MO-88833_96073_CA_IAR_ 20210423_Initial Abatement Report

;ETC
ENVIRONMENTAL • GEOTECHNICAL
BUILDING SCIENCES • MATERIALS TESTING
April 23, 2021
Ms. Trudy Beverly
North Carolina Department of Environmental Quality
Division of Waste Management, UST Section
Mooresville Regional Office
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Re: Soil Excavation Activities
Pepsi Emergency Response (Fuel Spill)
Pepsi Bottling Ventures, LLC Harrisburg Facility
22 Pepsi Way
Harrisburg, North Carolina 28075
ATC Project No. PEPSI043
Dear Ms. Beverly:
609A Piner Road, Suite 115
Wilmington, North Carolina 28409
Telephone [phone]
Fax [phone]
www.atcgroupservices.com
ATC Associates of North Carolina, P.C. (ATC), on behalf of Pepsi Bottling Ventures, LLC (PBV), has
prepared this letter report regarding soil excavation activities conducted at 22 Pepsi Way in Harrisburg, North
Carolina. These activities were conducted in response to a petroleum -release as a result of a malfunction of a
fire pump filter, which allowed approximately 35 to 40 gallons of diesel fuel to be released from the generator
system.
BACKGROUND
On March 18, 2021 at approximately 1:00 p.m., Pepsi personnel were notified that fuel was being discharged
from the fire pump building. Upon further inspection, it was noted that a recently replaced filter was leaking
and allowing diesel fuel to be released onto the floor. The diesel fuel flowed into the building floor drain and
discharged into a nearby grass/wooded area via the floor drain pipe. It is estimated approximately 35 to 40
gallons of diesel fuel were released onto the ground near the discharge pipe. The location of the release area is
shown on Attachment L
On March 18, 2021, Pepsi personnel contracted with Haz-Mat and ATC to perform initial spill response
activities. On this date, Haz-Mat personnel placed a granulated enzyme on the spill area. ATC personnel
submitted a UST-62: 24-Hour Notification of Discharge Form to the NCDEQ Mooresville Regional office via
email on March 19, 2021. A copy of the UST-62 form is attached in Attachment II. Photos of the spill area
are provided in Attachment III.

April 23, 2021
Page 2 of 4
SOIL EXCAVATION ACTIVITIES
Following initial response activities, Zebra Environmental and ATC conducted soil excavation activities of the
diesel fuel impacted soil. On March 25, 2021, Dewberry Engineers and ATC personnel met onsite to conduct
a private utility locate of the proposed excavation area using Ground Penetrating Radar (GPR) and other
traditional locating methods. On March 29, 2021, Zebra and ATC personnel excavated approximately 61.35
tons of petroleum -impacted soil from release area. The excavation measured approximately 60 feet in length,
25 feet in width, and varied between two and two and one-half feet in depth. The soil was mainly dark organic
topsoil to approximately six inches below ground surface (bgs). The soil from six inches to two and one-half
feet bgs was noted to be a brown to brownish -orange sandy clay. It should be noted the soil was noted to be
moist at an approximate depth of two and one-half feet bgs. Photos of excavation activities are provided in
Attachment III.
Excavated soils were placed directly into dump trucks and disposed of at AES of NC in Thomasville, North
Carolina. The soil excavation area, as well as the locations of the soil samples, is provided in Attachment
I. Copies of the soil disposal manifests are provided in Attachment IV.
ATC personnel performed confirmatory soil sampling prior to backfilling the excavated area. One sample
(Disp-1) was collected for disposal purposes and six samples were collected from the sidewalls of the
excavations at various locations (SW-1 through SW-6). These six samples were collected to determine the
effectiveness of the soil excavation activities. The locations of the confirmatory soil samples are depicted
on Attachment I.
All samples were collected in laboratory -supplied containers and shipped on ice to SGS North America,
Inc. (SGS) in Scott, Louisiana. The soil samples, SW-1 through SW-6, were requested to be analyzed by
EPA Method 8015 for Total Petroleum Hydrocarbons (TPH) — Gasoline Range Organics (GRO) and Diesel
Range Organics (DRO). Disposal sample Disp-1 was requested to be analyzed by TPH-GRO and
TPH-DRO.
Laboratory analyses of the soil samples did not detect TPH-GRO or TPH-DRO concentrations above
laboratory method detection limits (MDLs). Based on these results, it appears petroleum -impacted soil in
the spill area has been effectively removed. The analytical results are presented in Attachment V as Table
1. A copy of the laboratory report and chain -of -custody documents are provided in Attachment VT
Following completion of excavation activities, the excavated area was backfilled with clean soil and topped
with grass seed and straw. Photos of the completed excavations are provided in Attachment III.

April 23, 2021
Page 3 of 4
TEMPORARY WELL INSTALLATION
Due to the possibility of shallow groundwater in the excavated area, on April 12, 2021, a temporary
monitoring well GW-1 was installed by a North Carolina licensed driller with Carolina Soil Investigations
(CSI), under supervision of personnel from ATC. The location of the temporary monitoring well is depicted
on Attachment L
Temporary monitoring well GW-1 was installed to a depth of approximately 17 feet below ground surface
(bgs). The well was installed using direct -push technology and constructed of one -inch diameter well
casing made of flush joint, threaded schedule-40 poly vinyl chloride (PVC) pipe. The PVC well screen is
0.010-inch slot with a screened interval of ten feet. Following sample collection, the temporary monitoring
well was removed and the boring was properly abandoned.
On April 12, 2021, a groundwater sample was collected from temporary monitoring well GW-1. Prior to
sample collection, the temporary well was purged with a field -decontaminated peristaltic pump and
dedicated tubing. The sample was collected directly into laboratory -approved containers, packed in ice,
and delivered under chain -of -custody to SGS in Scott, Louisiana for analyses. The groundwater sample
from monitoring well GW-1 was analyzed by Environmental Protection Agency (EPA) Method 602, EPA
Method 625 plus ten highest non -target peaks, and Massachusetts Department of Environmental Protection
(MADEP) Methods for volatile petroleum hydrocarbons (VPH) and extractable petroleum hydrocarbons
(EPH).
Laboratory analytical results of the groundwater sample from temporary well GW-1 detected a dissolved
naphthalene and dissolved bis(2-ethylhexyl)phthalate concentrations above laboratory MDLs. It should be
noted the dissolved bis(2-ethylhexyl)phthalate concentration was detected above its established 2L
Standard. This compound typically is not associated with petroleum releases. The presence of this
compound may be a laboratory artifact or from the breakdown of plastic in the environmental as it is a
plasticizer. The tabulated groundwater analytical results are provided in Attachment V as Table 2. The
laboratory report and chain -of -custody documents are provided in Attachment VT
CONCLUSIONS
Based on the above activities and subsequent laboratory results, it appears diesel fuel impacted soil has
been effectively removed from the area of the spill. Additionally, the petroleum -related impacts to
groundwater in the spill area appear negligible. No other activities are warranted at this time.

April 23, 2021
Page 4 of 4
If you have any questions or require additional information, please contact our office at [phone].
Sincerely,
ATC Associates of No'rtR,; C urfhiI14 P.0
sR
Maureen Jacksor = Gabriel Araos, P.E.
Senior Project Mina r 2 _ = Senior Project Manager
s �� f Cb
G " O L G
cc: Mr. Bill Peterson, �3Aail ntures. LLC
+wur0
Attachments
r

Attachment I

19 `m
EHVIHGNMEHTAL • GEGTECHNICAL
6 I GIN • I •N MATERIALSMAIERIALS T S-
Project No. PEPS1043
pep l WaY
609A Piner Road, Suite 115
Wilmington, North Carolina 28409
[phone]
DATE: 04/22/2021
PM: Maureen Jackson
Figure 1 - Soil Excavation — Diesel Fuel Spill
PBV Harrisburg
22 Pepsi Way
Harrisburg, North Carolina
Not to

Attachment II

UST-62
24-Hour Notification of Discharge Form
For Non -UST This form should be completed and submitted to the UST Section's regional office following a known or suspected release of
Releases of petroleum from a source other than an underground storage tank. This form is required to be submitted within 24 hours of
Petroleum in NC discovery of a known or suspected petroleum release
(DWM USE ONLY)
Suspected Contamination? (Y/N) Y
Release discovered
Incident # Priority Rank (H,I,L,U)
Confirmed GW Contamination? (Y/N) N
(time/date): 3/18/21 13:00
Received (time/date)
Confirmed Soil Contamination ?(Y/N) Y
Received by Region
Samples taken?(Y/N) _.NL Free product? (Y/N) N
Reported by (circle one): Phone, Fax or Report
If Yes(free product), state greatest thickness: feet
INCIDENT DESCRIPTION
Incident Name: Pepsi Harrisburg Facility
Address (street number/name): 22 Pepsi Way
County: Cabarrus
City/Town: Harrisburg Zip Code: 28075
Regional Office (circle one): Asheville Mooresville ayetteville,
Raleigh. Washington, Wilmington, Winston- a em
Latitude (decimal degrees): 35.31676 N Longitude (decimal degrees) : 80.66672 W Obtained by:
Describe suspected or confirmed release (nature of release, time/date of release, quantity of release, amount of free GPS
roduct: Fire pump filter allowed R]2roximatelv 35 to 40 galions of diesel fuel to be released and onto tit
ground adjacent to the building. Release was discovered today (3/18) at approx. l pm. ❑ Electronic topographic map
❑ GIS Address matching
Describe initial response/abatement (time/date release stopped, cleanup begun/completed, quantity of product ❑ Other
soil removed, confirmation sampling):
Pepsi, Haz-Mat, ATC, and Carolina Cat personnel responded and clean-up activities are being performed. ❑ Unknown
It is known
not at thi, time the amount of -oil to be removed.
Describe impacted receptors: Describe location:
None at this time
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
Observation of Release at Occurrence ❑ Water Supply Well Contamination
❑ Visual or Olfactory Evidence ❑ Surface Water Contamination
❑ Soil Contamination ❑ Other (specify)
❑ Groundwater Contamination
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release Product Type Released
(Check one to indicate primary (Check one to indicate primary (Check one) (Check one to indicate primary petroleum product
source) cause) type released)
❑ AST (tank). Spill (Accidental) Petroleum Gasoline/ Diesel) ❑ DieselNeg. Oil
❑ AST Piping/ Dispenser ❑ Spill (Intentional) ❑ Both Petroleum Kerosene Blend
❑ AST Delivery Problem ❑ Corrosion & Nan -Petroleum ❑ E11 — E20 ❑ Vegetable Oil 100%
❑ OTR Vehicle Tank ❑ Physical or Mechanical ❑ E21 — E84 ❑ Heating Oil
❑ OTR Bulk Transport Tank Damage Location ❑ E85 — E99 ❑ Waste Oil
❑ RR Bulk Transport Tank ❑ Equipment Failure (Check one) ❑ Ethanol 100% ❑ Mineral Oil -no
❑ Transformer ❑ AST Overfill PCBs
Facility ❑ Mineral Oil -PCBs
❑ Unknown ❑AST Installation Problem
Residence
Other ❑ Unknown ❑ Other Petroleum
❑ Highway/Road
Products
❑ Other
Definitions presented on reverse Definitions presented on reverse Railway
❑
Other
Ownership
5. Federal 6. County 7. State
1. Municipal 2. Military 3. Unknown CED
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial B. Commercia 7. Mining
Guidance presented on reverse
US I I-orm 52 (04/10) Page 1 of 2

