09018-Fieldcrest_Blanket_Mill- Post_EMP_Monitoring_Letter_Report

FRO'EHLING ?-;
OBERTC)N
Assess. Manage. Consult.
September 1, 2021
Ms. Sarah Hardison Young
Project Manager, Brownfields Property Management Unit
North Carolina Department of Environmental Quality
217 West Jones Street
Raleigh, NC 27603
Phone: [phone]
[e-mail]
and
Ms. Anita E. Robertson, PE
WK Dickson & Co., Inc.
720 Corporate Center Drive
Raleigh, NC 27607
Phone: [phone]
[e-mail]
Re: Brownfields Post Environmental Management Monitoring Report
20120031.20.RA Eden Sewer Construction
Fieldcrest Blanket Mill (09018-05-079)
Warehouse Street
Eden, Rockingham County, North Carolina
Froehling and Robertson, Inc. (F&R) has prepared this report on behalf of the City of Eden for the
subsurface sewer line work along Warehouse Street in accordance with the previously approved
Environmental Management Plan (EMP) prepared by F&R on behalf of the City of Eden.
Background
The EMP was submitted on June 17, 2021 (F&R Project Number 59Z-0119) and approved by the NCDEQ on
June 17, 2021. The EMP was required as planned subsurface sewer line work along Warehouse Street
encroached into the Field Crest Blanket Mill Brownfields Property. As a result, an EMP was required to be
submitted to the NCDEQ for approval prior to commencing with sewer utility work in this area. The NCDEQ
was notified on June 25, 2021 that pre -characterization of the soils was conducted by collecting two
composite samples from test pits at 50 foot intervals along the proposed sewer trench on June 22, 2021.
Each composite sample represented approximately half of the approximately 1,100 cubic yards to be
impacted by the sewer line trench excavation. The test pits were distributed to provide a representative
characterization of the sewer line trench area and extended to 12 feet below ground surface (bgs) the
maximum depth of the proposed sewer line excavation. A map showing these locations is included as
Figure 1. The samples were submitted to a North Carolina certified laboratory for analysis of volatile
organic compounds (VOCs), semi -volatile organic compounds (SVOCs), and Resource Conservation and
A Minority -Owned Business

9
Recovery Act (RCRA) metals plus hexavalent chromium. The data is summarized on Table 1 and the
complete laboratory analytical data is included as an attachment. Arsenic was the only target compounds
detected above the North Carolina Commercial Preliminary Soil Remediation Goal (PSRG), but the levels
were still generally consistent with naturally occurring background levels. The NCDEQ indicated on July 1,
2021, that based on the review of the data submitted for the composite soil samples that the soils could be
re -used at the Property as long as the proposed soil screening was still conducted, and that the EMP
required final grade sampling was completed, a copy of this approval is included as an attachment. The
required notifications were completed prior to beginning sewer line excavation activities. No excavation
activities were conducted on Parcels A or B. Subsequent review of the plans indicated that plugging of the
one line was not required, and the other line was actually located under the street outside the Brownfields
boundaries.
Soil Screening & Sewer Line Installation
Excavation at the site was conducted in two phases. The first phase consisted of the bore pit on the
western portion of the Property on July 6 through 8, 2021. The second phase consisted of the sewer line
trench and sewer line installation from July 20 to 21, 2021. An environmental scientist from F&R was
present during these activities to screen the soils with a Photo -ionization detector (PID). Evidence of odors,
staining, or PID readings above background were not encountered during the soil excavation activities. All
soils were staged on plastic in accordance with the approved EMP for screening prior to returning to the
sewer line trench after the pipe was installed. No import or export of soils was necessary during the
proposed work covered by the EMP.
Based on the results of the characterization samples collected from the soils in the proposed sewer line
excavation area on June 17, 2021, and screening of soils during excavation for the bore pit and sewer line
on July 6 through 8, and July 20 and 21, 2021 no evidence of impacts by VOCs was identified that
necessitate disposal of site soils, or which would require vapor assessment or mitigation in connection with
the sewer line installation.
Soil Sampling and Results
F&R conducted the required post grade soil sampling on August 10, 2021 in accordance with the sampling
plan provided in the approved EMP. Four composite samples each consisting of four aliquots were
collected from the zero to two foot interval from the soils along the sewer line excavation after backfilling
and final grade restoration in accordance with the EMP. The samples were analyzed for VOCs, SVOCs, and
RCRA metals plus hexavalent chromium. The VOC samples were collected as a grab sample from one of the
aliquots from the 1 to 2 foot bgs interval. Evidence of odors, staining, or PID readings above background
were not encountered during screening of soils for post grade soil sampling. The sample location plan is
included as Figure 2 and the results are summarized on Table 2. The complete laboratory analytical data is
included in Appendix A. Seed and straw will be applied over the final surface once conditions permit and all
staged equipment is removed from this parcel.
Conclusions and Recommendations
As discussed, F&R, WK Dickson, and the City of Eden are not responsible for the overall Brownfields
Summary Redevelopment Report as typically required in the Brownfields Agreement. Based on prior
WK Dickson & Co. RA Eden Sewer Construction — Brownfields EMP Post Construction Report
F&R Project No. 59Z-0119 2 September 1, 2021

9
correspondence, it is our understanding that this letter report signed by a North Carolina licensed PG
documenting the activities related to the sewer line installation, which includes documentation of final
grade sampling, under the previously approved EMP is sufficient for the activities related to the sewer line
installation as discussed in this report. No unexpected evidence of contamination or elevated PID readings
was identified during work activities.
The post construction grade samples indicated that target compounds were not detected above the
applicable North Carolina Commercial PSRGs except for arsenic. The levels of arsenic were consistent with
the pre -excavation characterization sample concentrations, and generally consistent with naturally
occurring background levels.
F&R on behalf of the City of Eden do not recommend additional assessment or action based on the
screening in accordance with the EMP during site work and the results of the post -grade surface sampling.
No additional action is recommended in regards to the sewer line utility installation, beyond maintaining
the controls in accordance with the EMP.
Please contact the undersigned at 704.409.7243 if you have any questions regarding this assessment
conducted in accordance with the EMP.
Sincerely,
..9L
ox ,
Brian T. Olin, P.G.
Environmental Project Manager
/?7 G.; �(_
Zachary C. Parker, PMP
Regional Manager, Environmental Services
Attachments: Limitations
Figure 1: Pre -Excavation Characterization Test Pit Location Map
Figure 2: Post Grade Sample Location Map
Table 1: Pre -Excavation Soil Sample Results Summary
Table 2: Post Grade Soil Sample Results Summary
NDEQ Soil Reuse Approval Email
Laboratory Analytical Data
WK Dickson & Co. RA Eden Sewer Construction — Brownfields EMP Post Construction Report
F&R Project No. 59Z-0119 3 September 1, 2021

Limitations
This report has been prepared for the exclusive use of the NCDEQ, the City of Eden, WK Dickson &
Company, and their agents. These services have been performed in accordance with generally accepted
environmental practices. As with any environmental investigation, actual conditions exist only at the
precise locations from which the observations were taken. Certain inferences are based on the results
of observations to form a professional opinion of conditions. Our observations and recommendations
are based upon conditions readily visible at the site at the time of our site visit. No other warranty,
expressed or implied, is made. Our conclusions and recommendations are based on information
provided to us by others and our Site observations.
F&R by virtue of providing the services described in this report, does not assume the responsibility of
the person(s) in charge of the Site, or otherwise take responsibility for reporting to local, state, or
federal public agencies any conditions that may present a potential danger to public health safety or the
environment. We understand that the client will notify appropriate regulatory agencies of potential
impact, risks, or other requirements as necessary. F&R assumes no responsibility for investigation,
remediation, or liability associated with environmental impact to or from the project property
regardless of the date of impact discovery. The contents of the report should not be construed in any
way as a recommendation to purchase, sell, or develop the project site. F&R retains the right to revise
this report if new information is later discovered or made available. The report must be presented in its
entirety.
WK Dickson & Co. RA Eden Sewer Construction — Brownfields EMP Post Construction Report
F&R Project No. 59Z-0119 4 August 23, 2021

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Note:
No asphalt or concrete surface is present in the Brownfields
Area.
No soils from inside the Brownfields area will be palced outside
the Brownfields area, and no soils form outside the Brown -
fields area will be used inside the Brownfields area unless the
are documented to be demonstrably clean fill as approved by
the NCDEQ.
Proposed Post Grade Soil Sample (Composite)
Post Grade VOC Grab Sample and Composite Aliquot Location
Pre -Excavation Characterization Test Pit Location Map
uien[: vvn vicrcson & moo.
F Froehling & Robertson, Inc. Project: 20120031.20.RA Eden Sewer Construction
306 Hubert Street Location: Warehouse Street Eden NC
Raleigh, North Carolina 27603 Project Number: 59Z-0119 FIGURE
T 919.828.3441 Data Source: Brownfields Plat
Date: Scale: r., F1111 pint No.:

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Wk 41:
•
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• V111 `;ITE, :ICY Mill f
'.I IE , (.:f NlYAf ()F V1(J
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_I. Emp-2,: 3
Note:
No asphalt or concrete surface is present in the Brownfields
Area.
No soils from inside the Brownfields area will be palced outside
the Brownfields area, and no soils form outside the Brown -
fields area will be used inside the Brownfields area unless the
are documented to be demonstrably clean fill as approved by
the NCDEQ.
PV
�:• I I
Post Grade VOC Grab Sample and Composite Aliquot Location
Post Grade Sample Location Map
uienr. VVA ul—Ull M —
Froehling & Robertson, Inc. Project: 20120031.20.RA Eden Sewer Construction
y 306 Hubert Street Location: warehouse Street, Eden, NC
Rale0igh, North Carolina 27603 Project Number: 59Z-0119 FIGURE
T 919.828.3441 Data Source: Brownfields Plat 2
�y�4
Date: Apugust, 2021 1 Scale: See Attached Full Plat No.:

Table 1- Summary of Stockpile Soil Analytical Results
20120031.20.RA Eden Sewer Construction - Fieldcrest Blanket Mill (09018-05-079)
Warehouse Street
Eden, North Carolina
Project No.: 59Z-0119
EPA Method
EPA 7471E
EPA Method 6020E
8260
EPA Method
Sample ID (Depth)
Date Collected
8270
Hex
Acetone
Mercury
Arsenic
Barium
Chromium
Lead
Selenium
Chromium
S-1
6/22/2021
BRL
BRL
0.0485
5.53
51.5
65.7
0.41 J
21.7
1.45
S-2
0.003
BRL
0.0264
11.7
51.6
104
0.29 J
39.3
1.7
North Carolina Commercial Soil Cleanup
Levels (MSCCs)
210,000
NSE
NSE
NSE
46,000
350,000
6.54
400
NSE
North Carolina Commercial Preliminary
Soil Remediation Goals (PSRGs)
140,000
NSE
9.7
3.0
47,000
350,000
6.50
800
1,200
Concentrations reported in mg/kg
Bolded results exceed their respective Commercial Prelimary Soil Remediation Goal (PSRG)
Compounds not listed were not detected above the laboratory method detection limits.
A complete list of target compounds is provided in the laboratory report
J = Detected below the laboratory reporting limit
BRL = Below Laboratory Reporting Laboratory
NSE = No Standard Established

Table 2 - Summary of Post -Grade Surface Soil Analytical Results
20120031.20.RA Eden Sewer Construction - Fieldcrest Blanket Mill (09018-05-079)
Warehouse Street
Eden, North Carolina
Project No.: 59Z-0119
EPA Method 8260
EPA Method 8270
EPA 7471B
Sample ID (Depth)
Date Collected
Methyl Ethyl
Benzo(b)
bis(2-ethylhexyl)
Acetone
n-Hexane
Acenaphthylene
Anthracene
Fluoranthene
Pyrene
Mercury
Ketone (MEK)
fluoranthene
pthalate
Comp -1
8/10/2021
0.026
0.001 J
0.001 J
0.204 J
BRL
BRL
BRL
BRL
BRL
0.045
Comp -2
0.03
0.001 J
0.003 J
0.158 J
BRL
0.171 J
BRL
0.166 J
0.198 J
0.0672
Comp -3
0.035
0.001 J
0.002 J
0.214 J
0.174 J
BRL
BRL
BRL
BRL
0.617
Comp-4
0.004J
BRL
BRL
0.238J
0.194J
BRL
0.713
0.199J
0.365J
0.617
North Carolina Commercial Soil Cleanup
Levels (MSCCs)
210,000
NSE
140,000
14,000
70,000
32
233
9,340
7,000
NSE
North Carolina Commercial Preliminary
Soil Remediation Goals (PSRGs)
140,000
540
40,000
9,000
45,000
21
160
6,000
4,500
9.7
Concentrations reported in mg/kg
Bolded results exceed their respective Commercial Prelimary Soil Remediation Goal (PSRG)
Compounds not listed were not detected above the laboratory method detection limits.
A complete list of target compounds is provided in the laboratory report
J = Detected below the laboratory reporting limit
BRL = Below Laboratory Reporting Laboratory
NSE = No Standard Established

Table 2 - Summary of Post -Grade Surface Soil Analytical Results
20120031.20.RA Eden Sewer Construction - Fieldcrest Blanket Mill (09018-05-079)
Warehouse Street
Eden, North Carolina
Project No.: 59Z-0119
EPA Method 6020B
Sample ID (Depth)
Date Collected
Hex
Arsenic
Barium
Chromium
Lead
Cadmium
Silver
Selenium
Chromium
Comp-1
8/10/2021
7.69
52.6
42.2
0.451
32.3
BRL
BRL
1.64J
Comp -2
7.29
90.0
43.6
0.39 J
1 40.7
0.1011
BRL
1.97 K
Comp -3
7.46
89.2
47.8
0.33 J
35.1
0.0788 J
BRL
2.16 J
Comp - 4
8.99
80.5
46.1
0.38 J
34.0
0.07381
0.0646 J
1.70 J
North Carolina Commercial Soil Cleanup
Levels (MSCCs)
NSE
46,000
350,000
6.54
400
NSE
1,160
NSE
North Carolina Commercial Preliminary
Soil Remediation Goals (PSRGs)
3.0
47,000
350,000
6.50
800
200
1,200
1,200
Concentrations reported in mg/kg
Bolded results exceed their respective Commercial Prelimary Soil Remediation Goal (PSRG)
Compounds not listed were not detected above the laboratory method detection limits.
A complete list of target compounds is provided in the laboratory report
J = Detected below the laboratory reporting limit
BRL = Below Laboratory Reporting Laboratory
NSE = No Standard Established

From: Hardison, Sarah <[e-mail]>
Sent: Thursday, July 01, 20214:14 PM
To: Brian Olin
Cc: Thompson, Jordan L; Anita Robertson
Subject: RE: [External] RE: 20120031.20.RA Eden Remediation Plan - Construction - Fieldcrest
Blanket Mill (09018-05-079)
Hi Brian —
We have reviewed the data for S-1 and S-2 stockpile soil samples and based on our review we believe the respective S-1
and S-2 stockpiled soil can be re -used on Parcel C of the subject Brownfields Property.
Please keep in mind ongoing soil screening should occur in accordance with the EMP and that final grade sampling will
still need to be conducted once work has concluded.
Thanks,
Sarah
Sarah Hardison Young
Project Manager, Brownfields Property Management Unit
North Carolina Department of Environmental Quality
919.707.8382 (Office)
919.441.7428 (Mobile)
[e-mail]
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
From: Brian Olin [mailto:[e-mail]]
Sent: Wednesday, June 30, 2021 3:27 PM
To: Hardison, Sarah <[e-mail]>
Cc: Thompson, Jordan L <[e-mail]>; Anita Robertson <[e-mail]>
Subject: RE: [External] RE: 20120031.20.RA Eden Remediation Plan - Construction - Fieldcrest Blanket Mill (09018-05-079)
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Sarah,
Here is the final laboratory report with the QA/QC data and the Hex Chromium results. Hex Chromium were estimated
concentrations at less than 0.5 mg/kg. Please let us know if you need any further information and as soon as you make a
determination on the re -use of soils.
Thank you
Brian T. Olin, PG
Lead Environmental Scientist, Project Manager
FROEHLING & ROBERTSON
3300 International Airport Drive, Suite 600, Charlotte, NC 28208
T: 704.409.7243
[e-mail] www.fandr.com

Waypointo
ANALYTICAL
6/30/2021
F&R, Inc. - Charlotte
Brian Olin
3300 International Airport Dr., Suite 600
Charlotte, NC, 28208
Ref: Analytical Testing
Lab Report Number: 21-173-0038
Client Project Description: RA Eden
Dear Brian Olin:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 6/22/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
a'-1
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 53

Waypoint.0
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2021
North Carolina
State Program
402
12/31/2021
South Carolina
State Program
99012
07/31/2021
South Carolina
State Program
99012
12/31/2021
Page 1 of 1 00016/21-173-0038
Page 2 of 53

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Sample Summary Table
Report Number: 21-173-0038
Client Project Description: RA Eden
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
90168
S-1
Solids
06/22/2021 10:15
06/22/2021 14:30 7199
90168
S-1
Solids
06/22/2021 10:15
06/22/2021 14:30
90169
S-2
Solids
06/22/2021 10:30
06/22/2021 14:30 7199
90169
S-2
Solids
06/22/2021 10:30
06/22/2021 14:30
Pace Analytical - Columbia, SC (Shealy), West Columbia, SC
Page 3 of 53

Waypoint (D 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytica Isom
Summary of Detected Analytes
Project: RA Eden
Report Number: 21-173-0038
Client Sample ID
Method
Lab Sample ID
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
S-1
V 90168
6020B
Arsenic
5.53
mg/Kg - dry
0.114
06/23/2021 15:34
6020E
Barium
51.5
mg/Kg - dry
1.70
06/23/2021 15:34
6020E
Chromium
65.7
mg/Kg - dry
0.351
06/23/2021 15:34
6020E
Lead
21.7
mg/Kg - dry
0.170
06/23/2021 15:34
6020B
Selenium
1.45
mg/Kg - dry
1.09
06/23/2021 15:34
J
7471 B
Mercury (Total)
0.0485
mg/Kg - dry
0.0145
06/24/2021 14:42
SW-DRYWT
Moisture
17.5
%
06/22/202115:37
S-2
V 90169
6020B
Arsenic
11.7
mg/Kg - dry
0.123
06/23/2021 16:20
6020E
Barium
51.6
mg/Kg - dry
1.83
06/23/2021 16:20
6020B
Chromium
104
mg/Kg - dry
0.379
06/23/2021 16:20
6020E
Lead
39.3
mg/Kg - dry
0.183
06/23/2021 16:20
6020B
Selenium
1.70
mg/Kg - dry
1.18
06/23/2021 16:20
J
7471 B
Mercury (Total)
0.0264
mg/Kg - dry
0.0157
06/24/2021 15:04
J
8260D
Acetone
0.003
mg/Kg - dry
0.003
06/23/2021 17:04
J
SW-DRYWT
Moisture
23.5
%
06/22/202115:37
Page 4 of 53

WavDdibnto
ANALYTICAL
00019
F&R, Inc. - Charlotte
Brian Olin
3300 International Airport Dr., Suite 600
Charlotte , NC 28208
Project RA Eden
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Report Date : 06/30/2021
Received : 06/22/2021
Lab No : 90168
Sample ID: S-1
Matrix: Solids
Sampled: 6/22/2021 10:15
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
17.5
%
1
06/22/2115:37
EDV
SW-DRYWT
Arsenic
5.53
mg/Kg - dry
0.114
1.21
10
06/23/21 15:34
EDV
6020B
Barium
51.5
mg/Kg - dry
1.70
12.1
10
06/23/21 15:34
EDV
6020E
Cadmium
<0.0666
mg/Kg - dry
0.0666
0.606
10
06/23/21 15:34
EDV
6020B
Chromium
65.7
mg/Kg - dry
0.351
1.21
10
06/23/21 15:34
EDV
6020E
Lead
21.7
mg/Kg - dry
0.170
1.21
10
06/23/21 15:34
EDV
6020B
Mercury (Total)
0.0485
mg/Kg - dry
0.0145
0.0364
1
06/24/21 14:42
EDV
7471E
Selenium
1.453
mg/Kg - dry
1.09
2.42
10
06/23/21 15:34
EDV
6020B
Silver
<0.0496
mg/Kg - dry
0.0496
0.606
10
06/23/21 15:34
EDV
6020E
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 5 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Lab No : 90168
Matrix: Solids
Sample ID: S-1
Sampled:
6/22/2021 10:15
Analytical Method: 8260D
Prep Batch(es):
V5728
06/23/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<0.002
mg/Kg - dry
0.002
0.024
1
06/23/21 16:34
TBL
V5732
Acrolein
<0.001
mg/Kg - dry
0.001
0.024
1
06/23/21 16:34
TBL
V5732
Acrylonitrile
<0.0009
mg/Kg - dry
0.0009
0.024
1
06/23/21 16:34
TBL
V5732
Benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 16:34
TBL
V5732
Bromobenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 16:34
TBL
V5732
Bromochloromethane
<0.0010
mg/Kg - dry
0.0010
0.006
1
06/23/21 16:34
TBL
V5732
Bromodichloromethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
Bromoform
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
Bromomethane
<0.002
mg/Kg - dry
0.002
0.012
1
06/23/21 16:34
TBL
V5732
n-Butylbenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 16:34
TBL
V5732
sec -Butyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 16:34
TBL
V5732
tert-Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 16:34
TBL
V5732
Carbon Disulfide
<0.0008
mg/Kg - dry
0.0008
0.006
1
06/23/21 16:34
TBL
V5732
Carbon Tetrachloride
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
Chlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.006
1
06/23/21 16:34
TBL
V5732
Chlorodibromomethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
Chloroethane
<0.001
mg/Kg - dry
0.001
0.012
1
06/23/21 16:34
TBL
V5732
Chloroform
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
Chloromethane
<0.0008
mg/Kg - dry
0.0008
0.012
1
06/23/21 16:34
TBL
V5732
2-Chlorotoluene
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 16:34
TBL
V5732
4-Chlorotoluene
<0.0005
mg/Kg - dry
0.0005
0.006
1
06/23/21 16:34
TBL
V5732
Di -Isopropyl Ether (DIPE)
<0.0009
mg/Kg - dry
0.0009
0.006
1
06/23/21 16:34
TBL
V5732
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 6 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Lab No : 90168
Matrix: Solids
Sample ID: S-1
Sampled:
6/22/2021 10:15
Analytical Method: 8260D
Prep Batch(es):
V5728
06/23/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.0005
mg/Kg - dry
0.0005
0.012
1
06/23/21 16:34
TBL
V5732
1,2-Dibromoethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 16:34
TBL
V5732
Dibromomethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 16:34
TBL
V5732
1,2-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.006
1
06/23/21 16:34
TBL
V5732
1,3-Dichlorobenzene
<0.0005
mg/Kg - dry
0.0005
0.006
1
06/23/21 16:34
TBL
V5732
1,4-Dichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 16:34
TBL
V5732
Dichlorodifluoromethane
<0.001
mg/Kg - dry
0.001
0.012
1
06/23/21 16:34
TBL
V5732
1,1-Dichloroethane
<0.0010
mg/Kg - dry
0.0010
0.006
1
06/23/21 16:34
TBL
V5732
1,2-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
1,1-Dichloroethene
<0.0009
mg/Kg - dry
0.0009
0.006
1
06/23/21 16:34
TBL
V5732
cis- 1,2-Dich loroethene
<0.0010
mg/Kg - dry
0.0010
0.006
1
06/23/21 16:34
TBL
V5732
trans-1,2-Dichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
1,2-Dichloropropane
<0.0005
mg/Kg - dry
0.0005
0.006
1
06/23/21 16:34
TBL
V5732
1,3-Dichloropropane
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 16:34
TBL
V5732
2,2-Dichloropropane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
1,1-Dichloropropene
<0.0009
mg/Kg - dry
0.0009
0.006
1
06/23/21 16:34
TBL
V5732
cis- 1,3-Dich loropropene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 16:34
TBL
V5732
trans-1,3-Dichloropropene
<0.0010
mg/Kg - dry
0.0010
0.006
1
06/23/21 16:34
TBL
V5732
Ethylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 16:34
TBL
V5732
Ethyl Tertiary Butyl Ether (ETBE)
<0.001
mg/Kg - dry
0.001
0.060
1
06/23/21 16:34
TBL
V5732
Hexachlorobutadiene
<0.0010
mg/Kg - dry
0.0010
0.012
1
06/23/21 16:34
TBL
V5732
n-Hexane
<0.0008
mg/Kg - dry
0.0008
0.012
1
06/23/21 16:34
TBL
V5732
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 7 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Lab No : 90168
Matrix: Solids
Sample ID: S-1
Sampled:
6/22/2021 10:15
Analytical Method: 8260D
Prep Batch(es):
V5728
06/23/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Hexanone
<0.0008
mg/Kg - dry
0.0008
0.024
1
06/23/21 16:34
TBL
V5732
Isopropyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 16:34
TBL
V5732
4-Isopropyl toluene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
Methyl Ethyl Ketone (MEK)
<0.0008
mg/Kg - dry
0.0008
0.024
1
06/23/21 16:34
TBL
V5732
Methyl tert-butyl ether (MTBE)
<0.0008
mg/Kg - dry
0.0008
0.006
1
06/23/21 16:34
TBL
V5732
4-Methyl-2-Pentanone
<0.018
mg/Kg - dry
0.018
0.024
1
06/23/21 16:34
TBL
V5732
Methylene Chloride
<0.001
mg/Kg - dry
0.001
0.012
1
06/23/21 16:34
TBL
V5732
Naphthalene
<0.001
mg/Kg - dry
0.001
0.012
1
06/23/21 16:34
TBL
V5732
n-Propylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 16:34
TBL
V5732
Styrene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
1,1,1,2-Tetrachloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
1,1,2,2-Tetrachloroethane
<0.0004
mg/Kg - dry
0.0004
0.006
1
06/23/21 16:34
TBL
V5732
Tetrachloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
Toluene
<0.0008
mg/Kg - dry
0.0008
0.006
1
06/23/21 16:34
TBL
V5732
1,2,3-Trichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.012
1
06/23/21 16:34
TBL
V5732
1,2,4-Trichlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.012
1
06/23/21 16:34
TBL
V5732
1,1,1-Trichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
1,1,2-Trichloroethane
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 16:34
TBL
V5732
Trichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 16:34
TBL
V5732
Trichlorofluoromethane
<0.002
mg/Kg - dry
0.002
0.012
1
06/23/21 16:34
TBL
V5732
1,2,3-Trichloropropane
<0.0009
mg/Kg - dry
0.0009
0.006
1
06/23/21 16:34
TBL
V5732
1,3,5-Trimethyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 16:34
TBL
V5732
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 8 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Lab No : 90168 Matrix: Solids
Sample ID: S-1 Sampled: 6/22/2021 10:15
Analytical Method: 8260D Prep Batch(es): V5728 06/23/21 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Vinyl Acetate
<0.0006
mg/Kg - dry
0.0006
0.012
1
06/23/21 16:34
TBL
V5732
Vinyl Chloride
<0.0006
mg/Kg - dry
0.0006
0.012
1
06/23/21 16:34
TBL
V5732
o-Xylene
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 16:34
TBL
V5732
m,p-Xylene
<0.001
mg/Kg - dry
0.001
0.012
1
06/23/21 16:34
TBL
V5732
Xylene (Total)
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 16:34
V5732
Surrogate:4-Bromofluorobenzene
99.2
Limits:70-130%
1 06/23/21 16:34 TBL
V5732
Surrogate: Dibromofluoromethane
101
Limits: 84-123%
1 06/23/21 16:34 TBL
V5732
Surrogate: Toluene-d8
99.4
Limits: 76-129%
1 06/23/21 16:34 TBL
V5732
Analytical Method: 8270E
Prep Batch(es):
V5705
06/23/21 10:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.140
mg/Kg - dry
0.140
0.800
1
06/23/21 18:26
JMV
V5743
Acenaphthylene
<0.127
mg/Kg - dry
0.127
0.800
1
06/23/21 18:26
JMV
V5743
Aniline
<0.184
mg/Kg - dry
0.184
0.800
1
06/23/21 18:26
JMV
V5743
Anthracene
<0.173
mg/Kg - dry
0.173
0.800
1
06/23/21 18:26
JMV
V5743
Benzo(a)anthracene
<0.168
mg/Kg - dry
0.168
0.800
1
06/23/21 18:26
JMV
V5743
Benzo(a)pyrene
<0.178
mg/Kg - dry
0.178
0.800
1
06/23/21 18:26
JMV
V5743
Benzo(b)fluoranthene
<0.176
mg/Kg - dry
0.176
0.800
1
06/23/21 18:26
JMV
V5743
Benzo(g,h,i)perylene
<0.164
mg/Kg - dry
0.164
0.800
1
06/23/21 18:26
JMV
V5743
Benzo(k)fluoranthene
<0.166
mg/Kg - dry
0.166
0.800
1
06/23/21 18:26
JMV
V5743
Benzoic Acid
<0.703
mg/Kg - dry
0.703
2.42
1
06/23/21 18:26
JMV
V5743
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 9 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Lab No : 90168
Matrix: Solids
Sample ID: S-1
Sampled:
6/22/2021 10:15
Analytical Method: 8270E
Prep Batch(es):
V570S
06/23/21 10:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzyl alcohol
<0.127
mg/Kg - dry
0.127
0.800
1
06/23/21 18:26
JMV
V5743
Bis(2-Chloroethoxy)methane
<0.143
mg/Kg - dry
0.143
0.800
1
06/23/21 18:26
JMV
V5743
Bis(2-Chloroethyl)ether
<0.129
mg/Kg - dry
0.129
0.800
1
06/23/21 18:26
JMV
V5743
Bis(2-Chloroisopropyl)ether
<0.164
mg/Kg - dry
0.164
0.400
1
06/23/21 18:26
JMV
V5743
Bis(2-ethylhexyl)phthalate
<0.145
mg/Kg - dry
0.145
0.800
1
06/23/21 18:26
JMV
V5743
4-Bromophenyl phenyl ether
<0.132
mg/Kg - dry
0.132
0.800
1
06/23/21 18:26
JMV
V5743
Butyl benzyl phthalate
<0.136
mg/Kg - dry
0.136
0.400
1
06/23/21 18:26
JMV
V5743
4-Chloro-3-methylphenol
<0.112
mg/Kg - dry
0.112
0.800
1
06/23/21 18:26
JMV
V5743
4-Chloroaniline
<0.135
mg/Kg - dry
0.135
0.400
1
06/23/21 18:26
JMV
V5743
2-Chloronaphthalene
<0.140
mg/Kg - dry
0.140
0.800
1
06/23/21 18:26
JMV
V5743
2-Chlorophenol
<0.119
mg/Kg - dry
0.119
0.800
1
06/23/21 18:26
JMV
V5743
4-Chlorophenyl phenyl ether
<0.152
mg/Kg - dry
0.152
1.21
1
06/23/21 18:26
JMV
V5743
Chrysene
<0.172
mg/Kg - dry
0.172
0.800
1
06/23/21 18:26
JMV
V5743
Dibenz(a,h)anthracene
<0.278
mg/Kg - dry
0.278
0.800
1
06/23/21 18:26
JMV
V5743
Dibenzofuran
<0.144
mg/Kg - dry
0.144
0.800
1
06/23/21 18:26
JMV
V5743
1,2-Dichlorobenzene
<0.114
mg/Kg - dry
0.114
0.800
1
06/23/21 18:26
JMV
V5743
1,3-Dichlorobenzene
<0.117
mg/Kg - dry
0.117
0.800
1
06/23/21 18:26
JMV
V5743
1,4-Dichlorobenzene
<0.118
mg/Kg - dry
0.118
0.400
1
06/23/21 18:26
JMV
V5743
3,3'-Dichlorobenzidine
<0.178
mg/Kg - dry
0.178
0.800
1
06/23/21 18:26
JMV
V5743
2,4-Dichlorophenol
<0.116
mg/Kg - dry
0.116
0.800
1
06/23/21 18:26
JMV
V5743
Diethyl phthalate
<0.218
mg/Kg - dry
0.218
0.800
1
06/23/21 18:26
JMV
V5743
Dimethyl phthalate
<0.210
mg/Kg - dry
0.210
0.800
1
06/23/21 18:26
JMV
V5743
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 10 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Lab No : 90168
Matrix: Solids
Sample ID: S-1
Sampled:
6/22/2021 10:15
Analytical Method: 8270E
Prep Batch(es):
V570S
06/23/21 10:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2,4-Dimethyl phenol
<0.130
mg/Kg - dry
0.130
0.400
1
06/23/21 18:26
JMV
V5743
Di-n-butyl phthalate
<0.129
mg/Kg - dry
0.129
0.800
1
06/23/21 18:26
JMV
V5743
4,6-Dinitro-2-methylphenol
<0.290
mg/Kg - dry
0.290
1.82
1
06/23/21 18:26
JMV
V5743
2,4-Dinitrophenol
<0.630
mg/Kg - dry
0.630
1.82
1
06/23/21 18:26
JMV
V5743
2,4-Dinitrotoluene
<0.117
mg/Kg - dry
0.117
0.800
1
06/23/21 18:26
JMV
V5743
2,6-Dinitrotoluene
<0.130
mg/Kg - dry
0.130
0.800
1
06/23/21 18:26
JMV
V5743
Di-n-Octyl Phthalate
<0.173
mg/Kg - dry
0.173
0.400
1
06/23/21 18:26
JMV
V5743
Fluoranthene
<0.149
mg/Kg - dry
0.149
0.800
1
06/23/21 18:26
JMV
V5743
Fluorene
<0.155
mg/Kg - dry
0.155
0.800
1
06/23/21 18:26
JMV
V5743
Hexachlorobenzene
<0.128
mg/Kg - dry
0.128
0.800
1
06/23/21 18:26
JMV
V5743
Hexachlorobutadiene
<0.118
mg/Kg - dry
0.118
0.800
1
06/23/21 18:26
JMV
V5743
Hexachlorocyclopentadiene
<0.190
mg/Kg - dry
0.190
0.800
1
06/23/21 18:26
JMV
V5743
Hexachloroethane
<0.096
mg/Kg - dry
0.096
0.800
1
06/23/21 18:26
JMV
V5743
Indeno(1,2,3-cd)pyrene
<0.216
mg/Kg - dry
0.216
0.800
1
06/23/21 18:26
JMV
V5743
Isophorone
<0.231
mg/Kg - dry
0.231
0.800
1
06/23/21 18:26
JMV
V5743
1-Methylnaphthalene
<0.128
mg/Kg - dry
0.128
0.800
1
06/23/21 18:26
JMV
V5743
2-Methylnaphthalene
<0.121
mg/Kg - dry
0.121
0.800
1
06/23/21 18:26
JMV
V5743
2-Methylphenol
<0.117
mg/Kg - dry
0.117
0.800
1
06/23/21 18:26
JMV
V5743
3&4 Methylphenol
<0.102
mg/Kg - dry
0.102
0.800
1
06/23/21 18:26
JMV
V5743
Naphthalene
<0.174
mg/Kg - dry
0.174
0.800
1
06/23/21 18:26
JMV
V5743
2-Nitroaniline
<0.117
mg/Kg - dry
0.117
0.800
1
06/23/21 18:26
JMV
V5743
3-Nitroaniline
<0.145
mg/Kg - dry
0.145
0.800
1
06/23/21 18:26
JMV
V5743
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 11 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038
REPORT OF ANAL YSIS
Lab No : 90168 Matrix: Solids
Sample ID: S-1 Sampled: 6/22/2021 10:15
Analytical Method: 8270E Prep Batch(es): V570S 06/23/21 10:30
Prep Method: 3546
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
4-Nitroaniline
<0.113
mg/Kg - dry
0.113
0.400
1
06/23/21 18:26 JMV
V5743
Nitrobenzene
<0.140
mg/Kg - dry
0.140
0.400
1
06/23/21 18:26 JMV
V5743
2-Nitrophenol
<0.107
mg/Kg - dry
0.107
0.800
1
06/23/21 18:26 JMV
V5743
4-Nitrophenol
<0.141
mg/Kg - dry
0.141
0.800
1
06/23/21 18:26 JMV
V5743
N-N itrosodimethyla mine
<0.318
mg/Kg - dry
0.318
0.800
1
06/23/21 18:26 JMV
V5743
N-Nitrosodiphenylamine
<0.219
mg/Kg - dry
0.219
0.800
1
06/23/21 18:26 JMV
V5743
N-Nitroso-di-n-propylamine
<0.143
mg/Kg - dry
0.143
0.800
1
06/23/21 18:26 JMV
V5743
Pentachlorophenol
<0.420
mg/Kg - dry
0.420
1.21
1
06/23/21 18:26 JMV
V5743
Phenanthrene
<0.252
mg/Kg - dry
0.252
0.800
1
06/23/21 18:26 JMV
V5743
Phenol
<0.135
mg/Kg - dry
0.135
0.800
1
06/23/21 18:26 JMV
V5743
Pyrene
<0.162
mg/Kg - dry
0.162
0.800
1
06/23/21 18:26 JMV
V5743
Pyridine
<0.096
mg/Kg - dry
0.096
0.400
1
06/23/21 18:26 JMV
V5743
1,2,4-Trichlorobenzene
<0.129
mg/Kg - dry
0.129
0.800
1
06/23/21 18:26 JMV
V5743
2,4,5-Trichlorophenol
<0.116
mg/Kg - dry
0.116
0.800
1
06/23/21 18:26 JMV
V5743
2,4,6-Trichlorophenol
<0.117
mg/Kg - dry
0.117
0.800
1
06/23/21 18:26 JMV
V5743
Surrogate: Phenol-d5
88.6
Limits: 34-121%
1 06/23/21 18:26 JMV
V5743
Surrogate:2-Fluorobiphenyl
94.4
Limits:44-115%
1 06/23/21 18:26 JMV
V5743
Surrogate:2-Fluorophenol
88.6
Limits:35-115%
1 06/23/21 18:26 JMV
V5743
Surrogate: Nitrobenzene-d5
83.3
Limits: 37-122%
1 06/23/21 18:26 JMV
V5743
Surrogate:4-Terphenyl-d14
110
Limits:54-127%
1 06/23/21 18:26 JMV
V5743
Surrogate: 2,4,6-Tribromophenol
100
Limits:39-132%
1 06/23/21 18:26 JMV
V5743
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 12 of 53

