MO-1570_47936_CA_LSA_20210827_Limited Site Assessment Report

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Via Email
August 27, 2021
North Carolina Department of Environmental Quality
Division of Waste Management, UST Section
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Attn: Ms. Trudy Beverly, PG
Re: Phase I Limited Site Assessment Report
Former Metrolina Steel
1118 West Craighead Road
Charlotte, North Carolina
NC DEQ Incident No. 47936
H&H Job No. AGL-003
Dear Ms. Beverly:
On behalf of EAA LLC c/o AVC Holding, LLC, Hart & Hickman, PC (H&H) is providing the
attached Phase I Limited Site Assessment Report for the above referenced site.
If you have any questions or require additional information, please do not hesitate to contact us
at [phone].
Very Truly Yours,
Hart & Hickman, PC
M
Brett Lawrence, PG
Sr. Project Geologist
Attachments
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

Phase I Limited Site Assessment
Former Metrol i na Steel
1118 West Craighead Road
Charlotte, North Carolina
Incident No.: 47936
H&H Job No. AGL-003
August 27, 2021
hart � hickman
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C#-1269 Engineering
C#-245 Geology
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.SB6.0007 main 919.847.4241 main

Phase I Limited Site Assessment Information
Site Location:
Former Metrolina Steel
1118 West Craighead Road
Mecklenburg County
Charlotte, NC 28206
Property Owner:
EAA LLC c/o AVC Holding, LLC
11220 Elm Lane, Suite 207
Charlotte, NC 28277
UST Operator: Metrolina Steel; Mr. Tom Hurt
General Site Information:
Facility ID Number: 00-0-0000025569
NC DEQ Incident Number: 47936
Site Priority Ranking: Anticipate Low
Land Use Category: Industrial
Latitude/Longitude : 35.2675990' / 80.8069650'
Release Discovery Date: May 2021
Estimated Quantity of Release: Unknown
Cause/Source of Release: Unknown
Sizes and contents of UST system: one (1) 8,000-gallon diesel and one (1) 1,000-gallon gasoline
I, C. Brett Lawrence, PG a Professional Geologist for Hart & Hickman, PC, do certify that the
information contained in this report ism ggect and accurate to the best of my knowledge.
'1*�► CAR0��''�.
Z
Hart & Hickman, PC is licensed to practice geology/engineering in North Carolina. The
certification numbers of the company are C-245/C-1269.
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LSA Report_Final.docx
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Phase I Limited Site Assessment
Former Metrolina Steel
1118 West Craighead Road
Charlotte, North Carolina
H&H Job No. AGL-003
Table of Contents
Section Pate No.
1.0 Executive Summary and Recommendations........................................................................1
2.0 Introduction and Site History................................................................................................6
3.0 Receptor Information and Risk Characterization...............................................................9
3.1 Receptor Information.............................................................................................................9
3.1.1 Water Supply Wells........................................................................................................9
3.1.2 Surface Water..................................................................................................................9
3.1.3 Subsurface Structures....................................................................................................10
3.1.4 Property Owners and Land Use....................................................................................10
3.1.5 Wellhead Protection Areas............................................................................................10
3.2 Risk and Land Use Characterization...................................................................................10
4.0 Geology and Hydrogeology..................................................................................................11
4.1 Regional Geology and Hydrogeology.................................................................................11
4.2 Site Geology and Hydrogeology.........................................................................................12
5.0 Field Activities and Sampling Results.................................................................................13
5.1 Geophysical Assessment/Utility Locate..............................................................................13
5.2 Soil Sampling Activities......................................................................................................13
5.3 Soil Sample Analytical Results...........................................................................................14
5.4 Groundwater Sampling Activities.......................................................................................15
5.5 Groundwater Sample Analytical Results.............................................................................16
6.0 Conclusions and Recommendations....................................................................................17
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Table 1
UST Information
Table 2
Summary of Adjacent Properties
Table 3
Summary of Soil Analytical Results
Table 4
Summary of Groundwater Analytical Results
List of Figures
Figure 1
Site Location Map
Figure 2
Site Map
Figure 3
Receptor Survey Map
Figure 4
LSA Sample Location Map
List of Appendices
Appendix A
Risk Classification and Land Use Form
Appendix B
Water Supply Well Information Survey Forms
Appendix C
Boring Log and Well Construction Record
Appendix D
Laboratory Analytical Report
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Phase I Limited Site Assessment
Former Metrolina Steel
1118 West Craighead Road
Charlotte, North Carolina
H&H Job No. AGL-003
1.0 Executive Summary and Recommendations
Hart & Hickman, PC (H&H) is providing this Phase I Limited Site Assessment (LSA) report on
behalf of EAA LLC c/o AVC Holding, LLC to document assessment activities conducted at the
former Metrolina Steel property located at 1118 West Craighead Road in Charlotte, Mecklenburg
County, North Carolina (Site). The Site consists of an irregular shaped parcel (Parcel ID:
08704120) that is approximately 5.6 acres and is developed with an 37,335 square foot (sq ft)
industrial warehouse building that was constructed in 1981. The Site is occupied by Master Auto
Pro, a used automotive parts dealer, and Alvinn Body Shop, an automotive body shop. The
majority of the Site is paved with asphalt or covered with crushed asphalt and is used to stage
junked vehicles. A permanent Piedmont Natural Gas Co. easement is located along the far eastern
Site boundary. The Site is located in an industrial area situated approximately three miles north
of Uptown Charlotte.
For due diligence purposes, H&H conducted a combined Phase I and II Environmental Site
Assessment (ESA) at the Site in May 2021. As part of the Phase I ESA, a regulatory database
search was conducted which indicated that the Site is listed on the North Carolina Department of
Environmental Quality (NC DEQ) Underground Storage Tank (UST) database. The UST database
indicates that two non -regulated commercial USTs were located at the Site and were registered to
former Site occupant Metrolina Steel. According to the database, one 8,000-gallon diesel UST
and one 1,000-gallon gasoline UST were installed at the Site in September 1982 and removed in
August 1992 (UST # MO-1570). No release incidents were reported associated with the former
USTs. The Site owner was vaguely aware of the former tanks and their general location near the
western exterior wall of the Site building. A review of historical aerial photographs indicated what
appears to be two fuel dispensers located overtop of a concrete pad in that area.
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H&H contacted the NC DEQ UST Section to inquire about tank closure and/or assessment
documentation associated with the former on -Site USTs. The NC DEQ responded to our request
and stated that no UST closure report was provided to the NC DEQ.
On May 6, 2021, H&H contracted Integrated Scanning Solutions (ISS) to conduct a geophysical
survey at the Site to evaluate for the presence of current or former tanks, tank basins, product lines,
fuel dispensers, or other subsurface structures associated with the reported USTs. ISS utilized
electromagnetic (EM) and ground penetrating radar (GPR) survey methods to estimate the
horizontal and vertical extent of subgrade features in the reported vicinity of the USTs. Prior to
data acquisition, a 10 ft by 10 ft survey grid was established along the western exterior wall of the
Site building using water -based marking paint.
The results of the geophysical survey confirmed the location of the former tank basin (evidence of
significant excavation observed) and indicated that the tanks and associated piping had been
removed. Based on the potential for impact from the former USTs and the lack of UST closure
documentation, H&H conducted a Phase II ESA at the Site on May 6, 2021. The Phase II ESA
included, in part, the collection of a soil and groundwater sample from within the former UST
basin for laboratory analysis. In addition, three other groundwater samples were collected from
across the Site, including one located approximately 150 feet east-southeast and topographically
downgradient of the former USTs. The results of analysis of the soil sample collected from the
former tank basin indicated that diesel and gasoline range total petroleum hydrocarbons (TPH-
DRO and TPH-GRO) were detected at concentrations above NC DEQ Action Levels. The results
of analysis of the groundwater sample collected from the former tank basin indicated that several
petroleum -related compounds were detected at concentrations above the NC DEQ Groundwater
Quality Standards (2L Standards) or Interim Maximum Allowable Concentrations (IMACs; if no
2L Standard is established), but below the NC DEQ UST Section -defined Gross Contamination
Levels (GCLs). No petroleum -related compounds were detected in the other groundwater samples
collected at the Site above laboratory detection limits (including the sample located downgradient
of the former USTs).
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Based on the results of the Phase II ESA, a release was confirmed associated with the former USTs.
Following approval from the Site owner, H&H submitted a 24-hr Release and UST Leak Report
Form (UST-61) on their behalf to NC DEQ on July 21, 2021. H&H subsequently completed
additional soil and groundwater assessment activities at the Site in general accordance with NC
DEQ's UST Section requirements for risk -based corrective action and closure of petroleum UST
releases. The methods and results of the assessment activities are provided below.
Phase I LSA Soil and Groundwater Sampling
On August 13, 2021, H&H contracted with Mid South to install one co -located LSA soil
boring/permanent monitoring well (identified as MW-1) within the former UST basin at the Site.
The soil boring was advanced using direct push technology (DPT) drilling methods. The DPT
borehole was then over -drilled using hollow stem auger (HSA) drilling methods and a permanent
Type -II monitoring well was installed.
In the LSA soil boring, obvious indication of backfill material (non-native sand) was observed
from directly beneath the asphalt pavement to approximately 7 feet below ground surface (ft bgs).
Because the fill material did not exhibit obvious indication of impact during field screening, soil
samples were not collected from that interval. H&H collected one soil sample from the first one -
foot interval located immediately below the fill material (7 to 8 ft bgs) and one soil sample just
above the saturated zone (10 to 11 ft bgs) for laboratory analysis. The soil samples were delivered
under standard chain -of -custody protocol to Pace Analytical Services, LLC (Pace), a NC -certified
laboratory, for analysis of volatile organic compounds (VOCs) by EPA Method 8260, semi -
volatile organic compounds (SVOCs) by EPA Method 8270, and volatile petroleum hydrocarbons
(VPH) and Extractable Petroleum Hydrocarbons (EPH) by the Massachusetts Department of
Environmental Protection (MADEP) method.
Following well development and stabilization of field parameters, the groundwater sample was
collected using low -flow sampling techniques and the "soda straw" sampling method for VOCs.
The groundwater sample was delivered under standard chain -of -custody protocol to Pace for
laboratory for analysis of VOCs/602 Volatiles by EPA Method 6200, Base Neutral and Acid
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Extractable SVOCs plus the 10 highest tentatively identified compounds (TICS) by EPA Method 625,
VPH and EPH by MADEP, and lead by EPA Method 6020.
Laboratory analytical results of the soil samples indicate that multiple petroleum -related VOCs,
SVOCs, and VPH hydrocarbon fractions were detected in the deeper 10 to 11 ft bgs sample interval
at concentrations above their respective Soil -to -Water Maximum Soil Contaminant
Concentrations (MSCCs). In addition, naphthalene (as a VOC) was detected in the deeper sample
interval at a concentration of 11.3 milligrams per kilogram (mg/kg) which is above the Soil -to -
Water MSCC of 0.2 mg/kg and the Residential MSCC of 5.5 mg/kg, but below the
Industrial/Commercial MSCC of 27 mg/kg. The VPH hydrocarbon fraction C5 to C8 aliphatics
was detected in the deeper sample interval at a concentration of 1,520 mg/kg, which is above the
Soil -to -Water MSCC of 68 mg/kg and the Residential MSCC of 625 mg/kg, but below the
Industrial/Commercial MSCC of 9,340 mg/kg. No other compounds were detected at
concentrations exceeding Residential MSCCs and no compounds were detected above
Industrial/Commercial MSCCs. No compounds were detected in the shallower 7 to 8 ft bgs
interval sample above MSCCs.
Laboratory analytical results of the groundwater sample indicate that naphthalene (as a VOC) was
detected at concentrations of up to 10.1 micrograms per liter (µg/L) in LSA monitoring well MW-
1 (former UST basin), which is above the 2L Standard of 6 µg/L and below the GCL of 6,000
µg/L. In addition, the VPH hydrocarbon fraction C9 to CIO aromatics was detected at a
concentration of 253 µg/L, which is above the 2L Standard of 200 µg/L. No GCLs have been
established for VPH. No other compounds were reported at concentrations above 2L Standards,
and no compounds were reported above GCLs. Lead was not detected in the groundwater sample
above the laboratory detection limit.
Land Use/Risk Characterization
As part of the Phase I LSA activities, H&H performed a Site land use and risk characterization survey.
The activities included a water supply well survey for the area within a 1,500-ft radius of the source
of the release (former USTs). Municipal water is available to the surrounding properties and no
water supply wells were identified within 1,500 feet of the source area.
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The Site is in an industrial area and is zoned for heavy industrial use. Surrounding properties are
zoned heavy industrial to the west and south, and light industrial to the north and east of the Site. The
nearest residences are located approximately 1,100 ft east of the source area, beyond Derita Branch.
Derita Branch is located approximately 950 ft east of the source area.
Recommendations
The results of the Phase I LSA indicate the presence of petroleum compounds in soil above
Residential MSCCs, but below Industrial/Commercial MSCCs. The results of the groundwater
sampling indicate that two compounds were detected above 2L Standards but below GCLs. In
addition, municipal water is supplied to properties located within the Site area and no water supply
wells used for any purpose were identified within 1,500 ft of the source of the release. Therefore,
the Site qualifies for a low -risk classification. The Site is zoned for heavy industrial use, and the
surrounding properties are zoned for industrial use. Based on its current and future use, the Site
qualifies as a commercial land use classification. Based upon the results of the Phase I LSA, H&H
recommends that NC DEQ issue a risk -based no further action (NFA) determination pending filing
of a Notice of Residual Petroleum (NORP) limiting the Site to commercial/ industrial use only and
restricting groundwater use at the Site.
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2.0 Introduction and Site History
This Phase I LSA report documents investigative activities conducted at the former Metrolina Steel
property located at 1118 West Craighead Road in Charlotte, Mecklenburg County, North Carolina.
A Site Location Map is presented as Figure 1, and a Site Map is presented as Figure 2. The Site
consists of an irregular shaped parcel (Parcel ID: 08704120) that is approximately 5.6 acres and is
developed with an 37,335 sq ft warehouse building that was constructed in 1981. The Site is
occupied by Master Auto Pro, a used automotive parts dealer, and Alvinn Body Shop, an
automotive body shop. The majority of the Site is paved with asphalt or covered with crushed
asphalt and is used to stage junked vehicles. A permanent Piedmont Natural Gas Co. easement is
located along the far eastern Site boundary. The Site is located in an industrial area situated
approximately three miles north of Uptown Charlotte.
The Site consisted of agricultural land and wooded land in the earliest historical resource reviewed,
a 1938 aerial photograph. By the late 1960s, agricultural use of the Site had ceased, and the Site
was cleared of vegetation. By 1976, the northeastern portion of the Site was developed with a
small warehouse building. The current warehouse building was developed in 1981. The Site was
occupied by Metrolina Steel, Inc. and used for the warehousing and distribution of raw steel
products between the late 1970s and mid-2000s. The small warehouse building was razed in the
early 2000s. The Site was occupied by Bunker Automation, LLC, an industrial automation and
conveyor system manufacturer in the late 2000s, by Auto Max Motor Co., a used car dealership,
and Master Towing, LLC, a tow -truck company in the early to mid-2010s, and by Master Auto
Pro and Alvinn Body Shop since 2014.
For due diligence purposes, H&H conducted a combined Phase I and II ESA at the Site in May
2021. As part of the Phase I ESA, a regulatory database search was conducted which indicated
that the Site is listed on the NC DEQ - UST database. The UST database indicates that two non -
regulated commercial USTs were located at the Site and were registered to former Site occupant
Metrolina Steel. According to the database, one 8,000-gallon diesel UST and one 1,000-gallon
gasoline UST were installed at the Site in September 1982 and removed in August 1992 (UST #
MO-1570). No release incidents have been reported at the Site. The Site owner was vaguely
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aware of the former tanks and their general location near the western exterior wall of the Site
building. A review of historical aerial photographs indicated what appears to be two fuel
dispensers located overtop of a concrete pad in that area.
H&H contacted the NC DEQ UST Section to inquire about tank closure and/or assessment
documentation associated with the former on -Site USTs. The NC DEQ responded to our request
and stated that no UST closure report was provided to the NC DEQ.
On May 6, 2021, H&H contracted ISS to conduct a geophysical survey at the Site to evaluate for
the presence of current or former tanks, tank basins, product lines, fuel dispensers, or other
subsurface structures associated with the reported USTs. ISS utilized EM and GPR survey
methods to estimate the horizontal and vertical extent of subgrade features in the reported vicinity
of the USTs. Prior to data acquisition, a 10 ft by 10 ft survey grid was established along the western
exterior wall of the Site building using water -based marking paint.
The results of the geophysical survey confirmed the location of the former tank basin (evidence of
significant excavation observed) and indicated that the tanks and associated piping had been
removed. Based on the potential for impact from the former USTs and the lack of UST closure
documentation, H&H conducted a Phase II ESA at the Site on May 6, 2021. The Phase II ESA
included, in part, the collection of a soil and groundwater sample from within the former UST
basin for laboratory analysis. In addition, three other groundwater samples were collected from
across the Site, including one located approximately 150 feet downgradient of the former USTs.
The results of analysis of the soil sample collected from the former tank basin indicated that TPH-
DRO and TPH-GRO were detected at concentrations above NC DEQ Action Levels. The results
of analysis of the groundwater sample collected from the former tank basin indicated that several
petroleum -related compounds were detected at concentrations above 2L Standards or IMACs (if
no 2L Standard is established), but below the GCLs. No petroleum -related compounds were
detected in the other groundwater samples collected at the Site above laboratory detection limits
(including the sample located downgradient of the former USTs).
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Based on the results of the Phase II ESA, a release was confirmed associated with the former USTs.
Following approval from the Site owner, H&H submitted a 24-hr Release and UST Leak Report
Form (UST-61) on their behalf to NC DEQ on July 21, 2021. H&H subsequently completed
additional soil and groundwater assessment activities at the Site in general accordance with NC
DEQ's UST Section requirements for risk -based corrective action and closure of petroleum UST
releases. The methods and results of the assessment activities are provided in the following
sections.
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3.0 Receptor Information and Risk Characterization
As part of the assessment activities, H&H performed a Site land use and risk characterization
survey. The LSA Risk Classification and Land Use Form is provided in Appendix A. A discussion
of potential receptors and land use is provided below.
3.1 Receptor Information
3.1.1 Water Supply Wells
H&H conducted a water supply well survey for the area within a 1,500-ft radius of the source of
the release. The survey was conducted by performing area reconnaissance, checking for municipal
water connections, and performing door-to-door interviews with available residential property
owners located within the survey area. No water supply wells are used for any purpose according
to information obtained during the water supply well survey. The receptor survey area is depicted
on Figure 3. Completed water supply information survey forms are provided in Appendix B.
H&H also reviewed the Mecklenburg County Land Use and Environmental Services Agency
(LUESA) online mapping database for registered supply wells. Based on a review of the LUESA
online mapping database, no active water supply wells were identified within a 1,500-ft radius of
the source area.
Based on Charlotte Water records, municipal water is provided to the Site and is available to
properties within a 1,500-ft radius of the source area. Additionally, H&H observed evidence of
municipal water availability (i.e., water meters and fire hydrants) throughout the survey area.
During the survey activities, available property owners/occupants interviewed within the 1,500-ft
radius of the source of the release confirmed connection to municipal services for water supply.
3.1.2 Surface Water
H&H conducted a survey for surface water bodies in the survey area. Derita Branch is located
approximately 950 ft east of the source area. Derita Branch is presented on Figure 3.
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3.1.3 Subsurface Structures
Visual observations were made for potential subsurface contamination conduits in the vicinity of
the former UST basin. Based upon our review, there are no anticipated subsurface contamination
conduits of concern in the area of the former UST basin.
3.1.4 Property Owners and Land Use
The Site is developed with an approximately 37,335 sq ft industrial warehouse building. The Site
is located in an industrial area. Access to the Site is restricted by perimeter fencing.
The Site is zoned for heavy industrial purposes. Surrounding properties are zoned heavy industrial
to the west and south, and light industrial to the north and east of the Site, based on Mecklenburg
County online records. The nearest residences are located approximately 1,100 ft east of the source
area, beyond Derita Branch. Adjacent property owner information is presented in Table 2, and
adjacent properties are shown on Figure 3.
3.1.5 Wellhead Protection Areas
Based on our review of the NC DEQ Source Water Assessment Program (SWAP) online mapping
tool (SWAP Info 2.0), the Site is not located in a wellhead protection area.
3.2 Risk and Land Use Characterization
Based upon the receptor survey results, as well as the soil and groundwater analytical data
presented in Section 5.0, the Site qualifies for a low -risk designation. In addition, based upon the
industrial zoning designation, the Site qualifies for a commercial land use classification.
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4.0 Geology and Hydrogeology
4.1 Regional Geology and Hydrogeology
The Site is located within the Piedmont Physiographic Province of North Carolina. The land
surface of the area is generally characterized as gently sloping. According to the Geologic Map of
North Carolina dated 1985, the subject Site lies within the Charlotte Belt of the Piedmont. In the
Site area, underlying bedrock is composed of metamorphosed quartz diorite.
In the Piedmont, the bedrock is overlain by a mantle of weathered rock termed saprolite or
residuum. The saprolite consists of unconsolidated clay, silt, and sand with lesser amounts of rock
fragments. Due to the range of parent rock types and their variable susceptibility to weathering,
the saprolite ranges widely in color, texture, and thickness. Generally, the saprolite is thickest near
interstream divides and thins toward streambeds. In profile, the saprolite normally grades from
clayey soils near the land surface to highly weathered rock above competent bedrock.
Regional Hydrogeology
The occurrence and movement of groundwater in the Piedmont is typically within two separate
but interconnected water -bearing zones. A shallow water -bearing zone occurs within the saprolite,
and a deeper water -bearing zone occurs within the underlying bedrock. Groundwater in the
shallow saprolite zone occurs in the interstitial pore spaces between the grains comprising the
saprolite soils. Groundwater in this zone is typically under water table or unconfined conditions.
In general, groundwater migrates laterally from recharge areas to small streams that serve as
localized discharge points.
The occurrence and movement of groundwater in the underlying water -bearing zone within the
bedrock is controlled by secondary joints, fractures, faults, and dikes within the bedrock. On a
regional scale, the direction of groundwater flow is typically from uplands to major streams and
groundwater sinks. The saprolite has a higher porosity than the bedrock and serves as a reservoir
that supplies water to a network of fractures in the bedrock.
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4.2 Site Geology and Hydrogeology
Based on previous assessment activities, the shallow soil at the Site consists primarily of silts and
sandy silts to the maximum depth of sampling of approximately 30 ft bgs. Partially weathered
rock (PWR) was encountered in the eastern portion of the Site at 15 ft bgs. Shallow soil observed
during sampling activities was comprised predominantly of red -brown silty clay. Deeper soil
observed during sampling activities was comprised predominately of dark -brown silt with trace
clay. In the LSA soil boring, obvious indication of backfill material (non-native sand) was
observed from directly beneath the asphalt pavement to approximately 7 ft bgs. A boring log with
lithologic description and monitoring well construction details is provided in Appendix C.
During previous assessment activities, groundwater was encountered at depths ranging from
approximately12 ft bgs in the central portion of the Site to 18 ft bgs in the northern portion of the
Site. The measured depth to water in the newly installed LSA monitoring well (discussed further
in Section 5.4) was approximately 13.6 ft bgs. Groundwater flow at the Site is expected to mimic
topography and flow to the east-southeast towards Derita Branch.
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5.0 Field Activities and Sampling Results
H&H conducted Phase I LSA soil and groundwater assessment activities on August 13, 2021 to
evaluate current subsurface conditions and potential risks associated with two former USTs at the
Site. The LSA sample location is depicted on Figure 4.
5.1 Geophysical Assessment/Utility Locate
Prior to conducting Phase I LSA sampling activities, H&H contacted North Carolina 811 One -
Call, the public utility locator service, to mark subsurface utilities at the Site. H&H also contracted
ISS to screen the proposed boring location for subgrade utilities. In addition to screening for
subgrade utilities, ISS conducted a geophysical survey at the Site to evaluate for the presence of
current or former tanks, tank basins, product lines, fuel dispensers, or other subsurface structures
associated with the reported USTs. The results of the geophysical survey are discussed in Section
2.0 above.
5.2 Soil Sampling Activities
On August 13, 2021, H&H contracted with Mid South to install one co -located LSA soil
boring/permanent monitoring well (identified as MW-1) within the former UST basin at the Site.
Mid South utilized a track -mounted DPT drill rig to advance the LSA soil boring to a depth of 19
ft bgs.
Continuous soil samples were collected from the boring using acetate -lined macro -core sleeves
and logged for lithologic description and screened using visual and olfactory methods for obvious
evidence of staining, unusual odors, and for the presence of volatile organic vapors using a
calibrated photoionization detector (PID). Groundwater was encountered in the soil boring at a
depth of approximately 13.6 ft bgs.
In the LSA soil boring, obvious indication of backfill material (non-native sand) was observed
from directly beneath the asphalt pavement to approximately 7 ft bgs. The results of the field
screening indicated PID readings of up to 384 parts per million -volume (ppm-v) in the residual
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SMAWER ENVIRONMENTAL SOLLMONS

soil located beneath the backfill material. No indications of impact were observed within the
backfill material. Because the fill material did not exhibit obvious indication of impact, soil
samples were not collected from that interval. H&H collected one soil sample from the first one -
foot interval located immediately below the fill material (7 to 8 ft bgs) and one soil sample just
above the saturated zone (10 to 11 ft bgs) for laboratory analysis. A boring log that includes a well
construction diagram and a well construction record are provided in Appendix C.
The soil samples were collected directly into laboratory supplied sample containers. The sample
containers were labeled with the sample identification, date, and requested analysis, placed in a
laboratory supplied cooler with ice, and delivered under standard chain -of -custody protocol to
Pace, a NC -certified laboratory, for analysis of the "risk -based" parameters including VOCs by
EPA Method 8260, SVOCs by EPA Method 8270, and EPH/VPH by the MADEP method.
5.3 Soil Sample Analytical Results
A tabular summary of soil sample analytical results is presented in Table 3. The laboratory
analytical report and chain of custody record are provided in Appendix D. The results were
compared to the DEQ UST Section Soil -to -Water, Residential, and Industrial/Commercial
MSCCs.
Laboratory analytical results indicate that multiple petroleum -related VOCs, SVOCs, and VPH
hydrocarbon fractions were detected in the deeper 10 to 11 ft bgs sample interval at concentrations
above their respective Soil -to -Water MSCCs. In addition, naphthalene (as a VOC) was detected
in the deeper sample interval at a concentration of 11.3 mg/kg which is above the Soil -to -Water
MSCC of 0.2 mg/kg and the Residential MSCC of 5.5 mg/kg, but below the Industrial/Commercial
MSCC of 27 mg/kg. The VPH hydrocarbon fraction C5 to C8 aliphatics was detected in the deeper
sample interval at a concentration of 1,520 mg/kg, which is above the Soil -to -Water MSCC of 68
mg/kg and the Residential MSCC of 625 mg/kg, but below the Industrial/Commercial MSCC of
9,340 mg/kg. No other compounds were detected at concentrations exceeding Residential MSCCs
and no compounds were detected above Industrial/Commercial MSCCs. No compounds were
detected in the shallower 7 to 8 ft bgs interval sample above MSCCs.
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SMARTER ENVIRONMENTAL SOLUTIONS