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. iV 3 Unknown Number of Water Supply Wells Affected
List of Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
PARTY RESPONSIBLE FOR RELEASE
(if the source of the release is not an AST system or if it is an AST system and there is a responsible party other than the AST system owner/ operator)
Name of Person/Company
Pepsi Bottling Ventures/Bill Patterson (Dir. Safety and Health
Address
4141 ParkLane Avenue
City Raleigh
g
State NC Zip Code 27612
Telephone Number
[phone]
AST SYSTEM OWNER (if the source of the release is an AST system)
AST Owner/Company
Address
City
State
Zip Code Telephone Number
AST SYSTEM OPERATOR (if the source of the release is an AST system)
UST Operator/Company
Address
City State
Zip Code Telephone Number
LANDOWNER AT LOCATION OF INCIDENT
Landowner
Pepsi Bottling Ventures
Address
4141 ParkLane Avenue
City
Raleigh
State
NC
Zip Code Telephone Number
27612 (9l9) 865-7416
Draw Sketch of Area or Provide Map (showing incident site, location of release, two major road intersections, potential
receptors)
Attach sketch or map to form.
Give Directions to Incident Site Attach directions to form if necessary.
Site Map Attached - Take a right off Hwy 49 onto Pepsi Way. Continue to end of
road to the Pepsi facility.
Person Reporting Incident M. Jackson, PG Company ATC Associates of NC on behalf of PBV
Telephone Number [phone]
Title Senior Project Manager Address 609A Piner Rd, Suite 115 Wilmington, NC 28409
1 Date March 18, 2021
US I form U (04/10) Page 2 of 2
Definitions of Sources
AST (Tank): means the tank is used to store product
AST Piping: means the piping and connectors running from the tank to the dispenser or other end -use equipment
AST Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping
AST Delivery Problem: identifies releases that occurred during product delivery to the tank.
OTR Vehicle Tank: means the tank is used to store product to fuel an over the road vehicle
OTR Bulk Transport Tank: means a tank that is used to transport product in bulk over the road (by truck)
RR :bulk Transport Tank: means a tank that is used to transport product in bulk by train
Transformer: means electrical transformer
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill (Accidental): use this cause when a spill occurs accidentally(e.g., when the delivery hose is disconnected from a fill pipe)
Spill (Intentional): use this cause when a spill occurs intentionally (e.g., intentional dumping or breakage)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion
Equipment failure: use when a release occurs due to equipment failure other than corrosion or physical or mechanical damage
AST Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
AST Installation Problem: use when the problem is determined to have occurred specifically because the AST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories
Unknown: use when the cause has not been determined
Guidance: Ownership and Operator Type
Ownership select the category which describes owner of the AST system, bulk transport tank, or other release source
Operator Type select the category which describes the operation in which owner uses the AST system, bulk transport tank, or other release source

Attachment III

Photo 1: View of initial spill area (drain pipe that diesel fuel travelled thru)
Photo 2: View of spill area.
22 Pepsi Way
Harrisburg, North Carolina
ATC Project No. PEPSI043

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Photo 5: Excavation Activities
Photo 6: Completed Excavation Activities
22 Pepsi Way
Harrisburg, North Carolina
ATC Project No. PEPSI043

Photo 7: Excavation Area Backfilled
Photo 8: Excavation Strawed and Seeded
22 Pepsi Way
Harrisburg, North Carolina
ATC Project No. PEPSI043

Photo 9: Excavation Completed
Photo 10: Excavation Completed
22 Pepsi Way
Harrisburg, North Carolina
ATC Project No. PEPSI043

Attachment IV

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Attachment V

TABLE 1
SOIL EXCAVATION CONFIRMATION LABORATORY RESULTS
PBV HARRISBURG
22 PEPSI WAY
HARRISBURG, NORTH CAROLINA
ATC PROJECT NO. PEPSI043
ANALTYICAL METHOD
EPA Method
8015
Sample ID
Date
Sampled
PID
Reading
(ppm)
Sample
Depth
(feet)
�
a
A
a
SW-1
3/29/2021
0.1
2
<6.6
<6.4
SW-2
3/29/2021
0.2
2.5
<7.0
<6.4
SW-3
3/29/2021
0.2
2.5
<5.7
<6.3
SW-4
3/29/2021
0.0
2.5
<5.9
<6.3
SW-5
3/29/2021
0.0
2
<5.5
<6.2
SW-6
3/29/2021
0.0
2
<7.0
<6.5
Disp-1
3/29/2021
1 24.2
--
15.3
122
State Action Level (mg/kg)
50
100
Notes:
1. Concentrations reported in milligrams per kilogram (mg/kg).
2. °<° = not detected at or above the laboratory detection limit.
3. Disp-1 is a soil sample collected for soil disposal purposes.

TABLE 2
GROUNDWATER ANALYTICAL RESULTS
PBV HARRISBURG
22 PEPSI WAY
HARRISBURG, NORTH CAROLINA
ATC PROJECT NO. PEPSI043
Analytical Method
EPA Method 625
b
o.
Date
�
Well ID
Sampled
1
*4 W
IF�
GW -1
14/12/2021
0.21
5.9
15 J
2L Standards (ug/L)
6
3
--
GCLs (ug/L)
6,000
135
--
Notes:
1. Concentrations reported in micrograms per liter (ug/L).
2. Concentrations in bold print equal or exceed the 2L Standard.
3. GCLs denotes Gross Contaminant Levels.
4. J denotes estimated concentration by laboratory.

Attachment VI

ffm
Scott, LA
The results set forth herein are provided by SGS North America Inc. a-Hl ydcopy 2. 0
Automated Report
Technical Report for
ATC Group Services LLC
PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
SGS Job Number: LA70390
Sampling Date: 03/29/21
Report to:
ATC Group Services LLC.
2725 East Millbrook Road Suite 121
Raleigh, NC 27604
maureen. jackson@atcgs. com; gabe. araos@atcgs.
ATTN: Maureen Jackson
Total number of pages in report: 28
Ac Fp
Ar .
Test results contained within this data package meet the requirements Ron Benj a illl n
of the National Environmental Laboratory Accreditation Program Lab Director
and/or state specific certification programs as applicable.
Client Service contact: Christina Larriviere 337-237-4775
Certifications: LDEQ(2048), LDHH(LA150012), AR(14-045-04), AZ(AZ0805), FL(E87657), IL(200082), KY(#31),
NC(487), SC(73004001), NJ(LA007), TX(T104704186-18-16), WV(257)
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 500 Ambassador Caffery • Scott, LA 70583 • tel: [phone]
SGS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about
Unauthorized modification of this report is strictly prohibited. how we can serve you better at:
Review standard terms at: http://www.sgs.com/en/terms-and-conditions [e-mail]
1 of 28
LA70390

Sections:
Table of Contents
-I-
Section1: Sample Summary...................................................................................................
3
Section2: Summary of Hits....................................................................................................
4
Section3: Sample Results........................................................................................................
5
3.1: LA70390-1: SW-1........................................................................................................
6
3.2: LA70390-2: SW-2........................................................................................................
8
3.3: LA70390-3: SW-3........................................................................................................
10
3.4: LA70390-4: SW-4........................................................................................................
12
3.5: LA70390-5: SW-5........................................................................................................
14
3.6: LA70390-6: SW-6........................................................................................................
16
3.7: LA70390-7: DISP-1......................................................................................................
18
Section4: Misc. Forms............................................................................................................
20
4.1: Chain of Custody...........................................................................................................
21
Section5: GC Volatiles - QC Data Summaries.....................................................................
24
5.1: Method Blank Summary................................................................................................
25
5.2: Blank Spike/Blank Spike Duplicate Summary..............................................................
26
Section 6: GC/LC Semi-volatiles - QC Data Summaries.....................................................
27
6.1: Blank Spike/Blank Spike Duplicate Summary..............................................................
28
W,

SGS North America Inc.
Sample Summary
ATC Group Services LLC
Job No: LA70390
PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample I D
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the RL
LA70390-1 03/29/21 12:10 CB 03/31/21 SO Soil SW-1
LA70390-2 03/29/21 12:15 CB 03/31/21 SO Soil SW-2
LA70390-3 03/29/21 12:20 CB 03/31/21 SO Soil SW-3
LA70390-4 03/29/21 12:25 CB 03/31/21 SO Soil SW-4
LA70390-5 03/29/21 12:30 CB 03/31/21 SO Soil SW-5
LA70390-6 03/29/21 12:35 CB 03/31/21 SO Soil SW-6
LA70390-7 03/29/21 10:30 CB 03/31/21 SO Soil DISP-1
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
6 3 of 28
LA70390

