 205-99-207/10/21 16:399.1 1
Benzo(g,h,i)perylene ND ug/L 07/12/21 22:55 191-24-207/10/21 16:399.1 1
Benzo(k)fluoranthene ND ug/L 07/12/21 22:55 207-08-907/10/21 16:399.1 1
Benzoic Acid ND ug/L 07/12/21 22:55 65-85-007/10/21 16:3945.5 1
Benzyl alcohol ND ug/L 07/12/21 22:55 100-51-607/10/21 16:3918.2 1
4-Bromophenylphenyl ether ND ug/L 07/12/21 22:55 101-55-307/10/21 16:399.1 1
Butylbenzylphthalate ND ug/L 07/12/21 22:55 85-68-707/10/21 16:399.1 1
4-Chloro-3-methylphenol ND ug/L 07/12/21 22:55 59-50-707/10/21 16:399.1 1
4-Chloroaniline ND ug/L 07/12/21 22:55 106-47-807/10/21 16:3918.2 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/21 22:55 111-91-107/10/21 16:399.1 1
bis(2-Chloroethyl) ether ND ug/L 07/12/21 22:55 111-44-407/10/21 16:399.1 1
2-Chloronaphthalene ND ug/L 07/12/21 22:55 91-58-707/10/21 16:399.1 1
2-Chlorophenol ND ug/L 07/12/21 22:55 95-57-807/10/21 16:399.1 1
4-Chlorophenylphenyl ether ND ug/L 07/12/21 22:55 7005-72-307/10/21 16:399.1 1
Chrysene ND ug/L 07/12/21 22:55 218-01-907/10/21 16:399.1 1
Dibenz(a,h)anthracene ND ug/L 07/12/21 22:55 53-70-307/10/21 16:399.1 1
Dibenzofuran ND ug/L 07/12/21 22:55 132-64-907/10/21 16:399.1 1
1,2-Dichlorobenzene ND ug/L 07/12/21 22:55 95-50-107/10/21 16:399.1 1
1,3-Dichlorobenzene ND ug/L 07/12/21 22:55 541-73-107/10/21 16:399.1 1
1,4-Dichlorobenzene ND ug/L 07/12/21 22:55 106-46-707/10/21 16:399.1 1
3,3'-Dichlorobenzidine ND ug/L 07/12/21 22:55 91-94-107/10/21 16:3918.2 1
2,4-Dichlorophenol ND ug/L 07/12/21 22:55 120-83-207/10/21 16:399.1 1
Diethylphthalate ND ug/L 07/12/21 22:55 84-66-207/10/21 16:399.1 1
2,4-Dimethylphenol ND ug/L 07/12/21 22:55 105-67-907/10/21 16:399.1 1
Dimethylphthalate ND ug/L 07/12/21 22:55 131-11-307/10/21 16:399.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-3 Lab ID: 92548712007 Collected: 07/07/21 18:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 07/12/21 22:55 84-74-207/10/21 16:399.1 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/21 22:55 534-52-107/10/21 16:3918.2 1
2,4-Dinitrophenol ND ug/L 07/12/21 22:55 51-28-507/10/21 16:3945.5 1
2,4-Dinitrotoluene ND ug/L 07/12/21 22:55 121-14-207/10/21 16:399.1 1
2,6-Dinitrotoluene ND ug/L 07/12/21 22:55 606-20-207/10/21 16:399.1 1
Di-n-octylphthalate ND ug/L 07/12/21 22:55 117-84-007/10/21 16:399.1 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/21 22:55 117-81-707/10/21 16:395.5 1
Fluoranthene ND ug/L 07/12/21 22:55 206-44-007/10/21 16:399.1 1
Fluorene ND ug/L 07/12/21 22:55 86-73-707/10/21 16:399.1 1
Hexachloro-1,3-butadiene ND ug/L 07/12/21 22:55 87-68-307/10/21 16:399.1 1
Hexachlorobenzene ND ug/L 07/12/21 22:55 118-74-107/10/21 16:399.1 1
Hexachlorocyclopentadiene ND ug/L 07/12/21 22:55 77-47-407/10/21 16:399.1 1
Hexachloroethane ND ug/L 07/12/21 22:55 67-72-107/10/21 16:399.1 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/21 22:55 193-39-507/10/21 16:399.1 1
Isophorone ND ug/L 07/12/21 22:55 78-59-107/10/21 16:399.1 1
1-Methylnaphthalene ND ug/L 07/12/21 22:55 90-12-007/10/21 16:399.1 1
2-Methylnaphthalene ND ug/L 07/12/21 22:55 91-57-607/10/21 16:399.1 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/21 22:55 95-48-707/10/21 16:399.1 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/21 22:55 15831-10-407/10/21 16:399.1 1
Naphthalene ND ug/L 07/12/21 22:55 91-20-307/10/21 16:399.1 1
2-Nitroaniline ND ug/L 07/12/21 22:55 88-74-407/10/21 16:3918.2 1
3-Nitroaniline ND ug/L 07/12/21 22:55 99-09-207/10/21 16:3918.2 1
4-Nitroaniline ND ug/L 07/12/21 22:55 100-01-607/10/21 16:3918.2 1
Nitrobenzene ND ug/L 07/12/21 22:55 98-95-307/10/21 16:399.1 1
2-Nitrophenol ND ug/L 07/12/21 22:55 88-75-5 v107/10/21 16:399.1 1
4-Nitrophenol ND ug/L 07/12/21 22:55 100-02-707/10/21 16:3945.5 1
N-Nitrosodimethylamine ND ug/L 07/12/21 22:55 62-75-907/10/21 16:399.1 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/21 22:55 621-64-707/10/21 16:399.1 1
N-Nitrosodiphenylamine ND ug/L 07/12/21 22:55 86-30-607/10/21 16:399.1 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/21 22:55 108-60-107/10/21 16:399.1 1
Pentachlorophenol ND ug/L 07/12/21 22:55 87-86-507/10/21 16:3918.2 1
Phenanthrene ND ug/L 07/12/21 22:55 85-01-807/10/21 16:399.1 1
Phenol ND ug/L 07/12/21 22:55 108-95-207/10/21 16:399.1 1
Pyrene ND ug/L 07/12/21 22:55 129-00-007/10/21 16:399.1 1
1,2,4-Trichlorobenzene ND ug/L 07/12/21 22:55 120-82-107/10/21 16:399.1 1
2,4,5-Trichlorophenol ND ug/L 07/12/21 22:55 95-95-407/10/21 16:399.1 1
2,4,6-Trichlorophenol ND ug/L 07/12/21 22:55 88-06-207/10/21 16:399.1 1
Surrogates
Nitrobenzene-d5 (S)40 %07/12/21 22:55 4165-60-007/10/21 16:3910-144 1
2-Fluorobiphenyl (S)41 %07/12/21 22:55 321-60-807/10/21 16:3910-130 1
Terphenyl-d14 (S)89 %07/12/21 22:55 1718-51-007/10/21 16:3934-163 1
Phenol-d6 (S)21 %07/12/21 22:55 13127-88-307/10/21 16:3910-130 1
2-Fluorophenol (S)26 %07/12/21 22:55 367-12-407/10/21 16:3910-130 1
2,4,6-Tribromophenol (S)73 %07/12/21 22:55 118-79-607/10/21 16:3910-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-3 Lab ID: 92548712007 Collected: 07/07/21 18:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 07/13/21 21:17 67-64-125.0 1
Benzene ND ug/L 07/13/21 21:17 71-43-21.0 1
Bromobenzene ND ug/L 07/13/21 21:17 108-86-11.0 1
Bromochloromethane ND ug/L 07/13/21 21:17 74-97-51.0 1
Bromodichloromethane ND ug/L 07/13/21 21:17 75-27-41.0 1
Bromoform ND ug/L 07/13/21 21:17 75-25-21.0 1
Bromomethane ND ug/L 07/13/21 21:17 74-83-92.0 1
2-Butanone (MEK)ND ug/L 07/13/21 21:17 78-93-35.0 1
Carbon tetrachloride ND ug/L 07/13/21 21:17 56-23-51.0 1
Chlorobenzene ND ug/L 07/13/21 21:17 108-90-71.0 1
Chloroethane ND ug/L 07/13/21 21:17 75-00-31.0 1
Chloroform ND ug/L 07/13/21 21:17 67-66-31.0 1
Chloromethane ND ug/L 07/13/21 21:17 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/13/21 21:17 95-49-81.0 1
4-Chlorotoluene ND ug/L 07/13/21 21:17 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 07/13/21 21:17 96-12-82.0 1
Dibromochloromethane ND ug/L 07/13/21 21:17 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 07/13/21 21:17 106-93-41.0 1