WavDdibnto
ANALYTICAL
00019
F&R, Inc. - Charlotte
Brian Olin
3300 International Airport Dr., Suite 600
Charlotte , NC 28208
Project RA Eden
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Report Date : 06/30/2021
Received : 06/22/2021
Lab No : 90169
Sample ID: S-2
Matrix: Solids
Sampled: 6/22/2021 10:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
23.5
%
1
06/22/2115:37
EDV
SW-DRYWT
Arsenic
11.7
mg/Kg - dry
0.123
1.31
10
06/23/21 16:20
EDV
6020B
Barium
51.6
mg/Kg - dry
1.83
13.1
10
06/23/21 16:20
EDV
6020E
Cadmium
<0.0718
mg/Kg - dry
0.0718
0.654
10
06/23/21 16:20
EDV
6020B
Chromium
104
mg/Kg - dry
0.379
1.31
10
06/23/21 16:20
EDV
6020E
Lead
39.3
mg/Kg - dry
0.183
1.31
10
06/23/21 16:20
EDV
6020B
Mercury (Total)
0.02643
mg/Kg - dry
0.0157
0.0392
1
06/24/21 15:04
EDV
7471E
Selenium
1.703
mg/Kg - dry
1.18
2.61
10
06/23/21 16:20
EDV
6020B
Silver
<0.0535
mg/Kg - dry
0.0535
0.654
10
06/23/21 16:20
EDV
6020E
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 13 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Lab No : 90169
Matrix: Solids
Sample ID: S-2
Sampled:
6/22/2021 10:30
Analytical Method: 8260D
Prep Batch(es):
V5728
06/23/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
0.0033
mg/Kg - dry
0.003
0.026
1
06/23/21 17:04
TBL
V5732
Acrolein
<0.001
mg/Kg - dry
0.001
0.026
1
06/23/21 17:04
TBL
V5732
Acrylonitrile
<0.0010
mg/Kg - dry
0.0010
0.026
1
06/23/21 17:04
TBL
V5732
Benzene
<0.0008
mg/Kg - dry
0.0008
0.006
1
06/23/21 17:04
TBL
V5732
Bromobenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 17:04
TBL
V5732
Bromochloromethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
Bromodichloromethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
Bromoform
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
Bromomethane
<0.002
mg/Kg - dry
0.002
0.013
1
06/23/21 17:04
TBL
V5732
n-Butylbenzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 17:04
TBL
V5732
sec -Butyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 17:04
TBL
V5732
tert-Butyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 17:04
TBL
V5732
Carbon Disulfide
<0.0008
mg/Kg - dry
0.0008
0.006
1
06/23/21 17:04
TBL
V5732
Carbon Tetrachloride
<0.002
mg/Kg - dry
0.002
0.006
1
06/23/21 17:04
TBL
V5732
Chlorobenzene
<0.0009
mg/Kg - dry
0.0009
0.006
1
06/23/21 17:04
TBL
V5732
Chlorodibromomethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
Chloroethane
<0.001
mg/Kg - dry
0.001
0.013
1
06/23/21 17:04
TBL
V5732
Chloroform
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
Chloromethane
<0.0008
mg/Kg - dry
0.0008
0.013
1
06/23/21 17:04
TBL
V5732
2-Chlorotoluene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 17:04
TBL
V5732
4-Chlorotoluene
<0.0005
mg/Kg - dry
0.0005
0.006
1
06/23/21 17:04
TBL
V5732
Di -Isopropyl Ether (DIPE)
<0.0010
mg/Kg - dry
0.0010
0.006
1
06/23/21 17:04
TBL
V5732
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 14 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Lab No : 90169
Matrix: Solids
Sample ID: S-2
Sampled:
6/22/2021 10:30
Analytical Method: 8260D
Prep Batch(es):
V5728
06/23/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.0006
mg/Kg - dry
0.0006
0.013
1
06/23/21 17:04
TBL
V5732
1,2-Dibromoethane
<0.0008
mg/Kg - dry
0.0008
0.006
1
06/23/21 17:04
TBL
V5732
Dibromomethane
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 17:04
TBL
V5732
1,2-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.006
1
06/23/21 17:04
TBL
V5732
1,3-Dichlorobenzene
<0.0005
mg/Kg - dry
0.0005
0.006
1
06/23/21 17:04
TBL
V5732
1,4-Dichlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.006
1
06/23/21 17:04
TBL
V5732
Dichlorodifluoromethane
<0.001
mg/Kg - dry
0.001
0.013
1
06/23/21 17:04
TBL
V5732
1,1-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
1,2-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
1,1-Dichloroethene
<0.0010
mg/Kg - dry
0.0010
0.006
1
06/23/21 17:04
TBL
V5732
cis- 1,2-Dich loroethene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
trans-1,2-Dichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
1,2-Dichloropropane
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 17:04
TBL
V5732
1,3-Dichloropropane
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 17:04
TBL
V5732
2,2-Dichloropropane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
1,1-Dichloropropene
<0.0010
mg/Kg - dry
0.0010
0.006
1
06/23/21 17:04
TBL
V5732
cis- 1,3-Dich loropropene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 17:04
TBL
V5732
trans-1,3-Dichloropropene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
Ethylbenzene
<0.0008
mg/Kg - dry
0.0008
0.006
1
06/23/21 17:04
TBL
V5732
Ethyl Tertiary Butyl Ether (ETBE)
<0.001
mg/Kg - dry
0.001
0.065
1
06/23/21 17:04
TBL
V5732
Hexachlorobutadiene
<0.001
mg/Kg - dry
0.001
0.013
1
06/23/21 17:04
TBL
V5732
n-Hexane
<0.0009
mg/Kg - dry
0.0009
0.013
1
06/23/21 17:04
TBL
V5732
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 15 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Lab No : 90169
Matrix: Solids
Sample ID: S-2
Sampled:
6/22/2021 10:30
Analytical Method: 8260D
Prep Batch(es):
V5728
06/23/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Hexanone
<0.0008
mg/Kg - dry
0.0008
0.026
1
06/23/21 17:04
TBL
V5732
Isopropyl benzene
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 17:04
TBL
V5732
4-Isopropyl toluene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
Methyl Ethyl Ketone (MEK)
<0.0008
mg/Kg - dry
0.0008
0.026
1
06/23/21 17:04
TBL
V5732
Methyl tert-butyl ether (MTBE)
<0.0008
mg/Kg - dry
0.0008
0.006
1
06/23/21 17:04
TBL
V5732
4-Methyl-2-Pentanone
<0.019
mg/Kg - dry
0.019
0.026
1
06/23/21 17:04
TBL
V5732
Methylene Chloride
<0.001
mg/Kg - dry
0.001
0.013
1
06/23/21 17:04
TBL
V5732
Naphthalene
<0.001
mg/Kg - dry
0.001
0.013
1
06/23/21 17:04
TBL
V5732
n-Propylbenzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 17:04
TBL
V5732
Styrene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
1,1,1,2-Tetrachloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
1,1,2,2-Tetrachloroethane
<0.0004
mg/Kg - dry
0.0004
0.006
1
06/23/21 17:04
TBL
V5732
Tetrachloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
Toluene
<0.0009
mg/Kg - dry
0.0009
0.006
1
06/23/21 17:04
TBL
V5732
1,2,3-Trichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.013
1
06/23/21 17:04
TBL
V5732
1,2,4-Trichlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.013
1
06/23/21 17:04
TBL
V5732
1,1,1-Trichloroethane
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
1,1,2-Trichloroethane
<0.0006
mg/Kg - dry
0.0006
0.006
1
06/23/21 17:04
TBL
V5732
Trichloroethene
<0.001
mg/Kg - dry
0.001
0.006
1
06/23/21 17:04
TBL
V5732
Trichlorofluoromethane
<0.002
mg/Kg - dry
0.002
0.013
1
06/23/21 17:04
TBL
V5732
1,2,3-Trichloropropane
<0.0009
mg/Kg - dry
0.0009
0.006
1
06/23/21 17:04
TBL
V5732
1,3,5-Trimethyl benzene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 17:04
TBL
V5732
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 16 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Lab No : 90169 Matrix: Solids
Sample ID: S-2 Sampled: 6/22/2021 10:30
Analytical Method: 8260D Prep Batch(es): V5728 06/23/21 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Vinyl Acetate
<0.0006
mg/Kg - dry
0.0006
0.013
1
06/23/21 17:04
TBL
V5732
Vinyl Chloride
<0.0006
mg/Kg - dry
0.0006
0.013
1
06/23/21 17:04
TBL
V5732
o-Xylene
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 17:04
TBL
V5732
m,p-Xylene
<0.001
mg/Kg - dry
0.001
0.013
1
06/23/21 17:04
TBL
V5732
Xylene (Total)
<0.0007
mg/Kg - dry
0.0007
0.006
1
06/23/21 17:04
V5732
Surrogate:4-Bromofluorobenzene
99.7
Limits:70-130%
1 06/23/21 17:04 TBL
V5732
Surrogate: Dibromofluoromethane
102
Limits: 84-123%
1 06/23/21 17:04 TBL
V5732
Surrogate: Toluene-d8
98.7
Limits: 76-129%
1 06/23/21 17:04 TBL
V5732
Analytical Method: 8270E
Prep Batch(es):
V5705
06/23/21 10:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.151
mg/Kg - dry
0.151
0.862
1
06/23/21 18:49
JMV
V5743
Acenaphthylene
<0.137
mg/Kg - dry
0.137
0.862
1
06/23/21 18:49
JMV
V5743
Aniline
<0.198
mg/Kg - dry
0.198
0.862
1
06/23/21 18:49
JMV
V5743
Anthracene
<0.186
mg/Kg - dry
0.186
0.862
1
06/23/21 18:49
JMV
V5743
Benzo(a)anthracene
<0.181
mg/Kg - dry
0.181
0.862
1
06/23/21 18:49
JMV
V5743
Benzo(a)pyrene
<0.192
mg/Kg - dry
0.192
0.862
1
06/23/21 18:49
JMV
V5743
Benzo(b)fluoranthene
<0.190
mg/Kg - dry
0.190
0.862
1
06/23/21 18:49
JMV
V5743
Benzo(g,h,i)perylene
<0.177
mg/Kg - dry
0.177
0.862
1
06/23/21 18:49
JMV
V5743
Benzo(k)fluoranthene
<0.179
mg/Kg - dry
0.179
0.862
1
06/23/21 18:49
JMV
V5743
Benzoic Acid
<0.758
mg/Kg - dry
0.758
2.61
1
06/23/21 18:49
JMV
V5743
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 17 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038 REPOR T OF A NA L YSIS
Lab No : 90169
Matrix: Solids
Sample ID: S-2
Sampled:
6/22/2021 10:30
Analytical Method: 8270E
Prep Batch(es):
VS70S
06/23/21 10:30
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzyl alcohol
<0.137
mg/Kg - dry
0.137
0.862
1
06/23/21 18:49
JMV
V5743
Bis(2-Chloroethoxy)methane
<0.154
mg/Kg - dry
0.154
0.862
1
06/23/21 18:49
JMV
V5743
Bis(2-Chloroethyl)ether
<0.139
mg/Kg - dry
0.139
0.862
1
06/23/21 18:49
JMV
V5743
Bis(2-Chloroisopropyl)ether
<0.177
mg/Kg - dry
0.177
0.431
1
06/23/21 18:49
JMV
V5743
Bis(2-ethylhexyl)phthalate
<0.156
mg/Kg - dry
0.156
0.862
1
06/23/21 18:49
JMV
V5743
4-Bromophenyl phenyl ether
<0.142
mg/Kg - dry
0.142
0.862
1
06/23/21 18:49
JMV
V5743
Butyl benzyl phthalate
<0.147
mg/Kg - dry
0.147
0.431
1
06/23/21 18:49
JMV
V5743
4-Chloro-3-methylphenol
<0.120
mg/Kg - dry
0.120
0.862
1
06/23/21 18:49
JMV
V5743
4-Chloroaniline
<0.146
mg/Kg - dry
0.146
0.431
1
06/23/21 18:49
JMV
V5743
2-Chloronaphthalene
<0.151
mg/Kg - dry
0.151
0.862
1
06/23/21 18:49
JMV
V5743
2-Chlorophenol
<0.128
mg/Kg - dry
0.128
0.862
1
06/23/21 18:49
JMV
V5743
4-Chlorophenyl phenyl ether
<0.164
mg/Kg - dry
0.164
1.31
1
06/23/21 18:49
JMV
V5743
Chrysene
<0.185
mg/Kg - dry
0.185
0.862
1
06/23/21 18:49
JMV
V5743
Dibenz(a,h)anthracene
<0.300
mg/Kg - dry
0.300
0.862
1
06/23/21 18:49
JMV
V5743
Dibenzofuran
<0.155
mg/Kg - dry
0.155
0.862
1
06/23/21 18:49
JMV
V5743
1,2-Dichlorobenzene
<0.123
mg/Kg - dry
0.123
0.862
1
06/23/21 18:49
JMV
V5743
1,3-Dichlorobenzene
<0.127
mg/Kg - dry
0.127
0.862
1
06/23/21 18:49
JMV
V5743
1,4-Dichlorobenzene
<0.127
mg/Kg - dry
0.127
0.431
1
06/23/21 18:49
JMV
V5743
3,3'-Dichlorobenzidine
<0.192
mg/Kg - dry
0.192
0.862
1
06/23/21 18:49
JMV
V5743
2,4-Dichlorophenol
<0.125
mg/Kg - dry
0.125
0.862
1
06/23/21 18:49
JMV
V5743
Diethyl phthalate
<0.235
mg/Kg - dry
0.235
0.862
1
06/23/21 18:49
JMV
V5743
Dimethyl phthalate
<0.227
mg/Kg - dry
0.227
0.862
1
06/23/21 18:49
JMV
V5743
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 18 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038
REPORT OF ANAL YSIS
Lab No : 90169 Matrix: Solids
Sample ID: S-2 Sampled: 6/22/2021 10:30
Analytical Method: 8270E Prep Batch(es): VS70S 06/23/21 10:30
Prep Method: 3546
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
2,4-Dimethyl phenol
<0.141
mg/Kg - dry
0.141
0.431
1
06/23/21 18:49
JMV
V5743
Di-n-butyl phthalate
<0.139
mg/Kg - dry
0.139
0.862
1
06/23/21 18:49
JMV
V5743
4,6-Dinitro-2-methylphenol
<0.313
mg/Kg - dry
0.313
1.96
1
06/23/21 18:49
JMV
V5743
2,4-Dinitrophenol
<0.679
mg/Kg - dry
0.679
1.96
1
06/23/21 18:49
JMV
V5743
2,4-Dinitrotoluene
<0.126
mg/Kg - dry
0.126
0.862
1
06/23/21 18:49
JMV
V5743
2,6-Dinitrotoluene
<0.141
mg/Kg - dry
0.141
0.862
1
06/23/21 18:49
JMV
V5743
Di-n-Octyl Phthalate
<0.186
mg/Kg - dry
0.186
0.431
1
06/23/21 18:49
JMV
V5743
Fluoranthene
<0.160
mg/Kg - dry
0.160
0.862
1
06/23/21 18:49
JMV
V5743
Fluorene
<0.167
mg/Kg - dry
0.167
0.862
1
06/23/21 18:49
JMV
V5743
Hexachlorobenzene
<0.138
mg/Kg - dry
0.138
0.862
1
06/23/21 18:49
JMV
V5743
Hexachlorobutadiene
<0.127
mg/Kg - dry
0.127
0.862
1
06/23/21 18:49
JMV
V5743
Hexachlorocyclopentadiene
<0.205
mg/Kg - dry
0.205
0.862
1
06/23/21 18:49
JMV
V5743
Hexachloroethane
<0.103
mg/Kg - dry
0.103
0.862
1
06/23/21 18:49
JMV
V5743
Indeno(1,2,3-cd)pyrene
<0.233
mg/Kg - dry
0.233
0.862
1
06/23/21 18:49
JMV
V5743
Isophorone
<0.249
mg/Kg - dry
0.249
0.862
1
06/23/21 18:49
JMV
V5743
1-Methylnaphthalene
<0.138
mg/Kg - dry
0.138
0.862
1
06/23/21 18:49
JMV
V5743
2-Methylnaphthalene
<0.130
mg/Kg - dry
0.130
0.862
1
06/23/21 18:49
JMV
V5743
2-Methylphenol
<0.126
mg/Kg - dry
0.126
0.862
1
06/23/21 18:49
JMV
V5743
3&4 Methylphenol
<0.110
mg/Kg - dry
0.110
0.862
1
06/23/21 18:49
JMV
V5743
Naphthalene
<0.188
mg/Kg - dry
0.188
0.862
1
06/23/21 18:49
JMV
V5743
2-Nitroaniline
<0.126
mg/Kg - dry
0.126
0.862
1
06/23/21 18:49
JMV
V5743
3-Nitroaniline
<0.156
mg/Kg - dry
0.156
0.862
1
06/23/21 18:49
JMV
V5743
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 19 of 53

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 06/30/2021
3300 International Airport Dr., Suite 600 Information : Received : 06/22/2021
Charlotte , NC 28208
Report Number : 21-173-0038
REPORT OF ANAL YSIS
Lab No : 90169 Matrix: Solids
Sample ID: S-2 Sampled: 6/22/2021 10:30
Analytical Method: 8270E Prep Batch(es): VS70S 06/23/21 10:30
Prep Method: 3546
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
4-Nitroaniline
<0.121
mg/Kg - dry
0.121
0.431
1
06/23/21 18:49 JMV
V5743
Nitrobenzene
<0.151
mg/Kg - dry
0.151
0.431
1
06/23/21 18:49 JMV
V5743
2-Nitrophenol
<0.116
mg/Kg - dry
0.116
0.862
1
06/23/21 18:49 JMV
V5743
4-Nitrophenol
<0.152
mg/Kg - dry
0.152
0.862
1
06/23/21 18:49 JMV
V5743
N-N itrosodimethyla mine
<0.343
mg/Kg - dry
0.343
0.862
1
06/23/21 18:49 JMV
V5743
N-Nitrosodiphenylamine
<0.236
mg/Kg - dry
0.236
0.862
1
06/23/21 18:49 JMV
V5743
N-Nitroso-di-n-propylamine
<0.154
mg/Kg - dry
0.154
0.862
1
06/23/21 18:49 JMV
V5743
Pentachlorophenol
<0.453
mg/Kg - dry
0.453
1.31
1
06/23/21 18:49 JMV
V5743
Phenanthrene
<0.271
mg/Kg - dry
0.271
0.862
1
06/23/21 18:49 JMV
V5743
Phenol
<0.146
mg/Kg - dry
0.146
0.862
1
06/23/21 18:49 JMV
V5743
Pyrene
<0.175
mg/Kg - dry
0.175
0.862
1
06/23/21 18:49 JMV
V5743
Pyridine
<0.103
mg/Kg - dry
0.103
0.431
1
06/23/21 18:49 JMV
V5743
1,2,4-Trichlorobenzene
<0.139
mg/Kg - dry
0.139
0.862
1
06/23/21 18:49 JMV
V5743
2,4,5-Trichlorophenol
<0.125
mg/Kg - dry
0.125
0.862
1
06/23/21 18:49 JMV
V5743
2,4,6-Trichlorophenol
<0.126
mg/Kg - dry
0.126
0.862
1
06/23/21 18:49 JMV
V5743
Surrogate: Phenol-d5
88.8
Limits: 34-121%
1 06/23/21 18:49 JMV
V5743
Surrogate:2-Fluorobiphenyl
92.2
Limits:44-115%
1 06/23/21 18:49 JMV
V5743
Surrogate:2-Fluorophenol
89.7
Limits:35-115%
1 06/23/21 18:49 JMV
V5743
Surrogate: Nitrobenzene-d5
83.1
Limits: 37-122%
1 06/23/21 18:49 JMV
V5743
Surrogate:4-Terphenyl-d14
104
Limits:54-127%
1 06/23/21 18:49 JMV
V5743
Surrogate: 2,4,6-Tribromophenol
96.4
Limits:39-132%
1 06/23/21 18:49 JMV
V5743
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 20 of 53

aceAnalytical
Report of Analysis
Waypoint Analytical
PO Box 240543
Charlotte, NC 28224
Attention: Angela Overcash
Project Name: 21-173-0038
Lot Number:WF24006
Date Completed:06/30/2021
06/30/2021 2:59 PM
Approved and released by:
Project Manager II: Lucas Odom
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12
Page 21 of 53

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Waypoint Analytical
Lot Number: WF24006
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] whw.pacelabs.com
Page 2 of 12
Page 22 of 53

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: WF24006
Sample Number Sample ID Matrix Date Sampled Date Received
001 S-1 Solid 06/22/20211015 06/23/2021
002 S-2 Solid 06/22/20211030 06/23/2021
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Waypoint Analytical
Lot Number: WF24006
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 S-1 Solid Hexavalent Chromium 7199 0.41 J mg/kg 5
002 S-2 Solid Hexavalent Chromium 7199 0.29 J mg/kg 6
(2 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 12

Client:Waypoint Analytical Laboratory ID: WF24006-001
Description: S-1 Matrix: Solid
Date Sampled:06/22/2021 1015 % Solids: 78.1 06/25/2021 0009
Date Received:06/23/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 06/28/2021 1824 AMR 06/25/2021 1155 96476
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexavalent Chromium
18540-29-9 7199 0.41 J 1.3 0.26 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client:Waypoint Analytical Laboratory ID: WF24006-002
Description: S-2 Matrix: Solid
Date Sampled:06/22/2021 1030 % Solids: 76.9 06/25/2021 0009
Date Received:06/23/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 06/28/2021 1903 AMR 06/25/2021 1155 96476
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexavalent Chromium
18540-29-9 7199 0.29 J 1.3 0.26 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 12

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 12

Inorganic non-metals - MB
Sample ID: WQ96476-001 Matrix: Solid
Batch: 96476 Prep Method: 3060A
Analytical Method: 7199 Prep Date: 06/25/2021 1155
Parameter Result Q Dil LOQ DL Units Analysis Date
Hexavalent Chromium ND 1 1.0 0.20 mg/kg 06/28/2021 1352
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 12

Inorganic non-metals - LCS
Sample ID: WQ96476-002 Matrix: Solid
Batch: 96476 Prep Method: 3O6OA
Analytical Method: 7199 Prep Date: 06/25/2021 1155
Spike
Amount Result %Rec
Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date
Hexavalent Chromium 10 9.7 1 97 80-120 06/28/2021 1405
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 12

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
Samples Receipt Checklist [SRC] (MEl 0IM-151 Revised,,/29/2020
"ff1 lri0iC,tt IssuingAat.n�rity-PaexENV -1AIC L Page of 1
arJllple Reeeipl Checklist (RQ
Glicut; 'd+A 'W INr Gao�LlrLTjs rctCrl !dWL;: M2 re U23.QM1 * �,L ;;
Nuns of receipt Pace r-lienl UPS Fe.dF.x 01h�r:
J , wgro ouAody $Cali I S4pt 0a1 She ogpler?
Yes
I Nok J NA 12L IFcustody seals werr} preswt, w4rcih�,,y intact and mbrok=7
pH Strip ID; `I" (�lllQrine $t1 ip la TeS ed bV_ NA
C]rigilsal CempemiLtm uop1i receijt? Ekaiived(ConTeted) teirpemtw�e Fipon-eceip' 4ASalid Srwp Cup 1D; 2i-2�8
2,, 12_1 oC MA DNA or+ MA [NA cC KA }HA oC
Mnthodi; Q'rempr-nt1w, Rim,( EIAZrrM Fiollles I {'run Mr. 5 TR OlLn ('.ILrmulion PHcfcw- 0 °{
Method ;jf-^_w'.ant, IEWu Jiro Oleo hocks © Dry Ir: ❑ Nanc
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0 No
❑d NA
-
NA
3, 1,` txtrLpera#urc A by cooler Cxt;elxlotl ,{1°f', wtts i'roj;,C# [�I�lnagryr lkl•,t;t1; ��
TAM was'Jntrf"H by; plione f mnMI r fnc�to-face {circle one),
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'I- 1s-th._e _.c._omm__r.. re--ial cour-ier's pec€:ing aiip attac[2cd to thi4 #nrm'?
5_ Vk+Lrc T��per ccsiL�L€y prna rdure� (relingµisFled,'rcc�ivcd] f411vw�d':
Yee
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ND
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Nu
6. YY k'I t` $dIIL IC II7s 114LCSl UL. jlC �{��'�
q(
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Nr�
17. Were sample IDs listed on all sample containers?
,r
Yeb
Nip
8. Was collecton da-e & time listed on Lhe COC ?
,f
Yes
No
9_ "as collect-_= da'e & tiutia 1_sted on all sample containers?
Yes
Na
11). Did all -onrairwr Jabol inliarr zbmi ;ID, date, time) agree vEti3 the C~QCf?
,r YZ
NL>'
11. Wa tests t0 be per:amec listed all IV C OC9
© Yw
0 No
12. ID u1 all snmpin diri ve i11 LI IG pj-.L p4:r Up3MUinl;r5 FUT Bach Lust PmFor in goad condition
1111 L41-en, IMF, on, etc_)'?
Yea
7dn
13, Was adequate sar_yple volume avai'able?
d Y_es
N{I
m 14_ Were 3aplesreceived %viLhirl ;Le
� LITIu'ding;wm ir;L4 ur48 hours, which�worca!st? s Fir
C;'es
0 No
l a. W u any samples rortminers missin Wexcem (circle one) Sam [es h10 listed on C()C7
Yes
El No
A
16, For VOA and RSX-! 75 samples, wc:e Imbbles praseuL 'pea-;ize' (A"or 6113us in rliurLlder)
In Lmy of tho VOA vimis?
Yes
Lj No
d
_
17_ Were all D>1<OkeeralxlnutrianLaars l t mec!j r r[ era PIA of<
Yrn
No'
_A
J NA
] 9. Were a Il V� miidc samples rooeived at a plrl. > 12 and rsulfj o S0.1rL[71gs mocivcd aL 4 pH?
9 ?
Yes
❑No
❑NA
ICJ. Weraall applicable NHIAKN+cyanide,phat�o[1 25.1163E-3 (<0.5mWjj samples k,.c of
re€idual C1Llariue?
❑ Yr"
r,Nol
I
71Nn
21 Werecliem iuuarksrrNu.n—,LS(i.e_ Mgnamicrl rilut,una. IvISIMSD deli.onations, etc.__)
correctiy transcribed from the C30C, Into The Omw cilt section in L M5?
Yes
,f NTol
J21.
Was tte gnote n u m her li uefl rm thr containcr labe I? if yes, Quote #
Sumplc
Preservation (Must he completed for ary mrApla(s) inc'.onwdy preserved er with headspace-)
sample(&) _�'� were received ircL]'recLlu :srm;L:_,+,d and wt'erc Adjusted RGODrr:Er_gly
in sample receiving with ^ ml, of oifclo one; kS01, HNO3, HCJ, NlaO14 u3Jdp, SR 4 NA
'1 tme ofPresenution If Mow Lhwi ono prescTmti%-c is ncedcd, please note in the cornw. tnM Isolow.
SAmlAc(S) NA wax rcc�ivcd withbubbks>6 mm in diameter,
S MPlw(s� �^ warts rrmivcd w=1h '17t > 0.5 Tng/>~ (If#19 is no.) and were
adjust moL)3nlirLg_y i_I �;kupiTl[e rcu:ivinF, w4b Sodium thioudfate (Naz$3Qp);Y[LIt Shealy ID; "A
S(t barcooe labels applied by;[2C;2 - Date: {42ar31
COtt Mr mT4;
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 12

Waypointo
ANALYTICAL
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-173-0038
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep:
V5678
QC Analytical Batch(es): V5729
QC Prep Batch Method:
3050B
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Lab Reagent Blank
LRB-V5678
Matrix: SOL
Associated Lab Samples:
90168, 90169
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Arsenic
mg/Kg
<0.0940
0.0940
1.00
06/23/2115:21
Barium
mg/Kg
<1.40
1.40
10.0
06/23/2115:21
Cadmium
mg/Kg
<0.0550
0.0550
0.500
06/23/2115:21
Chromium
mg/Kg
<0.290
0.290
1.00
06/23/2115:21
Lead
mg/Kg
<0.140
0.140
1.00
06/23/2115:21
Selenium
mg/Kg
<0.900
0.900
2.00
06/23/2115:21
Silver
mg/Kg
<0.0410
0.0410
0.500
06/23/2115:21
Laboratory Control Sample
LCS-V5678
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Arsenic
mg/Kg
12.5
11.9
95.0
80-120
Barium
mg/Kg
12.5
11.9
95.0
80-120
Cadmium
mg/Kg
12.5
11.8
94.0
80-120
Chromium
mg/Kg
12.5
12.2
98.0
80-120
Lead
mg/Kg
12.5
12.1
97.0
80-120
Selenium
mg/Kg
12.5
11.2
90.0
80-120
Silver
mg/Kg
5.00
4.69
94.0
80-120
Matrix Spike & Matrix Spike Duplicate
V 90168-MS-V5678
V 90168-MSD-V5678
MS Spike
MSD
MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Arsenic
mg/Kg
4.56
12.5
12.5
16.9
17.3
99.0
102
75-125
2.3
20
Barium
mg/Kg
42.5
12.5
12.5
68.4
70.4
207*
223*
75-125
2.8
20
Cadmium
mg/Kg
<0.0550
12.5
12.5
12.5
12.6
100
101
75-125
0.7
20
Chromium
mg/Kg
54.2
12.5
12.5
109
135
438*
646*
75-125
21.3*
20
* QC Fail Date: 06/30/2021 03:19 PM Page 1 of 19
Page 33 of 53

