MO-28024_47305_CA_IAR_20200720_Initial Abatement Action Report

-J -J CHARTER
J_j PROPERTIES INC.
July 20, 2020
Underground Storage Tanks Section
NCDEQ, Mooresville Regional Office
610 East Center Avenue, Suite 301
Mooresville, NC 28115
To Whom It May Concern:
We are the owner of property at 3808 Johnston Oehler Road in Charlotte. During a Phase 1
investigation we became aware of an existing underground storage tank that had leaked heating oil. In
association with preparation work for future development of the site, we removed this tank and the
surrounding contaminated soil. This work was conducted under the advisement and observation of ECS
Southeast, LLP with Geologist Roger A. Smith making the final certification. The cleanup work is
documented, and testing data is contained in the enclosed report prepared by ECS and dated July 15,
2020. We submit this report to you for record and consider this remediation action closed with no
further action required.
Sincerely,
/4 V
Phil Vetter
Vice -President Construction
Cc: Roger A. Smith, ECS
SUITE 215 • 1520 SOUTH BOULEVARD, CHARLOTTE, NC 28203-4724
MAIL ADDRESS: P.O. BOX 37166, ZIP 28237-7166 [phone] FAX: [phone]

INITIAL ABATEMENT ACTION REPORT
JOHNSTON OEHLER ROAD APARTMENT SITE
3808 JOHNSTON OEHLER ROAD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS SOUTHEAST, LLP
PROJECT 49-8590D
PREPARED FOR:
CHARTER PROPERTIES, INC.
J U LY 15, 2020

ECS SOUTHEAST, LLP „Setting fhe Standard for Service"
Geotechnical * Constructicn Materials * Environmental * Facilities K Rrgls r d-G dq ip Firm C-5
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July 15, 2020
Mr. Phil Vetter
Charter Properties, Inc.
1520 South Blvd #125
Charlotte, North Carolina 28203
Reference: Initial Abatement Action Report
Johnston Oehler Road Apartment Site
3808 Johnston Oehler Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49-8590D
Dear Mr. Vetter:
ECS Southeast, LLP (ECS) is pleased to provide you with our Initial Abatement Action Report
(IAA) for the above referenced site. Environmental services were provided in general
accordance with ECS Proposal 49:18527-P dated April 2, 2020 and authorized on May 28,
2020. Included in this report is a description of the field activities, the results obtained, and our
conclusions and recommendations.
ECS appreciates the opportunity to provide our environmental consulting services to you on this
project. If you have any questions concerning this report or this project, please contact ECS at
[phone].
Respectfully submitted,
ECS SOUTHEAST, LLP
Rana H. Cavallier
Assistant Staff Environmental Project Manager
loger A. P.G. -
Principal Geologist
ECS C=dpiloi Semon. PL4C - E Florida. L4C * FCZ Mid-Allanklr,, LLQ • EC$ MOA L L- C - ECS 5oulhead. LiP - ECS Soqthwesf, I,LP
W-6W.&GSIIM -1001T!

TABLE OF CONTENTS
SECTION
PAGE
1.0 SITE INFORMATION.....................................................................................................1
2.0 SITE CHARACTERIZATION.......................................................................................... 3
3.0 UST CLOSURE ACTIVITIES.........................................................................................4
4.0 SITE INVESTIGATION...................................................................................................5
5.0 RESULTS - UST CLOSURE ACTIVITIES......................................................................5
6.0 SOIL REMEDIATION ACTIVITIES.................................................................................5
7.0 RESULTS - SOIL REMEDIATION..................................................................................6
8.0 CONCLUSIONS RECOMMENDATIONS.......................................................................6
9.0 RECOMMENDATIONS................................................................................................. 6
10.0 QUALIFICATIONS.......................................................................................................7
FIGURES
Figure 1 Site Topographic Location Map
Figure 2 Aerial Site Map
Figure 3 Sample Location Map
TABLES
Table 1 UST Information
Table 2 Summary of Soil Sample Results
APPENDICES
Appendix A Site Photographs
Appendix B Liquid Manifest
Appendix C Tank Manifest
Appendix D Laboratory Data Sheets and Chain of Custody Records
Appendix E UST-61 Form
Appendix F Non -Hazardous Material Manifests (soil)

Initial Action Abatement Report
Johnston Oehler Road Apartment Site
3808 Johnston Oehler Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49-8590D
July 15, 2020
FACILITY INFORMATION
PARCEL INFORMATION
PROPERTY OWNER
LOCATION
CONTACTS
1.0 SITE INFORMATION
Johnston Oehler Road Apartment Site
3808 Johnston Oehler Road
Charlotte, Mecklenburg County, North Carolina
Mecklenburg County (PINs) 02930132, 02931108A,
02931108B, 02930133, 02930127, and 02930198
Highland Ridge Apartments, LLC
1520 South Blvd, Suite 215
Charlotte, NC 28203
Latitude:-35.365560 N
Longitude:-80.767780 W
Primary Contact: Mr. Phil Vetter
Charter Properties, Inc.
P.O. Box 37166
Charlotte, North Carolina 28237
704-806-1805
Remediation Contractor:
Primary Consultant:
Trifecta Services Company
1722 Toal Street
Charlotte, NC 28206
704-940-3913
c/o Joe Stritmatter
ECS Southeast, LLP
1812 Center Park Drive, Suite D
Charlotte, North Carolina 28217
704-525-5152
Laboratory: Pace Analytical Services, LLC (Pace)
9800 Kincey Avenue, Suite 100
Huntersville, North Carolina 28078
[phone]
State Certification # 12

Initial Action Abatement Report
Johnston Oehler Road Apartment Site
3808 Johnston Oehler Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49-8590D
July 14, 2020
RELEASE INFORMATION
In March 2019 ECS conducted environmental site assessment activities (Phase 11 ESA) at the
site as part of due diligence activities for a potential real estate transaction. In general, the
Phase €1 ESA consisted of the collection and laboratory analysis of four soil samples and five
soil -gas samples at the subject site.
The results of the Phase 1€ ESA identified the following results that exceeded their respective
guidance levels:
Laboratory analysis of soil sample SS-1 (collected adjacent to the heating oil UST)
contained total petroleum hydrocarbons — diesel range organics (TPH-DRO) at a
concentration of 2,223 milligrams per kilogram (mg/kg), which exceeds the North
Carolina Department of Environmenta€ Quality (NCDEQ) State Action level of 100
mg/kg.
■ Laboratory analysis of soil -gas sample SGA (collected adjacent to the heating oil UST)
contained 1,1,2-trichloroethane (280 micrograms per cubic meter or pglm3); 1,2,4-
trimethylbenzene (570 pglm3); ethy€benzene (630 pglm3); and total xylenes (790 Pglm3)
at concentrations above their respective NCDEQ residential soil -gas screening levels
(residential SGSLs) of 1.4 pgfm3; 420 pgfm3; 370 pglm3; and 700 pglm3, respectively.
Although the detections are typically constituents associated with petroleum products
such as heating oil, the detection of 1,1,2-trlchloroethane is a chlorinated solvent and
would not be expected to be associated with heating oil.
Seal and Si nature of Certif inq Licensed Geolo ist
€, Roge'AA),@M4k A Licensed Geologist for ECS Southeast, LLP, do certify that the information
cor +n%...s lsrsis correct and accurate to the best of my knowledge.
i
AL
Roger A. rMUP_G.
NC License No. 1724
ECS Southeast, LLP is permitted to practice geology/engineering in North Carolina. The
certification number of the corporation is C-406.

Initial Action Abatement Report
Johnston Oehler Road Apartment Site
3808 Johnston Oehler Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49-8590D
July 15, 2020
2.0 SITE CHARACTERIZATION
The subject property is located at 3808 Johnston Oehler Road in Charlotte, Mecklenburg
County, North Carolina (Figure 1 and Figure 2). The approximately 40.85-acre subject property
was occupied by two residences, several shed buildings, and several dilapidated buildings. The
subject property is serviced by groundwater supply wells and septic systems. The buildings
were heated with heating oil stored in above -ground storage tanks (ASTs) and underground
storage tanks (USTs).
ECS performed a Phase I Environmental Site Assessment (Phase I ESA) for the subject
property (ECS Project No. 49:8590) which was summarized in a report dated January 31, 2019.
Three recognized environmental conditions (RECs) were identified in the Phase I ESA report
and are listed below:
• ECS considered the presence of the fill port and vent pipe indicative of an underground
storage tank (UST) reportedly used for storing heating oil is located at the residence on
the eastern portion of the subject property to represent a REC.
• A heating oil above ground storage tank (AST) with heavy staining on the surface of the
AST was observed at the eastern residence. ECS considered the presence of this AST
as well as the staining observed to represent a REC.
ECS considered the possibility for the migration of the known groundwater
contamination resulting from a release of heating oil on the west adjacent property
(Johnston Property at 4414 Johnston -Oehler Road) to be a REC for the subject property.
Based upon conversations between Mr. Joseph Nestor of ECS and Charter Properties, Inc.
(Charter) on February 12, 2019, ECS understood that Charter intends to develop the subject
property as an apartment complex and/or condominium complex.
In order to further evaluate the RECs identified during the Phase I ESA, ECS conducted
environmental site assessment activities (Phase II ESA) and reported to results in a March 27,
2019 report (ECS project No. 49-8590-A). In general, the Phase II ESA consisted of the
collection and laboratory analysis of four soil samples and five soil -gas samples at the subject
site. The results of the Phase II ESA identified the following results that exceeded their
respective guidance levels:
Laboratory analysis of soil sample SS-1 (collected adjacent to the heating oil UST)
contained TPH-DRO at a concentration of 2,223 mg/kg, which exceeds the NCDEQ
State Action level of 100 mg/kg.
Laboratory analysis of soil -gas sample SG-1 (collected adjacent to the heating oil UST)
contained 1,1,2-trichloroethane (280 pg/m3); 1,2,4-trimethyl benzene (570 pg/m3);
ethylbenzene (630 pg/m3); and total xylenes (790 fag/m3) at concentrations above their
respective NCDEQ residential SGSLs of 1.4 lag/m3; 420 fag/m3; 370 fag/m3; and 700
fag/m3, respectively. Although the detections are typically constituents associated with
petroleum products such as heating oil, the detection of 1,1,2-trichloroethane is a
chlorinated solvent and would not be expected to be associated with heating oil.
3

Initial Action Abatement Report
Johnston Oehler Road Apartment Site
3808 Johnston Oehler Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49-8590D
July 15, 2020
Based on a conversation between Mr. Vetter of Charter and Mr. Smith of ECS on March 30,
2020, ECS understands that Charter has completed the purchase of the properties and have
demolishing the site structures, thereby allowing access to remove the referenced AST, UST,
and the identified impacted soils.
As determined from the USGS topographical map, D e r i t a, North Carolina (dated 2 0 19 )
North Carolina quadrangle, the subject site is situated approximately 770 feet above mean sea
level with topography sloping to the s o u t h e a s t. Based on a review of the topographic map
and observations of general area and site topography, surface run-off would be expected to
flow to the southeast, towards Stoney Creek.
The subject site is located within the Charlotte Belt of the Piedmont Physiographic
Province. The soils encountered in this area are the residual product of in -place chemical
weathering of rock presently underlying the site and/or historic depositional events. In
general, shallow unconfined groundwater movement within the overlying soils is controlled
largely by topographic gradients. However, as the groundwater percolates downward, it
becomes controlled by the subsurface geologic conditions. Thus, the direction of
groundwater movement in the deeper aquifers may not be consistent with the reflecting
topography.
Surface waters primarily recharge shallow aquifers by infiltration along higher elevations. Once
in the shallow aquifer, the groundwater typically discharges into streams or other surface
water bodies at lower elevations. The depth of the shallow water table is transient and
can vary with seasonal fluctuations in precipitation. Groundwater movement in the shallow
aquifer is generally from higher to lower elevations. As such, shallow groundwater is
expected to flow generally to the southeast.
3.0 UST CLOSURE ACTIVITIES
On June 8, 2020, , ECS personnel met personnel from Trifecta Services Company (Trifecta) of
Charlotte, North Carolina at the site to begin closure activities. Closure activities included the
removal of the 350-gallon non-commercial heating oil UST. Site photographs of the UST closure
activities are include in Appendix A. Approximately 287 gallons of liquid was removed from the
UST by Legacy Environmental services, LLC (Legacy) using a vacuum truck. The liquid was
transported to the Legacy facility in Charlotte, North Carolina for disposal. A liquid manifest is
included in Appendix B. The top of the UST was located approximately two (2) feet below the
ground surface (bgs).
A tracked mini -excavator was used to complete the removal activities. Overlying soil was removed
with the excavator to expose the UST. The UST was removed from the exaction, cleaned, and
inspected. Multiple holes were observed on the surface of the UST. The UST measured
approximately 32 inches in diameter and 62 inches in length. UST information is summarized in
Table 1. The UST was transported by Trifecta to their facility in Charlotte, North Carolina for
disposal. A UST disposal manifestis included in Appendix C. Groundwater or bedrock was not
encountered during closure activities.
4

Initial Action Abatement Report
Johnston Oehler Road Apartment Site
3808 Johnston Oehler Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49-8590D
July 15, 2020
4.0 SITE INVESTIGATION
4.1 Field Screening
Following removal of the UST from the site, Trifecta used the excavator to assist the ECS
environmental professional in collecting a representative closure samples of soil from the base of
the tank excavation. The sample was screened using visual and olfactory observations as well as
with a Foxboro Model 2020 total vapor analyzer which is a flame ionization detector (FID). A
portion of soil was placed in a re -sealable plastic bag for the purpose of field screening. The plastic
bag was placed in a warm location for approximately ten minutes to allow the headspace in the bag
to equilibrate. The probe of the FID was inserted into the bag, and the bag was immediately
resealed. The FID meter was monitored and the readings recorded. The FID readings are
summarized in Table 2. Field screening indicated that a release had occurred from the UST.
4.2 Sample Collection and Analysis
The excavator was used to assist in the collection of closure soil sample UST-1A from the base of
the excavation. The sample was collected from an approximate depth of 6-7 feet below ground
surface (bgs). The ECS personnel on site manually collected the samples directly from the bucket
of the excavator. The sampler wore new, disposable powder free nitrile gloves to collect the
sample from each sample location. Petroleum odors and staining were observed during collection
of the soil sample. The sample location is illustrated on Figure 3.
The soil sample was placed into laboratory prepared containers. After being filled, the sample
containers were labeled and placed into a cooler containing ice to maintain the samples at
approximately 4° Celsius. The samples were transported to Pace Analytical Services, LLC
(Pace), a North Carolina licensed laboratory located in Huntersville, North Carolina to be
analyzed for TPH-GRO/DRO using EPA Methods 5035/8010 and 3550/8010, respectively. The
samples were transported to the laboratory under chain of custody. A copy of the chain of
custody is included in Appendix D.
5.0 RESULTS - UST CLOSURE ACTIVITIES
Laboratory analysis of closure soil sample UST-1 collected from beneath the UST detected
TPH-GRO and TPH-DRO above the NCDEQ Action Levels of 50 parts per million (ppm) and
100 ppm, respectively. A summary of the analytical results are shown on Table2. The laboratory
data sheets and Chain -of -Custody Records are found in Appendix E. Upon receipt of the
laboratory analytical results, ECS submitted the North Carolina Department of Environmental
Quality (NCDEQ) Form UST-61 to the NCDEQ, Mooresville Regional Office. A copy of the
submitted UST-61 form is included in Appendix E.
6.0 SOIL REMEDIATION/INITIAL ABATEMENT ACTIVITIES
Based on the field observations and the Phase II analytical results, ECS personnel observed
and documented the removal of approximately 77.72 tons of petroleum impacted soil from the
UST excavation by Trifecta. As the soil was being excavated, ECS screened soil samples
collected from the sidewalls and base of the excavation with the FID. Excavation continued until
FID readings were below 50 ppm. The final excavation was approximately 17 feet long 12 feet
5

Initial Action Abatement Report
Johnston Oehler Road Apartment Site
3808 Johnston Oehler Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49-8590D
July 15, 2020
wide and 10 feet deep. The impacted soil was transported to Environmental Soils of North
Carolina in Shelby, North Carolina for disposal. The Non -Hazardous Materials Manifests for the
soil is included in Appendix F.
Over-excavation/confirmation soil samples SW-1, SW-2, SW-3 and SW-4 were collected from
each sidewall at a depth of 9-10 feet bgs and sample B-1 was collected from the base of the
excavation at a depth of 10 to 11 feet bgs. The approximate location of the soil samples are
indicated on Figure 3.
The sampler, wearing a new pair of nitrile gloves, placed the samples in laboratory prepared
containers. Each container was labeled and placed in a cooler containing ice to maintain the
samples at approximately 4° Celsius. The samples were submitted to Pace for risk -based
analysis, in accordance with NCDEQ, UST guidance for volatile organic compounds (VOCs)
and semi -volatile organic compounds (SVOCs) using EPA Methods 8260 and 8270,
respectively and for extractible and volatile petroleum hydrocarbons (EPH and VPH) using the
Massachusetts Department of Environmental Protection (MADEP) Methods. Chain -of -Custody
Records are included in Appendix D.
7.0 RESULTS -SOIL REMEDIATION
Laboratory analysis of soil samples SW-2, SW-4, and B-1 did not detect targeted compounds
above the laboratory detection limits. Laboratory analysis of soil sample SW-1 detected C9-C18
aliphatic hydrocarbons above the laboratory detection limits but below its Soil -to -Water,
residential, and industrial/commercial MSCCs. Laboratory analysis of soil sample SW-3
detected toluene above the laboratory detection limits but below its Soil -to -Water, residential,
and industrial/commercial MSCCs. A summary of the analytical results are shown on Table 2.
The laboratory data sheets and Chain -of -Custody Records are found in Appendix D.
8.0 CONCLUSIONS RECOMMENDATIONS
Based on the results of the investigation, ECS has the following conclusions:
• A release of petroleum had occurred from the UST.
• Approximately 78 tons of impacted was removed for off -site disposal.
• Laboratory results of over-excavation/confirmation soil samples collected from the sidewalls
and floor of the final excavation did not detect petroleum related compounds above their
respective Soil -to -Water MSCCs.
9.0 RECOMMENDATIONS
Based on the results of the investigation, ECS recommends that:
• A copy of this report be provided to the current property owner and that a copy be
submitted to the NCDEQ Mooresville Regional Office for their review.
• The NCDEQ issue a Notice of No Further Action (NFA) and the incident be closed.
C1