5.4 Groundwater Sampling Activities
On August 13, 2021, H&H contracted with Mid South to install one co -located LSA soil
boring/permanent monitoring well (identified as MW-1) within the former UST basin at the Site.
MW-1 was installed with a Geoprobe 6610 DPT drill rig using HSA drilling methods and was
completed as a shallow Type II monitoring well.
The monitoring well was constructed with 2-inch diameter PVC casing with 10 ft of 0.010-inch
slotted well screen set to bracket the shallow water table. A sand filter pack was placed around
the annulus of the screened interval of the well and extended to approximately two ft above the
top of the well screen. A minimum two-ft thick bentonite seal was placed above the sand pack
and hydrated. The remaining portion of the borehole annulus was filled with cement grout to
grade. The well was completed with a steel flush -mount cover set inside a two ft by two ft concrete
pad.
The newly installed monitoring well was developed using a decontaminated submersible pump
and dedicated tubing until field parameters of pH, temperature, turbidity, and specific conductivity
stabilized, the water was visually clear, and a minimum of three well volumes were removed. The
monitoring well was allowed to equilibrate to static conditions and a decontaminated electronic
water level indicator was used to measure the depth to the water table relative to the top of the
casing. The measured depth to water in the well was 13.59 ft below the top of the casing.
The groundwater sample was collected for laboratory analysis using low flow/low stress purging
techniques with a peristaltic pump and dedicated polyethylene tubing. The intake point of the
pump tubing was placed in the approximate mid -portion of the submerged well screen and
groundwater was removed at a rate of approximately 200 milliliters per minute. A water quality
meter was utilized to collect measurements of pH, temperature, dissolved oxygen, oxidation
reduction potential, turbidity, and specific conductivity at 3-5-minute intervals during the purging
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SMAWER E F IRONMEWAL SOLLMONS

process. Purging was considered complete when field parameters stabilized (pH ± 0.1 SU,
conductivity varied no more than 5%).
Following stabilization of field parameters, the groundwater sample was collected using low -flow
sampling techniques and the "soda straw" sampling method for VOCs. The groundwater sample
was collected directly into laboratory supplied sample containers. The sample containers were
labeled with the sample identification, date, and requested analysis, placed in a laboratory supplied
cooler, covered with ice, and delivered under standard chain -of -custody protocol to Pace for
laboratory analysis of VOCs/602 Volatiles by EPA Method 6200, Base Neutral and Acid Extractable
SVOCs plus the 10 highest TICS by EPA Method 625, VPH and EPH by MADEP, and lead by EPA
Method 6020.
5.5 Groundwater Sample Analytical Results
Laboratory analytical results indicate that naphthalene (as a VOC) was detected at concentrations
of up to 10.1 µg/L in LSA monitoring well MW-1 (former UST basin), which is above the 2L
Standard of 6 µg/L and below the GCL of 6,000 µg/L. In addition, the VPH hydrocarbon fraction
C9 to C10 aromatics was detected at a concentration of 253 µg/L, which is above the 2L Standard
of 200 µg/L. No GCLs have been established for VPH. No other compounds were reported at
concentrations above 2L Standards, and no compounds were reported above GCLs. Lead was not
detected in the groundwater sample above the laboratory detection limit. The laboratory analytical
report and chain of custody record are provided in Appendix D.
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SMARTER EIMROFMENOLL SOLUTIONS

6.0 Conclusions and Recommendations
The results of the Phase I LSA indicate the presence of petroleum compounds in soil above
Residential MSCCs, but below Industrial/Commercial MSCCs. The results of the groundwater
sampling indicate that two compounds were detected above 2L Standards but below GCLs. In
addition, municipal water is supplied to properties located within the Site area and no water supply
wells used for any purpose were identified within 1,500 ft of the source of the release. Therefore,
the Site qualifies for a low -risk classification. The Site is zoned for heavy industrial use, and the
surrounding properties are zoned for industrial use. Based on its current and future use, the Site
qualifies as a commercial land use classification. Based upon the results of the Phase I LSA, H&H
recommends that NC DEQ issue a risk -based NFA determination pending filing of a NORP
limiting the Site to commercial/industrial use and restricting groundwater use at the Site.
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SMARTER ENVIRONMENOLL SOLUTIONS

Tables

Table 1
UST Information
Former Metrolina Steel
1118 West Craighead Road
Charlotte, North Carolina
H&H Job No. AGL-003
DECRIPTION OF
RELEASE
UST ID
CAPACITY
CONSTRUCTION
PIPING AND
ASSOCIATED WITH
NUMBER
PREVIOUS CONTENTS
(GALLONS)
DETAILS
PUMPS
STATUS OF UST
SYSTEM?
INCIDENT NUMBER
1
Diesel
8,000
Single -Walled Steel
Unknown
Permanently Closed by Removal
Yes
47936
2
Gasoline
1,000
Single -Walled Steel
Unknown
Permanently Closed by Removal
Yes
47936
Notes:
UST information obtained from NC DEQ UST Database
Table 1 (Page 1 of 1)
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Table 2
Summary of Adjacent Properties
Former Metrolina Steel
1118 West Craighead Road
Charlotte, North Carolina
H&H Job No. AGL-003
Direction
Parcel ID No.
Map ID
Zoning
Property Street Address
Owner
Owner Address
From Site
8704104
A
Heavy
Industrial
1200 W Craighead Road
LMA Transportation, Inc.
1200 W Craighead Road, Charlotte, NC 28206
West and
Southwest
8704115
B
Light Industrial
3901 Pine Grove Circle
Sparcraft America, Inc.
3901 Pine Grove Circle, Charlotte, NC 28206
West and North
8704118
C
Light Industrial
1007 Amble Drive
Mecklenburg County
600 E 4th Street, 11th Floor, Charlotte, NC 28202
East
8704108
D
Light Industrial
926 W Craighead Road
Mecklenburg County
600 E 4th Street, 11th Floor, Charlotte, NC 28202
Southeast
8704106
E
Heavy
848 W Craighead Road
T L and Cornelisa G Shoupe
1100 Dooley Drive, Charlotte, NC 28212
Southeast
Industrial
8704111
F
Heavy
Industrial
1016 W Craighead Road
Legacy Capital Investments, Inc.
P.O. Box 37333, Charlotte, NC 28237
Southeast
8704112
G
Heavy
1100 W Craighead Road
Allman Company Charlotte, LLC
496 W Ann Arbor Trail, Suite 204, Plymouth, MI 48170
Southeast
Industrial
8509111
H
Heavy
2020 Derita Creek Road
Phillip Teller and Amy Li Matlock
45 Wall Street, Apt 705, New York, NY 10005
South
Industrial
Irrevocable Trust
8509103
1
Heavy
1101 W Craighead Road
SAIA Motor Freight Line, Inc.
P.O. Box A Station, Houma, LA 70363
South
Industrial
Notes:
Property and zoning information obtained from Mecklenburg County Polaris 3G online database
Adjacent properties are shown on Figure 3
Table 2 (Page 1 of 1)
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Table 3
Summary of Soil Analytical Results
Former Metrolina Steel
1118 West Craighead Road
Charlotte, North Carolina
H&H Job No. AGL-003
Screening Levels'
Former UST Basin
Area of Concern
Soil -to -Water
Residential
Industrial/
Sample ID
MW-1 (7-8)
MW-1 (10-11)
Commercial
Depth (ft bgs)
7-8
10-11
MSCCs
MSCCs
MSCCs
Sample Date
08/13/21
08/13/21
VOCs (8260)
Benzene
<0.0036
0.146
0.0072
12
59.4
Chloroform
0.0069 J
<0.0697
0.34
21
105
n-Butylbenzene
<0.0043
7.01
2.4
782
11,600
1,3-Dichlorobenzene
<0.0028
0.145
7.6
460
7,000
Ethylbenzene
<0.0042
13.6
8.0
60.3
297
Methyl isobutyl ketone (MIBK)
<0.0087
2.31
0.42
1,250
18,600
Naphthalene
<0.0048
11.3
0.2
5.5
27
Styrene
<0.0024
0.196
0.9
3,120
46,700
Toluene
<0.0026
0.262
5.4
1,250
18,600
1,2,4-Trimethylbenzene
<0.0025
84.3
6.6
156
2,330
1,3,5-Trimethylbenzene
<0.003
23.6
6.6
156
2,330
Xylene (total)
<0.0052
44.4
6.0
3,120
46,700
m&p-Xylene
<0.0062
37.5
6.0
3,120
46,700
o-Xylene
<0.004
6.87
6.0
3120
46,700
SVOCs (8270)
1 -M ethyl naphthalene
<0.138
0.856
0.054
22.8
112
2-Methyl naphthalene
<0.157
1.7
1.5
62.5
934
Naphthalene
<0.133
1.36
0.2
5.5
27
VPH (MADEP)
C5-C8 Aliphatics
<4.9
1,520
68
625
9,340
C9-C12Aliphatics
<4.9
703
540
1,560
23,300
C9-C10 Aromatics
<4.9
457
31
469
7,000
EPH (MADEP)
C9-C18Aliphatics
<11.8
<12.7
540
1,560
23,300
C19-C36 Aliphatics
<11.8
<12.7
NE
31,200
467,000
C11-C22 Aromatics
<11.8
<12.7
31
469
7,000
Notes:
1) NC DEQ UST Section Maximum Soil Contaminant Concentration Levels (MSCCs; dated July 9, 2021)
All concentrations are shown in milligrams per kilogram (mg/kg)
Bold indicates an exceedance of the Soil -to -Water MSCC
Underlined indicates an exceedance of the Residential MSCC
Method number follows parameter in parenthesis
VOCs = volatile organic compounds; SVOCs = semi -volatile organic compounds
EPH = exctractable petroleum hydrocarbons; VPH = volatile petroleum hydrocarbons; NE = not established
Table 3 (Page 1 of 1)
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Table 4
Summary of Groundwater Analytical Results
Former Metrolina Steel
1118 West Craighead Road
Charlotte, North Carolina
H&H Job No. AGL-003
Screening Criteria
Former UST Basin
Area of Concern
2L Groundwater
Gross Contamination
Sample ID
MW-1
Quality Standard'
Levels2
Sample Date
8/13/21
VOCs (6200)
Benzene
0.44 J
1
5,000
n-Butylbenzene
3.3
70
5,900
Ethylbenzene
29.5
600
80,000
Isopropylbenzene (Cumene)
4.0
70
30,500
Methyl-tert-butyl ether
0.53
20
20,000
Naphthalene
9.9
6
6,000
n-Propylbenzene
11.6
70
26,100
Toluene
0.66
600
260,000
1,2,4-Trimethylbenzene
68.2
400
28,500
1,3,5-Trimethylbenzene
16.9
400
24,100
m&p-Xylene
68.8
500
50,000
o-Xylene
13.7
500
50,000
602 VOCs + Xylenes (6200)
Ethylbenzene
29.2
600
80,000
Isopropylbenzene (Cumene)
4.0
70
30,500
Methyl-tert-butyl ether
0.54 J
20
20,000
Naphthalene
10.1
6
6,000
Toluene
0.65 J
600
260,000
m&p-Xylene
68.6
500
50,000
o-Xylene
13.7
500
50,000
Base/Neutral and Acid (625.11
Naphthalene
5.0
6
6,000
1,2-Dibromoethane (EDB; 504.1)
EDB
<0.013
0.02
50
VPH (MADEP)
C5-C8 Aliphatics
171
400
NE
C9-C12 Aliphatics
305
700
NE
C9-C10 Aromatics
253
200
NE
EPH (MADEP)
C9-C18 Aliphatics
<99.0
700
NE
C19-C36 Aliphatics
<99.0
10,000
NE
C11-C22 Aromatics
<99.0
200
NE
Lead (6020)
Lead
<0.14
15
15,000
Notes:
1) NCAC 02L Groundwater Quality Standards (April 2013)
2) Gross Contamination Levels (GCLs) from Tables for STIRA, Sampling, Assessment,
and Corrective Action Guidelines (July 9, 2021)
Bold indicates an exceedance of the 2L Groundwater Quality Standard
Method number follows parameter in parenthesis
VOCs = volatile organic compounds; VPH = volatile petroleum hydrocarbons
EPH = extractable petroleum hydrocarbons; NE = not established
Concentrations are presented in micrograms per liter (pg/L)
Table 4 (Page 1 of 1)
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SCALE IN FEET
U.S.G.S. QUADRANGLE MAP
DERITA, NORTH CAROLINA 2013
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)

LEGEND
SPARCRAFT AMERICA, INC.
3901 PINE GROVE CIRCLE SITE PROPERTY BOUNDARY
t
' PARCELBOUNDARY
AO AIR COMPRESSOR
AUTO BODY PARTS STORAGE
_ 0­0 ABOVEGROUND HYDRAULIC LIFT
FORMER UNDERGROUND
STORAGE TANK
t
(UST)
ALVINN BODY
}`
Do USED OIL TOTE
SHOP GARAGE
AUTO PARTS STORAGE;
1
(1) 230-GALLON
USED OIL TOTE
/
FORMER UST BASIN
+ �
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1) 8,000-GALLON DIESEL UST
2) 1,000-GALLON GASOLINE UST
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_ _
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7
HUCK'S PIGGYBACK SERVICE, INC.
USED OIL TOTE
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1200 W CRAIGHEAD ROAD
Ik
RE -COMMUNITY RECYCLING NOTES:
u Inlvrn
1007 AMBLE DRIVE -
` F 1. AERIAL IMAGERY OBTAINED FROM NC ONEMAP, 2019.
IL
f' 2. PARCEL DATA OBTAINED FROM MECKLENBURG COUNTY
I I " T ' GIS,2021.
r 'FR
T'AVIS/BUDGET CAR RENTAL
1100 W CRAIGHEAD ROAD I r r
I
/ � v
It
i/
J t
CHARLOTTE TRUCK & AUTO REPAIR
1016 W CRAIGHEAD ROAD _
850 W CRAIGHEAD
8
APPROXIMATE
0 100 200
iiiiiiiia
SCALE IN FEET
TLE
SITE MAP
RWECt FORMER METROLINA STEEL
1118 WEST CRAIGHEAD ROAD
CHARLOTTE, NORTH CAROLINA
14 2923 South Tryon Street -Suite 100
hart � hickman Charlottc,North Carolina 28203
704-586-0007(p) 704-586-0373(f
SMARTER ENVIRONMENTAL SOLUTIONS Licensc # C-1269 / #C-245 Gcolop
DATE: 8-19-21 REVISION NO. 0
JOB NO. AGL-003 FIGURE NO. 2

csq
001,
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4
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
1,500 FT — — SURFACE WATER FEATURE
GENERAL INDUSTRIAL ZONING
HEAVY INDUSTRIAL ZONING
LIGHT INDUSTRIAL ZONING
_ SINGLE FAMILY RESIDENTIAL ZONING
ADJACENT PROPERTY OWNER
(SEE TABLE 2)
NOTES:
1. PARCEL DATA, ZONING, AND AERIAL IMAGERY OBTAINED
FROM MECKLENBURG COUNTY GIS, 2021.
0 300 600
iiii
SCALE IN FEET
RECEPTOR SURVEY MAP
-� FORMER METROLINA STEEL
1118 WEST CRAIGHEAD ROAD
CHARLOTTE, NORTH CAROLINA
2923 South Tryon Street - Suite 100
hart '%• hickman Charlotte, North Carolina28203
704-586-0007 (p) 704-586-0373 (f)
RO SMARTER ENVIRONMENTAL S
• License # C-1269 / # C-245 Geology
a OLUTIONS
� • r. JOB NO. AGL-003 FRIGIRE NO O: 0

-9&
FORMER UST BASIN
1) 8,000-GALLON DIESEL UST
2) 1,000-GALLON GASOLINE UST
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LEGEND
SITE PROPERTY BOUNDARY
CO -LOCATED SOIL BORING/
MONITORING WELL LOCATION
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS, 2021.
8
APPROXIMATE
0 15 30
SCALE IN FEET
TLE
LSA SAMPLE LOCATION MAP
RWECt FORMER METROLINA STEEL
1118 WEST CRAIGHEAD ROAD
CHARLOTTE, NORTH CAROLINA
14 2923 South Tryon Street -Suite 100
hart � hickman Charlottc,NorthCarolina 28203
704-586-0007(p) 704-586-0373(f
SMARTER ENVIRONMENTAL SOLUTIONS Licensc # C-1269 / #C-245 Gcolop
DATE: 8-25-21 REVISION NO. 0
JOB NO. AGL-003 FIGURE NO. 4

Appendix A
Risk Classification and Land Use Form

Limited Site Assessment Risk Classification and Land Use Form
Part I - Groundwater/Surface WaterNapor Impacts
High Risk
1. Has the discharge or release contaminated any water supply well including
any used for non -drinking purposes?
No known water supply wells have been contaminated by the release.
2. Is a water supply well used for drinking water located within 1,000 feet of the
source area of the discharge or release?
There are no known water supply wells used for drinking water located within
1, 000 ft of the source area.
3. Is a water supply well used for any purpose (e.g., irrigation, washing cars,
industrial cooling water, filling swimming pools) located within 250 feet of
the source area of the release or discharge?
There are no known water supply wells used for any purpose located within
250 ft of the source area.
4. Does groundwater within 500 feet of the source area of the discharge or
release have the potential for future use in that there is no other source of
water supply other than the groundwater?
The subject Site and surrounding properties are serviced by the municipal
water supply.
5. Do vapors from the discharge or release pose a threat of explosion because of
accumulation of the vapors in a confined space, or pose any other serious
threat to public health, public safety or the environment?
Vapors from the discharge or release do not currently pose a threat of
explosion and do not currently pose a serious threat to public health, public
safety, or the environment.
6. Are there any other factors that would cause the discharge or release to pose
an imminent danger to public health, public safety, or the environment?
No other factors would cause the discharge or release to pose an imminent
danger to public health, public safety, or the environment.
1

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the
discharge or release?
Derita Branch is located approximately 950 ft east of the source area.
8. Is the source area of the discharge or release located within a designated
wellhead protection area as defined in 42 USC 300h-7(e)?
No, the source area is not located within a designated wellhead protection
area.
9. Is the discharge or release located in the Coastal Plain physiographic region as
designated on a map entitled "Geology of North Carolina" published by the
Department in 1985? If yes, is the source area of the discharge or release
located in an area in which there is recharge to an unconfined or semi -
confined deeper aquifer that is being used or may be used as a source of
drinking water?
No, the discharge or release is not located in the Coastal Plain physiographic
region.
10. Do the levels of groundwater contamination for any contaminant exceed the
gross contamination levels established (see Table 3) by the Department?
No, compound concentrations do not exceed their respective gross
contamination levels.
Part II - Land Use
Property Containing Source Area of Discharge or Release
1. Does the property contain one or more primary or secondary residences
(permanent or temporary)?
The property does not contain primary or secondary residences.
2. Does the property contain a school, daycare center, hospital, playground, park,
recreation area, church, nursing home, or other place of public assembly?
The property does not contain a place of public assembly.
3. Does the property contain a commercial (e.g., retail, warehouse,
officeibusiness space, etc.) or industrial (e.g., manufacturing, utilities,
industrial research and development, chemical/petroleum bulk storage, etc.)
enterprise, an inactive commercial or industrial enterprise, or is the land
undeveloped?
2

The property is developed with an industrial warehouse and is surrounded by
industrial use properties.
4. Do children visit the property?
No, children will likely not visit the property.
5. Is access to the property reliably restricted consistent with its use (e.g., by
fences, security personnel or both)?
Yes, access to the property is restricted by perimeter fencing.
6. Do pavement, buildings, or other structures cap the contaminated soil?
Yes, residual soil impacts are capped with asphalt pavement.
7. What is the zoning status of the property?
The property is zoned as Heavy Industrial (I--2).
8. Is the use of the property likely to change in the next 20 years?
The property is located within an industrial area along W. Craighead Road;
therefore, the property use is not likely to change in the next 20 years.
Property Surrounding Source Area of Discharge or Release
The questions below pertain to the area within 1500 feet of the source area of the
discharge or release (excludes property containing source area of the release):
9. What is the distance from the source area of the release to the nearest primary
or secondary residence (permanent or temporary)?
The nearest residences are located approximately 1,100 ft east of the source
area, beyond Derita Branch.
10. What is the distance from the source area of the release to the nearest school,
daycare center, hospital, playground, park, recreation area, church, nursing
home or other place of public assembly?
The Church of Christ at Sugar Creek (3932 Sofley Road) is the nearest place
of public assembly and is located approximately 2,200 feet southeast from the
source area.
11. What is the zoning status of properties in the surrounding area?
The surrounding properties are zoned as Heavy Industrial (I--2) and Light
Industrial (I-1).
3

12. Briefly characterize the use and activities of the land in the surrounding area.
The surrounding properties are occupied by various commercial/industrial
businesses, including a boat and marine manufacturing company, a towing
and trucking company, a recycling plant, a truck repair facility, a truck rental
company, and a trucking terminal. The nearest residences are located
approximately 1,100 ft east of the source area, beyond Derita Branch.
T

Appendix B
Water Supply Well Information Survey Forms

Water Supply Well Information Survey
(This line to be completed by Responsible Party or their representative)
Incident Number: 47936 Incident Name: Former Metrolina Steel
Please Provide the Following Information (to the bet of your knowledge)
Name and telephone number of person completing the survey:
Name: /%40E-' tiAIIKo
Phone #:
Address of property receiving survey:
City: Charlotte County: Mecklenburg
What is the source of your drinking wa(_bater. Pulic Water / Supply Well !Stream Intake /Other (please
explain below)
Is there a water supply well on this propert ? Yes o f "No" disregard remaining questions and return survey
Name and address of owner(s) of property with water supply well; Name:
How many water supply wells are on your property?
What is the well(s) used for? (check all that apply) Drinking , Irrigation , Swimming Pool
Water Livestock , Other (specify) You do not use the Well
How many residences are connected to the well (list addresses below)?
How deep is the well(s)? Date well was installed?
What is the casing depth of the well(s)?
What is the screen interval of the well(s)?
Additional water supply well information:
(This part to be completed by Responsible Party or their representative)
Please return completed survey to Hart & Hickman PC using one of the following methods:
1. Fax to [phone]
2. Mail to Hart & Hickman, PC
Attn: Mr. Brett Lawrence
2923 South Tryon Street, Suite 100
Charlotte, North Carolina 28203
3. Telephone [phone]
4. E-mail to [e-mail]
If you have any questions, please contact the consultant indicated above or the Mooresville UST Section Office at
[phone].

Water Supply Well Information Survey
(This line to be completed by Responsible Party or their representative)
Incident Number: 47936 Incident Name: Former Metrolina Steel
Please Provide the Following Information (to the bet of your knowledge)
Name and telephone number of person completing the survey:
Name: Alkle4,i �� to
Phone #:
Address of property receiving survey: 6Z``��
City: Charlotte County: Mecklenburg
What is the source of your drinking wat ? Public Water ater Supply Well / Stream Intake I Other (please
explain below)
Is there a water supply well on this property? Ye o If "No" disregard remaining questions and return survey
Name and address of owner(s) of property with water supply well; Name:
How many water supply wells are on your property?
What is the well(s) used for? (check all that apply) Drinking , Irrigation , Swimming Pool
Water Livestock , Other (specify) You do not use the Well
How many residences are connected to the well (list addresses below)?
How deep is the well(s)? Date well was installed?
What is the casing depth of the well(s)?
What is the screen interval of the well(s)?
Additional water supply well information:
(This part to be completed by Responsible Party or their representative)
Please return completed survey to Hart & Hickman, PC using one of the following methods:
1. Fax to [phone]
2. Mail to Hart & Hickman, PC
Attn: Mr. Brett Lawrence
2923 South Tryon Street, Suite 100
Charlotte, North Carolina 28203
3. Telephone [phone]
4. E-mail to [e-mail]
If you have any questions, please contact the consultant indicated above or the Mooresville UST Section Office at
[phone].

Water Supply Well Information Survey
(This line to be completed by Responsible Party or their representative)
Incident Number: 47936 Incident Name: Former Metrolina Steel
Please Provide the Following Information (to the bet of your knowledge)
Name and telephone number of person completing the survey:
Name: jt'm t4'01
Phone #:
Address of property receiving survey: eires
City: Charlotte County: Mecklenburg
What is the source of your drinking wat . Public Water Water Supply Well / Stream Intake / Other (please
explain below)
Is there a water supply well on this property? Yes /No If "No" disregard remaining questions and return survey
Name and address of owner(s) of property with water supply well; Name:
How many water supply wells are on your property?
What is the well(s) used for? (check all that apply) Drinking , Irrigation , Swimming Pool
Water Livestock , Other (specify) _You do not use the Well
How many residences are connected to the well (list addresses below)?
How deep is the well(s)? Date well was installed?
What is the casing depth of the well(s)?
What is the screen interval of the well(s)?
Additional water supply well information:
(This part to be completed by Responsible Party or their representative)
Please return completed survey to Hart & Hickman, PC using one of the following methods:
1. Fax to [phone]
2. Mail to Hart & Hickman, PC
Attn: Mr. Brett Lawrence
2923 South Tryon Street, Suite 100
Charlotte, North Carolina 28203
3. Telephone [phone]
4. E-mail to [e-mail]
If you have any questions, please contact the consultant indicated above or the Mooresville UST Section Office at
[phone].

Water Supply Well Information Survey
(This line to be completed by Responsible Party or their representative)
Incident Number: 47936 Incident Name: Former Metrolina Steel
Please Provide the Following Information (to the bet of your knowledge)
Name and telephone number of person completing the survey:
Name: Fp,-4 ices eA
Phone #:
Address of property receiving survey: 6167 � ��� bf�
City: Charlotte County: Mecklenburg
What is the source of your drinking wat ? Public Wate Water Supply Well / Stream Intake / Other (please
explain below)
Is there a water supply well on this property? Yes/1 No If "No" disregard remaining questions and return survey
Name and address of owner(s) of property with water supply well; Name:
How many water supply wells are on your property?
What is the well(s) used for? (check all that apply) Drinking , Irrigation , Swimming Pool
Water Livestock , Other (specify) You do not use the Well
How many residences are connected to the well (list addresses below)?
How deep is the well(s)? Date well was installed?
What is the casing depth of the well(s)?
What is the screen interval of the well(s)?
Additional water supply well information:
(This part to be completed by Responsible Party or their representative)
Please return completed survey to Hart & Hickman, PC using one of the following methods:
1. Fax to [phone]
2. Mail to Hart & Hickman, PC
Attn: Mr. Brett Lawrence
2923 South Tryon Street, Suite 100
Charlotte, North Carolina 28203
3. Telephone [phone]
4. E-mail to [e-mail]
If you have any questions, please contact the consultant indicated above or the Mooresville UST Section Office at
[phone].

Water Supply Well Information Survey
(This line to be completed by Responsible Party or their representative)
Incident Number: 47936 Incident Name: Former Metrolina Steel
Please Provide the Following Information (to the bet of your knowledge)
Name and telephone number of person completing the survey:
Name: J'1 % SfeUm.5, 1if/CleS lz �r7 e elz ,11
Phone #: /
Address of property receiving survey:
City: Charlotte County: Mecklenburg
What is the source of your drinking wa r. Public Water Water Supply Well / Stream Intake / Other (please
explain below)
Is there a water supply well on this property? Ye o If "No" disregard remaining questions and return survey
Name and address of owner(s) of property with water supply well; Name:
How many water supply wells are on your property?
What is the well(s) used for? (check all that apply) Drinking Irrigation , Swimming Pool
Water Livestock , Other (specify) You do not use the Well
How many residences are connected to the well (list addresses below)?
How deep is the well(s)? Date well was installed?
What is the casing depth of the well(s)?
What is the screen interval of the well(s)?
Additional water supply well information:
(This part to be completed by Responsible Party or their representative)
Please return completed survey to Hart & Hickman, PC using one of the following methods:
1. Fax to [phone]
2. Mail to Hart & Hickman, PC
Attn: Mr. Brett Lawrence
2923 South Tryon Street, Suite 100
Charlotte, North Carolina 28203
3. Telephone [phone]
4. E-mail to [e-mail]
If you have any questions, please contact the consultant indicated above or the Mooresville UST Section Office at
[phone].

Water Supply Well Information Survey
(This line to be completed by Responsible Party or their representative)
Incident Number: 47936 Incident Name: Former Metrolina Steel
. ........ ..
Please Provide the Following Information (to the bet of your knowledge)
Name and telephone number of person coomleting the survey: r
Name: 4&"
Phone #:
Address of property receiving survey: 12Z Z. (/,
City: Charlotte County: Mecklenburg
What is the source of your drinking w !. Public Water Water Supply Well / Stream Intake / Other (please
explain below)
Is there a water supply well on this property? Yes 6o If "No" disregard remaining questions and return survey
Name and address of owner(s) of property with water supply well; Name:
How many water supply wells are on your property?
What is the well(s) used for? (check all that apply) Drinking , Irrigation , Swimming Pool
Water Livestock , Other (specify) You do not use the Well
How many residences are connected to the well (list addresses below)?
How deep is the well(s)? Date well was installed?
What is the casing depth of the well(s)?
What is the screen interval of the well(s)?
Additional water supply well information:
(This part to be completed by Responsible Party or their representative)
Please return completed survey to Hart & Hickman, PC using one of the following methods:
1. Fax to [phone]
2. Mail to Hart & Hickman, PC
Attn: Mr. Brett Lawrence
2923 South Tryon Street, Suite 100
Charlotte, North Carolina 28203
3. Telephone [phone]
4. E-mail to [e-mail]
If you have any questions, please contact the consultant indicated above or the Mooresville UST Section Office at
[phone].

Water Supply Well Information Survey
(This line to be completed by Responsible Party or their representative)
Incident Number: 47936 Incident Name: Former Metrolina Steel
Please Provide the Following Information (to the bet of your knowledge)
Name and telleeFhone number of person completing the survey:
Name: feY� Cl/f . / rsGi��t� ����
Phone #:
Address of property receiving survey:
City: Charlotte County: Mecklenburg
What is the source of your drinking w er? Public Water / ater Supply Well / Stream Intake / Other (please
explain below)
Is there a water supply well on this property? Yes No If "No" disregard remaining questions and return survey
Name and address of owner(s) of property with water supply well; Name:
How many water supply wells are on your property?
What is the well(s) used for? (check all that apply) Drinking , Irrigation . Swimming Pool
Water Livestock , Other (specify) You do not use the Well
How many residences are connected to the well (list addresses below)?
How deep is the well(s)? Date well was installed?
What is the casing depth of the well(s)?
What is the screen interval of the well(s)?
Additional water supply well information:
(This part to be completed by Responsible Party or their representative)
Please return completed survey to Hart & Hickman, PC using one of the following methods:
1. Fax to [phone]
2. Mail to Hart & Hickman, PC
Attn: Mr. Brett Lawrence
2923 South Tryon Street, Suite 100
Charlotte, North Carolina 28203
3. Telephone [phone]
4. E-mail to [e-mail]
If you have any questions, please contact the consultant indicated above or the Mooresville UST Section Office at
[phone].

