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HomeMy WebLinkAboutMO-9187_40659_CA_IAR_20160923_Initial Abatement Action ReportUST CLOSURE AND INITIAL ABATEMENT ACTION REPORT SWANS RUN CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA ECS PROJECT NO. 49-2115-A PREPARED FOR CAROLINA CAPITAL INVESTMENT PARTNERS 831 EAST MOREHEAD STREET, SUITE 750 CHARLOTTE, NORTH CAROLINA 28202-2731 SEPTEMBER 23, 2016 ECS CAROLINAS, LLP "Setting the Standard for Service" Geotechnical • Construction Materials • Environmental • Facilities NC Registered Lngineering i-irrn F-JOB 8 NC Registered Geologists Firm C-406 SC Registered Engineering Firm 3239 September 23, 2016 Mr. Todd Harrison Carolina Capital Investment Partners 831 East Morehead Street, Suite 750 Charlotte, North Carolina 28202-2731 Reference: UST Closure and Initial Abatement Action Report Swans Run Charlotte, Mecklenburg County, North Carolina ECS Project # 49-2115-A Dear Mr. Harrison: ECS Carolinas, LLP (ECS) is pleased to provide you with the results of our UST Closure and Initial Abatement Action Report that documents the oversight of removal of three residential heating oil underground storage tanks (UST) as well as petroleum impacted soil, and confirmatory soil sampling at the above referenced site. Environmental services were provided in general accordance with ECS Proposal No. 49-1614P dated June 13, 2016 and 49-1897P dated July 12, 2016. ECS appreciates the opportunity to provide our environmental consulting services to you on this project. If you have any questions concerning this report or this project, please contact ECS at (704) 525-5152. Respectfully submitted, ECS CAROLINAS, LLP r Christopher D. Orrell Staff Geologist �*- .-,f, -, - John S. Lair, P.G. Principal Geologist Brian T. Olin, P.G. Senior Project Manager ECS Capitol Services, PLLC • ECS Carolinas, LLP • ECS Central, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLC • ECS Texas, LLP wvwd.ecslimited.com UST Closure and Initial Abatement Action Report Swans Run Charlotte, Mecklenburg County, North Carolina ECS Project # 49-2115-A September 23, 2016 TABLE OF CONTENTS 1.0 EXECUTIVE SUMMARY................................................................................................1 2.0 UST CLOSURE PROCEDURES....................................................................................4 3.0 SOIL SCREENING AND EXCAVATION PROCEDURES..............................................4 4.0 RESULTS........................................................................................................................5 5.0 CONCLUSIONS..............................................................................................................5 6.0 RECOMMENDATIONS...................................................................................................5 7.0 QUALIFICATIONS..........................................................................................................5 FIGURES Figure 1 — Site Location Map Figure 2 — Site Map Figure 3 — UST Location Map Figure 4A — 7501 Sample Location Map Figure 413 — 7515 Sample Location Map Figure 4C — 7507 Sample Location Map TABLES Table 1 — Summary of Soil Analytical Results (7501) Table 2 — Summary of Soil Analytical Results (7515) Table 3 — Summary of Soil Analytical Results (7507) APPENDICES Appendix A — Non -Hazardous Liquid and UST Disposal Manifests Appendix B — 24-Hour Release and UST Leak Reporting Form (UST-61) Appendix C — Laboratory Data Sheets and Chain of Custody Records Appendix D — Photographic Log Appendix E — Soil Disposal Manifests UST Closure and Initial Abatement Action Report Swans Run Charlotte, Mecklenburg County, North Carolina ECS Project # 49-2115-A September 23, 2016 1.0 EXECUTIVE SUMMARY The subject site is located at 7501, 7507, 7515, 7513, and 7417 Swans Run Road in Charlotte, Mecklenburg County, North Carolina (Figures 1 and 2). According to the Mecklenburg County GIS website, the site consists of part of an approximate 4.74-acre site identified as Mecklenburg County Parcel Identification Number 21127326. On July 7, 2016, ECS observed the removal of three on -site residential heating oil underground storage tanks (USTs) located at the residences located at 7501, 7507, and 7515 Swans Run Road and collected UST closure samples. Evidence of a release was noted On August 11, 2016, ECS observed the over -excavation of petroleum impacted soil. ECS collected soil samples during the tank removal and over -excavation events. Approximately 225 tons of petroleum -impacted soils were removed from the area around the USTs and transported off -site for disposal. Laboratory analysis of confirmation soil samples did not detect targeted compounds at concentrations that exceed the North Carolina Soil -to -Groundwater Maximum Soil Contaminant Concentrations (MSCCs) in the samples collected from the excavation base or sidewalls except for in sample EW-1 located at the southwestern residence (7501 Swans Run Road). This sample had contamination above the North Carolina Soil -to -Groundwater MSCC as well as the Residential MSCCs. A. OWNERSHIP OF PROPERTY: One To One Realty 6617 Alexander Road Charlotte, North Carolina, 28270 B. RESPONSIBLE PARTY: One To One Realty 6617 Alexander Road Charlotte, North Carolina, 28270 C. FACILITY INFORMATION: 7501, 7507, and 7515 Swans Run Road Charlotte, Mecklenburg County, North Carolina Latitude: 35° 06' 18.80" N Longitude: 80° 47' 29.29" W (From Google Earth) D. CONTACTS: Primary Contact: Ms. Teresa Wilson One To One Realty 6617 Alexander Road Charlotte, North Carolina, 28270 UST Closure and Initial Abatement Action Report Swans Run Charlotte, Mecklenburg County, North Carolina ECS Project # 49-2115-A September 23, 2016 UST Closure Contractor: Dennis Joy Soil Excavation Contractor: Renee's Demolition Attn: Roy Sikes 980-521-2436 Consultant: ECS Carolinas, LLP 1812 Center Park Drive, Suite D Charlotte, North Carolina 28217 (704) 525-5152 Laboratory: Prism Laboratories, Inc. 48 Springbrook Road Charlotte, North Carolina 28078 E. SITE CHARACTERISTICS: The subject site is located at 7501, 7507, and 7515 Swans Run Road in Charlotte, Mecklenburg County, North Carolina (Figures 1 and 2). According to the Mecklenburg County GIS website, the site consists of part of an approximate 4.74-acre site identified as Mecklenburg County Parcel Identification Number 21127326. The site is currently developed with multiple single- family residences. As determined from the USGS Topographic Map Charlotte, North Carolina Quadrangle (Figure 1), the site's elevation is approximately 600 to 620 feet above mean sea level (msl). Surface runoff on the site is generally to the south towards an unnamed tributary. According to the Geologic Map of North Carolina (1985), the subject property is situated in the Charlotte Belt of the Piedmont Physiographic Province with the underlying bedrock composed of metavolcanic rock. The Piedmont Physiographic Province is characterized by gently rolling topography, deeply weathered bedrock, and a relative paucity of solid outcrop. Rocks are strongly weathered in the Piedmont's humid climate and bedrock is generally buried under a thick (2-20 m) blanket of saprolite. Outcrops are commonly restricted to stream valleys where saprolite has been removed by erosion. The soils encountered in this area are the residual product of in -place chemical weathering of rock presently underlying the site. In general, shallow unconfined groundwater movement within the overlying soils is controlled largely by topographic gradients. However, as the groundwater percolates downward to the bedrock, it becomes controlled by the orientation of the rock fracture systems. Thus, the direction of groundwater movement may not be consistent with the reflecting topography. In the Piedmont Physiographic region, groundwater generally occurs under water table conditions. Movement of groundwater under water table conditions is generally from higher to lower elevations. Please note that fluctuations in the groundwater level can be expected depending on variations in precipitation, run-off, and other factors not evident at the time of subsurface exploration. Normally, the highest groundwater levels occur in late winter and spring and the lowest levels occur in the late summer and fall. Groundwater was not encountered during excavation. Excavation refusal in weathered rock was encountered at approximately 18 feet during excavation activities at 7515 Swans Run Road. 2 UST Closure and Initial Abatement Action Report Swans Run Charlotte, Mecklenburg County, North Carolina ECS Project # 49-2115-A September 23, 2016 F. CERTIFICATION: I, Brian T. Olin, P.G. , a Professional Engineer/License Geologist r ECS Carolinas, LLP, do certify that thgejnkMw@Dion contained in this report is and accurate to the best of my knowledo* CAkk IQD/'�e, ore SEAL K. 06 i r z 2229 q NC License No. j22!� c �: ECS Carolinas, LLP" is licensed to practice geology/engineering in North Carolina. The certification number of the company/corporation is C-406 . 3 UST Closure and Initial Abatement Action Report Swans Run Charlotte, Mecklenburg County, North Carolina ECS Project # 49-2115-A September 23, 2016 2.0 UST CLOSURE PROCEDURES On July 7, 2016, ECS observed the removal of three residential heating oil USTs (Figure 2 and 3). The USTs were estimated to be 550-gallons in capacity based on dimensions. Approximately 400 gallons of residual product were removed from the USTs prior to removal. UST disposal documentation is included in Appendix A. The soils were screened with a photo - ionization detector (PID) for relative levels of organic vapors and checked for visual and olfactory evidence of contamination. Evidence of soil contamination including odors and elevated PID readings was identified beneath each UST. Two samples were collected from beneath each UST for total petroleum hydrocarbon (TPH) gasoline range organics (GRO) and diesel range organics (DRO). The sampler, wearing new nitrile gloves for each sample, placed the soil into laboratory supplied sample containers which were shipped to Prism Laboratory under chain -of -custody protocol. Laboratory data sheets and chain -of -custody records for post excavation samples are provided in Appendix C. A 24-hour release notification was completed and sent to the North Carolina Department of Environmental Quality (NCDEQ). A copy of the notification is included in Appendix B. 3.0 SOIL SCREENING AND EXCAVATION PROCEDURES On August 11 and 12, 2016, ECS observed the excavation of petroleum -impacted soils. Soils were screened in the field for relative levels of organic vapors using a PID until elevated PID readings were not detected to determine excavation limits. The final excavation area at the 7501 Swans Run Road address measured approximately 10 feet by 15 feet by 17 feet deep. The final excavation area at the 7515 Swans Run Road address measured approximately 13 feet by 15 feet by 18 feet deep. The final excavation area at the 7507 Swans Run Road address measured approximately 7 feet by 7 feet by 8 feet deep. Groundwater was not encountered during excavation activities. Approximately 225 tons of petroleum -impacted soils were removed from the site and transported off -site for disposal. The over -excavation activities and transport of the materials were conducted by the onsite general contractor with the petroleum -impacted soils disposed at the Environmental Soils Inc. facility in Lattimore, North Carolina. The Non -Hazardous Soil Disposal Manifests are included in Appendix E. Following completion of petroleum -impacted soil excavation activities, ECS personnel collected five confirmation soil samples from each excavation. Soil samples were collected from each sidewall and the base of each excavation. Confirmation soil sample locations are shown on Figure 4. The sampler, wearing new nitrile gloves for each sample, placed the soil into laboratory supplied sample containers which were shipped to Prism Laboratory under chain -of -custody protocol. Laboratory data sheets and chain -of -custody records for post excavation samples are provided in Appendix C. Photographs of the area are provided in Appendix D. In accordance with NCDEQ guidance, the soil samples were analyzed for volatile organic compounds (VOCs) by EPA Method 8260, semi -volatile organic compounds (SVOCs) by EPA Method 8270, and extractable and volatile petroleum hydrocarbon fractions (EPH/VPH) by the Massachusetts Department of Environmental Protection (MADEP) Method. Laboratory analysis of confirmation soil samples did not detect targeted compounds at concentrations that exceed the North Carolina Soil -to -Groundwater Maximum Soil Contaminant Concentrations (MSCCs) in the samples collected, except for sample EW-1 from 7501 Swans Run Road. The results of post - excavation soil sampling are summarized in Table 1. 4 UST Closure and Initial Abatement Action Report Swans Run Charlotte, Mecklenburg County, North Carolina ECS Project # 49-2115-A September 23, 2016 4.0 RESULTS Laboratory analysis of post -excavation confirmation soil samples did not detect targeted compounds at concentrations that exceed the North Carolina Soil -to -Groundwater Maximum Soil Contaminant Concentrations (MSCCs) in the samples collected except for EW-1, located at 7501 Swans Run Road. Sample EW-1, located adjacent to the 7501 residence had detection of EPH at levels above the Residential MSCCs. Further excavation was not feasible in this area without undermining the currently occupied residence. The results are summarized in Table 1. 5.0 CONCLUSIONS A release was identified from heating oil USTs associated with three residences at 7501, 7507, and 7515 Swans Run Road in Charlotte, North Carolina. ECS observed the excavation of approximately 225 tons of petroleum impacted soils from the area. Laboratory analysis of confirmation soil samples did not detect targeted compounds at concentrations that exceed the North Carolina Soil -to -Groundwater or Residential Maximum Soil Contaminant Concentrations (MSCCs) in the samples collected except for EW-1. Sample EW-1, located adjacent to the 7501 residence had detection of EPH at levels above the Residential MSCCs. Further excavation was not feasible in this area without undermining the currently occupied residence. 6.0 RECOMMENDATIONS Based on laboratory analytical results the 7501 Swans Run residence cannot be closed out at this time without a Notice of Residual Petroleum with restrictions on residential site use until the remaining impacted soils have been removed. No further assessment or sampling is required at the 7507 or 7515 Swans Run Road residences. ECS recommends that a copy of this report be submitted to the NCDEQ — Mooresville Regional Office (MRO), Division of Waste Management, UST Section for their review after the demolition of the house and removal of the remaining petroleum impacted soil beneath the 7501 Swans Run Road residence. 7.0 QUALIFICATIONS The activities and evaluative approaches used in this assessment are consistent with those normally employed in assessments and remediation projects of this type. ECS' evaluation of site conditions has been based on our understanding of the project information and the data obtained during our field activities. This report is provided for the use of Carolina Capital Investment Partners and the NCDEQ. This report is not intended to be used or relied upon in connection with other projects or by other unidentified third parties. The use of this report by undesignated third party or parties will be at such party's sole risk and ECS disclaims liability for such third party use or reliance. 5 FIGURES 4 ob dLJti } .w' 1 �— "� SITE ° �s� JU � 1 I 1 O7L1 I sue. 1 o I � f vu M E [ �� e h {IR f " p a - PC. - 1 It SOURCE: N FIGURE 1 USGS SITE LOCATION MAP 7.5-MINUTE TOPO MAPS WEDDINGTON SWANS RUN NORTH CAROLINA CHARLOTTE, MECKLENBURG COUNTY, QUADRANGLE, DATED 2016 NORTH CAROLINA SCALE = 1" = 24,000' ECS PROJECT NO. 49:2115-A1 F - F OF • i 04 # + i t A f .06 A • 16+ -� Legend } * T1-1 Initial Soil Sample Location 1 WW-1 Confirmatory Soil Sample Location - I Excavation Limit UST Limit SOURCE: FIGURE 413 7501 SAMPLE LOCATION MAP r �<" SCALE AS SHOWN 7501 SWANS RUN CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA ECS PROJECT NO. 49:2115-A1 JIFF 4K qP& X" alb "t *� dk - 4L p OF Vop f SOURCE: SCALE AS SHOWN 1k Ae� 1P Apr 40 IF do IL rr Opp + r ■ 0-0 4D M Legend T1-1 Initial Soil Sample Location ' WW-1 Confirmatory Soil Sample Location Excavation Limit L UST Limit FIGURE 413 7515 SAMPLE LOCATION MAP 7515 SWANS RUN CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA ECS PROJECT NO. 49:2115-A1 SOURCE: SCALE AS SHOWN N r \� I IF f Legend T1-1 Initial Soil Sample Location ® WW-1 Confirmatory Soil Sample Location IDExcavation Limit UST Limit FIGURE 4C 7507 SAMPLE LOCATION MAP 7507 SWANS RUN CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA ECS PROJECT NO. 49:2115-A1 TABLES TABLE 1: SUMMARY OF SOIL ANALYTICAL RESULTS (7501) 7501 SWANS RUN ROAD CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA❑ ECS PROJECT NO. 49-2115-A1 ❑ Parameter ANALYTICAL RESULTS COMPARISION CRITERIA Sample ID T1-1 T1-2 NW-1 EW-1 SW-1 WW-1 B-1 NC Action Level or Soil -to- Groundwater MSCC (mg/kg) North Carolina Residential MSCC (mg/kg) North Carolina Commercial MSCC (mg/kg) Collection Depth (feet bgs) 6-8 6-8 12-14 12-14 12-14 12-14 14 Collection Date 7/7/16 7/7/16 8/11/16 8/11/16 8/11/16 8/11/16 8/11/16 Diesel Range Organics by GC/FID Diesel Range Organics 14,000 12,000 NA NA NA NA NA 100 NA NA Gasoline Range Organics by GC/FID Gasoline Range Organics BRL BRL NA NA NA NA NA 50 NA NA Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics NA NA BRL 4,500 BRL BRL BRL 540 1,500 40,000 C19-C36 Aliphatics NA NA BRL 2,100 BRL BRL BRL # 31,000 810,000 C11-C22 Aromatics NA NA BRL 2,300 BRL BRL BRL 31 469 12,264 Volatile Petroleum Hydrocarbons by GC/PID/FID Total VPHs NA I NA BRL BRL BRL BRL BRL 68 939 24,528 Semivolatile Organic Compounds by GC/MS Total SVOCs NA I NA BRL BRL BRL BRL BRL NS NS NS Volatile Organic Compounds by GC/MS Acetone NA I NA BRL 0.120 BRL 0.037 BRL 24 14,000 360,000 Notes: Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm) Feet bgs = Feet below ground surface BRL = Compound not detected at a concentration above the method reporting limit MSCC = Maximum Soil Contaminant Concentration Bold denotes concentration exceeds the Soil -to -Groundwater MSCC # = Health based level >100% NS= No Standard TABLE 2: SUMMARY OF SOIL ANALYTICAL RESULTS (7515) 7515 SWANS RUN ROAD CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA❑ ECS PROJECT NO. 49-2115-A1 ❑ Parameter ANALYTICAL RESULTS COMPARISION CRITERIA Sample ID T2-1 T2-2 SW-2 WW-2 EW-2 NW-2 B-2 NC Action Level or Soil -to- Groundwater MSCC (mg/kg) North Carolina Residential MSCC (mg/kg) North Carolina Commercial MSCC (mg/kg) Collection Depth (feet bgs) 6-8 6-8 12-14 12-14 12-14 12-14 14 Collection Date 7/7/16 7/7/16 8/11/16 8/11/16 8/11/16 8/12/16 8/12/16 Diesel Range Organics by GC/FID Diesel Range Organics 24,000 16,000 NA NA NA NA NA 100 NA NA Gasoline Range Organics by GC/FID Gasoline Range Organics 8.4 5.4 NA NA NA NA NA 50 NA NA Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics NA NA BRL BRL BRL BRL BRL 540 1,500 40,000 C19-C36 Aliphatics NA NA BRL BRL BRL BRL BRL # 31,000 810,000 C11-C22 Aromatics NA NA BRL BRL BRL BRL BRL 31 469 12,264 Volatile Petroleum Hydrocarbons by GC/PID/FID Total VPHs NA I NA BRL BRL BRL BRL BRL 68 939 24,528 Semivolatile Organic Compounds by GC/MS Total SVOCs NA I NA BRL BRL BRL BRL BRL NS NS NS Volatile Organic Compounds by GC/MS Acetone NA I NA BRL 0.030 BRL BRL BRL 24 14,000 360,000 Notes: Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm) Feet bgs = Feet below ground surface BRL = Compound not detected at a concentration above the method reporting limit MSCC = Maximum Soil Contaminant Concentration Bold denotes concentration exceeds the Soil -to -Groundwater MSCC # = Health based level >100% NS= No Standard TABLE 3: SUMMARY OF SOIL ANALYTICAL RESULTS (7507) 7507 SWANS RUN ROAD CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA❑ ECS PROJECT NO. 49-2115-A1 ❑ Parameter ANALYTICAL RESULTS COMPARISION CRITERIA Sample ID T3-1 T3-2 E-3 N-3 W-3 S-3 B-3 NC Action Level or Soil -to- Groundwater MSCC (mg/kg) North Carolina Residential MSCC (mg/kg) North Carolina Commercial MSCC (mg/kg) Collection Depth (feet bgs) 6-8 6-8 12-14 12-14 12-14 12-14 14 Collection Date 7/7/16 7/7/16 8/12/16 8/12/16 8/12/16 8/12/16 8/12/16 Diesel Range Organics by GC/FID Diesel Range Organics 7,400 19,000 NA NA NA NA NA 100 NA NA Gasoline Range Organics by GC/FID Gasoline Range Organics 14 71 NA NA NA NA NA 50 NA NA Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics NA NA 6.5 BRL BRL BRL BRL 540 1,500 40,000 C19-C36 Aliphatics NA NA 3.5 BRL BRL BRL BRL # 31,000 810,000 C11-C22 Aromatics NA NA 5.3 BRL BRL BRL BRL 31 469 12,264 Volatile Petroleum Hydrocarbons by GC/PID/FID Total VPHs NA I NA BRL BRL BRL BRL BRL 68 939 24,528 Semivolatile Organic Compounds by GC/MS Total SVOCs NA I NA BRL BRL BRL BRL BRL NS NS NS Volatile Organic Compounds by GC/MS Acetone NA I NA BRL BRL BRL BRL 0.020 J 24 14,000 360,000 Notes: Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm) Feet bgs = Feet below ground surface BRL = Compound not detected at a concentration above the method reporting limit MSCC = Maximum Soil Contaminant Concentration Bold denotes concentration exceeds the Soil -to -Groundwater MSCC # = Health based level >100% NS= No Standard APPENDICES Appendix A Non -Hazardous Liquid and UST Disposal Manifests MANIFEST HAZ-MAT ENVIRONMEWAL SERVICES mAt%FmT4 112045 w Appendix B 24-Hour Release and UST Leak Reporting Form (UST-61) UST-61 24-Hour Release and UST Leak Reporting Form. For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or in NC suspected release (DWM USE ONLY) Suspected Contamination? (Y/N) _Y Facility ID Number Incident # Risk (H,I,L,U) Confirmed GW Contamination? (Y/N) —N Date Leak Discovered _7-7-16 Received On Received By Confirmed Soil Contamination ?(Y/N) —Y Comm/Non-Commercial? _Non_ Reported by (circle one): Phone, Fax or Report Samples Taken?(Y/N) _Y Reg/Non-regulated? _Non Region Free Product? (Y/N) _N If Yes, State Greatest Thickness INCIDENT DESCRIPTION Incident Name: Swans Run Address: 7501, 7515, 7507 Swans Run Road County: Mecklenburg Regional Office (circle one): Asheville, Mooresville, Fayetteville, City/Town: Charlotte Zip Code: 28226 Raleigh, Washington, Wilmington, Winston-Salem Latitude (decimal degrees): 35.105213 Longitude (decimal degrees) :-80.791153 Obtained by: GPS Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors ❑ Topographic map A release was identified upon the removal of three heating oil UST's located at the residences listed above on Jul 7, 2016. ❑ GIS Address matching ❑ Other ❑ Unknown Describe location: HOW RELEASE WAS DISCOVERED (Release code) (Check one) ❑ Release Detection Equipment or Methods Visual/Odor ❑ Groundwater Contamination U During UST Closure/Removal ❑ Water in Tank ❑ Surface Water Contamination ❑ Property Transfer ❑ Water Supply Well Contamination ❑ Other (specify) SOURCE OF CONTAMINATION Source of Release Cause of Release Type of Release Product Type Released (Check one to indicate primary (Check one to indicate primary (Check one) (Check one to indicate primary product type source) cause) released) / Tank ❑ Spill U Petroleum ❑ Gasoline/ Diesel/ ❑ Diesel/Veg. Oil Kerosene Blend ❑ Piping ❑/Overfill ❑Non -Petroleum 4 Heating Oil ❑ Vegetable Oil 100% ❑ Dispenser l�7 Corrosion ❑ Both ❑ Other Petroleum ❑ E10 — E20 ❑ Submersible Turbine Pump ❑ Physical or Mechanical Products ❑ E21 E84 — Damage Location ❑ Metals ❑ Delivery Problem ❑ E85 E99 ❑ oOther Inorganics — ❑ Install Problem (Checkne ) ❑ Other ❑ Other ❑ Other Organics ❑ Ethanol 100% Facility ❑ Unknown ,❑/ ❑ Unknown Residence ❑ E01 — E09 U Definitions presented on reverse I Definitions presented on reverse I ❑ Other Ownership 1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining UST Form 61 (02/08) Page 1 of 2 IMPACT ON DRINKING WATER SUPPLIES Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1. 2. 3. UST SYSTEM OWNER UST Owner/Company One To One Realty Point of Contact Address Ms. Teresa Wilson 6617 Alexander Road City State Zip Code Telephone Number Charlotte NC 28270 UST SYSTEM OPERATOR UST Operator/Company Address City State Zip Code Telephone Number LANDOWNER AT LOCATION OF UST INCIDENT Landowner Address One To One Realty 6617 Alexander Road City State Zip Code Telephone Number Charlotte NC 28270 Draw Sketch of Area (showing two major road intersections) or Attach Map SEE ATTACHED Person Reporting Incident Chris Orrell Company ECS Carolinas, LLP Telephone Number 704-525-5152 Title Environmental Scientist I Address 1812 Center Park Drive, Suite D Date 8-31-16 UST Form 61 (02/08) Page 2 of 2 Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined • �" CO _ 4 = - I m + 1 • • 1 4 . Y +. 1 f , • mow�z l ~ O 1 ° •` CL N A i Z Z 0 O t W a�OQ N W(°zQL v) >�F-z w rr f xx S V (n .rYx3 k 0 F7 14- .' da Nil V'wA wipr'4* 4-k�*4 Appendix C Laboratory Data Sheets and Chain of Custody Records PRISM Full -Service Analytical & Environmental Solutions `,. LABORATORIES, INC. ECS Carolinas, LLP (Charlotte) Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 FL NELAC Cert No. E87519 VA NELAC Cent No. 460211 Project: Swans Run Lab Submittal Date: 07/08/2016 Prism Work Order: 6070131 Case Narrative 07/18/2016 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a,j Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference: BC Sample prepared from bulk container. DO Surrogates diluted out. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Reviewed By Terri W. Cole For Angela D. Overcash Project Manager * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 12 /P R I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Sample Receipt Summary 07/18/2016 Prism Work Order: 6070131 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received T1-1 6070131-01 Solid 07/07/16 07/08/16 T1-2 6070131-02 Solid 07/07/16 07/08/16 T2-1 6070131-03 Solid 07/07/16 07/08/16 T2-2 6070131-04 Solid 07/07/16 07/08/16 T3-1 6070131-05 Solid 07/07/16 07/08/16 T3-2 6070131-06 Solid 07/07/16 07/08/16 Samples were received in good condition at 5.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 12 Full -Service Analytical & P R I S M Environmental Solutions LABORATORIES, INC. Summary of Detections 07/18/2016 Prism Work Order: 6070131 Prism ID Client ID Parameter Method Result Units 6070131-01 T1-1 Diesel Range Organics `8015C 14000 mg/kg dry 6070131-02 T1-2 Diesel Range Organics '8015C 12000 mg/kg dry 6070131-03 T2-1 Diesel Range Organics "8015C 24000 mg/kg dry 6070131-03 T2-1 Gasoline Range Organics `8015C 8.4 mg/kg dry 6070131-04 T2-2 Diesel Range Organics '8015C 16000 mg/kg dry 6070131-04 T2-2 Gasoline Range Organics "8015C 5.4 mg/kg dry 6070131-05 T3-1 Diesel Range Organics '8015C 7400 mg/kg dry 6070131-05 T3-1 Gasoline Range Organics `8015C 14 mg/kg dry 6070131-06 T3-2 Diesel Range Organics *8015C 19000 mg/kg dry 6070131-06 T3-2 Gasoline Range Organics '8015C 71 mg/kg dry This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 12 Laboratory Report ` Full -Service Analytical & P R S M / Environmental Solutions LABORATORIES INC. 07/18/2016 ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: T1-1 Attn: Brian Olin Prism Sample ID: 6070131-01 1812 Center Park Drive, Suite D Prism Work Order: 6070131 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/07/16 13:40 Time Submitted: 07/08/16 10:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics 14000 mg/kg dry 970 220 100 *8015C 7/15/16 18:03 ZRC P6G0172 Surrogate Recovery Control Limits o-Terphenyl 0 % 49-124 DO Gasoline Range Organics by GC/FID Gasoline Range Organics BRL mg/kg dry 3.4 0.52 50 *8015C 7/14/16 8:38 ANG P6G0213 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 76 % 50-137 General Chemistry Parameters % Solids 70.8 % by 0.100 0.100 1 *SM2540 G 7/11/16 16:00 JLB P6G0180 Weight This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 12 Laboratory Report ` Full -Service Analytical & P R S M / Environmental Solutions LABORATORIES INC. 07/18/2016 ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: T1-2 Attn: Brian Olin Prism Sample ID: 6070131-02 1812 Center Park Drive, Suite D Prism Work Order: 6070131 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/07/16 13:45 Time Submitted: 07/08/16 10:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics 12000 mg/kg dry 960 220 100 *8015C 7/15/16 18:40 ZRC P6G0172 Surrogate Recovery Control Limits o-Terphenyl 0 % 49-124 DO Gasoline Range Organics by GC/FID BC Gasoline Range Organics BRL mg/kg dry 7.1 1.1 50 *8015C 7/14/16 9:06 ANG P6G0213 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 94 % 50-137 General Chemistry Parameters % Solids 72.1 % by 0.100 0.100 1 *SM2540 G 7/11/16 16:00 JLB P6G0180 Weight This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 12 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 07/18/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: T2-1 Attn: Brian Olin Prism Sample ID: 6070131-03 1812 Center Park Drive, Suite D Prism Work Order: 6070131 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/07/16 14:15 Time Submitted: 07/08/16 10:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics 24000 mg/kg dry 2100 480 200 *8015C 7/15/16 19:17 ZRC P6G0172 Surrogate Recovery Control Limits o-Terphenyl 0 % 49-124 DO Gasoline Range Organics by GC/FID Gasoline Range Organics 8.4 mg/kg dry 2.1 0.31 50 *8015C 7/14/16 9:34 ANG P6G0213 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 77 % 50-137 General Chemistry Parameters % Solids 67.2 % by 0.100 0.100 1 *SM2540 G 7/11/16 16:00 JLB P6G0180 Weight This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 12 Laboratory Report ` Full -Service Analytical & P R S M / Environmental Solutions LABORATORIES INC. 07/18/2016 ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: T2-2 Attn: Brian Olin Prism Sample ID: 6070131-04 1812 Center Park Drive, Suite D Prism Work Order: 6070131 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/07/16 14:20 Time Submitted: 07/08/16 10:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics 16000 mg/kg dry 2000 460 200 *8015C 7/15/16 19:54 ZRC P6G0172 Surrogate Recovery Control Limits o-Terphenyl 0 % 49-124 DO Gasoline Range Organics by GC/FID Gasoline Range Organics 5.4 mg/kg dry 3.2 0.48 50 *8015C 7/14/16 4:25 ANG P6G0213 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 89 % 50-137 General Chemistry Parameters % Solids 68.9 % by 0.100 0.100 1 *SM2540 G 7/11/16 16:00 JLB P6G0180 Weight This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 12 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 07/18/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: T3-1 Attn: Brian Olin Prism Sample ID: 6070131-05 1812 Center Park Drive, Suite D Prism Work Order: 6070131 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/07/16 16:15 Time Submitted: 07/08/16 10:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics 7400 mg/kg dry 450 100 50 *8015C 7/15/16 14:17 ZRC P6G0172 Surrogate Recovery Control Limits o-Terphenyl 0 % 49-124 DO Gasoline Range Organics by GC/FID Gasoline Range Organics 14 mg/kg dry 3.5 0.52 50 *8015C 7/14/16 10:01 ANG P6G0213 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 68 % 50-137 General Chemistry Parameters % Solids 76.2 % by 0.100 0.100 1 *SM2540 G 7/11/16 16:00 JLB P6G0180 Weight This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 12 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 07/18/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: T3-2 Attn: Brian Olin Prism Sample ID: 6070131-06 1812 Center Park Drive, Suite D Prism Work Order: 6070131 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/07/16 16:20 Time Submitted: 07/08/16 10:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics 19000 mg/kg dry 850 190 100 *8015C 7/15/16 14:57 ZRC P6G0172 Surrogate Recovery Control Limits o-Terphenyl 0 % 49-124 DO Gasoline Range Organics by GC/FID Gasoline Range Organics 71 mg/kg dry 3.6 0.55 50 *8015C 7/14/16 10:29 ANG P6G0213 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 74 % 50-137 General Chemistry Parameters % Solids 82.2 % by 0.100 0.100 1 *SM2540 G 7/11/16 16:00 JLB P6G0180 Weight This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 12 P R I IS M Full -Service Analytical Environmental Solutions LABORATORIES, INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Gasoline Range Organics by GC/FID - Quality Control Level II QC Report 7/18/16 Prism Work Order: 6070131 Time Submitted: 7/8/2016 10:45:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6GO213 - 5035 Blank (P6G0213-BLK1) Prepared & Analyzed: 07/13/16 Gasoline Range Organics BRL 5.0 mg/kg wet Surrogate: a,a,a-Trifluorotoluene 5.20 mg/kg wet 5.000 104 50-137 LCS (P6G0213-BS1) Prepared & Analyzed: 07/13/16 Gasoline Range Organics 45.6 5.0 mg/kg wet 50.00 91 41-138 Surrogate: a,a,a-Trifluorotoluene 5.15 mg/kg wet 5.000 103 50-137 LCS Dup (P6130213-113SD1) Prepared & Analyzed: 07/13/16 Gasoline Range Organics 52.0 5.0 mg/kg wet 50.00 104 41-138 13 20 Surrogate: a,a,a-Trifluorotoluene 5.45 mg/kg wet 5.000 109 50-137 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 12 Level II QC Report P R I S M Full -Service Analytical & 7/18/16 Environmental Solutions LABORATOR, ECS Carolinas, LLP (Charlotte) Project: Swans Run Prism Work Order: 6070131 Attn: Brian Olin Time Submitted: 7/8/2016 10:45:OOAM 1812 Center Park Drive, Suite D Charlotte, NC 28217 Diesel Range Organics by GC/FID - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6GO172 - 3546 Blank (P6G0172-BLK1) Prepared: 07/12/16 Analyzed: 07/13/16 Diesel Range Organics BRL 7.0 mg/kg wet Surrogate: o-Terphenyl 0.941 mg/kg wet 1.327 71 49-124 LCS (P6G0172-BS1) Prepared: 07/12/16 Analyzed: 07/13/16 Diesel Range Organics 62.1 7.0 mg/kg wet 66.67 93 55-109 Surrogate: o-Terphenyl 0.956 mg/kg wet 1.333 72 49-124 LCS Dup (P6G0172-BSD1) Prepared: 07/12/16 Analyzed: 07/13/16 Diesel Range Organics 67.4 6.9 mg/kg wet 66.14 102 55-109 8 20 Surrogate: o-Terphenyl 0.998 mg/kg wet 1.323 75 49-124 Prep Method: 3546 Lab Number Batch Initial Sample Extraction Data Final Date/Time 6070131-01 P6G0172 30.53 g 1 mL 07/12/16 13:05 6070131-02 P6G0172 30.4 g 1 mL 07/12/16 13:05 6070131-03 P6G0172 30.03 g 1 mL 07/12/16 13:05 6070131-04 P6G0172 30.17 g 1 mL 07/12/16 13:05 6070131-05 P6G0172 30.34 g 1 mL 07/12/16 13:05 6070131-06 P6G0172 30.21 g 1 mL 07/12/16 13:05 Prep Method: 5035 Lab Number Batch Initial Final DatelTime 6070131-01 P6G0213 10.25 g 5 mL 07/13/16 16:27 6070131-02 P6G0213 4.87 g 5 mL 07/13/16 16:27 6070131-03 P6G0213 17.88 g 5 mL 07/13/16 16:27 6070131-04 P6G0213 11.35 g 5 mL 07/13/16 16:27 6070131-05 P6G0213 9.51 g 5 mL 07/13/16 16:27 6070131-06 P6G0213 8.34 g 5 mL 07/13/16 16:27 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 6070131-01 P6G0180 30 g 30 g 07/11/16 16:00 6070131-02 P6G0180 30 g 30 g 07/11/16 16:00 6070131-03 P6G0180 30 g 30 g 07/11/16 16:00 6070131-04 P6G0180 30 g 30 g 07/11/16 16:00 6070131-05 P6G0180 30 g 30 g 07/11/16 16:00 6070131-06 P6G0180 30 g 30 g 07/11/16 16:00 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 12 alaly- Envi LABORATOMES, INC, 44Kwlngb rook Road Chadc Phont* -;&/529-6-364 Fax: -1 Client Company NaMG'. Report To/Contact Name: Reporting Address: 'ii X 6 --------- --- ................ CHAIN OF CUSTODY RECORD e Analytical & OF _ QUOTE # TO ENSURE PROPER BILLING: imenW SOILItions PAGE— Projectillame: (NO) NC 28217 Short Hold Analysis' (Yes) (No) UST Project: (Yes) '525-0409 *Please ATTACH any project specific reporting (QC LEVEL 111111 IV) provisions and/or QC Requirements Invoice To: 21 ILL Address: Fax (Yes) (No): Phon Email Address: EDD Type: PDF—Excel—Other Site Location Site Location Physical Address: TIME MATRIX CLIENT DATE COLLECTED (SOIL, SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR HOURS SLUDGE) 7— ,4 Purchase Order No./Billing Reference FTOBE FILLED IN BY CLIENT/SAMPLING PERSONNEL Requested Due Date E3 1 Day 13 2 Days 0 3 Days El 4 Days L4'5 Days Certification: NEL� AC_ Do®_ FL_ NC 1 0 Rush Work Must Be SC -Working Days" El 6-9 Days El standard 10 days Pre -Approved Sc OTHER_ NIA Samples received after 14:00 will be processed next business day. Water I.., r ri t ,hJ. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO — (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon collection: YES® NO — RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) ANALYSIS REQUESTED 7PRISM SAMPLE CONTAINER PRESERVA- *TYPE NO. SIZE TIVES SEE BELOW N07 S Affiliation i ,,, Sampler --- Sampled By (Print Name) 's Signature requested above. Any changes must be Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as submitted in writing to the Prism Project Manager. There will be charges f ' any changes after analyseshave been initialized. Date Military/F Received By: (Si lure) Relinquished By: (Signature) Date Received BY: (Signature) --------------- Relinq.iE;K-ed'El;'f7s:,g.