Summary of Hits
Job Number:
LA70390
Account:
ATC Group Services LLC
Project:
PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Collected:
03/29/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA70390-1 SW-1
No hits reported in this sample.
LA70390-2 SW-2
No hits reported in this sample.
LA70390-3 SW-3
No hits reported in this sample.
LA70390-4 SW-4
No hits reported in this sample.
LA70390-5 SW-5
No hits reported in this sample.
LA70390-6 SW-6
No hits reported in this sample.
LA70390-7 DISP-1
TPH-GRO (C6-C10) 15.3 10 mg/kg SW846 8015C
TPH-DRO (C10-C28) 122 7.8 mg/kg SW846 8015C
Page 1 of 1
6 4 of 28
LA70390

i
SGS
Scott, LA
Section 3
Sample Results
Report of Analysis
6 5 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: SW-1
Lab Sample ID: LA70390-1 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C Percent Solids: 77.4
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 j
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA397266.13 1 03/31/21 20:13 NN n/a n/a GLA3313
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.30 g 5.0 ml 100 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C 10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
540-36-3
1,4-Difluorobenzene
Result
RL Units Q
ND
6.6 mg/kg
Run# 1
Run# 2 Limits
88%
63-139%
91%
52-140%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 6 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: SW-1
Lab Sample ID: LA70390-1 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C SW846 3546 Percent Solids: 77.4
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 j
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LG008183.13 1 04/02/21 00:01 LL 04/01/21 07:20 OP18343 GLG1085
Run #2
Initial Weight Final Volume
Run # 1 20.1 g 1.0 ml
Run #2
CAS No. Compound
TPH-DRO (C 10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
Result
RL Units Q
ND
6.4 mg/kg
Run# 1
Run# 2 Limits
64%
31-127%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 7 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: SW-2
Lab Sample ID: LA70390-2 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C Percent Solids: 76.6
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 N
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA397268.13 1 03/31/21 20:36 NN n/a n/a GLA3313
Run #2
Initial Weight Final Volume Methanol Aliquot
Run # 1 6.00 g 5.0 ml 100 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C 10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
540-36-3
1,4-Difluorobenzene
Result
RL Units Q
ND
7.0 mg/kg
Run# 1
Run# 2 Limits
86%
63-139%
90%
52-140%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 8 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: SW-2
Lab Sample ID: LA70390-2 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C SW846 3546 Percent Solids: 76.6
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 N
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LG008184.13 1 04/02/21 00:22 LL 04/01/21 07:20 OP18343 GLG1085
Run #2
Initial Weight Final Volume
Run # 1 20.3 g 1.0 ml
Run #2
CAS No. Compound
TPH-DRO (C 10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
Result
RL Units Q
ND
6.4 mg/kg
Run# 1
Run# 2 Limits
71%
31-127%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 9 of 28
LA70390

SGS North America Inc.
Report of Analysis
Page 1 of 1 w
Client Sample ID:
SW-3
Lab Sample ID:
LA70390-3 Date Sampled: 03/29/21
Matrix:
SO - Soil Date Received: 03/31/21
Method:
SW846 8015C Percent Solids: 79.1
Project:
PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA397270.13 1 03/31/21 20:59 NN n/a n/a GLA3313
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 7.20 g 5.0 ml 100 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C 10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
540-36-3
1,4-Difluorobenzene
Result
RL Units Q
ND
5.7 mg/kg
Run# 1
Run# 2 Limits
88%
63-139%
93%
52-140%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 10 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: SW-3
Lab Sample ID: LA70390-3 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C SW846 3546 Percent Solids: 79.1
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 w
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LG008185.13 1 04/02/21 00:43 LL 04/01/21 07:20 OP18343 GLG1085
Run #2
Initial Weight Final Volume
Run # 1 20.0 g 1.0 ml
Run #2
CAS No. Compound
TPH-DRO (C 10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
Result
RL Units Q
ND
6.3 mg/kg
Run# 1
Run# 2 Limits
72%
31-127%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 11 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: SW-4
Lab Sample ID: LA70390-4 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C Percent Solids: 79.4
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 P
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA397246.13 1 03/31/21 16:27 NN n/a n/a GLA3313
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.80 g 5.0 ml 100 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C 10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
540-36-3
1,4-Difluorobenzene
Result
RL Units Q
ND
5.9 mg/kg
Run# 1
Run# 2 Limits
88%
63-139%
93%
52-140%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
� 12 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: SW-4
Lab Sample ID: LA70390-4 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C SW846 3546 Percent Solids: 79.4
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 P
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LG008186.13 1 04/02/21 01:04 LL 04/01/21 07:20 OP18343 GLG1085
Run #2
Initial Weight Final Volume
Run # 1 20.1 g 1.0 ml
Run #2
CAS No. Compound
TPH-DRO (C 10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
Result
RL Units Q
ND
6.3 mg/kg
Run# 1
Run# 2 Limits
70%
31-127%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
� 13 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: SW-5
Lab Sample ID: LA70390-5 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C Percent Solids: 79.9
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 P
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA397248.13 1 03/31/21 16:49 NN n/a n/a GLA3313
Run #2
Initial Weight Final Volume Methanol Aliquot
Run # 1 7.40 g 5.0 ml 100 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C 10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
540-36-3
1,4-Difluorobenzene
Result
RL Units Q
ND
5.5 mg/kg
Run# 1
Run# 2 Limits
86%
63-139%
92%
52-140%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 14of28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: SW-5
Lab Sample ID: LA70390-5 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C SW846 3546 Percent Solids: 79.9
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 P
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LG008187.1) 1 04/02/21 01:25 LL 04/01/21 07:20 OP18343 GLG1085
Run #2
Initial Weight Final Volume
Run # 1 20.1 g 1.0 ml
Run #2
CAS No. Compound
TPH-DRO (C 10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
Result
RL Units Q
ND
6.2 mg/kg
Run# 1
Run# 2 Limits
72%
31-127%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 15 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: SW-6
Lab Sample ID: LA70390-6 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C Percent Solids: 76.4
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA397272.13 1 03/31/21 21:22 NN n/a n/a GLA3313
Run #2
Initial Weight Final Volume Methanol Aliquot
Run # 1 6.00 g 5.0 ml 100 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C 10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
540-36-3
1,4-Difluorobenzene
Result
RL Units Q
ND
7.0 mg/kg
Run# 1
Run# 2 Limits
88%
63-139%
93%
52-140%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 16 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: SW-6
Lab Sample ID: LA70390-6 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C SW846 3546 Percent Solids: 76.4
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LG008188.13 1 04/02/21 01:46 LL 04/01/21 07:20 OP18343 GLG1085
Run #2
Initial Weight Final Volume
Run # 1 20.2 g 1.0 ml
Run #2
CAS No. Compound
TPH-DRO (C 10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
Result
RL Units Q
ND
6.5 mg/kg
Run# 1
Run# 2 Limits
71%
31-127%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 17 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: DISP-1
Lab Sample ID: LA70390-7 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C Percent Solids: 62.9
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 P
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA397274.13 1 03/31/21 21:44 NN n/a n/a GLA3313
Run #2
Initial Weight Final Volume Methanol Aliquot
Run # 1 5.40 g 5.0 ml 100 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C 10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
540-36-3
1,4-Difluorobenzene
Result
RL Units Q
15.3
10 mg/kg
Run# 1
Run# 2 Limits
88%
63-139%
93%
52-140%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 18 of 28
LA70390

SGS North America Inc.
Report of Analysis
Client Sample ID: DISP-1
Lab Sample ID: LA70390-7 Date Sampled: 03/29/21
Matrix: SO - Soil Date Received: 03/31/21
Method: SW846 8015C SW846 3546 Percent Solids: 62.9
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 P
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LG008189.13 1 04/02/21 02:07 LL 04/01/21 07:20 OP18343 GLG1085
Run #2
Initial Weight Final Volume
Run # 1 20.3 g 1.0 ml
Run #2
CAS No. Compound
TPH-DRO (C 10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
Result
RL Units Q
122
7.8 mg/kg
Run# 1
Run# 2 Limits
73%
31-127%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 19 of 28
LA70390

ffm
Scott, LA
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
1
Section 4
6 20 of 28
LA70390

AAA D O M A CHAIN OF CUSTODY
PAGE 1 OF i
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LA70390: Chain of Custody
Page 1 of 3
i 21 of 28
LA70390

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LA70390: Chain of Custody
Page 2 of 3
6 22 of 28
LA70390

SGS Sample Receipt Summary
Job Number: LA70390 Client: ATC
Date / Time Received: 3/31/2021 8:45:00 AM Delivery Method:
Cooler Temps (Initial/Adjusted): #1: (1.4/1.4): DV462
Cooler Security Y or N
Y or N
1. Custody Seals Present: W
❑
3. COC Present: ❑J ❑
2. Custody Seals Intact: 2
❑
4. Smpl
Dates/Time OK ❑,i ❑
Cooler Temperature
Y or N
1. Temp criteria achieved:
❑�
❑
2. Thermometer ID:
DV462;
3. Cooler media:
Ice (direct contact)
4. No. Coolers:
1
Quality Control Preservation
Y
or N
N/A
1. Trip Blank present / cooler:
❑
❑
❑J
2. Trip Blank listed on COC:
❑
❑
W
3. Samples preserved properly:
❑d
❑
4. VOCs headspace free:
❑
❑
W
Comments Received 1 of 2 vials with caps broken for sw-4 & sw-5.
FedEx
Project: PBV- HARRISBURG
Airbill Ws: 4920 6967 9016
Sample Intearity - Documentation
Y or N
1. Sample labels present on bottles:
❑
2. Container labeling complete:
❑
3. Sample container label / COC agree:
❑
Sample Intearity- Condition
Y
or N
1. Sample recvd within HT:
W
❑
2. All containers accounted for:
❑d
❑
3. Condition of sample:
Broken
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Sample Intearity - Instructions
Y
or N N/A
1. Analysis requested is clear:
❑d
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2. Bottles received for unspecified tests
❑
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3. Sufficient volume recvd for analysis:
❑d
❑
4. Compositing instructions clear:
❑
❑ W
5. Filtering instructions clear:
❑
❑ k
LA70390: Chain of Custody
Page 3 of 3
6 23 of 28
LA70390

ffm
Scott, LA
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
i
no
Section 5
6 24 of 28
LA70390

Method Blank Summary
Job Number: LA70390
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GLA3313-MB1
LA397232.1)
1
03/31/21
NN
n/a
n/a
GLA3313
The QC reported here applies to the following samples: Method: SW846 8015C
LA70390-1, LA70390-2, LA70390-3, LA70390-4, LA70390-5, LA70390-6, LA70390-7
CAS No.
Compound
Result
RL Units Q
TPH-GRO (C6-C 10)
ND
5.0 mg/kg
CAS No.
Surrogate Recoveries
Limits
460-00-4
4-Bromofluorobenzene
81%
63-139%
540-36-3
1,4-Difluorobenzene
94%
52-140%
6 25 of 28
LA70390

Blank Spike/Blank Spike Duplicate Summary
Job Number: LA70390
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GLA3313-BS2
LA397228.1)
1
03/31/21
NN
n/a
n/a
GLA3313
GLA3313-BSD2
LA397230.1)
1
03/31/21
NN
n/a
n/a
GLA3313
The QC reported here applies to the following samples: Method: SW846 8015C
LA70390-1, LA70390-2, LA70390-3, LA70390-4, LA70390-5, LA70390-6, LA70390-7
Spike
BSP BSP
BSD BSD Limits
CAS No.
Compound
mg/kg
mg/kg %
mg/kg % RPD Rec/RPD
TPH-GRO (C6-C10)
50
43.1 86
43.6 87 1 79-121/6
CAS No.
Surrogate Recoveries
BSP
BSD
Limits
460-00-4
4-Bromofluorobenzene
86%
85%
63-139%
540-36-3
1,4-Difluorobenzene
92%
94%
52-140%
* = Outside of Control Limits.
6 26 of 28
LA70390

i
Sri$ -
Scott, LA ME
Section 6
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
0
6 27 of 28
LA70390