Initial Action Abatement Report
Johnston Oehler Road Apartment Site
3808 Johnston Oehler Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49-8590D
July 15, 2020
10.0 QUALIFICATIONS
The activities and evaluative approaches used in this assessment are generally consistent with
those normally employed in assessments and remediation projects of this type. ECS' evaluation of
site conditions has been based on our understanding of the project information and the data
obtained during our field activities.
7

FIGURES

dta= a._ I.I.,
�irnr� i_k- t&rdL FN
SITE
4?4?7 =
WIC.
qmr
0
NJ
R,y_ d,�yl�r•�L�Ir — APPROXIMATE SITE BOUNDARY
SOURCE: �i
USGS TOPOGRAPHIC MAP FIGURE 1
7.5 —MINUTE SERIES s SITE TOPOGRAPHIC LOCATION MAP
DERITA, NCEro
DATED: 2019 3808 JOHNSTON OEHLER ROAD
SCALE: 1 : 24,000 CHARLOTTE, MECKLENBURG COUNTY, NC
CONTOUR INTERVAL = 10' ECS PROJECT NO. 49-8590D
TM

�T
%1 k
71
4
Al 1 71 1
- See Figure 3
44.
161 ! 1
_IL
-p
16
- L ti a1�
1''•*�y jp 1 1
W� .
� � r
A ton
IM
r r �
J
I
SOURCE: FIGURE 2
i s AERIALSITE MAP
GOOGLE EARTH
2016 3808 JOHNSTON OEHLER ROAD
�\ CHARLOTTE, MECKLENBURG COUNTY, NC
' ' = 300 FEET IT. ECS PROJECT NO. 49-8590D

Former House
SOURCE:
ECS FIELD NOTES
Approximate Area of Excavation
mer UST
W _-� � FIGURE 3
E
s SAMPLE LOCATION MAP
3808 JOHNSTON OEHLER ROAD
CHARLOTTE, MECKLENBURG COUNTY, NC
= 10 FEET
7M
ECS PROJECT NO. 49-8590D

TABLES

TABLE 1: UST INFORMATION
Johnston Oehler Road Apartment Site
3808 Johnston Oehler Road
Charlotte, Mecklenburg County, North Carolina
ECS Project 49-8590D
UST ID
Last
Previous
Capacity
Construction
Tank
Installation
Status
Release
Number
Contents
Contents
(Gallons)
Details
Dimensions
Date
Removed
1
Fuel Oil
Fuel Oil
350
Single Wall Steel
62" X 32"
Unknown
Yes
6/8/2020

TABLE 1: SUMMARY OF SOIL SAMPLE RESULTS
Johnston Oehler Road Apartment Site
3808 Johnston Oehler Road
Charlotte, Mecklenburg County, North Carolina
ECS Project 49-8590D
Sample Identification
UST-1A
SW-1
SW-2
SW-3
SW-4
B-1
ACTION
LEVEL
(mg/kg)
Soil -to -Water
MSCC (mg/kg)
Residential
MSCC
(mg/kg)
Industrial
Commercial
MSCC
m /k
Sample Date
6/8/2020
FID Readings
358 10.6
16.4
1 7.9
18.8
26.3
Sample Depth (ft. bgs)
6-7
8-9
9-10
TPH by EPA 3550/5035
GRO
130
--
--
--
--
--
50
--
--
--
DRO
3,760
--
--
--
--
--
100
--
--
--
VOCs by EPA 8260 (mg/kg)
Toluene
--
ND
0.0068
Nr
--
0.12
100
4,000
SVOCs by EPA 8270BN (mg/kg)
All Target Compounds
--
4L
ND
ND
--
--
--
--
EPH and VPH by MADEP (mg/kg)
C5-C8 Aliphatics
--
ND
ND
ND
ND
ND
--
68
939
24,528
C9-Cl8 Aliphatics
--
12.1
ND
ND
ND
ND
--
540
1,500
40,000
C19-C36 Aliphatics
--
ND
ND
ND
ND
ND
--
--
31,000
810,000
C9-C22 Aromatics
--
ND
ND
ND
ND
ND
--
31
469
12,264
NOTES:
bgs = below the ground surface
TPH = Total Petroleum Hydrocarbons
UVF = Ultraviolet Flourescence
GRO = Gasoline Range Organic
DRO = Diesel Range Organic
EPH = Extractable Petroleum Hydrocarbons
VPH = Volatile Petroleum Hydrocarbons
MADEP = Massachuttets Deparetmen of Environmental Protection
mg/kg = milligrams per kilogram = ppm (parts per million)
BOLD = Concentration Exceeds Action Level or Soil -to -Water MSCC

APPENDIX A
(Site Photographs)

•'r
Photograph 1: UST Discovered During Site Grading Activities
J Jam} 3 .pc �} t' s
Photograph 2: Excavation of UST
PHOTOGRAPH LOG
3808 JOHNSTON OEHLER ROAD
CHARLOTTE, MECKLENBURG COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-8590D

APPENDIX B
(Liquid Manifest)

Legacy
ENVIRONMENTAL SERVICES, LLC
P.O. BOX 37333 - CHARLOTTE, N.C. 28237
[phone]
FAX [phone]
NON -HAZARDOUS SPECIAL WASTE
Manifest No.
Job No. �
9837
P.O. No.
Trk. No.VT - t5
MAILING ADORE I ADDRESS
CITY / STATE f�i CITY STATE ZIP
PHONE NO.
DES. OF WASTE:
PHONE Ni
CONTACT
Section1I. INVOICE INFORMATION SOLIDSGALLONS DRUMS
DESCRIPTION
QUANTITY
LINE TOTAL
1. NON-HAZ MINERAL OIL FOR RECYCLE
2. PETROLEUM CONTACTWATER PUMPED FROM TANKS, DRUMS OR CONTAINMENTAREA
3. OFF -SPEC LIGHT OIL, DIESEL OR GAS PUMPED FROM TANKS OR DRUMS
4. SEDIMENTOR SOLIDS VACUUMED FROM CONTAINMENTAREA
5. 55-GALLON DRUMS REMOVED - LIQUID, SOLID OR EMPTY
6. LIQUIDS & SOLIDS REMOVED FROM CAR WASH
7.
8.
9.
10.
GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR Part 261 or any applicable state law, has been properly
described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if the waste is a treatment residue of a previously restricted
hazardous waste subject to the Land Disposal Restrictions, I certify and warrant that the waste has been treated in accordancewith the requirements of 40 CFR Part 268 and is no longer
a hazardous waste as defined by 40 CFR Part 261.
4r1'tP I(A dw 1 (1" / Q 1
GeneraAAAuthorized Agent Nn� Sign ure shipment Date
Section III. TRANSPORTER
Legacy TRANSPORTER II
ENVIRONMENTAL SERVICES, LLC e. Name
P.O. BOX 37333• CHARLOTTE, N.C. 28237 f. Address
a. Driver
b. Phone P
Hazardous
EPA NCDD
Envir. Serv.
Site Name:
c. Truck No. V
15
rIvan a Fri
g. Driver Name/Title
In. Phone No.
j. Transporter II Permit Nos.
Dever Signature
Truck No.
Ship
704-361-5837
a. Phone No. P.O. Box 37333
Physical Address: Charlotte, NC 28206 b. Mailing Address: Charlotte, NC 28237
e: Discrepancy Indication Space
This is to clarify that all non-hazantous material removed from above location has been transported and will be disposed of In accordance wM applicable local, state and federal regulations in the fdbwing manner: (1) Petideum
products are blended into a beneficial reusable fuel for use in large industrial bumers. (2) Waste waters are to be tested wth polymers, pH adjusters, and a flooarlant than flows through a dissolved air flotation system for paceatnent
separation. (3) Solids from treatment systems are hauled to E.P.A. approved facilities for proper disposal. Manifest and certificate of disposal are on file. (4) Our treatment system operates on a first in, first out basis
and product should be processed within seven days.
SIGNATURE OF FACILITVAGENT 'C_ JW ffjid'�, MONTH DATE p
� (p 1 DAY '76, VEAR;;�Cj

APPENDIX C
(Tank Manifest)

SOUTHERN METALS COMPANY
6-25-2020
To whom it may concern,
This letter states that the fully drained fuel(oil) tank hauled
to SMC by Trifecta from the Highland ridge apartment job
on 3808Johnston Oehler Rd, Charlotte NC 28269 for
Charter Properties will be destroyed by shearing and sold to
a mill for remelting purposes only.
Witness: Andy in
J
P.O. BOX 668923. 2200 DONALD ROSS ROAD, CHARLOTTE, NORTH CAROLINA 28266-8923 [phone]

APPENDIX D
(Laboratory Data Sheets and Chain of Custody Records)

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 18, 2020
Mr. Randy Cavallier
ECS Southeast, LLP
4811 Koger Blvd.
Greensboro, NC 27407
RE: Project: Johnson Oehler
Pace Project No.: 92480851
Dear Mr. Cavallier:
Enclosed are the analytical results for sample(s) received by the laboratory on June 08, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
[phone]
Project Manager
Enclosures
cc: ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 48

lacieAnalyfica('
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Johnson Oehler
Pace Project No.: 92480851
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A21LA 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 48

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Johnson Oehler
92480851
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92480851001
UST-1
EPA 8015C Modified
JMS1
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92480851002
SW-1
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
ACG
5
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KBC
1
PAN
92480851003
SW-2
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
ACG
5
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KBC
1
PAN
92480851004
SW-3
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
ACG
5
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KBC
1
PAN
92480851005
SW-4
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
ACG
5
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KBC
1
PAN
92480851006
B-1
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
ACG
5
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KBC
1
PAN
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: UST-1
Lab ID: 92480851001 Collected: 06/08/20 09:15 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-C28)
3760 mg/kg 74.0 10 06/09/20 20:21
06/11/20 21:37
Surrogates
n-Pentacosane (S)
0 % 33-129 10 06/09/20 20:21
06/11/20 21:37
629-99-2 S4
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
130 mg/kg 6.4 1 06/09/20 12:15
06/09/20 22:38
Surrogates
4-Bromofluorobenzene (S)
266 % 63-130 1 06/09/20 12:15
06/09/20 22:38
460-00-4 S5
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
32.2 % 0.10 1
06/09/20 13:33
Sample: SW-1
Lab ID: 92480851002 Collected: 06/08/20 10:10 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
Aliphatic (C09-C18)
ND mg/kg 12.7 1 06/11/20 11:22
06/15/20 11:26
N2
Aliphatic (C19-C36)
ND mg/kg 12.7 1 06/11/20 11:22
06/15/20 11:26
N2
Aromatic (C11-C22)
ND mg/kg 12.7 1 06/11/20 11:22
06/15/20 11:26
N2
Surrogates
Nonatriacontane (S)
62 % 40-140 1 06/11/20 11:22
06/15/20 11:26
7194-86-7
o-Terphenyl (S)
83 % 40-140 1 06/11/20 11:22
06/15/20 11:26
84-15-1
2-Fluorobiphenyl (S)
113 % 40-140 1 06/11/20 11:22
06/15/20 11:26
321-60-8
2-Bromonaphthalene (S)
65 % 40-140 1 06/11/20 11:22
06/15/20 11:26
580-13-2
MADEPV
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
Aliphatic (C05-CO8)
ND mg/kg 6.01 1 06/08/20 10:10
06/16/20 00:40
Aliphatic (C09-C12)
12.1 mg/kg 6.01 1 06/08/20 10:10
06/16/20 00:40
Aromatic (C09-C10),Unadjusted
ND mg/kg 6.01 1 06/08/20 10:10
06/16/20 00:40
TPHC9C10A
Surrogates
2,5-Dibromotoluene (FID)
108 % 70.0-130 1 06/08/20 10:10
06/16/20 00:40
615-59-8FID
2,5-Dibromotoluene (PID)
89.8 % 70.0-130 1 06/08/20 10:10
06/16/20 00:40
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Acenaphthene
ND mg/kg 0.42 1 06/09/20 21:16
06/11/20 11:19
83-32-9
Acenaphthylene
ND mg/kg 0.42 1 06/09/20 21:16
06/11/20 11:19
208-96-8
Aniline
ND mg/kg 0.42 1 06/09/20 21:16
06/11/20 11:19
62-53-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 48

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-1
Lab ID: 92480851002 Collected:
06/08/20
10:10
Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Anthracene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
207-08-9
Benzoic Acid
ND
mg/kg
2.1
1
06/09/20 21:16
06/11/20 11:19
65-85-0
Benzyl alcohol
ND
mg/kg
0.85
1
06/09/20 21:16
06/11/20 11:19
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.85
1
06/09/20 21:16
06/11/20 11:19
59-50-7
4-Chloroaniline
ND
mg/kg
0.85
1
06/09/20 21:16
06/11/20 11:19
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
91-58-7
2-Chlorophenol
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
7005-72-3
Chrysene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
53-70-3
Dibenzofuran
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.85
1
06/09/20 21:16
06/11/20 11:19
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
120-83-2
Diethylphthalate
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
105-67-9
Dimethylphthalate
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.85
1
06/09/20 21:16
06/11/20 11:19
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.1
1
06/09/20 21:16
06/11/20 11:19
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
606-20-2 L2,v2
Di-n-octylphthalate
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
117-84-0 v1
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
117-81-7
Fluoranthene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
206-44-0
Fluorene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
87-68-3
Hexachlorobenzene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
77-47-4
Hexachloroethane
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
193-39-5
Isophorone
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
91-57-6
REPORT OF LABORATORY ANALYSIS
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Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 48

