23057_CharlotteVan&Storage_Soil Export Options SP-2 Package_20210915

September 15, 2021
Sent Via E-mail
Mr. Jeffrey W. Harris
Lennar Multifamily Communities, LLC 500 East Morehead Street, Suite 300 Charlotte, North Carolina 28202 [e-mail]

Subject: Brownfields Soil Management Options for SP-2 Charlotte Van & Storage Co. Brownfield Property Charlotte, Mecklenburg County Brownfields Project No. 23057-19-060

Dear Mr. Harris: The North Carolina Department of Environmental Quality (DEQ) Brownfields Program received a request to export soil from the Charlotte Van & Storage Co. Brownfields Property. This request
was submitted on your behalf by Ms. Haley Martin, PG of Hart & Hickman, PC via email on
September 14, 2021, and requests approval to export approximately 900 cubic yards of stockpiled soil from grubbing and stripping activities to a beneficial fill reuse site known as Fleet Maintenance facility in Mt. Holly, North Carolina. On September 7, 2021, DEQ Brownfields provided a letter approving soil export options for areas identified as EX-1 through EX-6 and SP-1, and the current
request is to export stockpiled soil identified as SP-2.
For this request, DEQ Brownfields reviewed the September 14, 2021, Data Summary Package which includes analytical results for soil samples collected at SP-2, as well as summaries of the previous soil analytical data from the Brownfields Property and the proposed Fleet Maintenance
receiving facility.
Based on our review of the data, the DEQ Brownfield determines that soils may be exported as outlined in the table below. Please note that the “Beneficial Fill” option listed in the table below is specifically approved for the Fleet Maintenance facility in Mt. Holly, NC. Other Beneficial
Fill and Land Clearing & Inert Debris Landfill (LCID) options may be available; however, DEQ
requires that the receiving facility be identified and approved prior to export. The receiving facility should have metals concentrations which are consistent with those from the Brownfields Property. Similarly, many site soils, including those with impacts, may be suitable for use at another Brownfields Property that has similar impacts.
Mr. Jeffery Harris September 15, 2021 Page 2

Upon determination of the export facility, whether another Brownfields Property, LCID, or
another beneficial fill reuse, please contact us and we will assist you in determining if additional sampling is needed for the receiving facility.
LOCATION ID DEPTH (Ft)1 MANAGEMENT OPTIONS2
SP-2 stockpile BFILL, LCID, CDLF, MSWLF
Notes: 1) Depth listed is total depth of available analytical data. Additional sampling would potentially be required beyond these depths prior to export.
2) BFILL= Beneficial Fill; LCID = Land Clearing & Inert Debris Landfill; CDLF = Construction & Demolition landfill; MSWLF = Municipal Solid Waste landfill (MSWLF) facility.
Per the Charlotte Van & Storage Co.’s approved Environmental Management Plan (EMP), the soils will be field screened during excavation prior to export from the property. If unanticipated impacts are identified during excavation, please refer to the EMP for further actions and cease transfer until appropriate characterization can be completed. In addition, and also in accordance
with the site’s approved EMP, an annual Redevelopment Summary Report will be submitted to
DEQ Brownfields. Details related to the disposition of this soil including but not limited to, total volume, general description of field screening efforts, etc. should be included with the Redevelopment Summary Report.
Please be advised that this approval does not waive any applicable requirement to obtain any
necessary permits, licenses or certifications which may be required from other state or local entities. If you have questions about this correspondence or require additional information, please feel free to contact Pete Doorn by phone at 984-275-5391 or by email at [e-mail].
Sincerely,
Peter L. Doorn, Project Manager Brownfields Program
Ec: Haley Martin, Hart & Hickman, PC Ralph McGee, Hart & Hickman, PC Tracy Wahl, DEQ Brownfields
Table 1
Summary of Soil Analytical Data
Charlotte Van & Storage Co.
Verbena Street and Gilead Street
Charlotte, North Carolina
H&H Job No. LEN-008
Sample ID
Sample Type Composite Grab Composite Grab Composite Grab Composite Grab
Depth (ft bgs)0-2 0-1 0-2 0-1 0-2 0-1 0-2 0-1
Date Range Range Mean
Units
VOCs (8260D)
Acetone NA <0.057 NA <0.075 NA <0.050 NA <0.057 25 12,000 140,000 ------
2-Butanone NA <0.043 NA <0.056 NA <0.037 NA <0.043 17 5,500 40,000 ------
Ethanol NA NA NA NA NA NA NA NA NE NE NE ------
p-isopropyltoluene NA <0.0044 NA <0.0057 NA <0.0038 NA <0.0044 NE NE NE ------
Methylene Chloride NA <0.024 NA <0.032 NA <0.021 NA <0.024 0.025 58 650 ------
Naphthalene NA <0.0047 NA 0.019 NA <0.0041 NA <0.0047 0.39 2.1 8.8 ------
n-Propylbenzene NA <0.0032 NA <0.0041 NA <0.0028 NA 0.0085 J 2.6 780 5,100 ------
Toluene NA <0.0025 NA 0.038 NA <0.0022 NA <0.0025 8.3 990 9,700 ------
1,2,4-Trimethylbenzene NA <0.0024 NA 0.0076 J NA <0.0021 NA <0.0024 12 63 370 ------
Xylene (total) NA <0.0051 NA 0.0092 J NA <0.0044 NA <0.0051 9.9 120 530 ------
m&p-Xylene NA <0.0061 NA <0.0080 NA <0.0053 NA <0.0061 9.8 120 500 ------
o-Xylene NA <0.0039 NA 0.0092 J NA <0.0034 NA <0.0039 9.8 140 590 ------
SVOCs (8270E)
Anthracene <0.74 NA <0.14 NA <0.14 NA <0.67 NA 1,300 3,600 45,000 ------
Benzo(a)anthracene <0.76 NA <0.14 NA 0.19 J NA <0.68 NA 0.35 1.1 21 ------
Benzo(a)pyrene <0.78 NA <0.15 NA 0.18 J NA <0.71 NA 0.12 0.11 2.1 ------
Benzo(b)fluoranthene <0.76 NA <0.14 NA 0.28 J NA <0.68 NA 1.2 1.1 21 ------
Benzo(g,h,i)perylene <0.88 NA <0.17 NA <0.16 NA <0.80 NA NE NE NE ------
Benzo(k)fluoranthene <0.80 NA <0.15 NA <0.15 NA <0.72 NA 12 11 210 ------
Butylbenzylphthalate <0.96 NA 0.22 J NA <0.18 NA <0.86 NA 290 290 1,200 ------
Chrysene <0.83 NA <0.16 NA 0.19 J NA <0.75 NA 36 110 2,100 ------
Dibenz(a,h)anthracene <0.87 NA <0.17 NA <0.16 NA <0.79 NA 0.38 0.11 2.1 ------
Fluoranthene <0.78 NA <0.15 NA 0.39 J NA <0.70 NA 670 480 6,000 ------
Indeno(1,2,3-cd)pyrene <0.894 NA <0.17 NA <0.17 NA <0.81 NA 3.9 1.1 21 ------
Phenanthrene <0.74 NA <0.14 NA 0.19 J NA <0.67 NA NE NE NE ------
Pyrene <0.92 NA <0.18 NA 0.31 J NA <0.83 NA 440 360 4,500 ------
Metals (6020/7471/7199)
Arsenic 6.35 NA 2.39 NA 1.29 J NA 1.34 NA 5.8 0.68 3.0 1.28 - 3.03 1.0 - 18 4.8
Barium 50.1 NA 97.2 NA 55.3 NA 88.4 NA 580 3,100 47,000 38.1 - 94.6 50 - 1,000 356
Cadmium 0.209 J NA 0.484 J NA 0.124 J NA 0.344 J NA 3.0 14 200 ND - 0.434 1.0 - 10*4.3
Chromium (total)40.4 NA 33.6 NA 48.6 NA 26.6 NA ------47.1 - 59.9 7.0 - 300 65
Hexavalent Chromium 2.46 NA <0.366 NA 0.682 J NA <0.316 NA 3.8 0.31 6.5 ND - 0.540 NS NS
Trivalent Chromium 37.94 NA 33.6 NA 47.92 NA 26.6 NA 360,000 23,000 350,000 47.1 - 59.4 NS NS
Lead 14.3 NA 48.6 NA 14.7 NA 11.5 NA 270 400 800 7.33 - 11.6 ND - 50 16
Mercury 0.0464 J NA <0.0259 NA <0.0247 NA 0.0474 J NA NE 4.7 70 0.0365 - 0.0502 0.03 - 0.52 0.121
Selenium 0.878 J NA 0.596 J NA 0.716 J NA 0.550 J NA 2.1 78 1,200 0.586 - 1.04 <0.1 - 0.8 0.42
Silver <0.110 NA <0.124 NA <0.119 NA <0.107 NA 3.4 78 1,200 ND ND - 5.0 NS
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021)
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Background Cd and Ag concentrations were taken from Southeastern and Conterminous US soils.
