24039_Jones Electric_Phase II ESA_20200127

SUMMIT Engineering, Laboratory & Testing, Inc. 3575 Centre Circle Fort Mill, South Carolina 29715 www.SUMMIT-companies.com Phone: [phone] Fax: [phone]
January 27, 2020 Mr. Ronn Stewart
Laurel Street Residential, LLC
511 East Boulevard Charlotte, NC 28203
Subject: Limited Phase II Environmental Site Assessment 7th Street Apartments 705 E. 7th Street Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 4164.11
Dear Mr. Stewart:
SUMMIT ENGINEERING, LABRATORY & TESTING, INC. (SUMMIT) is pleased to submit the
following report of our Limited Phase II Environmental Site Assessment (ESA) of the 7th Street
Apartments property in Charlotte, Mecklenburg County, North Carolina (Mecklenburg County Tax IDs: 08010402 and portion of 08010408).
This report includes a description of the methodology of our investigation and a summary of our findings and conclusions. If you have any questions regarding our assessment of the subject property or our conclusions, please do not hesitate to call us at [phone].
Sincerely,
SUMMIT
Patrick W. Lowery, PG Michael D. Zavislak, NRCC-EAC, CIH, PE
Senior Environmental Manager Environmental Department Manager
NC LG No: 2421 SUMMIT’s NC Engineering Firm License No. C-2530

LIMITED PHASE II ENVIRONMENTAL SITE ASSESSMENT 7TH STREET APARTMENTS CHARLOTTE MECKLENBURG COUNTY
NORTH CAROLINA SUMMIT PROJECT NO. 4164.11
Prepared For: Laurel Street Residential, LLC 511 East Boulevard Charlotte, NC 28226
Prepared By: SUMMIT ENGINEERING, LABRATORY & TESTING, Inc. 3575 Centre Circle
Fort Mill, South Carolina 29715 704-504-1717
January 27, 2020
Limited Phase II ESA – 7th Street Apartments SUMMIT Project No. 4164.11
Charlotte, North Carolina January 27, 2020

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TABLE OF CONTENTS
1.0 EXECUTIVE SUMMARY ...................................................................................................... 1
2.0 INTRODUCTION .................................................................................................................... 3
2.1. PURPOSE .......................................................................................................................................... 3
2.2. SITE DESCRIPTION ........................................................................................................................ 3
2.3. ASSESSMENT HISTORY ................................................................................................................ 3
2.4. WORK PLAN OBJECTIVES ........................................................................................................... 4
3.0 PROPERTY SETTING ............................................................................................................. 5
3.1. TOPOGRAPHIC SETTING .............................................................................................................. 5
3.2. GEOLOGIC SETTING ..................................................................................................................... 5
3.3. HYDROLOGIC SETTING ............................................................................................................... 6
4.0 SUMMARY OF FIELD ACTIVITIES .................................................................................... 7
4.1. DRILLING ACTIVITES AND METHODS ..................................................................................... 7
4.2. SAMPLING ....................................................................................................................................... 8
4.3. PACKING AND SHIPMENT ........................................................................................................... 9
4.4. SAMPLING POINT ABANDONMENT.......................................................................................... 9
5.0 SUMMARY OF LABORATORY ANALYSIS ..................................................................... 10
6.0 DATA QUALITY.................................................................................................................... 11
6.1. QUALITY CONTROL SAMPLES ................................................................................................. 11
6.2. SENSITIVITY ................................................................................................................................. 11
6.3. LABORATORY DATA EVALUATION ......................................................................................... 11
7.0 FINDINGS & CONCLUSIONS ............................................................................................ 12
8.0 QUALIFICATION OF REPORT ........................................................................................... 14
9.0 ADDITIONAL SERVICES .................................................................................................... 15
10.0 REFERENCES ....................................................................................................................... 16

APPENDICES
Appendix I: FIGURES Appendix II: ANALYTICAL SUMMARY Appendix III: ANALYTICAL RESULTS Appendix IV: WELL RECORDS/PERMITS
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1.0 EXECUTIVE SUMMARY

SUMMIT Engineering, Laboratory and Testing, Inc. (SUMMIT) personnel conducted a Limited
Phase II ESA of the 7th Street Apartments property, based on environmental concerns identified
during the course of conducting a Phase I ESA for the property. Field work was completed by
SUMMIT on December 31, 2019.

In summary, four (4) soil and two (2) groundwater samples were collected from the subject site to
identify if concerns observed in the Phase I ESA have impacted the subject site. Soil samples were
analyzed for the presence of VOCs, SVOCs, RCRA Metals and Hexavalent Chromium. All
collected groundwater samples were analyzed for the presence of VOCs and SVOCs.

During the completion of the soil borings for this assessment, debris and fill soils were encountered
at various depths resulting in shallow refusal and boring off-sets. This material was encountered at
varying depths and consisted of construction materials (concrete, brick, asphalt) and loose fill. The
presence of these materials suggests that the property was infilled with uncontrolled fill and debris.

One (1) of the collected subsurface soil samples (SB-1) detected the presence of Benzo(a)pyrene
above the respective IHSB Preliminary Soil Remediation Goal (PSRG) for Residential/Unrestricted
Use soils. One (1) soil sample from SB-4 detected Hexavalent Chromium above the IHSB
Preliminary Soil Remediation Goal (PSRG) for Residential/Unrestricted Use soils. Additional low
concentration SVOCs and VOCs were reported in the soil analysis below IHSB PSRGs.

All of the collected subsurface soil samples detected the presence of Arsenic above the respective
IHSB PSRG for Residential/Unrestricted Use soils. While these concentrations are above the IHSB
PSRG reference values, SUMMIT considered the reported concentrations to be within observed
naturally occurring background levels.

SUMMIT attempted to collect four (4) groundwater samples from temporary wells installed for this
assessment. Two (2) temporary monitoring wells (TMW-1 & TMW-2) were dry following
installation and did not yield groundwater for this assessment. TMW-3 and TMW-4 were collected
and submitted to the lab for analysis. Detections of Naphthalene, Pyrene and 3+4-Methylphenol
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were reported at concentrations that do not exceed NCDEQ Groundwater Standards (15A NCAC
02L) reference values. No other groundwater detections were reported in the laboratory analysis.

SUMMIT concludes that subject sites subsurface soils of the property have been impacted with
SVOC compounds and Hexavalent Chromium above regulatory concentrations. A source of the
impacts is unknown at the time of this report.

SUMMIT further concludes that the groundwater beneath the site has not been significantly
impacted at the locations tested at the subject property.

Lastly, based on the field conditions indicating subsurface construction debris and fill soils,
SUMMIT concludes that the materials in place likely differ from location to location as the fill
material source is unknown.

Based the soil sampling results, impacts above unrestricted use are present in the subject property
soils. SUMMIT recommends that he perspective buyer of the property consult with legal counsel
and consider redevelopment of the property utilizing the North Carolina Brownfields Program.
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2.0 INTRODUCTION 2.1. PURPOSE SUMMIT was retained by Laurel Street Residential, LLC, to perform a Limited Phase II ESA of
the 7th Street Apartments property, located in Charlotte, Mecklenburg County, North Carolina
(Mecklenburg County Tax IDs: 08010402 and portion of 08010408). The Limited Phase II ESA
was requested in order to assess environmental concerns identified during the completion of a Phase
I ESA for the subject site. This report presents the results of our Limited Phase II ESA of the 7th
Street Apartments site.

2.2. SITE DESCRIPTION

The subject site is an irregular shaped tract of commercial land totaling 1.21 acres in area, located in
downtown Charlotte, North Carolina. Parcel 08010402 of the site consists of an open grassed field
with two (2) historical residential properties located in the southern portion of the parcel. These
historical structures are denoted by signage as “Shotgun homes” and appear to be associated with
the City of Charlotte and adjoining Cultural Center building to the south. The portion of parcel
08010408 making up the site is partially developed with an asphalt parking lot used by the adjoining
Cultural Center building and partially undeveloped and grassed open area. According to
Mecklenburg County, the following physical addresses are associated with the site; 705, 711, 715 E.
7th Street, 405 N. Alexander Street and 415 N. Myers Street.

Access to the subject site is from E. 7th Street, N. Myers, Street, Parkside Terrace Lane and N.
Alexander Street. The vicinity of the property can be generally described as urban residential.
Refer to the Site Location Map shown in Figure 2 of Appendix I for the location of the subject
property.
2.3. ASSESSMENT HISTORY
SUMMIT completed a Phase I ESA for the subject property, dated September 27, 2019. The
following environmental concerns were noted:

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• Historical use of the site included Jones Electric Repair, operating onsite for 20 years in a
large “L” shaped structure. Similar repair operations are known to have utilized petroleum
products or hazardous materials, representing a REC at the time of the Phase I ESA report.

• Environmental Database Records indicate multiple DRYCLEANERS listings in close
proximity to the subject property. The state database lists addresses with known drycleaning
sites, active and/or abandoned. These database listings represent a REC at the time of the
Phase I ESA report.

• Historical use of the surrounding area and adjoining properties include drycleaning and
furniture repair in close proximity to the subject property. These types of operations are
known to utilize petroleum product and hazardous materials, representing a REC at the time
of the Phase I ESA report.

No other site specific or surrounding area assessment history is known at the time of this report.

2.4. WORK PLAN OBJECTIVES

SUMMIT proposed to perform a Limited Phase II ESA according to our understanding of the most
likely potential for impact, in general accordance with ASTM E1903, and in accordance with the
USEPA Field Branches Quality System and Technical Procedures Manual. The proposed scope of
services included the installation and sampling of four (4) temporary monitoring wells in order to
assess the soil and groundwater quality adjacent to the debris area on the site. The proposed
sampling locations were placed in locations and in areas that may help identify migrating
contaminants from the areas of concern. All samples collected were scheduled to be relinquished to
a NC certified laboratory for analysis. Collected soil samples were submitted for of Volatile Organic
Compounds by EPA method 8260, Semi-Volatile Organic Compounds (SVOCs) by EPA method
8270, RCRA Metals by EPA method 6010 and Hexavalent Chromium by EPA method 7199.
Collected groundwater samples were submitted for of Volatile Organic Compounds by EPA method
8260 and Semi-Volatile Organic Compounds by EPA method 8270.

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3.0 PROPERTY SETTING

3.1. TOPOGRAPHIC SETTING

The United States Geological Survey (USGS) “Charlotte East” topographic quadrangle map was
reviewed for this report. According to the contour lines on the topographic maps, the elevation of
the subject property averages 690 feet above Mean Sea Level (MSL) with a slight slope to the
south. The contour lines indicate the general direction of downward slope is to the south. The
USGS maps a blue lined stream traversing north to south through the site, however this stream is
not present at the surface of this property. It is assumed that this stream has been culverted
beneath/besides the property. Refer to Figure 1 in Appendix I of this report.

3.2. GEOLOGIC SETTING

The property is located in Mecklenburg County, North Carolina, which is located in the south
central Piedmont Physiographic Province. The Piedmont Province generally consists of well-
rounded hills and ridges which are dissected by a well-developed system of draws and streams. The
Piedmont Province is predominantly underlain by metamorphic rock (formed by heat, pressure
and/or chemical action) and igneous rock (formed directly from molten material) which were
initially formed during the Precambrian and Paleozoic eras. The volcanic and sedimentary rocks
deposited in the Piedmont Province during the Precambrian era were the host from the
metamorphism and were changed to gneiss and schist. The more recent Paleozoic era had periods
of igneous emplacement, with at least episodes of regional metamorphism resulting in the majority
of the rock types seen today.

The topography and relief of the Piedmont Province has developed from differential weathering of
the igneous and metamorphic rock. Ridges and hills have been developed on the more easily
weathered and erodible rock. Because of the continued chemical and physical weathering, the rocks
in the Piedmont Province are now generally covered with a mantle of soil that has weathered in
place from the parent bedrock. These soils vary in thickness and are referred to as residuum or
residual soils. The residuum is typically finer grained and has higher clay content near the surface
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because of the advanced weathering. Similarly, the soils typically become coarser grained with
increasing depth because of decreased weathering. As the weathering decreases, the residual soils
generally retain the overall appearance, texture, gradation and foliations of the parent rock.

3.3. HYDROLOGIC SETTING

Based on a review of the United States Geological Survey (USGS) “Charlotte East” quadrangle
topographic map, the inferred groundwater flow direction based on topography appears to be to the
south towards Sugar Creek. Refer to Figure 1 in Appendix I for a topographic map for the subject
property.
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4.0 SUMMARY OF FIELD ACTIVITIES

4.1. DRILLING ACTIVITES AND METHODS

On December 30, 2019, SUMMIT personnel conducted the temporary monitoring well installation
scope of the Limited Phase II ESA. The proposed temporary monitoring well (TMW) locations
were placed in locations and in areas that may help identify migrating contaminants from the site or
off-site properties. The locations of the TMW locations can be viewed on the attached Sampling
Location Map, Figure 3, in appendix I.

SUMMIT utilized a GeoProbe direct push drill rig to complete the soil borings and TMW
installation. At each location, a boring was attempted to be advanced to 20 feet below ground
surface (bgs). MacroCore samplers were utilized for the collection of soil samples from the upper
20 feet of each boring for field screening purposes and soil sample collection. At termination
depths, the TMWs were constructed and placed in the resulting borehole. All borings encountered
refusal prior to reaching the planned 20 feet depths. SB-1/TMW-1 encountered refusal at 10 feet
bgs on suspected debris material. SB-2/TMW-2 encountered refusal at 7’ bgs on suspected debris
material. SB-3/TMW-3 encountered refusal at 8’ bgs on suspected debris material. SB-4/TMW-4
encountered refusal at 15’ bgs on suspected debris material. The TMWs consisted of 1-inch
Schedule 20 PVC 0.01-inch slotted well screen. The well screens were encased in #3 filter sand
from the base of the boring to approximately 2 feet above the well screen.

Each boring typically encountered fill soils and debris material consisting of concrete, brick, asphalt
or gravel. Low soil recovery was noted in all borings at varying depths. The materials encountered
suggests that the property has been infilled with non-native fill and debris.

Groundwater was only encountered in all TMW-3 and TMW-4. Approximate depth to water
(DTW) ranged from 6 ft bgs to 8 ft bgs in the TMWs after installation. New disposable tubing and
peristaltic pump was utilized to purge each temporary following installation. At each location,
three (3) well volumes were purged prior to sample collection.

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Upon completion of the drilling activities, the drilling equipment was decontaminated by the well
driller by use of a steam cleaner or Alconox and tap water wash, tap water rinse, isopropanol rinse
(sampling equipment), and deionized water rinse. Decontamination of the drilling equipment was
performed prior to starting drilling activities, and upon the completion of drilling activities at each
boring/well location.

4.2. SAMPLING
Soil:
Soil samples were collected based on field screening results obtained utilizing a calibrated photo-
ionizing detector (PID). If field screening results were inconclusive, the 0-2 ft soil interval was
selected for analysis. Field screening indicated detectible VOCs at in SB-1 at 0-2 ft interval, SB-2
at 4-8 ft interval, SB-3 at 2-4 ft interval and SB-4 at 2-4 ft interval. Soil samples collected from the
temporary well locations were submitted for the analysis of Volatile Organic Compounds by EPA
method 8260, Semi-Volatile Organic Compounds (SVOCs) by EPA method 8270, RCRA Metals by
EPA method 6010 and Hexavalent Chromium by EPA method 7199

Groundwater:
Groundwater was sampled form the installed TMWs on December 31, 2019. Following installation
the TMWs were attempted to be purged of approximately 3 well volumes. Water elevations were
measured following installation and prior to sampling. The depth to water measurements are
provided below:

Well ID Depth to Water (bgs)
TMW-1 DRY
TMW-2 DRY
TMW-3 8’
TMW-4 6’
All measurements are represented in Feet
Based on the field data it appears that groundwater flow in the assessment area is to the south.

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On December 31st, samples were collected utilizing new disposable tubing and peristaltic low flow
pump. Groundwater samples were containerized in laboratory provided vials and containers, placed
on ice and transported to the laboratory for analysis. All groundwater samples were analyzed for
Volatile Organic Compounds by EPA method 8260 and Semi-Volatile Organic Compounds by EPA
method 8270.

4.3. PACKING AND SHIPMENT
Upon securing the samples in laboratory provided containers, the vial and jar lids were tightly
fastened, and the jars encapsulated in shock-resistant plastic bags. The samples and ice were
double-bagged in large plastic bags, tied off with rubber bands, and packed into a cooler. The
samples were delivered to Shealy Environmental Services, Inc, in West Columbia, SC. The vials
and jars used for the collection of the samples at this site were prepared by Shealy, and were pre-
labeled and contained analyte-appropriate preservatives. A listing of the preservatives in the sample
containers utilized for the collection of the samples at this site are cataloged in the Chain-Of-
Custody record, attached in Appendix III of this report. The secured samples were relinquished to
laboratory on December 31, 2019 for laboratory analysis.

4.4. SAMPLING POINT ABANDONMENT

All boreholes were abandoned on December 31, 2019 by a NC Well Driller. Copies of the
abandonment records are included in Appendix IV of this report.
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5.0 SUMMARY OF LABORATORY ANALYSIS

All samples were relinquished to Shealy Environmental Services on December 31, 2019 for the
prescribe analysis. Table’s 1 and 2 in Appendix II of this report summarizes all detections. The
analytical detections are summarized below:

• Trichloroethene detections were reported in the soil samples collected from SB-3 & SB-4.
Reported concentrations of 0.0019 mg/kg and 0.002 mg/kg were below the established
IHSB PSRGs for Unrestricted Use. No other VOC constituents were reported in the soil
analysis.

• Soil samples collected reported the detections of multiple SVOCs. Benzo(a)pyrene was
reported at a concentration of 0.14 mg/kg, exceeding established IHSB PSRGs for
Unrestricted Use in soils collected from SB-1 (0-2’). The remaining SVOC detections were
reported below the regulatory concentrations.

• Hexavalent Chromium was detected above the established residential IHSB PSRGs at 0.35
mg/kg in soil collected from boring SB-4.

• Soil samples SB-1, SB-2, SB-3 and SB-4 reported detections of Arsenic at concentrations
exceeding the established IHSB PSRGS for Unrestricted Use (0.68 mg/kg) but below the
Protection of Groundwater screening levels (5.8mg/kg). The concentrations reported are
considered to likely be a result of naturally occurring concentrations at the site.

• Groundwater samples submitted from TMW-3 and TMW-4 reported low concentrations of
SVOC compounds (naphthalene, pyrene & 3+4-Methylphenol). The reported detections did
not exceed the established North Carolina Groundwater Standards (NC 2L).

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6.0 DATA QUALITY

6.1. QUALITY CONTROL SAMPLES
No Quality Control Samples were collected during the completion of this Phase II ESA.

6.2. SENSITIVITY
Laboratory RDLs and method detection limits (MDLs) were sufficient to report concentrations
below regulatory standards for the majority of analytes.

6.3. LABORATORY DATA EVALUATION

The laboratory completed validation and verification of laboratory processes and data, and delivered
a laboratory report to SUMMIT. The laboratory report and the QC information provide
documentation of compliance with the industry standards.

