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HomeMy WebLinkAboutMO-88833_96073_CA_O_20210518_Groundwater Monitoring Report;ETC ENVIRONMENTAL • GEOTECHNICAL BUILDING SCIENCES • MATERIALS TESTING May 18, 2021 Ms. Trudy Beverly North Carolina Department of Environmental Quality Division of Waste Management, UST Section Mooresville Regional Office 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115 Re: Groundwater Sampling Activities Pepsi Emergency Response (Fuel Spill) Pepsi Bottling Ventures, LLC Harrisburg Facility 22 Pepsi Way Harrisburg, North Carolina 28075 ATC Project No. PEPSI043 Dear Ms. Beverly: 609A Piner Road, Suite 115 Wilmington, North Carolina 28409 Telephone 919-871-0999 Fax 919-871-0335 www.atcgroupservices.com ATC Associates of North Carolina, P.C. (ATC), on behalf of Pepsi Bottling Ventures, LLC (PBV), has prepared this letter report regarding groundwater sampling activities conducted at 22 Pepsi Way in Harrisburg, North Carolina. These activities were conducted in response to a petroleum -release as a result of a malfunction of a fire pump filter, which allowed approximately 35 to 40 gallons of diesel fuel to be released from the generator system, as previous reported in a letter report dated April 23, 2021. TEMPORARY WELL INSTALLATION Due to the presence of a dissolved bis(2-Ethylhexyl)phthalate concentration above its established 2L Standard in temporary monitoring well GW-1, a second temporary monitoring well (GW-2) was installed in approximately the same location as GW-1 so a groundwater sample could be collected to confirm the presence or absence of this compound above its established 2L Standard. On May 7, 2021, temporary monitoring well GW-2 was installed by a North Carolina licensed driller with SAEDACCO, Inc., under supervision of personnel from ATC. The location of the temporary monitoring well is depicted on Attachment T Temporary monitoring well GW-2 was installed to a depth of approximately 17 feet below ground surface (bgs). The well was installed using direct -push technology and constructed of one -inch diameter well casing made of flush joint, threaded schedule-40 poly vinyl chloride (PVC) pipe. The PVC well screen is 0.010-inch slot with a screened interval often feet. Following sample collection, the temporary monitoring well was removed and the boring was properly abandoned. ;ETC May 18, 2021 Page 2 of 2 On May 7, 2021, a groundwater sample was collected from temporary monitoring well GW-2. Prior to sample collection, the temporary well was purged with a field -decontaminated peristaltic pump and dedicated tubing. The sample was collected directly into laboratory -approved containers, packed in ice, and delivered under chain -of -custody to SGS in Scott, Louisiana for analyses. The groundwater sample from monitoring well GW-2 was analyzed by Environmental Protection Agency (EPA) Method 625 plus ten highest non -target peaks. Laboratory analytical results of the groundwater sample from temporary well GW-2 detected a dissolved naphthalene concentration above the laboratory method detection limit (MDL). It should be noted dissolved bis(2-Ethyl hexyl)phthal ate was not detected above its laboratory MDL. The tabulated groundwater analytical results are provided in Attachment 11. The laboratory report and chain -of -custody documents are provided in Attachment 111. CONCLUSIONS Based on the above activities and subsequent laboratory results, the petroleum -related impacts to groundwater in the spill area appear negligible. No other activities are warranted at this time. If you have any questions or require additional information, please contact our office at (919) 871-0999. Sincerely, ATC Associates of N ENS < Maureen lacksor>! 