Soil concentrations are reported in milligrams per kilogram (mg/kg).
Compound concentrations are reported to the laboratory method detection limits.
Aside from metals, only those compounds detected in at least one sample are shown above.
Laboratory analytical methods are shown in parentheses.
Shaded values exceed the Protection of Groundwater PSRG.
Bold values exceed the Residential PSRG.
Underlined values exceed the Industrial/Commercial PSRG.
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface
NS= not specified; NA = not analyzed; -- = not applicable; NE = not established; ND = not detected at concentration above laboratory detection limit
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
EX-2 EX-3 EX-4
Sample Location
Screening Criteria
Protection of
Groundwater
PSRGs (1)
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Site-Specific
Background
Metals
Background
Metals (2)
EX-1
mg/kg
Proposed Area of Cut
8/4/2021
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Lennar (LEN)/LEN-008 Verbena Assemblage/In Situ Assessment/Tables/Charlotte Van & Storage Co. (LEN-008) Data Tables aem.xlsx
9/14/2021
Table 1 (Page 1 of 2)
Hart & Hickman, PC
Table 1
Summary of Soil Analytical Data
Charlotte Van & Storage Co.
Verbena Street and Gilead Street
Charlotte, North Carolina
H&H Job No. LEN-008
Sample ID SB-1 SB-2 SB-3
Sample Type Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab
Depth (ft bgs)0-2 1-2 0-2 1-2 0-2 1-2
Date Range Range Mean
Units
VOCs (8260D)
Acetone NA <0.055 NA 1.1 NA 0.80 NA <0.0427 NA 0.017 J NA NA NA 25 12,000 140,000 ------
2-Butanone NA <0.041 NA <0.081 NA 0.15 J NA <0.0319 NA 0.002 J NA NA NA 17 5,500 40,000 ------
Ethanol NA NA NA NA NA NA NA NA NA 0.057 J NA NA NA NE NE NE ------
p-isopropyltoluene NA <0.0042 NA 0.27 NA 0.048 NA <0.0033 NA <0.001 NA NA NA NE NE NE ------
Methylene Chloride NA <0.024 NA <0.046 NA 0.13 NA <0.0182 NA <0.001 NA NA NA 0.025 58 650 ------
Naphthalene NA <0.0045 NA <0.0089 NA <0.0073 NA <0.0035 NA <0.001 NA NA NA 0.39 2.1 8.8 ------
n-Propylbenzene NA <0.0031 NA <0.0060 NA <0.0049 NA <0.0024 NA <0.0007 NA NA NA 2.6 780 5,100 ------
Toluene NA <0.0024 NA 0.011 J NA 0.010 J NA 0.0314 NA <0.0008 NA NA NA 8.3 990 9,700 ------
1,2,4-Trimethylbenzene NA <0.0024 NA <0.0046 NA 0.0074 J NA <0.0018 NA <0.0006 NA NA NA 12 63 370 ------
Xylene (total) NA <0.0049 NA <0.0097 NA 0.011 J NA 0.0072 J NA <0.0006 NA NA NA 9.9 120 530 ------
m&p-Xylene NA <0.0059 NA <0.012 NA 0.011 J NA 0.0072 J NA <0.001 NA NA NA 9.8 120 500 ------
o-Xylene NA <0.0038 NA <0.0075 NA <0.0061 NA <0.0029 NA <0.0006 NA NA NA 9.8 140 590 ------
SVOCs (8270E)
Anthracene <0.15 NA <0.15 NA 0.36 J NA <0.130 NA <0.172 NA NA NA NA 1,300 3,600 45,000 ------
Benzo(a)anthracene <0.16 NA <0.15 NA 2.4 NA <0.132 NA <0.172 NA NA NA NA 0.35 1.1 21 ------
Benzo(a)pyrene <0.16 NA <0.16 NA 2.4 NA <0.137 NA <0.182 NA NA NA NA 0.12 0.11 2.1 ------
Benzo(b)fluoranthene <0.16 NA 0.22 J NA 4.0 NA <0.132 NA <0.181 NA NA NA NA 1.2 1.1 21 ------
Benzo(g,h,i)perylene <0.18 NA <0.18 NA 2.0 NA <0.154 NA <0.168 NA NA NA NA NE NE NE ------
Benzo(k)fluoranthene <0.16 NA <0.16 NA 1.4 NA <0.139 NA <0.170 NA NA NA NA 12 11 210 ------
Butylbenzylphthalate <0.20 NA <0.19 NA <0.19 NA <0.167 NA <0.140 NA NA NA NA 290 290 1,200 ------
Chrysene <0.17 NA <0.17 NA 2.4 NA <0.144 NA <0.176 NA NA NA NA 36 110 2,100 ------
Dibenz(a,h)anthracene <0.18 NA <0.17 NA 0.52 NA <0.152 NA <0.285 NA NA NA NA 0.38 0.11 2.10 ------
Fluoranthene <0.16 NA 0.28 J NA 5.3 NA <0.136 NA <0.152 NA NA NA NA 670 480 6,000 ------
Indeno(1,2,3-cd)pyrene <0.18 NA <0.18 NA 1.8 NA <0.156 NA <0.222 NA NA NA NA 3.9 1.1 21 ------
Phenanthrene <0.15 NA <0.15 NA 2.1 NA <0.130 NA <0.285 NA NA NA NA NE NE NE ------
Pyrene <0.19 NA 0.22 J NA 4.0 NA <0.161 NA <0.166 NA NA NA NA 440 360 4,500 ------
Metals (6020/7471/7199)
Arsenic 1.33 NA 1.82 NA 0.985 J NA 0.978 J NA 2.40 NA 1.11 J 0.391 J 3.52 5.8 0.68 3.0 1.28 - 3.03 1.0 - 18 4.8
Barium 251 NA 226 NA 256 NA 96.0 NA 65.2 NA 66.2 44.3 68.7 580 3,100 47,000 38.1 - 94.6 50 - 1,000 356
Cadmium 0.295 J NA 0.970 J NA 0.391 J NA <0.109 NA <0.0683 NA <0.0655 <0.0649 0.207 J 3.0 14 200 ND - 0.434 1.0 - 10*4.3
Chromium (total)56.3 NA 29.8 NA 28.5 NA 60.0 NA 32.2 NA 80.8 30.9 25.7 ------47.1 - 59.9 7.0 - 300 65
Hexavalent Chromium 2.53 NA 0.640 J NA 0.763 J NA 3.65 NA <0.26 NA 1.3 <0.26 <0.26 3.8 0.31 6.5 ND - 0.540 NS NS
Trivalent Chromium 53.77 NA 29.16 NA 27.74 NA 56.35 NA 32.2 NA 79.5 30.9 25.7 360,000 23,000 350,000 47.1 - 59.4 NS NS
Lead 14.0 NA 34.2 NA 17.1 NA 6.37 NA 16.4 NA 6.13 6.3 10.3 270 400 800 7.33 - 11.6 ND - 50 16
Mercury 0.0484 J NA <0.0231 NA <0.0271 NA <0.0229 NA 0.0421 NA 0.0155 J <0.0142 <0.0156 NE 4.7 70 0.0365 - 0.0502 0.03 - 0.52 0.121
Selenium 0.651 J NA 0.308 J NA 0.402 J NA 0.458 J NA 1.24 J NA 10.8 J <1.06 <1.47 J 2.1 78 1,200 0.586 - 1.04 <0.1 - 0.8 0.42
Silver <0.109 NA 0.118 J NA <0.130 NA <0.110 NA <0.0509 NA <0.0488 <0.0484 <0.0534 3.4 78 1,200 ND ND - 5.0 NS
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021)
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Background Cd and Ag concentrations were taken from Southeastern and Conterminous US soils.
Soil concentrations are reported in milligrams per kilogram (mg/kg).
Compound concentrations are reported to the laboratory method detection limits.
Aside from metals, only those compounds detected in at least one sample are shown above.
Laboratory analytical methods are shown in parentheses.
Shaded values exceed the Protection of Groundwater PSRG.
Bold values exceed the Residential PSRG.
Underlined values exceed the Industrial/Commercial PSRG.