In reviewing the laboratory results, several analytes are reported as detections with “J” data
qualifiers, indicating the reported value is an estimate reported within the 95% confidence interval.
These compounds were detected above the MDL, but below the RDL. The MDL is the lowest
concentration at which an analyte can be detected in a sample by the particular laboratory method
used. “Detected” indicates that the analyte can be distinguished from the blank with reasonable
certainty. The RDL (also called practical quantitation limit, or PQL) is approximately five times the
MDL or the lower calibration standard, whichever is higher. Results above the report limit can be
distinguished from the blank and fall within applicable standard curves. For the purposes of this
assessment, all “J” qualified data are considered acceptable for making site management decisions.

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7.0 FINDINGS & CONCLUSIONS

In summary, four (4) soil and two (2) groundwater samples were collected from the subject site to
identify if concerns observed in the Phase I ESA have impacted the subject site. Soil samples were
analyzed for the presence of VOCs, SVOCs, RCRA Metals and Hexavalent Chromium. All
collected groundwater samples were analyzed for the presence of VOCs and SVOCs.

During the completion of the soil borings for this assessment, debris and fill soils were encountered
at various depths resulting in shallow refusal and boring off-sets. This material was encountered at
varying depths and consisted of construction materials (concrete, brick, asphalt) and loose fill. The
presence of there materials suggests that the property was infilled with uncontrolled fill and debris.

One (1) of the collected subsurface soil samples (SB-1) detected the presence of Benzo(a)pyrene
above the respective IHSB Preliminary Soil Remediation Goal (PSRG) for Residential/Unrestricted
Use soils. One (1) soil sample from SB-4 detected Hexavalent Chromium above the IHSB
Preliminary Soil Remediation Goal (PSRG) for Residential/Unrestricted Use soils. Additional low
concentration SVOCs and VOCs were reported in the soil analysis below IHSB PSRGs.

All of the collected subsurface soil samples detected the presence of Arsenic above the respective
IHSB PSRG for Residential/Unrestricted Use soils. While these concentrations are above the IHSB
PSRG reference values, SUMMIT considered the reported concentrations to be within observed
naturally occurring background levels.

Low concentration SVOC compounds were detected in the two (2) collected groundwater samples
(TMW-3 & TMW-4). Naphthalene, pyrene and 3+4-Mthylnaphthlene were detected at
concentrations below NCDEQ Groundwater Standards (15A NCAC 02L) reference values. No
other groundwater detections were reported.

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SUMMIT concludes that subject sites subsurface soils of the property have been impacted with
SVOC compounds and Hexavalent Chromium above regulatory concentrations. A source of the
impacts is unknown at the time of this report.

SUMMIT further concludes that the groundwater beneath the site has not been significantly
impacted at the locations tested at the subject property.

Lastly, based on the field conditions indicating subsurface construction debris and fill soils,
SUMMIT concludes that the materials in place likely differ from location to location as the fill
material source is unknown.

Based the soil sampling results, impacts above unrestricted use are present in the subject property
soils. SUMMIT recommends that he perspective buyer of the property consult with legal counsel
and consider redevelopment of the property utilizing the North Carolina Brownfields Program.
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8.0 QUALIFICATION OF REPORT

The Limited Phase II ESA was performed in general accordance with the approved assessment
work plan, the Inactive Hazardous Sites Branch Guidelines for Assessment and Cleanup (October
2015 edition) and EPA Region IV SESD Field Branches Quality System and Technical Procedures.
The findings detailed in this report are specific to the conditions in the immediate vicinity of the
sample locations for this particular project.

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9.0 ADDITIONAL SERVICES

This report does not include any environmental assessment of surface water, the determination of
wetlands, the determination of noise impact, the assessment of air quality, the identification of
cultural resources, or the identification of endangered species. These services are beyond the scope
of services of this limited sampling and analysis.

No additional services were provided.
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10.0 REFERENCES
United States Geological Survey (USGS) 7.5 minute Topographic Map of the Charlotte East Topographic Quadrangle, 2002.
EPA National Primary Drinking Water Regulations -
http://water.epa.gov/drink/contaminants/index.cfm 15A NCAC 2L Standards – http://portal.ncdenr.org/web/wq/ps/csu/gwstandards
North Carolina Inactive Hazardous Site Branch, Preliminary Remediation Goals Table HTTPS://NCDENR.S3.AMAZONAWS.COM/S3FS-PUBLIC/WASTE%20MANAGEMENT/DWM/SF/IHS/GUIDANCE/SOILTABLE%20APRIL%202016%20-FINAL-1PCB1.PDF

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APPENDIX I
FIGURES
Not to Scale
Image Provided By EDR USGS Topographic Maps
Boundaries are approximate
Figure 1
Prepared For:
7TH STREET APARTMENTS Topographic Map705 E 7th Street 11/19/2019Charlotte, North Carolina 28202 Drawn By:
Not to Scale
Image Provided By ESRI Street Map
Boundaries are approximate
Figure 2
Prepared For:
7TH STREET APARTMENTS Site Location Map705 E 7th Street 11/19/2019Charlotte, North Carolina 28202 Drawn By:
Source: Drawn by SUMMITPrepared By\Date: PL/11/19Checked By\Date: MZ/11/19ScaleFigure 1NTSGroundwater Sampling Plan7th Street ApartmentsLaurel Street Residential7th Street511 East BoulevardCharlotte, NC Charlotte, NC 28203NKEYTemporary Monitoring WellSoil Boring Location
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C:\plowery\Documents\2-Projects\4164.11 7th Street Apartments - Phase I Wetlands\Phase II ESA\Appendix II.rtf

APPENDIX II
ANALYTICAL SUMMARY

Page 1 of 2
CAS Metals PSRG-Res
Protection
of GW
79-01-6 Trichloroethene 8.70E-01 2.10E-02 BRL 0.0057 BRL 0.0058 0.0019 J 0.0046 0.002 J 0.005
CAS SVOC Analyte PSRG-Res
Protection
of GW Result RL Result RL Result RL Result RL
83-32-9 Acenaphthene 7.20E+02 1.60E+01 0.02 J 0.032 BRL 0.0029 BRL 0.063 BRL 0.063
120-12-7 Anthracene 3.60E+03 1.30E+03 0.043 0.032 BRL 0.0029 BRL 0.063 BRL 0.063
56-55-3 Benzo(a)anthracene 1.10E+00 3.50E-01 0.15 0.032 BRL 0.0029 0.086 0.063 0.074 0.063
50-32-8 Benzo(a)pyrene 1.10E-01 1.20E-01 0.14 0.032 BRL 0.0029 0.1 0.063 0.079 0.063205-99-2 Benzo(b)fluoranthene 1.10E+00 1.20E+00 0.2 0.032 BRL 0.0029 0.14 0.063 0.11 0.063191-24-2 Benzo(g,h,i)perylene NA 1.56E+04 0.063 0.032 BRL 0.0029 0.043 J 0.063 0.06 J 0.063
207-08-9 Benzo(k)fluoranthene 1.10E+01 1.20E+01 0.071 0.032 BRL 0.0029 0.041 J 0.063 0.042 J 0.063
218-01-9 Chrysene 1.10E+02 3.60E+01 0.17 0.032 BRL 0.0029 0.067 0.063 0.056 J 0.063
84-74-2 Di-n-butyl phthalate 1.30E+03 3.50E+01 BRL 0.15 0.0073 J 0.014 BRL 0.31 BRL 0.3
206-44-0 Fluoranthene 4.80E+02 6.70E+02 0.36 0.032 BRL 0.0029 0.15 0.063 0.092 0.063
193-39-5 lndeno(1,2,3-c,d)pyrene 1.10E+00 3.90E+00 0.057 0.032 BRL 0.0029 0.042 J 0.063 0.045 J 0.063
91-57-6 2-Methylnaphthalene 4.80E+01 3.10E+00 BRL 0.032 BRL 0.0029 0.034 J 0.063 BRL 0.063
91-20-3 Naphthalene 4.10E+00 3.90E-01 BRL 0.032 BRL 0.0029 0.033 J 0.063 BRL 0.063
85-01-8 Phenanthrene NA 1.34E+02 0.5 0.032 BRL 0.0029 0.086 0.063 0.059 J 0.063
129-00-0 Pyrene 3.60E+02 4.40E+02 0.26 0.032 BRL 0.0029 0.11 0.063 0.081 0.063
CAS Metals PSRG-Res
Protection
of GW
7440-38-2 Arsenic 6.80E-01 5.80E+00 3.8 1.7 1.9 0.81 3.8 1.6 8 1.6
7440-39-3 Barium 3.10E+03 5.80E+02 130 1.5 44 1.4 130 1.4 100 1.4
16065-83-1 Chromium (III)*2.30E+04 3.60E+05 43 0.043 23 0.54 42 0.55 54 0.55
18540-29-9 Chromium (VI)3.10E-01 3.80E+00 BRL 1.2 BRL 1.1 BRL 1.2 0.35 J 1.2
7439-92-1 Lead NA 2.70E+02 31 1.1 7.9 1.6 55 1.1 45 1.1
7439-97-6 Mercury 2.30E+00 1.00E+00 0.081 J 0.096 BRL 0.09 0.067 J 0.093 0.089 J 0.096
BRL = Below Reporting Limit J = Estimated Concentration RL = Lab Reporting LimitBOLD = Concentration Above Reference Values NT = Not Tested
*-Chromium (III) determined by speciation from Total Chromium and Chromium (VI)
Table 1: Soil Sample Detection Summary Table
DEQ Reference Values SB-1 SB-2 SB-3 SB-4
All Values in mg/kg 0-2' bgs
12/31/2019 12/31/2019 12/31/2019 12/31/2019
4-8' bgs 2-4' bg 2-4' bgs
7th Street Apartments
Charlotte, NC
January 27, 2020
SUMMIT Project No: 4164.11
Page 2 of 2
CAS VOCs
All VOCs
CAS SVOC Analyte Result RL Result RL Result RL Result RL
91-20-3 Naphthalene 0.041 J 0.16 BRL 0.16
129-00-0 Pyrene 0.049 J 0.16 BRL 0.16
106-44-5 3+4-Methylphenol BRL 1.6 1.9 1.6
BRL = Below Reporting Limit J = Estimated Concentration RL = Lab Reporting LimitBOLD = Concentration Above Reference Values NT = Not Tested*-Chromium (III) determined by speciation from Total Chromium and Chromium (VI)
NC 2L Groundwater
Standards
6.00E+00
2.00E+02
4.40E+02
NT
NT
NT
NT NT
NT
NT
BRL
DTW 6'
NT
BRL
12/31/2019 12/31/2019 12/31/2019 12/31/2019
Table 2:Groundwater Sample Detection Summary Table
DEQ Reference Values GW-1 GW-2 GW-3 GW-4
All Values in mg/kg DRY at 10'DRY at 7'DTW 8'
7th Street Apartments
Charlotte, NC
January 27, 2020
SUMMIT Project No: 4164.11
Limited Phase II ESA – 7th Street Apartments SUMMIT Project No. 4164.11 Charlotte, North Carolina January 27, 2020

C:\plowery\Documents\2-Projects\4164.11 7th Street Apartments - Phase I Wetlands\Phase II ESA\Appendix III.rtf

APPENDIX III
ANALYTICAL RESULTS

SHEALY ENVIRONMENTAL SERVICES,INC.
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Report of Analysis
SUMMIT Engineering,Laboratory &Testing,P.C.
3575 Centre Circle
Fort Mill,SC 28715
Attention:Patrick Lowery
Project Name:7th St.Apartments
Project Number:4164.11
Lot Number:UL31060
Date Completed:01/07/2020
01/07/2020 4:23 PM
Approved and released by:
Lab Director -Greenville:Lucas Odom
Page 1 of 73
SHEALY ENVIRONMENTAL SERVICES,INC.
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Case Narrative
SUMMIT Engineering,Laboratory &Testing,P.C.
Lot Number:UL31060
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved NELAC standards,the Shealy Environmental Services,Inc.("Shealy")Quality
Assurance Management Plan (QAMP),standard operating procedures (SOPs),and Shealy policies.Any
exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the results page or
discussed below.
Where applicable,all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
RCRA Metals
The following samples were diluted due to the nature of the sample matrix:UL31060-001,UL31060-003,
UL31060-004.The LOQ has been elevated to reflect the dilution.
VOCs by GC/MS
The continuing calibration verification (CCV)associated with samples UL31060-001,UL31060-002,
UL31060-003,UL31060-004 recovered Dichlorodifluoromethane above the upper control limit.The
samples associated with this CCV are non-detect for the affected analytes;therefore,the data has been
reported.
SVOCs by GC/MS
Surrogate recovery for the following sample was outside of acceptance limits:UL31060-006.There was
insufficient sample to perform a re-extraction;therefore,the data has been reported.
Due to the large number of spiked analytes,there is a high probability that one or more analytes will
recover outside acceptance limits.The laboratory's SOP allows for 10%of analytes to recover marginally
outside criteria.The following analytes recovered marginally outside LCS criteria:4-Chloroaniline.
Page 2 of 73
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: UL31060

Sample Number Sample ID Matrix Date Sampled Date Received
001 12/31/2019 1050SB-1 Solid 12/31/2019
002 12/31/2019 1100SB-2 Solid 12/31/2019
003 12/31/2019 1115SB-3 Solid 12/31/2019
004 12/31/2019 1130SB-4 Solid 12/31/2019
005 12/31/2019 1110GW-3 Aqueous 12/31/2019
006 12/31/2019 1050GW-4 Aqueous 12/31/2019
(6 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 3 of 73
SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: UL31060