Appendix C
Boring Log and Well Construction Record

.
hart hickman
Client: Automotive Group, LLC
Project: AGL-003
WELL LOG
Well No. MW-1
I
SMARTER ENVIRONMENTAL SOLUTIONS
Address: 1118 W Craighead Rd, Charlotte, NC
Page: 1 of 1
Drilling Start Date: 8/13/2021
Boring Depth (ft): 19
Well Depth (ft): 19
Drilling End Date: 8/13/2021
Boring Diameter (in): 4.25
Well Diameter (in): 2
Drilling Company: Mid South
Sampling Method(s): Grab
Screen Slot (in): 0.010
Drilling Method: DPT/HSA
DTW During Drilling (ft):
Riser Material: Sch 40 PVC
Drilling Equipment: Geoprobe 661ODT
DTW After Drilling (ft): 13.59
Screen Material: Sch 40 PVC Slotted
Driller: Don Warren
Top of Casing Elev. (ft):
Seal Material(s): Bent. -Cement Grout/Bent.
Chips
Logged By: Thomas Vaughan
Location (X,Y):
Filter Pack: Sand Pack
COLLECT
MEASURE
_J
LU
W
z
O
_
w
O
p
J
a
N
Z
o
N
SOIL/ROCK VISUAL DESCRIPTION
n
E
a
a-
LU
w
g
�9
E
CO)
w
Q
O
U
H
o
p
o
m
m
a
m
0 0
(0') Asphalt /
0.0
(0.5') Fill: Silty Sand, moist, loose, light brown, Fill Material
0.0
10 I
0.0
Vki
0�
0.0
0.0
5
0,>
- -_
0.0
5
0.00
4.9
G
(T) Clayey SILT (ML); trace fine -medium sand, medium stiff, moist, orange and brown
383.6
(9.5') Clayey SILT (ML); stiff, moist, gray, odor
10
10
0.00
53.8
40.7
(14') Clayey SILT (ML); soft, very moist, gray, odor
15
19.7
15
(16') Silty SAND (SM); medium dense, wet, orange and brown
20
20
25 25
NOTES: Hole precleared to 5' using hand auger. Soil samples were collected from 7 to 8 and 10 to 11 ft bgs and analyzed for VOCs,
SVOCs, EPH, and VPH
generated using GroundLogs.onhne

WELL CONSTRUCTION RECORD (GW 1)
L Well Contractor Information:
For Internal Use
Donald Warren
Well Contractor Name
3581-A
NC Well Contractor Certification Number
Mid South Environmental, Inc
Company Name 2. Well Construction Permit #: SIP 70002872
List all applicable well construction permns (i. e. UIC. County, State. Variance, etc.)
3. Well Use (check well use):
Water Supply
Geothermal (Heating/Cooling Supply)
Industrial/Commercial
Non -Water Supply Well:
Aquifer Recharge
Aquifer Storage and Recovery
Aquifer Test
Experimental Technology
Geothermal (Closed Loop)
[3Municipal/Public
Residential Water Supply (single)
Residential Water Supply (shared)
Groundwater Remediation
Salinity Barrier
DStormwater Drainage
Subsidence Control
Tracer
)lain under 421 Remarks
4. Date Well(s) Completed: 8/1 3/2021 Well ID# MW-1
5a. Well Location:
Automotive Group, LLC
Facility/Owner Name Facility ID# (ifapplicable)
1118 W Craighead Rd, Charlotte, NC 28206
Physical Address, City, and Zip
Mecklenburg
County
Parcel Identification No. (PiN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
35 16' 03.32" N 80 48' 26.60"
6. Is(are) the well(s)OX Permanent or Temporary
7. Is this a repair to an existing well: ©Yes or EJNo
if this is a repair, fill out known well construction information and explain the nature of the
repair under -21 remarks section or on the hack ofthic form.
8. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same
construction, only I GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled: t
9. Total well depth below land surface: 19 (ft.)
For multiple wells list all depths ifdifferent (example- 3 2200' and 2@I00')
10. Static water level below top of casing:
Ijwater level is above casing, use "+ -
11. Borehole diameter: 4.25
12. Well construction method: Auger
(i.e. auger, rotary, cable, direct push, etc.)
14. WATER ZONES
FROM
TO
DESCRD'7'ION
fL
ft.
ft.
{t
i5.OUTER CASING for in cased wells R OLINER if a licable
FROM
TO
DlA M1fETER
THICKNESS
MATERL4L
0 ft
9 ft
2 'n'
SCh 40
PVC
16. INNER CASING OR TUBING eothermal closed -loop)
FROM
TO
DIAMETER
THICKNESS
MATERIAL
ft
ft.
in.
ft.
ft.
in.
17. SCREEN
FROM
TO
DIAMETER
SLOT SIZE
THICKNESS
M1IATERIAL
g ft.
19 ft.
2 in.
0.10
SCh 40
PVC
ft.
ft.
in.
18. GROUT
FROM
5 e.
TOIf'*Bentonite
7
ERIAL
EMPLACEMENT METHOD & AMOUNT
Pour from top
0 f`
5land
Pour from top
ft.
19. SAND/GRAVEL PACK
if a licable
FROM
TO
MATERIAL
EMPLACEMENT METHOD
7 ft-
19 ft.
Sand
Pour from top
ft.
ft.
20. DRILLING LOG attach additional sheets if necesss
FROM
TO
DESCRIPTION color, hardness, soiVmck type, grain size, Mc
0 ft-
17.5 ft-
Silt/Clay/Sand
ft.
ft
ft.
ft.
ft.
fr.
fL
ft.
fL
ft.
ft.
ft.
21. REMARKS
2I Vertification:
Signature ofCer fled Well Contractor
8/26/2021
Uate
By signing this form, 1 hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C.0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
(ft) Division of Water Resources, information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Iniection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground injection Control Program,
FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636
13a. Yield (gpm) Method or test. 24c. For Water Suvoly & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
13b. Disinfection type: Amount: completion of well construction to the county health department of the county
where constructed.
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016