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface
NS= not specified; NA = not analyzed; -- = not applicable; NE = not established; ND = not detected at concentration above laboratory detection limit
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
1-3
SP-2
Stockpile
--
8/27/2021
Industrial/
Commercial
PSRGs (1)
Site-Specific
Background
Metals in Soil
Background
Metals (2)Protection of
Groundwater
PSRGs (1)
mg/kg
Residential
PSRGs (1)
Sample Location Fleet Maintenance Facility
Grab
8/27/2021
EX-6/DUP-01 SP-1EX-5
Proposed Area of Cut
8/4/2021
Screening Criteria
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Lennar (LEN)/LEN-008 Verbena Assemblage/In Situ Assessment/Tables/Charlotte Van & Storage Co. (LEN-008) Data Tables aem.xlsx
9/14/2021
Table 1 (Page 2 of 2)
Hart & Hickman, PC

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

9/3/2021
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 21-239-0018 Client Project Description: LEN-008
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 8/27/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 45
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-239-0018
Page 2 of 45
Report Number:
Sample Summary Table
Client Project Description:
21-239-0018
LEN-008
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
08/27/2021 12:30Solids 94457 SP-2 08/27/2021 13:00 7199
08/27/2021 12:30Solids 94457 SP-2 08/27/2021 13:00
: Pace Analytical - Columbia, SC (Shealy), West Columbia, SC
Page 3 of 45
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-239-0018
Report Limit
Project:LEN-008
V 94457SP-2
2.40 09/01/2021 21:146020BArsenicmg/Kg - dry 0.117
65.2 09/01/2021 21:146020BBariummg/Kg - dry 1.74
32.2 09/01/2021 21:146020BChromiummg/Kg - dry 0.360
16.4 09/01/2021 21:146020BLeadmg/Kg - dry 0.174
J1.24 09/01/2021 21:146020BSeleniummg/Kg - dry 1.12
0.0421 08/31/2021 15:377471BMercury (Total)mg/Kg - dry 0.0149
J0.017 08/30/2021 19:028260DAcetonemg/Kg - dry 0.002
J0.057 08/30/2021 19:028260DEthanolmg/Kg - dry 0.017
J0.002 08/30/2021 19:028260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
19.5 09/02/2021 11:10SW-DRYWT Moisture %
Page 4 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-239-0018
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 08/27/2021
LEN-008
Report Date : 09/03/2021
Sample ID :
Lab No :
Sampled:SP-2
94457 Matrix:
8/27/2021 12:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.5 %Moisture 1 09/02/21 11:10 SW-DRYWTBAM
2.40 mg/Kg - dry 0.117 1.24Arsenic 10 09/01/21 21:14 6020BEDV
65.2 mg/Kg - dry 1.74 12.4Barium 10 09/01/21 21:14 6020BEDV
<0.0683 mg/Kg - dry 0.0683 0.621Cadmium 10 09/01/21 21:14 6020BEDV
32.2 mg/Kg - dry 0.360 1.24Chromium 10 09/01/21 21:14 6020BEDV
16.4 mg/Kg - dry 0.174 1.24
Lead 10 09/01/21 21:14 6020BEDV
0.0421 mg/Kg - dry 0.0149 0.0373Mercury (Total)1 08/31/21 15:37 7471BEDV
1.24 J mg/Kg - dry 1.12 2.48Selenium 10 09/01/21 21:14 6020BEDV
<0.0509 mg/Kg - dry 0.0509 0.621Silver 10 09/01/21 21:14 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 5 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-239-0018
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 08/27/2021
LEN-008
Report Date : 09/03/2021
Sample ID :
Lab No :
Sampled:SP-2
94457 Matrix:
8/27/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8220 08/30/21 08:00
0.017 J mg/Kg - dry 0.002 0.024Acetone 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 08/30/21 19:02 V8221TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 08/30/21 19:02 V8221TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 08/30/21 19:02 V8221TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 08/30/21 19:02 V8221TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 08/30/21 19:02 V8221TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 08/30/21 19:02 V8221TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 08/30/21 19:02 V8221TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 08/30/21 19:02 V8221TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 08/30/21 19:02 V8221TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 08/30/21 19:02 V8221TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 08/30/21 19:02 V8221TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 08/30/21 19:02 V8221TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 08/30/21 19:02 V8221TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 08/30/21 19:02 V8221TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 08/30/21 19:02 V8221TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-239-0018
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 08/27/2021
LEN-008
Report Date : 09/03/2021
Sample ID :
Lab No :
Sampled:SP-2
94457 Matrix:
8/27/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8220 08/30/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 08/30/21 19:02 V8221TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 08/30/21 19:02 V8221TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 08/30/21 19:02 V8221TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 08/30/21 19:02 V8221TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 08/30/21 19:02 V8221TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 08/30/21 19:02 V8221TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 08/30/21 19:02 V8221TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 08/30/21 19:02 V8221TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 08/30/21 19:02 V8221TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 08/30/21 19:02 V8221TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 08/30/21 19:02 V8221TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 08/30/21 19:02 V8221TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 08/30/21 19:02 V8221TBL
0.057 J mg/Kg - dry 0.017 0.310Ethanol 1 08/30/21 19:02 V8221TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 08/30/21 19:02 V8221TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 08/30/21 19:02 V8221TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-239-0018
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 08/27/2021
LEN-008
Report Date : 09/03/2021
Sample ID :
Lab No :
Sampled:SP-2
94457 Matrix:
8/27/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8220 08/30/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 08/30/21 19:02 V8221TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 08/30/21 19:02 V8221TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 08/30/21 19:02 V8221TBL
0.002 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 08/30/21 19:02 V8221TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 08/30/21 19:02 V8221TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 08/30/21 19:02 V8221TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 08/30/21 19:02 V8221TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 08/30/21 19:02 V8221TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 08/30/21 19:02 V8221TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 08/30/21 19:02 V8221TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 08/30/21 19:02 V8221TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 08/30/21 19:02 V8221TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 08/30/21 19:02 V8221TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 08/30/21 19:02 V8221TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-239-0018
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 08/27/2021
LEN-008
Report Date : 09/03/2021
Sample ID :
Lab No :
Sampled:SP-2
94457 Matrix:
8/27/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V8220 08/30/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 08/30/21 19:02 V8221TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 08/30/21 19:02 V8221TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 08/30/21 19:02 V8221TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 08/30/21 19:02 V8221TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 08/30/21 19:02 V8221TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 08/30/21 19:02 V8221TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 08/30/21 19:02 V8221