Dibromomethane ND ug/L 07/13/21 21:17 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 07/13/21 21:17 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 07/13/21 21:17 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 07/13/21 21:17 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 07/13/21 21:17 75-71-8 v11.0 1
1,1-Dichloroethane ND ug/L 07/13/21 21:17 75-34-31.0 1
1,2-Dichloroethane ND ug/L 07/13/21 21:17 107-06-21.0 1
1,1-Dichloroethene ND ug/L 07/13/21 21:17 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 07/13/21 21:17 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 07/13/21 21:17 156-60-51.0 1
1,2-Dichloropropane ND ug/L 07/13/21 21:17 78-87-51.0 1
1,3-Dichloropropane ND ug/L 07/13/21 21:17 142-28-91.0 1
2,2-Dichloropropane ND ug/L 07/13/21 21:17 594-20-71.0 1
1,1-Dichloropropene ND ug/L 07/13/21 21:17 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 07/13/21 21:17 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 07/13/21 21:17 10061-02-61.0 1
Diisopropyl ether ND ug/L 07/13/21 21:17 108-20-31.0 1
Ethylbenzene ND ug/L 07/13/21 21:17 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 07/13/21 21:17 87-68-32.0 1
2-Hexanone ND ug/L 07/13/21 21:17 591-78-65.0 1
p-Isopropyltoluene ND ug/L 07/13/21 21:17 99-87-61.0 1
Methylene Chloride ND ug/L 07/13/21 21:17 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/13/21 21:17 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 07/13/21 21:17 1634-04-41.0 1
Naphthalene ND ug/L 07/13/21 21:17 91-20-31.0 1
Styrene ND ug/L 07/13/21 21:17 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 07/13/21 21:17 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 07/13/21 21:17 79-34-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: MW-3 Lab ID: 92548712007 Collected: 07/07/21 18:50 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Tetrachloroethene ND ug/L 07/13/21 21:17 127-18-41.0 1
Toluene ND ug/L 07/13/21 21:17 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 07/13/21 21:17 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 07/13/21 21:17 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 07/13/21 21:17 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 07/13/21 21:17 79-00-51.0 1
Trichloroethene ND ug/L 07/13/21 21:17 79-01-61.0 1
Trichlorofluoromethane ND ug/L 07/13/21 21:17 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/13/21 21:17 96-18-41.0 1
Vinyl acetate ND ug/L 07/13/21 21:17 108-05-42.0 1
Vinyl chloride ND ug/L 07/13/21 21:17 75-01-41.0 1
Xylene (Total)ND ug/L 07/13/21 21:17 1330-20-71.0 1
m&p-Xylene ND ug/L 07/13/21 21:17 179601-23-12.0 1
o-Xylene ND ug/L 07/13/21 21:17 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)96 %07/13/21 21:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %07/13/21 21:17 17060-07-070-130 1
Toluene-d8 (S)101 %07/13/21 21:17 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 07/20/21 14:47 18540-29-907/20/21 14:470.500 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: TW-1 Lab ID: 92548712008 Collected: 07/07/21 19:40 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND ug/L 07/19/21 20:31 7440-38-207/16/21 12:2010.0 1
Barium 37.4 ug/L 07/19/21 20:31 7440-39-307/16/21 12:205.0 1
Cadmium ND ug/L 07/19/21 20:31 7440-43-907/16/21 12:201.0 1
Chromium ND ug/L 07/19/21 20:31 7440-47-307/16/21 12:205.0 1
Lead ND ug/L 07/19/21 20:31 7439-92-107/16/21 12:205.0 1
Selenium ND ug/L 07/19/21 20:31 7782-49-2 BC07/16/21 12:2010.0 1
Silver ND ug/L 07/19/21 20:31 7440-22-407/16/21 12:205.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 07/13/21 13:57 7439-97-607/12/21 14:590.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/12/21 23:25 83-32-907/10/21 16:398.3 1
Acenaphthylene ND ug/L 07/12/21 23:25 208-96-807/10/21 16:398.3 1
Aniline ND ug/L 07/12/21 23:25 62-53-307/10/21 16:398.3 1
Anthracene ND ug/L 07/12/21 23:25 120-12-707/10/21 16:398.3 1
Benzo(a)anthracene ND ug/L 07/12/21 23:25 56-55-307/10/21 16:398.3 1
Benzo(a)pyrene ND ug/L 07/12/21 23:25 50-32-807/10/21 16:398.3 1
Benzo(b)fluoranthene ND ug/L 07/12/21 23:25 205-99-207/10/21 16:398.3 1
Benzo(g,h,i)perylene ND ug/L 07/12/21 23:25 191-24-207/10/21 16:398.3 1
Benzo(k)fluoranthene ND ug/L 07/12/21 23:25 207-08-907/10/21 16:398.3 1
Benzoic Acid ND ug/L 07/12/21 23:25 65-85-007/10/21 16:3941.7 1
Benzyl alcohol ND ug/L 07/12/21 23:25 100-51-607/10/21 16:3916.7 1
4-Bromophenylphenyl ether ND ug/L 07/12/21 23:25 101-55-307/10/21 16:398.3 1
Butylbenzylphthalate ND ug/L 07/12/21 23:25 85-68-707/10/21 16:398.3 1
4-Chloro-3-methylphenol ND ug/L 07/12/21 23:25 59-50-707/10/21 16:398.3 1
4-Chloroaniline ND ug/L 07/12/21 23:25 106-47-807/10/21 16:3916.7 1
bis(2-Chloroethoxy)methane ND ug/L 07/12/21 23:25 111-91-107/10/21 16:398.3 1
bis(2-Chloroethyl) ether ND ug/L 07/12/21 23:25 111-44-407/10/21 16:398.3 1
2-Chloronaphthalene ND ug/L 07/12/21 23:25 91-58-707/10/21 16:398.3 1
2-Chlorophenol ND ug/L 07/12/21 23:25 95-57-807/10/21 16:398.3 1
4-Chlorophenylphenyl ether ND ug/L 07/12/21 23:25 7005-72-307/10/21 16:398.3 1
Chrysene ND ug/L 07/12/21 23:25 218-01-907/10/21 16:398.3 1
Dibenz(a,h)anthracene ND ug/L 07/12/21 23:25 53-70-307/10/21 16:398.3 1
Dibenzofuran ND ug/L 07/12/21 23:25 132-64-907/10/21 16:398.3 1
1,2-Dichlorobenzene ND ug/L 07/12/21 23:25 95-50-107/10/21 16:398.3 1
1,3-Dichlorobenzene ND ug/L 07/12/21 23:25 541-73-107/10/21 16:398.3 1
1,4-Dichlorobenzene ND ug/L 07/12/21 23:25 106-46-707/10/21 16:398.3 1
3,3'-Dichlorobenzidine ND ug/L 07/12/21 23:25 91-94-107/10/21 16:3916.7 1
2,4-Dichlorophenol ND ug/L 07/12/21 23:25 120-83-207/10/21 16:398.3 1
Diethylphthalate ND ug/L 07/12/21 23:25 84-66-207/10/21 16:398.3 1
2,4-Dimethylphenol ND ug/L 07/12/21 23:25 105-67-907/10/21 16:398.3 1
Dimethylphthalate ND ug/L 07/12/21 23:25 131-11-307/10/21 16:398.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: TW-1 Lab ID: 92548712008 Collected: 07/07/21 19:40 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 07/12/21 23:25 84-74-207/10/21 16:398.3 1
4,6-Dinitro-2-methylphenol ND ug/L 07/12/21 23:25 534-52-107/10/21 16:3916.7 1
2,4-Dinitrophenol ND ug/L 07/12/21 23:25 51-28-507/10/21 16:3941.7 1
2,4-Dinitrotoluene ND ug/L 07/12/21 23:25 121-14-207/10/21 16:398.3 1
2,6-Dinitrotoluene ND ug/L 07/12/21 23:25 606-20-207/10/21 16:398.3 1