1'.C:. i Senior Project MV �0 lO L QG�SfG�� ,� y ♦ N A- �Pa�♦♦ cc: Mr. Bill Peterson, Attachments Gabriel Araos, P.E. Senior Project Manager entures, LLC Attachment I 19 `m EHVIHGNMEHTAL • GEGTECHNICAL 6 I GIN • I •N MATERIALSMAIERIALS T S- Project No. PEPS1043 pep l WaY 609A Piner Road, Suite 115 Wilmington, North Carolina 28409 (919)871-0999 DATE: 04/22/2021 PM: Maureen Jackson Figure 1 - Soil Excavation — Diesel Fuel Spill PBV Harrisburg 22 Pepsi Way Harrisburg, North Carolina Not to Attachment II TABLE 1 GROUNDWATER ANALYTICAL RESULTS PBV HARRISBURG 22 PEPSI WAY HARRISBURG, NORTH CAROLINA ATC PROJECT NO. PEPSI043 Analytical Method EPA Method 625 b o. Date � Well ID Sampled 1 *4 W IE� G W -1 4/ 12/2021 0.21 5.9 15' GW-2 5/7/2021 0.26 <4.7 26.9' 2L Standards (ug/L) 6 3 -- GCLs (ug/L) 6,000 135 -- Notes: 1. Concentrations reported in micrograms per liter (ug/L). 2. Concentrations in bold print equal or exceed the 2L Standard. 3. GCLs denotes Gross Contaminant Levels. 4. J denotes estimated concentration by laboratory. Attachment III ffm Scott, LA The results set forth herein are provided by SGS North America Inc. a-Hl ydcopy 2. 0 Automated Report Technical Report for ATC Group Services LLC PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC PEPSI043 SGS Job Number: LA71238 Sampling Date: 05/07/21 Report to: ATC Group Services LLC. 2725 East Millbrook Road Suite 121 Raleigh, NC 27604 maureen. jackson@atcgs. com; gabe. araos@atcgs. ATTN: Maureen Jackson Total number of pages in report: 19 Ac Fp Ar . Test results contained within this data package meet the requirements Ron Benj a illl n of the National Environmental Laboratory Accreditation Program Lab Director and/or state specific certification programs as applicable. Client Service contact: Christina Larriviere 337-237-4775 Certifications: LDEQ(2048), LDHH(LA150012), AR(14-045-04), AZ(AZ0805), FL(E87657), IL(200082), KY(#31), NC(487), SC(73004001), NJ(LA007), TX(T104704186-18-16), WV(257) This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 500 Ambassador Caffery • Scott, LA 70583 • tel: 337-237-4775 SGS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about Unauthorized modification of this report is strictly prohibited. how we can serve you better at: Review standard terms at: http://www.sgs.com/en/terms-and-conditions EHS.US.CustomerCare@sgs.com 1 of 19 LA71238 Sections: Table of Contents -I- Section1: Sample Summary................................................................................................... 3 Section2: Summary of Hits.................................................................................................... 4 Section3: Sample Results........................................................................................................ 5 3.1 LA71238-1: GW-2........................................................................................................ 6 Section4: Misc. Forms............................................................................................................ 9 4.1: Chain of Custody........................................................................................................... 10 Section 5: MS Semi-volatiles - QC Data Summaries............................................................ 12 5.1: Method Blank Summary................................................................................................ 13 5.2: Blank Spike/Blank Spike Duplicate Summary.............................................................. 