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
F&R, Inc. - Charlotte
Project Description:
RA Eden
Report No:
21-173-0038
QC Prep:
V5678
QC Analytical Batch(es): V5729
QC Prep Batch Method:
3050B
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Matrix Spike & Matrix Spike
Duplicate
V 90168-MS-V5678
V 90168-MSD-V5678
MS Spike
MSD MS Result
MSD MS
MSD
%Rec Max
Parameter
Units
Result
Conc.
Spike
Result a/oRec
%Rec
Limits RPD RPD
Conc.
Lead
mg/Kg
17.9
12.5
12.5 33.0
32.3 121
115
75-125 2.1 20
Selenium
mg/Kg
1.20
12.5
12.5 13.5
12.0 108
96.0
75-125 11.7 20
Silver
mg/Kg
<0.0410
5.00
5.00 4.93
4.93 99.0
99.0
75-125 0.0 20
Post Digestion Spike
V 90168-PDS-V5678
PDS
%
Analyzed
Parameter
Units
Result
Recovery
Arsenic
mg/Kg
15.1
102
06/23/2116:07
Barium
mg/Kg
34.0
101
06/23/2116:07
Cadmium
mg/Kg
12.5
100
06/23/2116:07
Chromium
mg/Kg
38.1
96.0
06/23/2116:07
Lead
mg/Kg
21.2
99.0
06/23/21 16:07
Selenium
mg/Kg
13.0
104
06/23/2116:07
Silver
mg/Kg
12.4
100
06/23/2116:07
Date: 06/30/2021 03:19 PM Page 2 of 19
Page 34 of 53

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-173-0038
QC Prep: V5771
QC Analytical Batch(es): V5778
QC Prep Batch Method: 7471B (Prep)
Analysis Method:
7471B
Analysis Description:
Solids Total Mercury Analysis - CVAA
Lab Reagent Blank
LRB-V5771
Matrix: SOL
Associated Lab Samples: 90168, 90169
Blank MDL
MQL
Analyzed
Parameter Units
Result
Mercury (Total) mg/Kg
<0.0120 0.0120
0.0300
06/24/21 14:32
Laboratory Control Sample
LCS-V5771
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Mercury (Total) mg/Kg
0.417
0.408
98.0 80-120
Matrix Spike & Matrix Spike Duplicate
V 90168-MS-V5771
V 90168-MSD-V5771
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Mercury (Total) mg/Kg
0.0400 0.417
0.417 0.446
0.458 97.0 100 80-120 2.6 20
Post Digestion Spike
V 90168-PDS-V5771
PDS
%
Analyzed
Parameter Units
Result
Recovery
Mercury (Total) mg/Kg
0.223
98.0
06/24/21 14:55
Date: 06/30/2021 03:19 PM Page 3 of 19
Page 35 of 53

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-173-0038
QC Prep: V5728
QC Prep Batch Method: 5035 LOW
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V5732
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V5728 Matrix: SOL
Associated Lab Samples: 90168, 90169
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
mg/Kg
<0.002
0.002
0.020
06/23/21 13:35
Acrolein
mg/Kg
<0.001
0.001
0.020
06/23/21 13:35
Acrylonitrile
mg/Kg
<0.0008
0.0008
0.020
06/23/21 13:35
Benzene
mg/Kg
<0.0006
0.0006
0.005
06/23/21 13:35
Bromobenzene
mg/Kg
<0.0005
0.0005
0.005
06/23/21 13:35
Bromochloromethane
mg/Kg
<0.0008
0.0008
0.005
06/23/21 13:35
Bromodichloromethane
mg/Kg
<0.001
0.001
0.005
06/23/21 13:35
Bromoform
mg/Kg
<0.001
0.001
0.005
06/23/21 13:35
Bromomethane
mg/Kg
<0.001
0.001
0.010
06/23/21 13:35
n-Butylbenzene
mg/Kg
<0.0005
0.0005
0.005
06/23/21 13:35
sec -Butyl benzene
mg/Kg
<0.0006
0.0006
0.005
06/23/21 13:35
tert-Butyl benzene
mg/Kg
<0.0005
0.0005
0.005
06/23/21 13:35
Carbon Disulfide
mg/Kg
<0.0006
0.0006
0.005
06/23/21 13:35
Carbon Tetrachloride
mg/Kg
<0.001
0.001
0.005
06/23/21 13:35
Chlorobenzene
mg/Kg
<0.0007
0.0007
0.005
06/23/21 13:35
Chlorodibromomethane
mg/Kg
<0.0009
0.0009
0.005
06/23/21 13:35
Chloroethane
mg/Kg
<0.0009
0.0009
0.010
06/23/21 13:35
Chloroform
mg/Kg
<0.001
0.001
0.005
06/23/21 13:35
Chloromethane
mg/Kg
<0.0006
0.0006
0.010
06/23/21 13:35
2-Chlorotoluene
mg/Kg
<0.0005
0.0005
0.005
06/23/21 13:35
4-Chlorotoluene
mg/Kg
<0.0004
0.0004
0.005
06/23/21 13:35
Di -Isopropyl Ether (DIPE)
mg/Kg
<0.0007
0.0007
0.005
06/23/21 13:35
1,2-Dibromo-3-Chloropropane
mg/Kg
<0.0004
0.0004
0.010
06/23/21 13:35
1,2-Dibromoethane
mg/Kg
<0.0006
0.0006
0.005
06/23/21 13:35
Dibromomethane
mg/Kg
<0.0006
0.0006
0.005
06/23/21 13:35
1,2-Dichlorobenzene
mg/Kg
<0.0003
0.0003
0.005
06/23/21 13:35
1,3-Dichlorobenzene
mg/Kg
<0.0004
0.0004
0.005
06/23/21 13:35
Date:
06/30/2021 03:19 PM
Page 4 of 19
Page 36 of 53

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-173-0038
QC Prep: V5728
QC Prep Batch Method: 5035 LOW
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V5732
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V5728 Matrix: SOL
Associated Lab Samples: 90168, 90169
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.0006
0.0006
0.005
06/23/21 13:35
Dichlorodifluoromethane
mg/Kg
<0.001
0.001
0.010
06/23/21 13:35
1,1-Dichloroethane
mg/Kg
<0.0008
0.0008
0.005
06/23/21 13:35
1,2-Dichloroethane
mg/Kg
<0.001
0.001
0.005
06/23/21 13:35
1,1-Dichloroethene
mg/Kg
<0.0007
0.0007
0.005
06/23/21 13:35
cis-1,2-Dichloroethene
mg/Kg
<0.0008
0.0008
0.005
06/23/21 13:35
trans-1,2-Dichloroethene
mg/Kg
<0.001
0.001
0.005
06/23/21 13:35
1,2-Dichloropropane
mg/Kg
<0.0004
0.0004
0.005
06/23/21 13:35
1,3-Dichloropropane
mg/Kg
<0.0006
0.0006
0.005
06/23/21 13:35
2,2-Dichloropropane
mg/Kg
<0.001
0.001
0.005
06/23/21 13:35
1,1-Dichloropropene
mg/Kg
<0.0008
0.0008
0.005
06/23/21 13:35
cis-1,3-Dichloropropene
mg/Kg
<0.0005
0.0005
0.005
06/23/21 13:35
trans-1,3-Dichloropropene
mg/Kg
<0.0008
0.0008
0.005
06/23/21 13:35
Ethylbenzene
mg/Kg
<0.0006
0.0006
0.005
06/23/21 13:35
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
<0.0008
0.0008
0.050
06/23/21 13:35
Hexachlorobutadiene
mg/Kg
<0.0008
0.0008
0.010
06/23/21 13:35
n-Hexane
mg/Kg
<0.0007
0.0007
0.010
06/23/21 13:35
2-Hexanone
mg/Kg
<0.0006
0.0006
0.020
06/23/21 13:35
Isopropyl benzene
mg/Kg
<0.0005
0.0005
0.005
06/23/21 13:35
4-Isopropyl toluene
mg/Kg
<0.001
0.001
0.005
06/23/21 13:35
Methyl Ethyl Ketone (MEK)
mg/Kg
<0.0007
0.0007
0.020
06/23/21 13:35
Methyl tert-butyl ether (MTBE)
mg/Kg
<0.0006
0.0006
0.005
06/23/21 13:35
4-Methyl-2-Pentanone
mg/Kg
<0.015
0.015
0.020
06/23/21 13:35
Methylene Chloride
mg/Kg
<0.001
0.001
0.010
06/23/21 13:35
Naphthalene
mg/Kg
<0.0010
0.0010
0.010
06/23/21 13:35
n-Propylbenzene
mg/Kg
<0.0005
0.0005
0.005
06/23/21 13:35
Styrene
mg/Kg
<0.001
0.001
0.005
06/23/21 13:35
Date:
06/30/2021 03:19 PM
Page 5 of 19
Page 37 of 53

Waypointo
ANALYTICAL
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-173-0038
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V5728 QC Analytical Batch(es): V5732
QC Prep Batch Method: 5035 LOW Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V5728 Matrix: SOL
Associated Lab Samples: 90168, 90169
Parameter
Units
Blank
Result
MDL
MQL
Analyzed
%
Recovery
% Rec
Limits
1,1,1,2-Tetrachloroethane
mg/Kg
<0.001
0.001
0.005
06/23/21 13:35
1,1,2,2-Tetrachloroethane
mg/Kg
<0.0003
0.0003
0.005
06/23/21 13:35
Tetrachloroethene
mg/Kg
<0.0009
0.0009
0.005
06/23/21 13:35
Toluene
mg/Kg
<0.0007
0.0007
0.005
06/23/21 13:35
1,2,3-Trichlorobenzene
mg/Kg
<0.0005
0.0005
0.010
06/23/21 13:35
1,2,4-Trichlorobenzene
mg/Kg
<0.0006
0.0006
0.010
06/23/21 13:35
1,1,1-Trichloroethane
mg/Kg
<0.001
0.001
0.005
06/23/21 13:35
1,1,2-Trichloroethane
mg/Kg
<0.0005
0.0005
0.005
06/23/21 13:35
Trichloroethene
mg/Kg
<0.0009
0.0009
0.005
06/23/21 13:35
Trichlorofluoromethane
mg/Kg
<0.002
0.002
0.010
06/23/21 13:35
1,2,3-Trichloropropane
mg/Kg
<0.0007
0.0007
0.005
06/23/21 13:35
1,3,5-Trimethyl benzene
mg/Kg
<0.0005
0.0005
0.005
06/23/21 13:35
Vinyl Acetate
mg/Kg
<0.0005
0.0005
0.010
06/23/21 13:35
Vinyl Chloride
mg/Kg
<0.0005
0.0005
0.010
06/23/21 13:35
o-Xylene
mg/Kg
<0.0005
0.0005
0.005
06/23/21 13:35
m,p-Xylene
mg/Kg
<0.001
0.001
0.010
06/23/21 13:35
4-Bromofluorobenzene (S)
06/23/21 13:35
101
70-130
Dibromofluoromethane (S)
06/23/21 13:35
99.8
84-123
Toluene-d8 (S)
06/23/21 13:35
99.8
76-129
Laboratory Control Sample & LCSD
LCS-V5728
LCSD-V5728
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter Units
Conc.
Result
Result
%Rec
% Rec
Limits
RPD
Max
RPD
Acetone mg/Kg
0.100
0.129
0.124
129
124
29-198
3.9
20
Acrolein mg/Kg
0.100
0.119
0.118
119
118
70-130
0.8
20
Acrylonitrile mg/Kg
0.100
0.106
0.105
106
105
65-134
0.9
20
Date: 06/30/2021 03:19 PM Page 6 of 19
Page 38 of 53

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-173-0038
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V5728 QC Analytical Batch(es): V5732
QC Prep Batch Method: 5035 LOW Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V5728 LCSD-V5728
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Benzene
mg/Kg
0.050
0.051
0.050
102
101
74-127
1.3
20
Bromobenzene
mg/Kg
0.050
0.050
0.050
102
101
73-125
0.1
20
Bromochloromethane
mg/Kg
0.050
0.048
0.048
96.8
97.6
72-134
0.8
20
Bromodichloromethane
mg/Kg
0.050
0.050
0.050
100
100
75-122
0.0
20
Bromoform
mg/Kg
0.050
0.052
0.052
106
104
66-135
1.3
20
Bromomethane
mg/Kg
0.050
0.062
0.061
125
122
20-180
2.5
20
n-Butylbenzene
mg/Kg
0.050
0.055
0.054
111
109
65-135
1.4
20
sec -Butyl benzene
mg/Kg
0.050
0.054
0.052
108
105
66-131
2.9
20
tert-Butyl benzene
mg/Kg
0.050
0.052
0.051
105
102
67-132
2.5
20
Carbon Disulfide
mg/Kg
0.050
0.051
0.050
104
101
61-129
2.1
20
Carbon Tetrachloride
mg/Kg
0.050
0.053
0.051
106
103
64-143
3.4
20
Chlorobenzene
mg/Kg
0.050
0.050
0.049
102
99.8
74-118
1.7
20
Chlorodibromomethane
mg/Kg
0.050
0.051
0.050
103
102
73-122
1.1
20
Chloroethane
mg/Kg
0.050
0.052
0.052
105
106
33-149
0.5
20
Chloroform
mg/Kg
0.050
0.048
0.048
97.8
97.0
73-127
0.8
20
Chloromethane
mg/Kg
0.050
0.055
0.054
111
109
45-143
1.8
20
2-Chlorotoluene
mg/Kg
0.050
0.052
0.051
104
103
67-124
0.9
20
4-Chlorotoluene
mg/Kg
0.050
0.052
0.051
104
103
71-126
0.9
20
Di -Isopropyl Ether (DIPE)
mg/Kg
0.050
0.050
0.050
101
100
59-159
0.5
20
1,2-Dibromo-3-Chloropropane
mg/Kg
0.050
0.054
0.053
109
107
55-157
1.2
20
1,2-Dibromoethane
mg/Kg
0.050
0.050
0.050
102
100
70-132
1.7
20
Dibromomethane
mg/Kg
0.050
0.050
0.050
100
101
74-133
1.1
20
1,2-Dichlorobenzene
mg/Kg
0.050
0.051
0.050
103
101
72-123
2.1
20
1,3-Dichlorobenzene
mg/Kg
0.050
0.052
0.051
104
103
71-120
1.3
20
1,4-Dichlorobenzene
mg/Kg
0.050
0.052
0.051
104
103
71-123
1.1
20
Dichlorodifluoromethane
mg/Kg
0.050
0.054
0.053
110
106
26-146
3.3
20
Date: 06/30/2021 03:19 PM Page 7 of 19
Page 39 of 53

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-173-0038
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V5728 QC Analytical Batch(es): V5732
QC Prep Batch Method: 5035 LOW Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V5728 LCSD-V5728
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
1,1-Dichloroethane
mg/Kg
0.050
0.050
0.050
101
100
74-127
0.9
20
1,2-Dichloroethane
mg/Kg
0.050
0.049
0.049
98.4
98.6
68-128
0.2
20
1,1-Dichloroethene
mg/Kg
0.050
0.052
0.051
105
103
67-149
2.5
20
cis-1,2-Dichloroethene
mg/Kg
0.050
0.049
0.049
99.8
99.8
76-134
0.0
20
trans-1,2-Dichloroethene
mg/Kg
0.050
0.051
0.050
102
100
73-132
1.5
20
1,2-Dichloropropane
mg/Kg
0.050
0.050
0.049
100
98.4
73-130
1.6
20
1,3-Dichloropropane
mg/Kg
0.050
0.051
0.050
103
101
75-124
2.3
20
2,2-Dichloropropane
mg/Kg
0.050
0.053
0.052
107
106
50-142
1.6
20
1,1-Dichloropropene
mg/Kg
0.050
0.052
0.051
105
102
71-130
2.6
20
cis-1,3-Dichloropropene
mg/Kg
0.050
0.051
0.051
103
103
71-125
0.1
20
trans-1,3-Dichloropropene
mg/Kg
0.050
0.051
0.051
103
102
68-123
0.7
20
Ethylbenzene
mg/Kg
0.050
0.052
0.051
105
102
74-128
2.5
20
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
0.100
0.103
0.103
103
103
70-130
0.0
20
Hexachlorobutadiene
mg/Kg
0.050
0.055
0.053
110
107
64-125
2.9
20
n-Hexane
mg/Kg
0.050
0.054
0.052
109
106
70-130
3.3
20
2-Hexanone
mg/Kg
0.050
0.068
0.065
137
130
61-157
5.0
20
Isopropyl benzene
mg/Kg
0.050
0.053
0.052
107
104
68-126
2.2
20
4-Isopropyl toluene
mg/Kg
0.050
0.054
0.053
110
107
68-129
2.5
20
Methyl Ethyl Ketone (MEK)
mg/Kg
0.050
0.063
0.061
127
122
63-149
3.5
20
Methyl tert-butyl ether (MTBE)
mg/Kg
0.050
0.050
0.050
102
101
70-130
0.1
20
4-Methyl-2-Pentanone
mg/Kg
0.050
0.052
0.051
106
103
57-162
2.6
20
Methylene Chloride
mg/Kg
0.050
0.048
0.048
97.2
97.6
74-129
0.4
20
Naphthalene
mg/Kg
0.050
0.051
0.052
104
105
57-157
0.9
20
n-Propylbenzene
mg/Kg
0.050
0.053
0.052
108
106
67-130
2.0
20
Styrene
mg/Kg
0.050
0.052
0.051
105
103
77-121
2.1
20
1,1,1,2-Tetrachloroethane
mg/Kg
0.050
0.051
0.049
102
99.8
72-115
2.1
20
Date: 06/30/2021 03:19 PM Page 8 of 19
Page 40 of 53

Waypointo
ANALYTICAL
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-173-0038
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V5728 QC Analytical Batch(es): V5732
QC Prep Batch Method: 5035 LOW Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V5728 LCSD-V5728
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD Max
RPD
1,1,2,2-Tetrachloroethane
mg/Kg
0.050
0.051
0.050
103
101
56-126
1.7
Tetrachloroethene
mg/Kg
0.050
0.053
0.052
107
106
68-130
1.1
Toluene
mg/Kg
0.050
0.050
0.050
102
101
71-129
0.3
1,2,3-Trichlorobenzene
mg/Kg
0.050
0.051
0.052
104
106
68-130
1.7
1,2,4-Trichlorobenzene
mg/Kg
0.050
0.054
0.053
110
108
66-125
2.0
1,1,1-Trichloroethane
mg/Kg
0.050
0.051
0.050
103
102
67-131
1.5
1,1,2-Trichloroethane
mg/Kg
0.050
0.051
0.050
103
101
70-133
1.3
Trichloroethene
mg/Kg
0.050
0.052
0.051
104
102
75-133
1.9
Trichlorofluoromethane
mg/Kg
0.050
0.053
0.052
107
105
44-146
1.1
1,2,3-Trichloropropane
mg/Kg
0.050
0.052
0.049
105
99.6
60-137
5.0
1,3,5-Trimethylbenzene
mg/Kg
0.050
0.053
0.052
107
104
69-128
2.2
Vinyl Acetate
mg/Kg
0.050
0.060
0.059
120
119
85-161
0.6
Vinyl Chloride
mg/Kg
0.050
0.052
0.051
106
103
48-147
2.8
o-Xylene
mg/Kg
0.050
0.051
0.050
103
101
74-126
1.7
m,p-Xylene
mg/Kg
0.100
0.107
0.104
107
104
75-124
2.8
4-Bromofluorobenzene (S)
99.8
97.8
70-130
Dibromofluoromethane (S)
99.8
98.6
84-123
Toluene-d8(S)
101
99.2
76-129
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Date: 06/30/2021 03:19 PM Page 9 of 19
Page 41 of 53

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-173-0038
QC Prep: V5705
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V5743,V5763
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V5705 Matrix: SOL
Associated Lab Samples: 90168, 90169
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acenaphthene
mg/Kg
<0.116
0.116
0.660
06/23/21 17:42
Acenaphthylene
mg/Kg
<0.105
0.105
0.660
06/23/21 17:42
Aniline
mg/Kg
<0.152
0.152
0.660
06/23/21 17:42
Anthracene
mg/Kg
<0.143
0.143
0.660
06/23/21 17:42
Benzo(a)anthracene
mg/Kg
<0.139
0.139
0.660
06/23/21 17:42
Benzo(a)pyrene
mg/Kg
<0.147
0.147
0.660
06/23/21 17:42
Benzo(b)fluoranthene
mg/Kg
<0.146
0.146
0.660
06/23/21 17:42
Benzo(g,h,i)perylene
mg/Kg
<0.136
0.136
0.660
06/23/21 17:42
Benzo(k)fluoranthene
mg/Kg
<0.137
0.137
0.660
06/23/21 17:42
Benzoic Acid
mg/Kg
<0.580
0.580
2.00
06/23/21 17:42
Benzyl alcohol
mg/Kg
<0.105
0.105
0.660
06/23/21 17:42
Bis(2-Chloroethoxy)methane
mg/Kg
<0.118
0.118
0.660
06/23/21 17:42
Bis(2-Chloroethyl)ether
mg/Kg
<0.107
0.107
0.660
06/23/21 17:42
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.136
0.136
0.330
06/23/21 17:42
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.120
0.120
0.660
06/23/21 17:42
4-Bromophenyl phenyl ether
mg/Kg
<0.109
0.109
0.660
06/23/21 17:42
Butyl benzyl phthalate
mg/Kg
<0.113
0.113
0.330
06/23/21 17:42
4-Chloro-3-methylphenol
mg/Kg
<0.092
0.092
0.660
06/23/21 17:42
4-Chloroaniline
mg/Kg
<0.112
0.112
0.330
06/23/21 17:42
2-Chloronaphthalene
mg/Kg
<0.116
0.116
0.660
06/23/21 17:42
2-Chlorophenol
mg/Kg
<0.098
0.098
0.660
06/23/21 17:42
4-Chlorophenyl phenyl ether
mg/Kg
<0.126
0.126
1.00
06/23/21 17:42
Chrysene
mg/Kg
<0.142
0.142
0.660
06/23/21 17:42
Dibenz(a,h)anth racene
mg/Kg
<0.230
0.230
0.660
06/23/21 17:42
Dibenzofuran
mg/Kg
<0.119
0.119
0.660
06/23/21 17:42
1,2-Dichlorobenzene
mg/Kg
<0.094
0.094
0.660
06/23/21 17:42
1,3-Dichlorobenzene
mg/Kg
<0.097
0.097
0.660
06/23/21 17:42
Date:
06/30/2021 03:19 PM
Page 10 of 19
Page 42 of 53

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-173-0038
QC Prep: V5705
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V5743,V5763
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V5705 Matrix: SOL
Associated Lab Samples: 90168, 90169
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.097
0.097
0.330
06/23/21 17:42
3,3'-Dichlorobenzidine
mg/Kg
<0.147
0.147
0.660
06/23/21 17:42
2,4-Dichlorophenol
mg/Kg
<0.095
0.095
0.660
06/23/21 17:42
Diethyl phthalate
mg/Kg
<0.180
0.180
0.660
06/23/21 17:42
Dimethyl phthalate
mg/Kg
<0.174
0.174
0.660
06/23/21 17:42
2,4-Dimethylphenol
mg/Kg
<0.108
0.108
0.330
06/23/21 17:42
Di-n-butyl phthalate
mg/Kg
<0.107
0.107
0.660
06/23/21 17:42
4,6- Din itro-2-methylphenol
mg/Kg
<0.240
0.240
1.50
06/23/21 17:42
2,4-Dinitrophenol
mg/Kg
<0.520
0.520
1.50
06/23/21 17:42
2,4-Dinitrotoluene
mg/Kg
<0.096
0.096
0.660
06/23/21 17:42
2,6-Dinitrotoluene
mg/Kg
<0.108
0.108
0.660
06/23/21 17:42
Di-n-Octyl Phthalate
mg/Kg
<0.143
0.143
0.330
06/23/21 17:42
Fluoranthene
mg/Kg
<0.123
0.123
0.660
06/23/21 17:42
Fluorene
mg/Kg
<0.128
0.128
0.660
06/23/21 17:42
Hexachlorobenzene
mg/Kg
<0.106
0.106
0.660
06/23/21 17:42
Hexachlorobutadiene
mg/Kg
<0.097
0.097
0.660
06/23/21 17:42
Hexachlorocyclopentadiene
mg/Kg
<0.157
0.157
0.660
06/23/21 17:42
Hexachloroethane
mg/Kg
<0.079
0.079
0.660
06/23/21 17:42
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.179
0.179
0.660
06/23/21 17:42
Isophorone
mg/Kg
<0.191
0.191
0.660
06/23/21 17:42
1-Methylnaphthalene
mg/Kg
<0.106
0.106
0.660
06/23/21 17:42
2-Methylnaphthalene
mg/Kg
<0.100
0.100
0.660
06/23/21 17:42
2-Methylphenol
mg/Kg
<0.097
0.097
0.660
06/23/21 17:42
3&4 Methylphenol
mg/Kg
<0.084
0.084
0.660
06/23/21 17:42
Naphthalene
mg/Kg
<0.144
0.144
0.660
06/23/21 17:42
2-Nitroaniline
mg/Kg
<0.096
0.096
0.660
06/23/21 17:42
3-Nitroaniline
mg/Kg
<0.120
0.120
0.660
06/23/21 17:42
Date:
06/30/2021 03:19 PM
Page 11 of 19
Page 43 of 53

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
F&R, Inc. - Charlotte
Project Description:
RA Eden
Report No:
21-173-0038
QC Prep:
V5705
QC Analytical Batch(es): V5743,V5763
QC Prep Batch Method:
3546
Analysis Method:
8270E
Analysis Description:
Semivolatile Organic Compounds -
GC/MS
Lab Reagent Blank
LRB-V5705
Matrix: SOL
Associated Lab Samples:
90168, 90169
Blank
MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
4-Nitroaniline
mg/Kg
<0.093
0.093
0.330
06/23/21 17:42
Nitrobenzene
mg/Kg
<0.116
0.116
0.330
06/23/21 17:42
2-Nitrophenol
mg/Kg
<0.088
0.088
0.660
06/23/21 17:42
4-Nitrophenol
mg/Kg
<0.117
0.117
0.660
06/23/21 17:42
N-Nitrosodimethylamine
mg/Kg
<0.263
0.263
0.660
06/23/21 17:42
N-Nitrosodiphenylamine
mg/Kg
<0.181
0.181
0.660
06/23/21 17:42
N-Nitroso-di-n-propylamine
mg/Kg
<0.118
0.118
0.660
06/23/21 17:42
Pentachlorophenol
mg/Kg
<0.347
0.347
1.00
06/23/21 17:42
Phenanthrene
mg/Kg
<0.208
0.208
0.660
06/23/21 17:42
Phenol
mg/Kg
<0.112
0.112
0.660
06/23/21 17:42
Pyrene
mg/Kg
<0.134
0.134
0.660
06/23/21 17:42
Pyridine
mg/Kg
<0.079
0.079
0.330
06/23/21 17:42
1,2,4-Trichlorobenzene
mg/Kg
<0.107
0.107
0.660
06/23/21 17:42
2,4,5-Trichlorophenol
mg/Kg
<0.096
0.096
0.660
06/23/21 17:42
2,4,6-Trichlorophenol
mg/Kg
<0.096
0.096
0.660
06/23/21 17:42
2-Fluorobiphenyl (S)
06/23/21 17:42
101
44-115
2-Fluorophenol (S)
06/23/21 17:42
101
35-115
Nitrobenzene-d5 (S)
06/23/21 17:42
89.2
37-122
4-Terphenyl-d14 (S)
06/23/21 17:42
114
54-127
2,4,6-Tribromophenol (S)
06/23/21 17:42
106
39-132
Phenol-d5 (S)
06/23/21 17:42
98.4
34-121
Laboratory Control Sample
LCS-V5705
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Acenaphthene
mg/Kg
1.67
1.46
87.4
40-123
Acenaphthylene
mg/Kg
1.67
1.54
92.2
32-132
Date:
06/30/2021 03:19 PM
Page 12 of 19
Page 44 of 53

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-173-0038
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V5705 QC Analytical Batch(es): V5743,V5763
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V5705
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Aniline
mg/Kg
1.67
1.28
76.6
12-197
Anthracene
mg/Kg
1.67
1.53
91.6
47-123
Benzo(a)anthracene
mg/Kg
1.67
1.55
92.8
49-126
Benzo(a)pyrene
mg/Kg
1.67
1.58
94.6
45-129
Benzo(b)fluoranthene
mg/Kg
1.67
1.44
86.2
45-132
Benzo(g,h,i)perylene
mg/Kg
1.67
1.31
78.4
43-134
Benzo(k)fluoranthene
mg/Kg
1.67
1.36
81.4
47-132
Benzoic Acid
mg/Kg
1.67
1.72
0.0*
10-83
Benzyl alcohol
mg/Kg
1.67
1.38
82.6
29-122
Bis(2-Chloroethoxy)methane
mg/Kg
1.67
1.51
90.4
36-121
Bis(2-Chloroethyl)ether
mg/Kg
1.67
1.32
79.0
31-120
Bis(2-Chloroisopropyl)ether
mg/Kg
1.67
1.34
80.2
33-131
Bis(2-ethylhexyl)phthalate
mg/Kg
1.67
1.75
105
51-133
4-Bromophenyl phenyl ether
mg/Kg
1.67
1.46
87.4
46-124
Butyl benzyl phthalate
mg/Kg
1.67
1.68
101
48-132
4-Chloro-3-methyl phenol
mg/Kg
1.67
1.53
91.6
45-122
4-Chloroaniline
mg/Kg
1.67
1.27
76.0
17-106
2-Chloronaphthalene
mg/Kg
1.67
1.45
86.8
41-114
2-Chlorophenol
mg/Kg
1.67
1.45
86.8
34-121
4-Chlorophenyl phenyl ether
mg/Kg
1.67
1.49
89.2
45-121
Chrysene
mg/Kg
1.67
1.57
94.0
50-124
Dibenz(a,h)anthracene
mg/Kg
1.67
1.05
62.8
45-134
Dibenzofuran
mg/Kg
1.67
1.48
88.6
44-120
1,2-Dichlorobenzene
mg/Kg
1.67
1.29
77.2
33-117
1,3-Dichlorobenzene
mg/Kg
1.67
1.29
77.2
30-115
1,4-Dichlorobenzene
mg/Kg
1.67
1.27
76.0
31-115
3,3'-Dichlorobenzidine
mg/Kg
1.67
1.61
96.4
22-121
* QC Fail Date: 06/30/2021 03:19 PM Page 13 of 19
Page 45 of 53

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-173-0038
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V5705 QC Analytical Batch(es): V5743,V5763
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V5705
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
2,4-Dichlorophenol
mg/Kg
1.67
1.48
88.6
40-122
Diethyl phthalate
mg/Kg
1.67
1.52
91.0
50-124
Dimethyl phthalate
mg/Kg
1.67
1.48
88.6
48-124
2,4-Dimethylphenol
mg/Kg
1.67
1.56
93.4
30-127
Di-n-butyl phthalate
mg/Kg
1.67
1.71
102
51-128
4,6- Din itro-2-methylphenol
mg/Kg
1.67
1.37
0.0*
29-132
2,4-Dinitrophenol
mg/Kg
1.67
1.41
0.0*
27-129
2,4-Dinitrotoluene
mg/Kg
1.67
1.62
97.0
48-126
2,6-Dinitrotoluene
mg/Kg
1.67
1.57
94.0
46-124
Di-n-Octyl Phthalate
mg/Kg
1.67
1.52
91.0
45-140
Fluoranthene
mg/Kg
1.67
1.58
94.6
50-127
Fluorene
mg/Kg
1.67
1.52
91.0
43-125
Hexachlorobenzene
mg/Kg
1.67
1.49
89.2
45-122
Hexachlorobutadiene
mg/Kg
1.67
1.33
79.6
32-123
Hexachlorocyclopentadiene
mg/Kg
1.67
1.07
64.0
32-117
Hexachloroethane
mg/Kg
1.67
1.28
76.6
28-117
Indeno(1,2,3-cd)pyrene
mg/Kg
1.67
1.31
78.4
45-133
Isophorone
mg/Kg
1.67
1.34
80.2
30-122
1-Methylnaphthalene
mg/Kg
1.67
1.36
81.4
40-119
2-Methylnaphthalene
mg/Kg
1.67
1.34
80.2
38-122
2-Methylphenol
mg/Kg
1.67
1.50
89.8
32-122
3&4 Methylphenol
mg/Kg
1.67
1.27
76.0
34-119
Naphthalene
mg/Kg
1.67
1.35
80.8
35-123
2-Nitroaniline
mg/Kg
1.67
1.46
87.4
44-127
3-Nitroaniline
mg/Kg
1.67
1.45
86.8
33-119
4-Nitroaniline
mg/Kg
1.67
1.48
88.6
63-147
Nitrobenzene
mg/Kg
1.67
1.30
77.8
34-122
* QC Fail Date: 06/30/2021 03:19 PM Page 14 of 19
Page 46 of 53

Waypointo
ANALYTICAL
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-173-0038
QC Prep: V5705
QC Prep Batch Method: 3546
Laboratory Control Sample
Parameter
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-N itroso-d i-n-propyl a m i ne
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
4-Terphenyl-d14 (S)
2,4,6-Tribromophenol (S)
Phenol-d5 (S)
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
LCS-V5705
Spike
Units Conc.
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
QC Analytical Batch(es): V5743,V5763
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
LCS
Result
1.36
1.85
1.25
1.85
1.37
2.12
1.54
1.46
1.67
0.713
1.28
1.47
1.51
LCS %Rec
81.4
111
74.8
111
82.0
127
92.2
87.4
100
42.6
76.6
88.0
90.4
87.4
88.8
76.6
99.4
99.3
85.2
Rec
Limits
36-123
30-132
10-146
38-127
36-120
25-133
50-121
34-121
47-127
10-80
34-118
41-124
39-126
44-115
35-115
37-122
54-127
39-132
34-121
Matrix Spike & Matrix Spike Duplicate
V 90105-MS-V5705
V 90105-MSD-V5705
MS Spike
MSD
MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Acenaphthene
mg/Kg
<0.116
1.66
1.65
1.58
1.64
95.1
99.3
40-123
3.7
20
Acenaphthylene
mg/Kg
<0.105
1.66
1.65
1.63
1.70
98.1
103
32-132
4.2
20
Aniline
mg/Kg
<0.152
1.66
1.65
1.45
1.46
87.3
88.4
12-197
0.6
20
Date: 06/30/2021 03:19 PM Page 15 of 19
Page 47 of 53

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-173-0038
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V5705 QC Analytical Batch(es): V5743,V5763
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 90105-MS-V5705 V 90105-MSD-V5705
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Anthracene
mg/Kg
<0.143
1.66
1.65
1.70
1.69
102
102
47-123
0.5
20
Benzo(a)anthracene
mg/Kg
<0.139
1.66
1.65
1.71
1.71
103
104
49-126
0.0
20
Benzo(a)pyrene
mg/Kg
<0.147
1.66
1.65
1.73
1.71
104
104
45-129
1.1
20
Benzo(b)fluoranthene
mg/Kg
<0.146
1.66
1.65
1.55
1.52
93.3
92.1
45-132
1.9
20
Benzo(g,h,i)perylene
mg/Kg
<0.136
1.66
1.65
1.47
1.47
88.5
89.0
43-134
0.0
20
Benzo(k)fluoranthene
mg/Kg
<0.137
1.66
1.65
1.52
1.49
91.5
90.3
47-132
1.9
20
Benzoic Acid
mg/Kg
<0.580
1.66
1.65
<0.580
0.687
0.0*
0.0*
10-83
0.0
20
Benzyl alcohol
mg/Kg
<0.105
1.66
1.65
1.38
1.54
83.1
93.3
29-122
10.9
20
Bis(2-Chloroethoxy)methane
mg/Kg
<0.118
1.66
1.65
1.50
1.67
90.3
101
36-121
10.7
20
Bis(2-Chloroethyl)ether
mg/Kg
<0.107
1.66
1.65
1.10
1.47
66.2
89.0
31-120
28.7*
20
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.136
1.66
1.65
1.33
1.53
80.1
92.7
33-131
13.9
20
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.120
1.66
1.65
2.11
2.01
127
122
51-133
4.8
20
4-Bromophenyl phenyl ether
mg/Kg
<0.109
1.66
1.65
1.62
1.66
97.5
101
46-124
2.4
20
Butyl benzyl phthalate
mg/Kg
<0.113
1.66
1.65
1.97
1.89
119
115
48-132
4.1
20
4-Chloro-3-methyl phenol
mg/Kg
<0.092
1.66
1.65
1.60
1.67
96.3
101
45-122
4.2
20
4-Chloroaniline
mg/Kg
<0.112
1.66
1.65
1.34
1.41
80.7
85.4
17-106
5.0
20
2-Chloronaphthalene
mg/Kg
<0.116
1.66
1.65
1.52
1.62
91.5
98.1
41-114
6.3
20
2-Chlorophenol
mg/Kg
<0.098
1.66
1.65
1.43
1.60
86.1
96.9
34-121
11.2
20
4-Chlorophenyl phenyl ether
mg/Kg
<0.126
1.66
1.65
1.57
1.64
94.5
99.3
45-121
4.3
20
Chrysene
mg/Kg
<0.142
1.66
1.65
1.76
1.75
106
106
50-124
0.5
20
Dibenz(a,h)anth racene
mg/Kg
<0.230
1.66
1.65
1.22
1.19
73.4
72.1
45-134
2.4
20
Dibenzofuran
mg/Kg
<0.119
1.66
1.65
1.58
1.63
95.1
98.7
44-120
3.1
20
1,2-Dichlorobenzene
mg/Kg
<0.094
1.66
1.65
1.26
1.45
75.9
87.8
33-117
14.0
20
1,3-Dichlorobenzene
mg/Kg
<0.097
1.66
1.65
1.22
1.42
73.4
86.0
30-115
15.1
20
1,4-Dichlorobenzene
mg/Kg
<0.097
1.66
1.65
1.23
1.42
74.0
86.0
31-115
14.3
20
3,3'-Dichlorobenzidine
mg/Kg
<0.147
1.66
1.65
1.87
1.86
113
113
22-121
0.5
20
* QC Fail Date: 06/30/2021 03:19 PM Page 16 of 19
Page 48 of 53

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-173-0038
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V5705 QC Analytical Batch(es): V5743,V5763
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 90105-MS-V5705 V 90105-MSD-V5705
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
2,4-Dichlorophenol
mg/Kg
<0.095
1.66
1.65
1.53
1.66
92.1
101
40-122
8.1
20
Diethyl phthalate
mg/Kg
<0.180
1.66
1.65
1.65
1.68
99.3
102
50-124
1.8
20
Dimethyl phthalate
mg/Kg
<0.174
1.66
1.65
1.59
1.61
95.7
97.5
48-124
1.2
30
2,4-Dimethylphenol
mg/Kg
<0.108
1.66
1.65
1.62
1.76
97.5
107
30-127
8.2
20
Di-n-butyl phthalate
mg/Kg
<0.107
1.66
1.65
1.88
1.88
113
114
51-128
0.0
20
4,6- Din itro-2-methylphenol
mg/Kg
<0.240
1.66
1.65
1.58
1.54
95.1
93.3
29-132
2.5
20
2,4-Dinitrophenol
mg/Kg
<0.520
1.66
1.65
1.48
1.40
0.0*
0.0*
27-129
0.0
20
2,4-Dinitrotoluene
mg/Kg
<0.096
1.66
1.65
1.73
1.79
104
108
48-126
3.4
20
2,6-Dinitrotoluene
mg/Kg
<0.108
1.66
1.65
1.69
1.72
102
104
46-124
1.7
20
Di-n-Octyl Phthalate
mg/Kg
<0.143
1.66
1.65
1.66
1.65
100
100
45-140
0.6
20
Fluoranthene
mg/Kg
<0.123
1.66
1.65
1.68
1.68
101
102
50-127
0.0
20
Fluorene
mg/Kg
<0.128
1.66
1.65
1.65
1.68
99.3
102
43-125
1.8
20
Hexachlorobenzene
mg/Kg
<0.106
1.66
1.65
1.65
1.67
99.3
101
45-122
1.2
20
Hexachlorobutadiene
mg/Kg
<0.097
1.66
1.65
1.33
1.54
80.1
93.3
32-123
14.6
20
Hexachlorocyclopentadiene
mg/Kg
<0.157
1.66
1.65
1.10
1.07
66.2
64.8
32-117
2.7
20
Hexachloroethane
mg/Kg
<0.079
1.66
1.65
1.29
1.40
77.7
84.8
28-117
8.1
20
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.179
1.66
1.65
1.46
1.47
87.9
89.0
45-133
0.6
20
Isophorone
mg/Kg
<0.191
1.66
1.65
1.30
1.48
78.3
89.6
30-122
12.9
20
1-Methylnaphthalene
mg/Kg
<0.106
1.66
1.65
1.40
1.54
84.3
93.3
40-119
9.5
20
2-Methylnaphthalene
mg/Kg
<0.100
1.66
1.65
1.40
1.52
84.3
92.1
38-122
8.2
20
2-Methylphenol
mg/Kg
<0.097
1.66
1.65
1.53
1.67
92.1
101
32-122
8.7
20
3&4 Methylphenol
mg/Kg
<0.084
1.66
1.65
1.33
1.40
80.1
84.8
34-119
5.1
20
Naphthalene
mg/Kg
<0.144
1.66
1.65
1.34
1.49
80.7
90.3
35-123
10.6
20
2-Nitroaniline
mg/Kg
<0.096
1.66
1.65
1.60
1.64
96.3
99.3
44-127
2.4
20
3-Nitroaniline
mg/Kg
<0.120
1.66
1.65
1.58
1.63
95.1
98.7
33-119
3.1
20
4-Nitroaniline
mg/Kg
<0.093
1.66
1.65
1.69
1.63
102
98.7
63-147
3.6
20
* QC Fail Date: 06/30/2021 03:19 PM Page 17 of 19
Page 49 of 53

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-173-0038
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V5705 QC Analytical Batch(es): V5743,V5763
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 90105-MS-V5705 V 90105-MSD-V5705
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Nitrobenzene
mg/Kg
<0.116
1.66
1.65
1.28
1.44
77.1
87.2
34-122
11.7
20
2-Nitrophenol
mg/Kg
<0.088
1.66
1.65
1.29
1.54
77.7
93.3
32-123
17.6
20
4-Nitrophenol
mg/Kg
<0.117
1.66
1.65
2.02
2.08
122
126
30-132
2.9
20
N-Nitrosodimethylamine
mg/Kg
<0.263
1.66
1.65
1.11
1.28
66.8
77.5
10-146
14.2
30
N-Nitrosodiphenylamine
mg/Kg
<0.181
1.66
1.65
2.02
2.05
122
124
38-127
1.4
20
N-Nitroso-di-n-propylamine
mg/Kg
<0.118
1.66
1.65
1.31
1.51
78.9
91.5
36-120
14.1
20
Pentachlorophenol
mg/Kg
<0.347
1.66
1.65
2.32
2.29
140*
139*
25-133
1.3
20
Phenanthrene
mg/Kg
<0.208
1.66
1.65
1.71
1.69
103
102
50-121
1.1
20
Phenol
mg/Kg
<0.112
1.66
1.65
1.48
1.63
89.1
98.7
34-121
9.6
20
Pyrene
mg/Kg
<0.134
1.66
1.65
1.87
1.87
113
113
47-127
0.0
20
Pyridine
mg/Kg
<0.079
1.66
1.65
0.798
0.990
48.0
60.0
10-80
21.4*
20
1,2,4-Trichlorobenzene
mg/Kg
<0.107
1.66
1.65
1.32
1.47
79.5
89.0
34-118
10.7
20
2,4,5-Trichlorophenol
mg/Kg
<0.096
1.66
1.65
1.68
1.69
101
102
41-124
0.5
20
2,4,6-Trichlorophenol
mg/Kg
<0.096
1.66
1.65
1.64
1.68
98.7
102
39-126
2.4
20
* QC Fail Date: 06/30/2021 03:19 PM Page 18 of 19
Page 50 of 53

Waypointo
ANALYTICAL
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-173-0038
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch: V5660
Analysis Method: SW-DRYWT
Analysis Description: Dry Weight Determination
Duplicate V 90168-DUP
Result DUP
Parameter Units Result
Moisture % 17.5 19.5
Duplicate V 89859-DUP
RPD Max RPD Analyzed
10.8 20.0 06/22/2115:37
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Moisture % 18.0 19.1 5.9 20.0 06/22/2115:37
Date: 06/30/2021 03:19 PM Page 19 of 19
Page 51 of 53

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 00019
Customer Name: F&R, Inc. - Charlotte
Report Number: 21-173-0038
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS ® Client 0 Courier
0 Other:
Thermometer ID:
IRT-15 3.1C
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
I* Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
I* Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample Iabel(s)?
0 Yes
0 No
COC properly completed
® Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
® Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
• Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) I✓ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Talon J Yelton Date & Time: 06/22/2021 15:02:02
Page 52 of 53

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Page 53 of 53

Waypointo
ANALYTICAL
8/18/2021
F&R, Inc. - Charlotte
Brian Olin
3300 International Airport Dr., Suite 600
Charlotte, NC, 28208
Ref: Analytical Testing
Lab Report Number: 21-222-0026
Client Project Description: RA Eden
Dear Brian Olin:
449 5pringbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 8/10/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
a'-1
Angela D Overcash
Senior Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 81

Waypoint.0
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2022
North Carolina
State Program
402
12/31/2021
South Carolina
State Program
99012
07/31/2022
South Carolina
State Program
99012
12/31/2021
Page 1 of 1 00016/21-222-0026
Page 2 of 81

Waypoint. (2) 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointana lyti ca I som
Sample Summary Table
Report Number: 21-222-0026
Client Project Description: RA Eden
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
93306
Comp-1
Solids
08/10/202111:25
08/10/202115:10
7199
93306
Comp-1
Solids
08/10/202111:25
08/10/202115:10
93307
Comp-2
Solids
08/10/202111:35
08/10/202115:10
7199
93307
Comp-2
Solids
08/10/202111:35
08/10/202115:10
93308
Comp-3
Solids
08/10/202111:45
08/10/202115:10
7199
93308
Comp-3
Solids
08/10/202111:45
08/10/202115:10
93309
Comp-4
Solids
08/10/202112:00
08/10/202115:10
7199
93309
Comp-4
Solids
08/10/202112:00
08/10/202115:10
Pace Analytical - Columbia, SC (Shealy), West Columbia, SC
Page 3 of 81

Waypoint (D 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
AN LYT I CAL www.waypointanalytica Isom
Summary of Detected Analytes
Project: RA Eden
Report Number: 21-222-0026
Client Sample ID Lab Sample ID
Method Parameters
Result Units Report Limit Analyzed
Comp-1
V 93306
6020B
Arsenic
7.69
mg/Kg - dry
0.107
08/12/2021 13:31
6020E
Barium
52.6
mg/Kg - dry
1.60
08/12/2021 13:31
6020E
Chromium
42.2
mg/Kg - dry
0.330
08/12/2021 13:31
6020E
Lead
32.3
mg/Kg - dry
0.160
08/12/2021 13:31
6020B
Selenium
1.64
mg/Kg - dry
1.03
08/12/2021 13:31
7471 B
Mercury (Total)
0.0450
mg/Kg - dry
0.0137
08/12/2021 15:33
8260D
Acetone
0.026
mg/Kg - dry
0.002
08/11/2021 12:08
8260D
n-Hexane
0.001
mg/Kg - dry
0.0008
08/11/2021 12:08
8260D
Methyl Ethyl Ketone (MEK)
0.001
mg/Kg - dry
0.0007
08/11/2021 12:08
8270E
Acenaphthylene
0.204
mg/Kg - dry
0.119
08/13/2021 16:56
SW-DRYWT
Moisture
12.3
%
08/12/202117:20
Comp-2
V 93307
6020E
Arsenic
7.29
mg/Kg - dry
0.106
08/12/2021 14:09
6020E
Barium
90.0
mg/Kg - dry
1.57
08/12/2021 14:09
6020E
Cadmium
0.101
mg/Kg - dry
0.0617
08/12/2021 14:09
6020E
Chromium
43.6
mg/Kg - dry
0.325
08/12/2021 14:09
6020E
Lead
40.7
mg/Kg - dry
0.157
08/12/2021 14:09
6020E
Selenium
1.97
mg/Kg - dry
1.01
08/12/2021 14:09
7471 B
Mercury (Total)
0.0672
mg/Kg - dry
0.0135
08/12/2021 15:35
8260D
Acetone
0.043
mg/Kg - dry
0.002
08/11/2021 12:38
8260D
n-Hexane
0.001
mg/Kg - dry
0.0007
08/11/2021 12:38
8260D
Methyl Ethyl Ketone (MEK)
0.003
mg/Kg - dry
0.0007
08/11/2021 12:38
8270E
Acenaphthylene
0.158
mg/Kg - dry
0.117
08/17/2021 22:04
8270E
Benzo(b)fluoranthene
0.171
mg/Kg - dry
0.164
08/17/2021 22:04
8270E
Fluoranthene
0.166
mg/Kg - dry
0.138
08/17/2021 22:04
8270E
Pyrene
0.198
mg/Kg - dry
0.150
08/17/2021 22:04
SW-DRYWT
Moisture
11.0
%
08/12/202117:20
Comp-3
V 93308
6020B
Arsenic
7.46
mg/Kg - dry
0.104
08/12/2021 14:16
6020B
Barium
89.2
mg/Kg - dry
1.55
08/12/2021 14:16
6020E
Cadmium
0.0788
mg/Kg - dry
0.0607
08/12/2021 14:16
6020B
Chromium
47.8
mg/Kg - dry
0.320
08/12/2021 14:16
6020E
Lead
35.1
mg/Kg - dry
0.155
08/12/2021 14:16
6020B
Selenium
2.16
mg/Kg - dry
0.994
08/12/2021 14:16
7471 B
Mercury (Total)
0.0617
mg/Kg - dry
0.0133
08/12/2021 15:38
8260D
Acetone
0.035
mg/Kg - dry
0.002
08/11/2021 13:07
Page 4 of 81
Qualifiers
0
I
0
0
J
J
J
J
J
J
0
0

(D
Waypoint
449 Springbrook Rd, Charlotte, NC
28217
Main 704.529.6364
ANALYTICAL
www.waypointanalytica l.com
Summary of Detected Analytes
Project:
RA Eden
Report Number:
21-222-0026
Client Sample ID
Lab Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
Comp-3
V 93308
8260D
n-Hexane
0.001
mg/Kg - dry
0.0007
08/11/2021 13:07
J
8260D
Methyl Ethyl Ketone (MEK)
0.002
mg/Kg - dry
0.0007
08/11/2021 13:07
J
8270E
Acenaphthylene
0.214
mg/Kg - dry
0.116
08/13/2021 15:46
J
8270E
Anthracene
0.174
mg/Kg - dry
0.158
08/13/2021 15:46
J
SW-DRYWT
Moisture
9.53
%
08/12/202117:20
Comp-4
V 93309
6020B
Arsenic
8.99
mg/Kg - dry
0.0984
08/12/2021 14:35
6020E
Barium
80.5
mg/Kg - dry
1.47
08/12/2021 14:35
6020B
Cadmium
0.0738
mg/Kg - dry
0.0575
08/12/2021 14:35
J
6020E
Chromium
46.1
mg/Kg - dry
0.303
08/12/2021 14:35
6020B
Lead
34.0
mg/Kg - dry
0.147
08/12/2021 14:35
6020B
Selenium
1.70
mg/Kg - dry
0.942
08/12/2021 14:35
J
6020B
Silver
0.0646
mg/Kg - dry
0.0429
08/12/2021 14:35
J
7471 B
Mercury (Total)
0.0617
mg/Kg - dry
0.0126
08/12/2021 15:40
8260D
Acetone
0.004
mg/Kg - dry
0.002
08/11/2021 13:37
J
8270E
Acenaphthylene
0.238
mg/Kg - dry
0.109
08/13/2021 16:09
J
8270E
Anthracene
0.194
mg/Kg - dry
0.149
08/13/2021 16:09
J
8270E
Bis(2-ethyl hexyl)phthalate
0.713
mg/Kg - dry
0.125
08/13/2021 16:09
8270E
Fluoranthene
0.199
mg/Kg - dry
0.128
08/13/2021 16:09
J
8270E
Pyrene
0.365
mg/Kg - dry
0.140
08/13/2021 16:09
J
SW-DRYWT
Moisture
4.48
%
08/12/202117:20
Page 5 of 81

WavDdibnto
ANALYTICAL
00019
F&R, Inc. - Charlotte
Brian Olin
3300 International Airport Dr., Suite 600
Charlotte , NC 28208
Project RA Eden
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Report Date : 08/18/2021
Received : 08/10/2021
Lab No : 93306
Sample ID: Comp-1
Matrix: Solids
Sampled: 8/10/2021 11:25
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
12.3
%
1
08/12/2117:20
EDV
SW-DRYWT
Arsenic
7.69
mg/Kg - dry
0.107
1.14
10
08/12/21 13:31
EDV
6020B
Barium
52.6
mg/Kg - dry
1.60
11.4
10
08/12/21 13:31
EDV
6020E
Cadmium
<0.0627
mg/Kg - dry
0.0627
0.570
10
08/12/21 13:31
EDV
6020B
Chromium
42.2
mg/Kg - dry
0.330
1.14
10
08/12/21 13:31
EDV
6020E
Lead
32.3
mg/Kg - dry
0.160
1.14
10
08/12/21 13:31
EDV
6020B
Mercury (Total)
0.0450
mg/Kg - dry
0.0137
0.0342
1
08/12/21 15:33
EDV
7471E
Selenium
1.643
mg/Kg - dry
1.03
2.28
10
08/12/21 13:31
EDV
6020B
Silver
<0.0467
mg/Kg - dry
0.0467
0.570
10
08/12/21 13:31
EDV
6020E
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 6 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93306
Matrix: Solids
Sample ID: Comp-1
Sampled:
8/10/2021 11:25
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
0.026
mg/Kg - dry
0.002
0.022
1
08/11/21 12:08
TBL
V7515
Acrolein
<0.001
mg/Kg - dry
0.001
0.022
1
08/11/21 12:08
TBL
V7515
Acrylonitrile
<0.0009
mg/Kg - dry
0.0009
0.022
1
08/11/21 12:08
TBL
V7515
Benzene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:08
TBL
V7515
Bromobenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
Bromochloromethane
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 12:08
TBL
V7515
Bromodichloromethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
Bromoform
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
Bromomethane
<0.002
mg/Kg - dry
0.002
0.011
1
08/11/21 12:08
TBL
V7515
n-Butylbenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
sec -Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
tert-Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
Carbon Disulfide
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:08
TBL
V7515
Carbon Tetrachloride
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
Chlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 12:08
TBL
V7515
Chlorodibromomethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
Chloroethane
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 12:08
TBL
V7515
Chloroform
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
Chloromethane
<0.0007
mg/Kg - dry
0.0007
0.011
1
08/11/21 12:08
TBL
V7515
2-Chlorotoluene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
4-Chlorotoluene
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 12:08
TBL
V7515
Di -Isopropyl Ether (DIPE)
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 12:08
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 7 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93306
Matrix: Solids
Sample ID: Comp-1
Sampled:
8/10/2021 11:25
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.0005
mg/Kg - dry
0.0005
0.011
1
08/11/21 12:08
TBL
V7515
1,2-Dibromoethane
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:08
TBL
V7515
Dibromomethane
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
1,2-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 12:08
TBL
V7515
1,3-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 12:08
TBL
V7515
1,4-Dichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:08
TBL
V7515
Dichlorodifluoromethane
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 12:08
TBL
V7515
1,1-Dichloroethane
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 12:08
TBL
V7515
1,2-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
1,1-Dichloroethene
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 12:08
TBL
V7515
cis- 1,2-Dich loroethene
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 12:08
TBL
V7515
trans-1,2-Dichloroethene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
1,2-Dichloropropane
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 12:08
TBL
V7515
1,3-Dichloropropane
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
2,2-Dichloropropane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
1,1-Dichloropropene
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 12:08
TBL
V7515
cis- 1,3-Dich loropropene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
trans-1,3-Dichloropropene
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 12:08
TBL
V7515
Ethylbenzene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:08
TBL
V7515
Ethyl Tertiary Butyl Ether (ETBE)
<0.0009
mg/Kg - dry
0.0009
0.057
1
08/11/21 12:08
TBL
V7515
Hexachlorobutadiene
<0.0009
mg/Kg - dry
0.0009
0.011
1
08/11/21 12:08
TBL
V7515
n-Hexane
0.0013
mg/Kg - dry
0.0008
0.011
1
08/11/21 12:08
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 8 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93306
Matrix: Solids
Sample ID: Comp-1
Sampled:
8/10/2021 11:25
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Hexanone
<0.0007
mg/Kg - dry
0.0007
0.022
1
08/11/21 12:08
TBL
V7515
Isopropyl benzene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 12:08
TBL
V7515
4-Isopropyl toluene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
Methyl Ethyl Ketone (MEK)
0.0013
mg/Kg - dry
0.0007
0.022
1
08/11/21 12:08
TBL
V7515
Methyl tert-butyl ether (MTBE)
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:08
TBL
V7515
4-Methyl-2-Pentanone
<0.017
mg/Kg - dry
0.017
0.022
1
08/11/21 12:08
TBL
V7515
Methylene Chloride
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 12:08
TBL
V7515
Naphthalene
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 12:08
TBL
V7515
n-Propylbenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
Styrene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
1,1,1,2-Tetrachloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
1,1,2,2-Tetrachloroethane
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 12:08
TBL
V7515
Tetrachloroethene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
Toluene
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 12:08
TBL
V7515
1,2,3-Trichlorobenzene
<0.0006
mg/Kg - dry
0.0006
0.011
1
08/11/21 12:08
TBL
V7515
1,2,4-Trichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.011
1
08/11/21 12:08
TBL
V7515
1,1,1-Trichloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
1,1,2-Trichloroethane
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 12:08
TBL
V7515
Trichloroethene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:08
TBL
V7515
Trichlorofluoromethane
<0.002
mg/Kg - dry
0.002
0.011
1
08/11/21 12:08
TBL
V7515
1,2,3-Trichloropropane
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 12:08
TBL
V7515
1,2,4-Trimethyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 9 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93306 Matrix: Solids
Sample ID: Comp-1 Sampled: 8/10/2021 11:25
Analytical Method: 8260D Prep Batch(es): V7514 08/11/21 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,3,5-Trimethyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
Vinyl Acetate
<0.0005
mg/Kg - dry
0.0005
0.011
1
08/11/21 12:08
TBL
V7515
Vinyl Chloride
<0.0005
mg/Kg - dry
0.0005
0.011
1
08/11/21 12:08
TBL
V7515
o-Xylene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
TBL
V7515
m,p-Xylene
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 12:08
TBL
V7515
Xylene (Total)
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:08
V7515
Surrogate:4-Bromofluorobenzene
101
Limits:70-130%
1 08/11/21 12:08 TBL
V7515
Surrogate: Dibromofluoromethane
99.4
Limits: 84-123%
1 08/11/21 12:08 TBL
V7515
Surrogate: Toluene-d8
95.5
Limits: 76-129%
1 08/11/21 12:08 TBL
V7515
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21
12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.132
mg/Kg - dry
0.132
0.752
1
08/13/21 16:56
JMV
V7647
Acenaphthylene
0.2043
mg/Kg - dry
0.119
0.752
1
08/13/21 16:56
JMV
V7647
Aniline
<0.173
mg/Kg - dry
0.173
0.752
1
08/13/21 16:56
JMV
V7647
Anthracene
<0.163
mg/Kg - dry
0.163
0.752
1
08/13/21 16:56
JMV
V7647
Benzo(a)anthracene
<0.158
mg/Kg - dry
0.158
0.752
1
08/13/21 16:56
JMV
V7647
Benzo(a)pyrene
<0.167
mg/Kg - dry
0.167
0.752
1
08/13/21 16:56
JMV
V7647
Benzo(b)fluoranthene
<0.166
mg/Kg - dry
0.166
0.752
1
08/13/21 16:56
JMV
V7647
Benzo(g,h,i)perylene
<0.155
mg/Kg - dry
0.155
0.752
1
08/13/21 16:56
JMV
V7647
Benzo(k)fluoranthene
<0.156
mg/Kg - dry
0.156
0.752
1
08/13/21 16:56
JMV
V7647
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 10 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93306
Matrix: Solids
Sample ID: Comp-1
Sampled:
8/10/2021 11:25
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21 12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzoic Acid
<0.661
mg/Kg - dry
0.661
2.28
1
08/13/21 16:56
JMV
V7647
Benzyl alcohol
<0.119
mg/Kg - dry
0.119
0.752
1
08/13/21 16:56
JMV
V7647
Bis(2-Chloroethoxy)methane
<0.134
mg/Kg - dry
0.134
0.752
1
08/13/21 16:56
JMV
V7647
Bis(2-Chloroethyl)ether
<0.122
mg/Kg - dry
0.122
0.752
1
08/13/21 16:56
JMV
V7647
Bis(2-Chloroisopropyl)ether
<0.155
mg/Kg - dry
0.155
0.376
1
08/13/21 16:56
JMV
V7647
Bis(2-ethylhexyl)phthalate
<0.136
mg/Kg - dry
0.136
0.752
1
08/13/21 16:56
JMV
V7647
4-Bromophenyl phenyl ether
<0.124
mg/Kg - dry
0.124
0.752
1
08/13/21 16:56
JMV
V7647
Butyl benzyl phthalate
<0.128
mg/Kg - dry
0.128
0.376
1
08/13/21 16:56
JMV
V7647
4-Chloro-3-methyl phenol
<0.105
mg/Kg - dry
0.105
0.752
1
08/13/21 16:56
JMV
V7647
4-Chloroaniline
<0.127
mg/Kg - dry
0.127
0.376
1
08/13/21 16:56
JMV
V7647
2-Chloronaphthalene
<0.132
mg/Kg - dry
0.132
0.752
1
08/13/21 16:56
JMV
V7647
2-Chlorophenol
<0.111
mg/Kg - dry
0.111
0.752
1
08/13/21 16:56
JMV
V7647
4-Chlorophenyl phenyl ether
<0.143
mg/Kg - dry
0.143
1.14
1
08/13/21 16:56
JMV
V7647
Chrysene
<0.161
mg/Kg - dry
0.161
0.752
1
08/13/21 16:56
JMV
V7647
Dibenz(a,h)anthracene
<0.262
mg/Kg - dry
0.262
0.752
1
08/13/21 16:56
JMV
V7647
Dibenzofuran
<0.135
mg/Kg - dry
0.135
0.752
1
08/13/21 16:56
JMV
V7647
1,2-Dichlorobenzene
<0.107
mg/Kg - dry
0.107
0.752
1
08/13/21 16:56
JMV
V7647
1,3-Dichlorobenzene
<0.110
mg/Kg - dry
0.110
0.752
1
08/13/21 16:56
JMV
V7647
1,4-Dichlorobenzene
<0.111
mg/Kg - dry
0.111
0.376
1
08/13/21 16:56
JMV
V7647
3,3'-Dichlorobenzidine
<0.167
mg/Kg - dry
0.167
0.752
1
08/13/21 16:56
JMV
V7647
2,4-Dichlorophenol
<0.109
mg/Kg - dry
0.109
0.752
1
08/13/21 16:56
JMV
V7647
Diethyl phthalate
<0.205
mg/Kg - dry
0.205
0.752
1
08/13/21 16:56
JMV
V7647
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 11 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93306
Matrix: Solids
Sample ID: Comp-1
Sampled:
8/10/2021 11:25
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21 12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Dimethyl phthalate
<0.198
mg/Kg - dry
0.198
0.752
1
08/13/21 16:56
JMV
V7647
2,4-Dimethylphenol
<0.123
mg/Kg - dry
0.123
0.376
1
08/13/21 16:56
JMV
V7647
Di-n-butyl phthalate
<0.122
mg/Kg - dry
0.122
0.752
1
08/13/21 16:56
JMV
V7647
4,6- Din itro-2-methylphenol
<0.273
mg/Kg - dry
0.273
1.71
1
08/13/21 16:56
JMV
V7647
2,4-Dinitrophenol
<0.592
mg/Kg - dry
0.592
1.71
1
08/13/21 16:56
JMV
V7647
2,4-Dinitrotoluene
<0.110
mg/Kg - dry
0.110
0.752
1
08/13/21 16:56
JMV
V7647
2,6-Dinitrotoluene
<0.123
mg/Kg - dry
0.123
0.752
1
08/13/21 16:56
JMV
V7647
Di-n-Octyl Phthalate
<0.163
mg/Kg - dry
0.163
0.376
1
08/13/21 16:56
JMV
V7647
Fluoranthene
<0.140
mg/Kg - dry
0.140
0.752
1
08/13/21 16:56
JMV
V7647
Fluorene
<0.145
mg/Kg - dry
0.145
0.752
1
08/13/21 16:56
JMV
V7647
Hexachlorobenzene
<0.120
mg/Kg - dry
0.120
0.752
1
08/13/21 16:56
JMV
V7647
Hexachlorobutadiene
<0.111
mg/Kg - dry
0.111
0.752
1
08/13/21 16:56
JMV
V7647
Hexachlorocyclopentadiene
<0.179
mg/Kg - dry
0.179
0.752
1
08/13/21 16:56
JMV
V7647
Hexachloroethane
<0.090
mg/Kg - dry
0.090
0.752
1
08/13/21 16:56
JMV
V7647
Indeno(1,2,3-cd)pyrene
<0.204
mg/Kg - dry
0.204
0.752
1
08/13/21 16:56
JMV
V7647
Isophorone
<0.217
mg/Kg - dry
0.217
0.752
1
08/13/21 16:56
JMV
V7647
1-Methylnaphthalene
<0.120
mg/Kg - dry
0.120
0.752
1
08/13/21 16:56
JMV
V7647
2-Methylnaphthalene
<0.114
mg/Kg - dry
0.114
0.752
1
08/13/21 16:56
JMV
V7647
2-Methylphenol
<0.110
mg/Kg - dry
0.110
0.752
1
08/13/21 16:56
JMV
V7647
3&4 Methylphenol
<0.096
mg/Kg - dry
0.096
0.752
1
08/13/21 16:56
JMV
V7647
Naphthalene
<0.164
mg/Kg - dry
0.164
0.752
1
08/13/21 16:56
JMV
V7647
2-Nitroaniline
<0.110
mg/Kg - dry
0.110
0.752
1
08/13/21 16:56
JMV
V7647
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 12 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93306
Matrix: Solids
Sample ID: Comp-1
Sampled: 8/10/2021
11:25
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21 12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
3-Nitroaniline
<0.136
mg/Kg - dry
0.136
0.752
1
08/13/21 16:56 JMV
V7647
4-Nitroaniline
<0.106
mg/Kg - dry
0.106
0.376
1
08/13/21 16:56 JMV
V7647
Nitrobenzene
<0.132
mg/Kg - dry
0.132
0.376
1
08/13/21 16:56 JMV
V7647
2-Nitrophenol
<0.101
mg/Kg - dry
0.101
0.752
1
08/13/21 16:56 JMV
V7647
4-Nitrophenol
<0.133
mg/Kg - dry
0.133
0.752
1
08/13/21 16:56 JMV
V7647
N-N itrosodimethyla mine
<0.299
mg/Kg - dry
0.299
0.752
1
08/13/21 16:56 JMV
V7647
N-Nitrosodiphenylamine
<0.206
mg/Kg - dry
0.206
0.752
1
08/13/21 16:56 JMV
V7647
N-Nitroso-di-n-propylamine
<0.134
mg/Kg - dry
0.134
0.752
1
08/13/21 16:56 JMV
V7647
Pentachlorophenol
<0.395
mg/Kg - dry
0.395
1.14
1
08/13/21 16:56 JMV
V7647
Phenanthrene
<0.237
mg/Kg - dry
0.237
0.752
1
08/13/21 16:56 JMV
V7647
Phenol
<0.127
mg/Kg - dry
0.127
0.752
1
08/13/21 16:56 JMV
V7647
Pyrene
<0.152
mg/Kg - dry
0.152
0.752
1
08/13/21 16:56 JMV
V7647
Pyridine
<0.090
mg/Kg - dry
0.090
0.376
1
08/13/21 16:56 JMV
V7647
1,2,4-Trichlorobenzene
<0.122
mg/Kg - dry
0.122
0.752
1
08/13/21 16:56 JMV
V7647
2,4,5-Trichlorophenol
<0.109
mg/Kg - dry
0.109
0.752
1
08/13/21 16:56 JMV
V7647
2,4,6-Trichlorophenol
<0.110
mg/Kg - dry
0.110
0.752
1
08/13/21 16:56 JMV
V7647
Surrogate: Phenol-d5
63.3
Limits: 34-121%
1 08/13/21 16:56 JMV
V7647
Surrogate:2-Fluorobiphenyl
74.5
Limits:44-115%
1 08/13/21 16:56 JMV
V7647
Surrogate:2-Fluorophenol
63.6
Limits:35-115%
1 08/13/21 16:56 JMV
V7647
Surrogate: Nitrobenzene-d5
68.5
Limits: 37-122%
1 08/13/21 16:56 JMV
V7647
Surrogate:4-Terphenyl-d14
76.4
Limits:54-127%
1 08/13/21 16:56 JMV
V7647
Surrogate: 2,4,6-Tribromophenol
65.2
Limits:39-132%
1 08/13/21 16:56 JMV
V7647
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 13 of 81

WavDdibnto
ANALYTICAL
00019
F&R, Inc. - Charlotte
Brian Olin
3300 International Airport Dr., Suite 600
Charlotte , NC 28208
Project RA Eden
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Report Date : 08/18/2021
Received : 08/10/2021
Lab No : 93307
Sample ID: Comp-2
Matrix: Solids
Sampled: 8/10/2021 11:35
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
11.0
%
1
08/12/2117:20
EDV
SW-DRYWT
Arsenic
7.29
mg/Kg - dry
0.106
1.12
10
08/12/21 14:09
EDV
6020B
Barium
90.0
mg/Kg - dry
1.57
11.2
10
08/12/21 14:09
EDV
6020E
Cadmium
0.101 J
mg/Kg - dry
0.0617
0.562
10
08/12/21 14:09
EDV
6020B
Chromium
43.6
mg/Kg - dry
0.325
1.12
10
08/12/21 14:09
EDV
6020E
Lead
40.7
mg/Kg - dry
0.157
1.12
10
08/12/21 14:09
EDV
6020B
Mercury (Total)
0.0672
mg/Kg - dry
0.0135
0.0337
1
08/12/21 15:35
EDV
7471E
Selenium
1.973
mg/Kg - dry
1.01
2.25
10
08/12/21 14:09
EDV
6020B
Silver
<0.0460
mg/Kg - dry
0.0460
0.562
10
08/12/21 14:09
EDV
6020E
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 14 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93307
Matrix: Solids
Sample ID: Comp-2
Sampled:
8/10/2021 11:35
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
0.043
mg/Kg - dry
0.002
0.022
1
08/11/21 12:38
TBL
V7515
Acrolein
<0.001
mg/Kg - dry
0.001
0.022
1
08/11/21 12:38
TBL
V7515
Acrylonitrile
<0.0008
mg/Kg - dry
0.0008
0.022
1
08/11/21 12:38
TBL
V7515
Benzene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:38
TBL
V7515
Bromobenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
Bromochloromethane
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 12:38
TBL
V7515
Bromodichloromethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
Bromoform
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
Bromomethane
<0.002
mg/Kg - dry
0.002
0.011
1
08/11/21 12:38
TBL
V7515
n-Butylbenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
sec -Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
tert-Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
Carbon Disulfide
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:38
TBL
V7515
Carbon Tetrachloride
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
Chlorobenzene
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 12:38
TBL
V7515
Chlorodibromomethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
Chloroethane
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 12:38
TBL
V7515
Chloroform
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
Chloromethane
<0.0007
mg/Kg - dry
0.0007
0.011
1
08/11/21 12:38
TBL
V7515
2-Chlorotoluene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
4-Chlorotoluene
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 12:38
TBL
V7515
Di -Isopropyl Ether (DIPE)
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 12:38
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 15 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93307
Matrix: Solids
Sample ID: Comp-2
Sampled:
8/10/2021 11:35
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.0005
mg/Kg - dry
0.0005
0.011
1
08/11/21 12:38
TBL
V7515
1,2-Dibromoethane
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:38
TBL
V7515
Dibromomethane
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
1,2-Dichlorobenzene
<0.0003
mg/Kg - dry
0.0003
0.005
1
08/11/21 12:38
TBL
V7515
1,3-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 12:38
TBL
V7515
1,4-Dichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:38
TBL
V7515
Dichlorodifluoromethane
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 12:38
TBL
V7515
1,1-Dichloroethane
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 12:38
TBL
V7515
1,2-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
1,1-Dichloroethene
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 12:38
TBL
V7515
cis- 1,2-Dich loroethene
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 12:38
TBL
V7515
trans-1,2-Dichloroethene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
1,2-Dichloropropane
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 12:38
TBL
V7515
1,3-Dichloropropane
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
2,2-Dichloropropane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
1,1-Dichloropropene
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 12:38
TBL
V7515
cis- 1,3-Dich loropropene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
trans-1,3-Dichloropropene
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 12:38
TBL
V7515
Ethylbenzene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:38
TBL
V7515
Ethyl Tertiary Butyl Ether (ETBE)
<0.0009
mg/Kg - dry
0.0009
0.056
1
08/11/21 12:38
TBL
V7515
Hexachlorobutadiene
<0.0009
mg/Kg - dry
0.0009
0.011
1
08/11/21 12:38
TBL
V7515
n-Hexane
0.0013
mg/Kg - dry
0.0007
0.011
1
08/11/21 12:38
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 16 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93307
Matrix: Solids
Sample ID: Comp-2
Sampled:
8/10/2021 11:35
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Hexanone
<0.0007
mg/Kg - dry
0.0007
0.022
1
08/11/21 12:38
TBL
V7515
Isopropyl benzene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 12:38
TBL
V7515
4-Isopropyl toluene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
Methyl Ethyl Ketone (MEK)
0.0033
mg/Kg - dry
0.0007
0.022
1
08/11/21 12:38
TBL
V7515
Methyl tert-butyl ether (MTBE)
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:38
TBL
V7515
4-Methyl-2-Pentanone
<0.016
mg/Kg - dry
0.016
0.022
1
08/11/21 12:38
TBL
V7515
Methylene Chloride
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 12:38
TBL
V7515
Naphthalene
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 12:38
TBL
V7515
n-Propylbenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
Styrene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
1,1,1,2-Tetrachloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
1,1,2,2-Tetrachloroethane
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 12:38
TBL
V7515
Tetrachloroethene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
Toluene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 12:38
TBL
V7515
1,2,3-Trichlorobenzene
<0.0006
mg/Kg - dry
0.0006
0.011
1
08/11/21 12:38
TBL
V7515
1,2,4-Trichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.011
1
08/11/21 12:38
TBL
V7515
1,1,1-Trichloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
1,1,2-Trichloroethane
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 12:38
TBL
V7515
Trichloroethene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 12:38
TBL
V7515
Trichlorofluoromethane
<0.002
mg/Kg - dry
0.002
0.011
1
08/11/21 12:38
TBL
V7515
1,2,3-Trichloropropane
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 12:38
TBL
V7515
1,2,4-Trimethyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 17 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93307 Matrix: Solids
Sample ID: Comp-2 Sampled: 8/10/2021 11:35
Analytical Method: 8260D Prep Batch(es): V7514 08/11/21 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,3,5-Trimethyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
Vinyl Acetate
<0.0005
mg/Kg - dry
0.0005
0.011
1
08/11/21 12:38
TBL
V7515
Vinyl Chloride
<0.0005
mg/Kg - dry
0.0005
0.011
1
08/11/21 12:38
TBL
V7515
o-Xylene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
TBL
V7515
m,p-Xylene
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 12:38
TBL
V7515
Xylene (Total)
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 12:38
V7515
Surrogate:4-Bromofluorobenzene
102
Limits:70-130%
1 08/11/21 12:38 TBL
V7515
Surrogate: Dibromofluoromethane
102
Limits: 84-123%
1 08/11/21 12:38 TBL
V7515
Surrogate: Toluene-d8
96.8
Limits: 76-129%
1 08/11/21 12:38 TBL
V7515
Analytical Method: 8270E
Prep Batch(es):
V7702
08/16/21
09:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.130
mg/Kg - dry
0.130
0.742
1
08/17/21 22:04
JMV
V7735
Acenaphthylene
0.1583
mg/Kg - dry
0.117
0.742
1
08/17/21 22:04
JMV
V7735
Aniline
<0.170
mg/Kg - dry
0.170
0.742
1
08/17/21 22:04
JMV
V7735
Anthracene
<0.160
mg/Kg - dry
0.160
0.742
1
08/17/21 22:04
JMV
V7735
Benzo(a)anthracene
<0.156
mg/Kg - dry
0.156
0.742
1
08/17/21 22:04
JMV
V7735
Benzo(a)pyrene
<0.165
mg/Kg - dry
0.165
0.742
1
08/17/21 22:04
JMV
V7735
Benzo(b)fluoranthene
0.1713
mg/Kg - dry
0.164
0.742
1
08/17/21 22:04
JMV
V7735
Benzo(g,h,i)perylene
<0.152
mg/Kg - dry
0.152
0.742
1
08/17/21 22:04
JMV
V7735
Benzo(k)fluoranthene
<0.153
mg/Kg - dry
0.153
0.742
1
08/17/21 22:04
JMV
V7735
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 18 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026
REPORT OF ANAL YSIS
Lab No : 93307 Matrix: Solids
Sample ID: Comp-2 Sampled: 8/10/2021 11:35
Analytical Method: 8270E Prep Batch(es): V7702 08/16/21 09:00
Prep Method: 3546
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Benzoic Acid
<0.651
mg/Kg - dry
0.651
2.25
1
08/17/21 22:04
JMV
V7735
Benzyl alcohol
<0.117
mg/Kg - dry
0.117
0.742
1
08/17/21 22:04
JMV
V7735
Bis(2-Chloroethoxy)methane
<0.132
mg/Kg - dry
0.132
0.742
1
08/17/21 22:04
JMV
V7735
Bis(2-Chloroethyl)ether
<0.120
mg/Kg - dry
0.120
0.742
1
08/17/21 22:04
JMV
V7735
Bis(2-Chloroisopropyl)ether
<0.152
mg/Kg - dry
0.152
0.370
1
08/17/21 22:04
JMV
V7735
Bis(2-ethylhexyl)phthalate
<0.134
mg/Kg - dry
0.134
0.742
1
08/17/21 22:04
JMV
V7735
4-Bromophenyl phenyl ether
<0.122
mg/Kg - dry
0.122
0.742
1
08/17/21 22:04
JMV
V7735
Butyl benzyl phthalate
<0.126
mg/Kg - dry
0.126
0.370
1
08/17/21 22:04
JMV
V7735
4-Chloro-3-methyl phenol
<0.103
mg/Kg - dry
0.103
0.742
1
08/17/21 22:04
JMV
V7735
4-Chloroaniline
<0.125
mg/Kg - dry
0.125
0.370
1
08/17/21 22:04
JMV
V7735
2-Chloronaphthalene
<0.130
mg/Kg - dry
0.130
0.742
1
08/17/21 22:04
JMV
V7735
2-Chlorophenol
<0.110
mg/Kg - dry
0.110
0.742
1
08/17/21 22:04
JMV
V7735
4-Chlorophenyl phenyl ether
<0.141
mg/Kg - dry
0.141
1.12
1
08/17/21 22:04
JMV
V7735
Chrysene
<0.159
mg/Kg - dry
0.159
0.742
1
08/17/21 22:04
JMV
V7735
Dibenz(a,h)anthracene
<0.258
mg/Kg - dry
0.258
0.742
1
08/17/21 22:04
JMV
V7735
Dibenzofuran
<0.133
mg/Kg - dry
0.133
0.742
1
08/17/21 22:04
JMV
V7735
1,2-Dichlorobenzene
<0.106
mg/Kg - dry
0.106
0.742
1
08/17/21 22:04
JMV
V7735
1,3-Dichlorobenzene
<0.109
mg/Kg - dry
0.109
0.742
1
08/17/21 22:04
JMV
V7735
1,4-Dichlorobenzene
<0.109
mg/Kg - dry
0.109
0.370
1
08/17/21 22:04
JMV
V7735
3,3'-Dichlorobenzidine
<0.165
mg/Kg - dry
0.165
0.742
1
08/17/21 22:04
JMV
V7735
2,4-Dichlorophenol
<0.107
mg/Kg - dry
0.107
0.742
1
08/17/21 22:04
JMV
V7735
Diethyl phthalate
<0.202
mg/Kg - dry
0.202
0.742
1
08/17/21 22:04
JMV
V7735
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 19 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026
REPORT OF ANAL YSIS
Lab No : 93307 Matrix: Solids
Sample ID: Comp-2 Sampled: 8/10/2021 11:35
Analytical Method: 8270E Prep Batch(es): V7702 08/16/21 09:00
Prep Method: 3546
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Dimethyl phthalate
<0.195
mg/Kg - dry
0.195
0.742
1
08/17/21 22:04
JMV
V7735
2,4-Dimethylphenol
<0.121
mg/Kg - dry
0.121
0.370
1
08/17/21 22:04
JMV
V7735
Di-n-butyl phthalate
<0.120
mg/Kg - dry
0.120
0.742
1
08/17/21 22:04
JMV
V7735
4,6- Din itro-2-methylphenol
<0.269
mg/Kg - dry
0.269
1.69
1
08/17/21 22:04
JMV
V7735
2,4-Dinitrophenol
<0.584
mg/Kg - dry
0.584
1.69
1
08/17/21 22:04
JMV
V7735
2,4-Dinitrotoluene
<0.108
mg/Kg - dry
0.108
0.742
1
08/17/21 22:04
JMV
V7735
2,6-Dinitrotoluene
<0.121
mg/Kg - dry
0.121
0.742
1
08/17/21 22:04
JMV
V7735
Di-n-Octyl Phthalate
<0.160
mg/Kg - dry
0.160
0.370
1
08/17/21 22:04
JMV
V7735
Fluoranthene
0.1663
mg/Kg - dry
0.138
0.742
1
08/17/21 22:04
JMV
V7735
Fluorene
<0.143
mg/Kg - dry
0.143
0.742
1
08/17/21 22:04
JMV
V7735
Hexachlorobenzene
<0.119
mg/Kg - dry
0.119
0.742
1
08/17/21 22:04
JMV
V7735
Hexachlorobutadiene
<0.109
mg/Kg - dry
0.109
0.742
1
08/17/21 22:04
JMV
V7735
Hexachlorocyclopentadiene
<0.176
mg/Kg - dry
0.176
0.742
1
08/17/21 22:04
JMV
V7735
Hexachloroethane
<0.089
mg/Kg - dry
0.089
0.742
1
08/17/21 22:04
JMV
V7735
Indeno(1,2,3-cd)pyrene
<0.201
mg/Kg - dry
0.201
0.742
1
08/17/21 22:04
JMV
V7735
Isophorone
<0.214
mg/Kg - dry
0.214
0.742
1
08/17/21 22:04
JMV
V7735
1-Methylnaphthalene
<0.119
mg/Kg - dry
0.119
0.742
1
08/17/21 22:04
JMV
V7735
2-Methylnaphthalene
<0.112
mg/Kg - dry
0.112
0.742
1
08/17/21 22:04
JMV
V7735
2-Methylphenol
<0.109
mg/Kg - dry
0.109
0.742
1
08/17/21 22:04
JMV
V7735
3&4 Methylphenol
<0.095
mg/Kg - dry
0.095
0.742
1
08/17/21 22:04
JMV
V7735
Naphthalene
<0.161
mg/Kg - dry
0.161
0.742
1
08/17/21 22:04
JMV
V7735
2-Nitroaniline
<0.108
mg/Kg - dry
0.108
0.742
1
08/17/21 22:04
JMV
V7735
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 20 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93307
Matrix: Solids
Sample ID: Comp-2
Sampled: 8/10/2021
11:35
Analytical Method: 8270E
Prep Batch(es):
V7702
08/16/21 09:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
3-Nitroaniline
<0.134
mg/Kg - dry
0.134
0.742
1
08/17/21 22:04 JMV
V7735
4-Nitroaniline
<0.104
mg/Kg - dry
0.104
0.370
1
08/17/21 22:04 JMV
V7735
Nitrobenzene
<0.130
mg/Kg - dry
0.130
0.370
1
08/17/21 22:04 JMV
V7735
2-Nitrophenol
<0.099
mg/Kg - dry
0.099
0.742
1
08/17/21 22:04 JMV
V7735
4-Nitrophenol
<0.131
mg/Kg - dry
0.131
0.742
1
08/17/21 22:04 JMV
V7735
N-N itrosodimethyla mine
<0.295
mg/Kg - dry
0.295
0.742
1
08/17/21 22:04 JMV
V7735
N-Nitrosodiphenylamine
<0.203
mg/Kg - dry
0.203
0.742
1
08/17/21 22:04 JMV
V7735
N-Nitroso-di-n-propylamine
<0.132
mg/Kg - dry
0.132
0.742
1
08/17/21 22:04 JMV
V7735
Pentachlorophenol
<0.389
mg/Kg - dry
0.389
1.12
1
08/17/21 22:04 JMV
V7735
Phenanthrene
<0.233
mg/Kg - dry
0.233
0.742
1
08/17/21 22:04 JMV
V7735
Phenol
<0.125
mg/Kg - dry
0.125
0.742
1
08/17/21 22:04 JMV
V7735
Pyrene
0.1981
mg/Kg - dry
0.150
0.742
1
08/17/21 22:04 JMV
V7735
Pyridine
<0.088
mg/Kg - dry
0.088
0.370
1
08/17/21 22:04 JMV
V7735
1,2,4-Trichlorobenzene
<0.120
mg/Kg - dry
0.120
0.742
1
08/17/21 22:04 JMV
V7735
2,4,5-Trichlorophenol
<0.108
mg/Kg - dry
0.108
0.742
1
08/17/21 22:04 JMV
V7735
2,4,6-Trichlorophenol
<0.108
mg/Kg - dry
0.108
0.742
1
08/17/21 22:04 JMV
V7735
Surrogate: Phenol-d5
73.4
Limits: 34-121%
1 08/17/21 22:04 JMV
V7735
Surrogate:2-Fluorobiphenyl
79.6
Limits:44-115%
1 08/17/21 22:04 JMV
V7735
Surrogate:2-Fluorophenol
75.7
Limits:35-115%
1 08/17/21 22:04 JMV
V7735
Surrogate: Nitrobenzene-d5
70.1
Limits: 37-122%
1 08/17/21 22:04 JMV
V7735
Surrogate:4-Terphenyl-d14
85.0
Limits:54-127%
1 08/17/21 22:04 JMV
V7735
Surrogate: 2,4,6-Tribromophenol
78.4
Limits:39-132%
1 08/17/21 22:04 JMV
V7735
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 21 of 81

WavDdibnto
ANALYTICAL
00019
F&R, Inc. - Charlotte
Brian Olin
3300 International Airport Dr., Suite 600
Charlotte , NC 28208
Project RA Eden
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Report Date : 08/18/2021
Received : 08/10/2021
Lab No : 93308
Sample ID: Comp-3
Matrix: Solids
Sampled: 8/10/2021 11:45
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
9.53
%
1
08/12/2117:20
EDV
SW-DRYWT
Arsenic
7.46
mg/Kg - dry
0.104
1.11
10
08/12/21 14:16
EDV
6020B
Barium
89.2
mg/Kg - dry
1.55
11.1
10
08/12/21 14:16
EDV
6020E
Cadmium
0.0788 J
mg/Kg - dry
0.0607
0.553
10
08/12/21 14:16
EDV
6020B
Chromium
47.8
mg/Kg - dry
0.320
1.11
10
08/12/21 14:16
EDV
6020E
Lead
35.1
mg/Kg - dry
0.155
1.11
10
08/12/21 14:16
EDV
6020B
Mercury (Total)
0.0617
mg/Kg - dry
0.0133
0.0332
1
08/12/21 15:38
EDV
7471E
Selenium
2.16 J
mg/Kg - dry
0.994
2.21
10
08/12/21 14:16
EDV
6020B
Silver
<0.0453
mg/Kg - dry
0.0453
0.553
10
08/12/21 14:16
EDV
6020E
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 22 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93308
Matrix: Solids
Sample ID: Comp-3
Sampled:
8/10/2021 11:45
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
0.035
mg/Kg - dry
0.002
0.022
1
08/11/21 13:07
TBL
V7515
Acrolein
<0.001
mg/Kg - dry
0.001
0.022
1
08/11/21 13:07
TBL
V7515
Acrylonitrile
<0.0008
mg/Kg - dry
0.0008
0.022
1
08/11/21 13:07
TBL
V7515
Benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
Bromobenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
Bromochloromethane
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 13:07
TBL
V7515
Bromodichloromethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
Bromoform
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
Bromomethane
<0.002
mg/Kg - dry
0.002
0.011
1
08/11/21 13:07
TBL
V7515
n-Butylbenzene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:07
TBL
V7515
sec -Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
tert-Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
Carbon Disulfide
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 13:07
TBL
V7515
Carbon Tetrachloride
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
Chlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 13:07
TBL
V7515
Chlorodibromomethane
<0.0010
mg/Kg - dry
0.0010
0.005
1
08/11/21 13:07
TBL
V7515
Chloroethane
<0.0010
mg/Kg - dry
0.0010
0.011
1
08/11/21 13:07
TBL
V7515
Chloroform
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
Chloromethane
<0.0007
mg/Kg - dry
0.0007
0.011
1
08/11/21 13:07
TBL
V7515
2-Chlorotoluene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
4-Chlorotoluene
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 13:07
TBL
V7515
Di -Isopropyl Ether (DIPE)
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 13:07
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 23 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93308
Matrix: Solids
Sample ID: Comp-3
Sampled:
8/10/2021 11:45
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.0005
mg/Kg - dry
0.0005
0.011
1
08/11/21 13:07
TBL
V7515
1,2-Dibromoethane
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 13:07
TBL
V7515
Dibromomethane
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
1,2-Dichlorobenzene
<0.0003
mg/Kg - dry
0.0003
0.005
1
08/11/21 13:07
TBL
V7515
1,3-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 13:07
TBL
V7515
1,4-Dichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 13:07
TBL
V7515
Dichlorodifluoromethane
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 13:07
TBL
V7515
1,1-Dichloroethane
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 13:07
TBL
V7515
1,2-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
1,1-Dichloroethene
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 13:07
TBL
V7515
cis- 1,2-Dich loroethene
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 13:07
TBL
V7515
trans-1,2-Dichloroethene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
1,2-Dichloropropane
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:07
TBL
V7515
1,3-Dichloropropane
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
2,2-Dichloropropane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
1,1-Dichloropropene
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 13:07
TBL
V7515
cis- 1,3-Dich loropropene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
trans-1,3-Dichloropropene
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 13:07
TBL
V7515
Ethylbenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
Ethyl Tertiary Butyl Ether (ETBE)
<0.0009
mg/Kg - dry
0.0009
0.055
1
08/11/21 13:07
TBL
V7515
Hexachlorobutadiene
<0.0009
mg/Kg - dry
0.0009
0.011
1
08/11/21 13:07
TBL
V7515
n-Hexane
0.0013
mg/Kg - dry
0.0007
0.011
1
08/11/21 13:07
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 24 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93308
Matrix: Solids
Sample ID: Comp-3
Sampled:
8/10/2021 11:45
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Hexanone
<0.0007
mg/Kg - dry
0.0007
0.022
1
08/11/21 13:07
TBL
V7515
Isopropyl benzene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:07
TBL
V7515
4-Isopropyl toluene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
Methyl Ethyl Ketone (MEK)
0.0023
mg/Kg - dry
0.0007
0.022
1
08/11/21 13:07
TBL
V7515
Methyl tert-butyl ether (MTBE)
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 13:07
TBL
V7515
4-Methyl-2-Pentanone
<0.016
mg/Kg - dry
0.016
0.022
1
08/11/21 13:07
TBL
V7515
Methylene Chloride
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 13:07
TBL
V7515
Naphthalene
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 13:07
TBL
V7515
n-Propylbenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
Styrene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
1,1,1,2-Tetrachloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
1,1,2,2-Tetrachloroethane
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 13:07
TBL
V7515
Tetrachloroethene
<0.0010
mg/Kg - dry
0.0010
0.005
1
08/11/21 13:07
TBL
V7515
Toluene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 13:07
TBL
V7515
1,2,3-Trichlorobenzene
<0.0006
mg/Kg - dry
0.0006
0.011
1
08/11/21 13:07
TBL
V7515
1,2,4-Trichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.011
1
08/11/21 13:07
TBL
V7515
1,1,1-Trichloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
1,1,2-Trichloroethane
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:07
TBL
V7515
Trichloroethene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:07
TBL
V7515
Trichlorofluoromethane
<0.002
mg/Kg - dry
0.002
0.011
1
08/11/21 13:07
TBL
V7515
1,2,3-Trichloropropane
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 13:07
TBL
V7515
1,2,4-Trimethyl benzene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:07
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 25 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93308 Matrix: Solids
Sample ID: Comp-3 Sampled: 8/10/2021 11:45
Analytical Method: 8260D Prep Batch(es): V7514 08/11/21 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,3,5-Trimethyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
Vinyl Acetate
<0.0005
mg/Kg - dry
0.0005
0.011
1
08/11/21 13:07
TBL
V7515
Vinyl Chloride
<0.0005
mg/Kg - dry
0.0005
0.011
1
08/11/21 13:07
TBL
V7515
o-Xylene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
TBL
V7515
m,p-Xylene
<0.001
mg/Kg - dry
0.001
0.011
1
08/11/21 13:07
TBL
V7515
Xylene (Total)
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:07
V7515
Surrogate:4-Bromofluorobenzene
100
Limits:70-130%
1 08/11/21 13:07 TBL
V7515
Surrogate: Dibromofluoromethane
99.8
Limits: 84-123%
1 08/11/21 13:07 TBL
V7515
Surrogate: Toluene-d8
95.8
Limits: 76-129%
1 08/11/21 13:07 TBL
V7515
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21
12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.128
mg/Kg - dry
0.128
0.729
1
08/13/21 15:46
JMV
V7647
Acenaphthylene
0.2143
mg/Kg - dry
0.116
0.729
1
08/13/21 15:46
JMV
V7647
Aniline
<0.168
mg/Kg - dry
0.168
0.729
1
08/13/21 15:46
JMV
V7647
Anthracene
0.1743
mg/Kg - dry
0.158
0.729
1
08/13/21 15:46
JMV
V7647
Benzo(a)anthracene
<0.153
mg/Kg - dry
0.153
0.729
1
08/13/21 15:46
JMV
V7647
Benzo(a)pyrene
<0.162
mg/Kg - dry
0.162
0.729
1
08/13/21 15:46
JMV
V7647
Benzo(b)fluoranthene
<0.161
mg/Kg - dry
0.161
0.729
1
08/13/21 15:46
JMV
V7647
Benzo(g,h,i)perylene
<0.150
mg/Kg - dry
0.150
0.729
1
08/13/21 15:46
JMV
V7647
Benzo(k)fluoranthene
<0.151
mg/Kg - dry
0.151
0.729
1
08/13/21 15:46
JMV
V7647
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 26 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93308
Matrix: Solids
Sample ID: Comp-3
Sampled:
8/10/2021 11:45
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21 12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzoic Acid
<0.641
mg/Kg - dry
0.641
2.21
1
08/13/21 15:46
JMV
V7647
Benzyl alcohol
<0.116
mg/Kg - dry
0.116
0.729
1
08/13/21 15:46
JMV
V7647
Bis(2-Chloroethoxy)methane
<0.130
mg/Kg - dry
0.130
0.729
1
08/13/21 15:46
JMV
V7647
Bis(2-Chloroethyl)ether
<0.118
mg/Kg - dry
0.118
0.729
1
08/13/21 15:46
JMV
V7647
Bis(2-Chloroisopropyl)ether
<0.150
mg/Kg - dry
0.150
0.364
1
08/13/21 15:46
JMV
V7647
Bis(2-ethylhexyl)phthalate
<0.132
mg/Kg - dry
0.132
0.729
1
08/13/21 15:46
JMV
V7647
4-Bromophenyl phenyl ether
<0.120
mg/Kg - dry
0.120
0.729
1
08/13/21 15:46
JMV
V7647
Butyl benzyl phthalate
<0.124
mg/Kg - dry
0.124
0.364
1
08/13/21 15:46
JMV
V7647
4-Chloro-3-methyl phenol
<0.102
mg/Kg - dry
0.102
0.729
1
08/13/21 15:46
JMV
V7647
4-Chloroaniline
<0.123
mg/Kg - dry
0.123
0.364
1
08/13/21 15:46
JMV
V7647
2-Chloronaphthalene
<0.128
mg/Kg - dry
0.128
0.729
1
08/13/21 15:46
JMV
V7647
2-Chlorophenol
<0.108
mg/Kg - dry
0.108
0.729
1
08/13/21 15:46
JMV
V7647
4-Chlorophenyl phenyl ether
<0.139
mg/Kg - dry
0.139
1.11
1
08/13/21 15:46
JMV
V7647
Chrysene
<0.156
mg/Kg - dry
0.156
0.729
1
08/13/21 15:46
JMV
V7647
Dibenz(a,h)anthracene
<0.254
mg/Kg - dry
0.254
0.729
1
08/13/21 15:46
JMV
V7647
Dibenzofuran
<0.131
mg/Kg - dry
0.131
0.729
1
08/13/21 15:46
JMV
V7647
1,2-Dichlorobenzene
<0.104
mg/Kg - dry
0.104
0.729
1
08/13/21 15:46
JMV
V7647
1,3-Dichlorobenzene
<0.107
mg/Kg - dry
0.107
0.729
1
08/13/21 15:46
JMV
V7647
1,4-Dichlorobenzene
<0.107
mg/Kg - dry
0.107
0.364
1
08/13/21 15:46
JMV
V7647
3,3'-Dichlorobenzidine
<0.162
mg/Kg - dry
0.162
0.729
1
08/13/21 15:46
JMV
V7647
2,4-Dichlorophenol
<0.105
mg/Kg - dry
0.105
0.729
1
08/13/21 15:46
JMV
V7647
Diethyl phthalate
<0.198
mg/Kg - dry
0.198
0.729
1
08/13/21 15:46
JMV
V7647
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 27 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93308
Matrix: Solids
Sample ID: Comp-3
Sampled:
8/10/2021 11:45
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21 12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Dimethyl phthalate
<0.192
mg/Kg - dry
0.192
0.729
1
08/13/21 15:46
JMV
V7647
2,4-Dimethylphenol
<0.119
mg/Kg - dry
0.119
0.364
1
08/13/21 15:46
JMV
V7647
Di-n-butyl phthalate
<0.118
mg/Kg - dry
0.118
0.729
1
08/13/21 15:46
JMV
V7647
4,6- Din itro-2-methylphenol
<0.265
mg/Kg - dry
0.265
1.66
1
08/13/21 15:46
JMV
V7647
2,4-Dinitrophenol
<0.574
mg/Kg - dry
0.574
1.66
1
08/13/21 15:46
JMV
V7647
2,4-Dinitrotoluene
<0.106
mg/Kg - dry
0.106
0.729
1
08/13/21 15:46
JMV
V7647
2,6-Dinitrotoluene
<0.119
mg/Kg - dry
0.119
0.729
1
08/13/21 15:46
JMV
V7647
Di-n-Octyl Phthalate
<0.158
mg/Kg - dry
0.158
0.364
1
08/13/21 15:46
JMV
V7647
Fluoranthene
<0.135
mg/Kg - dry
0.135
0.729
1
08/13/21 15:46
JMV
V7647
Fluorene
<0.141
mg/Kg - dry
0.141
0.729
1
08/13/21 15:46
JMV
V7647
Hexachlorobenzene
<0.117
mg/Kg - dry
0.117
0.729
1
08/13/21 15:46
JMV
V7647
Hexachlorobutadiene
<0.107
mg/Kg - dry
0.107
0.729
1
08/13/21 15:46
JMV
V7647
Hexachlorocyclopentadiene
<0.173
mg/Kg - dry
0.173
0.729
1
08/13/21 15:46
JMV
V7647
Hexachloroethane
<0.087
mg/Kg - dry
0.087
0.729
1
08/13/21 15:46
JMV
V7647
Indeno(1,2,3-cd)pyrene
<0.197
mg/Kg - dry
0.197
0.729
1
08/13/21 15:46
JMV
V7647
Isophorone
<0.211
mg/Kg - dry
0.211
0.729
1
08/13/21 15:46
JMV
V7647
1-Methylnaphthalene
<0.117
mg/Kg - dry
0.117
0.729
1
08/13/21 15:46
JMV
V7647
2-Methylnaphthalene
<0.110
mg/Kg - dry
0.110
0.729
1
08/13/21 15:46
JMV
V7647
2-Methylphenol
<0.107
mg/Kg - dry
0.107
0.729
1
08/13/21 15:46
JMV
V7647
3&4 Methylphenol
<0.093
mg/Kg - dry
0.093
0.729
1
08/13/21 15:46
JMV
V7647
Naphthalene
<0.159
mg/Kg - dry
0.159
0.729
1
08/13/21 15:46
JMV
V7647
2-Nitroaniline
<0.106
mg/Kg - dry
0.106
0.729
1
08/13/21 15:46
JMV
V7647
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 28 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93308
Matrix: Solids
Sample ID: Comp-3
Sampled: 8/10/2021
11:45
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21 12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
3-Nitroaniline
<0.132
mg/Kg - dry
0.132
0.729
1
08/13/21 15:46 JMV
V7647
4-Nitroaniline
<0.103
mg/Kg - dry
0.103
0.364
1
08/13/21 15:46 JMV
V7647
Nitrobenzene
<0.128
mg/Kg - dry
0.128
0.364
1
08/13/21 15:46 JMV
V7647
2-Nitrophenol
<0.098
mg/Kg - dry
0.098
0.729
1
08/13/21 15:46 JMV
V7647
4-Nitrophenol
<0.129
mg/Kg - dry
0.129
0.729
1
08/13/21 15:46 JMV
V7647
N-N itrosodimethyla mine
<0.290
mg/Kg - dry
0.290
0.729
1
08/13/21 15:46 JMV
V7647
N-Nitrosodiphenylamine
<0.200
mg/Kg - dry
0.200
0.729
1
08/13/21 15:46 JMV
V7647
N-Nitroso-di-n-propylamine
<0.130
mg/Kg - dry
0.130
0.729
1
08/13/21 15:46 JMV
V7647
Pentachlorophenol
<0.383
mg/Kg - dry
0.383
1.11
1
08/13/21 15:46 JMV
V7647
Phenanthrene
<0.229
mg/Kg - dry
0.229
0.729
1
08/13/21 15:46 JMV
V7647
Phenol
<0.123
mg/Kg - dry
0.123
0.729
1
08/13/21 15:46 JMV
V7647
Pyrene
<0.148
mg/Kg - dry
0.148
0.729
1
08/13/21 15:46 JMV
V7647
Pyridine
<0.087
mg/Kg - dry
0.087
0.364
1
08/13/21 15:46 JMV
V7647
1,2,4-Trichlorobenzene
<0.118
mg/Kg - dry
0.118
0.729
1
08/13/21 15:46 JMV
V7647
2,4,5-Trichlorophenol
<0.106
mg/Kg - dry
0.106
0.729
1
08/13/21 15:46 JMV
V7647
2,4,6-Trichlorophenol
<0.106
mg/Kg - dry
0.106
0.729
1
08/13/21 15:46 JMV
V7647
Surrogate: Phenol-d5
64.4
Limits: 34-121%
1 08/13/21 15:46 JMV
V7647
Surrogate:2-Fluorobiphenyl
75.9
Limits:44-115%
1 08/13/21 15:46 JMV
V7647
Surrogate:2-Fluorophenol
63.4
Limits:35-115%
1 08/13/21 15:46 JMV
V7647
Surrogate: Nitrobenzene-d5
65.7
Limits: 37-122%
1 08/13/21 15:46 JMV
V7647
Surrogate:4-Terphenyl-d14
80.7
Limits:54-127%
1 08/13/21 15:46 JMV
V7647
Surrogate: 2,4,6-Tribromophenol
65.3
Limits:39-132%
1 08/13/21 15:46 JMV
V7647
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 29 of 81

WavDdibnto
ANALYTICAL
00019
F&R, Inc. - Charlotte
Brian Olin
3300 International Airport Dr., Suite 600
Charlotte , NC 28208
Project RA Eden
Information :
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointana lyti ca Isom
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Report Date : 08/18/2021
Received : 08/10/2021
Lab No : 93309
Sample ID: Comp-4
Matrix: Solids
Sampled: 8/10/2021 12:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
4.48
%
1
08/12/2117:20
EDV
SW-DRYWT
Arsenic
8.99
mg/Kg - dry
0.0984
1.05
10
08/12/21 14:35
EDV
6020B
Barium
80.5
mg/Kg - dry
1.47
10.5
10
08/12/21 14:35
EDV
6020E
Cadmium
0.0738J
mg/Kg - dry
0.0575
0.523
10
08/12/21 14:35
EDV
6020B
Chromium
46.1
mg/Kg - dry
0.303
1.05
10
08/12/21 14:35
EDV
6020E
Lead
34.0
mg/Kg - dry
0.147
1.05
10
08/12/21 14:35
EDV
6020B
Mercury (Total)
0.0617
mg/Kg - dry
0.0126
0.0314
1
08/12/21 15:40
EDV
7471E
Selenium
1.70J
mg/Kg - dry
0.942
2.09
10
08/12/21 14:35
EDV
6020B
Silver
0.0646J
mg/Kg - dry
0.0429
0.523
10
08/12/21 14:35
EDV
6020E
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 30 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93309
Matrix: Solids
Sample ID: Comp-4
Sampled:
8/10/2021 12:00
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
0.0043
mg/Kg - dry
0.002
0.020
1
08/11/21 13:37
TBL
V7515
Acrolein
<0.001
mg/Kg - dry
0.001
0.020
1
08/11/21 13:37
TBL
V7515
Acrylonitrile
<0.0008
mg/Kg - dry
0.0008
0.020
1
08/11/21 13:37
TBL
V7515
Benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:37
TBL
V7515
Bromobenzene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:37
TBL
V7515
Bromochloromethane
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 13:37
TBL
V7515
Bromodichloromethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:37
TBL
V7515
Bromoform
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:37
TBL
V7515
Bromomethane
<0.001
mg/Kg - dry
0.001
0.010
1
08/11/21 13:37
TBL
V7515
n-Butylbenzene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:37
TBL
V7515
sec -Butyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:37
TBL
V7515
tert-Butyl benzene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:37
TBL
V7515
Carbon Disulfide
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 13:37
TBL
V7515
Carbon Tetrachloride
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:37
TBL
V7515
Chlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 13:37
TBL
V7515
Chlorodibromomethane
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 13:37
TBL
V7515
Chloroethane
<0.0009
mg/Kg - dry
0.0009
0.010
1
08/11/21 13:37
TBL
V7515
Chloroform
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:37
TBL
V7515
Chloromethane
<0.0007
mg/Kg - dry
0.0007
0.010
1
08/11/21 13:37
TBL
V7515
2-Chlorotoluene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:37
TBL
V7515
4-Chlorotoluene
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 13:37
TBL
V7515
Di -Isopropyl Ether (DIPE)
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 13:37
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 31 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93309
Matrix: Solids
Sample ID: Comp-4
Sampled:
8/10/2021 12:00
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
1,2-Dibromo-3-Chloropropane
<0.0005
mg/Kg - dry
0.0005
0.010
1
08/11/21 13:37
TBL
V7515
1,2-Dibromoethane
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:37
TBL
V7515
Dibromomethane
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:37
TBL
V7515
1,2-Dichlorobenzene
<0.0003
mg/Kg - dry
0.0003
0.005
1
08/11/21 13:37
TBL
V7515
1,3-Dichlorobenzene
<0.0004
mg/Kg - dry
0.0004
0.005
1
08/11/21 13:37
TBL
V7515
1,4-Dichlorobenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:37
TBL
V7515
Dichlorodifluoromethane
<0.001
mg/Kg - dry
0.001
0.010
1
08/11/21 13:37
TBL
V7515
1,1-Dichloroethane
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 13:37
TBL
V7515
1,2-Dichloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:37
TBL
V7515
1,1-Dichloroethene
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 13:37
TBL
V7515
cis- 1,2-Dich loroethene
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 13:37
TBL
V7515
trans-1,2-Dichloroethene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:37
TBL
V7515
1,2-Dichloropropane
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:37
TBL
V7515
1,3-Dichloropropane
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:37
TBL
V7515
2,2-Dichloropropane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:37
TBL
V7515
1,1-Dichloropropene
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 13:37
TBL
V7515
cis- 1,3-Dich loropropene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:37
TBL
V7515
trans-1,3-Dichloropropene
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 13:37
TBL
V7515
Ethylbenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:37
TBL
V7515
Ethyl Tertiary Butyl Ether (ETBE)
<0.0009
mg/Kg - dry
0.0009
0.052
1
08/11/21 13:37
TBL
V7515
Hexachlorobutadiene
<0.0008
mg/Kg - dry
0.0008
0.010
1
08/11/21 13:37
TBL
V7515
n-Hexane
<0.0007
mg/Kg - dry
0.0007
0.010
1
08/11/21 13:37
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 32 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93309
Matrix: Solids
Sample ID: Comp-4
Sampled:
8/10/2021 12:00
Analytical Method: 8260D
Prep Batch(es):
V7514
08/11/21 08:00
Prep Method: 5035 LOW
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2-Hexanone
<0.0006
mg/Kg - dry
0.0006
0.020
1
08/11/21 13:37
TBL
V7515
Isopropyl benzene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:37
TBL
V7515
4-Isopropyl toluene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:37
TBL
V7515
Methyl Ethyl Ketone (MEK)
<0.0007
mg/Kg - dry
0.0007
0.020
1
08/11/21 13:37
TBL
V7515
Methyl tert-butyl ether (MTBE)
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:37
TBL
V7515
4-Methyl-2-Pentanone
<0.015
mg/Kg - dry
0.015
0.020
1
08/11/21 13:37
TBL
V7515
Methylene Chloride
<0.001
mg/Kg - dry
0.001
0.010
1
08/11/21 13:37
TBL
V7515
Naphthalene
<0.001
mg/Kg - dry
0.001
0.010
1
08/11/21 13:37
TBL
V7515
n-Propylbenzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:37
TBL
V7515
Styrene
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:37
TBL
V7515
1,1,1,2-Tetrachloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:37
TBL
V7515
1,1,2,2-Tetrachloroethane
<0.0003
mg/Kg - dry
0.0003
0.005
1
08/11/21 13:37
TBL
V7515
Tetrachloroethene
<0.0009
mg/Kg - dry
0.0009
0.005
1
08/11/21 13:37
TBL
V7515
Toluene
<0.0007
mg/Kg - dry
0.0007
0.005
1
08/11/21 13:37
TBL
V7515
1,2,3-Trichlorobenzene
<0.0006
mg/Kg - dry
0.0006
0.010
1
08/11/21 13:37
TBL
V7515
1,2,4-Trichlorobenzene
<0.0007
mg/Kg - dry
0.0007
0.010
1
08/11/21 13:37
TBL
V7515
1,1,1-Trichloroethane
<0.001
mg/Kg - dry
0.001
0.005
1
08/11/21 13:37
TBL
V7515
1,1,2-Trichloroethane
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:37
TBL
V7515
Trichloroethene
<0.0010
mg/Kg - dry
0.0010
0.005
1
08/11/21 13:37
TBL
V7515
Trichlorofluoromethane
<0.002
mg/Kg - dry
0.002
0.010
1
08/11/21 13:37
TBL
V7515
1,2,3-Trichloropropane
<0.0008
mg/Kg - dry
0.0008
0.005
1
08/11/21 13:37
TBL
V7515
1,2,4-Trimethyl benzene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:37
TBL
V7515
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 33 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93309 Matrix: Solids
Sample ID: Comp-4 Sampled: 8/10/2021 12:00
Analytical Method: 8260D Prep Batch(es): V7514 08/11/21 08:00
Prep Method: 5035 LOW
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
1,3,5-Trimethyl benzene
<0.0006
mg/Kg - dry
0.0006
0.005
1
08/11/21 13:37
TBL
V7515
Vinyl Acetate
<0.0005
mg/Kg - dry
0.0005
0.010
1
08/11/21 13:37
TBL
V7515
Vinyl Chloride
<0.0005
mg/Kg - dry
0.0005
0.010
1
08/11/21 13:37
TBL
V7515
o-Xylene
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:37
TBL
V7515
m,p-Xylene
<0.001
mg/Kg - dry
0.001
0.010
1
08/11/21 13:37
TBL
V7515
Xylene (Total)
<0.0005
mg/Kg - dry
0.0005
0.005
1
08/11/21 13:37
V7515
Surrogate:4-Bromofluorobenzene
102
Limits:70-130%
1 08/11/21 13:37 TBL
V7515
Surrogate: Dibromofluoromethane
102
Limits: 84-123%
1 08/11/21 13:37 TBL
V7515
Surrogate: Toluene-d8
95.1
Limits: 76-129%
1 08/11/21 13:37 TBL
V7515
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21
12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acenaphthene
<0.121
mg/Kg - dry
0.121
0.690
1
08/13/21 16:09
JMV
V7647
Acenaphthylene
0.2383
mg/Kg - dry
0.109
0.690
1
08/13/21 16:09
JMV
V7647
Aniline
<0.159
mg/Kg - dry
0.159
0.690
1
08/13/21 16:09
JMV
V7647
Anthracene
0.1943
mg/Kg - dry
0.149
0.690
1
08/13/21 16:09
JMV
V7647
Benzo(a)anthracene
<0.145
mg/Kg - dry
0.145
0.690
1
08/13/21 16:09
JMV
V7647
Benzo(a)pyrene
<0.153
mg/Kg - dry
0.153
0.690
1
08/13/21 16:09
JMV
V7647
Benzo(b)fluoranthene
<0.152
mg/Kg - dry
0.152
0.690
1
08/13/21 16:09
JMV
V7647
Benzo(g,h,i)perylene
<0.142
mg/Kg - dry
0.142
0.690
1
08/13/21 16:09
JMV
V7647
Benzo(k)fluoranthene
<0.143
mg/Kg - dry
0.143
0.690
1
08/13/21 16:09
JMV
V7647
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation
Limit
Page 34 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93309
Matrix: Solids
Sample ID: Comp-4
Sampled:
8/10/2021 12:00
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21 12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Benzoic Acid
<0.607
mg/Kg - dry
0.607
2.09
1
08/13/21 16:09
JMV
V7647
Benzyl alcohol
<0.109
mg/Kg - dry
0.109
0.690
1
08/13/21 16:09
JMV
V7647
Bis(2-Chloroethoxy)methane
<0.123
mg/Kg - dry
0.123
0.690
1
08/13/21 16:09
JMV
V7647
Bis(2-Chloroethyl)ether
<0.112
mg/Kg - dry
0.112
0.690
1
08/13/21 16:09
JMV
V7647
Bis(2-Chloroisopropyl)ether
<0.142
mg/Kg - dry
0.142
0.345
1
08/13/21 16:09
JMV
V7647
Bis(2-ethylhexyl)phthalate
0.713
mg/Kg - dry
0.125
0.690
1
08/13/21 16:09
JMV
V7647
4-Bromophenyl phenyl ether
<0.114
mg/Kg - dry
0.114
0.690
1
08/13/21 16:09
JMV
V7647
Butyl benzyl phthalate
<0.118
mg/Kg - dry
0.118
0.345
1
08/13/21 16:09
JMV
V7647
4-Chloro-3-methyl phenol
<0.096
mg/Kg - dry
0.096
0.690
1
08/13/21 16:09
JMV
V7647
4-Chloroaniline
<0.117
mg/Kg - dry
0.117
0.345
1
08/13/21 16:09
JMV
V7647
2-Chloronaphthalene
<0.121
mg/Kg - dry
0.121
0.690
1
08/13/21 16:09
JMV
V7647
2-Chlorophenol
<0.102
mg/Kg - dry
0.102
0.690
1
08/13/21 16:09
JMV
V7647
4-Chlorophenyl phenyl ether
<0.131
mg/Kg - dry
0.131
1.05
1
08/13/21 16:09
JMV
V7647
Chrysene
<0.148
mg/Kg - dry
0.148
0.690
1
08/13/21 16:09
JMV
V7647
Dibenz(a,h)anthracene
<0.240
mg/Kg - dry
0.240
0.690
1
08/13/21 16:09
JMV
V7647
Dibenzofuran
<0.124
mg/Kg - dry
0.124
0.690
1
08/13/21 16:09
JMV
V7647
1,2-Dichlorobenzene
<0.098
mg/Kg - dry
0.098
0.690
1
08/13/21 16:09
JMV
V7647
1,3-Dichlorobenzene
<0.101
mg/Kg - dry
0.101
0.690
1
08/13/21 16:09
JMV
V7647
1,4-Dichlorobenzene
<0.102
mg/Kg - dry
0.102
0.345
1
08/13/21 16:09
JMV
V7647
3,3'-Dichlorobenzidine
<0.153
mg/Kg - dry
0.153
0.690
1
08/13/21 16:09
JMV
V7647
2,4-Dichlorophenol
<0.100
mg/Kg - dry
0.100
0.690
1
08/13/21 16:09
JMV
V7647
Diethyl phthalate
<0.188
mg/Kg - dry
0.188
0.690
1
08/13/21 16:09
JMV
V7647
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 35 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93309
Matrix: Solids
Sample ID: Comp-4
Sampled:
8/10/2021 12:00
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21 12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Dimethyl phthalate
<0.182
mg/Kg - dry
0.182
0.690
1
08/13/21 16:09
JMV
V7647
2,4-Dimethylphenol
<0.113
mg/Kg - dry
0.113
0.345
1
08/13/21 16:09
JMV
V7647
Di-n-butyl phthalate
<0.112
mg/Kg - dry
0.112
0.690
1
08/13/21 16:09
JMV
V7647
4,6- Din itro-2-methylphenol
<0.251
mg/Kg - dry
0.251
1.57
1
08/13/21 16:09
JMV
V7647
2,4-Dinitrophenol
<0.544
mg/Kg - dry
0.544
1.57
1
08/13/21 16:09
JMV
V7647
2,4-Dinitrotoluene
<0.101
mg/Kg - dry
0.101
0.690
1
08/13/21 16:09
JMV
V7647
2,6-Dinitrotoluene
<0.113
mg/Kg - dry
0.113
0.690
1
08/13/21 16:09
JMV
V7647
Di-n-Octyl Phthalate
<0.149
mg/Kg - dry
0.149
0.345
1
08/13/21 16:09
JMV
V7647
Fluoranthene
0.1993
mg/Kg - dry
0.128
0.690
1
08/13/21 16:09
JMV
V7647
Fluorene
<0.134
mg/Kg - dry
0.134
0.690
1
08/13/21 16:09
JMV
V7647
Hexachlorobenzene
<0.110
mg/Kg - dry
0.110
0.690
1
08/13/21 16:09
JMV
V7647
Hexachlorobutadiene
<0.102
mg/Kg - dry
0.102
0.690
1
08/13/21 16:09
JMV
V7647
Hexachlorocyclopentadiene
<0.164
mg/Kg - dry
0.164
0.690
1
08/13/21 16:09
JMV
V7647
Hexachloroethane
<0.082
mg/Kg - dry
0.082
0.690
1
08/13/21 16:09
JMV
V7647
Indeno(1,2,3-cd)pyrene
<0.187
mg/Kg - dry
0.187
0.690
1
08/13/21 16:09
JMV
V7647
Isophorone
<0.199
mg/Kg - dry
0.199
0.690
1
08/13/21 16:09
JMV
V7647
1-Methylnaphthalene
<0.110
mg/Kg - dry
0.110
0.690
1
08/13/21 16:09
JMV
V7647
2-Methylnaphthalene
<0.104
mg/Kg - dry
0.104
0.690
1
08/13/21 16:09
JMV
V7647
2-Methylphenol
<0.101
mg/Kg - dry
0.101
0.690
1
08/13/21 16:09
JMV
V7647
3&4 Methylphenol
<0.088
mg/Kg - dry
0.088
0.690
1
08/13/21 16:09
JMV
V7647
Naphthalene
<0.150
mg/Kg - dry
0.150
0.690
1
08/13/21 16:09
JMV
V7647
2-Nitroaniline
<0.101
mg/Kg - dry
0.101
0.690
1
08/13/21 16:09
JMV
V7647
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 36 of 81

Waypoint. 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00019
F&R, Inc. - Charlotte Project RA Eden
Brian Olin Report Date : 08/18/2021
3300 International Airport Dr., Suite 600 Information : Received : 08/10/2021
Charlotte , NC 28208
Report Number : 21-222-0026 REPOR T OF A NA L YSIS
Lab No : 93309
Matrix: Solids
Sample ID: Comp-4
Sampled: 8/10/2021
12:00
Analytical Method: 8270E
Prep Batch(es):
V7552
08/12/21 12:00
Prep Method: 3546
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
3-Nitroaniline
<0.125
mg/Kg - dry
0.125
0.690
1
08/13/21 16:09 JMV
V7647
4-Nitroaniline
<0.097
mg/Kg - dry
0.097
0.345
1
08/13/21 16:09 JMV
V7647
Nitrobenzene
<0.121
mg/Kg - dry
0.121
0.345
1
08/13/21 16:09 JMV
V7647
2-Nitrophenol
<0.092
mg/Kg - dry
0.092
0.690
1
08/13/21 16:09 JMV
V7647
4-Nitrophenol
<0.122
mg/Kg - dry
0.122
0.690
1
08/13/21 16:09 JMV
V7647
N-N itrosodimethyla mine
<0.275
mg/Kg - dry
0.275
0.690
1
08/13/21 16:09 JMV
V7647
N-Nitrosodiphenylamine
<0.189
mg/Kg - dry
0.189
0.690
1
08/13/21 16:09 JMV
V7647
N-Nitroso-di-n-propylamine
<0.123
mg/Kg - dry
0.123
0.690
1
08/13/21 16:09 JMV
V7647
Pentachlorophenol
<0.363
mg/Kg - dry
0.363
1.05
1
08/13/21 16:09 JMV
V7647
Phenanthrene
<0.217
mg/Kg - dry
0.217
0.690
1
08/13/21 16:09 JMV
V7647
Phenol
<0.117
mg/Kg - dry
0.117
0.690
1
08/13/21 16:09 JMV
V7647
Pyrene
0.365J
mg/Kg - dry
0.140
0.690
1
08/13/21 16:09 JMV
V7647
Pyridine
<0.082
mg/Kg - dry
0.082
0.345
1
08/13/21 16:09 JMV
V7647
1,2,4-Trichlorobenzene
<0.112
mg/Kg - dry
0.112
0.690
1
08/13/21 16:09 JMV
V7647
2,4,5-Trichlorophenol
<0.100
mg/Kg - dry
0.100
0.690
1
08/13/21 16:09 JMV
V7647
2,4,6-Trichlorophenol
<0.101
mg/Kg - dry
0.101
0.690
1
08/13/21 16:09 JMV
V7647
Surrogate: Phenol-d5
61.6
Limits: 34-121%
1 08/13/21 16:09 JMV
V7647
Surrogate:2-Fluorobiphenyl
71.3
Limits:44-115%
1 08/13/21 16:09 JMV
V7647
Surrogate:2-Fluorophenol
61.9
Limits:35-115%
1 08/13/21 16:09 JMV
V7647
Surrogate: Nitrobenzene-d5
62.9
Limits: 37-122%
1 08/13/21 16:09 JMV
V7647
Surrogate:4-Terphenyl-d14
79.0
Limits:54-127%
1 08/13/21 16:09 JMV
V7647
Surrogate: 2,4,6-Tribromophenol
64.3
Limits:39-132%
1 08/13/21 16:09 JMV
V7647
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions MQL Method Quantitation Limit
Page 37 of 81

aceAnalytical
Report of Analysis
Waypoint Analytical
PO Box 240543
Charlotte, NC 28224
Attention: Angela Overcash
Project Name: 21-222-0026
Lot Number:WH13096
Date Completed:08/18/2021
08/18/2021 4:53 PM
Approved and released by:
Project Manager II: Lucas Odom
A C C A E D I T E❑
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 14
Page 38 of 81

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Waypoint Analytical
Lot Number: WH13096
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] whw.pacelabs.com
Page 2 of 14
Page 39 of 81

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: WH13096
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
Comp-1
Solid
08/10/20211125
08/13/2021
002
Comp-2
Solid
08/10/20211135
08/13/2021
003
Comp-3
Solid
08/10/20211145
08/13/2021
004
Comp-4
Solid
08/10/20211200
08/13/2021
(4 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 14

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Waypoint Analytical
Lot Number: WH13096
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
Comp-1
Solid
Hexavalent Chromium
7199
0.45
J
mg/kg
5
002
Comp-2
Solid
Hexavalent Chromium
7199
0.39
J
mg/kg
6
003
Comp-3
Solid
Hexavalent Chromium
7199
0.33
J
mg/kg
7
004
Comp-4
Solid
Hexavalent Chromium
7199
0.38
J
mg/kg
8
(4 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 14

Client: Waypoint Analytical Laboratory ID: WH13096-001
Description: Comp-1 Matrix: Solid
Date Sampled:08/10/2021 1125 % Solids: 88.5 08/14/2021 1950
Date Received:08/13/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 08/17/2021 1236 AMR 08/16/2021 1409 12295
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexavalent Chromium
18540-29-9 7199 0.45 J 1.1 0.23 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 14

Client: Waypoint Analytical Laboratory ID: WH13096-002
Description: Comp-2 Matrix: Solid
Date Sampled:08/10/2021 1135 % Solids: 86.5 08/14/2021 1950
Date Received:08/13/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 08/17/2021 1249 AMR 08/16/2021 1409 12295
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexavalent Chromium
18540-29-9 7199 0.39 J 1.2 0.23 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 14

Client: Waypoint Analytical Laboratory ID: WH13096-003
Description: Comp-3 Matrix: Solid
Date Sampled:08/10/2021 1145 % Solids: 83.3 08/14/2021 1950
Date Received:08/13/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 08/17/2021 1302 AMR 08/16/2021 1409 12295
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexavalent Chromium
18540-29-9 7199 0.33 J 1.2 0.24 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 14

Client: Waypoint Analytical Laboratory ID: WH13096-004
Description: Comp-4 Matrix: Solid
Date Sampled:08/10/2021 1200 % Solids: 95.0 08/14/2021 1950
Date Received:08/13/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 08/17/2021 1315 AMR 08/16/2021 1409 12295
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexavalent Chromium
18540-29-9 7199 0.38 J 1.1 0.21 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 14

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 14

Inorganic non-metals - MB
Sample ID: WQ12295-001 Matrix: Solid
Batch: 12295 Prep Method: 3060A
Analytical Method: 7199 Prep Date: 08/16/2021 1409
Parameter Result Q Dil LOQ DL Units Analysis Date
Hexavalent Chromium ND 1 1.0 0.20 mg/kg 08/17/2021 1157
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 14

Inorganic non-metals - LCS
Sample ID: WQ12295-002 Matrix: Solid
Batch: 12295 Prep Method: 3O6OA
Analytical Method: 7199 Prep Date: 08/16/2021 1409
Spike
Amount Result %Rec
Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date
Hexavalent Chromium 10 8.5 1 85 80-120 08/17/2021 1223
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria
J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 14

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 14

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 14

PACE ANALYTICAL SERVICES, LLC
Samplas R-PeeTpt Checklrst (SRC) I ME001$�15) Ctirlri� r�= I29f 2L720
raP.AIF71y�iC3i Ic;s„i-1,3 AuthoF�ly: Pace L NIJ- WCUL Page 1 & 1
Sample Receipt Checklist (SRC)
li 1r1; �'aypoia- UM16rintpa'LY1 iay:Idmte: 3RC? 031]]t i12] Lola'- W1115096
cans of receipt_
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pl-r Strip [D_
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Z Wul 1cc U lee Packs ❑ Dry 1co ❑ None
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3. If tempoM[ure of any crral:cr cxcerkd 6,0uc '.vas Prej&n Maniar Notified? --
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6. VWerc sample 'LDr, Fmiml on thm M7 - -
7- Were swuple la Estrd an al' wmple containers?
S, Was collection dale & ,imc listed on Bc COC?
9_ WUV ; collcWor. darc L% cime lEglad an all-L;ample Omit9inel,02 - --
10, DW Ail container label iufranlnaticm jD, dnGc, timcj agree v.ith the CQC?
No
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Lj No
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I I , Wgm tests to be pe_ forned limd on the COO
12. laid all saerlpIrk arrive in the proper cutAAners for each IL-4 ankWor in good condition
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14- Wur-_ all mraple-s received wirll itn K Lhe holding title or 48 l ours, wh=ehcv_r WmO5 tirsr!
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15- Were en � S9lmpla;y contaMcrs L�issinerexce�s {corr��G 0:3G� 4Ari1 Ens [<ot :ista:l ou �0�'
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in any. oCthc VDA viaM?
17. Ware all DRO!rredalrJnedrirmt samples r�ceiired aL a of k 2'e -
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were receives Hum- ctly pis rvmd wW were adjusted aocordingly
h NA LnL ofoircle Dip:M5O4, HNO3, HCJr HaOI4 Using SR fe 14A
lfmore tba monc presvrvat ve is needed, plea%TLotc in the commegas below,
WCH, received vvLl s hi: 'nI 1fi >6 mni in dimneteu.
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in Sam rAe receiving
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 14

Waypointo
ANALYTICAL
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep:
V7520
QC Analytical Batch(es): V7551
QC Prep Batch Method:
3050B
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Lab Reagent Blank
LRB-V7520
Matrix: SOL
Associated Lab Samples:
93306, 93307, 93308,
93309
Blank
MDL
MQL
Analyzed
Parameter
Units
Result
Arsenic
mg/Kg
<0.0940
0.0940
1.00
08/12/2113:18
Barium
mg/Kg
<1.40
1.40
10.0
08/12/2113:18
Cadmium
mg/Kg
<0.0550
0.0550
0.500
08/12/2113:18
Chromium
mg/Kg
<0.290
0.290
1.00
08/12/2113:18
Lead
mg/Kg
<0.140
0.140
1.00
08/12/21 13:18
Selenium
mg/Kg
<0.900
0.900
2.00
08/12/2113:18
Silver
mg/Kg
<0.0410
0.0410
0.500
08/12/2113:18
Laboratory Control Sample
LCS-V7520
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Arsenic
mg/Kg
12.5
12.1
97.0
80-120
Barium
mg/Kg
12.5
12.1
97.0
80-120
Cadmium
mg/Kg
12.5
12.5
100
80-120
Chromium
mg/Kg
12.5
12.5
100
80-120
Lead
mg/Kg
12.5
12.5
100
80-120
Selenium
mg/Kg
12.5
11.9
95.0
80-120
Silver
mg/Kg
5.00
4.98
100
80-120
Matrix Spike & Matrix Spike Duplicate
V 93306-MS-V7520
V 93306-MSD-V7520
MS Spike
MSD
MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Arsenic
mg/Kg
6.74
12.5
12.5
19.8
17.8
104
88.0
75-125
10.6
20
Barium
mg/Kg
46.1
12.5
12.5
71.7
67.1
205*
168*
75-125
6.6
20
Cadmium
mg/Kg
<0.0550
12.5
12.5
12.6
12.4
101
99.0
75-125
1.6
20
Chromium
mg/Kg
37.0
12.5
12.5
57.3
64.4
162*
219*
75-125
11.6
20
* QC Fail Date: 08/18/2021 05:22 PM Page 1 of 28
Page 52 of 81

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Client ID:
F&R, Inc. - Charlotte
Project Description:
RA Eden
Report No:
21-222-0026
QC Prep:
V7520
QC Analytical Batch(es): V7551
QC Prep Batch Method:
3050B
Analysis Method:
6020B
Analysis Description:
Metals Analyses
Matrix Spike & Matrix Spike
Duplicate
V 93306-MS-V7520
V 93306-MSD-V7520
MS Spike
MSD MS Result
MSD MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Spike
Result a/oRec
%Rec
Limits RPD
RPD
Conc.
Lead
mg/Kg
28.3
12.5
12.5 42.3
40.9 112
101
75-125 3.3
20
Selenium
mg/Kg
1.44
12.5
12.5 12.4
11.9 99.0
95.0
75-125 4.1
20
Silver
mg/Kg
<0.0410
5.00
5.00 4.97
4.93 99.0
99.0
75-125 0.8
20
Post Digestion Spike
V 93306-PDS-V7520
PDS
%
Analyzed
Parameter
Units
Result
Recovery
Arsenic
mg/Kg
15.8
99.0
08/12/2113:50
Barium
mg/Kg
35.1
99.0
08/12/2113:50
Cadmium
mg/Kg
12.6
101
08/12/2113:50
Chromium
mg/Kg
30.8
99.0
08/12/2113:50
Lead
mg/Kg
26.0
98.0
08/12/21 13:50
Selenium
mg/Kg
13.5
108
08/12/2113:50
Silver
mg/Kg
12.6
101
08/12/2113:50
Date: 08/18/2021 05:22 PM Page 2 of 28
Page 53 of 81

•
Waypoint,
449 Springbrook Rd, Ch
Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL
www.waypoi ntana lytica l.com
Quality Control Data
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-222-0026
QC Prep: V7543
QC Analytical Batch(es): V7550
QC Prep Batch Method: 7471B (Prep)
Analysis Method:
7471B
Analysis Description:
Solids Total Mercury Analysis - CVAA
Lab Reagent Blank
LRB-V7543
Matrix: SOL
Associated Lab Samples: 93306, 93307, 93308, 93309
Blank MDL
MQL
Analyzed
Parameter Units
Result
Mercury (Total) mg/Kg
<0.0120 0.0120
0.0300
08/12/21 14:57
Laboratory Control Sample
LCS-V7543
Spike
LCS
LCS %Rec % Rec
Parameter Units
Conc.
Result
Limits
Mercury (Total) mg/Kg
0.417
0.406
97.0 80-120
Matrix Spike & Matrix Spike Duplicate
V 92846-MS-V7543
V 92846-MSD-V7543
MS Spike
MSD MS Result
MSD MS MSD %Rec Max
Parameter Units
Result Conc.
Spike
Result %Rec %Rec Limits RPD RPD
Conc.
Mercury (Total) mg/Kg
0.0380 0.417
0.417 0.427
0.436 93.0 96.0 80-120 2.0 20
Post Digestion Spike
V 92846-PDS-V7543
PDS
%
Analyzed
Parameter Units
Result
Recovery
Mercury (Total) mg/Kg
0.227
100
08/12/21 15:12
Date: 08/18/2021 05:22 PM Page 3 of 28
Page 54 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
QC Prep: V7514
QC Prep Batch Method: 5035 LOW
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V7514
Associated Lab Samples: 93306, 93307, 93308, 93309
QC Analytical Batch(es): V7515
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Matrix: SOL
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
mg/Kg
<0.002
0.002
0.020
08/11/21 11:38
Acrolein
mg/Kg
<0.001
0.001
0.020
08/11/21 11:38
Acrylonitrile
mg/Kg
<0.0008
0.0008
0.020
08/11/21 11:38
Benzene
mg/Kg
<0.0006
0.0006
0.005
08/11/21 11:38
Bromobenzene
mg/Kg
<0.0005
0.0005
0.005
08/11/21 11:38
Bromochloromethane
mg/Kg
<0.0008
0.0008
0.005
08/11/21 11:38
Bromodichloromethane
mg/Kg
<0.001
0.001
0.005
08/11/21 11:38
Bromoform
mg/Kg
<0.001
0.001
0.005
08/11/21 11:38
Bromomethane
mg/Kg
<0.001
0.001
0.010
08/11/21 11:38
n-Butylbenzene
mg/Kg
<0.0005
0.0005
0.005
08/11/21 11:38
sec -Butyl benzene
mg/Kg
<0.0006
0.0006
0.005
08/11/21 11:38
tert-Butyl benzene
mg/Kg
<0.0005
0.0005
0.005
08/11/21 11:38
Carbon Disulfide
mg/Kg
<0.0006
0.0006
0.005
08/11/21 11:38
Carbon Tetrachloride
mg/Kg
<0.001
0.001
0.005
08/11/21 11:38
Chlorobenzene
mg/Kg
<0.0007
0.0007
0.005
08/11/21 11:38
Chlorodibromomethane
mg/Kg
<0.0009
0.0009
0.005
08/11/21 11:38
Chloroethane
mg/Kg
<0.0009
0.0009
0.010
08/11/21 11:38
Chloroform
mg/Kg
<0.001
0.001
0.005
08/11/21 11:38
Chloromethane
mg/Kg
<0.0006
0.0006
0.010
08/11/21 11:38
2-Chlorotoluene
mg/Kg
<0.0005
0.0005
0.005
08/11/21 11:38
4-Chlorotoluene
mg/Kg
<0.0004
0.0004
0.005
08/11/21 11:38
Di -Isopropyl Ether (DIPE)
mg/Kg
<0.0007
0.0007
0.005
08/11/21 11:38
1,2-Dibromo-3-Chloropropane
mg/Kg
<0.0004
0.0004
0.010
08/11/21 11:38
1,2-Dibromoethane
mg/Kg
<0.0006
0.0006
0.005
08/11/21 11:38
Dibromomethane
mg/Kg
<0.0006
0.0006
0.005
08/11/21 11:38
1,2-Dichlorobenzene
mg/Kg
<0.0003
0.0003
0.005
08/11/21 11:38
1,3-Dichlorobenzene
mg/Kg
<0.0004
0.0004
0.005
08/11/21 11:38
Date:
08/18/2021 05:22 PM
Page 4 of 28
Page 55 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
QC Prep: V7514
QC Prep Batch Method: 5035 LOW
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V7514
Associated Lab Samples: 93306, 93307, 93308, 93309
QC Analytical Batch(es): V7515
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Matrix: SOL
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.0006
0.0006
0.005
08/11/21 11:38
Dichlorodifluoromethane
mg/Kg
<0.001
0.001
0.010
08/11/21 11:38
1,1-Dichloroethane
mg/Kg
<0.0008
0.0008
0.005
08/11/21 11:38
1,2-Dichloroethane
mg/Kg
<0.001
0.001
0.005
08/11/21 11:38
1,1-Dichloroethene
mg/Kg
<0.0007
0.0007
0.005
08/11/21 11:38
cis-1,2-Dichloroethene
mg/Kg
<0.0008
0.0008
0.005
08/11/21 11:38
trans-1,2-Dichloroethene
mg/Kg
<0.001
0.001
0.005
08/11/21 11:38
1,2-Dichloropropane
mg/Kg
<0.0004
0.0004
0.005
08/11/21 11:38
1,3-Dichloropropane
mg/Kg
<0.0006
0.0006
0.005
08/11/21 11:38
2,2-Dichloropropane
mg/Kg
<0.001
0.001
0.005
08/11/21 11:38
1,1-Dichloropropene
mg/Kg
<0.0008
0.0008
0.005
08/11/21 11:38
cis-1,3-Dichloropropene
mg/Kg
<0.0005
0.0005
0.005
08/11/21 11:38
trans-1,3-Dichloropropene
mg/Kg
<0.0008
0.0008
0.005
08/11/21 11:38
Ethylbenzene
mg/Kg
<0.0006
0.0006
0.005
08/11/21 11:38
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
<0.0008
0.0008
0.050
08/11/21 11:38
Hexachlorobutadiene
mg/Kg
<0.0008
0.0008
0.010
08/11/21 11:38
n-Hexane
mg/Kg
<0.0007
0.0007
0.010
08/11/21 11:38
2-Hexanone
mg/Kg
<0.0006
0.0006
0.020
08/11/21 11:38
Isopropyl benzene
mg/Kg
<0.0005
0.0005
0.005
08/11/21 11:38
4-Isopropyl toluene
mg/Kg
<0.001
0.001
0.005
08/11/21 11:38
Methyl Ethyl Ketone (MEK)
mg/Kg
<0.0007
0.0007
0.020
08/11/21 11:38
Methyl tert-butyl ether (MTBE)
mg/Kg
<0.0006
0.0006
0.005
08/11/21 11:38
4-Methyl-2-Pentanone
mg/Kg
<0.015
0.015
0.020
08/11/21 11:38
Methylene Chloride
mg/Kg
<0.001
0.001
0.010
08/11/21 11:38
Naphthalene
mg/Kg
<0.0010
0.0010
0.010
08/11/21 11:38
n-Propylbenzene
mg/Kg
<0.0005
0.0005
0.005
08/11/21 11:38
Styrene
mg/Kg
<0.001
0.001
0.005
08/11/21 11:38
Date:
08/18/2021 05:22 PM
Page 5 of 28
Page 56 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
QC Prep: V7514
QC Prep Batch Method: 5035 LOW
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank
LRB-V7514
Associated Lab Samples:
93306, 93307, 93308,
93309
Blank
MDL
Parameter
Units
Result
1,1,1,2-Tetrachloroethane
mg/Kg
<0.001
0.001
1,1,2,2-Tetrachloroethane
mg/Kg
<0.0003
0.0003
Tetrachloroethene
mg/Kg
<0.0009
0.0009
Toluene
mg/Kg
<0.0007
0.0007
1,2,3-Trichlorobenzene
mg/Kg
<0.0005
0.0005
1,2,4-Trichlorobenzene
mg/Kg
<0.0006
0.0006
1,1,1-Trichloroethane
mg/Kg
<0.001
0.001
1,1,2-Trichloroethane
mg/Kg
<0.0005
0.0005
Trichloroethene
mg/Kg
<0.0009
0.0009
Trichlorofluoromethane
mg/Kg
<0.002
0.002
1,2,3-Trichloropropane
mg/Kg
<0.0007
0.0007
1,2,4-Trimethyl benzene
mg/Kg
<0.0005
0.0005
1,3,5-Trimethyl benzene
mg/Kg
<0.0005
0.0005
Vinyl Acetate
mg/Kg
<0.0005
0.0005
Vinyl Chloride
mg/Kg
<0.0005
0.0005
o-Xylene
mg/Kg
<0.0005
0.0005
m,p-Xylene
mg/Kg
<0.001
0.001
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
QC Analytical Batch(es): V7515
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Matrix: SOL
MQL Analyzed % % Rec
Recovery Limits
0.005
08/11/21
11:38
0.005
08/11/21
11:38
0.005
08/11/21
11:38
0.005
08/11/21
11:38
0.010
08/11/21
11:38
0.010
08/11/21
11:38
0.005
08/11/21
11:38
0.005
08/11/21
11:38
0.005
08/11/21
11:38
0.010
08/11/21
11:38
0.005
08/11/21
11:38
0.005
08/11/21
11:38
0.005
08/11/21
11:38
0.010
08/11/21
11:38
0.010
08/11/21
11:38
0.005
08/11/21
11:38
0.010
08/11/21
11:38
08/11/21
11:38 98.8 70-130
08/11/21
11:38 99.2 84-123
08/11/21
11:38 97.2 76-129
Laboratory Control Sample & LCSD LCS-V7514 LCSD-V7514
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits
Acetone mg/Kg 0.100 0.087 0.087 87.6 87.3 29-198
Acrolein mg/Kg 0.100 0.111 0.109 111 109 70-130
RPD Max
RPD
0.3 20
1.8 20
Date: 08/18/2021 05:22 PM
Page 57 of 81
Page 6 of 28

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7514 QC Analytical Batch(es): V7515
QC Prep Batch Method: 5035 LOW Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V7514 LCSD-V7514
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Acrylonitrile
mg/Kg
0.100
0.111
0.111
111
111
65-134
0.0
20
Benzene
mg/Kg
0.050
0.049
0.046
99.4
92.6
74-127
7.0
20
Bromobenzene
mg/Kg
0.050
0.047
0.045
94.4
91.2
73-125
3.4
20
Bromochloromethane
mg/Kg
0.050
0.049
0.045
98.6
91.8
72-134
7.1
20
Bromodichloromethane
mg/Kg
0.050
0.050
0.046
100
93.8
75-122
6.3
20
Bromoform
mg/Kg
0.050
0.050
0.050
102
101
66-135
0.9
20
Bromomethane
mg/Kg
0.050
0.044
0.043
89.2
86.4
20-180
3.1
20
n-Butylbenzene
mg/Kg
0.050
0.048
0.045
97.8
90.2
65-135
8.0
20
sec -Butyl benzene
mg/Kg
0.050
0.048
0.044
96.6
89.0
66-131
8.1
20
tert-Butyl benzene
mg/Kg
0.050
0.047
0.044
94.8
88.6
67-132
6.7
20
Carbon Disulfide
mg/Kg
0.050
0.048
0.043
96.0
87.8
61-129
8.9
20
Carbon Tetrachloride
mg/Kg
0.050
0.047
0.044
95.6
88.6
64-143
7.6
20
Chlorobenzene
mg/Kg
0.050
0.048
0.045
97.2
91.4
74-118
6.1
20
Chlorodibromomethane
mg/Kg
0.050
0.049
0.048
99.2
96.6
73-122
2.6
20
Chloroethane
mg/Kg
0.050
0.043
0.039
86.6
78.6
33-149
9.6
20
Chloroform
mg/Kg
0.050
0.047
0.045
95.8
91.0
73-127
5.1
20
Chloromethane
mg/Kg
0.050
0.049
0.046
98.8
92.4
45-143
6.6
20
2-Chlorotoluene
mg/Kg
0.050
0.047
0.045
95.6
90.0
67-124
6.0
20
4-Chlorotoluene
mg/Kg
0.050
0.047
0.045
95.6
90.0
71-126
6.0
20
Di -Isopropyl Ether (DIPE)
mg/Kg
0.050
0.050
0.048
101
96.6
59-159
4.8
20
1,2-Dibromo-3-Chloropropane
mg/Kg
0.050
0.050
0.049
101
99.6
55-157
1.5
20
1,2-Dibromoethane
mg/Kg
0.050
0.049
0.048
98.6
96.8
70-132
1.8
20
Dibromomethane
mg/Kg
0.050
0.049
0.048
99.2
97.4
74-133
1.8
20
1,2-Dichlorobenzene
mg/Kg
0.050
0.047
0.045
94.2
90.6
72-123
3.8
20
1,3-Dichlorobenzene
mg/Kg
0.050
0.047
0.044
94.6
89.6
71-120
5.4
20
1,4-Dichlorobenzene
mg/Kg
0.050
0.047
0.045
94.6
91.0
71-123
3.8
20
Date: 08/18/2021 05:22 PM Page 7 of 28
Page 58 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7514 QC Analytical Batch(es): V7515
QC Prep Batch Method: 5035 LOW Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V7514 LCSD-V7514
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Dichlorodifluoromethane
mg/Kg
0.050
0.047
0.041
94.6
83.2
26-146
12.8
20
1,1-Dichloroethane
mg/Kg
0.050
0.049
0.046
99.2
92.8
74-127
6.6
20
1,2-Dichloroethane
mg/Kg
0.050
0.048
0.047
97.8
94.8
68-128
3.1
20
1,1-Dichloroethene
mg/Kg
0.050
0.048
0.044
97.4
89.2
67-149
8.7
20
cis-1,2-Dichloroethene
mg/Kg
0.050
0.049
0.046
98.4
93.2
76-134
5.4
20
trans-1,2-Dichloroethene
mg/Kg
0.050
0.049
0.045
98.6
90.0
73-132
9.1
20
1,2-Dichloropropane
mg/Kg
0.050
0.049
0.047
99.2
94.8
73-130
4.5
20
1,3-Dichloropropane
mg/Kg
0.050
0.049
0.047
98.4
94.6
75-124
3.9
20
2,2-Dichloropropane
mg/Kg
0.050
0.048
0.044
96.4
88.4
50-142
8.6
20
1,1-Dichloropropene
mg/Kg
0.050
0.049
0.044
98.2
89.2
71-130
9.6
20
cis-1,3-Dichloropropene
mg/Kg
0.050
0.050
0.048
100
96.0
71-125
4.0
20
trans-1,3-Dichloropropene
mg/Kg
0.050
0.051
0.049
103
99.0
68-123
3.7
20
Ethylbenzene
mg/Kg
0.050
0.048
0.045
97.4
90.6
74-128
7.2
20
Ethyl Tertiary Butyl Ether (ETBE)
mg/Kg
0.100
0.102
0.099
102
99.7
70-130
2.2
20
Hexachlorobutadiene
mg/Kg
0.050
0.047
0.044
95.0
88.4
64-125
7.1
20
n-Hexane
mg/Kg
0.050
0.051
0.045
104
90.0
70-130
14.0
20
2-Hexanone
mg/Kg
0.050
0.053
0.053
107
108
61-157
0.9
20
Isopropyl benzene
mg/Kg
0.050
0.048
0.044
96.0
88.8
68-126
7.7
20
4-Isopropyl toluene
mg/Kg
0.050
0.048
0.045
97.4
90.4
68-129
7.4
20
Methyl Ethyl Ketone (MEK)
mg/Kg
0.050
0.034
0.034
69.4
69.0
63-149
0.5
20
Methyl tert-butyl ether (MTBE)
mg/Kg
0.050
0.050
0.049
101
98.4
70-130
3.0
20
4-Methyl-2-Pentanone
mg/Kg
0.050
0.054
0.054
109
110
57-162
0.9
20
Methylene Chloride
mg/Kg
0.050
0.043
0.041
87.6
83.8
74-129
4.4
20
Naphthalene
mg/Kg
0.050
0.049
0.049
98.6
98.6
57-157
0.0
20
n-Propylbenzene
mg/Kg
0.050
0.049
0.045
98.2
91.4
67-130
7.1
20
Styrene
mg/Kg
0.050
0.049
0.046
98.8
93.2
77-121
5.8
20
Date: 08/18/2021 05:22 PM Page 8 of 28
Page 59 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7514 QC Analytical Batch(es): V7515
QC Prep Batch Method: 5035 LOW Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-V7514 LCSD-V7514
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD
1,1,1,2-Tetrachloroethane
mg/Kg
0.050
0.049
0.046
98.0
93.4
72-115
4.8
1,1,2,2-Tetrachloroethane
mg/Kg
0.050
0.050
0.049
101
98.2
56-126
2.6
Tetrachloroethene
mg/Kg
0.050
0.047
0.045
95.8
90.4
68-130
5.8
Toluene
mg/Kg
0.050
0.049
0.046
98.2
92.8
71-129
5.6
1,2,3-Trichlorobenzene
mg/Kg
0.050
0.047
0.046
94.4
92.8
68-130
1.7
1,2,4-Trichlorobenzene
mg/Kg
0.050
0.048
0.045
96.2
91.8
66-125
4.6
1,1,1-Trichloroethane
mg/Kg
0.050
0.048
0.044
97.6
89.8
67-131
8.3
1,1,2-Trichloroethane
mg/Kg
0.050
0.049
0.047
99.2
95.6
70-133
3.6
Trichloroethene
mg/Kg
0.050
0.049
0.045
99.2
91.0
75-133
8.6
Trichlorofluoromethane
mg/Kg
0.050
0.047
0.043
95.8
86.8
44-146
9.8
1,2,3-Trichloropropane
mg/Kg
0.050
0.049
0.048
98.6
96.8
60-137
1.8
1,2,4-Trimethyl benzene
mg/Kg
0.050
0.047
0.045
95.8
90.4
69-129
5.8
1,3,5-Trimethylbenzene
mg/Kg
0.050
0.048
0.044
96.0
88.8
69-128
7.7
Vinyl Acetate
mg/Kg
0.050
0.057
0.054
115
108
85-161
6.0
Vinyl Chloride
mg/Kg
0.050
0.049
0.044
98.8
89.8
48-147
9.5
o-Xylene
mg/Kg
0.050
0.048
0.045
97.4
91.2
74-126
6.5
m,p-Xylene
mg/Kg
0.100
0.099
0.094
99.8
94.0
75-124
5.9
4-Bromofluorobenzene (S)
99.2
99.0
70-130
Dibromofluoromethane (S)
97.2
96.6
84-123
Toluene-d8 (S)
97.0
97.2
76-129
Max
RPD
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Date: 08/18/2021 05:22 PM Page 9 of 28
Page 60 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
QC Prep: V7552
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V7552
Associated Lab Samples: 93306, 93308, 93309
QC Analytical Batch(es): V7647
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix: SOL
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acenaphthene
mg/Kg
<0.116
0.116
0.660
08/12/21 18:39
Acenaphthylene
mg/Kg
<0.105
0.105
0.660
08/12/21 18:39
Aniline
mg/Kg
<0.152
0.152
0.660
08/12/21 18:39
Anthracene
mg/Kg
<0.143
0.143
0.660
08/12/21 18:39
Benzo(a)anthracene
mg/Kg
<0.139
0.139
0.660
08/12/21 18:39
Benzo(a)pyrene
mg/Kg
<0.147
0.147
0.660
08/12/21 18:39
Benzo(b)fluoranthene
mg/Kg
<0.146
0.146
0.660
08/12/21 18:39
Benzo(g,h,i)perylene
mg/Kg
<0.136
0.136
0.660
08/12/21 18:39
Benzo(k)fluoranthene
mg/Kg
<0.137
0.137
0.660
08/12/21 18:39
Benzoic Acid
mg/Kg
<0.580
0.580
2.00
08/12/21 18:39
Benzyl alcohol
mg/Kg
<0.105
0.105
0.660
08/12/21 18:39
Bis(2-Chloroethoxy)methane
mg/Kg
<0.118
0.118
0.660
08/12/21 18:39
Bis(2-Chloroethyl)ether
mg/Kg
<0.107
0.107
0.660
08/12/21 18:39
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.136
0.136
0.330
08/12/21 18:39
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.120
0.120
0.660
08/12/21 18:39
4-Bromophenyl phenyl ether
mg/Kg
<0.109
0.109
0.660
08/12/21 18:39
Butyl benzyl phthalate
mg/Kg
<0.113
0.113
0.330
08/12/21 18:39
4-Chloro-3-methylphenol
mg/Kg
<0.092
0.092
0.660
08/12/21 18:39
4-Chloroaniline
mg/Kg
<0.112
0.112
0.330
08/12/21 18:39
2-Chloronaphthalene
mg/Kg
<0.116
0.116
0.660
08/12/21 18:39
2-Chlorophenol
mg/Kg
<0.098
0.098
0.660
08/12/21 18:39
4-Chlorophenyl phenyl ether
mg/Kg
<0.126
0.126
1.00
08/12/21 18:39
Chrysene
mg/Kg
<0.142
0.142
0.660
08/12/21 18:39
Dibenz(a,h)anth racene
mg/Kg
<0.230
0.230
0.660
08/12/21 18:39
Dibenzofuran
mg/Kg
<0.119
0.119
0.660
08/12/21 18:39
1,2-Dichlorobenzene
mg/Kg
<0.094
0.094
0.660
08/12/21 18:39
1,3-Dichlorobenzene
mg/Kg
<0.097
0.097
0.660
08/12/21 18:39
Date:
08/18/2021 05:22 PM
Page 10 of 28
Page 61 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
QC Prep: V7552
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-V7552
Associated Lab Samples: 93306, 93308, 93309
QC Analytical Batch(es): V7647
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix: SOL
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.097
0.097
0.330
08/12/21 18:39
3,3'-Dichlorobenzidine
mg/Kg
<0.147
0.147
0.660
08/12/21 18:39
2,4-Dichlorophenol
mg/Kg
<0.095
0.095
0.660
08/12/21 18:39
Diethyl phthalate
mg/Kg
<0.180
0.180
0.660
08/12/21 18:39
Dimethyl phthalate
mg/Kg
<0.174
0.174
0.660
08/12/21 18:39
2,4-Dimethylphenol
mg/Kg
<0.108
0.108
0.330
08/12/21 18:39
Di-n-butyl phthalate
mg/Kg
<0.107
0.107
0.660
08/12/21 18:39
4,6- Din itro-2-methylphenol
mg/Kg
<0.240
0.240
1.50
08/12/21 18:39
2,4-Dinitrophenol
mg/Kg
<0.520
0.520
1.50
08/12/21 18:39
2,4-Dinitrotoluene
mg/Kg
<0.096
0.096
0.660
08/12/21 18:39
2,6-Dinitrotoluene
mg/Kg
<0.108
0.108
0.660
08/12/21 18:39
Di-n-Octyl Phthalate
mg/Kg
<0.143
0.143
0.330
08/12/21 18:39
Fluoranthene
mg/Kg
<0.123
0.123
0.660
08/12/21 18:39
Fluorene
mg/Kg
<0.128
0.128
0.660
08/12/21 18:39
Hexachlorobenzene
mg/Kg
<0.106
0.106
0.660
08/12/21 18:39
Hexachlorobutadiene
mg/Kg
<0.097
0.097
0.660
08/12/21 18:39
Hexachlorocyclopentadiene
mg/Kg
<0.157
0.157
0.660
08/12/21 18:39
Hexachloroethane
mg/Kg
<0.079
0.079
0.660
08/12/21 18:39
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.179
0.179
0.660
08/12/21 18:39
Isophorone
mg/Kg
<0.191
0.191
0.660
08/12/21 18:39
1-Methylnaphthalene
mg/Kg
<0.106
0.106
0.660
08/12/21 18:39
2-Methylnaphthalene
mg/Kg
<0.100
0.100
0.660
08/12/21 18:39
2-Methylphenol
mg/Kg
<0.097
0.097
0.660
08/12/21 18:39
3&4 Methylphenol
mg/Kg
<0.084
0.084
0.660
08/12/21 18:39
Naphthalene
mg/Kg
<0.144
0.144
0.660
08/12/21 18:39
2-Nitroaniline
mg/Kg
<0.096
0.096
0.660
08/12/21 18:39
3-Nitroaniline
mg/Kg
<0.120
0.120
0.660
08/12/21 18:39
Date:
08/18/2021 05:22 PM
Page 11 of 28
Page 62 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep:
V7552
QC Analytical Batch(es): V7647
QC Prep Batch Method:
3546
Analysis Method:
8270E
Analysis Description:
Semivolatile Organic Compounds -
GC/MS
Lab Reagent Blank
LRB-V7552
Matrix: SOL
Associated Lab Samples:
93306, 93308, 93309
Blank
MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
4-Nitroaniline
mg/Kg
<0.093
0.093
0.330
08/12/21 18:39
Nitrobenzene
mg/Kg
<0.116
0.116
0.330
08/12/21 18:39
2-Nitrophenol
mg/Kg
<0.088
0.088
0.660
08/12/21 18:39
4-Nitrophenol
mg/Kg
<0.117
0.117
0.660
08/12/21 18:39
N-Nitrosodimethylamine
mg/Kg
<0.263
0.263
0.660
08/12/21 18:39
N-Nitrosodiphenylamine
mg/Kg
<0.181
0.181
0.660
08/12/21 18:39
N-Nitroso-di-n-propylamine
mg/Kg
<0.118
0.118
0.660
08/12/21 18:39
Pentachlorophenol
mg/Kg
<0.347
0.347
1.00
08/12/21 18:39
Phenanthrene
mg/Kg
<0.208
0.208
0.660
08/12/21 18:39
Phenol
mg/Kg
<0.112
0.112
0.660
08/12/21 18:39
Pyrene
mg/Kg
<0.134
0.134
0.660
08/12/21 18:39
Pyridine
mg/Kg
<0.079
0.079
0.330
08/12/21 18:39
1,2,4-Trichlorobenzene
mg/Kg
<0.107
0.107
0.660
08/12/21 18:39
2,4,5-Trichlorophenol
mg/Kg
<0.096
0.096
0.660
08/12/21 18:39
2,4,6-Trichlorophenol
mg/Kg
<0.096
0.096
0.660
08/12/21 18:39
2-Fluorobiphenyl (S)
08/12/21 18:39
86.2
44-115
2-Fluorophenol (S)
08/12/21 18:39
87.9
35-115
Nitrobenzene-d5 (S)
08/12/21 18:39
81.4
37-122
4-Terphenyl-d14 (S)
08/12/21 18:39
94.0
54-127
2,4,6-Tribromophenol (S)
08/12/21 18:39
88.5
39-132
Phenol-d5 (S)
08/12/21 18:39
87.3
34-121
Laboratory Control Sample LCS-V7552
Spike
Parameter Units Conc.
LCS LCS %Rec % Rec
Result Limits
Acenaphthene mg/Kg 1.67 1.46 87.4 40-123
Acenaphthylene mg/Kg 1.67 1.55 92.8 32-132
Date: 08/18/2021 05:22 PM Page 12 of 28
Page 63 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7552 QC Analytical Batch(es): V7647
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V7552
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Aniline
mg/Kg
1.67
1.39
83.2
12-197
Anthracene
mg/Kg
1.67
1.55
92.8
47-123
Benzo(a)anthracene
mg/Kg
1.67
1.51
90.4
49-126
Benzo(a)pyrene
mg/Kg
1.67
1.69
101
45-129
Benzo(b)fluoranthene
mg/Kg
1.67
1.59
95.2
45-132
Benzo(g,h,i)perylene
mg/Kg
1.67
1.48
88.6
43-134
Benzo(k)fluoranthene
mg/Kg
1.67
1.42
85.0
47-132
Benzoic Acid
mg/Kg
1.67
1.31
0.0*
10-83
Benzyl alcohol
mg/Kg
1.67
1.43
85.6
29-122
Bis(2-Chloroethoxy)methane
mg/Kg
1.67
1.60
95.8
36-121
Bis(2-Chloroethyl)ether
mg/Kg
1.67
1.34
80.2
31-120
Bis(2-Chloroisopropyl)ether
mg/Kg
1.67
1.40
83.8
33-131
Bis(2-ethylhexyl)phthalate
mg/Kg
1.67
1.72
103
51-133
4-Bromophenyl phenyl ether
mg/Kg
1.67
1.46
87.4
46-124
Butyl benzyl phthalate
mg/Kg
1.67
1.63
97.6
48-132
4-Chloro-3-methylphenol
mg/Kg
1.67
1.66
99.4
45-122
4-Chloroaniline
mg/Kg
1.67
1.40
83.8
17-106
2-Chloronaphthalene
mg/Kg
1.67
1.43
85.6
41-114
2-Chlorophenol
mg/Kg
1.67
1.45
86.8
34-121
4-Chlorophenyl phenyl ether
mg/Kg
1.67
1.51
90.4
45-121
Chrysene
mg/Kg
1.67
1.55
92.8
50-124
Dibenz(a,h)anthracene
mg/Kg
1.67
1.38
82.6
45-134
Dibenzofuran
mg/Kg
1.67
1.47
88.0
44-120
1,2-Dichlorobenzene
mg/Kg
1.67
1.31
78.4
33-117
1,3-Dichlorobenzene
mg/Kg
1.67
1.28
76.6
30-115
1,4-Dichlorobenzene
mg/Kg
1.67
1.28
76.6
31-115
3,3'-Dichlorobenzidine
mg/Kg
1.67
1.42
85.0
22-121
* QC Fail Date: 08/18/2021 05:22 PM Page 13 of 28
Page 64 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7552 QC Analytical Batch(es): V7647
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V7552
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
2,4-Dichlorophenol
mg/Kg
1.67
1.60
95.8
40-122
Diethyl phthalate
mg/Kg
1.67
1.57
94.0
50-124
Dimethyl phthalate
mg/Kg
1.67
1.49
89.2
48-124
2,4-Dimethylphenol
mg/Kg
1.67
1.61
96.4
30-127
Di-n-butyl phthalate
mg/Kg
1.67
1.73
104
51-128
4,6- Din itro-2-methylphenol
mg/Kg
1.67
1.39
0.0*
29-132
2,4-Dinitrophenol
mg/Kg
1.67
1.36
0.0*
27-129
2,4-Dinitrotoluene
mg/Kg
1.67
1.60
95.8
48-126
2,6-Dinitrotoluene
mg/Kg
1.67
1.59
95.2
46-124
Di-n-Octyl Phthalate
mg/Kg
1.67
1.63
97.6
45-140
Fluoranthene
mg/Kg
1.67
1.55
92.8
50-127
Fluorene
mg/Kg
1.67
1.55
92.8
43-125
Hexachlorobenzene
mg/Kg
1.67
1.49
89.2
45-122
Hexachlorobutadiene
mg/Kg
1.67
1.36
81.4
32-123
Hexachlorocyclopentadiene
mg/Kg
1.67
1.04
62.2
32-117
Hexachloroethane
mg/Kg
1.67
1.27
76.0
28-117
Indeno(1,2,3-cd)pyrene
mg/Kg
1.67
1.46
87.4
45-133
Isophorone
mg/Kg
1.67
1.26
75.4
30-122
1-Methylnaphthalene
mg/Kg
1.67
1.44
86.2
40-119
2-Methylnaphthalene
mg/Kg
1.67
1.44
86.2
38-122
2-Methylphenol
mg/Kg
1.67
1.54
92.2
32-122
3&4 Methylphenol
mg/Kg
1.67
1.35
80.8
34-119
Naphthalene
mg/Kg
1.67
1.40
83.8
35-123
2-Nitroaniline
mg/Kg
1.67
1.56
93.4
44-127
3-Nitroaniline
mg/Kg
1.67
1.52
91.0
33-119
4-Nitroaniline
mg/Kg
1.67
1.61
96.4
63-147
Nitrobenzene
mg/Kg
1.67
1.37
82.0
34-122
* QC Fail Date: 08/18/2021 05:22 PM Page 14 of 28
Page 65 of 81

Waypointo
ANALYTICAL
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-222-0026
QC Prep: V7552
QC Prep Batch Method: 3546
Laboratory Control Sample
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
LCS-V7552
QC Analytical Batch(es): V7647
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
2-Nitrophenol
mg/Kg
1.67
1.40
83.8
36-123
4-Nitrophenol
mg/Kg
1.67
1.80
108
30-132
N-Nitrosodimethylamine
mg/Kg
1.67
1.15
68.8
10-146
N-Nitrosodiphenylamine
mg/Kg
1.67
1.81
108
38-127
N-Nitroso-di-n-propylamine
mg/Kg
1.67
1.36
81.4
36-120
Pentachlorophenol
mg/Kg
1.67
1.56
93.4
25-133
Phenanthrene
mg/Kg
1.67
1.56
93.4
50-121
Phenol
mg/Kg
1.67
1.44
86.2
34-121
Pyrene
mg/Kg
1.67
1.62
97.0
47-127
Pyridine
mg/Kg
1.67
0.934
55.9
10-80
1,2,4-Trichlorobenzene
mg/Kg
1.67
1.35
80.8
34-118
2,4,5-Trichlorophenol
mg/Kg
1.67
1.47
88.0
41-124
2,4,6-Trichlorophenol
mg/Kg
1.67
1.51
90.4
39-126
2-Fluorobiphenyl (S)
85.0
44-115
2-Fluorophenol (S)
88.8
35-115
Nitrobenzene-d5 (S)
80.8
37-122
4-Terphenyl-d14 (S)
93.4
54-127
2,4,6-Tribromophenol (S)
94.8
39-132
Phenol-d5 (S)
85.5
34-121
Matrix Spike & Matrix Spike Duplicate
V 93140-MS-V7552
V 93140-MSD-V7552
MS Spike
MSD
MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Acenaphthene
mg/Kg
<0.116
1.66
1.66
1.38
1.29
83.1
77.7
40-123
6.7
20
Acenaphthylene
mg/Kg
<0.105
1.66
1.66
1.45
1.37
87.3
82.5
32-132
5.6
20
Aniline
mg/Kg
<0.152
1.66
1.66
1.23
1.24
74.0
74.6
12-197
0.8
20
Date: 08/18/2021 05:22 PM Page 15 of 28
Page 66 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7552 QC Analytical Batch(es): V7647
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 93140-MS-V7552 V 93140-MSD-V7552
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Anthracene
mg/Kg
<0.143
1.66
1.66
1.40
1.32
84.3
79.5
47-123
5.8
20
Benzo(a)anthracene
mg/Kg
<0.139
1.66
1.66
1.41
1.30
84.9
78.3
49-126
8.1
20
Benzo(a)pyrene
mg/Kg
<0.147
1.66
1.66
1.57
1.43
94.5
86.1
45-129
9.3
20
Benzo(b)fluoranthene
mg/Kg
<0.146
1.66
1.66
1.45
1.39
87.3
83.7
45-132
4.2
20
Benzo(g,h,i)perylene
mg/Kg
<0.136
1.66
1.66
1.35
1.25
81.3
75.3
43-134
7.6
20
Benzo(k)fluoranthene
mg/Kg
<0.137
1.66
1.66
1.31
1.20
78.9
72.2
47-132
8.7
20
Benzoic Acid
mg/Kg
<0.580
1.66
1.66
0.832
1.00
0.0*
0.0*
10-83
0.0
20
Benzyl alcohol
mg/Kg
<0.105
1.66
1.66
1.37
1.32
82.5
79.5
29-122
3.7
20
Bis(2-Chloroethoxy)methane
mg/Kg
<0.118
1.66
1.66
1.43
1.38
86.1
83.1
36-121
3.5
20
Bis(2-Chloroethyl)ether
mg/Kg
<0.107
1.66
1.66
1.16
1.12
69.8
67.4
31-120
3.5
20
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.136
1.66
1.66
1.26
1.23
75.9
74.0
33-131
2.4
20
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.120
1.66
1.66
1.62
1.47
97.5
88.5
51-133
9.7
20
4-Bromophenyl phenyl ether
mg/Kg
<0.109
1.66
1.66
1.34
1.24
80.7
74.6
46-124
7.7
20
Butyl benzyl phthalate
mg/Kg
<0.113
1.66
1.66
1.52
1.39
91.5
83.7
48-132
8.9
20
4-Chloro-3-methyl phenol
mg/Kg
<0.092
1.66
1.66
1.44
1.34
86.7
80.7
45-122
7.1
20
4-Chloroaniline
mg/Kg
<0.112
1.66
1.66
1.14
1.14
68.6
68.6
17-106
0.0
20
2-Chloronaphthalene
mg/Kg
<0.116
1.66
1.66
1.37
1.29
82.5
77.7
41-114
6.0
20
2-Chlorophenol
mg/Kg
<0.098
1.66
1.66
1.36
1.32
81.9
79.5
34-121
2.9
20
4-Chlorophenyl phenyl ether
mg/Kg
<0.126
1.66
1.66
1.42
1.30
85.5
78.3
45-121
8.8
20
Chrysene
mg/Kg
<0.142
1.66
1.66
1.42
1.32
85.5
79.5
50-124
7.2
20
Dibenz(a,h)anth racene
mg/Kg
<0.230
1.66
1.66
1.24
1.15
74.6
69.2
45-134
7.5
20
Dibenzofuran
mg/Kg
<0.119
1.66
1.66
1.40
1.31
84.3
78.9
44-120
6.6
20
1,2-Dichlorobenzene
mg/Kg
<0.094
1.66
1.66
1.20
1.16
72.2
69.8
33-117
3.3
20
1,3-Dichlorobenzene
mg/Kg
<0.097
1.66
1.66
1.17
1.14
70.4
68.6
30-115
2.5
20
1,4-Dichlorobenzene
mg/Kg
<0.097
1.66
1.66
1.15
1.11
69.2
66.8
31-115
3.5
20
3,3'-Dichlorobenzidine
mg/Kg
<0.147
1.66
1.66
1.25
1.18
75.3
71.0
22-121
5.7
20
* QC Fail Date: 08/18/2021 05:22 PM Page 16 of 28
Page 67 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7552 QC Analytical Batch(es): V7647
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 93140-MS-V7552 V 93140-MSD-V7552
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
2,4-Dichlorophenol
mg/Kg
<0.095
1.66
1.66
1.41
1.32
84.9
79.5
40-122
6.5
20
Diethyl phthalate
mg/Kg
<0.180
1.66
1.66
1.45
1.32
87.3
79.5
50-124
9.3
20
Dimethyl phthalate
mg/Kg
<0.174
1.66
1.66
1.39
1.29
83.7
77.7
48-124
7.4
30
2,4-Dimethylphenol
mg/Kg
<0.108
1.66
1.66
1.49
1.38
89.7
83.1
30-127
7.6
20
Di-n-butyl phthalate
mg/Kg
<0.107
1.66
1.66
1.54
1.46
92.7
87.9
51-128
5.3
20
4,6- Din itro-2-methylphenol
mg/Kg
<0.240
1.66
1.66
<0.240
<0.240
0.0*
0.0*
29-132
0.0
20
2,4-Dinitrophenol
mg/Kg
<0.520
1.66
1.66
<0.520
<0.520
0.0*
0.0*
27-129
0.0
20
2,4-Dinitrotoluene
mg/Kg
<0.096
1.66
1.66
1.45
1.33
87.3
80.1
48-126
8.6
20
2,6-Dinitrotoluene
mg/Kg
<0.108
1.66
1.66
1.46
1.35
87.9
81.3
46-124
7.8
20
Di-n-Octyl Phthalate
mg/Kg
<0.143
1.66
1.66
1.83
1.71
110
103
45-140
6.7
20
Fluoranthene
mg/Kg
<0.123
1.66
1.66
1.45
1.35
87.3
81.3
50-127
7.1
20
Fluorene
mg/Kg
<0.128
1.66
1.66
1.44
1.34
86.7
80.7
43-125
7.1
20
Hexachlorobenzene
mg/Kg
<0.106
1.66
1.66
1.35
1.27
81.3
76.5
45-122
6.1
20
Hexachlorobutadiene
mg/Kg
<0.097
1.66
1.66
1.22
1.19
73.4
71.6
32-123
2.4
20
Hexachlorocyclopentadiene
mg/Kg
<0.157
1.66
1.66
0.588
0.529
0.0*
0.0*
32-117
0.0
20
Hexachloroethane
mg/Kg
<0.079
1.66
1.66
1.16
1.14
69.8
68.6
28-117
1.7
20
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.179
1.66
1.66
1.36
1.26
81.9
75.9
45-133
7.6
20
Isophorone
mg/Kg
<0.191
1.66
1.66
1.11
1.05
66.8
63.2
30-122
5.5
20
1-Methylnaphthalene
mg/Kg
<0.106
1.66
1.66
1.27
1.23
76.5
74.0
40-119
3.2
20
2-Methylnaphthalene
mg/Kg
<0.100
1.66
1.66
1.30
1.24
78.3
74.6
38-122
4.7
20
2-Methylphenol
mg/Kg
<0.097
1.66
1.66
1.40
1.36
84.3
81.9
32-122
2.8
20
3&4 Methylphenol
mg/Kg
<0.084
1.66
1.66
1.23
1.19
74.0
71.6
34-119
3.3
20
Naphthalene
mg/Kg
<0.144
1.66
1.66
1.26
1.21
75.9
72.8
35-123
4.0
20
2-Nitroaniline
mg/Kg
<0.096
1.66
1.66
1.47
1.36
88.5
81.9
44-127
7.7
20
3-Nitroaniline
mg/Kg
<0.120
1.66
1.66
1.40
1.29
84.3
77.7
33-119
8.1
20
4-Nitroaniline
mg/Kg
<0.093
1.66
1.66
1.40
1.25
84.3
75.3
63-147
11.3
20
* QC Fail Date: 08/18/2021 05:22 PM Page 17 of 28
Page 68 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7552 QC Analytical Batch(es): V7647
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 93140-MS-V7552 V 93140-MSD-V7552
MS Spike MSD MS Result MSD MS MSD %Rec Max
Parameter Units Result Conc. Spike Result a/oRec %Rec Limits RPD RPD
Conc.
Nitrobenzene
mg/Kg
<0.116
1.66
1.66
1.20
1.18
72.2
71.0
34-122
2-Nitrophenol
mg/Kg
<0.088
1.66
1.66
1.23
1.17
74.0
70.4
32-123
4-Nitrophenol
mg/Kg
<0.117
1.66
1.66
1.51
1.41
90.9
84.9
30-132
N-Nitrosodimethylamine
mg/Kg
<0.263
1.66
1.66
1.00
0.977
60.2
58.8
10-146
N-Nitrosodiphenylamine
mg/Kg
<0.181
1.66
1.66
1.67
1.55
101
93.3
38-127
N-Nitroso-di-n-propylamine
mg/Kg
<0.118
1.66
1.66
1.28
1.21
77.1
72.8
36-120
Pentachlorophenol
mg/Kg
<0.347
1.66
1.66
1.15
1.08
69.2
65.0
25-133
Phenanthrene
mg/Kg
<0.208
1.66
1.66
1.42
1.33
85.5
80.1
50-121
Phenol
mg/Kg
<0.112
1.66
1.66
1.36
1.32
81.9
79.5
34-121
Pyrene
mg/Kg
<0.134
1.66
1.66
1.51
1.41
90.9
84.9
47-127
Pyridine
mg/Kg
<0.079
1.66
1.66
0.794
0.788
47.8
47.4
10-80
1,2,4-Trichlorobenzene
mg/Kg
<0.107
1.66
1.66
1.18
1.15
71.0
69.2
34-118
2,4,5-Trichlorophenol
mg/Kg
<0.096
1.66
1.66
1.36
1.26
81.9
75.9
41-124
2,4,6-Trichlorophenol
mg/Kg
<0.096
1.66
1.66
1.41
1.31
84.9
78.9
39-126
2-Fluorobiphenyl (S)
80.1
75.3
44-115
2-Fluorophenol (S)
82.5
78.9
35-115
Nitrobenzene-d5 (S)
72.2
69.2
37-122
4-Terphenyl-d14 (S)
85.5
78.9
54-127
2,4,6-Tribromophenol (S)
85.5
78.0
39-132
Phenol-d5(S)
79.2
75.6
34-121
1.6
5.0
6.8
2.3
7.4
5.6
6.2
6.5
2.9
6.8
0.7
2.5
7.6
7.3
20
20
20
30
20
20
20
20
20
20
20
20
20
20
Date: 08/18/2021 05:22 PM Page 18 of 28
Page 69 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
QC Prep: V7702
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V7735
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V7702 Matrix: SOL
Associated Lab Samples: 93307
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acenaphthene
mg/Kg
<0.116
0.116
0.660
08/17/21 14:59
Acenaphthylene
mg/Kg
<0.105
0.105
0.660
08/17/21 14:59
Aniline
mg/Kg
<0.152
0.152
0.660
08/17/21 14:59
Anthracene
mg/Kg
<0.143
0.143
0.660
08/17/21 14:59
Benzo(a)anthracene
mg/Kg
<0.139
0.139
0.660
08/17/21 14:59
Benzo(a)pyrene
mg/Kg
<0.147
0.147
0.660
08/17/21 14:59
Benzo(b)fluoranthene
mg/Kg
<0.146
0.146
0.660
08/17/21 14:59
Benzo(g,h,i)perylene
mg/Kg
<0.136
0.136
0.660
08/17/21 14:59
Benzo(k)fluoranthene
mg/Kg
<0.137
0.137
0.660
08/17/21 14:59
Benzoic Acid
mg/Kg
<0.580
0.580
2.00
08/17/21 14:59
Benzyl alcohol
mg/Kg
<0.105
0.105
0.660
08/17/21 14:59
Bis(2-Chloroethoxy)methane
mg/Kg
<0.118
0.118
0.660
08/17/21 14:59
Bis(2-Chloroethyl)ether
mg/Kg
<0.107
0.107
0.660
08/17/21 14:59
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.136
0.136
0.330
08/17/21 14:59
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.120
0.120
0.660
08/17/21 14:59
4-Bromophenyl phenyl ether
mg/Kg
<0.109
0.109
0.660
08/17/21 14:59
Butyl benzyl phthalate
mg/Kg
<0.113
0.113
0.330
08/17/21 14:59
4-Chloro-3-methylphenol
mg/Kg
<0.092
0.092
0.660
08/17/21 14:59
4-Chloroaniline
mg/Kg
<0.112
0.112
0.330
08/17/21 14:59
2-Chloronaphthalene
mg/Kg
<0.116
0.116
0.660
08/17/21 14:59
2-Chlorophenol
mg/Kg
<0.098
0.098
0.660
08/17/21 14:59
4-Chlorophenyl phenyl ether
mg/Kg
<0.126
0.126
1.00
08/17/21 14:59
Chrysene
mg/Kg
<0.142
0.142
0.660
08/17/21 14:59
Dibenz(a,h)anth racene
mg/Kg
<0.230
0.230
0.660
08/17/21 14:59
Dibenzofuran
mg/Kg
<0.119
0.119
0.660
08/17/21 14:59
1,2-Dichlorobenzene
mg/Kg
<0.094
0.094
0.660
08/17/21 14:59
1,3-Dichlorobenzene
mg/Kg
<0.097
0.097
0.660
08/17/21 14:59
Date:
08/18/2021 05:22 PM
Page 19 of 28
Page 70 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
QC Prep: V7702
QC Prep Batch Method: 3546
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): V7735
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-V7702 Matrix: SOL
Associated Lab Samples: 93307
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,4-Dichlorobenzene
mg/Kg
<0.097
0.097
0.330
08/17/21 14:59
3,3'-Dichlorobenzidine
mg/Kg
<0.147
0.147
0.660
08/17/21 14:59
2,4-Dichlorophenol
mg/Kg
<0.095
0.095
0.660
08/17/21 14:59
Diethyl phthalate
mg/Kg
<0.180
0.180
0.660
08/17/21 14:59
Dimethyl phthalate
mg/Kg
<0.174
0.174
0.660
08/17/21 14:59
2,4-Dimethylphenol
mg/Kg
<0.108
0.108
0.330
08/17/21 14:59
Di-n-butyl phthalate
mg/Kg
<0.107
0.107
0.660
08/17/21 14:59
4,6- Din itro-2-methylphenol
mg/Kg
<0.240
0.240
1.50
08/17/21 14:59
2,4-Dinitrophenol
mg/Kg
<0.520
0.520
1.50
08/17/21 14:59
2,4-Dinitrotoluene
mg/Kg
<0.096
0.096
0.660
08/17/21 14:59
2,6-Dinitrotoluene
mg/Kg
<0.108
0.108
0.660
08/17/21 14:59
Di-n-Octyl Phthalate
mg/Kg
<0.143
0.143
0.330
08/17/21 14:59
Fluoranthene
mg/Kg
<0.123
0.123
0.660
08/17/21 14:59
Fluorene
mg/Kg
<0.128
0.128
0.660
08/17/21 14:59
Hexachlorobenzene
mg/Kg
<0.106
0.106
0.660
08/17/21 14:59
Hexachlorobutadiene
mg/Kg
<0.097
0.097
0.660
08/17/21 14:59
Hexachlorocyclopentadiene
mg/Kg
<0.157
0.157
0.660
08/17/21 14:59
Hexachloroethane
mg/Kg
<0.079
0.079
0.660
08/17/21 14:59
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.179
0.179
0.660
08/17/21 14:59
Isophorone
mg/Kg
<0.191
0.191
0.660
08/17/21 14:59
1-Methylnaphthalene
mg/Kg
<0.106
0.106
0.660
08/17/21 14:59
2-Methylnaphthalene
mg/Kg
<0.100
0.100
0.660
08/17/21 14:59
2-Methylphenol
mg/Kg
<0.097
0.097
0.660
08/17/21 14:59
3&4 Methylphenol
mg/Kg
<0.084
0.084
0.660
08/17/21 14:59
Naphthalene
mg/Kg
<0.144
0.144
0.660
08/17/21 14:59
2-Nitroaniline
mg/Kg
<0.096
0.096
0.660
08/17/21 14:59
3-Nitroaniline
mg/Kg
<0.120
0.120
0.660
08/17/21 14:59
Date:
08/18/2021 05:22 PM
Page 20 of 28
Page 71 of 81

Waypointo
ANALYTICAL
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7702
QC Prep Batch Method: 3546
QC Analytical Batch(es): V7735
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank
LRB-V7702
Matrix: SOL
Associated Lab Samples: 93307
Blank
MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
4-Nitroaniline
mg/Kg
<0.093
0.093
0.330
08/17/21 14:59
Nitrobenzene
mg/Kg
<0.116
0.116
0.330
08/17/21 14:59
2-Nitrophenol
mg/Kg
<0.088
0.088
0.660
08/17/21 14:59
4-Nitrophenol
mg/Kg
<0.117
0.117
0.660
08/17/21 14:59
N-Nitrosodimethylamine
mg/Kg
<0.263
0.263
0.660
08/17/21 14:59
N-Nitrosodiphenylamine
mg/Kg
<0.181
0.181
0.660
08/17/21 14:59
N-Nitroso-di-n-propylamine
mg/Kg
<0.118
0.118
0.660
08/17/21 14:59
Pentachlorophenol
mg/Kg
<0.347
0.347
1.00
08/17/21 14:59
Phenanthrene
mg/Kg
<0.208
0.208
0.660
08/17/21 14:59
Phenol
mg/Kg
<0.112
0.112
0.660
08/17/21 14:59
Pyrene
mg/Kg
<0.134
0.134
0.660
08/17/21 14:59
Pyridine
mg/Kg
<0.079
0.079
0.330
08/17/21 14:59
1,2,4-Trichlorobenzene
mg/Kg
<0.107
0.107
0.660
08/17/21 14:59
2,4,5-Trichlorophenol
mg/Kg
<0.096
0.096
0.660
08/17/21 14:59
2,4,6-Trichlorophenol
mg/Kg
<0.096
0.096
0.660
08/17/21 14:59
2-Fluorobiphenyl(S)
08/17/21 14:59
89.8
44-115
2-Fluorophenol(S)
08/17/21 14:59
88.5
35-115
Nitrobenzene-d5 (S)
08/17/21 14:59
81.4
37-122
4-Terphenyl-d14 (S)
08/17/21 14:59
104
54-127
2,4,6-Tribromophenol (S)
08/17/21 14:59
98.7
39-132
Phenol-d5 (S)
08/17/21 14:59
84.6
34-121
Laboratory Control Sample
Parameter
LCS-V7702
Spike
Units Conc.
LCS LCS %Rec % Rec
Result Limits
Acenaphthene mg/Kg 1.67 1.34 80.2 40-123
Acenaphthylene mg/Kg 1.67 1.41 84.4 32-132
Date: 08/18/2021 05:22 PM
Page 72 of 81
Page 21 of 28

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7702 QC Analytical Batch(es): V7735
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V7702
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Aniline
mg/Kg
1.67
1.28
76.6
12-197
Anthracene
mg/Kg
1.67
1.40
83.8
47-123
Benzo(a)anthracene
mg/Kg
1.67
1.40
83.8
49-126
Benzo(a)pyrene
mg/Kg
1.67
2.11
126
45-129
Benzo(b)fluoranthene
mg/Kg
1.67
1.96
117
45-132
Benzo(g,h,i)perylene
mg/Kg
1.67
1.85
111
43-134
Benzo(k)fluoranthene
mg/Kg
1.67
1.75
105
47-132
Benzoic Acid
mg/Kg
1.67
1.23
0.0*
10-83
Benzyl alcohol
mg/Kg
1.67
1.27
76.0
29-122
Bis(2-Chloroethoxy)methane
mg/Kg
1.67
1.44
86.2
36-121
Bis(2-Chloroethyl)ether
mg/Kg
1.67
1.02
61.0
31-120
Bis(2-Chloroisopropyl)ether
mg/Kg
1.67
1.22
73.0
33-131
Bis(2-ethylhexyl)phthalate
mg/Kg
1.67
1.65
98.8
51-133
4-Bromophenyl phenyl ether
mg/Kg
1.67
1.37
82.0
46-124
Butyl benzyl phthalate
mg/Kg
1.67
1.53
91.6
48-132
4-Chloro-3-methyl phenol
mg/Kg
1.67
1.43
85.6
45-122
4-Chloroaniline
mg/Kg
1.67
1.17
70.0
17-106
2-Chloronaphthalene
mg/Kg
1.67
1.32
79.0
41-114
2-Chlorophenol
mg/Kg
1.67
1.29
77.2
34-121
4-Chlorophenyl phenyl ether
mg/Kg
1.67
1.40
83.8
45-121
Chrysene
mg/Kg
1.67
1.46
87.4
50-124
Dibenz(a,h)anthracene
mg/Kg
1.67
1.31
78.4
45-134
Dibenzofuran
mg/Kg
1.67
1.37
82.0
44-120
1,2-Dichlorobenzene
mg/Kg
1.67
1.15
68.8
33-117
1,3-Dichlorobenzene
mg/Kg
1.67
1.15
68.8
30-115
1,4-Dichlorobenzene
mg/Kg
1.67
1.12
67.0
31-115
3,3'-Dichlorobenzidine
mg/Kg
1.67
1.20
71.8
22-121
* QC Fail Date: 08/18/2021 05:22 PM Page 22 of 28
Page 73 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7702 QC Analytical Batch(es): V7735
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-V7702
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
2,4-Dichlorophenol
mg/Kg
1.67
1.41
84.4
40-122
Diethyl phthalate
mg/Kg
1.67
1.45
86.8
50-124
Dimethyl phthalate
mg/Kg
1.67
1.37
82.0
48-124
2,4-Dimethylphenol
mg/Kg
1.67
1.40
83.8
30-127
Di-n-butyl phthalate
mg/Kg
1.67
1.60
95.8
51-128
4,6- Din itro-2-methylphenol
mg/Kg
1.67
1.31
0.0*
29-132
2,4-Dinitrophenol
mg/Kg
1.67
1.26
0.0*
27-129
2,4-Dinitrotoluene
mg/Kg
1.67
1.45
86.8
48-126
2,6-Dinitrotoluene
mg/Kg
1.67
1.46
87.4
46-124
Di-n-Octyl Phthalate
mg/Kg
1.67
2.03
122
45-140
Fluoranthene
mg/Kg
1.67
1.44
86.2
50-127
Fluorene
mg/Kg
1.67
1.41
84.4
43-125
Hexachlorobenzene
mg/Kg
1.67
1.38
82.6
45-122
Hexachlorobutadiene
mg/Kg
1.67
1.27
76.0
32-123
Hexachlorocyclopentadiene
mg/Kg
1.67
0.969
58.0
32-117
Hexachloroethane
mg/Kg
1.67
1.12
67.0
28-117
Indeno(1,2,3-cd)pyrene
mg/Kg
1.67
1.80
108
45-133
Isophorone
mg/Kg
1.67
1.09
65.2
30-122
1-Methylnaphthalene
mg/Kg
1.67
1.27
76.0
40-119
2-Methylnaphthalene
mg/Kg
1.67
1.29
77.2
38-122
2-Methylphenol
mg/Kg
1.67
1.30
77.8
32-122
3&4 Methylphenol
mg/Kg
1.67
1.15
68.8
34-119
Naphthalene
mg/Kg
1.67
1.24
74.2
35-123
2-Nitroaniline
mg/Kg
1.67
1.44
86.2
44-127
3-Nitroaniline
mg/Kg
1.67
1.31
78.4
33-119
4-Nitroaniline
mg/Kg
1.67
1.40
83.8
63-147
Nitrobenzene
mg/Kg
1.67
1.22
73.0
34-122
* QC Fail Date: 08/18/2021 05:22 PM Page 23 of 28
Page 74 of 81

Waypointo
ANALYTICAL
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-222-0026
QC Prep: V7702
QC Prep Batch Method: 3546
Laboratory Control Sample
Parameter
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
N-N itroso-d i-n-propyl a m i ne
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
4-Terphenyl-d14 (S)
2,4,6-Tribromophenol (S)
Phenol-d5 (S)
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
LCS-V7702
Spike
Units Conc.
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
mg/Kg 1.67
QC Analytical Batch(es): V7735
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
LCS
Result
1.31
1.84
0.835
1.66
1.20
1.40
1.44
1.27
1.48
0.729
1.19
1.36
1.38
LCS %Rec
78.4
110
50.0
99.4
71.8
83.8
86.2
76.0
88.6
43.6
71.2
81.4
82.6
80.8
80.1
73.0
90.4
90.9
77.1
Rec
Limits
36-123
30-132
10-146
38-127
36-120
25-133
50-121
34-121
47-127
10-80
34-118
41-124
39-126
44-115
35-115
37-122
54-127
39-132
34-121
Matrix Spike & Matrix Spike Duplicate
V 92884-MS-V7702
V 92884-MSD-V7702
MS Spike
MSD
MS Result
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Spike
Result
%Rec
%Rec
Limits
RPD
RPD
Conc.
Acenaphthene
mg/Kg
<0.117
1.69
1.67
1.42
1.28
84.0
76.6
40-123
10.3
20
Acenaphthylene
mg/Kg
<0.106
1.69
1.67
1.45
1.29
85.7
77.2
32-132
11.6
20
Aniline
mg/Kg
<0.154
1.69
1.67
0.745
0.820
44.0
49.1
12-197
9.5
20
Date: 08/18/2021 05:22 PM Page 24 of 28
Page 75 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7702 QC Analytical Batch(es): V7735
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 92884-MS-V7702 V 92884-MSD-V7702
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Anthracene
mg/Kg
<0.145
1.69
1.67
1.52
1.36
89.9
81.4
47-123
11.1
20
Benzo(a)anthracene
mg/Kg
<0.141
1.69
1.67
1.45
1.34
85.7
80.2
49-126
7.8
20
Benzo(a)pyrene
mg/Kg
<0.149
1.69
1.67
2.14
1.97
127
118
45-129
8.2
20
Benzo(b)fluoranthene
mg/Kg
<0.148
1.69
1.67
1.95
1.82
115
109
45-132
6.8
20
Benzo(g,h,i)perylene
mg/Kg
<0.138
1.69
1.67
1.87
1.74
111
104
43-134
7.2
20
Benzo(k)fluoranthene
mg/Kg
<0.139
1.69
1.67
1.83
1.71
108
102
47-132
6.7
20
Benzoic Acid
mg/Kg
<0.589
1.69
1.67
1.84
1.65
0.0*
0.0*
10-83
0.0
20
Benzyl alcohol
mg/Kg
<0.106
1.69
1.67
1.28
1.22
75.7
73.0
29-122
4.8
20
Bis(2-Chloroethoxy)methane
mg/Kg
<0.119
1.69
1.67
1.44
1.34
85.2
80.2
36-121
7.1
20
Bis(2-Chloroethyl)ether
mg/Kg
<0.108
1.69
1.67
1.25
1.05
73.9
62.8
31-120
17.3
20
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.138
1.69
1.67
1.23
1.16
72.7
69.4
33-131
5.8
20
Bis(2-ethylhexyl)phthalate
mg/Kg
<0.121
1.69
1.67
1.69
1.57
100
94.0
51-133
7.3
20
4-Bromophenyl phenyl ether
mg/Kg
<0.110
1.69
1.67
1.44
1.31
85.2
78.4
46-124
9.4
20
Butyl benzyl phthalate
mg/Kg
<0.114
1.69
1.67
1.52
1.40
89.9
83.8
48-132
8.2
20
4-Chloro-3-methyl phenol
mg/Kg
<0.093
1.69
1.67
1.43
1.33
84.6
79.6
45-122
7.2
20
4-Chloroaniline
mg/Kg
<0.113
1.69
1.67
1.09
1.04
64.4
62.2
17-106
4.6
20
2-Chloronaphthalene
mg/Kg
<0.117
1.69
1.67
1.39
1.24
82.2
74.2
41-114
11.4
20
2-Chlorophenol
mg/Kg
<0.099
1.69
1.67
1.29
1.22
76.3
73.0
34-121
5.5
20
4-Chlorophenyl phenyl ether
mg/Kg
<0.127
1.69
1.67
1.45
1.29
85.7
77.2
45-121
11.6
20
Chrysene
mg/Kg
<0.144
1.69
1.67
1.47
1.37
86.9
82.0
50-124
7.0
20
Dibenz(a,h)anth racene
mg/Kg
<0.233
1.69
1.67
1.34
1.25
79.2
74.8
45-134
6.9
20
Dibenzofuran
mg/Kg
<0.120
1.69
1.67
1.41
1.29
83.4
77.2
44-120
8.8
20
1,2-Dichlorobenzene
mg/Kg
<0.095
1.69
1.67
1.19
1.12
70.4
67.0
33-117
6.0
20
1,3-Dichlorobenzene
mg/Kg
<0.098
1.69
1.67
1.15
1.08
68.0
64.6
30-115
6.2
20
1,4-Dichlorobenzene
mg/Kg
<0.098
1.69
1.67
1.13
1.06
66.8
63.4
31-115
6.3
20
3,3'-Dichlorobenzidine
mg/Kg
<0.149
1.69
1.67
1.04
0.950
61.5
56.8
22-121
9.0
20
* QC Fail Date: 08/18/2021 05:22 PM Page 25 of 28
Page 76 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7702 QC Analytical Batch(es): V7735
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 92884-MS-V7702 V 92884-MSD-V7702
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
2,4-Dichlorophenol
mg/Kg
<0.097
1.69
1.67
1.39
1.29
82.2
77.2
40-122
7.4
20
Diethyl phthalate
mg/Kg
<0.182
1.69
1.67
1.49
1.30
88.1
77.8
50-124
13.6
20
Dimethyl phthalate
mg/Kg
<0.176
1.69
1.67
1.41
1.26
83.4
75.4
48-124
11.2
30
2,4-Dimethylphenol
mg/Kg
<0.109
1.69
1.67
1.47
1.38
86.9
82.6
30-127
6.3
20
Di-n-butyl phthalate
mg/Kg
<0.108
1.69
1.67
1.67
1.56
98.8
93.4
51-128
6.8
20
4,6- Din itro-2-methylphenol
mg/Kg
<0.243
1.69
1.67
1.38
1.24
0.0*
0.0*
29-132
0.0
20
2,4-Dinitrophenol
mg/Kg
<0.527
1.69
1.67
1.42
1.31
0.0*
0.0*
27-129
0.0
20
2,4-Dinitrotoluene
mg/Kg
<0.097
1.69
1.67
1.48
1.35
87.5
80.8
48-126
9.1
20
2,6-Dinitrotoluene
mg/Kg
<0.109
1.69
1.67
1.49
1.35
88.1
80.8
46-124
9.8
20
Di-n-Octyl Phthalate
mg/Kg
<0.145
1.69
1.67
2.10
1.91
124
114
45-140
9.4
20
Fluoranthene
mg/Kg
<0.124
1.69
1.67
1.52
1.37
89.9
82.0
50-127
10.3
20
Fluorene
mg/Kg
<0.130
1.69
1.67
1.47
1.31
86.9
78.4
43-125
11.5
20
Hexachlorobenzene
mg/Kg
<0.107
1.69
1.67
1.48
1.33
87.5
79.6
45-122
10.6
20
Hexachlorobutadiene
mg/Kg
<0.098
1.69
1.67
1.27
1.18
75.1
70.6
32-123
7.3
20
Hexachlorocyclopentadiene
mg/Kg
<0.159
1.69
1.67
1.08
0.979
63.9
58.6
32-117
9.8
20
Hexachloroethane
mg/Kg
<0.080
1.69
1.67
1.17
1.09
69.2
65.2
28-117
7.0
20
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.181
1.69
1.67
1.79
1.68
106
101
45-133
6.3
20
Isophorone
mg/Kg
<0.193
1.69
1.67
1.08
1.03
63.9
61.6
30-122
4.7
20
1-Methylnaphthalene
mg/Kg
<0.107
1.69
1.67
1.28
1.21
75.7
72.4
40-119
5.6
20
2-Methylnaphthalene
mg/Kg
<0.101
1.69
1.67
1.30
1.20
76.9
71.8
38-122
8.0
20
2-Methylphenol
mg/Kg
<0.098
1.69
1.67
1.33
1.28
78.6
76.6
32-122
3.8
20
3&4 Methylphenol
mg/Kg
<0.085
1.69
1.67
1.18
1.10
69.8
65.8
34-119
7.0
20
Naphthalene
mg/Kg
<0.146
1.69
1.67
1.26
1.19
74.5
71.2
35-123
5.7
20
2-Nitroaniline
mg/Kg
<0.097
1.69
1.67
1.50
1.35
88.7
80.8
44-127
10.5
20
3-Nitroaniline
mg/Kg
<0.121
1.69
1.67
1.38
1.23
81.6
73.6
33-119
11.4
20
4-Nitroaniline
mg/Kg
<0.094
1.69
1.67
1.42
1.19
84.0
71.2
63-147
17.6
20
* QC Fail Date: 08/18/2021 05:22 PM Page 26 of 28
Page 77 of 81

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
F&R, Inc. - Charlotte
RA Eden
21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Prep: V7702 QC Analytical Batch(es): V7735
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix Spike & Matrix Spike Duplicate V 92884-MS-V7702 V 92884-MSD-V7702
Parameter
Units
Result
MS Spike
Conc.
MSD
Spike
Conc.
MS Result
MSD
Result
MS
a/oRec
MSD
%Rec
%Rec
Limits
RPD
Max
RPD
Nitrobenzene
mg/Kg
<0.117
1.69
1.67
1.23
1.14
72.7
68.2
34-122
7.5
20
2-Nitrophenol
mg/Kg
<0.089
1.69
1.67
1.25
1.18
73.9
70.6
32-123
5.7
20
4-Nitrophenol
mg/Kg
<0.118
1.69
1.67
2.11
1.55
125
92.8
30-132
30.6*
20
N-Nitrosodimethylamine
mg/Kg
<0.266
1.69
1.67
1.05
0.986
62.1
59.0
10-146
6.2
30
N-Nitrosodiphenylamine
mg/Kg
<0.183
1.69
1.67
1.79
1.62
106
97.0
38-127
9.9
20
N-Nitroso-di-n-propylamine
mg/Kg
<0.119
1.69
1.67
1.21
1.16
71.5
69.4
36-120
4.2
20
Pentachlorophenol
mg/Kg
<0.350
1.69
1.67
1.57
1.44
92.8
86.2
25-133
8.6
20
Phenanthrene
mg/Kg
<0.211
1.69
1.67
1.52
1.37
89.9
82.0
50-121
10.3
20
Phenol
mg/Kg
<0.113
1.69
1.67
1.24
1.18
73.3
70.6
34-121
4.9
20
Pyrene
mg/Kg
<0.136
1.69
1.67
1.50
1.40
88.7
83.8
47-127
6.8
20
Pyridine
mg/Kg
<0.080
1.69
1.67
0.186
0.177
0.0*
0.0*
10-80
0.0
20
1,2,4-Trichlorobenzene
mg/Kg
<0.108
1.69
1.67
1.22
1.14
72.1
68.2
34-118
6.7
20
2,4,5-Trichlorophenol
mg/Kg
<0.097
1.69
1.67
1.41
1.24
83.4
74.2
41-124
12.8
20
2,4,6-Trichlorophenol
mg/Kg
<0.097
1.69
1.67
1.47
1.31
86.9
78.4
39-126
11.5
20
2-Fluorobiphenyl (S)
80.4
74.8
44-115
2-Fluorophenol (S)
78.6
75.3
35-115
Nitrobenzene-d5 (S)
71.0
68.2
37-122
4-Terphenyl-d14 (S)
87.5
82.0
54-127
2,4,6-Tribromophenol (S)
91.7
82.8
39-132
Phenol-d5(S)
75.1
72.0
34-121
* QC Fail Date: 08/18/2021 05:22 PM Page 27 of 28
Page 78 of 81

Waypointo
ANALYTICAL
Client ID: F&R, Inc. - Charlotte
Project Description: RA Eden
Report No: 21-222-0026
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch: V7556
Analysis Method: SW-DRYWT
Analysis Description: Dry Weight Determination
Duplicate V 92912-DUP
Result DUP
Parameter Units Result
Moisture % 22.3 21.7
Duplicate V 93180-DUP
RPD Max RPD Analyzed
2.7 20.0 08/12/21 17:20
Result DUP RPD Max RPD Analyzed
Parameter Units Result
Moisture % 18.0 17.6 2.2 20.0 08/12/2117:20
Date: 08/18/2021 05:22 PM Page 28 of 28
Page 79 of 81

WayPAoint.
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 00019
Customer Name: F&R, Inc. - Charlotte
Report Number: 21-222-0026
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IRT-15 5.2 C
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample Iabel(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
U Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
U Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
CO,) N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No 0 N/A
F Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
0Yes ONo
Signature: Angela D Overcash
Date & Time: 08/10/2021 15:36:17
Page 80 of 81

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Page 81 of 81