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%08/30/21 19:021 TBL V8221
Surrogate: Dibromofluoromethane 109 Limits: 84-123%08/30/21 19:021 TBL V8221
Surrogate: Toluene-d8 121 Limits: 76-129%08/30/21 19:021 TBL V8221
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8207 08/30/21 12:00
<0.144 mg/Kg - dry 0.144 0.819Acenaphthene 1 08/31/21 17:25 V8269JMV
<0.130 mg/Kg - dry 0.130 0.819Acenaphthylene 1 08/31/21 17:25 V8269JMV
<0.188 mg/Kg - dry 0.188 0.819Aniline 1 08/31/21 17:25 V8269JMV
<0.177 mg/Kg - dry 0.177 0.819Anthracene 1 08/31/21 17:25 V8269JMV
<0.172 mg/Kg - dry 0.172 0.819
Benzo(a)anthracene 1 08/31/21 17:25 V8269JMV
<0.182 mg/Kg - dry 0.182 0.819Benzo(a)pyrene 1 08/31/21 17:25 V8269JMV
<0.181 mg/Kg - dry 0.181 0.819Benzo(b)fluoranthene 1 08/31/21 17:25 V8269JMV
<0.168 mg/Kg - dry 0.168 0.819Benzo(g,h,i)perylene 1 08/31/21 17:25 V8269JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-239-0018
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 08/27/2021
LEN-008
Report Date : 09/03/2021
Sample ID :
Lab No :
Sampled:SP-2
94457 Matrix:
8/27/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8207 08/30/21 12:00
<0.170 mg/Kg - dry 0.170 0.819Benzo(k)fluoranthene 1 08/31/21 17:25 V8269JMV
<0.720 mg/Kg - dry 0.720 2.48Benzoic Acid 1 08/31/21 17:25 V8269JMV
<0.130 mg/Kg - dry 0.130 0.819Benzyl alcohol 1 08/31/21 17:25 V8269JMV
<0.146 mg/Kg - dry 0.146 0.819Bis(2-Chloroethoxy)methane 1 08/31/21 17:25 V8269JMV
<0.132 mg/Kg - dry 0.132 0.819Bis(2-Chloroethyl)ether 1 08/31/21 17:25 V8269JMV
<0.168 mg/Kg - dry 0.168 0.409Bis(2-Chloroisopropyl)ether 1 08/31/21 17:25 V8269JMV
<0.149 mg/Kg - dry 0.149 0.819Bis(2-ethylhexyl)phthalate 1 08/31/21 17:25 V8269JMV
<0.135 mg/Kg - dry 0.135 0.8194-Bromophenyl phenyl ether 1 08/31/21 17:25 V8269JMV
<0.140 mg/Kg - dry 0.140 0.409
Butyl benzyl phthalate 1 08/31/21 17:25 V8269JMV
<0.114 mg/Kg - dry 0.114 0.8194-Chloro-3-methylphenol 1 08/31/21 17:25 V8269JMV
<0.139 mg/Kg - dry 0.139 0.4094-Chloroaniline 1 08/31/21 17:25 V8269JMV
<0.144 mg/Kg - dry 0.144 0.8192-Chloronaphthalene 1 08/31/21 17:25 V8269JMV
<0.121 mg/Kg - dry 0.121 0.8192-Chlorophenol 1 08/31/21 17:25 V8269JMV
<0.156 mg/Kg - dry 0.156 1.244-Chlorophenyl phenyl ether 1 08/31/21 17:25 V8269JMV
<0.176 mg/Kg - dry 0.176 0.819Chrysene 1 08/31/21 17:25 V8269JMV
<0.285 mg/Kg - dry 0.285 0.819
Dibenz(a,h)anthracene 1 08/31/21 17:25 V8269JMV
<0.147 mg/Kg - dry 0.147 0.819Dibenzofuran 1 08/31/21 17:25 V8269JMV
<0.117 mg/Kg - dry 0.117 0.8191,2-Dichlorobenzene 1 08/31/21 17:25 V8269JMV
<0.120 mg/Kg - dry 0.120 0.8191,3-Dichlorobenzene 1 08/31/21 17:25 V8269JMV
<0.121 mg/Kg - dry 0.121 0.4091,4-Dichlorobenzene 1 08/31/21 17:25 V8269JMV
<0.182 mg/Kg - dry 0.182 0.8193,3'-Dichlorobenzidine 1 08/31/21 17:25 V8269JMV
<0.119 mg/Kg - dry 0.119 0.8192,4-Dichlorophenol 1 08/31/21 17:25 V8269JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-239-0018
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 08/27/2021
LEN-008
Report Date : 09/03/2021
Sample ID :
Lab No :
Sampled:SP-2
94457 Matrix:
8/27/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8207 08/30/21 12:00
<0.223 mg/Kg - dry 0.223 0.819Diethyl phthalate 1 08/31/21 17:25 V8269JMV
<0.216 mg/Kg - dry 0.216 0.819Dimethyl phthalate 1 08/31/21 17:25 V8269JMV
<0.134 mg/Kg - dry 0.134 0.4092,4-Dimethylphenol 1 08/31/21 17:25 V8269JMV
<0.132 mg/Kg - dry 0.132 0.819Di-n-butyl phthalate 1 08/31/21 17:25 V8269JMV
<0.298 mg/Kg - dry 0.298 1.864,6-Dinitro-2-methylphenol 1 08/31/21 17:25 V8269JMV
<0.645 mg/Kg - dry 0.645 1.862,4-Dinitrophenol 1 08/31/21 17:25 V8269JMV
<0.120 mg/Kg - dry 0.120 0.8192,4-Dinitrotoluene 1 08/31/21 17:25 V8269JMV
<0.134 mg/Kg - dry 0.134 0.8192,6-Dinitrotoluene 1 08/31/21 17:25 V8269JMV
<0.177 mg/Kg - dry 0.177 0.409
Di-n-Octyl Phthalate 1 08/31/21 17:25 V8269JMV
<0.152 mg/Kg - dry 0.152 0.819Fluoranthene 1 08/31/21 17:25 V8269JMV
<0.159 mg/Kg - dry 0.159 0.819Fluorene 1 08/31/21 17:25 V8269JMV
<0.131 mg/Kg - dry 0.131 0.819Hexachlorobenzene 1 08/31/21 17:25 V8269JMV
<0.121 mg/Kg - dry 0.121 0.819Hexachlorobutadiene 1 08/31/21 17:25 V8269JMV
<0.195 mg/Kg - dry 0.195 0.819Hexachlorocyclopentadiene 1 08/31/21 17:25 V8269JMV
<0.098 mg/Kg - dry 0.098 0.819Hexachloroethane 1 08/31/21 17:25 V8269JMV
<0.222 mg/Kg - dry 0.222 0.819
Indeno(1,2,3-cd)pyrene 1 08/31/21 17:25 V8269JMV
<0.237 mg/Kg - dry 0.237 0.819Isophorone 1 08/31/21 17:25 V8269JMV
<0.131 mg/Kg - dry 0.131 0.8191-Methylnaphthalene 1 08/31/21 17:25 V8269JMV
<0.124 mg/Kg - dry 0.124 0.8192-Methylnaphthalene 1 08/31/21 17:25 V8269JMV
<0.120 mg/Kg - dry 0.120 0.8192-Methylphenol 1 08/31/21 17:25 V8269JMV
<0.105 mg/Kg - dry 0.105 0.8193&4 Methylphenol 1 08/31/21 17:25 V8269JMV
<0.178 mg/Kg - dry 0.178 0.819Naphthalene 1 08/31/21 17:25 V8269JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-239-0018
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 08/27/2021
LEN-008
Report Date : 09/03/2021
Sample ID :
Lab No :
Sampled:SP-2
94457 Matrix:
8/27/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8207 08/30/21 12:00
<0.120 mg/Kg - dry 0.120 0.8192-Nitroaniline 1 08/31/21 17:25 V8269JMV
<0.149 mg/Kg - dry 0.149 0.8193-Nitroaniline 1 08/31/21 17:25 V8269JMV
<0.115 mg/Kg - dry 0.115 0.4094-Nitroaniline 1 08/31/21 17:25 V8269JMV
<0.144 mg/Kg - dry 0.144 0.409Nitrobenzene 1 08/31/21 17:25 V8269JMV
<0.110 mg/Kg - dry 0.110 0.8192-Nitrophenol 1 08/31/21 17:25 V8269JMV
<0.145 mg/Kg - dry 0.145 0.8194-Nitrophenol 1 08/31/21 17:25 V8269JMV
<0.326 mg/Kg - dry 0.326 0.819N-Nitrosodimethylamine 1 08/31/21 17:25 V8269JMV
<0.224 mg/Kg - dry 0.224 0.819N-Nitrosodiphenylamine 1 08/31/21 17:25 V8269JMV
<0.146 mg/Kg - dry 0.146 0.819
N-Nitroso-di-n-propylamine 1 08/31/21 17:25 V8269JMV
<0.431 mg/Kg - dry 0.431 1.24Pentachlorophenol 1 08/31/21 17:25 V8269JMV
<0.258 mg/Kg - dry 0.258 0.819Phenanthrene 1 08/31/21 17:25 V8269JMV
<0.139 mg/Kg - dry 0.139 0.819Phenol 1 08/31/21 17:25 V8269JMV
<0.166 mg/Kg - dry 0.166 0.819Pyrene 1 08/31/21 17:25 V8269JMV
<0.098 mg/Kg - dry 0.098 0.409Pyridine 1 08/31/21 17:25 V8269JMV
<0.132 mg/Kg - dry 0.132 0.8191,2,4-Trichlorobenzene 1 08/31/21 17:25 V8269JMV
<0.119 mg/Kg - dry 0.119 0.819
2,4,5-Trichlorophenol 1 08/31/21 17:25 V8269JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-239-0018
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 08/27/2021
LEN-008
Report Date : 09/03/2021
Sample ID :
Lab No :
Sampled:SP-2
94457 Matrix:
8/27/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V8207 08/30/21 12:00
<0.120 mg/Kg - dry 0.120 0.8192,4,6-Trichlorophenol 1 08/31/21 17:25 V8269JMV
Surrogate: Phenol-d5 67.6 Limits: 34-121%08/31/21 17:251 JMV V8269
Surrogate: 2-Fluorobiphenyl 76.6 Limits: 44-115%08/31/21 17:251 JMV V8269
Surrogate: 2-Fluorophenol 70.3 Limits: 35-115%08/31/21 17:251 JMV V8269
Surrogate: Nitrobenzene-d5 69.5 Limits: 37-122%08/31/21 17:251 JMV V8269
Surrogate: 4-Terphenyl-d14 84.4 Limits: 54-127%08/31/21 17:251 JMV V8269
Surrogate: 2,4,6-Tribromophenol 70.6 Limits: 39-132%08/31/21 17:251 JMV V8269
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 45
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172Tel: [phone] Fax: [phone] www.pacelabs.com
Report of Analysis
Waypoint Analytical
PO Box 240543Charlotte, NC 28224Attention: Angela Overcash
Project Name: 21-239-0018
Lot Number:WH28013
Date Completed:08/31/2021
09/01/2021 11:53 AMApproved and released by:
Project Manager II:Lucas Odom
Page 1 of 11
Page 14 of 45
PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Waypoint Analytical
Lot Number: WH28013
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header informationassociated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page ordiscussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on thecover page.