16 W, SGS North America Inc. Sample Summary ATC Group Services LLC Job No: LA71238 PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC Project No: PEPSI043 Sample Collected Matrix Client Number Date Time By Received Code Type Sample I D This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the RL LA71238-1 05/07/21 11:00 CB 05/08/21 AQ Ground Water GW-2 6 3of19 LA71238 Summary of Hits Page 1 of 1 Job Number: LA71238 Account: ATC Group Services LLC Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC Collected: 05/07/21 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method LA71238-1 GW-2 Naphthalene 0.26 0.19 ug/1 EPA 625.1 Total TIC, Semi -Volatile 26.9 J ug/1 6 4of19 LA71238 FM Scott, LA Sample Results Report of Analysis i Section 3 6 5of19 LA71238 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID: GW-2 Lab Sample ID: LA71238-1 Date Sampled: 05/07/21 Matrix: AQ - Ground Water Date Received: 05/08/21 Method: EPA 625.1 EPA 625.1 Percent Solids: n/a Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 170073984.1) 1 05/11/21 14:43 BH 05/09/21 10:10 OP18562 EF2567 Run #2 Initial Volume Final Volume Run # 1 1070 ml 1.0 ml Run #2 ABN List for NC, May 2012 CAS No. Compound Result RL Units Q 65-85-0 Benzoic Acid ND 19 ug/l 59-50-7 4-Chloro-3-methyl Phenol ND 4.7 ug/l 95-57-8 2-Chlorophenol ND 4.7 ug/l 120-83-2 2,4-Dichlorophenol a ND 4.7 ug/1 105-67-9 2,4-Dimethylphenol ND 4.7 ug/l 51-28-5 2,4-Dinitrophenol ND 19 ug/l 534-52-1 4,6-Dinitro-o-cresol ND 9.3 ug/l 95-48-7 2-Methylphenol ND 4.7 ug/l 3&4-Methylphenol ND 4.7 ug/l 88-75-5 2-Nitrophenol ND 4.7 ug/l 100-02-7 4-Nitrophenol ND 23 ug/l 87-86-5 Pentachlorophenol a ND 9.3 ug/l 108-95-2 Phenol ND 4.7 ug/l 88-06-2 2,4,6-Trichlorophenol ND 4.7 ug/1 83-32-9 Acenaphthene ND 0.19 ug/l 208-96-8 Acenaphthylene ND 0.19 ug/l 120-12-7 Anthracene ND 0.19 ug/l 56-55-3 Benzo(a)anthracene ND 0.19 ug/l 50-32-8 Benzo(a)pyrene ND 0.19 ug/l 205-99-2 Benzo(b)fluoranthene ND 0.19 ug/1 191-24-2 Benzo(g,h,i)perylene ND 0.19 ug/l 207-08-9 Benzo(k)fluoranthene b ND 0.19 ug/l 100-51-6 Benzyl Alcohol ND 9.3 ug/l 101-55-3 4-13romophenyl Phenyl Ether a ND 4.7 ug/l 85-68-7 Butyl Benzyl Phthalate ND 4.7 ug/l 106-47-8 4-Chloroaniline ND 4.7 ug/l 111-91-1 bis(2-Chloroethoxy)methane ND 4.7 ug/l 111-44-4 bis(2-Chloroethyl)ether ND 4.7 ug/l 108-60-1 2,2'-Oxybis(1-chloropropane) ND 4.7 ug/l 91-58-7 2-Chloronaphthalene ND 4.7 ug/1 7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.7 ug/l 218-01-9 Chrysene ND 0.19 ug/l ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6of19 LA71238 SGS North America Inc. Report of Analysis Client Sample ID: GW-2 Lab Sample ID: LA71238-1 Date Sampled: 05/07/21 Matrix: AQ - Ground Water Date Received: 05/08/21 Method: EPA 625.1 EPA 625.1 Percent Solids: n/a Project: PBV-Harrisburg 22 Pepsi Way, Harrisburg, NC ABN List for NC, May 2012 CAS No. Compound Result RL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 0.19 ug/l 132-64-9 Dibenzofaran ND 4.7 ug/l 95-50-1 1,2-Dichlorobenzene ND 4.7 ug/l 541-73-1 1,3-Dichlorobenzene ND 4.7 ug/l 106-46-7 1,4-Dichlorobenzene ND 4.7 ug/1 91-94-1 3,3'-Dichlorobenzidine ND 9.3 ug/l 84-66-2 Diethyl Phthalate ND 4.7 ug/l 131-11-3 Dimethyl Phthalate ND 4.7 ug/l 84-74-2 Di-n-butyl Phthalate ND 4.7 ug/l 117-84-0 Di-n-octyl Phthalate ND 4.7 ug/l 122-66-7 1,2-Diphenylhydrazine ND 4.7 ug/l 117-81-7 bis(2-Ethylhexyl)phthalate ND 4.7 ug/1 206-44-0 Fluoranthene ND 0.19 ug/l 86-73-7 Fluorene ND 0.19 ug/l 118-74-1 Hexachlorobenzene a ND 4.7 ug/l 87-68-3 Hexachlorobutadiene a ND 4.7 ug/l 77-47-4 Hexachlorocyclopentadiene ND 9.3 ug/l 67-72-1 Hexachloroethane ND 4.7 ug/l 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.19 ug/l 78-59-1 Isophorone ND 4.7 ug/l 90-12-0 1-Methylnaphthalene ND 0.19 ug/l 91-57-6 2-Methylnaphthalene ND 0.19 ug/1 91-20-3 Naphthalene 0.26 0.19 ug/l 98-95-3 Nitrobenzene ND 4.7 ug/l 621-64-7 N-Nitroso-di-n-propylamine