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Home My WebLink AboutMO-28338_47594_CA_IAR_20201113_Initial Abatement Report Soil Samples//AAk SUMMIT 0 LOUMN INITIAL ABATEMENT ACTION REPORT 61 Union Street South Concord, NC SUMMIT PROJECT NO.4314.E0006 Prepared For: Cabarrus County PO Box 707 Concord, NC 28026 Prepared By: SUMMIT Engineering, Laboratory & Testing, P.C. PO Box 7384 Concord, NC 28241 (704)504-1717 November 13, 2020 I, Michael D. Zavislak, NRCC-EAC, CHMM, CIH, PE, a Professional Engineer for SUMMIT, do certify that the information contained in this report is correct and accurate to the best of my knowledge. 18CAR,"/- :A SEAL r-a 0338G� .• �y yGlxE�4.' Michael D. Zavislak, NRCC-EAC, CHMM, CIH, PE SUMMIT Engineering, Laboratory & Testing, PC SUMMIT Engineering, Laboratory & Testing, PC is licensed to practice engineering in the State of North Carolina. The certification number of SUMMIT Engineering, Laboratory & Testing, PC is C-4361. D:\!Michael!\! SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\reportfiles\R- UST - Tank Closure Report.doc UST Closure Report SUMMIT Project No. 4314.E0006 61 Union Street South, Concord, North Carolina November 13, 202G TABLE OF CONTENTS 1.0 TANK CLOSURE REPORT......................................................................................................1 A. SITE INFORMATION......................................................................................................................... I A.1. Site Identification................................................................................................................ I A.2. Contact Information............................................................................................................ I A.3. Release Information............................................................................................................2 A.4. Certification.........................................................................................................................2 B. SITE HISTORY AND CHARACTERIZATION................................................................................2 B.1. UST Owner and Information..............................................................................................2 13.2. UST Information................................................................................................................. 2 B.3. Non -UST Information.........................................................................................................3 BA. Release Information............................................................................................................3 13.5. Site Characteristics..............................................................................................................3 C. SITE CHECK........................................................................................................................................4 D. CHANGE IN SERVICE.......................................................................................................................4 E. FREE PRODUCT INVESTIGATION.................................................................................................4 F. GROUNDWATER AND SURFACE WATER INVESTIGATION...................................................4 G. INITIAL RESPONSE AND ABATEMENT ACTION.......................................................................4 G.1. Notification..........................................................................................................................4 H. EXCAVATION OF CONTAMINATED SOIL....................................................................................4 H.1. Initial Investigation.............................................................................................................4 H.2. Excavation...........................................................................................................................4 H.3. Post Excavation Sampling.................................................................................................. 5 H.4 Soil Investigation.................................................................................................................6 H.5. Disposal...............................................................................................................................6 H.6. Conclusions and Recommendations..................................................................................6 1. CONCLUSIONS...................................................................................................................................6 D:\!Michael!\! SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\reportfiles\R- UST -Tank Closure 1 Report.doc UST Closure Report 61 Union Street South, Concord, North Carolina APPENDICES FIGURES Figure 1.0 Topographic Map Figure 2.0 Site Map Figure 3.0 Sampling Map Figure 3.1 Cross Sectional Sampling Map Figure 4.0 Aerial Photograph NRCS Soil Survey Site Photographs TABLES Table B- I Table B-2 Table B-3 Table B-4 APPENDIX C: UST-61 24-Hour Notice of Release APPENDIX E: Certificate of UST Disposal APPENDIX I: Chain of Custody APPENDIX J: Analytical Results SUMMIT Project No. 4314.E0006 November 13, 2020 D:\!Michael!\! SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\reportfiles\R- UST -Tank Closure ii Report.doc UST Closure Report 61 Union Street South, Concord, North Carolina 1.0 TANK CLOSURE REPORT A. SITE INFORMATION A.I. Site Identification Date of Report: November 13, 2020 Facility ID: N/A Incident Number: Unknown Site Rank: N/A Site Name: 61 Union Street South Site Street Address: 61 Union Street South Concord, NC Geographic Data Point: Tank Basin Location Method: GPS Latitude: 35024'35.82" N Longitude: -80034'46.16" W A.2. Contact Information Property Owner: Cabarrus County PO Box 707 Concord, NC 28026 Property Occupant: Vacant SUMMIT Project No. 4314.E0006 November 13, 2020 Consultant: SUMMIT Engineering, Laboratory & Testing, P.C. 3575 Centre Circle Fort Mill, SC 29715 (704)504-1717 North Carolina Professional Engineer's License Number: C-4361 Laboratory: Pace Analytical Services, LLC 106 Vantage Point Drive DA!Michael!\! SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\reportfiles\R- UST - Tank Closure I Report.doc UST Closure Report 61 Union Street South, Concord, North Carolina A.3. Release Information Date Discovered: Estimated Release: Cause of Release: Source of Release: Size and Contents: A.4. Certification See Cover Page. SUMMIT Project No. 4314.E0006 November 13, 2020 West Columbia, SC 29172 (803)791-9700 State of North Carolina Certification Number: 329 September 14, 2020 Unknown Unknown UST 96" x 40" — Home Heating Fuel B. SITE HISTORY AND CHARACTERIZATION B.1. UST Owner and Information Table B-2: Site History - Owner and Operator Information ID Number UST-1 Facility ID Number N/A Name of Owner Dates of Operation mm/dd/ to mm/dd/ Cabarrus County Unknown to current Street Address PO Box 707 city State zip Telephone Number Concord NC 28026 704-305-9723 Name of Operator Dates of Operation mm/dd/ to mm/dd/ N/A Unknown to current Street Address city State zip Telephone Number B.2. UST Information Table B-1: Site History — System Information DA!Michael!\! SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\reportfiles\R- UST - Tank Closure 2 Report.doc UST Closure Report 61 Union Street South, Concord, North Carolina SUMMIT Project No. 4314.E0006 November 13, 2020 AST ID Current Previous Capacity Construction Tank Description Date Tank Status Was Number /Last Contents (in Details Dimensions of Installed of release Contents gallons) Associated UST associated Piping and with the Pumps UST System? UST-1 Home N/A 500 Steel 96" x 40" unknown unknown removed Yes Heating Fuel B.3. Non -UST Information There are no other UST's, AST's, piping and dispensers located on the site. There are no historical compliance issues. B.4. Release Information On September 14, 2020, the grading contractor was grading for the new utility installation and struck the UST. SUMMIT arrived onsite and instructed the grading contractor to excavate the UST and contaminated soils. Approximately 445 tons of contaminated soils were stockpiled onsite, on plastic and covered with plastic until disposal. The UST was crushed and taken with the contaminated soils. The contaminated soils were transported to Republic Services landfill in Concord, NC on October 9, 2020. B.S. Site Characteristics The United States Geological Survey (USGS) "Concord, North Carolina, United States" topographic quadrangle map was reviewed. According to the contour lines on the topographic maps, the elevation of the subject site is approximately 710 feet above Mean Sea Level (MSL). The inferred groundwater flow direction based on topography appears to be to the east towards an un- named creek. The un-named creek flows into Threemile Branch. Threemile Branch flows into Cold Water Creek. Cold Water Creek flows into the Rocky River. This site contains the soil types: Ur —Urban land The surface cover of the UST basin was a concrete sidewalk. D:\!Michael!\! SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\report files\R- UST - Tank Closure 3 Report.doc UST Closure Report 61 Union Street South, Concord, North Carolina C. SITE CHECK Not Applicable. D. CHANGE IN SERVICE Not Applicable. E. FREE PRODUCT INVESTIGATION Not applicable. SUMMIT Project No. 4314.E0006 November 13, 2020 F. GROUNDWATER AND SURFACE WATER INVESTIGATION Not applicable. G. INITIAL RESPONSE AND ABATEMENT ACTION G.1. Notification On September 14, 2020, the grading contractor was grading for the new utility installation and struck the UST. SUMMIT arrived onsite and instructed the grading contractor to excavate the UST and contaminated soils. Approximately 445 tons of contaminated soils were stockpiled onsite, on plastic and covered with plastic until disposal. The UST was crushed and taken with the contaminated soils. The contaminated soils were transported to Republic Services landfill in Concord, NC on October 9, 2020. H. EXCAVATION OF CONTAMINATED SOIL H.I. Initial Investigation On September 14, 2020, the grading contractor was grading for the new utility installation and struck the UST. SUMMIT arrived onsite and instructed the grading contractor to excavate the UST and contaminated soils. Approximately 445 tons of contaminated soils were stockpiled onsite, on plastic and covered with plastic until disposal. H.2. Excavation On September 14, 2020, the grading contractor was grading for the new utility installation and struck the UST. SUMMIT arrived onsite and instructed the grading contractor to excavate the UST D:\!Michael!\! SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\USTreportfiles\R- UST - Tank Closure 4 Report.doc UST Closure Report 61 Union Street South, Concord, North Carolina SUMMIT Project No. 4314.E0006 November 13, 2020 and contaminated soils. Approximately 445 tons of contaminated soils were stockpiled onsite, on plastic and covered with plastic until disposal. H.3. Post Excavation Sampling SUMMIT was retained to collect soil samples during the removal of the UST system and. SUMMIT collected four (4) soil samples from the sidewalls of the tank basin and one (1) soil sample from the base of the excavation on October 15, 2020. The sidewall samples were collected at approximately 10 feet from the top of the excavation. The bottom sample was collected from the center of the tank basin. Sample Date 9/15/2020 9/15/2020 9/15/2020 9/15/2020 9/15/2020 CONSTITUENT RSCL2 MSCC BOTTOM N-WALL S-WALL E-WALL W-WALL 8260 BRL BRL BRL BRL BRL 8270 BRL BRL BRL BRL BRL Table B-4: Summary of Soil Sampling Results Analytical Method e.., VOC by EPA 8260 8260 8270 EPH VPH Contaminant of Concern Sample ID Date Collected (mm/dd/yy) Source Area (eg. Tank pt 1) Sample Depth (ft BGS) Incident Phase (Closure, 20Day, LSA, etc.) Bot-1 9/15/2020 confirmation 4 Closure Exceeds Exceeds Exceeds Exceeds B-1 9/15/2020 bottom 12 Closure BRL BRL BRL BRL N-1 9/15/2020 sidewall 10 Closure BRL BRL BRL BRL E-1 9/15/2020 sidewall 10 Closure BRL BRL BRL BRL S-1 9/15/2020 sidewall 10 Closure BRL BRL BRL BRL W-1 9/15/2020 sidewall 10 Closure BRL BRL BRL BRL Soil to groundwater MSCC (mg/kg) BRL BRL Residential MSCC (mg/kg) BRL BRL Industrial/Commercial MSCC (mg/kg) N/A N/A Indicate method detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42) List any contaminant detected above the method detection limit Results must be reported in ug/1 ug/1=micrograms per liter GCL = gross contamination level D:\!Michael!\! SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\reportfiles\R- UST - Tank Closure 5 Report.doc UST Closure Report SUMMIT Project No. 4314.E0006 61 Union Street South, Concord, North Carolina November 13, 2020 HA Soil Investigation New, clean disposable latex gloves were used for the collection of each soil or groundwater sample. Samples collected for laboratory analyses were placed in laboratory -supplied containers with the sampler's name, time and date the sample was collected, and laboratory analyses to be performed. The samples were packed on ice and taken to Pace Analytical Services, LLC in Columbia, South Carolina. For a drawing detailing the locations of the soil samples, please refer to Figure 3.0 in the appendices. Groundwater was not encountered in the excavation. The samples were grab samples. Standard chain -of -custody procedures were followed. Field screening was based on visual and olfactory observations. In addition, soil samples were taken from the excavation and were analyzed onsite using an IAQRAE Indoor Air Quality Monitor w/ VOC Measurement. Prior to each analysis, the IAQRAE was allowed to equilibrate to the area temperature and ambient air conditions. H.S. Disposal Approximately 445 tons of contaminated soils were removed from the site on October 9, 2020 and taken to Republic Service, Inc. in Concord, NC. H.6. Conclusions and Recommendations After the contaminated soils were excavated, the soil contamination levels were below the regulatory levels: No free product was encountered. Groundwater was not encountered. I. Conclusions Based on the concentrations of the analytical results reported in the soil samples collected, no additional assessment is recommended. DA!Michael!\! SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\reportfiles\R- UST - Tank Closure 6 Report.doc UST Closure Report SUMMIT Project No. 4314.E0006 61 Union Street South, Concord, North Carolina November 13, 2020 FIGURES D:\!Michael!\!SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\report files\R- UST - Tank Closure 18 Report.doc � 1 �►� 73 A P s a P m Site r nn" � ' RD T I n C% DR`SE 1500' Radius CH�YNUT boy y��1V N VL •��o CN VV W, Figure 1 61 Union St S SUMMIT ELT, PC �. USGS Topographic Map Concord, NC Project:4314.E0006 SUMMIT DA!MichaelNSUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\report files\UST - Figure 1 Topo.doc 1P"Jemw 29 601 c• 0 f TO St AlV r i§a Are & 73 y C 0 �"l neon St s rn Lrn m Lq rr, Figure 2 Site Location Map 61 Union St S Concord, NC s max. SUMMIT ELT, PC AAProject:4314.E0006 SUMMIT D:\!Michael!\!SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\report files\UST - Figure 2 Site Map.doc Source: Drawn by SUMMIT off of field notes 11A& SUMMIT N S-1 S-S :' • ® S-2 �••• S-a S-3 KEY Soil Sampling Location Prepared By\Date: MZ/11/2020 Checked By\Date: MZ/11/2020 Sampling Location Plan 61 Union St S Concord, NC Scale NTS Figure 3.0 Sandy CIE 15 FEET 10. B-1 Note: Cross Section Sketch for UST KEY Soil Sampling Location Source: Drawn by SUMMIT off of field notes //Ad& SUMMIT Scale Depth Below Ground Surface (BGS) 9 W -10 -15 -20 Prepared By\Date: MZ/11/2020 Checked By\Date: MZ/11/2020 Sample Map Cross Section 61 Union St S Concord, NC As Shown Figure 3.1 ............. _0 A 3 538171 35o 24' 36' N Soil Map—Cabarrus County, North Carolina 538175 538179 538183 538187 538191 ■ Soil Map may not be valid at this scale. 35o 24' 35" N I i 538171 538175 538179 538183 538187 538191 3 Map Scale: 1:170 if printed on A portrait (8.5" x 11") sheet. Meters N 0 2 5 10 15 Feet 0 5 10 20 30 Map projection: Web Mercator Comer coordinates: WGS84 Edge tics: UTM Zone 17N WGS84 U}DA Natural Resources Web Soil Survey Conservation Service National Cooperative Soil Survey r 3 a 538195 35' 24' 36" N r 35' 24' 39' N 538195 3 11 /13/2020 Page 1 of 3 MAP LEGEND Area of Interest (AOI) 0 Area of Interest (AOI) Soils 0 Soil Map Unit Polygons rwr Soil Map Unit Lines 0 Soil Map Unit Points Special Point Features Vo Blowout Borrow Pit Clay Spot Closed Depression Gravel Pit .14 Gravelly Spot 0 Landfill Lava Flow Marsh or swamp + Mine or Quarry Miscellaneous Water Perennial Water Rock Outcrop Saline Spot 4 Sandy Spot Severely Eroded Spot Sinkhole Slide or Slip oa Sodic Spot Soil Map—Cabarrus County, North Carolina MAP INFORMATION Spoil Area The soil surveys that comprise your AOI were mapped at 1:24,000. Stony Spot Very Stony Spot Warning: Soil Map may not be valid at this scale. Wet Spot Enlargement of maps beyond the scale of mapping can cause misunderstanding of the detail of mapping and accuracy of soil Other line placement. The maps do not show the small areas of .- Special Line Features contrasting soils that could have been shown at a more detailed scale. Water Features Streams and Canals Please rely on the bar scale on each map sheet for map measurements. Transportation Rails Source of Map: Natural Resources Conservation Service Web Soil Survey URL: rwr Interstate Highways Coordinate System: Web Mercator (EPSG:3857) US Routes Maps from the Web Soil Survey are based on the Web Mercator L Major Roads projection, which preserves direction and shape but distorts distance and area. A projection that preserves area, such as the Local Roads Albers equal-area conic projection, should be used if more accurate calculations of distance or area are required. Background . Aerial Photography This product is generated from the USDA-NRCS certified data as of the version date(s) listed below. Soil Survey Area: Cabarrus County, North Carolina Survey Area Data: Version 19, Jun 2, 2020 Soil map units are labeled (as space allows) for map scales 1:50,000 or larger. Date(s) aerial images were photographed: Nov 6, 2019—Nov 20, 2019 The orthophoto or other base map on which the soil lines were compiled and digitized probably differs from the background imagery displayed on these maps. As a result, some minor shifting of map unit boundaries may be evident. USDA Natural Resources Web Soil Survey 11/13/2020 Conservation Service National Cooperative Soil Survey Page 2 of 3 Soil Map—Cabarrus County, North Carolina Map Unit Legend Map Unit Symbol Map Unit Name Acres in AOI Percent of AOI Ur Urban land Totals for Area of Interest 0.1 0.1 100.0% 100.0% usDA Natural Resources Web Soil Survey 11/13/2020 Conservation Service National Cooperative Soil Survey Page 3 of 3 UST Closure Report 61 Union St. South, Concord, NC Tank under sidewalk Tank under sidewalk SUMMIT Project No. 4314.E0006 November 13, 2020 UST Closure Report 61 Union St. South, Concord, NC SUMMIT Project No. 4314.E0006 November 13, 2020 r I I UST Closure Report 61 Union St. South, Concord, NC SUMMIT Project No. 4314.E0006 November 13, 2020 UST Closure Report 61 Union St. South, Concord, NC UST SUMMIT Project No. 4314.E0006 November 13, 2020 UST Closure Report 61 Union St. South, Concord, NC APPENDIX C UST-61 SUMMIT Project No. 4314.E0006 November 13, 2020 DA!Michael!\!SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\report files\Appendix C UST 61.docx UST-61 24-Hour Release and UST Leak Reporting Form. For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or in NC suspected release (DWM USE ONLY) Suspected Contamination? (Y/N) Y Facility ID Number Incident # Risk (H,I,L,U) Confirmed GW Contamination? (Y/N) Date Leak Discovered Received On Received By Confirmed Soil Contamination ?(Y/N) Comm/Non-Commercial? Reported by (circle one): Phone, Fax or Report Samples Taken?(Y/N) Y Reg/Non-regulated? Region Free Product? (Y/N) N If Yes, State Greatest Thickness N/A INCIDENT DESCRIPTION Incident Name: fy! tJnion Street S. Concord, NC Address: 61 pinion Street S County: Cabarrus 28025 Regional Office (circle one): Asheville. Mooresville. Fayetteville. City/Town: Concord Zip Code: Raleigh, Washington, Wilmington, Winston-Salem Latitude (deamai degrees): 35'24'35.62"N Longitude (deamai degrees) : 80'34'46.32"W Obtained by: Briefly describe suspected or confirmed release: (including but not limited to. nature of release, date of release, amount x❑GPS of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors) On September 14, during excavation for sewer lines, a UST was encountered. On September 15, the UST was ❑Topographic map excavated along with the contaminated soils. The soil contamination could not be successfully excavated from ❑GIS Address matching the site due to property boundaries, utilities and existing buildings. ❑Other ❑ Unknown Describe location: HOW RELEASE WAS DISCOVERED (Release Code) (Check one) ❑Release Detection Equipment or Methods IX Visual/Odor ❑Groundwater Contamination QDuring UST Closure/Removal ❑Water in Tank ❑Surface Water Contamination ❑Property Transfer ❑Water Supply Well Contamination ❑Other (specify) SOURCE OF CONTAMINATION Source of Release Cause of Release Type of Release Product Type Released (Check primary source) (Check primary cause) (Check one) (Check primary product type released) Q Tank ❑ Spill Q Petroleum ❑ Gasoline/ Diesel/ ❑ Diesel/Veg. Oil ❑ Piping ❑ Overfill ❑ Non -Petroleum Kerosene Blend x❑ Heating Oil ❑ Vegetable Oil 100% El Dispenser El Corrosion ❑Both ❑ Other Petroleum ❑ E10 — E20 ❑ Submersible Turbine Pump ❑Physical/Mechanical Location Products ❑ Delivery Problem Damage ❑ E21 — E84 (Check one) ❑ Metals ❑ Install Problem ❑ E85 — E99 ❑ Spill Bucket ❑ Other Inorganics ❑ Other [:]Facility❑Ethanol 100% ❑ Other ❑ Other Organics Other ❑ Unknown [:]Residence E01 — E09 ❑ Unknown [K]Other Definitions presented on reverse Definitions presented on reverse Ownership 1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State aeration Type Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining IL UST Form 61 (02/19) Page 1 of 2 IMPACT ON DRINKING WATER SUPPLIES Water Supply Wells Affected? 1. Yes 2. No Unknown Number of Water Supply Wells Affected Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1 2. 