Page 2 of 11
Page 15 of 45
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: WH28013

Sample Number Sample ID Matrix Date Sampled Date Received
001 08/27/2021 1230SP-2 Solid 08/28/2021
(1 sample)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 11
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Waypoint Analytical
Lot Number: WH28013

Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 11
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
SP-2
WH28013-001
08/27/2021 1230
08/28/2021
Solid
% Solids:77.3 08/28/2021 2020
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 08/30/2021 2325 AMR 08/30/2021 1222 13771
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 11
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 11
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ13771-001
13771 3060A
08/30/2021 1222Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 08/30/2021 19451.0 0.20 mg/kg1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 11
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ13771-002
13771 3060A
08/30/2021 1222Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg) (mg/kg)
Hexavalent Chromium 9.5 08/30/2021 2010951080-1201
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 11
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 11
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 11
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 11
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Metals Analyses
6020B
V8316,V8335QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V8248
Associated Lab Samples: 94457
LRB-V8248 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/01/21 14:151.000.0940<0.0940mg/KgArsenic
09/01/21 14:1510.01.40<1.40mg/KgBarium
09/01/21 14:150.5000.0550<0.0550mg/KgCadmium
09/01/21 14:151.000.290<0.290mg/KgChromium
09/01/21 14:151.000.140<0.140mg/KgLead
09/01/21 14:152.000.900<0.900mg/KgSelenium
09/01/21 14:150.5000.0410<0.0410mg/KgSilver
LCS-V8248Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10413.012.5mg/KgArsenic 80-120
10212.812.5mg/KgBarium 80-120
10613.312.5mg/KgCadmium 80-120
10613.212.5mg/KgChromium 80-120
10513.112.5mg/KgLead 80-120
10713.412.5mg/KgSelenium 80-120
1045.225.00mg/KgSilver 80-120
V 94452-MS-V8248 V 94452-MSD-V8248Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
13.1 10511.612.512.50.933mg/KgArsenic 93.0 75-125 12.1 20
52.7 -22*55.712.512.555.5mg/KgBarium 2.0*75-125 5.5 20
12.9 10313.112.512.5<0.0550mg/KgCadmium 105 75-125 1.5 20
79.7 95.077.712.512.567.8mg/KgChromium 79.0 75-125 2.5 20
Page 1 of 19* QC Fail Date:09/03/2021 02:01 PM
Page 25 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Metals Analyses
6020B
V8316,V8335QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V8248
V 94452-MS-V8248 V 94452-MSD-V8248Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
23.5 147*17.712.512.55.14mg/KgLead 100 75-125 28.1*20
12.5 10012.112.512.50.902mg/KgSelenium 97.0 75-125 3.2 20
4.99 1005.085.005.00<0.0410mg/KgSilver 102 75-125 1.7 20
V 94452-PDS-V8248Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/01/21 21:0110713.3mg/KgArsenic
09/01/21 21:0110743.1mg/KgBarium
09/01/21 21:0110613.3mg/KgCadmium
09/01/21 21:0110146.7mg/KgChromium
09/01/21 21:0110115.3mg/KgLead
09/01/21 21:0110613.3mg/KgSelenium
09/01/21 21:0110413.0mg/KgSilver
Page 2 of 19* QC Fail Date:09/03/2021 02:01 PM
Page 26 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V8277QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V8260
Associated Lab Samples: 94457
LRB-V8260 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
08/31/21 14:420.03000.0120<0.0120mg/KgMercury (Total)
LCS-V8260Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1030.4290.417mg/KgMercury (Total)80-120
V 94580-MS-V8260 V 94580-MSD-V8260Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.353 85.00.3590.4170.417<0.0120mg/KgMercury (Total)86.0 80-120 1.6 20
V 94580-PDS-V8260Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
08/31/21 14:5993.00.194mg/KgMercury (Total)
Page 3 of 19Date:09/03/2021 02:01 PM
Page 27 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8221QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8220
Associated Lab Samples: 94457
LRB-V8220 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/30/21 13:350.0200.002<0.002mg/KgAcetone
08/30/21 13:350.0200.001<0.001mg/KgAcrolein
08/30/21 13:350.0200.0008<0.0008mg/KgAcrylonitrile
08/30/21 13:350.0050.0006<0.0006mg/KgBenzene
08/30/21 13:350.0050.0005<0.0005mg/KgBromobenzene
08/30/21 13:350.0050.0008<0.0008mg/KgBromochloromethane
08/30/21 13:350.0050.001<0.001mg/KgBromodichloromethane
08/30/21 13:350.0050.001<0.001mg/KgBromoform
08/30/21 13:350.0100.001<0.001mg/KgBromomethane
08/30/21 13:350.0050.0005<0.0005mg/Kgn-Butylbenzene
08/30/21 13:350.0050.0006<0.0006mg/Kgsec-Butyl benzene
08/30/21 13:350.0050.0005<0.0005mg/Kgtert-Butyl benzene
08/30/21 13:350.0050.0006<0.0006mg/KgCarbon Disulfide
08/30/21 13:350.0050.001<0.001mg/KgCarbon Tetrachloride
08/30/21 13:350.0050.0007<0.0007mg/KgChlorobenzene
08/30/21 13:350.0050.0009<0.0009mg/KgChlorodibromomethane
08/30/21 13:350.0100.0009<0.0009mg/KgChloroethane
08/30/21 13:350.0050.001<0.001mg/KgChloroform
08/30/21 13:350.0100.0006<0.0006mg/KgChloromethane
08/30/21 13:350.0050.0005<0.0005mg/Kg2-Chlorotoluene
08/30/21 13:350.0050.0004<0.0004mg/Kg4-Chlorotoluene
08/30/21 13:350.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
08/30/21 13:350.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
08/30/21 13:350.0050.0006<0.0006mg/Kg1,2-Dibromoethane
08/30/21 13:350.0050.0006<0.0006mg/KgDibromomethane
08/30/21 13:350.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
08/30/21 13:350.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 19Date:09/03/2021 02:01 PM
Page 28 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8221QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8220
Associated Lab Samples: 94457
LRB-V8220 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/30/21 13:350.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
08/30/21 13:350.0100.001<0.001mg/KgDichlorodifluoromethane
08/30/21 13:350.0050.0008<0.0008mg/Kg1,1-Dichloroethane
08/30/21 13:350.0050.001<0.001mg/Kg1,2-Dichloroethane
08/30/21 13:350.0050.0007<0.0007mg/Kg1,1-Dichloroethene
08/30/21 13:350.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
08/30/21 13:350.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
08/30/21 13:350.0050.0004<0.0004mg/Kg1,2-Dichloropropane
08/30/21 13:350.0050.0006<0.0006mg/Kg1,3-Dichloropropane
08/30/21 13:350.0050.001<0.001mg/Kg2,2-Dichloropropane
08/30/21 13:350.0050.0008<0.0008mg/Kg1,1-Dichloropropene
08/30/21 13:350.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
08/30/21 13:350.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
08/30/21 13:350.2500.014<0.014mg/KgEthanol
08/30/21 13:350.0050.0006<0.0006mg/KgEthylbenzene
08/30/21 13:350.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
08/30/21 13:350.0100.0008<0.0008mg/KgHexachlorobutadiene
08/30/21 13:350.0100.0007<0.0007mg/Kgn-Hexane
08/30/21 13:350.0200.0006<0.0006mg/Kg2-Hexanone
08/30/21 13:350.0050.0005<0.0005mg/KgIsopropylbenzene
08/30/21 13:350.0050.001<0.001mg/Kg4-Isopropyl toluene
08/30/21 13:350.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
08/30/21 13:350.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
08/30/21 13:350.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
08/30/21 13:350.0100.001<0.001mg/KgMethylene Chloride
08/30/21 13:350.0100.0010<0.0010mg/KgNaphthalene