ND 4.7 ug/l 86-30-6 N-Nitrosodiphenylamine ND 4.7 ug/l 85-01-8 Phenanthrene ND 0.19 ug/l 129-00-0 Pyrene ND 0.19 ug/1 120-82-1 1,2,4-Trichlorobenzene ND 4.7 ug/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 28% 20-75% 4165-62-2 Phenol-d5 19% 10-60% 118-79-6 2,4,6-Tribromophenol 77% 38-138% 4165-60-0 Nitrobenzene-d5 82% 44-132% 321-60-8 2-Fluorobiphenyl 69% 40-119% 1718-51-0 Terphenyl-dl4 58% 40-127% Page 2 of 3 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7of19 LA71238 SGS North America Inc. Report of Analysis Client Sample ID: GW-2 Lab Sample ID: LA71238-1 Date Sampled: 05/07/21 Matrix: AQ - Ground Water Date Received: 05/08/21 Method: EPA 625.1 EPA 625.1 Percent Solids: n/a Project: PBV-Harrisburg 22 Pepsi Way, Harrisburg, NC ABN List for NC, May 2012 CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q unknown 4.65 14 ug/1 J unknown 8.08 8.5 ug/1 J 6946-24-3 Tetracosane, 1-bromo- 13.97 4.4 ug/1 JN Total TIC, Semi -Volatile 26.9 ug/1 J (a) Associated CCV outside of control limits high, sample was ND. (b) Associated CCV and BS/BSD outside of control limits high, sample was ND. Page 3 of 3 L ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 8of19 LA71238 ffm Scott, LA Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody 1 Section 4 6 9of19 LA71238 I ' CHAIN OF CUSTODY PAGE 1 OF � AAA a $ tr - ... _ .. 500 Ambassador Caffery Parkway, Scott, LA 70583 TEL. 337.237A775 FAX: 337.237.783814 —tigs.com/ehsusa reo-ExTnumsp mme o�aercowax __. o„p„y scs�xbN Client / Reporting information Pro ect Information Re auested Analysis see TEST CODE sheet Matrix Codes Company Name A 6 � u fr:{UiLcJ Project Na— r }��� - HarrLs,lf 1rr a \ (� i GIN-G king Water GIN -Grountl Wekr W W - Water SW - Surface Water so - soil SL-Sludge sEDs_ONant UD-Otherr Uqu0 aR-ar SOL-Other Solitl WP-Wipe FB-Fielaelank EB a -Mn. Blank RB -Rin Blank TD-Trip Blank Street Address �y,f {) /� n. (' 7tp06 W101-11 Rec rAl 1) ODr� Steel 6 /,,' ago 7-Z �C SI •=a -::' . Blllingin/or run if different from Re ort to city Skk Zip aMsk NL Z&Z73 City State Y*vrisbvr• NC Company Name Pmkct Conkct E-mail vv-en,)a4kSdneotc S•rom Pmiact# ��P51 Gti3 Steel gdemss Ph n # ^� I- ��+ _ 3 6 p 3 1 I Cbent Purchase Older# City State Tip Samplar(s) Names) Phone C � �Cwt�t C�IriG✓�.G �L(t trz-35y-v•n plalecl Manager gryentiore v V sanp.N Field ID I Point of Collection Callacaon NumbvdpresemaBpltles Lo ,Kheb Dam Tm. samwed Br MaldN xmes 8 a i W LqB USE ONLv - 2. 1100 L6 6W z I I X I Iz X Tumamuntl Tme Buslness V" knaartl ID Businesa Dayc a➢PrPye4 By(sGS PB):IDete: QSBusiness Oays RUSH 9 48mtness Days RUSH , //f 3 Business Days RUSH / t / 2 Business Days RUSH 1 Busiaoss Day EMERGENCY Other EmoM,e,yERshTlqdataavaiabievafablek.Aprovelneededfor RUSHIEmergeney TAT '" "p. Daly Deliverable lnfomtalion Commem5lS Ilnstnwtlons Qs Commer i I A '1-11) 0 TRRP Q Lommemlal'B"(Lavel2) Q RECAP Q FULLTI (Leve13+4) Q State Forms Q REDT1(Levo13+S) Q EDO Format Q Commombl "C" Q Other Commamlal'A' = Resuns Only. Commerdal'B' = Results+DC Summary Commercial'C'-Resulls+DCSummary+Par4al Raw Dak Ote: Sample inventory is verOV Upon receipt iR th}e� L'aborat✓o/ry 7.-VLt�✓'� i L✓V{� (�La y7� rz-zy -i� I) y} 17 1 / p +ry j //LtN� �Nj r rn a" `aL� f IV) y ` �_i'rs � 1 T / o " ✓i e�CLL'{'L r'Sr Lim PA G4ven ULYL j,;.n Sample Custody must be documented below each time samples change poesoasion, including courier daiivery. I nvu vabrs miler. S to Lkw: I'M Gr v 'ecelvode anguHlxtlO 2 o�r maj6; v i 2 elingriizM1e46 p r 3 L- ReesWe y' 3 Re" puts ea By'. ma: ,.S !'