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SB-1 Solid Acenaphthene 8270E 20 J ug/kg 8
001 SB-1 Solid Anthracene 8270E 43 ug/kg 8
001 SB-1 Solid Benzo(a)anthracene 8270E 150 ug/kg 8
001 SB-1 Solid Benzo(a)pyrene 8270E 140 ug/kg 8
001 SB-1 Solid Benzo(b)fluoranthene 8270E 200 ug/kg 8
001 SB-1 Solid Benzo(g,h,i)perylene 8270E 63 ug/kg 8
001 SB-1 Solid Benzo(k)fluoranthene 8270E 71 ug/kg 8
001 SB-1 Solid Chrysene 8270E 170 ug/kg 9
001 SB-1 Solid Fluoranthene 8270E 360 ug/kg 9
001 SB-1 Solid Indeno(1,2,3-c,d)pyrene 8270E 57 ug/kg 9
001 SB-1 Solid Phenanthrene 8270E 200 ug/kg 10
001 SB-1 Solid Pyrene 8270E 260 ug/kg 10
001 SB-1 Solid Arsenic 6010D 3.8 mg/kg 10
001 SB-1 Solid Barium 6010D 130 mg/kg 10
001 SB-1 Solid Chromium 6010D 43 mg/kg 10
001 SB-1 Solid Lead 6010D 31 mg/kg 10
001 SB-1 Solid Mercury 7471B 0.081 J mg/kg 10
002 SB-2 Solid Di-n-butyl phthalate 8270E 7.3 J ug/kg 13
002 SB-2 Solid Arsenic 6010D 1.9 mg/kg 14
002 SB-2 Solid Barium 6010D 44 mg/kg 14
002 SB-2 Solid Chromium 6010D 23 mg/kg 14
002 SB-2 Solid Lead 6010D 7.9 mg/kg 14
003 SB-3 Solid Trichloroethene 8260D 1.9 J ug/kg 16
003 SB-3 Solid Benzo(a)anthracene 8270E 86 ug/kg 16
003 SB-3 Solid Benzo(a)pyrene 8270E 100 ug/kg 16
003 SB-3 Solid Benzo(b)fluoranthene 8270E 140 ug/kg 16
003 SB-3 Solid Benzo(g,h,i)perylene 8270E 43 J ug/kg 16
003 SB-3 Solid Benzo(k)fluoranthene 8270E 41 J ug/kg 16
003 SB-3 Solid Chrysene 8270E 67 ug/kg 17
003 SB-3 Solid Fluoranthene 8270E 150 ug/kg 17
003 SB-3 Solid Indeno(1,2,3-c,d)pyrene 8270E 42 J ug/kg 17
003 SB-3 Solid 2-Methylnaphthalene 8270E 34 J ug/kg 17
003 SB-3 Solid Naphthalene 8270E 33 J ug/kg 17
003 SB-3 Solid Phenanthrene 8270E 86 ug/kg 18
003 SB-3 Solid Pyrene 8270E 110 ug/kg 18
003 SB-3 Solid Arsenic 6010D 3.8 mg/kg 18
003 SB-3 Solid Barium 6010D 130 mg/kg 18
003 SB-3 Solid Chromium 6010D 42 mg/kg 18
003 SB-3 Solid Lead 6010D 55 mg/kg 18
003 SB-3 Solid Mercury 7471B 0.067 J mg/kg 18
004 SB-4 Solid Hexavalent Chromium 7199 0.35 J mg/kg 19
004 SB-4 Solid Trichloroethene 8260D 2.0 J ug/kg 20
004 SB-4 Solid Benzo(a)anthracene 8270E 74 ug/kg 20
004 SB-4 Solid Benzo(a)pyrene 8270E 79 ug/kg 20
004 SB-4 Solid Benzo(b)fluoranthene 8270E 110 ug/kg 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 4 of 73
Detection Summary (Continued)
Lot Number: UL31060
Sample Sample ID Matrix Parameter Method Result Q Units Page
004 SB-4 Solid Benzo(g,h,i)perylene 8270E 60 J ug/kg 20
004 SB-4 Solid Benzo(k)fluoranthene 8270E 42 J ug/kg 20
004 SB-4 Solid Chrysene 8270E 56 J ug/kg 21
004 SB-4 Solid Fluoranthene 8270E 92 ug/kg 21
004 SB-4 Solid Indeno(1,2,3-c,d)pyrene 8270E 45 J ug/kg 21
004 SB-4 Solid Phenanthrene 8270E 59 J ug/kg 22
004 SB-4 Solid Pyrene 8270E 81 ug/kg 22
004 SB-4 Solid Arsenic 6010D 8.0 mg/kg 22
004 SB-4 Solid Barium 6010D 100 mg/kg 22
004 SB-4 Solid Chromium 6010D 54 mg/kg 22
004 SB-4 Solid Lead 6010D 45 mg/kg 22
004 SB-4 Solid Mercury 7471B 0.089 J mg/kg 22
005 GW-3 Aqueous Naphthalene 8270E 0.041 J ug/L 25
005 GW-3 Aqueous Pyrene 8270E 0.049 J ug/L 26
006 GW-4 Aqueous 3+4-Methylphenol 8270E 1.9 ug/L 29
(60 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 5 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1
UL31060-001
12/31/2019 1050
12/31/2019
Solid
% Solids:85.0 01/02/2020 2024
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 01/04/2020 1847 HKL 01/02/2020 1447 40691
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.241.2
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 01/02/2020 1201 JM1 40716 5.20
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/kg9.023
Benzene 71-43-2 8260D ND 1ug/kg2.35.7
Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.35.7
Bromoform 75-25-2 8260D ND 1ug/kg2.35.7
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.45.7
2-Butanone (MEK)78-93-3 8260D ND 1ug/kg4.523
Carbon disulfide 75-15-0 8260D ND 1ug/kg2.35.7
Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.35.7
Chlorobenzene 108-90-7 8260D ND 1ug/kg2.35.7
Chloroethane 75-00-3 8260D ND 1ug/kg2.35.7
Chloroform 67-66-3 8260D ND 1ug/kg2.35.7
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.45.7
Cyclohexane 110-82-7 8260D ND 1ug/kg2.35.7
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.35.7
Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.35.7
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.35.7
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.35.7
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.35.7
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.35.7
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.45.7
1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.35.7
1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.35.7
1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.35.7
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.35.7
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.35.7
1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.35.7
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.35.7
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.35.7
Ethylbenzene 100-41-4 8260D ND 1ug/kg2.35.7
2-Hexanone 591-78-6 8260D ND 1ug/kg4.511
Isopropylbenzene 98-82-8 8260D ND 1ug/kg2.35.7
Methyl acetate 79-20-9 8260D ND 1ug/kg2.35.7
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 6 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1
UL31060-001
12/31/2019 1050
12/31/2019
Solid
% Solids:85.0 01/02/2020 2024
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 01/02/2020 1201 JM1 40716 5.20
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.35.7
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.511
Methylcyclohexane 108-87-2 8260D ND 1ug/kg2.35.7
Methylene chloride 75-09-2 8260D ND 1ug/kg2.35.7
Styrene 100-42-5 8260D ND 1ug/kg2.35.7
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.35.7
Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.35.7
Toluene 108-88-3 8260D ND 1ug/kg2.35.7
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.35.7
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.35.7
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.35.7
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.35.7
Trichloroethene 79-01-6 8260D ND 1ug/kg2.35.7
Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.35.7
Vinyl chloride 75-01-4 8260D ND 1ug/kg3.45.7
Xylenes (total)1330-20-7 8260D ND 1ug/kg4.511
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 95 47-138
1,2-Dichloroethane-d4 89 53-142
Toluene-d8 109 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 10 01/06/2020 2038 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E 20 J 1ug/kg9.732
Acenaphthylene 208-96-8 8270E ND 1ug/kg1132
Acetophenone 98-86-2 8270E ND 1ug/kg58150
Anthracene 120-12-7 8270E 43 1ug/kg6.032
Atrazine 1912-24-9 8270E ND 1ug/kg58150
Benzaldehyde 100-52-7 8270E ND 1ug/kg58150
Benzo(a)anthracene 56-55-3 8270E 150 1ug/kg6.932
Benzo(a)pyrene 50-32-8 8270E 140 1ug/kg7.732
Benzo(b)fluoranthene 205-99-2 8270E 200 1ug/kg5.832
Benzo(g,h,i)perylene 191-24-2 8270E 63 1ug/kg7.632
Benzo(k)fluoranthene 207-08-9 8270E 71 1ug/kg5.632
1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg58150
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 7 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1
UL31060-001
12/31/2019 1050
12/31/2019
Solid
% Solids:85.0 01/02/2020 2024
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 10 01/06/2020 2038 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg58150
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg58150
Caprolactam 105-60-2 8270E ND 1ug/kg58150
Carbazole 86-74-8 8270E ND 1ug/kg58150
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg58150
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg58150
4-Chloroaniline 106-47-8 8270E ND 1ug/kg58150
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg58150
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg58150
2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg58150
2-Chlorophenol 95-57-8 8270E ND 1ug/kg58150
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg58150
Chrysene 218-01-9 8270E 170 1ug/kg5.332
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg6.032
Dibenzofuran 132-64-9 8270E ND 1ug/kg58150
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg58150
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg58150
Diethylphthalate 84-66-2 8270E ND 1ug/kg58150
Dimethyl phthalate 131-11-3 8270E ND 1ug/kg86150
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg58150
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg58150
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg290780
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg290780
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg120320
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg120320
Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg58150
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg290780
Fluoranthene 206-44-0 8270E 360 1ug/kg4.932
Fluorene 86-73-7 8270E ND 1ug/kg6.732
Hexachlorobenzene 118-74-1 8270E ND 1ug/kg58150
Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg58150
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg290780
Hexachloroethane 67-72-1 8270E ND 1ug/kg58150
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E 57 1ug/kg1232
Isophorone 78-59-1 8270E ND 1ug/kg58150
2-Methylnaphthalene 91-57-6 8270E ND 1ug/kg1232
2-Methylphenol 95-48-7 8270E ND 1ug/kg58150
3+4-Methylphenol 106-44-5 8270E ND 1ug/kg120320
Naphthalene 91-20-3 8270E ND 1ug/kg1132
2-Nitroaniline 88-74-4 8270E ND 1ug/kg120320
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 8 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1
UL31060-001
12/31/2019 1050
12/31/2019
Solid
% Solids:85.0 01/02/2020 2024
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 10 01/06/2020 2038 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3-Nitroaniline 99-09-2 8270E ND 1ug/kg120320
4-Nitroaniline 100-01-6 8270E ND 1ug/kg120320
Nitrobenzene 98-95-3 8270E ND 1ug/kg58150
2-Nitrophenol 88-75-5 8270E ND 1ug/kg120320
4-Nitrophenol 100-02-7 8270E ND 1ug/kg290780
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg58150
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg58150
Pentachlorophenol 87-86-5 8270E ND 1ug/kg290780
Phenanthrene 85-01-8 8270E 200 1ug/kg8.432
Phenol 108-95-2 8270E ND 1ug/kg58150
Pyrene 129-00-0 8270E 260 1ug/kg5.832
Pyridine 110-86-1 8270E ND 1ug/kg58150
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg58150
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg58150
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 51 33-102
2-Fluorophenol 65 35-115
Nitrobenzene-d5 58 22-109
Phenol-d5 61 33-122
Terphenyl-d14 56 41-120
2,4,6-Tribromophenol 61 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/06/2020 0608 LLL 01/05/2020 1437 40813
1 7471B 7471B 1 01/04/2020 1057 KSH2 01/03/2020 1317 40814
2 3050B 6010D 2 01/06/2020 0805 LLL 01/05/2020 1437 40813
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010D 3.8 2mg/kg0.561.7
Barium 7440-39-3 6010D 130 1mg/kg0.361.5
Cadmium 7440-43-9 6010D ND 2mg/kg0.140.56
Chromium 7440-47-3 6010D 43 1mg/kg0.140.56
Lead 7439-92-1 6010D 31 2mg/kg0.501.1
Mercury 7439-97-6 7471B 0.081 J 1mg/kg0.0230.096
Selenium 7782-49-2 6010D ND 2mg/kg0.912.2
Silver 7440-22-4 6010D ND 1mg/kg0.140.56
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 9 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-2
UL31060-002
12/31/2019 1100
12/31/2019
Solid
% Solids:90.9 01/02/2020 2024
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 01/04/2020 1900 HKL 01/02/2020 1447 40691
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.221.1
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 01/02/2020 1224 JM1 40716 4.72
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/kg9.323
Benzene 71-43-2 8260D ND 1ug/kg2.35.8
Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.35.8
Bromoform 75-25-2 8260D ND 1ug/kg2.35.8
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.55.8
2-Butanone (MEK)78-93-3 8260D ND 1ug/kg4.723
Carbon disulfide 75-15-0 8260D ND 1ug/kg2.35.8
Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.35.8
Chlorobenzene 108-90-7 8260D ND 1ug/kg2.35.8
Chloroethane 75-00-3 8260D ND 1ug/kg2.35.8
Chloroform 67-66-3 8260D ND 1ug/kg2.35.8
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.55.8
Cyclohexane 110-82-7 8260D ND 1ug/kg2.35.8
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.35.8
Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.35.8
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.35.8
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.35.8
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.35.8
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.35.8
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.55.8
1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.35.8
1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.35.8
1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.35.8
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.35.8
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.35.8
1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.35.8
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.35.8
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.35.8
Ethylbenzene 100-41-4 8260D ND 1ug/kg2.35.8
2-Hexanone 591-78-6 8260D ND 1ug/kg4.712
Isopropylbenzene 98-82-8 8260D ND 1ug/kg2.35.8
Methyl acetate 79-20-9 8260D ND 1ug/kg2.35.8
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 10 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-2
UL31060-002
12/31/2019 1100
12/31/2019
Solid
% Solids:90.9 01/02/2020 2024
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 01/02/2020 1224 JM1 40716 4.72
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.35.8
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.712
Methylcyclohexane 108-87-2 8260D ND 1ug/kg2.35.8
Methylene chloride 75-09-2 8260D ND 1ug/kg2.35.8
Styrene 100-42-5 8260D ND 1ug/kg2.35.8
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.35.8
Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.35.8
Toluene 108-88-3 8260D ND 1ug/kg2.35.8
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.35.8
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.35.8
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.35.8
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.35.8
Trichloroethene 79-01-6 8260D ND 1ug/kg2.35.8
Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.35.8
Vinyl chloride 75-01-4 8260D ND 1ug/kg3.55.8
Xylenes (total)1330-20-7 8260D ND 1ug/kg4.712
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 102 47-138
1,2-Dichloroethane-d4 88 53-142
Toluene-d8 101 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 01/06/2020 2103 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E ND 1ug/kg0.902.9
Acenaphthylene 208-96-8 8270E ND 1ug/kg1.02.9
Acetophenone 98-86-2 8270E ND 1ug/kg5.414
Anthracene 120-12-7 8270E ND 1ug/kg0.552.9
Atrazine 1912-24-9 8270E ND 1ug/kg5.414
Benzaldehyde 100-52-7 8270E ND 1ug/kg5.414
Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg0.642.9
Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg0.712.9
Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg0.542.9
Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg0.702.9
Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg0.522.9
1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg5.414
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 11 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-2
UL31060-002
12/31/2019 1100
12/31/2019
Solid
% Solids:90.9 01/02/2020 2024
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 01/06/2020 2103 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg5.414
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg5.414
Caprolactam 105-60-2 8270E ND 1ug/kg5.414
Carbazole 86-74-8 8270E ND 1ug/kg5.414
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg5.414
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg5.414
4-Chloroaniline 106-47-8 8270E ND 1ug/kg5.414
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg5.414
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg5.414
2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg5.414
2-Chlorophenol 95-57-8 8270E ND 1ug/kg5.414
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg5.414
Chrysene 218-01-9 8270E ND 1ug/kg0.492.9
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.552.9
Dibenzofuran 132-64-9 8270E ND 1ug/kg5.414
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg5.414
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg5.414
Diethylphthalate 84-66-2 8270E ND 1ug/kg5.414
Dimethyl phthalate 131-11-3 8270E ND 1ug/kg8.014
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg5.414
Di-n-butyl phthalate 84-74-2 8270E 7.3 J 1ug/kg5.414
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg2772
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg2772
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1129
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1129
Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg5.414
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg2772
Fluoranthene 206-44-0 8270E ND 1ug/kg0.452.9
Fluorene 86-73-7 8270E ND 1ug/kg0.612.9
Hexachlorobenzene 118-74-1 8270E ND 1ug/kg5.414
Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg5.414
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg2772
Hexachloroethane 67-72-1 8270E ND 1ug/kg5.414
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1.12.9
Isophorone 78-59-1 8270E ND 1ug/kg5.414
2-Methylnaphthalene 91-57-6 8270E ND 1ug/kg1.12.9
2-Methylphenol 95-48-7 8270E ND 1ug/kg5.414