Blank Spike/Blank Spike Duplicate Summary
Job Number: LA70390
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP18343-BS
LG008158.1)
1
04/01/21
LL
04/01/21
OP18343
GLG1085
OP18343-BSD
LG008159.1)
1
04/01/21
LL
04/01/21
OP18343
GLG1085
The QC reported here applies to the following samples: Method: SW846 8015C
LA70390-1, LA70390-2, LA70390-3, LA70390-4, LA70390-5, LA70390-6, LA70390-7
Spike
BSP BSP
BSD BSD Limits
CAS No. Compound
mg/kg
mg/kg %
mg/kg % RPD Rec/RPD
TPH-DRO (C 10-C28)
149
116 78
119 80 3 49-118/ 19
CAS No. Surrogate Recoveries
BSP
BSD
Limits
84-15-1 o-Terphenyl
60% a
60% a
31-127%
(a) Recoveries were corrected for spike
concentration.
* = Outside of Control Limits.
6 28 of 28
LA70390

ffm
Scott, LA
The results set forth herein are provided by SGS North America Inc. a-Hl ydcopy 2. 0
Automated Report
Technical Report for
ATC Group Services LLC
PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
PEPSI043
SGS Job Number: LA70636
Sampling Date: 04/ 12/21
Report to:
ATC Group Services LLC.
2725 East Millbrook Road Suite 121
Raleigh, NC 27604
maureen. jackson@atcgs. com; gabe. araos@atcgs.
ATTN: Maureen Jackson
Total number of pages in report: 36
Ac Fp
Ar .
Test results contained within this data package meet the requirements Ron Benj a illl n
of the National Environmental Laboratory Accreditation Program Lab Director
and/or state specific certification programs as applicable.
Client Service contact: Christina Larriviere 337-237-4775
Certifications: LDEQ(2048), LDHH(LA150012), AR(14-045-04), AZ(AZ0805), FL(E87657), IL(200082), KY(#31),
NC(487), SC(73004001), NJ(LA007), TX(T104704186-18-16), WV(257)
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 500 Ambassador Caffery • Scott, LA 70583 • tel: [phone]
SGS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about
Unauthorized modification of this report is strictly prohibited. how we can serve you better at:
Review standard terms at: http://www.sgs.com/en/terms-and-conditions [e-mail]
1 of 36
LA70636

Sections:
Table of Contents
-I-
Section1: Sample Summary...................................................................................................
3
Section2: Summary of Hits....................................................................................................
4
Section3: Sample Results........................................................................................................
5
3.1; LA70636-1: GW-1........................................................................................................
6
Section4: Misc. Forms............................................................................................................
12
4.1: Chain of Custody...........................................................................................................
13
Section 5: MS Semi-volatiles - QC Data Summaries............................................................
16
5.1: Method Blank Summary................................................................................................
17
5.2: Blank Spike/Blank Spike Duplicate Summary..............................................................
23
Section 6: GC Volatiles - QC Data Summaries.....................................................................
27
6.1: Method Blank Summary................................................................................................
28
6.2: Blank Spike/Blank Spike Duplicate Summary..............................................................
30
6.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
32
6.4: Duplicate Summary.......................................................................................................
33
Section 7: GC/LC Semi-volatiles - QC Data Summaries.....................................................
34
7.1: Method Blank Summary................................................................................................
35
7.2: Blank Spike/Blank Spike Duplicate Summary..............................................................
36
W,

SGS North America Inc.
Sample Summary
ATC Group Services LLC
Job No: LA70636
PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Project No: PEPSI043
Sample Collected Matrix Client
number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the RL
LA70636-1 04/12/21 11:30 CB 04/13/21 AQ Ground Water GW-1
6 3 of 36
LA70636

Summary of Hits Page 1 of 1
Job Number: LA70636
Account: ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Collected: 04/ 12/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA70636-1 GW-1
bis(2-Ethylhexyl)phthalate 5.9 4.8 ug/1 EPA 625.1
Naphthalene 0.21 0.19 ug/1 EPA 625.1
Total TIC, Semi -Volatile 15 J ug/1
6 4 of 36
LA70636

i
SGS
Scott, LA
Section 3
Sample Results
Report of Analysis
6 5 of 36
LA70636

SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID: GW-1
Lab Sample ID: LA70636-1 Date Sampled: 04/12/21
Matrix: AQ - Ground Water Date Received: 04/ 13/21
Method: EPA 625.1 EPA 625.1 Percent Solids: n/a
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0065626.1) 1 04/14/21 23:56 LL 04/13/21 02:00 OP18408 EC2574
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
Units Q
65-85-0
Benzoic Acid a
ND
19
ug/l
59-50-7
4-Chloro-3-methyl Phenol
ND
4.8
ug/l
95-57-8
2-Chlorophenol
ND
4.8
ug/l
120-83-2
2,4-Dichlorophenol
ND
4.8
ug/1
105-67-9
2,4-Dimethylphenol
ND
4.8
ug/l
51-28-5
2,4-Dinitrophenol
ND
19
ug/l
534-52-1
4,6-Dinitro-o-cresol
ND
9.5
ug/l
95-48-7
2-Methylphenol
ND
4.8
ug/l
3&4-Methylphenol
ND
4.8
ug/l
88-75-5
2-Nitrophenol
ND
4.8
ug/l
100-02-7
4-Nitrophenol
ND
24
ug/l
87-86-5
Pentachlorophenol
ND
9.5
ug/l
108-95-2
Phenol
ND
4.8
ug/l
88-06-2
2,4,6-Trichlorophenol
ND
4.8
ug/1
83-32-9
Acenaphthene
ND
0.19
ug/l
208-96-8
Acenaphthylene
ND
0.19
ug/l
120-12-7
Anthracene
ND
0.19
ug/l
56-55-3
Benzo(a)anthracene
ND
0.19
ug/l
50-32-8
Benzo(a)pyrene
ND
0.19
ug/l
205-99-2
Benzo(b)fluoranthene
ND
0.19
ug/1
191-24-2
Benzo(g,h,i)perylene
ND
0.19
ug/l
207-08-9
Benzo(k)fluoranthene
ND
0.19
ug/l
100-51-6
Benzyl Alcohol
ND
9.5
ug/l
101-55-3
4-13romophenyl Phenyl Ether
ND
4.8
ug/l
85-68-7
Butyl Benzyl Phthalate
ND
4.8
ug/l
106-47-8
4-Chloroaniline
ND
4.8
ug/l
111-91-1
bis(2-Chloroethoxy)methane
ND
4.8
ug/l
111-44-4
bis(2-Chloroethyl)ether a
ND
4.8
ug/l
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
4.8
ug/l
91-58-7
2-Chloronaphthalene
ND
4.8
ug/1
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
4.8
ug/l
218-01-9
Chrysene
ND
0.19
ug/l
ND = Not detected
J = Indicates an estimated value
RL = Reporting Limit
B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range
N = Indicates presumptive evidence of a compound
01
6 of 36
LA70636

SGS North America Inc.
Report of Analysis
Client Sample ID: GW-1
Lab Sample ID: LA70636-1 Date Sampled: 04/12/21
Matrix: AQ - Ground Water Date Received: 04/ 13/21
Method: EPA 625.1 EPA 625.1 Percent Solids: n/a
Project: PBV-Harrisburg 22 Pepsi Way, Harrisburg, NC
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
Units Q
53-70-3
Dibenzo(a,h)anthracene
ND
0.19
ug/l
132-64-9
Dibenzofaran
ND
4.8
ug/l
95-50-1
1,2-Dichlorobenzene
ND
4.8
ug/l
541-73-1
1,3-Dichlorobenzene
ND
4.8
ug/l
106-46-7
1,4-Dichlorobenzene
ND
4.8
ug/1
91-94-1
3,3'-Dichlorobenzidine
ND
9.5
ug/l
84-66-2
Diethyl Phthalate
ND
4.8
ug/l
131-11-3
Dimethyl Phthalate
ND
4.8
ug/l
84-74-2
Di-n-butyl Phthalate
ND
4.8
ug/l
117-84-0
Di-n-octyl Phthalate
ND
4.8
ug/l
122-66-7
1,2-Diphenylhydrazine
ND
4.8
ug/l
117-81-7
bis(2-Ethylhexyl)phthalate
5.9
4.8
ug/l
206-44-0
Fluoranthene
ND
0.19
ug/l
86-73-7
Fluorene
ND
0.19
ug/l
118-74-1
Hexachlorobenzene
ND
4.8
ug/l
87-68-3
Hexachlorobutadiene
ND
4.8
ug/l
77-47-4
Hexachlorocyclopentadiene a
ND
9.5
ug/l
67-72-1
Hexachloroethane
ND
4.8
ug/l
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.19
ug/l
78-59-1
Isophorone
ND
4.8
ug/l
90-12-0
1-Methylnaphthalene
ND
0.19
ug/l
91-57-6
2-Methylnaphthalene
ND
0.19
ug/1
91-20-3
Naphthalene
0.21
0.19
ug/l
98-95-3
Nitrobenzene
ND
4.8
ug/l
621-64-7
N-Nitroso-di-n-propylamine a
ND
4.8
ug/l
86-30-6
N-Nitrosodiphenylamine
ND
4.8
ug/l
85-01-8
Phenanthrene
ND
0.19
ug/l
129-00-0
Pyrene
ND
0.19
ug/1
120-82-1
1,2,4-Trichlorobenzene
ND
4.8
ug/l
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
37% b
20-75%
4165-62-2
Phenol-d5
25% b
10-60%
118-79-6
2,4,6-Tribromophenol
112% b
38-138%
4165-60-0
Nitrobenzene-d5
79%
44-132%
321-60-8
2-Fluorobiphenyl
76%
40-119%
1718-51-0
Terphenyl-dl4
89%
40-127%
Page 2 of 3
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
7 of 36
LA70636

SGS North America Inc.
Report of Analysis
'lient Sample ID: GW-1
,ab Sample ID: LA70636-1 Date Sampled: 04/12/21
Ratrix: AQ - Ground Water Date Received: 04/ 13/21
mthod: EPA 625.1 EPA 625.1 Percent Solids: n/a
'roject: PBV-Harrisburg 22 Pepsi Way, Harrisburg, NC
ABN List for NC, May 2012
CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q
Page 3 of 3 L
296-56-0 Cycloeicosane 13.37 15 ug/1 JN
Total TIC, Semi -Volatile 15 ug/1 J
(a) Associated CCV outside control limits low. A sensitivity check was analyzed at the project reporting limit
and met 8270D criteria. Sample ND.
(b) Recoveries were corrected for spike concentration.
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
8 of 36
LA70636

SGS North America Inc.
Report of Analysis
Client Sample ID: GW-1
Lab Sample ID: LA70636-1 Date Sampled: 04/12/21
Matrix: AQ - Ground Water Date Received: 04/13/21
Method: EPA 602 Percent Solids: n/a
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 j
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LP303565.1) 1 04/14/21 17:05 NN n/a n/a GLP2998
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
Purgeable Aromatics, Full List
CAS No.
Compound
71-43-2
Benzene
108-90-7
Chlorobenzene
95-50-1
1,2-Dichlorobenzene
541-73-1
1,3-Dichlorobenzene
106-46-7
1,4-Dichlorobenzene
100-41-4
Ethylbenzene
1634-04-4
Methyl Tert Butyl Ether
108-88-3
Toluene
1330-20-7
Xylenes (total)
CAS No.
Surrogate Recoveries
540-36-3
1,4-Difluorobenzene
460-00-4
4-Bromofluorobenzene
Result
RL
Units Q
ND
1.0
ug/l
ND
1.0
ug/l
ND
1.0
ug/l
ND
1.0
ug/l
ND
1.0
ug/l
ND
1.0
ug/l
ND
8.0
ug/l
ND
1.0
ug/l
ND
3.0
ug/l
Run# 1 Run# 2 Limits
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
103% 83-115%
108% 74-131%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 9 of 36
LA70636

SGS North America Inc.
Report of Analysis
Client Sample ID: GW-1
Lab Sample ID: LA70636-1 Date Sampled: 04/12/21
Matrix: AQ - Ground Water Date Received: 04/13/21
Method: MADEP VPH REV 2.1 Percent Solids: n/a
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 j
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LE375863.1) 1 04/14/21 00:55 NN n/a n/a GLE2168
Run #2
Purge Volume
Run # 1 5.0 ml
Run #2
MA VPH list
CAS No. Compound
Result
RL
Units Q
C5- C8 Aliphatics (Unadj.)
ND
100
ug/l
C9- C12 Aliphatics (Unadj.)
ND
100
ug/l
C9- C10 Aromatics (Unadj.)
ND
100
ug/l
CAS No. Surrogate Recoveries
Run# 1
Run# 2
Limits
615-59-8 2,5-Dibromotoluene
98% a
70-130%
615-59-8 2,5-Dibromotoluene
110% b
70-130%
(a) Recovery from Aliphatics fraction.
(b) Recovery from Aromatics fraction.
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 10 of 36
LA70636

SGS North America Inc.
Report of Analysis
Client Sample ID: GW-1
Lab Sample ID: LA70636-1 Date Sampled: 04/12/21
Matrix: AQ - Ground Water Date Received: 04/ 13/21
Method: MADEP EPH REV 2.1 SW846 3511 Percent Solids: n/a
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1 j
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LZ0010793.1) 1 04/16/21 14:56 PC 04/14/21 14:00 OP18417 GLZ231
Run #2
Initial Volume Final Volume
Run #1 50.0 ml 4.0 ml
Run #2
MAEPH List
CAS No.
Compound
Result
C11-C22 Aromatics (Unadj.)
ND
C9-C18 Aliphatics
ND
C19-C36 Aliphatics
ND
CAS No.
Surrogate Recoveries
Run# 1
3386-33-2
1-Chlorooctadecane
74%
84-15-1
o-Terphenyl
75%
321-60-8
2-Fluorobiphenyl
68%
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
RL Units Q
400 ug/l
400 ug/l
400 ug/l
Run# 2 Limits
40-140%
40-140%
40-140%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 11 of 36
LA70636

ffm
Scott, LA
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
1
Section 4
6 12 of 36
LA70636

CHAIN OF CUSTODY PAGE i OF f
[�ta�' SGS North Amenw Inc. - Scott
f f!"� ` 500 Ambassador CaHery Parkway, Scott, LA 70583 Fiao.p T8ck1nga eaNe sax canoes
_...__.-._____..._._.._..--.__;__. {{{ E TEL. 337.237A775 FAX: [phone]
aGSpudna SGSJobN
wwwsgs.comlehsusa
' Cllent / Reporting Information Protect Information Requested Ana! vsis see TEST CODE sheet Matrix Codes
Co pany Name Project Name:
i 1a
vaow,
>�) Se4i c- c�ndele
cow-water
svlee_eAdd rassjj.. t� I ��II / ,t [ skkp'a'44t`` ,n1 �S Sw-Swlaeewatar
L[rok. LA'1 wAI kgCGfw)-f pP' (�'rl U Z� h i WLBiltln Inro—ation t if diHaront from Report to) SD - $oil
City SIffia Lp City State Company Name SL-Sludge
\l SED-Sediment
JI L ZSZ 3 W L oN N 01-00
Prole1te' W CAjQrn 1%
onbct 12-11 project SVeet—as " LIO-Other Liquid
dV r : li3 sic lGi ^ ZG9 CZAR -Air
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ph 9# 2 Client Purcnase Order# city State p (� wP-wipa
,I— J��3 + FB-uiamBlank
`lS �(' E.-Eq timent Blank
SamW nu)Nemels) g Phoyn�e�# Protect Manager ( Iy.a Aaenlion: RB-Rm Blank
t.S2'131-a15 { � TB-TnP Blank
col— Numbmafiaa—daoelea E I
p
spa eel �a2a€�a
smPaa Field ID I Point of COIIeCtiOn comWGrab Date Tyne SunWed By IJabN botlloe i i '�' -i o E w LL) LAB USE ONLY
-1 fare U iz z) nu K
ma —al Time(Businew days) Data Deliverable lreofmation : .:: Comments /Special Instructions
standard 10 Business Days approved av eP .l aro. Q Comroeral.I W (Cavell) Q TRRP Note: Sample inventory is verified upon receipt in the Laboratory
5 Buslness Days RUSH Q Commercial "B" (Level 2) Q RECAP 3�i'A' 1FL'
4 Buslness Days RUSH Q FULLTI (Leve13 4) 0 State Forms • ,�
❑ 3 Buslness Days RUSH 5 / Q REDT1 (Level3a5) Q EDD Format 9,ltA R u ��
2 Business Days RUSH Q Comme"Iel-C" Q Other
❑ 1 Business Day EMERGENCY Cemmeroial'A"=Results Only, avI{en ' L.y1Qa J, 04
Other Commercial "B" = Results DC Summary ',vt
EmergencyB RusM1 TlA tlata available via Lahlink. A proval needed fw RUSH/Emergenc TAT Commemiel'C'=Results♦ QC Summarya PaNal Raw DaW r' ,d a �iiiL �a�L J
Sample Custody must be documented below each time samples change possession, Including courier tlelivery.
PqulsbedU S inPlcr. D bl q: - Rawlvc l RBanWlaa Dabl Imv: Row By:
L y Z tit 3 /L /2: N'i, .�- / --- 2 /-'- %G-'�(. 2
Relinqulehotl Recelveday: Re Wabed 6y:- eel lnw lQ Rene y:
3 3 d nn 7 4
RellnqulaMdby: Dare Tlme. Re -day: Curtotlyaeala .' ❑ IfIRr Proeerved--PPa—. w � Mr�y/tA�/ 1
5 5 ❑ Not elan ❑ AMen1 �- T -ID:
EHSA-DAC-0026-00-FORM-Scoll-Standard COC
http./tw .sgs.mm/er)/terms-and- ndi0ons.
LA70636: Chain of Custody
Page 1 of 3
6 13 of 36
LA70636
EHSA-DAC-0026-00-FORM-Scoll-Standard COC
http./tw .sgs.mm/er)/terms-and- ndi0ons.
LA70636: Chain of Custody
Page 1 of 3
6 13 of 36
LA70636

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LA70636: Chain of Custody
Page 2 of 3
6 14 of 36
LA70636

SGS Sample Receipt Summary
Job Number: LA70636 Client: ATC
Date / Time Received: 4/13/2021 9:40:00 AM Delivery Method:
Cooler Temps (Initial/Adjusted): #1: (1.3/1.3): DV462
Cooler Security Y or N
Y or N
1. Custody Seals Present: ❑d
❑ 3. COC Present:
❑d ❑
2. Custody Seals Intact: W
❑ 4. Smpl Dates/Time OK
❑J ❑
Cooler Temperature
Y or N
1. Temp criteria achieved:
❑� ❑
2. Thermometer ID:
DV462;
3. Cooler media:
Ice (direct contact)
4. No. Coolers:
1
Quality Control Preservation
Y or N N/A
1. Trip Blank present / cooler:
❑ 0 ❑
2. Trip Blank listed on COC:
❑ 0 ❑
3. Samples preserved properly:
F/I ❑
4. VOCs headspace free:
0 ❑ ❑
Comments
FedEx
Project: PBV - HORNSBURG
Airbill Vs: 4920 6966 8340
A
Sample Integrity - Documentation
Y
or N :A
1. Sample labels present on bottles:
W
❑
2. Container labeling complete:
W
❑
3. Sample container label / COC agree:
W
❑
Sample Integrity - Condition
Y
or N
1. Sample recvd within HT:
❑d
❑
2. All containers accounted for:
❑d
❑
3. Condition of sample:
Intact
Sample Intearity - Instructions
Y
or N N/A
1. Analysis requested is clear:
F/A
❑
2. Bottles received for unspecified tests
❑
W
3. Sufficient volume recvd for analysis:
❑/
❑
4. Compositing instructions clear:
❑
❑ 0
5. Filtering instructions clear:
❑
❑ W
LA70636: Chain of Custody
Page 3 of 3
6 15 of 36
LA70636

i
SGS
Scott, LA
Section 5
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
6 16 of 36
LA70636

Method Blank Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP 18408-MB
C0065604A. D
1
04/ 14/21
LL
04/ 13/21
OP 18408
EC2574
The QC reported here applies to the following samples: Method: EPA 625.1
LA70636-1
CAS No. Compound
Result RL Units Q
65-85-0
Benzoic Acid
ND
20
ug/l
59-50-7
4-Chloro-3-methyl Phenol
ND
5.0
ug/l
95-57-8
2-Chlorophenol
ND
5.0
ug/l
120-83-2
2,4-Dichlorophenol
ND
5.0
ug/l
105-67-9
2,4-Dimethylphenol
ND
5.0
ug/l
51-28-5
2,4-Dinitrophenol
ND
20
ug/l
534-52-1
4,6-Dinitro-o-cresol
ND
10
ug/l
95-48-7
2-Methylphenol
ND
5.0
ug/l
3&4-Methylphenol
ND
5.0
ug/l
88-75-5
2-Nitrophenol
ND
5.0
ug/l
100-02-7
4-Nitrophenol
ND
25
ug/l
87-86-5
Pentachlorophenol
ND
10
ug/l
108-95-2
Phenol
ND
5.0
ug/l
88-06-2
2,4,6-Trichlorophenol
ND
5.0
ug/l
83-32-9
Acenaphthene
ND
0.20
ug/1
208-96-8
Acenaphthylene
ND
0.20
ug/l
120-12-7
Anthracene
ND
0.20
ug/l
56-55-3
Benzo(a)anthracene
ND
0.20
ug/l
50-32-8
Benzo(a)pyrene
ND
0.20
ug/l
205-99-2
Benzo(b)fluoranthene
ND
0.20
ug/1
191-24-2
Benzo(g,h,i)perylene
ND
0.20
ug/l
207-08-9
Benzo(k)fluoranthene
ND
0.20
ug/l
100-51-6
Benzyl Alcohol
ND
10
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.0
ug/l
85-68-7
Butyl Benzyl Phthalate
ND
5.0
ug/l
106-47-8
4-Chloroaniline
ND
5.0
ug/l
111-91-1
bis(2-Chloroethoxy)methane
ND
5.0
ug/l
111-44-4
bis(2-Chloroethyl)ether
ND
5.0
ug/l
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
5.0
ug/l
91-58-7
2-Chloronaphthalene
ND
5.0
ug/l
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
5.0
ug/1
218-01-9
Chrysene
ND
0.20
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
0.20
ug/l
132-64-9
Dibenzofuran
ND
5.0
ug/l
95-50-1
1,2-Dichlorobenzene
ND
5.0
ug/l
541-73-1
1,3-Dichlorobenzene
ND
5.0
ug/1
6 17 of 36
LA70636

Method Blank Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 2 of 3
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
)P 18408-MB
C0065604A. D
1
04/ 14/21
LL
04/ 13/21
OP 18408
EC2574
The QC reported here applies to the following samples:
LA70636-1
CAS No.
Compound
Result
RL
Units Q
106-46-7
1,4-Dichlorobenzene
ND
5.0
ug/l
91-94-1
3,3'-Dichlorobenzidine
ND
10
ug/l
84-66-2
Diethyl Phthalate
ND
5.0
ug/l
131-11-3
Dimethyl Phthalate
ND
5.0
ug/l
84-74-2
Di-n-butyl Phthalate
ND
5.0
ug/l
117-84-0
Di-n-octyl Phthalate
ND
5.0
ug/l
122-66-7
1,2-Diphenylhydrazine
ND
5.0
ug/l
117-81-7
bis(2-Ethylhexyl)phthalate
ND
5.0
ug/l
206-44-0
Fluoranthene
ND
0.20
ug/l
86-73-7
Fluorene
ND
0.20
ug/l
118-74-1
Hexachlorobenzene
ND
5.0
ug/l
87-68-3
Hexachlorobutadiene
ND
5.0
ug/l
77-47-4
Hexachlorocyclopentadiene
ND
10
ug/l
67-72-1
Hexachloroethane
ND
5.0
ug/l
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.20
ug/l
78-59-1
Isophorone
ND
5.0
ug/l
90-12-0
1-Methylnaphthalene
ND
0.20
ug/l
91-57-6
2-Methylnaphthalene
ND
0.20
ug/l
91-20-3
Naphthalene
ND
0.20
ug/l
98-95-3
Nitrobenzene
ND
5.0
ug/1
621-64-7
N-Nitroso-di-n-propylamine
ND
5.0
ug/l
86-30-6
N-Nitrosodiphenylamine
ND
5.0
ug/l
85-01-8
Phenanthrene
ND
0.20
ug/1
129-00-0
Pyrene
ND
0.20
ug/l
120-82-1
1,2,4-Trichlorobenzene
ND
5.0
ug/l
CAS No.
Surrogate Recoveries
Limits
367-12-4
2-Fluorophenol
44% a
20-75%
4165-62-2
Phenol-d5
29% a
10-60%
118-79-6
2,4,6-Tribromophenol
105% a
38-138%
4165-60-0
Nitrobenzene-d5
86%
44-132%
321-60-8
2-Fluorobiphenyl
83%
40-119%
1718-51-0
Terphenyl-d14
95%
40-127%
Method: EPA 625.1
6 18 of 36
LA70636

Method Blank Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 3 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP 18408-MB
C0065604A. D
1
04/ 14/21
LL
04/ 13/21
OP 18408
EC2574
The QC reported here applies to the following samples: Method:
LA70636-1
CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q
Total TIC, Semi -Volatile 0 ug/1
(a) Recoveries were corrected for spike concentration.
6 19 of 36
LA70636

Method Blank Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
DP18408-MB
C0065649.1)
1
04/15/21
BH
04/13/21
OP18408
EC2575
The QC reported here applies to the following samples: Method: EPA 625.1
LA70636-1
CAS No. Compound
Result RL Units Q
65-85-0
Benzoic Acid
ND
20
ug/l
59-50-7
4-Chloro-3-methyl Phenol
ND
5.0
ug/l
95-57-8
2-Chlorophenol
ND
5.0
ug/l
120-83-2
2,4-Dichlorophenol
ND
5.0
ug/l
105-67-9
2,4-Dimethylphenol
ND
5.0
ug/l
51-28-5
2,4-Dinitrophenol
ND
20
ug/l
534-52-1
4,6-Dinitro-o-cresol
ND
10
ug/l
95-48-7
2-Methylphenol
ND
5.0
ug/l
3&4-Methylphenol
ND
5.0
ug/l
88-75-5
2-Nitrophenol
ND
5.0
ug/l
100-02-7
4-Nitrophenol
ND
25
ug/l
87-86-5
Pentachlorophenol
ND
10
ug/l
108-95-2
Phenol
ND
5.0
ug/l
88-06-2
2,4,6-Trichlorophenol
ND
5.0
ug/l
83-32-9
Acenaphthene
ND
0.20
ug/1
208-96-8
Acenaphthylene
ND
0.20
ug/l
120-12-7
Anthracene
ND
0.20
ug/l
56-55-3
Benzo(a)anthracene
ND
0.20
ug/l
50-32-8
Benzo(a)pyrene
ND
0.20
ug/l
205-99-2
Benzo(b)fluoranthene
ND
0.20
ug/1
191-24-2
Benzo(g,h,i)perylene
ND
0.20
ug/l
207-08-9
Benzo(k)fluoranthene
ND
0.20
ug/l
100-51-6
Benzyl Alcohol
ND
10
ug/1
101-55-3
4-Bromophenyl Phenyl Ether
ND
5.0
ug/l
85-68-7
Butyl Benzyl Phthalate
ND
5.0
ug/l
106-47-8
4-Chloroaniline
ND
5.0
ug/l
111-91-1
bis(2-Chloroethoxy)methane
ND
5.0
ug/l
111-44-4
bis(2-Chloroethyl)ether
ND
5.0
ug/l
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
5.0
ug/l
91-58-7
2-Chloronaphthalene
ND
5.0
ug/l
7005-72-3
4-Chlorophenyl Phenyl Ether
ND
5.0
ug/1
218-01-9
Chrysene
ND
0.20
ug/1
53-70-3
Dibenzo(a,h)anthracene
ND
0.20
ug/l
132-64-9
Dibenzofuran
ND
5.0
ug/l
95-50-1
1,2-Dichlorobenzene
ND
5.0
ug/l
541-73-1
1,3-Dichlorobenzene
ND
5.0
ug/1
6 20 of 36
LA70636

Method Blank Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 2 of 3
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
)P18408-MB
C0065649.D
1
04/15/21
BH
04/13/21
OP18408
EC2575
The QC reported here applies to the following samples:
LA70636-1
CAS No.
Compound
Result
RL
Units Q
106-46-7
1,4-Dichlorobenzene
ND
5.0
ug/l
91-94-1
3,3'-Dichlorobenzidine
ND
10
ug/l
84-66-2
Diethyl Phthalate
ND
5.0
ug/l
131-11-3
Dimethyl Phthalate
ND
5.0
ug/l
84-74-2
Di-n-butyl Phthalate
ND
5.0
ug/l
117-84-0
Di-n-octyl Phthalate
ND
5.0
ug/l
122-66-7
1,2-Diphenylhydrazine
ND
5.0
ug/l
117-81-7
bis(2-Ethylhexyl)phthalate
ND
5.0
ug/l
206-44-0
Fluoranthene
ND
0.20
ug/l
86-73-7
Fluorene
ND
0.20
ug/l
118-74-1
Hexachlorobenzene
ND
5.0
ug/l
87-68-3
Hexachlorobutadiene
ND
5.0
ug/l
77-47-4
Hexachlorocyclopentadiene
ND
10
ug/l
67-72-1
Hexachloroethane
ND
5.0
ug/l
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.20
ug/l
78-59-1
Isophorone
ND
5.0
ug/l
90-12-0
1-Methylnaphthalene
ND
0.20
ug/l
91-57-6
2-Methylnaphthalene
ND
0.20
ug/l
91-20-3
Naphthalene
ND
0.20
ug/l
98-95-3
Nitrobenzene
ND
5.0
ug/1
621-64-7
N-Nitroso-di-n-propylamine
ND
5.0
ug/l
86-30-6
N-Nitrosodiphenylamine
ND
5.0
ug/l
85-01-8
Phenanthrene
ND
0.20
ug/1
129-00-0
Pyrene
ND
0.20
ug/l
120-82-1
1,2,4-Trichlorobenzene
ND
5.0
ug/l
CAS No.
Surrogate Recoveries
Limits
367-12-4
2-Fluorophenol
43% a
20-75%
4165-62-2
Phenol-d5
27% a
10-60%
118-79-6
2,4,6-Tribromophenol
116% a
38-138%
4165-60-0
Nitrobenzene-d5
86%
44-132%
321-60-8
2-Fluorobiphenyl
82%
40-119%
1718-51-0
Terphenyl-d14
95%
40-127%
Method: EPA 625.1
6 21 of 36
LA70636

Method Blank Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 3 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP18408-MB
C0065649.D
1
04/15/21
BH
04/13/21
OP18408
EC2575
The QC reported here applies to the following samples: Method:
LA70636-1
(a) Recovery corrected for spike concentration.
6 22 of 36
LA70636

Blank Spike/Blank Spike Duplicate Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP 18408-BS
C0065605A. D
1
04/ 14/21
LL
04/ 13/21
OP 18408
EC2574
OP 18408-BSD
C0065606A. D
1
04/ 14/21
LL
04/ 13/21
OP 18408
EC2574
The QC reported here applies to the following samples: Method: EPA 625.1
LA70636-1
Spike
BSP
BSP
BSD
BSD
Limits
CAS No.
Compound
ug/1
ug/l
%
ug/1
%
RPD
Rec/RPD
65-85-0
Benzoic Acid
100
14.0
14
14.4
14
3
12-61/34
59-50-7
4-Chloro-3-methyl Phenol
50
39.5
79
40.1
80
2
66-103/19
95-57-8
2-Chlorophenol
50
37.0
74
35.2
70
5
63-93/17
120-83-2
2,4-Dichlorophenol
50
45.7
91
46.5
93
2
70-104/18
105-67-9
2,4-Dimethylphenol
50
39.5
79
39.8
80
1
64-98/20
51-28-5
2,4-Dinitrophenol
50
44.6
89
50.2
100
12
40-138/24
534-52-1
4,6-Dinitro-o-cresol
50
50.5
101
51.2
102
1
57-131/21
95-48-7
2-Methylphenol
50
29.4
59
27.5
55
7
53-83/18
3&4-Methylphenol
50
25.9
52
24.5
49* a
6
51-77/18
88-75-5
2-Nitrophenol
50
48.9
98
50.0
100
2
67-114/18
100-02-7
4-Nitrophenol
50
13.3
27
13.2
26
1
23-62/28
87-86-5
Pentachlorophenol
50
40.7
81
43.0
86
5
56-113/22
108-95-2
Phenol
50
13.6
27
12.8
26
6
24-50/24
88-06-2
2,4,6-Trichlorophenol
50
45.1
90
46.7
93
3
65-116/19
83-32-9
Acenaphthene
50
40.5
81
40.4
81
0
69-107/18
208-96-8
Acenaphthylene
50
41.1
82
41.3
83
0
67-114/20
120-12-7
Anthracene
50
43.8
88
43.4
87
1
73-109/19
56-55-3
Benzo(a)anthracene
50
42.1
84
41.9
84
0
71-109/19
50-32-8
Benzo(a)pyrene
50
51.8
104
51.6
103
0
73-116/19
205-99-2
Benzo(b)fluoranthene
50
47.2
94
45.7
91
3
73-114/21
191-24-2
Benzo(g,h,i)perylene
50
45.9
92
46.6
93
2
75-113/19
207-08-9
Benzo(k)fluoranthene
50
47.5
95
49.3
99
4
71-118/19
100-51-6
Benzyl Alcohol
50
30.9
62
31.2
62
1
57-90/17
101-55-3
4-BromophenylPhenyl Ether
50
53.9
108
54.1
108
0
70-112/20
85-68-7
Butyl Benzyl Phthalate
50
42.8
86
43.2
86
1
72-118/20
106-47-8
4-Chloroaniline
50
30.2
60
32.5
65
7
60-105/17
111-91-1
bis(2-Chloroethoxy)methane
50
41.5
83
42.0
84
1
68-107/19
111-44-4
bis(2-Chloroethyl)ether
50
33.7
67
32.5
65
4
60-109/18
108-60-1
2,2'-Oxybis(1-chloropropane)
50
28.9
58
28.6
57
1
48-119/18
91-58-7
2-Chloronaphthalene
50
42.7
85
43.1
86
1
67-106/19
7005-72-3
4-Chlorophenyl Phenyl Ether
50
47.6
95
48.2
96
1
67-115/19
218-01-9
Chrysene
50
44.1
88
43.2
86
2
74-108/19
53-70-3
Dibenzo(a,h)anthracene
50
46.7
93
46.4
93
1
75-115/19
132-64-9
Dibenzofuran
50
43.6
87
43.9
88
1
69-110/19
95-50-1
1,2-Dichlorobenzene
50
36.8
74
37.2
74
1
56-95/19
541-73-1
1,3-Dichlorobenzene
50
36.1
72
36.4
73
1
53-93/20
* = Outside of Control Limits.
6 23 of 36
LA70636

Blank Spike/Blank Spike Duplicate Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 2 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP 18408-BS
C0065605A. D
1
04/ 14/21
LL
04/ 13/21
OP 18408
EC2574
OP 18408-BSD
C0065606A. D
1
04/ 14/21
LL
04/ 13/21
OP 18408
EC2574
The QC reported here applies to the following samples:
LA70636-1
CAS No. Compound
Spike BSP BSP BSD
ug/1 ug/l % ug/1
Method: EPA 625.1
BSD Limits
% RPD Rec/RPD
106-46-7
1,4-Dichlorobenzene
50
35.9
72
35.3
71
2
54-93/19
91-94-1
3,3'-Dichlorobenzidine
50
49.7
99
49.5
99
0
67-114/19
84-66-2
Diethyl Phthalate
50
43.4
87
43.8
88
1
72-115/19
131-11-3
Dimethyl Phthalate
50
45.5
91
47.1
94
3
71-114/19
84-74-2
Di-n-butyl Phthalate
50
45.0
90
44.9
90
0
74-113/20
117-84-0
Di-n-octyl Phthalate
50
42.6
85
43.3
87
2
69-118/20
122-66-7
1,2-Diphenylhydrazine
50
46.2
92
46.6
93
1
70-114/19
117-81-7
bis(2-Ethylhexyl)phthalate
50
41.4
83
41.7
83
1
69-118/20
206-44-0
Fluoranthene
50
46.6
93
46.5
93
0
73-113/20
86-73-7
Fluorene
50
44.7
89
44.5
89
0
70-112/19
118-74-1
Hexachlorobenzene
50
49.1
98
49.5
99
1
71-111/20
87-68-3
Hexachlorobutadiene
50
38.9
78
40.4
81
4
45-101/21
77-47-4
Hexachlorocyclopentadiene
50
30.3
61
35.2
70
15
36-109/25
67-72-1
Hexachloroethane
50
31.2
62
31.2
62
0
47-94/20
193-39-5
Indeno(1,2,3-cd)pyrene
50
46.3
93
46.6
93
1
75-114/19
78-59-1
Isophorone
50
37.1
74
38.1
76
3
67-111/18
90-12-0
1-Methylnaphthalene
50
43.5
87
43.0
86
1
67-102/19
91-57-6
2-Methylnaphthalene
50
43.2
86
43.0
86
0
67-102/18
91-20-3
Naphthalene
50
40.0
80
40.6
81
1
66-100/18
98-95-3
Nitrobenzene
50
39.1
78
39.1
78
0
69-109/18
621-64-7
N-Nitroso-di-n-propylamine
50
36.0
72
34.5
69
4
62-113/18
86-30-6
N-Nitrosodiphenylamine
50
44.6
89
44.3
89
1
69-110/20
85-01-8
Phenanthrene
50
41.4
83
41.8
84
1
73-106/20
129-00-0
Pyrene
50
43.8
88
43.6
87
0
74-111/18
120-82-1
1,2,4-Trichlorobenzene
50
41.8
84
42.9
86
3
57-99/19
CAS No.
Surrogate Recoveries
BSP
BSD
Limits
367-12-4
2-Fluorophenol
41% b
39%
b
20-75%
4165-62-2
Phenol-d5
28% b
24%
b
10-60%
118-79-6
2,4,6-Tribromophenol
108% b
108% b
38-138%
4165-60-0
Nitrobenzene-d5
87%
89%
44-132%
321-60-8
2-Fluorobiphenyl
82%
81%
40-119%
1718-51-0
Terphenyl-d14
92%
91%
40-127%
* = Outside of Control Limits.
6 24 of 36
LA70636

Blank Spike/Blank Spike Duplicate Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 3 of 3
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
)P 18408-BS
C0065605A. D
1
04/ 14/21
LL
04/ 13/21
OP 18408
EC2574
)P 18408-BSD
C0065606A. D
1
04/ 14/21
LL
04/ 13/21
OP 18408
EC2574
The QC reported here applies to the following samples: Method: EPA 625.1
LA70636-1
(a) Recovery of this analyte marginally exceeded lower statistical control limits.
(b) Recoveries were corrected for spike concentration.
* = Outside of Control Limits.
6 25 of 36
LA70636

Blank Spike/Blank Spike Duplicate Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP18408-BS
C0065645.D
1
04/15/21
BH
04/13/21
OP18408
EC2575
OP18408-BSD
C0065646.D
1
04/15/21
BH
04/13/21
OP18408
EC2575
The QC reported here applies to the following samples: Method: EPA 625.1
LA70636-1
Spike BSP BSP BSD BSD Limits
CAS No. Compound ug/1 ug/l % ug/l % RPD Rec/RPD
CAS No.
Surrogate Recoveries
BSP
BSD
Limits
367-12-4
2-Fluorophenol
39% a
40% a
20-75%
4165-62-2
Phenol-d5
24% a
26% a
10-60%
118-79-6
2,4,6-Tribromophenol
112% a
108% a
38-138%
4165-60-0
Nitrobenzene-d5
82%
74%
44-132%
321-60-8
2-Fluorobiphenyl
85%
78%
40-119%
1718-51-0
Terphenyl-d14
94%
88%
40-127%
(a) Recovery corrected for spike concentration.
* = Outside of Control Limits.
6 26 of 36
LA70636

i
SGS
Scott, LA AN
Section 6
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
0
6 27 of 36
LA70636

Method Blank Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GLE2168-MBI
LE375858.D
1
04/13/21
NN
n/a
n/a
GLE2168
The QC reported here applies to the following samples:
LA70636-1
CAS No. Compound Result RL Units Q
C5- C8 Aliphatics (Unadj.) ND 100 ug/1
C9- C12 Aliphatics (Unadj.) ND 100 ug/1
C9- C10 Aromatics (Unadj.) ND 100 ug/1
CAS No. Surrogate Recoveries Limits
615-59-8 2,5-Dibromotoluene 98% a 70-130%
615-59-8 2,5-Dibromotoluene 105% b 70-130%
(a) Recovery from Aliphatics fraction.
(b) Recovery from Aromatics fraction.
Method: MADEP VPH REV 2.1
CD
3
6 28 of 36
LA70636

Method Blank Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GLP2998-MBI
LP303562.D
1
04/14/21
NN
n/a
n/a
GLP2998
The QC reported here applies to the following samples:
LA70636-1
CAS No.
Compound
Result
RL
Units Q
71-43-2
Benzene
ND
1.0
ug/l
108-90-7
Chlorobenzene
0.34
1.0
ug/l J
95-50-1
1,2-Dichlorobenzene
0.87
1.0
ug/l J
541-73-1
1,3-Dichlorobenzene
0.63
1.0
ug/l J
106-46-7
1,4-Dichlorobenzene
0.63
1.0
ug/l J
100-41-4
Ethylbenzene
0.23
1.0
ug/l J
1634-04-4
Methyl Tert Butyl Ether
ND
8.0
ug/l
108-88-3
Toluene
ND
1.0
ug/l
1330-20-7
Xylenes (total)
ND
3.0
ug/l
CAS No.
Surrogate Recoveries
Limits
540-36-3
1,4-Difluorobenzene
101%
83-115%
460-00-4
4-Bromofluorobenzene
108%
74-131%
Method: EPA 602
6 29 of 36
LA70636