3 UST SYSTEM OWNER UST OwnedCompany 3454o Gi ti4-rc,\ OS AfR►ALs A r., �-o Point of Contact Address City State Zip Code Telephone Number UST SYSTEM OPERATOR UST Operator/Company Address N/A N/A City State Zip Code Telephone Number N/A N/A NIA N/A LANDOWNER AT LOCATION OF UST INCIDENT Landowner Address CA3, Re,s `o,n T Po 3or 707 City State Zip Code Telephone Number CONCORo OVA a,8oac"' 764-3c5-coa Draw Sketch of Area (showing two major road intersections) or Attach Map erson Reporting Incident KA-f. (ail Af:t C LTitle Company ,.hasCu -n� Te lephone Number 7�y-;c5 5ct7a; AaA4 NP o�: Address 170 '&,.ti 707 Lw'J.QL) a8o� Date UST Form 61 (02119) Page 2 of 2 Definitions of Sources Tank. means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not tit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined UST Closure Report 61 Union St. South, Concord, NC APPENDIX E SUMMIT Project No. 4314.E0006 November 13, 2020 DISPOSAL CERTIFICATE D:A!Michae1!V!SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\report files\Appendix E COD.docx Michael Zavislak From: Kevin Aguilera <kevin.aguilera@waynebrothers.com> Sent: Thursday, November 12, 2020 9:39 AM To: Michael Zavislak Cc: Mike Fitzsimmons Subject: RE: Republic Services Michael, The tank was in pieces and with the soil when disposed. Thanks, L" Y� tim■'s CML Kevin Aguilera Assistant Project Engineer Commercial Group (704)305-1956 (704)305-1956 www.WayneBrothers.com 357 Concrescere Parkway I Davidson I NC 1 28036 From: Michael Zavislak <mzavislak@summit-companies.com> Sent: Thursday, November 12, 2020 9:32 AM To: Steffens, Steven <ssteffens@messer.com>; John Marston <jmarston@republicservices.com> Cc: Kevin Aguilera <kevin.aguilera@waynebrothers.com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com>; Kyle Bilafer <KDBilafer@cabarruscounty.us>; trudy.beverly@ncdenr.gov Subject: RE: Republic Services Yes, if I can get the tank disposal manifest of the certificate of disposal. From: Steffens, Steven <ssteffens@messer.com> Sent: Thursday, November 12, 2020 9:30 AM To: Michael Zavislak <mzavislak@summit-companies.com>; Marston, John <JMarston@republicservices.com> Cc: Kevin Aguilera <kevin.aguilera@waynebrothers.com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com>; Steffens, Steven <ssteffens@messer.com>; Kyle Bilafer <KDBilafer@cabarruscounty.us>; trudy.beverly@ncdenr.gov Subject: RE: Republic Services Great. Do you think this can be closed out by COB tomorrow? Steve Steffens Sr. Superintendent Messer Construction Co. 2400 Executive St. I Charlotte, NC 128208 i NC License #: 70194 (704) 679-6000 Office (704) 679-6090 Fax (513) 600-1434 Mobile messer.com I Twitter I LinkedIn ssteffenskmesser. corn 0 From: Michael Zavislak <mzavislak(@summit-comoanies.com> Sent: Thursday, November 12, 2020 9:23 AM To: Steffens, Steven <ssteffens@messer.com>; Marston, John <JMarston@republicservices.com> Cc: Kevin Aguilera <kevin.aguilera@waynebrothers.com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com> Subject: RE: Republic Services **** Unverified External Email - Click With Caution! **** Yes, this is what I needed for the soil disposal, for the NCDEQ report. From: Steffens, Steven <ssteffens@messer.com> Sent: Thursday, November 12, 2020 9:09 AM To: Michael Zavislak <mzavislak@summit-companies.com>; Marston, John <JMarston@republicservices.com> Cc: Kevin Aguilera <kevin.aguilera@waynebrothers.com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com> Subject: FW: Republic Services Michael and John, Is this what you are looking for? Steve Steffens Sr. Superintendent Messer Construction Co. 2400 Executive St. I Charlotte, NC 128208 NC License #: 70194 (704) 679-6000 Office (704) 679-6090 Fax (513) 600-1434 Mobile messer.com I Twitter I LinkedIn ssteffenskmesser. corn 0 From: Kevin Aguilera<kevin.aguilera@waynebrothers.com> Sent: Thursday, November 12, 2020 8:51 AM To: Steffens, Steven <ssteffens@messer.com> Cc: Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com> Subject: Republic Services * * * * Unverified External Email - Click With Caution! Steve, Please see attached Manifest and sales tickets from Republic Services. Thanks, L" WyM a'olWI WJIL 0 0 Kevin Aguilera Assistant Project Engineer Commercial Group (704)305-1956 (704)305-1956 www.WayneBrothers.com 357 Concrescere Parkway I Davidson I NC 1 28036 UST Closure Report 61 Union St. South, Concord, NC APPENDIX H DISPOSAL MANIFESTS SUMMIT Project No. 4314.E0006 November 13, 2020 DA!Michael!\!SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\report files\Appendix H Manifests.docx REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. If waste Is asbestos waste, Complete Sections I, II, 111 and IV If waste is NOT asbestos waste, complete Sections 1, [land III �% // ,^, (X1 / /! GENERATOR (Generator completes la-r1 ) / l-l� U L l Oi / Y a. Generators US EPA ID Number b. Manifest Document Number C. Page 1 of 1 d. Generator's Name and Location: e. Generators Mailing Address: Cabanas County 65 Church St. S Concord, NO 28025 g. Phone: f. Phone: If owner of the generating facility differs from the generator, provide: h. Owners Name: I. Owners Phone No.- J. Waste Profile If k. Exp. Date I. Waste Shipping Name and m. Containers I. Total o. Unit No. I Type Description Quantity vWVOI 5010 20 12767 soil 53 BILL TO: Wayne Brothers 11700 1j , vapplicable �1�D bl GENERATOR'S CERTIFICATION: I hereby cenify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any state law, has been property described, classified and packaged, and is In proper Condition for transportation according to applicable regulations; AND, dthis waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I Certify and warrant that the waste has been treated in accortiance with the Mons is of 40 CFR 268 end m n n er a hazardous waste as defined b 40 CFR 261. r . G rAutho etl ant Name Print _ q, Signature L Data a. Tran Wayne III -1 TINATIRN IOn—M, Ili.— end rleelinnfinn Cilo Illds\ a. Disposal Facility and Site Address: C. US EPA Number d. Discrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concord, NC 26027 b. Phone: 70L7824004 I herby Certify that t bova nametl materiel has been accisled and to the bast of Irviedoethefomoomaisinusandaccu W. e. Noma o(Aumo edA ant rinl f. Si nature .Date IV. ASBESTOS Gen rator completes IVa-f and Operator complet IV ) a. Operators Name and Atltlres: b. Phone: c. Responsible Agency Name and Address: d. Phone: e. Spacial Handling Instructions and Additional Information: f. 0 Friable 0 Non -Friable Q Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignmem am fully and accumte y described shows by proper shipping name and are classified, packed marked and labeled and are in all respects in proper condition for transport by highway according to applicable intemational and national goVernmennal mutations. . Operat.e. Name and Tdle Pant h. SI natum 1 I. Date 'Operator reform to the company which owns, leases, operates, controls, or supervises the fatality being demolished or Renovated. or the demolition or renovation operation or both REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. If waste is asbestos waste, complete Sections I, II, III and IV If waste Is NOT asbestos waste, complete Sections I, II and III GENERATOR (Generator completes R-r) )'M 0 C3% P� a. Generators US EPA ID Number b. Manifest Document Number C. kge 1 0 1 d. Generator's Name and Location: e. Generators Mailing Address: Cabanus County 65 Church St. S Concord, NC 28025 g. Phone: f. Phone: If owner of the generating facility differs from the generator, provide: h. Owners Name: 1. Owners Phone No.: I. Waste Profile If k. Exp. Date I. Waste Shipping Name and m. Containers n. Total o. Unit Description No. I Type Quantity WWoI 5010 2012767 soil O BILL TO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is in proper Condition for transportation according to applicable regulations: AND,'d this waste Is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I cer ihj and warrant that the waste has been freatetl in a rdanc Cosh the uire ants of 40 CFR 268 and Is no n er a aste as defined b 40 CFR 261. r . G rator Aut ortzedA ant rime Pri . Si ura r. Date n. 1 KAIVJ"PUKI FR (Generator completes Ila-b and Transporter comDletes Ilc-e) a. Transporters Name and Address: Wayne Brothers b. hone: 09 qo'� i ril vl K• to c. Driver Name Print d. Signaturee. Date III. DESTINATION (Generator complete Illac and Destination Site completes Illd-g) a. Disposal Facility and Sita Address: c. US EPA Number d. Discrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concord, NC 28027 b. Phone: 704-782-20N I nemy canny that the above named material has been acre tact and to the best of my knowledge the foregfIng is hu antl accurate. "6 Aj a. Name of or¢ ent Print f. SI natu .Data IV. ASBESTOS (Generator completes IVa-f and Operator complete IVr i) a. Operators Name and Address: —7c. b. Phone: Responsible Agency Name and Address: d. Phone: e. Special Handling Instructions and Additional Infomurgan: I. EI Friable M Non -Friable ❑ Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the contents of this Consignment are fully and accurately described above by proper shipping new and are classified, packed, marked and labeled and are in all respects in proper condition for transport by highway according to applicable international and national governmentalregulations. . Operator's Name and This Print In. SI nature I I. Date 'operator refers to the Company which owns, Saws, operates, controls, or supervises the facility being demolished or renovated, or the demolition or Renovation operation or both C REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. If waste is asbestos waste, Complete Sections I, II, III and IV If waste is NOT asbestos waste, complete Sections I, II and III GENERATOR ff-lpneratnr 1. •1 %-I t A(-?? 12 ators US EPA ID Number b. Man"aest Document Number C. Page 1 of ators Name end Location: e. Generators Meiling Address: County ChuCabannrch h St. S =28025 , NC 28025g. Phone: f the generating facility diffelafrom the generator, provide:'s Name: 1. Owners Phone No.: I. Waste Profile # k. Exp. Date I. Waste Shipping Name and m. Containers: n. Total o. Unit 20 12767 DesLA bon No. T Ouant' WI/Vol5010 soil BILL TO: Wayne Brothers 11700 applicable GENERATOR'S CERTIFICATION: I hereby certify that the above named material rs not a hazardous waste es defined by 40 CFR 281 or any state law, has been properly described, classiAetl antl packaged, antl is in proper contlaion for transportation according to applicable regulations; AND, d his waste u a treatment residue of a prev' usty restricted hazardous waste sub t osal Restrkllona. I certify end warrant that the waste has been treated in accordance with the ulrements of 40 CFR 268 and Is n er a hazardous teas defined b 40 CFR 261. ; . Gan rAut deed ant Name riot . SI n ore r. Da e .._..._. _..._.. a. Transporters Name and Address. Wayne Brothers b. Phone: / 7 c. Driver Name (Print) tl Skinabst, Date III. DESTI ATION' .pnpratnr emm�lplp Ills endIll. n «,.,Ie•e.. uu ..ruu ..t a. Disposal Facikty and Site Address: CMS Landfill c. US EPA Number tl. Discrepancy Intllcotlon Space: 5105 Morehead Rd Concord, NC 28027 b. Phone: 704782-2004 I nemy co that the above named material has been accepted and to the best of M knowledge the loMohM Is two and accumIg. / e. Narita ofA t . hdaedA nt Pdnl f. Si nelu .Date III. ASBESTOS (Generator c01"InDlete6 lVa-f and Operator complete lVe-1) a. Operators Name and Address: b. Phone: C. Responsible Agency Name and Address: d. Phone: e. Special Handling Inslruc ions and Additional Information: LEI Friable N Non -Friable Q Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled and are in all respects In proper condition for transport by highway according to applicable inremalional and national novenum.mal regulations. if Q. O rato's Name and Title Print h. SI nature I. Data 'Operator refers to the Company which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or me demolition or renovation operation or both REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. If waste is asbestos waste, complete Sections I, II, III and IV If waste is NOT asbestos waste, complete Sections I, II and III ,�/ GENERATOR fGend eratnr Pmm�lmoc i� I '' / l OC/7 n'o1 a. Generator's US EPA ID Number b. Man'dast Document Number c. Page 1 of 1 d. Generator's Name and Location: CabanaCounty a. Genemmes Meiling Address: 65 Church S Concord, NC 28025 g. Phone: I. Phone: If owner of the generating facilitydHfers from the generator, provide: h. Chaves Name: 1. Owner's Phone No.: J. Waste Profile # k. "P. Date I. Waste Shipping Name and m. Containers n. Total o. Unit Descri lion No. 7 e QuentWWaI 5010 20 72787 soil 1 "Ll BILL TO: Wayne Brothers 11700 (90 GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste -as —defined by 40 CFR 261 or any applicable state law, has been Properly described. classified and packaged, and is in proper Condition for transportation according to applicable regulations; AND, ifthis waste is a treatment residue of a previous) restricted hazardous waste subject to the Land Disposal Restrictions. I cerlNy and warrant that the waste has been treated in rdance there wtih ui mans of 40 CFR 268 and Is no losera aste as defined b 40 CFR 261. . Gan or Authorized Agent Nam. 1-Flu I q. SQm,,m I r. Data n a. Trenspoder's Name and Address; Wayne Brothers Is. Ph a: c. river Name Print d. Si nature e. Data III. DESTINATION !Gene tnr rmm.lam Illor —A a- ___ ..r.,I— rrr' a. Disposal Facility and Site Add c. US EPA Number d. Dkcrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concord, NC 28027 b. Phone: 704-782-20D4 I herby cemlyt e m above named matedal has been acre m end o he best of m Knowledge the fo cin true and accurate. .Jigs e, theme of A horded a Prim (. S' nature S. pa ra. naaea erator completes Iva-f and Up to complete Ng-i) a. Operelor's Name aM Address: b. Phone: e. Responsible Agency Name and Address: d. Phone: 8. Special Handling Instructions and Additional Information: f. Friable Non-Frabb Bolh %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the Contents of this Consignment are full and accurately described above by proper shipping name and are classified, packed, marked and labeled and are In all respects in proper condition for transport by highway according to applicable International and national gmemmental reaculations. . O eralor's Name antl Title Print h. SI nature i. Date 'Operator refers to the company which owns, leases, operates, controls, or supervises me facility being demolished or renovated, or the demolition or renovation operation or both REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. If waste Is asbestos waste, complete Sections I, II, 111 and IV If waste is NOT asbestos waste, complete Sections I, Hard If am/ �� GENERATOR (Generator comoletes la-r) 'ry7641-vT a. Generator's US EPA ID Number b. Manifest Document Number c. age 101 f d. Generator's Name and Location: a. Generator's Mailing Address: Cabanus County 65 Church St. S Concord, NO 2W25 g. Phone: f. Phone: If owner of the generating facility differs from the generator, provide: In. Owners Name: i. Owner's Phone No.: 1. Waste Profile If k. Exp. bete 1. Waste Shipping Name and Desertiption on. Containers I n. Total Quantity 0. Unit Wwo1 No. I Type 5010 2012767 soil BILL TO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: I hereby sanity that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of a previously restricted hazardous waste a bleat to the Land Disposal Restrictions. I certify and warrant that the waste has been treated In rdance with there Imments of 40 CFR 268 ant U n on er hazer pus waste as defined b 40 CFR 287. -?-zeze P. GenerMAuthorized Anent Name . Sin ure r. Date II. TRANSPORTER Generator completes Ila-b and Transporter completes Ilc-e) a. Transporter's Name and Address: Wayne Brothers b. Phone: c. Driver Name Print . Signature e. Data III. DESTINATIO fGeneratnr pmmnlete Illac and es mation Site completes Illd-al a. Disposal Facility and Site Address: c. US EPA Number d. Discrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concord, NC 28027 b. Phone: 704-782-2004 1 herby certify that the a a ametl materiel has been accetad and t t e best ofmy knowledge the foren me is tme an ex le. e. Name of Authorzed A enl Print f. SI nature . Dare IV. ASBESTOS (Generfitor completes IVa-f and Ope complete IVg-i) a. Operators Name and Address. b. Phone: C. Responsible Agency Name and Address: d. Phone: a. Special Handling Instructions and Additional Information: f. 0 Friable M Non -Friable 0 Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that me contents of fins; consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled and are in all respects in proper condition for transport by highway according to applicable intematlonal and national novernmental regulations. . Operators Name and Tkle Print h. Signet 1. Date 'Operator refers to the company which owns, leases, operates, controls, or supervises the facility being demolished or renovated. or the tlamolition or renovation operation or be REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. If waste is asbestos waste, complete Sections I, II, III and IV If waste is NOT asbestos waste, complete Sections I, II and III GENERATOR (Generator wmoletes Ie-rl I f / l"(2 llnr/ 1 a. Generators US EPA ID Number b. Manifest Document Number C. Page 1 of d. Generators Name and Location : e. Ganerelols Melling Address: rCounty 65 Chu 85 Church S Concord, NC 28025 g. Phone: I. Phone: If owner of the generating facility differs from the generator, provide: It. Owners Name: I. Owner's Phone No.: j. Waste Profile # k. Ezp. Date I. Waste Shipping Name and In. Containers n. Total o. Unit DescriDescriptionNo. Ouanti WWoI T 5010 20 12767 soil BILLTO: Wayne Brothels 11700 GENERATOR'S CERTIFICATION: I hereby certify that the above named malarial ts not a hazaroous waste as definetl by 40 CFR 261 or any applicable state law, has been properly dasctlbed, classed and packaged, and is in proper contlition kr Imnsport hou" accortling to applicable regulations; AND, ff this waste Is a treatment rasitlue o/ a p viously restrlcted hazaroous weal. subject to the LarM Disposal Reatdctions. cerity antl warrant that the waste has been treated' awomence with .1s mants of 40 CFR 268 and is no n er a hazardo a waste as definetl b 40 CFR 261. narator Authorized A am a Print . S' nature r. Data n lvcuaos- .s wmpmuee is-o gnu I ransponler wmpieres IIC-e) e. Transporters Name antl Address: Wayne Brothers b. Phone: c. Driver Neme (Print1 . ti i a d blumalum qy7"4 I e Dale III. nESTINATInM K]non M, r..,.., 1-.e ale , -., a. Disposal Facility and Site Atltlress: CMS Landfill e. US EPA Number d. Disuapency Indication Spare: 5105 Morehead Rd Concob, NC 28027 b. Phone: 704-782-2004 I herby cerfily that the above named material has been accepted and t t beat of my knowled a the foreclum is true and am to. e. Name of Authorizetl nt Fmnt I. Signature . Data IV. ASBESTOS (Q2ene or completes IVa-f and Operator mDlete IVa-i) a. Operators Name and Addre. b. Phone: c. Responsible Agency Name and Address- d. Phone: e. Special Handling InsWctions and Additional IMormation: f. Friable Non -Friable Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: 1 hereby declare that the contents of this consignment are fully and accurately dascribatl above by proper shipping name and ere classilled, parked, marked and labeled and are In all respects in proper contlition fortrensportby highway accortling to applicable International and national flo,emersuntal regulations. . O rators Name and True PBM h. SI nature i. Date 'Operator refer to the company which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or the demolition or renovation operation or both REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. If waste Is asbestos waste, Complete Sections I, 11, III and IV If waste is NOT asbestos waste, complete Sections I, II and III J� I. GENERATOR Iromarafnr rmm�lmec 1-1 I / /Q�i/1.pq ) a. Generators US EPA ID Number b. Manifest Document Number rv— C. Page 1 of tl. Generators Name and Location: e. Generators Meiling Address: rCounty 65 Chu 65 Church S Concord, NC 28025 g. Phone: f. Phone: If owner of the generating facility ddlers from the generator, provide: h. Owners Name: I. Owner's Phone No.: j. Waste Profile # k. Exp. Dale I. Waste Shipping Name and m. Containers n. Total o. Unit Descri Ion OuaM' WWoI Nc. T 5010 0012767 soil BILL TO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: I hereby tangy that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been property described, clasaified and packaged, and is in proper condition for transportation according to applicable regulations: AND, If this waste is a treatm nt residue of a previously restrkted hazardous waste subject to the Land Disposal Restrictions. I cedgy and warrant that the waste has been treated in a rdance with there uire nts of 40 CFR 268 and is no to r a It 9v waste as defined by 40 CFR 261. J . Ga Authormed en Nama Print . Sipstum I I. Date n 1��..C101V1 tAlnl Initls nE-U 0na I ranspor[er complems nc-2J a. Transporters Nama and Atldpey , . ,r C,/ Wayne Brothers b. Phone: V c. Driver Name PrintI d. Si nature e. Date III. DESTINATION Ir:nnamtnr romnl>a Ill.