3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1129
Naphthalene 91-20-3 8270E ND 1ug/kg1.02.9
2-Nitroaniline 88-74-4 8270E ND 1ug/kg1129
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 12 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-2
UL31060-002
12/31/2019 1100
12/31/2019
Solid
% Solids:90.9 01/02/2020 2024
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 01/06/2020 2103 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3-Nitroaniline 99-09-2 8270E ND 1ug/kg1129
4-Nitroaniline 100-01-6 8270E ND 1ug/kg1129
Nitrobenzene 98-95-3 8270E ND 1ug/kg5.414
2-Nitrophenol 88-75-5 8270E ND 1ug/kg1129
4-Nitrophenol 100-02-7 8270E ND 1ug/kg2772
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg5.414
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg5.414
Pentachlorophenol 87-86-5 8270E ND 1ug/kg2772
Phenanthrene 85-01-8 8270E ND 1ug/kg0.782.9
Phenol 108-95-2 8270E ND 1ug/kg5.414
Pyrene 129-00-0 8270E ND 1ug/kg0.542.9
Pyridine 110-86-1 8270E ND 1ug/kg5.414
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg5.414
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg5.414
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 48 33-102
2-Fluorophenol 53 35-115
Nitrobenzene-d5 58 22-109
Phenol-d5 54 33-122
Terphenyl-d14 54 41-120
2,4,6-Tribromophenol 53 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/06/2020 0625 LLL 01/05/2020 1437 40813
1 7471B 7471B 1 01/04/2020 1059 KSH2 01/03/2020 1317 40814
2 3050B 6010D 3 01/06/2020 0811 LLL 01/05/2020 1437 40813
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010D 1.9 1mg/kg0.270.81
Barium 7440-39-3 6010D 44 1mg/kg0.351.4
Cadmium 7440-43-9 6010D ND 1mg/kg0.0680.27
Chromium 7440-47-3 6010D 23 1mg/kg0.130.54
Lead 7439-92-1 6010D 7.9 2mg/kg0.731.6
Mercury 7439-97-6 7471B ND 1mg/kg0.0220.090
Selenium 7782-49-2 6010D ND 1mg/kg0.441.1
Silver 7440-22-4 6010D ND 1mg/kg0.130.54
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 13 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3
UL31060-003
12/31/2019 1115
12/31/2019
Solid
% Solids:85.2 01/02/2020 2024
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 01/04/2020 1913 HKL 01/02/2020 1447 40691
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.231.2
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 01/02/2020 1249 JM1 40716 6.33
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/kg7.419
Benzene 71-43-2 8260D ND 1ug/kg1.94.6
Bromodichloromethane 75-27-4 8260D ND 1ug/kg1.94.6
Bromoform 75-25-2 8260D ND 1ug/kg1.94.6
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg2.84.6
2-Butanone (MEK)78-93-3 8260D ND 1ug/kg3.719
Carbon disulfide 75-15-0 8260D ND 1ug/kg1.94.6
Carbon tetrachloride 56-23-5 8260D ND 1ug/kg1.94.6
Chlorobenzene 108-90-7 8260D ND 1ug/kg1.94.6
Chloroethane 75-00-3 8260D ND 1ug/kg1.94.6
Chloroform 67-66-3 8260D ND 1ug/kg1.94.6
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg2.84.6
Cyclohexane 110-82-7 8260D ND 1ug/kg1.94.6
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg1.94.6
Dibromochloromethane 124-48-1 8260D ND 1ug/kg1.94.6
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg1.94.6
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg1.94.6
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg1.94.6
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg1.94.6
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg2.84.6
1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg1.94.6
1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg1.94.6
1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg1.94.6
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg1.94.6
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg1.94.6
1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg1.94.6
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg1.94.6
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg1.94.6
Ethylbenzene 100-41-4 8260D ND 1ug/kg1.94.6
2-Hexanone 591-78-6 8260D ND 1ug/kg3.79.3
Isopropylbenzene 98-82-8 8260D ND 1ug/kg1.94.6
Methyl acetate 79-20-9 8260D ND 1ug/kg1.94.6
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 14 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3
UL31060-003
12/31/2019 1115
12/31/2019
Solid
% Solids:85.2 01/02/2020 2024
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 01/02/2020 1249 JM1 40716 6.33
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg1.94.6
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg3.79.3
Methylcyclohexane 108-87-2 8260D ND 1ug/kg1.94.6
Methylene chloride 75-09-2 8260D ND 1ug/kg1.94.6
Styrene 100-42-5 8260D ND 1ug/kg1.94.6
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg1.94.6
Tetrachloroethene 127-18-4 8260D ND 1ug/kg1.94.6
Toluene 108-88-3 8260D ND 1ug/kg1.94.6
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg1.94.6
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg1.94.6
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg1.94.6
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg1.94.6
Trichloroethene 79-01-6 8260D 1.9 J 1ug/kg1.94.6
Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg1.94.6
Vinyl chloride 75-01-4 8260D ND 1ug/kg2.84.6
Xylenes (total)1330-20-7 8260D ND 1ug/kg3.79.3
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 98 47-138
1,2-Dichloroethane-d4 93 53-142
Toluene-d8 109 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 20 01/06/2020 2127 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E ND 1ug/kg1963
Acenaphthylene 208-96-8 8270E ND 1ug/kg2263
Acetophenone 98-86-2 8270E ND 1ug/kg120310
Anthracene 120-12-7 8270E ND 1ug/kg1263
Atrazine 1912-24-9 8270E ND 1ug/kg120310
Benzaldehyde 100-52-7 8270E ND 1ug/kg120310
Benzo(a)anthracene 56-55-3 8270E 86 1ug/kg1463
Benzo(a)pyrene 50-32-8 8270E 100 1ug/kg1563
Benzo(b)fluoranthene 205-99-2 8270E 140 1ug/kg1263
Benzo(g,h,i)perylene 191-24-2 8270E 43 J 1ug/kg1563
Benzo(k)fluoranthene 207-08-9 8270E 41 J 1ug/kg1163
1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg120310
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 15 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3
UL31060-003
12/31/2019 1115
12/31/2019
Solid
% Solids:85.2 01/02/2020 2024
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 20 01/06/2020 2127 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg120310
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg120310
Caprolactam 105-60-2 8270E ND 1ug/kg120310
Carbazole 86-74-8 8270E ND 1ug/kg120310
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg120310
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg120310
4-Chloroaniline 106-47-8 8270E ND 1ug/kg120310
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg120310
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg120310
2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg120310
2-Chlorophenol 95-57-8 8270E ND 1ug/kg120310
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg120310
Chrysene 218-01-9 8270E 67 1ug/kg1163
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg1263
Dibenzofuran 132-64-9 8270E ND 1ug/kg120310
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg120310
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg120310
Diethylphthalate 84-66-2 8270E ND 1ug/kg120310
Dimethyl phthalate 131-11-3 8270E ND 1ug/kg170310
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg120310
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg120310
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg5901600
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg5901600
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg230630
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg230630
Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg120310
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg5901600
Fluoranthene 206-44-0 8270E 150 1ug/kg9.963
Fluorene 86-73-7 8270E ND 1ug/kg1363
Hexachlorobenzene 118-74-1 8270E ND 1ug/kg120310
Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg120310
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg5901600
Hexachloroethane 67-72-1 8270E ND 1ug/kg120310
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E 42 J 1ug/kg2363
Isophorone 78-59-1 8270E ND 1ug/kg120310
2-Methylnaphthalene 91-57-6 8270E 34 J 1ug/kg2363
2-Methylphenol 95-48-7 8270E ND 1ug/kg120310
3+4-Methylphenol 106-44-5 8270E ND 1ug/kg230630
Naphthalene 91-20-3 8270E 33 J 1ug/kg2363
2-Nitroaniline 88-74-4 8270E ND 1ug/kg230630
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 16 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3
UL31060-003
12/31/2019 1115
12/31/2019
Solid
% Solids:85.2 01/02/2020 2024
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 20 01/06/2020 2127 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3-Nitroaniline 99-09-2 8270E ND 1ug/kg230630
4-Nitroaniline 100-01-6 8270E ND 1ug/kg230630
Nitrobenzene 98-95-3 8270E ND 1ug/kg120310
2-Nitrophenol 88-75-5 8270E ND 1ug/kg230630
4-Nitrophenol 100-02-7 8270E ND 1ug/kg5901600
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg120310
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg120310
Pentachlorophenol 87-86-5 8270E ND 1ug/kg5901600
Phenanthrene 85-01-8 8270E 86 1ug/kg1763
Phenol 108-95-2 8270E ND 1ug/kg120310
Pyrene 129-00-0 8270E 110 1ug/kg1263
Pyridine 110-86-1 8270E ND 1ug/kg120310
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg120310
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg120310
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 55 33-102
2-Fluorophenol 67 35-115
Nitrobenzene-d5 65 22-109
Phenol-d5 55 33-122
Terphenyl-d14 60 41-120
2,4,6-Tribromophenol 50 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/06/2020 0631 LLL 01/05/2020 1437 40813
1 7471B 7471B 1 01/04/2020 1102 KSH2 01/03/2020 1317 40814
2 3050B 6010D 2 01/06/2020 0816 LLL 01/05/2020 1437 40813
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010D 3.8 2mg/kg0.551.6
Barium 7440-39-3 6010D 130 1mg/kg0.361.4
Cadmium 7440-43-9 6010D ND 2mg/kg0.140.55
Chromium 7440-47-3 6010D 42 1mg/kg0.140.55
Lead 7439-92-1 6010D 55 2mg/kg0.491.1
Mercury 7439-97-6 7471B 0.067 J 1mg/kg0.0220.093
Selenium 7782-49-2 6010D ND 2mg/kg0.892.2
Silver 7440-22-4 6010D ND 1mg/kg0.140.55
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 17 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-4
UL31060-004
12/31/2019 1130
12/31/2019
Solid
% Solids:83.9 01/02/2020 2024
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 01/04/2020 1926 HKL 01/02/2020 1447 40691
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.35 J 1mg/kg0.241.2
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 01/02/2020 1312 JM1 40716 5.99
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/kg8.020
Benzene 71-43-2 8260D ND 1ug/kg2.05.0
Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.05.0
Bromoform 75-25-2 8260D ND 1ug/kg2.05.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.05.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/kg4.020
Carbon disulfide 75-15-0 8260D ND 1ug/kg2.05.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.05.0
Chlorobenzene 108-90-7 8260D ND 1ug/kg2.05.0
Chloroethane 75-00-3 8260D ND 1ug/kg2.05.0
Chloroform 67-66-3 8260D ND 1ug/kg2.05.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.05.0
Cyclohexane 110-82-7 8260D ND 1ug/kg2.05.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.05.0
Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.05.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.05.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.05.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.05.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.05.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.05.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.05.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.05.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.05.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.05.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.05.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.05.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.05.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.05.0
Ethylbenzene 100-41-4 8260D ND 1ug/kg2.05.0
2-Hexanone 591-78-6 8260D ND 1ug/kg4.010
Isopropylbenzene 98-82-8 8260D ND 1ug/kg2.05.0
Methyl acetate 79-20-9 8260D ND 1ug/kg2.05.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 18 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-4
UL31060-004
12/31/2019 1130
12/31/2019
Solid
% Solids:83.9 01/02/2020 2024
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 01/02/2020 1312 JM1 40716 5.99
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.05.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.010
Methylcyclohexane 108-87-2 8260D ND 1ug/kg2.05.0
Methylene chloride 75-09-2 8260D ND 1ug/kg2.05.0
Styrene 100-42-5 8260D ND 1ug/kg2.05.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.05.0
Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.05.0
Toluene 108-88-3 8260D ND 1ug/kg2.05.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.05.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.05.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.05.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.05.0
Trichloroethene 79-01-6 8260D 2.0 J 1ug/kg2.05.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.05.0
Vinyl chloride 75-01-4 8260D ND 1ug/kg3.05.0
Xylenes (total)1330-20-7 8260D ND 1ug/kg4.010
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 96 47-138
1,2-Dichloroethane-d4 90 53-142
Toluene-d8 105 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 20 01/06/2020 2241 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E ND 1ug/kg1963
Acenaphthylene 208-96-8 8270E ND 1ug/kg2263
Acetophenone 98-86-2 8270E ND 1ug/kg120300
Anthracene 120-12-7 8270E ND 1ug/kg1263
Atrazine 1912-24-9 8270E ND 1ug/kg120300
Benzaldehyde 100-52-7 8270E ND 1ug/kg120300
Benzo(a)anthracene 56-55-3 8270E 74 1ug/kg1463
Benzo(a)pyrene 50-32-8 8270E 79 1ug/kg1563
Benzo(b)fluoranthene 205-99-2 8270E 110 1ug/kg1263
Benzo(g,h,i)perylene 191-24-2 8270E 60 J 1ug/kg1563
Benzo(k)fluoranthene 207-08-9 8270E 42 J 1ug/kg1163
1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg120300
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 19 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-4
UL31060-004
12/31/2019 1130
12/31/2019
Solid
% Solids:83.9 01/02/2020 2024
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 20 01/06/2020 2241 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg120300
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg120300
Caprolactam 105-60-2 8270E ND 1ug/kg120300
Carbazole 86-74-8 8270E ND 1ug/kg120300
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg120300
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg120300
4-Chloroaniline 106-47-8 8270E ND 1ug/kg120300
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg120300
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg120300
2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg120300
2-Chlorophenol 95-57-8 8270E ND 1ug/kg120300
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg120300
Chrysene 218-01-9 8270E 56 J 1ug/kg1163
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg1263
Dibenzofuran 132-64-9 8270E ND 1ug/kg120300
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg120300
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg120300
Diethylphthalate 84-66-2 8270E ND 1ug/kg120300
Dimethyl phthalate 131-11-3 8270E ND 1ug/kg170300
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg120300
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg120300
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg5801600
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg5801600
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg230630
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg230630
Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg120300
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg5801600
Fluoranthene 206-44-0 8270E 92 1ug/kg9.863
Fluorene 86-73-7 8270E ND 1ug/kg1363
Hexachlorobenzene 118-74-1 8270E ND 1ug/kg120300
Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg120300
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg5801600
Hexachloroethane 67-72-1 8270E ND 1ug/kg120300
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E 45 J 1ug/kg2363
Isophorone 78-59-1 8270E ND 1ug/kg120300
2-Methylnaphthalene 91-57-6 8270E ND 1ug/kg2363
2-Methylphenol 95-48-7 8270E ND 1ug/kg120300
3+4-Methylphenol 106-44-5 8270E ND 1ug/kg230630
Naphthalene 91-20-3 8270E ND 1ug/kg2363
2-Nitroaniline 88-74-4 8270E ND 1ug/kg230630
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 20 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-4
UL31060-004
12/31/2019 1130
12/31/2019
Solid
% Solids:83.9 01/02/2020 2024
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 20 01/06/2020 2241 JCG 01/02/2020 1850 40761
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3-Nitroaniline 99-09-2 8270E ND 1ug/kg230630
4-Nitroaniline 100-01-6 8270E ND 1ug/kg230630
Nitrobenzene 98-95-3 8270E ND 1ug/kg120300
2-Nitrophenol 88-75-5 8270E ND 1ug/kg230630
4-Nitrophenol 100-02-7 8270E ND 1ug/kg5801600
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg120300
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg120300
Pentachlorophenol 87-86-5 8270E ND 1ug/kg5801600
Phenanthrene 85-01-8 8270E 59 J 1ug/kg1763
Phenol 108-95-2 8270E ND 1ug/kg120300
Pyrene 129-00-0 8270E 81 1ug/kg1263
Pyridine 110-86-1 8270E ND 1ug/kg120300
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg120300
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg120300