Di-n-octylphthalate ND ug/L 07/12/21 23:25 117-84-007/10/21 16:398.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/12/21 23:25 117-81-707/10/21 16:395.0 1
Fluoranthene ND ug/L 07/12/21 23:25 206-44-007/10/21 16:398.3 1
Fluorene ND ug/L 07/12/21 23:25 86-73-707/10/21 16:398.3 1
Hexachloro-1,3-butadiene ND ug/L 07/12/21 23:25 87-68-307/10/21 16:398.3 1
Hexachlorobenzene ND ug/L 07/12/21 23:25 118-74-107/10/21 16:398.3 1
Hexachlorocyclopentadiene ND ug/L 07/12/21 23:25 77-47-407/10/21 16:398.3 1
Hexachloroethane ND ug/L 07/12/21 23:25 67-72-107/10/21 16:398.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/12/21 23:25 193-39-507/10/21 16:398.3 1
Isophorone ND ug/L 07/12/21 23:25 78-59-107/10/21 16:398.3 1
1-Methylnaphthalene ND ug/L 07/12/21 23:25 90-12-007/10/21 16:398.3 1
2-Methylnaphthalene ND ug/L 07/12/21 23:25 91-57-607/10/21 16:398.3 1
2-Methylphenol(o-Cresol)ND ug/L 07/12/21 23:25 95-48-707/10/21 16:398.3 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/12/21 23:25 15831-10-407/10/21 16:398.3 1
Naphthalene ND ug/L 07/12/21 23:25 91-20-307/10/21 16:398.3 1
2-Nitroaniline ND ug/L 07/12/21 23:25 88-74-407/10/21 16:3916.7 1
3-Nitroaniline ND ug/L 07/12/21 23:25 99-09-207/10/21 16:3916.7 1
4-Nitroaniline ND ug/L 07/12/21 23:25 100-01-607/10/21 16:3916.7 1
Nitrobenzene ND ug/L 07/12/21 23:25 98-95-307/10/21 16:398.3 1
2-Nitrophenol ND ug/L 07/12/21 23:25 88-75-5 v107/10/21 16:398.3 1
4-Nitrophenol ND ug/L 07/12/21 23:25 100-02-707/10/21 16:3941.7 1
N-Nitrosodimethylamine ND ug/L 07/12/21 23:25 62-75-907/10/21 16:398.3 1
N-Nitroso-di-n-propylamine ND ug/L 07/12/21 23:25 621-64-707/10/21 16:398.3 1
N-Nitrosodiphenylamine ND ug/L 07/12/21 23:25 86-30-607/10/21 16:398.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/12/21 23:25 108-60-107/10/21 16:398.3 1
Pentachlorophenol ND ug/L 07/12/21 23:25 87-86-507/10/21 16:3916.7 1
Phenanthrene ND ug/L 07/12/21 23:25 85-01-807/10/21 16:398.3 1
Phenol ND ug/L 07/12/21 23:25 108-95-207/10/21 16:398.3 1
Pyrene ND ug/L 07/12/21 23:25 129-00-007/10/21 16:398.3 1
1,2,4-Trichlorobenzene ND ug/L 07/12/21 23:25 120-82-107/10/21 16:398.3 1
2,4,5-Trichlorophenol ND ug/L 07/12/21 23:25 95-95-407/10/21 16:398.3 1
2,4,6-Trichlorophenol ND ug/L 07/12/21 23:25 88-06-207/10/21 16:398.3 1
Surrogates
Nitrobenzene-d5 (S)73 %07/12/21 23:25 4165-60-007/10/21 16:3910-144 1
2-Fluorobiphenyl (S)68 %07/12/21 23:25 321-60-807/10/21 16:3910-130 1
Terphenyl-d14 (S)102 %07/12/21 23:25 1718-51-007/10/21 16:3934-163 1
Phenol-d6 (S)35 %07/12/21 23:25 13127-88-307/10/21 16:3910-130 1
2-Fluorophenol (S)51 %07/12/21 23:25 367-12-407/10/21 16:3910-130 1
2,4,6-Tribromophenol (S)93 %07/12/21 23:25 118-79-607/10/21 16:3910-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: TW-1 Lab ID: 92548712008 Collected: 07/07/21 19:40 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 07/13/21 21:35 67-64-125.0 1
Benzene ND ug/L 07/13/21 21:35 71-43-21.0 1
Bromobenzene ND ug/L 07/13/21 21:35 108-86-11.0 1
Bromochloromethane ND ug/L 07/13/21 21:35 74-97-51.0 1
Bromodichloromethane ND ug/L 07/13/21 21:35 75-27-41.0 1
Bromoform ND ug/L 07/13/21 21:35 75-25-21.0 1
Bromomethane ND ug/L 07/13/21 21:35 74-83-92.0 1
2-Butanone (MEK)ND ug/L 07/13/21 21:35 78-93-35.0 1
Carbon tetrachloride ND ug/L 07/13/21 21:35 56-23-51.0 1
Chlorobenzene ND ug/L 07/13/21 21:35 108-90-71.0 1
Chloroethane ND ug/L 07/13/21 21:35 75-00-31.0 1
Chloroform ND ug/L 07/13/21 21:35 67-66-31.0 1
Chloromethane ND ug/L 07/13/21 21:35 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/13/21 21:35 95-49-81.0 1
4-Chlorotoluene ND ug/L 07/13/21 21:35 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 07/13/21 21:35 96-12-82.0 1
Dibromochloromethane ND ug/L 07/13/21 21:35 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 07/13/21 21:35 106-93-41.0 1
Dibromomethane ND ug/L 07/13/21 21:35 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 07/13/21 21:35 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 07/13/21 21:35 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 07/13/21 21:35 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 07/13/21 21:35 75-71-8 v11.0 1
1,1-Dichloroethane ND ug/L 07/13/21 21:35 75-34-31.0 1
1,2-Dichloroethane ND ug/L 07/13/21 21:35 107-06-21.0 1
1,1-Dichloroethene ND ug/L 07/13/21 21:35 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 07/13/21 21:35 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 07/13/21 21:35 156-60-51.0 1
1,2-Dichloropropane ND ug/L 07/13/21 21:35 78-87-51.0 1
1,3-Dichloropropane ND ug/L 07/13/21 21:35 142-28-91.0 1
2,2-Dichloropropane ND ug/L 07/13/21 21:35 594-20-71.0 1
1,1-Dichloropropene ND ug/L 07/13/21 21:35 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 07/13/21 21:35 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 07/13/21 21:35 10061-02-61.0 1
Diisopropyl ether ND ug/L 07/13/21 21:35 108-20-31.0 1
Ethylbenzene ND ug/L 07/13/21 21:35 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 07/13/21 21:35 87-68-32.0 1
2-Hexanone ND ug/L 07/13/21 21:35 591-78-65.0 1
p-Isopropyltoluene ND ug/L 07/13/21 21:35 99-87-61.0 1
Methylene Chloride ND ug/L 07/13/21 21:35 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/13/21 21:35 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 07/13/21 21:35 1634-04-41.0 1
Naphthalene ND ug/L 07/13/21 21:35 91-20-31.0 1
Styrene ND ug/L 07/13/21 21:35 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 07/13/21 21:35 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 07/13/21 21:35 79-34-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Sample: TW-1 Lab ID: 92548712008 Collected: 07/07/21 19:40 Received: 07/08/21 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Tetrachloroethene ND ug/L 07/13/21 21:35 127-18-41.0 1
Toluene ND ug/L 07/13/21 21:35 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 07/13/21 21:35 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 07/13/21 21:35 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 07/13/21 21:35 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 07/13/21 21:35 79-00-51.0 1
Trichloroethene ND ug/L 07/13/21 21:35 79-01-61.0 1
Trichlorofluoromethane ND ug/L 07/13/21 21:35 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/13/21 21:35 96-18-41.0 1