-aTu,—n), Date -� Received For P i Lab ones Ay, Relinquished y: (Signature) PED SH T WITH uu y =ALS F­ C IAI IUN I V THE LABORATORY. COC Group NO. Method of �Shlpment. NOTE. AS ARE NOT P �L SAMPLE COOLERS 6 AND OU D BIFIED AGAINST TAPED SH T COC TIL RECEIVED AT THE LABORATORY. SAMPLEACCETED VER 0 Fad Ex Q UPS 0 Hand -delivered Prism Field Service U Other—, - ­=�c '11, CERCLA LANUI-ILL OTHER: DRINKING WATER: SOLID WA RCRA: S --si,15—UNDWATER: El NC U SC 0 NC El C L] NC E3 SC N DES. El NC 0 SC El NC El S E3 NC El El NC El SC Q P C 0 T C3 L3 N ®NC C3 SC _ a _ 0— 0 r,­ r-'l— p = Plastic; TL = Teflon -Lined Cap VOA � Volatile Organics Analysis (Zero Head Space) REMARKS Comments: *CONTAINER TYPE CODES: A = Amber C = Clear 7- PRISM Full -Service Analytical & Environmental Solutions `,. LABORATORIES, INC. ECS Carolinas, LLP (Charlotte) Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 FL NELAC Cert No. E87519 VA NELAC Cent No. 460211 Project: Swans Run Lab Submittal Date: 08/15/2016 Prism Work Order: 6080270 Case Narrative 08/22/2016 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a,j Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference: Reviewed By Terri W. Cole For Angela D. Overcash Project Manager D RPD value outside of the control limits. DO Surrogates diluted out. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. M Matrix spike outside of the control limits. RLM Sample container suspected to have low methanol content. Results possibly biased high. SR Surrogate recovery outside the QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 87 /P R I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Sample Receipt Summary 08/22/2016 Prism Work Order: 6080270 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received NW-1 6080270-01 Solid 08/11/16 08/15/16 EW-1 6080270-02 Solid 08/11/16 08/15/16 SW-1 6080270-03 Solid 08/11/16 08/15/16 WW-1 6080270-04 Solid 08/11/16 08/15/16 B-1 6080270-05 Solid 08/11/16 08/15/16 SW-2 6080270-06 Solid 08/11/16 08/15/16 WW-2 6080270-07 Solid 08/11/16 08/15/16 EW-2 6080270-08 Solid 08/11/16 08/15/16 B-3 6080270-09 Solid 08/12/16 08/15/16 E-3 6080270-10 Solid 08/12/16 08/15/16 N-3 6080270-11 Solid 08/12/16 08/15/16 W-3 6080270-12 Solid 08/12/16 08/15/16 S-3 6080270-13 Solid 08/12/16 08/15/16 NW-2 6080270-14 Solid 08/12/16 08/15/16 B-2 6080270-15 Solid 08/12/16 08/15/16 Samples were received in good condition at 3.2 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 87 P R I S M Full Service Analytical & Environmental Solutions LABORATORIES, INC. Summary of Detections 08/22/2016 Prism Work Order: 6080270 Prism ID Client ID Parameter Method Result Units 6080270-02 EW-1 C9-Cl8 Aliphatics MADEP EPH 4500 mg/kg dry 6080270-02 EW-1 C19-C36 Aliphatics MADEP EPH 2100 mg/kg dry 6080270-02 EW-1 C11-C22 Aromatics MADEP EPH 2300 mg/kg dry 6080270-02 EW-1 Acetone 8260B 0.12 mg/kg dry 6080270-04 WW-1 Acetone 8260E 0.037 mg/kg dry 6080270-07 WW-2 Acetone 8260E 0.030 mg/kg dry 6080270-09 B-3 Acetone 8260B 0.020 1 mg/kg dry 6080270-10 E-3 C9-Cl8 Aliphatics MADEP EPH 6.5 1 mg/kg dry 6080270-10 E-3 C19-C36 Aliphatics MADEP EPH 3.5 1 mg/kg dry 6080270-10 E-3 C11-C22 Aromatics MADEP EPH 5.3 1 mg/kg dry This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: NW-1 Attn: Brian Olin Prism Sample ID: 6080270-01 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 11:40 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 30 1.3 1 MADEP EPH 8/18/16 13:34 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 30 2.4 1 MADEP EPH 8/18/16 13:34 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 12 1.6 1 MADEP EPH 8/18/16 13:34 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 53 % 40-140 o-Terphenyl 58 % 40-140 2-Fluorobiphenyl 87 % 40-140 2-Bromonaphthalene 102 % 40-140 General Chemistry Parameters % Solids 83.6 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.39 0.062 1 8270D 8/18/16 16:23 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.39 0.060 1 8270D 8/18/16 16:23 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.39 0.056 1 8270D 8/18/16 16:23 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.39 0.058 1 8270D 8/18/16 16:23 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.39 0.076 1 8270D 8/18/16 16:23 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.39 0.074 1 8270D 8/18/16 16:23 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.39 0.076 1 8270D 8/18/16 16:23 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.39 0.060 1 8270D 8/18/16 16:23 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.39 0.055 1 8270D 8/18/16 16:23 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.39 0.048 1 8270D 8/18/16 16:23 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.39 0.052 1 8270D 8/18/16 16:23 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.39 0.057 1 8270D 8/18/16 16:23 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.39 0.056 1 8270D 8/18/16 16:23 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.39 0.063 1 8270D 8/18/16 16:23 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.39 0.051 1 8270D 8/18/16 16:23 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.39 0.072 1 8270D 8/18/16 16:23 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.39 0.078 1 8270D 8/18/16 16:23 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.39 0.049 1 8270D 8/18/16 16:23 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.39 0.059 1 8270D 8/18/16 16:23 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.39 0.068 1 8270D 8/18/16 16:23 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.39 0.055 1 8270D 8/18/16 16:23 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.39 0.047 1 8270D 8/18/16 16:23 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.39 0.051 1 8270D 8/18/16 16:23 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.39 0.061 1 8270D 8/18/16 16:23 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.39 0.054 1 8270D 8/18/16 16:23 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.39 0.057 1 8270D 8/18/16 16:23 JMV P61-10314 Anthracene BRL mg/kg dry 0.39 0.064 1 8270D 8/18/16 16:23 JMV P61-10314 Azobenzene BRL mg/kg dry 0.39 0.052 1 8270D 8/18/16 16:23 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.39 0.052 1 8270D 8/18/16 16:23 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.39 0.043 1 8270D 8/18/16 16:23 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: NW-1 Prism Sample ID: 6080270-01 Prism Work Order: 6080270 Time Collected: 08/11/16 11:40 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.39 0.046 1 8270D 8/18/16 16:23 Benzo(g,h,i)perylene BRL mg/kg dry 0.39 0.043 1 8270D 8/18/16 16:23 Benzo(k)fluoranthene BRL mg/kg dry 0.39 0.052 1 8270D 8/18/16 16:23 Benzoic Acid BRL mg/kg dry 0.39 0.033 1 8270D 8/18/16 16:23 Benzyl alcohol BRL mg/kg dry 0.39 0.052 1 8270D 8/18/16 16:23 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.39 0.068 1 8270D 8/18/16 16:23 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.39 0.056 1 8270D 8/18/16 16:23 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.39 0.067 1 8270D 8/18/16 16:23 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.39 0.059 1 8270D 8/18/16 16:23 Butyl benzyl phthalate BRL mg/kg dry 0.39 0.056 1 8270D 8/18/16 16:23 Chrysene BRL mg/kg dry 0.39 0.050 1 8270D 8/18/16 16:23 Dibenzo(a,h)anthracene BRL mg/kg dry 0.39 0.048 1 8270D 8/18/16 16:23 Dibenzofuran BRL mg/kg dry 0.39 0.060 1 8270D 8/18/16 16:23 Diethyl phthalate BRL mg/kg dry 0.39 0.054 1 8270D 8/18/16 16:23 Dimethyl phthalate BRL mg/kg dry 0.39 0.052 1 8270D 8/18/16 16:23 Di-n-butyl phthalate BRL mg/kg dry 0.39 0.056 1 8270D 8/18/16 16:23 Di-n-octyl phthalate BRL mg/kg dry 0.39 0.048 1 8270D 8/18/16 16:23 Fluoranthene BRL mg/kg dry 0.39 0.050 1 8270D 8/18/16 16:23 Fluorene BRL mg/kg dry 0.39 0.057 1 8270D 8/18/16 16:23 Hexachlorobenzene BRL mg/kg dry 0.39 0.063 1 8270D 8/18/16 16:23 Hexachlorobutadiene BRL mg/kg dry 0.39 0.071 1 8270D 8/18/16 16:23 Hexachlorocyclopentadiene BRL mg/kg dry 0.39 0.070 1 8270D 8/18/16 16:23 Hexachloroethane BRL mg/kg dry 0.39 0.066 1 8270D 8/18/16 16:23 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.39 0.045 1 8270D 8/18/16 16:23 Isophorone BRL mg/kg dry 0.39 0.053 1 8270D 8/18/16 16:23 Naphthalene BRL mg/kg dry 0.39 0.063 1 8270D 8/18/16 16:23 Nitrobenzene BRL mg/kg dry 0.39 0.056 1 8270D 8/18/16 16:23 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.39 0.062 1 8270D 8/18/16 16:23 N-Nitrosodiphenylamine BRL mg/kg dry 0.39 0.060 1 8270D 8/18/16 16:23 Pentachlorophenol BRL mg/kg dry 0.39 0.047 1 8270D 8/18/16 16:23 Phenanthrene BRL mg/kg dry 0.39 0.051 1 8270D 8/18/16 16:23 Phenol BRL mg/kg dry 0.39 0.058 1 8270D 8/18/16 16:23 Pyrene BRL mg/kg dry 0.39 0.052 1 8270D 8/18/16 16:23 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 56 % 39-132 2-Fluorobiphenyl 52 % 44-115 2-Fluorophenol 53 % 35-115 Nitrobenzene-d5 48 % 37-122 Phenol-d5 54 % 34-121 Terphenyl-d14 51 % 54-127 SR Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0032 0.00026 1 8260B 8/18/16 20:44 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0032 0.00016 1 8260B 8/18/16 20:44 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: NW-1 Prism Sample ID: 6080270-01 Prism Work Order: 6080270 Time Collected: 08/11/16 11:40 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0032 0.00022 1 8260B 8/18/16 20:44 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0032 0.00028 1 8260B 8/18/16 20:44 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0032 0.000089 1 8260B 8/18/16 20:44 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0032 0.00014 1 8260B 8/18/16 20:44 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0032 0.00018 1 8260B 8/18/16 20:44 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0032 0.00018 1 8260B 8/18/16 20:44 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0032 0.00041 1 8260B 8/18/16 20:44 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0032 0.00024 1 8260B 8/18/16 20:44 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0032 0.00025 1 8260B 8/18/16 20:44 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0032 0.00013 1 8260B 8/18/16 20:44 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0032 0.00015 1 8260B 8/18/16 20:44 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0032 0.00019 1 8260B 8/18/16 20:44 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0032 0.00020 1 8260B 8/18/16 20:44 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0032 0.00024 1 8260B 8/18/16 20:44 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0032 0.00021 1 8260B 8/18/16 20:44 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0032 0.00016 1 8260B 8/18/16 20:44 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0032 0.00013 1 8260B 8/18/16 20:44 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0032 0.00015 1 8260B 8/18/16 20:44 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0032 0.00017 1 8260B 8/18/16 20:44 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0032 0.00019 1 8260B 8/18/16 20:44 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0032 0.00015 1 8260B 8/18/16 20:44 ANG P61-10336 Acetone BRL mg/kg dry 0.032 0.00078 1 8260B 8/18/16 20:44 ANG P61-10336 Benzene BRL mg/kg dry 0.0019 0.00019 1 8260B 8/18/16 20:44 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0032 0.00027 1 8260B 8/18/16 20:44 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0032 0.00018 1 8260B 8/18/16 20:44 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0032 0.00018 1 8260B 8/18/16 20:44 ANG P61-10336 Bromoform BRL mg/kg dry 0.0032 0.00037 1 8260B 8/18/16 20:44 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0064 0.00040 1 8260B 8/18/16 20:44 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0032 0.00016 1 8260B 8/18/16 20:44 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0032 0.00017 1 8260B 8/18/16 20:44 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0064 0.00027 1 8260B 8/18/16 20:44 ANG P61-10336 Chloroform BRL mg/kg dry 0.0032 0.00023 1 8260B 8/18/16 20:44 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0032 0.00022 1 8260B 8/18/16 20:44 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0032 0.00014 1 8260B 8/18/16 20:44 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0032 0.00011 1 8260B 8/18/16 20:44 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0032 0.00013 1 8260B 8/18/16 20:44 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0032 0.00015 1 8260B 8/18/16 20:44 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0032 0.00012 1 8260B 8/18/16 20:44 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0032 0.00013 1 8260B 8/18/16 20:44 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0032 0.00019 1 8260B 8/18/16 20:44 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0064 0.00030 1 8260B 8/18/16 20:44 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.032 0.00029 1 8260B 8/18/16 20:44 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.064 0.00029 1 8260B 8/18/16 20:44 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: NW-1 Attn: Brian Olin Prism Sample ID: 6080270-01 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 11:40 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.032 0.00027 1 8260B 8/18/16 20:44 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0032 0.00018 1 8260B 8/18/16 20:44 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0064 0.00010 1 8260B 8/18/16 20:44 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0064 0.00010 1 8260B 8/18/16 20:44 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0032 0.00016 1 8260B 8/18/16 20:44 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0032 0.00019 1 8260B 8/18/16 20:44 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0032 0.00013 1 8260B 8/18/16 20:44 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0032 0.00016 1 8260B 8/18/16 20:44 ANG P61-10336 Styrene BRL mg/kg dry 0.0032 0.00019 1 8260B 8/18/16 20:44 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0032 0.00011 1 8260B 8/18/16 20:44 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0032 0.00015 1 8260B 8/18/16 20:44 ANG P61-10336 Toluene BRL mg/kg dry 0.0032 0.00018 1 8260B 8/18/16 20:44 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0032 0.00019 1 8260B 8/18/16 20:44 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0032 0.00017 1 8260B 8/18/16 20:44 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0032 0.00021 1 8260B 8/18/16 20:44 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0032 0.00021 1 8260B 8/18/16 20:44 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.016 0.00044 1 8260B 8/18/16 20:44 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0032 0.00016 1 8260B 8/18/16 20:44 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0096 0.00060 1 8260B 8/18/16 20:44 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 103 % 70-130 Dibromofluoromethane 92 % 84-123 Toluene-d8 104 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 16 0.50 100 MADEP VPH 8/19/16 16:14 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 16 1.9 100 MADEP VPH 8/19/16 16:14 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 16 0.16 100 MADEP VPH 8/19/16 16:14 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 104 % 70-130 2,5-Dibromotoluene (FID) 131 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: EW-1 Attn: Brian Olin Prism Sample ID: 6080270-02 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 11:50 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics 4500 mg/kg dry 310 13 10 MADEP EPH 8/18/16 23:17 ZRC P6H0227 C19-C36 Aliphatics 2100 mg/kg dry 310 25 10 MADEP EPH 8/18/16 23:17 ZRC P6H0227 C11-C22 Aromatics 2300 mg/kg dry 120 17 10 MADEP EPH 8/18/16 23:17 ZRC P6H0227 Surrogate Recovery Control Limits 1-Chlorooctadecane 0 % 40-140 DO o-Terphenyl 0 % 40-140 DO 2-Fluorobiphenyl 0 % 40-140 DO 2-Bromonaphthalene 0 % 40-140 DO General Chemistry Parameters % Solids 81.3 % by 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.81 0.13 1 8270D 8/18/16 23:02 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.81 0.16 1 8270D 8/18/16 23:02 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.81 0.15 1 8270D 8/18/16 23:02 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.81 0.16 1 8270D 8/18/16 23:02 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.81 0.098 1 8270D 8/18/16 23:02 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.81 0.13 1 8270D 8/18/16 23:02 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.81 0.10 1 8270D 8/18/16 23:02 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.81 0.15 1 8270D 8/18/16 23:02 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.81 0.16 1 8270D 8/18/16 23:02 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.81 0.10 1 8270D 8/18/16 23:02 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.81 0.14 1 8270D 8/18/16 23:02 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.81 0.097 1 8270D 8/18/16 23:02 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.81 0.13 1 8270D 8/18/16 23:02 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 Anthracene BRL mg/kg dry 0.81 0.13 1 8270D 8/18/16 23:02 JMV P61-10314 Azobenzene BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.81 0.088 1 8270D 8/18/16 23:02 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 87 Laboratory Report ` Full -Service Analytical & P R S M / environmental Solutions LABORATORIES INC. 08/22/2016 ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: EW-1 Attn: Brian Olin Prism Sample ID: 6080270-02 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 11:50 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.81 0.094 1 8270D 8/18/16 23:02 JMV P61-10314 Benzo(g,h,i)perylene BRL mg/kg dry 0.81 0.089 1 8270D 8/18/16 23:02 JMV P61-10314 Benzo(k)fluoranthene BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 Benzoic Acid BRL mg/kg dry 0.81 0.068 1 8270D 8/18/16 23:02 JMV P61-10314 Benzyl alcohol BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.81 0.14 1 8270D 8/18/16 23:02 JMV P61-10314 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.81 0.14 1 8270D 8/18/16 23:02 JMV P61-10314 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 Butyl benzyl phthalate BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 Chrysene BRL mg/kg dry 0.81 0.10 1 8270D 8/18/16 23:02 JMV P61-10314 Dibenzo(a,h)anthracene BRL mg/kg dry 0.81 0.099 1 8270D 8/18/16 23:02 JMV P61-10314 Dibenzofuran BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 Diethyl phthalate BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 Dimethyl phthalate BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 Di-n-butyl phthalate BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 Di-n-octyl phthalate BRL mg/kg dry 0.81 0.10 1 8270D 8/18/16 23:02 JMV P61-10314 Fluoranthene BRL mg/kg dry 0.81 0.10 1 8270D 8/18/16 23:02 JMV P61-10314 Fluorene BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 Hexachlorobenzene BRL mg/kg dry 0.81 0.13 1 8270D 8/18/16 23:02 JMV P61-10314 Hexachlorobutadiene BRL mg/kg dry 0.81 0.15 1 8270D 8/18/16 23:02 JMV P61-10314 Hexachlorocyclopentadiene BRL mg/kg dry 0.81 0.14 1 8270D 8/18/16 23:02 JMV P61-10314 Hexachloroethane BRL mg/kg dry 0.81 0.14 1 8270D 8/18/16 23:02 JMV P61-10314 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.81 0.093 1 8270D 8/18/16 23:02 JMV P61-10314 Isophorone BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 Naphthalene BRL mg/kg dry 0.81 0.13 1 8270D 8/18/16 23:02 JMV P61-10314 Nitrobenzene BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.81 0.13 1 8270D 8/18/16 23:02 JMV P61-10314 N-Nitrosodiphenylamine BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 Pentachlorophenol BRL mg/kg dry 0.81 0.096 1 8270D 8/18/16 23:02 JMV P61-10314 Phenanthrene BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 Phenol BRL mg/kg dry 0.81 0.12 1 8270D 8/18/16 23:02 JMV P61-10314 Pyrene BRL mg/kg dry 0.81 0.11 1 8270D 8/18/16 23:02 JMV P61-10314 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 154 % 39-132 SR 2-Fluorobiphenyl 94 % 44-115 SR 2-Fluorophenol 88 % 35-115 Nitrobenzene-d5 102 % 37-122 Phenol-d5 93 % 34-121 Terphenyl-d14 76 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0056 0.00046 1 8260B 8/19/16 23:53 ANG P61-10365 1,1,1-Trichloroethane BRL mg/kg dry 0.0056 0.00027 1 8260B 8/19/16 23:53 ANG P61-10365 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: EW-1 Prism Sample ID: 6080270-02 Prism Work Order: 6080270 Time Collected: 08/11/16 11:50 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0056 0.00038 1 8260B 8/19/16 23:53 ANG P61-10365 1,1,2-Trichloroethane BRL mg/kg dry 0.0056 0.00050 1 8260B 8/19/16 23:53 ANG P61-10365 1,1-Dichloroethane BRL mg/kg dry 0.0056 0.00016 1 8260B 8/19/16 23:53 ANG P61-10365 1,1-Dichloroethylene BRL mg/kg dry 0.0056 0.00025 1 8260B 8/19/16 23:53 ANG P61-10365 1,1-Dichloropropylene BRL mg/kg dry 0.0056 0.00031 1 8260B 8/19/16 23:53 ANG P61-10365 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0056 0.00032 1 8260B 8/19/16 23:53 ANG P61-10365 1,2,3-Trichloropropane BRL mg/kg dry 0.0056 0.00071 1 8260B 8/19/16 23:53 ANG P61-10365 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0056 0.00042 1 8260B 8/19/16 23:53 ANG P61-10365 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0056 0.00043 1 8260B 8/19/16 23:53 ANG P61-10365 1,2-Dibromoethane BRL mg/kg dry 0.0056 0.00022 1 8260B 8/19/16 23:53 ANG P61-10365 1,2-Dichlorobenzene BRL mg/kg dry 0.0056 0.00026 1 8260B 8/19/16 23:53 ANG P61-10365 1,2-Dichloroethane BRL mg/kg dry 0.0056 0.00033 1 8260B 8/19/16 23:53 ANG P61-10365 1,2-Dichloropropane BRL mg/kg dry 0.0056 0.00035 1 8260B 8/19/16 23:53 ANG P61-10365 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0056 0.00042 1 8260B 8/19/16 23:53 ANG P61-10365 1,3-Dichlorobenzene BRL mg/kg dry 0.0056 0.00037 1 8260B 8/19/16 23:53 ANG P61-10365 1,3-Dichloropropane BRL mg/kg dry 0.0056 0.00028 1 8260B 8/19/16 23:53 ANG P61-10365 1,4-Dichlorobenzene BRL mg/kg dry 0.0056 0.00022 1 8260B 8/19/16 23:53 ANG P61-10365 2,2-Dichloropropane BRL mg/kg dry 0.0056 0.00027 1 8260B 8/19/16 23:53 ANG P61-10365 2-Chlorotoluene BRL mg/kg dry 0.0056 0.00029 1 8260B 8/19/16 23:53 ANG P61-10365 4-Chlorotoluene BRL mg/kg dry 0.0056 0.00033 1 8260B 8/19/16 23:53 ANG P61-10365 4-Isopropyltoluene BRL mg/kg dry 0.0056 0.00027 1 8260B 8/19/16 23:53 ANG P61-10365 Acetone 0.12 mg/kg dry 0.056 0.0014 1 8260B 8/19/16 23:53 ANG P6H0365 Benzene BRL mg/kg dry 0.0034 0.00033 1 8260B 8/19/16 23:53 ANG P61-10365 Bromobenzene BRL mg/kg dry 0.0056 0.00047 1 8260B 8/19/16 23:53 ANG P61-10365 Bromochloromethane BRL mg/kg dry 0.0056 0.00031 1 8260B 8/19/16 23:53 ANG P61-10365 Bromodichloromethane BRL mg/kg dry 0.0056 0.00031 1 8260B 8/19/16 23:53 ANG P61-10365 Bromoform BRL mg/kg dry 0.0056 0.00063 1 8260B 8/19/16 23:53 ANG P61-10365 Bromomethane BRL mg/kg dry 0.011 0.00069 1 8260B 8/19/16 23:53 ANG P61-10365 Carbon Tetrachloride BRL mg/kg dry 0.0056 0.00028 1 8260B 8/19/16 23:53 ANG P61-10365 Chlorobenzene BRL mg/kg dry 0.0056 0.00030 1 8260B 8/19/16 23:53 ANG P61-10365 Chloroethane BRL mg/kg dry 0.011 0.00047 1 8260B 8/19/16 23:53 ANG P61-10365 Chloroform BRL mg/kg dry 0.0056 0.00040 1 8260B 8/19/16 23:53 ANG P61-10365 Chloromethane BRL mg/kg dry 0.0056 0.00038 1 8260B 8/19/16 23:53 ANG P61-10365 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0056 0.00024 1 8260B 8/19/16 23:53 ANG P61-10365 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0056 0.00019 1 8260B 8/19/16 23:53 ANG P61-10365 Dibromochloromethane BRL mg/kg dry 0.0056 0.00023 1 8260B 8/19/16 23:53 ANG P61-10365 Dichlorodifluoromethane BRL mg/kg dry 0.0056 0.00025 1 8260B 8/19/16 23:53 ANG P61-10365 Ethylbenzene BRL mg/kg dry 0.0056 0.00021 1 8260B 8/19/16 23:53 ANG P61-10365 Isopropyl Ether BRL mg/kg dry 0.0056 0.00023 1 8260B 8/19/16 23:53 ANG P61-10365 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0056 0.00033 1 8260B 8/19/16 23:53 ANG P61-10365 m,p-Xylenes BRL mg/kg dry 0.011 0.00052 1 8260B 8/19/16 23:53 ANG P61-10365 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.056 0.00051 1 8260B 8/19/16 23:53 ANG P61-10365 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.11 0.00051 1 8260B 8/19/16 23:53 ANG P61-10365 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: EW-1 Attn: Brian Olin Prism Sample ID: 6080270-02 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 11:50 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.056 0.00048 1 8260B 8/19/16 23:53 ANG P61-10365 Methylene Chloride BRL mg/kg dry 0.0056 0.00031 1 8260B 8/19/16 23:53 ANG P61-10365 Methyl-tert-Butyl Ether BRL mg/kg dry 0.011 0.00018 1 8260B 8/19/16 23:53 ANG P61-10365 Naphthalene BRL mg/kg dry 0.011 0.00018 1 8260B 8/19/16 23:53 ANG P61-10365 n-Butylbenzene BRL mg/kg dry 0.0056 0.00029 1 8260B 8/19/16 23:53 ANG P61-10365 n-Propylbenzene BRL mg/kg dry 0.0056 0.00033 1 8260B 8/19/16 23:53 ANG P61-10365 o-Xylene BRL mg/kg dry 0.0056 0.00023 1 8260B 8/19/16 23:53 ANG P61-10365 sec-Butylbenzene BRL mg/kg dry 0.0056 0.00027 1 8260B 8/19/16 23:53 ANG P61-10365 Styrene BRL mg/kg dry 0.0056 0.00034 1 8260B 8/19/16 23:53 ANG P61-10365 tert-Butylbenzene BRL mg/kg dry 0.0056 0.00019 1 8260B 8/19/16 23:53 ANG P61-10365 Tetrachloroethylene BRL mg/kg dry 0.0056 0.00027 1 8260B 8/19/16 23:53 ANG P61-10365 Toluene BRL mg/kg dry 0.0056 0.00032 1 8260B 8/19/16 23:53 ANG P61-10365 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0056 0.00033 1 8260B 8/19/16 23:53 ANG P61-10365 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0056 0.00029 1 8260B 8/19/16 23:53 ANG P61-10365 Trichloroethylene BRL mg/kg dry 0.0056 0.00036 1 8260B 8/19/16 23:53 ANG P61-10365 Trichlorofluoromethane BRL mg/kg dry 0.0056 0.00036 1 8260B 8/19/16 23:53 ANG P61-10365 Vinyl acetate BRL mg/kg dry 0.028 0.00077 1 8260B 8/19/16 23:53 ANG P61-10365 Vinyl chloride BRL mg/kg dry 0.0056 0.00027 1 8260B 8/19/16 23:53 ANG P61-10365 Xylenes, total BRL mg/kg dry 0.017 0.0010 1 8260B 8/19/16 23:53 ANG P61-10365 Surrogate Recovery Control Limits 4-Bromofluorobenzene 92 % 70-130 Dibromofluoromethane 105 % 84-123 Toluene-d8 104 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 21 0.65 100 MADEP VPH 8/20/16 0:24 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 21 2.5 100 MADEP VPH 8/20/16 0:24 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 21 0.20 100 MADEP VPH 8/20/16 0:24 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 94 % 70-130 2,5-Dibromotoluene (FID) 123 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: SW-1 Attn: Brian Olin Prism Sample ID: 6080270-03 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 12:05 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 27 1.2 1 MADEP EPH 8/18/16 14:46 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 27 2.2 1 MADEP EPH 8/18/16 14:46 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 11 1.5 1 MADEP EPH 8/18/16 14:46 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 78 % 40-140 o-Terphenyl 76 % 40-140 2-Fluorobiphenyl 96 % 40-140 2-Bromonaphthalene 112 % 40-140 General Chemistry Parameters % Solids 91.3 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.36 0.056 1 8270D 8/18/16 16:45 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 16:45 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 16:45 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.36 0.053 1 8270D 8/18/16 16:45 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.36 0.070 1 8270D 8/18/16 16:45 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.36 0.068 1 8270D 8/18/16 16:45 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.36 0.070 1 8270D 8/18/16 16:45 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 16:45 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.36 0.050 1 8270D 8/18/16 16:45 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 16:45 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 16:45 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 16:45 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 16:45 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.36 0.058 1 8270D 8/18/16 16:45 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.36 0.046 1 8270D 8/18/16 16:45 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.36 0.066 1 8270D 8/18/16 16:45 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.36 0.071 1 8270D 8/18/16 16:45 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 16:45 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.36 0.054 1 8270D 8/18/16 16:45 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.36 0.062 1 8270D 8/18/16 16:45 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 16:45 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.36 0.043 1 8270D 8/18/16 16:45 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 16:45 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.36 0.056 1 8270D 8/18/16 16:45 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.36 0.049 1 8270D 8/18/16 16:45 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 16:45 JMV P61-10314 Anthracene BRL mg/kg dry 0.36 0.058 1 8270D 8/18/16 16:45 JMV P61-10314 Azobenzene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 16:45 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 16:45 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.36 0.039 1 8270D 8/18/16 16:45 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: SW-1 Prism Sample ID: 6080270-03 Prism Work Order: 6080270 Time Collected: 08/11/16 12:05 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.36 0.042 1 8270D 8/18/16 16:45 Benzo(g,h,i)perylene BRL mg/kg dry 0.36 0.040 1 8270D 8/18/16 16:45 Benzo(k)fluoranthene BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 16:45 Benzoic Acid BRL mg/kg dry 0.36 0.030 1 8270D 8/18/16 16:45 Benzyl alcohol BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 16:45 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.36 0.063 1 8270D 8/18/16 16:45 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 16:45 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.36 0.062 1 8270D 8/18/16 16:45 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.36 0.054 1 8270D 8/18/16 16:45 Butyl benzyl phthalate BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 16:45 Chrysene BRL mg/kg dry 0.36 0.045 1 8270D 8/18/16 16:45 Dibenzo(a,h)anthracene BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 16:45 Dibenzofuran BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 16:45 Diethyl phthalate BRL mg/kg dry 0.36 0.050 1 8270D 8/18/16 16:45 Dimethyl phthalate BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 16:45 Di-n-butyl phthalate BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 16:45 Di-n-octyl phthalate BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 16:45 Fluoranthene BRL mg/kg dry 0.36 0.046 1 8270D 8/18/16 16:45 Fluorene BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 16:45 Hexachlorobenzene BRL mg/kg dry 0.36 0.057 1 8270D 8/18/16 16:45 Hexachlorobutadiene BRL mg/kg dry 0.36 0.065 1 8270D 8/18/16 16:45 Hexachlorocyclopentadiene BRL mg/kg dry 0.36 0.064 1 8270D 8/18/16 16:45 Hexachloroethane BRL mg/kg dry 0.36 0.060 1 8270D 8/18/16 16:45 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.36 0.041 1 8270D 8/18/16 16:45 Isophorone BRL mg/kg dry 0.36 0.049 1 8270D 8/18/16 16:45 Naphthalene BRL mg/kg dry 0.36 0.058 1 8270D 8/18/16 16:45 Nitrobenzene BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 16:45 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.36 0.057 1 8270D 8/18/16 16:45 N-Nitrosodiphenylamine BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 16:45 Pentachlorophenol BRL mg/kg dry 0.36 0.043 1 8270D 8/18/16 16:45 Phenanthrene BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 16:45 Phenol BRL mg/kg dry 0.36 0.053 1 8270D 8/18/16 16:45 Pyrene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 16:45 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 64 % 39-132 2-Fluorobiphenyl 61 % 44-115 2-Fluorophenol 64 % 35-115 Nitrobenzene-d5 58 % 37-122 Phenol-d5 64 % 34-121 Terphenyl-d14 66 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0033 0.00027 1 8260B 8/18/16 21:11 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0033 0.00016 1 8260B 8/18/16 21:11 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: SW-1 Prism Sample ID: 6080270-03 Prism Work Order: 6080270 Time Collected: 08/11/16 12:05 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0033 0.00022 1 8260B 8/18/16 21:11 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0033 0.00029 1 8260B 8/18/16 21:11 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0033 0.000090 1 8260B 8/18/16 21:11 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0033 0.00014 1 8260B 8/18/16 21:11 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0033 0.00018 1 8260B 8/18/16 21:11 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0033 0.00018 1 8260B 8/18/16 21:11 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0033 0.00042 1 8260B 8/18/16 21:11 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0033 0.00024 1 8260B 8/18/16 21:11 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0033 0.00025 1 8260B 8/18/16 21:11 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0033 0.00013 1 8260B 8/18/16 21:11 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0033 0.00015 1 8260B 8/18/16 21:11 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0033 0.00019 1 8260B 8/18/16 21:11 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0033 0.00020 1 8260B 8/18/16 21:11 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0033 0.00025 1 8260B 8/18/16 21:11 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0033 0.00022 1 8260B 8/18/16 21:11 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0033 0.00016 1 8260B 8/18/16 21:11 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0033 0.00013 1 8260B 8/18/16 21:11 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0033 0.00015 1 8260B 8/18/16 21:11 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0033 0.00017 1 8260B 8/18/16 21:11 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0033 0.00019 1 8260B 8/18/16 21:11 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0033 0.00016 1 8260B 8/18/16 21:11 ANG P61-10336 Acetone BRL mg/kg dry 0.033 0.00079 1 8260B 8/18/16 21:11 ANG P61-10336 Benzene BRL mg/kg dry 0.0020 0.00019 1 8260B 8/18/16 21:11 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0033 0.00027 1 8260B 8/18/16 21:11 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0033 0.00018 1 8260B 8/18/16 21:11 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0033 0.00018 1 8260B 8/18/16 21:11 ANG P61-10336 Bromoform BRL mg/kg dry 0.0033 0.00037 1 8260B 8/18/16 21:11 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0065 0.00040 1 8260B 8/18/16 21:11 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0033 0.00016 1 8260B 8/18/16 21:11 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0033 0.00017 1 8260B 8/18/16 21:11 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0065 0.00027 1 8260B 8/18/16 21:11 ANG P61-10336 Chloroform BRL mg/kg dry 0.0033 0.00023 1 8260B 8/18/16 21:11 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0033 0.00022 1 8260B 8/18/16 21:11 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0033 0.00014 1 8260B 8/18/16 21:11 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0033 0.00011 1 8260B 8/18/16 21:11 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0033 0.00013 1 8260B 8/18/16 21:11 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0033 0.00015 1 8260B 8/18/16 21:11 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0033 0.00012 1 8260B 8/18/16 21:11 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0033 0.00013 1 8260B 8/18/16 21:11 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0033 0.00019 1 8260B 8/18/16 21:11 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0065 0.00030 1 8260B 8/18/16 21:11 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.033 0.00029 1 8260B 8/18/16 21:11 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.065 0.00029 1 8260B 8/18/16 21:11 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: SW-1 Attn: Brian Olin Prism Sample ID: 6080270-03 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 12:05 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.033 0.00028 1 8260B 8/18/16 21:11 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0033 0.00018 1 8260B 8/18/16 21:11 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0065 0.00010 1 8260B 8/18/16 21:11 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0065 0.00010 1 8260B 8/18/16 21:11 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0033 0.00017 1 8260B 8/18/16 21:11 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0033 0.00019 1 8260B 8/18/16 21:11 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0033 0.00013 1 8260B 8/18/16 21:11 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0033 0.00016 1 8260B 8/18/16 21:11 ANG P61-10336 Styrene BRL mg/kg dry 0.0033 0.00020 1 8260B 8/18/16 21:11 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0033 0.00011 1 8260B 8/18/16 21:11 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0033 0.00015 1 8260B 8/18/16 21:11 ANG P61-10336 Toluene BRL mg/kg dry 0.0033 0.00019 1 8260B 8/18/16 21:11 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0033 0.00019 1 8260B 8/18/16 21:11 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0033 0.00017 1 8260B 8/18/16 21:11 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0033 0.00021 1 8260B 8/18/16 21:11 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0033 0.00021 1 8260B 8/18/16 21:11 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.016 0.00045 1 8260B 8/18/16 21:11 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0033 0.00016 1 8260B 8/18/16 21:11 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0098 0.00061 1 8260B 8/18/16 21:11 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 70-130 Dibromofluoromethane 92 % 84-123 Toluene-d8 102 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 16 0.49 100 MADEP VPH 8/19/16 16:44 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 16 1.9 100 MADEP VPH 8/19/16 16:44 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 16 0.15 100 MADEP VPH 8/19/16 16:44 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 99 % 70-130 2,5-Dibromotoluene (FID) 124 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: WW-1 Attn: Brian Olin Prism Sample ID: 6080270-04 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 12:20 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 26 1.1 1 MADEP EPH 8/18/16 15:23 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 26 2.1 1 MADEP EPH 8/18/16 15:23 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 10 1.4 1 MADEP EPH 8/18/16 15:23 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 67 % 40-140 o-Terphenyl 66 % 40-140 2-Fluorobiphenyl 93 % 40-140 2-Bromonaphthalene 104 % 40-140 General Chemistry Parameters % Solids 95.1 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.34 0.053 1 8270D 8/18/16 17:07 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.34 0.052 1 8270D 8/18/16 17:07 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.34 0.048 1 8270D 8/18/16 17:07 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.34 0.050 1 8270D 8/18/16 17:07 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.34 0.066 1 8270D 8/18/16 17:07 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.34 0.064 1 8270D 8/18/16 17:07 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.34 0.066 1 8270D 8/18/16 17:07 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.34 0.052 1 8270D 8/18/16 17:07 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.34 0.048 1 8270D 8/18/16 17:07 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.34 0.042 1 8270D 8/18/16 17:07 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.34 0.046 1 8270D 8/18/16 17:07 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.34 0.050 1 8270D 8/18/16 17:07 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.34 0.049 1 8270D 8/18/16 17:07 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.34 0.055 1 8270D 8/18/16 17:07 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.34 0.044 1 8270D 8/18/16 17:07 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.34 0.062 1 8270D 8/18/16 17:07 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.34 0.068 1 8270D 8/18/16 17:07 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.34 0.042 1 8270D 8/18/16 17:07 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.34 0.051 1 8270D 8/18/16 17:07 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.34 0.059 1 8270D 8/18/16 17:07 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.34 0.048 1 8270D 8/18/16 17:07 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.34 0.041 1 8270D 8/18/16 17:07 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.34 0.044 1 8270D 8/18/16 17:07 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.34 0.053 1 8270D 8/18/16 17:07 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.34 0.047 1 8270D 8/18/16 17:07 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.34 0.050 1 8270D 8/18/16 17:07 JMV P61-10314 Anthracene BRL mg/kg dry 0.34 0.055 1 8270D 8/18/16 17:07 JMV P61-10314 Azobenzene BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 17:07 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 17:07 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.34 0.037 1 8270D 8/18/16 17:07 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: WW-1 Prism Sample ID: 6080270-04 Prism Work Order: 6080270 Time Collected: 08/11/16 12:20 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.34 0.040 1 8270D 8/18/16 17:07 Benzo(g,h,i)perylene BRL mg/kg dry 0.34 0.038 1 8270D 8/18/16 17:07 Benzo(k)fluoranthene BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 17:07 Benzoic Acid BRL mg/kg dry 0.34 0.029 1 8270D 8/18/16 17:07 Benzyl alcohol BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 17:07 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.34 0.059 1 8270D 8/18/16 17:07 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.34 0.048 1 8270D 8/18/16 17:07 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.34 0.058 1 8270D 8/18/16 17:07 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.34 0.051 1 8270D 8/18/16 17:07 Butyl benzyl phthalate BRL mg/kg dry 0.34 0.049 1 8270D 8/18/16 17:07 Chrysene BRL mg/kg dry 0.34 0.043 1 8270D 8/18/16 17:07 Dibenzo(a,h)anthracene BRL mg/kg dry 0.34 0.042 1 8270D 8/18/16 17:07 Dibenzofuran BRL mg/kg dry 0.34 0.052 1 8270D 8/18/16 17:07 Diethyl phthalate BRL mg/kg dry 0.34 0.047 1 8270D 8/18/16 17:07 Dimethyl phthalate BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 17:07 Di-n-butyl phthalate BRL mg/kg dry 0.34 0.049 1 8270D 8/18/16 17:07 Di-n-octyl phthalate BRL mg/kg dry 0.34 0.042 1 8270D 8/18/16 17:07 Fluoranthene BRL mg/kg dry 0.34 0.044 1 8270D 8/18/16 17:07 Fluorene BRL mg/kg dry 0.34 0.049 1 8270D 8/18/16 17:07 Hexachlorobenzene BRL mg/kg dry 0.34 0.054 1 8270D 8/18/16 17:07 Hexachlorobutadiene BRL mg/kg dry 0.34 0.061 1 8270D 8/18/16 17:07 Hexachlorocyclopentadiene BRL mg/kg dry 0.34 0.061 1 8270D 8/18/16 17:07 Hexachloroethane BRL mg/kg dry 0.34 0.057 1 8270D 8/18/16 17:07 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.34 0.039 1 8270D 8/18/16 17:07 Isophorone BRL mg/kg dry 0.34 0.046 1 8270D 8/18/16 17:07 Naphthalene BRL mg/kg dry 0.34 0.055 1 8270D 8/18/16 17:07 Nitrobenzene BRL mg/kg dry 0.34 0.049 1 8270D 8/18/16 17:07 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.34 0.054 1 8270D 8/18/16 17:07 N-Nitrosodiphenylamine BRL mg/kg dry 0.34 0.052 1 8270D 8/18/16 17:07 Pentachlorophenol BRL mg/kg dry 0.34 0.040 1 8270D 8/18/16 17:07 Phenanthrene BRL mg/kg dry 0.34 0.044 1 8270D 8/18/16 17:07 Phenol BRL mg/kg dry 0.34 0.051 1 8270D 8/18/16 17:07 Pyrene BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 17:07 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 78 % 39-132 2-Fluorobiphenyl 68 % 44-115 2-Fluorophenol 68 % 35-115 Nitrobenzene-d5 62 % 37-122 Phenol-d5 69 % 34-121 Terphenyl-d14 73 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0027 0.00022 1 8260B 8/18/16 21:39 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0027 0.00013 1 8260B 8/18/16 21:39 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: WW-1 Prism Sample ID: 6080270-04 Prism Work Order: 6080270 Time Collected: 08/11/16 12:20 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0027 0.00018 1 8260B 8/18/16 21:39 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0027 0.00024 1 8260B 8/18/16 21:39 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0027 0.000075 1 8260B 8/18/16 21:39 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0027 0.00012 1 8260B 8/18/16 21:39 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0027 0.00015 1 8260B 8/18/16 21:39 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0027 0.00015 1 8260B 8/18/16 21:39 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0027 0.00034 1 8260B 8/18/16 21:39 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0027 0.00020 1 8260B 8/18/16 21:39 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0027 0.00021 1 8260B 8/18/16 21:39 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0027 0.00011 1 8260B 8/18/16 21:39 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/18/16 21:39 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0027 0.00016 1 8260B 8/18/16 21:39 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0027 0.00017 1 8260B 8/18/16 21:39 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0027 0.00020 1 8260B 8/18/16 21:39 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0027 0.00018 1 8260B 8/18/16 21:39 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0027 0.00013 1 8260B 8/18/16 21:39 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0027 0.00011 1 8260B 8/18/16 21:39 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0027 0.00013 1 8260B 8/18/16 21:39 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/18/16 21:39 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/18/16 21:39 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/18/16 21:39 ANG P61-10336 Acetone 0.037 mg/kg dry 0.027 0.00066 1 8260B 8/18/16 21:39 ANG P6H0336 Benzene BRL mg/kg dry 0.0016 0.00016 1 8260B 8/18/16 21:39 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0027 0.00022 1 8260B 8/18/16 21:39 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0027 0.00015 1 8260B 8/18/16 21:39 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0027 0.00015 1 8260B 8/18/16 21:39 ANG P61-10336 Bromoform BRL mg/kg dry 0.0027 0.00031 1 8260B 8/18/16 21:39 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0054 0.00033 1 8260B 8/18/16 21:39 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0027 0.00013 1 8260B 8/18/16 21:39 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/18/16 21:39 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0054 0.00022 1 8260B 8/18/16 21:39 ANG P61-10336 Chloroform BRL mg/kg dry 0.0027 0.00019 1 8260B 8/18/16 21:39 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0027 0.00018 1 8260B 8/18/16 21:39 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0027 0.00011 1 8260B 8/18/16 21:39 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0027 0.000090 1 8260B 8/18/16 21:39 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0027 0.00011 1 8260B 8/18/16 21:39 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0027 0.00012 1 8260B 8/18/16 21:39 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0027 0.00010 1 8260B 8/18/16 21:39 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0027 0.00011 1 8260B 8/18/16 21:39 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0027 0.00016 1 8260B 8/18/16 21:39 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0054 0.00025 1 8260B 8/18/16 21:39 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.027 0.00024 1 8260B 8/18/16 21:39 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.054 0.00024 1 8260B 8/18/16 21:39 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: WW-1 Attn: Brian Olin Prism Sample ID: 6080270-04 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 12:20 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.027 0.00023 1 8260B 8/18/16 21:39 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0027 0.00015 1 8260B 8/18/16 21:39 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0054 0.000086 1 8260B 8/18/16 21:39 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0054 0.000085 1 8260B 8/18/16 21:39 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/18/16 21:39 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/18/16 21:39 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0027 0.00011 1 8260B 8/18/16 21:39 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/18/16 21:39 ANG P61-10336 Styrene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/18/16 21:39 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0027 0.000091 1 8260B 8/18/16 21:39 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/18/16 21:39 ANG P61-10336 Toluene BRL mg/kg dry 0.0027 0.00015 1 8260B 8/18/16 21:39 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/18/16 21:39 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/18/16 21:39 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0027 0.00017 1 8260B 8/18/16 21:39 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0027 0.00017 1 8260B 8/18/16 21:39 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.013 0.00037 1 8260B 8/18/16 21:39 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0027 0.00013 1 8260B 8/18/16 21:39 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0081 0.00050 1 8260B 8/18/16 21:39 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 100 % 70-130 Dibromofluoromethane 91 % 84-123 Toluene-d8 103 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 17 0.52 100 MADEP VPH 8/19/16 17:15 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 17 2.0 100 MADEP VPH 8/19/16 17:15 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 17 0.16 100 MADEP VPH 8/19/16 17:15 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 97 % 70-130 2,5-Dibromotoluene (FID) 122 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: B-1 Attn: Brian Olin Prism Sample ID: 6080270-05 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 12:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 28 1.2 1 MADEP EPH 8/18/16 15:59 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 28 2.3 1 MADEP EPH 8/18/16 15:59 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 11 1.5 1 MADEP EPH 8/18/16 15:59 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 76 % 40-140 o-Terphenyl 70 % 40-140 2-Fluorobiphenyl 99 % 40-140 2-Bromonaphthalene 115 % 40-140 General Chemistry Parameters % Solids 90.4 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.36 0.057 1 8270D 8/18/16 17:29 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 17:29 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 17:29 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.36 0.053 1 8270D 8/18/16 17:29 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.36 0.070 1 8270D 8/18/16 17:29 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.36 0.068 1 8270D 8/18/16 17:29 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.36 0.070 1 8270D 8/18/16 17:29 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.36 0.056 1 8270D 8/18/16 17:29 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 17:29 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 17:29 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 17:29 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.36 0.053 1 8270D 8/18/16 17:29 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 17:29 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.36 0.058 1 8270D 8/18/16 17:29 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 17:29 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.36 0.066 1 8270D 8/18/16 17:29 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.36 0.072 1 8270D 8/18/16 17:29 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.36 0.045 1 8270D 8/18/16 17:29 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 17:29 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.36 0.062 1 8270D 8/18/16 17:29 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 17:29 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 17:29 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 17:29 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.36 0.056 1 8270D 8/18/16 17:29 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.36 0.049 1 8270D 8/18/16 17:29 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.36 0.053 1 8270D 8/18/16 17:29 JMV P61-10314 Anthracene BRL mg/kg dry 0.36 0.059 1 8270D 8/18/16 17:29 JMV P61-10314 Azobenzene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 17:29 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 17:29 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.36 0.039 1 8270D 8/18/16 17:29 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: B-1 Prism Sample ID: 6080270-05 Prism Work Order: 6080270 Time Collected: 08/11/16 12:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.36 0.042 1 8270D 8/18/16 17:29 Benzo(g,h,i)perylene BRL mg/kg dry 0.36 0.040 1 8270D 8/18/16 17:29 Benzo(k)fluoranthene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 17:29 Benzoic Acid BRL mg/kg dry 0.36 0.031 1 8270D 8/18/16 17:29 Benzyl alcohol BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 17:29 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.36 0.063 1 8270D 8/18/16 17:29 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 17:29 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.36 0.062 1 8270D 8/18/16 17:29 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.36 0.054 1 8270D 8/18/16 17:29 Butyl benzyl phthalate BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 17:29 Chrysene BRL mg/kg dry 0.36 0.046 1 8270D 8/18/16 17:29 Dibenzo(a,h)anthracene BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 17:29 Dibenzofuran BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 17:29 Diethyl phthalate BRL mg/kg dry 0.36 0.050 1 8270D 8/18/16 17:29 Dimethyl phthalate BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 17:29 Di-n-butyl phthalate BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 17:29 Di-n-octyl phthalate BRL mg/kg dry 0.36 0.045 1 8270D 8/18/16 17:29 Fluoranthene BRL mg/kg dry 0.36 0.046 1 8270D 8/18/16 17:29 Fluorene BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 17:29 Hexachlorobenzene BRL mg/kg dry 0.36 0.058 1 8270D 8/18/16 17:29 Hexachlorobutadiene BRL mg/kg dry 0.36 0.065 1 8270D 8/18/16 17:29 Hexachlorocyclopentadiene BRL mg/kg dry 0.36 0.065 1 8270D 8/18/16 17:29 Hexachloroethane BRL mg/kg dry 0.36 0.061 1 8270D 8/18/16 17:29 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.36 0.042 1 8270D 8/18/16 17:29 Isophorone BRL mg/kg dry 0.36 0.049 1 8270D 8/18/16 17:29 Naphthalene BRL mg/kg dry 0.36 0.059 1 8270D 8/18/16 17:29 Nitrobenzene BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 17:29 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.36 0.057 1 8270D 8/18/16 17:29 N-Nitrosodiphenylamine BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 17:29 Pentachlorophenol BRL mg/kg dry 0.36 0.043 1 8270D 8/18/16 17:29 Phenanthrene BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 17:29 Phenol BRL mg/kg dry 0.36 0.054 1 8270D 8/18/16 17:29 Pyrene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 17:29 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 73 % 39-132 2-Fluorobiphenyl 65 % 44-115 2-Fluorophenol 69 % 35-115 Nitrobenzene-d5 63 % 37-122 Phenol-d5 71 % 34-121 Terphenyl-d14 70 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0028 0.00023 1 8260B 8/18/16 22:06 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0028 0.00014 1 8260B 8/18/16 22:06 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: B-1 Prism Sample ID: 6080270-05 Prism Work Order: 6080270 Time Collected: 08/11/16 12:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0028 0.00019 1 8260B 8/18/16 22:06 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0028 0.00025 1 8260B 8/18/16 22:06 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0028 0.000078 1 8260B 8/18/16 22:06 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0028 0.00012 1 8260B 8/18/16 22:06 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0028 0.00015 1 8260B 8/18/16 22:06 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0028 0.00016 1 8260B 8/18/16 22:06 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0028 0.00036 1 8260B 8/18/16 22:06 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0028 0.00021 1 8260B 8/18/16 22:06 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0028 0.00022 1 8260B 8/18/16 22:06 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0028 0.00011 1 8260B 8/18/16 22:06 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0028 0.00013 1 8260B 8/18/16 22:06 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0028 0.00017 1 8260B 8/18/16 22:06 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0028 0.00017 1 8260B 8/18/16 22:06 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0028 0.00021 1 8260B 8/18/16 22:06 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0028 0.00019 1 8260B 8/18/16 22:06 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0028 0.00014 1 8260B 8/18/16 22:06 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0028 0.00011 1 8260B 8/18/16 22:06 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0028 0.00013 1 8260B 8/18/16 22:06 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0028 0.00015 1 8260B 8/18/16 22:06 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0028 0.00017 1 8260B 8/18/16 22:06 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0028 0.00014 1 8260B 8/18/16 22:06 ANG P61-10336 Acetone BRL mg/kg dry 0.028 0.00069 1 8260B 8/18/16 22:06 ANG P61-10336 Benzene BRL mg/kg dry 0.0017 0.00016 1 8260B 8/18/16 22:06 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0028 0.00023 1 8260B 8/18/16 22:06 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0028 0.00015 1 8260B 8/18/16 22:06 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0028 0.00016 1 8260B 8/18/16 22:06 ANG P61-10336 Bromoform BRL mg/kg dry 0.0028 0.00032 1 8260B 8/18/16 22:06 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0056 0.00035 1 8260B 8/18/16 22:06 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0028 0.00014 1 8260B 8/18/16 22:06 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0028 0.00015 1 8260B 8/18/16 22:06 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0056 0.00023 1 8260B 8/18/16 22:06 ANG P61-10336 Chloroform BRL mg/kg dry 0.0028 0.00020 1 8260B 8/18/16 22:06 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0028 0.00019 1 8260B 8/18/16 22:06 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0028 0.00012 1 8260B 8/18/16 22:06 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0028 0.000095 1 8260B 8/18/16 22:06 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0028 0.00012 1 8260B 8/18/16 22:06 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0028 0.00013 1 8260B 8/18/16 22:06 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0028 0.00011 1 8260B 8/18/16 22:06 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0028 0.00011 1 8260B 8/18/16 22:06 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0028 0.00017 1 8260B 8/18/16 22:06 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0056 0.00026 1 8260B 8/18/16 22:06 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.028 0.00025 1 8260B 8/18/16 22:06 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.056 0.00025 1 8260B 8/18/16 22:06 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: B-1 Attn: Brian Olin Prism Sample ID: 6080270-05 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 12:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.028 0.00024 1 8260B 8/18/16 22:06 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0028 0.00016 1 8260B 8/18/16 22:06 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0056 0.000090 1 8260B 8/18/16 22:06 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0056 0.000089 1 8260B 8/18/16 22:06 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0028 0.00014 1 8260B 8/18/16 22:06 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0028 0.00017 1 8260B 8/18/16 22:06 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0028 0.00012 1 8260B 8/18/16 22:06 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0028 0.00014 1 8260B 8/18/16 22:06 ANG P61-10336 Styrene BRL mg/kg dry 0.0028 0.00017 1 8260B 8/18/16 22:06 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0028 0.000095 1 8260B 8/18/16 22:06 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0028 0.00013 1 8260B 8/18/16 22:06 ANG P61-10336 Toluene BRL mg/kg dry 0.0028 0.00016 1 8260B 8/18/16 22:06 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0028 0.00017 1 8260B 8/18/16 22:06 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0028 0.00015 1 8260B 8/18/16 22:06 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0028 0.00018 1 8260B 8/18/16 22:06 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0028 0.00018 1 8260B 8/18/16 22:06 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.014 0.00039 1 8260B 8/18/16 22:06 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0028 0.00014 1 8260B 8/18/16 22:06 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0084 0.00053 1 8260B 8/18/16 22:06 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 97 % 70-130 Dibromofluoromethane 90 % 84-123 Toluene-d8 103 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 14 0.42 100 MADEP VPH 8/19/16 17:45 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 14 1.7 100 MADEP VPH 8/19/16 17:45 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 14 0.13 100 MADEP VPH 8/19/16 17:45 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 97 % 70-130 2,5-Dibromotoluene (FID) 122 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: SW-2 Attn: Brian Olin Prism Sample ID: 6080270-06 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 12:55 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 27 1.1 1 MADEP EPH 8/18/16 16:36 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 27 2.2 1 MADEP EPH 8/18/16 16:36 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 11 1.4 1 MADEP EPH 8/18/16 16:36 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 65 % 40-140 o-Terphenyl 59 % 40-140 2-Fluorobiphenyl 96 % 40-140 2-Bromonaphthalene 103 % 40-140 General Chemistry Parameters % Solids 94.1 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.35 0.055 1 8270D 8/18/16 17:52 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.35 0.053 1 8270D 8/18/16 17:52 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.35 0.049 1 8270D 8/18/16 17:52 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.35 0.051 1 8270D 8/18/16 17:52 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.35 0.068 1 8270D 8/18/16 17:52 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.35 0.066 1 8270D 8/18/16 17:52 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.35 0.068 1 8270D 8/18/16 17:52 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.35 0.054 1 8270D 8/18/16 17:52 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.35 0.049 1 8270D 8/18/16 17:52 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.35 0.043 1 8270D 8/18/16 17:52 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.35 0.047 1 8270D 8/18/16 17:52 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.35 0.051 1 8270D 8/18/16 17:52 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 17:52 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.35 0.056 1 8270D 8/18/16 17:52 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.35 0.045 1 8270D 8/18/16 17:52 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.35 0.064 1 8270D 8/18/16 17:52 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.35 0.069 1 8270D 8/18/16 17:52 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.35 0.043 1 8270D 8/18/16 17:52 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.35 0.053 1 8270D 8/18/16 17:52 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.35 0.060 1 8270D 8/18/16 17:52 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.35 0.049 1 8270D 8/18/16 17:52 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.35 0.042 1 8270D 8/18/16 17:52 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 17:52 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.35 0.054 1 8270D 8/18/16 17:52 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.35 0.048 1 8270D 8/18/16 17:52 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.35 0.051 1 8270D 8/18/16 17:52 JMV P61-10314 Anthracene BRL mg/kg dry 0.35 0.056 1 8270D 8/18/16 17:52 JMV P61-10314 Azobenzene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 17:52 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 17:52 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.35 0.038 1 8270D 8/18/16 17:52 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: SW-2 Prism Sample ID: 6080270-06 Prism Work Order: 6080270 Time Collected: 08/11/16 12:55 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.35 0.041 1 8270D 8/18/16 17:52 Benzo(g,h,i)perylene BRL mg/kg dry 0.35 0.038 1 8270D 8/18/16 17:52 Benzo(k)fluoranthene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 17:52 Benzoic Acid BRL mg/kg dry 0.35 0.030 1 8270D 8/18/16 17:52 Benzyl alcohol BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 17:52 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.35 0.061 1 8270D 8/18/16 17:52 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.35 0.049 1 8270D 8/18/16 17:52 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.35 0.060 1 8270D 8/18/16 17:52 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.35 0.052 1 8270D 8/18/16 17:52 Butyl benzyl phthalate BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 17:52 Chrysene BRL mg/kg dry 0.35 0.044 1 8270D 8/18/16 17:52 Dibenzo(a,h)anthracene BRL mg/kg dry 0.35 0.043 1 8270D 8/18/16 17:52 Dibenzofuran BRL mg/kg dry 0.35 0.053 1 8270D 8/18/16 17:52 Diethyl phthalate BRL mg/kg dry 0.35 0.048 1 8270D 8/18/16 17:52 Dimethyl phthalate BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 17:52 Di-n-butyl phthalate BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 17:52 Di-n-octyl phthalate BRL mg/kg dry 0.35 0.043 1 8270D 8/18/16 17:52 Fluoranthene BRL mg/kg dry 0.35 0.045 1 8270D 8/18/16 17:52 Fluorene BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 17:52 Hexachlorobenzene BRL mg/kg dry 0.35 0.056 1 8270D 8/18/16 17:52 Hexachlorobutadiene BRL mg/kg dry 0.35 0.063 1 8270D 8/18/16 17:52 Hexachlorocyclopentadiene BRL mg/kg dry 0.35 0.063 1 8270D 8/18/16 17:52 Hexachloroethane BRL mg/kg dry 0.35 0.059 1 8270D 8/18/16 17:52 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.35 0.040 1 8270D 8/18/16 17:52 Isophorone BRL mg/kg dry 0.35 0.047 1 8270D 8/18/16 17:52 Naphthalene BRL mg/kg dry 0.35 0.056 1 8270D 8/18/16 17:52 Nitrobenzene BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 17:52 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.35 0.055 1 8270D 8/18/16 17:52 N-Nitrosodiphenylamine BRL mg/kg dry 0.35 0.053 1 8270D 8/18/16 17:52 Pentachlorophenol BRL mg/kg dry 0.35 0.041 1 8270D 8/18/16 17:52 Phenanthrene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 17:52 Phenol BRL mg/kg dry 0.35 0.052 1 8270D 8/18/16 17:52 Pyrene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 17:52 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 72 % 39-132 2-Fluorobiphenyl 74 % 44-115 2-Fluorophenol 77 % 35-115 Nitrobenzene-d5 73 % 37-122 Phenol-d5 77 % 34-121 Terphenyl-d14 68 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0028 0.00023 1 8260B 8/19/16 2:15 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:15 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: SW-2 Prism Sample ID: 6080270-06 Prism Work Order: 6080270 Time Collected: 08/11/16 12:55 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0028 0.00019 1 8260B 8/19/16 2:15 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0028 0.00025 1 8260B 8/19/16 2:15 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0028 0.000077 1 8260B 8/19/16 2:15 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0028 0.00012 1 8260B 8/19/16 2:15 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0028 0.00015 1 8260B 8/19/16 2:15 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0028 0.00016 1 8260B 8/19/16 2:15 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0028 0.00036 1 8260B 8/19/16 2:15 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0028 0.00021 1 8260B 8/19/16 2:15 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0028 0.00021 1 8260B 8/19/16 2:15 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:15 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:15 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0028 0.00017 1 8260B 8/19/16 2:15 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0028 0.00017 1 8260B 8/19/16 2:15 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0028 0.00021 1 8260B 8/19/16 2:15 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0028 0.00018 1 8260B 8/19/16 2:15 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0028 0.00014 1 8260B 8/19/16 2:15 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:15 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:15 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0028 0.00014 1 8260B 8/19/16 2:15 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0028 0.00017 1 8260B 8/19/16 2:15 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:15 ANG P61-10336 Acetone BRL mg/kg dry 0.028 0.00068 1 8260B 8/19/16 2:15 ANG P61-10336 Benzene BRL mg/kg dry 0.0017 0.00016 1 8260B 8/19/16 2:15 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0028 0.00023 1 8260B 8/19/16 2:15 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0028 0.00015 1 8260B 8/19/16 2:15 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0028 0.00016 1 8260B 8/19/16 2:15 ANG P61-10336 Bromoform BRL mg/kg dry 0.0028 0.00032 1 8260B 8/19/16 2:15 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0056 0.00034 1 8260B 8/19/16 2:15 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0028 0.00014 1 8260B 8/19/16 2:15 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0028 0.00015 1 8260B 8/19/16 2:15 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0056 0.00023 1 8260B 8/19/16 2:15 ANG P61-10336 Chloroform BRL mg/kg dry 0.0028 0.00020 1 8260B 8/19/16 2:15 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0028 0.00019 1 8260B 8/19/16 2:15 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0028 0.00012 1 8260B 8/19/16 2:15 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0028 0.000094 1 8260B 8/19/16 2:15 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:15 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:15 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:15 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:15 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0028 0.00017 1 8260B 8/19/16 2:15 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0056 0.00026 1 8260B 8/19/16 2:15 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.028 0.00025 1 8260B 8/19/16 2:15 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.056 0.00025 1 8260B 8/19/16 2:15 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: SW-2 Attn: Brian Olin Prism Sample ID: 6080270-06 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 12:55 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.028 0.00024 1 8260B 8/19/16 2:15 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0028 0.00016 1 8260B 8/19/16 2:15 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0056 0.000089 1 8260B 8/19/16 2:15 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0056 0.000088 1 8260B 8/19/16 2:15 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0028 0.00014 1 8260B 8/19/16 2:15 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0028 0.00017 1 8260B 8/19/16 2:15 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:15 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:15 ANG P61-10336 Styrene BRL mg/kg dry 0.0028 0.00017 1 8260B 8/19/16 2:15 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0028 0.000094 1 8260B 8/19/16 2:15 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:15 ANG P61-10336 Toluene BRL mg/kg dry 0.0028 0.00016 1 8260B 8/19/16 2:15 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0028 0.00017 1 8260B 8/19/16 2:15 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0028 0.00015 1 8260B 8/19/16 2:15 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0028 0.00018 1 8260B 8/19/16 2:15 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0028 0.00018 1 8260B 8/19/16 2:15 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.014 0.00038 1 8260B 8/19/16 2:15 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:15 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0084 0.00052 1 8260B 8/19/16 2:15 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 100 % 70-130 Dibromofluoromethane 94 % 84-123 Toluene-d8 104 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 14 0.43 100 MADEP VPH 8/19/16 23:23 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 14 1.7 100 MADEP VPH 8/19/16 23:23 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 14 0.13 100 MADEP VPH 8/19/16 23:23 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 89 % 70-130 2,5-Dibromotoluene (FID) 113 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: WW-2 Attn: Brian Olin Prism Sample ID: 6080270-07 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 13:10 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 27 1.1 1 MADEP EPH 8/18/16 17:12 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 27 2.2 1 MADEP EPH 8/18/16 17:12 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 11 1.4 1 MADEP EPH 8/18/16 17:12 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 69 % 40-140 o-Terphenyl 63 % 40-140 2-Fluorobiphenyl 74 % 40-140 2-Bromonaphthalene 84 % 40-140 General Chemistry Parameters % Solids 93.5 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.35 0.055 1 8270D 8/18/16 18:14 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.35 0.053 1 8270D 8/18/16 18:14 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.35 0.049 1 8270D 8/18/16 18:14 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.35 0.051 1 8270D 8/18/16 18:14 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.35 0.067 1 8270D 8/18/16 18:14 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.35 0.066 1 8270D 8/18/16 18:14 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.35 0.068 1 8270D 8/18/16 18:14 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.35 0.054 1 8270D 8/18/16 18:14 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.35 0.049 1 8270D 8/18/16 18:14 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.35 0.042 1 8270D 8/18/16 18:14 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 18:14 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.35 0.051 1 8270D 8/18/16 18:14 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 18:14 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.35 0.056 1 8270D 8/18/16 18:14 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.35 0.045 1 8270D 8/18/16 18:14 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.35 0.064 1 8270D 8/18/16 18:14 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.35 0.069 1 8270D 8/18/16 18:14 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.35 0.043 1 8270D 8/18/16 18:14 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.35 0.052 1 8270D 8/18/16 18:14 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.35 0.060 1 8270D 8/18/16 18:14 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.35 0.049 1 8270D 8/18/16 18:14 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.35 0.042 1 8270D 8/18/16 18:14 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.35 0.045 1 8270D 8/18/16 18:14 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.35 0.054 1 8270D 8/18/16 18:14 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.35 0.048 1 8270D 8/18/16 18:14 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.35 0.051 1 8270D 8/18/16 18:14 JMV P61-10314 Anthracene BRL mg/kg dry 0.35 0.056 1 8270D 8/18/16 18:14 JMV P61-10314 Azobenzene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 18:14 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 18:14 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.35 0.038 1 8270D 8/18/16 18:14 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: WW-2 Prism Sample ID: 6080270-07 Prism Work Order: 6080270 Time Collected: 08/11/16 13:10 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.35 0.041 1 8270D 8/18/16 18:14 Benzo(g,h,i)perylene BRL mg/kg dry 0.35 0.038 1 8270D 8/18/16 18:14 Benzo(k)fluoranthene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 18:14 Benzoic Acid BRL mg/kg dry 0.35 0.029 1 8270D 8/18/16 18:14 Benzyl alcohol BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 18:14 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.35 0.061 1 8270D 8/18/16 18:14 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.35 0.049 1 8270D 8/18/16 18:14 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.35 0.060 1 8270D 8/18/16 18:14 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.35 0.052 1 8270D 8/18/16 18:14 Butyl benzyl phthalate BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 18:14 Chrysene BRL mg/kg dry 0.35 0.044 1 8270D 8/18/16 18:14 Dibenzo(a,h)anthracene BRL mg/kg dry 0.35 0.043 1 8270D 8/18/16 18:14 Dibenzofuran BRL mg/kg dry 0.35 0.053 1 8270D 8/18/16 18:14 Diethyl phthalate BRL mg/kg dry 0.35 0.048 1 8270D 8/18/16 18:14 Dimethyl phthalate BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 18:14 Di-n-butyl phthalate BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 18:14 Di-n-octyl phthalate BRL mg/kg dry 0.35 0.043 1 8270D 8/18/16 18:14 Fluoranthene BRL mg/kg dry 0.35 0.045 1 8270D 8/18/16 18:14 Fluorene BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 18:14 Hexachlorobenzene BRL mg/kg dry 0.35 0.055 1 8270D 8/18/16 18:14 Hexachlorobutadiene BRL mg/kg dry 0.35 0.063 1 8270D 8/18/16 18:14 Hexachlorocyclopentadiene BRL mg/kg dry 0.35 0.062 1 8270D 8/18/16 18:14 Hexachloroethane BRL mg/kg dry 0.35 0.059 1 8270D 8/18/16 18:14 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.35 0.040 1 8270D 8/18/16 18:14 Isophorone BRL mg/kg dry 0.35 0.047 1 8270D 8/18/16 18:14 Naphthalene BRL mg/kg dry 0.35 0.056 1 8270D 8/18/16 18:14 Nitrobenzene BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 18:14 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.35 0.055 1 8270D 8/18/16 18:14 N-Nitrosodiphenylamine BRL mg/kg dry 0.35 0.053 1 8270D 8/18/16 18:14 Pentachlorophenol BRL mg/kg dry 0.35 0.041 1 8270D 8/18/16 18:14 Phenanthrene BRL mg/kg dry 0.35 0.045 1 8270D 8/18/16 18:14 Phenol BRL mg/kg dry 0.35 0.052 1 8270D 8/18/16 18:14 Pyrene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 18:14 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 80 % 39-132 2-Fluorobiphenyl 67 % 44-115 2-Fluorophenol 68 % 35-115 Nitrobenzene-d5 63 % 37-122 Phenol-d5 70 % 34-121 Terphenyl-d14 77 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0028 0.00023 1 8260B 8/19/16 2:42 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:42 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: WW-2 Prism Sample ID: 6080270-07 Prism Work Order: 6080270 Time Collected: 08/11/16 13:10 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0028 0.00019 1 8260B 8/19/16 2:42 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0028 0.00025 1 8260B 8/19/16 2:42 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0028 0.000077 1 8260B 8/19/16 2:42 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0028 0.00012 1 8260B 8/19/16 2:42 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0028 0.00015 1 8260B 8/19/16 2:42 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0028 0.00016 1 8260B 8/19/16 2:42 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0028 0.00035 1 8260B 8/19/16 2:42 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0028 0.00021 1 8260B 8/19/16 2:42 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0028 0.00021 1 8260B 8/19/16 2:42 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:42 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:42 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0028 0.00016 1 8260B 8/19/16 2:42 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0028 0.00017 1 8260B 8/19/16 2:42 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0028 0.00021 1 8260B 8/19/16 2:42 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0028 0.00018 1 8260B 8/19/16 2:42 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0028 0.00014 1 8260B 8/19/16 2:42 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:42 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:42 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0028 0.00014 1 8260B 8/19/16 2:42 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0028 0.00016 1 8260B 8/19/16 2:42 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:42 ANG P61-10336 Acetone 0.030 mg/kg dry 0.028 0.00067 1 8260B 8/19/16 2:42 ANG P6H0336 Benzene BRL mg/kg dry 0.0017 0.00016 1 8260B 8/19/16 2:42 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0028 0.00023 1 8260B 8/19/16 2:42 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0028 0.00015 1 8260B 8/19/16 2:42 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0028 0.00015 1 8260B 8/19/16 2:42 ANG P61-10336 Bromoform BRL mg/kg dry 0.0028 0.00031 1 8260B 8/19/16 2:42 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0055 0.00034 1 8260B 8/19/16 2:42 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0028 0.00014 1 8260B 8/19/16 2:42 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0028 0.00015 1 8260B 8/19/16 2:42 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0055 0.00023 1 8260B 8/19/16 2:42 ANG P61-10336 Chloroform BRL mg/kg dry 0.0028 0.00020 1 8260B 8/19/16 2:42 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0028 0.00019 1 8260B 8/19/16 2:42 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0028 0.00012 1 8260B 8/19/16 2:42 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0028 0.000093 1 8260B 8/19/16 2:42 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:42 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:42 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:42 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:42 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0028 0.00016 1 8260B 8/19/16 2:42 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0055 0.00026 1 8260B 8/19/16 2:42 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.028 0.00025 1 8260B 8/19/16 2:42 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.055 0.00025 1 8260B 8/19/16 2:42 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 30 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: WW-2 Attn: Brian Olin Prism Sample ID: 6080270-07 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 13:10 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.028 0.00024 1 8260B 8/19/16 2:42 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0028 0.00016 1 8260B 8/19/16 2:42 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0055 0.000089 1 8260B 8/19/16 2:42 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0055 0.000087 1 8260B 8/19/16 2:42 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0028 0.00014 1 8260B 8/19/16 2:42 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0028 0.00016 1 8260B 8/19/16 2:42 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0028 0.00011 1 8260B 8/19/16 2:42 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:42 ANG P61-10336 Styrene BRL mg/kg dry 0.0028 0.00017 1 8260B 8/19/16 2:42 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0028 0.000093 1 8260B 8/19/16 2:42 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:42 ANG P61-10336 Toluene BRL mg/kg dry 0.0028 0.00016 1 8260B 8/19/16 2:42 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0028 0.00017 1 8260B 8/19/16 2:42 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0028 0.00015 1 8260B 8/19/16 2:42 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0028 0.00018 1 8260B 8/19/16 2:42 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0028 0.00018 1 8260B 8/19/16 2:42 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.014 0.00038 1 8260B 8/19/16 2:42 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0028 0.00013 1 8260B 8/19/16 2:42 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0083 0.00052 1 8260B 8/19/16 2:42 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 70-130 Dibromofluoromethane 95 % 84-123 Toluene-d8 104 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 15 0.45 100 MADEP VPH 8/19/16 23:53 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 15 1.8 100 MADEP VPH 8/19/16 23:53 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 15 0.14 100 MADEP VPH 8/19/16 23:53 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 88 % 70-130 2,5-Dibromotoluene (FID) 113 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 31 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: EW-2 Attn: Brian Olin Prism Sample ID: 6080270-08 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 13:25 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 27 1.2 1 MADEP EPH 8/18/16 17:49 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 27 2.2 1 MADEP EPH 8/18/16 17:49 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 11 1.5 1 MADEP EPH 8/18/16 17:49 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 70 % 40-140 o-Terphenyl 70 % 40-140 2-Fluorobiphenyl 89 % 40-140 2-Bromonaphthalene 103 % 40-140 General Chemistry Parameters % Solids 91.0 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.36 0.056 1 8270D 8/18/16 18:36 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 18:36 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 18:36 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.36 0.053 1 8270D 8/18/16 18:36 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.36 0.070 1 8270D 8/18/16 18:36 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.36 0.068 1 8270D 8/18/16 18:36 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.36 0.070 1 8270D 8/18/16 18:36 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 18:36 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 18:36 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 18:36 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 18:36 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 18:36 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 18:36 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.36 0.058 1 8270D 8/18/16 18:36 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.36 0.046 1 8270D 8/18/16 18:36 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.36 0.066 1 8270D 8/18/16 18:36 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.36 0.071 1 8270D 8/18/16 18:36 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.36 0.045 1 8270D 8/18/16 18:36 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.36 0.054 1 8270D 8/18/16 18:36 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.36 0.062 1 8270D 8/18/16 18:36 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 18:36 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.36 0.043 1 8270D 8/18/16 18:36 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 18:36 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.36 0.056 1 8270D 8/18/16 18:36 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.36 0.049 1 8270D 8/18/16 18:36 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 18:36 JMV P61-10314 Anthracene BRL mg/kg dry 0.36 0.058 1 8270D 8/18/16 18:36 JMV P61-10314 Azobenzene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 18:36 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 18:36 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.36 0.039 1 8270D 8/18/16 18:36 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 32 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: EW-2 Prism Sample ID: 6080270-08 Prism Work Order: 6080270 Time Collected: 08/11/16 13:25 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.36 0.042 1 8270D 8/18/16 18:36 Benzo(g,h,i)perylene BRL mg/kg dry 0.36 0.040 1 8270D 8/18/16 18:36 Benzo(k)fluoranthene BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 18:36 Benzoic Acid BRL mg/kg dry 0.36 0.030 1 8270D 8/18/16 18:36 Benzyl alcohol BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 18:36 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.36 0.063 1 8270D 8/18/16 18:36 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 18:36 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.36 0.062 1 8270D 8/18/16 18:36 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.36 0.054 1 8270D 8/18/16 18:36 Butyl benzyl phthalate BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 18:36 Chrysene BRL mg/kg dry 0.36 0.046 1 8270D 8/18/16 18:36 Dibenzo(a,h)anthracene BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 18:36 Dibenzofuran BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 18:36 Diethyl phthalate BRL mg/kg dry 0.36 0.050 1 8270D 8/18/16 18:36 Dimethyl phthalate BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 18:36 Di-n-butyl phthalate BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 18:36 Di-n-octyl phthalate BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 18:36 Fluoranthene BRL mg/kg dry 0.36 0.046 1 8270D 8/18/16 18:36 Fluorene BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 18:36 Hexachlorobenzene BRL mg/kg dry 0.36 0.057 1 8270D 8/18/16 18:36 Hexachlorobutadiene BRL mg/kg dry 0.36 0.065 1 8270D 8/18/16 18:36 Hexachlorocyclopentadiene BRL mg/kg dry 0.36 0.065 1 8270D 8/18/16 18:36 Hexachloroethane BRL mg/kg dry 0.36 0.061 1 8270D 8/18/16 18:36 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.36 0.042 1 8270D 8/18/16 18:36 Isophorone BRL mg/kg dry 0.36 0.049 1 8270D 8/18/16 18:36 Naphthalene BRL mg/kg dry 0.36 0.058 1 8270D 8/18/16 18:36 Nitrobenzene BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 18:36 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.36 0.057 1 8270D 8/18/16 18:36 N-Nitrosodiphenylamine BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 18:36 Pentachlorophenol BRL mg/kg dry 0.36 0.043 1 8270D 8/18/16 18:36 Phenanthrene BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 18:36 Phenol BRL mg/kg dry 0.36 0.053 1 8270D 8/18/16 18:36 Pyrene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 18:36 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 65 % 39-132 2-Fluorobiphenyl 54 % 44-115 2-Fluorophenol 53 % 35-115 Nitrobenzene-d5 49 % 37-122 Phenol-d5 57 % 34-121 Terphenyl-d14 78 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0030 0.00025 1 8260B 8/18/16 22:34 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0030 0.00015 1 8260B 8/18/16 22:34 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: EW-2 Prism Sample ID: 6080270-08 Prism Work Order: 6080270 Time Collected: 08/11/16 13:25 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0030 0.00020 1 8260B 8/18/16 22:34 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0030 0.00027 1 8260B 8/18/16 22:34 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0030 0.000084 1 8260B 8/18/16 22:34 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0030 0.00013 1 8260B 8/18/16 22:34 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0030 0.00017 1 8260B 8/18/16 22:34 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0030 0.00017 1 8260B 8/18/16 22:34 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0030 0.00039 1 8260B 8/18/16 22:34 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0030 0.00022 1 8260B 8/18/16 22:34 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0030 0.00023 1 8260B 8/18/16 22:34 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0030 0.00012 1 8260B 8/18/16 22:34 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0030 0.00014 1 8260B 8/18/16 22:34 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0030 0.00018 1 8260B 8/18/16 22:34 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0030 0.00019 1 8260B 8/18/16 22:34 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0030 0.00023 1 8260B 8/18/16 22:34 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0030 0.00020 1 8260B 8/18/16 22:34 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0030 0.00015 1 8260B 8/18/16 22:34 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0030 0.00012 1 8260B 8/18/16 22:34 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0030 0.00014 1 8260B 8/18/16 22:34 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0030 0.00016 1 8260B 8/18/16 22:34 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0030 0.00018 1 8260B 8/18/16 22:34 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0030 0.00015 1 8260B 8/18/16 22:34 ANG P61-10336 Acetone BRL mg/kg dry 0.030 0.00074 1 8260B 8/18/16 22:34 ANG P61-10336 Benzene BRL mg/kg dry 0.0018 0.00018 1 8260B 8/18/16 22:34 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0030 0.00025 1 8260B 8/18/16 22:34 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0030 0.00017 1 8260B 8/18/16 22:34 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0030 0.00017 1 8260B 8/18/16 22:34 ANG P61-10336 Bromoform BRL mg/kg dry 0.0030 0.00034 1 8260B 8/18/16 22:34 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0060 0.00037 1 8260B 8/18/16 22:34 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0030 0.00015 1 8260B 8/18/16 22:34 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0030 0.00016 1 8260B 8/18/16 22:34 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0060 0.00025 1 8260B 8/18/16 22:34 ANG P61-10336 Chloroform BRL mg/kg dry 0.0030 0.00022 1 8260B 8/18/16 22:34 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0030 0.00020 1 8260B 8/18/16 22:34 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0030 0.00013 1 8260B 8/18/16 22:34 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0030 0.00010 1 8260B 8/18/16 22:34 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0030 0.00012 1 8260B 8/18/16 22:34 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0030 0.00014 1 8260B 8/18/16 22:34 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0030 0.00012 1 8260B 8/18/16 22:34 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0030 0.00012 1 8260B 8/18/16 22:34 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0030 0.00018 1 8260B 8/18/16 22:34 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0060 0.00028 1 8260B 8/18/16 22:34 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.030 0.00027 1 8260B 8/18/16 22:34 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.060 0.00027 1 8260B 8/18/16 22:34 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 34 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: EW-2 Attn: Brian Olin Prism Sample ID: 6080270-08 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/11/16 13:25 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.030 0.00026 1 8260B 8/18/16 22:34 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0030 0.00017 1 8260B 8/18/16 22:34 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0060 0.000097 1 8260B 8/18/16 22:34 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0060 0.000095 1 8260B 8/18/16 22:34 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0030 0.00015 1 8260B 8/18/16 22:34 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0030 0.00018 1 8260B 8/18/16 22:34 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0030 0.00012 1 8260B 8/18/16 22:34 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0030 0.00015 1 8260B 8/18/16 22:34 ANG P61-10336 Styrene BRL mg/kg dry 0.0030 0.00018 1 8260B 8/18/16 22:34 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0030 0.00010 1 8260B 8/18/16 22:34 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0030 0.00014 1 8260B 8/18/16 22:34 ANG P61-10336 Toluene BRL mg/kg dry 0.0030 0.00017 1 8260B 8/18/16 22:34 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0030 0.00018 1 8260B 8/18/16 22:34 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0030 0.00016 1 8260B 8/18/16 22:34 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0030 0.00020 1 8260B 8/18/16 22:34 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0030 0.00020 1 8260B 8/18/16 22:34 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.015 0.00041 1 8260B 8/18/16 22:34 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0030 0.00015 1 8260B 8/18/16 22:34 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0091 0.00057 1 8260B 8/18/16 22:34 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 70-130 Dibromofluoromethane 94 % 84-123 Toluene-d8 103 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 15 0.47 100 MADEP VPH 8/19/16 18:16 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 15 1.8 100 MADEP VPH 8/19/16 18:16 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 15 0.15 100 MADEP VPH 8/19/16 18:16 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 93 % 70-130 2,5-Dibromotoluene (FID) 117 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 35 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: B-3 Attn: Brian Olin Prism Sample ID: 6080270-09 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 10:15 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 28 1.2 1 MADEP EPH 8/18/16 18:26 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 28 2.3 1 MADEP EPH 8/18/16 18:26 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 11 1.5 1 MADEP EPH 8/18/16 18:26 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 80 % 40-140 o-Terphenyl 71 % 40-140 2-Fluorobiphenyl 90 % 40-140 2-Bromonaphthalene 106 % 40-140 General Chemistry Parameters % Solids 88.2 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.37 0.058 1 8270D 8/18/16 18:58 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.37 0.057 1 8270D 8/18/16 18:58 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.37 0.053 1 8270D 8/18/16 18:58 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.37 0.055 1 8270D 8/18/16 18:58 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.37 0.072 1 8270D 8/18/16 18:58 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.37 0.070 1 8270D 8/18/16 18:58 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.37 0.072 1 8270D 8/18/16 18:58 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.37 0.057 1 8270D 8/18/16 18:58 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.37 0.052 1 8270D 8/18/16 18:58 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.37 0.045 1 8270D 8/18/16 18:58 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.37 0.050 1 8270D 8/18/16 18:58 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.37 0.054 1 8270D 8/18/16 18:58 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.37 0.053 1 8270D 8/18/16 18:58 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.37 0.060 1 8270D 8/18/16 18:58 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.37 0.048 1 8270D 8/18/16 18:58 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.37 0.068 1 8270D 8/18/16 18:58 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.37 0.074 1 8270D 8/18/16 18:58 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.37 0.046 1 8270D 8/18/16 18:58 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.37 0.056 1 8270D 8/18/16 18:58 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.37 0.064 1 8270D 8/18/16 18:58 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.37 0.052 1 8270D 8/18/16 18:58 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.37 0.045 1 8270D 8/18/16 18:58 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.37 0.048 1 8270D 8/18/16 18:58 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.37 0.058 1 8270D 8/18/16 18:58 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.37 0.051 1 8270D 8/18/16 18:58 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.37 0.054 1 8270D 8/18/16 18:58 JMV P61-10314 Anthracene BRL mg/kg dry 0.37 0.060 1 8270D 8/18/16 18:58 JMV P61-10314 Azobenzene BRL mg/kg dry 0.37 0.049 1 8270D 8/18/16 18:58 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.37 0.049 1 8270D 8/18/16 18:58 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.37 0.040 1 8270D 8/18/16 18:58 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 36 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: B-3 Prism Sample ID: 6080270-09 Prism Work Order: 6080270 Time Collected: 08/12/16 10:15 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.37 0.043 1 8270D 8/18/16 18:58 Benzo(g,h,i)perylene BRL mg/kg dry 0.37 0.041 1 8270D 8/18/16 18:58 Benzo(k)fluoranthene BRL mg/kg dry 0.37 0.049 1 8270D 8/18/16 18:58 Benzoic Acid BRL mg/kg dry 0.37 0.031 1 8270D 8/18/16 18:58 Benzyl alcohol BRL mg/kg dry 0.37 0.049 1 8270D 8/18/16 18:58 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.37 0.065 1 8270D 8/18/16 18:58 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.37 0.053 1 8270D 8/18/16 18:58 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.37 0.064 1 8270D 8/18/16 18:58 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.37 0.055 1 8270D 8/18/16 18:58 Butyl benzyl phthalate BRL mg/kg dry 0.37 0.053 1 8270D 8/18/16 18:58 Chrysene BRL mg/kg dry 0.37 0.047 1 8270D 8/18/16 18:58 Dibenzo(a,h)anthracene BRL mg/kg dry 0.37 0.045 1 8270D 8/18/16 18:58 Dibenzofuran BRL mg/kg dry 0.37 0.057 1 8270D 8/18/16 18:58 Diethyl phthalate BRL mg/kg dry 0.37 0.051 1 8270D 8/18/16 18:58 Dimethyl phthalate BRL mg/kg dry 0.37 0.049 1 8270D 8/18/16 18:58 Di-n-butyl phthalate BRL mg/kg dry 0.37 0.053 1 8270D 8/18/16 18:58 Di-n-octyl phthalate BRL mg/kg dry 0.37 0.046 1 8270D 8/18/16 18:58 Fluoranthene BRL mg/kg dry 0.37 0.048 1 8270D 8/18/16 18:58 Fluorene BRL mg/kg dry 0.37 0.054 1 8270D 8/18/16 18:58 Hexachlorobenzene BRL mg/kg dry 0.37 0.059 1 8270D 8/18/16 18:58 Hexachlorobutadiene BRL mg/kg dry 0.37 0.067 1 8270D 8/18/16 18:58 Hexachlorocyclopentadiene BRL mg/kg dry 0.37 0.067 1 8270D 8/18/16 18:58 Hexachloroethane BRL mg/kg dry 0.37 0.062 1 8270D 8/18/16 18:58 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.37 0.043 1 8270D 8/18/16 18:58 Isophorone BRL mg/kg dry 0.37 0.051 1 8270D 8/18/16 18:58 Naphthalene BRL mg/kg dry 0.37 0.060 1 8270D 8/18/16 18:58 Nitrobenzene BRL mg/kg dry 0.37 0.053 1 8270D 8/18/16 18:58 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.37 0.059 1 8270D 8/18/16 18:58 N-Nitrosodiphenylamine BRL mg/kg dry 0.37 0.057 1 8270D 8/18/16 18:58 Pentachlorophenol BRL mg/kg dry 0.37 0.044 1 8270D 8/18/16 18:58 Phenanthrene BRL mg/kg dry 0.37 0.048 1 8270D 8/18/16 18:58 Phenol BRL mg/kg dry 0.37 0.055 1 8270D 8/18/16 18:58 Pyrene BRL mg/kg dry 0.37 0.049 1 8270D 8/18/16 18:58 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 74 % 39-132 2-Fluorobiphenyl 65 % 44-115 2-Fluorophenol 66 % 35-115 Nitrobenzene-d5 62 % 37-122 Phenol-d5 68 % 34-121 Terphenyl-d14 71 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0031 0.00025 1 8260B 8/18/16 23:02 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:02 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 37 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: B-3 Prism Sample ID: 6080270-09 Prism Work Order: 6080270 Time Collected: 08/12/16 10:15 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0031 0.00021 1 8260B 8/18/16 23:02 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0031 0.00027 1 8260B 8/18/16 23:02 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0031 0.000086 1 8260B 8/18/16 23:02 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0031 0.00014 1 8260B 8/18/16 23:02 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0031 0.00017 1 8260B 8/18/16 23:02 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:02 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0031 0.00040 1 8260B 8/18/16 23:02 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0031 0.00023 1 8260B 8/18/16 23:02 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0031 0.00024 1 8260B 8/18/16 23:02 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0031 0.00012 1 8260B 8/18/16 23:02 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:02 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:02 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0031 0.00019 1 8260B 8/18/16 23:02 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0031 0.00023 1 8260B 8/18/16 23:02 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0031 0.00021 1 8260B 8/18/16 23:02 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0031 0.00016 1 8260B 8/18/16 23:02 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0031 0.00012 1 8260B 8/18/16 23:02 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:02 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0031 0.00016 1 8260B 8/18/16 23:02 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:02 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:02 ANG P61-10336 Acetone 0.020 J mg/kg dry 0.031 0.00076 1 8260B 8/18/16 23:02 ANG P6H0336 Benzene BRL mg/kg dry 0.0019 0.00018 1 8260B 8/18/16 23:02 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0031 0.00026 1 8260B 8/18/16 23:02 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0031 0.00017 1 8260B 8/18/16 23:02 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0031 0.00017 1 8260B 8/18/16 23:02 ANG P61-10336 Bromoform BRL mg/kg dry 0.0031 0.00035 1 8260B 8/18/16 23:02 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0062 0.00038 1 8260B 8/18/16 23:02 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:02 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0031 0.00016 1 8260B 8/18/16 23:02 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0062 0.00026 1 8260B 8/18/16 23:02 ANG P61-10336 Chloroform BRL mg/kg dry 0.0031 0.00022 1 8260B 8/18/16 23:02 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0031 0.00021 1 8260B 8/18/16 23:02 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0031 0.00013 1 8260B 8/18/16 23:02 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0031 0.00010 1 8260B 8/18/16 23:02 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0031 0.00013 1 8260B 8/18/16 23:02 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0031 0.00014 1 8260B 8/18/16 23:02 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0031 0.00012 1 8260B 8/18/16 23:02 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0031 0.00013 1 8260B 8/18/16 23:02 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:02 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0062 0.00029 1 8260B 8/18/16 23:02 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.031 0.00028 1 8260B 8/18/16 23:02 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.062 0.00028 1 8260B 8/18/16 23:02 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 38 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: B-3 Attn: Brian Olin Prism Sample ID: 6080270-09 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 10:15 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.031 0.00026 1 8260B 8/18/16 23:02 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0031 0.00017 1 8260B 8/18/16 23:02 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0062 0.000099 1 8260B 8/18/16 23:02 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0062 0.000098 1 8260B 8/18/16 23:02 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0031 0.00016 1 8260B 8/18/16 23:02 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:02 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0031 0.00013 1 8260B 8/18/16 23:02 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:02 ANG P61-10336 Styrene BRL mg/kg dry 0.0031 0.00019 1 8260B 8/18/16 23:02 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0031 0.00010 1 8260B 8/18/16 23:02 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:02 ANG P61-10336 Toluene BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:02 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0031 0.00019 1 8260B 8/18/16 23:02 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0031 0.00016 1 8260B 8/18/16 23:02 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0031 0.00020 1 8260B 8/18/16 23:02 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0031 0.00020 1 8260B 8/18/16 23:02 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.015 0.00042 1 8260B 8/18/16 23:02 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:02 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0093 0.00058 1 8260B 8/18/16 23:02 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 70-130 Dibromofluoromethane 95 % 84-123 Toluene-d8 105 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID RLM C5-C8 Aliphatics BRL mg/kg dry 8.0 0.25 100 MADEP VPH 8/19/16 18:47 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 8.0 0.96 100 MADEP VPH 8/19/16 18:47 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 8.0 0.077 100 MADEP VPH 8/19/16 18:47 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 115 % 70-130 2,5-Dibromotoluene (FID) 145 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 39 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: E-3 Attn: Brian Olin Prism Sample ID: 6080270-10 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 10:20 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics 6.5 J mg/kg dry 30 1.3 1 MADEP EPH 8/18/16 19:02 ZRC P6H0227 C19-C36 Aliphatics 3.5 J mg/kg dry 30 2.4 1 MADEP EPH 8/18/16 19:02 ZRC P6H0227 C11-C22 Aromatics 5.3 J mg/kg dry 12 1.6 1 MADEP EPH 8/18/16 19:02 ZRC P6H0227 Surrogate Recovery Control Limits 1-Chlorooctadecane 75 % 40-140 o-Terphenyl 78 % 40-140 2-Fluorobiphenyl 98 % 40-140 2-Bromonaphthalene 111 % 40-140 General Chemistry Parameters % Solids 84.4 % by 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.78 0.15 1 8270D 8/18/16 22:39 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.78 0.15 1 8270D 8/18/16 22:39 