— —A a. Disposal Facility and Site Address- CMS Landfill C. US EPA Number d. Discrepancy Indication Space: 5105 Morehead Rd Concord, NC 28027 b. Phone: 704-782-2004 1 neMY many that the above material has been aae led and to Illue.hast of m m.led a the fomg[Ing is anK accu te. e. Name of Authorized A an not I. S re natuate IV. AeitlCD 105 tuanengtor Commletee IVA-f and OnwratnNMmnlBfo lVn-il a. Operators Name and Addres : to. Phone: C. Responsible Agency Name and Address: d. Phone: a. Special Handling Instructions and Additional Information: f. 0 Friable 0 Non -Friable Q Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the Contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled and are in all respects in proper condition for transport by highway according to applicable international and national governmental regulations. . Operators Name and Title Print h. Skinaturre 1. Date 'Operator Were to the Company which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or the demoldion or renovation operation or both ,$ REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. It waste is asbestos waste, complete Sections I, II, III and IV If waste is NOT asbestos waste, complete Sections I, II and III NUM yi GENERATOR (Generator completes la-r) ' / UM I115 a. Generators US EPA ID Number b. Manifest Document Number Page 1 of F. 1 d. Generators Name and Location: a. Generators Meiling Address: Cabaoue County 65 Church St. S Concord, NC 28025 g. Phone: f. Phone: If owner of the generating facility tl8f ns from the generator, provide: In Owners Name: i. Owners Phone No.: j. Waste Profile 8 k. Exp. Date I. Waste Shipping Name and m. Containers n. Total o. Unit Description No. T Quantity WWoI 5010 20 12767 soil 1 BILLTO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: I hereby badity, that the above named materiel is not a hazardous waste as defined by 40 CFR 261 or any applicable state lax, has been property described, classified and packaged, and Is In proper condition for transportation according to applicable regulations; AND, 'dthis waste Is a treatment residue of a previou resmated hazardous waste subject to the Land Disposal Restrictions. I certify and warrant that me waste has been treated Ina ordanco with me remenLs of 40 CFR 268 and Is no I er a hazareou defined b 40 CFR 287. IV?1 2 or Aut prizeuJ Agtril Name not . SI nature r. Date H. TRANSPORTER (Generator completes Ila-b and Transporter completes IIc e) a. Transporters Name and Address: Wayne Brothers b. P ne: c. river Nam Pdnt 41 d. S nature e. Date III. DESTINATION rr pnp.mtnr emmnlete Illa-c and Destination Site completes llld-o) a. Disposal Facility and Site Address: G. US EPA Number d. Discrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concord, NC 28027 b. Phone: 704-782-20N I herby certify that the ab a amed material has been acce letl and to a best of m knowled a the fore oIn is e a rota. e. Noma of Authorized ant do f. SI nature I I.Date IV. ASBESTOS (Generator completes IVa-f and OpEratoy complete Wg-i) a. Operators Name and AdTqi.E b. Phone: c. Responsible Agency Name and Address: d. Phone: e. Special Handling Insinuations and Additional Information: f. El Friable 0 Non -Friable Ej Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that me contents of this consignment ere fully and.ccurately described above by proper shipping name and are classified, packed, marked and labeled and are In all respects in proper condition for transport by highway awarding to applicable international and national novernarrental Mutations. . O rotors Name and Idle Print It. S' nature L Data 'Operator refers to the company which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or the demolition or renovation 222ration or both REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST ,waste is asbestos waste, complete Sectlons I, II, III ant IV e01 waste is NOT asbestos waste, complete Sections I, II and III GENERATOR (Generator completes la-r) a. Gen ratoes US EPA ID Number b. Manifest Document Number c. Page 1 of d. Generator's Name and Location: e. Generator's Melling Address: Cabareas County 65 Church St. S Conceal NC 28025 g. Phone: I. Pha If owngr of the generating facility differs from the generator, provide - In. Owners Nam.: i. Owners Phone No.: j. Waste Profile # k. Fxp. Date I. Waste Shipping Name and M. Containers n. Total a. Unit No. I Typa Description Dumb WW01 5010 20 12767 soil l `T) BILL TO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable state law. has been property described, classified and packaged, and is in proper condition for transportation eccordlng to applicable regulations; AND, if this waste Is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warrant that the waste has x been treated In ordance with uirements of 4no 0 CFR 268 and Is Ion er a h ous waste as defined b 40 CFR 6.1. t 9- P. Generator Authorized Agent Na Print . S nature IL 1 TRANSPORTER (Generator completes Ila-b and Transporter completes lie-e) a. Transporters Wayne b. Maker Name and Address: Brothers c. Driver Name Ptlnt d. e. Date �L Ill. DESTINATION (Gi6nerator complete Illa-c and Destination Site completes Illd-g) a. Disposal Facility and Site Address: c. US EPA Number d. Discrepancy Indication Space: CMS Landfill 5105 orehead Rd Conco ,NC28027 b. Pho a: 704482-2004 I heO ced named material has been acca2rnd to the best of my knowledge the foreq ing is 'I e antl ac orate Me I 71, e. Name of uthoriz ant Print) lure I.Date IV. ASBESTOS (Generator completes IVa-f and Operator complete IVg-1) a. Operator's Name and Address: b. Phone: c. Responsible Agency Name and Address: d. Phone: e. Speclal Handling Instruction and Additional Information: LEI Friable ® Non -Friable Q Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the contents of mis consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled and are in all respects In proper condition for transport by highway according to applicable international and national governmental regulations. . O rotor's Name and Title Print h. Signat 'Operator refers to me company which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or the demol8lon or renovation operation or both REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. K 1 If waste is asbestos waste, complete Sections I, II, III and IV �tjJKt. If waste is NOT asbestos waste, complete Sections I, II and III I I/ 77 /// CG 70R Generator completes la-r U' o a. Generator's US EPA ID Number b. Manifest Document Number c. Page 1 of 1 d. Generator's Name and Location: e. Generators Mailing Address: Cabartus County 65 Church St. S Concord, NC 28025 g. Phone: I. Phone: If owner of the generating facility differs from the generator, provide: h. Owners Name: i. Owners Phone No.: j. Waste Profile M k. Esp. Date I. Waste Shipping Name and m. Comainers n. Total o. Unit Description No. I T I Quantity WWoI 5010 20 12767 soil .g BILL TO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a huamaus waste as defined by 40 CFR 261 or any applicable state law, has been property described, classified and packaged, and is in proper condition for transportation according to applicable regulations: AND, If the waste Is a treatment residue of a previously restricted hazaroous waste subject to the Land Deposal Restrictions. I certify and warrant that the waste has been treated in acc rdance wRh the ulmments of 40 CFR 268 and a no Ion us waste as definetl b 40 CFR 261, t . Genera or Autho ed ant Name Print .Sin re r. Date tl. 1KAN51-VR1 tli (Generatorcompletes im-D and I ransportercompletes Uc-e) a. Transporters Name and Address: Wayne Brothers b. P _*J. cot Vj ktz to Z.D c. Driver Name PrintT I d. Si na e. Date III. DESTINATION (Generator comolete Ills-c and Destination Site completes Illd-01 a. Disposal Facility and Site Address: C. US EPA Number d. Discrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concord, NC 28027 b. Phone: 704-782-2004 I herby card t the above named material has been accer and to the bast of my knowled a the fo of b t e arM a la. e. Name of'Authorized All Print f. SI nature .Data IV. ASBESTOS (Generator completes IVa-f and Operator complete Wg-i) a. Operators Name and Address: It. Phone: C. Responsible Agency Name and Address: d. Phone: a. Sp cial Handling Instructions and Additional Information: f. riabla 0 Non-Fdable 0 Both %Friable %Non -Friable OPE1 ATOR'S CERTIFICATION: I hereby declare that me contents of the consignment are fully and accurately described above by proper shipping name and a a classified, packed, marked and labeled and are in all aspects in proper Condition for transport by highway according to applicable International and ng!lkar at governmental re ulations. . Op nature Name and THE Print h. Signature I. Date 'Opatator refers to the Company which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or the demolition or renovation a ration ar both REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. /D If waste is asbestos waste, complete Sections I, II, III and IV If waste is NOT asbestos waste, complete Sections I, II and III Iy�� UENERATOR (Generator completes la-r) II nn 9\r-y a. Generators US EPA ID Number b. Manifest Document Number C. Page 1 of 1 d. Generators Name and Location: a. Generators Mailing Address: Cabanus County 65 Church St. S Concord, NC 28025 g. Phone: f. Phone: If owner of the generating facility differs from the generator, provide: h. Owners Name: i. Owners Phone No.: j. Waste Profile # k. Exp. Date I. Waste Shipping Name and m. Contalne rs n. Total o. Unit Description No. T e Quantilb, WWaI 5010 20 12767 stillLq V 1 I BILLTO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: 1 hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is In proper condition for transportation according to applicable regulations; AND. If this waste is a treatment residue of a previously restricted hazardous waste object to the Land Disposal Restrictions. I cortgy and warrant that the waste has been treated in accordance w8h require, of 40 CFR 268 aM o Ion g a hour us waste as defined b 40 CFR 261. 1 c:f . Generator Authorized enl Na Print . Si ne re r. D a 11. 1 rwNDrUKI etc tl enerator completes na-D anti I transporter completes lic-e) a. Transporters Name and Address: Wayne Brothers b. Phone: 1 I-PIGIAsiV' rx�l c. Driver Name print d. Sighatum e. Date III. DESTINATION (Generator complete Illa-c and Destination Site mmnlntre Illri,1 a. Disposal Facility and Site Address: e. US EPA Number tl. Discrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concord, NC 28027 b. Phone: 704-782-2004 herb ced' mat me above named material has been acre led tl to the best of my knowledt,a the foregoing is t e and accumte e. Name rf Author¢ enl Print f. Si nature .Date IV. ASBESTOS (Generator completes IVa-f and Operator complete IVg-1) a. Operators Name and Address: b. Phone: c. Responsible Agency Name and Address' d. Phone: e. Special Handling Instructions and Additional Information: f. Friable ® Non -Friable El Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately describetl above by proper shipping name and are classed, pecked, marked and labeled and are in all respects in proper condition for transport by highway according to applicable international and national governmental regulations. . Operators Name and Ti Is Print h. SI nature 1. Date *Operator refers to the company which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or the demolition or renovation operation or both REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST SERVICES, INC. _ a L/Oq If waste is asbestos waste, complete Sections I, II, III and IV 1 I'w If waste is Q asbestos waste, complete Sections I, II and III lJ LGXENERATOR Generator completes IS I o gt a. Generator's US EPA ID Number mber b. Manifest Docum!e.Ge.e c. Page 1 of J. Generators Name and Location: ators Mailing Atltlrass: Cabamrs65Churc County 65 Church S Concord. NC 28025 C ne: f. Phone: if owner of the generating facility di6are irom the generator, provide: h. Owner's Name: I. Owner's Phone No.: J. Waste Profile # k. EXP. Data I. Waste Shipping Name and m. Comamers I. Total o. Unit 50102012767 Descifoon soil No. T Quanti Wt/vol U q BILLTO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: I hereby certify that the above named material h not a hazareoue waste as defined by 40 CFR 261 or any applicable state law, has been property described, classified and packaged, and Is in proper condition for transportation according to applicable regulations; AND, If this waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I cadify and warrant that the waste has been Treated in omance wdh the irements of 40 CFR 266 ant is no Ion era azanfous waste as defined b 40 CFR 261. . Gen Or Authorized Anent Name Pant . SI nature F. Date II. TRANSPORTER (Generator completes Ila-b and Transporter completes lic-e) a. Transposers Name antl Address: Wayne Brothers b. Phone: c. DrNer Name Pdnt r d. Si nature e. wereIII IV M. ULST nvn r iUN tuenera[of Com0 erce Ilia-c and uestmation Site nmmnleteS IIIH-1 a. Disposal Facility and Site Address: C. US EPA Number 0. Discrepancy Indlcation Space: CMS Landfill 5105 Morehead Rd Concord. NC 28027 b. Phone: 704-782-2004 1 hemby canny igig the above named material has been a tad antl to the best of my knoWetl a the foregoing Is time and accurat . ' e. Noma of Au or¢ad t Print f. Si nature .Dale o 1 w. I Vmnelalla Completes iva-r ana uperator complete lvg-i) a. Operelor's Name and Adtlress: b. Phone: c. Responsible Agency Name and Address: d. Phone: e. Special Handling Instmctions and Additional Infonnalion: f. Friable Non -Friable ❑Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the contents of uns consignment are WIty and accurately described above by proper shipping name and are classified. packed, marked and labeled and are in all respects In proper condition for transport by highway according to applcable intematlonal and national governmental regulations. . O ramr's Name and I me Print h. Si nature i. Data 'Operator refers to the company which owns, leases, operates, controls, or supervises the facility being de111016hed or renovated, or the demoldion or renovation operation or both REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST pErtylpFS. INC. If waste is asbestos waste, complete Sections I, II, III and IV If waste Is NOT asbestos waste, complete Sections I, II and III � � l �� I� GENERATOR (Generator completes B-r) /4/,�,. a. Generators US EPA ID Number b. Manifest Document Number c. Page 1 of 1 d. Generators Name and Location: e. Generator's Mailing Address: Cebam. s County 65 Church St. S Concord, NC 28025 g. Phone: f. Phone: If owner of the generating facility di firs from the generator, provide: If. Owners Name: I. Owners Phone No.: j. Waste Profile IF k. Exp. Data I. Waste Shipping Name and m. Containers n. Total o. Unit Description No. T e Quantity NNVoI 5010 20 12767 soil O BILL TO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged. and is in proper condition for transportation according to applicable regulations; AND, If this waste Is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I curably and warrant that the waste has been treated In aaordance with the 4guirermentir of 40 CFR 268 and is no longer a hazardous waste as defined b 40 CFR 261. f . Genera uthorized Agent Name Int . SI n re r. Date If. I K NSYVKI GK tenerator completes Ile-D ano I ransporter completes UcC e) a. Transporters Name and Address: Wayne Brothers b. Phone: c. Dnver Name Print tl. S nature e. Date III. DESTINATION (Generator complete Illac and anon Site completes Ilid-a) a. Disposal Facility and Site Address: c. US EPA Number d. Discrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concord, NC 28027 b. Phone: 704-782-2004 1 herby certify the the above named material has been acre and to me best of my knowled a the fonall[ing is t e and a re e. Name of Authitzed Agen"Print)f. SI nature .Data IV. ASBESTOS (Generator completes IVa-f and Operator complete IVg-i) a. Operators Name and Address: b. Phone: C. Responsible Agency Name and Address: d. Phone: e. Special Handling Instructions and Additional Information: f. El Friable R Non -Friable ❑ Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that me contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled and are In all respects In proper condition for transport by highway according to applicable international and national governmental sgulations. . Operators Name and Title Print If. Si nature I I. Date 'Operator refers to the company which owns, leases, operates, controls, or supervises the Wilily being demolished or renovated, or the demolition or renovation operation or both REPUBLIC NON -HAZARDOUS SPECIAL_ WASTE & ASBESTOS MANIFEST - SERVICES, INC. Cp qLPwaste Is asbestos waste, complete Sections I, II, III and IV If waste is NOT asbestos waste, complete Sections I, II and III GENERATOR (Generator completes la-r) zu t I '/V• o -) a. Generators US EPA ID Number b. Manifest Document Number c. Page 1 of 1 d. Generators Name and Location: e. Generator's Mailing Address: Cabamus County 65 Church St. S Concord, NO 28025 g. Phone: f. Phone: If owner of the generating facility differs from the generator, provide: In. Owner's Name: I. Owners Phone No.: j. Waste Profile # k. Exp. Date I. Waste Shipping Name and m. Containers n. Total o. Unit Description No. TV. Quantity WWoI 5010 2012767 soil ^/ lq_ BILL TO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: I hereby cer ify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is In proper condition for transportation according to applicable regulations; AND, 0 this waste is a treatment residue of a previously restricted hi urdous waste subjectto the Land Disposal Restrictions. I certify and warrant that the waste has been treated In accordance with th muftements of 40 CFR 268 and is no Ion era haurdous waste as defined b 40 CFR 2611. . Generator Authorizer! Agent Name Pnnt . SI nature r. Date n lvcucmwi w...... nc-u orlu nanayuuern crnnpieres lu; e) a. Transporters Name and Address: Wayne Brothers hPhojel c. Driver a e Pnm d. e. Date III. DESTINATION (Generak6r cam fete Illa-c and Destination Site completes Illd-0) a. Disposal Facility and Site Add C. US EPA Number d. Discrepancy IlMkatbn Space: CMS Landfill 5105 Morehead Rd Concord, NC 28027 b. Phone: 704-782-2004 1 herby certify that a above named material has been accept a to the best ofmy knowledge the forregoinq is hrg antlTIM-- ldri,eu AgentErint)f. i nature .Dale IV. ASBESTOS (Generator completes IVa-f and Operator complete IVe-i) a. Operators Name and Address: b. Phone: C. Responsible Agency Name and Address: d. Phone: e. Special Handling Instructions and Additional IMormatton: I.D Friable 0 Non-Fdable ❑ Both %Friable %Non-Fdable OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled and are In all respects In proper condition for transport by highway according to applicable international and national governmental regulations. . Operatoes Name and TRIG Print h. Signature 1 I. Date 'Operator refers to the company which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or the demolition or renovation operation or both REPUBLIC NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST /SER'ICE..9t C. l (y1`/%] ( Q 1 _��J(�(/V) If waste is asbestos waste, complete Sections 1, II, III and IV I t // p ! 2— waste is NOT asbestos waste, complete Sections I, II and III /�"•�,�'1��1r- v-C GENERATOR (Generator completes la-r) I 1 \Nyll//Y6/ a. Generators US EPA ID Number b. Manifest Document Number c. Page 1 of 1 tl. Ganerelors Name and Loeallon: e. Generators Mailing Address. Cabanus County 65 Church St. S Concord, NC 28025 g. Phone: f. Phona: If owner of the generating facility differs from the generator, provide: h. Owners Name: 1. Owners Phone No.: J. Waste Profile M k. Exp. Date I. Waste Shipping Name and it Containers n. Total o. Unit Description No. T QuantityWWoI 5010 soil 19, j � I BILL TO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: I hereby coddy that the above named material is not a hazardous waste as definetl by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is in proper condition for transpor ezion according to applicable regulations; AND, if this waste Is a tree ment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warrant that the waste has been treated I accordance with the re uirements of 40 CFR 268 and is no longer a h mous waste as deffnetl by 40 CFR 261. c -O .Gene or Aumor¢atl ant Na ePrint .Si re rDat® . IovuGI MWI b II IVIMLUJ na-u GUV I IGnbj)VILWI UUMPIUW5 nc$j Wayne Brothers Name and Address n ^ ,n I,1 � �v � � Wayne Brothers f/�I "l.a� b. Phone: c. Driver Nama Print d. S nature e. Date IIL nFRTINATION rr:encrnlnr a. Disposal Facility, and Sile Address: c. US EPA Number d. Discrepancy Intliration Space: CMS Landfill 5105 Morehead Rd Concord, NC 28027 b. Phone: 704-782-2004 I nerov cemplyAnatme above n d matel has been acts tad and to the bast m knowled a the fo pin is hue end aaurete. e. Name uthodz enl tlnl f. SI, 1 g. Dale IV. ASBESTOS (Generator completes IVa-f and Operator complete IVc-i) a. Operators Name and Address: b. Phone: nsible Agency Name and Address: FdPhnoe: e. Special Handling Inslmctions and Additional Information: f.El Friable 0 Non-Fdable Q Both %Friable %Non -Friable OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and ere classified, packed, marked and labeled and are in all respects in proper condition for transport by highway according to applicable international and national governmental regulations. . operators Name and Tttle Print In. SI nature I I. Date 'Operator refers to the company which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or the demolition or renovation operation or both a REPUBLIC NON -HAZARDOUS SFECIAL WASTE & ASBESTOS MANIFEST //✓L If waste Is asbestos waste, complete Sections I, II, III and IV ^ n DI m If waste is NOT asbestos waste, complete Sections I, II and III �� `. I ' GENERATOR (Generator comoletes la-r) I`l1� ) (6 a. Generators US EPA ID Number b. Manifest Document Number C. Page 1 of 1 d. Generators Name and Location: e. Generators Mailing Address: Cabamis County 65 Church St. S Concord, NC 28025 g. Phone: J. Phone: If owner of the generating facility differs from the generator, provide: h. Owner's Name: I. Owners Phone No.: j. Waste Profile # k. Exp. Date I. Waste Shipping Name and m. Containers n. Total o. Unit Description No. T Ouen WlIVOi 5010 2012767 soil F\ J SILLTO: Wayne Brothers 11700 GENERATOR'S CERTIFICATION: I hereby certHy that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste Is a treatment residue of a previously restricted hazardous waste subj to the Land Disposal Restrictions. I candy and warrant that the waste has been!! In aordance with iha uirements of 40 CFR 288 antl is no I n er aste as canned b 40 CFR 261. 'a 1 -cue . Genera orAuthonzetl Agent Ned rint . Signature I I. Diffe It. TRANSPORTER (Generator comoletes Ila-b and Transporter comoletes Ilc-e) Ill. DESTINATION (Generator complete Illac and Destination Site completes llld-g) a. Disposal Facility and Site Address: C. US EPA Number d. Discrepancy Indication Space: CMS Landfill 5105 Morehead Rd Concord, NC 28027 b. Phone: 7044824004 I herb certi ih t th above named material has been acca t ntl to the best of knowledge the to monola a and ccu 1 , LID e. Nema of ihanze Agerj (PI iliplature Q. Data IV. ASBESTOS (benerator completes IVa-f and Operator complete IVg-i) e. Operators Name and Address: b. Phone: C. Responsible Agency Name and Address- d. Phone: e. Special Handling Instructions and AtldPoonal Information: f.❑ Friable 0 Non -Friable El Both %Friable %Non-Fdable OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classHled, packed, marked and labeled and are in all respects In proper condition for transport by highway according to applicable international and national governmental regulations. Q. Operators Name and Tithe Print h. SI nature 1. Data -Operator refers to the company which owns, leases, operates, controls, or supervises the mclury being demolished or renovated, of the demolibon or renovalion operation or both UST Closure Report 61 Union St. South, Concord, NC APPENDIX I & J CHAIN OF CUSTODY SUMMIT Project No. 4314.E0006 November 13, 2020 And ANALYTICAL RESULTS D:A!Michae1!V!SUMMIT!\4314 - Trifecta Services Company\4314.E0006 - 77 Union St. S Concord NC\UST\report files\Appendix T COC.docx 0 aceAnalytical Report of Analysis SUMMIT Engineering, Laboratory & Testing, P.C. 3575 Centre Circle Fort Mill, SC 28715 Attention: Michael Zavislak Project Name: Cabarrus County Court House Lot Number:V116120 Date Completed:09/29/2020 09/29/2020 1:45 PM Approved and released by: Project Manager II: Lucas Odom pCCgF� 24r�A SOA ANSI National Accreditation Board A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page 1 of 87 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative SUMMIT Engineering, Laboratory & Testing, P.C. Lot Number: V116120 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Pace policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. SVOCs by GC/MS The following sample was diluted due to appearance or color: V116120-005. The LOQ has been elevated to reflect the dilution. Sample -006 was diluted due to large detections of target compounds causing multiple surrogates to recover outside of method criteria. No corrective action is required as it is known that dilutions of 5X and greater may impact surrogate recoveries. Due to the large number of spiked analytes, there is a high probability that one or more analytes will recover outside acceptance limits. The laboratory's SOP allows for 10% of analytes to recover marginally outside criteria. The following analyte recovered marginally outside LCS criteria: 4-Chloroaniline. Data has been reported. VOCs by GC/MS Due to the large number of spiked analytes, there is a high probability that one or more analytes will recover outside acceptance limits. The laboratory's SOP allows for 10% of analytes to recover marginally outside criteria. The following analytes recovered marginally outside LCS/LCSD criteria: 2-hexanone. The laboratory control sample (LCS) for analytical batch 67242 exceeded acceptance criteria for 1,2,4- Trichlorobenzene. This analyte is biased high but is not detected in the samples affected. Surrogate recovery for the following samplee was outside of acceptance limits: V116120-006. This sample was analyzed at a high dilution; therefore, re -extraction and/or re -analysis was not performed. VPH Surrogate recovery for the following sample was outside control limits: V116120-006. Evidence of matrix interference is present; therefore, re -extraction and/or re -analysis was not performed. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 2 of 87 PACE ANALYTICAL SERVICES, LLC Sample Summary SUMMIT Engineering, Laboratory & Testing, P.C. Lot Number: V116120 Sample Number Sample ID Matrix Date Sampled Date Received 001 3-1 NORTH Solid 09/15/2020 1300 09/16/2020 002 S-2 BOTTOM Solid 09/15/2020 1305 09/16/2020 003 S-3 SOUTH Solid 09/15/2020 1310 09/16/2020 004 S-4 EAST Solid 09/15/2020 1315 09/16/2020 005 S-5 WEST Solid 09/15/2020 1320 09/16/2020 006 S-6 RELEASE Solid 09/15/2020 1200 09/16/2020 007 S-7 STOCKPILE Solid 09/15/2020 1330 09/16/2020 (7 samples) Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 87 PACE ANALYTICAL SERVICES, LLC Detection Summary SUMMIT Engineering, Laboratory & Testing, P.C. Lot Number: V116120 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 S-1 NORTH Solid Di-n-butyl phthalate 8270E 7.9 J ug/kg 8 002 S-2 BOTTOM Solid Caprolactam 8270E 11 J ug/kg 12 002 S-2 BOTTOM Solid Di-n-butyl phthalate 8270E 6.7 J ug/kg 13 003 S-3 SOUTH Solid Acetone 8260D 11 J ug/kg 16 003 S-3 SOUTH Solid Methyl acetate 8260D 1.6 J ug/kg 16 003 S-3 SOUTH Solid Xylenes (total) 8260D 5.1 J ug/kg 17 003 S-3 SOUTH Solid Di-n-butyl phthalate 8270E 7.7 J ug/kg 18 004 S-4 EAST Solid Caprolactam 8270E 16 J ug/kg 22 006 S-6 RELEASE Solid Ethylbenzene 8260D 9600 ug/kg 31 006 S-6 RELEASE Solid Isopropylbenzene 8260D 4800 J ug/kg 31 006 S-6 RELEASE Solid Methylcyclohexane 8260D 5400 J ug/kg 31 006 S-6 RELEASE Solid Xylenes (total) 8260D 120000 ug/kg 32 006 S-6 RELEASE Solid 2-Methylnaphthalene 8270E 6000 ug/kg 33 006 S-6 RELEASE Solid Naphthalene 8270E 5700 ug/kg 33 006 S-6 RELEASE Solid C11 - C22 Aromatics MADEP-EPH- 89 mg/kg 34 006 S-6 RELEASE Solid C9 - C18 Aliphatics MADEP-EPH- 200 mg/kg 34 006 S-6 RELEASE Solid C19 - C36 Aliphatics MADEP-EPH- 46 mg/kg 34 006 S-6 RELEASE Solid C5 - C8 Aliphatics MADEP-VPH- 990 mg/kg 35 006 S-6 RELEASE Solid C9 - C12 Aliphatics MADEP-VPH- 2400 mg/kg 35 006 S-6 RELEASE Solid C9 - C10 Aromatics MADEP-VPH- 1500 mg/kg 35 007 S-7 STOCKPILE Solid Xylenes (total) 8260D 990 ug/kg 37 007 S-7 STOCKPILE Solid 2-Methylnaphthalene 8270E 350 ug/kg 38 007 S-7 STOCKPILE Solid Naphthalene 8270E 290 ug/kg 38 007 S-7 STOCKPILE Solid TPH-GRO 8015C 140000 ug/kg 39 (24 detections) Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-001 Description: S-1 NORTH Matrix: Solid Date Sampled:09/15/2020 1300 % Solids: 81.8 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 09/18/20201421 JM1 67142 5.88 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D ND 21 8.3 ug/kg Benzene 71-43-2 8260D ND 5.2 2.1 ug/kg Bromodichloromethane 75-27-4 8260D ND 5.2 2.1 ug/kg Bromoform 75-25-2 8260D ND 5.2 2.1 ug/kg Bromomethane (Methyl bromide) 74-83-9 8260D ND 5.2 3.1 ug/kg 2-Butanone (MEK) 78-93-3 8260D ND 21 4.2 ug/kg Carbon disulfide 75-15-0 8260D ND 5.2 2.1 ug/kg Carbon tetrachloride 56-23-5 8260D ND 5.2 2.1 ug/kg Chlorobenzene 108-90-7 8260D ND 5.2 2.1 ug/kg Chloroethane 75-00-3 8260D ND 5.2 2.1 ug/kg Chloroform 67-66-3 8260D ND 5.2 2.1 ug/kg Chloromethane (Methyl chloride) 74-87-3 8260D ND 5.2 3.1 ug/kg Cyclohexane 110-82-7 8260D ND 5.2 2.1 ug/kg 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D ND 5.2 2.1 ug/kg Dibromochloromethane 124-48-1 8260D ND 5.2 2.1 ug/kg 1,2-Dibromoethane (EDB) 106-93-4 8260D ND 5.2 2.1 ug/kg 1,2-Dichlorobenzene 95-50-1 8260D ND 5.2 2.1 ug/kg 1,3-Dichlorobenzene 541-73-1 8260D ND 5.2 2.1 ug/kg 1,4-Dichlorobenzene 106-46-7 8260D ND 5.2 2.1 ug/kg Dichlorodifluoromethane 75-71-8 8260D ND 5.2 3.1 ug/kg 1,1-Dichloroethane 75-34-3 8260D ND 5.2 2.1 ug/kg 1,2-Dichloroethane 107-06-2 8260D ND 5.2 2.1 ug/kg 1,1-Dichloroethene 75-35-4 8260D ND 5.2 2.1 ug/kg cis- 1,2-Dichloroethene 156-59-2 8260D ND 5.2 2.1 ug/kg trans-1,2-Dichloroethene 156-60-5 8260D ND 5.2 2.1 ug/kg 1,2-Dichloropropane 78-87-5 8260D ND 5.2 2.1 ug/kg cis- 1,3-Dichloropropene 10061-01-5 8260D ND 5.2 2.1 ug/kg trans- 1,3-Dichloropropene 10061-02-6 8260D ND 5.2 2.1 ug/kg Ethylbenzene 100-41-4 8260D ND 5.2 2.1 ug/kg 2-Hexanone 591-78-6 8260D ND 10 4.2 ug/kg Isopropylbenzene 98-82-8 8260D ND 5.2 2.1 ug/kg Methyl acetate 79-20-9 8260D ND 5.2 2.1 ug/kg Methyl tertiary butyl ether (MTBE) 1634-04-4 8260D ND 5.2 2.1 ug/kg 4-Methyl-2-pentanone 108-10-1 8260D ND 10 4.2 ug/kg Methylcyclohexane 108-87-2 8260D ND 5.2 2.1 ug/kg Methylene chloride 75-09-2 8260D ND 5.2 2.1 ug/kg Styrene 100-42-5 8260D ND 5.2 2.1 ug/kg 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 5.2 2.1 ug/kg Tetrachloroethene 127-18-4 8260D ND 5.2 2.1 ug/kg Toluene 108-88-3 8260D ND 5.2 2.1 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-001 Description: S-1 NORTH Matrix: Solid Date Sampled:09/15/2020 1300 % Solids: 81.8 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 09/18/20201421 JM1 67142 5.88 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 5.2 2.1 ug/kg 1 1,2,4-Trichlorobenzene 120-82-1 8260D ND 5.2 2.1 ug/kg 1 1,1,1-Trichloroethane 71-55-6 8260D ND 5.2 2.1 ug/kg 1 1,1,2-Trichloroethane 79-00-5 8260D ND 5.2 2.1 ug/kg 1 Trichloroethene 79-01-6 8260D ND 5.2 2.1 ug/kg 1 Trichlorofluoromethane 75-69-4 8260D ND 5.2 2.1 ug/kg 1 Vinyl chloride 75-01-4 8260D ND 5.2 3.1 ug/kg 1 Xylenes (total) 1330-20-7 8260D ND 10 4.2 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 108 47-138 1,2-Dichloroethane-d4 93 53-142 Toluene-d8 115 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1319 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 8270E ND 3.3 1.0 ug/kg 2 Acenaphthylene 208-96-8 8270E ND 3.3 1.2 ug/kg 2 Acetophenone 98-86-2 8270E ND 16 6.1 ug/kg 2 Anthracene 120-12-7 8270E ND 3.3 0.62 ug/kg 2 Atrazine 1912-24-9 8270E ND 16 6.1 ug/kg 2 Benzaldehyde 100-52-7 8270E ND 16 6.1 ug/kg 2 Benzo(a)anthracene 56-55-3 8270E ND 3.3 0.72 ug/kg 2 Benzo(a)pyrene 50-32-8 8270E ND 3.3 0.81 ug/kg 2 Benzo(b)fluoranthene 205-99-2 8270E ND 3.3 0.61 ug/kg 2 Benzo(g,h,i)perylene 191-24-2 8270E ND 3.3 0.79 ug/kg 2 Benzo(k)fluoranthene 207-08-9 8270E ND 3.3 0.59 ug/kg 2 1,1'-Biphenyl 92-52-4 8270E ND 16 6.1 ug/kg 2 4-Bromophenyl phenyl ether 101-55-3 8270E ND 16 6.1 ug/kg 2 Butyl benzyl phthalate 85-68-7 8270E ND 16 6.1 ug/kg 2 Caprolactam 105-60-2 8270E ND 16 6.1 ug/kg 2 Carbazole 86-74-8 8270E ND 16 6.1 ug/kg 2 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 16 6.1 ug/kg 2 4-Chloro-3-methyl phenol 59-50-7 8270E ND 16 6.1 ug/kg 2 4-Chloroaniline 106-47-8 8270E ND 16 6.1 ug/kg 2 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 16 6.1 ug/kg 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-001 Description: S-1 NORTH Matrix: Solid Date Sampled:09/15/2020 1300 % Solids: 81.8 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1319 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run bis(2-Chloroethyl)ether 111-44-4 8270E ND 16 6.1 ug/kg 2-Chloronaphthalene 91-58-7 8270E ND 16 6.1 ug/kg 2-Chlorophenol 95-57-8 8270E ND 16 6.1 ug/kg 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 16 6.1 ug/kg Chrysene 218-01-9 8270E ND 3.3 0.55 ug/kg Dibenzo(a,h)anthracene 53-70-3 8270E ND 3.3 0.62 ug/kg Dibenzofuran 132-64-9 8270E ND 16 6.1 ug/kg 3,3'-Dichlorobenzidine 91-94-1 8270E ND 16 6.1 ug/kg 2,4-Dichlorophenol 120-83-2 8270E ND 16 6.1 ug/kg Diethylphthalate 84-66-2 8270E ND 16 6.1 ug/kg Dimethyl phthalate 131-11-3 8270E ND 16 9.0 ug/kg 2,4-Dimethylphenol 105-67-9 8270E ND 16 6.1 ug/kg Di-n-butyl phthalate 84-74-2 8270E 7.9 J 16 6.1 ug/kg 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 82 31 ug/kg 2,4-Dinitrophenol 51-28-5 8270E ND 82 31 ug/kg 2,4-Dinitrotoluene 121-14-2 8270E ND 33 12 ug/kg 2,6-Dinitrotoluene 606-20-2 8270E ND 33 12 ug/kg Di-n-octylphthalate 117-84-0 8270E ND 16 6.1 ug/kg bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 82 31 ug/kg Fluoranthene 206-44-0 8270E ND 3.3 0.51 ug/kg Fluorene 86-73-7 8270E ND 3.3 0.70 ug/kg Hexachlorobenzene 118-74-1 8270E ND 16 6.1 ug/kg Hexachlorobutadiene 87-68-3 8270E ND 16 6.1 ug/kg Hexachlorocyclopentadiene 77-47-4 8270E ND 82 31 ug/kg Hexachloroethane 67-72-1 8270E ND 16 6.1 ug/kg Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 3.3 1.2 ug/kg Isophorone 78-59-1 8270E ND 16 6.1 ug/kg 2-Methylnaphthalene 91-57-6 8270E ND 3.3 1.2 ug/kg 2-Methylphenol 95-48-7 8270E ND 16 6.1 ug/kg 3+4-Methylphenol 106-44-5 8270E ND 33 12 ug/kg Naphthalene 91-20-3 8270E ND 3.3 1.2 ug/kg 2-Nitroaniline 88-74-4 8270E ND 33 12 ug/kg 3-Nitroaniline 99-09-2 8270E ND 33 12 ug/kg 4-Nitroaniline 100-01-6 8270E ND 33 12 ug/kg Nitrobenzene 98-95-3 8270E ND 16 6.1 ug/kg 2-Nitrophenol 88-75-5 8270E ND 33 12 ug/kg 4-Nitrophenol 100-02-7 8270E ND 82 31 ug/kg N-Nitrosodi-n-propylamine 621-64-7 8270E ND 16 6.1 ug/kg N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270E ND 16 6.1 ug/kg Pentachlorophenol 87-86-5 8270E ND 82 31 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-001 Description: S-1 NORTH Matrix: Solid Date Sampled:09/15/2020 1300 % Solids: 81.8 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1319 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Phenanthrene 85-01-8 8270E ND 3.3 0.88 ug/kg 2 Phenol 108-95-2 8270E ND 16 6.1 ug/kg 2 Pyrene 129-00-0 8270E ND 3.3 0.61 ug/kg 2 Pyridine 110-86-1 8270E ND 16 6.1 ug/kg 2 2,4,5-Trichlorophenol 95-95-4 8270E ND 16 6.1 ug/kg 2 2,4,6-Trichlorophenol 88-06-2 8270E ND 16 6.1 ug/kg 2 Run 2 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 59 33-102 2-Fluorophenol 50 35-115 Nitrobenzene-d5 66 22-109 Phenol-d5 61 33-122 Terphenyl-d14 68 41-120 2,4,6-Tribromophenol 53 30-117 MA EPH (aliphatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/28/2020 2259 JJG 09/21/2020 0856 68223 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C19 - C36 Aliphatics - Unfractionated MADEP-EPH-04 ND 12 12 mg/kg 1 C9 - C18 Aliphatics - Unfractionated MADEP-EPH-04 ND 12 12 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) - Unfractionated 94 40-140 MA EPH (aromatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/28/2020 2259 JJG 09/21/2020 0856 68230 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics - Unfractionated MADEP-EPH-04 ND 12 12 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) - Unfractionated 80 40-140 2-Fluorobiphenyl (fractionation 1) 100 40-140 2-Bromonaphthalene (fractionation 2) 102 40-140 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 8 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-001 Description: S-1 NORTH Matrix: Solid Date Sampled:09/15/2020 1300 % Solids: 81.8 09/17/2020 0057 Date Received:09/16/2020 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 09/19/20201950 STM 67245 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH-18- ND 5.1 1.0 mg/kg 1 C9 - C12 Aliphatics MADEP-VPH-18- ND 5.1 1.0 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 89 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 09/19/20201950 STM 67246 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH-18- ND 1.7 0.68 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 93 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 9 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-002 Description: S-2 BOTTOM Matrix: Solid Date Sampled:09/15/2020 1305 % Solids: 88.8 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 09/18/20201444 JM1 67142 5.04 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D ND 22 8.9 ug/kg Benzene 71-43-2 8260D ND 5.6 2.2 ug/kg Bromodichloromethane 75-27-4 8260D ND 5.6 2.2 ug/kg Bromoform 75-25-2 8260D ND 5.6 2.2 ug/kg Bromomethane (Methyl bromide) 74-83-9 8260D ND 5.6 3.4 ug/kg 2-Butanone (MEK) 78-93-3 8260D ND 22 4.5 ug/kg Carbon disulfide 75-15-0 8260D ND 5.6 2.2 ug/kg Carbon tetrachloride 56-23-5 8260D ND 5.6 2.2 ug/kg Chlorobenzene 108-90-7 8260D ND 5.6 2.2 ug/kg Chloroethane 75-00-3 8260D ND 5.6 2.2 ug/kg Chloroform 67-66-3 8260D ND 5.6 2.2 ug/kg Chloromethane (Methyl chloride) 74-87-3 8260D ND 5.6 3.4 ug/kg Cyclohexane 110-82-7 8260D ND 5.6 2.2 ug/kg 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D ND 5.6 2.2 ug/kg Dibromochloromethane 124-48-1 8260D ND 5.6 2.2 ug/kg 1,2-Dibromoethane (EDB) 106-93-4 8260D ND 5.6 2.2 ug/kg 1,2-Dichlorobenzene 95-50-1 8260D ND 5.6 2.2 ug/kg 1,3-Dichlorobenzene 541-73-1 8260D ND 5.6 2.2 ug/kg 1,4-Dichlorobenzene 106-46-7 8260D ND 5.6 2.2 ug/kg Dichlorodifluoromethane 75-71-8 8260D ND 5.6 3.4 ug/kg 1,1-Dichloroethane 75-34-3 8260D ND 5.6 2.2 ug/kg 1,2-Dichloroethane 107-06-2 8260D ND 5.6 2.2 ug/kg 1,1-Dichloroethene 75-35-4 8260D ND 5.6 2.2 ug/kg cis- 1,2-Dichloroethene 156-59-2 8260D ND 5.6 2.2 ug/kg trans-1,2-Dichloroethene 156-60-5 8260D ND 5.6 2.2 ug/kg 1,2-Dichloropropane 78-87-5 8260D ND 5.6 2.2 ug/kg cis- 1,3-Dichloropropene 10061-01-5 8260D ND 5.6 2.2 ug/kg trans- 1,3-Dichloropropene 10061-02-6 8260D ND 5.6 2.2 ug/kg Ethylbenzene 100-41-4 8260D ND 5.6 2.2 ug/kg 2-Hexanone 591-78-6 8260D ND 11 4.5 ug/kg Isopropylbenzene 98-82-8 8260D ND 5.6 2.2 ug/kg Methyl acetate 79-20-9 8260D ND 5.6 2.2 ug/kg Methyl tertiary butyl ether (MTBE) 1634-04-4 8260D ND 5.6 2.2 ug/kg 4-Methyl-2-pentanone 108-10-1 8260D ND 11 4.5 ug/kg Methylcyclohexane 108-87-2 8260D ND 5.6 2.2 ug/kg Methylene chloride 75-09-2 8260D ND 5.6 2.2 ug/kg Styrene 100-42-5 8260D ND 5.6 2.2 ug/kg 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 5.6 2.2 ug/kg Tetrachloroethene 127-18-4 8260D ND 5.6 2.2 ug/kg Toluene 108-88-3 8260D ND 5.6 2.2 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 10 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-002 Description: S-2 BOTTOM Matrix: Solid Date Sampled:09/15/2020 1305 % Solids: 88.8 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 09/18/20201444 JM1 67142 5.04 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 5.6 2.2 ug/kg 1 1,2,4-Trichlorobenzene 120-82-1 8260D ND 5.6 2.2 ug/kg 1 1,1,1-Trichloroethane 71-55-6 8260D ND 5.6 2.2 ug/kg 1 1,1,2-Trichloroethane 79-00-5 8260D ND 5.6 2.2 ug/kg 1 Trichloroethene 79-01-6 8260D ND 5.6 2.2 ug/kg 1 Trichlorofluoromethane 75-69-4 8260D ND 5.6 2.2 ug/kg 1 Vinyl chloride 75-01-4 8260D ND 5.6 3.4 ug/kg 1 Xylenes (total) 1330-20-7 8260D ND 11 4.5 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 108 47-138 1,2-Dichloroethane-d4 97 53-142 Toluene-d8 114 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1343 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 8270E ND 3.0 0.93 ug/kg 2 Acenaphthylene 208-96-8 8270E ND 3.0 1.1 ug/kg 2 Acetophenone 98-86-2 8270E ND 15 5.6 ug/kg 2 Anthracene 120-12-7 8270E ND 3.0 0.57 ug/kg 2 Atrazine 1912-24-9 8270E ND 15 5.6 ug/kg 2 Benzaldehyde 100-52-7 8270E ND 15 5.6 ug/kg 2 Benzo(a)anthracene 56-55-3 8270E ND 3.0 0.66 ug/kg 2 Benzo(a)pyrene 50-32-8 8270E ND 3.0 0.74 ug/kg 2 Benzo(b)fluoranthene 205-99-2 8270E ND 3.0 0.56 ug/kg 2 Benzo(g,h,i)perylene 191-24-2 8270E ND 3.0 0.73 ug/kg 2 Benzo(k)fluoranthene 207-08-9 8270E ND 3.0 0.54 ug/kg 2 1,1'-Biphenyl 92-52-4 8270E ND 15 5.6 ug/kg 2 4-Bromophenyl phenyl ether 101-55-3 8270E ND 15 5.6 ug/kg 2 Butyl benzyl phthalate 85-68-7 8270E ND 15 5.6 ug/kg 2 Caprolactam 105-60-2 8270E 11 J 15 5.6 ug/kg 2 Carbazole 86-74-8 8270E ND 15 5.6 ug/kg 2 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 15 5.6 ug/kg 2 4-Chloro-3-methyl phenol 59-50-7 8270E ND 15 5.6 ug/kg 2 4-Chloroaniline 106-47-8 8270E ND 15 5.6 ug/kg 2 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 15 5.6 ug/kg 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 11 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-002 Description: S-2 BOTTOM Matrix: Solid Date Sampled:09/15/2020 1305 % Solids: 88.8 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1343 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run bis(2-Chloroethyl)ether 111-44-4 8270E ND 15 5.6 ug/kg 2-Chloronaphthalene 91-58-7 8270E ND 15 5.6 ug/kg 2-Chlorophenol 95-57-8 8270E ND 15 5.6 ug/kg 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 15 5.6 ug/kg Chrysene 218-01-9 8270E ND 3.0 0.51 ug/kg Dibenzo(a,h)anthracene 53-70-3 8270E ND 3.0 0.57 ug/kg Dibenzofuran 132-64-9 8270E ND 15 5.6 ug/kg 3,3'-Dichlorobenzidine 91-94-1 8270E ND 15 5.6 ug/kg 2,4-Dichlorophenol 120-83-2 8270E ND 15 5.6 ug/kg Diethylphthalate 84-66-2 8270E ND 15 5.6 ug/kg Dimethyl phthalate 131-11-3 8270E ND 15 8.3 ug/kg 2,4-Dimethylphenol 105-67-9 8270E ND 15 5.6 ug/kg Di-n-butyl phthalate 84-74-2 8270E 6.7 J 15 5.6 ug/kg 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 75 28 ug/kg 2,4-Dinitrophenol 51-28-5 8270E ND 75 28 ug/kg 2,4-Dinitrotoluene 121-14-2 8270E ND 30 11 ug/kg 2,6-Dinitrotoluene 606-20-2 8270E ND 30 11 ug/kg Di-n-octylphthalate 117-84-0 8270E ND 15 5.6 ug/kg bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 75 28 ug/kg Fluoranthene 206-44-0 8270E ND 3.0 0.47 ug/kg Fluorene 86-73-7 8270E ND 3.0 0.64 ug/kg Hexachlorobenzene 118-74-1 8270E ND 15 5.6 ug/kg Hexachlorobutadiene 87-68-3 8270E ND 15 5.6 ug/kg Hexachlorocyclopentadiene 77-47-4 8270E ND 75 28 ug/kg Hexachloroethane 67-72-1 8270E ND 15 5.6 ug/kg Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 3.0 1.1 ug/kg Isophorone 78-59-1 8270E ND 15 5.6 ug/kg 2-Methylnaphthalene 91-57-6 8270E ND 3.0 1.1 ug/kg 2-Methylphenol 95-48-7 8270E ND 15 5.6 ug/kg 3+4-Methylphenol 106-44-5 8270E ND 30 11 ug/kg Naphthalene 91-20-3 8270E ND 3.0 1.1 ug/kg 2-Nitroaniline 88-74-4 8270E ND 30 11 ug/kg 3-Nitroaniline 99-09-2 8270E ND 30 11 ug/kg 4-Nitroaniline 100-01-6 8270E ND 30 11 ug/kg Nitrobenzene 98-95-3 8270E ND 15 5.6 ug/kg 2-Nitrophenol 88-75-5 8270E ND 30 11 ug/kg 4-Nitrophenol 100-02-7 8270E ND 75 28 ug/kg N-Nitrosodi-n-propylamine 621-64-7 8270E ND 15 5.6 ug/kg N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270E ND 15 5.6 ug/kg Pentachlorophenol 87-86-5 8270E ND 75 28 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 12 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-002 Description: S-2 BOTTOM Matrix: Solid Date Sampled:09/15/2020 1305 % Solids: 88.8 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1343 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Phenanthrene 85-01-8 8270E ND 3.0 0.81 ug/kg 2 Phenol 108-95-2 8270E ND 15 5.6 ug/kg 2 Pyrene 129-00-0 8270E ND 3.0 0.56 ug/kg 2 Pyridine 110-86-1 8270E ND 15 5.6 ug/kg 2 2,4,5-Trichlorophenol 95-95-4 8270E ND 15 5.6 ug/kg 2 2,4,6-Trichlorophenol 88-06-2 8270E ND 15 5.6 ug/kg 2 Run 2 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 58 33-102 2-Fluorophenol 48 35-115 Nitrobenzene-d5 61 22-109 Phenol-d5 57 33-122 Terphenyl-d14 65 41-120 2,4,6-Tribromophenol 55 30-117 MA EPH (aliphatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/28/2020 2329 JJG 09/21/2020 0856 68223 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C19 - C36 Aliphatics - Unfractionated MADEP-EPH-04 ND 10 10 mg/kg 1 C9 - C18 Aliphatics - Unfractionated MADEP-EPH-04 ND 10 10 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) - Unfractionated 89 40-140 MA EPH (aromatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/28/2020 2329 JJG 09/21/2020 0856 68230 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics - Unfractionated MADEP-EPH-04 ND 10 10 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) - Unfractionated 76 40-140 2-Fluorobiphenyl (fractionation 1) 95 40-140 2-Bromonaphthalene (fractionation 2) 95 40-140 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 13 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-002 Description: S-2 BOTTOM Matrix: Solid Date Sampled:09/15/2020 1305 % Solids: 88.8 09/17/2020 0057 Date Received:09/16/2020 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 09/19/2020 2019 STM 67245 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH-18- ND 4.4 0.88 mg/kg 1 C9 - C12 Aliphatics MADEP-VPH-18- ND 4.4 0.88 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 101 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 09/19/2020 2019 STM 67246 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH-18- ND 1.5 0.58 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 100 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 14 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-003 Description: S-3 SOUTH Matrix: Solid Date Sampled:09/15/2020 1310 % Solids: 89.9 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 09/18/20201507 JM1 67142 7.87 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 11 J 14 5.7 ug/kg Benzene 71-43-2 8260D ND 3.5 1.4 ug/kg Bromodichloromethane 75-27-4 8260D ND 3.5 1.4 ug/kg Bromoform 75-25-2 8260D ND 3.5 1.4 ug/kg Bromomethane (Methyl bromide) 74-83-9 8260D ND 3.5 2.1 ug/kg 2-Butanone (MEK) 78-93-3 8260D ND 14 2.8 ug/kg Carbon disulfide 75-15-0 8260D ND 3.5 1.4 ug/kg Carbon tetrachloride 56-23-5 8260D ND 3.5 1.4 ug/kg Chlorobenzene 108-90-7 8260D ND 3.5 1.4 ug/kg Chloroethane 75-00-3 8260D ND 3.5 1.4 ug/kg Chloroform 67-66-3 8260D ND 3.5 1.4 ug/kg Chloromethane (Methyl chloride) 74-87-3 8260D ND 3.5 2.1 ug/kg Cyclohexane 110-82-7 8260D ND 3.5 1.4 ug/kg 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D ND 3.5 1.4 ug/kg Dibromochloromethane 124-48-1 8260D ND 3.5 1.4 ug/kg 1,2-Dibromoethane (EDB) 106-93-4 8260D ND 3.5 1.4 ug/kg 1,2-Dichlorobenzene 95-50-1 8260D ND 3.5 1.4 ug/kg 1,3-Dichlorobenzene 541-73-1 8260D ND 3.5 1.4 ug/kg 1,4-Dichlorobenzene 106-46-7 8260D ND 3.5 1.4 ug/kg Dichlorodifluoromethane 75-71-8 8260D ND 3.5 2.1 ug/kg 1,1-Dichloroethane 75-34-3 8260D ND 3.5 1.4 ug/kg 1,2-Dichloroethane 107-06-2 8260D ND 3.5 1.4 ug/kg 1,1-Dichloroethene 75-35-4 8260D ND 3.5 1.4 ug/kg cis- 1,2-Dichloroethene 156-59-2 8260D ND 3.5 1.4 ug/kg trans-1,2-Dichloroethene 156-60-5 8260D ND 3.5 1.4 ug/kg 1,2-Dichloropropane 78-87-5 8260D ND 3.5 1.4 ug/kg cis- 1,3-Dichloropropene 10061-01-5 8260D ND 3.5 1.4 ug/kg trans- 1,3-Dichloropropene 10061-02-6 8260D ND 3.5 1.4 ug/kg Ethylbenzene 100-41-4 8260D ND 3.5 1.4 ug/kg 2-Hexanone 591-78-6 8260D ND 7.1 2.8 ug/kg Isopropylbenzene 98-82-8 8260D ND 3.5 1.4 ug/kg Methyl acetate 79-20-9 8260D 1.6 J 3.5 1.4 ug/kg Methyl tertiary butyl ether (MTBE) 1634-04-4 8260D ND 3.5 1.4 ug/kg 4-Methyl-2-pentanone 108-10-1 8260D ND 7.1 2.8 ug/kg Methylcyclohexane 108-87-2 8260D ND 3.5 1.4 ug/kg Methylene chloride 75-09-2 8260D ND 3.5 1.4 ug/kg Styrene 100-42-5 8260D ND 3.5 1.4 ug/kg 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 3.5 1.4 ug/kg Tetrachloroethene 127-18-4 8260D ND 3.5 1.4 ug/kg Toluene 108-88-3 8260D ND 3.5 1.4 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 15 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-003 Description: S-3 SOUTH Matrix: Solid Date Sampled:09/15/2020 1310 % Solids: 89.9 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 09/18/20201507 JM1 67142 7.87 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 3.5 1.4 ug/kg 1 1,2,4-Trichlorobenzene 120-82-1 8260D ND 3.5 1.4 ug/kg 1 1,1,1-Trichloroethane 71-55-6 8260D ND 3.5 1.4 ug/kg 1 1,1,2-Trichloroethane 79-00-5 8260D ND 3.5 1.4 ug/kg 1 Trichloroethene 79-01-6 8260D ND 3.5 1.4 ug/kg 1 Trichlorofluoromethane 75-69-4 8260D ND 3.5 1.4 ug/kg 1 Vinyl chloride 75-01-4 8260D ND 3.5 2.1 ug/kg 1 Xylenes (total) 1330-20-7 8260D 