Vinyl acetate ND ug/L 07/13/21 21:35 108-05-42.0 1
Vinyl chloride ND ug/L 07/13/21 21:35 75-01-41.0 1
Xylene (Total)ND ug/L 07/13/21 21:35 1330-20-71.0 1
m&p-Xylene ND ug/L 07/13/21 21:35 179601-23-12.0 1
o-Xylene ND ug/L 07/13/21 21:35 95-47-61.0 1
Surrogates4-Bromofluorobenzene (S)97 %07/13/21 21:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %07/13/21 21:35 17060-07-070-130 1
Toluene-d8 (S)103 %07/13/21 21:35 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.559 ug/L 07/20/21 14:54 18540-29-907/20/21 14:540.500 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 36 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
632759
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92548712001, 92548712002, 92548712003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3323911
Associated Lab Samples:92548712001, 92548712002, 92548712003
Matrix: Water
Analyzed
Mercury ug/L ND 0.20 07/13/21 11:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3323912LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3323913MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92547472014
3323914
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 78 75-12580 22.5ND 2.0 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
632760
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92548712004, 92548712005, 92548712006, 92548712007, 92548712008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3323917
Associated Lab Samples:92548712004, 92548712005, 92548712006, 92548712007, 92548712008
Matrix: Water
Analyzed
Mercury ug/L ND 0.20 07/13/21 13:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3323918LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.32.5 94 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3323919MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92548712004
3323920
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L M1,R12.5 63 75-12591 352.5ND 1.6 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
633866
EPA 3010A
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92548712001, 92548712002, 92548712003, 92548712004, 92548712005, 92548712006, 92548712007,92548712008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3329186
Associated Lab Samples: 92548712001, 92548712002, 92548712003, 92548712004, 92548712005, 92548712006, 92548712007,92548712008
Matrix: Water
Analyzed
Arsenic ug/L ND 10.0 07/19/21 19:25
Barium ug/L ND 5.0 07/19/21 19:25
Cadmium ug/L ND 1.0 07/19/21 19:25
Chromium ug/L ND 5.0 07/19/21 19:25
Lead ug/L ND 5.0 07/19/21 19:25
Selenium ug/L ND 10.0 07/19/21 19:25
Silver ug/L ND 5.0 07/19/21 19:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3329187LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 529500 106 80-120
Barium ug/L 515500 103 80-120
Cadmium ug/L 525500 105 80-120
Chromium ug/L 526500 105 80-120
Lead ug/L 512500 102 80-120
Selenium ug/L 510500 102 80-120
Silver ug/L 267250 107 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3329188MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92548049001
3329189
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 97 75-12597 1500ND487 489
Barium ug/L 500 95 75-12595 050031.7 506 508
Cadmium ug/L 500 99 75-12598 1500ND497 491
Chromium ug/L 500 98 75-12597 15008.1 497 491
Lead ug/L 500 94 75-12593 1500ND471 469
Selenium ug/L 500 101 75-125101 0500ND508 508
Silver ug/L 250 100 75-125102 2250ND251 256
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
633012
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92548712001, 92548712002, 92548712003, 92548712004, 92548712005, 92548712006, 92548712007,92548712008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3324930
Associated Lab Samples: 92548712001, 92548712002, 92548712003, 92548712004, 92548712005, 92548712006, 92548712007,92548712008
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/13/21 12:50
1,1,1-Trichloroethane ug/L ND 1.0 07/13/21 12:50
1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/13/21 12:50
1,1,2-Trichloroethane ug/L ND 1.0 07/13/21 12:50
1,1-Dichloroethane ug/L ND 1.0 07/13/21 12:50
1,1-Dichloroethene ug/L ND 1.0 07/13/21 12:50
1,1-Dichloropropene ug/L ND 1.0 07/13/21 12:50
1,2,3-Trichlorobenzene ug/L ND 1.0 07/13/21 12:50
1,2,3-Trichloropropane ug/L ND 1.0 07/13/21 12:50
1,2,4-Trichlorobenzene ug/L ND 1.0 07/13/21 12:50
1,2-Dibromo-3-chloropropane ug/L ND 2.0 07/13/21 12:50
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/13/21 12:50
1,2-Dichlorobenzene ug/L ND 1.0 07/13/21 12:50
1,2-Dichloroethane ug/L ND 1.0 07/13/21 12:50
1,2-Dichloropropane ug/L ND 1.0 07/13/21 12:50
1,3-Dichlorobenzene ug/L ND 1.0 07/13/21 12:50
1,3-Dichloropropane ug/L ND 1.0 07/13/21 12:50
1,4-Dichlorobenzene ug/L ND 1.0 07/13/21 12:50
2,2-Dichloropropane ug/L ND 1.0 07/13/21 12:50
2-Butanone (MEK)ug/L ND 5.0 07/13/21 12:50
2-Chlorotoluene ug/L ND 1.0 07/13/21 12:50
2-Hexanone ug/L ND 5.0 07/13/21 12:50
4-Chlorotoluene ug/L ND 1.0 07/13/21 12:50
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/13/21 12:50
Acetone ug/L ND 25.0 07/13/21 12:50
Benzene ug/L ND 1.0 07/13/21 12:50
Bromobenzene ug/L ND 1.0 07/13/21 12:50
Bromochloromethane ug/L ND 1.0 07/13/21 12:50
Bromodichloromethane ug/L ND 1.0 07/13/21 12:50
Bromoform ug/L ND 1.0 07/13/21 12:50
Bromomethane ug/L ND 2.0 07/13/21 12:50
Carbon tetrachloride ug/L ND 1.0 07/13/21 12:50
Chlorobenzene ug/L ND 1.0 07/13/21 12:50
Chloroethane ug/L ND 1.0 07/13/21 12:50
Chloroform ug/L ND 1.0 07/13/21 12:50
Chloromethane ug/L ND 1.0 07/13/21 12:50
cis-1,2-Dichloroethene ug/L ND 1.0 07/13/21 12:50
cis-1,3-Dichloropropene ug/L ND 1.0 07/13/21 12:50
Dibromochloromethane ug/L ND 1.0 07/13/21 12:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3324930
Associated Lab Samples: 92548712001, 92548712002, 92548712003, 92548712004, 92548712005, 92548712006, 92548712007,92548712008
Matrix: Water
Analyzed
Dibromomethane ug/L ND 1.0 07/13/21 12:50
Dichlorodifluoromethane ug/L ND 1.0 v107/13/21 12:50
Diisopropyl ether ug/L ND 1.0 07/13/21 12:50
Ethylbenzene ug/L ND 1.0 07/13/21 12:50
Hexachloro-1,3-butadiene ug/L ND 2.0 07/13/21 12:50
m&p-Xylene ug/L ND 2.0 07/13/21 12:50
Methyl-tert-butyl ether ug/L ND 1.0 07/13/21 12:50
Methylene Chloride ug/L ND 5.0 07/13/21 12:50