� Recei 4 ROI1neulsMaby: 5 Immo. R By: 5 C toNy Src+ala .._ Prewrveaw tie Onice �-- Ta UrJ Gi Cl c ❑ axe- M �� Tnem� 0: r EHSA-OAC D02"0-FORMSWft-Standard COO http:/A W.sgs.mm/en/tenns-ands ndiUons. LA71238: Chain of Custody Page 1 of 2 6 10 of 19 LA71238 2tl9 3L2tl/2JU95 f x S = i tea. �C.03cm s �z CC LL COC ae� OJU �G V J yF... ~ Q®. (HIRE RE Qr m LLU Q J G - L� Ui 0 - r N W wZ 1+ ¢r am N m � p 4 _ cm ZQC.0 J ..� r' LU WLU .Q O _—� cm CV Ec�xod V rrn y U- _ a� y y w C LA71238: Chain of Custody Page 2 of 2 6 11 of 19 LA71238 ffm Scott, LA MS Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries i no Section 5 6 12 of 19 LA71238 Method Blank Summary Job Number: LA71238 Account: ATCNCR ATC Group Services LLC Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC Page 1 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch DP18562-MB F0073975.D 1 05/11/21 BH 05/09/21 OP18562 EF2567 The QC reported here applies to the following samples: Method: EPA 625.1 LA71238-1 CAS No. Compound Result RL Units Q 65-85-0 Benzoic Acid ND 20 ug/l 59-50-7 4-Chloro-3-methyl Phenol ND 5.0 ug/l 95-57-8 2-Chlorophenol ND 5.0 ug/l 120-83-2 2,4-Dichlorophenol ND 5.0 ug/l 105-67-9 2,4-Dimethylphenol ND 5.0 ug/l 51-28-5 2,4-Dinitrophenol ND 20 ug/l 534-52-1 4,6-Dinitro-o-cresol ND 10 ug/l 95-48-7 2-Methylphenol ND 5.0 ug/l 3&4-Methylphenol ND 5.0 ug/l 88-75-5 2-Nitrophenol ND 5.0 ug/l 100-02-7 4-Nitrophenol ND 25 ug/l 87-86-5 Pentachlorophenol ND 10 ug/l 108-95-2 Phenol ND 5.0 ug/l 88-06-2 2,4,6-Trichlorophenol ND 5.0 ug/l 83-32-9 Acenaphthene ND 0.20 ug/1 208-96-8 Acenaphthylene ND 0.20 ug/l 120-12-7 Anthracene ND 0.20 ug/l 56-55-3 Benzo(a)anthracene ND 0.20 ug/l 50-32-8 Benzo(a)pyrene ND 0.20 ug/l 205-99-2 Benzo(b)fluoranthene ND 0.20 ug/1 191-24-2 Benzo(g,h,i)perylene ND 0.20 ug/l 207-08-9 Benzo(k)fluoranthene ND 0.20 ug/l 100-51-6 Benzyl Alcohol ND 10 ug/1 101-55-3 4-Bromophenyl Phenyl Ether ND 5.0 ug/l 85-68-7 Butyl Benzyl Phthalate ND 5.0 ug/l 106-47-8 4-Chloroaniline ND 5.0 ug/l 111-91-1 bis(2-Chloroethoxy)methane ND 5.0 ug/l 111-44-4 bis(2-Chloroethyl)ether ND 5.0 ug/l 108-60-1 2,2'-Oxybis(1-chloropropane) ND 5.0 ug/l 91-58-7 2-Chloronaphthalene ND 5.0 ug/l 7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.0 ug/1 218-01-9 Chrysene ND 0.20 ug/1 53-70-3 Dibenzo(a,h)anthracene ND 0.20 ug/l 132-64-9 Dibenzofuran ND 5.0 ug/l 95-50-1 1,2-Dichlorobenzene ND 5.0 ug/l 541-73-1 1,3-Dichlorobenzene ND 5.0 ug/1 6 13 of 19 LA71238 Method Blank Summary Job Number: LA71238 Account: ATCNCR ATC Group Services LLC Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC Page 2 of 3 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl )P18562-MB F0073975.D 1 05/11/21 BH 05/09/21 OP18562 EF2567 The QC reported here applies to the following samples: LA71238-1 CAS No. Compound Result RL Units Q 106-46-7 1,4-Dichlorobenzene ND 5.0 ug/l 91-94-1 3,3'-Dichlorobenzidine ND 10 ug/l 84-66-2 Diethyl Phthalate ND 5.0 ug/l 131-11-3 Dimethyl Phthalate ND 5.0 ug/l 84-74-2 Di-n-butyl Phthalate ND 5.0 ug/l 117-84-0 Di-n-octyl Phthalate ND 5.0 ug/l 122-66-7 1,2-Diphenylhydrazine ND 5.0 ug/l 117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 ug/l 206-44-0 Fluoranthene ND 0.20 ug/l 86-73-7 Fluorene ND 0.20 ug/l 118-74-1 Hexachlorobenzene ND 5.0 ug/l 87-68-3 Hexachlorobutadiene ND 5.0 ug/l 77-47-4 Hexachlorocyclopentadiene ND 10 ug/l 67-72-1 Hexachloroethane ND 5.0 ug/l 193-39-5 Indeno(1,2,3-cd)pyrene ND 0.20 ug/l 78-59-1 Isophorone ND 5.0 ug/l 90-12-0 1-Methylnaphthalene ND 0.20 ug/l 91-57-6 2-Methylnaphthalene ND 0.20 ug/l 91-20-3 Naphthalene ND 0.20 ug/l 98-95-3 Nitrobenzene ND 5.0 ug/1 621-64-7 N-Nitroso-di-n-propylamine ND 5.0 ug/l 86-30-6 N-Nitrosodiphenylamine ND 5.0 ug/l 85-01-8 Phenanthrene ND 0.20 ug/1 129-00-0 Pyrene ND 0.20 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 5.0 ug/l CAS No. Surrogate Recoveries Limits 367-12-4 2-Fluorophenol 47% 20-75% 4165-62-2 