Appendix D
Laboratory Analytical Report

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
August 23, 2021
Brett Lawrence
Hart & Hickman
2923 South Tryon St.
Suite 100
Charlotte, NC 28203
RE: Project: AGL-003
Pace Project No.: 92555464
Dear Brett Lawrence:
Enclosed are the analytical results for sample(s) received by the laboratory on August 13, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
1(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: AGL-003
Pace Project No.: 92555464
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: AGL-003
Pace Project No.: 92555464
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92555464001
MW-1 (7-8)
Solid
08/13/21 09:50
08/13/21 14:18
92555464002
MW-1 (10-11)
Solid
08/13/21 10:00
08/13/21 14:18
92555464003
MW-1
Water
08/13/2112:55
08/13/21 14:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
AGL-003
92555464
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92555464001
MW-1 (7-8)
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
MAD
5
PASI-C
EPA 8270E
PKS
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
92555464002
MW-1 (10-11)
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
MAD
5
PASI-C
EPA 8270E
PKS
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
92555464003
MW-1
EPA504.1
HH
2
PASI-C
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
MAD
5
PASI-C
EPA 625.1
PKS
67
PASI-C
SM 6200B
SAS
16
PASI-C
SM 6200B
SAS
61
PASI-C
PASI-C = Pace Analytical
Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1 (7-8)
Lab ID:
92555464001
Collected:
08/13/21 09:50
Received: 08/13/21 14:18 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
MADEP EPH NC Soil
Analytical
Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services
- Charlotte
Aliphatic (C09-C18)
ND
mg/kg
11.8
11.8
1
08/17/21 10:05
08/18/21 11:53
N2
Aliphatic (C19-C36)
ND
mg/kg
11.8
11.8
1
08/17/21 10:05
08/18/21 11:53
N2
Aromatic (C11-C22)
ND
mg/kg
11.8
11.8
1
08/17/21 10:05
08/18/21 11:53
N2
Surrogates
1-Chlorooctadecane (S)
86
%
40-140
1
08/17/21 10:05
08/18/21 11:53
3386-33-2
o-Terphenyl (S)
63
%
40-140
1
08/17/21 10:05
08/18/21 11:53
84-15-1
2-Fluorobiphenyl (S)
60
%
40-140
1
08/17/21 10:05
08/18/21 11:53
321-60-8
2-Bromonaphthalene (S)
47
%
40-140
1
08/17/21 10:05
08/18/21 11:53
580-13-2
VPH NC Soil
Analytical
Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services
- Charlotte
Aliphatic (C05-008)
ND
mg/kg
4.9
4.9
1
08/16/21 14:06
08/16/21 18:58
N2
Aliphatic(C09-C12)Adjusted
ND
mg/kg
4.9
4.9
1
08/16/21 14:06
08/16/21 18:58
N2
Aromatic (C09-C10)
ND
mg/kg
4.9
4.9
1
08/16/21 14:06
08/16/21 18:58
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
99
%
70-130
1
08/16/21 14:06
08/16/21 18:58
460-00-4
4-Bromofluorobenzene (PID) (S)
104
%
70-130
1
08/16/21 14:06
08/16/21 18:58
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E
Preparation Method: EPA 3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
392
138
1
08/17/21 16:34
08/18/21 22:34
83-32-9
Acenaphthylene
ND
ug/kg
392
138
1
08/17/21 16:34
08/18/21 22:34
208-96-8
Aniline
ND
ug/kg
392
153
1
08/17/21 16:34
08/18/21 22:34
62-53-3
Anthracene
ND
ug/kg
392
128
1
08/17/21 16:34
08/18/21 22:34
120-12-7
Benzo(a)anthracene
ND
ug/kg
392
131
1
08/17/21 16:34
08/18/21 22:34
56-55-3
Benzo(a)pyrene
ND
ug/kg
392
136
1
08/17/21 16:34
08/18/21 22:34
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
392
131
1
08/17/21 16:34
08/18/21 22:34
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
392
152
1
08/17/21 16:34
08/18/21 22:34
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
392
138
1
08/17/21 16:34
08/18/21 22:34
207-08-9
Benzoic Acid
ND
ug/kg
1960
843
1
08/17/21 16:34
08/18/21 22:34
65-85-0
Benzyl alcohol
ND
ug/kg
785
297
1
08/17/21 16:34
08/18/21 22:34
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
392
151
1
08/17/21 16:34
08/18/21 22:34
101-55-3
Butylbenzylphthalate
ND
ug/kg
392
165
1
08/17/21 16:34
08/18/21 22:34
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
785
276
1
08/17/21 16:34
08/18/21 22:34
59-50-7
4-Chloroaniline
ND
ug/kg
785
308
1
08/17/21 16:34
08/18/21 22:34
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
392
163
1
08/17/21 16:34
08/18/21 22:34
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
392
147
1
08/17/21 16:34
08/18/21 22:34
111-44-4
2-Chloronaphthalene
ND
ug/kg
392
156
1
08/17/21 16:34
08/18/21 22:34
91-58-7
2-Chlorophenol
ND
ug/kg
392
147
1
08/17/21 16:34
08/18/21 22:34
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
392
146
1
08/17/21 16:34
08/18/21 22:34
7005-72-3
Chrysene
ND
ug/kg
392
143
1
08/17/21 16:34
08/18/21 22:34
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
392
151
1
08/17/21 16:34
08/18/21 22:34
53-70-3
Dibenzofuran
ND
ug/kg
392
141
1
08/17/21 16:34
08/18/21 22:34
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
392
141
1
08/17/21 16:34
08/18/21 22:34
95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1 (7-8) Lab ID: 92555464001 Collected: 08/13/21 09:50 Received: 08/13/21 14:18 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
1,3-Dichlorobenzene
ND
ug/kg
392
139
1
08/17/2116:34
08/18/2122:34
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
392
150
1
08/17/2116:34
08/18/2122:34
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
785
265
1
08/17/2116:34
08/18/2122:34
91-94-1
2,4-Dichlorophenol
ND
ug/kg
392
153
1
08/17/2116:34
08/18/2122:34
120-83-2
Diethylphthalate
ND
ug/kg
392
144
1
08/17/2116:34
08/18/2122:34
84-66-2
2,4-Dimethylphenol
ND
ug/kg
392
163
1
08/17/2116:34
08/18/2122:34
105-67-9
Dimethylphthalate
ND
ug/kg
392
143
1
08/17/2116:34
08/18/2122:34
131-11-3
Di-n-butylphthalate
ND
ug/kg
392
132
1
08/17/2116:34
08/18/2122:34
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
785
366
1
08/17/2116:34
08/18/2122:34
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1960
1210
1
08/17/2116:34
08/18/2122:34
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
392
151
1
08/17/2116:34
08/18/2122:34
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
392
144
1
08/17/2116:34
08/18/2122:34
606-20-2
Di-n-octylphthalate
ND
ug/kg
392
155
1
08/17/2116:34
08/18/2122:34
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
392
152
1
08/17/2116:34
08/18/2122:34
117-81-7
Fluoranthene
ND
ug/kg
392
134
1
08/17/2116:34
08/18/2122:34
206-44-0
Fluorene
ND
ug/kg
392
138
1
08/17/2116:34
08/18/2122:34
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
392
170
1
08/17/2116:34
08/18/2122:34
87-68-3
Hexachlorobenzene
ND
ug/kg
392
153
1
08/17/2116:34
08/18/2122:34
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
392
225
1
08/17/2116:34
08/18/2122:34
77-47-4
Hexachloroethane
ND
ug/kg
392
150
1
08/17/2116:34
08/18/2122:34
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
392
155
1
08/17/2116:34
08/18/2122:34
193-39-5
Isophorone
ND
ug/kg
392
175
1
08/17/2116:34
08/18/2122:34
78-59-1
1-Methylnaphthalene
ND
ug/kg
392
138
1
08/17/2116:34
08/18/2122:34
90-12-0
2-Methylnaphthalene
ND
ug/kg
392
157
1
08/17/2116:34
08/18/2122:34
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
392
160
1
08/17/2116:34
08/18/2122:34
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
392
158
1
08/17/21 16:34
08/18/21 22:34
15831-10-4
Naphthalene
ND
ug/kg
392
133
1
08/17/2116:34
08/18/2122:34
91-20-3
2-Nitroaniline
ND
ug/kg
1960
321
1
08/17/2116:34
08/18/2122:34
88-74-4
3-Nitroaniline
ND
ug/kg
1960
308
1
08/17/2116:34
08/18/2122:34
99-09-2
4-Nitroaniline
ND
ug/kg
785
298
1
08/17/2116:34
08/18/2122:34
100-01-6
Nitrobenzene
ND
ug/kg
392
182
1
08/17/2116:34
08/18/2122:34
98-95-3
2-Nitrophenol
ND
ug/kg
392
170
1
08/17/2116:34
08/18/2122:34
88-75-5
4-Nitrophenol
ND
ug/kg
1960
759
1
08/17/2116:34
08/18/2122:34
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
392
132
1
08/17/2116:34
08/18/2122:34
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
392
147
1
08/17/2116:34
08/18/2122:34
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
392
139
1
08/17/2116:34
08/18/2122:34
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
392
187
1
08/17/2116:34
08/18/2122:34
108-60-1
Pentachlorophenol
ND
ug/kg
785
384
1
08/17/2116:34
08/18/2122:34
87-86-5
Phenanthrene
ND
ug/kg
392
128
1
08/17/2116:34
08/18/2122:34
85-01-8
Phenol
ND
ug/kg
392
175
1
08/17/2116:34
08/18/2122:34
108-95-2
Pyrene
ND
ug/kg
392
159
1
08/17/2116:34
08/18/2122:34
129-00-0
Pyridine
ND
ug/kg
392
124
1
08/17/2116:34
08/18/2122:34
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
392
155
1
08/17/2116:34
08/18/2122:34
120-82-1
2,4,5-TrichIorophenol
ND
ug/kg
392
180
1
08/17/2116:34
08/18/2122:34
95-95-4
REPORT OF LABORATORY ANALYSIS
IL
v1
v2
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1 (7-8) Lab ID: 92555464001 Collected: 08/13/21 09:50 Received: 08/13/21 14:18 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,4,6-Trichlorophenol
ND
ug/kg
392
162
1
08/17/21 16:34
08/18/21 22:34
88-06-2
Surrogates
Nitrobenzene-d5 (S)
38
%
21-130
1
08/17/21 16:34
08/18/21 22:34
4165-60-0
2-Fluorobiphenyl (S)
41
%
19-130
1
08/17/21 16:34
08/18/21 22:34
321-60-8
Terphenyl-d14 (S)
51
%
15-130
1
08/17/21 16:34
08/18/21 22:34
1718-51-0
Phenol-d6 (S)
36
%
18-130
1
08/17/21 16:34
08/18/21 22:34
13127-88-3
2-Fluorophenol (S)
36
%
18-130
1
08/17/21 16:34
08/18/21 22:34
367-12-4
2,4,6-Tribromophenol (S)
47
%
18-130
1
08/17/21 16:34
08/18/21 22:34
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method: EPA
5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
181
58.1
1
08/18/21 13:05
08/18/21 22:07
67-64-1
Benzene
ND
ug/kg
9.0
3.6
1
08/18/21 13:05
08/18/21 22:07
71-43-2
Bromobenzene
ND
ug/kg
9.0
2.9
1
08/18/21 13:05
08/18/21 22:07
108-86-1
Bromochloromethane
ND
ug/kg
9.0
2.7
1
08/18/21 13:05
08/18/21 22:07
74-97-5
Bromodichloromethane
ND
ug/kg
9.0
3.5
1
08/18/21 13:05
08/18/21 22:07
75-27-4
Bromoform
ND
ug/kg
9.0
3.2
1
08/18/21 13:05
08/18/21 22:07
75-25-2
Bromomethane
ND
ug/kg
18.1
14.3
1
08/18/21 13:05
08/18/21 22:07
74-83-9
2-Butanone (MEK)
ND
ug/kg
181
43.4
1
08/18/21 13:05
08/18/21 22:07
78-93-3
n-Butylbenzene
ND
ug/kg
9.0
4.3
1
08/18/21 13:05
08/18/21 22:07
104-51-8
sec-Butylbenzene
ND
ug/kg
9.0
4.0
1
08/18/21 13:05
08/18/21 22:07
135-98-8
tert-Butyl benzene
ND
ug/kg
9.0
3.2
1
08/18/21 13:05
08/18/21 22:07
98-06-6
Carbon tetrachloride
ND
ug/kg
9.0
3.4
1
08/18/21 13:05
08/18/21 22:07
56-23-5
Chlorobenzene
ND
ug/kg
9.0
1.7
1
08/18/21 13:05
08/18/21 22:07
108-90-7
Chloroethane
ND
ug/kg
18.1
7.0
1
08/18/21 13:05
08/18/21 22:07
75-00-3
Chloroform
6.9J
ug/kg
9.0
5.5
1
08/18/21 13:05
08/18/21 22:07
67-66-3
Chloromethane
ND
ug/kg
18.1
7.6
1
08/18/21 13:05
08/18/21 22:07
74-87-3
2-Chlorotoluene
ND
ug/kg
9.0
3.2
1
08/18/21 13:05
08/18/21 22:07
95-49-8
4-Chlorotoluene
ND
ug/kg
9.0
1.6
1
08/18/21 13:05
08/18/21 22:07
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
9.0
3.5
1
08/18/21 13:05
08/18/21 22:07
96-12-8
Dibromochloromethane
ND
ug/kg
9.0
5.1
1
08/18/21 13:05
08/18/21 22:07
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
9.0
4.0
1
08/18/21 13:05
08/18/21 22:07
106-93-4
Dibromomethane
ND
ug/kg
9.0
1.9
1
08/18/21 13:05
08/18/21 22:07
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
9.0
3.3
1
08/18/21 13:05
08/18/21 22:07
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
9.0
2.8
1
08/18/21 13:05
08/18/21 22:07
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
9.0
2.4
1
08/18/21 13:05
08/18/21 22:07
106-46-7
Dichlorodifluoromethane
ND
ug/kg
18.1
3.9
1
08/18/21 13:05
08/18/21 22:07
75-71-8
1,1-Dichloroethane
ND
ug/kg
9.0
3.7
1
08/18/21 13:05
08/18/21 22:07
75-34-3
1,2-Dichloroethane
ND
ug/kg
9.0
6.0
1
08/18/21 13:05
08/18/21 22:07
107-06-2
1,1-Dichloroethene
ND
ug/kg
9.0
3.7
1
08/18/21 13:05
08/18/21 22:07
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
9.0
3.1
1
08/18/21 13:05
08/18/21 22:07
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
9.0
3.2
1
08/18/21 13:05
08/18/21 22:07
156-60-5
1,2-Dichloropropane
ND
ug/kg
9.0
2.7
1
08/18/21 13:05
08/18/21 22:07
78-87-5
1,3-Dichloropropane
ND
ug/kg
9.0
2.8
1
08/18/21 13:05
08/18/21 22:07
142-28-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1 (7-8)
Lab ID:
92555464001
Collected:
08/13/21
09:50
Received: 08/13/21
14:18 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services
- Charlotte
2,2-Dichloropropane
ND
ug/kg
9.0
2.9
1
08/18/21 13:05
08/18/21 22:07
594-20-7
1,1-Dichloropropene
ND
ug/kg
9.0
4.3
1
08/18/21 13:05
08/18/21 22:07
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
9.0
2.5
1
08/18/21 13:05
08/18/21 22:07
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
9.0
3.1
1
08/18/21 13:05
08/18/21 22:07
10061-02-6
Diisopropyl ether
ND
ug/kg
9.0
2.4
1
08/18/21 13:05
08/18/21 22:07
108-20-3
Ethylbenzene
ND
ug/kg
9.0
4.2
1
08/18/21 13:05
08/18/21 22:07
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
18.1
14.8
1
08/18/21 13:05
08/18/21 22:07
87-68-3
2-Hexanone
ND
ug/kg
90.5
8.7
1
08/18/21 13:05
08/18/21 22:07
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
9.0
3.1
1
08/18/21 13:05
08/18/21 22:07
98-82-8
p-Isopropyltoluene
ND
ug/kg
9.0
4.5
1
08/18/21 13:05
08/18/21 22:07
99-87-6
Methylene Chloride
ND
ug/kg
36.2
24.8
1
08/18/21 13:05
08/18/21 22:07
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
90.5
8.7
1
08/18/21 13:05
08/18/21 22:07
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
9.0
3.4
1
08/18/21 13:05
08/18/21 22:07
1634-04-4
Naphthalene
ND
ug/kg
9.0
4.8
1
08/18/21 13:05
08/18/21 22:07
91-20-3
n-Propylbenzene
ND
ug/kg
9.0
3.2
1
08/18/21 13:05
08/18/21 22:07
103-65-1
Styrene
ND
ug/kg
9.0
2.4
1
08/18/21 13:05
08/18/21 22:07
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
9.0
3.5
1
08/18/21 13:05
08/18/21 22:07
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
9.0
2.4
1
08/18/21 13:05
08/18/21 22:07
79-34-5
Tetrachloroethene
ND
ug/kg
9.0
2.9
1
08/18/21 13:05
08/18/21 22:07
127-18-4
Toluene
ND
ug/kg
9.0
2.6
1
08/18/21 13:05
08/18/21 22:07
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
9.0
7.3
1
08/18/21 13:05
08/18/21 22:07
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
9.0
7.6
1
08/18/21 13:05
08/18/21 22:07
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
9.0
4.7
1
08/18/21 13:05
08/18/21 22:07
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
9.0
3.0
1
08/18/21 13:05
08/18/21 22:07
79-00-5
Trichloroethene
ND
ug/kg
9.0
2.3
1
08/18/21 13:05
08/18/21 22:07
79-01-6
Trichlorofluoromethane
ND
ug/kg
9.0
5.0
1
08/18/21 13:05
08/18/21 22:07
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
9.0
4.6
1
08/18/21 13:05
08/18/21 22:07
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
9.0
2.5
1
08/18/21 13:05
08/18/21 22:07
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
9.0
3.0
1
08/18/21 13:05
08/18/21 22:07
108-67-8
Vinyl acetate
ND
ug/kg
90.5
6.6
1
08/18/21 13:05
08/18/21 22:07
108-05-4
Vinyl chloride
ND
ug/kg
18.1
4.6
1
08/18/21 13:05
08/18/21 22:07
75-01-4
Xylene (Total)
ND
ug/kg
18.1
5.2
1
08/18/21 13:05
08/18/21 22:07
1330-20-7
m&p-Xylene
ND
ug/kg
18.1
6.2
1
08/18/21 13:05
08/18/21 22:07
179601-23-1
o-Xylene
ND
ug/kg
9.0
4.0
1
08/18/21 13:05
08/18/21 22:07
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
08/18/21 13:05
08/18/21 22:07
2037-26-5
4-Bromofluorobenzene (S)
95
%
69-134
1
08/18/21 13:05
08/18/21 22:07
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
08/18/21 13:05
08/18/21 22:07
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical Services
- Charlotte
Percent Moisture
16.4
%
0.10
0.10
1
08/16/21 12:30
N2
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM
without the written
consent of Pace Analytical Services, LLC.
Page 8 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1 (10-11)
Lab ID:
92555464002
Collected:
08/13/21 10:00
Received: 08/13/21 14:18 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
MADEP EPH NC Soil
Analytical
Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services
- Charlotte
Aliphatic (C09-C18)
ND
mg/kg
12.7
12.7
1
08/17/21 10:05
08/18/21 12:21
N2
Aliphatic (C19-C36)
ND
mg/kg
12.7
12.7
1
08/17/21 10:05
08/18/21 12:21
N2
Aromatic (C11-C22)
ND
mg/kg
12.7
12.7
1
08/17/21 10:05
08/18/21 12:21
N2
Surrogates
1-Chlorooctadecane (S)
82
%
40-140
1
08/17/21 10:05
08/18/21 12:21
3386-33-2
o-Terphenyl (S)
75
%
40-140
1
08/17/21 10:05
08/18/21 12:21
84-15-1
2-Fluorobiphenyl (S)
70
%
40-140
1
08/17/21 10:05
08/18/21 12:21
321-60-8
2-Bromonaphthalene (S)
70
%
40-140
1
08/17/21 10:05
08/18/21 12:21
580-13-2
VPH NC Soil
Analytical
Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical
Services
- Charlotte
Aliphatic (C05-CO8)
1520
mg/kg
13.6
13.6
2
08/17/21 14:56
08/18/21 06:23
N2
Aliphatic(C09-C12) Adjusted
703
mg/kg
13.6
13.6
2
08/17/21 14:56
08/18/21 06:23
N2
Aromatic (C09-C10)
457
mg/kg
13.6
13.6
2
08/17/21 14:56
08/18/21 06:23
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
298
%
70-130
2
08/17/21 14:56
08/18/21 06:23
460-00-4
S2
4-Bromofluorobenzene (PID) (S)
122
%
70-130
2
08/17/21 14:56
08/18/21 06:23
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E
Preparation Method:
EPA 3546
Pace Analytical
Services
- Charlotte
Acenaphthene
ND
ug/kg
423
149
1
08/17/21 16:34
08/18/21 23:03
83-32-9
Acenaphthylene
ND
ug/kg
423
149
1
08/17/21 16:34
08/18/21 23:03
208-96-8
Aniline
ND
ug/kg
423
165
1
08/17/21 16:34
08/18/21 23:03
62-53-3
Anthracene
ND
ug/kg
423
138
1
08/17/21 16:34
08/18/21 23:03
120-12-7
Benzo(a)anthracene
ND
ug/kg
423
141
1
08/17/21 16:34
08/18/21 23:03
56-55-3
Benzo(a)pyrene
ND
ug/kg
423
146
1
08/17/21 16:34
08/18/21 23:03
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
423
141
1
08/17/21 16:34
08/18/21 23:03
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
423
164
1
08/17/21 16:34
08/18/21 23:03
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
423
149
1
08/17/21 16:34
08/18/21 23:03
207-08-9
Benzoic Acid
ND
ug/kg
2110
908
1
08/17/21 16:34
08/18/21 23:03
65-85-0
Benzyl alcohol
ND
ug/kg
845
320
1
08/17/21 16:34
08/18/21 23:03
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
423
163
1
08/17/21 16:34
08/18/21 23:03
101-55-3
Butylbenzylphthalate
ND
ug/kg
423
178
1
08/17/21 16:34
08/18/21 23:03
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
845
297
1
08/17/21 16:34
08/18/21 23:03
59-50-7
4-Chloroaniline
ND
ug/kg
845
332
1
08/17/21 16:34
08/18/21 23:03
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
423
175
1
08/17/21 16:34
08/18/21 23:03
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
423
159
1
08/17/21 16:34
08/18/21 23:03
111-44-4
2-Chloronaphthalene
ND
ug/kg
423
168
1
08/17/21 16:34
08/18/21 23:03
91-58-7
2-Chlorophenol
ND
ug/kg
423
159
1
08/17/21 16:34
08/18/21 23:03
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
423
158
1
08/17/21 16:34
08/18/21 23:03
7005-72-3
Chrysene
ND
ug/kg
423
154
1
08/17/21 16:34
08/18/21 23:03
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
423
163
1
08/17/21 16:34
08/18/21 23:03
53-70-3
Dibenzofuran
ND
ug/kg
423
152
1
08/17/21 16:34
08/18/21 23:03
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
423
152
1
08/17/21 16:34
08/18/21 23:03
95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1 (10-11) Lab ID: 92555464002 Collected: 08/13/21 10:00 Received: 08/13/21 14:18 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
1,3-Dichlorobenzene
ND
ug/kg
423
150
1
08/17/2116:34
08/18/2123:03
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
423
161
1
08/17/2116:34
08/18/2123:03
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
845
286
1
08/17/2116:34
08/18/2123:03
91-94-1
2,4-Dichlorophenol
ND
ug/kg
423
165
1
08/17/2116:34
08/18/2123:03
120-83-2
Diethylphthalate
ND
ug/kg
423
155
1
08/17/2116:34
08/18/2123:03
84-66-2
2,4-Dimethylphenol
ND
ug/kg
423
175
1
08/17/2116:34
08/18/2123:03
105-67-9
Dimethylphthalate
ND
ug/kg
423
154
1
08/17/2116:34
08/18/2123:03
131-11-3
Di-n-butylphthalate
ND
ug/kg
423
142
1
08/17/2116:34
08/18/2123:03
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
845
395
1
08/17/2116:34
08/18/2123:03
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2110
1310
1
08/17/2116:34
08/18/2123:03
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
423
163
1
08/17/2116:34
08/18/2123:03
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
423
155
1
08/17/2116:34
08/18/2123:03
606-20-2
Di-n-octylphthalate
ND
ug/kg
423
167
1
08/17/2116:34
08/18/2123:03
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
423
164
1
08/17/2116:34
08/18/2123:03
117-81-7
Fluoranthene
ND
ug/kg
423
145
1
08/17/2116:34
08/18/2123:03
206-44-0
Fluorene
ND
ug/kg
423
149
1
08/17/2116:34
08/18/2123:03
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
423
183
1
08/17/2116:34
08/18/2123:03
87-68-3
Hexachlorobenzene
ND
ug/kg
423
165
1
08/17/2116:34
08/18/2123:03
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
423
242
1
08/17/2116:34
08/18/2123:03
77-47-4
Hexachloroethane
ND
ug/kg
423
161
1
08/17/2116:34
08/18/2123:03
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
423
167
1
08/17/2116:34
08/18/2123:03
193-39-5
Isophorone
ND
ug/kg
423
188
1
08/17/2116:34
08/18/2123:03
78-59-1
1-Methylnaphthalene
856
ug/kg
423
149
1
08/17/2116:34
08/18/2123:03
90-12-0
2-Methylnaphthalene
1700
ug/kg
423
169
1
08/17/2116:34
08/18/2123:03
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
423
173
1
08/17/2116:34
08/18/2123:03
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
423
170
1
08/17/21 16:34
08/18/21 23:03
15831-10-4
Naphthalene
1360
ug/kg
423
143
1
08/17/2116:34
08/18/2123:03
91-20-3
2-Nitroaniline
ND
ug/kg
2110
346
1
08/17/2116:34
08/18/2123:03
88-74-4
3-Nitroaniline
ND
ug/kg
2110
332
1
08/17/2116:34
08/18/2123:03
99-09-2
4-Nitroaniline
ND
ug/kg
845
322
1
08/17/2116:34
08/18/2123:03
100-01-6
Nitrobenzene
ND
ug/kg
423
196
1
08/17/2116:34
08/18/2123:03
98-95-3
2-Nitrophenol
ND
ug/kg
423
183
1
08/17/2116:34
08/18/2123:03
88-75-5
4-Nitrophenol
ND
ug/kg
2110
817
1
08/17/2116:34
08/18/2123:03
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
423
142
1
08/17/2116:34
08/18/2123:03
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
423
159
1
08/17/2116:34
08/18/2123:03
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
423
150
1
08/17/2116:34
08/18/2123:03
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
423
201
1
08/17/2116:34
08/18/2123:03
108-60-1
Pentachlorophenol
ND
ug/kg
845
414
1
08/17/2116:34
08/18/2123:03
87-86-5
Phenanthrene
ND
ug/kg
423
138
1
08/17/2116:34
08/18/2123:03
85-01-8
Phenol
ND
ug/kg
423
188
1
08/17/2116:34
08/18/2123:03
108-95-2
Pyrene
ND
ug/kg
423
172
1
08/17/2116:34
08/18/2123:03
129-00-0
Pyridine
ND
ug/kg
423
133
1
08/17/2116:34
08/18/2123:03
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
423
167
1
08/17/2116:34
08/18/2123:03
120-82-1
2,4,5-TrichIorophenol
ND
ug/kg
423
193
1
08/17/2116:34
08/18/2123:03
95-95-4
REPORT OF LABORATORY ANALYSIS
IL
v1
v2
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1 (10-11)
Lab ID:
92555464002
Collected:
08/13/21
10:00
Received: 08/13/21
14:18 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services
- Charlotte
2,4,6-Trichlorophenol
ND
ug/kg
423
174
1
08/17/21 16:34
08/18/21 23:03
88-06-2
Surrogates
Nitrobenzene-d5 (S)
57
%
21-130
1
08/17/21 16:34
08/18/21 23:03
4165-60-0
2-Fluorobiphenyl (S)
59
%
19-130
1
08/17/21 16:34
08/18/21 23:03
321-60-8
Terphenyl-d14 (S)
55
%
15-130
1
08/17/21 16:34
08/18/21 23:03
1718-51-0
Phenol-d6 (S)
51
%
18-130
1
08/17/21 16:34
08/18/21 23:03
13127-88-3
2-Fluorophenol (S)
50
%
18-130
1
08/17/21 16:34
08/18/21 23:03
367-12-4
2,4,6-Tribromophenol (S)
63
%
18-130
1
08/17/21 16:34
08/18/21 23:03
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
Acetone
ND
ug/kg
2290
736
10
08/19/21 10:23
08/19/21 12:38
67-64-1
Benzene
146
ug/kg
115
45.6
10
08/19/21 10:23
08/19/21 12:38
71-43-2
Bromobenzene
ND
ug/kg
115
37.4
10
08/19/21 10:23
08/19/21 12:38
108-86-1
Bromochloromethane
ND
ug/kg
115
33.9
10
08/19/21 10:23
08/19/21 12:38
74-97-5
Bromodichloromethane
ND
ug/kg
115
44.2
10
08/19/21 10:23
08/19/21 12:38
75-27-4
Bromoform
ND
ug/kg
115
40.3
10
08/19/21 10:23
08/19/21 12:38
75-25-2
Bromomethane
ND
ug/kg
229
181
10
08/19/21 10:23
08/19/21 12:38
74-83-9 IK
2-Butanone (MEK)
ND
ug/kg
2290
550
10
08/19/21 10:23
08/19/21 12:38
78-93-3
n-Butylbenzene
7010
ug/kg
115
54.1
10
08/19/21 10:23
08/19/21 12:38
104-51-8
sec-Butylbenzene
ND
ug/kg
115
50.4
10
08/19/21 10:23
08/19/21 12:38
135-98-8 M1
tert-Butyl benzene
ND
ug/kg
115
40.8
10
08/19/21 10:23
08/19/21 12:38
98-06-6
Carbon tetrachloride
ND
ug/kg
115
42.9
10
08/19/21 10:23
08/19/21 12:38
56-23-5
Chlorobenzene
ND
ug/kg
115
22.0
10
08/19/21 10:23
08/19/21 12:38
108-90-7
Chloroethane
ND
ug/kg
229
88.5
10
08/19/21 10:23
08/19/21 12:38
75-00-3 M1
Chloroform
ND
ug/kg
115
69.7
10
08/19/21 10:23
08/19/21 12:38
67-66-3
Chloromethane
ND
ug/kg
229
96.3
10
08/19/21 10:23
08/19/21 12:38
74-87-3
2-Chlorotoluene
ND
ug/kg
115
40.6
10
08/19/21 10:23
08/19/21 12:38
95-49-8
4-Chlorotoluene
ND
ug/kg
115
20.3
10
08/19/21 10:23
08/19/21 12:38
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
115
44.5
10
08/19/21 10:23
08/19/21 12:38
96-12-8
Dibromochloromethane
ND
ug/kg
115
64.4
10
08/19/21 10:23
08/19/21 12:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
115
50.4
10
08/19/21 10:23
08/19/21 12:38
106-93-4
Dibromomethane
ND
ug/kg
115
24.5
10
08/19/21 10:23
08/19/21 12:38
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
115
41.3
10
08/19/21 10:23
08/19/21 12:38
95-50-1
1,3-Dichlorobenzene
145
ug/kg
115
35.5
10
08/19/21 10:23
08/19/21 12:38
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
115
29.8
10
08/19/21 10:23
08/19/21 12:38
106-46-7
Dichlorodifluoromethane
ND
ug/kg
229
49.7
10
08/19/21 10:23
08/19/21 12:38
75-71-8
1,1-Dichloroethane
ND
ug/kg
115
47.2
10
08/19/21 10:23
08/19/21 12:38
75-34-3
1,2-Dichloroethane
ND
ug/kg
115
75.9
10
08/19/21 10:23
08/19/21 12:38
107-06-2
1,1-Dichloroethene
ND
ug/kg
115
47.2
10
08/19/21 10:23
08/19/21 12:38
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
115
39.2
10
08/19/21 10:23
08/19/21 12:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
115
40.1
10
08/19/21 10:23
08/19/21 12:38
156-60-5
1,2-Dichloropropane
ND
ug/kg
115
34.4
10
08/19/21 10:23
08/19/21 12:38
78-87-5
1,3-Dichloropropane
ND
ug/kg
115
35.8
10
08/19/21 10:23
08/19/21 12:38
142-28-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1 (10-11)
Lab ID:
92555464002
Collected:
08/13/21
10:00
Received: 08/13/21
14:18 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services
- Charlotte
2,2-Dichloropropane
ND
ug/kg
115
37.4
10
08/19/21 10:23
08/19/21 12:38
594-20-7
1,1-Dichloropropene
ND
ug/kg
115
55.0
10
08/19/21 10:23
08/19/21 12:38
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
115
31.2
10
08/19/21 10:23
08/19/21 12:38
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
115
39.4
10
08/19/21 10:23
08/19/21 12:38
10061-02-6
Diisopropyl ether
ND
ug/kg
115
30.9
10
08/19/21 10:23
08/19/21 12:38
108-20-3
Ethylbenzene
13600
ug/kg
115
53.4
10
08/19/21 10:23
08/19/21 12:38
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
229
187
10
08/19/21 10:23
08/19/21 12:38
87-68-3
2-Hexanone
ND
ug/kg
1150
110
10
08/19/21 10:23
08/19/21 12:38
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
115
39.0
10
08/19/21 10:23
08/19/21 12:38
98-82-8
M1
p-Isopropyltoluene
ND
ug/kg
115
56.4
10
08/19/21 10:23
08/19/21 12:38
99-87-6
M1
Methylene Chloride
ND
ug/kg
458
314
10
08/19/21 10:23
08/19/21 12:38
75-09-2
4-Methyl-2-pentanone (MIBK)
2310
ug/kg
1150
110
10
08/19/21 10:23
08/19/21 12:38
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
115
42.9
10
08/19/21 10:23
08/19/21 12:38
1634-04-4
Naphthalene
11300
ug/kg
115
60.3
10
08/19/21 10:23
08/19/21 12:38
91-20-3
n-Propylbenzene
ND
ug/kg
115
40.8
10
08/19/21 10:23
08/19/21 12:38
103-65-1
M1
Styrene
196
ug/kg
115
30.3
10
08/19/21 10:23
08/19/21 12:38
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
115
44.0
10
08/19/21 10:23
08/19/21 12:38
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
115
30.3
10
08/19/21 10:23
08/19/21 12:38
79-34-5
Tetrachloroethene
ND
ug/kg
115
36.2
10
08/19/21 10:23
08/19/21 12:38
127-18-4
Toluene
262
ug/kg
115
32.5
10
08/19/21 10:23
08/19/21 12:38
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
115
92.6
10
08/19/21 10:23
08/19/21 12:38
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
115
96.3
10
08/19/21 10:23
08/19/21 12:38
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
115
59.6
10
08/19/21 10:23
08/19/21 12:38
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
115
38.0
10
08/19/21 10:23
08/19/21 12:38
79-00-5
Trichloroethene
ND
ug/kg
115
29.6
10
08/19/21 10:23
08/19/21 12:38
79-01-6
Trichlorofluoromethane
ND
ug/kg
115
63.0
10
08/19/21 10:23
08/19/21 12:38
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
115
58.0
10
08/19/21 10:23
08/19/21 12:38
96-18-4
1,2,4-Trimethylbenzene
84300
ug/kg
115
31.4
10
08/19/21 10:23
08/19/21 12:38
95-63-6
M1
1,3,5-Trimethylbenzene
23600
ug/kg
115
38.5
10
08/19/21 10:23
08/19/21 12:38
108-67-8
M1
Vinyl acetate
ND
ug/kg
1150
83.4
10
08/19/21 10:23
08/19/21 12:38
108-05-4
Vinyl chloride
ND
ug/kg
229
58.2
10
08/19/21 10:23
08/19/21 12:38
75-01-4
Xylene (Total)
44400
ug/kg
229
65.3
10
08/19/21 10:23
08/19/21 12:38
1330-20-7
m&p-Xylene
37500
ug/kg
229
78.4
10
08/19/21 10:23
08/19/21 12:38
179601-23-1
o-Xylene
6870
ug/kg
115
50.7
10
08/19/21 10:23
08/19/21 12:38
95-47-6
Surrogates
Toluene-d8 (S)
97
%
70-130
10
08/19/21 10:23
08/19/21 12:38
2037-26-5
4-Bromofluorobenzene (S)
99
%
69-134
10
08/19/21 10:23
08/19/21 12:38
460-00-4
1,2-Dichloroethane-d4 (S)
93
%
70-130
10
08/19/21 10:23
08/19/21 12:38
17060-07-0
Percent Moisture
Analytical
Method: SW-846
Pace Analytical
Services
- Charlotte
Percent Moisture
21.4
%
0.10
0.10
1
08/16/21 12:30
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1
Lab ID: 92555464003
Collected:
08/13/21 12:55
Received: 08/13/21 14:18 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
504 GCS EDB and DBCP
Analytical Method: EPA 504.1 Preparation Method:
EPA 504.1
Pace Analytical Services
- Charlotte
1,2-Dibromoethane (EDB)
ND ug/L
0.020
0.013
1
08/17/21 11:36
08/17/21 19:54
106-93-4
Surrogates
1-Chloro-2-bromopropane (S)
92 %
70-130
1
08/17/21 11:36
08/17/21 19:54
301-79-56
MADEP EPH NC Water
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services
- Charlotte
Aliphatic (C09-C18)
ND ug/L
99.0
99.0
1
08/20/21 09:48
08/23/21 11:35
N2
Aliphatic (C19-C36)
ND ug/L
99.0
99.0
1
08/20/21 09:48
08/23/21 11:35
N2
Aromatic (C11-C22)
ND ug/L
99.0
99.0
1
08/20/21 09:48
08/23/21 11:35
N2
Surrogates
1-Chlorooctadecane (S)
27 %
40-140
1
08/20/21 09:48
08/23/21 11:35
3386-33-2
P2,S0
o-Terphenyl (S)
60 %
40-140
1
08/20/21 09:48
08/23/21 11:35
84-15-1
2-Fluorobiphenyl (S)
64 %
40-140
1
08/20/21 09:48
08/23/21 11:35
321-60-8
2-Bromonaphthalene (S)
67 %
40-140
1
08/20/21 09:48
08/23/21 11:35
580-13-2
VPH NC Water
Analytical Method: MADEP VPH
Pace Analytical Services
- Charlotte
Aliphatic (C05-008)
171 ug/L
50.0
50.0
1
08/17/21 02:35
N2
Aliphatic(C09-C12) Adjusted
305 ug/L
50.0
50.0
1
08/17/21 02:35
N2
Aromatic (C09-C10)
253 ug/L
50.0
50.0
1
08/17/21 02:35
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
95 %
70-130
1
08/17/21 02:35
460-00-4
4-Bromofluorobenzene (PID) (S)
102 %
70-130
1
08/17/21 02:35
460-00-4
625 RVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methyl phenol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
3,3'-Dichlorobenzidine
Date: 08/23/2021 04:29 PM
Analytical Method: EPA 625.1
Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
ND
ug/L
4.2
1.7
1
08/18/2106:26
08/20/2113:39
83-32-9
ND
ug/L
4.2
1.6
1
08/18/2106:26
08/20/2113:39
208-96-8
ND
ug/L
4.2
1.9
1
08/18/2106:26
08/20/2113:39
120-12-7
ND
ug/L
4.2
2.2
1
08/18/2106:26
08/20/2113:39
56-55-3
ND
ug/L
4.2
2.3
1
08/18/2106:26
08/20/2113:39
50-32-8
ND
ug/L
4.2
2.2
1
08/18/2106:26
08/20/2113:39
205-99-2
ND
ug/L
4.2
2.4
1
08/18/2106:26
08/20/2113:39
191-24-2
ND
ug/L
4.2
2.3
1
08/18/2106:26
08/20/2113:39
207-08-9
ND
ug/L
4.2
1.5
1
08/18/2106:26
08/20/2113:39
101-55-3
ND
ug/L
4.2
2.6
1
08/18/2106:26
08/20/2113:39
85-68-7
ND
ug/L
4.2
2.8
1
08/18/2106:26
08/20/2113:39
59-50-7
ND
ug/L
8.3
1.5
1
08/18/2106:26
08/20/2113:39
111-91-1
ND
ug/L
4.2
1.6
1
08/18/2106:26
08/20/2113:39
111-44-4
ND
ug/L
4.2
1.4
1
08/18/2106:26
08/20/2113:39
91-58-7
ND
ug/L
4.2
1.0
1
08/18/2106:26
08/20/2113:39
95-57-8
ND
ug/L
4.2
1.7
1
08/18/2106:26
08/20/2113:39
7005-72-3
ND
ug/L
4.2
2.3
1
08/18/2106:26
08/20/2113:39
218-01-9
ND
ug/L
4.2
2.5
1
08/18/2106:26
08/20/2113:39
53-70-3
ND
ug/L
8.3
6.8
1
08/18/2106:26
08/20/2113:39
91-94-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1 Lab ID: 92555464003 Collected: 08/13/21 12:55 Received: 08/13/21 14:18 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methyl phenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2- Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,6-TrichIorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Tentatively Identified Compounds
Ethylbenzene
o-Xylene
o-Xylene
Benzene, 1-ethyl-3-methy
ND
ug/L
4.2
1.2
1
08/18/2106:26
08/20/21 13:39
120-83-2
ND
ug/L
4.2
1.7
1
08/18/2106:26
08/20/21 13:39
84-66-2
ND
ug/L
8.3
1.4
1
08/18/2106:26
08/20/21 13:39
105-67-9
ND
ug/L
4.2
1.8
1
08/18/2106:26
08/20/21 13:39
131-11-3
ND
ug/L
4.2
1.8
1
08/18/2106:26
08/20/21 13:39
84-74-2
ND
ug/L
8.3
2.8
1
08/18/2106:26
08/20/21 13:39
534-52-1
ND
ug/L
41.7
21.7
1
08/18/2106:26
08/20/21 13:39
51-28-5
ND
ug/L
4.2
1.4
1
08/18/2106:26
08/20/21 13:39
121-14-2
ND
ug/L
4.2
1.4
1
08/18/2106:26
08/20/21 13:39
606-20-2
ND
ug/L
4.2
3.3
1
08/18/2106:26
08/20/21 13:39
117-84-0
ND
ug/L
4.2
3.1
1
08/18/2106:26
08/20/21 13:39
117-81-7
ND
ug/L
4.2
1.8
1
08/18/2106:26
08/20/21 13:39
206-44-0
ND
ug/L
4.2
1.7
1
08/18/2106:26
08/20/21 13:39
86-73-7
ND
ug/L
4.2
1.5
1
08/18/2106:26
08/20/21 13:39
87-68-3
ND
ug/L
4.2
1.8
1
08/18/2106:26
08/20/21 13:39
118-74-1
ND
ug/L
8.3
1.3
1
08/18/2106:26
08/20/21 13:39
77-47-4
ND
ug/L
4.2
1.2
1
08/18/2106:26
08/20/21 13:39
67-72-1
ND
ug/L
4.2
2.4
1
08/18/2106:26
08/20/21 13:39
193-39-5
ND
ug/L
8.3
1.4
1
08/18/2106:26
08/20/21 13:39
78-59-1
5.0
ug/L
4.2
1.7
1
08/18/2106:26
08/20/21 13:39
91-20-3
ND
ug/L
4.2
1.6
1
08/18/2106:26
08/20/21 13:39
98-95-3
ND
ug/L
4.2
1.2
1
08/18/2106:26
08/20/21 13:39
88-75-5
ND
ug/L
8.3
5.5
1
08/18/2106:26
08/20/21 13:39
100-02-7
ND
ug/L
4.2
1.6
1
08/18/2106:26
08/20/21 13:39
62-75-9
ND
ug/L
4.2
1.1
1
08/18/2106:26
08/20/21 13:39
621-64-7
ND
ug/L
8.3
2.5
1
08/18/2106:26
08/20/21 13:39
86-30-6
ND
ug/L
4.2
0.96
1
08/18/2106:26
08/20/21 13:39
108-60-1
ND
ug/L
8.3
3.1
1
08/18/2106:26
08/20/21 13:39
87-86-5
ND
ug/L
4.2
1.7
1
08/18/2106:26
08/20/21 13:39
85-01-8
ND
ug/L
4.2
1.1
1
08/18/2106:26
08/20/21 13:39
108-95-2
ND
ug/L
4.2
1.8
1
08/18/2106:26
08/20/21 13:39
129-00-0
ND
ug/L
4.2
1.4
1
08/18/2106:26
08/20/21 13:39
120-82-1
ND
ug/L
8.3
1.3
1
08/18/2106:26
08/20/21 13:39
88-06-2
59
%
10-120
1
08/18/2106:26
08/20/21 13:39
4165-60-0
50
%
15-120
1
08/18/2106:26
08/20/21 13:39
321-60-8
90
%
11-131
1
08/18/2106:26
08/20/21 13:39
1718-51-0
28
%
10-120
1
08/18/2106:26
08/20/21 13:39
13127-88-3
38
%
10-120
1
08/18/2106:26
08/20/21 13:39
367-12-4
63
%
10-137
1
08/18/2106:26
08/20/21 13:39
118-79-6
L1
L1
13.2J
ug/L
1
08/18/2106:26
08/20/21
13:39
100-41-4 N
29.8J
ug/L
1
08/18/2106:26
08/20/21
13:39
95-47-6 N
7.OJ
ug/L
1
08/18/2106:26
08/20/21
13:39
95-47-6 N
15.2J
ug/L
1
08/18/2106:26
08/20/21
13:39
620-14-4 N
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 72

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1
Lab ID:
92555464003
Collected:
08/13/21
12:55 Received: 08/13/21
14:18 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF Prepared
Analyzed
CAS No.
Qual
625 RVE
Analytical
Method: EPA 625.1 Preparation Method:
EPA 625.1
Pace Analytical Services
- Charlotte
Tentatively Identified Compounds
Benzene, 1-ethyl-2-methy
8.5J
ug/L
1 08/18/21 06:26
08/20/21 13:39
611-14-3
N
Benzene, 1,2,4-trimethyl
9.6J
ug/L
1 08/18/21 06:26
08/20/21 13:39
95-63-6
N
Benzene, 1,2,4-trimethyl
37.OJ
ug/L
1 08/18/21 06:26
08/20/21 13:39
95-63-6
N
Benzene, 1-ethyl-3-methy
9.51
ug/L
1 08/18/21 06:26
08/20/21 13:39
620-14-4
N
Unknown
5.4J
ug/L
1 08/18/21 06:26
08/20/21 13:39
602 Volatiles by Method 6200
Analytical
Method: SM 6200B
Pace Analytical Services
- Charlotte
Benzene
ND
ug/L
1.0
0.34
1
08/17/21 13:13
71-43-2
Chlorobenzene
ND
ug/L
1.0
0.28
1
08/17/21 13:13
108-90-7
1,2-Dichlorobenzene
ND
ug/L
1.0
0.34
1
08/17/21 13:13
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
0.34
1
08/17/21 13:13
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
08/17/21 13:13
106-46-7
Diisopropyl ether
ND
ug/L
1.0
0.31
1
08/17/21 13:13
108-20-3
Ethylbenzene
29.2
ug/L
1.0
0.30
1
08/17/21 13:13
100-41-4
Isopropylbenzene (Cumene)
4.0
ug/L
1.0
0.33
1
08/17/21 13:13
98-82-8
Methyl-tert-butyl ether
0.54J
ug/L
1.0
0.42
1
08/17/21 13:13
1634-04-4
Naphthalene
10.1
ug/L
2.0
0.64
1
08/17/21 13:13
91-20-3
Toluene
0.65J
ug/L
1.0
0.48
1
08/17/21 13:13
108-88-3
m&p-Xylene
68.6
ug/L
2.0
0.71
1
08/17/21 13:13
179601-23-1
o-Xylene
13.7
ug/L
1.0
0.34
1
08/17/21 13:13
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
08/17/21 13:13
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
08/17/21 13:13
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
08/17/21 13:13
2037-26-5
6200B MSV
Analytical
Method: SM 6200B
Pace Analytical Services
- Charlotte
Benzene
0.44J
ug/L
0.50
0.34
1
08/16/2118:44
71-43-2
Bromobenzene
ND
ug/L
0.50
0.29
1
08/16/2118:44
108-86-1
Bromochloromethane
ND
ug/L
0.50
0.47
1
08/16/2118:44
74-97-5
Bromodichloromethane
ND
ug/L
0.50
0.31
1
08/16/2118:44
75-27-4
Bromoform
ND
ug/L
0.50
0.34
1
08/16/2118:44
75-25-2
Bromomethane
ND
ug/L
5.0
1.7
1
08/16/2118:44
74-83-9
n-Butylbenzene
3.3
ug/L
0.50
0.49
1
08/16/2118:44
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
0.40
1
08/16/2118:44
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
0.32
1
08/16/2118:44
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
0.33
1
08/16/21 18:44
56-23-5
Chlorobenzene
ND
ug/L
0.50
0.28
1
08/16/2118:44
108-90-7
Chloroethane
ND
ug/L
1.0
0.65
1
08/16/2118:44
75-00-3
Chloroform
ND
ug/L
0.50
0.35
1
08/16/2118:44
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
08/16/2118:44
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
0.32
1
08/16/2118:44
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
0.32
1
08/16/2118:44
106-43-4
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM
without the written
consent of Pace Analytical Services, LLC.
Page 15 of 72