Naphthalene ug/L ND 1.0 07/13/21 12:50
o-Xylene ug/L ND 1.0 07/13/21 12:50
p-Isopropyltoluene ug/L ND 1.0 07/13/21 12:50
Styrene ug/L ND 1.0 07/13/21 12:50
Tetrachloroethene ug/L ND 1.0 07/13/21 12:50
Toluene ug/L ND 1.0 07/13/21 12:50
trans-1,2-Dichloroethene ug/L ND 1.0 07/13/21 12:50
trans-1,3-Dichloropropene ug/L ND 1.0 07/13/21 12:50
Trichloroethene ug/L ND 1.0 07/13/21 12:50
Trichlorofluoromethane ug/L ND 1.0 07/13/21 12:50
Vinyl acetate ug/L ND 2.0 07/13/21 12:50
Vinyl chloride ug/L ND 1.0 07/13/21 12:50
Xylene (Total)ug/L ND 1.0 07/13/21 12:50
1,2-Dichloroethane-d4 (S)%104 70-130 07/13/21 12:50
4-Bromofluorobenzene (S)%99 70-130 07/13/21 12:50
Toluene-d8 (S)%103 70-130 07/13/21 12:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3324931LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.750 105 70-130
1,1,1-Trichloroethane ug/L 59.350 119 70-130
1,1,2,2-Tetrachloroethane ug/L 52.150 104 70-130
1,1,2-Trichloroethane ug/L 50.950 102 70-130
1,1-Dichloroethane ug/L 57.350 115 70-130
1,1-Dichloroethene ug/L 56.950 114 70-132
1,1-Dichloropropene ug/L 59.250 118 70-131
1,2,3-Trichlorobenzene ug/L 53.850 108 70-134
1,2,3-Trichloropropane ug/L 53.150 106 70-130
1,2,4-Trichlorobenzene ug/L 52.850 106 70-130
1,2-Dibromo-3-chloropropane ug/L 56.450 113 70-132
1,2-Dibromoethane (EDB)ug/L 53.250 106 70-130
1,2-Dichlorobenzene ug/L 51.050 102 70-130
1,2-Dichloroethane ug/L 55.750 111 70-130
1,2-Dichloropropane ug/L 51.850 104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3324931LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 51.350 103 70-130
1,3-Dichloropropane ug/L 52.250 104 70-130
1,4-Dichlorobenzene ug/L 50.650 101 70-130
2,2-Dichloropropane ug/L 63.150 126 70-130
2-Butanone (MEK)ug/L 108100 108 70-133
2-Chlorotoluene ug/L 54.550 109 70-130
2-Hexanone ug/L 104100 104 70-130
4-Chlorotoluene ug/L 53.250 106 70-130
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 70-130
Acetone ug/L 114100 114 70-144
Benzene ug/L 50.550 101 70-130
Bromobenzene ug/L 51.150 102 70-130
Bromochloromethane ug/L 59.350 119 70-130
Bromodichloromethane ug/L 55.850 112 70-130
Bromoform ug/L 55.850 112 70-131
Bromomethane ug/L 43.550 87 30-177
Carbon tetrachloride ug/L 55.950 112 70-130
Chlorobenzene ug/L 50.350 101 70-130
Chloroethane ug/L 50.250 100 46-131
Chloroform ug/L 58.950 118 70-130
Chloromethane ug/L 56.750 113 49-130
cis-1,2-Dichloroethene ug/L 57.350 115 70-130
cis-1,3-Dichloropropene ug/L 55.450 111 70-130
Dibromochloromethane ug/L 55.850 112 70-130
Dibromomethane ug/L 50.750 101 70-130
Dichlorodifluoromethane ug/L 63.0 v150126 52-134
Diisopropyl ether ug/L 54.650 109 70-131
Ethylbenzene ug/L 52.150 104 70-130
Hexachloro-1,3-butadiene ug/L 52.750 105 70-131
m&p-Xylene ug/L 105100 105 70-130
Methyl-tert-butyl ether ug/L 56.850 114 70-130
Methylene Chloride ug/L 55.850 112 68-130
Naphthalene ug/L 54.450 109 70-133
o-Xylene ug/L 52.150 104 70-130
p-Isopropyltoluene ug/L 53.950 108 70-130
Styrene ug/L 54.250 108 70-130
Tetrachloroethene ug/L 49.950 100 70-130
Toluene ug/L 50.550 101 70-130
trans-1,2-Dichloroethene ug/L 58.950 118 70-130
trans-1,3-Dichloropropene ug/L 56.050 112 70-130
Trichloroethene ug/L 50.450 101 70-130
Trichlorofluoromethane ug/L 53.150 106 61-130
Vinyl acetate ug/L 122100 122 70-140
Vinyl chloride ug/L 56.150 112 59-142
Xylene (Total)ug/L 157150 105 70-130
1,2-Dichloroethane-d4 (S)%114 70-130
4-Bromofluorobenzene (S)%106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3324931LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3324932MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92548712008
3324933
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 116 70-135113 320ND23.2 22.6
1,1,1-Trichloroethane ug/L 20 125 70-148116 720ND25.1 23.3
1,1,2,2-Tetrachloroethane ug/L 20 114 70-131108 520ND22.7 21.5
1,1,2-Trichloroethane ug/L 20 124 70-136111 1120ND24.9 22.2
1,1-Dichloroethane ug/L 20 117 70-147109 720ND23.5 21.8
1,1-Dichloroethene ug/L 20 120 70-158112 720ND24.0 22.4
1,1-Dichloropropene ug/L 20 115 70-149108 620ND23.1 21.7
1,2,3-Trichlorobenzene ug/L 20 123 68-140118 420ND24.6 23.6
1,2,3-Trichloropropane ug/L 20 104 67-137100 320ND20.7 20.1
1,2,4-Trichlorobenzene ug/L 20 121 70-139115 620ND24.3 22.9
1,2-Dibromo-3-chloropropane ug/L 20 113 69-136110 220ND22.5 22.1
1,2-Dibromoethane (EDB)ug/L 20 116 70-137113 320ND23.2 22.6
1,2-Dichlorobenzene ug/L 20 122 70-133112 820ND24.3 22.3
1,2-Dichloroethane ug/L 20 111 67-138106 420ND22.2 21.3
1,2-Dichloropropane ug/L 20 120 70-138114 520ND23.9 22.7
1,3-Dichlorobenzene ug/L 20 122 70-133112 820ND24.4 22.4
1,3-Dichloropropane ug/L 20 114 70-136108 520ND22.7 21.5
1,4-Dichlorobenzene ug/L 20 120 70-133113 620ND24.0 22.7
2,2-Dichloropropane ug/L 20 124 52-155116 620ND24.7 23.3
2-Butanone (MEK)ug/L 40 118 61-147113 540ND47.4 45.2
2-Chlorotoluene ug/L 20 120 70-141113 620ND24.0 22.5
2-Hexanone ug/L 40 117 67-139113 440ND46.9 45.2
4-Chlorotoluene ug/L 20 114 70-135107 720ND22.9 21.3
4-Methyl-2-pentanone (MIBK) ug/L 40 117 67-136110 740ND46.9 43.8
Acetone ug/L 40 115 55-159119 340ND46.2 47.7
Benzene ug/L 20 118 67-150111 520ND23.5 22.3
Bromobenzene ug/L 20 120 70-134114 520ND24.0 22.7
Bromochloromethane ug/L 20 123 70-146114 720ND24.5 22.8
Bromodichloromethane ug/L 20 117 70-138111 520ND23.5 22.3
Bromoform ug/L 20 111 57-138102 820ND22.2 20.5
Bromomethane ug/L 20 126 10-200122 420ND25.2 24.3
Carbon tetrachloride ug/L 20 129 70-147121 620ND25.8 24.2
Chlorobenzene ug/L 20 118 70-137112 520ND23.5 22.3
Chloroethane ug/L 20 141 51-166127 1020ND28.2 25.5
Chloroform ug/L 20 115 70-144116 120ND22.9 23.2
Chloromethane ug/L 20 122 24-161116 520ND24.4 23.3
cis-1,2-Dichloroethene ug/L 20 118 67-148112 520ND23.5 22.5
cis-1,3-Dichloropropene ug/L 20 117 70-142108 820ND23.3 21.5
Dibromochloromethane ug/L 20 120 68-138114 620ND24.1 22.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3324932MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92548712008
3324933
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Dibromomethane ug/L 20 123 70-134114 820ND24.6 22.8
Dichlorodifluoromethane ug/L 20 146 43-155139 520ND29.1 27.7
Diisopropyl ether ug/L 20 111 65-146108 220ND22.2 21.7