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.78 0.15 1 8270D 8/18/16 22:39 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.78 0.094 1 8270D 8/18/16 22:39 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.78 0.10 1 8270D 8/18/16 22:39 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.78 0.099 1 8270D 8/18/16 22:39 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.78 0.14 1 8270D 8/18/16 22:39 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.78 0.15 1 8270D 8/18/16 22:39 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.78 0.096 1 8270D 8/18/16 22:39 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.78 0.13 1 8270D 8/18/16 22:39 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.78 0.093 1 8270D 8/18/16 22:39 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.78 0.10 1 8270D 8/18/16 22:39 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 JMV P61-10314 Anthracene BRL mg/kg dry 0.78 0.13 1 8270D 8/18/16 22:39 JMV P61-10314 Azobenzene BRL mg/kg dry 0.78 0.10 1 8270D 8/18/16 22:39 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.78 0.10 1 8270D 8/18/16 22:39 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.78 0.084 1 8270D 8/18/16 22:39 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 40 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: E-3 Prism Sample ID: 6080270-10 Prism Work Order: 6080270 Time Collected: 08/12/16 10:20 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.78 0.090 1 8270D 8/18/16 22:39 Benzo(g,h,i)perylene BRL mg/kg dry 0.78 0.085 1 8270D 8/18/16 22:39 Benzo(k)fluoranthene BRL mg/kg dry 0.78 0.10 1 8270D 8/18/16 22:39 Benzoic Acid BRL mg/kg dry 0.78 0.065 1 8270D 8/18/16 22:39 Benzyl alcohol BRL mg/kg dry 0.78 0.10 1 8270D 8/18/16 22:39 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.78 0.13 1 8270D 8/18/16 22:39 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.78 0.13 1 8270D 8/18/16 22:39 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 Butyl benzyl phthalate BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 Chrysene BRL mg/kg dry 0.78 0.098 1 8270D 8/18/16 22:39 Dibenzo(a,h)anthracene BRL mg/kg dry 0.78 0.094 1 8270D 8/18/16 22:39 Dibenzofuran BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 Diethyl phthalate BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 Dimethyl phthalate BRL mg/kg dry 0.78 0.10 1 8270D 8/18/16 22:39 Di-n-butyl phthalate BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 Di-n-octyl phthalate BRL mg/kg dry 0.78 0.095 1 8270D 8/18/16 22:39 Fluoranthene BRL mg/kg dry 0.78 0.099 1 8270D 8/18/16 22:39 Fluorene BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 Hexachlorobenzene BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 Hexachlorobutadiene BRL mg/kg dry 0.78 0.14 1 8270D 8/18/16 22:39 Hexachlorocyclopentadiene BRL mg/kg dry 0.78 0.14 1 8270D 8/18/16 22:39 Hexachloroethane BRL mg/kg dry 0.78 0.13 1 8270D 8/18/16 22:39 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.78 0.089 1 8270D 8/18/16 22:39 Isophorone BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 Naphthalene BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 Nitrobenzene BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 N-Nitrosodiphenylamine BRL mg/kg dry 0.78 0.12 1 8270D 8/18/16 22:39 Pentachlorophenol BRL mg/kg dry 0.78 0.092 1 8270D 8/18/16 22:39 Phenanthrene BRL mg/kg dry 0.78 0.10 1 8270D 8/18/16 22:39 Phenol BRL mg/kg dry 0.78 0.11 1 8270D 8/18/16 22:39 Pyrene BRL mg/kg dry 0.78 0.10 1 8270D 8/18/16 22:39 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 97 % 39-132 2-Fluorobiphenyl 76 % 44-115 2-Fluorophenol 68 % 35-115 Nitrobenzene-d5 69 % 37-122 Phenol-d5 75 % 34-121 Terphenyl-d14 72 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0031 0.00025 1 8260B 8/18/16 23:29 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:29 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 41 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: E-3 Prism Sample ID: 6080270-10 Prism Work Order: 6080270 Time Collected: 08/12/16 10:20 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0031 0.00021 1 8260B 8/18/16 23:29 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0031 0.00027 1 8260B 8/18/16 23:29 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0031 0.000085 1 8260B 8/18/16 23:29 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0031 0.00014 1 8260B 8/18/16 23:29 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0031 0.00017 1 8260B 8/18/16 23:29 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0031 0.00017 1 8260B 8/18/16 23:29 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0031 0.00039 1 8260B 8/18/16 23:29 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0031 0.00023 1 8260B 8/18/16 23:29 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0031 0.00023 1 8260B 8/18/16 23:29 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0031 0.00012 1 8260B 8/18/16 23:29 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0031 0.00014 1 8260B 8/18/16 23:29 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:29 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0031 0.00019 1 8260B 8/18/16 23:29 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0031 0.00023 1 8260B 8/18/16 23:29 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0031 0.00020 1 8260B 8/18/16 23:29 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:29 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0031 0.00012 1 8260B 8/18/16 23:29 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:29 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0031 0.00016 1 8260B 8/18/16 23:29 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:29 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:29 ANG P61-10336 Acetone BRL mg/kg dry 0.031 0.00075 1 8260B 8/18/16 23:29 ANG P61-10336 Benzene BRL mg/kg dry 0.0018 0.00018 1 8260B 8/18/16 23:29 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0031 0.00026 1 8260B 8/18/16 23:29 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0031 0.00017 1 8260B 8/18/16 23:29 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0031 0.00017 1 8260B 8/18/16 23:29 ANG P61-10336 Bromoform BRL mg/kg dry 0.0031 0.00035 1 8260B 8/18/16 23:29 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0061 0.00038 1 8260B 8/18/16 23:29 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:29 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0031 0.00016 1 8260B 8/18/16 23:29 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0061 0.00026 1 8260B 8/18/16 23:29 ANG P61-10336 Chloroform BRL mg/kg dry 0.0031 0.00022 1 8260B 8/18/16 23:29 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0031 0.00021 1 8260B 8/18/16 23:29 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0031 0.00013 1 8260B 8/18/16 23:29 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0031 0.00010 1 8260B 8/18/16 23:29 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0031 0.00013 1 8260B 8/18/16 23:29 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0031 0.00014 1 8260B 8/18/16 23:29 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0031 0.00012 1 8260B 8/18/16 23:29 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0031 0.00013 1 8260B 8/18/16 23:29 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:29 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0061 0.00028 1 8260B 8/18/16 23:29 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.031 0.00028 1 8260B 8/18/16 23:29 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.061 0.00028 1 8260B 8/18/16 23:29 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 42 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: E-3 Attn: Brian Olin Prism Sample ID: 6080270-10 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 10:20 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.031 0.00026 1 8260B 8/18/16 23:29 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0031 0.00017 1 8260B 8/18/16 23:29 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0061 0.000098 1 8260B 8/18/16 23:29 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0061 0.000097 1 8260B 8/18/16 23:29 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0031 0.00016 1 8260B 8/18/16 23:29 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:29 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0031 0.00013 1 8260B 8/18/16 23:29 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:29 ANG P61-10336 Styrene BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:29 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0031 0.00010 1 8260B 8/18/16 23:29 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:29 ANG P61-10336 Toluene BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:29 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0031 0.00018 1 8260B 8/18/16 23:29 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0031 0.00016 1 8260B 8/18/16 23:29 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0031 0.00020 1 8260B 8/18/16 23:29 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0031 0.00020 1 8260B 8/18/16 23:29 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.015 0.00042 1 8260B 8/18/16 23:29 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0031 0.00015 1 8260B 8/18/16 23:29 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0092 0.00057 1 8260B 8/18/16 23:29 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 70-130 Dibromofluoromethane 95 % 84-123 Toluene-d8 103 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 15 0.47 100 MADEP VPH 8/19/16 19:18 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 15 1.8 100 MADEP VPH 8/19/16 19:18 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 15 0.15 100 MADEP VPH 8/19/16 19:18 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 99 % 70-130 2,5-Dibromotoluene (FID) 125 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 43 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: N-3 Attn: Brian Olin Prism Sample ID: 6080270-11 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 10:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 27 1.2 1 MADEP EPH 8/18/16 20:15 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 27 2.2 1 MADEP EPH 8/18/16 20:15 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 11 1.5 1 MADEP EPH 8/18/16 20:15 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 73 % 40-140 o-Terphenyl 74 % 40-140 2-Fluorobiphenyl 90 % 40-140 2-Bromonaphthalene 105 % 40-140 General Chemistry Parameters % Solids 92.9 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.35 0.055 1 8270D 8/18/16 19:20 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.35 0.053 1 8270D 8/18/16 19:20 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.35 0.049 1 8270D 8/18/16 19:20 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.35 0.051 1 8270D 8/18/16 19:20 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.35 0.068 1 8270D 8/18/16 19:20 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.35 0.066 1 8270D 8/18/16 19:20 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.35 0.068 1 8270D 8/18/16 19:20 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.35 0.054 1 8270D 8/18/16 19:20 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.35 0.049 1 8270D 8/18/16 19:20 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.35 0.043 1 8270D 8/18/16 19:20 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.35 0.047 1 8270D 8/18/16 19:20 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.35 0.051 1 8270D 8/18/16 19:20 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 19:20 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.35 0.056 1 8270D 8/18/16 19:20 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.35 0.045 1 8270D 8/18/16 19:20 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.35 0.064 1 8270D 8/18/16 19:20 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.35 0.069 1 8270D 8/18/16 19:20 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.35 0.043 1 8270D 8/18/16 19:20 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.35 0.053 1 8270D 8/18/16 19:20 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.35 0.060 1 8270D 8/18/16 19:20 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.35 0.049 1 8270D 8/18/16 19:20 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.35 0.042 1 8270D 8/18/16 19:20 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 19:20 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.35 0.054 1 8270D 8/18/16 19:20 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.35 0.048 1 8270D 8/18/16 19:20 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.35 0.051 1 8270D 8/18/16 19:20 JMV P61-10314 Anthracene BRL mg/kg dry 0.35 0.057 1 8270D 8/18/16 19:20 JMV P61-10314 Azobenzene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 19:20 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 19:20 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.35 0.038 1 8270D 8/18/16 19:20 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 44 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: N-3 Prism Sample ID: 6080270-11 Prism Work Order: 6080270 Time Collected: 08/12/16 10:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.35 0.041 1 8270D 8/18/16 19:20 Benzo(g,h,i)perylene BRL mg/kg dry 0.35 0.038 1 8270D 8/18/16 19:20 Benzo(k)fluoranthene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 19:20 Benzoic Acid BRL mg/kg dry 0.35 0.030 1 8270D 8/18/16 19:20 Benzyl alcohol BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 19:20 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.35 0.061 1 8270D 8/18/16 19:20 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 19:20 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.35 0.060 1 8270D 8/18/16 19:20 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.35 0.052 1 8270D 8/18/16 19:20 Butyl benzyl phthalate BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 19:20 Chrysene BRL mg/kg dry 0.35 0.044 1 8270D 8/18/16 19:20 Dibenzo(a,h)anthracene BRL mg/kg dry 0.35 0.043 1 8270D 8/18/16 19:20 Dibenzofuran BRL mg/kg dry 0.35 0.053 1 8270D 8/18/16 19:20 Diethyl phthalate BRL mg/kg dry 0.35 0.048 1 8270D 8/18/16 19:20 Dimethyl phthalate BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 19:20 Di-n-butyl phthalate BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 19:20 Di-n-octyl phthalate BRL mg/kg dry 0.35 0.043 1 8270D 8/18/16 19:20 Fluoranthene BRL mg/kg dry 0.35 0.045 1 8270D 8/18/16 19:20 Fluorene BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 19:20 Hexachlorobenzene BRL mg/kg dry 0.35 0.056 1 8270D 8/18/16 19:20 Hexachlorobutadiene BRL mg/kg dry 0.35 0.063 1 8270D 8/18/16 19:20 Hexachlorocyclopentadiene BRL mg/kg dry 0.35 0.063 1 8270D 8/18/16 19:20 Hexachloroethane BRL mg/kg dry 0.35 0.059 1 8270D 8/18/16 19:20 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.35 0.040 1 8270D 8/18/16 19:20 Isophorone BRL mg/kg dry 0.35 0.047 1 8270D 8/18/16 19:20 Naphthalene BRL mg/kg dry 0.35 0.056 1 8270D 8/18/16 19:20 Nitrobenzene BRL mg/kg dry 0.35 0.050 1 8270D 8/18/16 19:20 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.35 0.055 1 8270D 8/18/16 19:20 N-Nitrosodiphenylamine BRL mg/kg dry 0.35 0.053 1 8270D 8/18/16 19:20 Pentachlorophenol BRL mg/kg dry 0.35 0.041 1 8270D 8/18/16 19:20 Phenanthrene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 19:20 Phenol BRL mg/kg dry 0.35 0.052 1 8270D 8/18/16 19:20 Pyrene BRL mg/kg dry 0.35 0.046 1 8270D 8/18/16 19:20 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 66 % 39-132 2-Fluorobiphenyl 66 % 44-115 2-Fluorophenol 67 % 35-115 Nitrobenzene-d5 63 % 37-122 Phenol-d5 68 % 34-121 Terphenyl-d14 63 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0029 0.00024 1 8260B 8/18/16 23:57 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0029 0.00014 1 8260B 8/18/16 23:57 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 45 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: N-3 Prism Sample ID: 6080270-11 Prism Work Order: 6080270 Time Collected: 08/12/16 10:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0029 0.00020 1 8260B 8/18/16 23:57 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0029 0.00026 1 8260B 8/18/16 23:57 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0029 0.000081 1 8260B 8/18/16 23:57 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0029 0.00013 1 8260B 8/18/16 23:57 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0029 0.00016 1 8260B 8/18/16 23:57 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0029 0.00017 1 8260B 8/18/16 23:57 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0029 0.00037 1 8260B 8/18/16 23:57 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0029 0.00022 1 8260B 8/18/16 23:57 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0029 0.00022 1 8260B 8/18/16 23:57 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0029 0.00012 1 8260B 8/18/16 23:57 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0029 0.00014 1 8260B 8/18/16 23:57 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0029 0.00017 1 8260B 8/18/16 23:57 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0029 0.00018 1 8260B 8/18/16 23:57 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0029 0.00022 1 8260B 8/18/16 23:57 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0029 0.00019 1 8260B 8/18/16 23:57 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0029 0.00015 1 8260B 8/18/16 23:57 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0029 0.00012 1 8260B 8/18/16 23:57 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0029 0.00014 1 8260B 8/18/16 23:57 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0029 0.00015 1 8260B 8/18/16 23:57 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0029 0.00017 1 8260B 8/18/16 23:57 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0029 0.00014 1 8260B 8/18/16 23:57 ANG P61-10336 Acetone BRL mg/kg dry 0.029 0.00071 1 8260B 8/18/16 23:57 ANG P61-10336 Benzene BRL mg/kg dry 0.0018 0.00017 1 8260B 8/18/16 23:57 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0029 0.00024 1 8260B 8/18/16 23:57 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0029 0.00016 1 8260B 8/18/16 23:57 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0029 0.00016 1 8260B 8/18/16 23:57 ANG P61-10336 Bromoform BRL mg/kg dry 0.0029 0.00033 1 8260B 8/18/16 23:57 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0059 0.00036 1 8260B 8/18/16 23:57 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0029 0.00015 1 8260B 8/18/16 23:57 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0029 0.00016 1 8260B 8/18/16 23:57 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0059 0.00024 1 8260B 8/18/16 23:57 ANG P61-10336 Chloroform BRL mg/kg dry 0.0029 0.00021 1 8260B 8/18/16 23:57 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0029 0.00020 1 8260B 8/18/16 23:57 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0029 0.00012 1 8260B 8/18/16 23:57 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0029 0.000098 1 8260B 8/18/16 23:57 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0029 0.00012 1 8260B 8/18/16 23:57 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0029 0.00013 1 8260B 8/18/16 23:57 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0029 0.00011 1 8260B 8/18/16 23:57 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0029 0.00012 1 8260B 8/18/16 23:57 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0029 0.00017 1 8260B 8/18/16 23:57 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0059 0.00027 1 8260B 8/18/16 23:57 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.029 0.00026 1 8260B 8/18/16 23:57 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.059 0.00026 1 8260B 8/18/16 23:57 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 46 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: N-3 Attn: Brian Olin Prism Sample ID: 6080270-11 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 10:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.029 0.00025 1 8260B 8/18/16 23:57 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0029 0.00016 1 8260B 8/18/16 23:57 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0059 0.000094 1 8260B 8/18/16 23:57 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0059 0.000092 1 8260B 8/18/16 23:57 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0029 0.00015 1 8260B 8/18/16 23:57 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0029 0.00017 1 8260B 8/18/16 23:57 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0029 0.00012 1 8260B 8/18/16 23:57 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0029 0.00014 1 8260B 8/18/16 23:57 ANG P61-10336 Styrene BRL mg/kg dry 0.0029 0.00018 1 8260B 8/18/16 23:57 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0029 0.000099 1 8260B 8/18/16 23:57 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0029 0.00014 1 8260B 8/18/16 23:57 ANG P61-10336 Toluene BRL mg/kg dry 0.0029 0.00017 1 8260B 8/18/16 23:57 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0029 0.00018 1 8260B 8/18/16 23:57 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0029 0.00015 1 8260B 8/18/16 23:57 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0029 0.00019 1 8260B 8/18/16 23:57 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0029 0.00019 1 8260B 8/18/16 23:57 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.015 0.00040 1 8260B 8/18/16 23:57 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0029 0.00014 1 8260B 8/18/16 23:57 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0088 0.00055 1 8260B 8/18/16 23:57 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 70-130 Dibromofluoromethane 94 % 84-123 Toluene-d8 104 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 6.3 0.20 100 MADEP VPH 8/19/16 19:48 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 6.3 0.76 100 MADEP VPH 8/19/16 19:48 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 6.3 0.061 100 MADEP VPH 8/19/16 19:48 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 109 % 70-130 2,5-Dibromotoluene (FID) 137 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 47 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: W-3 Attn: Brian Olin Prism Sample ID: 6080270-12 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 10:40 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 29 1.2 1 MADEP EPH 8/18/16 20:52 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 29 2.4 1 MADEP EPH 8/18/16 20:52 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 12 1.6 1 MADEP EPH 8/18/16 20:52 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 75 % 40-140 o-Terphenyl 73 % 40-140 2-Fluorobiphenyl 89 % 40-140 2-Bromonaphthalene 101 % 40-140 General Chemistry Parameters % Solids 85.1 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.39 0.060 1 8270D 8/18/16 19:42 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.39 0.059 1 8270D 8/18/16 19:42 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.39 0.054 1 8270D 8/18/16 19:42 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.39 0.056 1 8270D 8/18/16 19:42 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.39 0.074 1 8270D 8/18/16 19:42 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.39 0.072 1 8270D 8/18/16 19:42 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.39 0.075 1 8270D 8/18/16 19:42 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.39 0.059 1 8270D 8/18/16 19:42 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.39 0.054 1 8270D 8/18/16 19:42 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.39 0.047 1 8270D 8/18/16 19:42 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.39 0.051 1 8270D 8/18/16 19:42 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.39 0.056 1 8270D 8/18/16 19:42 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.39 0.055 1 8270D 8/18/16 19:42 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.39 0.062 1 8270D 8/18/16 19:42 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.39 0.049 1 8270D 8/18/16 19:42 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.39 0.070 1 8270D 8/18/16 19:42 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.39 0.076 1 8270D 8/18/16 19:42 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.39 0.048 1 8270D 8/18/16 19:42 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.39 0.058 1 8270D 8/18/16 19:42 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.39 0.066 1 8270D 8/18/16 19:42 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.39 0.054 1 8270D 8/18/16 19:42 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.39 0.046 1 8270D 8/18/16 19:42 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.39 0.050 1 8270D 8/18/16 19:42 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.39 0.059 1 8270D 8/18/16 19:42 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.39 0.052 1 8270D 8/18/16 19:42 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.39 0.056 1 8270D 8/18/16 19:42 JMV P61-10314 Anthracene BRL mg/kg dry 0.39 0.062 1 8270D 8/18/16 19:42 JMV P61-10314 Azobenzene BRL mg/kg dry 0.39 0.051 1 8270D 8/18/16 19:42 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.39 0.050 1 8270D 8/18/16 19:42 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.39 0.042 1 8270D 8/18/16 19:42 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 48 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: W-3 Prism Sample ID: 6080270-12 Prism Work Order: 6080270 Time Collected: 08/12/16 10:40 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.39 0.045 1 8270D 8/18/16 19:42 Benzo(g,h,i)perylene BRL mg/kg dry 0.39 0.042 1 8270D 8/18/16 19:42 Benzo(k)fluoranthene BRL mg/kg dry 0.39 0.051 1 8270D 8/18/16 19:42 Benzoic Acid BRL mg/kg dry 0.39 0.032 1 8270D 8/18/16 19:42 Benzyl alcohol BRL mg/kg dry 0.39 0.051 1 8270D 8/18/16 19:42 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.39 0.067 1 8270D 8/18/16 19:42 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.39 0.054 1 8270D 8/18/16 19:42 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.39 0.066 1 8270D 8/18/16 19:42 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.39 0.057 1 8270D 8/18/16 19:42 Butyl benzyl phthalate BRL mg/kg dry 0.39 0.055 1 8270D 8/18/16 19:42 Chrysene BRL mg/kg dry 0.39 0.049 1 8270D 8/18/16 19:42 Dibenzo(a,h)anthracene BRL mg/kg dry 0.39 0.047 1 8270D 8/18/16 19:42 Dibenzofuran BRL mg/kg dry 0.39 0.059 1 8270D 8/18/16 19:42 Diethyl phthalate BRL mg/kg dry 0.39 0.053 1 8270D 8/18/16 19:42 Dimethyl phthalate BRL mg/kg dry 0.39 0.051 1 8270D 8/18/16 19:42 Di-n-butyl phthalate BRL mg/kg dry 0.39 0.055 1 8270D 8/18/16 19:42 Di-n-octyl phthalate BRL mg/kg dry 0.39 0.047 1 8270D 8/18/16 19:42 Fluoranthene BRL mg/kg dry 0.39 0.049 1 8270D 8/18/16 19:42 Fluorene BRL mg/kg dry 0.39 0.055 1 8270D 8/18/16 19:42 Hexachlorobenzene BRL mg/kg dry 0.39 0.061 1 8270D 8/18/16 19:42 Hexachlorobutadiene BRL mg/kg dry 0.39 0.069 1 8270D 8/18/16 19:42 Hexachlorocyclopentadiene BRL mg/kg dry 0.39 0.069 1 8270D 8/18/16 19:42 Hexachloroethane BRL mg/kg dry 0.39 0.065 1 8270D 8/18/16 19:42 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.39 0.044 1 8270D 8/18/16 19:42 Isophorone BRL mg/kg dry 0.39 0.052 1 8270D 8/18/16 19:42 Naphthalene BRL mg/kg dry 0.39 0.062 1 8270D 8/18/16 19:42 Nitrobenzene BRL mg/kg dry 0.39 0.055 1 8270D 8/18/16 19:42 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.39 0.061 1 8270D 8/18/16 19:42 N-Nitrosodiphenylamine BRL mg/kg dry 0.39 0.059 1 8270D 8/18/16 19:42 Pentachlorophenol BRL mg/kg dry 0.39 0.046 1 8270D 8/18/16 19:42 Phenanthrene BRL mg/kg dry 0.39 0.050 1 8270D 8/18/16 19:42 Phenol BRL mg/kg dry 0.39 0.057 1 8270D 8/18/16 19:42 Pyrene BRL mg/kg dry 0.39 0.051 1 8270D 8/18/16 19:42 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 83 % 39-132 2-Fluorobiphenyl 78 % 44-115 2-Fluorophenol 80 % 35-115 Nitrobenzene-d5 75 % 37-122 Phenol-d5 81 % 34-121 Terphenyl-d14 74 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0059 0.00048 1 8260B 8/19/16 0:24 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0059 0.00028 1 8260B 8/19/16 0:24 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 49 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: W-3 Prism Sample ID: 6080270-12 Prism Work Order: 6080270 Time Collected: 08/12/16 10:40 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0059 0.00040 1 8260B 8/19/16 0:24 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0059 0.00052 1 8260B 8/19/16 0:24 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0059 0.00016 1 8260B 8/19/16 0:24 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0059 0.00026 1 8260B 8/19/16 0:24 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0059 0.00032 1 8260B 8/19/16 0:24 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0059 0.00033 1 8260B 8/19/16 0:24 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0059 0.00075 1 8260B 8/19/16 0:24 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0059 0.00044 1 8260B 8/19/16 0:24 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0059 0.00045 1 8260B 8/19/16 0:24 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0059 0.00024 1 8260B 8/19/16 0:24 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0059 0.00028 1 8260B 8/19/16 0:24 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0059 0.00035 1 8260B 8/19/16 0:24 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0059 0.00036 1 8260B 8/19/16 0:24 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0059 0.00044 1 8260B 8/19/16 0:24 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0059 0.00039 1 8260B 8/19/16 0:24 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0059 0.00030 1 8260B 8/19/16 0:24 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0059 0.00023 1 8260B 8/19/16 0:24 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0059 0.00028 1 8260B 8/19/16 0:24 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0059 0.00030 1 8260B 8/19/16 0:24 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0059 0.00035 1 8260B 8/19/16 0:24 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0059 0.00028 1 8260B 8/19/16 0:24 ANG P61-10336 Acetone BRL mg/kg dry 0.059 0.0014 1 8260B 8/19/16 0:24 ANG P61-10336 Benzene BRL mg/kg dry 0.0035 0.00034 1 8260B 8/19/16 0:24 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0059 0.00049 1 8260B 8/19/16 0:24 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0059 0.00032 1 8260B 8/19/16 0:24 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0059 0.00033 1 8260B 8/19/16 0:24 ANG P61-10336 Bromoform BRL mg/kg dry 0.0059 0.00067 1 8260B 8/19/16 0:24 ANG P61-10336 Bromomethane BRL mg/kg dry 0.012 0.00073 1 8260B 8/19/16 0:24 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0059 0.00029 1 8260B 8/19/16 0:24 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0059 0.00031 1 8260B 8/19/16 0:24 ANG P61-10336 Chloroethane BRL mg/kg dry 0.012 0.00049 1 8260B 8/19/16 0:24 ANG P61-10336 Chloroform BRL mg/kg dry 0.0059 0.00042 1 8260B 8/19/16 0:24 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0059 0.00039 1 8260B 8/19/16 0:24 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0059 0.00025 1 8260B 8/19/16 0:24 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0059 0.00020 1 8260B 8/19/16 0:24 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0059 0.00024 1 8260B 8/19/16 0:24 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0059 0.00027 1 8260B 8/19/16 0:24 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0059 0.00023 1 8260B 8/19/16 0:24 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0059 0.00024 1 8260B 8/19/16 0:24 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0059 0.00035 1 8260B 8/19/16 0:24 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.012 0.00054 1 8260B 8/19/16 0:24 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.059 0.00053 1 8260B 8/19/16 0:24 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.12 0.00053 1 8260B 8/19/16 0:24 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 50 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: W-3 Attn: Brian Olin Prism Sample ID: 6080270-12 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 10:40 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.059 0.00050 1 8260B 8/19/16 0:24 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0059 0.00033 1 8260B 8/19/16 0:24 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.012 0.00019 1 8260B 8/19/16 0:24 ANG P61-10336 Naphthalene BRL mg/kg dry 0.012 0.00019 1 8260B 8/19/16 0:24 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0059 0.00030 1 8260B 8/19/16 0:24 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0059 0.00035 1 8260B 8/19/16 0:24 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0059 0.00024 1 8260B 8/19/16 0:24 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0059 0.00028 1 8260B 8/19/16 0:24 ANG P61-10336 Styrene BRL mg/kg dry 0.0059 0.00035 1 8260B 8/19/16 0:24 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0059 0.00020 1 8260B 8/19/16 0:24 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0059 0.00028 1 8260B 8/19/16 0:24 ANG P61-10336 Toluene BRL mg/kg dry 0.0059 0.00034 1 8260B 8/19/16 0:24 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0059 0.00035 1 8260B 8/19/16 0:24 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0059 0.00031 1 8260B 8/19/16 0:24 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0059 0.00038 1 8260B 8/19/16 0:24 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0059 0.00038 1 8260B 8/19/16 0:24 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.029 0.00081 1 8260B 8/19/16 0:24 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0059 0.00028 1 8260B 8/19/16 0:24 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.018 0.0011 1 8260B 8/19/16 0:24 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 70-130 Dibromofluoromethane 92 % 84-123 Toluene-d8 104 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID RLM C5-C8 Aliphatics BRL mg/kg dry 8.7 0.27 100 MADEP VPH 8/19/16 20:19 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 8.7 1.0 100 MADEP VPH 8/19/16 20:19 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 8.7 0.084 100 MADEP VPH 8/19/16 20:19 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 124 % 70-130 2,5-Dibromotoluene (FID) 157 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 51 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: S-3 Attn: Brian Olin Prism Sample ID: 6080270-13 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 10:50 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 31 1.3 1 MADEP EPH 8/18/16 21:28 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 31 2.5 1 MADEP EPH 8/18/16 21:28 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 12 1.7 1 MADEP EPH 8/18/16 21:28 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 76 % 40-140 o-Terphenyl 68 % 40-140 2-Fluorobiphenyl 92 % 40-140 2-Bromonaphthalene 106 % 40-140 General Chemistry Parameters % Solids 81.2 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.40 0.063 1 8270D 8/18/16 20:04 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.40 0.061 1 8270D 8/18/16 20:04 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.40 0.057 1 8270D 8/18/16 20:04 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.40 0.059 1 8270D 8/18/16 20:04 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.40 0.077 1 8270D 8/18/16 20:04 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.40 0.075 1 8270D 8/18/16 20:04 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.40 0.078 1 8270D 8/18/16 20:04 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.40 0.062 1 8270D 8/18/16 20:04 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.40 0.056 1 8270D 8/18/16 20:04 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.40 0.049 1 8270D 8/18/16 20:04 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.40 0.053 1 8270D 8/18/16 20:04 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.40 0.058 1 8270D 8/18/16 20:04 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.40 0.057 1 8270D 8/18/16 20:04 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.40 0.064 1 8270D 8/18/16 20:04 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.40 0.051 1 8270D 8/18/16 20:04 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.40 0.073 1 8270D 8/18/16 20:04 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.40 0.079 1 8270D 8/18/16 20:04 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.40 0.050 1 8270D 8/18/16 20:04 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.40 0.060 1 8270D 8/18/16 20:04 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.40 0.069 1 8270D 8/18/16 20:04 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.40 0.056 1 8270D 8/18/16 20:04 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.40 0.048 1 8270D 8/18/16 20:04 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.40 0.052 1 8270D 8/18/16 20:04 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.40 0.062 1 8270D 8/18/16 20:04 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.40 0.055 1 8270D 8/18/16 20:04 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.40 0.058 1 8270D 8/18/16 20:04 JMV P61-10314 Anthracene BRL mg/kg dry 0.40 0.065 1 8270D 8/18/16 20:04 JMV P61-10314 Azobenzene BRL mg/kg dry 0.40 0.053 1 8270D 8/18/16 20:04 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.40 0.053 1 8270D 8/18/16 20:04 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.40 0.043 1 8270D 8/18/16 20:04 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 52 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: S-3 Prism Sample ID: 6080270-13 Prism Work Order: 6080270 Time Collected: 08/12/16 10:50 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.40 0.047 1 8270D 8/18/16 20:04 Benzo(g,h,i)perylene BRL mg/kg dry 0.40 0.044 1 8270D 8/18/16 20:04 Benzo(k)fluoranthene BRL mg/kg dry 0.40 0.053 1 8270D 8/18/16 20:04 Benzoic Acid BRL mg/kg dry 0.40 0.034 1 8270D 8/18/16 20:04 Benzyl alcohol BRL mg/kg dry 0.40 0.053 1 8270D 8/18/16 20:04 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.40 0.070 1 8270D 8/18/16 20:04 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.40 0.057 1 8270D 8/18/16 20:04 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.40 0.069 1 8270D 8/18/16 20:04 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.40 0.060 1 8270D 8/18/16 20:04 Butyl benzyl phthalate BRL mg/kg dry 0.40 0.057 1 8270D 8/18/16 20:04 Chrysene BRL mg/kg dry 0.40 0.051 1 8270D 8/18/16 20:04 Dibenzo(a,h)anthracene BRL mg/kg dry 0.40 0.049 1 8270D 8/18/16 20:04 Dibenzofuran BRL mg/kg dry 0.40 0.061 1 8270D 8/18/16 20:04 Diethyl phthalate BRL mg/kg dry 0.40 0.055 1 8270D 8/18/16 20:04 Dimethyl phthalate BRL mg/kg dry 0.40 0.053 1 8270D 8/18/16 20:04 Di-n-butyl phthalate BRL mg/kg dry 0.40 0.057 1 8270D 8/18/16 20:04 Di-n-octyl phthalate BRL mg/kg dry 0.40 0.049 1 8270D 8/18/16 20:04 Fluoranthene BRL mg/kg dry 0.40 0.051 1 8270D 8/18/16 20:04 Fluorene BRL mg/kg dry 0.40 0.058 1 8270D 8/18/16 20:04 Hexachlorobenzene BRL mg/kg dry 0.40 0.064 1 8270D 8/18/16 20:04 Hexachlorobutadiene BRL mg/kg dry 0.40 0.072 1 8270D 8/18/16 20:04 Hexachlorocyclopentadiene BRL mg/kg dry 0.40 0.072 1 8270D 8/18/16 20:04 Hexachloroethane BRL mg/kg dry 0.40 0.067 1 8270D 8/18/16 20:04 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.40 0.046 1 8270D 8/18/16 20:04 Isophorone BRL mg/kg dry 0.40 0.054 1 8270D 8/18/16 20:04 Naphthalene BRL mg/kg dry 0.40 0.065 1 8270D 8/18/16 20:04 Nitrobenzene BRL mg/kg dry 0.40 0.057 1 8270D 8/18/16 20:04 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.40 0.063 1 8270D 8/18/16 20:04 N-Nitrosodiphenylamine BRL mg/kg dry 0.40 0.061 1 8270D 8/18/16 20:04 Pentachlorophenol BRL mg/kg dry 0.40 0.047 1 8270D 8/18/16 20:04 Phenanthrene BRL mg/kg dry 0.40 0.052 1 8270D 8/18/16 20:04 Phenol BRL mg/kg dry 0.40 0.059 1 8270D 8/18/16 20:04 Pyrene BRL mg/kg dry 0.40 0.053 1 8270D 8/18/16 20:04 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 77 % 39-132 2-Fluorobiphenyl 78 % 44-115 2-Fluorophenol 79 % 35-115 Nitrobenzene-d5 75 % 37-122 Phenol-d5 80 % 34-121 Terphenyl-d14 75 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0027 0.00022 1 8260B 8/19/16 0:52 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 0:52 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 53 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: S-3 Prism Sample ID: 6080270-13 Prism Work Order: 6080270 Time Collected: 08/12/16 10:50 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0027 0.00018 1 8260B 8/19/16 0:52 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0027 0.00024 1 8260B 8/19/16 0:52 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0027 0.000076 1 8260B 8/19/16 0:52 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0027 0.00012 1 8260B 8/19/16 0:52 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0027 0.00015 1 8260B 8/19/16 0:52 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 0:52 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0027 0.00035 1 8260B 8/19/16 0:52 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0027 0.00020 1 8260B 8/19/16 0:52 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0027 0.00021 1 8260B 8/19/16 0:52 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0027 0.00011 1 8260B 8/19/16 0:52 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 0:52 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 0:52 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0027 0.00017 1 8260B 8/19/16 0:52 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0027 0.00021 1 8260B 8/19/16 0:52 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0027 0.00018 1 8260B 8/19/16 0:52 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 0:52 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0027 0.00011 1 8260B 8/19/16 0:52 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 0:52 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 0:52 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 0:52 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 0:52 ANG P61-10336 Acetone BRL mg/kg dry 0.027 0.00067 1 8260B 8/19/16 0:52 ANG P61-10336 Benzene BRL mg/kg dry 0.0016 0.00016 1 8260B 8/19/16 0:52 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0027 0.00023 1 8260B 8/19/16 0:52 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0027 0.00015 1 8260B 8/19/16 0:52 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0027 0.00015 1 8260B 8/19/16 0:52 ANG P61-10336 Bromoform BRL mg/kg dry 0.0027 0.00031 1 8260B 8/19/16 0:52 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0055 0.00034 1 8260B 8/19/16 0:52 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 0:52 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 0:52 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0055 0.00023 1 8260B 8/19/16 0:52 ANG P61-10336 Chloroform BRL mg/kg dry 0.0027 0.00020 1 8260B 8/19/16 0:52 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0027 0.00018 1 8260B 8/19/16 0:52 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0027 0.00012 1 8260B 8/19/16 0:52 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0027 0.000092 1 8260B 8/19/16 0:52 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0027 0.00011 1 8260B 8/19/16 0:52 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0027 0.00012 1 8260B 8/19/16 0:52 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0027 0.00010 1 8260B 8/19/16 0:52 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0027 0.00011 1 8260B 8/19/16 0:52 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 0:52 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0055 0.00025 1 8260B 8/19/16 0:52 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.027 0.00025 1 8260B 8/19/16 0:52 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.055 0.00025 1 8260B 8/19/16 0:52 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 54 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: S-3 Attn: Brian Olin Prism Sample ID: 6080270-13 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 10:50 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.027 0.00023 1 8260B 8/19/16 0:52 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0027 0.00015 1 8260B 8/19/16 0:52 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0055 0.000087 1 8260B 8/19/16 0:52 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0055 0.000086 1 8260B 8/19/16 0:52 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 0:52 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 0:52 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0027 0.00011 1 8260B 8/19/16 0:52 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 0:52 ANG P61-10336 Styrene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 0:52 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0027 0.000092 1 8260B 8/19/16 0:52 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 0:52 ANG P61-10336 Toluene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 0:52 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 0:52 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 0:52 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0027 0.00018 1 8260B 8/19/16 0:52 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0027 0.00018 1 8260B 8/19/16 0:52 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.014 0.00037 1 8260B 8/19/16 0:52 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 0:52 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0082 0.00051 1 8260B 8/19/16 0:52 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 70-130 Dibromofluoromethane 93 % 84-123 Toluene-d8 105 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID RLM C5-C8 Aliphatics BRL mg/kg dry 7.3 0.23 100 MADEP VPH 8/19/16 20:49 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 7.3 0.88 100 MADEP VPH 8/19/16 20:49 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 7.3 0.070 100 MADEP VPH 8/19/16 20:49 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 120 % 70-130 2,5-Dibromotoluene (FID) 152 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 55 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: NW-2 Attn: Brian Olin Prism Sample ID: 6080270-14 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 15:00 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 27 1.2 1 MADEP EPH 8/18/16 22:04 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 27 2.2 1 MADEP EPH 8/18/16 22:04 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 11 1.5 1 MADEP EPH 8/18/16 22:04 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 68 % 40-140 o-Terphenyl 61 % 40-140 2-Fluorobiphenyl 85 % 40-140 2-Bromonaphthalene 101 % 40-140 General Chemistry Parameters % Solids 90.0 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.36 0.056 1 8270D 8/18/16 20:27 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 20:27 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 20:27 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.36 0.053 1 8270D 8/18/16 20:27 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.36 0.070 1 8270D 8/18/16 20:27 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.36 0.068 1 8270D 8/18/16 20:27 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.36 0.070 1 8270D 8/18/16 20:27 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 20:27 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.36 0.050 1 8270D 8/18/16 20:27 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 20:27 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 20:27 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 20:27 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 20:27 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.36 0.058 1 8270D 8/18/16 20:27 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.36 0.046 1 8270D 8/18/16 20:27 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.36 0.066 1 8270D 8/18/16 20:27 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.36 0.071 1 8270D 8/18/16 20:27 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.36 0.045 1 8270D 8/18/16 20:27 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.36 0.054 1 8270D 8/18/16 20:27 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.36 0.062 1 8270D 8/18/16 20:27 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 20:27 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.36 0.043 1 8270D 8/18/16 20:27 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 20:27 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.36 0.056 1 8270D 8/18/16 20:27 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.36 0.049 1 8270D 8/18/16 20:27 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 20:27 JMV P61-10314 Anthracene BRL mg/kg dry 0.36 0.058 1 8270D 8/18/16 20:27 JMV P61-10314 Azobenzene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 20:27 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 20:27 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.36 0.039 1 8270D 8/18/16 20:27 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 56 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: NW-2 Prism Sample ID: 6080270-14 Prism Work Order: 6080270 Time Collected: 08/12/16 15:00 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.36 0.042 1 8270D 8/18/16 20:27 Benzo(g,h,i)perylene BRL mg/kg dry 0.36 0.040 1 8270D 8/18/16 20:27 Benzo(k)fluoranthene BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 20:27 Benzoic Acid BRL mg/kg dry 0.36 0.030 1 8270D 8/18/16 20:27 Benzyl alcohol BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 20:27 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.36 0.063 1 8270D 8/18/16 20:27 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 20:27 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.36 0.062 1 8270D 8/18/16 20:27 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.36 0.054 1 8270D 8/18/16 20:27 Butyl benzyl phthalate BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 20:27 Chrysene BRL mg/kg dry 0.36 0.046 1 8270D 8/18/16 20:27 Dibenzo(a,h)anthracene BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 20:27 Dibenzofuran BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 20:27 Diethyl phthalate BRL mg/kg dry 0.36 0.050 1 8270D 8/18/16 20:27 Dimethyl phthalate BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 20:27 Di-n-butyl phthalate BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 20:27 Di-n-octyl phthalate BRL mg/kg dry 0.36 0.044 1 8270D 8/18/16 20:27 Fluoranthene BRL mg/kg dry 0.36 0.046 1 8270D 8/18/16 20:27 Fluorene BRL mg/kg dry 0.36 0.052 1 8270D 8/18/16 20:27 Hexachlorobenzene BRL mg/kg dry 0.36 0.057 1 8270D 8/18/16 20:27 Hexachlorobutadiene BRL mg/kg dry 0.36 0.065 1 8270D 8/18/16 20:27 Hexachlorocyclopentadiene BRL mg/kg dry 0.36 0.064 1 8270D 8/18/16 20:27 Hexachloroethane BRL mg/kg dry 0.36 0.061 1 8270D 8/18/16 20:27 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.36 0.042 1 8270D 8/18/16 20:27 Isophorone BRL mg/kg dry 0.36 0.049 1 8270D 8/18/16 20:27 Naphthalene BRL mg/kg dry 0.36 0.058 1 8270D 8/18/16 20:27 Nitrobenzene BRL mg/kg dry 0.36 0.051 1 8270D 8/18/16 20:27 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.36 0.057 1 8270D 8/18/16 20:27 N-Nitrosodiphenylamine BRL mg/kg dry 0.36 0.055 1 8270D 8/18/16 20:27 Pentachlorophenol BRL mg/kg dry 0.36 0.043 1 8270D 8/18/16 20:27 Phenanthrene BRL mg/kg dry 0.36 0.047 1 8270D 8/18/16 20:27 Phenol BRL mg/kg dry 0.36 0.053 1 8270D 8/18/16 20:27 Pyrene BRL mg/kg dry 0.36 0.048 1 8270D 8/18/16 20:27 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 71 % 39-132 2-Fluorobiphenyl 74 % 44-115 2-Fluorophenol 76 % 35-115 Nitrobenzene-d5 73 % 37-122 Phenol-d5 79 % 34-121 Terphenyl-d14 76 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0029 0.00024 1 8260B 8/19/16 1:19 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0029 0.00014 1 8260B 8/19/16 1:19 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 57 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: NW-2 Prism Sample ID: 6080270-14 Prism Work Order: 6080270 Time Collected: 08/12/16 15:00 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0029 0.00020 1 8260B 8/19/16 1:19 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0029 0.00026 1 8260B 8/19/16 1:19 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0029 0.000082 1 8260B 8/19/16 1:19 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0029 0.00013 1 8260B 8/19/16 1:19 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0029 0.00016 1 8260B 8/19/16 1:19 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0029 0.00017 1 8260B 8/19/16 1:19 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0029 0.00038 1 8260B 8/19/16 1:19 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0029 0.00022 1 8260B 8/19/16 1:19 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0029 0.00023 1 8260B 8/19/16 1:19 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0029 0.00012 1 8260B 8/19/16 1:19 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0029 0.00014 1 8260B 8/19/16 1:19 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0029 0.00018 1 8260B 8/19/16 1:19 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0029 0.00018 1 8260B 8/19/16 1:19 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0029 0.00022 1 8260B 8/19/16 1:19 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0029 0.00020 1 8260B 8/19/16 1:19 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0029 0.00015 1 8260B 8/19/16 1:19 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0029 0.00012 1 8260B 8/19/16 1:19 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0029 0.00014 1 8260B 8/19/16 1:19 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0029 0.00015 1 8260B 8/19/16 1:19 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0029 0.00018 1 8260B 8/19/16 1:19 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0029 0.00014 1 8260B 8/19/16 1:19 ANG P61-10336 Acetone BRL mg/kg dry 0.029 0.00072 1 8260B 8/19/16 1:19 ANG P61-10336 Benzene BRL mg/kg dry 0.0018 0.00017 1 8260B 8/19/16 1:19 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0029 0.00025 1 8260B 8/19/16 1:19 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0029 0.00016 1 8260B 8/19/16 1:19 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0029 0.00016 1 8260B 8/19/16 1:19 ANG P61-10336 Bromoform BRL mg/kg dry 0.0029 0.00033 1 8260B 8/19/16 1:19 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0059 0.00036 1 8260B 8/19/16 1:19 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0029 0.00015 1 8260B 8/19/16 1:19 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0029 0.00016 1 8260B 8/19/16 1:19 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0059 0.00025 1 8260B 8/19/16 1:19 ANG P61-10336 Chloroform BRL mg/kg dry 0.0029 0.00021 1 8260B 8/19/16 1:19 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0029 0.00020 1 8260B 8/19/16 1:19 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0029 0.00013 1 8260B 8/19/16 1:19 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0029 0.000099 1 8260B 8/19/16 1:19 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0029 0.00012 1 8260B 8/19/16 1:19 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0029 0.00013 1 8260B 8/19/16 1:19 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0029 0.00011 1 8260B 8/19/16 1:19 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0029 0.00012 1 8260B 8/19/16 1:19 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0029 0.00017 1 8260B 8/19/16 1:19 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0059 0.00027 1 8260B 8/19/16 1:19 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.029 0.00027 1 8260B 8/19/16 1:19 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.059 0.00027 1 8260B 8/19/16 1:19 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 58 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: NW-2 Attn: Brian Olin Prism Sample ID: 6080270-14 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 15:00 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.029 0.00025 1 8260B 8/19/16 1:19 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0029 0.00017 1 8260B 8/19/16 1:19 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0059 0.000094 1 8260B 8/19/16 1:19 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0059 0.000093 1 8260B 8/19/16 1:19 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0029 0.00015 1 8260B 8/19/16 1:19 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0029 0.00018 1 8260B 8/19/16 1:19 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0029 0.00012 1 8260B 8/19/16 1:19 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0029 0.00014 1 8260B 8/19/16 1:19 ANG P61-10336 Styrene BRL mg/kg dry 0.0029 0.00018 1 8260B 8/19/16 1:19 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0029 0.00010 1 8260B 8/19/16 1:19 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0029 0.00014 1 8260B 8/19/16 1:19 ANG P61-10336 Toluene BRL mg/kg dry 0.0029 0.00017 1 8260B 8/19/16 1:19 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0029 0.00018 1 8260B 8/19/16 1:19 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0029 0.00015 1 8260B 8/19/16 1:19 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0029 0.00019 1 8260B 8/19/16 1:19 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0029 0.00019 1 8260B 8/19/16 1:19 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.015 0.00040 1 8260B 8/19/16 1:19 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0029 0.00014 1 8260B 8/19/16 1:19 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0088 0.00055 1 8260B 8/19/16 1:19 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 70-130 Dibromofluoromethane 97 % 84-123 Toluene-d8 104 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 7.3 0.23 100 MADEP VPH 8/19/16 22:21 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 7.3 0.88 100 MADEP VPH 8/19/16 22:21 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 7.3 0.070 100 MADEP VPH 8/19/16 22:21 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 104 % 70-130 2,5-Dibromotoluene (FID) 132 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 59 of 87 P R S M Laboratory Report ` Full -Service Analytical & / environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: B-2 Attn: Brian Olin Prism Sample ID: 6080270-15 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 15:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 26 1.1 1 MADEP EPH 8/18/16 22:41 ZRC P61-10227 C19-C36 Aliphatics BRL mg/kg dry 26 2.1 1 MADEP EPH 8/18/16 22:41 ZRC P61-10227 C11-C22 Aromatics BRL mg/kg dry 10 1.4 1 MADEP EPH 8/18/16 22:41 ZRC P61-10227 Surrogate Recovery Control Limits 1-Chlorooctadecane 59 % 40-140 o-Terphenyl 55 % 40-140 2-Fluorobiphenyl 97 % 40-140 2-Bromonaphthalene 112 % 40-140 General Chemistry Parameters % Solids 95.4 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 SM2540 G 8/18/16 15:45 JLB P6H0334 1,2,4-Trichlorobenzene BRL mg/kg dry 0.34 0.054 1 8270D 8/18/16 20:49 JMV P61-10314 1,2-Dichlorobenzene BRL mg/kg dry 0.34 0.052 1 8270D 8/18/16 20:49 JMV P61-10314 1,3-Dichlorobenzene BRL mg/kg dry 0.34 0.048 1 8270D 8/18/16 20:49 JMV P61-10314 1,4-Dichlorobenzene BRL mg/kg dry 0.34 0.050 1 8270D 8/18/16 20:49 JMV P61-10314 1-Methyl naphthalene BRL mg/kg dry 0.34 0.066 1 8270D 8/18/16 20:49 JMV P61-10314 2,4,6-Trichlorophenol BRL mg/kg dry 0.34 0.064 1 8270D 8/18/16 20:49 JMV P61-10314 2,4-Dichlorophenol BRL mg/kg dry 0.34 0.066 1 8270D 8/18/16 20:49 JMV P61-10314 2,4-Dimethylphenol BRL mg/kg dry 0.34 0.053 1 8270D 8/18/16 20:49 JMV P61-10314 2,4-Dinitrophenol BRL mg/kg dry 0.34 0.048 1 8270D 8/18/16 20:49 JMV P61-10314 2,4-Dinitrotoluene BRL mg/kg dry 0.34 0.042 1 8270D 8/18/16 20:49 JMV P61-10314 2,6-Dinitrotoluene BRL mg/kg dry 0.34 0.046 1 8270D 8/18/16 20:49 JMV P61-10314 2-Chloronaphthalene BRL mg/kg dry 0.34 0.050 1 8270D 8/18/16 20:49 JMV P61-10314 2-Chlorophenol BRL mg/kg dry 0.34 0.049 1 8270D 8/18/16 20:49 JMV P61-10314 2-Methyl naphthalene BRL mg/kg dry 0.34 0.055 1 8270D 8/18/16 20:49 JMV P61-10314 2-Methylphenol BRL mg/kg dry 0.34 0.044 1 8270D 8/18/16 20:49 JMV P61-10314 2-Nitrophenol BRL mg/kg dry 0.34 0.062 1 8270D 8/18/16 20:49 JMV P61-10314 3,3'-Dichlorobenzidine BRL mg/kg dry 0.34 0.068 1 8270D 8/18/16 20:49 JMV P61-10314 3/4-Methyl phenol BRL mg/kg dry 0.34 0.042 1 8270D 8/18/16 20:49 JMV P61-10314 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.34 0.052 1 8270D 8/18/16 20:49 JMV P61-10314 4-Bromophenyl phenyl ether BRL mg/kg dry 0.34 0.059 1 8270D 8/18/16 20:49 JMV P61-10314 4-Chloro-3-methylphenol BRL mg/kg dry 0.34 0.048 1 8270D 8/18/16 20:49 JMV P61-10314 4-Chloroaniline BRL mg/kg dry 0.34 0.041 1 8270D 8/18/16 20:49 JMV P61-10314 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 20:49 JMV P61-10314 4-Nitrophenol BRL mg/kg dry 0.34 0.053 1 8270D 8/18/16 20:49 JMV P61-10314 Acenaphthene BRL mg/kg dry 0.34 0.047 1 8270D 8/18/16 20:49 JMV P61-10314 Acenaphthylene BRL mg/kg dry 0.34 0.050 1 8270D 8/18/16 20:49 JMV P61-10314 Anthracene BRL mg/kg dry 0.34 0.055 1 8270D 8/18/16 20:49 JMV P61-10314 Azobenzene BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 20:49 JMV P61-10314 Benzo(a)anthracene BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 20:49 JMV P61-10314 Benzo(a)pyrene BRL mg/kg dry 0.34 0.037 1 8270D 8/18/16 20:49 JMV P61-10314 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 60 of 87 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 08/22/2016 ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Client Sample ID: B-2 Prism Sample ID: 6080270-15 Prism Work Order: 6080270 Time Collected: 08/12/16 15:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.34 0.040 1 8270D 8/18/16 20:49 Benzo(g,h,i)perylene BRL mg/kg dry 0.34 0.038 1 8270D 8/18/16 20:49 Benzo(k)fluoranthene BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 20:49 Benzoic Acid BRL mg/kg dry 0.34 0.029 1 8270D 8/18/16 20:49 Benzyl alcohol BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 20:49 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.34 0.060 1 8270D 8/18/16 20:49 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.34 0.048 1 8270D 8/18/16 20:49 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.34 0.059 1 8270D 8/18/16 20:49 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.34 0.051 1 8270D 8/18/16 20:49 Butyl benzyl phthalate BRL mg/kg dry 0.34 0.049 1 8270D 8/18/16 20:49 Chrysene BRL mg/kg dry 0.34 0.043 1 8270D 8/18/16 20:49 Dibenzo(a,h)anthracene BRL mg/kg dry 0.34 0.042 1 8270D 8/18/16 20:49 Dibenzofuran BRL mg/kg dry 0.34 0.052 1 8270D 8/18/16 20:49 Diethyl phthalate BRL mg/kg dry 0.34 0.047 1 8270D 8/18/16 20:49 Dimethyl phthalate BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 20:49 Di-n-butyl phthalate BRL mg/kg dry 0.34 0.049 1 8270D 8/18/16 20:49 Di-n-octyl phthalate BRL mg/kg dry 0.34 0.042 1 8270D 8/18/16 20:49 Fluoranthene BRL mg/kg dry 0.34 0.044 1 8270D 8/18/16 20:49 Fluorene BRL mg/kg dry 0.34 0.049 1 8270D 8/18/16 20:49 Hexachlorobenzene BRL mg/kg dry 0.34 0.054 1 8270D 8/18/16 20:49 Hexachlorobutadiene BRL mg/kg dry 0.34 0.062 1 8270D 8/18/16 20:49 Hexachlorocyclopentadiene BRL mg/kg dry 0.34 0.061 1 8270D 8/18/16 20:49 Hexachloroethane BRL mg/kg dry 0.34 0.057 1 8270D 8/18/16 20:49 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.34 0.039 1 8270D 8/18/16 20:49 Isophorone BRL mg/kg dry 0.34 0.046 1 8270D 8/18/16 20:49 Naphthalene BRL mg/kg dry 0.34 0.055 1 8270D 8/18/16 20:49 Nitrobenzene BRL mg/kg dry 0.34 0.049 1 8270D 8/18/16 20:49 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.34 0.054 1 8270D 8/18/16 20:49 N-Nitrosodiphenylamine BRL mg/kg dry 0.34 0.052 1 8270D 8/18/16 20:49 Pentachlorophenol BRL mg/kg dry 0.34 0.041 1 8270D 8/18/16 20:49 Phenanthrene BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 20:49 Phenol BRL mg/kg dry 0.34 0.051 1 8270D 8/18/16 20:49 Pyrene BRL mg/kg dry 0.34 0.045 1 8270D 8/18/16 20:49 Surrogate Recovery JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 JMV P61-10314 Control Limits 2,4,6-Tribromophenol 72 % 39-132 2-Fluorobiphenyl 73 % 44-115 2-Fluorophenol 77 % 35-115 Nitrobenzene-d5 72 % 37-122 Phenol-d5 78 % 34-121 Terphenyl-d14 73 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0027 0.00022 1 8260B 8/19/16 1:47 ANG P61-10336 1,1,1-Trichloroethane BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 1:47 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 61 of 87 ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Project: Swans Run Sample Matrix: Solid Laboratory Report 08/22/2016 Client Sample ID: B-2 Prism Sample ID: 6080270-15 Prism Work Order: 6080270 Time Collected: 08/12/16 15:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0027 0.00018 1 8260B 8/19/16 1:47 ANG P61-10336 1,1,2-Trichloroethane BRL mg/kg dry 0.0027 0.00024 1 8260B 8/19/16 1:47 ANG P61-10336 1,1-Dichloroethane BRL mg/kg dry 0.0027 0.000076 1 8260B 8/19/16 1:47 ANG P61-10336 1,1-Dichloroethylene BRL mg/kg dry 0.0027 0.00012 1 8260B 8/19/16 1:47 ANG P61-10336 1,1-Dichloropropylene BRL mg/kg dry 0.0027 0.00015 1 8260B 8/19/16 1:47 ANG P61-10336 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0027 0.00015 1 8260B 8/19/16 1:47 ANG P61-10336 1,2,3-Trichloropropane BRL mg/kg dry 0.0027 0.00035 1 8260B 8/19/16 1:47 ANG P61-10336 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0027 0.00020 1 8260B 8/19/16 1:47 ANG P61-10336 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0027 0.00021 1 8260B 8/19/16 1:47 ANG P61-10336 1,2-Dibromoethane BRL mg/kg dry 0.0027 0.00011 1 8260B 8/19/16 1:47 ANG P61-10336 1,2-Dichlorobenzene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 1:47 ANG P61-10336 1,2-Dichloroethane BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 1:47 ANG P61-10336 1,2-Dichloropropane BRL mg/kg dry 0.0027 0.00017 1 8260B 8/19/16 1:47 ANG P61-10336 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0027 0.00021 1 8260B 8/19/16 1:47 ANG P61-10336 1,3-Dichlorobenzene BRL mg/kg dry 0.0027 0.00018 1 8260B 8/19/16 1:47 ANG P61-10336 1,3-Dichloropropane BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 1:47 ANG P61-10336 1,4-Dichlorobenzene BRL mg/kg dry 0.0027 0.00011 1 8260B 8/19/16 1:47 ANG P61-10336 2,2-Dichloropropane BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 1:47 ANG P61-10336 2-Chlorotoluene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 1:47 ANG P61-10336 4-Chlorotoluene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 1:47 ANG P61-10336 4-Isopropyltoluene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 1:47 ANG P61-10336 Acetone BRL mg/kg dry 0.027 0.00066 1 8260B 8/19/16 1:47 ANG P61-10336 Benzene BRL mg/kg dry 0.0016 0.00016 1 8260B 8/19/16 1:47 ANG P61-10336 Bromobenzene BRL mg/kg dry 0.0027 0.00023 1 8260B 8/19/16 1:47 ANG P61-10336 Bromochloromethane BRL mg/kg dry 0.0027 0.00015 1 8260B 8/19/16 1:47 ANG P61-10336 Bromodichloromethane BRL mg/kg dry 0.0027 0.00015 1 8260B 8/19/16 1:47 ANG P61-10336 Bromoform BRL mg/kg dry 0.0027 0.00031 1 8260B 8/19/16 1:47 ANG P61-10336 Bromomethane BRL mg/kg dry 0.0054 0.00034 1 8260B 8/19/16 1:47 ANG P61-10336 Carbon Tetrachloride BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 1:47 ANG P61-10336 Chlorobenzene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 1:47 ANG P61-10336 Chloroethane BRL mg/kg dry 0.0054 0.00023 1 8260B 8/19/16 1:47 ANG P61-10336 Chloroform BRL mg/kg dry 0.0027 0.00020 1 8260B 8/19/16 1:47 ANG P61-10336 Chloromethane BRL mg/kg dry 0.0027 0.00018 1 8260B 8/19/16 1:47 ANG P61-10336 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0027 0.00012 1 8260B 8/19/16 1:47 ANG P61-10336 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0027 0.000091 1 8260B 8/19/16 1:47 ANG P61-10336 Dibromochloromethane BRL mg/kg dry 0.0027 0.00011 1 8260B 8/19/16 1:47 ANG P61-10336 Dichlorodifluoromethane BRL mg/kg dry 0.0027 0.00012 1 8260B 8/19/16 1:47 ANG P61-10336 Ethylbenzene BRL mg/kg dry 0.0027 0.00010 1 8260B 8/19/16 1:47 ANG P61-10336 Isopropyl Ether BRL mg/kg dry 0.0027 0.00011 1 8260B 8/19/16 1:47 ANG P61-10336 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 1:47 ANG P61-10336 m,p-Xylenes BRL mg/kg dry 0.0054 0.00025 1 8260B 8/19/16 1:47 ANG P61-10336 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.027 0.00025 1 8260B 8/19/16 1:47 ANG P61-10336 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.054 0.00025 1 8260B 8/19/16 1:47 ANG P61-10336 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 62 of 87 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 08/22/2016 LABORATORIES INC. ECS Carolinas, LLP (Charlotte) Project: Swans Run Client Sample ID: B-2 Attn: Brian Olin Prism Sample ID: 6080270-15 1812 Center Park Drive, Suite D Prism Work Order: 6080270 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 08/12/16 15:30 Time Submitted: 08/15/16 11:51 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0.027 0.00023 1 8260B 8/19/16 1:47 ANG P61-10336 Methylene Chloride BRL mg/kg dry 0.0027 0.00015 1 8260B 8/19/16 1:47 ANG P61-10336 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0054 0.000087 1 8260B 8/19/16 1:47 ANG P61-10336 Naphthalene BRL mg/kg dry 0.0054 0.000086 1 8260B 8/19/16 1:47 ANG P61-10336 n-Butylbenzene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 1:47 ANG P61-10336 n-Propylbenzene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 1:47 ANG P61-10336 o-Xylene BRL mg/kg dry 0.0027 0.00011 1 8260B 8/19/16 1:47 ANG P61-10336 sec-Butylbenzene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 1:47 ANG P61-10336 Styrene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 1:47 ANG P61-10336 tert-Butylbenzene BRL mg/kg dry 0.0027 0.000092 1 8260B 8/19/16 1:47 ANG P61-10336 Tetrachloroethylene BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 1:47 ANG P61-10336 Toluene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 1:47 ANG P61-10336 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0027 0.00016 1 8260B 8/19/16 1:47 ANG P61-10336 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0027 0.00014 1 8260B 8/19/16 1:47 ANG P61-10336 Trichloroethylene BRL mg/kg dry 0.0027 0.00018 1 8260B 8/19/16 1:47 ANG P61-10336 Trichlorofluoromethane BRL mg/kg dry 0.0027 0.00018 1 8260B 8/19/16 1:47 ANG P61-10336 Vinyl acetate BRL mg/kg dry 0.014 0.00037 1 8260B 8/19/16 1:47 ANG P61-10336 Vinyl chloride BRL mg/kg dry 0.0027 0.00013 1 8260B 8/19/16 1:47 ANG P61-10336 Xylenes, total BRL mg/kg dry 0.0082 0.00051 1 8260B 8/19/16 1:47 ANG P61-10336 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 70-130 Dibromofluoromethane 96 % 84-123 Toluene-d8 104 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 6.0 0.18 100 MADEP VPH 8/19/16 22:52 ANG P61-10361 C9-Cl2 Aliphatics BRL mg/kg dry 6.0 0.71 100 MADEP VPH 8/19/16 22:52 ANG P61-10361 C9-Cl0 Aromatics BRL mg/kg dry 6.0 0.057 100 MADEP VPH 8/19/16 22:52 ANG P61-10361 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 92 % 70-130 2,5-Dibromotoluene (FID) 118 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 63 of 87 P R I IS M EService Analytical Environmental Solutions LABORATORIES, INC. Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Prism Work Order: 6080270 Attn: Brian Olin Time Submitted: 8/15/2016 11:51:OOAM 1812 Center Park Drive, Suite D Charlotte, NC 28217 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6HO336 - 5035 Blank (P6H0336-BLK1) Prepared & Analyzed: 08/18/16 1,1,1,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1,1,2,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,2-Trichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,3-Trichloropropane BRL 0.0050 mg/kg wet 1,2,4-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,4-Trimethyl benzene BRL 0.0050 mg/kg wet 1,2-Dibromoethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0.0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Trimethyl benzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0.0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chlorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.050 mg/kg wet Benzene BRL 0.0030 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromoform BRL 0.0050 mg/kg wet Bromomethane BRL 0.010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chloroethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethane BRL 0.0050 mg/kg wet cis-1,2-Dichloroethylene BRL 0.0050 mg/kg wet cis-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodifluoromethane BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbenzene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.050 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0.10 mg/kg wet Methyl Isobutyl Ketone BRL 0.050 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 64 of 87 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO336 - 5035 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P6H0336-BLK1) Prepared & Analyzed: 08/18/16 Methylene Chloride BRL 0.0050 mg/kg wet Methyl-tert-Butyl Ether BRL 0.010 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet sec-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butyl benzene BRL 0.0050 mg/kg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet trans- 1,2-Dichloroethylene BRL 0.0050 mg/kg wet trans- 1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichloroethylene BRL 0.0050 mg/kg wet Trichlorofluoromethane BRL 0.0050 mg/kg wet Vinyl acetate BRL 0.025 mg/kg wet Vinyl chloride BRL 0.0050 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate:4-Bromofluorobenzene 50.9 ug/L 50.00 102 70-130 Surrogate: Dibromofluoromethane 44.9 ug/L 50.00 90 84-123 Surrogate: Toluene-d8 52.6 ug/L 50.00 105 76-129 LCS (P6HO336-BS1) Prepared & Analyzed: 08/18/16 1,1,1,2-Tetrachloroethane 0.0421 0.0050 mg/kg wet 0.05000 84 72-115 1,1,1-Trichloroethane 0.0336 0.0050 mg/kg wet 0.05000 67 67-131 1,1,2,2-Tetrachloroethane 0.0558 0.0050 mg/kg wet 0.05000 112 56-126 1,1,2-Trichloroethane 0.0481 0.0050 mg/kg wet 0.05000 96 70-133 1,1-Dichloroethane 0.0437 0.0050 mg/kg wet 0.05000 87 74-127 1,1-Dichloroethylene 0.0429 0.0050 mg/kg wet 0.05000 86 67-149 1, 1 -Dichloropropylene 0.0426 0.0050 mg/kg wet 0.05000 85 71-130 1,2,3-Trichlorobenzene 0.0559 0.0050 mg/kg wet 0.05000 112 68-130 1,2,3-Trichloropropane 0.0434 0.0050 mg/kg wet 0.05000 87 60-137 1,2,4-Trichlorobenzene 0.0537 0.0050 mg/kg wet 0.05000 107 66-125 1,2,4-Trimethylbenzene 0.0480 0.0050 mg/kg wet 0.05000 96 69-129 1,2-Dibromoethane 0.0472 0.0050 mg/kg wet 0.05000 94 70-132 1,2-Dichlorobenzene 0.0518 0.0050 mg/kg wet 0.05000 104 72-123 1,2-Dichloroethane 0.0337 0.0050 mg/kg wet 0.05000 67 68-128 L 1,2-Dichloropropane 0.0494 0.0050 mg/kg wet 0.05000 99 73-130 1,3,5-Trimethylbenzene 0.0477 0.0050 mg/kg wet 0.05000 95 69-128 1,3-Dichlorobenzene 0.0525 0.0050 mg/kg wet 0.05000 105 71-120 1,3-Dichloropropane 0.0465 0.0050 mg/kg wet 0.05000 93 75-124 1,4-Dichlorobenzene 0.0523 0.0050 mg/kg wet 0.05000 105 71-123 2,2-Dichloropropane 0.0366 0.0050 mg/kg wet 0.05000 73 50-142 2-Chlorotoluene 0.0483 0.0050 mg/kg wet 0.05000 97 67-124 4-Chlorotoluene 0.0498 0.0050 mg/kg wet 0.05000 100 71-126 4-Isopropyltoluene 0.0498 0.0050 mg/kg wet 0.05000 100 68-129 Acetone 0.0778 0.050 mg/kg wet 0.1000 78 29-198 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 65 of 87 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO336 - 5035 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P6110336-113SI) Prepared & Analyzed: 08/18/16 Benzene 0.0491 0.0030 mg/kg wet 0.05000 98 74-127 Bromobenzene 0.0471 0.0050 mg/kg wet 0.05000 94 73-125 Bromochloromethane 0.0456 0.0050 mg/kg wet 0.05000 91 72-134 Bromodichloromethane 0.0369 0.0050 mg/kg wet 0.05000 74 75-122 L Bromoform 0.0388 0.0050 mg/kg wet 0.05000 78 66-135 Bromomethane 0.0426 0.010 mg/kg wet 0.05000 85 20-180 Carbon Tetrachloride 0.0324 0.0050 mg/kg wet 0.05000 65 64-143 Chlorobenzene 0.0484 0.0050 mg/kg wet 0.05000 97 74-118 Chloroethane 0.0541 0.010 mg/kg wet 0.05000 108 33-149 Chloroform 0.0372 0.0050 mg/kg wet 0.05000 74 73-127 Chloromethane 0.0651 0.0050 mg/kg wet 0.05000 130 45-143 cis-1,2-Dichloroethylene 0.0436 0.0050 mg/kg wet 0.05000 87 76-134 cis-1,3-Dichloropropylene 0.0452 0.0050 mg/kg wet 0.05000 90 71-125 Dibromochloromethane 0.0405 0.0050 mg/kg wet 0.05000 81 73-122 Dichlorodifluoromethane 0.0426 0.0050 mg/kg wet 0.05000 85 26-146 Ethylbenzene 0.0440 0.0050 mg/kg wet 0.05000 88 74-128 Isopropyl Ether 0.0506 0.0050 mg/kg wet 0.05000 101 59-159 Isopropylbenzene (Cumene) 0.0502 0.0050 mg/kg wet 0.05000 100 68-126 m,p-Xylenes 0.0874 0.010 mg/kg wet 0.1000 87 75-124 Methyl Butyl Ketone (2-Hexanone) 0.0508 0.050 mg/kg wet 0.05000 102 61-157 Methyl Ethyl Ketone (2-Butanone) 0.0565 0.10 mg/kg wet 0.05000 113 63-149 J Methyl Isobutyl Ketone 0.0438 0.050 mg/kg wet 0.05000 88 57-162 J Methylene Chloride 0.0457 0.0050 mg/kg wet 0.05000 91 74-129 Methyl-tert-Butyl Ether 0.0402 0.010 mg/kg wet 0.05000 80 70-130 Naphthalene 0.0546 0.010 mg/kg wet 0.05000 109 57-157 n-Butylbenzene 0.0490 0.0050 mg/kg wet 0.05000 98 65-135 n-Propylbenzene 0.0507 0.0050 mg/kg wet 0.05000 101 67-130 o-Xylene 0.0453 0.0050 mg/kg wet 0.05000 91 74-126 sec-Butylbenzene 0.0509 0.0050 mg/kg wet 0.05000 102 66-131 Styrene 0.0512 0.0050 mg/kg wet 0.05000 102 77-121 tert-Butyl benzene 0.0495 0.0050 mg/kg wet 0.05000 99 67-132 Tetrachloroethylene 0.0419 0.0050 mg/kg wet 0.05000 84 68-130 Toluene 0.0457 0.0050 mg/kg wet 0.05000 91 71-129 trans- 1,2-Dichloroethylene 0.0433 0.0050 mg/kg wet 0.05000 87 73-132 trans- 1,3-Dichloropropylene 0.0396 0.0050 mg/kg wet 0.05000 79 68-123 Trichloroethylene 0.0451 0.0050 mg/kg wet 0.05000 90 75-133 Trichlorofluoromethane 0.0214 0.0050 mg/kg wet 0.05000 43 44-146 L Vinyl acetate 0.0500 0.025 mg/kg wet 0.05000 100 85-161 Vinyl chloride 0.0590 0.0050 mg/kg wet 0.05000 118 48-147 Xylenes, total 0.133 0.015 mg/kg wet 0.1500 88 74-126 Surrogate:4-Bromofluorobenzene 51.9 ug/L 50.00 104 70-130 Surrogate: Dibromofluoromethane 44.9 ug/L 50.00 90 84-123 Surrogate: Toluene-d8 52.9 ug/L 50.00 106 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 66 of 87 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO336 - 5035 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P6HO336-BSD1) Prepared & Analyzed: 08/18/16 1,1,1,2-Tetrachloroethane 0.0416 0.0050 mg/kg wet 0.05000 83 72-115 1 20 1,1,1-Trichloroethane 0.0338 0.0050 mg/kg wet 0.05000 68 67-131 0.7 20 1,1,2,2-Tetrachloroethane 0.0559 0.0050 mg/kg wet 0.05000 112 56-126 0.2 20 1,1,2-Trichloroethane 0.0486 0.0050 mg/kg wet 0.05000 97 70-133 1 20 1,1-Dichloroethane 0.0452 0.0050 mg/kg wet 0.05000 90 74-127 3 20 1,1-Dichloroethylene 0.0429 0.0050 mg/kg wet 0.05000 86 67-149 0.1 20 1, 1 -Dichloropropylene 0.0418 0.0050 mg/kg wet 0.05000 84 71-130 2 20 1,2,3-Trichlorobenzene 0.0564 0.0050 mg/kg wet 0.05000 113 68-130 0.9 20 1,2,3-Trichloropropane 0.0432 0.0050 mg/kg wet 0.05000 86 60-137 0.6 20 1,2,4-Trichlorobenzene 0.0545 0.0050 mg/kg wet 0.05000 109 66-125 1 20 1,2,4-Trimethylbenzene 0.0491 0.0050 mg/kg wet 0.05000 98 69-129 2 20 1,2-Dibromoethane 0.0481 0.0050 mg/kg wet 0.05000 96 70-132 2 20 1,2-Dichlorobenzene 0.0530 0.0050 mg/kg wet 0.05000 106 72-123 2 20 1,2-Dichloroethane 0.0339 0.0050 mg/kg wet 0.05000 68 68-128 0.4 20 1,2-Dichloropropane 0.0498 0.0050 mg/kg wet 0.05000 100 73-130 0.6 20 1,3,5-Trimethylbenzene 0.0490 0.0050 mg/kg wet 0.05000 98 69-128 3 20 1,3-Dichlorobenzene 0.0540 0.0050 mg/kg wet 0.05000 108 71-120 3 20 1,3-Dichloropropane 0.0469 0.0050 mg/kg wet 0.05000 94 75-124 0.9 20 1,4-Dichlorobenzene 0.0532 0.0050 mg/kg wet 0.05000 106 71-123 2 20 2,2-Dichloropropane 0.0371 0.0050 mg/kg wet 0.05000 74 50-142 1 20 2-Chlorotoluene 0.0507 0.0050 mg/kg wet 0.05000 101 67-124 5 20 4-Chlorotoluene 0.0520 0.0050 mg/kg wet 0.05000 104 71-126 4 20 4-Isopropyltoluene 0.0505 0.0050 mg/kg wet 0.05000 101 68-129 1 20 Acetone 0.0751 0.050 mg/kg wet 0.1000 75 29-198 4 20 Benzene 0.0504 0.0030 mg/kg wet 0.05000 101 74-127 3 20 Bromobenzene 0.0478 0.0050 mg/kg wet 0.05000 96 73-125 1 20 Bromochloromethane 0.0465 0.0050 mg/kg wet 0.05000 93 72-134 2 20 Bromodichloromethane 0.0365 0.0050 mg/kg wet 0.05000 73 75-122 1 20 Bromoform 0.0350 0.0050 mg/kg wet 0.05000 70 66-135 10 20 Bromomethane 0.0476 0.010 mg/kg wet 0.05000 95 20-180 11 20 Carbon Tetrachloride 0.0317 0.0050 mg/kg wet 0.05000 63 64-143 2 20 Chlorobenzene 0.0488 0.0050 mg/kg wet 0.05000 98 74-118 0.8 20 Chloroethane 0.0557 0.010 mg/kg wet 0.05000 111 33-149 3 20 Chloroform 0.0378 0.0050 mg/kg wet 0.05000 76 73-127 2 20 Chloromethane 0.0667 0.0050 mg/kg wet 0.05000 133 45-143 2 20 cis-1,2-Dichloroethylene 0.0437 0.0050 mg/kg wet 0.05000 87 76-134 0.3 20 cis-1,3-Dichloropropylene 0.0456 0.0050 mg/kg wet 0.05000 91 71-125 0.9 20 Dibromochloromethane 0.0390 0.0050 mg/kg wet 0.05000 78 73-122 4 20 Dichlorodifluoromethane 0.0438 0.0050 mg/kg wet 0.05000 88 26-146 3 20 Ethylbenzene 0.0454 0.0050 mg/kg wet 0.05000 91 74-128 3 20 Isopropyl Ether 0.0518 0.0050 mg/kg wet 0.05000 104 59-159 2 20 Isopropylbenzene (Cumene) 0.0527 0.0050 mg/kg wet 0.05000 105 68-126 5 20 m,p-Xylenes 0.0893 0.010 mg/kg wet 0.1000 89 75-124 2 20 Methyl Butyl Ketone (2-Hexanone) 0.0484 0.050 mg/kg wet 0.05000 97 61-157 5 20 Methyl Ethyl Ketone (2-Butanone) 0.0551 0.10 mg/kg wet 0.05000 110 63-149 3 20 Methyl Isobutyl Ketone 0.0433 0.050 mg/kg wet 0.05000 87 57-162 1 20 L L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 67 of 87 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO336 - 5035 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P6H0336-BSD1) Prepared & Analyzed: 08/18/16 Methylene Chloride 0.0569 0.0050 mg/kg wet 0.05000 114 74-129 22 20 D Methyl-tert-Butyl Ether 0.0409 0.010 mg/kg wet 0.05000 82 70-130 2 20 Naphthalene 0.0548 0.010 mg/kg wet 0.05000 110 57-157 0.4 20 n-Butylbenzene 0.0503 0.0050 mg/kg wet 0.05000 101 65-135 3 20 n-Propylbenzene 0.0528 0.0050 mg/kg wet 0.05000 106 67-130 4 20 o-Xylene 0.0463 0.0050 mg/kg wet 0.05000 93 74-126 2 20 sec-Butylbenzene 0.0522 0.0050 mg/kg wet 0.05000 104 66-131 3 20 Styrene 0.0515 0.0050 mg/kg wet 0.05000 103 77-121 0.6 20 tert-Butylbenzene 0.0513 0.0050 mg/kg wet 0.05000 103 67-132 4 20 Tetrachloroethylene 0.0442 0.0050 mg/kg wet 0.05000 88 68-130 5 20 Toluene 0.0476 0.0050 mg/kg wet 0.05000 95 71-129 4 20 trans-1,2-Dichloroethylene 0.0447 0.0050 mg/kg wet 0.05000 89 73-132 3 20 trans- 1,3-Dichloropropylene 0.0395 0.0050 mg/kg wet 0.05000 79 68-123 0.2 20 Trichloroethylene 0.0457 0.0050 mg/kg wet 0.05000 91 75-133 1 20 Trichlorofluoromethane 0.0213 0.0050 mg/kg wet 0.05000 43 44-146 0.6 20 L Vinyl acetate 0.0509 0.025 mg/kg wet 0.05000 102 85-161 2 20 Vinyl chloride 0.0625 0.0050 mg/kg wet 0.05000 125 48-147 6 20 Xylenes, total 0.136 0.015 mg/kg wet 0.1500 90 74-126 2 20 Surrogate:4-Bromofluorobenzene 51.8 ug/L 50.00 104 70-130 Surrogate: Dibromofluoromethane 42.8 ug/L 50.00 86 84-123 Surrogate: Toluene-d8 53.2 ug/L 50.00 106 76-129 Batch P6HO365 - 5035 Blank (P6H0365-BLK1) Prepared & Analyzed: 08/19/16 1,1,1,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1,1,2,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,2-Trichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,3-Trichloropropane BRL 0.0050 mg/kg wet 1,2,4-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,4-Trimethyl benzene BRL 0.0050 mg/kg wet 1,2-Dibromoethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0.0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Trimethyl benzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0.0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chlorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 68 of 87 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Prism Work Order: 6080270 Attn: Brian Olin Time Submitted: 8/15/2016 11:51:OOAM 1812 Center Park Drive, Suite D Charlotte, NC 28217 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6HO365 - 5035 Blank (P6H0365-BLK1) Prepared & Analyzed: 08/19/16 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.050 mg/kg wet Benzene BRL 0.0030 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromoform BRL 0.0050 mg/kg wet Bromomethane BRL 0.010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chloroethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethane BRL 0.0050 mg/kg wet cis-1,2-Dichloroethylene BRL 0.0050 mg/kg wet cis-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodifluoromethane BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbenzene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.050 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0.10 mg/kg wet Methyl Isobutyl Ketone BRL 0.050 mg/kg wet Methylene Chloride BRL 0.0050 mg/kg wet Methyl-tert-Butyl Ether BRL 0.010 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet sec-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butylbenzene BRL 0.0050 mg/kg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet trans-1,2-Dichloroethylene BRL 0.0050 mg/kg wet trans-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichloroethylene BRL 0.0050 mg/kg wet Trichlorofluoromethane BRL 0.0050 mg/kg wet Vinyl acetate BRL 0.025 mg/kg wet Vinyl chloride BRL 0.0050 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate:4-Bromofluorobenzene 48.2 ug/L 50.00 96 70-130 Surrogate: Dibromofluoromethane 50.1 ug/L 50.00 100 84-123 Surrogate: Toluene-d8 49.1 ug/L 50.00 98 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 69 of 87 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO365 - 5035 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P6110365-113SI) Prepared & Analyzed: 08/19/16 1,1,1,2-Tetrachloroethane 0.0480 0.0050 mg/kg wet 0.05000 96 72-115 1,1,1-Trichloroethane 0.0482 0.0050 mg/kg wet 0.05000 96 67-131 1,1,2,2-Tetrachloroethane 0.0479 0.0050 mg/kg wet 0.05000 96 56-126 1,1,2-Trichloroethane 0.0455 0.0050 mg/kg wet 0.05000 91 70-133 1,1-Dichloroethane 0.0489 0.0050 mg/kg wet 0.05000 98 74-127 1,1-Dichloroethylene 0.0518 0.0050 mg/kg wet 0.05000 104 67-149 1, 1 -Dichloropropylene 0.0486 0.0050 mg/kg wet 0.05000 97 71-130 1,2,3-Trichlorobenzene 0.0493 0.0050 mg/kg wet 0.05000 99 68-130 1,2,3-Trichloropropane 0.0459 0.0050 mg/kg wet 0.05000 92 60-137 1,2,4-Trichlorobenzene 0.0489 0.0050 mg/kg wet 0.05000 98 66-125 1,2,4-Trimethylbenzene 0.0496 0.0050 mg/kg wet 0.05000 99 69-129 1,2-Dibromoethane 0.0475 0.0050 mg/kg wet 0.05000 95 70-132 1,2-Dichlorobenzene 0.0495 0.0050 mg/kg wet 0.05000 99 72-123 1,2-Dichloroethane 0.0477 0.0050 mg/kg wet 0.05000 95 68-128 1,2-Dichloropropane 0.0479 0.0050 mg/kg wet 0.05000 96 73-130 1,3,5-Trimethylbenzene 0.0494 0.0050 mg/kg wet 0.05000 99 69-128 1,3-Dichlorobenzene 0.0495 0.0050 mg/kg wet 0.05000 99 71-120 1,3-Dichloropropane 0.0464 0.0050 mg/kg wet 0.05000 93 75-124 1,4-Dichlorobenzene 0.0495 0.0050 mg/kg wet 0.05000 99 71-123 2,2-Dichloropropane 0.0497 0.0050 mg/kg wet 0.05000 99 50-142 2-Chlorotoluene 0.0502 0.0050 mg/kg wet 0.05000 100 67-124 4-Chlorotoluene 0.0505 0.0050 mg/kg wet 0.05000 101 71-126 4-Isopropyltoluene 0.0489 0.0050 mg/kg wet 0.05000 98 68-129 Acetone 0.0891 0.050 mg/kg wet 0.1000 89 29-198 Benzene 0.0492 0.0030 mg/kg wet 0.05000 98 74-127 Bromobenzene 0.0490 0.0050 mg/kg wet 0.05000 98 73-125 Bromochloromethane 0.0495 0.0050 mg/kg wet 0.05000 99 72-134 Bromodichloromethane 0.0496 0.0050 mg/kg wet 0.05000 99 75-122 Bromoform 0.0448 0.0050 mg/kg wet 0.05000 90 66-135 Bromomethane 0.0429 0.010 mg/kg wet 0.05000 86 20-180 Carbon Tetrachloride 0.0478 0.0050 mg/kg wet 0.05000 96 64-143 Chlorobenzene 0.0474 0.0050 mg/kg wet 0.05000 95 74-118 Chloroethane 0.0348 0.010 mg/kg wet 0.05000 70 33-149 Chloroform 0.0466 0.0050 mg/kg wet 0.05000 93 73-127 Chloromethane 0.0455 0.0050 mg/kg wet 0.05000 91 45-143 cis-1,2-Dichloroethylene 0.0507 0.0050 mg/kg wet 0.05000 101 76-134 cis-1,3-Dichloropropylene 0.0513 0.0050 mg/kg wet 0.05000 103 71-125 Dibromochloromethane 0.0481 0.0050 mg/kg wet 0.05000 96 73-122 Dichlorodifluoromethane 0.0476 0.0050 mg/kg wet 0.05000 95 26-146 Ethylbenzene 0.0474 0.0050 mg/kg wet 0.05000 95 74-128 Isopropyl Ether 0.0462 0.0050 mg/kg wet 0.05000 92 59-159 Isopropylbenzene (Cumene) 0.0501 0.0050 mg/kg wet 0.05000 100 68-126 m,p-Xylenes 0.0962 0.010 mg/kg wet 0.1000 96 75-124 Methyl Butyl Ketone (2-Hexanone) 0.0455 0.050 mg/kg wet 0.05000 91 61-157 Methyl Ethyl Ketone (2-Butanone) 0.0433 0.10 mg/kg wet 0.05000 87 63-149 Methyl Isobutyl Ketone 0.0458 0.050 mg/kg wet 0.05000 92 57-162 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 70 of 87 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO365 - 5035 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P6H0365-BS1) Prepared & Analyzed: 08/19/16 Methylene Chloride 0.0476 0.0050 mg/kg wet 0.05000 95 74-129 Methyl-tert-Butyl Ether 0.0475 0.010 mg/kg wet 0.05000 95 70-130 Naphthalene 0.0478 0.010 mg/kg wet 0.05000 96 57-157 n-Butylbenzene 0.0496 0.0050 mg/kg wet 0.05000 99 65-135 n-Propylbenzene 0.0512 0.0050 mg/kg wet 0.05000 102 67-130 o-Xylene 0.0483 0.0050 mg/kg wet 0.05000 97 74-126 sec-Butylbenzene 0.0498 0.0050 mg/kg wet 0.05000 100 66-131 Styrene 0.0498 0.0050 mg/kg wet 0.05000 100 77-121 tert-Butyl benzene 0.0502 0.0050 mg/kg wet 0.05000 100 67-132 Tetrachloroethylene 0.0477 0.0050 mg/kg wet 0.05000 95 68-130 Toluene 0.0491 0.0050 mg/kg wet 0.05000 98 71-129 trans- 1,2-Dichloroethylene 0.0506 0.0050 mg/kg wet 0.05000 101 73-132 trans- 1,3-Dichloropropylene 0.0486 0.0050 mg/kg wet 0.05000 97 68-123 Trichloroethylene 0.0504 0.0050 mg/kg wet 0.05000 101 75-133 Trichlorofluoromethane 0.0484 0.0050 mg/kg wet 0.05000 97 44-146 Vinyl acetate 0.0463 0.025 mg/kg wet 0.05000 93 85-161 Vinyl chloride 0.0490 0.0050 mg/kg wet 0.05000 98 48-147 Xylenes, total 0.144 0.015 mg/kg wet 0.1500 96 74-126 Surrogate:4-Bromofluorobenzene 50.8 ug/L 50.00 102 70-130 Surrogate: Dibromofluoromethane 50.6 ug/L 50.00 101 84-123 Surrogate: Toluene-d8 49.1 ug/L 50.00 98 76-129 LCS Dup (P6H0365-BSD1) Prepared & Analyzed: 08/19/16 1,1,1,2-Tetrachloroethane 0.0463 0.0050 mg/kg wet 0.05000 93 72-115 4 20 1,1,1-Trichloroethane 0.0460 0.0050 mg/kg wet 0.05000 92 67-131 5 20 1,1,2,2-Tetrachloroethane 0.0461 0.0050 mg/kg wet 0.05000 92 56-126 4 20 1,1,2-Trichloroethane 0.0466 0.0050 mg/kg wet 0.05000 93 70-133 2 20 1,1-Dichloroethane 0.0460 0.0050 mg/kg wet 0.05000 92 74-127 6 20 1,1-Dichloroethylene 0.0494 0.0050 mg/kg wet 0.05000 99 67-149 5 20 1, 1 -Dichloropropylene 0.0457 0.0050 mg/kg wet 0.05000 91 71-130 6 20 1,2,3-Trichlorobenzene 0.0487 0.0050 mg/kg wet 0.05000 97 68-130 1 20 1,2,3-Trichloropropane 0.0453 0.0050 mg/kg wet 0.05000 91 60-137 1 20 1,2,4-Trichlorobenzene 0.0487 0.0050 mg/kg wet 0.05000 97 66-125 0.2 20 1,2,4-Trimethylbenzene 0.0472 0.0050 mg/kg wet 0.05000 94 69-129 5 20 1,2-Dibromoethane 0.0469 0.0050 mg/kg wet 0.05000 94 70-132 1 20 1,2-Dichlorobenzene 0.0481 0.0050 mg/kg wet 0.05000 96 72-123 3 20 1,2-Dichloroethane 0.0457 0.0050 mg/kg wet 0.05000 91 68-128 4 20 1,2-Dichloropropane 0.0447 0.0050 mg/kg wet 0.05000 89 73-130 7 20 1,3,5-Trimethylbenzene 0.0472 0.0050 mg/kg wet 0.05000 94 69-128 5 20 1,3-Dichlorobenzene 0.0476 0.0050 mg/kg wet 0.05000 95 71-120 4 20 1,3-Dichloropropane 0.0463 0.0050 mg/kg wet 0.05000 93 75-124 0.2 20 1,4-Dichlorobenzene 0.0484 0.0050 mg/kg wet 0.05000 97 71-123 2 20 2,2-Dichloropropane 0.0478 0.0050 mg/kg wet 0.05000 96 50-142 4 20 2-Chlorotoluene 0.0487 0.0050 mg/kg wet 0.05000 97 67-124 3 20 4-Chlorotoluene 0.0491 0.0050 mg/kg wet 0.05000 98 71-126 3 20 4-Isopropyltoluene 0.0473 0.0050 mg/kg wet 0.05000 95 68-129 3 20 Acetone 0.0872 0.050 mg/kg wet 0.1000 87 29-198 2 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 71 of 87 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO365 - 5035 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (1361-10365-13SD1) Prepared & Analyzed: 08/19/16 Benzene 0.0469 0.0030 mg/kg wet 0.05000 94 74-127 5 20 Bromobenzene 0.0478 0.0050 mg/kg wet 0.05000 96 73-125 3 20 Bromochloromethane 0.0469 0.0050 mg/kg wet 0.05000 94 72-134 5 20 Bromodichloromethane 0.0474 0.0050 mg/kg wet 0.05000 95 75-122 5 20 Bromoform 0.0448 0.0050 mg/kg wet 0.05000 90 66-135 0.07 20 Bromomethane 0.0414 0.010 mg/kg wet 0.05000 83 20-180 4 20 Carbon Tetrachloride 0.0454 0.0050 mg/kg wet 0.05000 91 64-143 5 20 Chlorobenzene 0.0469 0.0050 mg/kg wet 0.05000 94 74-118 1 20 Chloroethane 0.0325 0.010 mg/kg wet 0.05000 65 33-149 7 20 Chloroform 0.0444 0.0050 mg/kg wet 0.05000 89 73-127 5 20 Chloromethane 0.0443 0.0050 mg/kg wet 0.05000 89 45-143 3 20 cis-1,2-Dichloroethylene 0.0477 0.0050 mg/kg wet 0.05000 95 76-134 6 20 cis-1,3-Dichloropropylene 0.0481 0.0050 mg/kg wet 0.05000 96 71-125 6 20 Dibromochloromethane 0.0464 0.0050 mg/kg wet 0.05000 93 73-122 4 20 Dichlorodifluoromethane 0.0439 0.0050 mg/kg wet 0.05000 88 26-146 8 20 Ethylbenzene 0.0452 0.0050 mg/kg wet 0.05000 90 74-128 5 20 Isopropyl Ether 0.0445 0.0050 mg/kg wet 0.05000 89 59-159 4 20 Isopropylbenzene (Cumene) 0.0483 0.0050 mg/kg wet 0.05000 97 68-126 4 20 m,p-Xylenes 0.0929 0.010 mg/kg wet 0.1000 93 75-124 3 20 Methyl Butyl Ketone (2-Hexanone) 0.0448 0.050 mg/kg wet 0.05000 90 61-157 2 20 Methyl Ethyl Ketone (2-Butanone) 0.0406 0.10 mg/kg wet 0.05000 81 63-149 6 20 Methyl Isobutyl Ketone 0.0444 0.050 mg/kg wet 0.05000 89 57-162 3 20 Methylene Chloride 0.0459 0.0050 mg/kg wet 0.05000 92 74-129 4 20 Methyl-tert-Butyl Ether 0.0465 0.010 mg/kg wet 0.05000 93 70-130 2 20 Naphthalene 0.0467 0.010 mg/kg wet 0.05000 93 57-157 2 20 n-Butylbenzene 0.0478 0.0050 mg/kg wet 0.05000 96 65-135 4 20 n-Propylbenzene 0.0490 0.0050 mg/kg wet 0.05000 98 67-130 4 20 o-Xylene 0.0473 0.0050 mg/kg wet 0.05000 95 74-126 2 20 sec-Butylbenzene 0.0478 0.0050 mg/kg wet 0.05000 96 66-131 4 20 Styrene 0.0488 0.0050 mg/kg wet 0.05000 98 77-121 2 20 tert-Butyl benzene 0.0479 0.0050 mg/kg wet 0.05000 96 67-132 5 20 Tetrachloroethylene 0.0451 0.0050 mg/kg wet 0.05000 90 68-130 6 20 Toluene 0.0461 0.0050 mg/kg wet 0.05000 92 71-129 6 20 trans- 1,2-Dichloroethylene 0.0479 0.0050 mg/kg wet 0.05000 96 73-132 6 20 trans- 1,3-Dichloropropylene 0.0476 0.0050 mg/kg wet 0.05000 95 68-123 2 20 Trichloroethylene 0.0469 0.0050 mg/kg wet 0.05000 94 75-133 7 20 Trichlorofluoromethane 0.0439 0.0050 mg/kg wet 0.05000 88 44-146 10 20 Vinyl acetate 0.0428 0.025 mg/kg wet 0.05000 86 85-161 8 20 Vinyl chloride 0.0454 0.0050 mg/kg wet 0.05000 91 48-147 8 20 Xylenes, total 0.140 0.015 mg/kg wet 0.1500 93 74-126 3 20 Surrogate:4-Bromofluorobenzene 51.0 ug/L 50.00 102 70-130 Surrogate: Dibromofluoromethane 51.0 ug/L 50.00 102 84-123 Surrogate: Toluene-d8 50.0 ug/L 50.00 100 76-129 J J J This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 72 of 87 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Prism Work Order: 6080270 Attn: Brian Olin Time Submitted: 8/15/2016 11:51:OOAM 1812 Center Park Drive, Suite D Charlotte, NC 28217 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6HO314 - 3546 Blank (P6H0314-BLK1) Prepared & Analyzed: 08/18/16 1,2,4-Trichlorobenzene BRL 0.33 mg/kg wet 1,2-Dichlorobenzene BRL 0.33 mg/kg wet 1,3-Dichlorobenzene BRL 0.33 mg/kg wet 1,4-Dichlorobenzene BRL 0.33 mg/kg wet 1-Methyl naphthalene BRL 0.33 mg/kg wet 2,4,6-Trichlorophenol BRL 0.33 mg/kg wet 2,4-Dichlorophenol BRL 0.33 mg/kg wet 2,4-Dimethylphenol BRL 0.33 mg/kg wet 2,4-Dinitrophenol BRL 0.33 mg/kg wet 2,4-Dinitrotoluene BRL 0.33 mg/kg wet 2,6-Dinitrotoluene BRL 0.33 mg/kg wet 2-Chloronaphthalene BRL 0.33 mg/kg wet 2-Chlorophenol BRL 0.33 mg/kg wet 2-Methyl naphthalene BRL 0.33 mg/kg wet 2-Methylphenol BRL 0.33 mg/kg wet 2-Nitrophenol BRL 0.33 mg/kg wet 3,3'-Dichlorobenzidine BRL 0.33 mg/kg wet 3/4-Methyl phenol BRL 0.33 mg/kg wet 4,6-Dinitro-2-methylphenol BRL 0.33 mg/kg wet 4-Bromophenyl phenyl ether BRL 0.33 mg/kg wet 4-Chloro-3-methylphenol BRL 0.33 mg/kg wet 4-Chloroaniline BRL 0.33 mg/kg wet 4-Chlorophenyl phenyl ether BRL 0.33 mg/kg wet 4-Nitrophenol BRL 0.33 mg/kg wet Acenaphthene BRL 0.33 mg/kg wet Acenaphthylene BRL 0.33 mg/kg wet Anthracene BRL 0.33 mg/kg wet Azobenzene BRL 0.33 mg/kg wet Benzo(a)anthracene BRL 0.33 mg/kg wet Benzo(a)pyrene BRL 0.33 mg/kg wet Benzo(b)fluoranthene BRL 0.33 mg/kg wet Benzo(g,h,i)perylene BRL 0.33 mg/kg wet Benzo(k)fluoranthene BRL 0.33 mg/kg wet Benzoic Acid BRL 0.33 mg/kg wet Benzyl alcohol BRL 0.33 mg/kg wet bis(2-Chloroethoxy)methane BRL 0.33 mg/kg wet Bis(2-Chloroethyl)ether BRL 0.33 mg/kg wet Bis(2-chloroisopropyl)ether BRL 0.33 mg/kg wet Bis(2-Ethylhexyl)phthalate BRL 0.33 mg/kg wet Butyl benzyl phthalate BRL 0.33 mg/kg wet Chrysene BRL 0.33 mg/kg wet Dibenzo(a,h)anthracene BRL 0.33 mg/kg wet Dibenzofuran BRL 0.33 mg/kg wet Diethyl phthalate BRL 0.33 mg/kg wet Dimethyl phthalate BRL 0.33 mg/kg wet Di-n-butyl phthalate BRL 0.33 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 73 of 87 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO314 - 3546 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P6H0314-BLK1) Prepared & Analyzed: 08/18/16 Di-n-octyl phthalate BRL 0.33 mg/kg wet Fluoranthene BRL 0.33 mg/kg wet Fluorene BRL 0.33 mg/kg wet Hexachlorobenzene BRL 0.33 mg/kg wet Hexachlorobutadiene BRL 0.33 mg/kg wet Hexachlorocyclopentadiene BRL 0.33 mg/kg wet Hexachloroethane BRL 0.33 mg/kg wet Indeno(1,2,3-cd)pyrene BRL 0.33 mg/kg wet Isophorone BRL 0.33 mg/kg wet Naphthalene BRL 0.33 mg/kg wet Nitrobenzene BRL 0.33 mg/kg wet N-Nitroso-di-n-propylamine BRL 0.33 mg/kg wet N-Nitrosodiphenylamine BRL 0.33 mg/kg wet Pentachlorophenol BRL 0.33 mg/kg wet Phenanthrene BRL 0.33 mg/kg wet Phenol BRL 0.33 mg/kg wet Pyrene BRL 0.33 mg/kg wet Surrogate: 2,4,6-Tribromophenol 3.16 mg/kg wet 3.329 95 39-132 Surrogate: 2-Fluorobiphenyl 1.46 mg/kg wet 1.664 88 44-115 Surrogate: 2-Fluorophenol 3.07 mg/kg wet 3.329 92 35-115 Surrogate: Nitrobenzene-d5 1.38 mg/kg wet 1.664 83 37-122 Surrogate: Phenol-d5 3.11 mg/kg wet 3.329 94 34-121 Surrogate: Terphenyl-d14 1.49 mg/kg wet 1.664 89 54-127 LCS (KH0314-113SI) Prepared & Analyzed: 08/18/16 1,2,4-Trichlorobenzene 1.05 0.33 mg/kg wet 1.666 63 34-118 1,2-Dichlorobenzene 0.952 0.33 mg/kg wet 1.666 57 33-117 1,3-Dichlorobenzene 0.903 0.33 mg/kg wet 1.666 54 30-115 1,4-Dichlorobenzene 0.918 0.33 mg/kg wet 1.666 55 31-115 1-Methyl naphthalene 1.23 0.33 mg/kg wet 1.666 74 40-119 2,4,6-Trichlorophenol 1.28 0.33 mg/kg wet 1.666 77 39-126 2,4-Dichlorophenol 1.26 0.33 mg/kg wet 1.666 76 40-122 2,4-Dimethylphenol 1.27 0.33 mg/kg wet 1.666 76 30-127 2,4-Dinitrophenol 1.03 0.33 mg/kg wet 1.666 62 27-129 2,4-Dinitrotoluene 1.46 0.33 mg/kg wet 1.666 87 48-126 2,6-Dinitrotoluene 1.33 0.33 mg/kg wet 1.666 80 46-124 2-Chloronaphthalene 1.62 0.33 mg/kg wet 1.666 97 41-114 2-Chlorophenol 1.10 0.33 mg/kg wet 1.666 66 34-121 2-Methyl naphthalene 1.18 0.33 mg/kg wet 1.666 71 38-122 2-Methylphenol 1.16 0.33 mg/kg wet 1.666 70 32-122 2-Nitrophenol 1.11 0.33 mg/kg wet 1.666 67 36-123 3,3'-Dichlorobenzidine 1.37 0.33 mg/kg wet 1.666 82 22-121 3/4-Methyl phenol 1.22 0.33 mg/kg wet 1.666 73 34-119 4,6-Dinitro-2-methylphenol 1.25 0.33 mg/kg wet 1.666 75 29-132 4-Bromophenyl phenyl ether 1.45 0.33 mg/kg wet 1.666 87 46-124 4-Chloro-3-methylphenol 1.32 0.33 mg/kg wet 1.666 79 45-122 4-Chloroaniline 1.22 0.33 mg/kg wet 1.666 73 17-106 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 74 of 87 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO314 - 3546 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P6H0314-BSI) Prepared & Analyzed: 08/18/16 4-Chlorophenyl phenyl ether 1.43 0.33 mg/kg wet 1.666 86 45-121 4-Nitrophenol 1.47 0.33 mg/kg wet 1.666 88 30-132 Acenaphthene 1.36 0.33 mg/kg wet 1.666 82 40-123 Acenaphthylene 1.38 0.33 mg/kg wet 1.666 83 32-132 Anthracene 1.58 0.33 mg/kg wet 1.666 95 47-123 Azobenzene 1.41 0.33 mg/kg wet 1.666 84 39-125 Benzo(a)anthracene 1.54 0.33 mg/kg wet 1.666 92 49-126 Benzo(a)pyrene 1.48 0.33 mg/kg wet 1.666 89 45-129 Benzo(b)fluoranthene 1.43 0.33 mg/kg wet 1.666 86 45-132 Benzo(g,h,i)perylene 1.41 0.33 mg/kg wet 1.666 84 43-134 Benzo(k)fluoranthene 1.44 0.33 mg/kg wet 1.666 86 47-132 Benzoic Acid 0.905 0.33 mg/kg wet 1.666 54 10-83 Benzyl alcohol 1.11 0.33 mg/kg wet 1.666 67 29-122 bis(2-Chloroethoxy)methane 1.18 0.33 mg/kg wet 1.666 71 36-121 Bis(2-Chloroethyl)ether 1.05 0.33 mg/kg wet 1.666 63 31-120 Bis(2-chloroisopropyl)ether 1.14 0.33 mg/kg wet 1.666 68 33-131 Bis(2-Ethylhexyl)phthalate 1.49 0.33 mg/kg wet 1.666 89 51-133 Butyl benzyl phthalate 1.50 0.33 mg/kg wet 1.666 90 48-132 Chrysene 1.58 0.33 mg/kg wet 1.666 95 50-124 Dibenzo(a,h)anthracene 1.41 0.33 mg/kg wet 1.666 85 45-134 Dibenzofuran 1.39 0.33 mg/kg wet 1.666 83 44-120 Diethyl phthalate 1.44 0.33 mg/kg wet 1.666 86 50-124 Dimethyl phthalate 1.36 0.33 mg/kg wet 1.666 82 48-124 Di-n-butyl phthalate 1.55 0.33 mg/kg wet 1.666 93 51-128 Di-n-octyl phthalate 1.39 0.33 mg/kg wet 1.666 84 45-140 Fluoranthene 1.52 0.33 mg/kg wet 1.666 91 50-127 Fluorene 1.49 0.33 mg/kg wet 1.666 90 43-125 Hexachlorobenzene 1.38 0.33 mg/kg wet 1.666 83 45-122 Hexachlorobutadiene 1.03 0.33 mg/kg wet 1.666 62 32-123 Hexachlorocyclopentadiene 1.03 0.33 mg/kg wet 1.666 62 32-117 Hexachloroethane 0.911 0.33 mg/kg wet 1.666 55 28-117 Indeno(1,2,3-cd)pyrene 1.45 0.33 mg/kg wet 1.666 87 45-133 Isophorone 1.20 0.33 mg/kg wet 1.666 72 30-122 Naphthalene 1.15 0.33 mg/kg wet 1.666 69 35-123 Nitrobenzene 1.11 0.33 mg/kg wet 1.666 67 34-122 N-Nitroso-di-n-propylamine 1.14 0.33 mg/kg wet 1.666 68 36-120 N-Nitrosodiphenylamine 1.45 0.33 mg/kg wet 1.666 87 38-127 Pentachlorophenol 1.39 0.33 mg/kg wet 1.666 84 25-133 Phenanthrene 1.54 0.33 mg/kg wet 1.666 92 50-121 Phenol 1.18 0.33 mg/kg wet 1.666 71 34-121 Pyrene 1.52 0.33 mg/kg wet 1.666 91 47-127 Surrogate: 2,4,6-Tribromophenol 3.01 mg/kg wet 3.332 90 39-132 Surrogate: 2-Fluorobiphenyl 1.26 mg/kg wet 1.666 76 44-115 Surrogate: 2-Fluorophenol 2.41 mg/kg wet 3.332 72 35-115 Surrogate: Nitrobenzene-d5 1.12 mg/kg wet 1.666 68 37-122 Surrogate: Phenol-d5 2.48 mg/kg wet 3.332 75 34-121 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 75 of 87 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO314 - 3546 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P6H0314-BS1) Prepared & Analyzed: 08/18/16 Surrogate: Terphenyl-d14 1.28 mg/kg wet 1.666 77 54-127 LCS Dup (P6H0314-BSD1) Prepared & Analyzed: 08/18/16 1,2,4-Trichlorobenzene 0.984 0.33 mg/kg wet 1.666 59 34-118 6 20 1,2-Dichlorobenzene 0.867 0.33 mg/kg wet 1.666 52 33-117 9 20 1,3-Dichlorobenzene 0.834 0.33 mg/kg wet 1.666 50 30-115 8 20 1,4-Dichlorobenzene 0.857 0.33 mg/kg wet 1.666 51 31-115 7 20 1-Methyl naphthalene 1.20 0.33 mg/kg wet 1.666 72 40-119 2 20 2,4,6-Trichlorophenol 1.29 0.33 mg/kg wet 1.666 78 39-126 1 20 2,4-Dichlorophenol 1.25 0.33 mg/kg wet 1.666 75 40-122 0.3 20 2,4-Dimethylphenol 1.26 0.33 mg/kg wet 1.666 76 30-127 0.8 20 2,4-Dinitrophenol 1.10 0.33 mg/kg wet 1.666 66 27-129 7 20 2,4-Dinitrotoluene 1.49 0.33 mg/kg wet 1.666 89 48-126 2 20 2,6-Dinitrotoluene 1.36 0.33 mg/kg wet 1.666 81 46-124 2 20 2-Chloronaphthalene 1.60 0.33 mg/kg wet 1.666 96 41-114 2 20 2-Chlorophenol 1.05 0.33 mg/kg wet 1.666 63 34-121 5 20 2-Methyl naphthalene 1.14 0.33 mg/kg wet 1.666 69 38-122 3 20 2-Methylphenol 1.13 0.33 mg/kg wet 1.666 68 32-122 3 20 2-Nitrophenol 1.06 0.33 mg/kg wet 1.666 64 36-123 5 20 3,3'-Dichlorobenzidine 1.47 0.33 mg/kg wet 1.666 88 22-121 7 20 3/4-Methyl phenol 1.22 0.33 mg/kg wet 1.666 74 34-119 0.4 20 4,6-Dinitro-2-methylphenol 1.33 0.33 mg/kg wet 1.666 80 29-132 6 20 4-Bromophenyl phenyl ether 1.46 0.33 mg/kg wet 1.666 88 46-124 0.5 20 4-Chloro-3-methylphenol 1.35 0.33 mg/kg wet 1.666 81 45-122 2 20 4-Chloroaniline 1.22 0.33 mg/kg wet 1.666 74 17-106 0.02 20 4-Chlorophenyl phenyl ether 1.42 0.33 mg/kg wet 1.666 85 45-121 0.8 20 4-Nitrophenol 1.51 0.33 mg/kg wet 1.666 91 30-132 2 20 Acenaphthene 1.33 0.33 mg/kg wet 1.666 80 40-123 2 20 Acenaphthylene 1.39 0.33 mg/kg wet 1.666 83 32-132 0.6 20 Anthracene 1.61 0.33 mg/kg wet 1.666 96 47-123 1 20 Azobenzene 1.41 0.33 mg/kg wet 1.666 84 39-125 0.08 20 Benzo(a)anthracene 1.60 0.33 mg/kg wet 1.666 96 49-126 4 20 Benzo(a)pyrene 1.51 0.33 mg/kg wet 1.666 91 45-129 2 20 Benzo(b)fluoranthene 1.47 0.33 mg/kg wet 1.666 88 45-132 3 20 Benzo(g,h,i)perylene 1.43 0.33 mg/kg wet 1.666 86 43-134 2 20 Benzo(k)fluoranthene 1.51 0.33 mg/kg wet 1.666 91 47-132 5 20 Benzoic Acid 0.954 0.33 mg/kg wet 1.666 57 10-83 5 20 Benzyl alcohol 1.06 0.33 mg/kg wet 1.666 64 29-122 4 20 bis(2-Chloroethoxy)methane 1.14 0.33 mg/kg wet 1.666 68 36-121 3 20 Bis(2-Chloroethyl)ether 0.959 0.33 mg/kg wet 1.666 58 31-120 9 20 Bis(2-chloroisopropyl)ether 1.07 0.33 mg/kg wet 1.666 64 33-131 6 20 Bis(2-Ethylhexyl)phthalate 1.56 0.33 mg/kg wet 1.666 94 51-133 5 20 Butyl benzyl phthalate 1.55 0.33 mg/kg wet 1.666 93 48-132 4 20 Chrysene 1.65 0.33 mg/kg wet 1.666 99 50-124 4 20 Dibenzo(a,h)anthracene 1.45 0.33 mg/kg wet 1.666 87 45-134 3 20 Dibenzofuran 1.37 0.33 mg/kg wet 1.666 82 44-120 1 20 Diethyl phthalate 1.48 0.33 mg/kg wet 1.666 89 50-124 3 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 76 of 87 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO314 - 3546 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P6H0314-BSD1) Prepared & Analyzed: 08/18/16 Dimethyl phthalate 1.38 0.33 mg/kg wet 1.666 83 48-124 2 20 Di-n-butyl phthalate 1.59 0.33 mg/kg wet 1.666 95 51-128 2 20 Di-n-octyl phthalate 1.42 0.33 mg/kg wet 1.666 85 45-140 2 20 Fluoranthene 1.55 0.33 mg/kg wet 1.666 93 50-127 2 20 Fluorene 1.49 0.33 mg/kg wet 1.666 89 43-125 0.3 20 Hexachlorobenzene 1.42 0.33 mg/kg wet 1.666 85 45-122 3 20 Hexachlorobutadiene 0.951 0.33 mg/kg wet 1.666 57 32-123 8 20 Hexachlorocyclopentadiene 0.936 0.33 mg/kg wet 1.666 56 32-117 9 20 Hexachloroethane 0.854 0.33 mg/kg wet 1.666 51 28-117 6 20 Indeno(1,2,3-cd)pyrene 1.49 0.33 mg/kg wet 1.666 89 45-133 3 20 Isophorone 1.19 0.33 mg/kg wet 1.666 71 30-122 0.6 20 Naphthalene 1.11 0.33 mg/kg wet 1.666 67 35-123 3 20 Nitrobenzene 1.04 0.33 mg/kg wet 1.666 63 34-122 6 20 N-Nitroso-di-n-propylamine 1.13 0.33 mg/kg wet 1.666 68 36-120 1 20 N-Nitrosodiphenylamine 1.47 0.33 mg/kg wet 1.666 88 38-127 1 20 Pentachlorophenol 1.44 0.33 mg/kg wet 1.666 86 25-133 3 20 Phenanthrene 1.60 0.33 mg/kg wet 1.666 96 50-121 4 20 Phenol 1.16 0.33 mg/kg wet 1.666 69 34-121 2 20 Pyrene 1.56 0.33 mg/kg wet 1.666 94 47-127 3 20 Surrogate: 2,4,6-Tribromophenol 3.03 mg/kg wet 3.331 91 39-132 Surrogate: 2-Fluorobiphenyl 1.23 mg/kg wet 1.666 74 44-115 Surrogate: 2-Fluorophenol 2.28 mg/kg wet 3.331 68 35-115 Surrogate: Nitrobenzene-d5 1.07 mg/kg wet 1.666 64 37-122 Surrogate: Phenol-d5 2.39 mg/kg wet 3.331 72 34-121 Surrogate: Terphenyl-d14 1.30 mg/kg wet 1.666 78 54-127 Matrix Spike (P6H0314-MS1) Source: 6080270-03 Prepared & Analyzed: 08/18/16 1,2,4-Trichlorobenzene 0.935 0.36 mg/kg dry 1.825 BRL 51 34-118 1,2-Dichlorobenzene 0.831 0.36 mg/kg dry 1.825 BRL 46 33-117 1,3-Dichlorobenzene 0.789 0.36 mg/kg dry 1.825 BRL 43 30-115 1,4-Dichlorobenzene 0.813 0.36 mg/kg dry 1.825 BRL 45 31-115 1-Methyl naphthalene 1.08 0.36 mg/kg dry 1.825 BRL 59 40-119 2,4,6-Trichlorophenol 1.12 0.36 mg/kg dry 1.825 BRL 61 39-126 2,4-Dichlorophenol 1.12 0.36 mg/kg dry 1.825 BRL 61 40-122 2,4-Dimethyl phenol 1.10 0.36 mg/kg dry 1.825 BRL 60 30-127 2,4-Dinitrophenol 0.734 0.36 mg/kg dry 1.825 BRL 40 27-129 2,4-Dinitrotoluene 1.22 0.36 mg/kg dry 1.825 BRL 67 48-126 2,6-Dinitrotoluene 1.14 0.36 mg/kg dry 1.825 BRL 63 46-124 2-Chloronaphthalene 1.24 0.36 mg/kg dry 1.825 BRL 68 41-114 2-Chlorophenol 0.978 0.36 mg/kg dry 1.825 BRL 54 34-121 2-Methyl naphthalene 1.05 0.36 mg/kg dry 1.825 BRL 57 38-122 2-Methylphenol 1.00 0.36 mg/kg dry 1.825 BRL 55 32-122 2-Nitrophenol 0.982 0.36 mg/kg dry 1.825 BRL 54 36-123 3,3'-Dichlorobenzidine 1.19 0.36 mg/kg dry 1.825 BRL 65 22-121 3/4-Methyl phenol 1.08 0.36 mg/kg dry 1.825 BRL 59 34-119 4,6-Dinitro-2-methylphenol 1.02 0.36 mg/kg dry 1.825 BRL 56 29-132 4-Bromophenyl phenyl ether 1.21 0.36 mg/kg dry 1.825 BRL 66 46-124 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 77 of 87 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO314 - 3546 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike (1261-10314-MS1) Source: 6080270-03 Prepared & Analyzed: 08/18/16 4-Chloro-3-methyl phenol 1.16 0.36 mg/kg dry 1.825 BRL 63 45-122 4-Chloroaniline 1.05 0.36 mg/kg dry 1.825 BRL 58 17-106 4-Chlorophenyl phenyl ether 1.22 0.36 mg/kg dry 1.825 BRL 67 45-121 4-Nitrophenol 1.46 0.36 mg/kg dry 1.825 BRL 80 30-132 Acenaphthene 1.18 0.36 mg/kg dry 1.825 BRL 64 40-123 Acenaphthylene 1.20 0.36 mg/kg dry 1.825 BRL 66 32-132 Anthracene 1.35 0.36 mg/kg dry 1.825 BRL 74 47-123 Azobenzene 1.20 0.36 mg/kg dry 1.825 BRL 66 39-125 Benzo(a)anthracene 1.36 0.36 mg/kg dry 1.825 BRL 74 49-126 Benzo(a)pyrene 1.25 0.36 mg/kg dry 1.825 BRL 69 45-129 Benzo(b)fluoranthene 1.19 0.36 mg/kg dry 1.825 BRL 65 45-132 Benzo(g,h,i)perylene 1.17 0.36 mg/kg dry 1.825 BRL 64 43-134 Benzo(k)fluoranthene 1.27 0.36 mg/kg dry 1.825 BRL 69 47-132 Benzoic Acid 0.246 0.36 mg/kg dry 1.825 BRL 14 10-83 Benzyl alcohol 0.923 0.36 mg/kg dry 1.825 BRL 51 29-122 bis(2-Chloroethoxy)methane 1.04 0.36 mg/kg dry 1.825 BRL 57 36-121 Bis(2-Chloroethyl)ether 0.927 0.36 mg/kg dry 1.825 BRL 51 31-120 Bis(2-chloroisopropyl)ether 1.02 0.36 mg/kg dry 1.825 BRL 56 33-131 Bis(2-Ethylhexyl)phthalate 1.34 0.36 mg/kg dry 1.825 BRL 73 51-133 Butyl benzyl phthalate 1.36 0.36 mg/kg dry 1.825 BRL 75 48-132 Chrysene 1.38 0.36 mg/kg dry 1.825 BRL 75 50-124 Dibenzo(a,h)anthracene 1.18 0.36 mg/kg dry 1.825 BRL 65 45-134 Dibenzofuran 1.22 0.36 mg/kg dry 1.825 BRL 67 44-120 Diethyl phthalate 1.26 0.36 mg/kg dry 1.825 BRL 69 50-124 Dimethyl phthalate 1.17 0.36 mg/kg dry 1.825 BRL 64 48-124 Di-n-butyl phthalate 1.36 0.36 mg/kg dry 1.825 BRL 74 51-128 Di-n-octyl phthalate 1.19 0.36 mg/kg dry 1.825 BRL 65 45-140 Fluoranthene 1.30 0.36 mg/kg dry 1.825 BRL 71 50-127 Fluorene 1.27 0.36 mg/kg dry 1.825 BRL 70 43-125 Hexachlorobenzene 1.19 0.36 mg/kg dry 1.825 BRL 65 45-122 Hexachlorobutadiene 0.913 0.36 mg/kg dry 1.825 BRL 50 32-123 Hexachlorocyclopentadiene 0.857 0.36 mg/kg dry 1.825 BRL 47 32-117 Hexachloroethane 0.816 0.36 mg/kg dry 1.825 BRL 45 28-117 Indeno(1,2,3-cd)pyrene 1.22 0.36 mg/kg dry 1.825 BRL 67 45-133 Isophorone 1.05 0.36 mg/kg dry 1.825 BRL 57 30-122 Naphthalene 1.03 0.36 mg/kg dry 1.825 BRL 56 35-123 Nitrobenzene 0.977 0.36 mg/kg dry 1.825 BRL 54 34-122 N-Nitroso-di-n-propylamine 1.02 0.36 mg/kg dry 1.825 BRL 56 36-120 N-Nitrosodiphenylamine 1.24 0.36 mg/kg dry 1.825 BRL 68 38-127 Pentachlorophenol 1.14 0.36 mg/kg dry 1.825 BRL 62 25-133 Phenanthrene 1.35 0.36 mg/kg dry 1.825 BRL 74 50-121 Phenol 1.03 0.36 mg/kg dry 1.825 BRL 57 34-121 Pyrene 1.36 0.36 mg/kg dry 1.825 BRL 74 47-127 Surrogate: 2,4,6-Tribromophenol 2.48 mg/kg dry 3.649 68 39-132 Surrogate: 2-Fluorobiphenyl 1.08 mg/kg dry 1.825 59 44-115 Surrogate: 2-Fluorophenol 2.08 mg/kg dry 3.649 57 35-115 J This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 78 of 87 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P6HO314 - 3546 Reporting Result