Phenol-d5 31% 10-60% 118-79-6 2,4,6-Tribromophenol 117% 38-138% 4165-60-0 Nitrobenzene-d5 98% 44-132% 321-60-8 2-Fluorobiphenyl 88% 40-119% 1718-51-0 Terphenyl-d14 99% 40-127% Method: EPA 625.1 6 14 of 19 LA71238 Method Blank Summary Job Number: LA71238 Account: ATCNCR ATC Group Services LLC Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC Page 3 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP18562-MB 170073975.1) 1 05/11/21 BH 05/09/21 OP18562 EF2567 The QC reported here applies to the following samples: LA71238-1 Method: CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q Total TIC, Semi -Volatile 0 ug/1 6 15 of 19 LA71238 Blank Spike/Blank Spike Duplicate Summary Job Number: LA71238 Account: ATCNCR ATC Group Services LLC Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC Page 1 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP18562-BS F0073976.D 1 05/11/21 BH 05/09/21 OP18562 EF2567 OP18562-BSD F0073977.D 1 05/11/21 BH 05/09/21 OP18562 EF2567 The QC reported here applies to the following samples: Method: EPA 625.1 LA71238-1 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/1 % ug/1 % RPD Rec/RPD 65-85-0 Benzoic Acid 100 25.1 25 30.2 30 18 12-61/34 59-50-7 4-Chloro-3-methyl Phenol 50 46.5 93 47.1 94 1 66-103/19 95-57-8 2-Chlorophenol 50 41.8 84 43.9 88 5 63-93/17 120-83-2 2,4-Dichlorophenol 50 51.4 103 52.3 105* a 2 70-104/18 105-67-9 2,4-Dimethylphenol 50 47.3 95 47.6 95 1 64-98/20 51-28-5 2,4-Dinitrophenol 50 49.8 100 51.7 103 4 40-138/24 534-52-1 4,6-Dinitro-o-cresol 50 57.2 114 57.7 115 1 57-131/21 95-48-7 2-Methylphenol 50 35.2 70 36.2 72 3 53-83/18 3&4-Methylphenol 50 32.9 66 33.6 67 2 51-77/18 88-75-5 2-Nitrophenol 50 52.9 106 54.5 109 3 67-114/18 100-02-7 4-Nitrophenol 50 21.0 42 20.9 42 0 23-62/28 87-86-5 Pentachlorophenol 50 59.0 118* a 58.0 116* a 2 56-113/22 108-95-2 Phenol 50 17.3 35 17.5 35 1 24-50/24 88-06-2 2,4,6-Trichlorophenol 50 54.7 109 54.8 110 0 65-116/19 83-32-9 Acenaphthene 50 46.2 92 46.6 93 1 69-107/18 208-96-8 Acenaphthylene 50 46.6 93 46.7 93 0 67-114/20 120-12-7 Anthracene 50 52.1 104 51.6 103 1 73-109/19 56-55-3 Benzo(a)anthracene 50 47.1 94 47.4 95 1 71-109/19 50-32-8 Benzo(a)pyrene 50 59.1 118* a 59.0 118* a 0 73-116/19 205-99-2 Benzo(b)fluoranthene 50 52.3 105 52.0 104 1 73-114/21 191-24-2 Benzo(g,h,i)perylene 50 49.8 100 50.1 100 1 75-113/19 207-08-9 Benzo(k)fluoranthene 50 62.9 126* b 62.5 125* b 1 71-118/19 100-51-6 Benzyl Alcohol 50 38.1 76 38.7 77 2 57-90/17 101-55-3 4-Bromophenyl Phenyl Ether 50 59.6 119* a 58.6 117* a 2 70-112/20 85-68-7 Butyl Benzyl Phthalate 50 49.0 98 49.4 99 1 72-118/20 106-47-8 4-Chloroaniline 50 45.6 91 44.4 89 3 60-105/17 111-91-1 bis(2-Chloroethoxy)methane 50 49.6 99 50.0 100 1 68-107/19 111-44-4 bis(2-Chloroethyl)ether 50 42.6 85 43.8 88 3 60-109/18 108-60-1 2,2'-Oxybis(1-chloropropane) 50 36.7 73 37.9 76 3 48-119/18 91-58-7 2-Chloronaphthalene 50 47.3 95 48.9 98 3 67-106/19 7005-72-3 4-Chlorophenyl Phenyl Ether 50 53.8 108 54.8 110 2 67-115/19 218-01-9 Chrysene 50 50.9 102 50.5 101 1 74-108/19 53-70-3 Dibenzo(a,h)anthracene 50 51.3 103 51.1 102 0 75-115/19 132-64-9 Dibenzofuran 50 50.7 101 51.3 103 1 69-110/19 95-50-1 1,2-Dichlorobenzene 50 38.4 77 40.9 82 6 56-95/19 541-73-1 1,3-Dichlorobenzene 50 36.6 73 38.7 77 6 53-93/20 * = Outside of Control Limits. 6 16 of 19 LA71238 Blank Spike/Blank Spike Duplicate Summary Job Number: LA71238 Account: ATCNCR ATC Group Services LLC Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC Page 2 of 3 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP18562-BS F0073976.D 1 05/11/21 BH 05/09/21 OP18562 EF2567 OP18562-BSD F0073977.D 1 05/11/21 BH 05/09/21 OP18562 EF2567 The QC reported here applies to the following samples: LA71238-1 CAS No. Compound Spike BSP BSP BSD ug/1 ug/1 % ug/l Method: EPA 625.1 BSD Limits % RPD Rec/RPD 106-46-7 1,4-Dichlorobenzene 50 37.9 76 40.0 80 5 54-93/19 91-94-1 3,3'-Dichlorobenzidine 50 56.3 113 56.1 112 0 67-114/19 84-66-2 Diethyl Phthalate 50 51.1 102 51.2 102 0 72-115/19 131-11-3 Dimethyl Phthalate 50 50.5 101 50.4 101 0 71-114/19 84-74-2 Di-n-butyl Phthalate 50 53.3 107 53.1 106 0 74-113/20 117-84-0 Di-n-octyl Phthalate 50 53.3 107 53.4 107 0 69-118/20 122-66-7 1,2-Diphenylhydrazine 50 54.2 108 54.1 108 0 70-114/19 117-81-7 bis(2-Ethylhexyl)phthalate 50 51.9 104 52.0 104 0 69-118/20 206-44-0 Fluoranthene 50 55.8 112 55.4 111 1 73-113/20 86-73-7 Fluorene 50 50.8 102 51.2 102 1 70-112/19 118-74-1 Hexachlorobenzene 50 59.3 119* a 59.2 118* a 0 71-111/20 87-68-3 Hexachlorobutadiene 50 41.5 83 42.8 86 3 45-101/21 77-47-4 Hexachlorocyclopentadiene 50 34.8 70 36.4 73 4 36-109/25 67-72-1 Hexachloroethane 50 33.4 67 35.5 71 6 47-94/20 193-39-5 Indeno(1,2,3-cd)pyrene 50 50.5 101 51.0 102 1 75-114/19 78-59-1 Isophorone 50 44.5 89 45.0 90 1 67-111/18 90-12-0 1-Methylnaphthalene 50 46.2 92 47.4 95 3 67-102/19 91-57-6 2-Methylnaphthalene 50 46.4 93 47.0 94 1 67-102/18 91-20-3 Naphthalene 50 45.3 91 45.7 91 1 66-100/18 98-95-3 Nitrobenzene 50 48.5 97 49.9 100 3 69-109/18 621-64-7 N-Nitroso-di-n-propylamine 50 44.2 88 45.9 92 4 62-113/18 86-30-6 N-Nitrosodiphenylamine 50 52.5 105 52.2 104 1 69-110/20 85-01-8 Phenanthrene 50 49.9 100 49.9 100 0 73-106/20 129-00-0 Pyrene 50 48.0 96 48.7 97 1 74-111/18 120-82-1 1,2,4-Trichlorobenzene 50 43.2 86 45.2 90 5 57-99/19 CAS No. Surrogate Recoveries BSP BSD Limits 367-12-4 2-Fluorophenol 50% 52% 20-75% 4165-62-2 Phenol-d5 34% 34% 10-60% 118-79-6 2,4,6-Tribromophenol 130% 128% 38-138% 4165-60-0 Nitrobenzene-d5 104% 106% 44-132% 321-60-8 2-Fluorobiphenyl 90% 92% 40-119% 1718-51-0 Terphenyl-d14 99% 98% 40-127% * = Outside of Control Limits. 6 17 of 19 LA71238 Blank Spike/Blank Spike Duplicate Summary Job Number: LA71238 Account: ATCNCR ATC Group Services LLC Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC Page 3 of 3 ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl )P18562-13S F0073976.D 1 05/11/21 BH 05/09/21 OP18562 EF2567 )P18562-BSD F0073977.D 1 05/11/21 BH 05/09/21 OP18562 EF2567 The QC reported here applies to the following samples: Method: EPA 625.1 LA71238-1 (a) Outside laboratory control limits but within reasonable method acceptance limits. (b) Outside control limits biased high. Analyte not detected in associated samples. * = Outside of Control Limits. 6 18 of 19 LA71238 Blank Spike/Blank Spike Duplicate Summary Job Number: LA71238 Account: ATCNCR ATC Group Services LLC Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC Page 1 of 1 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP18562-BS F0073978.D 1 05/11/21 BH 05/09/21 OP18562 EF2567 OP18562-BSD F0073979.D 1 05/11/21 BH 05/09/21 OP18562 EF2567 The QC reported here applies to the following samples: Method: EPA 625.1 LA71238-1 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/l % ug/l % RPD Rec/RPD CAS No. Surrogate Recoveries BSP BSD Limits 367-12-4 2-Fluorophenol 47% 53% 20-75% 4165-62-2 Phenol-d5 32% 35% 10-60% 118-79-6 2,4,6-Tribromophenol 113% 132% 38-138% 4165-60-0 Nitrobenzene-d5 86% 98% 44-132% 321-60-8 2-Fluorobiphenyl 81% 94% 40-119% 1718-51-0 Terphenyl-d14 96% 107% 40-127% * = Outside of Control Limits. 