Ethylbenzene ug/L 20 117 68-143112 520ND23.4 22.4
Hexachloro-1,3-butadiene ug/L 20 126 62-151122 320ND25.2 24.5
m&p-Xylene ug/L 40 116 53-157110 540ND46.3 44.2
Methyl-tert-butyl ether ug/L 20 112 59-156112 020ND22.4 22.4
Methylene Chloride ug/L 20 117 64-148111 620ND23.4 22.2
Naphthalene ug/L 20 121 57-150113 720ND24.2 22.6
o-Xylene ug/L 20 119 68-143113 520ND23.8 22.7
p-Isopropyltoluene ug/L 20 119 70-141114 520ND23.8 22.7
Styrene ug/L 20 117 70-136113 420ND23.5 22.6
Tetrachloroethene ug/L 20 117 70-139113 420ND23.4 22.5
Toluene ug/L 20 117 47-157113 420ND23.4 22.5
trans-1,2-Dichloroethene ug/L 20 120 70-149115 420ND23.9 23.0
trans-1,3-Dichloropropene ug/L 20 117 70-138111 520ND23.3 22.1
Trichloroethene ug/L 20 119 70-149113 520ND23.8 22.6
Trichlorofluoromethane ug/L 20 126 61-154126 020ND25.1 25.1
Vinyl acetate ug/L 40 117 48-156110 640ND46.9 44.0
Vinyl chloride ug/L 20 127 55-172126 120ND25.5 25.2
Xylene (Total)ug/L 60 117 66-145111 560ND70.1 66.9
1,2-Dichloroethane-d4 (S)%96 70-13096
4-Bromofluorobenzene (S)%101 70-13099
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
632616
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92548712001, 92548712002, 92548712003, 92548712004, 92548712005, 92548712006, 92548712007,92548712008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3323214
Associated Lab Samples: 92548712001, 92548712002, 92548712003, 92548712004, 92548712005, 92548712006, 92548712007,92548712008
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 07/12/21 17:58
1,2-Dichlorobenzene ug/L ND 10.0 07/12/21 17:58
1,3-Dichlorobenzene ug/L ND 10.0 07/12/21 17:58
1,4-Dichlorobenzene ug/L ND 10.0 07/12/21 17:58
1-Methylnaphthalene ug/L ND 10.0 07/12/21 17:58
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 07/12/21 17:58
2,4,5-Trichlorophenol ug/L ND 10.0 07/12/21 17:58
2,4,6-Trichlorophenol ug/L ND 10.0 07/12/21 17:58
2,4-Dichlorophenol ug/L ND 10.0 07/12/21 17:58
2,4-Dimethylphenol ug/L ND 10.0 07/12/21 17:58
2,4-Dinitrophenol ug/L ND 50.0 07/12/21 17:58
2,4-Dinitrotoluene ug/L ND 10.0 07/12/21 17:58
2,6-Dinitrotoluene ug/L ND 10.0 07/12/21 17:58
2-Chloronaphthalene ug/L ND 10.0 07/12/21 17:58
2-Chlorophenol ug/L ND 10.0 07/12/21 17:58
2-Methylnaphthalene ug/L ND 10.0 07/12/21 17:58
2-Methylphenol(o-Cresol)ug/L ND 10.0 07/12/21 17:58
2-Nitroaniline ug/L ND 20.0 07/12/21 17:58
2-Nitrophenol ug/L ND 10.0 v107/12/21 17:58
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 07/12/21 17:58
3,3'-Dichlorobenzidine ug/L ND 20.0 07/12/21 17:58
3-Nitroaniline ug/L ND 20.0 07/12/21 17:58
4,6-Dinitro-2-methylphenol ug/L ND 20.0 07/12/21 17:58
4-Bromophenylphenyl ether ug/L ND 10.0 07/12/21 17:58
4-Chloro-3-methylphenol ug/L ND 10.0 07/12/21 17:58
4-Chloroaniline ug/L ND 20.0 07/12/21 17:58
4-Chlorophenylphenyl ether ug/L ND 10.0 07/12/21 17:58
4-Nitroaniline ug/L ND 20.0 07/12/21 17:58
4-Nitrophenol ug/L ND 50.0 07/12/21 17:58
Acenaphthene ug/L ND 10.0 07/12/21 17:58
Acenaphthylene ug/L ND 10.0 07/12/21 17:58
Aniline ug/L ND 10.0 07/12/21 17:58
Anthracene ug/L ND 10.0 07/12/21 17:58
Benzo(a)anthracene ug/L ND 10.0 07/12/21 17:58
Benzo(a)pyrene ug/L ND 10.0 07/12/21 17:58
Benzo(b)fluoranthene ug/L ND 10.0 07/12/21 17:58
Benzo(g,h,i)perylene ug/L ND 10.0 07/12/21 17:58
Benzo(k)fluoranthene ug/L ND 10.0 07/12/21 17:58
Benzoic Acid ug/L ND 50.0 07/12/21 17:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3323214
Associated Lab Samples: 92548712001, 92548712002, 92548712003, 92548712004, 92548712005, 92548712006, 92548712007,92548712008
Matrix: Water
Analyzed
Benzyl alcohol ug/L ND 20.0 07/12/21 17:58
bis(2-Chloroethoxy)methane ug/L ND 10.0 07/12/21 17:58
bis(2-Chloroethyl) ether ug/L ND 10.0 07/12/21 17:58
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 07/12/21 17:58
Butylbenzylphthalate ug/L ND 10.0 07/12/21 17:58
Chrysene ug/L ND 10.0 07/12/21 17:58
Di-n-butylphthalate ug/L ND 10.0 07/12/21 17:58
Di-n-octylphthalate ug/L ND 10.0 07/12/21 17:58
Dibenz(a,h)anthracene ug/L ND 10.0 07/12/21 17:58
Dibenzofuran ug/L ND 10.0 07/12/21 17:58
Diethylphthalate ug/L ND 10.0 07/12/21 17:58
Dimethylphthalate ug/L ND 10.0 07/12/21 17:58
Fluoranthene ug/L ND 10.0 07/12/21 17:58
Fluorene ug/L ND 10.0 07/12/21 17:58
Hexachloro-1,3-butadiene ug/L ND 10.0 07/12/21 17:58
Hexachlorobenzene ug/L ND 10.0 07/12/21 17:58
Hexachlorocyclopentadiene ug/L ND 10.0 07/12/21 17:58
Hexachloroethane ug/L ND 10.0 07/12/21 17:58
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/12/21 17:58
Isophorone ug/L ND 10.0 07/12/21 17:58
N-Nitroso-di-n-propylamine ug/L ND 10.0 07/12/21 17:58
N-Nitrosodimethylamine ug/L ND 10.0 07/12/21 17:58
N-Nitrosodiphenylamine ug/L ND 10.0 07/12/21 17:58
Naphthalene ug/L ND 10.0 07/12/21 17:58
Nitrobenzene ug/L ND 10.0 07/12/21 17:58
Pentachlorophenol ug/L ND 20.0 07/12/21 17:58
Phenanthrene ug/L ND 10.0 07/12/21 17:58
Phenol ug/L ND 10.0 07/12/21 17:58
Pyrene ug/L ND 10.0 07/12/21 17:58
2,4,6-Tribromophenol (S)%68 10-144 07/12/21 17:58
2-Fluorobiphenyl (S)%81 10-130 07/12/21 17:58
2-Fluorophenol (S)%38 10-130 07/12/21 17:58
Nitrobenzene-d5 (S)%111 10-144 07/12/21 17:58
Phenol-d6 (S)%42 10-130 07/12/21 17:58
Terphenyl-d14 (S)%107 34-163 07/12/21 17:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3323215LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 16.850 34 18-130
1,2-Dichlorobenzene ug/L 18.150 36 20-130
1,3-Dichlorobenzene ug/L 17.550 35 18-130
1,4-Dichlorobenzene ug/L 17.950 36 18-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3323215LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/L 20.350 41 29-130
2,2'-Oxybis(1-chloropropane)ug/L 24.450 49 28-130
2,4,5-Trichlorophenol ug/L 23.750 47 35-130
2,4,6-Trichlorophenol ug/L 23.450 47 31-130
2,4-Dichlorophenol ug/L 23.350 47 35-130
2,4-Dimethylphenol ug/L 25.350 51 34-130
2,4-Dinitrophenol ug/L 104250 41 10-153
2,4-Dinitrotoluene ug/L 26.450 53 37-136
2,6-Dinitrotoluene ug/L 24.250 48 33-136
2-Chloronaphthalene ug/L 19.850 40 26-130
2-Chlorophenol ug/L 22.350 45 37-130
2-Methylnaphthalene ug/L 19.950 40 29-130
2-Methylphenol(o-Cresol)ug/L 23.150 46 35-130
2-Nitroaniline ug/L 50.0100 50 37-130
2-Nitrophenol ug/L 24.050 48 32-130
3&4-Methylphenol(m&p Cresol)ug/L 21.250 42 34-130