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-1
Lab ID: 92480851002 Collected:
06/08/20
10:10
Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report
Limit
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
2-Methylphenol(o-Cresol)
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
15831-10-4
Naphthalene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
91-20-3
2-Nitroaniline
ND
mg/kg
2.1
1
06/09/20 21:16
06/11/20 11:19
88-74-4
3-Nitroaniline
ND
mg/kg
2.1
1
06/09/20 21:16
06/11/20 11:19
99-09-2
4-Nitroaniline
ND
mg/kg
0.85
1
06/09/20 21:16
06/11/20 11:19
100-01-6
Nitrobenzene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
98-95-3
2-Nitrophenol
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
88-75-5
4-Nitrophenol
ND
mg/kg
2.1
1
06/09/20 21:16
06/11/20 11:19
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
108-60-1
Pentachlorophenol
ND
mg/kg
0.85
1
06/09/20 21:16
06/11/20 11:19
87-86-5
Phenanthrene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
85-01-8
Phenol
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
108-95-2
Pyrene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
129-00-0
Pyridine
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.42
1
06/09/20 21:16
06/11/20 11:19
88-06-2
Surrogates
Nitrobenzene-d5 (S)
71
%
23-110
1
06/09/20 21:16
06/11/20 11:19
4165-60-0
2-Fluorobiphenyl (S)
68
%
30-110
1
06/09/20 21:16
06/11/20 11:19
321-60-8
Terphenyl-d14 (S)
73
%
28-110
1
06/09/20 21:16
06/11/20 11:19
1718-51-0
Phenol-d6 (S)
70
%
22-110
1
06/09/20 21:16
06/11/20 11:19
13127-88-3
2-Fluorophenol (S)
70
%
13-110
1
06/09/20 21:16
06/11/20 11:19
367-12-4
2,4,6-Tribromophenol (S)
68
%
27-110
1
06/09/20 21:16
06/11/20 11:19
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation
Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.10
1
06/10/20 15:16
06/10/20 17:47
67-64-1
Benzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
71-43-2
Bromobenzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
108-86-1
Bromochloromethane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
74-97-5
Bromodichloromethane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
75-27-4
Bromoform
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
75-25-2
Bromomethane
ND
mg/kg
0.010
1
06/10/20 15:16
06/10/20 17:47
74-83-9 IK
2-Butanone (MEK)
ND
mg/kg
0.10
1
06/10/20 15:16
06/10/20 17:47
78-93-3
n-Butylbenzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
56-23-5
Chlorobenzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
108-90-7
Chloroethane
ND
mg/kg
0.010
1
06/10/20 15:16
06/10/20 17:47
75-00-3
REPORT OF LABORATORY ANALYSIS
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Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-1
Lab ID: 92480851002 Collected:
06/08/20
10:10
Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report
Limit
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Chloroform
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
67-66-3
Chloromethane
ND
mg/kg
0.010
1
06/10/20 15:16
06/10/20 17:47
74-87-3 v2
2-Chlorotoluene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
96-12-8
Dibromochloromethane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
106-93-4
Dibromomethane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.010
1
06/10/20 15:16
06/10/20 17:47
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
108-20-3
Ethylbenzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
87-68-3
2-Hexanone
ND
mg/kg
0.050
1
06/10/20 15:16
06/10/20 17:47
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
99-87-6
Methylene Chloride
ND
mg/kg
0.020
1
06/10/20 15:16
06/10/20 17:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.050
1
06/10/20 15:16
06/10/20 17:47
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
1634-04-4
Naphthalene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
91-20-3
n-Propylbenzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
103-65-1
Styrene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
79-34-5
Tetrachloroethene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
127-18-4
Toluene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
79-00-5
Trichloroethene
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0050
1
06/10/20 15:16
06/10/20 17:47
75-69-4
REPORT OF LABORATORY ANALYSIS
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Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-1 Lab ID: 92480851002 Collected: 06/08/20 10:10 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
mg/kg
0.0050
1
06/10/2015:16
06/10/2017:47
96-18-4
ND
mg/kg
0.0050
1
06/10/2015:16
06/10/2017:47
95-63-6
ND
mg/kg
0.0050
1
06/10/2015:16
06/10/2017:47
108-67-8
ND
mg/kg
0.050
1
06/10/2015:16
06/10/2017:47
108-05-4
ND
mg/kg
0.010
1
06/10/2015:16
06/10/2017:47
75-01-4
ND
mg/kg
0.010
1
06/10/2015:16
06/10/2017:47
1330-20-7
ND
mg/kg
0.010
1
06/10/2015:16
06/10/2017:47
179601-23-1
ND
mg/kg
0.0050
1
06/10/2015:16
06/10/2017:47
95-47-6
96
%
70-130
1
06/10/2015:16
06/10/2017:47
2037-26-5
100
%
70-130
1
06/10/2015:16
06/10/2017:47
460-00-4
80
%
70-132
1
06/10/2015:16
06/10/2017:47
17060-07-0
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
20.7 % 0.10 1 06/09/2013:33
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
83.1 % 1 06/16/2013:10 06/16/2013:18
Sample: SW-2 Lab ID: 92480851003 Collected: 06/08/20 10:20 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
MADEPV
Aliphatic (C05-CO8)
Aliphatic (C09-C12)
Aromatic (C09-C10),Unadjusted
Surrogates
2,5-Dibromotoluene (FID)
Date: 06/18/2020 07:33 AM
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
ND mg/kg
11.5
1
06/11/2011:22
06/15/2011:53
ND mg/kg
11.5
1
06/11/2011:22
06/15/2011:53
ND mg/kg
11.5
1
06/11/2011:22
06/15/2011:53
60 %
40-140
1
06/11/2011:22
06/15/2011:53
7194-86-7
77 %
40-140
1
06/11/2011:22
06/15/2011:53
84-15-1
109 %
40-140
1
06/11/2011:22
06/15/2011:53
321-60-8
77 %
40-140
1
06/11/2011:22
06/15/2011:53
580-13-2
Analytical Method: MADEP VPH Preparation
Method:
MADEPV
Pace National - Mt. Juliet
ND mg/kg
5.68
1
06/08/20 10:20
06/16/20 01:13
ND mg/kg
5.68
1
06/08/20 10:20
06/16/20 01:13
ND mg/kg
5.68
1
06/08/20 10:20
06/16/20 01:13
TPHC9C10A
N2
N2
N2
106 % 70.0-130 1 06/08/20 10:20 06/16/20 01:13 615-59-8FID
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 8 of 48

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-2
Lab ID: 92480851003
Collected: 06/08/20
10:20
Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
MADEPV
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National
- Mt. Juliet
Surrogates
2,5-Dibromotoluene (PID)
88.2
%
70.0-130
1
06/08/20 10:20
06/16/20 01:13
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Pace Analytical
Services -
Charlotte
Acenaphthene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
83-32-9
Acenaphthylene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
208-96-8
Aniline
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
62-53-3
Anthracene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
207-08-9
Benzoic Acid
ND
mg/kg
1.9
1
06/09/20 21:16
06/11/20 11:49
65-85-0
Benzyl alcohol
ND
mg/kg
0.77
1
06/09/20 21:16
06/11/20 11:49
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
85-68-7
4-ChIoro-3-methyl phenol
ND
mg/kg
0.77
1
06/09/20 21:16
06/11/20 11:49
59-50-7
4-Chloroaniline
ND
mg/kg
0.77
1
06/09/20 21:16
06/11/20 11:49
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
91-58-7
2-Chlorophenol
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
7005-72-3
Chrysene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
53-70-3
Dibenzofuran
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.77
1
06/09/20 21:16
06/11/20 11:49
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
120-83-2
Diethylphthalate
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
105-67-9
Dimethylphthalate
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.77
1
06/09/20 21:16
06/11/20 11:49
534-52-1
2,4-Dinitrophenol
ND
mg/kg
1.9
1
06/09/20 21:16
06/11/20 11:49
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
606-20-2 L2,v2
Di-n-octylphthalate
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
117-84-0 v1
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
117-81-7
Fluoranthene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
206-44-0
Fluorene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
86-73-7
REPORT OF LABORATORY ANALYSIS
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Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-2 Lab ID: 92480851003 Collected: 06/08/20 10:20 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Hexachloro-1,3-butadiene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
87-68-3
Hexachlorobenzene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
77-47-4
Hexachloroethane
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
193-39-5
Isophorone
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
15831-10-4
Naphthalene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
91-20-3
2-Nitroaniline
ND
mg/kg
1.9
1
06/09/20 21:16
06/11/20 11:49
88-74-4
3-Nitroaniline
ND
mg/kg
1.9
1
06/09/20 21:16
06/11/20 11:49
99-09-2
4-Nitroaniline
ND
mg/kg
0.77
1
06/09/20 21:16
06/11/20 11:49
100-01-6
Nitrobenzene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
98-95-3
2-Nitrophenol
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
88-75-5
4-Nitrophenol
ND
mg/kg
1.9
1
06/09/20 21:16
06/11/20 11:49
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
108-60-1
Pentachlorophenol
ND
mg/kg
0.77
1
06/09/20 21:16
06/11/20 11:49
87-86-5
Phenanthrene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
85-01-8
Phenol
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
108-95-2
Pyrene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
129-00-0
Pyridine
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 11:49
88-06-2
Surrogates
Nitrobenzene-d5 (S)
63
%
23-110
1
06/09/20 21:16
06/11/20 11:49
4165-60-0
2-Fluorobiphenyl (S)
61
%
30-110
1
06/09/20 21:16
06/11/20 11:49
321-60-8
Terphenyl-d14 (S)
75
%
28-110
1
06/09/20 21:16
06/11/20 11:49
1718-51-0
Phenol-d6 (S)
64
%
22-110
1
06/09/20 21:16
06/11/20 11:49
13127-88-3
2-Fluorophenol (S)
64
%
13-110
1
06/09/20 21:16
06/11/20 11:49
367-12-4
2,4,6-Tribromophenol (S)
62
%
27-110
1
06/09/20 21:16
06/11/20 11:49
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.074
1
06/10/2015:16
06/10/2018:05
67-64-1
Benzene
ND
mg/kg
0.0037
1
06/10/2015:16
06/10/2018:05
71-43-2
Bromobenzene
ND
mg/kg
0.0037
1
06/10/2015:16
06/10/2018:05
108-86-1
Bromochloromethane
ND
mg/kg
0.0037
1
06/10/2015:16
06/10/2018:05
74-97-5
Bromodichloromethane
ND
mg/kg
0.0037
1
06/10/2015:16
06/10/2018:05
75-27-4
Bromoform
ND
mg/kg
0.0037
1
06/10/2015:16
06/10/2018:05
75-25-2
REPORT OF LABORATORY ANALYSIS
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Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-2 Lab ID: 92480851003 Collected: 06/08/20 10:20 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Bromomethane
ND
mg/kg
0.0074
1
06/10/20 15:16
06/10/20 18:05
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.074
1
06/10/20 15:16
06/10/20 18:05
78-93-3
n-Butylbenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
56-23-5
Chlorobenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
108-90-7
Chloroethane
ND
mg/kg
0.0074
1
06/10/20 15:16
06/10/20 18:05
75-00-3
Chloroform
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
67-66-3
Chloromethane
ND
mg/kg
0.0074
1
06/10/20 15:16
06/10/20 18:05
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
96-12-8
Dibromochloromethane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
106-93-4
Dibromomethane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.0074
1
06/10/20 15:16
06/10/20 18:05
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
108-20-3
Ethylbenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
87-68-3
2-Hexanone
ND
mg/kg
0.037
1
06/10/20 15:16
06/10/20 18:05
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
99-87-6
Methylene Chloride
ND
mg/kg
0.015
1
06/10/20 15:16
06/10/20 18:05
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.037
1
06/10/20 15:16
06/10/20 18:05
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
1634-04-4
Naphthalene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
91-20-3
n-Propylbenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
103-65-1
Styrene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
79-34-5
REPORT OF LABORATORY ANALYSIS
IK
v2
Qual
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-2 Lab ID: 92480851003 Collected: 06/08/20 10:20 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Tetrachloroethene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
127-18-4
Toluene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
79-00-5
Trichloroethene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
96-18-4
1,2,4-Trimethylbenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
108-67-8
Vinyl acetate
ND
mg/kg
0.037
1
06/10/20 15:16
06/10/20 18:05
108-05-4
Vinyl chloride
ND
mg/kg
0.0074
1
06/10/20 15:16
06/10/20 18:05
75-01-4
Xylene (Total)
ND
mg/kg
0.0074
1
06/10/20 15:16
06/10/20 18:05
1330-20-7
m&p-Xylene
ND
mg/kg
0.0074
1
06/10/20 15:16
06/10/20 18:05
179601-23-1
o-Xylene
ND
mg/kg
0.0037
1
06/10/20 15:16
06/10/20 18:05
95-47-6
Surrogates
Toluene-d8 (S)
95
%
70-130
1
06/10/20 15:16
06/10/20 18:05
2037-26-5
4-Bromofluorobenzene (S)
98
%
70-130
1
06/10/20 15:16
06/10/20 18:05
460-00-4
1,2-Dichloroethane-d4 (S)
78
%
70-132
1
06/10/20 15:16
06/10/20 18:05
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical
Services - Charlotte
Percent Moisture
12.3
%
0.10
1
06/09/20 13:33
Total Solids 2540 G-2011
Analytical Method:
SM 2540G Preparation
Method: SM 2540 G
Pace National
- Mt. Juliet
Total Solids
88.0
%
1
06/16/20 13:10
06/16/20 13:18
Sample: SW-3 Lab ID: 92480851004 Collected: 06/08/20 10:45 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
ND
mg/kg
13.2
1
06/15/20 12:52
06/16/20 20:29
ND
mg/kg
13.2
1
06/15/20 12:52
06/16/20 20:29
ND
mg/kg
13.2
1
06/15/20 12:52
06/16/20 20:29
56
%
40-140
1
06/15/20 12:52
06/16/20 20:29
7194-86-7
71
%
40-140
1
06/15/20 12:52
06/16/20 20:29
84-15-1
90
%
40-140
1
06/15/20 12:52
06/16/20 20:29
321-60-8
89
%
40-140
1
06/15/20 12:52
06/16/20 20:29
580-13-2
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-3
Lab ID: 92480851004
Collected: 06/08/20
10:45
Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
MADEPV
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National
- Mt. Juliet
Aliphatic (C05-CO8)
ND
mg/kg
6.15
1
06/08/20 10:45
06/16/20 01:46
Aliphatic (C09-C12)
ND
mg/kg
6.15
1
06/08/20 10:45
06/16/20 01:46
Aromatic (C09-C10),Unadjusted
ND
mg/kg
6.15
1
06/08/20 10:45
06/16/20 01:46
TPHC9C10A
Surrogates
2,5-Dibromotoluene (FID)
107
%
70.0-130
1
06/08/20 10:45
06/16/20 01:46
615-59-8FID
2,5-Dibromotoluene (PID)
89.0
%
70.0-130
1
06/08/20 10:45
06/16/20 01:46
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Pace Analytical
Services -
Charlotte
Acenaphthene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
83-32-9
Acenaphthylene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
208-96-8
Aniline
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
62-53-3
Anthracene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
207-08-9
Benzoic Acid
ND
mg/kg
2.2
1
06/09/20 21:16
06/11/20 12:20
65-85-0
Benzyl alcohol
ND
mg/kg
0.86
1
06/09/20 21:16
06/11/20 12:20
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
85-68-7
4-ChIoro-3-methyl phenol
ND
mg/kg
0.86
1
06/09/20 21:16
06/11/20 12:20
59-50-7
4-Chloroaniline
ND
mg/kg
0.86
1
06/09/20 21:16
06/11/20 12:20
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
91-58-7
2-Chlorophenol
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
7005-72-3
Chrysene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
53-70-3
Dibenzofuran
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.86
1
06/09/20 21:16
06/11/20 12:20
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
120-83-2
Diethylphthalate
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
105-67-9
Dimethylphthalate
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.86
1
06/09/20 21:16
06/11/20 12:20
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.2
1
06/09/20 21:16
06/11/20 12:20
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
606-20-2 L2,v2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-3 Lab ID: 92480851004 Collected: 06/08/20 10:45 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
Di-n-octylphthalate
bis(2- Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
117-84-0
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
117-81-7
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
206-44-0
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
86-73-7
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
87-68-3
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
118-74-1
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
77-47-4
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
67-72-1
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
193-39-5
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
78-59-1
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
90-12-0
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
91-57-6
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
95-48-7
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
15831-10-4
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
91-20-3
ND
mg/kg
2.2
1
06/09/20 21:16
06/11/20 12:20
88-74-4
ND
mg/kg
2.2
1
06/09/20 21:16
06/11/20 12:20
99-09-2
ND
mg/kg
0.86
1
06/09/20 21:16
06/11/20 12:20
100-01-6
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
98-95-3
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
88-75-5
ND
mg/kg
2.2
1
06/09/20 21:16
06/11/20 12:20
100-02-7
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
62-75-9
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
621-64-7
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
86-30-6
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
108-60-1
ND
mg/kg
0.86
1
06/09/20 21:16
06/11/20 12:20
87-86-5
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
85-01-8
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
108-95-2
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
129-00-0
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
110-86-1
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
120-82-1
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
95-95-4
ND
mg/kg
0.43
1
06/09/20 21:16
06/11/20 12:20
88-06-2
67
%
23-110
1
06/09/20 21:16
06/11/20 12:20
4165-60-0
66
%
30-110
1
06/09/20 21:16
06/11/20 12:20
321-60-8
77
%
28-110
1
06/09/20 21:16
06/11/20 12:20
1718-51-0
69
%
22-110
1
06/09/20 21:16
06/11/20 12:20
13127-88-3
70
%
13-110
1
06/09/20 21:16
06/11/20 12:20
367-12-4
68
%
27-110
1
06/09/20 21:16
06/11/20 12:20
118-79-6
8260D/5035A/5030B Volatiles Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone ND mg/kg 0.11 1 06/10/2015:16 06/10/2018:24 67-64-1
Benzene ND mg/kg 0.0054 1 06/10/2015:16 06/10/2018:24 71-43-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC.
v1
Page 14 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-3 Lab ID: 92480851004 Collected: 06/08/20 10:45 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Bromobenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
108-86-1
Bromochloromethane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
74-97-5
Bromodichloromethane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
75-27-4
Bromoform
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
75-25-2
Bromomethane
ND
mg/kg
0.011
1
06/10/20 15:16
06/10/20 18:24
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.11
1
06/10/20 15:16
06/10/20 18:24
78-93-3
n-Butylbenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
56-23-5
Chlorobenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
108-90-7
Chloroethane
ND
mg/kg
0.011
1
06/10/20 15:16
06/10/20 18:24
75-00-3
Chloroform
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
67-66-3
Chloromethane
ND
mg/kg
0.011
1
06/10/20 15:16
06/10/20 18:24
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
96-12-8
Dibromochloromethane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
106-93-4
Dibromomethane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.011
1
06/10/20 15:16
06/10/20 18:24
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
108-20-3
Ethylbenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
87-68-3
2-Hexanone
ND
mg/kg
0.054
1
06/10/20 15:16
06/10/20 18:24
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
99-87-6
Methylene Chloride
ND
mg/kg
0.022
1
06/10/20 15:16
06/10/20 18:24
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.054
1
06/10/20 15:16
06/10/20 18:24
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
1634-04-4
Naphthalene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
91-20-3
REPORT OF LABORATORY ANALYSIS
IK
v2
Qual
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-3 Lab ID: 92480851004 Collected: 06/08/20 10:45 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
n-Propylbenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
103-65-1
Styrene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
79-34-5
Tetrachloroethene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
127-18-4
Toluene
0.0068
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
79-00-5
Trichloroethene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
96-18-4
1,2,4-Trimethylbenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
108-67-8
Vinyl acetate
ND
mg/kg
0.054
1
06/10/20 15:16
06/10/20 18:24
108-05-4
Vinyl chloride
ND
mg/kg
0.011
1
06/10/20 15:16
06/10/20 18:24
75-01-4
Xylene (Total)
ND
mg/kg
0.011
1
06/10/20 15:16
06/10/20 18:24
1330-20-7
m&p-Xylene
ND
mg/kg
0.011
1
06/10/20 15:16
06/10/20 18:24
179601-23-1
o-Xylene
ND
mg/kg
0.0054
1
06/10/20 15:16
06/10/20 18:24
95-47-6
Surrogates
Toluene-d8 (S)
95
%
70-130
1
06/10/20 15:16
06/10/20 18:24
2037-26-5
4-Bromofluorobenzene (S)
99
%
70-130
1
06/10/20 15:16
06/10/20 18:24
460-00-4
1,2-Dichloroethane-d4 (S)
81
%
70-132
1
06/10/20 15:16
06/10/20 18:24
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical
Services - Charlotte
Percent Moisture
24.6
%
0.10
1
06/09/20 13:33
Total Solids 2540 G-2011
Analytical Method:
SM 2540G Preparation
Method: SM 2540 G
Pace National
- Mt. Juliet
Total Solids
81.3
%
1
06/16/20 13:10
06/16/20 13:18
Sample: SW-4 Lab ID: 92480851005 Collected: 06/08/20 11:30 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
Aliphatic (C09-C18) ND mg/kg 11.5 1 06/11/20 11:22 06/15/20 12:48 N2
Aliphatic (C19-C36) ND mg/kg 11.5 1 06/11/20 11:22 06/15/20 12:48 N2
Aromatic (C11-C22) ND mg/kg 11.5 1 06/11/20 11:22 06/15/20 12:48 N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-4 Lab ID: 92480851005 Collected: 06/08/20 11:30 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
Surrogates
Nonatriacontane (S)
63
%
40-140
1
06/11/20 11:22
06/15/20 12:48
7194-86-7
o-Terphenyl (S)
77
%
40-140
1
06/11/20 11:22
06/15/20 12:48
84-15-1
2-Fluorobiphenyl (S)
107
%
40-140
1
06/11/20 11:22
06/15/20 12:48
321-60-8
2-Bromonaphthalene (S)
94
%
40-140
1
06/11/20 11:22
06/15/20 12:48
580-13-2
MADEPV
Analytical Method: MADEP VPH Preparation Method:
MADEPV
Pace National
- Mt. Juliet
Aliphatic (C05-CO8)
ND
mg/kg
5.95
1
06/08/20 11:30
06/16/20 02:19
Aliphatic (C09-C12)
ND
mg/kg
5.95
1
06/08/20 11:30
06/16/20 02:19
Aromatic (C09-C10),Unadjusted
ND
mg/kg
5.95
1
06/08/20 11:30
06/16/20 02:19
TPHC9C10A
Surrogates
2,5-Dibromotoluene (FID)
103
%
70.0-130
1
06/08/20 11:30
06/16/20 02:19
615-59-8FID
2,5-Dibromotoluene (PID)
85.8
%
70.0-130
1
06/08/20 11:30
06/16/20 02:19
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Acenaphthene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
83-32-9
Acenaphthylene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
208-96-8
Aniline
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
62-53-3
Anthracene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
207-08-9
Benzoic Acid
ND
mg/kg
1.9
1
06/09/20 21:16
06/11/20 12:51
65-85-0
Benzyl alcohol
ND
mg/kg
0.76
1
06/09/20 21:16
06/11/20 12:51
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.76
1
06/09/20 21:16
06/11/20 12:51
59-50-7
4-Chloroaniline
ND
mg/kg
0.76
1
06/09/20 21:16
06/11/20 12:51
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
91-58-7
2-Chlorophenol
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
7005-72-3
Chrysene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
53-70-3
Dibenzofuran
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.76
1
06/09/20 21:16
06/11/20 12:51
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
120-83-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-4 Lab ID: 92480851005 Collected: 06/08/20 11:30 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8270E MSSV Microwave
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methyl phenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2- Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
84-66-2
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
105-67-9
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
131-11-3
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
84-74-2
ND
mg/kg
0.76
1
06/09/20 21:16
06/11/20 12:51
534-52-1
ND
mg/kg
1.9
1
06/09/20 21:16
06/11/20 12:51
51-28-5
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
121-14-2
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
606-20-2
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
117-84-0
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
117-81-7
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
206-44-0
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
86-73-7
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
87-68-3
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
118-74-1
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
77-47-4
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
67-72-1
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
193-39-5
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
78-59-1
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
90-12-0
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
91-57-6
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
95-48-7
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
15831-10-4
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
91-20-3
ND
mg/kg
1.9
1
06/09/20 21:16
06/11/20 12:51
88-74-4
ND
mg/kg
1.9
1
06/09/20 21:16
06/11/20 12:51
99-09-2
ND
mg/kg
0.76
1
06/09/20 21:16
06/11/20 12:51
100-01-6
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
98-95-3
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
88-75-5
ND
mg/kg
1.9
1
06/09/20 21:16
06/11/20 12:51
100-02-7
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
62-75-9
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
621-64-7
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
86-30-6
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
108-60-1
ND
mg/kg
0.76
1
06/09/20 21:16
06/11/20 12:51
87-86-5
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
85-01-8
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
108-95-2
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
129-00-0
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
110-86-1
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
120-82-1
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
95-95-4
ND
mg/kg
0.38
1
06/09/20 21:16
06/11/20 12:51
88-06-2
71
%
23-110
1
06/09/20 21:16
06/11/20 12:51
4165-60-0
69
%
30-110
1
06/09/20 21:16
06/11/20 12:51
321-60-8
79
%
28-110
1
06/09/20 21:16
06/11/20 12:51
1718-51-0
REPORT OF LABORATORY ANALYSIS
L2,v2
v1
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-4 Lab ID: 92480851005 Collected: 06/08/20 11:30 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Phenol-d6 (S)
72
%
22-110
1
06/09/20 21:16
06/11/20 12:51
13127-88-3
2-Fluorophenol (S)
71
%
13-110
1
06/09/20 21:16
06/11/20 12:51
367-12-4
2,4,6-Tribromophenol (S)
69
%
27-110
1
06/09/20 21:16
06/11/20 12:51
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.080
1
06/10/20 15:16
06/10/20 18:42
67-64-1
Benzene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
71-43-2
Bromobenzene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
108-86-1
Bromochloromethane
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
74-97-5
Bromodichloromethane
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
75-27-4
Bromoform
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
75-25-2
Bromomethane
ND
mg/kg
0.0080
1
06/10/20 15:16
06/10/20 18:42
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.080
1
06/10/20 15:16
06/10/20 18:42
78-93-3
n-Butylbenzene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
56-23-5
Chlorobenzene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
108-90-7
Chloroethane
ND
mg/kg
0.0080
1
06/10/20 15:16
06/10/20 18:42
75-00-3
Chloroform
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
67-66-3
Chloromethane
ND
mg/kg
0.0080
1
06/10/20 15:16
06/10/20 18:42
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
96-12-8
Dibromochloromethane
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
106-93-4
Dibromomethane
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.0080
1
06/10/20 15:16
06/10/20 18:42
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0040
1
06/10/20 15:16
06/10/20 18:42
108-20-3
REPORT OF LABORATORY ANALYSIS
IK
v2
Qual
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: SW-4 Lab ID: 92480851005 Collected: 06/08/20 11:30 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
100-41-4
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
87-68-3
ND
mg/kg
0.040
1
06/10/2015:16
06/10/2018:42
591-78-6
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
98-82-8
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
99-87-6
ND
mg/kg
0.016
1
06/10/2015:16
06/10/2018:42
75-09-2
ND
mg/kg
0.040
1
06/10/2015:16
06/10/2018:42
108-10-1
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
1634-04-4
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
91-20-3
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
103-65-1
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
100-42-5
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
630-20-6
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
79-34-5
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
127-18-4
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
108-88-3
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
87-61-6
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
120-82-1
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
71-55-6
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
79-00-5
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
79-01-6
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
75-69-4
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
96-18-4
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
95-63-6
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
108-67-8
ND
mg/kg
0.040
1
06/10/2015:16
06/10/2018:42
108-05-4
ND
mg/kg
0.0080
1
06/10/2015:16
06/10/2018:42
75-01-4
ND
mg/kg
0.0080
1
06/10/2015:16
06/10/2018:42
1330-20-7
ND
mg/kg
0.0080
1
06/10/2015:16
06/10/2018:42
179601-23-1
ND
mg/kg
0.0040
1
06/10/2015:16
06/10/2018:42
95-47-6
94
%
70-130
1
06/10/2015:16
06/10/2018:42
2037-26-5
99
%
70-130
1
06/10/2015:16
06/10/2018:42
460-00-4
79
%
70-132
1
06/10/2015:16
06/10/2018:42
17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 14.4 % 0.10 1 06/09/20 13:33
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 84.0 % 1 06/16/20 13:10 06/16/20 13:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: B-1 Lab ID: 92480851006 Collected: 06/08/20 09:55 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
MADEPV
Aliphatic (C05-CO8)
Aliphatic (C09-C12)
Aromatic (C09-C10),Unadjusted
Surrogates
2,5-Dibromotoluene (FID)
2,5-Dibromotoluene (PID)
8270E MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
ND
mg/kg
11.1
1
06/11/2011:22
06/15/2013:15
ND
mg/kg
11.1
1
06/11/2011:22
06/15/2013:15
ND
mg/kg
11.1
1
06/11/2011:22
06/15/2013:15
60
%
40-140
1
06/11/2011:22
06/15/2013:15
7194-86-7
81
%
40-140
1
06/11/2011:22
06/15/2013:15
84-15-1
114
%
40-140
1
06/11/2011:22
06/15/2013:15
321-60-8
119
%
40-140
1
06/11/2011:22
06/15/2013:15
580-13-2
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
ND
mg/kg
5.44
1
06/08/20 09:55
06/16/20 02:52
ND
mg/kg
5.44
1
06/08/20 09:55
06/16/20 02:52
ND
mg/kg
5.44
1
06/08/20 09:55
06/16/20 02:52
TPHC9C10A
108
%
70.0-130
1
06/08/20 09:55
06/16/20 02:52
615-59-8FID
89.2
%
70.0-130
1
06/08/20 09:55
06/16/20 02:52
615-59-8PID
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
83-32-9
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
208-96-8
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
62-53-3
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
120-12-7
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
56-55-3
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
50-32-8
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
205-99-2
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
191-24-2
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
207-08-9
ND
mg/kg
1.8
1
06/09/20 21:16
06/11/20 13:22
65-85-0
ND
mg/kg
0.73
1
06/09/20 21:16
06/11/20 13:22
100-51-6
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
101-55-3
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
85-68-7
ND
mg/kg
0.73
1
06/09/20 21:16
06/11/20 13:22
59-50-7
ND
mg/kg
0.73
1
06/09/20 21:16
06/11/20 13:22
106-47-8
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
111-91-1
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
111-44-4
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
91-58-7
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
95-57-8
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
7005-72-3
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
218-01-9
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
53-70-3
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
132-64-9
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
95-50-1
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
541-73-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: B-1 Lab ID: 92480851006 Collected: 06/08/20 09:55 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,4-Dichlorobenzene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
0.73
1
06/09/20 21:16
06/11/20 13:22
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
120-83-2
Diethylphthalate
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
105-67-9
Dimethylphthalate
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.73
1
06/09/20 21:16
06/11/20 13:22
534-52-1
2,4-Dinitrophenol
ND
mg/kg
1.8
1
06/09/20 21:16
06/11/20 13:22
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
117-81-7
Fluoranthene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
206-44-0
Fluorene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
87-68-3
Hexachlorobenzene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
77-47-4
Hexachloroethane
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
193-39-5
Isophorone
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
15831-10-4
Naphthalene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
91-20-3
2-Nitroaniline
ND
mg/kg
1.8
1
06/09/20 21:16
06/11/20 13:22
88-74-4
3-Nitroaniline
ND
mg/kg
1.8
1
06/09/20 21:16
06/11/20 13:22
99-09-2
4-Nitroaniline
ND
mg/kg
0.73
1
06/09/20 21:16
06/11/20 13:22
100-01-6
Nitrobenzene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
98-95-3
2-Nitrophenol
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
88-75-5
4-Nitrophenol
ND
mg/kg
1.8
1
06/09/20 21:16
06/11/20 13:22
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
108-60-1
Pentachlorophenol
ND
mg/kg
0.73
1
06/09/20 21:16
06/11/20 13:22
87-86-5
Phenanthrene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
85-01-8
Phenol
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
108-95-2
Pyrene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
129-00-0
Pyridine
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.37
1
06/09/20 21:16
06/11/20 13:22
88-06-2
REPORT OF LABORATORY ANALYSIS
Qual
L2,v2
v1
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: B-1 Lab ID: 92480851006 Collected: 06/08/20 09:55 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
71
%
23-110
1
06/09/20 21:16
06/11/20 13:22
4165-60-0
2-Fluorobiphenyl (S)
71
%
30-110
1
06/09/20 21:16
06/11/20 13:22
321-60-8
Terphenyl-d14 (S)
82
%
28-110
1
06/09/20 21:16
06/11/20 13:22
1718-51-0
Phenol-d6 (S)
71
%
22-110
1
06/09/20 21:16
06/11/20 13:22
13127-88-3
2-Fluorophenol (S)
71
%
13-110
1
06/09/20 21:16
06/11/20 13:22
367-12-4
2,4,6-Tribromophenol (S)
69
%
27-110
1
06/09/20 21:16
06/11/20 13:22
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
mg/kg
0.083
1
06/10/20 15:16
06/10/20 19:00
67-64-1
Benzene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
71-43-2
Bromobenzene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
108-86-1
Bromochloromethane
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
74-97-5
Bromodichloromethane
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
75-27-4
Bromoform
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
75-25-2
Bromomethane
ND
mg/kg
0.0083
1
06/10/20 15:16
06/10/20 19:00
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.083
1
06/10/20 15:16
06/10/20 19:00
78-93-3
n-Butylbenzene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
56-23-5
Chlorobenzene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
108-90-7
Chloroethane
ND
mg/kg
0.0083
1
06/10/20 15:16
06/10/20 19:00
75-00-3
Chloroform
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
67-66-3
Chloromethane
ND
mg/kg
0.0083
1
06/10/20 15:16
06/10/20 19:00
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
96-12-8
Dibromochloromethane
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
106-93-4
Dibromomethane
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.0083
1
06/10/20 15:16
06/10/20 19:00
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0041
1
06/10/20 15:16
06/10/20 19:00
563-58-6
REPORT OF LABORATORY ANALYSIS
IK
v2
Qual
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johnson Oehler
Pace Project No.: 92480851
Sample: B-1 Lab ID: 92480851006 Collected: 06/08/20 09:55 Received: 06/08/20 14:43 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
10061-01-5
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
10061-02-6
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
108-20-3
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
100-41-4
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
87-68-3
ND
mg/kg
0.041
1
06/10/2015:16
06/10/2019:00
591-78-6
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
98-82-8
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
99-87-6
ND
mg/kg
0.017
1
06/10/2015:16
06/10/2019:00
75-09-2
ND
mg/kg
0.041
1
06/10/2015:16
06/10/2019:00
108-10-1
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
1634-04-4
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
91-20-3
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
103-65-1
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
100-42-5
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
630-20-6
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
79-34-5
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
127-18-4
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
108-88-3
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
87-61-6
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
120-82-1
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
71-55-6
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
79-00-5
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
79-01-6
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
75-69-4
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
96-18-4
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
95-63-6
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
108-67-8
ND
mg/kg
0.041
1
06/10/2015:16
06/10/2019:00
108-05-4
ND
mg/kg
0.0083
1
06/10/2015:16
06/10/2019:00
75-01-4
ND
mg/kg
0.0083
1
06/10/2015:16
06/10/2019:00
1330-20-7
ND
mg/kg
0.0083
1
06/10/2015:16
06/10/2019:00
179601-23-1
ND
mg/kg
0.0041
1
06/10/2015:16
06/10/2019:00
95-47-6
94
%
70-130
1
06/10/2015:16
06/10/2019:00
2037-26-5
100
%
70-130
1
06/10/2015:16
06/10/2019:00
460-00-4
77
%
70-132
1
06/10/2015:16
06/10/2019:00
17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 9.8 % 0.10 1 06/09/20 13:33
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 92.0 % 1 06/16/20 13:10 06/16/20 13:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 24 of 48