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1 Lab ID: 92555464003 Collected: 08/13/21 12:55 Received: 08/13/21 14:18 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Dibromochloromethane
ND
ug/L
0.50
0.36
1
08/16/21 18:44
124-48-1
Dibromomethane
ND
ug/L
0.50
0.39
1
08/16/21 18:44
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
0.34
1
08/16/21 18:44
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
0.34
1
08/16/21 18:44
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
0.33
1
08/16/21 18:44
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
0.35
1
08/16/21 18:44
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
0.37
1
08/16/21 18:44
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
0.32
1
08/16/21 18:44
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
0.35
1
08/16/21 18:44
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
0.38
1
08/16/21 18:44
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
0.40
1
08/16/21 18:44
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
0.36
1
08/16/21 18:44
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
0.28
1
08/16/21 18:44
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
0.39
1
08/16/21 18:44
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
0.43
1
08/16/21 18:44
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
0.36
1
08/16/21 18:44
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
0.36
1
08/16/21 18:44
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
0.31
1
08/16/21 18:44
108-20-3
Ethylbenzene
29.5
ug/L
0.50
0.30
1
08/16/21 18:44
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1.5
1
08/16/21 18:44
87-68-3
Isopropylbenzene (Cumene)
4.0
ug/L
0.50
0.33
1
08/16/21 18:44
98-82-8
Methylene Chloride
ND
ug/L
2.0
2.0
1
08/16/21 18:44
75-09-2
Methyl-tert-butyl ether
0.53
ug/L
0.50
0.42
1
08/16/21 18:44
1634-04-4
Naphthalene
9.9
ug/L
2.0
0.64
1
08/16/21 18:44
91-20-3
n-Propylbenzene
11.6
ug/L
0.50
0.34
1
08/16/21 18:44
103-65-1
Styrene
ND
ug/L
0.50
0.29
1
08/16/21 18:44
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
0.31
1
08/16/21 18:44
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
0.22
1
08/16/21 18:44
79-34-5
Tetrachloroethene
ND
ug/L
0.50
0.29
1
08/16/21 18:44
127-18-4
Toluene
0.66
ug/L
0.50
0.48
1
08/16/21 18:44
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
0.81
1
08/16/21 18:44
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
0.64
1
08/16/21 18:44
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
0.33
1
08/16/21 18:44
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
0.32
1
08/16/21 18:44
79-00-5
Trichloroethene
ND
ug/L
0.50
0.38
1
08/16/21 18:44
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
08/16/21 18:44
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
0.26
1
08/16/21 18:44
96-18-4
1,2,4-Trimethylbenzene
68.2
ug/L
0.50
0.50
1
08/16/21 18:44
95-63-6
1,3,5-Trimethylbenzene
16.9
ug/L
0.50
0.33
1
08/16/21 18:44
108-67-8
Vinyl chloride
ND
ug/L
1.0
0.39
1
08/16/21 18:44
75-01-4
m&p-Xylene
68.8
ug/L
1.0
0.71
1
08/16/21 18:44
179601-23-1
o-Xylene
13.7
ug/L
0.50
0.34
1
08/16/21 18:44
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
08/16/21 18:44
17060-07-0
4-Bromofluorobenzene (S)
98
%
70-130
1
08/16/21 18:44
460-00-4
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 08/23/2021 04:29 PM
without the written
consent of Pace
Analytical Services, LLC.
Page 16 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: AGL-003
Pace Project No.: 92555464
Sample: MW-1 Lab ID: 92555464003 Collected: 08/13/21 12:55 Received: 08/13/21 14:18 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Surrogates
Toluene-d8 (S) 100 % 70-130 1 08/16/21 18:44 2037-26-5
Date: 08/23/2021 04:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 640758
Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH
Analysis Description: VPH NC Water
Laboratory: Pace
Analytical Services - Charlotte
Associated Lab Samples: 92555464003
METHOD BLANK: 3362973
Matrix: Water
Associated Lab Samples: 92555464003
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Aliphatic (C05-CO8)
ug/L
ND 50.0
50.0
08/16/21 15:10
N2
Aromatic (C09-C10)
ug/L
ND 50.0
50.0
08/16/21 15:10
N2
4-Bromofluorobenzene (FID) (S)
%
100 70-130
08/16/21 15:10
4-Bromofluorobenzene (PID) (S)
%
105 70-130
08/16/21 15:10
LABORATORY CONTROL SAMPLE & LCSD:
3362974
3362975
Spike LCS LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc. Result Result
% Rec % Rec
Limits RPD
RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300 332 321
111 107
70-130
3 25 N2
Aromatic (C09-C10)
ug/L
100 110 116
110 116
70-130
6 25 N2
4-Bromofluorobenzene (FID) (S)
%
95 103
70-130
4-Bromofluorobenzene (PID) (S)
%
98 105
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 640702
Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH
Analysis Description: VPH NC Soil
Laboratory: Pace
Analytical Services - Charlotte
Associated Lab Samples: 92555464001
METHOD BLANK: 3362574
Matrix: Solid
Associated Lab Samples: 92555464001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Aliphatic (C05-CO8)
mg/kg
ND 2.5
2.5
08/16/21 15:38
N2
Aromatic (C09-C10)
mg/kg
ND 2.5
2.5
08/16/21 15:38
N2
4-Bromofluorobenzene (FID) (S)
%
95 70-130
08/16/21 15:38
4-Bromofluorobenzene (PID) (S)
%
101 70-130
08/16/21 15:38
LABORATORY CONTROL SAMPLE & LCSD:
3362575
3362576
Spike LCS LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc. Result Result
% Rec % Rec
Limits RPD
RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
15.1 15.6 14.2
103 94
70-130
9 25 N2
Aromatic (C09-C10)
mg/kg
5 5.9 5.6
117 110
70-130
6 25 N2
4-Bromofluorobenzene (FID) (S)
%
97 102
70-130
4-Bromofluorobenzene (PID) (S)
%
99 104
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 641021
Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH
Analysis Description: VPH NC Soil
Laboratory: Pace
Analytical Services - Charlotte
Associated Lab Samples: 92555464002
METHOD BLANK: 3364458
Matrix: Solid
Associated Lab Samples: 92555464002
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed Qualifiers
Aliphatic (C05-CO8)
mg/kg
ND 2.5
2.5
08/18/21 12:33 N2
Aromatic (C09-C10)
mg/kg
ND 2.5
2.5
08/18/21 12:33 N2
4-Bromofluorobenzene (FID) (S)
%
97 70-130
08/18/21 12:33
4-Bromofluorobenzene (PID) (S)
%
102 70-130
08/18/21 12:33
LABORATORY CONTROL SAMPLE & LCSD:
3364459
3364460
Spike LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc. Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
15.1 16.4 14.5
108 96
70-130 13 25 N2
Aromatic (C09-C10)
mg/kg
5 6.1 5.2
121 102
70-130 17 25 N2
4-Bromofluorobenzene (FID) (S)
%
96 98
70-130
4-Bromofluorobenzene (PID) (S)
%
98 100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 640957 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 602 by 6200B
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92555464003
METHOD BLANK: 3363908
Associated Lab Samples: 92555464003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,2-Dichlorobenzene
ug/L
ND
1.0
0.34
08/17/21 12:37
1,3-Dichlorobenzene
ug/L
ND
1.0
0.34
08/17/21 12:37
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
08/17/21 12:37
Benzene
ug/L
ND
1.0
0.34
08/17/21 12:37
Chlorobenzene
ug/L
ND
1.0
0.28
08/17/21 12:37
Diisopropyl ether
ug/L
ND
1.0
0.31
08/17/21 12:37
Ethylbenzene
ug/L
ND
1.0
0.30
08/17/21 12:37
Isopropylbenzene (Cumene)
ug/L
ND
1.0
0.33
08/17/21 12:37
m&p-Xylene
ug/L
ND
2.0
0.71
08/17/21 12:37
Methyl-tert-butyl ether
ug/L
ND
1.0
0.42
08/17/21 12:37
Naphthalene
ug/L
ND
2.0
0.64
08/17/21 12:37
o-Xylene
ug/L
ND
1.0
0.34
08/17/21 12:37
Toluene
ug/L
ND
1.0
0.48
08/17/21 12:37
1,2-Dichloroethane-d4 (S)
%
98
70-130
08/17/21 12:37
4-Bromofluorobenzene (S)
%
100
70-130
08/17/21 12:37
Toluene-d8 (S)
%
100
70-130
08/17/21 12:37
LABORATORY CONTROL SAMPLE:
Parameter
3363909
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dichlorobenzene
ug/L
50
50.7
101
60-140
1,3-Dichlorobenzene
ug/L
50
51.4
103
60-140
1,4-Dichlorobenzene
ug/L
50
51.0
102
60-140
Benzene
ug/L
50
49.5
99
60-140
Chlorobenzene
ug/L
50
49.8
100
60-140
Diisopropyl ether
ug/L
50
46.7
93
60-140
Ethylbenzene
ug/L
50
49.7
99
60-140
Isopropylbenzene (Cumene)
ug/L
50
50.9
102
60-140
m&p-Xylene
ug/L
100
99.0
99
60-140
Methyl-tert-butyl ether
ug/L
50
46.6
93
60-140
Naphthalene
ug/L
50
45.8
92
60-140
o-Xylene
ug/L
50
48.0
96
60-140
Toluene
ug/L
50
49.5
99
60-140
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
99
70-130
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3363910
3363911
MS
MSD
92555464003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
1,2-Dichlorobenzene
ug/L
ND
20
20
22.0
21.7
110
108
60-140
1
30
1,3-Dichlorobenzene
ug/L
ND
20
20
22.5
21.8
113
109
60-140
3
30
1,4-Dichlorobenzene
ug/L
ND
20
20
22.1
21.8
110
109
60-140
1
30
Benzene
ug/L
ND
20
20
22.0
21.8
110
109
60-140
1
30
Chlorobenzene
ug/L
ND
20
20
22.5
22.5
112
113
60-140
0
30
Diisopropyl ether
ug/L
ND
20
20
21.3
20.6
106
102
60-140
3
30
Ethylbenzene
ug/L
29.2
20
20
54.3
53.7
125
123
60-140
1
30
Isopropylbenzene
ug/L
4.0
20
20
27.8
27.9
119
120
60-140
0
30
(Cumene)
m&p-Xylene
ug/L
68.6
40
40
119
117
126
120
60-140
2
30
Methyl-tert-butyl ether
ug/L
0.54J
20
20
21.8
21.2
106
103
60-140
3
30
Naphthalene
ug/L
10.1
20
20
32.4
32.4
112
112
60-140
0
30
o-Xylene
ug/L
13.7
20
20
37.3
36.8
118
115
60-140
1
30
Toluene
ug/L
0.65J
20
20
22.6
22.1
110
107
60-140
2
30
1,2-Dichloroethane-d4 (S)
%
101
101
70-130
4-Bromofluorobenzene (S)
%
99
100
70-130
Toluene-d8 (S)
%
98
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 640682 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92555464003
METHOD BLANK: 3362480
Associated Lab Samples: 92555464003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
0.31
08/16/21 11:12
1,1,1-Trichloroethane
ug/L
ND
0.50
0.33
08/16/21 11:12
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
0.22
08/16/21 11:12
1,1,2-Trichloroethane
ug/L
ND
0.50
0.32
08/16/21 11:12
1,1-Dichloroethane
ug/L
ND
0.50
0.37
08/16/21 11:12
1,1-Dichloroethene
ug/L
ND
0.50
0.35
08/16/21 11:12
1,1-Dichloropropene
ug/L
ND
0.50
0.43
08/16/21 11:12
1,2,3-Trichlorobenzene
ug/L
ND
2.0
0.81
08/16/21 11:12
1,2,3-Trichloropropane
ug/L
ND
0.50
0.26
08/16/21 11:12
1,2,4-Trichlorobenzene
ug/L
ND
2.0
0.64
08/16/21 11:12
1,2,4-Trimethylbenzene
ug/L
ND
0.50
0.50
08/16/21 11:12
1,2-Dichlorobenzene
ug/L
ND
0.50
0.34
08/16/21 11:12
1,2-Dichloroethane
ug/L
ND
0.50
0.32
08/16/21 11:12
1,2-Dichloropropane
ug/L
ND
0.50
0.36
08/16/21 11:12
1,3,5-Trimethylbenzene
ug/L
ND
0.50
0.33
08/16/21 11:12
1,3-Dichlorobenzene
ug/L
ND
0.50
0.34
08/16/21 11:12
1,3-Dichloropropane
ug/L
ND
0.50
0.28
08/16/21 11:12
1,4-Dichlorobenzene
ug/L
ND
0.50
0.33
08/16/21 11:12
2,2-Dichloropropane
ug/L
ND
0.50
0.39
08/16/21 11:12
2-Chlorotoluene
ug/L
ND
0.50
0.32
08/16/21 11:12
4-Chlorotoluene
ug/L
ND
0.50
0.32
08/16/21 11:12
Benzene
ug/L
ND
0.50
0.34
08/16/21 11:12
Bromobenzene
ug/L
ND
0.50
0.29
08/16/21 11:12
Bromochloromethane
ug/L
ND
0.50
0.47
08/16/21 11:12
Bromodichloromethane
ug/L
ND
0.50
0.31
08/16/21 11:12
Bromoform
ug/L
ND
0.50
0.34
08/16/21 11:12
Bromomethane
ug/L
ND
5.0
1.7
08/16/21 11:12
Carbon tetrachloride
ug/L
ND
0.50
0.33
08/16/21 11:12
Chlorobenzene
ug/L
ND
0.50
0.28
08/16/21 11:12
Chloroethane
ug/L
ND
1.0
0.65
08/16/21 11:12
Chloroform
ug/L
ND
0.50
0.35
08/16/21 11:12
Chloromethane
ug/L
ND
1.0
0.54
08/16/21 11:12
cis-1,2-Dichloroethene
ug/L
ND
0.50
0.38
08/16/21 11:12
cis-1,3-Dichloropropene
ug/L
ND
0.50
0.36
08/16/21 11:12
Dibromochloromethane
ug/L
ND
0.50
0.36
08/16/21 11:12
Dibromomethane
ug/L
ND
0.50
0.39
08/16/21 11:12
Dichlorodifluoromethane
ug/L
ND
0.50
0.35
08/16/21 11:12
Diisopropyl ether
ug/L
ND
0.50
0.31
08/16/21 11:12
Ethylbenzene
ug/L
ND
0.50
0.30
08/16/21 11:12
Hexachloro-1,3-butadiene
ug/L
ND
2.0
1.5
08/16/21 11:12
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
METHOD BLANK: 3362480
Associated Lab Samples: 92555464003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Isopropylbenzene (Cumene)
ug/L
ND
0.50
0.33
08/16/21 11:12
m&p-Xylene
ug/L
ND
1.0
0.71
08/16/21 11:12
Methyl-tert-butyl ether
ug/L
ND
0.50
0.42
08/16/21 11:12
Methylene Chloride
ug/L
ND
2.0
2.0
08/16/21 11:12
n-Butylbenzene
ug/L
ND
0.50
0.49
08/16/21 11:12
n-Propylbenzene
ug/L
ND
0.50
0.34
08/16/21 11:12
Naphthalene
ug/L
ND
2.0
0.64
08/16/21 11:12
o-Xylene
ug/L
ND
0.50
0.34
08/16/21 11:12
sec-Butylbenzene
ug/L
ND
0.50
0.40
08/16/21 11:12
Styrene
ug/L
ND
0.50
0.29
08/16/21 11:12
tert-Butyl benzene
ug/L
ND
0.50
0.32
08/16/21 11:12
Tetrachloroethene
ug/L
ND
0.50
0.29
08/16/21 11:12
Toluene
ug/L
ND
0.50
0.48
08/16/21 11:12
trans-1,2-Dichloroethene
ug/L
ND
0.50
0.40
08/16/21 11:12
trans- 1,3-Dichloropropene
ug/L
ND
0.50
0.36
08/16/21 11:12
Trichloroethene
ug/L
ND
0.50
0.38
08/16/21 11:12
Trichlorofluoromethane
ug/L
ND
1.0
0.30
08/16/21 11:12
Vinyl chloride
ug/L
ND
1.0
0.39
08/16/21 11:12
1,2-Dichloroethane-d4 (S)
%
102
70-130
08/16/21 11:12
4-Bromofluorobenzene (S)
%
98
70-130
08/16/21 11:12
Toluene-d8 (S)
%
100
70-130
08/16/21 11:12
LABORATORY CONTROL SAMPLE:
Parameter
3362481
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.3
103
60-140
1,1,1-Trichloroethane
ug/L
50
52.7
105
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
48.3
97
60-140
1,1,2-Trichloroethane
ug/L
50
49.1
98
60-140
1,1-Dichloroethane
ug/L
50
50.5
101
60-140
1,1-Dichloroethene
ug/L
50
53.1
106
60-140
1,1-Dichloropropene
ug/L
50
52.5
105
60-140
1,2,3-Trichlorobenzene
ug/L
50
47.2
94
60-140
1,2,3-Trichloropropane
ug/L
50
47.8
96
60-140
1,2,4-Trichlorobenzene
ug/L
50
48.3
97
60-140
1,2,4-Trimethylbenzene
ug/L
50
50.0
100
60-140
1,2-Dichlorobenzene
ug/L
50
51.2
102
60-140
1,2-Dichloroethane
ug/L
50
48.3
97
60-140
1,2-Dichloropropane
ug/L
50
51.1
102
60-140
1,3,5-Trimethylbenzene
ug/L
50
49.8
100
60-140
1,3-Dichlorobenzene
ug/L
50
52.1
104
60-140
1,3-Dichloropropane
ug/L
50
49.1
98
60-140
1,4-Dichlorobenzene
ug/L
50
50.3
101
60-140
2,2-Dichloropropane
ug/L
50
53.5
107
60-140
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
LABORATORY CONTROL SAMPLE:
Parameter
3362481
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2-Chlorotoluene
ug/L
50
51.8
104
60-140
4-Chlorotoluene
ug/L
50
49.9
100
60-140
Benzene
ug/L
50
51.2
102
60-140
Bromobenzene
ug/L
50
49.2
98
60-140
Bromochloromethane
ug/L
50
52.0
104
60-140
Bromodichloromethane
ug/L
50
48.9
98
60-140
Bromoform
ug/L
50
54.4
109
60-140
Bromomethane
ug/L
50
52.1
104
60-140
Carbon tetrachloride
ug/L
50
52.9
106
60-140
Chlorobenzene
ug/L
50
51.3
103
60-140
Chloroethane
ug/L
50
48.7
97
60-140
Chloroform
ug/L
50
51.3
103
60-140
Chloromethane
ug/L
50
42.8
86
60-140
cis-1,2-Dichloroethene
ug/L
50
49.3
99
60-140
cis-1,3-Dichloropropene
ug/L
50
52.2
104
60-140
Dibromochloromethane
ug/L
50
53.9
108
60-140
Dibromomethane
ug/L
50
52.2
104
60-140
Dichlorodifluoromethane
ug/L
50
47.8
96
60-140
Diisopropyl ether
ug/L
50
48.0
96
60-140
Ethylbenzene
ug/L
50
50.9
102
60-140
Hexachloro-1,3-butadiene
ug/L
50
50.4
101
60-140
Isopropylbenzene (Cumene)
ug/L
50
52.5
105
60-140
m&p-Xylene
ug/L
100
102
102
60-140
Methyl-tert-butyl ether
ug/L
50
47.6
95
60-140
Methylene Chloride
ug/L
50
50.4
101
60-140
n-Butylbenzene
ug/L
50
52.4
105
60-140
n-Propylbenzene
ug/L
50
50.3
101
60-140
Naphthalene
ug/L
50
45.6
91
60-140
o-Xylene
ug/L
50
49.8
100
60-140
sec-Butylbenzene
ug/L
50
50.4
101
60-140
Styrene
ug/L
50
51.1
102
60-140
tert-Butyl benzene
ug/L
50
42.6
85
60-140
Tetrachloroethene
ug/L
50
52.3
105
60-140
Toluene
ug/L
50
50.9
102
60-140
trans-1,2-Dichloroethene
ug/L
50
51.5
103
60-140
trans- 1,3-Dichloropropene
ug/L
50
52.1
104
60-140
Trichloroethene
ug/L
50
53.1
106
60-140
Trichlorofluoromethane
ug/L
50
49.9
100
60-140
Vinyl chloride
ug/L
50
47.7
95
60-140
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
100
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 72