3,3'-Dichlorobenzidine ug/L 48.7100 49 34-136
3-Nitroaniline ug/L 48.6100 49 37-138
4,6-Dinitro-2-methylphenol ug/L 48.6100 49 21-157
4-Bromophenylphenyl ether ug/L 27.350 55 38-130
4-Chloro-3-methylphenol ug/L 48.2100 48 37-130
4-Chloroaniline ug/L 48.7100 49 38-130
4-Chlorophenylphenyl ether ug/L 24.850 50 33-130
4-Nitroaniline ug/L 49.3100 49 42-137
4-Nitrophenol ug/L 79.1250 32 10-130
Acenaphthene ug/L 22.750 45 33-130
Acenaphthylene ug/L 23.350 47 35-130
Aniline ug/L 22.650 45 22-130
Anthracene ug/L 26.750 53 48-130
Benzo(a)anthracene ug/L 27.650 55 48-137
Benzo(a)pyrene ug/L 27.850 56 49-138
Benzo(b)fluoranthene ug/L 27.450 55 52-138
Benzo(g,h,i)perylene ug/L 26.750 53 48-140
Benzo(k)fluoranthene ug/L 28.650 57 48-139
Benzoic Acid ug/L 39.6J250 16 10-130
Benzyl alcohol ug/L 50.5100 51 35-130
bis(2-Chloroethoxy)methane ug/L 25.950 52 34-130
bis(2-Chloroethyl) ether ug/L 28.850 58 36-130
bis(2-Ethylhexyl)phthalate ug/L 30.750 61 32-165
Butylbenzylphthalate ug/L 29.050 58 34-161
Chrysene ug/L 27.750 55 47-131
Di-n-butylphthalate ug/L 28.150 56 39-144
Di-n-octylphthalate ug/L 25.950 52 30-170
Dibenz(a,h)anthracene ug/L 25.950 52 49-138
Dibenzofuran ug/L 24.250 48 33-130
Diethylphthalate ug/L 26.050 52 38-131
Dimethylphthalate ug/L 25.750 51 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3323215LABORATORY CONTROL SAMPLE:
LCSSpike
Fluoranthene ug/L 27.250 54 46-137
Fluorene ug/L 25.550 51 37-130
Hexachloro-1,3-butadiene ug/L 16.450 33 11-130
Hexachlorobenzene ug/L 22.850 46 38-130
Hexachlorocyclopentadiene ug/L 13.450 27 10-130
Hexachloroethane ug/L 17.450 35 14-130
Indeno(1,2,3-cd)pyrene ug/L 26.250 52 41-130
Isophorone ug/L 26.650 53 33-130
N-Nitroso-di-n-propylamine ug/L 27.850 56 36-130
N-Nitrosodimethylamine ug/L 25.7 v15051 34-130
N-Nitrosodiphenylamine ug/L 25.750 51 37-130
Naphthalene ug/L 19.850 40 30-130
Nitrobenzene ug/L 24.450 49 36-130
Pentachlorophenol ug/L 42.9 v310043 23-149
Phenanthrene ug/L 26.250 52 44-130
Phenol ug/L 15.450 31 18-130
Pyrene ug/L 30.250 60 47-134
2,4,6-Tribromophenol (S)%56 10-144
2-Fluorobiphenyl (S)%47 10-130
2-Fluorophenol (S)%38 10-130
Nitrobenzene-d5 (S)%55 10-144
Phenol-d6 (S)%31 10-130
Terphenyl-d14 (S)%64 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3323216MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92548712001
3323217
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 90.9 56 10-13045 2390.9ND 50.8 40.5
1,2-Dichlorobenzene ug/L 90.9 55 10-13042 2890.9ND 50.1 38.0
1,3-Dichlorobenzene ug/L 90.9 54 10-13040 2990.9ND 49.4 36.7
1,4-Dichlorobenzene ug/L 90.9 57 10-13042 2990.9ND 51.7 38.4
1-Methylnaphthalene ug/L 90.9 68 10-13068 090.9ND 61.8 61.9
2,2'-Oxybis(1-chloropropane) ug/L 90.9 80 12-14271 1290.9ND 72.8 64.5
2,4,5-Trichlorophenol ug/L 90.9 82 10-14382 090.9ND 74.3 74.2
2,4,6-Trichlorophenol ug/L 90.9 79 10-14788 1190.9ND 71.4 79.8
2,4-Dichlorophenol ug/L 90.9 80 10-13871 1290.9ND 73.1 64.8
2,4-Dimethylphenol ug/L 90.9 87 25-13074 1690.9ND 79.0 67.6
2,4-Dinitrophenol ug/L 455 90 10-16595 5455ND411 431
2,4-Dinitrotoluene ug/L 90.9 82 29-14878 590.9ND 74.9 71.0
2,6-Dinitrotoluene ug/L 90.9 91 26-14693 390.9ND 82.6 85.0
2-Chloronaphthalene ug/L 90.9 70 11-13064 890.9ND 63.4 58.2
2-Chlorophenol ug/L 90.9 76 10-13372 690.9ND 69.3 65.5
2-Methylnaphthalene ug/L 90.9 65 13-13068 490.9ND 59.5 61.6
2-Methylphenol(o-Cresol)ug/L 90.9 75 20-13068 990.9ND 67.7 62.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3323216MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92548712001
3323217
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2-Nitroaniline ug/L 182 82 24-13681 1182ND148 146
2-Nitrophenol ug/L v190.9 91 10-15382 1090.9ND 83.2 74.9
3&4-Methylphenol(m&pCresol)ug/L 90.9 68 16-13064 690.9ND 62.1 58.5
3,3'-Dichlorobenzidine ug/L 182 85 10-15388 3182ND155 160
3-Nitroaniline ug/L 182 84 22-15187 3182ND153 159
4,6-Dinitro-2-methylphenol ug/L 182 98 10-18099 1182ND178 180
4-Bromophenylphenyl ether ug/L 90.9 81 25-13077 590.9ND 73.8 70.4
4-Chloro-3-methylphenol ug/L 182 76 25-13387 13182ND138 157
4-Chloroaniline ug/L 182 71 14-13269 3182ND129 125
4-Chlorophenylphenyl ether ug/L 90.9 74 19-13069 790.9ND 67.2 62.8
4-Nitroaniline ug/L 182 85 29-15088 5182ND154 161
4-Nitrophenol ug/L 455 53 10-13058 9455ND242 264
Acenaphthene ug/L 90.9 79 16-13073 990.9ND 72.2 65.9
Acenaphthylene ug/L 90.9 78 15-13772 890.9ND 71.3 65.8
Aniline ug/L 90.9 47 10-13047 090.9ND 42.9 42.9
Anthracene ug/L 90.9 85 37-13685 090.9ND 77.7 77.4
Benzo(a)anthracene ug/L 90.9 86 40-14588 390.9ND 78.3 80.4
Benzo(a)pyrene ug/L 90.9 85 41-14691 690.9ND 77.7 82.6
Benzo(b)fluoranthene ug/L 90.9 81 39-15186 690.9ND 73.7 77.9
Benzo(g,h,i)perylene ug/L 90.9 90 40-14794 490.9ND 81.7 85.2
Benzo(k)fluoranthene ug/L 90.9 88 40-14691 490.9ND 79.7 83.1
Benzoic Acid ug/L 455 34 10-13038 11455ND154 171
Benzyl alcohol ug/L 182 70 25-13065 7182ND126 118
bis(2-Chloroethoxy)methane ug/L 90.9 75 23-13068 1090.9ND 68.5 61.8
bis(2-Chloroethyl) ether ug/L 90.9 84 25-13075 1190.9ND 76.6 68.6
bis(2-Ethylhexyl)phthalate ug/L 90.9 90 28-16693 490.9ND 81.6 84.8
Butylbenzylphthalate ug/L 90.9 88 33-16590 390.9ND 79.8 81.9
Chrysene ug/L 90.9 84 38-14188 490.9ND 76.6 79.8
Di-n-butylphthalate ug/L 90.9 105 32-15390 1590.9ND 95.3 81.9
Di-n-octylphthalate ug/L 90.9 90 30-17593 390.9ND 81.9 84.6
Dibenz(a,h)anthracene ug/L 90.9 91 39-14895 490.9ND 82.4 86.0
Dibenzofuran ug/L 90.9 74 20-13070 690.9ND 67.5 63.5
Diethylphthalate ug/L 90.9 78 28-14278 090.9ND 70.9 70.9
Dimethylphthalate ug/L 90.9 77 26-13676 290.9ND 70.0 68.8
Fluoranthene ug/L 90.9 108 39-14389 1990.9ND 97.9 80.6
Fluorene ug/L 90.9 79 24-13276 490.9ND 71.9 68.8
Hexachloro-1,3-butadiene ug/L 90.9 50 10-13041 2190.9ND 45.9 37.2
Hexachlorobenzene ug/L 90.9 82 29-13080 390.9ND 74.5 72.6
Hexachlorocyclopentadiene ug/L 90.9 56 10-13056 190.9ND 51.3 51.0
Hexachloroethane ug/L R190.9 54 10-13039 3290.9ND 48.7 35.2
Indeno(1,2,3-cd)pyrene ug/L 90.9 91 39-14895 490.9ND 82.8 86.4
Isophorone ug/L 90.9 74 23-13067 1190.9ND 67.3 60.5
N-Nitroso-di-n-propylamine ug/L 90.9 72 25-13067 890.9ND 65.5 60.5
N-Nitrosodimethylamine ug/L 90.9 71 22-13068 590.9ND 64.7 61.5