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 54 33-102
2-Fluorophenol 59 35-115
Nitrobenzene-d5 59 22-109
Phenol-d5 60 33-122
Terphenyl-d14 58 41-120
2,4,6-Tribromophenol 36 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/06/2020 0636 LLL 01/05/2020 1437 40813
1 7471B 7471B 1 01/04/2020 1104 KSH2 01/03/2020 1317 40814
2 3050B 6010D 2 01/06/2020 0822 LLL 01/05/2020 1437 40813
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010D 8.0 2mg/kg0.551.6
Barium 7440-39-3 6010D 100 1mg/kg0.351.4
Cadmium 7440-43-9 6010D ND 2mg/kg0.140.55
Chromium 7440-47-3 6010D 54 1mg/kg0.140.55
Lead 7439-92-1 6010D 45 2mg/kg0.491.1
Mercury 7439-97-6 7471B 0.089 J 1mg/kg0.0230.096
Selenium 7782-49-2 6010D ND 2mg/kg0.892.2
Silver 7440-22-4 6010D ND 1mg/kg0.140.55
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 21 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
GW-3
UL31060-005
12/31/2019 1110
12/31/2019
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 01/02/2020 1723 TML 40777
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromodichloromethane 75-27-4 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
Carbon disulfide 75-15-0 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
Cyclohexane 110-82-7 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
Methyl acetate 79-20-9 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylcyclohexane 108-87-2 8260D ND 1ug/L0.405.0
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 22 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
GW-3
UL31060-005
12/31/2019 1110
12/31/2019
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 01/02/2020 1723 TML 40777
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 94 70-130
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 01/06/2020 2305 SCD 01/02/2020 1408 40737
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E ND 1ug/L0.0400.16
Acenaphthylene 208-96-8 8270E ND 1ug/L0.0400.16
Acetophenone 98-86-2 8270E ND 1ug/L0.230.80
Anthracene 120-12-7 8270E ND 1ug/L0.0400.16
Atrazine 1912-24-9 8270E ND 1ug/L0.200.80
Benzaldehyde 100-52-7 8270E ND 1ug/L0.274.0
Benzo(a)anthracene 56-55-3 8270E ND 1ug/L0.0400.16
Benzo(a)pyrene 50-32-8 8270E ND 1ug/L0.0400.16
Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/L0.0400.16
Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/L0.0400.16
Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/L0.0400.16
1,1'-Biphenyl 92-52-4 8270E ND 1ug/L0.210.80
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/L0.150.80
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/L0.214.0
Caprolactam 105-60-2 8270E ND 1ug/L0.714.0
Carbazole 86-74-8 8270E ND 1ug/L0.0400.80
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/L0.170.80
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/L0.260.80
4-Chloroaniline 106-47-8 8270E ND 1ug/L0.130.80
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/L0.0600.80
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 23 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
GW-3
UL31060-005
12/31/2019 1110
12/31/2019
Aqueous
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 01/06/2020 2305 SCD 01/02/2020 1408 40737
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/L0.160.80
2-Chloronaphthalene 91-58-7 8270E ND 1ug/L0.150.80
2-Chlorophenol 95-57-8 8270E ND 1ug/L0.150.80
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/L0.160.80
Chrysene 218-01-9 8270E ND 1ug/L0.0400.16
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/L0.0400.16
Dibenzofuran 132-64-9 8270E ND 1ug/L0.160.80
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/L0.814.0
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/L0.190.80
Diethylphthalate 84-66-2 8270E ND 1ug/L0.194.0
Dimethyl phthalate 131-11-3 8270E ND 1ug/L0.184.0
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/L0.150.80
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/L0.424.0
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/L0.894.0
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/L1.34.0
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/L0.361.6
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/L0.341.6
Di-n-octylphthalate 117-84-0 8270E ND 1ug/L0.484.0
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/L0.384.0
Fluoranthene 206-44-0 8270E ND 1ug/L0.0400.16
Fluorene 86-73-7 8270E ND 1ug/L0.0400.16
Hexachlorobenzene 118-74-1 8270E ND 1ug/L0.150.80
Hexachlorobutadiene 87-68-3 8270E ND 1ug/L0.170.80
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/L1.14.0
Hexachloroethane 67-72-1 8270E ND 1ug/L0.170.80
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/L0.0400.16
Isophorone 78-59-1 8270E ND 1ug/L0.220.80
2-Methylnaphthalene 91-57-6 8270E ND 1ug/L0.0400.16
2-Methylphenol 95-48-7 8270E ND 1ug/L0.210.80
3+4-Methylphenol 106-44-5 8270E ND 1ug/L0.461.6
Naphthalene 91-20-3 8270E 0.041 J 1ug/L0.0400.16
2-Nitroaniline 88-74-4 8270E ND 1ug/L0.661.6
3-Nitroaniline 99-09-2 8270E ND 1ug/L0.151.6
4-Nitroaniline 100-01-6 8270E ND 1ug/L1.31.6
Nitrobenzene 98-95-3 8270E ND 1ug/L0.170.80
2-Nitrophenol 88-75-5 8270E ND 1ug/L0.441.6
4-Nitrophenol 100-02-7 8270E ND 1ug/L2.14.0
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/L0.280.80
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/L0.500.80
Pentachlorophenol 87-86-5 8270E ND 1ug/L1.34.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 24 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
GW-3
UL31060-005
12/31/2019 1110
12/31/2019
Aqueous
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 01/06/2020 2305 SCD 01/02/2020 1408 40737
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Phenanthrene 85-01-8 8270E ND 1ug/L0.0400.16
Phenol 108-95-2 8270E ND 1ug/L0.190.80
Pyrene 129-00-0 8270E 0.049 J 1ug/L0.0400.16
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/L0.190.80
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/L0.220.80
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 61 37-129
2-Fluorophenol 24 24-127
Nitrobenzene-d5 71 38-127
Phenol-d5 55 28-128
Terphenyl-d14 73 10-148
2,4,6-Tribromophenol 64 35-144
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 25 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
GW-4
UL31060-006
12/31/2019 1050
12/31/2019
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 01/02/2020 1746 TML 40777
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/L5.020
Benzene 71-43-2 8260D ND 1ug/L0.401.0
Bromodichloromethane 75-27-4 8260D ND 1ug/L0.401.0
Bromoform 75-25-2 8260D ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/L2.010
Carbon disulfide 75-15-0 8260D ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260D ND 1ug/L0.401.0
Chloroethane 75-00-3 8260D ND 1ug/L0.402.0
Chloroform 67-66-3 8260D ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/L0.501.0
Cyclohexane 110-82-7 8260D ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260D ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/L0.401.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/L0.602.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/L0.401.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260D ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260D ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260D ND 1ug/L0.401.0
Methyl acetate 79-20-9 8260D ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/L2.010
Methylcyclohexane 108-87-2 8260D ND 1ug/L0.405.0
Methylene chloride 75-09-2 8260D ND 1ug/L0.401.0
Styrene 100-42-5 8260D ND 1ug/L0.411.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260D ND 1ug/L0.401.0
Toluene 108-88-3 8260D ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 26 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
GW-4
UL31060-006
12/31/2019 1050
12/31/2019
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 01/02/2020 1746 TML 40777
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/L0.421.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260D ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260D ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260D ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 95 70-130
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 01/06/2020 2330 SCD 01/02/2020 1408 40737
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E ND 1ug/L0.0400.16
Acenaphthylene 208-96-8 8270E ND 1ug/L0.0400.16
Acetophenone 98-86-2 8270E ND 1ug/L0.230.80
Anthracene 120-12-7 8270E ND 1ug/L0.0400.16
Atrazine 1912-24-9 8270E ND 1ug/L0.200.80
Benzaldehyde 100-52-7 8270E ND 1ug/L0.274.0
Benzo(a)anthracene 56-55-3 8270E ND 1ug/L0.0400.16
Benzo(a)pyrene 50-32-8 8270E ND 1ug/L0.0400.16
Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/L0.0400.16
Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/L0.0400.16
Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/L0.0400.16
1,1'-Biphenyl 92-52-4 8270E ND 1ug/L0.210.80
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/L0.150.80
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/L0.214.0
Caprolactam 105-60-2 8270E ND 1ug/L0.714.0
Carbazole 86-74-8 8270E ND 1ug/L0.0400.80
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/L0.170.80
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/L0.260.80
4-Chloroaniline 106-47-8 8270E ND 1ug/L0.130.80
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/L0.0600.80
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 27 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
GW-4
UL31060-006
12/31/2019 1050
12/31/2019
Aqueous
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 01/06/2020 2330 SCD 01/02/2020 1408 40737
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/L0.160.80
2-Chloronaphthalene 91-58-7 8270E ND 1ug/L0.150.80
2-Chlorophenol 95-57-8 8270E ND 1ug/L0.150.80
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/L0.160.80
Chrysene 218-01-9 8270E ND 1ug/L0.0400.16
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/L0.0400.16
Dibenzofuran 132-64-9 8270E ND 1ug/L0.160.80
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/L0.814.0
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/L0.190.80
Diethylphthalate 84-66-2 8270E ND 1ug/L0.194.0
Dimethyl phthalate 131-11-3 8270E ND 1ug/L0.184.0
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/L0.150.80
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/L0.424.0
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/L0.894.0
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/L1.34.0
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/L0.361.6
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/L0.341.6
Di-n-octylphthalate 117-84-0 8270E ND 1ug/L0.484.0
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/L0.384.0
Fluoranthene 206-44-0 8270E ND 1ug/L0.0400.16
Fluorene 86-73-7 8270E ND 1ug/L0.0400.16
Hexachlorobenzene 118-74-1 8270E ND 1ug/L0.150.80
Hexachlorobutadiene 87-68-3 8270E ND 1ug/L0.170.80
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/L1.14.0
Hexachloroethane 67-72-1 8270E ND 1ug/L0.170.80
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/L0.0400.16
Isophorone 78-59-1 8270E ND 1ug/L0.220.80
2-Methylnaphthalene 91-57-6 8270E ND 1ug/L0.0400.16
2-Methylphenol 95-48-7 8270E ND 1ug/L0.210.80
3+4-Methylphenol 106-44-5 8270E 1.9 1ug/L0.461.6
Naphthalene 91-20-3 8270E ND 1ug/L0.0400.16
2-Nitroaniline 88-74-4 8270E ND 1ug/L0.661.6
3-Nitroaniline 99-09-2 8270E ND 1ug/L0.151.6
4-Nitroaniline 100-01-6 8270E ND 1ug/L1.31.6
Nitrobenzene 98-95-3 8270E ND 1ug/L0.170.80
2-Nitrophenol 88-75-5 8270E ND 1ug/L0.441.6
4-Nitrophenol 100-02-7 8270E ND 1ug/L2.14.0
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/L0.280.80
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/L0.500.80
Pentachlorophenol 87-86-5 8270E ND 1ug/L1.34.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 28 of 73
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
GW-4
UL31060-006
12/31/2019 1050
12/31/2019
Aqueous
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 01/06/2020 2330 SCD 01/02/2020 1408 40737
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Phenanthrene 85-01-8 8270E ND 1ug/L0.0400.16
Phenol 108-95-2 8270E ND 1ug/L0.190.80
Pyrene 129-00-0 8270E ND 1ug/L0.0400.16
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/L0.190.80
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/L0.220.80
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 54 37-129
2-Fluorophenol N 22 24-127
Nitrobenzene-d5 56 38-127
Phenol-d5 49 28-128
Terphenyl-d14 58 10-148
2,4,6-Tribromophenol 61 35-144
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 29 of 73
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 30 of 73
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:VQ40691-001
40691 3060A
01/02/2020 1447Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 01/04/2020 15591.0 0.20 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 31 of 73
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:VQ40691-002
40691 3060A
01/02/2020 1447Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Hexavalent Chromium 9.8 01/04/2020 1612981080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 32 of 73
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:VQ40716-001
40716 5035
Analytical Method:8260D
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 01/02/2020 0954208.0 ug/kg1
Benzene ND 01/02/2020 09545.0 2.0 ug/kg1
Bromodichloromethane ND 01/02/2020 09545.0 2.0 ug/kg1
Bromoform ND 01/02/2020 09545.0 2.0 ug/kg1
Bromomethane (Methyl bromide)ND 01/02/2020 09545.0 3.0 ug/kg1
2-Butanone (MEK)ND 01/02/2020 0954204.0 ug/kg1
Carbon disulfide ND 01/02/2020 09545.0 2.0 ug/kg1
Carbon tetrachloride ND 01/02/2020 09545.0 2.0 ug/kg1
Chlorobenzene ND 01/02/2020 09545.0 2.0 ug/kg1
Chloroethane ND 01/02/2020 09545.0 2.0 ug/kg1
Chloroform ND 01/02/2020 09545.0 2.0 ug/kg1
Chloromethane (Methyl chloride)ND 01/02/2020 09545.0 3.0 ug/kg1
Cyclohexane ND 01/02/2020 09545.0 2.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 01/02/2020 09545.0 2.0 ug/kg1
Dibromochloromethane ND 01/02/2020 09545.0 2.0 ug/kg1
1,2-Dibromoethane (EDB)ND 01/02/2020 09545.0 2.0 ug/kg1
1,2-Dichlorobenzene ND 01/02/2020 09545.0 2.0 ug/kg1
1,3-Dichlorobenzene ND 01/02/2020 09545.0 2.0 ug/kg1
1,4-Dichlorobenzene ND 01/02/2020 09545.0 2.0 ug/kg1
Dichlorodifluoromethane ND 01/02/2020 09545.0 3.0 ug/kg1
1,1-Dichloroethane ND 01/02/2020 09545.0 2.0 ug/kg1
1,2-Dichloroethane ND 01/02/2020 09545.0 2.0 ug/kg1
1,1-Dichloroethene ND 01/02/2020 09545.0 2.0 ug/kg1
cis-1,2-Dichloroethene ND 01/02/2020 09545.0 2.0 ug/kg1
trans-1,2-Dichloroethene ND 01/02/2020 09545.0 2.0 ug/kg1
1,2-Dichloropropane ND 01/02/2020 09545.0 2.0 ug/kg1
cis-1,3-Dichloropropene ND 01/02/2020 09545.0 2.0 ug/kg1
trans-1,3-Dichloropropene ND 01/02/2020 09545.0 2.0 ug/kg1
Ethylbenzene ND 01/02/2020 09545.0 2.0 ug/kg1
2-Hexanone ND 01/02/2020 0954104.0 ug/kg1
Isopropylbenzene ND 01/02/2020 09545.0 2.0 ug/kg1
Methyl acetate ND 01/02/2020 09545.0 2.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 01/02/2020 09545.0 2.0 ug/kg1
4-Methyl-2-pentanone ND 01/02/2020 0954104.0 ug/kg1
Methylcyclohexane ND 01/02/2020 09545.0 2.0 ug/kg1
Methylene chloride ND 01/02/2020 09545.0 2.0 ug/kg1
Styrene ND 01/02/2020 09545.0 2.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 01/02/2020 09545.0 2.0 ug/kg1
Tetrachloroethene ND 01/02/2020 09545.0 2.0 ug/kg1
Toluene ND 01/02/2020 09545.0 2.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 01/02/2020 09545.0 2.0 ug/kg1
1,2,4-Trichlorobenzene ND 01/02/2020 09545.0 2.0 ug/kg1
1,1,1-Trichloroethane ND 01/02/2020 09545.0 2.0 ug/kg1
1,1,2-Trichloroethane ND 01/02/2020 09545.0 2.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 33 of 73
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:VQ40716-001
40716 5035
Analytical Method:8260D
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Trichloroethene ND 01/02/2020 09545.0 2.0 ug/kg1
Trichlorofluoromethane ND 01/02/2020 09545.0 2.0 ug/kg1
Vinyl chloride ND 01/02/2020 09545.0 3.0 ug/kg1
Xylenes (total)ND 01/02/2020 0954104.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 103 47-138
1,2-Dichloroethane-d4 86 53-142
Toluene-d8 100 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 34 of 73
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:VQ40716-002
40716 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 93 01/02/2020 09099310060-1401
Benzene 52 01/02/2020 09091045070-1301
Bromodichloromethane 51 01/02/2020 09091025070-1301
Bromoform 51 01/02/2020 09091015070-1301
Bromomethane (Methyl bromide)54 01/02/2020 09091085070-1301
2-Butanone (MEK)93 01/02/2020 09099310060-1401
Carbon disulfide 54 01/02/2020 09091085070-1301
Carbon tetrachloride 52 01/02/2020 09091055070-1301
Chlorobenzene 53 01/02/2020 09091065070-1301
Chloroethane 54 01/02/2020 09091095070-1301
Chloroform 51 01/02/2020 09091025070-1301
Chloromethane (Methyl chloride)58 01/02/2020 09091155060-1401
Cyclohexane 49 01/02/2020 0909985070-1301
1,2-Dibromo-3-chloropropane (DBCP)48 01/02/2020 0909975070-1301
Dibromochloromethane 51 01/02/2020 09091025070-1301
1,2-Dibromoethane (EDB)49 01/02/2020 0909985070-1301
1,2-Dichlorobenzene 53 01/02/2020 09091065070-1301
1,3-Dichlorobenzene 55 01/02/2020 09091105070-1301
1,4-Dichlorobenzene 55 01/02/2020 09091095070-1301
Dichlorodifluoromethane 60 01/02/2020 09091215060-1401
1,1-Dichloroethane 51 01/02/2020 09091035070-1301
1,2-Dichloroethane 49 01/02/2020 0909985070-1301
1,1-Dichloroethene 53 01/02/2020 09091065070-1301
cis-1,2-Dichloroethene 52 01/02/2020 09091045070-1301
trans-1,2-Dichloroethene 53 01/02/2020 09091065070-1301
1,2-Dichloropropane 51 01/02/2020 09091025070-1301
cis-1,3-Dichloropropene 52 01/02/2020 09091045070-1301