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
QC Batch: 1493015
Analysis Method: MADEP VPH
QC Batch Method: MADEPV
Analysis Description: MADEPV
Laboratory: Pace National - Mt.
Juliet
Associated Lab Samples: 92480851002, 92480851003,
92480851004, 92480851005, 92480851006
METHOD BLANK: R3539239-2
Matrix: Solid
Associated Lab Samples: 92480851002, 92480851003,
92480851004, 92480851005, 92480851006
Blank Reporting
Parameter
Units
Result Limit Analyzed
Qualifiers
Aliphatic (C05-CO8)
mg/kg
ND 5.00 06/15/20 14:24
Aliphatic (C09-C12)
mg/kg
ND 5.00 06/15/20 14:24
Aromatic (C09-C10),Unadjusted
mg/kg
ND 5.00 06/15/20 14:24
2,5-Dibromotoluene (FID)
%
97.4 70.0-130 06/15/20 14:24
2,5-Dibromotoluene (PID)
%
81.7 70.0-130 06/15/20 14:24
LABORATORY CONTROL SAMPLE & LCSD:
R3539239-1 R3539239-3
Spike LCS LCSD LCS LCSD
% Rec Max
Parameter
Units
Conc. Result Result % Rec % Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
60.0 71.6 70.3 119 117
70.0-130 1.83 25
Aliphatic (C09-C12)
mg/kg
70.0 78.5 76.7 112 110
70.0-130 2.32 25
Aromatic (C09-C10),Unadjusted
mg/kg
10.0 9.17 8.87 91.7 88.7
70.0-130 3.33 25
2,5-Dibromotoluene (FID)
%
109 98.7
70.0-130
2,5-Dibromotoluene (PID)
%
92.6 79.7
70.0-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
QC Batch: 546048
Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E
Analysis Description: Gasoline Range Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92480851001
METHOD BLANK: 2906852
Matrix: Solid
Associated Lab Samples: 92480851001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 6.0 06/09/20 12:21
4-Bromofluorobenzene (S)
%
102 63-130 06/09/20 12:21
LABORATORY CONTROL SAMPLE:
2906853
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
50 50.2 100 70-130
4-Bromofluorobenzene (S)
%
97 63-130
MATRIX SPIKE SAMPLE:
2906855
92480641001 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
60.7 48 102 87
40-155
4-Bromofluorobenzene (S)
%
287
63-130 S2
SAMPLE DUPLICATE: 2906863
92480857001 Dup
Parameter
Units
Result Result RPD Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 4.3J
4-Bromofluorobenzene (S)
%
101 99
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
QC Batch: 546439 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92480851002, 92480851003, 92480851004, 92480851005, 92480851006
METHOD BLANK: 2908629 Matrix: Solid
Associated Lab Samples: 92480851002, 92480851003, 92480851004, 92480851005, 92480851006
Blank Reporting
Parameter Units Result Limit Analyzed
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0050
06/10/20 14:45
1,1,1-Trichloroethane
mg/kg
ND
0.0050
06/10/20 14:45
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0050
06/10/20 14:45
1,1,2-Trichloroethane
mg/kg
ND
0.0050
06/10/20 14:45
1,1-Dichloroethane
mg/kg
ND
0.0050
06/10/20 14:45
1,1-Dichloroethene
mg/kg
ND
0.0050
06/10/20 14:45
1,1-Dichloropropene
mg/kg
ND
0.0050
06/10/20 14:45
1,2,3-Trichlorobenzene
mg/kg
ND
0.0050
06/10/20 14:45
1,2,3-Trichloropropane
mg/kg
ND
0.0050
06/10/20 14:45
1,2,4-Trichlorobenzene
mg/kg
ND
0.0050
06/10/20 14:45
1,2,4-Trimethylbenzene
mg/kg
ND
0.0050
06/10/20 14:45
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0050
06/10/20 14:45
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0050
06/10/20 14:45
1,2-Dichlorobenzene
mg/kg
ND
0.0050
06/10/20 14:45
1,2-Dichloroethane
mg/kg
ND
0.0050
06/10/20 14:45
1,2-Dichloropropane
mg/kg
ND
0.0050
06/10/20 14:45
1,3,5-Trimethylbenzene
mg/kg
ND
0.0050
06/10/20 14:45
1,3-Dichlorobenzene
mg/kg
ND
0.0050
06/10/20 14:45
1,3-Dichloropropane
mg/kg
ND
0.0050
06/10/20 14:45
1,4-Dichlorobenzene
mg/kg
ND
0.0050
06/10/20 14:45
2,2-Dichloropropane
mg/kg
ND
0.0050
06/10/20 14:45
2-Butanone (MEK)
mg/kg
ND
0.10
06/10/20 14:45
2-Chlorotoluene
mg/kg
ND
0.0050
06/10/20 14:45
2-Hexanone
mg/kg
ND
0.050
06/10/20 14:45
4-Chlorotoluene
mg/kg
ND
0.0050
06/10/20 14:45
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.050
06/10/20 14:45
Acetone
mg/kg
ND
0.10
06/10/20 14:45
Benzene
mg/kg
ND
0.0050
06/10/20 14:45
Bromobenzene
mg/kg
ND
0.0050
06/10/20 14:45
Bromochloromethane
mg/kg
ND
0.0050
06/10/20 14:45
Bromodichloromethane
mg/kg
ND
0.0050
06/10/20 14:45
Bromoform
mg/kg
ND
0.0050
06/10/20 14:45
Bromomethane
mg/kg
ND
0.010
06/10/20 14:45
Carbon tetrachloride
mg/kg
ND
0.0050
06/10/20 14:45
Chlorobenzene
mg/kg
ND
0.0050
06/10/20 14:45
Chloroethane
mg/kg
ND
0.010
06/10/20 14:45
Chloroform
mg/kg
ND
0.0050
06/10/20 14:45
Chloromethane
mg/kg
ND
0.010
06/10/20 14:45
cis-1,2-Dichloroethene
mg/kg
ND
0.0050
06/10/20 14:45
cis-1,3-Dichloropropene
mg/kg
ND
0.0050
06/10/20 14:45
IK
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
METHOD BLANK: 2908629 Matrix: Solid
Associated Lab Samples: 92480851002, 92480851003, 92480851004, 92480851005, 92480851006
Blank Reporting
Parameter Units Result Limit Analyzed
Dibromochloromethane
mg/kg
ND
0.0050
06/10/20 14:45
Dibromomethane
mg/kg
ND
0.0050
06/10/20 14:45
Dichlorodifluoromethane
mg/kg
ND
0.010
06/10/20 14:45
Diisopropyl ether
mg/kg
ND
0.0050
06/10/20 14:45
Ethylbenzene
mg/kg
ND
0.0050
06/10/20 14:45
Hexachloro-1,3-butadiene
mg/kg
ND
0.0050
06/10/20 14:45
Isopropylbenzene (Cumene)
mg/kg
ND
0.0050
06/10/20 14:45
m&p-Xylene
mg/kg
ND
0.010
06/10/20 14:45
Methyl-tert-butyl ether
mg/kg
ND
0.0050
06/10/20 14:45
Methylene Chloride
mg/kg
ND
0.020
06/10/20 14:45
n-Butylbenzene
mg/kg
ND
0.0050
06/10/20 14:45
n-Propylbenzene
mg/kg
ND
0.0050
06/10/20 14:45
Naphthalene
mg/kg
ND
0.0050
06/10/20 14:45
o-Xylene
mg/kg
ND
0.0050
06/10/20 14:45
p-Isopropyltoluene
mg/kg
ND
0.0050
06/10/20 14:45
sec-Butylbenzene
mg/kg
ND
0.0050
06/10/20 14:45
Styrene
mg/kg
ND
0.0050
06/10/20 14:45
tert-Butyl benzene
mg/kg
ND
0.0050
06/10/20 14:45
Tetrachloroethene
mg/kg
ND
0.0050
06/10/20 14:45
Toluene
mg/kg
ND
0.0050
06/10/20 14:45
trans-1,2-Dichloroethene
mg/kg
ND
0.0050
06/10/20 14:45
trans- 1,3-Dichloropropene
mg/kg
ND
0.0050
06/10/20 14:45
Trichloroethene
mg/kg
ND
0.0050
06/10/20 14:45
Trichlorofluoromethane
mg/kg
ND
0.0050
06/10/20 14:45
Vinyl acetate
mg/kg
ND
0.050
06/10/20 14:45
Vinyl chloride
mg/kg
ND
0.010
06/10/20 14:45
Xylene (Total)
mg/kg
ND
0.010
06/10/20 14:45
1,2-Dichloroethane-d4 (S)
%
95
70-132
06/10/20 14:45
4-Bromofluorobenzene (S)
%
99
70-130
06/10/20 14:45
Toluene-d8 (S)
%
98
70-130
06/10/20 14:45
Qualifiers
LABORATORY CONTROL SAMPLE:
2908630
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
1.2
1.2
94
70-130
1,1,1-Trichloroethane
mg/kg
1.2
1.1
88
70-130
1,1,2,2-Tetrachloroethane
mg/kg
1.2
1.1
90
55-130
1,1,2-Trichloroethane
mg/kg
1.2
1.1
89
70-130
1,1-Dichloroethane
mg/kg
1.2
1.1
89
68-130
1,1-Dichloroethene
mg/kg
1.2
1.2
93
70-130
1,1-Dichloropropene
mg/kg
1.2
1.1
90
70-130
1,2,3-Trichlorobenzene
mg/kg
1.2
1.3
102
70-130
1,2,3-Trichloropropane
mg/kg
1.2
1.1
89
70-130
1,2,4-Trichlorobenzene
mg/kg
1.2
1.1
90
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
LABORATORY CONTROL SAMPLE:
Parameter
2908630
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trimethylbenzene
mg/kg
1.2
1.1
89
69-130
1,2-Dibromo-3-chloropropane
mg/kg
1.2
1.1
90
57-141
1,2-Dibromoethane (EDB)
mg/kg
1.2
1.2
94
70-130
1,2-Dichlorobenzene
mg/kg
1.2
1.1
88
70-130
1,2-Dichloroethane
mg/kg
1.2
1.2
93
70-130
1,2-Dichloropropane
mg/kg
1.2
1.1
90
70-130
1,3,5-Trimethylbenzene
mg/kg
1.2
1.1
90
70-130
1,3-Dichlorobenzene
mg/kg
1.2
1.1
89
70-130
1,3-Dichloropropane
mg/kg
1.2
1.1
91
70-130
1,4-Dichlorobenzene
mg/kg
1.2
1.1
87
70-130
2,2-Dichloropropane
mg/kg
1.2
1.0
81
70-130
2-Butanone (MEK)
mg/kg
2.5
2.2
87
60-130
2-Chlorotoluene
mg/kg
1.2
1.2
93
70-130
2-Hexanone
mg/kg
2.5
2.3
92
70-132
4-Chlorotoluene
mg/kg
1.2
1.1
90
70-130
4-Methyl-2-pentanone (MIBK)
mg/kg
2.5
2.2
90
69-130
Acetone
mg/kg
2.5
2.2
88
49-148
Benzene
mg/kg
1.2
1.1
89
70-130
Bromobenzene
mg/kg
1.2
1.1
91
70-130
Bromochloromethane
mg/kg
1.2
1.1
91
70-130
Bromodichloromethane
mg/kg
1.2
1.1
88
70-130
Bromoform
mg/kg
1.2
1.2
95
68-136
Bromomethane
mg/kg
1.2
1.4
110
60-140IK
Carbon tetrachloride
mg/kg
1.2
1.2
94
70-130
Chlorobenzene
mg/kg
1.2
1.1
92
70-130
Chloroethane
mg/kg
1.2
1.0
83
51-147
Chloroform
mg/kg
1.2
1.1
87
70-130
Chloromethane
mg/kg
1.2
0.99
79
48-130 v2
cis-1,2-Dichloroethene
mg/kg
1.2
1.1
87
70-130
cis-1,3-Dichloropropene
mg/kg
1.2
1.1
89
70-130
Dibromochloromethane
mg/kg
1.2
1.2
96
70-130
Dibromomethane
mg/kg
1.2
1.2
93
70-130
Dichlorodifluoromethane
mg/kg
1.2
1.1
87
49-130
Diisopropyl ether
mg/kg
1.2
1.1
86
66-130
Ethylbenzene
mg/kg
1.2
1.1
86
70-130
Hexachloro-1,3-butadiene
mg/kg
1.2
1.2
100
70-130
Isopropylbenzene (Cumene)
mg/kg
1.2
1.1
91
70-130
m&p-Xylene
mg/kg
2.5
2.3
91
70-130
Methyl-tert-butyl ether
mg/kg
1.2
1.1
86
70-130
Methylene Chloride
mg/kg
1.2
1.2
96
50-137
n-Butylbenzene
mg/kg
1.2
1.1
90
70-130
n-Propylbenzene
mg/kg
1.2
1.1
87
70-130
Naphthalene
mg/kg
1.2
1.1
90
70-131
o-Xylene
mg/kg
1.2
1.1
91
70-130
p-Isopropyltoluene
mg/kg
1.2
1.1
89
70-130
sec-Butylbenzene
mg/kg
1.2
1.1
89
70-130
Styrene
mg/kg
1.2
1.2
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
LABORATORY CONTROL SAMPLE:
Parameter
2908630
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
tert-Butyl benzene
mg/kg
1.2
1.1
89
69-130
Tetrachloroethene
mg/kg
1.2
1.2
94
56-130
Toluene
mg/kg
1.2
1.1
87
70-130
trans-1,2-Dichloroethene
mg/kg
1.2
1.2
93
70-130
trans- 1,3-Dichloropropene
mg/kg
1.2
1.0
84
70-130
Trichloroethene
mg/kg
1.2
1.2
92
70-141
Trichlorofluoromethane
mg/kg
1.2
1.1
86
67-130
Vinyl acetate
mg/kg
2.5
2.2
87
10-136
Vinyl chloride
mg/kg
1.2
1.1
91
67-130
Xylene (Total)
mg/kg
3.8
3.4
91
70-130
1,2-Dichloroethane-d4 (S)
%
91
70-132
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2908631
MS
92480851002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2908632
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.5
0.47
0.55
0.49
109
105
52-133
12
1,1,1-Trichloroethane
mg/kg
ND
0.5
0.47
0.60
0.53
120
116
49-137
12
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.5
0.47
0.52
0.47
105
102
39-150
11
1,1,2-Trichloroethane
mg/kg
ND
0.5
0.47
0.57
0.50
115
108
48-140
13
1,1-Dichloroethane
mg/kg
ND
0.5
0.47
0.57
0.50
114
107
46-135
14
1,1-Dichloroethene
mg/kg
ND
0.5
0.47
0.62
0.54
123
117
38-149
13
1,1-Dichloropropene
mg/kg
ND
0.5
0.47
0.60
0.54
120
118
41-140
10
1,2,3-Trichlorobenzene
mg/kg
ND
0.5
0.47
0.50
0.47
100
101
10-158
7
1,2,3-Trichloropropane
mg/kg
ND
0.5
0.47
0.51
0.47
102
102
33-157
8
1,2,4-Trichlorobenzene
mg/kg
ND
0.5
0.47
0.51
0.50
103
107
10-155
4
1,2,4-Trimethylbenzene
mg/kg
ND
0.5
0.47
0.53
0.50
105
107
24-154
6
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.5
0.47
0.44
0.44
88
96
33-158
0
1,2-Dibromoethane (EDB)
mg/kg
ND
0.5
0.47
0.53
0.47
106
101
40-136
13
1,2-Dichlorobenzene
mg/kg
ND
0.5
0.47
0.52
0.48
104
105
27-146
7
1,2-Dichloroethane
mg/kg
ND
0.5
0.47
0.53
0.45
106
98
49-140
15
1,2-Dichloropropane
mg/kg
ND
0.5
0.47
0.57
0.50
113
108
44-143
13
1,3,5-Trimethylbenzene
mg/kg
ND
0.5
0.47
0.54
0.51
108
111
40-144
5
1,3-Dichlorobenzene
mg/kg
ND
0.5
0.47
0.52
0.50
105
107
33-140
5
1,3-Dichloropropane
mg/kg
ND
0.5
0.47
0.53
0.47
107
103
47-147
12
1,4-Dichlorobenzene
mg/kg
ND
0.5
0.47
0.50
0.50
100
108
35-139
0
2,2-Dichloropropane
mg/kg
ND
0.5
0.47
0.59
0.51
117
109
41-140
15
2-Butanone (MEK)
mg/kg
ND
1
0.92
0.56
0.56
56
60
10-181
0
2-Chlorotoluene
mg/kg
ND
0.5
0.47
0.55
0.51
109
110
38-147
7
2-Hexanone
mg/kg
ND
1
0.92
0.86
0.85
86
92
18-169
1
4-Chlorotoluene
mg/kg
ND
0.5
0.47
0.54
0.50
108
109
36-145
7
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
1
0.92
1.0
0.97
105
105
16-175
8
Acetone
mg/kg
ND
1
0.92
0.75
0.69
74
73
10-200
8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2908631
MS
92480851002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2908632
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Benzene
mg/kg
ND
0.5
0.47
0.55
0.50
111
108
46-136
11
Bromobenzene
mg/kg
ND
0.5
0.47
0.54
0.51
109
109
38-149
7
Bromochloromethane
mg/kg
ND
0.5
0.47
0.63
0.55
126
118
44-142
14
Bromodichloromethane
mg/kg
ND
0.5
0.47
0.53
0.47
106
101
41-140
12
Bromoform
mg/kg
ND
0.5
0.47
0.51
0.46
103
100
34-145
10
Bromomethane
mg/kg
ND
0.5
0.47
0.57
0.50
113
108
14-162
13
Carbon tetrachloride
mg/kg
ND
0.5
0.47
0.59
0.54
118
117
44-141
8
Chlorobenzene
mg/kg
ND
0.5
0.47
0.54
0.49
108
106
39-141
9
Chloroethane
mg/kg
ND
0.5
0.47
0.12
0.097
24
21
10-182
21
Chloroform
mg/kg
ND
0.5
0.47
0.58
0.51
116
110
45-140
13
Chloromethane
mg/kg
ND
0.5
0.47
0.54
0.48
108
103
19-149
13
cis-1,2-Dichloroethene
mg/kg
ND
0.5
0.47
0.60
0.52
120
112
38-150
14
cis-1,3-Dichloropropene
mg/kg
ND
0.5
0.47
0.53
0.47
107
102
30-144
13
Dibromochloromethane
mg/kg
ND
0.5
0.47
0.54
0.48
108
104
36-145
12
Dibromomethane
mg/kg
ND
0.5
0.47
0.55
0.48
110
104
41-145
14
Dichlorodifluoromethane
mg/kg
ND
0.5
0.47
0.60
0.55
120
119
16-146
9
Diisopropyl ether
mg/kg
ND
0.5
0.47
0.57
0.49
114
105
41-143
16
Ethylbenzene
mg/kg
ND
0.5
0.47
0.50
0.46
100
100
35-144
7
Hexachloro-1,3-butadiene
mg/kg
ND
0.5
0.47
0.60
0.57
119
124
10-160
4
Isopropylbenzene (Cumene)
mg/kg
ND
0.5
0.47
0.54
0.51
107
110
30-152
6
m&p-Xylene
mg/kg
ND
1
0.92
1.0
0.94
100
101
33-145
7
Methyl-tert-butyl ether
mg/kg
ND
0.5
0.47
0.60
0.51
120
111
49-140
16
Methylene Chloride
mg/kg
ND
0.5
0.47
0.59
0.54
117
116
10-174
9
n-Butylbenzene
mg/kg
ND
0.5
0.47
0.52
0.51
104
111
10-160
1
n-Propylbenzene
mg/kg
ND
0.5
0.47
0.53
0.51
106
109
24-159
5
Naphthalene
mg/kg
ND
0.5
0.47
0.49
0.47
98
102
10-171
5
o-Xylene
mg/kg
ND
0.5
0.47
0.54
0.50
109
108
31-150
8
p-Isopropyltoluene
mg/kg
ND
0.5
0.47
0.52
0.51
103
110
21-154
2
sec-Butylbenzene
mg/kg
ND
0.5
0.47
0.54
0.52
107
112
19-159
4
Styrene
mg/kg
ND
0.5
0.47
0.55
0.50
110
109
15-152
8
tert-Butyl benzene
mg/kg
ND
0.5
0.47
0.54
0.51
108
110
31-141
5
Tetrachloroethene
mg/kg
ND
0.5
0.47
0.54
0.52
108
111
19-141
5
Toluene
mg/kg
ND
0.5
0.47
0.59
0.53
117
114
31-146
11
trans-1,2-Dichloroethene
mg/kg
ND
0.5
0.47
0.61
0.53
123
115
28-157
14
trans- 1,3-Dichloropropene
mg/kg
ND
0.5
0.47
0.50
0.44
100
96
25-146
12
Trichloroethene
mg/kg
ND
0.5
0.47
0.59
0.53
117
114
34-149
11
Trichlorofluoromethane
mg/kg
ND
0.5
0.47
0.14
0.11
27
24
10-167
19
Vinyl acetate
mg/kg
ND
1
0.92
1.0
0.89
102
97
10-200
13
Vinyl chloride
mg/kg
ND
0.5
0.47
0.71
0.62
143
133
36-155
15
Xylene (Total)
mg/kg
ND
1.5
1.4
1.5
1.4
103
104
29-148
7
1,2-Dichloroethane-d4 (S)
%
119
113
70-132
4-Bromofluorobenzene (S)
%
98
98
70-130
Toluene-d8(S)
%
101
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 31 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
QC Batch: 546213
Analysis Method:
EPA 8015C Modified
QC Batch Method: EPA 3546
Analysis Description:
8015 Solid GCSV
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92480851001
METHOD BLANK: 2907767
Matrix: Solid
Associated Lab Samples: 92480851001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND
5.0 06/11/20 03:36
n-Pentacosane (S)
%
48 33-129
06/11/20 03:36
LABORATORY CONTROL SAMPLE:
2907768
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
66.9 44.1
66 43-130
n-Pentacosane (S)
%
62 33-129
MATRIX SPIKE SAMPLE:
2907769
92480772001 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
6760 87.1
7560 920
10-130 M1
n-Pentacosane(S)
%
122
33-129
SAMPLE DUPLICATE: 2907770
92480857002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND
ND
n-Pentacosane (S)
%
50
20 SO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
QC Batch: 546176 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92480851002, 92480851003, 92480851004, 92480851005, 92480851006
METHOD BLANK: 2907543 Matrix: Solid
Associated Lab Samples: 92480851002, 92480851003, 92480851004, 92480851005, 92480851006
Blank Reporting
Parameter Units Result Limit Analyzed
1,2,4-Trichlorobenzene
mg/kg
ND
0.33
06/10/20 18:52
1,2-Dichlorobenzene
mg/kg
ND
0.33
06/10/20 18:52
1,3-Dichlorobenzene
mg/kg
ND
0.33
06/10/20 18:52
1,4-Dichlorobenzene
mg/kg
ND
0.33
06/10/20 18:52
1-Methylnaphthalene
mg/kg
ND
0.33
06/10/20 18:52
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
0.33
06/10/20 18:52
2,4,5-Trichlorophenol
mg/kg
ND
0.33
06/10/20 18:52
2,4,6-Trichlorophenol
mg/kg
ND
0.33
06/10/20 18:52
2,4-Dichlorophenol
mg/kg
ND
0.33
06/10/20 18:52
2,4-Dimethylphenol
mg/kg
ND
0.33
06/10/20 18:52
2,4-Dinitrophenol
mg/kg
ND
1.6
06/10/20 18:52
2,4-Dinitrotoluene
mg/kg
ND
0.33
06/10/20 18:52
2,6-Dinitrotoluene
mg/kg
ND
0.33
06/10/20 18:52
2-Chloronaphthalene
mg/kg
ND
0.33
06/10/20 18:52
2-Chlorophenol
mg/kg
ND
0.33
06/10/20 18:52
2-Methylnaphthalene
mg/kg
ND
0.33
06/10/20 18:52
2-Methylphenol(o-Cresol)
mg/kg
ND
0.33
06/10/20 18:52
2-Nitroaniline
mg/kg
ND
1.6
06/10/20 18:52
2-Nitrophenol
mg/kg
ND
0.33
06/10/20 18:52