Blank Spike/Blank Spike Duplicate Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GLE2168-BS1
LE375856.D
1
04/13/21
NN
n/a
n/a
GLE2168
GLE2168-BSD1
LE375857.D
1
04/13/21
NN
n/a
n/a
GLE2168
The QC reported here applies to the following samples: Method: MADEP VPH REV 2.1
LA70636-1
Spike
BSP
BSP
BSD
BSD
Limits
CAS No. Compound
ug/1
ug/l
%
ug/1
%
RPD Rec/RPD
C5- C8 Aliphatics (Unadj.)
120
127
106
127
106
0 70-130/25
C9- C12 Aliphatics (Unadj.)
120
112
93
108
90
4 70-130/25
C9- C10 Aromatics (Unadj.)
40
42.9
107
43.4
109
1 70-130/25
CAS No. Surrogate Recoveries
BSP
BSD
Limits
615-59-8 2,5-Dibromotoluene 102% a 102% a 70-130%
615-59-8 2,5-Dibromotoluene 110% b 110% b 70-130%
(a) Recovery from Aliphatics fraction.
(b) Recovery from Aromatics fraction.
* = Outside of Control Limits.
6 30 of 36
LA70636

Blank Spike/Blank Spike Duplicate Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GLP2998-BS1
LP303560.D
1
04/14/21
NN
n/a
n/a
GLP2998
GLP2998-BSD1
LP303561.D
1
04/14/21
NN
n/a
n/a
GLP2998
The QC reported here applies to the following samples: Method: EPA 602
LA70636-1
Spike
BSP
BSP
BSD
BSD
Limits
CAS No.
Compound
ug/l
ug/l
%
ug/l
%
RPD
Rec/RPD
71-43-2
Benzene
50
45.4
91
45.0
90
1
88-115/10
108-90-7
Chlorobenzene
50
49.1
98
49.9
100
2
88-114/10
95-50-1
1,2-Dichlorobenzene
50
42.9
86
44.9
90
5
54-142/10
541-73-1
1,3-Dichlorobenzene
50
45.1
90
47.2
94
5
83-118/10
106-46-7
1,4-Dichlorobenzene
50
45.1
90
47.2
94
5
80-121/10
100-41-4
Ethylbenzene
50
49.5
99
50.5
101
2
87-114/10
1634-04-4
Methyl Tert Butyl Ether
50
45.7
91
44.6
89
2
68-130/19
108-88-3
Toluene
50
49.0
98
49.3
99
1
88-114/10
1330-20-7
Xylenes (total)
150
149
99
153
102
3
86-114/10
CAS No.
Surrogate Recoveries
BSP
BSD
Limits
540-36-3
1,4-Difluorobenzene
98%
99%
83-115%
460-00-4
4-Bromofluorobenzene
100%
104%
74-131%
* = Outside of Control Limits.
6 31 of 36
LA70636

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
LA70562-5MS
LP303572.D
20
04/14/21
NN
n/a
n/a
GLP2998
LA70562-5MSD
LP303573.D
20
04/14/21
NN
n/a
n/a
GLP2998
LA70562-5
LP303567.D
5
04/14/21
NN
n/a
n/a
GLP2998
The QC reported here applies to the following samples: Method: EPA 602
LA70636-1
LA70562-5
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/l Q
ug/l
ug/l
%
ug/l
ug/l
%
RPD
Rec/RPD
71-43-2
Benzene
75.4
1000
1070
99
1000
1070
99
0
69-129/10
108-90-7
Chlorobenzene
ND
1000
1060
106
1000
1080
108
2
76-122/10
95-50-1
1,2-Dichlorobenzene
ND
1000
1010
101
1000
1040
104
3
37-154/14
541-73-1
1,3-Dichlorobenzene
ND
1000
979
98
1000
1010
101
3
67-129/12
106-46-7
1,4-Dichlorobenzene
ND
1000
979
98
1000
1010
101
3
66-131/13
100-41-4
Ethylbenzene
42.2
1000
1130
109
1000
1140
110
1
75-121/10
1634-04-4
Methyl Tert Butyl Ether
15.3
1000
994
98
1000
1040
102
5
63-136/22
108-88-3
Toluene
203
1000
1300
110
1000
1310
111
1
69-130/10
1330-20-7
Xylenes(total)
408
3000
3730
111
3000
3790
113
2
71-126/10
CAS No.
Surrogate Recoveries
MS
MSD
LA70562-5
Limits
540-36-3
1,4-Difluorobenzene
96%
97%
91%
83-115%
460-00-4
4-Bromofluorobenzene
101%
102%
93%
74-131%
* = Outside of Control Limits.
6 32 of 36
LA70636

Duplicate Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
LA70558-1DUP
LE375860.D
20
04/13/21
NN
n/a
n/a
GLE2168
LA70558-1
LE375861.D
10
04/13/21
NN
n/a
n/a
GLE2168
LA70558-1
LE375859.D
20
04/13/21
NN
n/a
n/a
GLE2168
The QC reported here applies to the following samples: Method: MADEP VPH REV 2.1
LA70636-1
LA70558-1
DUP
CAS No. Compound
ug/1 Q
ug/l
Q RPD
Limits
C5- C8 Aliphatics (Unadj.)
8900
8690
2
50
C9- C12 Aliphatics (Unadj.)
21200 a
21300
0
50
C9- C10 Aromatics (Unadj.)
5370 a
5440
1
50
CAS No. Surrogate Recoveries DUP
615-59-8 2, 5-Dibromotoluene 97% b
615-59-8 2, 5-Dibromotoluene 110%
(a) Result is from Run #2.
(b) Recovery from Aliphatics fraction.
(c) Recovery from Aromatics fraction.
* = Outside of Control Limits.
LA70558-1 LA70558-1 Limits
95% b 97% b 70-130%
112% ° 110% c 70-130%
CD
6 33 of 36
LA70636

SGS
Scott, LA
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
i
Section 7
6 34 of 36
LA70636

Method Blank Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP 18417-MB
LZ0010787. D
1
04/ 16/21
PC
04/ 14/21
OP 18417
GLZ231
The QC reported here applies to the following samples:
LA70636-1
CAS No.
Compound
Result
RL Units Q
C11-C22 Aromatics (Unadj.)
36.9
370 ug/1 J
C9-C18 Aliphatics
24.3
370 ug/1 J
C19-C36 Aliphatics
ND
370 ug/1
CAS No.
Surrogate Recoveries
Limits
3386-33-2
1-Chlorooctadecane
72%
40-140%
84-15-1
o-Terphenyl
70%
40-140%
321-60-8
2-Fluorobiphenyl
59%
40-140%
Method: MADEP EPH REV 2.1
6 35 of 36
LA70636

Blank Spike/Blank Spike Duplicate Summary
Job Number: LA70636
Account: ATCNCR ATC Group Services LLC
Project: PBV-Harrisburg, 22 Pepsi Way, Harrisburg, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP 18417-BS
LZ0010789. D
1
04/ 16/21
PC
04/ 14/21
OP 18417
GLZ231
OP 18417-BSD
LZ0010791. D
1
04/ 16/21
PC
04/ 14/21
OP 18417
GLZ231
The QC reported here applies to the following samples: Method: MADEP EPH REV 2.1
LA70636-1
Spike
BSP
BSP
BSD
BSD
Limits
CAS No. Compound
ug/1
ug/l
%
ug/1
%
RPD
Rec/RPD
C11-C22 Aromatics (Unadj.)
7870
5870
75
5590
71
5
40-140/30
C9-C18 Aliphatics
2780
1900
68
1890
68
1
40-140/30
C19-C36 Aliphatics
3700
2560
69
2620
71
2
40-140/30
CAS No. Surrogate Recoveries
BSP
BSD
Limits
3386-33-2 1-Chlorooctadecane
70%
69%
40-140%
84-15-1 o-Terphenyl
68%
65%
40-140%
321-60-8 2-Fluorobiphenyl
71%
68%
40-140%
Sample Compound
Col #1
Col #2
Breakthrough
Limit
OP 18417-BS 2-Methylnaphthalene
324
ND
0.0%
5.0
OP 18417-BS Naphthalene
317
ND
0.0%
5.0
OP 18417-BSD 2-Methylnaphthalene
313
ND
0.0%
5.0
OP 18417-BSD Naphthalene
306
ND
0.0%
5.0
* = Outside of Control Limits.
6 36 of 36
LA70636

Beverly, Trudy
From: Beverly, Trudy
Sent: Friday, April 23, 2021 10:41 AM
To: Maureen Jackson
Subject: RE: [External] PBV Harrisburg Soil Excavation Letter Report
Received.
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
D— I E North Carolina Department of Environmental Quality
LMpjrL��[0 � � �r UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: ht_pt s://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: hgps://deg.nc.gov/about/divisions/waste-management/ust/ast-proeram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httos://dea.nc. eov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaeement-eis-mans
File Review Procedures:
ht!ps:Hdeq.nc. gov/about/divisions/waste-manaeement/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
htips://deg.nc.gov/about/divisions/waste-manaaement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys://files.ne.tiov/nedea/Waste%2OManaeement/DWM/UST[W hatsNew/Final-Electronic-Document-Submittal-Policv.udf
htips://files.nc. gov/ncdeq/Waste%20Management/D WMJUST/Corrective%2OAction/UST%2Ofile%20names%20for%2OLaserfiche.docx
From: Maureen Jackson [mailto:[e-mail]]
Sent: Friday, April 23, 2021 6:33 AM
To: Beverly, Trudy <[e-mail]>
Subject: [External] PBV Harrisburg Soil Excavation Letter Report
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Good morning. A letter report is attached.
Pepsi would like an expedited response to this report if possible.
Thank you
Maureen
Maureen Jackson I SENIOR PROJECT MANAGER I ATC Group Services LLC
Direct [phone]

609A Piner Road Suite 115 1 Wilmington, NC 28409
maureenJackson@)atc_s.com I www.atcgroupservices.com
This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If you are
not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is strictly prohibited.
If you have received this email in error, please notify the sender by replying to this message and immediately delete and destroy any copies
of this email and any attachments. The views or opinions expressed are the author's own and may not reflect the views or opinions of ATC.