08/30/21 13:350.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 19Date:09/03/2021 02:01 PM
Page 29 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8221QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8220
Associated Lab Samples: 94457
LRB-V8220 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/30/21 13:350.0050.001<0.001mg/KgStyrene
08/30/21 13:350.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
08/30/21 13:350.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
08/30/21 13:350.0050.0009<0.0009mg/KgTetrachloroethene
08/30/21 13:350.0050.0007<0.0007mg/KgToluene
08/30/21 13:350.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
08/30/21 13:350.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
08/30/21 13:350.0050.001<0.001mg/Kg1,1,1-Trichloroethane
08/30/21 13:350.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
08/30/21 13:350.0050.0009<0.0009mg/KgTrichloroethene
08/30/21 13:350.0100.002<0.002mg/KgTrichlorofluoromethane
08/30/21 13:350.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
08/30/21 13:350.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
08/30/21 13:350.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
08/30/21 13:350.0100.0005<0.0005mg/KgVinyl Acetate
08/30/21 13:350.0100.0005<0.0005mg/KgVinyl Chloride
08/30/21 13:350.0050.0005<0.0005mg/Kgo-Xylene
08/30/21 13:350.0100.001<0.001mg/Kgm,p-Xylene
08/30/21 13:354-Bromofluorobenzene (S)103 70-130
08/30/21 13:35Dibromofluoromethane (S)106 84-123
08/30/21 13:35Toluene-d8 (S)117 76-129
LCS-V8220 LCSD-V8220Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.084 84.182.50.0820.100mg/KgAcetone 29-198 1.9 20
Page 6 of 19Date:09/03/2021 02:01 PM
Page 30 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8221QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8220
LCS-V8220 LCSD-V8220Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.101 1011020.1020.100mg/KgAcrolein 70-130 0.9 20
0.093 93.191.20.0910.100mg/KgAcrylonitrile 65-134 2.0 20
0.038 77.281.80.0400.050mg/KgBenzene 74-127 5.7 20
0.051 1041080.0540.050mg/KgBromobenzene 73-125 4.3 20
0.040 81.682.60.0410.050mg/KgBromochloromethane 72-134 1.2 20
0.040 81.883.80.0410.050mg/KgBromodichloromethane 75-122 2.4 20
0.053 1061070.0530.050mg/KgBromoform 66-135 0.9 20
0.038 76.481.40.0400.050mg/KgBromomethane 20-180 6.3 20
0.050 1011100.0550.050mg/Kgn-Butylbenzene 65-135 8.8 20
0.050 1011090.0540.050mg/Kgsec-Butyl benzene 66-131 7.2 20
0.050 1001080.0530.050mg/Kgtert-Butyl benzene 67-132 7.3 20
0.036 73.679.60.0390.050mg/KgCarbon Disulfide 61-129 7.8 20
0.036 72.880.00.0400.050mg/KgCarbon Tetrachloride 64-143 9.4 20
0.046 92.896.40.0480.050mg/KgChlorobenzene 74-118 3.8 20
0.049 99.61020.0510.050mg/KgChlorodibromomethane 73-122 2.5 20
0.032 65.471.60.0350.050mg/KgChloroethane 33-149 9.0 20
0.038 76.680.20.0400.050mg/KgChloroform 73-127 4.5 20
0.037 75.681.80.0400.050mg/KgChloromethane 45-143 7.8 20
0.052 1051090.0540.050mg/Kg2-Chlorotoluene 67-124 3.9 20
0.053 1081140.0560.050mg/Kg4-Chlorotoluene 71-126 5.6 20
0.041 83.685.40.0420.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.1 20
0.061 1231220.0600.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 0.6 20
0.050 1021020.0500.050mg/Kg1,2-Dibromoethane 70-132 0.0 20
0.040 81.083.40.0410.050mg/KgDibromomethane 74-133 2.9 20
0.052 1061090.0540.050mg/Kg1,2-Dichlorobenzene 72-123 2.7 20
0.051 1041080.0540.050mg/Kg1,3-Dichlorobenzene 71-120 3.9 20
Page 7 of 19Date:09/03/2021 02:01 PM
Page 31 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8221QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8220
LCS-V8220 LCSD-V8220Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1031080.0530.050mg/Kg1,4-Dichlorobenzene 71-123 4.7 20
0.034 68.076.00.0380.050mg/KgDichlorodifluoromethane 26-146 11.1 20
0.039 78.881.60.0400.050mg/Kg1,1-Dichloroethane 74-127 3.4 20
0.040 81.282.80.0410.050mg/Kg1,2-Dichloroethane 68-128 1.9 20
0.036 73.479.00.0390.050mg/Kg1,1-Dichloroethene 67-149 7.3 20
0.039 78.481.60.0400.050mg/Kgcis-1,2-Dichloroethene 76-134 4.0 20
0.038 76.880.80.0400.050mg/Kgtrans-1,2-Dichloroethene 73-132 5.0 20
0.040 81.083.20.0410.050mg/Kg1,2-Dichloropropane 73-130 2.6 20
0.049 99.41020.0500.050mg/Kg1,3-Dichloropropane 75-124 2.1 20
0.037 74.881.20.0400.050mg/Kg2,2-Dichloropropane 50-142 8.2 20
0.037 74.080.40.0400.050mg/Kg1,1-Dichloropropene 71-130 8.2 20
0.042 84.085.80.0420.050mg/Kgcis-1,3-Dichloropropene 71-125 2.1 20
0.042 85.086.80.0430.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.0 20
1.18 94.492.81.161.25mg/KgEthanol 70-130 1.7 20
0.045 91.697.00.0480.050mg/KgEthylbenzene 74-128 5.7 20
0.085 85.587.00.0870.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.7 20
0.048 97.81070.0530.050mg/KgHexachlorobutadiene 64-125 8.7 20
0.038 76.283.60.0410.050mg/Kgn-Hexane 70-130 9.2 20
0.057 1151140.0570.050mg/Kg2-Hexanone 61-157 1.0 20
0.050 1011090.0540.050mg/KgIsopropylbenzene 68-126 7.2 20
0.051 1031090.0540.050mg/Kg4-Isopropyl toluene 68-129 6.4 20
0.045 90.288.20.0440.050mg/KgMethyl Ethyl Ketone (MEK)63-149 2.2 20
0.042 84.684.80.0420.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.2 20
0.047 95.493.40.0460.050mg/Kg4-Methyl-2-Pentanone 57-162 2.1 20
0.040 81.082.80.0410.050mg/KgMethylene Chloride 74-129 2.1 20
0.058 1161170.0580.050mg/KgNaphthalene 57-157 0.1 20
Page 8 of 19Date:09/03/2021 02:01 PM
Page 32 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V8221QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V8220
LCS-V8220 LCSD-V8220Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1021090.0540.050mg/Kgn-Propylbenzene 67-130 6.4 20
0.047 95.899.80.0490.050mg/KgStyrene 77-121 4.0 20
0.047 94.81010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 5.9 20
0.058 1171160.0580.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.1 20
0.036 72.478.40.0390.050mg/KgTetrachloroethene 68-130 7.9 20
0.038 76.880.20.0400.050mg/KgToluene 71-129 4.3 20
0.054 1081110.0550.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.9 20
0.054 1091110.0550.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.6 20
0.036 72.880.00.0400.050mg/Kg1,1,1-Trichloroethane 67-131 9.4 20
0.050 1001010.0500.050mg/Kg1,1,2-Trichloroethane 70-133 0.7 20
0.037 74.6*80.00.0400.050mg/KgTrichloroethene 75-133 6.9 20
0.036 73.881.00.0400.050mg/KgTrichlorofluoromethane 44-146 9.3 20
0.057 1161130.0560.050mg/Kg1,2,3-Trichloropropane 60-137 2.0 20
0.052 1051100.0550.050mg/Kg1,2,4-Trimethylbenzene 69-129 5.0 20
0.050 1011090.0540.050mg/Kg1,3,5-Trimethylbenzene 69-128 7.2 20
0.050 1021060.0530.050mg/KgVinyl Acetate 85-161 4.6 20
0.037 74.080.20.0400.050mg/KgVinyl Chloride 48-147 8.0 20
0.046 93.498.60.0490.050mg/Kgo-Xylene 74-126 5.4 20
0.093 93.798.90.0980.100mg/Kgm,p-Xylene 75-124 5.3 20
1021034-Bromofluorobenzene (S)70-130
103104Dibromofluoromethane (S)84-123
116117Toluene-d8 (S)76-129
Page 9 of 19* QC Fail Date:09/03/2021 02:01 PM
Page 33 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8269QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8207
Associated Lab Samples: 94457
LRB-V8207 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/31/21 10:520.6600.116<0.116mg/KgAcenaphthene
08/31/21 10:520.6600.105<0.105mg/KgAcenaphthylene
08/31/21 10:520.6600.152<0.152mg/KgAniline
08/31/21 10:520.6600.143<0.143mg/KgAnthracene
08/31/21 10:520.6600.139<0.139mg/KgBenzo(a)anthracene
08/31/21 10:520.6600.147<0.147mg/KgBenzo(a)pyrene
08/31/21 10:520.6600.146<0.146mg/KgBenzo(b)fluoranthene
08/31/21 10:520.6600.136<0.136mg/KgBenzo(g,h,i)perylene