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3362482
MS
92554290005 Spike
Parameter Units Result Conc.
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1, 2,2-Tetrachloroethane
1,1, 2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethyl benzene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethyl benzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene
(Cumene)
m&p-Xylene
Methyl-tert-butyl ether
Methylene Chloride
n-Butylbenzene
3362483
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits
ug/L
ND
2500
2500
2420
2490
97
100
60-140
ug/L
ND
2500
2500
2780
2750
111
110
60-140
ug/L
ND
2500
2500
2350
2350
94
94
60-140
ug/L
ND
2500
2500
2340
2350
94
94
60-140
ug/L
ND
2500
2500
2650
2680
106
107
60-140
ug/L
ND
2500
2500
2960
2850
119
114
60-140
ug/L
ND
2500
2500
2830
2810
113
112
60-140
ug/L
ND
2500
2500
2360
2410
94
96
60-140
ug/L
ND
2500
2500
2330
2350
93
94
60-140
ug/L
ND
2500
2500
2410
2390
96
96
60-140
ug/L
ND
2500
2500
2480
2460
99
98
60-140
ug/L
ND
2500
2500
2500
2480
100
99
60-140
ug/L
ND
2500
2500
2490
2510
99
100
60-140
ug/L
ND
2500
2500
2480
2480
99
99
60-140
ug/L
ND
2500
2500
2480
2480
99
99
60-140
ug/L
ND
2500
2500
2590
2590
103
103
60-140
ug/L
ND
2500
2500
2420
2410
97
96
60-140
ug/L
ND
2500
2500
2490
2510
99
100
60-140
ug/L
ND
2500
2500
2780
2910
111
116
60-140
ug/L
ND
2500
2500
2540
2530
102
101
60-140
ug/L
ND
2500
2500
2490
2490
100
100
60-140
ug/L
49.8J
2500
2500
2550
2620
100
103
60-140
ug/L
ND
2500
2500
2460
2430
98
97
60-140
ug/L
ND
2500
2500
2580
2650
103
106
60-140
ug/L
ND
2500
2500
2250
2290
90
92
60-140
ug/L
ND
2500
2500
2340
2450
94
98
60-140
ug/L
ND
2500
2500
2640
2970
106
119
60-140
ug/L
ND
2500
2500
2570
2680
103
107
60-140
ug/L
ND
2500
2500
2520
2540
101
102
60-140
ug/L
ND
2500
2500
2680
2770
107
111
60-140
ug/L
ND
2500
2500
2630
2620
105
105
60-140
ug/L
ND
2500
2500
2040
2120
82
85
60-140
ug/L
ND
2500
2500
2590
2600
103
104
60-140
ug/L
ND
2500
2500
2450
2480
98
99
60-140
ug/L
ND
2500
2500
2480
2510
99
100
60-140
ug/L
ND
2500
2500
2500
2510
100
100
60-140
ug/L
ND
2500
2500
2220
2240
89
90
60-140
ug/L
ND
2500
2500
2420
2470
96
98
60-140
ug/L
ND
2500
2500
2510
2540
100
101
60-140
ug/L
ND
2500
2500
2550
2610
102
105
60-140
ug/L
ND
2500
2500
2580
2600
103
104
60-140
Max
RPD RPD Qual
3 30
1 30
0 30
0 30
1 30
4 30
0 30
2 30
1 30
1 30
1 30
1 30
1 30
0 30
0 30
0 30
1 30
1 30
4 30
0 30
0 30
3 30
1 30
3 30
2 30
4 30
12 30
4 30
1 30
3 30
0 30
4 30
0 30
1 30
1 30
0 30
1 30
2 30
1 30
2 30
1 30
ug/L
ND
5000
5000
5000
5030
100
101
60-140
1
30
ug/L
20100
2500
2500
22900
23200
114
124
60-140
1
30
ug/L
ND
2500
2500
2580
2570
103
103
60-140
0
30
ug/L
ND
2500
2500
2610
2630
104
105
60-140
1
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3362482
3362483
MS
MSD
92554290005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
n-Propylbenzene
ug/L
ND
2500
2500
2560
2560
102
102
60-140
0
30
Naphthalene
ug/L
ND
2500
2500
2230
2300
89
92
60-140
3
30
o-Xylene
ug/L
ND
2500
2500
2420
2440
97
98
60-140
1
30
sec-Butylbenzene
ug/L
ND
2500
2500
2570
2560
103
103
60-140
0
30
Styrene
ug/L
ND
2500
2500
2450
2480
98
99
60-140
1
30
tert-Butylbenzene
ug/L
ND
2500
2500
2160
2130
86
85
60-140
1
30
Tetrachloroethene
ug/L
ND
2500
2500
2620
2650
105
106
60-140
1
30
Toluene
ug/L
ND
2500
2500
2490
2570
100
103
60-140
3
30
trans-1,2-Dichloroethene
ug/L
ND
2500
2500
2690
2730
108
109
60-140
1
30
trans-1,3-Dichloropropene
ug/L
ND
2500
2500
2400
2450
96
98
60-140
2
30
Trichloroethene
ug/L
ND
2500
2500
2590
2620
104
105
60-140
1
30
Trichlorofluoromethane
ug/L
ND
2500
2500
2700
2780
108
111
60-140
3
30
Vinyl chloride
ug/L
ND
2500
2500
2450
2470
98
99
60-140
1
30
1,2-Dichloroethane-d4 (S)
%
103
102
70-130
4-Bromofluorobenzene (S)
%
99
99
70-130
Toluene-d8 (S)
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 641266 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92555464001
METHOD BLANK: 3365720
Associated Lab Samples: 92555464001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
1.9
08/18/21 21:49
1,1,1-Trichloroethane
ug/kg
ND
5.0
2.6
08/18/21 21:49
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
1.3
08/18/21 21:49
1,1,2-Trichloroethane
ug/kg
ND
5.0
1.7
08/18/21 21:49
1,1-Dichloroethane
ug/kg
ND
5.0
2.1
08/18/21 21:49
1,1-Dichloroethene
ug/kg
ND
5.0
2.1
08/18/21 21:49
1,1-Dichloropropene
ug/kg
ND
5.0
2.4
08/18/21 21:49
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
4.0
08/18/21 21:49
1,2,3-Trichloropropane
ug/kg
ND
5.0
2.5
08/18/21 21:49
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
4.2
08/18/21 21:49
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
1.4
08/18/21 21:49
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
1.9
08/18/21 21:49
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
2.2
08/18/21 21:49
1,2-Dichlorobenzene
ug/kg
ND
5.0
1.8
08/18/21 21:49
1,2-Dichloroethane
ug/kg
ND
5.0
3.3
08/18/21 21:49
1,2-Dichloropropane
ug/kg
ND
5.0
1.5
08/18/21 21:49
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
1.7
08/18/21 21:49
1,3-Dichlorobenzene
ug/kg
ND
5.0
1.6
08/18/21 21:49
1,3-Dichloropropane
ug/kg
ND
5.0
1.6
08/18/21 21:49
1,4-Dichlorobenzene
ug/kg
ND
5.0
1.3
08/18/21 21:49
2,2-Dichloropropane
ug/kg
ND
5.0
1.6
08/18/21 21:49
2-Butanone (MEK)
ug/kg
ND
100
24.0
08/18/21 21:49
2-Chlorotoluene
ug/kg
ND
5.0
1.8
08/18/21 21:49
2-Hexanone
ug/kg
ND
50.0
4.8
08/18/21 21:49
4-Chlorotoluene
ug/kg
ND
5.0
0.88
08/18/21 21:49
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
4.8
08/18/21 21:49
Acetone
ug/kg
ND
100
32.1
08/18/21 21:49
Benzene
ug/kg
ND
5.0
2.0
08/18/21 21:49
Bromobenzene
ug/kg
ND
5.0
1.6
08/18/21 21:49
Bromochloromethane
ug/kg
ND
5.0
1.5
08/18/21 21:49
Bromodichloromethane
ug/kg
ND
5.0
1.9
08/18/21 21:49
Bromoform
ug/kg
ND
5.0
1.8
08/18/21 21:49
Bromomethane
ug/kg
ND
10.0
7.9
08/18/21 21:49
Carbon tetrachloride
ug/kg
ND
5.0
1.9
08/18/21 21:49
Chlorobenzene
ug/kg
ND
5.0
0.96
08/18/21 21:49
Chloroethane
ug/kg
ND
10.0
3.9
08/18/21 21:49
Chloroform
ug/kg
ND
5.0
3.0
08/18/21 21:49
Chloromethane
ug/kg
ND
10.0
4.2
08/18/21 21:49
cis-1,2-Dichloroethene
ug/kg
ND
5.0
1.7
08/18/21 21:49
cis-1,3-Dichloropropene
ug/kg
ND
5.0
1.4
08/18/21 21:49
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
METHOD BLANK: 3365720
Associated Lab Samples: 92555464001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromochloromethane
ug/kg
ND
5.0
2.8
08/18/21 21:49
Dibromomethane
ug/kg
ND
5.0
1.1
08/18/21 21:49
Dichlorodifluoromethane
ug/kg
ND
10.0
2.2
08/18/21 21:49
Diisopropyl ether
ug/kg
ND
5.0
1.4
08/18/21 21:49
Ethylbenzene
ug/kg
ND
5.0
2.3
08/18/21 21:49
Hexachloro-1,3-butadiene
ug/kg
ND
10.0
8.2
08/18/21 21:49
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
1.7
08/18/21 21:49
m&p-Xylene
ug/kg
ND
10.0
3.4
08/18/21 21:49
Methyl-tert-butyl ether
ug/kg
ND
5.0
1.9
08/18/21 21:49
Methylene Chloride
ug/kg
ND
20.0
13.7
08/18/21 21:49
n-Butylbenzene
ug/kg
ND
5.0
2.4
08/18/21 21:49
n-Propylbenzene
ug/kg
ND
5.0
1.8
08/18/21 21:49
Naphthalene
ug/kg
ND
5.0
2.6
08/18/21 21:49
o-Xylene
ug/kg
ND
5.0
2.2
08/18/21 21:49
p-Isopropyltoluene
ug/kg
ND
5.0
2.5
08/18/21 21:49
sec-Butylbenzene
ug/kg
ND
5.0
2.2
08/18/21 21:49
Styrene
ug/kg
ND
5.0
1.3
08/18/21 21:49
tert-Butyl benzene
ug/kg
ND
5.0
1.8
08/18/21 21:49
Tetrachloroethene
ug/kg
ND
5.0
1.6
08/18/21 21:49
Toluene
ug/kg
ND
5.0
1.4
08/18/21 21:49
trans-1,2-Dichloroethene
ug/kg
ND
5.0
1.8
08/18/21 21:49
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
1.7
08/18/21 21:49
Trichloroethene
ug/kg
ND
5.0
1.3
08/18/21 21:49
Trichlorofluoromethane
ug/kg
ND
5.0
2.8
08/18/21 21:49
Vinyl acetate
ug/kg
ND
50.0
3.6
08/18/21 21:49
Vinyl chloride
ug/kg
ND
10.0
2.5
08/18/21 21:49
Xylene (Total)
ug/kg
ND
10.0
2.8
08/18/21 21:49
1,2-Dichloroethane-d4 (S)
%
98
70-130
08/18/21 21:49
4-Bromofluorobenzene (S)
%
100
69-134
08/18/21 21:49
Toluene-d8 (S)
%
100
70-130
08/18/21 21:49
Qualifiers
LABORATORY CONTROL SAMPLE:
3365721
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
1250
1090
87
70-130
1,1,1-Trichloroethane
ug/kg
1250
1110
89
70-130
1,1,2,2-Tetrachloroethane
ug/kg
1250
1070
86
70-130
1,1,2-Trichloroethane
ug/kg
1250
1110
89
70-130
1,1-Dichloroethane
ug/kg
1250
1160
93
70-130
1,1-Dichloroethene
ug/kg
1250
1210
97
70-130
1,1-Dichloropropene
ug/kg
1250
1100
88
70-130
1,2,3-Trichlorobenzene
ug/kg
1250
1200
96
65-130
1,2,3-Trichloropropane
ug/kg
1250
1150
92
70-130
1,2,4-Trichlorobenzene
ug/kg
1250
1190
95
68-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
LABORATORY CONTROL SAMPLE:
Parameter
3365721
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trimethylbenzene
ug/kg
1250
1110
89
70-130
1,2-Dibromo-3-chloropropane
ug/kg
1250
1160
93
70-130
1,2-Dibromoethane (EDB)
ug/kg
1250
1080
87
70-130
1,2-Dichlorobenzene
ug/kg
1250
1190
95
70-130
1,2-Dichloroethane
ug/kg
1250
1120
90
63-130
1,2-Dichloropropane
ug/kg
1250
1140
91
70-130
1,3,5-Trimethylbenzene
ug/kg
1250
1110
89
70-130
1,3-Dichlorobenzene
ug/kg
1250
1240
99
70-130
1,3-Dichloropropane
ug/kg
1250
1100
88
70-130
1,4-Dichlorobenzene
ug/kg
1250
1120
89
70-130
2,2-Dichloropropane
ug/kg
1250
1100
88
66-130
2-Butanone (MEK)
ug/kg
2500
2170
87
70-130
2-Chlorotoluene
ug/kg
1250
1120
90
70-130
2-Hexanone
ug/kg
2500
2250
90
70-130
4-Chlorotoluene
ug/kg
1250
1070
86
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
2500
2320
93
70-130
Acetone
ug/kg
2500
2360
95
69-130
Benzene
ug/kg
1250
1110
89
70-130
Bromobenzene
ug/kg
1250
1120
90
70-130
Bromochloromethane
ug/kg
1250
1240
99
70-130
Bromodichloromethane
ug/kg
1250
1110
89
69-130
Bromoform
ug/kg
1250
1090
88
70-130
Bromomethane
ug/kg
1250
1490
120
52-130
Carbon tetrachloride
ug/kg
1250
1190
96
70-130
Chlorobenzene
ug/kg
1250
1100
88
70-130
Chloroethane
ug/kg
1250
1400
112
65-130
Chloroform
ug/kg
1250
1180
95
70-130
Chloromethane
ug/kg
1250
1120
89
55-130
cis-1,2-Dichloroethene
ug/kg
1250
1160
93
70-130
cis-1,3-Dichloropropene
ug/kg
1250
1070
86
70-130
Dibromochloromethane
ug/kg
1250
1130
90
70-130
Dibromomethane
ug/kg
1250
1200
96
70-130
Dichlorodifluoromethane
ug/kg
1250
1550
124
45-156
Diisopropyl ether
ug/kg
1250
1040
84
70-130
Ethylbenzene
ug/kg
1250
1190
95
70-130
Hexachloro-1,3-butadiene
ug/kg
1250
1030
82
66-130
Isopropylbenzene (Cumene)
ug/kg
1250
1130
90
70-130
m&p-Xylene
ug/kg
2500
2210
88
70-130
Methyl-tert-butyl ether
ug/kg
1250
1090
87
70-130
Methylene Chloride
ug/kg
1250
1180
95
65-130
n-Butylbenzene
ug/kg
1250
1130
90
67-130
n-Propylbenzene
ug/kg
1250
1130
90
70-130
Naphthalene
ug/kg
1250
1160
93
70-130
o-Xylene
ug/kg
1250
1110
89
70-130
p-Isopropyltoluene
ug/kg
1250
1090
87
67-130
sec-Butylbenzene
ug/kg
1250
1060
85
69-130
Styrene
ug/kg
1250
1100
88
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
LABORATORY CONTROL SAMPLE:
Parameter
3365721
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
tert-Butyl benzene
ug/kg
1250
1080
87
67-130
Tetrachloroethene
ug/kg
1250
1120
90
70-130
Toluene
ug/kg
1250
1120
89
70-130
trans-1,2-Dichloroethene
ug/kg
1250
1180
95
70-130
trans- 1,3-Dichloropropene
ug/kg
1250
1170
93
68-130
Trichloroethene
ug/kg
1250
1130
90
70-130
Trichlorofluoromethane
ug/kg
1250
1230
99
70-130
Vinyl acetate
ug/kg
2500
2410
96
70-130
Vinyl chloride
ug/kg
1250
1370
110
61-130
Xylene (Total)
ug/kg
3750
3320
89
70-130
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
99
69-134
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
Parameter
3365723
Units
92555491002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
644
611
95
70-131
1,1,1-Trichloroethane
ug/kg
ND
644
621
96
65-133
1,1,2,2-Tetrachloroethane
ug/kg
ND
644
508
79
66-130
1,1,2-Trichloroethane
ug/kg
ND
644
525
82
66-133
1,1-Dichloroethane
ug/kg
ND
644
626
97
65-130
1,1-Dichloroethene
ug/kg
ND
644
643
100
10-158
1,1-Dichloropropene
ug/kg
ND
644
613
95
68-133
1,2,3-Trichlorobenzene
ug/kg
ND
644
658
102
27-138
1,2,3-Trichloropropane
ug/kg
ND
644
512
80
67-130
1,2,4-Trichlorobenzene
ug/kg
ND
644
664
103
51-134
1,2,4-Trimethylbenzene
ug/kg
ND
644
631
98
63-136
1,2-Dibromo-3-chloropropane
ug/kg
ND
644
518
80
32-130
1,2-Dibromoethane (EDB)
ug/kg
ND
644
555
86
70-130
1,2-Dichlorobenzene
ug/kg
ND
644
627
97
69-130
1,2-Dichloroethane
ug/kg
ND
644
562
87
59-130
1,2-Dichloropropane
ug/kg
ND
644
594
92
70-130
1,3,5-Trimethylbenzene
ug/kg
ND
644
634
98
65-137
1,3-Dichlorobenzene
ug/kg
ND
644
640
99
70-130
1,3-Dichloropropane
ug/kg
ND
644
574
89
70-130
1,4-Dichlorobenzene
ug/kg
ND
644
601
93
68-130
2,2-Dichloropropane
ug/kg
ND
644
507
79
32-130
2-Butanone (MEK)
ug/kg
ND
1290
878
68
10-136
2-Chlorotoluene
ug/kg
ND
644
601
93
69-141
2-Hexanone
ug/kg
ND
1290
916
71
10-144
4-Chlorotoluene
ug/kg
ND
644
585
91
70-132
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
1290
932
72
25-143
Acetone
ug/kg
ND
1290
919
71
10-130
Benzene
ug/kg
ND
644
613
95
67-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
MATRIX SPIKE SAMPLE:
Parameter
3365723
Units
92555491002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Bromobenzene
ug/kg
ND
644
593
92
70-130
Bromochloromethane
ug/kg
ND
644
597
93
69-134
Bromodichloromethane
ug/kg
ND
644
549
85
64-130
Bromoform
ug/kg
ND
644
493
77
62-130
Bromomethane
ug/kg
ND
644
601
93
20-176
Carbon tetrachloride
ug/kg
ND
644
639
99
65-140
Chlorobenzene
ug/kg
ND
644
614
95
70-130
Chloroethane
ug/kg
ND
644
402
62
10-130
Chloroform
ug/kg
4.5J
644
622
96
63-130
Chloromethane
ug/kg
ND
644
644
100
58-130
cis-1,2-Dichloroethene
ug/kg
ND
644
602
94
66-130
cis-1,3-Dichloropropene
ug/kg
ND
644
524
81
67-130
Dibromochloromethane
ug/kg
ND
644
562
87
67-130
Dibromomethane
ug/kg
ND
644
592
92
63-131
Dichlorodifluoromethane
ug/kg
ND
644
805
125
44-180
Diisopropyl ether
ug/kg
ND
644
532
83
63-130
Ethylbenzene
ug/kg
ND
644
684
106
66-130
Hexachloro-1,3-butadiene
ug/kg
ND
644
642
100
64-150
Isopropylbenzene (Cumene)
ug/kg
ND
644
660
102
69-135
m&p-Xylene
ug/kg
ND
1290
1270
98
60-133
Methyl-tert-butyl ether
ug/kg
ND
644
530
82
65-130
Methylene Chloride
ug/kg
ND
644
586
91
61-130
n-Butylbenzene
ug/kg
ND
644
650
101
65-140
n-Propylbenzene
ug/kg
ND
644
626
97
67-140
Naphthalene
ug/kg
ND
644
599
93
15-145
o-Xylene
ug/kg
ND
644
619
96
66-133
p-Isopropyltoluene
ug/kg
ND
644
621
96
56-147
sec-Butylbenzene
ug/kg
ND
644
598
93
65-139
Styrene
ug/kg
ND
644
586
91
70-132
tert-Butyl benzene
ug/kg
ND
644
633
98
62-135
Tetrachloroethene
ug/kg
ND
644
692
107
70-135
Toluene
ug/kg
ND
644
605
94
67-130
trans-1,2-Dichloroethene
ug/kg
ND
644
634
98
69-130
trans- 1,3-Dichloropropene
ug/kg
ND
644
548
85
62-130
Trichloroethene
ug/kg
ND
644
625
97
70-135
Trichlorofluoromethane
ug/kg
ND
644
430
67
10-130
Vinyl acetate
ug/kg
ND
1290
1080
84
53-130
Vinyl chloride
ug/kg
ND
644
752
117
61-148
Xylene (Total)
ug/kg
ND
1930
1880
98
63-132
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
98
69-134
Toluene-d8 (S)
%
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
SAMPLE DUPLICATE: 3365722
Parameter
Units
92555491001
Result
Dup
Result
Max
RPD RPD
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,1-Trichloroethane
ug/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,2-Trichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethene
ug/kg
ND
ND
30
1,1-Dichloropropene
ug/kg
ND
ND
30
1,2,3-Trichlorobenzene
ug/kg
ND
ND
30
1,2,3-Trichloropropane
ug/kg
ND
ND
30
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2,4-Trimethylbenzene
ug/kg
29.8
28.3
5 30
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
30
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,2-Dichloroethane
ug/kg
ND
ND
30
1,2-Dichloropropane
ug/kg
ND
ND
30
1,3,5-Trimethylbenzene
ug/kg
10
9.6
4 30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichloropropane
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
2,2-Dichloropropane
ug/kg
ND
ND
30
2-Butanone (MEK)
ug/kg
ND
ND
30
2-Chlorotoluene
ug/kg
ND
ND
30
2-Hexanone
ug/kg
ND
ND
30
4-Chlorotoluene
ug/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
30
Acetone
ug/kg
ND
ND
30
Benzene
ug/kg
ND
ND
30
Bromobenzene
ug/kg
ND
ND
30
Bromochloromethane
ug/kg
ND
ND
30
Bromodichloromethane
ug/kg
ND
ND
30
Bromoform
ug/kg
ND
ND
30
Bromomethane
ug/kg
ND
ND
30
Carbon tetrachloride
ug/kg
ND
ND
30
Chlorobenzene
ug/kg
ND
ND
30
Chloroethane
ug/kg
ND
ND
30
Chloroform
ug/kg
6.1J
6.6J
30
Chloromethane
ug/kg
ND
ND
30
cis-1,2-Dichloroethene
ug/kg
ND
ND
30
cis-1,3-Dichloropropene
ug/kg
ND
ND
30
Dibromochloromethane
ug/kg
ND
ND
30
Dibromomethane
ug/kg
ND
ND
30
Dichlorodifluoromethane
ug/kg
ND
ND
30
Diisopropyl ether
ug/kg
ND
ND
30
Ethylbenzene
ug/kg
ND
ND
30
Hexachloro-1,3-butadiene
ug/kg
ND
ND
30
Isopropylbenzene (Cumene)
ug/kg
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
SAMPLE DUPLICATE: 3365722
Parameter
Units
92555491001
Result
Dup
Result
RPD
Max
RPD
m&p-Xylene
ug/kg
21.0
17.1
21
30
Methyl-tert-butyl ether
ug/kg
ND
ND
30
Methylene Chloride
ug/kg
ND
ND
30
n-Butylbenzene
ug/kg
ND
ND
30
n-Propylbenzene
ug/kg
ND
ND
30
Naphthalene
ug/kg
12.5
10.5
18
30
o-Xylene
ug/kg
10.8
9.8
9
30
p-Isopropyltoluene
ug/kg
ND
ND
30
sec-Butylbenzene
ug/kg
ND
ND
30
Styrene
ug/kg
ND
ND
30
tert-Butyl benzene
ug/kg
ND
ND
30
Tetrachloroethene
ug/kg
ND
ND
30
Toluene
ug/kg
8.6
8.0
7
30
trans-1,2-Dichloroethene
ug/kg
ND
ND
30
trans- 1,3-Dichloropropene
ug/kg
ND
ND
30
Trichloroethene
ug/kg
ND
ND
30
Trichlorofluoromethane
ug/kg
ND
ND
30
Vinyl acetate
ug/kg
ND
ND
30
Vinyl chloride
ug/kg
ND
ND
30
Xylene (Total)
ug/kg
31.7
26.9
16
30
1,2-Dichloroethane-d4 (S)
%
97
95
4-Bromofluorobenzene (S)
%
100
97
Toluene-d8 (S)
%
100
99
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 34 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 641562 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92555464002
METHOD BLANK: 3367224
Matrix:
Solid
Associated Lab Samples: 92555464002
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
1.9
08/19/21 12:20
1,1,1-Trichloroethane
ug/kg
ND
5.0
2.6
08/19/21 12:20
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
1.3
08/19/21 12:20
1,1,2-Trichloroethane
ug/kg
ND
5.0
1.7
08/19/21 12:20
1,1-Dichloroethane
ug/kg
ND
5.0
2.1
08/19/21 12:20
1,1-Dichloroethene
ug/kg
ND
5.0
2.1
08/19/21 12:20
1,1-Dichloropropene
ug/kg
ND
5.0
2.4
08/19/21 12:20
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
4.0
08/19/21 12:20
1,2,3-Trichloropropane
ug/kg
ND
5.0
2.5
08/19/21 12:20
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
4.2
08/19/21 12:20
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
1.4
08/19/21 12:20
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
1.9
08/19/21 12:20
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
2.2
08/19/21 12:20
1,2-Dichlorobenzene
ug/kg
ND
5.0
1.8
08/19/21 12:20
1,2-Dichloroethane
ug/kg
ND
5.0
3.3
08/19/21 12:20
1,2-Dichloropropane
ug/kg
ND
5.0
1.5
08/19/21 12:20
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
1.7
08/19/21 12:20
1,3-Dichlorobenzene
ug/kg
ND
5.0
1.6
08/19/21 12:20
1,3-Dichloropropane
ug/kg
ND
5.0
1.6
08/19/21 12:20
1,4-Dichlorobenzene
ug/kg
ND
5.0
1.3
08/19/21 12:20
2,2-Dichloropropane
ug/kg
ND
5.0
1.6
08/19/21 12:20
2-Butanone (MEK)
ug/kg
ND
100
24.0
08/19/21 12:20
2-Chlorotoluene
ug/kg
ND
5.0
1.8
08/19/21 12:20
2-Hexanone
ug/kg
ND
50.0
4.8
08/19/21 12:20
4-Chlorotoluene
ug/kg
ND
5.0
0.88
08/19/21 12:20
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
4.8
08/19/21 12:20
Acetone
ug/kg
ND
100
32.1
08/19/21 12:20
Benzene
ug/kg
ND
5.0
2.0
08/19/21 12:20
Bromobenzene
ug/kg
ND
5.0
1.6
08/19/21 12:20
Bromochloromethane
ug/kg
ND
5.0
1.5
08/19/21 12:20
Bromodichloromethane
ug/kg
ND
5.0
1.9
08/19/21 12:20
Bromoform
ug/kg
ND
5.0
1.8
08/19/21 12:20
Bromomethane
ug/kg
ND
10.0
7.9
08/19/21 12:20 IK
Carbon tetrachloride
ug/kg
ND
5.0
1.9
08/19/21 12:20
Chlorobenzene
ug/kg
ND
5.0
0.96
08/19/21 12:20
Chloroethane
ug/kg
ND
10.0
3.9
08/19/21 12:20
Chloroform
ug/kg
ND
5.0
3.0
08/19/21 12:20
Chloromethane
ug/kg
ND
10.0
4.2
08/19/21 12:20
cis-1,2-Dichloroethene
ug/kg
ND
5.0
1.7
08/19/21 12:20
cis-1,3-Dichloropropene
ug/kg
ND
5.0
1.4
08/19/21 12:20
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 35 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
METHOD BLANK: 3367224
Associated Lab Samples: 92555464002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromochloromethane
ug/kg
ND
5.0
2.8
08/19/21 12:20
Dibromomethane
ug/kg
ND
5.0
1.1
08/19/21 12:20
Dichlorodifluoromethane
ug/kg
ND
10.0
2.2
08/19/21 12:20
Diisopropyl ether
ug/kg
ND
5.0
1.4
08/19/21 12:20
Ethylbenzene
ug/kg
ND
5.0
2.3
08/19/21 12:20
Hexachloro-1,3-butadiene
ug/kg
ND
10.0
8.2
08/19/21 12:20
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
1.7
08/19/21 12:20
m&p-Xylene
ug/kg
ND
10.0
3.4
08/19/21 12:20
Methyl-tert-butyl ether
ug/kg
ND
5.0
1.9
08/19/21 12:20
Methylene Chloride
ug/kg
ND
20.0
13.7
08/19/21 12:20
n-Butylbenzene
ug/kg
ND
5.0
2.4
08/19/21 12:20
n-Propylbenzene
ug/kg
ND
5.0
1.8
08/19/21 12:20
Naphthalene
ug/kg
ND
5.0
2.6
08/19/21 12:20
o-Xylene
ug/kg
ND
5.0
2.2
08/19/21 12:20
p-Isopropyltoluene
ug/kg
ND
5.0
2.5
08/19/21 12:20
sec-Butylbenzene
ug/kg
ND
5.0
2.2
08/19/21 12:20
Styrene
ug/kg
ND
5.0
1.3
08/19/21 12:20
tert-Butyl benzene
ug/kg
ND
5.0
1.8
08/19/21 12:20
Tetrachloroethene
ug/kg
ND
5.0
1.6
08/19/21 12:20
Toluene
ug/kg
ND
5.0
1.4
08/19/21 12:20
trans-1,2-Dichloroethene
ug/kg
ND
5.0
1.8
08/19/21 12:20
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
1.7
08/19/21 12:20
Trichloroethene
ug/kg
ND
5.0
1.3
08/19/21 12:20
Trichlorofluoromethane
ug/kg
ND
5.0
2.8
08/19/21 12:20
Vinyl acetate
ug/kg
ND
50.0
3.6
08/19/21 12:20
Vinyl chloride
ug/kg
ND
10.0
2.5
08/19/21 12:20
Xylene (Total)
ug/kg
ND
10.0
2.8
08/19/21 12:20
1,2-Dichloroethane-d4 (S)
%
117
70-130
08/19/21 12:20
4-Bromofluorobenzene (S)
%
104
69-134
08/19/21 12:20
Toluene-d8 (S)
%
102
70-130
08/19/21 12:20
Qualifiers
LABORATORY CONTROL SAMPLE:
3367225
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
1250
1110
89
70-130
1,1,1-Trichloroethane
ug/kg
1250
1160
93
70-130
1,1,2,2-Tetrachloroethane
ug/kg
1250
1110
89
70-130
1,1,2-Trichloroethane
ug/kg
1250
1170
94
70-130
1,1-Dichloroethane
ug/kg
1250
1200
96
70-130
1,1-Dichloroethene
ug/kg
1250
1210
97
70-130
1,1-Dichloropropene
ug/kg
1250
1230
98
70-130
1,2,3-Trichlorobenzene
ug/kg
1250
1320
106
65-130
1,2,3-Trichloropropane
ug/kg
1250
1140
91
70-130
1,2,4-Trichlorobenzene
ug/kg
1250
1330
107
68-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
LABORATORY CONTROL SAMPLE:
Parameter
3367225
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trimethylbenzene
ug/kg
1250
1290
103
70-130
1,2-Dibromo-3-chloropropane
ug/kg
1250
1170
94
70-130
1,2-Dibromoethane (EDB)
ug/kg
1250
1140
91
70-130
1,2-Dichlorobenzene
ug/kg
1250
1170
94
70-130
1,2-Dichloroethane
ug/kg
1250
1160
93
63-130
1,2-Dichloropropane
ug/kg
1250
1200
96
70-130
1,3,5-Trimethylbenzene
ug/kg
1250
1270
102
70-130
1,3-Dichlorobenzene
ug/kg
1250
1180
95
70-130
1,3-Dichloropropane
ug/kg
1250
1130
91
70-130
1,4-Dichlorobenzene
ug/kg
1250
1140
91
70-130
2,2-Dichloropropane
ug/kg
1250
1340
107
66-130
2-Butanone (MEK)
ug/kg
2500
2480
99
70-130
2-Chlorotoluene
ug/kg
1250
1220
98
70-130
2-Hexanone
ug/kg
2500
2420
97
70-130
4-Chlorotoluene
ug/kg
1250
1170
94
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
2500
2560
102
70-130
Acetone
ug/kg
2500
2430
97
69-130
Benzene
ug/kg
1250
1140
91
70-130
Bromobenzene
ug/kg
1250
1150
92
70-130
Bromochloromethane
ug/kg
1250
1270
101
70-130
Bromodichloromethane
ug/kg
1250
1150
92
69-130
Bromoform
ug/kg
1250
1150
92
70-130
Bromomethane
ug/kg
1250
1300
104
52-130IK
Carbon tetrachloride
ug/kg
1250
1250
100
70-130
Chlorobenzene
ug/kg
1250
1120
89
70-130
Chloroethane
ug/kg
1250
1460
117
65-130
Chloroform
ug/kg
1250
1280
102
70-130
Chloromethane
ug/kg
1250
1300
104
55-130
cis-1,2-Dichloroethene
ug/kg
1250
1210
97
70-130
cis-1,3-Dichloropropene
ug/kg
1250
1230
99
70-130
Dibromochloromethane
ug/kg
1250
1160
93
70-130
Dibromomethane
ug/kg
1250
1160
93
70-130
Dichlorodifluoromethane
ug/kg
1250
1370
109
45-156
Diisopropyl ether
ug/kg
1250
1220
98
70-130
Ethylbenzene
ug/kg
1250
1100
88
70-130
Hexachloro-1,3-butadiene
ug/kg
1250
1310
105
66-130
Isopropylbenzene (Cumene)
ug/kg
1250
1270
102
70-130
m&p-Xylene
ug/kg
2500
2350
94
70-130
Methyl-tert-butyl ether
ug/kg
1250
1120
89
70-130
Methylene Chloride
ug/kg
1250
1260
101
65-130
n-Butylbenzene
ug/kg
1250
1350
108
67-130
n-Propylbenzene
ug/kg
1250
1220
98
70-130
Naphthalene
ug/kg
1250
1230
99
70-130
o-Xylene
ug/kg
1250
1190
95
70-130
p-Isopropyltoluene
ug/kg
1250
1310
105
67-130
sec-Butylbenzene
ug/kg
1250
1280
103
69-130
Styrene
ug/kg
1250
1270
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
LABORATORY CONTROL SAMPLE:
Parameter
3367225
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
tert-Butyl benzene
ug/kg
1250
1280
102
67-130
Tetrachloroethene
ug/kg
1250
1140
92
70-130
Toluene
ug/kg
1250
1130
90
70-130
trans-1,2-Dichloroethene
ug/kg
1250
1240
99
70-130
trans- 1,3-Dichloropropene
ug/kg
1250
1220
98
68-130
Trichloroethene
ug/kg
1250
1160
93
70-130
Trichlorofluoromethane
ug/kg
1250
1190
95
70-130
Vinyl acetate
ug/kg
2500
2780
111
70-130
Vinyl chloride
ug/kg
1250
1250
100
61-130
Xylene (Total)
ug/kg
3750
3540
94
70-130
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
101
69-134
Toluene-d8 (S)
%
102
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3367226
MS
92555464002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3367227
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/kg
ND
11500
11500
11600
10400
101
90
70-131
11
30
1,1,1-Trichloroethane
ug/kg
ND
11500
11500
12000
11200
105
98
65-133
7
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
11500
11500
11700
10400
102
91
66-130
11
30
1,1,2-Trichloroethane
ug/kg
ND
11500
11500
12000
11000
105
96
66-133
8
30
1,1-Dichloroethane
ug/kg
ND
11500
11500
12500
11600
108
100
65-130
8
30
1,1-Dichloroethene
ug/kg
ND
11500
11500
12600
11700
110
102
10-158
8
30
1,1-Dichloropropene
ug/kg
ND
11500
11500
12900
12000
112
105
68-133
7
30
1,2,3-Trichlorobenzene
ug/kg
ND
11500
11500
14200
11700
124
102
27-138
19
30
1,2,3-Trichooropropane
ug/kg
ND
11500
11500
11600
10200
101
89
67-130
12
30
1,2,4-Trichlorobenzene
ug/kg
ND
11500
11500
14500
11600
127
101
51-134
22
30
1,2,4-Trimethyl benzene
ug/kg
84300
11500
11500
88300
74500
35
-86
63-136
17
30 M1
1,2-Dibromo-3-
ug/kg
ND
11500
11500
12700
10600
111
93
32-130
18
30
chloropropane
1,2-Dibromoethane (EDB)
ug/kg
ND
11500
11500
11800
10600
103
92
70-130
10
30
1,2-Dichlorobenzene
ug/kg
ND
11500
11500
13000
10700
113
94
69-130
19
30
1,2-Dichloroethane
ug/kg
ND
11500
11500
11600
10900
101
95
59-130
6
30
1,2-Dichloropropane
ug/kg
ND
11500
11500
12500
11500
109
100
70-130
8
30
1,3,5-Trimethyl benzene
ug/kg
23600
11500
11500
35100
30000
101
57
65-137
16
30 M1
1,3-Dichlorobenzene
ug/kg
145
11500
11500
12800
10800
110
93
70-130
16
30
1,3-Dichloropropane
ug/kg
ND
11500
11500
11900
10700
104
93
70-130
11
30
1,4-Dichlorobenzene
ug/kg
ND
11500
11500
12700
10500
111
92
68-130
19
30
2,2-Dichloropropane
ug/kg
ND
11500
11500
11900
11000
104
96
32-130
8
30
2-Butanone (MEK)
ug/kg
ND
22900
22900
26500
24000
116
105
10-136
10
30
2-Chlorotoluene
ug/kg
ND
11500
11500
16000
13100
140
114
69-141
20
30
2-Hexanone
ug/kg
ND
22900
22900
26000
22500
114
98
10-144
14
30
4-Chlorotoluene
ug/kg
ND
11500
11500
13800
11300
120
98
70-132
20
30
4-Methyl-2-pentanone
ug/kg
2310
22900
22900
27000
24200
108
95
25-143
11
30
(MIBK)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 38 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3367226
3367227
MS
MSD
92555464002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Acetone
ug/kg
ND
22900
22900
22600
20200
99
88
10-130
12
30
Benzene
ug/kg
146
11500
11500
11800
10800
102
93
67-130
9
30
Bromobenzene
ug/kg
ND
11500
11500
12800
10800
111
94
70-130
17
30
Bromochloromethane
ug/kg
ND
11500
11500
12300
11600
107
101
69-134
6
30
Bromodichloromethane
ug/kg
ND
11500
11500
11300
10500
99
92
64-130
7
30
Bromoform
ug/kg
ND
11500
11500
11100
10000
97
88
62-130
10
30
Bromomethane
ug/kg
ND
11500
11500
11600
9150
101
80
20-176
23
30 IK
Carbon tetrachloride
ug/kg
ND
11500
11500
12300
11400
107
100
65-140
7
30
Chlorobenzene
ug/kg
ND
11500
11500
12200
11000
107
96
70-130
11
30
Chloroethane
ug/kg
ND
11500
11500
16100
14900
140
130
10-130
8
30 M1
Chloroform
ug/kg
ND
11500
11500
13100
12200
112
104
63-130
7
30
Chloromethane
ug/kg
ND
11500
11500
14900
13100
130
114
58-130
13
30
cis-1,2-Dichloroethene
ug/kg
ND
11500
11500
12500
11500
108
99
66-130
8
30
cis-1,3-Dichloropropene
ug/kg
ND
11500
11500
11700
11100
102
96
67-130
6
30
Dibromochloromethane
ug/kg
ND
11500
11500
11600
10600
101
92
67-130
9
30
Dibromomethane
ug/kg
ND
11500
11500
11200
10300
98
90
63-131
8
30
Dichlorodifluoromethane
ug/kg
ND
11500
11500
14800
13300
130
116
44-180
11
30
Diisopropyl ether
ug/kg
ND
11500
11500
12100
11200
106
98
63-130
8
30
Ethylbenzene
ug/kg
13600
11500
11500
23800
21600
88
69
66-130
10
30
Hexachloro-1,3-butadiene
ug/kg
ND
11500
11500
16000
13200
140
115
64-150
19
30
Isopropylbenzene
ug/kg
ND
11500
11500
17300
15700
151
137
69-135
10
30 M1
(Cumene)
m&p-Xylene
ug/kg
37500
22900
22900
58400
53000
91
68
60-133
10
30
Methyl-tert-butyl ether
ug/kg
ND
11500
11500
10700
9960
93
87
65-130
7
30
Methylene Chloride
ug/kg
ND
11500
11500
13100
12100
114
105
61-130
8
30
n-Butylbenzene
ug/kg
7010
11500
11500
21800
17900
129
95
65-140
19
30
n-Propylbenzene
ug/kg
ND
11500
11500
28000
23000
245
200
67-140
20
30 M1
Naphthalene
ug/kg
11300
11500
11500
23800
19800
109
74
15-145
18
30
o-Xylene
ug/kg
6870
11500
11500
18800
16800
104
87
66-133
11
30
p-Isopropyltoluene
ug/kg
ND
11500
11500
19200
15900
168
139
56-147
19
30 M1
sec-Butylbenzene
ug/kg
ND
11500
11500
17000
14100
149
123
65-139
19
30 M1
Styrene
ug/kg
196
11500
11500
13500
12000
116
103
70-132
11
30
tert-Butylbenzene
ug/kg
ND
11500
11500
14800
11900
129
104
62-135
22
30
Tetrachloroethene
ug/kg
ND
11500
11500
12300
11200
108
98
70-135
10
30
Toluene
ug/kg
262
11500
11500
11700
10900
100
92
67-130
8
30
trans-1,2-Dichloroethene
ug/kg
ND
11500
11500
12800
11800
110
102
69-130
8
30
trans-1,3-Dichloropropene
ug/kg
ND
11500
11500
11400
10500
99
91
62-130
8
30
Trichloroethene
ug/kg
ND
11500
11500
11900
11100
102
96
70-135
6
30
Trichlorofluoromethane
ug/kg
ND
11500
11500
12700
11900
111
104
10-130
7
30
Vinyl acetate
ug/kg
ND
22900
22900
26000
23800
113
104
53-130
9
30
Vinyl chloride
ug/kg
ND
11500
11500
13600
12300
118
107
61-148
10
30
Xylene (Total)
ug/kg
44400
34400
34400
77200
69900
96
74
63-132
10
30
1,2-Dichloroethane-d4 (S)
%
100
107
70-130
4-Bromofluorobenzene (S)
%
99
102
69-134
Toluene-d8 (S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 640847
Analysis Method: EPA 504.1
QC Batch Method: EPA 504.1
Analysis Description: GCS 504 EDB DBCP
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92555464003
METHOD BLANK: 3363390
Matrix: Water
Associated Lab Samples: 92555464003
Blank Reporting
Parameter
Units
Result Limit
MDL Analyzed Qualifiers
1,2-Dibromoethane (EDB)
ug/L
ND 0.020
0.013 08/17/21 13:27
1-Chloro-2-bromopropane (S)
%
92 70-130
08/17/21 13:27
LABORATORY CONTROL SAMPLE & LCSD:
3363391
3363392
Spike LCS LCSD
LCS LCSD % Rec Max
Parameter
Units
Conc. Result Result
% Rec % Rec Limits RPD RPD
Qualifiers
1,2-Dibromoethane (EDB)
ug/L
0.25 0.25 0.28
101 113 70-130 11 20
1-Chloro-2-bromopropane (S)
%
96 107 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3363394 3363395
MS MSD
92555271013
Spike Spike MS
MSD MS MSD % Rec
Max
Parameter Units
Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD
RPD Qual
1,2-Dibromoethane (EDB) ug/L
ND
0.24 0.24 0.27
0.27 112 112 65-135 0
20
1-Chloro-2-bromopropane %
106 106 70-130
(S)
SAMPLE DUPLICATE: 3363393
92555271012 Dup
Max
Parameter
Units
Result Result
RPD RPD Qualifiers
1,2-Dibromoethane (EDB)
ug/L
ND ND
20
1-Chloro-2-bromopropane (S)
%
99 99
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 641142 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92555464003
METHOD BLANK: 3365110
Associated Lab Samples: 92555464003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
1.7
08/20/21 12:47
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
1.2
08/20/21 12:47
2,4,6-Trichlorophenol
ug/L
ND
10.0
1.6
08/20/21 12:47
2,4-Dichlorophenol
ug/L
ND
5.0
1.4
08/20/21 12:47
2,4-Dimethylphenol
ug/L
ND
10.0
1.7
08/20/21 12:47
2,4-Dinitrophenol
ug/L
ND
50.0
26.0
08/20/21 12:47
2,4-Dinitrotoluene
ug/L
ND
5.0
1.6
08/20/21 12:47
2,6-Dinitrotoluene
ug/L
ND
5.0
1.7
08/20/21 12:47
2-Chloronaphthalene
ug/L
ND
5.0
1.7
08/20/21 12:47
2-Chlorophenol
ug/L
ND
5.0
1.2
08/20/21 12:47
2-Nitrophenol
ug/L
ND
5.0
1.4
08/20/21 12:47
3,3'-Dichlorobenzidine
ug/L
ND
10.0
8.1
08/20/21 12:47
4,6-Dinitro-2-methyl phenol
ug/L
ND
10.0
3.4
08/20/21 12:47
4-Bromophenylphenyl ether
ug/L
ND
5.0
1.8
08/20/21 12:47
4-ChIoro-3-methyl phenol
ug/L
ND
5.0
3.3
08/20/21 12:47
4-Chlorophenylphenyl ether
ug/L
ND
5.0
2.0
08/20/21 12:47
4-Nitrophenol
ug/L
ND
10.0
6.6
08/20/21 12:47
Acenaphthene
ug/L
ND
5.0
2.0
08/20/21 12:47
Acenaphthylene
ug/L
ND
5.0
2.0
08/20/21 12:47
Anthracene
ug/L
ND
5.0
2.3
08/20/21 12:47
Benzo(a)anthracene
ug/L
ND
5.0
2.7
08/20/21 12:47
Benzo(a)pyrene
ug/L
ND
5.0
2.8
08/20/21 12:47
Benzo(b)fluoranthene
ug/L
ND
5.0
2.6
08/20/21 12:47
Benzo(g,h,i)perylene
ug/L
ND
5.0
2.8
08/20/21 12:47
Benzo(k)fluoranthene
ug/L
ND
5.0
2.7
08/20/21 12:47
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
1.8
08/20/21 12:47
bis(2-Chloroethyl) ether
ug/L
ND
5.0
1.9
08/20/21 12:47
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
3.7
08/20/21 12:47
Butylbenzylphthalate
ug/L
ND
5.0
3.1
08/20/21 12:47
Chrysene
ug/L
ND
5.0
2.8
08/20/21 12:47
Di-n-butylphthalate
ug/L
ND
5.0
2.2
08/20/21 12:47
Di-n-octylphthalate
ug/L
ND
5.0
3.9
08/20/21 12:47
Dibenz(a,h)anthracene
ug/L
ND
5.0
3.0
08/20/21 12:47
Diethylphthalate
ug/L
ND
5.0
2.0
08/20/21 12:47
Dimethylphthalate
ug/L
ND
5.0
2.1
08/20/21 12:47
Fluoranthene
ug/L
ND
5.0
2.2
08/20/21 12:47
Fluorene
ug/L
ND
5.0
2.1
08/20/21 12:47
Hexachloro-1,3-butadiene
ug/L
ND
5.0
1.8
08/20/21 12:47
Hexachlorobenzene
ug/L
ND
5.0
2.2
08/20/21 12:47
Hexachlorocyclopentadiene
ug/L
ND
10.0
1.6
08/20/21 12:47
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 41 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
METHOD BLANK: 3365110
Associated Lab Samples: 92555464003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Hexachloroethane
ug/L
ND
5.0
1.4
08/20/21 12:47
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
2.9
08/20/21 12:47
Isophorone
ug/L
ND
10.0
1.7
08/20/21 12:47
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
1.3
08/20/21 12:47
N-Nitrosodimethylamine
ug/L
ND
5.0
1.9
08/20/21 12:47
N-Nitrosodiphenylamine
ug/L
ND
10.0
3.0
08/20/21 12:47
Naphthalene
ug/L
ND
5.0
2.1
08/20/21 12:47
Nitrobenzene
ug/L
ND
5.0
1.9
08/20/21 12:47
Pentachlorophenol
ug/L
ND
10.0
3.8
08/20/21 12:47
Phenanthrene
ug/L
ND
5.0
2.0
08/20/21 12:47
Phenol
ug/L
ND
5.0
1.4
08/20/21 12:47
Pyrene
ug/L
ND
5.0
2.2
08/20/21 12:47
2,4,6-Tribromophenol (S)
%
93
10-137
08/20/21 12:47
2-Fluorobiphenyl (S)
%
72
15-120
08/20/21 12:47
2-Fluorophenol (S)
%
56
10-120
08/20/21 12:47
Nitrobenzene-d5 (S)
%
89
10-120
08/20/21 12:47
Phenol-d6 (S)
%
42
10-120
08/20/21 12:47
Terphenyl-d14 (S)
%
112
11-131
08/20/21 12:47
LABORATORY CONTROL SAMPLE:
Parameter
3365111
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
31.6
63
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
42.6
85
36-166
2,4,6-Trichlorophenol
ug/L
50
54.1
108
37-144
2,4-Dichlorophenol
ug/L
50
51.9
104
1-191
2,4-Dimethylphenol
ug/L
50
52.7
105
32-119
2,4-Dinitrophenol
ug/L
250
273
109
1-181
2,4-Dinitrotoluene
ug/L
50
55.2
110
39-139
2,6-Dinitrotoluene
ug/L
50
55.8
112
50-158
2-Chloronaphthalene
ug/L
50
40.3
81
60-118
2-Chlorophenol
ug/L
50
47.6
95
23-134
2-Nitrophenol
ug/L
50
53.1
106
29-182
3,3'-Dichlorobenzidine
ug/L
100
106
106
1-262
4,6-Dinitro-2-methyl phenol
ug/L
100
126
126
1-181
4-Bromophenylphenyl ether
ug/L
50
54.9
110
53-127
4-Chloro-3-methylphenol
ug/L
100
107
107
22-147
4-Chlorophenylphenyl ether
ug/L
50
47.6
95
25-158
4-Nitrophenol
ug/L
250
148
59
1-132
Acenaphthene
ug/L
50
45.5
91
47-145
Acenaphthylene
ug/L
50
48.1
96
33-145
Anthracene
ug/L
50
56.7
113
1-166
Benzo(a)anthracene
ug/L
50
56.0
112
33-143
Benzo(a)pyrene
ug/L
50
58.1
116
17-163
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
LABORATORY CONTROL SAMPLE:
Parameter
3365111
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Benzo(b)fluoranthene
ug/L
50
57.0
114
24-159
Benzo(g,h,i)perylene
ug/L
50
56.6
113
1-219
Benzo(k)fluoranthene
ug/L
50
61.1
122
11-162
bis(2-Chloroethoxy)methane
ug/L
50
51.3
103
33-184
bis(2-Chloroethyl) ether
ug/L
50
57.5
115
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
62.9
126
8-158
Butylbenzylphthalate
ug/L
50
62.9
126
1-152
Chrysene
ug/L
50
56.2
112
17-168
Di-n-butylphthalate
ug/L
50
60.3
121
1-118 L1
Di-n-octylphthalate
ug/L
50
62.4
125
4-146
Dibenz(a,h)anthracene
ug/L
50
54.5
109
1-227
Diethylphthalate
ug/L
50
54.1
108
1-114
Dimethylphthalate
ug/L
50
52.2
104
1-112
Fluoranthene
ug/L
50
56.6
113
26-137
Fluorene
ug/L
50
50.0
100
59-121
Hexachloro-1,3-butadiene
ug/L
50
28.1
56
24-116
Hexachlorobenzene
ug/L
50
49.5
99
1-152
Hexachlorocyclopentadiene
ug/L
50
26.6
53
25-150
Hexachloroethane
ug/L
50
28.8
58
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
56.2
112
1-171
Isophorone
ug/L
50
55.9
112
21-196
N-Nitroso-di-n-propylamine
ug/L
50
55.3
111
1-230
N-Nitrosodimethylamine
ug/L
50
44.8
90
25-150
N-Nitrosodiphenylamine
ug/L
50
55.0
110
25-150
Naphthalene
ug/L
50
39.1
78
21-133
Nitrobenzene
ug/L
50
49.7
99
35-180
Pentachlorophenol
ug/L
100
103
103
14-176
Phenanthrene
ug/L
50
54.2
108
54-120
Phenol
ug/L
50
30.5
61
5-112
Pyrene
ug/L
50
58.2
116
52-115 L1
2,4,6-Tribromophenol (S)
%
133
10-137
2-Fluorobiphenyl (S)
%
97
15-120
2-Fluorophenol(S)
%
76
10-120
Nitrobenzene-d5(S)
%
111
10-120
Phenol-d6 (S)
%
63
10-120
Terphenyl-d14 (S)
%
122
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3365112
3365113
MS
MSD
35655676001 Spike
Spike MS
MSD
MS MSD % Rec
Max
Parameter
Units
Result Conc.
Conc. Result
Result
% Rec % Rec Limits RPD
RPD Qual
1,2,4-Trichlorobenzene
ug/L
8.61-1 50
50 21.6J
16AJ
43 33 44-142
30 M1
2,2'-Oxybis(1-
ug/L
5.81-1 50
50 21.1J
23.7J
42 47 36-166
30
chloropropane)
2,4,6-Trichlorophenol
ug/L
7.81-1 50
50 ND
ND
3 6 37-144
30 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 43 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3365112
MS
35655676001 Spike
Parameter Units Result Conc.
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Nitrophenol
3,3'-Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenylphenyl ether
4-Chloro-3-methylphenol
4-Chlorophenylphenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anth race ne
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-
Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2- Ethyl hexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
3365113
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits
ug/L
7.OU
50
50
9.91
ND
20
0
1-191
ug/L
8.5U
50
50
19.01
25.1J
38
50
32-119
ug/L
130U
250
250
ND
ND
0
0
1-181
ug/L
8.1 U
50
50
28.3
31.2
57
62
39-139
ug/L
8.6U
50
50
23.8J
24.2J
48
48
50-158
ug/L
8.6U
50
50
22.3J
21.7J
45
43
60-118
ug/L
6.OU
50
50
12AJ
16.3J
25
33
23-134
ug/L
7.OU
50
50
9.91
14.6J
20
29
29-182
ug/L
40.6U
100
100
60.3
47.3J
60
47
1-262
ug/L
17.OU
100
100
ND
ND
0
0
1-181
ug/L
8.8U
50
50
28.3
29.1
57
58
53-127
ug/L
16.7U
100
100
43.6
51.6
44
52
22-147
ug/L
10.0U
50
50
27.3
30.2
55
60
25-158
ug/L
33.OU
250
250
ND
ND
0
0
1-132
ug/L
10.0U
50
50
25.1
26.9
50
54
47-145
ug/L
9.8U
50
50
24.OJ
25.8
48
52
33-145
ug/L
11.6U
50
50
32.3
30.2
65
60
1-166
ug/L
13AU
50
50
37.6
31.3
75
63
33-143
ug/L
13.9U
50
50
37.1
31.3
74
63
17-163
ug/L
13.OU
50
50
35.5
30.0
71
60
24-159
ug/L
14.2U
50
50
39.2
32.1
78
64
1-219
ug/L
13.6U
50
50
37.5
32.2
75
64
11-162
ug/L
9.1 U
50
50
18.9J
24.3J
38
49
33-184
Max
RPD RPD Qual
30 M1
30
30 M1
10 30
30 M1
30 M1
30
30 M1
30
30 M1
3 30
17 30
10 30
30 M1
7 30
30
7 30
18 30
17 30
17 30
20 30
15 30
30
ug/L
9.6U
50
50
21 AJ
29.2
43
58
12-158
30
ug/L
18.6U
50
50
34.8
29.5
70
59
8-158
16
30
ug/L
15.7U
50
50
35.0
30.5
70
61
1-152
14
30
ug/L
13.8U
50
50
38.7
32.5
77
65
17-168
17
30
ug/L
11.0U
50
50
34.5
30.8
69
62
1-118
11
30
ug/L
19.6U
50
50
32.9
26.8
66
54
4-146
21
30
ug/L
14.8U
50
50
38.9
32.1
78
64
1-227
19
30
ug/L
10.2U
50
50
30.7
30.8
61
62
1-114
0
30
ug/L
10.6U
50
50
24.7J
27.7
49
55
1-112
30
ug/L
11.0U
50
50
37.6
33.1
75
66
26-137
13
30
ug/L
10AU
50
50
28.1
30.7
56
61
59-121
9
30 M1
ug/L
8.8U
50
50
22.5J
16.OJ
45
32
24-116
30
ug/L
10.8U
50
50
31.0
29.9
62
60
1-152
4
30
ug/L
8.OU
50
50
20AJ
15.2J
41
30
25-150
30
ug/L
6.9U
50
50
17.8J
12.OJ
36
24
40-113
30 M1
ug/L
14AU
50
50
38.9
32.4
78
65
1-171
18
30
ug/L
8.3U
50
50
21.7J
26.1J
43
52
21-196
30
ug/L
6.6U
50
50
20.6J
25.2
41
50
1-230
30
ug/L
9AU
50
50
16.6J
18.5J
33
37
25-150
30
ug/L
15.OU
50
50
28AJ
27.9J
57
56
25-150
30
ug/L
10AU
50
50
23.2J
20AJ
46
41
21-133
30
ug/L
9AU
50
50
20.6J
25.9
41
52
35-180
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3365112
MS
35655676001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3365113
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
Max
RPD RPD Qual
Pentachlorophenol
ug/L
18.8U 100
100
ND
ND
0
0
14-176
30 M1
Phenanthrene
ug/L
10.0U 50
50
33.2
30.9
66
62
54-120
7 30
Phenol
ug/L
6.8U 50
50
8.3J
14.2J
17
28
5-112
30
Pyrene
ug/L
11.0U 50
50
35.6
30.5
71
61
52-115
15 30
2,4,6-Tribromophenol (S)
%
8
11
10-137
S2
2-Fluorobiphenyl (S)
%
45
46
15-120
2-Fluorophenol (S)
%
10
14
10-120
Nitrobenzene-d5 (S)
%
40
50
10-120
D3
Phenol-d6 (S)
%
21
27
10-120
Terphenyl-d14 (S)
%
75
65
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 45 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 640998 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92555464001, 92555464002
METHOD BLANK: 3364327
Associated Lab Samples: 92555464001, 92555464002
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
333
131
08/18/21 16:47
1,2-Dichlorobenzene
ug/kg
ND
333
120
08/18/21 16:47
1,3-Dichlorobenzene
ug/kg
ND
333
118
08/18/21 16:47
1,4-Dichlorobenzene
ug/kg
ND
333
127
08/18/21 16:47
1-Methylnaphthalene
ug/kg
ND
333
117
08/18/21 16:47
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
333
159
08/18/21 16:47
2,4,5-Trichlorophenol
ug/kg
ND
333
153
08/18/21 16:47
2,4,6-Trichlorophenol
ug/kg
ND
333
137
08/18/21 16:47
2,4-Dichlorophenol
ug/kg
ND
333
130
08/18/21 16:47
2,4-Dimethylphenol
ug/kg
ND
333
138
08/18/21 16:47
2,4-Dinitrophenol
ug/kg
ND
1670
1030
08/18/21 16:47
2,4-Dinitrotoluene
ug/kg
ND
333
128
08/18/21 16:47
2,6-Dinitrotoluene
ug/kg
ND
333
122
08/18/21 16:47
2-Chloronaphthalene
ug/kg
ND
333
132
08/18/21 16:47
2-Chlorophenol
ug/kg
ND
333
125
08/18/21 16:47
2-Methylnaphthalene
ug/kg
ND
333
133
08/18/21 16:47
2-Methylphenol(o-Cresol)
ug/kg
ND
333
136
08/18/21 16:47
2-Nitroaniline
ug/kg
ND
1670
273
08/18/21 16:47
2-Nitrophenol
ug/kg
ND
333
144
08/18/21 16:47
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
333
134
08/18/21 16:47
3,3'-Dichlorobenzidine
ug/kg
ND
667
225
08/18/21 16:47
3-Nitroaniline
ug/kg
ND
1670
262
08/18/21 16:47
4,6-Dinitro-2-methyl phenol
ug/kg
ND
667
311
08/18/21 16:47
4-Bromophenylphenyl ether
ug/kg
ND
333
128
08/18/21 16:47
4-ChIoro-3-methyl phenol
ug/kg
ND
667
234
08/18/21 16:47
4-Chloroaniline
ug/kg
ND
667
262
08/18/21 16:47
4-Chlorophenylphenyl ether
ug/kg
ND
333
124
08/18/21 16:47
4-Nitroaniline
ug/kg
ND
667
254
08/18/21 16:47
4-Nitrophenol
ug/kg
ND
1670
644
08/18/21 16:47
Acenaphthene
ug/kg
ND
333
117
08/18/21 16:47
Acenaphthylene
ug/kg
ND
333
117
08/18/21 16:47
Aniline
ug/kg
ND
333
130
08/18/21 16:47
Anthracene
ug/kg
ND
333
109
08/18/21 16:47
Benzo(a)anthracene
ug/kg
ND
333
111
08/18/21 16:47
Benzo(a)pyrene
ug/kg
ND
333
115
08/18/21 16:47
Benzo(b)fluoranthene
ug/kg
ND
333
111
08/18/21 16:47
Benzo(g,h,i)perylene
ug/kg
ND
333
129
08/18/21 16:47
Benzo(k)fluoranthene
ug/kg
ND
333
117
08/18/21 16:47
Benzoic Acid
ug/kg
ND
1670
716
08/18/21 16:47
Benzyl alcohol
ug/kg
ND
667
253
08/18/21 16:47
v2
v1
IL
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
METHOD BLANK: 3364327
Associated Lab Samples: 92555464001, 92555464002
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
bis(2-Chloroethoxy)methane
ug/kg
ND
333
138
08/18/21 16:47
bis(2-Chloroethyl) ether
ug/kg
ND
333
125
08/18/21 16:47
bis(2-Ethylhexyl)phthalate
ug/kg
ND
333
129
08/18/21 16:47
Butylbenzylphthalate
ug/kg
ND
333
140
08/18/21 16:47
Chrysene
ug/kg
ND
333
121
08/18/21 16:47
Di-n-butylphthalate
ug/kg
ND
333
112
08/18/21 16:47
Di-n-octylphthalate
ug/kg
ND
333
131
08/18/21 16:47
Dibenz(a,h)anthracene
ug/kg
ND
333
128
08/18/21 16:47
Dibenzofuran
ug/kg
ND
333
120
08/18/21 16:47
Diethylphthalate
ug/kg
ND
333
122
08/18/21 16:47
Dimethylphthalate
ug/kg
ND
333
121
08/18/21 16:47
Fluoranthene
ug/kg
ND
333
114
08/18/21 16:47
Fluorene
ug/kg
ND
333
117
08/18/21 16:47
Hexachloro-1,3-butadiene
ug/kg
ND
333
144
08/18/21 16:47
Hexachlorobenzene
ug/kg
ND
333
130
08/18/21 16:47
Hexachlorocyclopentadiene
ug/kg
ND
333
191
08/18/21 16:47
Hexachloroethane
ug/kg
ND
333
127
08/18/21 16:47
Indeno(1,2,3-cd)pyrene
ug/kg
ND
333
131
08/18/21 16:47
Isophorone
ug/kg
ND
333
148
08/18/21 16:47
N-Nitroso-di-n-propylamine
ug/kg
ND
333
125
08/18/21 16:47
N-Nitrosodimethylamine
ug/kg
ND
333
112
08/18/21 16:47
N-Nitrosodiphenylamine
ug/kg
ND
333
118
08/18/21 16:47
Naphthalene
ug/kg
ND
333
113
08/18/21 16:47
Nitrobenzene
ug/kg
ND
333
155
08/18/21 16:47
Pentachlorophenol
ug/kg
ND
667
326
08/18/21 16:47
Phenanthrene
ug/kg
ND
333
109
08/18/21 16:47
Phenol
ug/kg
ND
333
148
08/18/21 16:47
Pyrene
ug/kg
ND
333
135
08/18/21 16:47
Pyridine
ug/kg
ND
333
105
08/18/21 16:47
2,4,6-Tribromophenol (S)
%
71
18-130
08/18/21 16:47
2-Fluorobiphenyl (S)
%
69
19-130
08/18/21 16:47
2-Fluorophenol (S)
%
56
18-130
08/18/21 16:47
Nitrobenzene-d5 (S)
%
61
21-130
08/18/21 16:47
Phenol-d6 (S)
%
56
18-130
08/18/21 16:47
Terphenyl-d14 (S)
%
68
15-130
08/18/21 16:47
Qualifiers
LABORATORY CONTROL SAMPLE:
3364328
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1670
1410
84
47-130
1,2-Dichlorobenzene
ug/kg
1670
1240
74
49-130
1,3-Dichlorobenzene
ug/kg
1670
1200
72
48-130
1,4-Dichlorobenzene
ug/kg
1670
1250
74
49-130
1-Methylnaphthalene
ug/kg
1670
1430
85
54-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
LABORATORY CONTROL SAMPLE:
Parameter
3364328
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,2'-Oxybis(1-chloropropane)
ug/kg
1670
843
50
38-130 v3
2,4,5-Trichlorophenol
ug/kg
1670
1460
87
49-130
2,4,6-Trichlorophenol
ug/kg
1670
1400
84
50-130
2,4-Dichlorophenol
ug/kg
1670
1430
86
51-130
2,4-Dimethylphenol
ug/kg
1670
1350
81
53-130
2,4-Dinitrophenol
ug/kg
8360
8750
105
39-130 v1
2,4-Dinitrotoluene
ug/kg
1670
1400
84
53-130
2,6-Dinitrotoluene
ug/kg
1670
1410
84
55-130
2-Chloronaphthalene
ug/kg
1670
1300
78
48-130
2-Chlorophenol
ug/kg
1670
1190
71
54-130
2-Methylnaphthalene
ug/kg
1670
1420
85
57-130
2-Methylphenol(o-Cresol)
ug/kg
1670
1270
76
50-130
2-Nitroaniline
ug/kg
3340
2270
68
49-130
2-Nitrophenol
ug/kg
1670
1470
88
50-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1670
1220
73
50-130
3,3'-Dichlorobenzidine
ug/kg
3340
2630
79
47-130IL
3-Nitroaniline
ug/kg
3340
2850
85
45-130
4,6-Dinitro-2-methyl phenol
ug/kg
3340
3220
96
50-142
4-Bromophenylphenyl ether
ug/kg
1670
1430
86
55-130
4-ChIoro-3-methyl phenol
ug/kg
3340
2800
84
52-130
4-Chloroaniline
ug/kg
3340
2640
79
49-130
4-Chlorophenylphenyl ether
ug/kg
1670
1470
88
53-130
4-Nitroaniline
ug/kg
3340
2690
80
51-130
4-Nitrophenol
ug/kg
8360
6530
78
40-130
Acenaphthene
ug/kg
1670
1480
89
56-130
Acenaphthylene
ug/kg
1670
1470
88
58-130
Aniline
ug/kg
1670
1060
63
44-130
Anthracene
ug/kg
1670
1420
85
60-130
Benzo(a)anthracene
ug/kg
1670
1430
85
59-130
Benzo(a)pyrene
ug/kg
1670
1430
85
57-130
Benzo(b)fluoranthene
ug/kg
1670
1420
85
54-130
Benzo(g,h,i)perylene
ug/kg
1670
1460
88
59-130
Benzo(k)fluoranthene
ug/kg
1670
1410
84
54-130
Benzoic Acid
ug/kg
8360
5880
70
19-130
Benzyl alcohol
ug/kg
3340
2380
71
50-130
bis(2-Chloroethoxy)methane
ug/kg
1670
1240
74
55-130
bis(2-Chloroethyl) ether
ug/kg
1670
1180
70
53-130
bis(2-Ethylhexyl)phthalate
ug/kg
1670
1340
80
58-130
Butylbenzylphthalate
ug/kg
1670
1360
81
46-138
Chrysene
ug/kg
1670
1440
86
57-130
Di-n-butylphthalate
ug/kg
1670
1370
82
57-130
Di-n-octylphthalate
ug/kg
1670
1400
84
57-130
Dibenz(a,h)anthracene
ug/kg
1670
1460
87
60-130
Dibenzofuran
ug/kg
1670
1430
85
54-130
Diethylphthalate
ug/kg
1670
1450
87
55-130
Dimethylphthalate
ug/kg
1670
1390
83
57-130
Fluoranthene
ug/kg
1670
1530
92
57-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
LABORATORY CONTROL SAMPLE:
3364328
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Fluorene
ug/kg
1670
1450
87
56-130
Hexachloro-1,3-butadiene
ug/kg
1670
1520
91
41-130
Hexachlorobenzene
ug/kg
1670
1400
84
53-130
Hexachlorocyclopentadiene
ug/kg
1670
1080
65
23-130
Hexachloroethane
ug/kg
1670
1190
71
48-130
Indeno(1,2,3-cd)pyrene
ug/kg
1670
1480
88
61-130
Isophorone
ug/kg
1670
1290
77
49-130
N-Nitroso-di-n-propylamine
ug/kg
1670
1130
68
52-130
N-Nitrosodimethylamine
ug/kg
1670
1060
63
45-130
N-Nitrosodiphenylamine
ug/kg
1670
1310
78
56-130
Naphthalene
ug/kg
1670
1350
81
56-130
Nitrobenzene
ug/kg
1670
1250
75
50-130
Pentachlorophenol
ug/kg
3340
2670
80
33-130
Phenanthrene
ug/kg
1670
1420
85
60-130
Phenol
ug/kg
1670
1260
75
54-130
Pyrene
ug/kg
1670
1440
86
61-130
Pyridine
ug/kg
1670
842
50
35-130
2,4,6-Tribromophenol (S)
%
88
18-130
2-Fluorobiphenyl (S)
%
83
19-130
2-Fluorophenol (S)
%
68
18-130
Nitrobenzene-d5(S)
%
75
21-130
Phenol-d6 (S)
%
69
18-130
Terphenyl-d14 (S)
%
82
15-130
MATRIX SPIKE SAMPLE:
3364329
92555565001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
2200
1100
50
22-130
1,2-Dichlorobenzene
ug/kg
ND
2200
1010
46
23-130
1,3-Dichlorobenzene
ug/kg
ND
2200
978
45
26-130
1,4-Dichlorobenzene
ug/kg
ND
2200
1010
46
27-130
1-Methylnaphthalene
ug/kg
ND
2200
1100
50
30-130
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
2200
684
31
30-130 v3
2,4,5-Trichlorophenol
ug/kg
ND
2200
1130
51
26-130
2,4,6-Trichlorophenol
ug/kg
ND
2200
1100
50
23-130
2,4-Dichlorophenol
ug/kg
ND
2200
1100
50
29-130
2,4-Dimethylphenol
ug/kg
ND
2200
936
43
13-130
2,4-Dinitrophenol
ug/kg
ND
11000
6010
55
10-131 v1
2,4-Dinitrotoluene
ug/kg
ND
2200
1070
49
28-130
2,6-Dinitrotoluene
ug/kg
ND
2200
1090
50
36-130
2-Chloronaphthalene
ug/kg
ND
2200
1010
46
27-130
2-Chlorophenol
ug/kg
ND
2200
975
44
29-130
2-Methylnaphthalene
ug/kg
ND
2200
1060
48
29-130
2-Methylphenol(o-Cresol)
ug/kg
ND
2200
948
43
20-130
2-Nitroaniline
ug/kg
ND
4400
1710J
39
29-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
MATRIX SPIKE SAMPLE:
3364329
92555565001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Nitrophenol
ug/kg
ND
2200
1100
50
26-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
2200
931
42
10-176
3,3'-Dichlorobenzidine
ug/kg
ND
4400
1900
43
15-130IL
3-Nitroaniline
ug/kg
ND
4400
2140J
49
28-130
4,6-Dinitro-2-methyl phenol
ug/kg
ND
4400
2240
51
15-132
4-Bromophenylphenyl ether
ug/kg
ND
2200
1060
48
35-130
4-Chloro-3-methylphenol
ug/kg
ND
4400
2070
47
30-130
4-Chloroaniline
ug/kg
ND
4400
1960
45
28-130
4-Chlorophenylphenyl ether
ug/kg
ND
2200
1090
49
32-130
4-Nitroaniline
ug/kg
ND
4400
2030
46
30-130
4-Nitrophenol
ug/kg
ND
11000
5000
46
17-130
Acenaphthene
ug/kg
ND
2200
1130
51
29-130
Acenaphthylene
ug/kg
ND
2200
1130
51
31-130
Aniline
ug/kg
ND
2200
720
33
10-130
Anthracene
ug/kg
ND
2200
1070
49
33-130
Benzo(a)anthracene
ug/kg
ND
2200
1060
48
32-130
Benzo(a)pyrene
ug/kg
ND
2200
1040
47
32-130
Benzo(b)fluoranthene
ug/kg
ND
2200
1000
46
33-130
Benzo(g,h,i)perylene
ug/kg
ND
2200
1100
50
28-130
Benzo(k)fluoranthene
ug/kg
ND
2200
994
45
31-130
Benzoic Acid
ug/kg
ND
11000
3600
33
10-130
Benzyl alcohol
ug/kg
ND
4400
1810
41
31-130
bis(2-Chloroethoxy)methane
ug/kg
ND
2200
973
44
30-130
bis(2-Chloroethyl) ether
ug/kg
ND
2200
946
43
68-130 M1
bis(2-Ethylhexyl)phthalate
ug/kg
ND
2200
958
44
40-130
Butylbenzylphthalate
ug/kg
ND
2200
964
44
40-130
Chrysene
ug/kg
ND
2200
1060
48
30-130
Di-n-butylphthalate
ug/kg
ND
2200
999
45
41-130
Di-n-octylphthalate
ug/kg
ND
2200
982
45
42-130
Dibenz(a,h)anthracene
ug/kg
ND
2200
1050
48
27-130
Dibenzofuran
ug/kg
ND
2200
1110
50
32-130
Diethylphthalate
ug/kg
ND
2200
1130
51
40-130
Dimethylphthalate
ug/kg
ND
2200
1080
49
37-130
Fluoranthene
ug/kg
ND
2200
1130
52
26-130
Fluorene
ug/kg
ND
2200
1100
50
31-130
Hexachloro-1,3-butadiene
ug/kg
ND
2200
1190
54
20-130
Hexachlorobenzene
ug/kg
ND
2200
1030
47
29-130
Hexachlorocyclopentadiene
ug/kg
ND
2200
656
30
10-130
Hexachloroethane
ug/kg
ND
2200
968
44
21-130
Indeno(1,2,3-cd)pyrene
ug/kg
ND
2200
1100
50
28-130
Isophorone
ug/kg
ND
2200
977
44
32-130
N-Nitroso-di-n-propylamine
ug/kg
ND
2200
906
41
31-130
N-Nitrosodimethylamine
ug/kg
ND
2200
800
36
20-130
N-Nitrosodiphenylamine
ug/kg
ND
2200
1000
46
32-130
Naphthalene
ug/kg
ND
2200
1080
49
30-130
Nitrobenzene
ug/kg
ND
2200
955
43
25-130
Pentachlorophenol
ug/kg
ND
4400
1920
44
10-130
Results presented on this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
MATRIX SPIKE SAMPLE:
Parameter
3364329
Units
92555565001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Phenanthrene
ug/kg
ND
2200
1070
49
34-130
Phenol
ug/kg
ND
2200
984
45
14-130
Pyrene
ug/kg
ND
2200
1080
49
31-130
Pyridine
ug/kg
ND
2200
324J
15
10-130
2,4,6-Tribromophenol (S)
%
48
18-130
2-Fluorobiphenyl (S)
%
48
19-130
2-Fluorophenol (S)
%
40
18-130
Nitrobenzene-d5 (S)
%
44
21-130
Phenol-d6 (S)
%
40
18-130
Terphenyl-d14 (S)
%
43
15-130
SAMPLE DUPLICATE: 3364330
Parameter
Units
92555565003
Result
Dup
Result RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
1-Methylnaphthalene
ug/kg
ND
ND
30
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
30 v2
2,4,5-Trichlorophenol
ug/kg
ND
ND
30
2,4,6-Trichlorophenol
ug/kg
ND
ND
30
2,4-Dichlorophenol
ug/kg
ND
ND
30
2,4-Dimethylphenol
ug/kg
ND
ND
30
2,4-Dinitrophenol
ug/kg
ND
ND
30 v1
2,4-Dinitrotoluene
ug/kg
ND
ND
30
2,6-Dinitrotoluene
ug/kg
ND
ND
30
2-Chloronaphthalene
ug/kg
ND
ND
30
2-Chlorophenol
ug/kg
ND
ND
30
2-Methylnaphthalene
ug/kg
ND
ND
30
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
30
2-Nitroaniline
ug/kg
ND
ND
30
2-Nitrophenol
ug/kg
ND
ND
30
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
30
3,3'-Dichlorobenzidine
ug/kg
ND
ND
30 IL
3-Nitroaniline
ug/kg
ND
ND
30
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
30
4-Bromophenylphenyl ether
ug/kg
ND
ND
30
4-ChIoro-3-methyl phenol
ug/kg
ND
ND
30
4-Chloroaniline
ug/kg
ND
ND
30
4-Chlorophenylphenyl ether
ug/kg
ND
ND
30
4-Nitroaniline
ug/kg
ND
ND
30
4-Nitrophenol
ug/kg
ND
ND
30
Acenaphthene
ug/kg
ND
ND
30
Acenaphthylene
ug/kg
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 51 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: AGL-003
Pace Project No.: 92555464
SAMPLE DUPLICATE: 3364330
Parameter
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
Units
92555565003 Dup
Result Result
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
ug/kg
ND
46
%
52
41
46
42
44
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
52
56
44
50
45
50
Max
RPD RPD
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 52 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 640610 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92555464001, 92555464002
METHOD BLANK: 3362015
Matrix:
Solid
Associated Lab Samples:
92555464001, 92555464002
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
9.9
9.9 08/18/21 08:37 N2
Aliphatic (C19-C36)
mg/kg
ND
9.9
9.9 08/18/21 08:37 N2
Aromatic (C11-C22)
mg/kg
ND
9.9
9.9 08/18/21 08:37 N2
1-Chlorooctadecane (S)
%
76
40-140
08/18/21 08:37
2-Bromonaphthalene (S)
%
87
40-140
08/18/21 08:37
2-Fluorobiphenyl (S)
%
87
40-140
08/18/21 08:37
o-Terphenyl (S)
%
92
40-140
08/18/21 08:37
LABORATORY CONTROL SAMPLE & LCSD:
3362016
3362017
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
10
ND ND
67
78
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.4
12.0 12.3
90
92
40-140 2 50 N2
Aromatic (C11-C22)
mg/kg
28.4
21.4 21.5
75
76
40-140 0 50 N2
1-Chlorooctadecane (S)
%
84
86
40-140
2-Bromonaphthalene (S)
%
66
82
40-140
2-Fluorobiphenyl (S)
%
78
84
40-140
o-Terphenyl(S)
%
82
87
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 53 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 641869 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Water
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92555464003
METHOD BLANK: 3368632
Matrix:
Water
Associated Lab Samples: 92555464003
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Aliphatic (C09-C18)
ug/L
ND
100
100 08/23/21 10:07 N2
Aliphatic (C19-C36)
ug/L
ND
100
100 08/23/21 10:07 N2
Aromatic (C11-C22)
ug/L
ND
100
100 08/23/21 10:07 N2
1-Chlorooctadecane (S)
%
56
40-140
08/23/21 10:07
2-Bromonaphthalene (S)
%
81
40-140
08/23/21 10:07
2-Fluorobiphenyl (S)
%
78
40-140
08/23/21 10:07
o-Terphenyl (S)
%
81
40-140
08/23/21 10:07
LABORATORY CONTROL SAMPLE & LCSD:
3368633
3368634
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
ug/L
300
163
155
54
52
40-140 5 50 N2
Aliphatic (C19-C36)
ug/L
400
275
263
69
66
40-140 4 50 N2
Aromatic (C11-C22)
ug/L
850
489
712
58
84
40-140 37 50 N2
1-Chlorooctadecane (S)
%
41
45
40-140
2-Bromonaphthalene (S)
%
66
97
40-140
2-Fluorobiphenyl (S)
%
64
94
40-140
o-Terphenyl(S)
%
63
95
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 54 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: AGL-003
Pace Project No.: 92555464
QC Batch: 640655 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92555464001, 92555464002
SAMPLE DUPLICATE: 3362338
92555332001
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Percent Moisture
%
20.3
20.8
2 25 N2
SAMPLE DUPLICATE: 3362339
92555464002
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Percent Moisture
%
21.4
20.9
3 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: AGL-003
Pace Project No.: 92555464
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N The reported TIC has an 85% or higher match on a mass spectral library search.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
P2 Re -extraction or re -analysis could not be performed due to insufficient sample amount.
SO Surrogate recovery outside laboratory control limits.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 72