Limit Units Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike (P6H0314-MS1) Source: 6080270-03 Prepared & Analyzed: 08/18/16 Surrogate: Nitrobenzene-,:15 0.984 mg/kg dry 1.825 54 37-122 Surrogate: Phenol-d5 2.15 mg/kg dry 3.649 59 34-121 Surrogate: Terphenyl-d14 1.11 mg/kg dry 1.825 61 54-127 Matrix Spike Dup (P6H0314-MSD1) Source: 6080270-03 Prepared & Analyzed: 08/18/16 1,2,4-Trichlorobenzene 1.07 0.36 mg/kg dry 1.822 BRL 59 34-118 14 20 1,2-Dichlorobenzene 0.931 0.36 mg/kg dry 1.822 BRL 51 33-117 11 20 1,3-Dichlorobenzene 0.850 0.36 mg/kg dry 1.822 BRL 47 30-115 7 20 1,4-Dichlorobenzene 0.906 0.36 mg/kg dry 1.822 BRL 50 31-115 11 20 1-Methyl naphthalene 1.22 0.36 mg/kg dry 1.822 BRL 67 40-119 12 20 2,4,6-Trichlorophenol 1.21 0.36 mg/kg dry 1.822 BRL 66 39-126 8 20 2,4-Dichlorophenol 1.27 0.36 mg/kg dry 1.822 BRL 69 40-122 13 20 2,4-Dimethylphenol 1.23 0.36 mg/kg dry 1.822 BRL 67 30-127 11 20 2,4-Dinitrophenol 0.592 0.36 mg/kg dry 1.822 BRL 33 27-129 21 20 D 2,4-Dinitrotoluene 1.40 0.36 mg/kg dry 1.822 BRL 77 48-126 14 20 2,6-Dinitrotoluene 1.23 0.36 mg/kg dry 1.822 BRL 68 46-124 8 20 2-Chloronaphthalene 1.63 0.36 mg/kg dry 1.822 BRL 90 41-114 27 20 D 2-Chlorophenol 1.17 0.36 mg/kg dry 1.822 BRL 64 34-121 18 20 2-Methyl naphthalene 1.19 0.36 mg/kg dry 1.822 BRL 65 38-122 12 20 2-Methylphenol 1.19 0.36 mg/kg dry 1.822 BRL 65 32-122 17 20 2-Nitrophenol 1.17 0.36 mg/kg dry 1.822 BRL 64 36-123 18 20 3,3'-Dichlorobenzidine 1.38 0.36 mg/kg dry 1.822 BRL 76 22-121 15 20 3/4-Methyl phenol 1.26 0.36 mg/kg dry 1.822 BRL 69 34-119 15 20 4,6-Dinitro-2-methylphenol 1.16 0.36 mg/kg dry 1.822 BRL 64 29-132 14 20 4-Bromophenyl phenyl ether 1.37 0.36 mg/kg dry 1.822 BRL 75 46-124 13 20 4-Chloro-3-methylphenol 1.28 0.36 mg/kg dry 1.822 BRL 70 45-122 10 20 4-Chloroaniline 1.24 0.36 mg/kg dry 1.822 BRL 68 17-106 16 20 4-Chlorophenyl phenyl ether 1.29 0.36 mg/kg dry 1.822 BRL 71 45-121 5 20 4-Nitrophenol 1.48 0.36 mg/kg dry 1.822 BRL 81 30-132 2 20 Acenaphthene 1.29 0.36 mg/kg dry 1.822 BRL 71 40-123 9 20 Acenaphthylene 1.31 0.36 mg/kg dry 1.822 BRL 72 32-132 9 20 Anthracene 1.55 0.36 mg/kg dry 1.822 BRL 85 47-123 13 20 Azobenzene 1.32 0.36 mg/kg dry 1.822 BRL 73 39-125 9 20 Benzo(a)anthracene 1.62 0.36 mg/kg dry 1.822 BRL 89 49-126 18 20 Benzo(a)pyrene 1.54 0.36 mg/kg dry 1.822 BRL 85 45-129 21 20 D Benzo(b)fluoranthene 1.48 0.36 mg/kg dry 1.822 BRL 81 45-132 21 20 D Benzo(g,h,i)perylene 1.45 0.36 mg/kg dry 1.822 BRL 79 43-134 21 20 D Benzo(k)fluoranthene 1.47 0.36 mg/kg dry 1.822 BRL 81 47-132 15 20 Benzoic Acid BRL 0.36 mg/kg dry 1.822 BRL 10-83 20 M Benzyl alcohol 1.13 0.36 mg/kg dry 1.822 BRL 62 29-122 20 20 bis(2-Chloroethoxy)methane 1.24 0.36 mg/kg dry 1.822 BRL 68 36-121 18 20 Bis(2-Chloroethyl)ether 1.14 0.36 mg/kg dry 1.822 BRL 62 31-120 20 20 Bis(2-chloroisopropyl)ether 1.18 0.36 mg/kg dry 1.822 BRL 65 33-131 15 20 Bis(2-Ethylhexyl)phthalate 1.57 0.36 mg/kg dry 1.822 BRL 86 51-133 16 20 Butyl benzyl phthalate 1.61 0.36 mg/kg dry 1.822 BRL 88 48-132 17 20 Chrysene 1.69 0.36 mg/kg dry 1.822 BRL 93 50-124 20 20 Dibenzo(a,h)anthracene 1.45 0.36 mg/kg dry 1.822 BRL 79 45-134 20 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 79 of 87 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Prism Work Order: 6080270 Attn: Brian Olin Time Submitted: 8/15/2016 11:51:OOAM 1812 Center Park Drive, Suite D Charlotte, NC 28217 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6HO314 - 3546 Matrix Spike Dup (P6H0314-MSD1) Source: 6080270-03 Prepared & Analyzed: 08/18/16 Dibenzofuran 1.28 0.36 mg/kg dry 1.822 BRL 70 44-120 5 20 Diethyl phthalate 1.39 0.36 mg/kg dry 1.822 BRL 76 50-124 10 20 Dimethyl phthalate 1.30 0.36 mg/kg dry 1.822 BRL 71 48-124 10 20 Di-n-butyl phthalate 1.59 0.36 mg/kg dry 1.822 BRL 88 51-128 16 20 Di-n-octyl phthalate 1.44 0.36 mg/kg dry 1.822 BRL 79 45-140 19 20 Fluoranthene 1.53 0.36 mg/kg dry 1.822 BRL 84 50-127 16 20 Fluorene 1.37 0.36 mg/kg dry 1.822 BRL 75 43-125 7 20 Hexachlorobenzene 1.36 0.36 mg/kg dry 1.822 BRL 75 45-122 13 20 Hexachlorobutadiene 1.01 0.36 mg/kg dry 1.822 BRL 56 32-123 11 20 Hexachlorocyclopentadiene 1.02 0.36 mg/kg dry 1.822 BRL 56 32-117 17 20 Hexachloroethane 0.875 0.36 mg/kg dry 1.822 BRL 48 28-117 7 20 Indeno(1,2,3-cd)pyrene 1.50 0.36 mg/kg dry 1.822 BRL 82 45-133 21 20 D Isophorone 1.21 0.36 mg/kg dry 1.822 BRL 67 30-122 15 20 Naphthalene 1.18 0.36 mg/kg dry 1.822 BRL 65 35-123 14 20 Nitrobenzene 1.18 0.36 mg/kg dry 1.822 BRL 65 34-122 19 20 N-Nitroso-di-n-propylamine 1.20 0.36 mg/kg dry 1.822 BRL 66 36-120 16 20 N-Nitrosodiphenylamine 1.36 0.36 mg/kg dry 1.822 BRL 75 38-127 10 20 Pentachlorophenol 1.39 0.36 mg/kg dry 1.822 BRL 76 25-133 20 20 Phenanthrene 1.51 0.36 mg/kg dry 1.822 BRL 83 50-121 11 20 Phenol 1.25 0.36 mg/kg dry 1.822 BRL 68 34-121 19 20 Pyrene 1.60 0.36 mg/kg dry 1.822 BRL 88 47-127 16 20 Surrogate: 2,4,6-Tribromophenol 2.70 mg/kg dry 3.643 74 39-132 Surrogate: 2-Fluorobiphenyl 1.19 mg/kg dry 1.822 65 44-115 Surrogate: 2-Fluorophenol 2.51 mg/kg dry 3.643 69 35-115 Surrogate: Nitrobenzene-d5 1.17 mg/kg dry 1.822 64 37-122 Surrogate: Phenol-d5 2.56 mg/kg dry 3.643 70 34-121 Surrogate: Terphenyl-d14 1.29 mg/kg dry 1.822 71 54-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 80 of 87 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Prism Work Order: 6080270 Attn: Brian Olin Time Submitted: 8/15/2016 11:51:OOAM 1812 Center Park Drive, Suite D Charlotte, NC 28217 Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6H0361 - MADEP VPH (S) Blank (P6H0361-BLK1) Prepared & Analyzed: 08/19/16 C5-C8 Aliphatics BRL 5.0 mg/kg wet C9-Cl2 Aliphatics BRL 5.0 mg/kg wet C9-Cl0 Aromatics BRL 5.0 mg/kg wet Surrogate: 2,5-Dibromotoluene (PID) 9.01 mg/kg wet 10.67 85 70-130 Surrogate: 2,5-Dibromotoluene (FID) 11.3 mg/kg wet 10.67 106 70-130 LCS (P6H0361-BSI) Prepared & Analyzed: 08/19/16 C5-C8 Aliphatics 33.7 5.0 mg/kg wet 32.00 105 70-130 C9-Cl0 Aromatics 8.46 5.0 mg/kg wet 10.67 79 70-130 C9-Cl2 Aliphatic 30.7 5.0 mg/kg wet 32.00 96 70-130 Surrogate: 2,5-Dibromotoluene (PID) 9.16 mg/kg wet 10.67 86 70-130 Surrogate: 2,5-Dibromotoluene (FID) 11.3 mg/kg wet 10.67 106 70-130 LCS Dup (P6H0361-BSD1) Prepared & Analyzed: 08/19/16 C5-C8 Aliphatics 33.2 5.0 mg/kg wet 32.00 104 70-130 2 50 C9-Cl0 Aromatics 8.62 5.0 mg/kg wet 10.67 81 70-130 2 50 C9-Cl2 Aliphatic 30.8 5.0 mg/kg wet 32.00 96 70-130 0.4 50 Surrogate: 2,5-Dibromotoluene (PID) 8.58 mg/kg wet 10.67 80 70-130 Surrogate: 2,5-Dibromotoluene (FID) 10.6 mg/kg wet 10.67 99 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 81 of 87 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 Extractable Petroleum Hydrocarbons by GC/FID - Quality Control Reporting Analyte Result Limit Units Batch P6H0227 - 3546 Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P6H0227-BLK1) Prepared & Analyzed: 08/15/16 C9-Cl8 Aliphatics 1.22 25 mg/kg wet C19-C36 Aliphatics BRL 25 mg/kg wet C11-C22 Aromatics BRL 10 mg/kg wet Surrogate: 1-Chlorooctadecane 1.64 mg/kg wet 2.000 82 40-140 Surrogate: o-Terphenyl 1.56 mg/kg wet 2.000 78 40-140 Surrogate: 2-Fluorobiphenyl 3.34 mg/kg wet 4.000 84 40-140 Surrogate: 2-Bromonaphthalene 3.84 mg/kg wet 4.000 96 40-140 LCS (PM0227-13SI) Prepared & Analyzed: 08/15/16 C9-Cl8 Aliphatics 37.4 25 mg/kg wet 60.00 62 40-140 C19-C36 Aliphatics 65.6 25 mg/kg wet 80.00 82 40-140 C11-C22 Aromatics 145 10 mg/kg wet 170.0 85 40-140 Surrogate: 1-Chlorooctadecane 1.80 mg/kg wet 2.000 90 40-140 Surrogate: o-Terphenyl 1.77 mg/kg wet 2.000 89 40-140 Surrogate: 2-Fluorobiphenyl 3.56 mg/kg wet 4.000 89 40-140 Surrogate: 2-Bromonaphthalene 3.82 mg/kg wet 4.000 95 40-140 LCS Dup (P611-110227-13SD1) Prepared & Analyzed: 08/15/16 C9-Cl8 Aliphatics 32.7 25 mg/kg wet 60.00 54 40-140 C19-C36 Aliphatics 61.6 25 mg/kg wet 80.00 77 40-140 C11-C22 Aromatics 140 10 mg/kg wet 170.0 82 40-140 Surrogate: 1-Chlorooctadecane 1.64 mg/kg wet 2.000 82 40-140 Surrogate: o-Terphenyl 1.67 mg/kg wet 2.000 84 40-140 Surrogate: 2-Fluorobiphenyl 3.53 mg/kg wet 4.000 88 40-140 Surrogate: 2-Bromonaphthalene 3.81 mg/kg wet 4.000 95 40-140 13 50 6 50 3 50 J This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 82 of 87 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 8/22/16 ECS Carolinas, LLP (Charlotte) Project: Swans Run Attn: Brian Olin 1812 Center Park Drive, Suite D Charlotte, NC 28217 General Chemistry Parameters - Quality Control Prism Work Order: 6080270 Time Submitted: 8/15/2016 11:51:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6H0334 - Solids, Dry Weight Duplicate (P6H0334-DUP2) Source: 6080270-03 Prepared: 08/17/16 Analyzed: 08/18/16 % Solids 92.0 0.100 % by Weight 91.3 0.7 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 83 of 87 Sample Extraction Data Prep Method: 3546 Lab Number Batch Initial Final Date/Time 6080270-01 P61-10227 10.06 g 2 mL 08/16/16 8:00 6080270-02 P61-10227 10.02 g 2 mL 08/16/16 8:00 6080270-03 P61-10227 10.05 g 2 mL 08/16/16 8:00 6080270-04 P61-10227 10.02 g 2 mL 08/16/16 8:00 6080270-05 P61-10227 10.01 g 2 mL 08/16/16 8:00 6080270-06 P61-10227 10.02 g 2 mL 08/16/16 8:00 6080270-07 P61-10227 10.05 g 2 mL 08/16/16 8:00 6080270-08 P61-10227 10.01 g 2 mL 08/16/16 8:00 6080270-09 P61-10227 10.12 g 2 mL 08/16/16 8:00 6080270-10 P61-10227 10 g 2 mL 08/16/16 8:00 6080270-11 P61-10227 10 g 2 mL 08/16/16 8:00 6080270-12 P61-10227 10.07 g 2 mL 08/16/16 8:00 6080270-13 P61-10227 10.07 g 2 mL 08/16/16 8:00 6080270-14 P61-10227 10.11 g 2 mL 08/16/16 8:00 6080270-15 P61-10227 10.06 g 2 mL 08/16/16 8:00 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final DatelTime 6080270-01 P61-10334 30 g 30 g 08/18/16 14:39 6080270-02 P61-10334 30 g 30 g 08/18/16 14:39 6080270-03 P61-10334 30 g 30 g 08/18/16 14:39 6080270-04 P61-10334 30 g 30 g 08/18/16 14:39 6080270-05 P61-10334 30 g 30 g 08/18/16 14:39 6080270-06 P61-10334 30 g 30 g 08/18/16 14:39 6080270-07 P61-10334 30 g 30 g 08/18/16 14:39 6080270-08 P61-10334 30 g 30 g 08/17/16 14:39 6080270-09 P61-10334 30 g 30 g 08/17/16 14:39 6080270-10 P61-10334 30 g 30 g 08/17/16 14:39 6080270-11 P61-10334 30 g 30 g 08/17/16 14:39 6080270-12 P61-10334 30 g 30 g 08/17/16 14:39 6080270-13 P61-10334 30 g 30 g 08/17/16 14:39 6080270-14 P61-10334 30 g 30 g 08/17/16 14:39 6080270-15 P61-10334 30 g 30 g 08/17/16 14:39 Prep Method: 3546 Lab Number Batch Initial Final Date/Time 6080270-01 P61-10314 30.03 g 1 mL 08/18/16 8:58 6080270-02 P61-10314 30.04 g 2 mL 08/18/16 8:58 6080270-03 P61-10314 30.05 g 1 mL 08/18/16 8:58 6080270-04 P61-10314 30.42 g 1 mL 08/18/16 8:58 6080270-05 P61-10314 30.11 g 1 mL 08/18/16 8:58 6080270-06 P61-10314 30.03 g 1 mL 08/18/16 8:58 6080270-07 P61-10314 30.33 g 1 mL 08/18/16 8:58 6080270-08 P61-10314 30.09 g 1 mL 08/18/16 8:58 6080270-09 P61-10314 30.09 g 1 mL 08/18/16 8:58 6080270-10 P61-10314 30.23 g 2 mL 08/18/16 8:58 6080270-11 P61-10314 30.38 g 1 mL 08/18/16 8:58 6080270-12 P61-10314 30.17 g 1 mL 08/18/16 8:58 6080270-13 P61-10314 30.35 g 1 mL 08/18/16 8:58 6080270-14 P61-10314 30.45 g 1 mL 08/18/16 8:58 6080270-15 P61-10314 30.26 g 1 mL 08/18/16 8:58 Prep Method: 5035 Lab Number Batch Initial Final Date/Time This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 84 of 87 Sample Extraction Data Prep Method: 5035 Lab Number Batch Initial Final Date/Time 6080270-01 P61-10336 9.3 g 5 mL 08/18/16 16:24 6080270-02 P61-10365 5.5 g 5 mL 08/19/16 14:38 6080270-03 P61-10336 8.41 g 5 mL 08/18/16 16:24 6080270-04 P61-10336 9.78 g 5 mL 08/18/16 16:24 6080270-05 P61-10336 9.82 g 5 mL 08/18/16 16:24 6080270-06 P61-10336 9.53 g 5 mL 08/18/16 16:24 6080270-07 P61-10336 9.67 g 5 mL 08/18/16 16:24 6080270-08 P61-10336 9.09 g 5 mL 08/18/16 16:24 6080270-09 P61-10336 9.15 g 5 mL 08/18/16 16:24 6080270-10 P61-10336 9.66 g 5 mL 08/18/16 16:24 6080270-11 P61-10336 9.19 g 5 mL 08/18/16 16:24 6080270-12 P61-10336 5 g 5 mL 08/18/16 16:24 6080270-13 P61-10336 11.26 g 5 mL 08/18/16 16:24 6080270-14 P61-10336 9.43 g 5 mL 08/18/16 16:24 6080270-15 P61-10336 9.63 g 5 mL 08/18/16 16:24 Prep Method: MADEP VPH (S) Lab Number Batch Initial Final DatelTime 6080270-01 P61-10361 5.53 g 16 mL 08/19/16 13:15 6080270-02 P61-10361 4.4 g 16 mL 08/19/16 13:15 6080270-03 P61-10361 5.21 g 16 mL 08/19/16 13:15 6080270-04 P61-10361 4.71 g 16 mL 08/19/16 13:15 6080270-05 P61-10361 6.03 g 16 mL 08/19/16 13:15 6080270-06 P61-10361 5.74 g 16 mL 08/19/16 13:15 6080270-07 P61-10361 5.48 g 16 mL 08/19/16 13:15 6080270-08 P61-10361 5.42 g 16 mL 08/19/16 13:15 6080270-09 P61-10361 10.6 g 16 mL 08/19/16 13:15 6080270-10 P61-10361 5.8 g 16 mL 08/19/16 13:15 6080270-11 P61-10361 12.73 g 16 mL 08/19/16 13:15 6080270-12 P61-10361 10.13 g 16 mL 08/19/16 13:15 6080270-13 P61-10361 12.62 g 16 mL 08/19/16 13:15 6080270-14 P61-10361 11.41 g 16 mL 08/19/16 13:15 6080270-15 P61-10361 13.2 g 16 mL 08/19/16 13:15 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 85 of 87 1-0-Service Analytical & P R I S MI Er',,vironmental S6ut3ons L1,ROPMrORIES, INC 449 Sprinabrook Road - Charlotte, NC 28217 Phw641529-6364 - Fax: 1041525-0409 Client Company Name: 4- 3' Report To/Contact Name: r, -�, , u/,- I Reporting Add, ss r I CHAIN L, OF CUSTODY RECORD PAGE OF QUOTE # TO ENSURE PROPER BILLING: Project Name: y Short Hold Analysis: (Yes) No 1 UST Project: (Yes) _JNO) Phone- -D1 77_1111 -,7_ ) .4, ,19ax (Yes) (09). Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email Address: Requested Due Date El 1 Day Ll 2 Days Q 3 Days D 4 Days 5 Days Certification: NELAC DoD_ FL_ NC EDD Type: PDFExcel Other "Working Days" 0 6-9 Days LI Standard 10 days L] Rush Work Must Be Pre -Approved SC OTHER N/A /' Site Location Name: ) L,!, �L4 samples received after 14:00 will be processed next business day. Site Locati hysical ddress: 1�4 Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Water Chlorinated: YES NO 4 10; Y � 4,1" RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES NO_ TIME MATRIX SAM �L"ONTNI�R ANALYSIS REQUESTED PRISM CLIENT DATE COLLECTED COLLECTED MILITARY (SOIL, WATER OR PRESERVA- TIVE S REMARKS LAB *TYPE SAMPLE DESCRIPTION NO. SIZE ID NO. HOURS SLUDGE) SEE BELOW 'IX % 7, 4- -1 7 0, "i 4 a 6 Sampler's Signature Sampled By (Print Name)Affiliation Upon reflinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. Received By: (Signature) Date Military/Hours Relinquished By: Additional Comments: Site Arrival Time: Relinquished By: (Signature) Received By: (Signature) Date Site Departure Time: ---I Relinquished By: (Signature) Re ad For Trism Laboratories By: Da Field Tech Fee: `__ q- // — " tt�� , -/ / 11 ­1 Mileage: I f 15 Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH r oDY SEALS FOR TRANSPORTATION TO THE LABORATORY.-oup No. Coq 4pSAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST IL RECEIVED AT THE LABORATORY. -7 6 0 Fed Ex 0 UPS L3 Hand -delivered ® Prism Field Service 0 Other NPIDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CIE-RCLA LANDFILL OTHER: El NC El C E] SC SC 0 NC E3 SIC 0 NC El S El Ni E3 NC E3C LNC L3SC EJ NC Q SC U NC 0 SC � � � D D D D U *CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) CHAIN OF CUSTODY RECORD Puffl-Servica, Analytical & "'PRISMI uflons PAGE OF Environmenta� Sol, QUOTE 9 TO ENSURE PROPER BILLING! LASOHAMAIESC. Project Name: /Y ng 449 Spnbrook Road Chadotte, NC 28217 Phon,e70411529-6364 Fax: 7041525-0409 Short Hold Analysis: (Yes) ((bNeo), _ie, LIST Project: 'Yes),,) (NO) f L re Client Company Name: *Please ATTACH any project sp ific reporting (QC LEVEL III IV) provisions and/or QC Requirements Report To/Contact Narne: 1 7 a c), Invoice To: n Reporting, I dress :4 114 1 ('t"L-LLt Address: Z7 Phone: Fax (Yes) No: ) , Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email Address: Requested Due Date LJ 1 Day 0 2 Days J 3 Days U 4 Days Q 5 Days Certification: NELAC DoD_ FL_ NC EDD Type: PDF V' Excel Jk Other "Working Days" L3 6-9 Days U Standard 10 days Ej Rush Work Must Be Pre -Approved SC OTHER N/A Site Location Name: "!v �P Samples received after 14:00 will be processed next business day. NO Site0 ation Physical Address: 4 Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TIME TIME MATRIX SAMPLE CONTAINER PRI ESERVA ANALYSIS REQ STED PRISM CLIENT DATE D COLLECTED (SOIL, TIVES REMARKS R LAB *TYPE SAMPLE DESCRIPTION COLLECTED 7EE, MILITARY AR MILITARY Y WATER OR NO. SIZE ID NO. )URS HOURS SLUDGE) SEE BELOW 7 x "A Z 7 'N X(off i >1 47 V A Li �, q Sampler's Signature Sampled By (Print Name ,h Affiliation Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. — Relinquished By: (Signature) Received By: (Signature) Date o Military/Hours Additional Comments: Site Arrival Tirrie: Relinquished By: (Signature) Received By: (Signature) Date Site Departure Tlrne� art _h' 7 Relinquished By: (Signature) Rec6lved For rism Laboratories By: Date 4),, Fleld7'rech Fee: M, Mileage: Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITHOUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CgeUNTIL RECEIVED AT THE LABORATORY. -u LJ Fed Ex 0 UPS U Hand -delivered El Prism Field Service J Other NPDES: UMC GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: 0 NC 0 SC D NC ®SC ®NC D S I Ll SC � � ®NC LINCLISC� ®NC ®SC LIM ®NC LI SC F1 F1 [711 D D D D D 11 *CONTAINER TYPE CODES: A=Amber C=Clear G=Glass P=Plastic; TL = Teflon -Lined Cap VOA =Volatile Organics Analysis (Zero Head Space) Appendix D Photographic Log d-- E Photo 1: View of UST 1 (background) and UST 2 (foreground). Photo 2: View of UST 3. PHOTOGRAPH LOG SWANS RUN UST CLOSURE 7501, 7505, 7515, 7513, AND 7417 SWANS RUN ROAD CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA ECS PROJECT NO. 49-2115-A A Photo 3: View of the bottom of the UST 2 excavation post removal. Photo 4: View of the UST 1 excavation. PHOTOGRAPH LOG SWANS RUN UST CLOSURE 7501, 7505, 7515, 7513, AND 7417 SWANS RUN ROAD CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA ECS PROJECT NO. 49-2115-A Appendix E Soil Disposal Manifests Environmental Soils Inc. o PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # Date Load Number (numbered sequentially as trucks are dispatched) ENVIRONMENTAL CONSULTANT Contact: Phone: Fax: Address: County: Contact: Phone: -4STE ORIGINATIONPOINT Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTAMINATION.• (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS.In Zieu of submitting analytical data (methods 8240 and 8270) verfying that the waste in question sloes not contain organic constituents other than those which would norrn,ally appear in analysis of virgin ASetroleum�roduct residue, I rim submitting this Certificate of Waste Constituents. I certify thatl am familiar with the source of contamination of the soil and further certify the source, to the best of nay knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER. Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: VOLUME: TRUCK DRIVER SIGNATURE: DATE: DESTIN-ATION Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature: Date: Signature: Company Name Date: Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # Date Load Number (numbered sequentially as trucks are dispatched) ENIVIRONMENT 2L CONSULTANT Contact: Phone: Fax: GENER,4TOR. Address: County: Contact: Phone: W14STE ORIGEV14TIONPOINT.• Complete Address: Class &Type of Contaminate in soil SOURCE OF CONTIMEVATION..(ex. UST or other source) GENER,4TORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu ofsubmitting analytical data (methods 8240 and 5270) ver ing that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleumproduct residue, I iam submitting this Cert f cate o� f Waste Constituents. I certify that I am familiar with the source o, f contamination of the soil and farther cert f the source, to the best o, f my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: VOLUME: f TRUCK DRIVER SIGNATURE: DATE: DESTIM4TION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature: Signature: Company Name Date: Title: Datc: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator Environmental Soils Inc. PO Box 295 . Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # Date Load Number (numbered sequentially as trucks are dispatched) ENVIRONMENTAL CONS ULTAN7: Contact: Phone: Fax: GENERATOR: Address: County - Contact: Phone: W-4STE ORIGBVAYIONPOEVT: Complete Address: Class &.Type of Contaminate in soil SOURCE OF CDNTAMIN.4TION.• (ex. UST or other source) GENERATORS CERTIFICATION OF WWSTE CONSTITUENTS: In Zieu of submitting analytical data (methods 8240 and 5270) verifying that the waste in question does not contain organic constituents other than those which would normally a'p-bear in analysis o, f'virginpetroleumproduct residue, Cana submitting this Certificate of Waste Constituents. Icertify that I ain familiar with the source o, f'contamination of the soil and further certtry the source, to the best of nay knowledge, contains no contaminants other than that listed above. Generators Signature: Date: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TRUCK DRIVER SIGNATURE: TAG #: VOLUME: DATE: DESTINATION..: Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature: Signature: Company Name Date: Title: Date: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator Environmental Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075 - Fax 704-434-9533 Non -Hazardous Waste Manifest # 43942 Date Load Number (numbered sequentially as trucks are dispatched) ENHRONMEIML CONSULTANT- of T Contact: `3 Phone. v. Fax: GEAER,4T0R_- Address: . ".5, County - Contact: Phone: WASTE ORIGTVATIONPOEff.- Complete Address: Class &Type of Contaminate in soil SOURCE OFCONT4MIX4TION- (ex. UST or other source) GEAER-4TORS CERTIFICJTION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods 8240 and 8270) veribying that the in question does not contain organic constituents other than those which would normally ap pear in analysis of virgin petroleum Product residue, I am submitting this Certocate of Waste Constituents. IcertihY that IaInfamiliar with the source of contamination of the soil and further certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TR"SPORTEX- Contact: Phone: As ' the carrier, I certify that the Materials described above being shipped under this non -hazardous materials Manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerc, under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: VOLUME: TRUCK DRIVER SIGNATURE:. DATE: DEST17VATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, d anI hereby accept this material for treatment ga-d/-ox-disposal-irt-a-=manne—r-fh"-allFas--Fe-e--n-authoriz Carolina. edbytheState of North Caro Facility Signature: Signature: Company Name Date: Title: Date: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 #.' Non -Hazardous Waste Manifest #48935 Date Load Number (numbered sequentially as trucks are dispatched) � r ENVIRONMENTAL CONSULTANT -- Contact: Phone - t Fax: GENERATOR Address: 4 44County: Contact: fr;. Phone: WASTE ORIGIIVATIONPOINT.• Complete Address Class &Type of Contaminate in soil t . SOURCE OF CONTAMVV,4TION: (ex. UST or other source) GENERdTORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu ofsubmitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally a,ppear in analysis of vir,ginpetroleumproduct residue, Iam submitting this Cert icate of Waste Constituents. I certify that I am familiar with the source of contamination of the soil and further cert� the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRANSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: yTAG #: _ VOLUME: TRUCK DRIVER SIGNATURE: = ' - - DATE: DESTINATION- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature: Signature: Company Name White/Facility Date: Date: Title: Pink/Carrier Goldenrod/Generator GENERATOR A a-i-_--- 19f' _ POINT Complete Address: County: IV ] -71. x! ` Class &Type of Contaminate in soil F SOURCE OF CONTAMINATION (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleum product residue, tarn submitting this Certi, sate of Waste- Constituents. I certify that am familiar with the source of contamination of the soil andfuriher certtfy the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TR"SPORTER " Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are, in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK#: _ TA #= VOLUME: .�` TRUCK DRIVER SIGNATURE: :. DATE: , DESTINATION Environmental Soils Inc. 910 Crowder Rd, Shelby;'NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Stateof North Carolina. Facility Signature: wDate: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/C�rketor Class &Type of Contaminate in soil � -.�".b 1 SOURCE OF CONTAMVVATION (ex. UST or other source) A . GENERdTORS CERTI-F`IC,4770N OF WISTE CONSTITUENTS: In lieu of submitting an cal data (methods 8240 and 8270j verifying that the waste in question does not contain organic constituents other than those which would normally a0ear in analysis of virginpetr©leum_►roduct residue, Iam submitting this Certificate of Waste Constituents. I certify that I am familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, contains no contaminants other than that lasted above. Generators Signature: Date: TRANSPORTER. - Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are .'in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAG #: VOLUME: s F�TRUCK. DRIVER SIGNATURE:-_�� { �.., Wy ' �. �_ ,_. _ j�-..�� ` DATE: DESTIN�ITIOE tal Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application <., I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator Environmental Soils Inc, PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 - Fax 704-434-9533 Non -Hazardous Waste Manifest # 4 8 9 Date Load Number (numbered sequentially as trucks are dispatched) ENVIRONMENT4L CONSULTANT; Contact: _ )` j _ Phone: -_ t Fax: GENEPUTOR: ` i Address: County: _m e" Contact: Phone: WASTE ORIGLVJT[ONPOlNT.-Complete Address: Class &Type of Contaminate in soil i x ' SOURCE OFCONT1tHRUTION (ex. UST or oth r source) A GEATRATORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis ofvirgin petroleum product residue, lam submitting this Certificate of Waste Constituents. I certry that I am familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TR"SPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: } TRUCK #: TAG # M- VOLUME: -� TRUCK DRIVER SIGNATURE: DATE: r s DESTINATION Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Appliaux Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this ` terial for treatment and/or disposal in: a manner that has been authorized by the State of North Carolina. Facility Signature: Date: Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator .............� Environmental Soils Inca PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # 48940 Date Load Number (numbered sequentially as trucks are dispatched) ENVIRONMENT4L CONSULS C 5 ( Contact: Phone: 26, Fax: GENER,ITOR: Address:- County:- w , Contact: Phone: W,ISTE ORIGVVATI0NP0IN7 Complete Address: t Class &.Type of Contaminate in soil SOURCE OF CONTAH17VATION.- (ex. UST or other source) = a GENER,4TORS CERTIEIC,4TION OF WJSTE CONSTITUENTS. In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally apfiear in analysis of virginpetroleumproduct residue, lam submitting this Certificate of Waste Constituents. I certify thatl am familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: 4_ Date: TRANSPORTER ' _ � Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: 1 VOLUME: s _. TRUCK DRIVER SIGNATURE:- T _ w DATE: DESTLVATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature:-- Date: ; Signature: Date Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704-434-0075• Fax 704-434-9533 Non -Hazardous Waste Manifest # 48938 Date Load Number (numbered sequentially as trucks are dispatched) EAWRONMENTAL CONSULTANT 2 Contact: o r - i Phone ; Z, "- ,Fax: GENERATOR, - Address: County: Contact: Phone: WASTE ORIGINIITIONPOINT.• Complete Address: 7� S y,g Class & Type of Contaminate in soil SOURCE OF CONT,4MwATION (ex. UST or other source) GENER 4TORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally aPPear in analysis of virgin petroleum_product residue, I am submitting this Certificate of Waste Constituents. I certify tbat I am familiar with the source of contamination of the soil and further certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signatare�> . Date: .^ TMNSPORTER _ 5e, Contact: - Phone As the carrier, I certify that the materialsdescribed above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: - Date: T TRUCK #: TAC?-Z" VOLUME: r TRUCK DRIVER SIGNATURE:' DATE: DEST12VATION Environme Sqr s Inc, 9I0 Crow e Rd, Shelby, NC 28150 Dedicated Land Application Site Pe t # R0300038 I certify that the carrier bras vexed the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature: Date: Signature: Company Name White/Facility Canary/Invoice Date: Title: Pink/Carrier Goldenrod/Generator Environmental Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704-434-0075 • Fax 704-434-9533 Non -Hazardous Waste Manifest # 4 8 9 8 3 Date Load Number (numbered sequentially as trucks are dispatched) ENVIRONMENTAL CONSULTANT Contact: Phone - Fax: GENER.4TOX Address: County: Contact: Phone: WASTE ORIGEVATIONPOINT Complete Address: Class &Type of Contaminate in soil SOURCE OF CONT 4MINATION. (ex. UST or other source) GENERJTORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu ofsubmitting analytical data (methods 8240 and $270) verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virgin petroleuml5roduct residue, Iam submitting this Certocate of Waste Constituents. I certify that I am familiar with the source of contamination of the soil and further certjry the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: TRJNSPORTER: Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: TAC #. VOLUME: TRUCK DRIVER SIGNATURE; DATE � DESTIN14TION Environmental Soils Inc. 910. Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to'this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature: Signature. Company Name Date: Title: Date: White/Facility ` Canary/Iiavoice Pink/Carrier Goldenrod/Generator Environrnen,W Soils Inc. PO Box 295 - Lattimore, NC 28089 ,Phone 704-434-0075 - Fax 704-434-9533 Non -Hazardous Waste Manifest # 4 8 9 4 1 Date �..�... Load Number (numbered sequentially as trucks are dispatched) e- ENVIROAMENTAL CONSULTAW. 'Contact: -1— Phone. Fax: GENERATOR - Address: _ County: 2- Contact: Phone: WASTE ORIGLVATIONPOINT- Complete Address: Class &Type of Contaminate in soil SOURCE OF COATAMEVATION.- (ex. UST or other source) 'T GEAER.4TORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu ofsubmitting analytical data (methods 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would normally appear in analysis of virginpetroleumproduct residue, Iam submitting this Certificate of Waste Constituents. I certify that Iamfamiliar with the source of contamination of the soil and fiirtber certify the source, to the best of my knowledge, contains no contaminants other than that listed above. Generators Signature: Date: YA"SPORTEX- f Contact: Phone: As the, carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: ate: TRUCK #: TAG #: VOLUME: TRUCK DRIVER SIGNATURE:: DATE: D-kSTLV_4T[OX.- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated La Site Permit #SR0300038 , Land Application I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature: Signature: Company Name Date: Date: Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator Environmental Soils Inc., PO Box 295 - Lattimore, NC 28089. 9, Phone 704-434-0075 - Fax 704-434-9533 Non -Hazardous Waste Manifest . # 48933 Date __—Load Number {numbered sequentially as trucks are dispatched) ENVIRONMENTA CONSULTMW.- Contact: -Y Phone Fax: GENERATOR - Address: County: Contact: ph n WASTE OR1G]N,4T[0NP011W.- Complete Address: Class &Type of Contaminate in soil t I I SOURCE OF COATdMJN4TIOX.• (ex. UST or other sour GENERATORS CERTIFICATION OF WASTE CONSTITUENTS; In lieu of submitting analytical data (method's 8240 and 8270) verifying that the waste in question does not contain organic constituents other than those -which would normally a0pear in analysis of virgin petroleumproduct residue, Iam submitting this Certificate of Waste Constituents. I certify thatI rim familiar with the source of contamination of the soil airy further certify the source, to the best of my knowledge, contains no contaminants other than that listed above — Generators Signature: -Date: TRANSPORTER: - Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are property classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations'governing transportation, and I hereby receive this material for delivery to the facility designate. .".Carrier Signature- Date: TRUCK#: TAG #- VOLUME: TRUCK DRIVER SIGNATURE: DATE: DESTIN,4770N.- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature: Date: Signature: Company Name Date: Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator Beverly, Trudy From: Joe Fontana <jfontana@chelseabuildinggroup.com> Sent: Tuesday, April 6, 2021 3:11 PM To: Beverly, Trudy Subject: Re: [External] NCDEQ Report CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Thank you and you too! Sincerely, Joe Fontana (980) 221-0500 Chelsea Building Group From: Beverly, Trudy <trudy.beverly@ncdenr.gov> Sent: Tuesday, April 6, 2021 2:40 PM To: Joe Fontana <jfontana@chelseabuild inggroup.com> Subject: RE: [External] NCDEQ Report Hey Joe, Reports received. Thank you and have an excellent day, Trudy Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality UST Section, Mooresville Regional Office rt� n[ol 6mironniwt3l 4uaM 704.235.2182 (Office) Trudy.BeverlyAncdenr. gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: https:Hdeg.nc.gov/about/divisions/waste-manaizement/ust Branch's Above Ground Storage Tanks Website Address: https:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-program INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httpsagov/about/divisions/waste-management/waste-management-rules-data/waste-mana eg ment_ ig s-mates File Review Procedures: hftps:Hdeq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): ht!ps:Hdeq.nc.gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: https://files.nc.2ov/ncde(i/Waste%2OManaEement/D WMIUST[W hatsNew/Final-Electronic-Document-Submittal-Policv.pdf https:Hfiles.nc. gov/ncdeg/Waste%20Management/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx From: Joe Fontana [mailto:jfontana@chelseabuildinggroup.com] Sent: Tuesday, April 6, 2021 2:34 PM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: Re: [External] NCDEQ Report CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Hi Trudy, Please see attached and let me know if you need anything else. Sincerely, Joe Fontana (980) 221-0500 Chelsea Building Group From: Beverly, Trudy <trudy.beverly@ncdenr.gov> Sent: Tuesday, April 6, 2021 8:03 AM To: Joe Fontana<ifontana@chelseabuild inggroup.com> Subject: RE: [External] NCDEQ Report Good Morning Joe, Ron forwarded me the Swans Run Road Soil Excavation Report. I handle home heating oil usts for Mecklenburg County. The report does not have a licensed geologist or professional engineer's seal. The soil report also recommended that UST Closure and Initial Abatement Action Report dated September 23, 2016 be submitted for review as well. Please email a copy of the 2016 UST Closure/Initial Abatement reports as well as a sealed/stamped copy of the Soil Excavation Report when available for review. Have a wonderful day, Trudy Trudy Beverly, L.G. �� Hydrogeologist, Division of Waste Management �DENorth Carolina Department of Environmental Quality W� To i��m��� UST Section, Mooresville Regional Office 704.235.2182 (Office) Trudv.Beverlv(a)ncdenr. aov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: https:Hdeq.ne.gov/about/divisions/waste-management/ust/ast-program INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httDS: //dea.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-ais-maps File Review Procedures: https://deq.nc.,gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): htti)s://deo.nc. gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: https://riles.ne.gov/ncdeq/Waste%2OManagement/DWM/USTIW hatsNew/Final-Electronic-Document-Submittal-Policv.pdf https://fiIes.nc.gov/ncdeq/Waste%2OManagement/DWM[UST/Corrective%2OAction/UST%20file%2Onames%2Ofor%2OLaserfiche.doex From: Taraban, Ron Sent: Tuesday, April 6, 2021 7:42 AM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: FW: [External] NCDEQ Report From: Joe Fontana<ifontana@chelseabuildinggroup.com> Sent: Monday, April 05, 2021 3:09 PM To: Taraban, Ron <ron.taraban@ncdenr.gov> Subject: [External] NCDEQ Report CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Hi Ron, I hope you are well. I was told I needed to submit this report to you from one of our sites. Please let me know if there is anything else you need. Sincerely, Joe Fontana (980) 221-0500 Chelsea Building Group