08/31/21 10:520.6600.137<0.137mg/KgBenzo(k)fluoranthene
08/31/21 10:522.000.580<0.580mg/KgBenzoic Acid
08/31/21 10:520.6600.105<0.105mg/KgBenzyl alcohol
08/31/21 10:520.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
08/31/21 10:520.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
08/31/21 10:520.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
08/31/21 10:520.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
08/31/21 10:520.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
08/31/21 10:520.3300.113<0.113mg/KgButyl benzyl phthalate
08/31/21 10:520.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
08/31/21 10:520.3300.112<0.112mg/Kg4-Chloroaniline
08/31/21 10:520.6600.116<0.116mg/Kg2-Chloronaphthalene
08/31/21 10:520.6600.098<0.098mg/Kg2-Chlorophenol
08/31/21 10:521.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
08/31/21 10:520.6600.142<0.142mg/KgChrysene
08/31/21 10:520.6600.230<0.230mg/KgDibenz(a,h)anthracene
08/31/21 10:520.6600.119<0.119mg/KgDibenzofuran
08/31/21 10:520.6600.094<0.094mg/Kg1,2-Dichlorobenzene
08/31/21 10:520.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 10 of 19Date:09/03/2021 02:01 PM
Page 34 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8269QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8207
Associated Lab Samples: 94457
LRB-V8207 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/31/21 10:520.3300.097<0.097mg/Kg1,4-Dichlorobenzene
08/31/21 10:520.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
08/31/21 10:520.6600.095<0.095mg/Kg2,4-Dichlorophenol
08/31/21 10:520.6600.180<0.180mg/KgDiethyl phthalate
08/31/21 10:520.6600.174<0.174mg/KgDimethyl phthalate
08/31/21 10:520.3300.108<0.108mg/Kg2,4-Dimethylphenol
08/31/21 10:520.6600.107<0.107mg/KgDi-n-butyl phthalate
08/31/21 10:521.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
08/31/21 10:521.500.520<0.520mg/Kg2,4-Dinitrophenol
08/31/21 10:520.6600.096<0.096mg/Kg2,4-Dinitrotoluene
08/31/21 10:520.6600.108<0.108mg/Kg2,6-Dinitrotoluene
08/31/21 10:520.3300.143<0.143mg/KgDi-n-Octyl Phthalate
08/31/21 10:520.6600.123<0.123mg/KgFluoranthene
08/31/21 10:520.6600.128<0.128mg/KgFluorene
08/31/21 10:520.6600.106<0.106mg/KgHexachlorobenzene
08/31/21 10:520.6600.097<0.097mg/KgHexachlorobutadiene
08/31/21 10:520.6600.157<0.157mg/KgHexachlorocyclopentadiene
08/31/21 10:520.6600.079<0.079mg/KgHexachloroethane
08/31/21 10:520.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
08/31/21 10:520.6600.191<0.191mg/KgIsophorone
08/31/21 10:520.6600.106<0.106mg/Kg1-Methylnaphthalene
08/31/21 10:520.6600.100<0.100mg/Kg2-Methylnaphthalene
08/31/21 10:520.6600.097<0.097mg/Kg2-Methylphenol
08/31/21 10:520.6600.084<0.084mg/Kg3&4 Methylphenol
08/31/21 10:520.6600.144<0.144mg/KgNaphthalene
08/31/21 10:520.6600.096<0.096mg/Kg2-Nitroaniline
08/31/21 10:520.6600.120<0.120mg/Kg3-Nitroaniline
Page 11 of 19Date:09/03/2021 02:01 PM
Page 35 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8269QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8207
Associated Lab Samples: 94457
LRB-V8207 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/31/21 10:520.3300.093<0.093mg/Kg4-Nitroaniline
08/31/21 10:520.3300.116<0.116mg/KgNitrobenzene
08/31/21 10:520.6600.088<0.088mg/Kg2-Nitrophenol
08/31/21 10:520.6600.117<0.117mg/Kg4-Nitrophenol
08/31/21 10:520.6600.263<0.263mg/KgN-Nitrosodimethylamine
08/31/21 10:520.6600.181<0.181mg/KgN-Nitrosodiphenylamine
08/31/21 10:520.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
08/31/21 10:521.000.347<0.347mg/KgPentachlorophenol
08/31/21 10:520.6600.208<0.208mg/KgPhenanthrene
08/31/21 10:520.6600.112<0.112mg/KgPhenol
08/31/21 10:520.6600.134<0.134mg/KgPyrene
08/31/21 10:520.3300.079<0.079mg/KgPyridine
08/31/21 10:520.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
08/31/21 10:520.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
08/31/21 10:520.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
08/31/21 10:522-Fluorobiphenyl (S)88.0 44-115
08/31/21 10:522-Fluorophenol (S)81.3 35-115
08/31/21 10:52Nitrobenzene-d5 (S)83.8 37-122
08/31/21 10:524-Terphenyl-d14 (S)97.0 54-127
08/31/21 10:522,4,6-Tribromophenol (S)87.3 39-132
08/31/21 10:52Phenol-d5 (S)79.2 34-121
LCS-V8207Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
83.81.401.67mg/KgAcenaphthene 40-123
85.61.431.67mg/KgAcenaphthylene 32-132
Page 12 of 19Date:09/03/2021 02:01 PM
Page 36 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8269QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8207
LCS-V8207Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
68.81.151.67mg/KgAniline 12-197
87.41.461.67mg/KgAnthracene 47-123
85.61.431.67mg/KgBenzo(a)anthracene 49-126
1222.041.67mg/KgBenzo(a)pyrene 45-129
1171.961.67mg/KgBenzo(b)fluoranthene 45-132
1081.801.67mg/KgBenzo(g,h,i)perylene 43-134
1071.791.67mg/KgBenzo(k)fluoranthene 47-132
0.0*1.111.67mg/KgBenzoic Acid 10-83
74.81.251.67mg/KgBenzyl alcohol 29-122
79.61.331.67mg/KgBis(2-Chloroethoxy)methane 36-121
71.81.201.67mg/KgBis(2-Chloroethyl)ether 31-120
79.61.331.67mg/KgBis(2-Chloroisopropyl)ether 33-131
97.01.621.67mg/KgBis(2-ethylhexyl)phthalate 51-133
82.61.381.67mg/Kg4-Bromophenyl phenyl ether 46-124
96.41.611.67mg/KgButyl benzyl phthalate 48-132
77.81.301.67mg/Kg4-Chloro-3-methylphenol 45-122
68.21.141.67mg/Kg4-Chloroaniline 17-106
81.41.361.67mg/Kg2-Chloronaphthalene 41-114
74.21.241.67mg/Kg2-Chlorophenol 34-121
85.01.421.67mg/Kg4-Chlorophenyl phenyl ether 45-121
88.01.471.67mg/KgChrysene 50-124
71.21.191.67mg/KgDibenz(a,h)anthracene 45-134
83.81.401.67mg/KgDibenzofuran 44-120
68.81.151.67mg/Kg1,2-Dichlorobenzene 33-117
67.01.121.67mg/Kg1,3-Dichlorobenzene 30-115
66.41.111.67mg/Kg1,4-Dichlorobenzene 31-115
82.01.371.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 13 of 19* QC Fail Date:09/03/2021 02:01 PM
Page 37 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8269QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8207
LCS-V8207Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
74.21.241.67mg/Kg2,4-Dichlorophenol 40-122
85.01.421.67mg/KgDiethyl phthalate 50-124
82.01.371.67mg/KgDimethyl phthalate 48-124
78.41.311.67mg/Kg2,4-Dimethylphenol 30-127
96.41.611.67mg/KgDi-n-butyl phthalate 51-128
89.81.501.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
91.61.531.67mg/Kg2,4-Dinitrophenol 27-129
89.21.491.67mg/Kg2,4-Dinitrotoluene 48-126
85.01.421.67mg/Kg2,6-Dinitrotoluene 46-124
1232.061.67mg/KgDi-n-Octyl Phthalate 45-140
85.61.431.67mg/KgFluoranthene 50-127
83.81.401.67mg/KgFluorene 43-125
82.61.381.67mg/KgHexachlorobenzene 45-122
67.01.121.67mg/KgHexachlorobutadiene 32-123
59.00.9861.67mg/KgHexachlorocyclopentadiene 32-117
67.01.121.67mg/KgHexachloroethane 28-117
1111.861.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
58.80.9831.67mg/KgIsophorone 30-122
69.41.161.67mg/Kg1-Methylnaphthalene 40-119
68.21.141.67mg/Kg2-Methylnaphthalene 38-122
79.61.331.67mg/Kg2-Methylphenol 32-122
68.81.151.67mg/Kg3&4 Methylphenol 34-119
65.81.101.67mg/KgNaphthalene 35-123
83.21.391.67mg/Kg2-Nitroaniline 44-127
82.61.381.67mg/Kg3-Nitroaniline 33-119
89.21.491.67mg/Kg4-Nitroaniline 63-147
68.81.151.67mg/KgNitrobenzene 34-122
Page 14 of 19Date:09/03/2021 02:01 PM
Page 38 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8269QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8207
LCS-V8207Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
68.21.141.67mg/Kg2-Nitrophenol 36-123
96.41.611.67mg/Kg4-Nitrophenol 30-132
68.21.141.67mg/KgN-Nitrosodimethylamine 10-146
1051.751.67mg/KgN-Nitrosodiphenylamine 38-127
73.61.231.67mg/KgN-Nitroso-di-n-propylamine 36-120
89.21.491.67mg/KgPentachlorophenol 25-133
92.81.551.67mg/KgPhenanthrene 50-121
74.21.241.67mg/KgPhenol 34-121
94.61.581.67mg/KgPyrene 47-127
42.30.7081.67mg/KgPyridine 10-80
64.01.071.67mg/Kg1,2,4-Trichlorobenzene 34-118
80.21.341.67mg/Kg2,4,5-Trichlorophenol 41-124
82.01.371.67mg/Kg2,4,6-Trichlorophenol 39-126
82.02-Fluorobiphenyl (S)44-115
75.02-Fluorophenol (S)35-115
69.4Nitrobenzene-d5 (S)37-122
91.04-Terphenyl-d14 (S)54-127
84.02,4,6-Tribromophenol (S)39-132
72.6Phenol-d5 (S)34-121
V 94178-MS-V8207 V 94178-MSD-V8207Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.59 95.21.241.671.67<0.116mg/KgAcenaphthene 74.2 40-123 24.7*20
1.58 94.61.251.671.67<0.105mg/KgAcenaphthylene 74.8 32-132 23.3*20
1.13 67.60.8451.671.67<0.152mg/KgAniline 50.5 12-197 28.8*20
Page 15 of 19* QC Fail Date:09/03/2021 02:01 PM
Page 39 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8269QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8207
V 94178-MS-V8207 V 94178-MSD-V8207Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.65 98.81.251.671.67<0.143mg/KgAnthracene 74.8 47-123 27.5*20
1.59 95.21.221.671.67<0.139mg/KgBenzo(a)anthracene 73.0 49-126 26.3*20
2.24 134*1.741.671.67<0.147mg/KgBenzo(a)pyrene 104 45-129 25.1*20
2.14 1281.681.671.67<0.146mg/KgBenzo(b)fluoranthene 101 45-132 24.0*20
1.99 1191.521.671.67<0.136mg/KgBenzo(g,h,i)perylene 91.0 43-134 26.7*20
2.02 1211.521.671.67<0.137mg/KgBenzo(k)fluoranthene 91.0 47-132 28.2*20
1.54 0.0*1.161.671.67<0.580mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.47 88.01.131.671.67<0.105mg/KgBenzyl alcohol 67.6 29-122 26.1*20
1.42 85.01.111.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 66.4 36-121 24.5*20
1.22 73.01.061.671.67<0.107mg/KgBis(2-Chloroethyl)ether 63.4 31-120 14.0 20
1.50 89.81.151.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 68.8 33-131 26.4*20
1.87 1121.451.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 86.8 51-133 25.3*20
1.53 91.61.171.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 70.0 46-124 26.6*20
1.84 1101.751.671.67<0.113mg/KgButyl benzyl phthalate 105 48-132 5.0 20
1.46 87.41.131.671.67<0.092mg/Kg4-Chloro-3-methylphenol 67.6 45-122 25.4*20
1.15 68.80.9311.671.67<0.112mg/Kg4-Chloroaniline 55.7 17-106 21.0*20
1.51 90.41.191.671.67<0.116mg/Kg2-Chloronaphthalene 71.2 41-114 23.7*20
1.42 85.01.081.671.67<0.098mg/Kg2-Chlorophenol 64.6 34-121 27.2*20
1.56 93.41.221.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 73.0 45-121 24.4*20
1.64 98.21.251.671.67<0.142mg/KgChrysene 74.8 50-124 26.9*20
1.30 77.80.9861.671.67<0.230mg/KgDibenz(a,h)anthracene 59.0 45-134 27.4*20
1.55 92.81.221.671.67<0.119mg/KgDibenzofuran 73.0 44-120 23.8*20
1.28 76.61.001.671.67<0.094mg/Kg1,2-Dichlorobenzene 59.8 33-117 24.5*20
1.23 73.60.9491.671.67<0.097mg/Kg1,3-Dichlorobenzene 56.8 30-115 25.7*20
1.21 72.40.9541.671.67<0.097mg/Kg1,4-Dichlorobenzene 57.1 31-115 23.6*20
0.987 59.11.121.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 67.0 22-121 12.6 20
Page 16 of 19* QC Fail Date:09/03/2021 02:01 PM
Page 40 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8269QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8207
V 94178-MS-V8207 V 94178-MSD-V8207Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.42 85.01.101.671.67<0.095mg/Kg2,4-Dichlorophenol 65.8 40-122 25.3*20
1.58 94.61.241.671.67<0.180mg/KgDiethyl phthalate 74.2 50-124 24.1*20
1.56 93.41.231.671.67<0.174mg/KgDimethyl phthalate 73.6 48-124 23.6 30
1.47 88.01.161.671.67<0.108mg/Kg2,4-Dimethylphenol 69.4 30-127 23.5*20
1.78 1071.341.671.67<0.107mg/KgDi-n-butyl phthalate 80.2 51-128 28.2*20
1.69 1011.241.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 11.9 20
1.71 1021.341.671.67<0.520mg/Kg2,4-Dinitrophenol 0.0*27-129 13.0 20
1.61 96.41.241.671.67<0.096mg/Kg2,4-Dinitrotoluene 74.2 48-126 25.9*20
1.65 98.81.261.671.67<0.108mg/Kg2,6-Dinitrotoluene 75.4 46-124 26.8*20
2.37 142*1.841.671.67<0.143mg/KgDi-n-Octyl Phthalate 110 45-140 25.1*20
1.54 92.21.191.671.67<0.123mg/KgFluoranthene 71.2 50-127 25.6*20
1.56 93.41.221.671.67<0.128mg/KgFluorene 73.0 43-125 24.4*20
1.52 91.01.171.671.67<0.106mg/KgHexachlorobenzene 70.0 45-122 26.0*20
1.22 73.01.001.671.67<0.097mg/KgHexachlorobutadiene 59.8 32-123 19.8 20
0.916 54.80.7741.671.67<0.157mg/KgHexachlorocyclopentadiene 46.3 32-117 16.8 20
1.26 75.40.9541.671.67<0.079mg/KgHexachloroethane 57.1 28-117 27.6*20
2.05 1231.571.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 94.0 45-133 26.5*20
1.08 64.60.8561.671.67<0.191mg/KgIsophorone 51.2 30-122 23.1*20
1.28 76.61.021.671.67<0.106mg/Kg1-Methylnaphthalene 61.0 40-119 22.6*20
1.27 76.00.9981.671.67<0.100mg/Kg2-Methylnaphthalene 59.7 38-122 23.9*20
1.49 89.21.141.671.67<0.097mg/Kg2-Methylphenol 68.2 32-122 26.6*20
1.29 77.20.9671.671.67<0.084mg/Kg3&4 Methylphenol 57.9 34-119 28.6*20
1.21 72.40.9681.671.67<0.144mg/KgNaphthalene 57.9 35-123 22.2*20
1.57 94.01.251.671.67<0.096mg/Kg2-Nitroaniline 74.8 44-127 22.6*20
1.53 91.61.241.671.67<0.120mg/Kg3-Nitroaniline 74.2 33-119 20.9*20
1.56 93.41.271.671.67<0.093mg/Kg4-Nitroaniline 76.0 63-147 20.4*20
Page 17 of 19* QC Fail Date:09/03/2021 02:01 PM
Page 41 of 45
Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V8269QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V8207
V 94178-MS-V8207 V 94178-MSD-V8207Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.26 75.41.011.671.67<0.116mg/KgNitrobenzene 60.4 34-122 22.0*20
1.22 73.01.011.671.67<0.088mg/Kg2-Nitrophenol 60.4 32-123 18.8 20
1.79 1071.391.671.67<0.117mg/Kg4-Nitrophenol 83.2 30-132 25.1*20
1.16 69.40.9861.671.67<0.263mg/KgN-Nitrosodimethylamine 59.0 10-146 16.2 30
1.96 1171.491.671.67<0.181mg/KgN-Nitrosodiphenylamine 89.2 38-127 27.2*20
1.40 83.81.081.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 64.6 36-120 25.8*20
1.77 1061.281.671.67<0.347mg/KgPentachlorophenol 76.6 25-133 32.1*20
1.72 1031.311.671.67<0.208mg/KgPhenanthrene 78.4 50-121 27.0*20
1.37 82.01.041.671.67<0.112mg/KgPhenol 62.2 34-121 27.3*20
1.83 1101.441.671.67<0.134mg/KgPyrene 86.2 47-127 23.8*20
0.526 31.40.4661.671.67<0.079mg/KgPyridine 27.9 10-80 12.0 20
1.19 71.20.9491.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 56.8 34-118 22.5*20
1.52 91.01.191.671.67<0.096mg/Kg2,4,5-Trichlorophenol 71.2 41-124 24.3*20
1.55 92.81.211.671.67<0.096mg/Kg2,4,6-Trichlorophenol 72.4 39-126 24.6*20
91.02-Fluorobiphenyl (S)73.0 44-115
83.42-Fluorophenol (S)63.3 35-115
74.2Nitrobenzene-d5 (S)59.6 37-122
1044-Terphenyl-d14 (S)82.0 54-127
90.62,4,6-Tribromophenol (S)71.7 39-132
80.4Phenol-d5 (S)61.5 34-121
Page 18 of 19* QC Fail Date:09/03/2021 02:01 PM
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Quality Control Data
21-239-0018Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
Dry Weight Determination
SW-DRYWT
V8349QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94479-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/02/21 11:107.837.234.4%Moisture
V 94535-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/02/21 11:103.810.110.5%Moisture
Page 19 of 19Date:09/03/2021 02:01 PM
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Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-239-0018
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 4.0 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:08/27/2021 13:24:27
Special precautions or instructions included?
Comments:
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