N-Nitrosodiphenylamine ug/L 90.9 82 26-13481 190.9ND 74.6 74.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3323216MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92548712001
3323217
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Naphthalene ug/L 90.9 65 14-13052 2190.9ND 59.1 47.7
Nitrobenzene ug/L 90.9 79 25-13069 1390.9ND 71.4 62.5
Pentachlorophenol ug/L 182 87 10-17587 0182ND158 159
Phenanthrene ug/L 90.9 84 36-13384 090.9ND 76.3 76.4
Phenol ug/L 90.9 47 10-13046 190.9ND 42.8 42.3
Pyrene ug/L 90.9 80 40-14383 390.9ND 72.8 75.1
2,4,6-Tribromophenol (S)%93 10-14499
2-Fluorobiphenyl (S)%71 10-13073
2-Fluorophenol (S)%58 10-13057
Nitrobenzene-d5 (S)%80 10-14475
Phenol-d6 (S)%42 10-13042
Terphenyl-d14 (S)%81 34-16388
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1707678
7199
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92548712001, 92548712002, 92548712003, 92548712004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3681238-1
Associated Lab Samples:92548712001, 92548712002, 92548712003, 92548712004
Matrix: Water
Analyzed
Chromium, Hexavalent ug/L ND 0.500 07/19/21 13:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3681238-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent ug/L 2.122.00 106 90.0-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3681238-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1375410-01
R3681238-4
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chromium, Hexavalent ug/L 50.0 102 90.0-110103 0.47550.0ND 51.1 51.3
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3681238-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1376272-01
Chromium, Hexavalent ug/L 50.050.0 99.2 90.0-1100.400
Parameter Units
Dup
Result QualifiersRPDResult
L1375438-01
R3681238-5SAMPLE DUPLICATE:
Chromium, Hexavalent ug/L ND 0.00ND
Parameter Units
Dup
Result QualifiersRPDResult
L1376277-01
R3681238-7SAMPLE DUPLICATE:
Chromium, Hexavalent ug/L ND 0.00ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1707679
7199
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92548712005, 92548712006, 92548712007, 92548712008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3682155-1
Associated Lab Samples:92548712005, 92548712006, 92548712007, 92548712008
Matrix: Water
Analyzed
Chromium, Hexavalent ug/L ND 0.500 07/20/21 12:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3682155-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent ug/L 2.122.00 106 90.0-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3682155-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1375422-01
R3682155-4
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chromium, Hexavalent ug/L 50.0 90.9 90.0-11090.8 0.08250.03.17 48.6 48.6
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3682155-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1378544-01
Chromium, Hexavalent ug/L 49.750.0 99.5 90.0-110ND
Parameter Units
Dup
Result QualifiersRPDResult
L1375441-01
R3682155-5SAMPLE DUPLICATE:
Chromium, Hexavalent ug/L ND 0.00ND
Parameter Units
Dup
Result QualifiersRPDResult
L1378560-01
R3682155-7SAMPLE DUPLICATE:
Chromium, Hexavalent ug/L ND 0.00ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 57
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision andbias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below thelaboratory reporting limit.BC
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in theassociated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in theassociated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 57
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92548712
Brayton Intl 49-8056C
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92548712001 633866 634014TW-2 EPA 3010A EPA 6010D
92548712002 633866 634014MW-1 EPA 3010A EPA 6010D
92548712003 633866 634014DUP-1 EPA 3010A EPA 6010D
92548712004 633866 634014MW-5 EPA 3010A EPA 6010D
92548712005 633866 634014MW-2 EPA 3010A EPA 6010D
92548712006 633866 634014MW-4 EPA 3010A EPA 6010D
92548712007 633866 634014MW-3 EPA 3010A EPA 6010D
92548712008 633866 634014TW-1 EPA 3010A EPA 6010D
92548712001 632759 632838TW-2 EPA 7470A EPA 7470A
92548712002 632759 632838MW-1 EPA 7470A EPA 7470A
92548712003 632759 632838DUP-1 EPA 7470A EPA 7470A
92548712004 632760 632844MW-5 EPA 7470A EPA 7470A
92548712005 632760 632844MW-2 EPA 7470A EPA 7470A
92548712006 632760 632844MW-4 EPA 7470A EPA 7470A
92548712007 632760 632844MW-3 EPA 7470A EPA 7470A
92548712008 632760 632844TW-1 EPA 7470A EPA 7470A
92548712001 632616 632867TW-2 EPA 3510C EPA 8270E
92548712002 632616 632867MW-1 EPA 3510C EPA 8270E
92548712003 632616 632867DUP-1 EPA 3510C EPA 8270E
92548712004 632616 632867MW-5 EPA 3510C EPA 8270E
92548712005 632616 632867MW-2 EPA 3510C EPA 8270E
92548712006 632616 632867MW-4 EPA 3510C EPA 8270E
92548712007 632616 632867MW-3 EPA 3510C EPA 8270E
92548712008 632616 632867TW-1 EPA 3510C EPA 8270E
92548712001 633012TW-2 EPA 8260D
92548712002 633012MW-1 EPA 8260D
92548712003 633012DUP-1 EPA 8260D
92548712004 633012MW-5 EPA 8260D
92548712005 633012MW-2 EPA 8260D
92548712006 633012MW-4 EPA 8260D
92548712007 633012MW-3 EPA 8260D
92548712008 633012TW-1 EPA 8260D
92548712001 1707678 1707678TW-2 7199 EPA 7199
92548712002 1707678 1707678MW-1 7199 EPA 7199
92548712003 1707678 1707678DUP-1 7199 EPA 7199
92548712004 1707678 1707678MW-5 7199 EPA 7199
92548712005 1707679 1707679MW-2 7199 EPA 7199
92548712006 1707679 1707679MW-4 7199 EPA 7199
92548712007 1707679 1707679MW-3 7199 EPA 7199
92548712008 1707679 1707679TW-1 7199 EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/21/2021 03:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 57
Page 55 of 57
Page 56 of 57
Page 57 of 57

APPENDIX E

Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: Brayton International
Exposure Unit ID: MW-1
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 0.0E+00 1.1E+00 YES
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 0.0E+00 2.7E-01 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: Brayton International
Exposure Unit ID: MW-2
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 0.0E+00 7.5E-01 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 0.0E+00 1.8E-01 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator

APPENDIX F