5.1 J 7.1 2.8 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 108 47-138 1,2-Dichloroethane-d4 89 53-142 Toluene-d8 115 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1408 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 8270E ND 3.0 0.92 ug/kg 2 Acenaphthylene 208-96-8 8270E ND 3.0 1.1 ug/kg 2 Acetophenone 98-86-2 8270E ND 14 5.5 ug/kg 2 Anthracene 120-12-7 8270E ND 3.0 0.57 ug/kg 2 Atrazine 1912-24-9 8270E ND 14 5.5 ug/kg 2 Benzaldehyde 100-52-7 8270E ND 14 5.5 ug/kg 2 Benzo(a)anthracene 56-55-3 8270E ND 3.0 0.65 ug/kg 2 Benzo(a)pyrene 50-32-8 8270E ND 3.0 0.73 ug/kg 2 Benzo(b)fluoranthene 205-99-2 8270E ND 3.0 0.55 ug/kg 2 Benzo(g,h,i)perylene 191-24-2 8270E ND 3.0 0.72 ug/kg 2 Benzo(k)fluoranthene 207-08-9 8270E ND 3.0 0.53 ug/kg 2 1,1'-Biphenyl 92-52-4 8270E ND 14 5.5 ug/kg 2 4-Bromophenyl phenyl ether 101-55-3 8270E ND 14 5.5 ug/kg 2 Butyl benzyl phthalate 85-68-7 8270E ND 14 5.5 ug/kg 2 Caprolactam 105-60-2 8270E ND 14 5.5 ug/kg 2 Carbazole 86-74-8 8270E ND 14 5.5 ug/kg 2 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 14 5.5 ug/kg 2 4-Chloro-3-methyl phenol 59-50-7 8270E ND 14 5.5 ug/kg 2 4-Chloroaniline 106-47-8 8270E ND 14 5.5 ug/kg 2 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 14 5.5 ug/kg 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 16 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-003 Description: S-3 SOUTH Matrix: Solid Date Sampled:09/15/2020 1310 % Solids: 89.9 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1408 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run bis(2-Chloroethyl)ether 111-44-4 8270E ND 14 5.5 ug/kg 2-Chloronaphthalene 91-58-7 8270E ND 14 5.5 ug/kg 2-Chlorophenol 95-57-8 8270E ND 14 5.5 ug/kg 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 14 5.5 ug/kg Chrysene 218-01-9 8270E ND 3.0 0.50 ug/kg Dibenzo(a,h)anthracene 53-70-3 8270E ND 3.0 0.57 ug/kg Dibenzofuran 132-64-9 8270E ND 14 5.5 ug/kg 3,3'-Dichlorobenzidine 91-94-1 8270E ND 14 5.5 ug/kg 2,4-Dichlorophenol 120-83-2 8270E ND 14 5.5 ug/kg Diethylphthalate 84-66-2 8270E ND 14 5.5 ug/kg Dimethyl phthalate 131-11-3 8270E ND 14 8.2 ug/kg 2,4-Dimethylphenol 105-67-9 8270E ND 14 5.5 ug/kg Di-n-butyl phthalate 84-74-2 8270E 7.7 J 14 5.5 ug/kg 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 74 28 ug/kg 2,4-Dinitrophenol 51-28-5 8270E ND 74 28 ug/kg 2,4-Dinitrotoluene 121-14-2 8270E ND 30 11 ug/kg 2,6-Dinitrotoluene 606-20-2 8270E ND 30 11 ug/kg Di-n-octylphthalate 117-84-0 8270E ND 14 5.5 ug/kg bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 74 28 ug/kg Fluoranthene 206-44-0 8270E ND 3.0 0.47 ug/kg Fluorene 86-73-7 8270E ND 3.0 0.63 ug/kg Hexachlorobenzene 118-74-1 8270E ND 14 5.5 ug/kg Hexachlorobutadiene 87-68-3 8270E ND 14 5.5 ug/kg Hexachlorocyclopentadiene 77-47-4 8270E ND 74 28 ug/kg Hexachloroethane 67-72-1 8270E ND 14 5.5 ug/kg Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 3.0 1.1 ug/kg Isophorone 78-59-1 8270E ND 14 5.5 ug/kg 2-Methylnaphthalene 91-57-6 8270E ND 3.0 1.1 ug/kg 2-Methylphenol 95-48-7 8270E ND 14 5.5 ug/kg 3+4-Methylphenol 106-44-5 8270E ND 30 11 ug/kg Naphthalene 91-20-3 8270E ND 3.0 1.1 ug/kg 2-Nitroaniline 88-74-4 8270E ND 30 11 ug/kg 3-Nitroaniline 99-09-2 8270E ND 30 11 ug/kg 4-Nitroaniline 100-01-6 8270E ND 30 11 ug/kg Nitrobenzene 98-95-3 8270E ND 14 5.5 ug/kg 2-Nitrophenol 88-75-5 8270E ND 30 11 ug/kg 4-Nitrophenol 100-02-7 8270E ND 74 28 ug/kg N-Nitrosodi-n-propylamine 621-64-7 8270E ND 14 5.5 ug/kg N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270E ND 14 5.5 ug/kg Pentachlorophenol 87-86-5 8270E ND 74 28 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 17 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-003 Description: S-3 SOUTH Matrix: Solid Date Sampled:09/15/2020 1310 % Solids: 89.9 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1408 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Phenanthrene 85-01-8 8270E ND 3.0 0.80 ug/kg 2 Phenol 108-95-2 8270E ND 14 5.5 ug/kg 2 Pyrene 129-00-0 8270E ND 3.0 0.55 ug/kg 2 Pyridine 110-86-1 8270E ND 14 5.5 ug/kg 2 2,4,5-Trichlorophenol 95-95-4 8270E ND 14 5.5 ug/kg 2 2,4,6-Trichlorophenol 88-06-2 8270E ND 14 5.5 ug/kg 2 Run 2 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 47 33-102 2-Fluorophenol 45 35-115 Nitrobenzene-d5 60 22-109 Phenol-d5 56 33-122 Terphenyl-d14 52 41-120 2,4,6-Tribromophenol 48 30-117 MA EPH (aliphatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/28/2020 2359 JJG 09/21/2020 0856 68223 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C19 - C36 Aliphatics - Unfractionated MADEP-EPH-04 ND 11 11 mg/kg 1 C9 - C18 Aliphatics - Unfractionated MADEP-EPH-04 ND 11 11 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) - Unfractionated 88 40-140 MA EPH (aromatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/28/2020 2359 JJG 09/21/2020 0856 68230 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics - Unfractionated MADEP-EPH-04 ND 11 11 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) - Unfractionated 74 40-140 2-Fluorobiphenyl (fractionation 1) 93 40-140 2-Bromonaphthalene (fractionation 2) 95 40-140 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 18 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-003 Description: S-3 SOUTH Matrix: Solid Date Sampled:09/15/2020 1310 % Solids: 89.9 09/17/2020 0057 Date Received:09/16/2020 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 09/19/2020 2047 STM 67245 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH-18- ND 4.9 0.98 mg/kg 1 C9 - C12 Aliphatics MADEP-VPH-18- ND 4.9 0.98 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 105 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 09/19/2020 2047 STM 67246 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH-18- ND 1.6 0.66 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 107 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 19 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-004 Description: S-4 EAST Matrix: Solid Date Sampled:09/15/2020 1315 % Solids: 74.3 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 09/18/20201530 JM1 67142 5.05 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D ND 27 11 ug/kg Benzene 71-43-2 8260D ND 6.7 2.7 ug/kg Bromodichloromethane 75-27-4 8260D ND 6.7 2.7 ug/kg Bromoform 75-25-2 8260D ND 6.7 2.7 ug/kg Bromomethane (Methyl bromide) 74-83-9 8260D ND 6.7 4.0 ug/kg 2-Butanone (MEK) 78-93-3 8260D ND 27 5.3 ug/kg Carbon disulfide 75-15-0 8260D ND 6.7 2.7 ug/kg Carbon tetrachloride 56-23-5 8260D ND 6.7 2.7 ug/kg Chlorobenzene 108-90-7 8260D ND 6.7 2.7 ug/kg Chloroethane 75-00-3 8260D ND 6.7 2.7 ug/kg Chloroform 67-66-3 8260D ND 6.7 2.7 ug/kg Chloromethane (Methyl chloride) 74-87-3 8260D ND 6.7 4.0 ug/kg Cyclohexane 110-82-7 8260D ND 6.7 2.7 ug/kg 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D ND 6.7 2.7 ug/kg Dibromochloromethane 124-48-1 8260D ND 6.7 2.7 ug/kg 1,2-Dibromoethane (EDB) 106-93-4 8260D ND 6.7 2.7 ug/kg 1,2-Dichlorobenzene 95-50-1 8260D ND 6.7 2.7 ug/kg 1,3-Dichlorobenzene 541-73-1 8260D ND 6.7 2.7 ug/kg 1,4-Dichlorobenzene 106-46-7 8260D ND 6.7 2.7 ug/kg Dichlorodifluoromethane 75-71-8 8260D ND 6.7 4.0 ug/kg 1,1-Dichloroethane 75-34-3 8260D ND 6.7 2.7 ug/kg 1,2-Dichloroethane 107-06-2 8260D ND 6.7 2.7 ug/kg 1,1-Dichloroethene 75-35-4 8260D ND 6.7 2.7 ug/kg cis- 1,2-Dichloroethene 156-59-2 8260D ND 6.7 2.7 ug/kg trans-1,2-Dichloroethene 156-60-5 8260D ND 6.7 2.7 ug/kg 1,2-Dichloropropane 78-87-5 8260D ND 6.7 2.7 ug/kg cis- 1,3-Dichloropropene 10061-01-5 8260D ND 6.7 2.7 ug/kg trans- 1,3-Dichloropropene 10061-02-6 8260D ND 6.7 2.7 ug/kg Ethylbenzene 100-41-4 8260D ND 6.7 2.7 ug/kg 2-Hexanone 591-78-6 8260D ND 13 5.3 ug/kg Isopropylbenzene 98-82-8 8260D ND 6.7 2.7 ug/kg Methyl acetate 79-20-9 8260D ND 6.7 2.7 ug/kg Methyl tertiary butyl ether (MTBE) 1634-04-4 8260D ND 6.7 2.7 ug/kg 4-Methyl-2-pentanone 108-10-1 8260D ND 13 5.3 ug/kg Methylcyclohexane 108-87-2 8260D ND 6.7 2.7 ug/kg Methylene chloride 75-09-2 8260D ND 6.7 2.7 ug/kg Styrene 100-42-5 8260D ND 6.7 2.7 ug/kg 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 6.7 2.7 ug/kg Tetrachloroethene 127-18-4 8260D ND 6.7 2.7 ug/kg Toluene 108-88-3 8260D ND 6.7 2.7 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 20 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-004 Description: S-4 EAST Matrix: Solid Date Sampled:09/15/2020 1315 % Solids: 74.3 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 09/18/20201530 JM1 67142 5.05 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 6.7 2.7 ug/kg 1 1,2,4-Trichlorobenzene 120-82-1 8260D ND 6.7 2.7 ug/kg 1 1,1,1-Trichloroethane 71-55-6 8260D ND 6.7 2.7 ug/kg 1 1,1,2-Trichloroethane 79-00-5 8260D ND 6.7 2.7 ug/kg 1 Trichloroethene 79-01-6 8260D ND 6.7 2.7 ug/kg 1 Trichlorofluoromethane 75-69-4 8260D ND 6.7 2.7 ug/kg 1 Vinyl chloride 75-01-4 8260D ND 6.7 4.0 ug/kg 1 Xylenes (total) 1330-20-7 8260D ND 13 5.3 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 109 47-138 1,2-Dichloroethane-d4 92 53-142 Toluene-d8 113 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1433 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 8270E ND 3.6 1.1 ug/kg 2 Acenaphthylene 208-96-8 8270E ND 3.6 1.3 ug/kg 2 Acetophenone 98-86-2 8270E ND 17 6.7 ug/kg 2 Anthracene 120-12-7 8270E ND 3.6 0.69 ug/kg 2 Atrazine 1912-24-9 8270E ND 17 6.7 ug/kg 2 Benzaldehyde 100-52-7 8270E ND 17 6.7 ug/kg 2 Benzo(a)anthracene 56-55-3 8270E ND 3.6 0.79 ug/kg 2 Benzo(a)pyrene 50-32-8 8270E ND 3.6 0.89 ug/kg 2 Benzo(b)fluoranthene 205-99-2 8270E ND 3.6 0.67 ug/kg 2 Benzo(g,h,i)perylene 191-24-2 8270E ND 3.6 0.87 ug/kg 2 Benzo(k)fluoranthene 207-08-9 8270E ND 3.6 0.65 ug/kg 2 1,1'-Biphenyl 92-52-4 8270E ND 17 6.7 ug/kg 2 4-Bromophenyl phenyl ether 101-55-3 8270E ND 17 6.7 ug/kg 2 Butyl benzyl phthalate 85-68-7 8270E ND 17 6.7 ug/kg 2 Caprolactam 105-60-2 8270E 16 J 17 6.7 ug/kg 2 Carbazole 86-74-8 8270E ND 17 6.7 ug/kg 2 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 17 6.7 ug/kg 2 4-Chloro-3-methyl phenol 59-50-7 8270E ND 17 6.7 ug/kg 2 4-Chloroaniline 106-47-8 8270E ND 17 6.7 ug/kg 2 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 17 6.7 ug/kg 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 21 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-004 Description: S-4 EAST Matrix: Solid Date Sampled:09/15/2020 1315 % Solids: 74.3 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1433 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run bis(2-Chloroethyl)ether 111-44-4 8270E ND 17 6.7 ug/kg 2-Chloronaphthalene 91-58-7 8270E ND 17 6.7 ug/kg 2-Chlorophenol 95-57-8 8270E ND 17 6.7 ug/kg 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 17 6.7 ug/kg Chrysene 218-01-9 8270E ND 3.6 0.60 ug/kg Dibenzo(a,h)anthracene 53-70-3 8270E ND 3.6 0.69 ug/kg Dibenzofuran 132-64-9 8270E ND 17 6.7 ug/kg 3,3'-Dichlorobenzidine 91-94-1 8270E ND 17 6.7 ug/kg 2,4-Dichlorophenol 120-83-2 8270E ND 17 6.7 ug/kg Diethylphthalate 84-66-2 8270E ND 17 6.7 ug/kg Dimethyl phthalate 131-11-3 8270E ND 17 9.9 ug/kg 2,4-Dimethylphenol 105-67-9 8270E ND 17 6.7 ug/kg Di-n-butyl phthalate 84-74-2 8270E ND 17 6.7 ug/kg 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 90 34 ug/kg 2,4-Dinitrophenol 51-28-5 8270E ND 90 34 ug/kg 2,4-Dinitrotoluene 121-14-2 8270E ND 36 13 ug/kg 2,6-Dinitrotoluene 606-20-2 8270E ND 36 13 ug/kg Di-n-octylphthalate 117-84-0 8270E ND 17 6.7 ug/kg bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 90 34 ug/kg Fluoranthene 206-44-0 8270E ND 3.6 0.56 ug/kg Fluorene 86-73-7 8270E ND 3.6 0.77 ug/kg Hexachlorobenzene 118-74-1 8270E ND 17 6.7 ug/kg Hexachlorobutadiene 87-68-3 8270E ND 17 6.7 ug/kg Hexachlorocyclopentadiene 77-47-4 8270E ND 90 34 ug/kg Hexachloroethane 67-72-1 8270E ND 17 6.7 ug/kg Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 3.6 1.3 ug/kg Isophorone 78-59-1 8270E ND 17 6.7 ug/kg 2-Methylnaphthalene 91-57-6 8270E ND 3.6 1.3 ug/kg 2-Methylphenol 95-48-7 8270E ND 17 6.7 ug/kg 3+4-Methylphenol 106-44-5 8270E ND 36 13 ug/kg Naphthalene 91-20-3 8270E ND 3.6 1.3 ug/kg 2-Nitroaniline 88-74-4 8270E ND 36 13 ug/kg 3-Nitroaniline 99-09-2 8270E ND 36 13 ug/kg 4-Nitroaniline 100-01-6 8270E ND 36 13 ug/kg Nitrobenzene 98-95-3 8270E ND 17 6.7 ug/kg 2-Nitrophenol 88-75-5 8270E ND 36 13 ug/kg 4-Nitrophenol 100-02-7 8270E ND 90 34 ug/kg N-Nitrosodi-n-propylamine 621-64-7 8270E ND 17 6.7 ug/kg N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270E ND 17 6.7 ug/kg Pentachlorophenol 87-86-5 8270E ND 90 34 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 22 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-004 Description: S-4 EAST Matrix: Solid Date Sampled:09/15/2020 1315 % Solids: 74.3 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 1 09/23/2020 1433 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Phenanthrene 85-01-8 8270E ND 3.6 0.97 ug/kg 2 Phenol 108-95-2 8270E ND 17 6.7 ug/kg 2 Pyrene 129-00-0 8270E ND 3.6 0.67 ug/kg 2 Pyridine 110-86-1 8270E ND 17 6.7 ug/kg 2 2,4,5-Trichlorophenol 95-95-4 8270E ND 17 6.7 ug/kg 2 2,4,6-Trichlorophenol 88-06-2 8270E ND 17 6.7 ug/kg 2 Run 2 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 71 33-102 2-Fluorophenol 68 35-115 Nitrobenzene-d5 82 22-109 Phenol-d5 76 33-122 Terphenyl-d14 79 41-120 2,4,6-Tribromophenol 64 30-117 MA EPH (aliphatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/29/2020 0029 JJG 09/21/2020 0856 68223 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C19 - C36 Aliphatics - Unfractionated MADEP-EPH-04 ND 13 13 mg/kg 1 C9 - C18 Aliphatics - Unfractionated MADEP-EPH-04 ND 13 13 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) - Unfractionated 95 40-140 MA EPH (aromatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/29/2020 0029 JJG 09/21/2020 0856 68230 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics - Unfractionated MADEP-EPH-04 ND 13 13 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) - Unfractionated 79 40-140 2-Fluorobiphenyl (fractionation 1) 95 40-140 2-Bromonaphthalene (fractionation 2) 96 40-140 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 23 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-004 Description: S-4 EAST Matrix: Solid Date Sampled:09/15/2020 1315 % Solids: 74.3 09/17/2020 0057 Date Received:09/16/2020 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 09/19/2020 2116 STM 67245 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH-18- ND 6.4 1.3 mg/kg 1 C9 - C12 Aliphatics MADEP-VPH-18- ND 6.4 1.3 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 117 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 09/19/2020 2116 STM 67246 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH-18- ND 2.1 0.85 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 112 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 24 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-005 Description: S-5 WEST Matrix: Solid Date Sampled:09/15/2020 1320 % Solids: 81.2 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 09/18/20201552 JM1 67142 5.37 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D ND 23 9.2 ug/kg Benzene 71-43-2 8260D ND 5.7 2.3 ug/kg Bromodichloromethane 75-27-4 8260D ND 5.7 2.3 ug/kg Bromoform 75-25-2 8260D ND 5.7 2.3 ug/kg Bromomethane (Methyl bromide) 74-83-9 8260D ND 5.7 3.4 ug/kg 2-Butanone (MEK) 78-93-3 8260D ND 23 4.6 ug/kg Carbon disulfide 75-15-0 8260D ND 5.7 2.3 ug/kg Carbon tetrachloride 56-23-5 8260D ND 5.7 2.3 ug/kg Chlorobenzene 108-90-7 8260D ND 5.7 2.3 ug/kg Chloroethane 75-00-3 8260D ND 5.7 2.3 ug/kg Chloroform 67-66-3 8260D ND 5.7 2.3 ug/kg Chloromethane (Methyl chloride) 74-87-3 8260D ND 5.7 3.4 ug/kg Cyclohexane 110-82-7 8260D ND 5.7 2.3 ug/kg 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D ND 5.7 2.3 ug/kg Dibromochloromethane 124-48-1 8260D ND 5.7 2.3 ug/kg 1,2-Dibromoethane (EDB) 106-93-4 8260D ND 5.7 2.3 ug/kg 1,2-Dichlorobenzene 95-50-1 8260D ND 5.7 2.3 ug/kg 1,3-Dichlorobenzene 541-73-1 8260D ND 5.7 2.3 ug/kg 1,4-Dichlorobenzene 106-46-7 8260D ND 5.7 2.3 ug/kg Dichlorodifluoromethane 75-71-8 8260D ND 5.7 3.4 ug/kg 1,1-Dichloroethane 75-34-3 8260D ND 5.7 2.3 ug/kg 1,2-Dichloroethane 107-06-2 8260D ND 5.7 2.3 ug/kg 1,1-Dichloroethene 75-35-4 8260D ND 5.7 2.3 ug/kg cis- 1,2-Dichloroethene 156-59-2 8260D ND 5.7 2.3 ug/kg trans-1,2-Dichloroethene 156-60-5 8260D ND 5.7 2.3 ug/kg 1,2-Dichloropropane 78-87-5 8260D ND 5.7 2.3 ug/kg cis- 1,3-Dichloropropene 10061-01-5 8260D ND 5.7 2.3 ug/kg trans- 1,3-Dichloropropene 10061-02-6 8260D ND 5.7 2.3 ug/kg Ethylbenzene 100-41-4 8260D ND 5.7 2.3 ug/kg 2-Hexanone 591-78-6 8260D ND 11 4.6 ug/kg Isopropylbenzene 98-82-8 8260D ND 5.7 2.3 ug/kg Methyl acetate 79-20-9 8260D ND 5.7 2.3 ug/kg Methyl tertiary butyl ether (MTBE) 1634-04-4 8260D ND 5.7 2.3 ug/kg 4-Methyl-2-pentanone 108-10-1 8260D ND 11 4.6 ug/kg Methylcyclohexane 108-87-2 8260D ND 5.7 2.3 ug/kg Methylene chloride 75-09-2 8260D ND 5.7 2.3 ug/kg Styrene 100-42-5 8260D ND 5.7 2.3 ug/kg 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 5.7 2.3 ug/kg Tetrachloroethene 127-18-4 8260D ND 5.7 2.3 ug/kg Toluene 108-88-3 8260D ND 5.7 2.3 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 25 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-005 Description: S-5 WEST Matrix: Solid Date Sampled:09/15/2020 1320 % Solids: 81.2 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260D 1 09/18/20201552 JM1 67142 5.37 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 5.7 2.3 ug/kg 1 1,2,4-Trichlorobenzene 120-82-1 8260D ND 5.7 2.3 ug/kg 1 1,1,1-Trichloroethane 71-55-6 8260D ND 5.7 2.3 ug/kg 1 1,1,2-Trichloroethane 79-00-5 8260D ND 5.7 2.3 ug/kg 1 Trichloroethene 79-01-6 8260D ND 5.7 2.3 ug/kg 1 Trichlorofluoromethane 75-69-4 8260D ND 5.7 2.3 ug/kg 1 Vinyl chloride 75-01-4 8260D ND 5.7 3.4 ug/kg 1 Xylenes (total) 1330-20-7 8260D ND 11 4.6 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 110 47-138 1,2-Dichloroethane-d4 95 53-142 Toluene-d8 114 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 5 09/23/2020 1457 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 8270E ND 17 5.1 ug/kg 2 Acenaphthylene 208-96-8 8270E ND 17 5.8 ug/kg 2 Acetophenone 98-86-2 8270E ND 80 31 ug/kg 2 Anthracene 120-12-7 8270E ND 17 3.1 ug/kg 2 Atrazine 1912-24-9 8270E ND 80 31 ug/kg 2 Benzaldehyde 100-52-7 8270E ND 80 31 ug/kg 2 Benzo(a)anthracene 56-55-3 8270E ND 17 3.6 ug/kg 2 Benzo(a)pyrene 50-32-8 8270E ND 17 4.1 ug/kg 2 Benzo(b)fluoranthene 205-99-2 8270E ND 17 3.1 ug/kg 2 Benzo(g,h,i)perylene 191-24-2 8270E ND 17 4.0 ug/kg 2 Benzo(k)fluoranthene 207-08-9 8270E ND 17 3.0 ug/kg 2 1,1'-Biphenyl 92-52-4 8270E ND 80 31 ug/kg 2 4-Bromophenyl phenyl ether 101-55-3 8270E ND 80 31 ug/kg 2 Butyl benzyl phthalate 85-68-7 8270E ND 80 31 ug/kg 2 Caprolactam 105-60-2 8270E ND 80 31 ug/kg 2 Carbazole 86-74-8 8270E ND 80 31 ug/kg 2 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 80 31 ug/kg 2 4-Chloro-3-methyl phenol 59-50-7 8270E ND 80 31 ug/kg 2 4-Chloroaniline 106-47-8 8270E ND 80 31 ug/kg 2 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 80 31 ug/kg 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 26 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-005 Description: S-5 WEST Matrix: Solid Date Sampled:09/15/2020 1320 % Solids: 81.2 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 5 09/23/2020 1457 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run bis(2-Chloroethyl)ether 111-44-4 8270E ND 80 31 ug/kg 2-Chloronaphthalene 91-58-7 8270E ND 80 31 ug/kg 2-Chlorophenol 95-57-8 8270E ND 80 31 ug/kg 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 80 31 ug/kg Chrysene 218-01-9 8270E ND 17 2.8 ug/kg Dibenzo(a,h)anthracene 53-70-3 8270E ND 17 3.1 ug/kg Dibenzofuran 132-64-9 8270E ND 80 31 ug/kg 3,3'-Dichlorobenzidine 91-94-1 8270E ND 80 31 ug/kg 2,4-Dichlorophenol 120-83-2 8270E ND 80 31 ug/kg Diethylphthalate 84-66-2 8270E ND 80 31 ug/kg Dimethyl phthalate 131-11-3 8270E ND 80 46 ug/kg 2,4-Dimethylphenol 105-67-9 8270E ND 80 31 ug/kg Di-n-butyl phthalate 84-74-2 8270E ND 80 31 ug/kg 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 410 150 ug/kg 2,4-Dinitrophenol 51-28-5 8270E ND 410 150 ug/kg 2,4-Dinitrotoluene 121-14-2 8270E ND 170 62 ug/kg 2,6-Dinitrotoluene 606-20-2 8270E ND 170 62 ug/kg Di-n-octylphthalate 117-84-0 8270E ND 80 31 ug/kg bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 410 150 ug/kg Fluoranthene 206-44-0 8270E ND 17 2.6 ug/kg Fluorene 86-73-7 8270E ND 17 3.5 ug/kg Hexachlorobenzene 118-74-1 8270E ND 80 31 ug/kg Hexachlorobutadiene 87-68-3 8270E ND 80 31 ug/kg Hexachlorocyclopentadiene 77-47-4 8270E ND 410 150 ug/kg Hexachloroethane 67-72-1 8270E ND 80 31 ug/kg Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 17 6.2 ug/kg Isophorone 78-59-1 8270E ND 80 31 ug/kg 2-Methylnaphthalene 91-57-6 8270E ND 17 6.1 ug/kg 2-Methylphenol 95-48-7 8270E ND 80 31 ug/kg 3+4-Methylphenol 106-44-5 8270E ND 170 62 ug/kg Naphthalene 91-20-3 8270E ND 17 6.0 ug/kg 2-Nitroaniline 88-74-4 8270E ND 170 62 ug/kg 3-Nitroaniline 99-09-2 8270E ND 170 62 ug/kg 4-Nitroaniline 100-01-6 8270E ND 170 62 ug/kg Nitrobenzene 98-95-3 8270E ND 80 31 ug/kg 2-Nitrophenol 88-75-5 8270E ND 170 62 ug/kg 4-Nitrophenol 100-02-7 8270E ND 410 150 ug/kg N-Nitrosodi-n-propylamine 621-64-7 8270E ND 80 31 ug/kg N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270E ND 80 31 ug/kg Pentachlorophenol 87-86-5 8270E ND 410 150 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 27 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-005 Description: S-5 WEST Matrix: Solid Date Sampled:09/15/2020 1320 % Solids: 81.2 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 5 09/23/2020 1457 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Phenanthrene 85-01-8 8270E ND 17 4.4 ug/kg 2 Phenol 108-95-2 8270E ND 80 31 ug/kg 2 Pyrene 129-00-0 8270E ND 17 3.1 ug/kg 2 Pyridine 110-86-1 8270E ND 80 31 ug/kg 2 2,4,5-Trichlorophenol 95-95-4 8270E ND 80 31 ug/kg 2 2,4,6-Trichlorophenol 88-06-2 8270E ND 80 31 ug/kg 2 Run 2 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 65 33-102 2-Fluorophenol 53 35-115 Nitrobenzene-d5 68 22-109 Phenol-d5 54 33-122 Terphenyl-d14 67 41-120 2,4,6-Tribromophenol 45 30-117 MA EPH (aliphatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/29/2020 0059 JJG 09/21/2020 0856 68223 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C19 - C36 Aliphatics - Unfractionated MADEP-EPH-04 ND 12 12 mg/kg 1 C9 - C18 Aliphatics - Unfractionated MADEP-EPH-04 ND 12 12 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) - Unfractionated 103 40-140 MA EPH (aromatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/29/2020 0059 JJG 09/21/2020 0856 68230 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics - Unfractionated MADEP-EPH-04 ND 12 12 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) - Unfractionated 85 40-140 2-Fluorobiphenyl (fractionation 1) 111 40-140 2-Bromonaphthalene (fractionation 2) 113 40-140 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 28 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-005 Description: S-5 WEST Matrix: Solid Date Sampled:09/15/2020 1320 % Solids: 81.2 09/17/2020 0057 Date Received:09/16/2020 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 09/19/2020 2144 STM 67245 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH-18- ND 5.4 1.1 mg/kg 1 C9 - C12 Aliphatics MADEP-VPH-18- ND 5.4 1.1 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 89 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 