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
0.33
06/10/20 18:52
3,3'-Dichlorobenzidine
mg/kg
ND
0.65
06/10/20 18:52
3-Nitroaniline
mg/kg
ND
1.6
06/10/20 18:52
4,6-Dinitro-2-methyl phenol
mg/kg
ND
0.65
06/10/20 18:52
4-Bromophenylphenyl ether
mg/kg
ND
0.33
06/10/20 18:52
4-ChIoro-3-methyl phenol
mg/kg
ND
0.65
06/10/20 18:52
4-Chloroaniline
mg/kg
ND
0.65
06/10/20 18:52
4-Chlorophenylphenyl ether
mg/kg
ND
0.33
06/10/20 18:52
4-Nitroaniline
mg/kg
ND
0.65
06/10/20 18:52
4-Nitrophenol
mg/kg
ND
1.6
06/10/20 18:52
Acenaphthene
mg/kg
ND
0.33
06/10/20 18:52
Acenaphthylene
mg/kg
ND
0.33
06/10/20 18:52
Aniline
mg/kg
ND
0.33
06/10/20 18:52
Anthracene
mg/kg
ND
0.33
06/10/20 18:52
Benzo(a)anthracene
mg/kg
ND
0.33
06/10/20 18:52
Benzo(a)pyrene
mg/kg
ND
0.33
06/10/20 18:52
Benzo(b)fluoranthene
mg/kg
ND
0.33
06/10/20 18:52
Benzo(g,h,i)perylene
mg/kg
ND
0.33
06/10/20 18:52
Benzo(k)fluoranthene
mg/kg
ND
0.33
06/10/20 18:52
Benzoic Acid
mg/kg
ND
1.6
06/10/20 18:52
Benzyl alcohol
mg/kg
ND
0.65
06/10/20 18:52
v1
v2
v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
METHOD BLANK: 2907543 Matrix: Solid
Associated Lab Samples: 92480851002, 92480851003, 92480851004, 92480851005, 92480851006
Blank Reporting
Parameter Units Result Limit Analyzed
bis(2-Chloroethoxy)methane
mg/kg
ND
0.33
06/10/20 18:52
bis(2-Chloroethyl) ether
mg/kg
ND
0.33
06/10/20 18:52
bis(2-Ethylhexyl)phthalate
mg/kg
ND
0.33
06/10/20 18:52
Butylbenzylphthalate
mg/kg
ND
0.33
06/10/20 18:52
Chrysene
mg/kg
ND
0.33
06/10/20 18:52
Di-n-butylphthalate
mg/kg
ND
0.33
06/10/20 18:52
Di-n-octylphthalate
mg/kg
ND
0.33
06/10/20 18:52
Dibenz(a,h)anthracene
mg/kg
ND
0.33
06/10/20 18:52
Dibenzofuran
mg/kg
ND
0.33
06/10/20 18:52
Diethylphthalate
mg/kg
ND
0.33
06/10/20 18:52
Dimethylphthalate
mg/kg
ND
0.33
06/10/20 18:52
Fluoranthene
mg/kg
ND
0.33
06/10/20 18:52
Fluorene
mg/kg
ND
0.33
06/10/20 18:52
Hexachloro-1,3-butadiene
mg/kg
ND
0.33
06/10/20 18:52
Hexachlorobenzene
mg/kg
ND
0.33
06/10/20 18:52
Hexachlorocyclopentadiene
mg/kg
ND
0.33
06/10/20 18:52
Hexachloroethane
mg/kg
ND
0.33
06/10/20 18:52
Indeno(1,2,3-cd)pyrene
mg/kg
ND
0.33
06/10/20 18:52
Isophorone
mg/kg
ND
0.33
06/10/20 18:52
N-Nitroso-di-n-propylamine
mg/kg
ND
0.33
06/10/20 18:52
N-Nitrosodimethylamine
mg/kg
ND
0.33
06/10/20 18:52
N-Nitrosodiphenylamine
mg/kg
ND
0.33
06/10/20 18:52
Naphthalene
mg/kg
ND
0.33
06/10/20 18:52
Nitrobenzene
mg/kg
ND
0.33
06/10/20 18:52
Pentachlorophenol
mg/kg
ND
0.65
06/10/20 18:52
Phenanthrene
mg/kg
ND
0.33
06/10/20 18:52
Phenol
mg/kg
ND
0.33
06/10/20 18:52
Pyrene
mg/kg
ND
0.33
06/10/20 18:52
Pyridine
mg/kg
ND
0.33
06/10/20 18:52
2,4,6-Tribromophenol (S)
%
74
27-110
06/10/20 18:52
2-Fluorobiphenyl (S)
%
72
30-110
06/10/20 18:52
2-Fluorophenol(S)
%
75
13-110
06/10/20 18:52
Nitrobenzene-d5 (S)
%
70
23-110
06/10/20 18:52
Phenol-d6 (S)
%
77
22-110
06/10/20 18:52
Terphenyl-d14 (S)
%
99
28-110
06/10/20 18:52
v1
v1
v1
Qualifiers
LABORATORY CONTROL SAMPLE:
2907544
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
1.7
1.2
70
52-130
1,2-Dichlorobenzene
mg/kg
1.7
1.3
78
51-130
1,3-Dichlorobenzene
mg/kg
1.7
1.3
78
50-130
1,4-Dichlorobenzene
mg/kg
1.7
1.3
81
49-130
1-Methylnaphthalene
mg/kg
1.7
1.2
72
55-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Johnson Oehler
Pace Project No.: 92480851
LABORATORY CONTROL SAMPLE: 2907544
Parameter
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
2,2'-Oxybis(1-chloropropane)
mg/kg
1.7
1.5
93
30-130 v1
2,4,5-Trichlorophenol
mg/kg
1.7
1.2
75
55-130
2,4,6-Trichlorophenol
mg/kg
1.7
1.3
76
57-130
2,4-Dichlorophenol
mg/kg
1.7
1.2
73
56-130
2,4-Dimethylphenol
mg/kg
1.7
1.3
76
51-130
2,4-Dinitrophenol
mg/kg
8.3
5.4
65
27-133
2,4-Dinitrotoluene
mg/kg
1.7
1.3
77
61-130
2,6-Dinitrotoluene
mg/kg
1.7
0.94
57
60-130 L2,v3
2-Chloronaphthalene
mg/kg
1.7
1.3
79
52-130
2-Chlorophenol
mg/kg
1.7
1.4
82
54-130
2-Methylnaphthalene
mg/kg
1.7
1.3
76
54-130
2-Methylphenol(o-Cresol)
mg/kg
1.7
1.4
82
51-130
2-Nitroaniline
mg/kg
3.3
2.7
81
51-130
2-Nitrophenol
mg/kg
1.7
1.3
78
49-130
3&4-Methyl phenol (m&p Cresol)
mg/kg
1.7
1.3
81
11-163
3,3'-Dichlorobenzidine
mg/kg
3.3
2.5
75
10-132
3-Nitroaniline
mg/kg
3.3
2.3
68
55-130
4,6-Dinitro-2-methyl phenol
mg/kg
3.3
2.6
78
47-142 v1
4-Bromophenylphenyl ether
mg/kg
1.7
1.2
73
59-130
4-ChIoro-3-methyl phenol
mg/kg
3.3
2.5
76
55-130
4-Chloroaniline
mg/kg
3.3
2.4
74
54-130
4-Chlorophenylphenyl ether
mg/kg
1.7
1.2
70
58-130
4-Nitroaniline
mg/kg
3.3
2.5
75
54-130
4-Nitrophenol
mg/kg
8.3
6.1
74
48-130
Acenaphthene
mg/kg
1.7
1.3
81
60-130
Acenaphthylene
mg/kg
1.7
1.4
82
60-130
Aniline
mg/kg
1.7
1.3
76
43-130
Anthracene
mg/kg
1.7
1.3
79
63-130
Benzo(a)anthracene
mg/kg
1.7
1.3
78
59-130
Benzo(a)pyrene
mg/kg
1.7
1.4
84
57-130
Benzo(b)fluoranthene
mg/kg
1.7
1.4
83
54-130
Benzo(g,h,i)perylene
mg/kg
1.7
1.4
83
59-130
Benzo(k)fluoranthene
mg/kg
1.7
1.3
80
54-130
Benzoic Acid
mg/kg
8.3
5.0
61
19-130
Benzyl alcohol
mg/kg
3.3
2.6
77
50-130
bis(2-Chloroethoxy)methane
mg/kg
1.7
1.3
77
54-130
bis(2-Chloroethyl) ether
mg/kg
1.7
1.3
78
48-130
bis(2-Ethylhexyl)phthalate
mg/kg
1.7
1.5
89
45-134
Butylbenzylphthalate
mg/kg
1.7
1.5
89
46-138 v1
Chrysene
mg/kg
1.7
1.2
75
58-130
Di-n-butylphthalate
mg/kg
1.7
1.4
86
60-130
Di-n-octylphthalate
mg/kg
1.7
1.5
93
53-130 v1
Dibenz(a,h)anthracene
mg/kg
1.7
1.3
79
59-130
Dibenzofuran
mg/kg
1.7
1.3
76
60-130
Diethylphthalate
mg/kg
1.7
1.3
79
60-130
Dimethylphthalate
mg/kg
1.7
1.3
78
60-130
Fluoranthene
mg/kg
1.7
1.3
77
65-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
LABORATORY CONTROL SAMPLE:
Parameter
2907544
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Fluorene
mg/kg
1.7
1.3
78
63-130
Hexachloro-1,3-butadiene
mg/kg
1.7
1.0
60
46-130
Hexachlorobenzene
mg/kg
1.7
1.2
74
58-130
Hexachlorocyclopentadiene
mg/kg
1.7
0.93
56
23-130
Hexachloroethane
mg/kg
1.7
1.3
79
47-130
Indeno(1,2,3-cd)pyrene
mg/kg
1.7
1.4
83
60-130
Isophorone
mg/kg
1.7
1.2
75
49-130
N-Nitroso-di-n-propylamine
mg/kg
1.7
1.3
77
47-130
N-Nitrosodimethylamine
mg/kg
1.7
1.3
78
45-130
N-Nitrosodiphenylamine
mg/kg
1.7
1.3
81
59-130
Naphthalene
mg/kg
1.7
1.3
78
55-130
Nitrobenzene
mg/kg
1.7
1.3
76
49-130
Pentachlorophenol
mg/kg
3.3
2.6
78
10-132
Phenanthrene
mg/kg
1.7
1.3
80
62-130
Phenol
mg/kg
1.7
1.5
90
46-130 v1
Pyrene
mg/kg
1.7
1.3
78
53-130
Pyridine
mg/kg
1.7
1.1
65
37-130
2,4,6-Tribromophenol (S)
%
78
27-110
2-Fluorobiphenyl (S)
%
75
30-110
2-Fluorophenol(S)
%
81
13-110
Nitrobenzene-d5 (S)
%
74
23-110
Phenol-d6 (S)
%
81
22-110
Terphenyl-d14 (S)
%
87
28-110
MATRIX SPIKE SAMPLE:
Parameter
2907545
Units
92476354004
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
ND
1.7
1.1
67
18-130
1,2-Dichlorobenzene
mg/kg
ND
1.7
1.1
67
14-130
1,3-Dichlorobenzene
mg/kg
ND
1.7
1.2
69
12-130
1,4-Dichlorobenzene
mg/kg
ND
1.7
1.2
72
10-130
1-Methylnaphthalene
mg/kg
ND
1.7
1.1
69
12-130
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
1.7
1.2
69
10-130
2,4,5-Trichlorophenol
mg/kg
ND
1.7
1.2
72
13-130
2,4,6-Trichlorophenol
mg/kg
ND
1.7
1.1
68
17-130
2,4-Dichlorophenol
mg/kg
ND
1.7
1.2
72
10-130
2,4-Dimethylphenol
mg/kg
ND
1.7
1.2
70
10-130
2,4-Dinitrophenol
mg/kg
ND
8.4
2.4
28
10-130
2,4-Dinitrotoluene
mg/kg
ND
1.7
1.2
73
24-130
2,6-Dinitrotoluene
mg/kg
ND
1.7
1.2
71
23-130
2-Chloronaphthalene
mg/kg
ND
1.7
1.1
66
19-130
2-Chlorophenol
mg/kg
ND
1.7
1.3
75
10-130
2-Methylnaphthalene
mg/kg
ND
1.7
1.2
70
18-130
2-Methylphenol(o-Cresol)
mg/kg
ND
1.7
1.2
74
10-130
2-Nitroaniline
mg/kg
ND
3.3
2.5
74
17-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 36 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
MATRIX SPIKE SAMPLE:
2907545
92476354004
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Nitrophenol
mg/kg
ND
1.7
1.1
68
10-130
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
1.7
1.3
76
10-130
3,3'-Dichlorobenzidine
mg/kg
ND
3.3
2.4
72
10-130
3-Nitroaniline
mg/kg
ND
3.3
2.3
70
24-130
4,6-Dinitro-2-methyl phenol
mg/kg
ND
3.3
1.3
39
10-152
4-Bromophenylphenyl ether
mg/kg
ND
1.7
1.0
61
29-130
4-Chloro-3-methylphenol
mg/kg
ND
3.3
2.5
76
17-130
4-Chloroaniline
mg/kg
ND
3.3
2.4
71
14-130
4-Chlorophenylphenyl ether
mg/kg
ND
1.7
1.1
63
25-130
4-Nitroaniline
mg/kg
ND
3.3
2.5
74
22-130
4-Nitrophenol
mg/kg
ND
8.4
6.6
79
10-130
Acenaphthene
mg/kg
ND
1.7
1.1
68
20-130
Acenaphthylene
mg/kg
ND
1.7
1.2
69
25-130
Aniline
mg/kg
ND
1.7
1.2
69
10-130
Anthracene
mg/kg
ND
1.7
1.1
65
29-130
Benzo(a)anthracene
mg/kg
ND
1.7
1.1
64
19-130
Benzo(a)pyrene
mg/kg
ND
1.7
1.0
60
12-130
Benzo(b)fluoranthene
mg/kg
ND
1.7
1.0
61
14-130
Benzo(g,h,i)perylene
mg/kg
ND
1.7
0.97
58
10-130
Benzo(k)fluoranthene
mg/kg
ND
1.7
1.0
62
14-130
Benzoic Acid
mg/kg
ND
8.4
1J
12
10-130
Benzyl alcohol
mg/kg
ND
3.3
2.4
73
13-130
bis(2-Chloroethoxy)methane
mg/kg
ND
1.7
1.1
66
16-130
bis(2-Chloroethyl) ether
mg/kg
ND
1.7
1.2
71
11-130
bis(2-Ethylhexyl)phthalate
mg/kg
ND
1.7
1.1
63
21-130
Butylbenzylphthalate
mg/kg
ND
1.7
1.1
63
23-130
Chrysene
mg/kg
ND
1.7
1.1
65
22-130
Di-n-butylphthalate
mg/kg
ND
1.7
1.0
61
30-130
Di-n-octylphthalate
mg/kg
ND
1.7
1.1
66
23-142
Dibenz(a,h)anthracene
mg/kg
ND
1.7
0.99
59
10-130
Dibenzofuran
mg/kg
ND
1.7
1.1
68
24-130
Diethylphthalate
mg/kg
ND
1.7
1.2
71
26-130
Dimethylphthalate
mg/kg
ND
1.7
1.2
70
22-130
Fluoranthene
mg/kg
ND
1.7
1.1
68
33-130
Fluorene
mg/kg
ND
1.7
1.1
69
22-130
Hexachloro-1,3-butadiene
mg/kg
ND
1.7
1.0
61
13-130
Hexachlorobenzene
mg/kg
ND
1.7
1.0
61
29-130
Hexachlorocyclopentadiene
mg/kg
ND
1.7
0.40
24
10-130
Hexachloroethane
mg/kg
ND
1.7
1.0
63
10-130
Indeno(1,2,3-cd)pyrene
mg/kg
ND
1.7
0.96
58
10-130
Isophorone
mg/kg
ND
1.7
1.2
70
13-130
N-Nitroso-di-n-propylamine
mg/kg
ND
1.7
1.2
73
12-130
N-Nitrosodimethylamine
mg/kg
ND
1.7
1.1
69
11-130
N-Nitrosodiphenylamine
mg/kg
ND
1.7
1.1
67
15-130
Naphthalene
mg/kg
ND
1.7
1.2
70
15-130
Nitrobenzene
mg/kg
ND
1.7
1.2
69
12-130
Pentachlorophenol
mg/kg
ND
3.3
2.4
72
10-130
Results presented on this
page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 37 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
MATRIX SPIKE SAMPLE:
Parameter
2907545
Units
92476354004
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Phenanthrene
mg/kg
ND
1.7
1.1
66
27-130
Phenol
mg/kg
ND
1.7
1.3
76
10-130
Pyrene
mg/kg
ND
1.7
1.1
66
19-130
Pyridine
mg/kg
ND
1.7
1.0
61
10-130
2,4,6-Tribromophenol (S)
%
72
27-110
2-Fluorobiphenyl (S)
%
59
30-110
2-Fluorophenol(S)
%
72
13-110
Nitrobenzene-d5 (S)
%
66
23-110
Phenol-d6 (S)
%
73
22-110
Terphenyl-d14 (S)
%
70
28-110
SAMPLE DUPLICATE: 2907546
Parameter
Units
92476354005
Result
Dup
Result
1,2,4-Trichlorobenzene
mg/kg
ND
ND
1,2-Dichlorobenzene
mg/kg
ND
ND
1,3-Dichlorobenzene
mg/kg
ND
ND
1,4-Dichlorobenzene
mg/kg
ND
ND
1-Methylnaphthalene
mg/kg
ND
ND
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
ND
2,4,5-Trichlorophenol
mg/kg
ND
ND
2,4,6-Trichlorophenol
mg/kg
ND
ND
2,4-Dichlorophenol
mg/kg
ND
ND
2,4-Dimethylphenol
mg/kg
ND
ND
2,4-Dinitrophenol
mg/kg
ND
ND
2,4-Dinitrotoluene
mg/kg
ND
ND
2,6-Dinitrotoluene
mg/kg
ND
ND
2-Chloronaphthalene
mg/kg
ND
ND
2-Chlorophenol
mg/kg
ND
ND
2-Methylnaphthalene
mg/kg
ND
ND
2-Methylphenol(o-Cresol)
mg/kg
ND
ND
2-Nitroaniline
mg/kg
ND
ND
2-Nitrophenol
mg/kg
ND
ND
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
ND
3,3'-Dichlorobenzidine
mg/kg
ND
ND
3-Nitroaniline
mg/kg
ND
ND
4,6-Dinitro-2-methyl phenol
mg/kg
ND
ND
4-Bromophenylphenyl ether
mg/kg
ND
ND
4-ChIoro-3-methyl phenol
mg/kg
ND
ND
4-Chloroaniline
mg/kg
ND
ND
4-Chlorophenylphenyl ether
mg/kg
ND
ND
4-Nitroaniline
mg/kg
ND
ND
4-Nitrophenol
mg/kg
ND
ND
Acenaphthene
mg/kg
ND
ND
Acenaphthylene
mg/kg
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 38 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
SAMPLE DUPLICATE: 2907546
Parameter
Units
92476354005
Result
Dup
Result
Aniline
mg/kg
ND
ND
Anthracene
mg/kg
ND
ND
Benzo(a)anthracene
mg/kg
ND
ND
Benzo(a)pyrene
mg/kg
ND
ND
Benzo(b)fluoranthene
mg/kg
ND
ND
Benzo(g,h,i)perylene
mg/kg
ND
ND
Benzo(k)fluoranthene
mg/kg
ND
ND
Benzoic Acid
mg/kg
ND
ND
Benzyl alcohol
mg/kg
ND
ND
bis(2-Chloroethoxy)methane
mg/kg
ND
ND
bis(2-Chloroethyl) ether
mg/kg
ND
ND
bis(2-Ethylhexyl)phthalate
mg/kg
ND
ND
Butylbenzylphthalate
mg/kg
ND
ND
Chrysene
mg/kg
ND
ND
Di-n-butylphthalate
mg/kg
ND
ND
Di-n-octylphthalate
mg/kg
ND
ND
Dibenz(a,h)anthracene
mg/kg
ND
ND
Dibenzofuran
mg/kg
ND
ND
Diethylphthalate
mg/kg
ND
ND
Dimethylphthalate
mg/kg
ND
ND
Fluoranthene
mg/kg
ND
ND
Fluorene
mg/kg
ND
ND
Hexachloro-1,3-butadiene
mg/kg
ND
ND
Hexachlorobenzene
mg/kg
ND
ND
Hexachlorocyclopentadiene
mg/kg
ND
ND
Hexachloroethane
mg/kg
ND
ND
Indeno(1,2,3-cd)pyrene
mg/kg
ND
ND
Isophorone
mg/kg
ND
ND
N-Nitroso-di-n-propylamine
mg/kg
ND
ND
N-Nitrosodimethylamine
mg/kg
ND
ND
N-Nitrosodiphenylamine
mg/kg
ND
ND
Naphthalene
mg/kg
ND
ND
Nitrobenzene
mg/kg
ND
ND
Pentachlorophenol
mg/kg
ND
ND
Phenanthrene
mg/kg
ND
ND
Phenol
mg/kg
ND
ND
Pyrene
mg/kg
ND
ND
Pyridine
mg/kg
ND
ND
2,4,6-Tribromophenol (S)
%
61
65
2-Fluorobiphenyl (S)
%
54
57
2-Fluorophenol (S)
%
59
63
Nitrobenzene-d5 (S)
%
61
65
Phenol-d6 (S)
%
61
64
Terphenyl-d14 (S)
%
75
78
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 39 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
QC Batch: 546610 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92480851002, 92480851003, 92480851005, 92480851006
METHOD BLANK: 2909288
Matrix:
Solid
Associated Lab Samples:
92480851002, 92480851003,
92480851005, 92480851006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
9.9
06/15/20 10:05 N2
Aliphatic (C19-C36)
mg/kg
ND
9.9
06/15/20 10:05 N2
Aromatic (C11-C22)
mg/kg
ND
9.9
06/15/20 10:05 N2
2-Bromonaphthalene (S)
%
100
40-140
06/15/20 10:05
2-Fluorobiphenyl (S)
%
100
40-140
06/15/20 10:05
Nonatriacontane (S)
%
65
40-140
06/15/20 10:05
o-Terphenyl (S)
%
83
40-140
06/15/20 10:05
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2909289
Units
Spike
Conc.
2909290
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec Max
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
10
ND ND
48
49
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.3
ND ND
61
54
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28.2
19.5 20.1
69
70
40-140 3 50 N2
2-Bromonaphthalene (S)
%
101
107
40-140
2-Fluorobiphenyl (S)
%
101
106
40-140
Nonatriacontane (S)
%
58
53
40-140
o-Terphenyl(S)
%
80
83
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 40 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
QC Batch: 547307 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92480851004
METHOD BLANK: 2912877
Matrix:
Solid
Associated Lab Samples: 92480851004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
10.1
06/16/20 18:40 N2
Aliphatic (C19-C36)
mg/kg
ND
10.1
06/16/20 18:40 N2
Aromatic (C11-C22)
mg/kg
ND
10.1
06/16/20 18:40 N2
2-Bromonaphthalene (S)
%
93
40-140
06/16/20 18:40
2-Fluorobiphenyl (S)
%
94
40-140
06/16/20 18:40
Nonatriacontane (S)
%
71
40-140
06/16/20 18:40
o-Terphenyl (S)
%
77
40-140
06/16/20 18:40
LABORATORY CONTROL SAMPLE & LCSD:
2912878
2912879
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
9.9
ND ND
53
52
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.2
ND ND
58
64
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28
17.7 20.2
63
72
40-140 13 50 N2
2-Bromonaphthalene (S)
%
82
87
40-140
2-Fluorobiphenyl (S)
%
79
82
40-140
Nonatriacontane (S)
%
60
65
40-140
o-Terphenyl(S)
%
68
77
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 41 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
QC Batch: 546123 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92480851001, 92480851002, 92480851003, 92480851004, 92480851005, 92480851006
SAMPLE DUPLICATE: 2907214
92480009001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 82.6 82.7 0
SAMPLE DUPLICATE: 2907215
92480920006 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 10.8 10.8 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 42 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johnson Oehler
Pace Project No.: 92480851
QC Batch: 1493107 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92480851002, 92480851003, 92480851004, 92480851005, 92480851006
METHOD BLANK: R3539541-1
Matrix:
Solid
Associated Lab Samples: 92480851002, 92480851003,
92480851004, 92480851005,
92480851006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Solids
%
ND
06/16/20 13:18
LABORATORY CONTROL SAMPLE:
R3539541-2
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Solids
%
50.0
50.0
100 85.0-115
SAMPLE DUPLICATE: R3539541-3
92480851006 Dup
Parameter Units Result Result RPD Qualifiers
Total Solids % 92.0 91.4 0.601
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC.
Page 43 of 48

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: Johnson Oehler
Pace Project No.: 92480851
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
SO Surrogate recovery outside laboratory control limits.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/18/2020 07:33 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 48

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Johnson Oehler
92480851
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92480851001
UST-1
EPA 3546
546213
EPA 8015C Modified
546516
92480851002
SW-1
MADEP EPH
546610
MADEP EPH
547280
92480851003
SW-2
MADEP EPH
546610
MADEP EPH
547280
92480851004
SW-3
MADEP EPH
547307
MADEP EPH
547621
92480851005
SW-4
MADEP EPH
546610
MADEP EPH
547280
92480851006
B-1
MADEP EPH
546610
MADEP EPH
547280
92480851002
SW-1
MADEPV
1493015
MADEP VPH
1493015
92480851003
SW-2
MADEPV
1493015
MADEP VPH
1493015
92480851004
SW-3
MADEPV
1493015
MADEP VPH
1493015
92480851005
SW-4
MADEPV
1493015
MADEP VPH
1493015
92480851006
B-1
MADEPV
1493015
MADEP VPH
1493015
92480851001
UST-1
EPA 5030B
546048
EPA 8015C Modified
546077
92480851002
SW-1
EPA 3546
546176
EPA 8270E
546380
92480851003
SW-2
EPA 3546
546176
EPA 8270E
546380
92480851004
SW-3
EPA 3546
546176
EPA 8270E
546380
92480851005
SW-4
EPA 3546
546176
EPA 8270E
546380
92480851006
B-1
EPA 3546
546176
EPA 8270E
546380
92480851002
SW-1
EPA 5035A/5030B
546439
EPA 8260D
546503
92480851003
SW-2
EPA 5035A/5030B
546439
EPA 8260D
546503
92480851004
SW-3
EPA 5035A/5030B
546439
EPA 8260D
546503
92480851005
SW-4
EPA 5035A/5030B
546439
EPA 8260D
546503
92480851006
B-1
EPA 5035A/5030B
546439
EPA 8260D
546503
92480851001
UST-1
ASTM D2974-87
546123
92480851002
SW-1
ASTM D2974-87
546123
92480851003
SW-2
ASTM D2974-87
546123
92480851004
SW-3
ASTM D2974-87
546123
92480851005
SW-4
ASTM D2974-87
546123
92480851006
B-1
ASTM D2974-87
546123
92480851002
SW-1
SM 2540 G
1493107
SM 254OG
1493107
92480851003
SW-2
SM 2540 G
1493107
SM 254OG
1493107
92480851004
SW-3
SM 2540 G
1493107
SM 254OG
1493107
92480851005
SW-4
SM 2540 G
1493107
SM 254OG
1493107
92480851006
B-1
SM 2540 G
1493107
SM 254OG
1493107
Date: 06/18/2020 07:33 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 45 of 48

Document Name:
Document Revised: February 7, 2018
ace Analytical
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[—] Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
SampledClient Name: �o,Q�t#: . WO# • 92480851
Upon Receipt
Courier: ❑Fed Ex ❑UPS ❑USPS Oclient 11111111111111111111111❑ Commercial ❑Pace ❑Other:
92480851
Custody Seal Present? ❑Yes E]4 Seals Intact? []Yes �JNa
Date/Initials Person Examining Contents:
Packing Material: []Bubble Wrap []Bubble Bags ❑None Other Biological Tissue Fen?
Thermometer: ❑Yes [:]No Q /A
92TO61 Type of Ice: et ❑Blue ❑None
❑IR Gun ID:
Cooler Temp (°C): - L j C— Correction Factor: Add/Subtract (*Cl +0.1
. � Temp should be above freezing to 6°C
Cooler Temp Corrected I'C): ❑Samples out of temp criteria. Samples an ice, cooling process
has begun
USDA Regulated �it (❑ N/A, water sample)
Did samples origirl3te in a quarantine zone within the United States: CA, NY, or 5[ (check maps)7 old samples originate from a foreign source lintern'jaiionally,
f—lva° rV . includin¢Hawall and Puerto Ricol? i—IYes S FINo
Cam ments/Dlscre ancy,
Chain of Custody Present
&34V
❑No
❑N/A
1.
Samples Arrived within Hold Time?
es
MNp
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
No
❑N/A
3.
Rush Turn Around Time Requested?
Dyes
[34c,
[]N/A
4.
Sufficient Volume?
❑ es
❑No
[]N/A
S.
Correct Containers Used?
-Pace Containers Used?
19
es
❑No
❑No
❑N/A
❑N/A
&.
Containers Intact?
es
t:]Na
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Y
❑No
ON7A
8.
Sample Labels Match CCIC?es
No
N A
9.
-Includes Date/Time/ID/Analysis Matrix:
Heads ace in VOA Vials (>5-6mm)?
❑Yes
❑No
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[-]Yes
❑Yes
[]NO
[]No
091A
ONJAI
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Lot ID of split containers:
Date:
Date:
field Data Required? ❑Yes (—]No
Page 46 of 48

Document Name:
Document Revised: February 7, 2018
a3CB�if18�I,`�lCc���
Y
Sample Condition Upon Recel t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carollnas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, 0110/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project tt Wa# ; 9248Q851
PM: ATE Due Date: 06/15/20
CLIENT: 92-ECS GBORO
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pH Adjustment Log for Preserved Samples
Sample 10
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot H
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina OEHNR Certification Office (i.e.
Out of hold, Incorrect preservative, out of temp, Incorrect containers.
Page 47 of 48

N M P
D m
A
C y A
m m m
o 0- D
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D O
N
m M z
al A -ai
G
!1 X
V
TEMP in C
Received on
Ice
(YIN)
ustZr ody
Sealed
Cooler
(YIN)
Samples
Intact
(YIN)
Qr
°n
m
ti
m
g
to I- i- 11 I- l- lA lW 1N i- I ITEM #
ons
n 1 p N
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c w ? A
u
a �
MATRIX CODE (Jee valid codes to lofl)
SAMPLE TYPE (G=GRAB C=COMP)
0
rn
m �
a
-A ,
M
m
m
z
SAMPLE TEMP AT COLLECTION
# OF CONTAINERS
t, Unpreserved
H2SO4
HNO3
d
HCI
m
NaOH
a2i
Na2S203
CD
N
Melhanol
Other
Analyses Test
YIN
vac by 8260
6[ Y27ii
Residual Chlorine (YIN)
Q p 0 G p
o 0 C, 0 C)
\-n
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Page 48 of 48

APPENDIX E
(UST-61 Form)

UST- 1 Haar Release and VIT Leak Reporting Form.
Of R �#2Y5 5 rr. s Porm should be completed and subm�ttad to the UST ^w�.liviI. rrrdirij,a; i:Nics followlr,y a kn,,wn u, suspected release from
31-1 underground Morago tank {LIST) sysiam. This farm is required to be aubmdted withln 24 hours of iilsaov�ry of a known or
i� suspected release
(DWM USE ONLY) Suspected Contamination? (Y/N) — Facility ID Number
IncidentReceived
# _ _ Risk (H,I,L,U) Confirmed GW Contamination? (Y/N) Date Leak Discovered L'a F(- 2�2
R6�Ived On— RiKaived BY Confirmed Soil Contamirlation ?(Y/N) Comm/Non-Commercial? {�y� -
RAparted by *6YO orra): Phone, Fax or Report Samples Taken?(Y/N)y Reg/Non-regulated? N Fr NA
Region Free Product? (Y/N) If Yes, State Greatest
Thickness
Incident Name'
INCIDENT DESCRIPTION
tt
Address: II
('h �./ 4 c County:
CityJTown: Zip Code: Regional Office (circle one): Asheville Mooresville Fayetteville
Z- _r 3 Raleigh, Washington, Wilmington, Wins m
Latitude (decimal degrees): N L G Longitude (decimal degrees) : �'� > Obtained by
J l
Briefly describe suspected or confirmed release: (including but not limited to' nature of release, date of release, amount �
of release, amount of free product present and recovery efforts initial responses conducted impacts to race tors Lt'J IDS
❑Topographic map
❑GIS Address matching
❑Other
❑ Unknown
Describe location:
HOW RELEASE WAS DISCOVERED (Release Code)
(Ctrech ohe)
Release Detection Equipment or Methods
wring UST ClosureJRemoval
❑Property Transfer
Sou e of Reloase
(Check primary source)
Es?/Tank
❑ Piping
Dispenser
❑ Submersible Turbine Pump
❑ Delivery Problem
❑ Spill Bucket
❑ Other
❑ Unknown
on
2/isual/Odor
❑Water in Tank
❑Water Supply Well Contamination
SOURCE OF CONTAMINATION
Ouse of JRe)ease T-Vpo of Release
(Check primary cause) (Check one)
❑ Spill L Petroleum
❑ Overfill ❑ Non -Petroleum
Corrosion ❑ Both
❑ Physical/Mechanical
Damage Location
❑ Install Problem (Check one)
❑ Other ❑Facility
0 Unknown QResidence
Definitions presented on reverse I ❑Other
9wriamm
I- MuniialPal 2, MltllarY 3, Unknown . Pn 5. Federal 6. County 7. State
❑Groundwater Contamination
❑Surface Water Contamination
[]Other (specify)
Product Type
Rele;lisad
(Check primary product type released)
$sola7e! "esel/
❑ Diesel/Veg. Oil
Blend
Heating Oil
❑ Vegetable Oil 100%
El Other Petroleum
❑ E9 0 — E20
Products
II --II
1J E21 — E84
❑ Metals
❑ Other Inorganics
Q E85 — E99
[]Ethanol 100%
❑ Other Organics
E01 — E09
OwatkmTypia
I. Public Service 2, Agricultural eidenila . Education/Relig. 5. Industrial 6. Commercial 7. Mining

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected?
1. Yes No 3. Unknown
Number of Water Supply Wells Affected
Water Supply Wells Contaminated- (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
S,
2,
UST SYSTEM OWNER
UST Owner/Company
LA
Point of Contact
Address
City
State Zip Code Telephone Number
UST SYSTEM OPERATOR
C
UST Operator/Company
_
Address
Glfy
State
Zip Code
Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner
J Y �IC� �,�
Address
�� 15 2-0 .sr�'�t �31 �Q 5w 2r
City
State Zip Code
Telephone Number
28,
WMyto lkbc
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident
m-
Company if
Telephone Number'
[#814 '� q
Title
-e G
Address
UJ I rorm b-I kurt I'd)
Page 2 of 2
Definitions of Sources
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or tiom components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g_, when the delivery hose is disconnected from the tank till pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (o.g., Puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e g., for steel, corrosion takes the torm of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the LIST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined

APPENDIX F
(Non -Hazardous Waste Manifest - Soil)

ENVIRONMENTAL SOILS, INC.
APPROVAL#
LOCATION OF SOIL:
TRANSPORTER:
TIME:
DATE:
DRIVER SIGNATURE
TIME:
DATE:
DRIVER SIGNATURE
TIME:
DATE:
DRIVER SIGNATURE
TIME:
DATE:
DRIVER SIGNATURE
P.O. BOX 295
LATTIMORE, N.C. 28089
704-434-0075
NON -HAZARDOUS PETROLEUM CONTAMINATED SOIL
TRUCK It -
LICENSE #_
TRUCK #-
LICENSE #
TRUCK #_
LICENSE #
TRUCK#,
LICENSE #
MANIFEST #
INSPECTED & ACCEPTED BY ENVIRONMENTAL SOILS, INC.
SUPERVISOR'S SIGNATURE
_ GROSS WT.
LBS.
_ TARE WT.
LBS.
I T .`:
LBS.
_ GROSS WT.
LBS.
_. TARE WT.
LBS.
F-T WT .
:ILBS <'
GROSS WT.
LBS.
_ TARE WT.
LBS.
4 f . € WT
LBS
- GROSS WT.
LBS,
TARE WT.
LBS.
TOTAL NET WT.
TOTAL EQUIV-TONS

Environmental Soils Inc.
PQ. Box 295 - Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest #
Date (9 "LL `L 0 Load Number
EAWRONMENML CONSULTzLVT
Contact: Randy Cavallier
ECS SouthE 5# LLsequentially as trucks are dispatched)
Phone: [phone]
GEIVERjTOR Charter Properties
Address: 1520 S Blvd St 215, Charlotte NC 287203
Contact:
Fax:
County: Mecklenburg
Phone: [phone]
WASTE 0RIGIN,4TI0NP0IIVT.• Complete Address: 3808 Johnston Oehler RD, Charlotte NC 28269
Class &- Type of Contaminate in soil
.SOURCE OF CONTXMIV�4TIO14' (ex. UST or other source) USi
GEAEK4TORS CERI'IF'C�4TION OF "W S7E CONSTITUENTS In lieu of submitttng analyt cal data (methods
8240 and 8270) Verifying -that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am suhmitting this Certificate of Waste
Constituents.I certify that I ant familiar with the source of contamination of the soil and further certify the source,. to
the Best of my knowledge, contains no contandnants other than that listed shove.
TRdiNSPORTER: South Creek Trucking
Contact_ Jake Palilko
Phone: [phone]
As the carrier, I cerfify that the materials described above being shipped under this nonT-hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Date;
�a
TRUCK #: AG # VOLUXIE:
TRUCK DRIVER SIGNATURE: � ,ice/ , E. Z DATE: Z Sao
t
DESMWTIONt to . n 4 Qrbwdy Rd : Sl�ell3 1 D sated .art4 = pp 0#01
Site Permit #SR0300038
I per* that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facility Signature: - ' t Date:
Signature: i
Company Name
Date: (Q , z. `I..- Z 0
Title: S i?v 1 S o
White/Facility Canary/Invoice Goldenrod/Generator Pink/Cam-er

Environmental Soilst nc.
PGBOX 295 -Lattimore; NC 28089
Phone [phone] Fax [phone]
I\on-Hazardous Waste Manifest #
Date , `, -�: Load Number.'
(numbered sequentially as trucks are dispatched)
EAWRONAIEN lL COMSULM1VT. ECS SouthEast LLP
Contact: Randy Cavallier Phone[phone] Fax:
GENERATOR: Charter. Properties
Address: 1520 S Blvd St 215, Charlotte NC 287203 Count. Mecklenburg
Contact Phone: [phone]
WASTE ORIG.UVATIONPOINT Complete Address :3808 Johnston Oehler RD Charlotte NC 28269.
Class &Type of Contaminate in soil
SOURCE OFCONT"LVl'7ION.- (,ex- UST or other source).UST
GENER4TORS CERTIFICATION OF WASTE CONSTITUENTS; In lieu ofsubmitting analytical data (methods
8240 and 8270) verifying that the waste in question, does not contain organic constituents other than those which would
.normally appear inanalysis of virgin petroleum product residue, lam submitting this Certificate of Waste
Constituents, cesixfy that l urn fanziLir r with the source of contanxinat on of the.soilandfarther certify the source, to
the best of my knowledge, contains no contaminants other than that listed above..
TRr4NSPORT South Cfeek° Trucking
Contact: Jake Palillo Phone: [phone]
As the carrier, I certify that the materials described above'being shipped under this non -hazardous materials
manifest are properly classified, packaged; labeled,.secured, and are in proper condition for transport in commerceunder the applicable regulation. s governing' trans portat on, and I hereby receive this material for delivery to the
facility designate:
Carrier Signature. Date:
TRUCK#: ZG #. VOLUIVITRUCK DRIVER SIGNATURE: DATE: a9
DESTl1L,' TION Envlronrnental Soil; Inc. 910 Crow=dy lid, Shelby, N?C 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facility Signature: Date:-aLl—a-6
Signature: _ G
Company Name
White/Facility
Canarny/Invoice
Date:
Title: . 5 � V &.r ►A3 or
Goldenrod/Generator Pink/Carrier

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone]• Fax [phone]
Non -Hazardous Waste Manifest #^
Da
EAWIRONMENT4L CONSULTANT. -
GENERATOR:
Address:
Contact:
Number
(numbered sequentially as trucks are dispatched)
Phone: Fax:
WASTE ORIGINATIONPOINT.• Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONTAMINATION.- (ex. UST or other source)
County:
Phone:
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods
8240 and 8270) ver�oing that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste
Constituents. I certify that I am familiar with the source of contamination of the soil and further certify the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signa
TRANSPORTER:
Contact: Phone:
Date:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
TRUCK #:
TAG #:
VOLUME:
TRUCK DRIVER SIGNATURE: DATE:
DESTINATION.- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
Ti
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 56931
Date Load Number
(numbered sequentially as trucks are dispatched)
ENYIRONMENTJL CONSULT4NT
Phone:
Contact:
WASTE ORIGIN4TI0NPOINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONT4MIX4TION.• (ex. UST or other source)
Fax:
County:
Phone:
GENERf4TORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu of submitting analytical data (methods
9240 and 9270) ver�ing that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am submitting this Cert�6cate of Waste
Constituents. I certify that I am familiar with the source of contamination of the soil and further cert� the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature:
TRfINSPORTER:
Contact:
Date:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
TRUCK #:
TRUCK DRIVER SIGNATURE:
TAG #:
VOLUME:
DATE:
DESTINATION.- Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
Date:
Title:
Date:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

ENVIRONMENTAL SOILS, INC.
P.O. BOX 295
LATTIMORE, N.C. 28089
704-434-0075
NON -HAZARDOUS PETROLEUM CONTAMINATED SOIL
APPROVAL # _ MANIFEST #
LOCATION OF SOIL:
TRANSPORTER:
TIME:
DATE:
DRIVER SIGNATURE,_
TIME:
DATE:
DRIVER SIGNATURE
TIME:
DATE:
DRIVER SIGNATURE
TIME:
DATE:
DRIVER SIGNATURE
TRUCK #_
LICENSE #
TRUCK #-
LICENSE #
TRUCK #-
LICENSE #
TRUCK #_
LICENSE #
INSPECTED & ACCEPTED BY ENVIRONMENTAL SOILS, INC.
SUPERVISOR'S SIGNATURE
GROSS WT.
LBS.
TARE: WT.
LBS.
_IT WT;'
LBS.'
GROSS WT.
LBS.
TARE WT.
LBS.
NET
GROSS WT.
LBS.
TARE WT,
LBS.
NET WT -
LS5
GROSS WT.
LBS,
TARE WT.
LBS.
TOTAL NET WT.
TOTAL EDUIV-TONS

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # q 2
Date Load Number
ENVIRONMENT 4L CONSULTANT -
Contact:
GENERATOP
(numbered sequentially as trucks are dispatched)
Phone:
Fax:
Address: County:
Contact: Phone:
W4STE ORIGINATIONPOINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OFCONE14MIMMON.• (ex. UST or other source)
GENER,4TORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods
8240 and 8270) ver�ing that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am submitting this Cert�ficate of Waste
Constituents. I certify that I am familiar with the source of contamination of the soil and further certify the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature:
TRANSPORTER:
Contact: Phone:
Date:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
TRUCK #: TAG #:
VOLUME:
TRUCK DRIVER SIGNATURE: DATE:
DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature:
Company Name
Date:
Title:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 56933
Date
ENVIRONMENE4L CONSULTANT
GENER,ITOR:
Number
(numbered sequentially as trucks are dispatched)
Phone:
WASTE ORIGIN,4TIONPOINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONTAMINATION (ex. UST or other source)
Fax:
County:
Phone:
GENER,4TORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleumproduct residue, I am submitting this Cert icate of Waste
Constituents. I certf� that I am familiar with the source of contamination of the soil and further cert� the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signa
TRANSPORTER -
Contact: Phone:
Date:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
TRUCK #:
TAG #:
VOLUME.
TRUCK DRIVER SIGNATURE: DATE:
DESTINfIT.ION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature. -
Signature:
Company Name
Date:
Title:
Date:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest #
Date
ENVIRONMENTI4L CONSULTANT
Contact:
GENERATOR:
Address:
Contact:
ad Number
6934
(numbered sequentially as trucks are dispatched)
Phone: Fax:
W14STE ORIGINI4TIONPO4N7: Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONTJMTV,4TION.• (ex. UST or other source)
County:
Phone:
GENERATORS CERTIFIC14TION OF W14STE CONSTITUENTS: In lieu of submitting analytical data (methods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, Iam submitting this Cert icate of Waste
Constituents. I cert� that I am familiar with the source of contamination of the soil and further cert v the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
TR,4NSPORTER:
Contact: Phone:
As the carrier, I certify that the materials described above being shipped -under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
TRUCK #:
TRUCK DRIVER SIGNATURE.
TAG #:
VOLUME:
DATE:
DESTINI4TION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
Date:
Title:
Date:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Beverly, Trudy
From:
Sent:
To:
Cc:
Subject:
Good Afternoon Phil,
Beverly, Trudy
Wednesday, August 26, 2020 3:44 PM
Phil A Vetter
Roger A Smith, P.G.
RE: [External] 3808 Johnston Oehler Rd
Received. Thank you for emailing the electronic copy.
Have a wonderful day,
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
Regional O UST Section, Mooresville Re Office
irvrc,� g
704.235.2182 (Office)
Trudy.Beverlykncdenr. ov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: ht_pt s:Hdeg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deg.nc.aov/about/divisions/waste-mana2ement/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httos://deo.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-ais-mans
File Review Procedures:
htlps://deg.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
httos: //deq.nc. gov/about/divisions/waste-manai4ement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httns://files.ne.izov/nedeafWaste%2OMana2ement/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policy.odf
https:Hfiles.nc.gov/ncdeq/Waste%20Management/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Phil A Vetter[mailto:[e-mail]]
Sent: Wednesday, August 26, 2020 3:32 PM
To: Beverly, Trudy <[e-mail]>
Cc: Roger A Smith, P.G. <[e-mail]>
Subject: [External] 3808 Johnston Oehler Rd
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
[e-mail]
Trudy,
As requested during our phone conversation yesterday, I have attached a digital copy of our transmittal letter and the
abatement report for the removal of one underground storage tank. Please let me know if you require anything
else. Thank you.
Phil Vetter

-J'JCHARTER
,J-1 PROPERTIES INC