6 19 of 19 LA71238 Beverly, Trudy From: Maureen Jackson <maureenjackson@atcgs.com> Sent: Tuesday, May 25, 2021 11:59 AM To: Beverly, Trudy Subject: RE: [External] RE: PBV Harrisburg Letter Report CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Understand and thanks. Pepsi is just asking about it so they can get it settled on their end. Thanks again Maureen Jackson I SENIOR PROJECT MANAGER I ATC Group Services LLC Direct +1 919 561 3893 ATC 609A Piner Road Suite 115 1 Wilmington, NC 28409 maureen.jackson@atc. s� I www.atcciroupservices.com This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If you are not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is strictly prohibited. If you have received this email in error, please notify the sender by replying to this message and immediately delete and destroy any copies of this email and any attachments. The views or opinions expressed are the author's own and may not reflect the views or opinions of ATC. From: Beverly, Trudy [mailto:trudy.beverly@ncdenr.gov] Sent: Tuesday, May 25, 2021 11:58 AM To: Maureen Jackson <maureen.jackson@atcgs.com> Subject: RE: [External] RE: PBV Harrisburg Letter Report Hey Maureen, I'm swamped. It may be next week before I can get to it. Monday is a holiday for us. I will get back with you as soon as it's been reviewed. Have a great day, Trudy Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management -DENorth Carolina Department of Environmental Quality LMpi�Lrmn �. UST Section, Mooresville Regional Office 704.235.2182 (Office) Trudy. B everly(Lncdenr. gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: https://deq.nc.Rov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-program INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: https://dea.nc. gov/about/divisions/wastc-management/waste-management-rules-data/waste-management-gis-mans File Review Procedures: https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): https://deu.nc. gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: https:Hflles.nc.2oy/nedeci/W aste%2OMana2ement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policv.pdf https://files.nc. gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx From: Maureen Jackson[mailto:maureen.jackson@atcRs.com] Sent: Tuesday, May 25, 2021 11:55 AM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: [External] RE: PBV Harrisburg Letter Report CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Good morning. Just curious if you have had a chance to review Thanks Maureen Jackson I SENIOR PROJECT MANAGER I ATC Group Services LLC Direct +1 919 561 3893 ATC 609A Piner Road Suite 115 1 Wilmington, NC 28409 maureen.jackson@atcgs.com I www.atcciroupservices.com This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If you are not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is strictly prohibited. If you have received this email in error, please notify the sender by replying to this message and immediately delete and destroy any copies of this email and any attachments. The views or opinions expressed are the author's own and may not reflect the views or opinions of ATC. From: Maureen Jackson Sent: Tuesday, May 18, 2021 9:07 AM To: 'Beverly, Trudy' <trudy.beverly@ncdenr.gov> Subject: PBV Harrisburg Letter Report Importance: High Good morning. A letter report is attached. Pepsi is looking for an expedited response. Thank you Maureen Maureen Jackson I SENIOR PROJECT MANAGER I ATC Group Services LLC Direct +1 919 561 3893 ATC 609A Piner Road Suite 115 1 Wilmington, NC 28409 maureen.iackson@atcgs.com I www.atcgroupservices.com This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If you are not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is strictly prohibited. If you have received this email in error, please notify the sender by replying to this message and immediately delete and destroy any copies of this email and any attachments. The views or opinions expressed are the author's own and may not reflect the views or opinions of ATC.