trans-1,3-Dichloropropene 52 01/02/2020 09091045070-1301
Ethylbenzene 55 01/02/2020 09091105070-1301
2-Hexanone 98 01/02/2020 09099810070-1301
Isopropylbenzene 55 01/02/2020 09091105070-1301
Methyl acetate 46 01/02/2020 0909935070-1301
Methyl tertiary butyl ether (MTBE)49 01/02/2020 0909985070-1301
4-Methyl-2-pentanone 95 01/02/2020 09099510070-1301
Methylcyclohexane 51 01/02/2020 09091025070-1301
Methylene chloride 50 01/02/2020 0909995070-1301
Styrene 54 01/02/2020 09091095070-1301
1,1,2,2-Tetrachloroethane 51 01/02/2020 09091015070-1301
Tetrachloroethene 56 01/02/2020 09091115070-1301
Toluene 54 01/02/2020 09091085070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 50 01/02/2020 0909995070-1301
1,2,4-Trichlorobenzene 58 01/02/2020 09091155070-1301
1,1,1-Trichloroethane 52 01/02/2020 09091055070-1301
1,1,2-Trichloroethane 49 01/02/2020 0909995070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 35 of 73
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:VQ40716-002
40716 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 52 01/02/2020 09091045070-1301
Trichlorofluoromethane 52 01/02/2020 09091055070-1301
Vinyl chloride 57 01/02/2020 09091155070-1301
Xylenes (total)110 01/02/2020 090910910070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 47-138
1,2-Dichloroethane-d4 94 53-142
Toluene-d8 103 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 36 of 73
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:UL31060-001DU
40716 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Acetone ND 01/02/2020 16150.00 20ND1
Benzene ND 01/02/2020 16150.00 20ND1
Bromodichloromethane ND 01/02/2020 16150.00 20ND1
Bromoform ND 01/02/2020 16150.00 20ND1
Bromomethane (Methyl bromide)ND 01/02/2020 16150.00 20ND1
2-Butanone (MEK)ND 01/02/2020 16150.00 20ND1
Carbon disulfide ND 01/02/2020 16150.00 20ND1
Carbon tetrachloride ND 01/02/2020 16150.00 20ND1
Chlorobenzene ND 01/02/2020 16150.00 20ND1
Chloroethane ND 01/02/2020 16150.00 20ND1
Chloroform ND 01/02/2020 16150.00 20ND1
Chloromethane (Methyl chloride)ND 01/02/2020 16150.00 20ND1
Cyclohexane ND 01/02/2020 16150.00 20ND1
1,2-Dibromo-3-chloropropane (DBCP)ND 01/02/2020 16150.00 20ND1
Dibromochloromethane ND 01/02/2020 16150.00 20ND1
1,2-Dibromoethane (EDB)ND 01/02/2020 16150.00 20ND1
1,2-Dichlorobenzene ND 01/02/2020 16150.00 20ND1
1,3-Dichlorobenzene ND 01/02/2020 16150.00 20ND1
1,4-Dichlorobenzene ND 01/02/2020 16150.00 20ND1
Dichlorodifluoromethane ND 01/02/2020 16150.00 20ND1
1,1-Dichloroethane ND 01/02/2020 16150.00 20ND1
1,2-Dichloroethane ND 01/02/2020 16150.00 20ND1
1,1-Dichloroethene ND 01/02/2020 16150.00 20ND1
cis-1,2-Dichloroethene ND 01/02/2020 16150.00 20ND1
trans-1,2-Dichloroethene ND 01/02/2020 16150.00 20ND1
1,2-Dichloropropane ND 01/02/2020 16150.00 20ND1
cis-1,3-Dichloropropene ND 01/02/2020 16150.00 20ND1
trans-1,3-Dichloropropene ND 01/02/2020 16150.00 20ND1
Ethylbenzene ND 01/02/2020 16150.00 20ND1
2-Hexanone ND 01/02/2020 16150.00 20ND1
Isopropylbenzene ND 01/02/2020 16150.00 20ND1
Methyl acetate ND 01/02/2020 16150.00 20ND1
Methyl tertiary butyl ether (MTBE)ND 01/02/2020 16150.00 20ND1
4-Methyl-2-pentanone ND 01/02/2020 16150.00 20ND1
Methylcyclohexane ND 01/02/2020 16150.00 20ND1
Methylene chloride ND 01/02/2020 16150.00 20ND1
Styrene ND 01/02/2020 16150.00 20ND1
1,1,2,2-Tetrachloroethane ND 01/02/2020 16150.00 20ND1
Tetrachloroethene ND 01/02/2020 16150.00 20ND1
Toluene ND 01/02/2020 16150.00 20ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 01/02/2020 16150.00 20ND1
1,2,4-Trichlorobenzene ND 01/02/2020 16150.00 20ND1
1,1,1-Trichloroethane ND 01/02/2020 16150.00 20ND1
1,1,2-Trichloroethane ND 01/02/2020 16150.00 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 37 of 73
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:UL31060-001DU
40716 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Trichloroethene ND 01/02/2020 16150.00 20ND1
Trichlorofluoromethane ND 01/02/2020 16150.00 20ND1
Vinyl chloride ND 01/02/2020 16150.00 20ND1
Xylenes (total)ND 01/02/2020 16150.00 20ND1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 99 47-138
1,2-Dichloroethane-d4 94 53-142
Toluene-d8 108 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 38 of 73
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:UL31060-002MS
40716 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acetone 80 01/02/2020 16577910070-130ND1
Benzene 43 01/02/2020 1657845170-130ND1
Bromodichloromethane 41 01/02/2020 1657815170-130ND1
Bromoform 41 01/02/2020 1657825170-130ND1
Bromomethane (Methyl bromide)45 01/02/2020 1657895170-130ND1
2-Butanone (MEK)71 01/02/2020 16577010070-130ND1
Carbon disulfide 44 01/02/2020 1657885170-130ND1
Carbon tetrachloride 47 01/02/2020 1657925170-130ND1
Chlorobenzene 42 01/02/2020 1657835170-130ND1
Chloroethane 50 01/02/2020 1657985170-130ND1
Chloroform 43 01/02/2020 1657865170-130ND1
Chloromethane (Methyl chloride)47 01/02/2020 1657935160-140ND1
Cyclohexane 47 01/02/2020 1657945170-130ND1
1,2-Dibromo-3-chloropropane (DBCP)43 01/02/2020 1657865170-130ND1
Dibromochloromethane 42 01/02/2020 1657835170-130ND1
1,2-Dibromoethane (EDB)42 01/02/2020 1657835170-130ND1
1,2-Dichlorobenzene 41 01/02/2020 1657815170-130ND1
1,3-Dichlorobenzene 42 01/02/2020 1657825170-130ND1
1,4-Dichlorobenzene 42 01/02/2020 1657845170-130ND1
Dichlorodifluoromethane 55 01/02/2020 16571085160-140ND1
1,1-Dichloroethane 43 01/02/2020 1657845170-130ND1
1,2-Dichloroethane 42 01/02/2020 1657845170-130ND1
1,1-Dichloroethene 51 01/02/2020 16571015170-130ND1
cis-1,2-Dichloroethene 44 01/02/2020 1657875170-130ND1
trans-1,2-Dichloroethene 47 01/02/2020 1657945170-130ND1
1,2-Dichloropropane 40 01/02/2020 1657805170-130ND1
cis-1,3-Dichloropropene 42 01/02/2020 1657825170-130ND1
trans-1,3-Dichloropropene 44 01/02/2020 1657885170-130ND1
Ethylbenzene 43 01/02/2020 1657865170-130ND1
2-Hexanone 69 01/02/2020 1657N6810070-130ND1
Isopropylbenzene 41 01/02/2020 1657825170-130ND1
Methyl acetate 50 01/02/2020 1657995170-130ND1
Methyl tertiary butyl ether (MTBE)43 01/02/2020 1657845170-130ND1
4-Methyl-2-pentanone 84 01/02/2020 16578310070-130ND1
Methylcyclohexane 40 01/02/2020 1657805170-130ND1
Methylene chloride 43 01/02/2020 1657845170-130ND1
Styrene 42 01/02/2020 1657845170-130ND1
1,1,2,2-Tetrachloroethane 43 01/02/2020 1657855170-130ND1
Tetrachloroethene 45 01/02/2020 1657895170-130ND1
Toluene 44 01/02/2020 1657885170-130ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane 49 01/02/2020 1657965170-130ND1
1,2,4-Trichlorobenzene 34 01/02/2020 1657N665170-130ND1
1,1,1-Trichloroethane 45 01/02/2020 1657885170-130ND1
1,1,2-Trichloroethane 41 01/02/2020 1657825170-130ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 39 of 73
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:UL31060-002MS
40716 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Trichloroethene 44 01/02/2020 1657875170-130ND1
Trichlorofluoromethane 51 01/02/2020 16571015170-130ND1
Vinyl chloride 48 01/02/2020 1657945170-130ND1
Xylenes (total)86 01/02/2020 16578510070-130ND1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 100 47-138
1,2-Dichloroethane-d4 89 53-142
Toluene-d8 101 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 40 of 73
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:VQ40777-001
40777 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 01/02/2020 1602205.0 ug/L1
Benzene ND 01/02/2020 16021.0 0.40 ug/L1
Bromodichloromethane ND 01/02/2020 16021.0 0.40 ug/L1
Bromoform ND 01/02/2020 16021.0 0.40 ug/L1
Bromomethane (Methyl bromide)ND 01/02/2020 16022.0 0.40 ug/L1
2-Butanone (MEK)ND 01/02/2020 1602102.0 ug/L1
Carbon disulfide ND 01/02/2020 16021.0 0.40 ug/L1
Carbon tetrachloride ND 01/02/2020 16021.0 0.40 ug/L1
Chlorobenzene ND 01/02/2020 16021.0 0.40 ug/L1
Chloroethane ND 01/02/2020 16022.0 0.40 ug/L1
Chloroform ND 01/02/2020 16021.0 0.40 ug/L1
Chloromethane (Methyl chloride)ND 01/02/2020 16021.0 0.50 ug/L1
Cyclohexane ND 01/02/2020 16021.0 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 01/02/2020 16021.0 0.40 ug/L1
Dibromochloromethane ND 01/02/2020 16021.0 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 01/02/2020 16021.0 0.40 ug/L1
1,2-Dichlorobenzene ND 01/02/2020 16021.0 0.40 ug/L1
1,3-Dichlorobenzene ND 01/02/2020 16021.0 0.40 ug/L1
1,4-Dichlorobenzene ND 01/02/2020 16021.0 0.40 ug/L1
Dichlorodifluoromethane ND 01/02/2020 16022.0 0.60 ug/L1
1,1-Dichloroethane ND 01/02/2020 16021.0 0.40 ug/L1
1,2-Dichloroethane ND 01/02/2020 16021.0 0.40 ug/L1
1,1-Dichloroethene ND 01/02/2020 16021.0 0.40 ug/L1
cis-1,2-Dichloroethene ND 01/02/2020 16021.0 0.40 ug/L1
trans-1,2-Dichloroethene ND 01/02/2020 16021.0 0.40 ug/L1
1,2-Dichloropropane ND 01/02/2020 16021.0 0.40 ug/L1
cis-1,3-Dichloropropene ND 01/02/2020 16021.0 0.40 ug/L1
trans-1,3-Dichloropropene ND 01/02/2020 16021.0 0.40 ug/L1
Ethylbenzene ND 01/02/2020 16021.0 0.40 ug/L1
2-Hexanone ND 01/02/2020 1602102.0 ug/L1
Isopropylbenzene ND 01/02/2020 16021.0 0.40 ug/L1
Methyl acetate ND 01/02/2020 16021.0 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 01/02/2020 16021.0 0.40 ug/L1
4-Methyl-2-pentanone ND 01/02/2020 1602102.0 ug/L1
Methylcyclohexane ND 01/02/2020 16025.0 0.40 ug/L1
Methylene chloride ND 01/02/2020 16021.0 0.40 ug/L1
Styrene ND 01/02/2020 16021.0 0.41 ug/L1
1,1,2,2-Tetrachloroethane ND 01/02/2020 16021.0 0.40 ug/L1
Tetrachloroethene ND 01/02/2020 16021.0 0.40 ug/L1
Toluene ND 01/02/2020 16021.0 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 01/02/2020 16021.0 0.42 ug/L1
1,2,4-Trichlorobenzene ND 01/02/2020 16021.0 0.40 ug/L1
1,1,1-Trichloroethane ND 01/02/2020 16021.0 0.40 ug/L1
1,1,2-Trichloroethane ND 01/02/2020 16021.0 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 41 of 73
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:VQ40777-001
40777 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Trichloroethene ND 01/02/2020 16021.0 0.40 ug/L1
Trichlorofluoromethane ND 01/02/2020 16021.0 0.40 ug/L1
Vinyl chloride ND 01/02/2020 16021.0 0.40 ug/L1
Xylenes (total)ND 01/02/2020 16021.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 94 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 42 of 73
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:VQ40777-002
40777 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 92 01/02/2020 13399210060-1401
Benzene 51 01/02/2020 13391025070-1301
Bromodichloromethane 51 01/02/2020 13391025070-1301
Bromoform 51 01/02/2020 13391035070-1301
Bromomethane (Methyl bromide)55 01/02/2020 13391105070-1301
2-Butanone (MEK)98 01/02/2020 13399810070-1301
Carbon disulfide 49 01/02/2020 1339985070-1301
Carbon tetrachloride 52 01/02/2020 13391035070-1301
Chlorobenzene 49 01/02/2020 1339985070-1301
Chloroethane 56 01/02/2020 13391135070-1301
Chloroform 52 01/02/2020 13391045070-1301
Chloromethane (Methyl chloride)53 01/02/2020 13391055060-1401
Cyclohexane 52 01/02/2020 13391045070-1301
1,2-Dibromo-3-chloropropane (DBCP)46 01/02/2020 1339915070-1301
Dibromochloromethane 50 01/02/2020 13391015070-1301
1,2-Dibromoethane (EDB)50 01/02/2020 13391015070-1301
1,2-Dichlorobenzene 47 01/02/2020 1339945070-1301
1,3-Dichlorobenzene 46 01/02/2020 1339925070-1301
1,4-Dichlorobenzene 46 01/02/2020 1339925070-1301
Dichlorodifluoromethane 51 01/02/2020 13391025060-1401
1,1-Dichloroethane 50 01/02/2020 1339995070-1301
1,2-Dichloroethane 51 01/02/2020 13391025070-1301
1,1-Dichloroethene 60 01/02/2020 13391195070-1301
cis-1,2-Dichloroethene 51 01/02/2020 13391025070-1301
trans-1,2-Dichloroethene 53 01/02/2020 13391075070-1301
1,2-Dichloropropane 52 01/02/2020 13391035070-1301
cis-1,3-Dichloropropene 52 01/02/2020 13391035070-1301
trans-1,3-Dichloropropene 52 01/02/2020 13391045070-1301
Ethylbenzene 51 01/02/2020 13391015070-1301
2-Hexanone 110 01/02/2020 133910810070-1301
Isopropylbenzene 51 01/02/2020 13391015070-1301
Methyl acetate 48 01/02/2020 1339965070-1301
Methyl tertiary butyl ether (MTBE)51 01/02/2020 13391025070-1301
4-Methyl-2-pentanone 110 01/02/2020 133910610070-1301
Methylcyclohexane 55 01/02/2020 13391105070-1301
Methylene chloride 49 01/02/2020 1339985070-1301
Styrene 50 01/02/2020 13391015070-1301
1,1,2,2-Tetrachloroethane 45 01/02/2020 1339905070-1301
Tetrachloroethene 51 01/02/2020 13391035070-1301
Toluene 50 01/02/2020 13391015070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 53 01/02/2020 13391055070-1301
1,2,4-Trichlorobenzene 45 01/02/2020 1339915070-1301
1,1,1-Trichloroethane 50 01/02/2020 13391015070-1301
1,1,2-Trichloroethane 49 01/02/2020 1339985070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 43 of 73
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:VQ40777-002
40777 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Trichloroethene 53 01/02/2020 13391055070-1301
Trichlorofluoromethane 56 01/02/2020 13391115070-1301
Vinyl chloride 51 01/02/2020 13391015070-1301
Xylenes (total)100 01/02/2020 133910110070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 96 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 44 of 73
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:VQ40777-003
40777 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Acetone 110 01/02/2020 144011010060-14018 201
Benzene 48 01/02/2020 1440965070-1306.4 201
Bromodichloromethane 48 01/02/2020 1440965070-1305.4 201
Bromoform 48 01/02/2020 1440965070-1306.9 201
Bromomethane (Methyl bromide)49 01/02/2020 1440985070-13011 201
2-Butanone (MEK)100 01/02/2020 144010210070-1303.9 201
Carbon disulfide 47 01/02/2020 1440955070-1304.0 201
Carbon tetrachloride 48 01/02/2020 1440965070-1307.2 201
Chlorobenzene 47 01/02/2020 1440935070-1304.6 201
Chloroethane 50 01/02/2020 14401005070-13012 201
Chloroform 49 01/02/2020 1440995070-1304.9 201
Chloromethane (Methyl chloride)46 01/02/2020 1440925060-14013 201
Cyclohexane 47 01/02/2020 1440955070-1309.1 201
1,2-Dibromo-3-chloropropane (DBCP)45 01/02/2020 1440905070-1301.2 201
Dibromochloromethane 48 01/02/2020 1440965070-1304.6 201
1,2-Dibromoethane (EDB)48 01/02/2020 1440965070-1305.2 201
1,2-Dichlorobenzene 46 01/02/2020 1440925070-1302.0 201
1,3-Dichlorobenzene 46 01/02/2020 1440925070-1300.38 201
1,4-Dichlorobenzene 45 01/02/2020 1440915070-1301.1 201
Dichlorodifluoromethane 43 01/02/2020 1440865060-14018 201
1,1-Dichloroethane 47 01/02/2020 1440955070-1305.0 201
1,2-Dichloroethane 48 01/02/2020 1440965070-1305.8 201
1,1-Dichloroethene 56 01/02/2020 14401125070-1306.4 201
cis-1,2-Dichloroethene 49 01/02/2020 1440985070-1304.1 201
trans-1,2-Dichloroethene 51 01/02/2020 14401015070-1305.1 201
1,2-Dichloropropane 48 01/02/2020 1440965070-1307.4 201
cis-1,3-Dichloropropene 50 01/02/2020 14401005070-1303.7 201
trans-1,3-Dichloropropene 50 01/02/2020 14401005070-1303.5 201
Ethylbenzene 48 01/02/2020 1440965070-1305.6 201
2-Hexanone 100 01/02/2020 144010010070-1307.7 201
Isopropylbenzene 47 01/02/2020 1440955070-1306.2 201
Methyl acetate 45 01/02/2020 1440915070-1305.9 201
Methyl tertiary butyl ether (MTBE)49 01/02/2020 1440995070-1303.6 201
4-Methyl-2-pentanone 97 01/02/2020 14409710070-1308.7 201
Methylcyclohexane 50 01/02/2020 14401005070-1309.8 201
Methylene chloride 48 01/02/2020 1440975070-1301.4 201
Styrene 48 01/02/2020 1440965070-1304.9 201
1,1,2,2-Tetrachloroethane 44 01/02/2020 1440885070-1302.8 201
Tetrachloroethene 49 01/02/2020 1440985070-1304.9 201
Toluene 48 01/02/2020 1440965070-1304.6 201
1,1,2-Trichloro-1,2,2-Trifluoroethane 50 01/02/2020 14401015070-1304.6 201
1,2,4-Trichlorobenzene 45 01/02/2020 1440905070-1300.81 201
1,1,1-Trichloroethane 46 01/02/2020 1440925070-1309.1 201
1,1,2-Trichloroethane 46 01/02/2020 1440935070-1305.5 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 45 of 73
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:VQ40777-003
40777 5030B
Analytical Method:8260D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Trichloroethene 49 01/02/2020 1440985070-1307.6 201
Trichlorofluoromethane 45 01/02/2020 1440915070-13020 201
Vinyl chloride 43 01/02/2020 1440875070-13015 201
Xylenes (total)97 01/02/2020 14409710070-1304.8 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 105 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 97 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 46 of 73
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:VQ40737-001
40737 3520C
01/02/2020 1408Analytical Method:8270E
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acenaphthene ND 01/06/2020 17470.16 0.040 ug/L1
Acenaphthylene ND 01/06/2020 17470.16 0.040 ug/L1
Acetophenone ND 01/06/2020 17470.80 0.23 ug/L1
Anthracene ND 01/06/2020 17470.16 0.040 ug/L1
Atrazine ND 01/06/2020 17470.80 0.20 ug/L1
Benzaldehyde ND 01/06/2020 17474.0 0.27 ug/L1
Benzo(a)anthracene ND 01/06/2020 17470.16 0.040 ug/L1
Benzo(a)pyrene ND 01/06/2020 17470.16 0.040 ug/L1
Benzo(b)fluoranthene ND 01/06/2020 17470.16 0.040 ug/L1
Benzo(g,h,i)perylene ND 01/06/2020 17470.16 0.040 ug/L1
Benzo(k)fluoranthene ND 01/06/2020 17470.16 0.040 ug/L1
1,1'-Biphenyl ND 01/06/2020 17470.80 0.21 ug/L1
4-Bromophenyl phenyl ether ND 01/06/2020 17470.80 0.15 ug/L1
Butyl benzyl phthalate ND 01/06/2020 17474.0 0.21 ug/L1
Caprolactam ND 01/06/2020 17474.0 0.71 ug/L1
Carbazole ND 01/06/2020 17470.80 0.040 ug/L1
bis (2-Chloro-1-methylethyl) ether ND 01/06/2020 17470.80 0.17 ug/L1
4-Chloro-3-methyl phenol ND 01/06/2020 17470.80 0.26 ug/L1
4-Chloroaniline ND 01/06/2020 17470.80 0.13 ug/L1
bis(2-Chloroethoxy)methane ND 01/06/2020 17470.80 0.060 ug/L1
bis(2-Chloroethyl)ether ND 01/06/2020 17470.80 0.16 ug/L1
2-Chloronaphthalene ND 01/06/2020 17470.80 0.15 ug/L1
2-Chlorophenol ND 01/06/2020 17470.80 0.15 ug/L1