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
AGL-003
92555464
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92555464003
MW-1
EPA 504.1
640847
EPA 504.1
640974
92555464001
MW-1 (7-8)
MADEP EPH
640610
MADEP EPH
641197
92555464002
MW-1 (10-11)
MADEP EPH
640610
MADEP EPH
641197
92555464003
MW-1
MADEP EPH
641869
MADEP EPH
642211
92555464001
MW-1 (7-8)
MADEP VPH
640702
MADEP VPH
640708
92555464002
MW-1 (10-11)
MADEP VPH
641021
MADEP VPH
641053
92555464003
MW-1
MADEP VPH
640758
92555464003
MW-1
EPA 625.1
641142
EPA 625.1
641973
92555464001
MW-1 (7-8)
EPA 3546
640998
EPA 8270E
641357
92555464002
MW-1 (10-11)
EPA 3546
640998
EPA 8270E
641357
92555464003
MW-1
SM 6200B
640957
92555464003
MW-1
SM 6200B
640682
92555464001
MW-1 (7-8)
EPA 5035A/5030B
641266
EPA 8260D
641285
92555464002
MW-1 (10-11)
EPA 5035A/5030B
641562
EPA 8260D
641609
92555464001
MW-1 (7-8)
SW-846
640655
92555464002
MW-1 (10-11)
SW-846
640655
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/23/2021 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 72