09/19/2020 2144 STM 67246 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH-18- ND 1.8 0.72 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 87 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 29 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-006 Description: S-6 RELEASE Matrix: Solid Date Sampled:09/15/2020 1200 % Solids: 71.1 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 High 8260D 20 09/18/2020 1819 JM1 67242 5.37 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D ND 34000 14000 ug/kg Benzene 71-43-2 8260D ND 8600 3400 ug/kg Bromodichloromethane 75-27-4 8260D ND 8600 3400 ug/kg Bromoform 75-25-2 8260D ND 8600 3400 ug/kg Bromomethane (Methyl bromide) 74-83-9 8260D ND 8600 5100 ug/kg 2-Butanone (MEK) 78-93-3 8260D ND 34000 6900 ug/kg Carbon disulfide 75-15-0 8260D ND 8600 3400 ug/kg Carbon tetrachloride 56-23-5 8260D ND 8600 3400 ug/kg Chlorobenzene 108-90-7 8260D ND 8600 3400 ug/kg Chloroethane 75-00-3 8260D ND 8600 3400 ug/kg Chloroform 67-66-3 8260D ND 8600 3400 ug/kg Chloromethane (Methyl chloride) 74-87-3 8260D ND 8600 5100 ug/kg Cyclohexane 110-82-7 8260D ND 8600 3400 ug/kg 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D ND 8600 3400 ug/kg Dibromochloromethane 124-48-1 8260D ND 8600 3400 ug/kg 1,2-Dibromoethane (EDB) 106-93-4 8260D ND 8600 3400 ug/kg 1,2-Dichlorobenzene 95-50-1 8260D ND 8600 3400 ug/kg 1,3-Dichlorobenzene 541-73-1 8260D ND 8600 3400 ug/kg 1,4-Dichlorobenzene 106-46-7 8260D ND 8600 3400 ug/kg Dichlorodifluoromethane 75-71-8 8260D ND 8600 5100 ug/kg 1,1-Dichloroethane 75-34-3 8260D ND 8600 3400 ug/kg 1,2-Dichloroethane 107-06-2 8260D ND 8600 3400 ug/kg 1,1-Dichloroethene 75-35-4 8260D ND 8600 3400 ug/kg cis- 1,2-Dichloroethene 156-59-2 8260D ND 8600 3400 ug/kg trans-1,2-Dichloroethene 156-60-5 8260D ND 8600 3400 ug/kg 1,2-Dichloropropane 78-87-5 8260D ND 8600 3400 ug/kg cis- 1,3-Dichloropropene 10061-01-5 8260D ND 8600 3400 ug/kg trans- 1,3-Dichloropropene 10061-02-6 8260D ND 8600 3400 ug/kg Ethylbenzene 100-41-4 8260D 9600 8600 3400 ug/kg 2-Hexanone 591-78-6 8260D ND 17000 6900 ug/kg Isopropylbenzene 98-82-8 8260D 4800 J 8600 3400 ug/kg Methyl acetate 79-20-9 8260D ND 8600 3400 ug/kg Methyl tertiary butyl ether (MTBE) 1634-04-4 8260D ND 8600 3400 ug/kg 4-Methyl-2-pentanone 108-10-1 8260D ND 17000 6900 ug/kg Methylcyclohexane 108-87-2 8260D 5400 J 8600 3400 ug/kg Methylene chloride 75-09-2 8260D ND 8600 3400 ug/kg Styrene 100-42-5 8260D ND 8600 3400 ug/kg 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 8600 3400 ug/kg Tetrachloroethene 127-18-4 8260D ND 8600 3400 ug/kg Toluene 108-88-3 8260D ND 8600 3400 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 30 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-006 Description: S-6 RELEASE Matrix: Solid Date Sampled:09/15/2020 1200 % Solids: 71.1 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 High 8260D 20 09/18/2020 1819 JM1 67242 5.37 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 8600 3400 ug/kg 1 1,2,4-Trichlorobenzene 120-82-1 8260D ND 8600 3400 ug/kg 1 1,1,1-Trichloroethane 71-55-6 8260D ND 8600 3400 ug/kg 1 1,1,2-Trichloroethane 79-00-5 8260D ND 8600 3400 ug/kg 1 Trichloroethene 79-01-6 8260D ND 8600 3400 ug/kg 1 Trichlorofluoromethane 75-69-4 8260D ND 8600 3400 ug/kg 1 Vinyl chloride 75-01-4 8260D ND 8600 5100 ug/kg 1 Xylenes (total) 1330-20-7 8260D 120000 17000 6900 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene N 254 47-138 1,2-Dichloroethane-d4 N 205 53-142 Toluene-d8 N 262 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 50 09/23/2020 1522 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 8270E ND 180 56 ug/kg 2 Acenaphthylene 208-96-8 8270E ND 180 64 ug/kg 2 Acetophenone 98-86-2 8270E ND 880 340 ug/kg 2 Anthracene 120-12-7 8270E ND 180 35 ug/kg 2 Atrazine 1912-24-9 8270E ND 880 340 ug/kg 2 Benzaldehyde 100-52-7 8270E ND 880 340 ug/kg 2 Benzo(a)anthracene 56-55-3 8270E ND 180 40 ug/kg 2 Benzo(a)pyrene 50-32-8 8270E ND 180 45 ug/kg 2 Benzo(b)fluoranthene 205-99-2 8270E ND 180 34 ug/kg 2 Benzo(g,h,i)perylene 191-24-2 8270E ND 180 44 ug/kg 2 Benzo(k)fluoranthene 207-08-9 8270E ND 180 33 ug/kg 2 1,1'-Biphenyl 92-52-4 8270E ND 880 340 ug/kg 2 4-Bromophenyl phenyl ether 101-55-3 8270E ND 880 340 ug/kg 2 Butyl benzyl phthalate 85-68-7 8270E ND 880 340 ug/kg 2 Caprolactam 105-60-2 8270E ND 880 340 ug/kg 2 Carbazole 86-74-8 8270E ND 880 340 ug/kg 2 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 880 340 ug/kg 2 4-Chloro-3-methyl phenol 59-50-7 8270E ND 880 340 ug/kg 2 4-Chloroaniline 106-47-8 8270E ND 880 340 ug/kg 2 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 880 340 ug/kg 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 31 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-006 Description: S-6 RELEASE Matrix: Solid Date Sampled:09/15/2020 1200 % Solids: 71.1 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 50 09/23/2020 1522 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run bis(2-Chloroethyl)ether 111-44-4 8270E ND 880 340 ug/kg 2-Chloronaphthalene 91-58-7 8270E ND 880 340 ug/kg 2-Chlorophenol 95-57-8 8270E ND 880 340 ug/kg 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 880 340 ug/kg Chrysene 218-01-9 8270E ND 180 30 ug/kg Dibenzo(a,h)anthracene 53-70-3 8270E ND 180 35 ug/kg Dibenzofuran 132-64-9 8270E ND 880 340 ug/kg 3,3'-Dichlorobenzidine 91-94-1 8270E ND 880 340 ug/kg 2,4-Dichlorophenol 120-83-2 8270E ND 880 340 ug/kg Diethylphthalate 84-66-2 8270E ND 880 340 ug/kg Dimethyl phthalate 131-11-3 8270E ND 880 500 ug/kg 2,4-Dimethylphenol 105-67-9 8270E ND 880 340 ug/kg Di-n-butyl phthalate 84-74-2 8270E ND 880 340 ug/kg 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 4500 1700 ug/kg 2,4-Dinitrophenol 51-28-5 8270E ND 4500 1700 ug/kg 2,4-Dinitrotoluene 121-14-2 8270E ND 1800 680 ug/kg 2,6-Dinitrotoluene 606-20-2 8270E ND 1800 680 ug/kg Di-n-octylphthalate 117-84-0 8270E ND 880 340 ug/kg bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 4500 1700 ug/kg Fluoranthene 206-44-0 8270E ND 180 28 ug/kg Fluorene 86-73-7 8270E ND 180 39 ug/kg Hexachlorobenzene 118-74-1 8270E ND 880 340 ug/kg Hexachlorobutadiene 87-68-3 8270E ND 880 340 ug/kg Hexachlorocyclopentadiene 77-47-4 8270E ND 4500 1700 ug/kg Hexachloroethane 67-72-1 8270E ND 880 340 ug/kg Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 180 68 ug/kg Isophorone 78-59-1 8270E ND 880 340 ug/kg 2-Methylnaphthalene 91-57-6 8270E 6000 180 67 ug/kg 2-Methylphenol 95-48-7 8270E ND 880 340 ug/kg 3+4-Methylphenol 106-44-5 8270E ND 1800 680 ug/kg Naphthalene 91-20-3 8270E 5700 180 66 ug/kg 2-Nitroaniline 88-74-4 8270E ND 1800 680 ug/kg 3-Nitroaniline 99-09-2 8270E ND 1800 680 ug/kg 4-Nitroaniline 100-01-6 8270E ND 1800 680 ug/kg Nitrobenzene 98-95-3 8270E ND 880 340 ug/kg 2-Nitrophenol 88-75-5 8270E ND 1800 680 ug/kg 4-Nitrophenol 100-02-7 8270E ND 4500 1700 ug/kg N-Nitrosodi-n-propylamine 621-64-7 8270E ND 880 340 ug/kg N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270E ND 880 340 ug/kg Pentachlorophenol 87-86-5 8270E ND 4500 1700 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 32 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-006 Description: S-6 RELEASE Matrix: Solid Date Sampled:09/15/2020 1200 % Solids: 71.1 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 50 09/23/2020 1522 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Phenanthrene 85-01-8 8270E ND 180 49 ug/kg 2 Phenol 108-95-2 8270E ND 880 340 ug/kg 2 Pyrene 129-00-0 8270E ND 180 34 ug/kg 2 Pyridine 110-86-1 8270E ND 880 340 ug/kg 2 2,4,5-Trichlorophenol 95-95-4 8270E ND 880 340 ug/kg 2 2,4,6-Trichlorophenol 88-06-2 8270E ND 880 340 ug/kg 2 Run 2 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 65 33-102 2-Fluorophenol N 29 35-115 Nitrobenzene-d5 N 202 22-109 Phenol-d5 N 210 33-122 Terphenyl-d14 72 41-120 2,4,6-Tribromophenol 35 30-117 MA EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/25/2020 2216 JJG 09/21/2020 0856 67275 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics MADEP-EPH-04 89 14 14 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Bromonaphthalene (fractionation 2) 75 40-140 2-Fluorobiphenyl (fractionation 1) 88 40-140 o - Terphenyl (aromatic) 73 40-140 MA EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 09/25/2020 1741 JJG 09/21/2020 0856 67274 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C18 Aliphatics MADEP-EPH-04 200 14 14 mg/kg 1 C19 - C36 Aliphatics MADEP-EPH-04 46 14 14 mg/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) 49 40-140 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 33 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-006 Description: S-6 RELEASE Matrix: Solid Date Sampled:09/15/2020 1200 % Solids: 71.1 09/17/2020 0057 Date Received:09/16/2020 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 3 VPH MADEP-VPH-18-2.1 10 09/22/20201739 ECB 67515 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH-18- 990 62 12 mg/kg 3 C9 - C12 Aliphatics MADEP-VPH-18- 2400 62 12 mg/kg 3 Run 3 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) N 45 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 3 VPH MADEP-VPH-18-2.1 10 09/22/20201739 ECB 67516 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH-18- 1500 21 8.2 mg/kg 3 Run 3 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 107 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 34 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-007 Description: S-7 STOCKPILE Matrix: Solid Date Sampled:09/15/2020 1330 % Solids: 85.5 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 High 8260D 1 09/18/2020 1842 JM1 67242 5.04 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D ND 1300 530 ug/kg 1 Benzene 71-43-2 8260D ND 330 130 ug/kg 1 Bromodichloromethane 75-27-4 8260D ND 330 130 ug/kg 1 Bromoform 75-25-2 8260D ND 330 130 ug/kg 1 Bromomethane (Methyl bromide) 74-83-9 8260D ND 330 200 ug/kg 1 2-Butanone (MEK) 78-93-3 8260D ND 1300 270 ug/kg 1 Carbon disulfide 75-15-0 8260D ND 330 130 ug/kg 1 Carbon tetrachloride 56-23-5 8260D ND 330 130 ug/kg 1 Chlorobenzene 108-90-7 8260D ND 330 130 ug/kg 1 Chloroethane 75-00-3 8260D ND 330 130 ug/kg 1 Chloroform 67-66-3 8260D ND 330 130 ug/kg 1 Chloromethane (Methyl chloride) 74-87-3 8260D ND 330 200 ug/kg 1 Cyclohexane 110-82-7 8260D ND 330 130 ug/kg 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D ND 330 130 ug/kg 1 Dibromochloromethane 124-48-1 8260D ND 330 130 ug/kg 1 1,2-Dibromoethane (EDB) 106-93-4 8260D ND 330 130 ug/kg 1 1,2-Dichlorobenzene 95-50-1 8260D ND 330 130 ug/kg 1 1,3-Dichlorobenzene 541-73-1 8260D ND 330 130 ug/kg 1 1,4-Dichlorobenzene 106-46-7 8260D ND 330 130 ug/kg 1 Dichlorodifluoromethane 75-71-8 8260D ND 330 200 ug/kg 1 1,1-Dichloroethane 75-34-3 8260D ND 330 130 ug/kg 1 1,2-Dichloroethane 107-06-2 8260D ND 330 130 ug/kg 1 1,1-Dichloroethene 75-35-4 8260D ND 330 130 ug/kg 1 cis- 1,2-Dichloroethene 156-59-2 8260D ND 330 130 ug/kg 1 trans-1,2-Dichloroethene 156-60-5 8260D ND 330 130 ug/kg 1 1,2-Dichloropropane 78-87-5 8260D ND 330 130 ug/kg 1 cis- 1,3-Dichloropropene 10061-01-5 8260D ND 330 130 ug/kg 1 trans- 1,3-Dichloropropene 10061-02-6 8260D ND 330 130 ug/kg 1 Ethylbenzene 100-41-4 8260D ND 330 130 ug/kg 1 2-Hexanone 591-78-6 8260D ND 660 270 ug/kg 1 Isopropylbenzene 98-82-8 8260D ND 330 130 ug/kg 1 Methyl acetate 79-20-9 8260D ND 330 130 ug/kg 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 8260D ND 330 130 ug/kg 1 4-Methyl-2-pentanone 108-10-1 8260D ND 660 270 ug/kg 1 Methylcyclohexane 108-87-2 8260D ND 330 130 ug/kg 1 Methylene chloride 75-09-2 8260D ND 330 130 ug/kg 1 Styrene 100-42-5 8260D ND 330 130 ug/kg 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 330 130 ug/kg 1 Tetrachloroethene 127-18-4 8260D ND 330 130 ug/kg 1 Toluene 108-88-3 8260D ND 330 130 ug/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 35 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-007 Description: S-7 STOCKPILE Matrix: Solid Date Sampled:09/15/2020 1330 % Solids: 85.5 09/17/2020 0057 Date Received:09/16/2020 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 High 8260D 1 09/18/2020 1842 JM1 67242 5.04 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 330 130 ug/kg 1 1,2,4-Trichlorobenzene 120-82-1 8260D ND 330 130 ug/kg 1 1,1,1-Trichloroethane 71-55-6 8260D ND 330 130 ug/kg 1 1,1,2-Trichloroethane 79-00-5 8260D ND 330 130 ug/kg 1 Trichloroethene 79-01-6 8260D ND 330 130 ug/kg 1 Trichlorofluoromethane 75-69-4 8260D ND 330 130 ug/kg 1 Vinyl chloride 75-01-4 8260D ND 330 200 ug/kg 1 Xylenes (total) 1330-20-7 8260D 990 660 270 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 107 47-138 1,2-Dichloroethane-d4 95 53-142 Toluene-d8 108 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 20 09/23/2020 1547 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 8270E ND 62 19 ug/kg 2 Acenaphthylene 208-96-8 8270E ND 62 22 ug/kg 2 Acetophenone 98-86-2 8270E ND 300 120 ug/kg 2 Anthracene 120-12-7 8270E ND 62 12 ug/kg 2 Atrazine 1912-24-9 8270E ND 300 120 ug/kg 2 Benzaldehyde 100-52-7 8270E ND 300 120 ug/kg 2 Benzo(a)anthracene 56-55-3 8270E ND 62 14 ug/kg 2 Benzo(a)pyrene 50-32-8 8270E ND 62 15 ug/kg 2 Benzo(b)fluoranthene 205-99-2 8270E ND 62 12 ug/kg 2 Benzo(g,h,i)perylene 191-24-2 8270E ND 62 15 ug/kg 2 Benzo(k)fluoranthene 207-08-9 8270E ND 62 11 ug/kg 2 1,1'-Biphenyl 92-52-4 8270E ND 300 120 ug/kg 2 4-Bromophenyl phenyl ether 101-55-3 8270E ND 300 120 ug/kg 2 Butyl benzyl phthalate 85-68-7 8270E ND 300 120 ug/kg 2 Caprolactam 105-60-2 8270E ND 300 120 ug/kg 2 Carbazole 86-74-8 8270E ND 300 120 ug/kg 2 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 300 120 ug/kg 2 4-Chloro-3-methyl phenol 59-50-7 8270E ND 300 120 ug/kg 2 4-Chloroaniline 106-47-8 8270E ND 300 120 ug/kg 2 bis(2-Chloroethoxy)methane 111-91-1 8270E ND 300 120 ug/kg 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 36 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-007 Description: S-7 STOCKPILE Matrix: Solid Date Sampled:09/15/2020 1330 % Solids: 85.5 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 20 09/23/2020 1547 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run bis(2-Chloroethyl)ether 111-44-4 8270E ND 300 120 ug/kg 2-Chloronaphthalene 91-58-7 8270E ND 300 120 ug/kg 2-Chlorophenol 95-57-8 8270E ND 300 120 ug/kg 4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 300 120 ug/kg Chrysene 218-01-9 8270E ND 62 10 ug/kg Dibenzo(a,h)anthracene 53-70-3 8270E ND 62 12 ug/kg Dibenzofuran 132-64-9 8270E ND 300 120 ug/kg 3,3'-Dichlorobenzidine 91-94-1 8270E ND 300 120 ug/kg 2,4-Dichlorophenol 120-83-2 8270E ND 300 120 ug/kg Diethylphthalate 84-66-2 8270E ND 300 120 ug/kg Dimethyl phthalate 131-11-3 8270E ND 300 170 ug/kg 2,4-Dimethylphenol 105-67-9 8270E ND 300 120 ug/kg Di-n-butyl phthalate 84-74-2 8270E ND 300 120 ug/kg 4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1500 580 ug/kg 2,4-Dinitrophenol 51-28-5 8270E ND 1500 580 ug/kg 2,4-Dinitrotoluene 121-14-2 8270E ND 620 230 ug/kg 2,6-Dinitrotoluene 606-20-2 8270E ND 620 230 ug/kg Di-n-octylphthalate 117-84-0 8270E ND 300 120 ug/kg bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1500 580 ug/kg Fluoranthene 206-44-0 8270E ND 62 9.7 ug/kg Fluorene 86-73-7 8270E ND 62 13 ug/kg Hexachlorobenzene 118-74-1 8270E ND 300 120 ug/kg Hexachlorobutadiene 87-68-3 8270E ND 300 120 ug/kg Hexachlorocyclopentadiene 77-47-4 8270E ND 1500 580 ug/kg Hexachloroethane 67-72-1 8270E ND 300 120 ug/kg Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 62 23 ug/kg Isophorone 78-59-1 8270E ND 300 120 ug/kg 2-Methylnaphthalene 91-57-6 8270E 350 62 23 ug/kg 2-Methylphenol 95-48-7 8270E ND 300 120 ug/kg 3+4-Methylphenol 106-44-5 8270E ND 620 230 ug/kg Naphthalene 91-20-3 8270E 290 62 22 ug/kg 2-Nitroaniline 88-74-4 8270E ND 620 230 ug/kg 3-Nitroaniline 99-09-2 8270E ND 620 230 ug/kg 4-Nitroaniline 100-01-6 8270E ND 620 230 ug/kg Nitrobenzene 98-95-3 8270E ND 300 120 ug/kg 2-Nitrophenol 88-75-5 8270E ND 620 230 ug/kg 4-Nitrophenol 100-02-7 8270E ND 1500 580 ug/kg N-Nitrosodi-n-propylamine 621-64-7 8270E ND 300 120 ug/kg N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270E ND 300 120 ug/kg Pentachlorophenol 87-86-5 8270E ND 1500 580 ug/kg LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 37 of 87 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:VI16120-007 Description: S-7 STOCKPILE Matrix: Solid Date Sampled:09/15/2020 1330 % Solids: 85.5 09/17/2020 0057 Date Received:09/16/2020 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3546 8270E 20 09/23/2020 1547 SCD 09/22/2020 1800 67519 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Phenanthrene 85-01-8 8270E ND 62 17 ug/kg 2 Phenol 108-95-2 8270E ND 300 120 ug/kg 2 Pyrene 129-00-0 8270E ND 62 12 ug/kg 2 Pyridine 110-86-1 8270E ND 300 120 ug/kg 2 2,4,5-Trichlorophenol 95-95-4 8270E ND 300 120 ug/kg 2 2,4,6-Trichlorophenol 88-06-2 8270E ND 300 120 ug/kg 2 Run 2 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 62 33-102 2-Fluorophenol 46 35-115 Nitrobenzene-d5 45 22-109 Phenol-d5 36 33-122 Terphenyl-d14 67 41-120 2,4,6-Tribromophenol 30 30-117 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3550C 8015C 1 09/26/2020 2321 JJG 09/24/2020 2302 67842 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run TPH-DRO 8015C ND 7800 3800 ug/kg 2 Run 2 Acceptance Surrogate Q % Recovery Limits o - Terphenyl 84 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 09/19/2020 0311 STM 67216 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run TPH-GRO 8015C 140000 6200 3100 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 81 23-179 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 38 of 87 QC Summary Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 39 of 87 Volatile Organic Compounds by GC/MS - MB Sample ID: VQ67142-001 Matrix: Solid Batch:67142 Prep Method: 5035 Analytical Method: 8260D Parameter Result Q Dil LOQ DL Units Analysis Date Acetone ND 1 20 8.0 ug/kg 09/18/2020 1130 Benzene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Bromodichloromethane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Bromoform ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Bromomethane (Methyl bromide) ND 1 5.0 3.0 ug/kg 09/18/2020 1130 2-Butanone (MEK) ND 1 20 4.0 ug/kg 09/18/2020 1130 Carbon disulfide ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Carbon tetrachloride ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Chlorobenzene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Chloroethane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Chloroform ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Chloromethane (Methyl chloride) ND 1 5.0 3.0 ug/kg 09/18/2020 1130 Cyclohexane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,2-Dibromo-3-chloropropane (DBCP) ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Dibromochloromethane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,2-Dibromoethane (EDB) ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,2-Dichlorobenzene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,3-Dichlorobenzene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,4-Dichlorobenzene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Dichlorodifluoromethane ND 1 5.0 3.0 ug/kg 09/18/2020 1130 1,1-Dichloroethane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,2-Dichloroethane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,1-Dichloroethene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 cis- 1,2-Dichloroethene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 trans- 1,2-Dichloroethene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,2-Dichloropropane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 cis- 1,3-Dichloropropene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 trans- 1,3-Dichloropropene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Ethylbenzene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 2-Hexanone ND 1 10 4.0 ug/kg 09/18/2020 1130 Isopropylbenzene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Methyl acetate ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Methyl tertiary butyl ether (MTBE) ND 1 5.0 2.0 ug/kg 09/18/2020 1130 4-Methyl-2-pentanone ND 1 10 4.0 ug/kg 09/18/2020 1130 Methylcyclohexane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Methylene chloride ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Styrene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,1,2,2-Tetrachloroethane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Tetrachloroethene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Toluene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,2,4-Trichlorobenzene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,1,1-Trichloroethane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 1,1,2-Trichloroethane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 40 of 87 Volatile Organic Compounds by GC/MS - MB Sample ID: VQ67142-001 Matrix: Solid Batch:67142 Prep Method: 5035 Analytical Method: 8260D Parameter Result Q Dil LOQ DL Units Analysis Date Trichloroethene ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Trichlorofluoromethane ND 1 5.0 2.0 ug/kg 09/18/2020 1130 Vinyl chloride ND 1 5.0 3.0 ug/kg 09/18/2020 1130 Xylenes (total) ND 1 10 4.0 ug/kg 09/18/2020 1130 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 111 47-138 1,2-Dichloroethane-d4 94 53-142 Toluene-d8 113 68-124 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 41 of 87 Volatile Organic Compounds by GC/MS - LCS Sample ID: VQ67142-002 Matrix: Solid Batch:67142 Prep Method: 5035 Analytical Method: 8260D Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Acetone 100 130 1 127 60-140 09/18/2020 1107 Benzene 50 53 1 107 70-130 09/18/2020 1107 Bromodichloromethane 50 51 1 102 70-130 09/18/2020 1107 Bromoform 50 53 1 106 70-130 09/18/2020 1107 Bromomethane (Methyl bromide) 50 54 1 109 70-130 09/18/2020 1107 2-Butanone (MEK) 100 120 1 121 60-140 09/18/2020 1107 Carbon disulfide 50 56 1 112 70-130 09/18/2020 1107 Carbon tetrachloride 50 50 1 100 70-130 09/18/2020 1107 Chlorobenzene 50 54 1 108 70-130 09/18/2020 1107 Chloroethane 50 54 1 108 70-130 09/18/2020 1107 Chloroform 50 50 1 101 70-130 09/18/2020 1107 Chloromethane (Methyl chloride) 50 57 1 114 60-140 09/18/2020 1107 Cyclohexane 50 50 1 100 70-130 09/18/2020 1107 1,2-Dibromo-3-chloropropane (DBCP) 50 50 1 101 70-130 09/18/2020 1107 Dibromochloromethane 50 52 1 105 70-130 09/18/2020 1107 1,2-Dibromoethane (EDB) 50 53 1 107 70-130 09/18/2020 1107 1,2-Dichlorobenzene 50 55 1 110 70-130 09/18/2020 1107 1,3-Dichlorobenzene 50 56 1 113 70-130 09/18/2020 1107 1,4-Dichlorobenzene 50 56 1 112 70-130 09/18/2020 1107 Dichlorodifluoromethane 50 45 1 90 60-140 09/18/2020 1107 1,1-Dichloroethane 50 52 1 105 70-130 09/18/2020 1107 1,2-Dichloroethane 50 51 1 101 70-130 09/18/2020 1107 1,1-Dichloroethene 50 54 1 107 70-130 09/18/2020 1107 cis- 1,2-Dichloroethene 50 51 1 102 70-130 09/18/2020 1107 trans- 1,2-Dichloroethene 50 53 1 107 70-130 09/18/2020 1107 1,2-Dichloropropane 50 52 1 105 70-130 09/18/2020 1107 cis- 1,3-Dichloropropene 50 53 1 105 70-130 09/18/2020 1107 trans- 1,3-Dichloropropene 50 53 1 107 70-130 09/18/2020 1107 Ethylbenzene 50 56 1 112 70-130 09/18/2020 1107 2-Hexanone 100 130 N 1 133 70-130 09/18/2020 1107 Isopropylbenzene 50 56 1 112 70-130 09/18/2020 1107 Methyl acetate 50 51 1 101 70-130 09/18/2020 1107 Methyl tertiary butyl ether (MTBE) 50 50 1 100 70-130 09/18/2020 1107 4-Methyl-2-pentanone 100 110 1 111 70-130 09/18/2020 1107 Methylcyclohexane 50 54 1 108 70-130 09/18/2020 1107 Methylene chloride 50 50 1 100 70-130 09/18/2020 1107 Styrene 50 56 1 111 70-130 09/18/2020 1107 1,1,2,2-Tetrachloroethane 50 53 1 106 70-130 09/18/2020 1107 Tetrachloroethene 50 58 1 115 70-130 09/18/2020 1107 Toluene 50 55 1 110 70-130 09/18/2020 1107 1,1,2-Trichloro-1,2,2-Trifluoroethane 50 52 1 103 70-130 09/18/2020 1107 1,2,4-Trichlorobenzene 50 63 1 126 70-130 09/18/2020 1107 1,1,1-Trichloroethane 50 50 1 100 70-130 09/18/2020 1107 1,1,2-Trichloroethane 50 51 1 102 70-130 09/18/2020 1107 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 42 of 87 Volatile Organic Compounds by GC/MS - LCS Sample ID: VQ67142-002 Matrix: Solid Batch:67142 Prep Method: 5035 Analytical Method: 8260D Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Trichloroethene 50 53 1 107 70-130 09/18/2020 1107 Trichlorofluoromethane 50 48 1 97 70-130 09/18/2020 1107 Vinyl chloride 50 58 1 115 70-130 09/18/2020 1107 Xylenes (total) 100 110 1 111 70-130 09/18/2020 1107 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 110 47-138 1,2-Dichloroethane-d4 98 53-142 Toluene-d8 109 68-124 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 43 of 87 Volatile Organic Compounds by GC/MS - Duplicate Sample ID: V116120-001 DU Matrix: Solid Batch:67142 Prep Method: 5035 Analytical Method: 8260D Sample Amount Result % RPD Parameter (ug/kg) (ug/kg) Q Dil % RPD Limit Analysis Date Acetone ND ND 1 0.00 20 09/18/2020 1904 Benzene ND ND 1 0.00 20 09/18/2020 1904 Bromodichloromethane ND ND 1 0.00 20 09/18/2020 1904 Bromoform ND ND 1 0.00 20 09/18/2020 1904 Bromomethane (Methyl bromide) ND ND 1 0.00 20 09/18/2020 1904 2-Butanone (MEK) ND ND 1 0.00 20 09/18/2020 1904 Carbon disulfide ND ND 1 0.00 20 09/18/2020 1904 Carbon tetrachloride ND ND 1 0.00 20 09/18/2020 1904 Chlorobenzene ND ND 1 0.00 20 09/18/2020 1904 Chloroethane ND ND 1 0.00 20 09/18/2020 1904 Chloroform ND ND 1 0.00 20 09/18/2020 1904 Chloromethane (Methyl chloride) ND ND 1 0.00 20 09/18/2020 1904 Cyclohexane ND ND 1 0.00 20 09/18/2020 1904 1,2-Dibromo-3-chloropropane (DBCP) ND ND 1 0.00 20 09/18/2020 1904 Dibromochloromethane ND ND 1 0.00 20 09/18/2020 1904 1,2-Dibromoethane (EDB) ND ND 1 0.00 20 09/18/2020 1904 1,2-Dichlorobenzene ND ND 1 0.00 20 09/18/2020 1904 1,3-Dichlorobenzene ND ND 1 0.00 20 09/18/2020 1904 1,4-Dichlorobenzene ND ND 1 0.00 20 09/18/2020 1904 Dichlorodifluoromethane ND ND 1 0.00 20 09/18/2020 1904 1,1-Dichloroethane ND ND 1 0.00 20 09/18/2020 1904 1,2-Dichloroethane ND ND 1 0.00 20 09/18/2020 1904 1,1-Dichloroethene ND ND 1 0.00 20 09/18/2020 1904 cis- 1,2-Dichloroethene ND ND 1 0.00 20 09/18/2020 1904 trans- 1,2-Dichloroethene ND ND 1 0.00 20 09/18/2020 1904 1,2-Dichloropropane ND ND 1 0.00 20 09/18/2020 1904 cis- 1,3-Dichloropropene ND ND 1 0.00 20 09/18/2020 1904 trans- 1,3-Dichloropropene ND ND 1 0.00 20 09/18/2020 1904 Ethylbenzene ND ND 1 0.00 20 09/18/2020 1904 2-Hexanone ND ND 1 0.00 20 09/18/2020 1904 1sopropylbenzene ND ND 1 0.00 20 09/18/2020 1904 Methyl acetate ND ND 1 0.00 20 09/18/2020 1904 Methyl tertiary butyl ether (MTBE) ND ND 1 0.00 20 09/18/2020 1904 4-Methyl-2-pentanone ND ND 1 0.00 20 09/18/2020 1904 Methylcyclohexane ND ND 1 0.00 20 09/18/2020 1904 Methylene chloride ND ND 1 0.00 20 09/18/2020 1904 Styrene ND ND 1 0.00 20 09/18/2020 1904 1,1,2,2-Tetrachloroethane ND ND 1 0.00 20 09/18/2020 1904 Tetrachloroethene ND ND 1 0.00 20 09/18/2020 1904 Toluene ND ND 1 0.00 20 09/18/2020 1904 1,1,2-Trichloro-1,2,2-Trifluoroethane ND ND 1 0.00 20 09/18/2020 1904 1,2,4-Trichlorobenzene ND ND 1 0.00 20 09/18/2020 1904 1,1,1-Trichloroethane ND ND 1 0.00 20 09/18/2020 1904 1,1,2-Trichloroethane ND ND 1 0.00 20 09/18/2020 1904 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 44 of 87 Volatile Organic Compounds by GC/MS - Duplicate Sample ID: V116120-001 DU Matrix: Solid Batch:67142 Prep Method: 5035 Analytical Method: 8260D Sample Amount Result % RPD Parameter (ug/kg) (ug/kg) Q Dil % RPD Limit Analysis Date Trichloroethene ND ND 1 0.00 20 09/18/2020 1904 Trichlorofluoromethane ND ND 1 0.00 20 09/18/2020 1904 Vinyl chloride ND ND 1 0.00 20 09/18/2020 1904 Xylenes (total) ND ND 1 0.00 20 09/18/2020 1904 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 111 47-138 1,2-Dichloroethane-d4 93 53-142 Toluene-d8 114 68-124 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 45 of 87 Volatile Organic Compounds by GC/MS - MS Sample ID: V116120-002MS Matrix: Solid Batch:67142 Prep Method: 5035 Analytical Method: 8260D Sample Spike Amount Amount Result % Rec Parameter (ug/kg) (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Acetone ND 95 110 1 117 70-130 09/18/2020 1927 Benzene ND 48 54 1 114 70-130 09/18/2020 1927 Bromodichloromethane ND 48 51 1 107 70-130 09/18/2020 1927 Bromoform ND 48 54 1 113 70-130 09/18/2020 1927 Bromomethane (Methyl bromide) ND 48 56 1 117 70-130 09/18/2020 1927 2-Butanone (MEK) ND 95 110 1 117 70-130 09/18/2020 1927 Carbon disulfide ND 48 61 1 127 70-130 09/18/2020 1927 Carbon tetrachloride ND 48 55 1 115 70-130 09/18/2020 1927 Chlorobenzene ND 48 55 1 115 70-130 09/18/2020 1927 Chloroethane ND 48 54 1 114 70-130 09/18/2020 1927 Chloroform ND 48 50 1 105 70-130 09/18/2020 1927 Chloromethane (Methyl chloride) ND 48 53 1 112 60-140 09/18/2020 1927 Cyclohexane ND 48 59 1 123 70-130 09/18/2020 1927 1,2-Dibromo-3-chloropropane (DBCP) ND 48 51 1 106 70-130 09/18/2020 1927 Dibromochloromethane ND 48 53 1 110 70-130 09/18/2020 1927 1,2-Dibromoethane (EDB) ND 48 53 1 ill 70-130 09/18/2020 1927 1,2-Dichlorobenzene ND 48 55 1 116 70-130 09/18/2020 1927 1,3-Dichlorobenzene ND 48 58 1 122 70-130 09/18/2020 1927 1,4-Dichlorobenzene ND 48 57 1 119 70-130 09/18/2020 1927 Dichlorodifluoromethane ND 48 51 1 108 60-140 09/18/2020 1927 1,1-Dichloroethane ND 48 53 1 111 70-130 09/18/2020 1927 1,2-Dichloroethane ND 48 50 1 106 70-130 09/18/2020 1927 1,1-Dichloroethene ND 48 59 1 124 70-130 09/18/2020 1927 cis- 1,2-Dichloroethene ND 48 52 1 108 70-130 09/18/2020 1927 trans- 1,2-Dichloroethene ND 48 55 1 116 70-130 09/18/2020 1927 1,2-Dichloropropane ND 48 52 1 110 70-130 09/18/2020 1927 cis- 1,3-Dichloropropene ND 48 52 1 110 70-130 09/18/2020 1927 trans- 1,3-Dichloropropene ND 48 53 1 112 70-130 09/18/2020 1927 Ethylbenzene ND 48 58 1 121 70-130 09/18/2020 1927 2-Hexanone ND 95 120 1 127 70-130 09/18/2020 1927 1sopropylbenzene ND 48 59 1 123 70-130 09/18/2020 1927 Methyl acetate ND 48 110 N 1 234 70-130 09/18/2020 1927 Methyl tertiary butyl ether (MTBE) ND 48 49 1 102 70-130 09/18/2020 1927 4-Methyl-2-pentanone ND 95 110 1 114 70-130 09/18/2020 1927 Methylcyclohexane ND 48 67 N 1 141 70-130 09/18/2020 1927 Methylene chloride ND 48 49 1 102 70-130 09/18/2020 1927 Styrene ND 48 56 1 118 70-130 09/18/2020 1927 1,1,2,2-Tetrachloroethane ND 48 53 1 112 70-130 09/18/2020 1927 Tetrachloroethene ND 48 63 N 1 132 70-130 09/18/2020 1927 Toluene ND 48 57 1 119 70-130 09/18/2020 1927 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 48 64 N 1 133 70-130 09/18/2020 1927 1,2,4-Trichlorobenzene ND 48 62 1 130 70-130 09/18/2020 1927 1,1,1-Trichloroethane ND 48 53 1 111 70-130 09/18/2020 1927 1,1,2-Trichloroethane ND 48 51 1 107 70-130 09/18/2020 1927 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 46 of 87 Volatile Organic Compounds by GC/MS - MS Sample ID: V116120-002MS Matrix: Solid Batch:67142 Prep Method: 5035 Analytical Method: 8260D Sample Spike Amount Amount Result % Rec Parameter (ug/kg) (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Trichloroethene ND 48 56 1 117 70-130 09/18/2020 1927 Trichlorofluoromethane ND 48 53 1 112 70-130 09/18/2020 1927 Vinyl chloride ND 48 60 1 126 70-130 09/18/2020 1927 Xylenes (total) ND 95 110 1 120 70-130 09/18/2020 1927 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 113 47-138 1,2-Dichloroethane-d4 90 53-142 Toluene-d8 110 68-124 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 47 of 87 Volatile Organic Compounds by GC/MS - MB Sample ID: VQ67242-001 Matrix: Solid Batch: 67242 Prep Method: 5035 High Analytical Method: 8260D Parameter Result Q Dil LOQ DL Units Analysis Date Acetone ND 1 1000 400 ug/kg 09/21/2020 1104 Benzene ND 1 250 100 ug/kg 09/21/2020 1104 Bromodichloromethane ND 1 250 100 ug/kg 09/21/2020 1104 Bromoform ND 1 250 100 ug/kg 09/21/2020 1104 Bromomethane (Methyl bromide) ND 1 250 150 ug/kg 09/21/2020 1104 2-Butanone (MEK) ND 1 1000 200 ug/kg 09/21/2020 1104 Carbon disulfide ND 1 250 100 ug/kg 09/21/2020 1104 Carbon tetrachloride ND 1 250 100 ug/kg 09/21/2020 1104 Chlorobenzene ND 1 250 100 ug/kg 09/21/2020 1104 Chloroethane ND 1 250 100 ug/kg 09/21/2020 1104 Chloroform ND 1 250 100 ug/kg 09/21/2020 1104 Chloromethane (Methyl chloride) ND 1 250 150 ug/kg 09/21/2020 1104 Cyclohexane ND 1 250 100 ug/kg 09/21/2020 1104 1,2-Dibromo-3-chloropropane (DBCP) ND 1 250 100 ug/kg 09/21/2020 1104 Dibromochloromethane ND 1 250 100 ug/kg 09/21/2020 1104 1,2-Dibromoethane (EDB) ND 1 250 100 ug/kg 09/21/2020 1104 1,2-Dichlorobenzene ND 1 250 100 ug/kg 09/21/2020 1104 1,3-Dichlorobenzene ND 1 250 100 ug/kg 09/21/2020 1104 1,4-Dichlorobenzene ND 1 250 100 ug/kg 09/21/2020 1104 Dichlorodifluoromethane ND 1 250 150 ug/kg 09/21/2020 1104 1,1-Dichloroethane ND 1 250 100 ug/kg 09/21/2020 1104 1,2-Dichloroethane ND 1 250 100 ug/kg 09/21/2020 1104 1,1-Dichloroethene ND 1 250 100 ug/kg 09/21/2020 1104 cis- 1,2-Dichloroethene ND 1 250 100 ug/kg 09/21/2020 1104 trans- 1,2-Dichloroethene ND 1 250 100 ug/kg 09/21/2020 1104 1,2-Dichloropropane ND 1 250 100 ug/kg 09/21/2020 1104 cis- 1,3-Dichloropropene ND 1 250 100 ug/kg 09/21/2020 1104 trans- 1,3-Dichloropropene ND 1 250 100 ug/kg 09/21/2020 1104 Ethylbenzene ND 1 250 100 ug/kg 09/21/2020 1104 2-Hexanone ND 1 500 200 ug/kg 09/21/2020 1104 Isopropylbenzene ND 1 250 100 ug/kg 09/21/2020 1104 Methyl acetate ND 1 250 100 ug/kg 09/21/2020 1104 Methyl tertiary butyl ether (MTBE) ND 1 250 100 ug/kg 09/21/2020 1104 4-Methyl-2-pentanone ND 1 500 200 ug/kg 09/21/2020 1104 Methylcyclohexane ND 1 250 100 ug/kg 09/21/2020 1104 Methylene chloride ND 1 250 100 ug/kg 09/21/2020 1104 Styrene ND 1 250 100 ug/kg 09/21/2020 1104 1,1,2,2-Tetrachloroethane ND 1 250 100 ug/kg 09/21/2020 1104 Tetrachloroethene ND 1 250 100 ug/kg 09/21/2020 1104 Toluene ND 1 250 100 ug/kg 09/21/2020 1104 1,1,2-Trichloro-1,2,2-Trifluoroethane ND 1 250 100 ug/kg 09/21/2020 1104 1,2,4-Trichlorobenzene ND 1 250 100 ug/kg 09/21/2020 1104 1,1,1-Trichloroethane ND 1 250 100 ug/kg 09/21/2020 1104 1,1,2-Trichloroethane ND 1 250 100 ug/kg 09/21/2020 1104 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 48 of 87 Volatile Organic Compounds by GC/MS - MB Sample ID: VQ67242-001 Matrix: Solid Batch: 67242 Prep Method: 5035 High Analytical Method: 8260D Parameter Result Q Dil LOQ DL Units Analysis Date Trichloroethene ND 1 250 100 ug/kg 09/21/2020 1104 Trichlorofluoromethane ND 1 250 100 ug/kg 09/21/2020 1104 Vinyl chloride ND 1 250 150 ug/kg 09/21/2020 1104 Xylenes (total) ND 1 500 200 ug/kg 09/21/2020 1104 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 110 47-138 1,2-Dichloroethane-d4 93 53-142 Toluene-d8 108 68-124 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 49 of 87 Volatile Organic Compounds by GC/MS - LCS Sample ID: VQ67242-002 Matrix: Solid Batch: 67242 Prep Method: 5035 High Analytical Method: 8260D Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Acetone 5000 5700 1 114 60-140 09/21/2020 1041 Benzene 2500 2600 1 105 70-130 09/21/2020 1041 Bromodichloromethane 2500 2500 1 101 70-130 09/21/2020 1041 Bromoform 2500 2500 1 101 70-130 09/21/2020 1041 Bromomethane (Methyl bromide) 2500 2800 1 111 70-130 09/21/2020 1041 2-Butanone (MEK) 5000 5500 1 111 60-140 09/21/2020 1041 Carbon disulfide 2500 2200 1 90 70-130 09/21/2020 1041 Carbon tetrachloride 2500 2600 1 104 70-130 09/21/2020 1041 Chlorobenzene 2500 2800 1 111 70-130 09/21/2020 1041 Chloroethane 2500 3200 1 130 70-130 09/21/2020 1041 Chloroform 2500 2500 1 100 70-130 09/21/2020 1041 Chloromethane (Methyl chloride) 2500 2500 1 101 60-140 09/21/2020 1041 Cyclohexane 2500 2500 1 102 70-130 09/21/2020 1041 1,2-Dibromo-3-chloropropane (DBCP) 2500 2300 1 91 70-130 09/21/2020 1041 Dibromochloromethane 2500 2600 1 105 70-130 09/21/2020 1041 1,2-Dibromoethane (EDB) 2500 2500 1 102 70-130 09/21/2020 1041 1,2-Dichlorobenzene 2500 2500 1 102 70-130 09/21/2020 1041 1,3-Dichlorobenzene 2500 2900 1 117 70-130 09/21/2020 1041 1,4-Dichlorobenzene 2500 2900 1 117 70-130 09/21/2020 1041 Dichlorodifluoromethane 2500 2100 1 83 60-140 09/21/2020 1041 1,1-Dichloroethane 2500 2500 1 101 70-130 09/21/2020 1041 1,2-Dichloroethane 2500 2400 1 98 70-130 09/21/2020 1041 1,1-Dichloroethene 2500 2600 1 103 70-130 09/21/2020 1041 cis- 1,2-Dichloroethene 2500 2500 1 101 70-130 09/21/2020 1041 trans- 1,2-Dichloroethene 2500 2500 1 101 70-130 09/21/2020 1041 1,2-Dichloropropane 2500 2600 1 103 70-130 09/21/2020 1041 cis- 1,3-Dichloropropene 2500 2600 1 104 70-130 09/21/2020 1041 trans- 1,3-Dichloropropene 2500 2400 1 96 70-130 09/21/2020 1041 Ethylbenzene 2500 3000 1 122 70-130 09/21/2020 1041 2-Hexanone 5000 6300 1 125 70-130 09/21/2020 1041 Isopropylbenzene 2500 3200 1 128 70-130 09/21/2020 1041 Methyl acetate 2500 2500 1 101 70-130 09/21/2020 1041 Methyl tertiary butyl ether (MTBE) 2500 2400 1 95 70-130 09/21/2020 1041 4-Methyl-2-pentanone 5000 5000 1 99 70-130 09/21/2020 1041 Methylcyclohexane 2500 3000 1 122 70-130 09/21/2020 1041 Methylene chloride 2500 2400 1 95 70-130 09/21/2020 1041 Styrene 2500 2900 1 117 70-130 09/21/2020 1041 1,1,2,2-Tetrachloroethane 2500 2300 1 92 70-130 09/21/2020 1041 Tetrachloroethene 2500 3000 1 121 70-130 09/21/2020 1041 Toluene 2500 2500 1 102 70-130 09/21/2020 1041 1,1,2-Trichloro-1,2,2-Trifluoroethane 2500 2800 1 112 70-130 09/21/2020 1041 1,2,4-Trichlorobenzene 2500 3500 N 1 141 70-130 09/21/2020 1041 1,1,1-Trichloroethane 2500 2500 1 100 70-130 09/21/2020 1041 1,1,2-Trichloroethane 2500 2300 1 93 70-130 09/21/2020 1041 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 50 of 87 Volatile Organic Compounds by GC/MS - LCS Sample ID: VQ67242-002 Matrix: Solid Batch: 67242 Prep Method: 5035 High Analytical Method: 8260D Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Trichloroethene 2500 2800 1 110 70-130 09/21/2020 1041 Trichlorofluoromethane 2500 2500 1 98 70-130 09/21/2020 1041 Vinyl chloride 2500 2900 1 114 70-130 09/21/2020 1041 Xylenes (total) 5000 5800 1 117 70-130 09/21/2020 1041 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 115 47-138 1,2-Dichloroethane-d4 94 53-142 Toluene-d8 99 68-124 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 51 of 87 Semivolatile Organic Compounds by GC/MS - MB Sample ID: VQ67519-001 Matrix: Solid Batch: 67519 Prep Method: 3546 Analytical Method: 8270E Prep Date: 09/22/2020 1800 Parameter Result Q Dil LOQ DL Units Analysis Date Acenaphthene ND 1 2.7 0.83 ug/kg 09/23/2020 1116 Acenaphthylene ND 1 2.7 0.95 ug/kg 09/23/2020 1116 Acetophenone ND 1 13 5.0 ug/kg 09/23/2020 1116 Anthracene ND 1 2.7 0.51 ug/kg 09/23/2020 1116 Atrazine ND 1 13 5.0 ug/kg 09/23/2020 1116 Benzaldehyde ND 1 13 5.0 ug/kg 09/23/2020 1116 Benzo(a)anthracene ND 1 2.7 0.59 ug/kg 09/23/2020 1116 Benzo(a)pyrene ND 1 2.7 0.66 ug/kg 09/23/2020 1116 Benzo(k)fluoranthene ND 1 2.7 0.50 ug/kg 09/23/2020 1116 Benzo(g,h,i)perylene ND 1 2.7 0.65 ug/kg 09/23/2020 1116 Benzo(k)fluoranthene ND 1 2.7 0.48 ug/kg 09/23/2020 1116 1,1'-Biphenyl ND 1 13 5.0 ug/kg 09/23/2020 1116 4-Bromophenyl phenyl ether ND 1 13 5.0 ug/kg 09/23/2020 1116 Butyl benzyl phthalate ND 1 13 5.0 ug/kg 09/23/2020 1116 Caprolactam ND 1 13 5.0 ug/kg 09/23/2020 1116 Carbazole ND 1 13 5.0 ug/kg 09/23/2020 1116 bis (2-Chloro-1-methylethyl) ether ND 1 13 5.0 ug/kg 09/23/2020 1116 4-Chloro-3-methyl phenol ND 1 13 5.0 ug/kg 09/23/2020 1116 4-Chloroaniline ND 1 13 5.0 ug/kg 09/23/2020 1116 bis(2-Chloroethoxy)methane ND 1 13 5.0 ug/kg 09/23/2020 1116 bis(2-Chloroethyl)ether ND 1 13 5.0 ug/kg 09/23/2020 1116 2-Chloronaphthalene ND 1 13 5.0 ug/kg 09/23/2020 1116 2-Chlorophenol ND 1 13 5.0 ug/kg 09/23/2020 1116 4-Chlorophenyl phenyl ether ND 1 13 5.0 ug/kg 09/23/2020 1116 Chrysene ND 1 2.7 0.45 ug/kg 09/23/2020 1116 Dibenzo(a,h)anthracene ND 1 2.7 0.51 ug/kg 09/23/2020 1116 Dibenzofuran ND 1 13 5.0 ug/kg 09/23/2020 1116 3,3'-Dichlorobenzidine ND 1 13 5.0 ug/kg 09/23/2020 1116 2,4-Dichlorophenol ND 1 13 5.0 ug/kg 09/23/2020 1116 Diethylphthalate ND 1 13 5.0 ug/kg 09/23/2020 1116 Dimethyl phthalate ND 1 13 7.4 ug/kg 09/23/2020 1116 2,4-Dimethylphenol ND 1 13 5.0 ug/kg 09/23/2020 1116 Di-n-butyl phthalate ND 1 13 5.0 ug/kg 09/23/2020 1116 4,6-Dinitro-2-methyl phenol ND 1 67 25 ug/kg 09/23/2020 1116 2,4-Dinitrophenol ND 1 67 25 ug/kg 09/23/2020 1116 2,4-Dinitrotoluene ND 1 27 10 ug/kg 09/23/2020 1116 2,6-Dinitrotoluene ND 1 27 10 ug/kg 09/23/2020 1116 Di-n-octylphthalate ND 1 13 5.0 ug/kg 09/23/2020 1116 bis(2-Ethylhexyl)phthalate ND 1 67 25 ug/kg 09/23/2020 1116 Fluoranthene ND 1 2.7 0.42 ug/kg 09/23/2020 1116 Fluorene ND 1 2.7 0.57 ug/kg 09/23/2020 1116 Hexachlorobenzene ND 1 13 5.0 ug/kg 09/23/2020 1116 Hexachlorobutadiene ND 1 13 5.0 ug/kg 09/23/2020 1116 Hexachlorocyclopentadiene ND 1 67 25 ug/kg 09/23/2020 1116 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 52 of 87 Semivolatile Organic Compounds by GC/MS - MB Sample ID: VQ67519-001 Matrix: Solid Batch: 67519 Prep Method: 3546 Analytical Method: 8270E Prep Date: 09/22/2020 1800 Parameter Result Q Dil LOQ DL Units Analysis Date Hexachloroethane ND 1 13 5.0 ug/kg 09/23/20201116 Indeno(1,2,3-c,d)pyrene ND 1 2.7 1.0 ug/kg 09/23/20201116 Isophorone ND 1 13 5.0 ug/kg 09/23/20201116 2-Methyl naphthalene ND 1 2.7 0.99 ug/kg 09/23/20201116 2-Methylphenol ND 1 13 5.0 ug/kg 09/23/20201116 3+4-Methylphenol ND 1 27 10 ug/kg 09/23/20201116 Naphthalene ND 1 2.7 0.97 ug/kg 09/23/20201116 2-Nitroaniline ND 1 27 10 ug/kg 09/23/20201116 3-Nitroaniline ND 1 27 10 ug/kg 09/23/20201116 4-Nitroaniline ND 1 27 10 ug/kg 09/23/20201116 Nitrobenzene ND 1 13 5.0 ug/kg 09/23/20201116 2-Nitrophenol ND 1 27 10 ug/kg 09/23/20201116 4-Nitrophenol ND 1 67 25 ug/kg 09/23/20201116 N-Nitrosodi-n-propylamine ND 1 13 5.0 ug/kg 09/23/20201116 N-Nitrosodiphenylamine (Diphenylamine) ND 1 13 5.0 ug/kg 09/23/2020 1116 Pentachlorophenol ND 1 67 25 ug/kg 09/23/20201116 Phenanthrene ND 1 2.7 0.72 ug/kg 09/23/20201116 Phenol ND 1 13 5.0 ug/kg 09/23/20201116 Pyrene ND 1 2.7 0.50 ug/kg 09/23/20201116 Pyridine ND 1 13 5.0 ug/kg 09/23/20201116 2,4,5-Trichlorophenol ND 1 13 5.0 ug/kg 09/23/20201116 2,4,6-Trichlorophenol ND 1 13 5.0 ug/kg 09/23/20201116 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 72 33-102 2-Fluorophenol 68 35-115 Nitrobenzene-d5 74 22-109 Phenol-d5 72 33-122 Terphenyl-d14 87 41-120 2,4,6-Tribromophenol 51 30-117 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 53 of 87 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: VQ67519-002 Matrix: Solid Batch: 67519 Prep Method: 3546 Analytical Method: 8270E Prep Date: 09/22/2020 1800 Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Acenaphthene 130 110 1 82 12-111 09/23/2020 1431 Acenaphthylene 130 110 1 84 44-122 09/23/2020 1431 Acetophenone 130 97 1 73 48-111 09/23/2020 1431 Anthracene 130 120 1 90 16-122 09/23/2020 1431 Atrazine 130 110 1 84 48-116 09/23/2020 1431 Benzaldehyde 130 110 1 84 10-110 09/23/2020 1431 Benzo(a)anthracene 130 130 1 96 40-121 09/23/2020 1431 Benzo(a)pyrene 130 130 1 97 36-114 09/23/2020 1431 Benzo(k)fluoranthene 130 120 1 93 38-123 09/23/2020 1431 Benzo(g,h,i)perylene 130 140 1 106 43-120 09/23/2020 1431 Benzo(k)fluoranthene 130 130 1 99 40-126 09/23/2020 1431 1,1'-Biphenyl 130 100 1 77 49-110 09/23/2020 1431 4-Bromophenyl phenyl ether 130 110 1 86 46-118 09/23/2020 1431 Butyl benzyl phthalate 130 130 1 97 46-128 09/23/2020 1431 Caprolactam 130 88 1 66 43-121 09/23/2020 1431 Carbazole 130 130 1 97 47-128 09/23/2020 1431 bis (2-Chloro-1-methylethyl) ether 130 110 1 82 31-102 09/23/2020 1431 4-Chloro-3-methyl phenol 130 110 1 79 49-118 09/23/2020 1431 4-Chloroaniline 130 13 N 1 10 17-106 09/23/2020 1431 bis(2-Chloroethoxy)methane 130 100 1 78 39-108 09/23/2020 1431 bis(2-Chloroethyl)ether 130 110 1 79 32-105 09/23/2020 1431 2-Chloronaphthalene 130 100 1 77 31-127 09/23/2020 1431 2-Chlorophenol 130 98 1 73 37-106 09/23/2020 1431 4-Chlorophenyl phenyl ether 130 110 1 83 47-116 09/23/2020 1431 Chrysene 130 130 1 98 41-124 09/23/2020 1431 Dibenzo(a,h)anthracene 130 130 1 101 38-125 09/23/2020 1431 Dibenzofuran 130 110 1 81 45-112 09/23/2020 1431 3,3'-Dichlorobenzidine 130 87 1 65 10-119 09/23/2020 1431 2,4-Dichlorophenol 130 97 1 73 41-113 09/23/2020 1431 Diethylphthalate 130 120 1 89 49-123 09/23/2020 1431 Dimethyl phthalate 130 110 1 84 48-120 09/23/2020 1431 2,4-Dimethylphenol 130 110 1 84 33-123 09/23/2020 1431 Di-n-butyl phthalate 130 130 1 96 51-129 09/23/2020 1431 4,6-Dinitro-2-methyl phenol 130 85 1 64 40-130 09/23/2020 1431 2,4-Dinitrophenol 270 94 1 35 32-115 09/23/2020 1431 2,4-Dinitrotoluene 130 130 1 94 48-124 09/23/2020 1431 2,6-Dinitrotoluene 130 130 1 96 47-125 09/23/2020 1431 Di-n-octylphthalate 130 130 1 100 49-142 09/23/2020 1431 bis(2-Ethylhexyl)phthalate 130 140 1 102 45-128 09/23/2020 1431 Fluoranthene 130 110 1 83 26-133 09/23/2020 1431 Fluorene 130 110 1 82 19-108 09/23/2020 1431 Hexachlorobenzene 130 110 1 86 44-122 09/23/2020 1431 Hexachlorobutadiene 130 110 1 80 33-103 09/23/2020 1431 Hexachlorocyclopentadiene 670 600 1 90 18-121 09/23/2020 1431 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 54 of 87 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: VQ67519-002 Matrix: Solid Batch: 67519 Prep Method: 3546 Analytical Method: 8270E Prep Date: 09/22/2020 1800 Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Hexachloroethane 130 110 1 80 30-96 09/23/20201431 Indeno(1,2,3-c,d)pyrene 130 130 1 94 42-123 09/23/20201431 Isophorone 130 130 1 95 41-113 09/23/20201431 2-Methyl naphthalene 130 110 1 83 10-107 09/23/20201431 2-Methylphenol 130 72 1 55 32-107 09/23/20201431 3+4-Methylphenol 130 92 1 69 39-108 09/23/20201431 Naphthalene 130 100 1 75 10-112 09/23/20201431 2-Nitroaniline 130 120 1 90 45-123 09/23/20201431 3-Nitroaniline 130 44 1 33 24-127 09/23/20201431 4-Nitroaniline 130 95 1 71 48-127 09/23/20201431 Nitrobenzene 130 120 1 91 33-114 09/23/20201431 2-Nitrophenol 130 110 1 80 35-108 09/23/20201431 4-Nitrophenol 270 170 1 62 18-154 09/23/20201431 N-Nitrosodi-n-propylamine 130 110 1 84 32-115 09/23/20201431 N-Nitrosodiphenylamine (Diphenylamine) 130 130 1 94 53-150 09/23/2020 1431 Pentachlorophenol 270 180 1 67 27-138 09/23/20201431 Phenanthrene 130 110 1 83 16-123 09/23/20201431 Phenol 130 90 1 68 36-108 09/23/20201431 Pyrene 130 130 1 97 34-121 09/23/20201431 Pyridine 130 120 1 94 30-130 09/23/20201431 2,4,5-Trichlorophenol 130 89 1 67 46-122 09/23/20201431 2,4,6-Trichlorophenol 130 70 1 53 38-115 09/23/20201431 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 75 33-102 2-Fluorophenol 74 35-115 Nitrobenzene-d5 92 22-109 Phenol-d5 73 33-122 Terphenyl-d14 93 41-120 2,4,6-Tribromophenol 63 30-117 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 55 of 87 MA EPH (aliphatics) - MB Sample ID: VQ67274-001 Matrix: Solid Batch: 67274 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Parameter Result Q Dil LOQ DL Units Analysis Date C9 - C18 Aliphatics ND 1 10 10 mg/kg 09/28/2020 1725 C19 - C36 Aliphatics ND 1 10 10 mg/kg 09/28/2020 1725 Acceptance Surrogate Q % Rec Limit 1-Chloro-octadecane (aliphatic) 69 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 56 of 87 MA EPH (aliphatics) - LCS Sample ID: VQ67274-002 Matrix: Solid Batch: 67274 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Spike Amount Result % Rec Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date C9 - C18 Aliphatics 30 17 1 56 40-140 09/25/2020 1356 C19 - C36 Aliphatics 40 24 1 61 40-140 09/25/2020 1356 Acceptance Surrogate Q % Rec Limit 1-Chloro-octadecane (aliphatic) 52 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 57 of 87 MA EPH (aliphatics) - LCSD Sample ID: VQ67274-003 Matrix: Solid Batch: 67274 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Spike Amount Result % Rec % RPD Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date C9 - C18 Aliphatics 30 18 1 60 7.0 40-140 25 09/25/2020 1426 C19 - C36 Aliphatics 40 25 1 63 4.0 40-140 25 09/25/2020 1426 Acceptance Surrogate Q % Rec Limit 1-Chloro-octadecane (aliphatic) 54 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 58 of 87 MA EPH (aromatics) - MB Sample ID: VQ67275-001 Matrix: Solid Batch: 67275 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Parameter Result Q Dil LOQ DL Units Analysis Date C11 - C22 Aromatics ND 1 10 10 mg/kg 09/28/2020 1755 Acceptance Surrogate Q % Rec Limit 2-Bromonaphthalene (fractionation 2) 89 40-140 2-Fluorobiphenyl (fractionation 1) 90 40-140 o - Terphenyl (aromatic) 75 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 59 of 87 MA EPH (aromatics) - LCS Sample ID: VQ67275-002 Matrix: Solid Batch: 67275 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Spike Amount Result % Rec Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date C11 - C22 Aromatics 85 42 1 49 40-140 09/25/2020 1843 Surrogate Q % Rec Acceptance Limit 2-Bromonaphthalene (fractionation 2) 76 40-140 2-Fluorobiphenyl (fractionation 1) 86 40-140 o - Terphenyl (aromatic) 72 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 60 of 87 MA EPH (aromatics) - LCSD Sample ID: VQ67275-003 Matrix: Solid Batch: 67275 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Spike Amount Result % Rec % RPD Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date C11 - C22 Aromatics 85 43 1 50 1.8 40-140 25 09/25/2020 1913 Acceptance Surrogate Q % Rec Limit 2-Bromonaphthalene (fractionation 2) 75 40-140 2-Fluorobiphenyl (fractionation 1) 84 40-140 o - Terphenyl (aromatic) 73 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 61 of 87 TPH - DRO - MB Sample ID: VQ67842-001 Matrix: Solid Batch:67842 Prep Method: 3550C Analytical Method: 8015C Prep Date: 09/24/2020 2302 Parameter Result Q Dil LOQ DL Units Analysis Date TPH-DRO ND 1 6700 3300 ug/kg 09/26/20201736 Acceptance Surrogate Q % Rec Limit o - Terphenyl 82 55-120 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 62 of 87 TPH - DRO - LCS Sample ID: VQ67842-002 Matrix: Solid Batch:67842 Prep Method: 3550C Analytical Method: 8015C Prep Date: 09/24/2020 2302 Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date TPH-DRO 83000 73000 1 88 70-130 09/26/20201755 Surrogate Q % Rec Acceptance Limit o - Terphenyl 86 55-120 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 63 of 87 MA EPH (aliphatics) - Unfractionated - MB Sample ID: VQ68223-001 Matrix: Solid Batch: 68223 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Parameter Result Q Dil LOQ DL Units Analysis Date C19 - C36 Aliphatics - Unfractionated ND 1 10 10 mg/kg 09/25/2020 2246 C9 - C18 Aliphatics - Unfractionated ND 1 10 10 mg/kg 09/25/2020 2246 Acceptance Surrogate Q % Rec Limit 1-Chloro-octadecane (aliphatic) - Unfractionated 50 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 64 of 87 MA EPH (aliphatics) - Unfractionated - LCS Sample ID: VQ68223-002 Matrix: Solid Batch: 68223 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Spike Amount Result % Rec Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date C19 - C36 Aliphatics - Unfractionated 90 84 1 93 40-140 09/28/2020 2158 C9 - C18 Aliphatics - Unfractionated 65 54 1 83 40-140 09/28/2020 2158 Acceptance Surrogate Q % Rec Limit 1-Chloro-octadecane (aliphatic) - Unfractionated 87 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 65 of 87 MA EPH (aliphatics) - Unfractionated - LCSD Sample ID: VQ68223-003 Matrix: Solid Batch: 68223 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Spike Amount Result % Rec % RPD Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date C19 - C36 Aliphatics - Unfractionated 90 89 1 99 5.9 40-140 25 09/28/2020 2228 C9 - C18 Aliphatics - Unfractionated 65 58 1 89 6.3 40-140 25 09/28/2020 2228 Acceptance Surrogate Q % Rec Limit 1-Chloro-octadecane (aliphatic) - Unfractionated 90 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 66 of 87 MA EPH (aromatics) - Unfractionated - MB Sample ID: VQ68230-001 Matrix: Solid Batch: 68230 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Parameter Result Q Dil LOQ DL Units Analysis Date C11 - C22 Aromatics - Unfractionated ND 1 10 10 mg/kg 09/25/2020 2246 Acceptance Surrogate Q % Rec Limit o - Terphenyl (aromatic) - Unfractionated 77 40-140 2-Fluorobiphenyl (fractionation 1) 97 40-140 2-Bromonaphthalene (fractionation 2) 84 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 67 of 87 MA EPH (aromatics) - Unfractionated - LCS Sample ID: VQ68230-002 Matrix: Solid Batch: 68230 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Spike Amount Result % Rec Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date C11 - C22 Aromatics - Unfractionated 140 110 1 78 40-140 09/28/2020 2158 Surrogate Q % Rec Acceptance Limit o - Terphenyl (aromatic) - Unfractionated 77 40-140 2-Fluorobiphenyl (fractionation 1) 94 40-140 2-Bromonaphthalene (fractionation 2) 97 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 68 of 87 MA EPH (aromatics) - Unfractionated - LCSD Sample ID: VQ68230-003 Matrix: Solid Batch: 68230 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 09/21/2020 0856 Spike Amount Result % Rec % RPD Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date C11 - C22 Aromatics - Unfractionated 140 120 1 84 6.5 40-140 25 09/28/2020 2228 Acceptance Surrogate Q % Rec Limit o - Terphenyl (aromatic) - Unfractionated 80 40-140 2-Fluorobiphenyl (fractionation 1) 96 40-140 2-Bromonaphthalene (fractionation 2) 98 40-140 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 69 of 87 TPH - GRO - MB Sample ID: VQ67216-001 Matrix: Solid Batch: 67216 Prep Method: 5030E Analytical Method: 8015C Parameter Result Q Dil LOQ DL Units Analysis Date TPH-GRO ND 1 5000 2500 ug/kg 09/17/2020 2242 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 104 23-179 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 70 of 87 TPH - GRO - LCS Sample ID: VQ67216-002 Matrix: Solid Batch: 67216 Prep Method: 5030E Analytical Method: 8015C Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date TPH-GRO 50000 58000 1 116 70-130 09/17/2020 2111 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 122 23-179 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 71 of 87 TPH - GRO - LCSD Sample ID: VQ67216-003 Matrix: Solid Batch: 67216 Prep Method: 5030E Analytical Method: 8015C Spike Amount Result % Rec % RPD Parameter (ug/kg) (ug/kg) Q Dil % Rec % RPD Limit Limit Analysis Date TPH-GRO 50000 51000 1 102 12 70-130 20 09/17/2020 2134 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 86 23-179 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 72 of 87 MADEP VPH (aliphatics) - MB Sample ID: VQ67245-001 Matrix: Solid Batch: 67245 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Parameter Result Q Dil LOQ DL Units Analysis Date C5 - C8 Aliphatics ND 1 3.8 0.75 mg/kg 09/19/2020 1806 C9 - C12 Aliphatics ND 1 3.8 0.75 mg/kg 09/19/2020 1806 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 91 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 73 of 87 MADEP VPH (aliphatics) - LCS Sample ID: VQ67245-002 Matrix: Solid Batch: 67245 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date C5 - C8 Aliphatics 7.5 6.6 1 87 70-130 09/19/2020 1723 C9 - C12 Aliphatics 8.8 8.9 1 102 70-130 09/19/2020 1723 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 91 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 74 of 87 MADEP VPH (aliphatics) - LCSD Sample ID: VQ67245-003 Matrix: Solid Batch: 67245 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec % RPD Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date C5 - C8 Aliphatics 7.5 7.9 1 105 18 70-130 25 09/19/2020 1634 C9 - C12 Aliphatics 8.8 9.7 1 ill 8.6 70-130 25 09/19/2020 1634 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 99 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 75 of 87 MADEP VPH (aromatics) - MB Sample ID: VQ67246-001 Matrix: Solid Batch: 67246 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Parameter Result Q Dil LOQ DL Units Analysis Date C9 - C10 Aromatics ND 1 1.3 0.50 mg/kg 09/19/2020 1806 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 92 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 76 of 87 MADEP VPH (aromatics) - LCS Sample ID: VQ67246-002 Matrix: Solid Batch: 67246 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date C9 - C10 Aromatics 1.3 1.2 1 96 70-130 09/19/2020 1723 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 92 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 77 of 87 MADEP VPH (aromatics) - LCSD Sample ID: VQ67246-003 Matrix: Solid Batch: 67246 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec % RPD Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date C9 - C10 Aromatics 1.3 1.4 1 112 15 70-130 25 09/19/2020 1634 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 100 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 78 of 87 MADEP VPH (aliphatics) - MB Sample ID: VQ67515-001 Matrix: Solid Batch: 67515 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Parameter Result Q Dil LOQ DL Units Analysis Date C5 - C8 Aliphatics ND 1 3.8 0.75 mg/kg 09/22/2020 1711 C9 - C12 Aliphatics ND 1 3.8 0.75 mg/kg 09/22/2020 1711 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 93 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 79 of 87 MADEP VPH (aliphatics) - LCS Sample ID: VQ67515-002 Matrix: Solid Batch: 67515 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date C5 - C8 Aliphatics 7.5 6.4 1 85 70-130 09/22/2020 1614 C9 - C12 Aliphatics 8.8 8.4 1 96 70-130 09/22/2020 1614 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 84 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 80 of 87 MADEP VPH (aliphatics) - LCSD Sample ID: VQ67515-003 Matrix: Solid Batch: 67515 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec % RPD Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date C5 - C8 Aliphatics 7.5 6.9 1 92 8.2 70-130 25 09/22/2020 1642 C9 - C12 Aliphatics 8.8 8.6 1 98 2.6 70-130 25 09/22/2020 1642 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 87 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 81 of 87 MADEP VPH (aromatics) - MB Sample ID: VQ67516-001 Matrix: Solid Batch: 67516 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Parameter Result Q Dil LOQ DL Units Analysis Date C9 - C10 Aromatics ND 1 1.3 0.50 mg/kg 09/22/2020 1711 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 100 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 82 of 87 MADEP VPH (aromatics) - LCS Sample ID: VQ67516-002 Matrix: Solid Batch: 67516 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date C9 - C10 Aromatics 1.3 1.2 1 96 70-130 09/22/2020 1614 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 83 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 83 of 87 MADEP VPH (aromatics) - LCSD Sample ID: VQ67516-003 Matrix: Solid Batch: 67516 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec % RPD Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date C9 - C10 Aromatics 1.3 1.2 1 96 0.00 70-130 25 09/22/2020 1642 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 92 70-130 LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 % + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 84 of 87 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 85 of 87 PACE ANALYTICAL SERVICES, LLC Lj J LU W � � o � W 31 a n /LV dp LJ L r am � I t a I agsa�nr� "• `"4 �+4 i"7 5wL wr ❑ Q Cy J x I l f u 4 o, C 1 tl 4 I ti a1 *sf �4 Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 86 of 87 PACE ANALYTICAL SERVICES, LLC paaim:iu hluuhct- h1013018C. t4 Ur'". �c riuc: aarzr�u I x Sample �t�ceipt Checklist (SRC) Client -SUMMIT Ooolcr Ins ected b kiate: KEE 1 9116lA) Loxil: V116120 11 MegriSufrceLipt; (( SLSI Cliesr.t ❑ UPS ❑ FolEx (Zer: — [ J Yes ❑ N0 I . Wurc custody snls pmsmt mi tho Cooler? Yes No 71A 2, ff eu t(,cl peals vet a pt ent w r lac y intac'_ altrk unh k lCen' pl I Strip 1D- NA - C hlr� tree Ship 1D: -KA ve-sted by: Original 1=pwatur,e upon rtemp� / Derived (Cornccle;J) J.crnperaturc upon racei-it %S41id SnLp-Cup 1lJ: H-143$ 3.7 f17 off± NA /-NA ¢C NA {NA NA INA oe Method; ®-Temperature Blank E]Against Bottles lid GLui Ir): 5 1R Can Carfection Fat;tw, I;t °C MetliodoC'coo]ant R) Wcl Tw,, El icepac'� El I) IU ❑ N*rc ~— Yes ❑ Nr) V NA 3. Iftemperature of anv cooler axjLcdad 6.011(, uaq Prr'ect Manager R oa 'fiod! PM wss NDti#ieal l,y: phone i eTml ! fie -to -face (C, i role oTL" CI Ym ❑ .,IL 0 Nei 4, Is [he tominerda[ tour''-er'A paQkbl slip 2raclarxl 10 Ibis f nin? Yes 1 Rln; i. Vk+ctr proper um ody procedures (ee[;netuishedfreceiwed) fulloti T&? ® Yrsl El No 6- WK-,ro simple IDS listed on the COC' 7. Wefe"urr,frll. 1DS listed an -311 snmplC Collta=,rcrs? ® Yes ❑ No Ycs ❑ No S. Was collectirn date & tune listed on the COC7 - ® Yes No 9. Was rullcod nn dae &lime Hsted ante!! satinolc eantairer5? 0 Yex g NO A Did all contaiacr :abet informatlan (1D, date, cirn{) aerce wish the COO ® Ycs Ll No 11. `Ncrc =s to he performed listed on tltc COO? � Yeses El No 12, Did a]I smrnples arrive in tho proper co-ntaine % for cxch teas[ and/or in gu4A condition (unbroker., ]ids on, ® YCS ❑ lD : 13- HR a-dequate sample valume ava,lablo$ Ya& 0 No 14. Wcre all 6arr1 Jcs mceivW w:1h:n �4 ahe holds-ng tune Or 8 hours. whicitev r comes lirsC? TNo 15- Were tmy sarri les containers inisslr5gfcxecss (circle one) samples Not limcxl on CoC? Q Ycs I] No ® NA 16. for VOA and RSK-J 7S sample,,, wom bubbles lrres��l "pea -sine" {'/a"ar t?in,rr in wiaantrter} is any of Ow VOA vials" Yes 77Nfi 61 NA 17- 1Wom all DJRWine+alsir uYient samples received at a pi -I of < 2? -- ❑ Yesi ❑ No NA 19. Were all oyatiide scrnplcs received ar a 7H> 12 and smMdc sample's reecIvod at a pH !;� 9'^ El Y Q R10 9. W"- all applicabIt- NH&rrK'+T uyHnidn; phenolJ62 ({ 0, M&IL sample.% free OfreSi-d ctl allJurn iy? LesV., ❑ N,) ® NA 20, Were Plicn4 r;,m3:'ks?req-,Ar is (Le- Ielncstud dilutions. MTMSD designatiot-►s, etc--,] eorrcclly transr;ribed from the COO into the Comment section in LIMS2 Na 21- %Vas the gate number li;_tad on the container label? Jf ye s,, Quote ' iwll Jnplc 1Prcservatina (Micst ba oorilpkicrl for 3ry carr.ple(s) incorreudy pmaerved or with hea LipmL-r.) Sampk(.3) NA were itccivcd incorren(ly Preserval and wcm adjusted accordinoy ' in .mmplc reveivitkl; with NA trll_. of circle olx-r: H2SO4, I IN01, HC'I, NvDI4 usiT�g SR # NA Time oFprescrvation H_'L If mare than orr-, preservn:ive is n=ded, please Note in the cr,rrtTrtcnts Meow. SainpAs, NA ~ were received with bubbles >G min in diatnator. Samples(s) NA _ received with T]RC > 0.51ngiL (If #r19 is Hrr) srncl kvem ad.j--isted atccurdingly� in sample receiv;ng with so&urn thiosulfate (Na,S20) ►,� th Shealy l'D: NA Slf Niruode. laltels applied tv}: KILH2 Tale; q}IIV20 i'�:n,ntcntr:= Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 87 of 87 Beverly, Trudy From: Beverly, Trudy Sent: Monday, November 16, 2020 6:53 AM To: Michael Zavislak; Steffens, Steven; Joseph Stritmatter Os@trifectainc.com) Cc: Kevin Aguilera; Mike Fitzsimmons; Kyle Bilafer Subject: RE: [External] RE: Republic Services Received. Have a great day, Trudy Trudy Beverly, L.G. D- I E Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality Q, Dr" 'el UST Section, Mooresville Regional Office 704.235.2182 (Office) Trudy. B everlykncdenn gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: ht_pt s://deg.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: https:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-program INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httos://dea.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-ais-mans File Review Procedures: hitps://deq.ne. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): bit.ps://deq.nc.gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: htti)s:Hfiles.ne.izov/ncdea[Waste%2OMana2ement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policv.l)df https:Hfiles.nc.gov/ncdeq/Waste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx From: Michael Zavislak [mailto:mzavislak@summit-companies.com] Sent: Friday, November 13, 2020 6:33 PM To: Beverly, Trudy <trudy.beverly@ncdenr.gov>; Steffens, Steven <ssteffens@messer.com>; Joseph Stritmatter (js@trifectainc.com) <js@trifectainc.com> Cc: Kevin Aguilera <kevin.aguilera@waynebrothers.com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com>; Kyle Bilafer <KDBilafer@cabarruscounty.us> Subject: RE: [External] RE: Republic Services ' • I email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to c. ov Initial Abatement Action Report attached. From: Beverly, Trudy <trudy.beverly@ncdenr.eov> Sent: Thursday, November 12, 2020 11:23 AM To: Michael Zavislak <mzavislak@summit-companies.com>; Steffens, Steven <ssteffens@messer.com>; Marston, John <JMarston@republicservices.com> Cc: Kevin Aguilera <kevin.aguilera@Wayne brothers. com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com>; Kyle Bilafer <KDBilafer@cabarruscounty.us> Subject: RE: [External] RE: Republic Services Michael, The disposal facility should provide you with a disposal certificate or a receipt for payment. Trudy Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management of D-. North Carolina Department of Environmental Quality UST Section, Mooresville Regional Office `�" t,l vly/ 704.235.2182 (Office) Trudy.BeverlyL&ncdenr.gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: https:Hdeq.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-program INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httns://deo.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-mans File Review Procedures: https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): https://deq.nc.gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: https:Hfiles.nc.izov/ncdeci/W aste%2OMana2ement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policv.pdf https://files.nc.gov/ncdeq/Waste%2OManagement/DWM/UST/Corrective%2OAction/UST%20file%20names%2Ofor%2OLaserfiche.docx From: Michael Zavislak [mailto:mzavislak@summit-companies.com] Sent: Thursday, November 12, 2020 10:28 AM To: Steffens, Steven <ssteffens@messer.com>; Marston, John <JMarston@republicservices.com> Cc: Kevin Aguilera <kevin.aguilera@waynebrothers.com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com>; Kyle Bilafer <KDBilafer@cabarruscounty.us>; Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: [External] RE: Republic Services External email. Do not click links or open attachments unless you verify. Send all suspi09 report.spam@nc.eov They sent me an email that the tank was sent as part of the soil disposal. I can use that email as documentation of disposal. From: Steffens, Steven <ssteffens@messer.com> Sent: Thursday, November 12, 2020 9:46 AM To: Michael Zavislak <mzavislak@summit-companies.com>; Marston, John <JMarston@republicservices.com> Cc: Kevin Aguilera <kevin.aguilera@waynebrothers.com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com>; Kyle Bilafer <KDBilafer@cabarruscounty.us>; trudy.beverly@ncdenr.gov; Steffens, Steven <ssteffens@messer.com> Subject: RE: Republic Services Michael, A couple emails below I asked is this what you needed and you replied yes. Did Wayne Brother's not send the tank manifest in the info they provided? Steve Steffens Sr. Superintendent Messer Construction Co. 2400 Executive St. I Charlotte, NC 128208 NC License #: 70194 (704) 679-6000 Office (704) 679-6090 Fax (513) 600-1434 Mobile messer.com I Twitter I LinkedIn ssteffenskmesser.com From: Michael Zavislak<mzavislak@summit-comaanies.com> Sent: Thursday, November 12, 2020 9:32 AM To: Steffens, Steven <ssteffens@messer.com>; Marston, John <JMarston@republicservices.com> Cc: Kevin Aguilera <kevin.aguilera@waynebrothers.com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com>; Kyle Bilafer <KDBilafer@cabarruscounty.us>; trudy.beverly@ncdenr.gov Subject: RE: Republic Services * * * * Unverified External Email - Click With Caution! * * * * Yes, if I can get the tank disposal manifest of the certificate of disposal. From: Steffens, Steven <ssteffens@messer.com> Sent: Thursday, November 12, 2020 9:30 AM To: Michael Zavislak <mzavislak@summit-companies.com>; Marston, John <JMarston@republicservices.com> Cc: Kevin Aguilera <kevin.aguilera@waynebrothers.com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com>; Steffens, Steven <ssteffens@messer.com>; Kyle Bilafer <KDBilafer@cabarruscounty.us>; trudy.beverly@ncdenr.gov Subject: RE: Republic Services Great. Do you think this can be closed out by COB tomorrow? Steve Steffens Sr. Superintendent Messer Construction Co. 2400 Executive St. I Charlotte, NC 128208 NC License #: 70194 704) 679-6000 Office 704) 679-6090 Fax (513) 600-1434 Mobile messer.com I Twitter I LinkedIn ssteffenskmesser.com ' .V vssar Verif-va .rtarrei =rrad From: Michael Zavislak <mzavislak(d)summit-comaanies.com> Sent: Thursday, November 12, 2020 9:23 AM To: Steffens, Steven <ssteffens@messer.com>; Marston, John <JMarston@republicservices.com> Cc: Kevin Aguilera <kevin.aguilera@waynebrothers.com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com> Subject: RE: Republic Services * * * * Unverified External Email - Click With Caution! * * * * Yes, this is what I needed for the soil disposal, for the NCDEQ report. From: Steffens, Steven <ssteffens@messer.com> Sent: Thursday, November 12, 2020 9:09 AM To: Michael Zavislak <mzavislak@summit-companies.com>; Marston, John <JMarston@republicservices.com> Cc: Kevin Aguilera <kevin.aguilera@waynebrothers.com>; Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com> Subject: FW: Republic Services Michael and John, Is this what you are looking for? Steve Steffens Sr. Superintendent Messer Construction Co. 2400 Executive St. I Charlotte, NC 128208 NC License #: 70194 (704) 679-6000 Office (704) 679-6090 Fax (513) 600-1434 Mobile messer.com I Twitter I LinkedIn ssteffenskmes ser. com Vpssar +ferif:pa `• .rtarrei =rrad From: Kevin Aguilera<kevin.aguilera@wavnebrothers.com> Sent: Thursday, November 12, 2020 8:51 AM To: Steffens, Steven <ssteffens@messer.com> Cc: Mike Fitzsimmons <mike.fitzsimmons@waynebrothers.com> Subject: Republic Services * * * * Unverified External Email - Click With Caution! **** Steve, Please see attached Manifest and sales tickets from Republic Services. Thanks, L" Nype bvftl Kevin Aguilera Assistant Project Engineer Commercial Group INI user INIesser WeAmBuDding. INIesser V*AmBu%dIny. (704)305-1956 (704)305-1956 www.WayneBrothers.com 357 Concrescere Parkway I Davidson I NC 1 28036 9