4-Chlorophenyl phenyl ether ND 01/06/2020 17470.80 0.16 ug/L1
Chrysene ND 01/06/2020 17470.16 0.040 ug/L1
Dibenzo(a,h)anthracene ND 01/06/2020 17470.16 0.040 ug/L1
Dibenzofuran ND 01/06/2020 17470.80 0.16 ug/L1
3,3'-Dichlorobenzidine ND 01/06/2020 17474.0 0.81 ug/L1
2,4-Dichlorophenol ND 01/06/2020 17470.80 0.19 ug/L1
Diethylphthalate ND 01/06/2020 17474.0 0.19 ug/L1
Dimethyl phthalate ND 01/06/2020 17474.0 0.18 ug/L1
2,4-Dimethylphenol ND 01/06/2020 17470.80 0.15 ug/L1
Di-n-butyl phthalate ND 01/06/2020 17474.0 0.42 ug/L1
4,6-Dinitro-2-methylphenol ND 01/06/2020 17474.0 0.89 ug/L1
2,4-Dinitrophenol ND 01/06/2020 17474.0 1.3 ug/L1
2,4-Dinitrotoluene ND 01/06/2020 17471.6 0.36 ug/L1
2,6-Dinitrotoluene ND 01/06/2020 17471.6 0.34 ug/L1
Di-n-octylphthalate ND 01/06/2020 17474.0 0.48 ug/L1
bis(2-Ethylhexyl)phthalate ND 01/06/2020 17474.0 0.38 ug/L1
Fluoranthene ND 01/06/2020 17470.16 0.040 ug/L1
Fluorene ND 01/06/2020 17470.16 0.040 ug/L1
Hexachlorobenzene ND 01/06/2020 17470.80 0.15 ug/L1
Hexachlorobutadiene ND 01/06/2020 17470.80 0.17 ug/L1
Hexachlorocyclopentadiene ND 01/06/2020 17474.0 1.1 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 47 of 73
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:VQ40737-001
40737 3520C
01/02/2020 1408Analytical Method:8270E
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Hexachloroethane ND 01/06/2020 17470.80 0.17 ug/L1
Indeno(1,2,3-c,d)pyrene ND 01/06/2020 17470.16 0.040 ug/L1
Isophorone ND 01/06/2020 17470.80 0.22 ug/L1
2-Methylnaphthalene ND 01/06/2020 17470.16 0.040 ug/L1
2-Methylphenol ND 01/06/2020 17470.80 0.21 ug/L1
3+4-Methylphenol ND 01/06/2020 17471.6 0.46 ug/L1
Naphthalene ND 01/06/2020 17470.16 0.040 ug/L1
2-Nitroaniline ND 01/06/2020 17471.6 0.66 ug/L1
3-Nitroaniline ND 01/06/2020 17471.6 0.15 ug/L1
4-Nitroaniline ND 01/06/2020 17471.6 1.3 ug/L1
Nitrobenzene ND 01/06/2020 17470.80 0.17 ug/L1
2-Nitrophenol ND 01/06/2020 17471.6 0.44 ug/L1
4-Nitrophenol ND 01/06/2020 17474.0 2.1 ug/L1
N-Nitrosodi-n-propylamine ND 01/06/2020 17470.80 0.28 ug/L1
N-Nitrosodiphenylamine (Diphenylamine)ND 01/06/2020 17470.80 0.50 ug/L1
Pentachlorophenol ND 01/06/2020 17474.0 1.3 ug/L1
Phenanthrene ND 01/06/2020 17470.16 0.040 ug/L1
Phenol ND 01/06/2020 17470.80 0.19 ug/L1
Pyrene ND 01/06/2020 17470.16 0.040 ug/L1
2,4,5-Trichlorophenol ND 01/06/2020 17470.80 0.19 ug/L1
2,4,6-Trichlorophenol ND 01/06/2020 17470.80 0.22 ug/L1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 58 37-129
2-Fluorophenol 24 24-127
Nitrobenzene-d5 63 38-127
Phenol-d5 67 28-128
Terphenyl-d14 72 10-148
2,4,6-Tribromophenol 70 35-144
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 48 of 73
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:VQ40737-002
40737 3520C
01/02/2020 1408Analytical Method:8270E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acenaphthene 4.9 01/06/2020 1658618.0 30-1221
Acenaphthylene 5.1 01/06/2020 1658648.0 30-1301
Acetophenone 5.6 01/06/2020 1658698.0 52-1251
Anthracene 5.4 01/06/2020 1658688.0 30-1231
Atrazine 6.1 01/06/2020 1658768.0 25-1211
Benzaldehyde 3.1 01/06/2020 1658398.0 20-1151
Benzo(a)anthracene 5.8 01/06/2020 1658728.0 40-1251
Benzo(a)pyrene 5.4 01/06/2020 1658688.0 40-1281
Benzo(b)fluoranthene 5.8 01/06/2020 1658728.0 30-1301
Benzo(g,h,i)perylene 5.5 01/06/2020 1658698.0 30-1301
Benzo(k)fluoranthene 5.8 01/06/2020 1658738.0 30-1301
1,1'-Biphenyl 4.7 01/06/2020 1658598.0 42-1201
4-Bromophenyl phenyl ether 5.0 01/06/2020 1658628.0 30-1241
Butyl benzyl phthalate 6.8 01/06/2020 1658858.0 54-1351
Caprolactam 5.9 01/06/2020 1658748.0 44-1521
Carbazole 5.9 01/06/2020 1658738.0 45-1011
bis (2-Chloro-1-methylethyl) ether 6.0 01/06/2020 1658758.0 42-1241
4-Chloro-3-methyl phenol 5.7 01/06/2020 1658718.0 30-1231
4-Chloroaniline 4.4 01/06/2020 1658568.0 12-1571
bis(2-Chloroethoxy)methane 5.1 01/06/2020 1658648.0 44-1271
bis(2-Chloroethyl)ether 5.5 01/06/2020 1658688.0 46-1201
2-Chloronaphthalene 4.8 01/06/2020 1658608.0 46-1001
2-Chlorophenol 5.5 01/06/2020 1658688.0 50-1171
4-Chlorophenyl phenyl ether 5.1 01/06/2020 1658648.0 30-1211
Chrysene 5.9 01/06/2020 1658748.0 30-1301
Dibenzo(a,h)anthracene 5.5 01/06/2020 1658698.0 30-1301
Dibenzofuran 5.1 01/06/2020 1658648.0 30-1181
3,3'-Dichlorobenzidine 4.0 01/06/2020 1658508.0 10-1261
2,4-Dichlorophenol 5.1 01/06/2020 1658648.0 30-1211
Diethylphthalate 5.7 01/06/2020 1658718.0 40-1251
Dimethyl phthalate 5.5 01/06/2020 1658698.0 40-1271
2,4-Dimethylphenol 6.0 01/06/2020 1658758.0 20-1251
Di-n-butyl phthalate 6.0 01/06/2020 1658768.0 40-1271
4,6-Dinitro-2-methylphenol 5.0 01/06/2020 1658628.0 56-1281
2,4-Dinitrophenol 6.6 01/06/2020 1658411611-1261
2,4-Dinitrotoluene 5.7 01/06/2020 1658718.0 59-1271
2,6-Dinitrotoluene 5.5 01/06/2020 1658698.0 59-1261
Di-n-octylphthalate 5.5 01/06/2020 1658698.0 50-1361
bis(2-Ethylhexyl)phthalate 5.9 01/06/2020 1658748.0 56-1281
Fluoranthene 5.6 01/06/2020 1658708.0 40-1281
Fluorene 5.2 01/06/2020 1658658.0 30-1241
Hexachlorobenzene 5.3 01/06/2020 1658668.0 30-1251
Hexachlorobutadiene 3.9 01/06/2020 1658498.0 24-1101
Hexachlorocyclopentadiene 15 01/06/2020 1658394016-961
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 49 of 73
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:VQ40737-002
40737 3520C
01/02/2020 1408Analytical Method:8270E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Hexachloroethane 3.7 01/06/2020 1658468.0 31-1101
Indeno(1,2,3-c,d)pyrene 5.4 01/06/2020 1658688.0 30-1301
Isophorone 5.5 01/06/2020 1658698.0 57-1231
2-Methylnaphthalene 4.7 01/06/2020 1658588.0 40-1321
2-Methylphenol 6.5 01/06/2020 1658818.0 56-1191
3+4-Methylphenol 7.2 01/06/2020 1658908.0 53-1191
Naphthalene 4.6 01/06/2020 1658578.0 30-1301
2-Nitroaniline 5.8 01/06/2020 1658738.0 60-1241
3-Nitroaniline 4.7 01/06/2020 1658588.0 43-1231
4-Nitroaniline 5.3 01/06/2020 1658668.0 30-1351
Nitrobenzene 5.1 01/06/2020 1658648.0 51-1221
2-Nitrophenol 4.9 01/06/2020 1658628.0 51-1181
4-Nitrophenol 12 01/06/2020 1658731653-1301
N-Nitrosodi-n-propylamine 5.9 01/06/2020 1658738.0 54-1271
N-Nitrosodiphenylamine (Diphenylamine)5.7 01/06/2020 1658718.0 30-1231
Pentachlorophenol 8.1 01/06/2020 1658511642-1311
Phenanthrene 5.3 01/06/2020 1658668.0 40-1231
Phenol 6.0 01/06/2020 1658758.0 49-1171
Pyrene 6.3 01/06/2020 1658798.0 40-1261
2,4,5-Trichlorophenol 5.1 01/06/2020 1658648.0 30-1231
2,4,6-Trichlorophenol 5.2 01/06/2020 1658658.0 30-1251
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 58 37-129
2-Fluorophenol 56 24-127
Nitrobenzene-d5 62 38-127
Phenol-d5 71 28-128
Terphenyl-d14 82 10-148
2,4,6-Tribromophenol 69 35-144
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 50 of 73
Semivolatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-006MS
40737 3520C
01/02/2020 1408Analytical Method:8270E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Acenaphthene 9.6 01/06/2020 2354601630-122ND1
Acenaphthylene 9.8 01/06/2020 2354621630-130ND1
Acetophenone 11 01/06/2020 2354681652-125ND1
Anthracene 9.5 01/06/2020 2354591630-123ND1
Atrazine 11 01/06/2020 2354661625-121ND1
Benzaldehyde 9.1 01/06/2020 2354571620-115ND1
Benzo(a)anthracene 10 01/06/2020 2354641640-125ND1
Benzo(a)pyrene 9.6 01/06/2020 2354601640-128ND1
Benzo(b)fluoranthene 11 01/06/2020 2354691630-130ND1
Benzo(g,h,i)perylene 5.1 01/06/2020 2354321630-130ND1
Benzo(k)fluoranthene 11 01/06/2020 2354681630-130ND1
1,1'-Biphenyl 9.7 01/06/2020 2354601642-120ND1
4-Bromophenyl phenyl ether 9.0 01/06/2020 2354561630-124ND1
Butyl benzyl phthalate 11 01/06/2020 2354701654-135ND1
Caprolactam 13 01/06/2020 2354791644-152ND1
Carbazole 11 01/06/2020 2354681645-101ND1
bis (2-Chloro-1-methylethyl) ether 12 01/06/2020 2354741642-124ND1
4-Chloro-3-methyl phenol 11 01/06/2020 2354661630-123ND1
4-Chloroaniline 4.4 01/06/2020 2354N271630-130ND1
bis(2-Chloroethoxy)methane 10 01/06/2020 2354631644-127ND1
bis(2-Chloroethyl)ether 11 01/06/2020 2354671646-120ND1
2-Chloronaphthalene 9.5 01/06/2020 2354591646-100ND1
2-Chlorophenol 11 01/06/2020 2354661650-117ND1
4-Chlorophenyl phenyl ether 9.6 01/06/2020 2354601630-121ND1
Chrysene 10 01/06/2020 2354661630-130ND1
Dibenzo(a,h)anthracene 6.1 01/06/2020 2354381630-130ND1
Dibenzofuran 9.8 01/06/2020 2354611630-118ND1
3,3'-Dichlorobenzidine ND 01/06/2020 2354N0.0016 10-126ND1
2,4-Dichlorophenol 10 01/06/2020 2354651630-121ND1
Diethylphthalate 11 01/06/2020 2354701640-125ND1
Dimethyl phthalate 11 01/06/2020 2354681640-127ND1
2,4-Dimethylphenol 15 01/06/2020 2354921620-125ND1
Di-n-butyl phthalate 12 01/06/2020 2354731640-127ND1
4,6-Dinitro-2-methylphenol 8.5 01/06/2020 2354N531656-128ND1
2,4-Dinitrophenol 14 01/06/2020 2354433230-130ND1
2,4-Dinitrotoluene 11 01/06/2020 2354691659-127ND1
2,6-Dinitrotoluene 11 01/06/2020 2354681659-126ND1
Di-n-octylphthalate 11 01/06/2020 2354671650-136ND1
bis(2-Ethylhexyl)phthalate 9.4 01/06/2020 2354591656-128ND1
Fluoranthene 11 01/06/2020 2354701640-128ND1
Fluorene 9.9 01/06/2020 2354621630-124ND1
Hexachlorobenzene 9.1 01/06/2020 2354571630-125ND1
Hexachlorobutadiene 7.7 01/06/2020 2354481630-130ND1
Hexachlorocyclopentadiene 18 01/06/2020 2354238016-96ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 51 of 73
Semivolatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-006MS
40737 3520C
01/02/2020 1408Analytical Method:8270E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Hexachloroethane 8.1 01/06/2020 2354511631-110ND1
Indeno(1,2,3-c,d)pyrene 5.8 01/06/2020 2354371630-130ND1
Isophorone 11 01/06/2020 2354691657-123ND1
2-Methylnaphthalene 8.7 01/06/2020 2354551640-132ND1
2-Methylphenol 11 01/06/2020 2354701656-119ND1
3+4-Methylphenol 15 01/06/2020 2354841653-1191.9 1
Naphthalene 8.9 01/06/2020 2354551630-130ND1
2-Nitroaniline 11 01/06/2020 2354691660-124ND1
3-Nitroaniline 5.4 01/06/2020 2354N341643-123ND1
4-Nitroaniline 9.2 01/06/2020 2354581630-135ND1
Nitrobenzene 11 01/06/2020 2354681651-122ND1
2-Nitrophenol 9.9 01/06/2020 2354621651-118ND1
4-Nitrophenol 27 01/06/2020 2354853253-130ND1
N-Nitrosodi-n-propylamine 11 01/06/2020 2354711654-127ND1
N-Nitrosodiphenylamine (Diphenylamine)10 01/06/2020 2354641630-123ND1
Pentachlorophenol 19 01/06/2020 2354583242-131ND1
Phenanthrene 9.4 01/06/2020 2354591640-123ND1
Phenol 12 01/06/2020 2354741649-117ND1
Pyrene 9.7 01/06/2020 2354601640-126ND1
2,4,5-Trichlorophenol 11 01/06/2020 2354671630-123ND1
2,4,6-Trichlorophenol 10 01/06/2020 2354641630-125ND1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 58 37-129
2-Fluorophenol 60 24-127
Nitrobenzene-d5 64 38-127
Phenol-d5 66 28-128
Terphenyl-d14 60 10-148
2,4,6-Tribromophenol 65 35-144
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 52 of 73
Semivolatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-006MD
40737 3520C
01/02/2020 1408Analytical Method:8270E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Acenaphthene 9.1 01/07/2020 0019571630-1225.5 40ND1
Acenaphthylene 9.4 01/07/2020 0019591630-1304.9 40ND1
Acetophenone 11 01/07/2020 0019681652-1250.020 40ND1
Anthracene 9.2 01/07/2020 0019571630-1232.7 40ND1
Atrazine 10 01/07/2020 0019641625-1212.4 40ND1
Benzaldehyde 8.9 01/07/2020 0019561620-1152.1 40ND1
Benzo(a)anthracene 9.9 01/07/2020 0019621640-1253.1 40ND1
Benzo(a)pyrene 8.5 01/07/2020 0019531640-12812 40ND1
Benzo(b)fluoranthene 9.9 01/07/2020 0019621630-13010 40ND1
Benzo(g,h,i)perylene 4.0 01/07/2020 0019N251630-13023 40ND1
Benzo(k)fluoranthene 10 01/07/2020 0019631630-1307.0 40ND1
1,1'-Biphenyl 9.0 01/07/2020 0019561642-1207.6 40ND1
4-Bromophenyl phenyl ether 8.7 01/07/2020 0019541630-1243.3 40ND1
Butyl benzyl phthalate 11 01/07/2020 0019691654-1352.1 40ND1
Caprolactam 11 01/07/2020 0019721644-15210 40ND1
Carbazole 11 01/07/2020 0019661645-1013.0 40ND1
bis (2-Chloro-1-methylethyl) ether 12 01/07/2020 0019751642-1240.63 40ND1
4-Chloro-3-methyl phenol 10 01/07/2020 0019641630-1234.0 40ND1
4-Chloroaniline 5.2 01/07/2020 0019321630-13017 40ND1
bis(2-Chloroethoxy)methane 9.6 01/07/2020 0019601644-1274.8 40ND1
bis(2-Chloroethyl)ether 12 01/07/2020 0019751646-12011 40ND1
2-Chloronaphthalene 9.1 01/07/2020 0019571646-1004.2 40ND1
2-Chlorophenol 12 01/07/2020 0019741650-11712 40ND1
4-Chlorophenyl phenyl ether 9.2 01/07/2020 0019571630-1214.1 40ND1
Chrysene 9.9 01/07/2020 0019621630-1306.1 40ND1
Dibenzo(a,h)anthracene 4.7 01/07/2020 0019N291630-13027 40ND1
Dibenzofuran 9.5 01/07/2020 0019591630-1183.5 40ND1
3,3'-Dichlorobenzidine ND 01/07/2020 0019N0.0016 10-1260.00 40ND1
2,4-Dichlorophenol 9.7 01/07/2020 0019611630-1217.1 40ND1
Diethylphthalate 11 01/07/2020 0019681640-1252.0 40ND1
Dimethyl phthalate 10 01/07/2020 0019641640-1275.7 40ND1
2,4-Dimethylphenol 12 01/07/2020 0019781620-12517 40ND1
Di-n-butyl phthalate 11 01/07/2020 0019661640-1279.3 40ND1
4,6-Dinitro-2-methylphenol 8.1 01/07/2020 0019N511656-1284.5 40ND1
2,4-Dinitrophenol 13 01/07/2020 0019403230-1306.7 40ND1
2,4-Dinitrotoluene 11 01/07/2020 0019671659-1272.0 40ND1
2,6-Dinitrotoluene 9.8 01/07/2020 0019611659-12610 40ND1
Di-n-octylphthalate 6.3 01/07/2020 0019N,[phone]ND1
bis(2-Ethylhexyl)phthalate 5.7 01/07/2020 0019N,[phone]ND1
Fluoranthene 10 01/07/2020 0019631640-1289.8 40ND1
Fluorene 9.3 01/07/2020 0019581630-1246.1 40ND1
Hexachlorobenzene 8.9 01/07/2020 0019551630-1252.7 40ND1
Hexachlorobutadiene 7.1 01/07/2020 0019441630-1307.7 40ND1
Hexachlorocyclopentadiene 15 01/07/2020 0019198016-9619 40ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 53 of 73
Semivolatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-006MD
40737 3520C
01/02/2020 1408Analytical Method:8270E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Hexachloroethane 7.2 01/07/2020 0019451631-11012 40ND1
Indeno(1,2,3-c,d)pyrene 4.6 01/07/2020 0019N291630-13025 40ND1
Isophorone 11 01/07/2020 0019671657-1233.6 40ND1
2-Methylnaphthalene 8.5 01/07/2020 0019531640-1323.1 40ND1
2-Methylphenol 11 01/07/2020 0019691656-1191.8 40ND1
3+4-Methylphenol 14 01/07/2020 0019781653-1196.8 401.9 1
Naphthalene 8.5 01/07/2020 0019531630-1304.3 40ND1
2-Nitroaniline 10 01/07/2020 0019631660-1247.8 40ND1
3-Nitroaniline 6.5 01/07/2020 0019N411643-12319 40ND1
4-Nitroaniline 9.6 01/07/2020 0019601630-1353.5 40ND1
Nitrobenzene 10 01/07/2020 0019621651-1228.8 40ND1
2-Nitrophenol 9.2 01/07/2020 0019571651-1187.6 40ND1
4-Nitrophenol 25 01/07/2020 0019793253-1306.7 40ND1
N-Nitrosodi-n-propylamine 12 01/07/2020 0019721654-1271.5 40ND1
N-Nitrosodiphenylamine (Diphenylamine)8.3 01/07/2020 0019521630-12320 40ND1
Pentachlorophenol 19 01/07/2020 0019583242-1310.27 40ND1
Phenanthrene 9.3 01/07/2020 0019581640-1232.1 40ND1
Phenol 13 01/07/2020 0019841649-11712 40ND1
Pyrene 9.7 01/07/2020 0019611640-1260.73 40ND1
2,4,5-Trichlorophenol 10 01/07/2020 0019641630-1234.7 40ND1
2,4,6-Trichlorophenol 9.5 01/07/2020 0019591630-1258.3 40ND1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 54 37-129
2-Fluorophenol 64 24-127
Nitrobenzene-d5 58 38-127
Phenol-d5 75 28-128
Terphenyl-d14 32 10-148
2,4,6-Tribromophenol 63 35-144
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 54 of 73
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:VQ40761-001
40761 3546
01/02/2020 1850Analytical Method:8270E
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Acenaphthene ND 01/03/2020 12082.7 0.83 ug/kg1
Acenaphthylene ND 01/03/2020 12082.7 0.95 ug/kg1
Acetophenone ND 01/03/2020 1208135.0 ug/kg1
Anthracene ND 01/03/2020 12082.7 0.51 ug/kg1
Atrazine ND 01/03/2020 1208135.0 ug/kg1
Benzaldehyde ND 01/03/2020 1208135.0 ug/kg1
Benzo(a)anthracene ND 01/03/2020 12082.7 0.59 ug/kg1
Benzo(a)pyrene ND 01/03/2020 12082.7 0.66 ug/kg1
Benzo(b)fluoranthene ND 01/03/2020 12082.7 0.50 ug/kg1
Benzo(g,h,i)perylene ND 01/03/2020 12082.7 0.65 ug/kg1
Benzo(k)fluoranthene ND 01/03/2020 12082.7 0.48 ug/kg1
1,1'-Biphenyl ND 01/03/2020 1208135.0 ug/kg1
4-Bromophenyl phenyl ether ND 01/03/2020 1208135.0 ug/kg1
Butyl benzyl phthalate ND 01/03/2020 1208135.0 ug/kg1
Caprolactam ND 01/03/2020 1208135.0 ug/kg1
Carbazole ND 01/03/2020 1208135.0 ug/kg1
bis (2-Chloro-1-methylethyl) ether ND 01/03/2020 1208135.0 ug/kg1
4-Chloro-3-methyl phenol ND 01/03/2020 1208135.0 ug/kg1
4-Chloroaniline ND 01/03/2020 1208135.0 ug/kg1
bis(2-Chloroethoxy)methane ND 01/03/2020 1208135.0 ug/kg1
bis(2-Chloroethyl)ether ND 01/03/2020 1208135.0 ug/kg1
2-Chloronaphthalene ND 01/03/2020 1208135.0 ug/kg1
2-Chlorophenol ND 01/03/2020 1208135.0 ug/kg1
4-Chlorophenyl phenyl ether ND 01/03/2020 1208135.0 ug/kg1
Chrysene ND 01/03/2020 12082.7 0.45 ug/kg1
Dibenzo(a,h)anthracene ND 01/03/2020 12082.7 0.51 ug/kg1
Dibenzofuran ND 01/03/2020 1208135.0 ug/kg1
3,3'-Dichlorobenzidine ND 01/03/2020 1208135.0 ug/kg1
2,4-Dichlorophenol ND 01/03/2020 1208135.0 ug/kg1
Diethylphthalate ND 01/03/2020 1208135.0 ug/kg1
Dimethyl phthalate ND 01/03/2020 1208137.4 ug/kg1
2,4-Dimethylphenol ND 01/03/2020 1208135.0 ug/kg1
Di-n-butyl phthalate ND 01/03/2020 1208135.0 ug/kg1
4,6-Dinitro-2-methylphenol ND 01/03/2020 12086725ug/kg1
2,4-Dinitrophenol ND 01/03/2020 12086725ug/kg1
2,4-Dinitrotoluene ND 01/03/2020 12082710ug/kg1
2,6-Dinitrotoluene ND 01/03/2020 12082710ug/kg1
Di-n-octylphthalate ND 01/03/2020 1208135.0 ug/kg1
bis(2-Ethylhexyl)phthalate ND 01/03/2020 12086725ug/kg1
Fluoranthene ND 01/03/2020 12082.7 0.42 ug/kg1
Fluorene ND 01/03/2020 12082.7 0.57 ug/kg1
Hexachlorobenzene ND 01/03/2020 1208135.0 ug/kg1
Hexachlorobutadiene ND 01/03/2020 1208135.0 ug/kg1
Hexachlorocyclopentadiene ND 01/03/2020 12086725ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 55 of 73
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:VQ40761-001
40761 3546
01/02/2020 1850Analytical Method:8270E
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexachloroethane ND 01/03/2020 1208135.0 ug/kg1
Indeno(1,2,3-c,d)pyrene ND 01/03/2020 12082.7 1.0 ug/kg1
Isophorone ND 01/03/2020 1208135.0 ug/kg1
2-Methylnaphthalene ND 01/03/2020 12082.7 0.99 ug/kg1
2-Methylphenol ND 01/03/2020 1208135.0 ug/kg1
3+4-Methylphenol ND 01/03/2020 12082710ug/kg1
Naphthalene ND 01/03/2020 12082.7 0.97 ug/kg1
2-Nitroaniline ND 01/03/2020 12082710ug/kg1
3-Nitroaniline ND 01/03/2020 12082710ug/kg1
4-Nitroaniline ND 01/03/2020 12082710ug/kg1
Nitrobenzene ND 01/03/2020 1208135.0 ug/kg1
2-Nitrophenol ND 01/03/2020 12082710ug/kg1
4-Nitrophenol ND 01/03/2020 12086725ug/kg1
N-Nitrosodi-n-propylamine ND 01/03/2020 1208135.0 ug/kg1
N-Nitrosodiphenylamine (Diphenylamine)ND 01/03/2020 1208135.0 ug/kg1
Pentachlorophenol ND 01/03/2020 12086725ug/kg1
Phenanthrene ND 01/03/2020 12082.7 0.72 ug/kg1
Phenol ND 01/03/2020 1208135.0 ug/kg1
Pyrene ND 01/03/2020 12082.7 0.50 ug/kg1
Pyridine ND 01/03/2020 1208135.0 ug/kg1
2,4,5-Trichlorophenol ND 01/03/2020 1208135.0 ug/kg1
2,4,6-Trichlorophenol ND 01/03/2020 1208135.0 ug/kg1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 61 33-102
2-Fluorophenol 57 35-115
Nitrobenzene-d5 64 22-109
Phenol-d5 64 33-122
Terphenyl-d14 58 41-120
2,4,6-Tribromophenol 56 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 56 of 73
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:VQ40761-002
40761 3546
01/02/2020 1850Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acenaphthene 89 01/03/2020 12326713012-1111
Acenaphthylene 89 01/03/2020 12326713044-1221
Acetophenone 79 01/03/2020 12325913048-1111
Anthracene 94 01/03/2020 12327013016-1221
Atrazine 89 01/03/2020 12326713048-1161
Benzaldehyde 41 01/03/2020 12323113010-1101
Benzo(a)anthracene 90 01/03/2020 12326813040-1211
Benzo(a)pyrene 92 01/03/2020 12326913036-1141
Benzo(b)fluoranthene 92 01/03/2020 12326913038-1231
Benzo(g,h,i)perylene 98 01/03/2020 12327413043-1201
Benzo(k)fluoranthene 88 01/03/2020 12326613040-1261
1,1'-Biphenyl 88 01/03/2020 12326713049-1101
4-Bromophenyl phenyl ether 86 01/03/2020 12326413046-1181
Butyl benzyl phthalate 96 01/03/2020 12327213046-1281
Caprolactam 98 01/03/2020 12327413043-1211
Carbazole 100 01/03/2020 12327613047-1281
bis (2-Chloro-1-methylethyl) ether 87 01/03/2020 12326513031-1021
4-Chloro-3-methyl phenol 87 01/03/2020 12326613049-1181
4-Chloroaniline 18 01/03/2020 1232N1413017-1061
bis(2-Chloroethoxy)methane 87 01/03/2020 12326513039-1081
bis(2-Chloroethyl)ether 87 01/03/2020 12326613032-1051
2-Chloronaphthalene 87 01/03/2020 12326613031-1271
2-Chlorophenol 90 01/03/2020 12326813037-1061
4-Chlorophenyl phenyl ether 92 01/03/2020 12326913047-1161
Chrysene 93 01/03/2020 12327013041-1241
Dibenzo(a,h)anthracene 96 01/03/2020 12327213038-1251
Dibenzofuran 91 01/03/2020 12326913045-1121
3,3'-Dichlorobenzidine 74 01/03/2020 12325513010-1191
2,4-Dichlorophenol 87 01/03/2020 12326513041-1131
Diethylphthalate 96 01/03/2020 12327213049-1231
Dimethyl phthalate 91 01/03/2020 12326913048-1201
2,4-Dimethylphenol 120 01/03/2020 12329013033-1231
Di-n-butyl phthalate 99 01/03/2020 12327513051-1291
4,6-Dinitro-2-methylphenol 99 01/03/2020 12327413040-1301
2,4-Dinitrophenol 200 01/03/2020 12327627032-1151
2,4-Dinitrotoluene 100 01/03/2020 12327513048-1241
2,6-Dinitrotoluene 100 01/03/2020 12327713047-1251
Di-n-octylphthalate 100 01/03/2020 12327613049-1421
bis(2-Ethylhexyl)phthalate 100 01/03/2020 12327713045-1281
Fluoranthene 70 01/03/2020 12325313026-1331
Fluorene 92 01/03/2020 12326913019-1081
Hexachlorobenzene 86 01/03/2020 12326413044-1221
Hexachlorobutadiene 78 01/03/2020 12325913033-1031
Hexachlorocyclopentadiene 400 01/03/2020 12326067018-1211
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 57 of 73
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:VQ40761-002
40761 3546
01/02/2020 1850Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Hexachloroethane 81 01/03/2020 12326113030-961
Indeno(1,2,3-c,d)pyrene 96 01/03/2020 12327213042-1231
Isophorone 89 01/03/2020 12326713041-1131
2-Methylnaphthalene 82 01/03/2020 12326213010-1071
2-Methylphenol 89 01/03/2020 12326713032-1071
3+4-Methylphenol 130 01/03/2020 12329813039-1081
Naphthalene 81 01/03/2020 12326113010-1121
2-Nitroaniline 100 01/03/2020 12327613045-1231
3-Nitroaniline 62 01/03/2020 12324613024-1271
4-Nitroaniline 94 01/03/2020 12327113048-1271
Nitrobenzene 89 01/03/2020 12326713033-1141
2-Nitrophenol 97 01/03/2020 12327313035-1081
4-Nitrophenol 210 01/03/2020 12327827018-1541
N-Nitrosodi-n-propylamine 100 01/03/2020 12327713032-1151
N-Nitrosodiphenylamine (Diphenylamine)93 01/03/2020 12327013053-1501
Pentachlorophenol 200 01/03/2020 12327627027-1381
Phenanthrene 90 01/03/2020 12326813016-1231
Phenol 100 01/03/2020 12327613036-1081
Pyrene 94 01/03/2020 12327013034-1211
Pyridine 74 01/03/2020 12325513030-1301
2,4,5-Trichlorophenol 93 01/03/2020 12327013046-1221
2,4,6-Trichlorophenol 89 01/03/2020 12326713038-1151
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 64 33-102
2-Fluorophenol 62 35-115
Nitrobenzene-d5 69 22-109
Phenol-d5 68 33-122
Terphenyl-d14 77 41-120
2,4,6-Tribromophenol 69 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 58 of 73
Semivolatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-003MS
40761 3546
01/02/2020 1850Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acenaphthene 68 01/06/2020 21524615012-111ND20
Acenaphthylene 75 01/06/2020 21525115044-122ND20
Acetophenone ND 01/06/2020 2152N0.00150 30-130ND20
Anthracene 86 01/06/2020 21525815016-122ND20
Atrazine ND 01/06/2020 2152N0.00150 30-130ND20
Benzaldehyde 190 01/06/2020 2152N13015010-110ND20
Benzo(a)anthracene 150 01/06/2020 21524415040-1218620
Benzo(a)pyrene 150 01/06/2020 2152N3415036-11410020
Benzo(b)fluoranthene 170 01/06/2020 2152N2215038-12314020
Benzo(g,h,i)perylene 65 01/06/2020 2152N1515043-1204320
Benzo(k)fluoranthene 120 01/06/2020 21525415040-1264120
1,1'-Biphenyl ND 01/06/2020 2152N0.00150 30-130ND20
4-Bromophenyl phenyl ether 68 01/06/2020 21524615030-130ND20
Butyl benzyl phthalate 95 01/06/2020 21526415030-130ND20
Caprolactam ND 01/06/2020 2152N0.00150 30-130ND20
Carbazole 86 01/06/2020 21525815030-130ND20
bis (2-Chloro-1-methylethyl) ether 86 01/06/2020 21525815030-130ND20
4-Chloro-3-methyl phenol ND 01/06/2020 2152N0.00150 30-130ND20
4-Chloroaniline ND 01/06/2020 2152N0.00150 17-106ND20
bis(2-Chloroethoxy)methane ND 01/06/2020 2152N0.00150 30-130ND20
bis(2-Chloroethyl)ether 75 01/06/2020 21525115030-130ND20
2-Chloronaphthalene ND 01/06/2020 2152N0.00150 30-130ND20
2-Chlorophenol ND 01/06/2020 2152N0.00150 30-130ND20
4-Chlorophenyl phenyl ether ND 01/06/2020 2152N0.00150 30-130ND20
Chrysene 140 01/06/2020 21524715041-1246720
Dibenzo(a,h)anthracene 53 01/06/2020 2152N3615038-125ND20
Dibenzofuran 75 01/06/2020 21525015030-130ND20
3,3'-Dichlorobenzidine ND 01/06/2020 2152N0.00150 10-119ND20
2,4-Dichlorophenol ND 01/06/2020 2152N0.00150 30-130ND20
Diethylphthalate ND 01/06/2020 2152N0.00150 30-130ND20
Dimethyl phthalate 76 01/06/2020 21525115030-130ND20
2,4-Dimethylphenol 82 01/06/2020 21525515030-130ND20
Di-n-butyl phthalate 82 01/06/2020 21525515030-130ND20
4,6-Dinitro-2-methylphenol ND 01/06/2020 2152N0.00150 30-130ND20
2,4-Dinitrophenol 620 01/06/2020 2152N20830030-130ND20
2,4-Dinitrotoluene ND 01/06/2020 2152N0.00150 30-130ND20
2,6-Dinitrotoluene 2600 01/06/2020 2152N177015030-130ND20
Di-n-octylphthalate ND 01/06/2020 2152N0.00150 30-130ND20
bis(2-Ethylhexyl)phthalate ND 01/06/2020 2152N0.00150 30-130ND20
Fluoranthene 170 01/06/2020 2152N1415026-13315020
Fluorene 70 01/06/2020 21524715019-108ND20
Hexachlorobenzene 59 01/06/2020 21524015030-130ND20
Hexachlorobutadiene ND 01/06/2020 2152N0.00150 30-130ND20
Hexachlorocyclopentadiene ND 01/06/2020 2152N0.00740 30-130ND20
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 59 of 73
Semivolatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-003MS
40761 3546
01/02/2020 1850Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Hexachloroethane ND 01/06/2020 2152N0.00150 30-130ND20
Indeno(1,2,3-c,d)pyrene 71 01/06/2020 2152N1915042-1234220
Isophorone 81 01/06/2020 21525515030-130ND20
2-Methylnaphthalene 96 01/06/2020 21524215010-1073420
2-Methylphenol ND 01/06/2020 2152N0.00150 30-130ND20
3+4-Methylphenol ND 01/06/2020 2152N0.00150 30-130ND20
Naphthalene 91 01/06/2020 21523915010-1123320
2-Nitroaniline ND 01/06/2020 2152N0.00150 30-130ND20
3-Nitroaniline ND 01/06/2020 2152N0.00150 30-130ND20
4-Nitroaniline ND 01/06/2020 2152N0.00150 30-130ND20
Nitrobenzene 90 01/06/2020 21526115030-130ND20
2-Nitrophenol ND 01/06/2020 2152N0.00150 30-130ND20
4-Nitrophenol ND 01/06/2020 2152N0.00300 30-130ND20
N-Nitrosodi-n-propylamine 85 01/06/2020 21525715030-130ND20
N-Nitrosodiphenylamine (Diphenylamine)ND 01/06/2020 2152N0.00150 30-130ND20
Pentachlorophenol 630 01/06/2020 2152N21330030-130ND20
Phenanthrene 130 01/06/2020 21522715016-1238620
Phenol 86 01/06/2020 21525815030-130ND20
Pyrene 150 01/06/2020 2152N2615034-12111020
Pyridine ND 01/06/2020 2152N0.00150 30-130ND20
2,4,5-Trichlorophenol 180 01/06/2020 215212215030-130ND20
2,4,6-Trichlorophenol ND 01/06/2020 2152N0.00150 30-130ND20
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 46 33-102
2-Fluorophenol 44 35-115
Nitrobenzene-d5 55 22-109
Phenol-d5 50 33-122
Terphenyl-d14 48 41-120
2,4,6-Tribromophenol 32 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 60 of 73
Semivolatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-003MD
40761 3546
01/02/2020 1850Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acenaphthene 96 01/06/2020 2217+63150 12-11134 30ND20
Acenaphthylene 110 01/06/2020 2217+70150 44-12235 30ND20
Acetophenone 90 01/06/2020 2217+59150 30-130200 40ND20
Anthracene 110 01/06/2020 22177515016-12228 30ND20
Atrazine 100 01/06/2020 2217+67150 30-130200 40ND20
Benzaldehyde 190 01/06/2020 2217N12515010-1101.0 40ND20
Benzo(a)anthracene 170 01/06/2020 22175815040-12114 308620
Benzo(a)pyrene 190 01/06/2020 22175515036-11420 3010020
Benzo(b)fluoranthene 220 01/06/2020 22175115038-12323 3014020
Benzo(g,h,i)perylene 92 01/06/2020 2217N,[phone] 304320
Benzo(k)fluoranthene 170 01/06/2020 2217+85150 40-12634 304120
1,1'-Biphenyl 93 01/06/2020 2217+61150 30-130200 40ND20
4-Bromophenyl phenyl ether 91 01/06/2020 22176015030-13029 40ND20
Butyl benzyl phthalate 130 01/06/2020 22178715030-13033 40ND20
Caprolactam 90 01/06/2020 2217+59150 30-130200 40ND20
Carbazole 110 01/06/2020 22177515030-13028 40ND20
bis (2-Chloro-1-methylethyl) ether 120 01/06/2020 22177615030-13030 40ND20
4-Chloro-3-methyl phenol 95 01/06/2020 2217+62150 30-130200 40ND20
4-Chloroaniline ND 01/06/2020 2217N0.00150 17-1060.00 40ND20
bis(2-Chloroethoxy)methane 100 01/06/2020 2217+68150 30-130200 40ND20
bis(2-Chloroethyl)ether 97 01/06/2020 22176415030-13025 40ND20
2-Chloronaphthalene 94 01/06/2020 2217+62150 30-130200 40ND20
2-Chlorophenol 97 01/06/2020 2217+64150 30-130200 40ND20
4-Chlorophenyl phenyl ether 95 01/06/2020 2217+62150 30-130200 40ND20
Chrysene 160 01/06/2020 22176315041-12418 306720
Dibenzo(a,h)anthracene 77 01/06/2020 2217+51150 38-12538 30ND20
Dibenzofuran 100 01/06/2020 22176915030-13033 40ND20
3,3'-Dichlorobenzidine ND 01/06/2020 2217N0.00150 10-1190.00 40ND20
2,4-Dichlorophenol 100 01/06/2020 2217+68150 30-130200 40ND20
Diethylphthalate 100 01/06/2020 2217+67150 30-130200 40ND20
Dimethyl phthalate 100 01/06/2020 22176815030-13030 40ND20
2,4-Dimethylphenol 130 01/06/2020 2217+83150 30-13043 40ND20
Di-n-butyl phthalate 110 01/06/2020 22177415030-13031 40ND20
4,6-Dinitro-2-methylphenol 430 01/06/2020 2217N,[phone] 40ND20
2,4-Dinitrophenol ND 01/06/2020 2217N,+0.00300 30-130200 40ND20
2,4-Dinitrotoluene ND 01/06/2020 2217N0.00150 30-1300.00 40ND20
2,6-Dinitrotoluene 91 01/06/2020 2217+60150 30-130190 40ND20
Di-n-octylphthalate ND 01/06/2020 2217N0.00150 30-1300.00 40ND20
bis(2-Ethylhexyl)phthalate ND 01/06/2020 2217N0.00150 30-1300.00 40ND20
Fluoranthene 190 01/06/2020 22172815026-13312 3015020
Fluorene 98 01/06/2020 2217+65150 19-10834 30ND20
Hexachlorobenzene 87 01/06/2020 22175715030-13038 40ND20
Hexachlorobutadiene 84 01/06/2020 2217+56150 30-130200 40ND20
Hexachlorocyclopentadiene ND 01/06/2020 2217N0.00760 30-1300.00 40ND20
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 61 of 73
Semivolatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-003MD
40761 3546
01/02/2020 1850Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Hexachloroethane 91 01/06/2020 2217+60150 30-130200 40ND20
Indeno(1,2,3-c,d)pyrene 100 01/06/2020 2217N,[phone] 304220
Isophorone 100 01/06/2020 22176615030-13022 40ND20
2-Methylnaphthalene 120 01/06/2020 22175415010-10720 303420
2-Methylphenol 81 01/06/2020 2217+54150 30-130200 40ND20
3+4-Methylphenol 110 01/06/2020 2217+71150 30-130200 40ND20
Naphthalene 120 01/06/2020 22175615010-11227 303320
2-Nitroaniline ND 01/06/2020 2217N0.00150 30-1300.00 40ND20
3-Nitroaniline ND 01/06/2020 2217N0.00150 30-1300.00 40ND20
4-Nitroaniline ND 01/06/2020 2217N0.00150 30-1300.00 40ND20
Nitrobenzene 110 01/06/2020 22177115030-13018 40ND20
2-Nitrophenol ND 01/06/2020 2217N0.00150 30-1300.00 40ND20
4-Nitrophenol ND 01/06/2020 2217N0.00300 30-1300.00 40ND20
N-Nitrosodi-n-propylamine 100 01/06/2020 22176815030-13019 40ND20
N-Nitrosodiphenylamine (Diphenylamine)100 01/06/2020 2217+67150 30-130200 40ND20
Pentachlorophenol 660 01/06/2020 2217N21730030-1304.7 40ND20
Phenanthrene 150 01/06/2020 22174315016-12318 308620
Phenol 100 01/06/2020 22176915030-13020 40ND20
Pyrene 170 01/06/2020 22174215034-12116 3011020
Pyridine ND 01/06/2020 2217N0.00150 30-1300.00 40ND20
2,4,5-Trichlorophenol 210 01/06/2020 2217N13615030-13013 40ND20
2,4,6-Trichlorophenol 95 01/06/2020 2217+62150 30-130200 40ND20
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 57 33-102
2-Fluorophenol 49 35-115
Nitrobenzene-d5 76 22-109
Phenol-d5 54 33-122
Terphenyl-d14 64 41-120
2,4,6-Tribromophenol 38 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 62 of 73
RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:VQ40813-001
40813 3050B
01/05/2020 1437Analytical Method:6010D
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Arsenic ND 01/06/2020 05570.75 0.25 mg/kg1
Barium ND 01/06/2020 05571.3 0.33 mg/kg1
Cadmium ND 01/06/2020 05570.25 0.063 mg/kg1
Chromium ND 01/06/2020 05570.50 0.13 mg/kg1
Lead ND 01/06/2020 05570.50 0.23 mg/kg1
Selenium ND 01/06/2020 05571.0 0.41 mg/kg1
Silver ND 01/06/2020 05570.50 0.13 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 63 of 73
RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:VQ40813-002
40813 3050B
01/05/2020 1437Analytical Method:6010D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Arsenic 270 01/06/2020 060310625080-1201
Barium 530 01/06/2020 060310650080-1201
Cadmium 48 01/06/2020 0603965080-1201
Chromium 260 01/06/2020 060310525080-1201
Lead 260 01/06/2020 060310325080-1201
Selenium 50 01/06/2020 06031015080-1201
Silver 51 01/06/2020 06031015080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 64 of 73
RCRA Metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-004MS
40813 3050B
01/05/2020 1437Analytical Method:6010D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
Arsenic 270 01/06/2020 08389229075-1258.0 2
Barium 630 01/06/2020 06429257075-1251001
Cadmium 51 01/06/2020 0838895775-125ND2
Chromium 570 01/06/2020 0642N18129075-125541
Lead 300 01/06/2020 08389029075-125452
Selenium 50 01/06/2020 0838875775-125ND2
Silver 54 01/06/2020 0642945775-125ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 65 of 73
RCRA Metals - MSD
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-004MD
40813 3050B
01/05/2020 1437Analytical Method:6010D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
Arsenic 300 01/06/2020 084410129075-1259.3 208.0 2
Barium 680 01/06/2020 064810158075-1257.9 201001
Cadmium 55 01/06/2020 0844955875-1257.4 20ND2
Chromium 340 01/06/2020 0648+99290 75-12551 20541
Lead 340 01/06/2020 084410229075-12511 20452
Selenium 53 01/06/2020 0844925875-1256.3 20ND2
Silver 57 01/06/2020 0648995875-1255.8 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 66 of 73
RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:VQ40814-001
40814 7471B
01/03/2020 1317Analytical Method:7471B
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Mercury ND 01/04/2020 10520.083 0.020 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 67 of 73
RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:VQ40814-002
40814 7471B
01/03/2020 1317Analytical Method:7471B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Mercury 0.85 01/04/2020 10551020.83 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 68 of 73
RCRA Metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-004MS
40814 7471B
01/03/2020 1317Analytical Method:7471B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
Mercury 1.2 01/04/2020 11061100.97 80-1200.089 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 69 of 73
RCRA Metals - MSD
Batch:Prep Method:
Prep Date:
Sample ID:UL31060-004MD
40814 7471B
01/03/2020 1317Analytical Method:7471B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
Mercury 1.1 01/04/2020 11091130.86 80-1208.7 200.089 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 70 of 73
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 71 of 73
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 72 of 73
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 73 of 73
Limited Phase II ESA – 7th Street Apartments SUMMIT Project No. 4164.11 Charlotte, North Carolina January 27, 2020

C:\plowery\Documents\2-Projects\4164.11 7th Street Apartments - Phase I Wetlands\Phase II ESA\Appendix IV.rtf

APPENDIX IV
WELL RECORDS
WELL PERMITS