Dacument Name:
Document Revised: October 28, 2020
�ceAnalyfical
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority;
F-CAR-CS-033-Rev.07
Pace Caralinas Quailty Office
Laboratory receiving samples -
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑
ConditionSample Client Name: W0# : 92555464
p'
V� C�" -Y � _J 7 V1, M Projecl1111
till 11111 it
Courler. ❑Fed Ex
❑UPS ❑U5P5 Client!1I
❑ Commercial ❑Pace ❑Other: 92555464
l
Custody Seal Present? Dyes QNo Seals Intact? []Yes ®No t
Date/InAIah Person Examining contents:C�
Packing Material: ❑Bubble Wrap ]Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: []Yes ❑No ❑N/A
r t-1 [:Wet ❑Blue ❑None
ype a ce:
t1, Correction Factor: 1
Cooler Temp; " Add/Subtract (IC) — b . I '' ( Temp should be above freezing to 6"C
Cooler Temp Corrected ('C): LJ , -7 r) ❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil ('❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationally,
Comments/Discrepancy:
Chain of Custody Present?
Yes
No
[]N/A
1.
Samples Arrived within Hold Time?
javres
[:]No
❑N/A
2.
Short Hold Time Analysis 02 hr.)?
❑Yes
faPJo
N/A
3.
Rush Turn Around Time Requested?
❑Yes
Q No
❑N/A
4.
Sufficient Volume?
Qves
❑No
❑N/A
S.
Correct Containers Used?
ElYes
❑No
[]N/A
6.
-Pace Containers Used?
_,]Yes
❑No
❑N/A
Containers Intact?
Yes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
N/A
g.
Sample Labels Match COC?
ElYes
❑No
[:]N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
/.1f
Headspace in VOA Vials (>5-6mm)?
Yes
d o
❑N/A
10.
Trip Blank Present? ?❑Yes
QNo
❑N/A
11.
Trip Blank Custody Seals Present?
[]Yes
[]No
[J /A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of splRcontainers:
CLIENT NOTIFICATION/RESOLUTION
—�Perso
Project Manager SCURF Review:
Project Manager 5RF Review:
Date:
Date:
Field Data Required? ❑Yes ❑No
Page 58 of 72

e
r . c?CeAnalytical
Document Name:
Sample Condition Upon Recelpt(SCUR)
Document Revised: October 28, 2020
Page 2 of 2
Document No.:
ossuing Authority:
F-CAR-0-0334(ev.07
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Colifnrm, TOC, Oil and Grease, DRO/8015 (water) DOC, 1LHg
*"Bottom half of box is to list number of bottles
Project #
Wp#:92555464
PM: KRIS Due Dale: 08/20/21
CLIENT: 92-Hari Hick
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PH Adjustment Log for Preserved Samples
Sample ID
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pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
lot a
Note: -When ever the re-is-adiscrepancy-affecting-North-Garolina-eomplian ce-samples,-a-copy-ot-thisform-will-be-sent-to-the-Nor-th-6arelina-DEHNHa.orurlcauon-urrice-I
Out of hold, Incorrect preservative, out of temp, incorrect containers.

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Page 60 of 72
In
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o

con -test®
A Pace Anaoicalg Laboratary
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
August 23, 2021
Kevin Godwin
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: NC
Client Job Number:
Project Number: 92555464
Laboratory Work Order Number: 21HO898
Enclosed are results of analyses for samples received by the laboratory on August 19, 2021. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
j�.unxtt
Kerry K. McGee
Project Manager
ST.T-WISEN (I
. • ' •

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
21 HO898-01
Sample Preparation Information
QC Data
Metals Analyses (Total)
B288547
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
5
5
6
7
7
7
8
9
10
�rrswasr�r

Table of Contents
con -test®
A Pace Analyticalg Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100 REPORT DATE: 8/23/2021
Huntersville, NC 28078 PURCHASE ORDER NUMBER:
ATTN: Kevin Godwin
PROJECT NUMBER: 92555464
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 21H0898
The results of analyses performed on the following samples submitted to CON -TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION: NC
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
MW-1 21H0898-01 Water SW-846 6020B
Page 3 of 12

con -test®
A Pace Analyticalg Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
ST.T3IIIEN
■ - 0

Table of Contents
con -test®
A Pace Analyticalg Laboratory
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: NC Sample Description: Work Order: 21H0898
Date Received: 8/19/2021
Field Sample #: MW-1 Sampled: 8/13/2021 12:55
Sample ID: 21H0898-01
Samule Matrix: Water
Metals Analyses (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Lead ND 0.50 0.14 µg/L 1 SW-846 6020B 8/19/21 8/20/21 12:39 QNW
Page 5 of 12

con -test®
A Pace Analyticalg Laboratory
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3005A Analytical Method: SW-846 6020B
Lab Number [Field ID] Batch Initial [mL] Final [mL] Date
21HO898-01 [MW-1] B288547 50.0 50.0 08/19/21
ST.T3YCT.Si(I

con -test®
A Pace Analyticalg Laboratary
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B288547 - SW-846 3005A
Blank (B288547-BLK1)
Prepared: 08/19/21 Analyzed: 08/20/21
Lead
LCS (B288547-BS1)
ND 0.50
µg/L
Prepared: 08/19/21 Analyzed: 08/20/21
Lead
LCS Dup (B288547-BSD1)
540 5.0
µg/L
500 108 80-120
Prepared: 08/19/21 Analyzed: 08/20/21
Lead
Duplicate (B288547-DUP1)
478 5.0
Source: 21HO898-01
µg/L
500 95.6 80-120 12.2 20
Prepared: 08/19/21 Analyzed: 08/20/21
Lead
Matrix Spike (B288547-MS1)
ND 0.50
Source: 21HO898-01
µg/L
ND NC 20
Prepared: 08/19/21 Analyzed: 08/20/21
Lead
487 5.0
µg/L
500 ND 97.4 75-125
Page 7 of 12

con -test®
A Pace Analytical*' Laboratary
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
FLAG/QUALIFIER SUMMARY
*
QC result is outside of established limits.
fi
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
ND
Not Detected
RL
Reporting Limit is at the level of quantitation (LOQ)
DL
Detection Limit is the lower limit of detection determined by the MDL study
MCL
Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
- - . - .:�Si(I
. • O i •

con -test®
A Pace Analyticalg Laboratet
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 6020B in Water
Lead CT,NH,NY,ME,VA,NC
Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditation:
Code Description Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2017
100033
03/l/2022
MA
Massachusetts DEP
M-MA100
06/30/2022
CT
Connecticut Department of Publilc Health
PH-0165
12/31/2022
NY
New York State Department of Health
10899 NELAP
04/l/2022
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2022
RI
Rhode Island Department of Health
LA000112
12/30/2021
NC
North Carolina Div. of Water Quality
652
12/31/2021
NJ
New Jersey DEP
MA007 NELAP
06/30/2022
FL
Florida Department of Health
E871027 NELAP
06/30/2022
VT
Vermont Department of Health Lead Laboratory
LL720741
07/30/2022
ME
State of Maine
MA00100
06/9/2023
VA
Commonwealth of Virginia
460217
12/14/2021
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2021
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2022
NC-DW
North Carolina Department of Health
25703
07/31/2022
PA
Commonwealth of Pennsylvania DEP
68-05812
06/30/2022
MI
Dept. of Env, Great Lakes, and Energy
9100
09/6/2021
ST.T34LSESi(I
■ •BOX.]

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Table of Contents
Page 10 of 12 1

Table of Contents
TRACK ANOTHER SHIPMENT
501389196940
ADD NICKNAME
Delivered
Thursday, August 19, 2021 at 10.16 am
FROM
ASHEVILLE, NC US
Travel History
TIME ZONE
Local Scan Time
Thursday, August 19, 2021
10:16 AM
EAST LONGMEADOW, MA
8 57 AM
WINDSOR LOCKS, CT
825 AM
WINDSOR LOCKS, CT
6:52 AM
EAST GRANBY, CT
3:42 AM
MEMPHIS, TN
Wednesday, August 18, 2021
DELIVERED
Signed for by: R.PATRATIS
GET STATUS UPDATES
OBTAIN PROOF OF DELIVERY
Delivered
On FedEx vehicle for delivery
At local FedEx facility
At destination sort facility
Departed FedEx hub
10:33 PM MEMPHIS, TN
Arrived at FedEx hub
7 48 PM ASHEVILLE, NC
Left FedEx origin facility
5:20 PM ASHEVILLE, NC
Picked up
2:58 PM
Shipment information sent to FedEx
Shiprnent Facts
TO
EAST LONGMEADOW, MA US
I\/
Page 11 of 12

Table of Contents
I Have Not Confirmed Sample Container C Co tv a'= t le ms t
Numbers With Lab Staff Before Relinquishing �.�sa�nicA� �o�ars�xv
Over Samples
Doc#:277 : Rey 62017
Login Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client
-
Received By
How were the samples
received?
Were samples within
Date
In Cooler No Cooler
Direct from Sampling
By Gun #
Time t�LIS
On Ice No Ice
Ambient
Actual Teme a
Melted Ice
Temperature? 2-6°C T By Blank # Actual Temp -
Was Custody Seal Intact? UA Were Samples Tampered with? U�
Was COC Relinquished ? -T Does Chain Agree With Samples? -T
Are there broken/leaking/loose caps on any samples?
Is CDC in ink/ Legible? Were samples received within holding time?
Did COC include all Client j Analysis 1 Sampler Name j
pertinent Information? Project ID`s 7 Collection Dates/Times ?
Are Sample labels filled out and legible? o
Are there Lab to Filters? I Who was notified?
Are there Rushes?
Are there Short Holds?
Is there enough Volume?
Is there Headspace where applicable?
Proper Media/Containers Used?
Were trip blanks received?
Do all samples have the proper pH?
Who was notified? l ti
Who was notified?
I
MS/MSD?
"r Is splitting samples required?
T— On COC?
Acid �� Base
Un -
1 Liter Amb.
'I Liter Plastic
16 oz Amb.
HCL-
500 mL Amb.
500 mL Plastic
8oz Amb/Clear
Meoh-
250 mL Amb.
250 mL Plastic
4oz AmblClear
Bisulfate-
Flashpoint
Col./Bacteria
2oz Amb/Clear
DI-
Other Glass
Other Plastic
Encore
Thiosulfate-
SOC Kit
Plastic Bag
Frozen:
Sulfuric-
Perchlorate
Ziplock
-
s,
Unp-
1 Liter Amb.
1 Liter Plastic
16 oz Amb.
HCL-
500 mL Amb.
500 mL Plastic
8oz AmblClear
Meoh-
250 mL Amb.
250 mL Plastic
4oz AmblClear
Bisulfate-
Col./Bacteria
Flashpoint
2oz AmblClear
DI-
Other Plastic
Other Glass
Encore
Thiosulfate-
SOC Kit
Plastic Ba
Frozen:
Sulfuric-
Perchlorate
Ziplock
Comments:
Page 12 of 12

Beverly, Trudy
From: Beverly, Trudy
Sent: Monday, August 30, 2021 6:56 AM
To: Brett Lawrence; Caldwell, Shawna; Morris, Brett L.; Yuriy Vaynshteyn; John Desiatnikov
Subject: RE: [External] RE: Metrolina Steel - UST Incident #47936 — Notice of Regulatory
Requirements
Received.
Trudy
Trudy Beverly, L.G.
D-�IE Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
IFepnrlr. en[ of Gmn-on mental 4w
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: hit2s://deq.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://dea.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-mans
File Review Procedures:
hops://deq.ne. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
fts://deq.nc.gov/about/divisions/waste-manaizement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
htti)s:Hfiles.ne.izov/nedeafWaste%2OMana2ement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policv.l)df
https:Hfiles.nc.gov/ncdeq/Waste%20Management/D WM/UST/Corrective%2OAction/UST%2Ofilc%20names%20for%2OLaserfiche.docx
From: Brett Lawrence [mailto:[e-mail]]
Sent: Friday, August 27, 2021 4:51 PM
To: Beverly, Trudy <[e-mail]>; Caldwell, Shawna <[e-mail]>;
Morris, Brett L. <[e-mail]>; Yuriy Vaynshteyn <[e-mail]>;
John Desiatnikov <[e-mail]>
Subject: [External] RE: Metrolina Steel - UST Incident #47936 — Notice of Regulatory Requirements
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Trudy,
Please see the attached Phase I LSA report for the above project site. A NRP is being drafted and will be sent to you for
review. Let me know if you have any questions or need anything further. Have a great weekend.
Thanks,
Brett

Id Brett Lawrence, PG, Sr. Project Geologist
Hart &Hickman, PC
2923 S Tryon Street, Suite 100 • Charlotte, NC 28203
Direct: [phone] • Mobile: [phone]
www.harthickman.com
From: Beverly, Trudy <[e-mail]>
Sent: Thursday, August 5, 20214:26 PM
To: Caldwell, Shawna <[e-mail]>; Morris, Brett L.
<[e-mail]>; Brett Lawrence <[e-mail]>; Yuriy Vaynshteyn
<[e-mail]>; John Desiatnikov <[e-mail]>
Subject: Metrolina Steel - UST Incident #47936 — Notice of Regulatory Requirements
Please see the attached Notice of Regulatory Requirements for Metrolina Steel located at 1118 West Craighead,
Charlotte, Mecklenburg County, North Carolina (UST Incident #47936).
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenn aov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: hgps://deg.nc.gov/about/divisions/waste-management/ust/ast-prosram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-maps
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hLtps://deg.nc.gov/about/divisions/waste-manaaement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https://files.nc.aov/ncdep/Waste%2OManaeement/DWM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policy.odf
https://files.nc.,gov/ncdegiWaste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx