MO-28509_47761_CA_UST-61_20210309_24-Hour Release and UST Leak Reporting Form

UST-61
I 24-Hour Release and UST Leak Reporting Form
For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release
in NC from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a
known or suspected release
(DWM USE ONLY)
Suspected Contamination? (Y/N) Y
Facility ID # N/A
Y
Incident # Risk (H,I,L,U)
Confirmed GW Contamination? (Y/N) N
Received On Received By
Confirmed Soil Contamination? (Y/N) Y
Date Leak Discovered 2/9/2021
Region
/ ? k T Samples Taken? YN
Sam p ( ) Y
Comm/Non-Commercial. Non -Comm
Reported by (circle one): Phone, Email or Report
NAPL? (Y/N) N
Reg/Non-regulated? Non -regulated
If Yes, State Greatest Thickness N/A
INCIDENT DESCRIPTION
Incident Camp Stewart Road Site
Name:
Address: Camp Stewart Road, Tax PIN 11109204
County: Mecklenburg
City/Town: Charlotte
Zip Code: 28215
Regional Office (circle one): Asheville, Fayetteville, Mooresville,
Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): 35.241186
Longitude (decimal degrees):-80.661215
Location Obtained by:
El GPS
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount of
release, amount of NAPL present and recovery efforts, initial responses conducted, impacts to receptors)
❑ Topographic map
As part of Pulte Home Company, LLC's due diligence in advance of purchasing the subject property, two approximate
adjacent 550- allon heating oil USTs, designated UST-2 and UST-3, were removed. Upon removal of the two USTs,
V GIS Address matching
two leak detection soil samples were collected from the base of each of the two UST pits for laboratory analysis of
TPH-DRO and TPH-GRO see Table B-3 attached). All 4 release detection samples exceeded NCDEQ's TPH-DRO
✓ Other — Google Earth
❑ Unknown
screening level of 100 ppm, with levels ranging from 2,040 to 10,500 ppm. One release detection sample exceeded
NCDEQ's TPH-GRO screening level of 50 ppm, with a level of 75 ppm. An attempt was made to excavate all
Describe location:
petroleum -impacted soil, confirmatory soil samples were collected for laboratory analysis, and an Initial Abatement
Action Report is under preparation. The confirmatory soil sample analytical results at the base and two sidewalls
of the excavation show exceedances of residential MSCCs; therefore, a Limited Site Assessment is being planned.
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
❑ Release Detection Equipment or Methods ❑ Visual/Odor ❑ Groundwater Contamination
✓ During UST Closure/Removal ❑ Water in Tank ❑ Surface Water Contamination
❑ Property Transfer ❑ Water Supply Well Contamination ❑ Other (specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release Product Type Released
(Check one to indicate primary source) (Check one to indicate primary cause) (Check one) (Check one to indicate primary product type released)
✓ Tank ❑ Spill ✓ Petroleum ❑ Gasoline/Diesel/ ❑ Diesel/Veg.Oil
❑ Piping ❑ Overfill ❑ Non -Petroleum Kerosene Blend
❑ Dispenser ✓ Corrosion ❑ Both `/ Heating Oil ❑ Veg. Oil 100%
❑ Submersible Turbine Pump ❑ Physical/Mechanical Damage Location ❑ Other Petroleum ❑ E10 — E20
(Check one) Products ❑ E21 — E84
❑ Delivery Problem ❑ Install Problem
❑ Metals
❑ Facility ❑ E85 — E99
❑ Other (specify) ❑Other (specify) ❑ Other Inorganics
❑ Unknown ❑ Unknown ❑ Residence ❑ Ethanol 100%
❑ Other Organics
Definitions printed on reverse Definitions printed on reverse ✓ Other Summer ❑ E1 — E9
camp office
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig 5. Industrial 6. Commercial 7. Mining
(Recreational)
UST Form 61 (05/17) Page 1 of 2

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 12. No 3. Unknown
Number of Water Supply Wells Affected: N/A
Water Supply Wells Contaminated: (Include Users' Names, Addresses, and Phone Numbers. Attach additional sheet if necessary.)
1. N/A
2.
3.
UST SYSTEM OWNER
UST Owner / Company:
Professional Child Centers, Inc.
Point of Contact:
Address:
Dean Davidson
505 Beachland Blvd, Suite #1
City:
State:
Zip Code:
Telephone Number:
Vero Beach
FL
32963
772-913-1152
UST SYSTEM OPERATOR
UST Owner / Company:
Same as UST System Owner
Point of Contact:
Address:
City:
State:
Zip Code:
Telephone Number:
LANDOWNER AT LOCATION OF UST INCIDENT
UST Owner / Company:
Same as UST System Owner
Point of Contact:
Address:
City:
State:
Zip Code:
Telephone Number:
Draw Sketch of Area (showing two major road intersections) or Attach Map
See attached map
Person Reporting Incident
Company
Telephone Number
Nora Zirps, PE, RSM
ESP Associates, Inc.
704-583-4949
Title
Address
Date
Senior Project Engineer
P.O. Box 7030, Charlotte, NC 28241
March 9, 2021
UST Form 61 (05/17)
Page 2 of 2
Definitions of Sources:
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP): Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes:
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined

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All locations are approximate.
PROJECT NO.
GP56.600
SHEET TITLE
FIGURE 1
ESP Associates, Inc.
N
SCALE
As Shown
USGS TOPOGRAPHIC SITE LOCATION MAP
P.O. Box 7030
Charlotte, NC 28241
0 330 660 w_ E
Feet S .
DRAWN BY
FN
PROJECT
CAMP STEWART ROAD SITE
phone [phone]
CHECKED BY
Cw
DATE 512312018
CHARLOTTE, NORTH CAROLINA
www.espassociates.com

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/9/2021 Incident Number: Pending — Camp Stewart Road Site, Charlotte, NC Facility ID#: N/A
Analytical Method (e.g., VOC by EPA 8260) 4
8015
8015
8260
8260
8260
8260
Contaminant of Concern 4
°
Q
°
Date
Source Area
Sample
Incident
Sample ID
Collected
(eg. Tank
Depth
phase
a
a
(Cl
(Cl
(Closure,
w
(m/dd/yy)
pit 1)
(ft BGS)
etc
Tank Pit 2
42 NS (4-4.5)
2/9/2021
4.5
Closure
10,500
75.0
BRL
BRL
BRL
0.528
Base
Tank Pit 2
#2 SS (4-4.5)
2/9/2021
4.5
Closure
4,720
4.9 J
BRL
BRL
BRL
BRL
Base
Tank Pit 3
#3 NS (4-4.5)
2/9/2021
4.5
Closure
3,040
19.1
BRL
BRL
BRL
0.0342
Base
Tank Pit 3
#3 SS (4-4.5)
2/9/2021
4.5
Closure
2,040
25.3
BRL
BRL
BRL
BRL
Base
Soil -to -Groundwater MSCC (mg/kg)
NE
NE
0.0072
8
5.4
6
Residential MSCC (mg/kg)
NE
NE
12
60.3
1,250
3,120
Industrial/Commercial MSCC (mg/kg)
NE
NE
59.4
297
18,600
46,700
Bold values exceed lowest MSCC. TPH-DRO and TPH-GRO screening levels are 100 mg/kg and 50 mg/kg, respectively.
BRL = below reporting limits
ft BGS = feet below ground surface
J = Analyte was positively identified but the value is estimated below the reporting limit.
mg/kg = milligrams per kilogram
MSCC = maximum soil contaminant concentration
NE = not established

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
February 24, 2021
Chris Ward
ESP Associates
3475 Lakemont Boulevard
Fort Mill, SC 29708
RE: Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Dear Chris Ward:
Enclosed are the analytical results for sample(s) received by the laboratory on February 11, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
[phone]
Project Manager
Enclosures
cc: Account Payable, ESP Associates
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 65

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21LA 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92521577001
#3 NS (4-4.5)
Solid
02/09/21 14:10
02/11/21 08:00
92521577002
#3 SS (4-4.5)
Solid
02/09/21 14:15
02/11/21 08:00
92521577003
#2 NS (4-4.5)
Solid
02/09/21 14:20
02/11/21 08:00
92521577004
#2 SS (4-4.5)
Solid
02/09/21 14:25
02/11/21 08:00
92521577005
#1 NS (5.5)
Solid
02/10/21 09:45
02/11/21 08:00
92521577006
#1 SS (5.5)
Solid
02/10/21 09:50
02/11/21 08:00
92521577007
#2 NW (6.5-7)
Solid
02/10/21 17:25
02/11/21 08:00
92521577008
#2 SW (6.5-7)
Solid
02/10/21 17:37
02/11/21 08:00
92521577009
#2 EW (6.5-7)
Solid
02/10/21 17:05
02/11/21 08:00
92521577010
#2 WW (6.5-7)
Solid
02/10/21 17:15
02/11/21 08:00
92521577011
#2 BASE (15.0)
Solid
02/10/21 16:55
02/11/21 08:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
CAMP STEWARD ROAD SITE
92521577
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92521577001
#3 NS (4-4.5)
EPA 8015C Modified
SEM
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577002
#3 SS (4-4.5)
EPA 8015C Modified
SEM
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577003
#2 NS (4-4.5)
EPA 8015C Modified
JMS1
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577004
#2 SS (4-4.5)
EPA 8015C Modified
JMS1
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577005
#1 NS (5.5)
EPA 8015C Modified
JMS1
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577006
#1 SS (5.5)
EPA 8015C Modified
JMS1
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577007
#2 NW (6.5-7)
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
ACG
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
92521577008
#2 SW (6.5-7)
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
JHH
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
92521577009
#2 EW (6.5-7)
MADEP EPH
BAJ
7
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Lab ID Sample ID
Method
Analysts
Analytes
Reported
Laboratory
MADEP VPH
JHH
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
92521577010 #2 WW (6.5-7)
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
ACG
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
92521577011 #2 BASE (15.0)
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
ACG, BMB
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #3 NS (4-4.5)
Lab ID: 92521577001 Collected:
02/09/21 14:10
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
3040 mg/kg 66.3
30.5 10
02/11/21 15:01
02/12/21 12:47
M1
C28)
Surrogates
n-Pentacosane (S)
92 % 32-130
10
02/11/21 15:01
02/12/21 12:47
629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
19.1 mg/kg 12.4
2.4 1
02/11/21 13:54
02/12/21 00:25
Surrogates
4-Bromofluorobenzene (S)
121 % 66-131
1
02/11/21 13:54
02/12/21 00:25
460-00-4
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Benzene
ND ug/kg 7.7
3.1 1
02/11/21 11:36
02/11/21 14:53
71-43-2
Ethylbenzene
ND ug/kg 7.7
3.6 1
02/11/21 11:36
02/11/21 14:53
100-41-4
Toluene
ND ug/kg 7.7
2.2 1
02/11/21 11:36
02/11/21 14:53
108-88-3
Xylene (Total)
34.2 ug/kg 15.4
4.4 1
02/11/21 11:36
02/11/21 14:53
1330-20-7
Surrogates
Toluene-d8 (S)
101 % 70-130
1
02/11/21 11:36
02/11/21 14:53
2037-26-5
4-Bromofluorobenzene (S)
125 % 69-134
1
02/11/21 11:36
02/11/21 14:53
460-00-4
1,2-Dichloroethane-d4 (S)
104 % 70-130
1
02/11/21 11:36
02/11/21 14:53
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
24.6 % 0.10
0.10 1
02/11/21 14:12
N2
Sample: #3 SS (4-4.5)
Lab ID: 92521577002 Collected:
02/09/21 14:15
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
2040 mg/kg 64.3
29.6 10
02/11/21 15:01
02/12/21 13:11
C28)
Surrogates
n-Pentacosane (S)
0 % 32-130
10
02/11/21 15:01
02/12/21 13:11
629-99-2 S4
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
25.3 mg/kg 10.8
2.1 1
02/12/21 11:17
02/13/21 00:21
Surrogates
4-Bromofluorobenzene (S)
110 % 66-131
1
02/12/21 11:17
02/13/21 00:21
460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #3 SS (4-4.5)
Lab ID: 92521577002 Collected:
02/09/21 14:15
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Benzene
ND ug/kg 7.8
3.1 1
02/11/21 11:36
02/11/21 15:11
71-43-2
Ethylbenzene
ND ug/kg 7.8
3.6 1
02/11/21 11:36
02/11/21 15:11
100-41-4
Toluene
ND ug/kg 7.8
2.2 1
02/11/21 11:36
02/11/21 15:11
108-88-3
Xylene (Total)
ND ug/kg 15.6
4.4 1
02/11/21 11:36
02/11/21 15:11
1330-20-7
Surrogates
Toluene-d8 (S)
96 % 70-130
1
02/11/21 11:36
02/11/21 15:11
2037-26-5
4-Bromofluorobenzene (S)
132 % 69-134
1
02/11/21 11:36
02/11/21 15:11
460-00-4
1,2-Dichloroethane-d4 (S)
102 % 70-130
1
02/11/21 11:36
02/11/21 15:11
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
21.7 % 0.10
0.10 1
02/11/21 14:13
N2
Sample: #2 NS (4-4.5) Lab ID: 92521577003 Collected: 02/09/21 14:20 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
10500 mg/kg 332
153 50
02/11/21 15:01
02/15/21 10:16
C28)
Surrogates
n-Pentacosane (S)
0 % 32-130
50
02/11/21 15:01
02/15/21 10:16
629-99-2 S4
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
75.0 mg/kg 11.2
2.1 1
02/12/21 11:17
02/13/21 01:45
Surrogates
4-Bromofluorobenzene (S)
141 % 66-131
1
02/12/21 11:17
02/13/21 01:45
460-00-4 S2
8260D/5035AI5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Benzene
ND ug/kg 9.4
3.7 1
02/11/21 11:36
02/11/21 15:29
71-43-2
Ethylbenzene
ND ug/kg 9.4
4.4 1
02/11/21 11:36
02/11/21 15:29
100-41-4
Toluene
ND ug/kg 9.4
2.7 1
02/11/21 11:36
02/11/21 15:29
108-88-3
Xylene (Total)
528 ug/kg 18.8
5.4 1
02/11/21 11:36
02/11/21 15:29
1330-20-7
Surrogates
Toluene-d8 (S)
97 % 70-130
1
02/11/21 11:36
02/11/21 15:29
2037-26-5
4-Bromofluorobenzene (S)
208 % 69-134
1
02/11/21 11:36
02/11/21 15:29
460-00-4 S5
1,2-Dichloroethane-d4 (S)
104 % 70-130
1
02/11/21 11:36
02/11/21 15:29
17060-07-0
Date: 02/24/2021 01:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 NS (4-4.5) Lab ID: 92521577003 Collected: 02/09/21 14:20 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture 24.6 % 0.10 0.10 1 02/11/21 14:13 N2
Sample: #2 SS (4-4.5) Lab ID: 92521577004 Collected: 02/09/21 14:25 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
C28)
Surrogates
n-Pentacosane(S)
Gasoline Range Organics
Gas Range Organics (C6-C10)
Surrogates
4-Bromofluorobenzene (S)
8260D/5035AI5030B Volatiles
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/24/2021 01:57 PM
4720 mg/kg 165
75.9
25
02/11/2115:01
02/15/2110:40
0 % 32-130
25
02/11/2115:01
02/15/2110:40
629-99-2 S4
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
4.9J mg/kg 10.6
2.0
1
02/12/2111:17
02/13/2103:10
98 % 66-131
1
02/12/21 11:17
02/13/2103:10
460-00-4
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND ug/kg 7.7
3.1
1
02/11/2111:36
02/11/2115:47
71-43-2
ND ug/kg 7.7
3.6
1
02/11/2111:36
02/11/2115:47
100-41-4
ND ug/kg 7.7
2.2
1
02/11/2111:36
02/11/2115:47
108-88-3
ND ug/kg 15.3
4.4
1
02/11/2111:36
02/11/2115:47
1330-20-7
102 % 70-130
1
02/11/2111:36
02/11/2115:47
2037-26-5
111 % 69-134
1
02/11/2111:36
02/11/2115:47
460-00-4
104 % 70-130
1
02/11/2111:36
02/11/2115:47
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
23.5 % 0.10
0.10
1
02/11/2114:13
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #1 NS (5.5) Lab ID: 92521577005 Collected: 02/10/21 09:45 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)
Surrogates
n-Pentacosane(S)
Gasoline Range Organics
Gas Range Organics (C6-C10)
Surrogates
4-Bromofluorobenzene (S)
8260D/5035A/5030B Volatiles
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND mg/kg 6.5 3.0 1 02/11/21 15:01 02/12/21 16:34
78 % 32-130 1 02/11/21 15:01 02/12/21 16:34 629-99-2
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
5.8J mg/kg 11.9 2.3 1 02/12/21 11:17 02/13/2104:34
100
%
66-131
1
02/12/21 11:17
02/13/2104:34
460-00-4
Analytical
Method: EPA 8260D Preparation Method:
EPA
5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
7.0
2.8
1
02/11/2111:36
02/11/2116:05
71-43-2
ND
ug/kg
7.0
3.3
1
02/11/2111:36
02/11/2116:05
100-41-4
ND
ug/kg
7.0
2.0
1
02/11/2111:36
02/11/2116:05
108-88-3
ND
ug/kg
14.1
4.0
1
02/11/2111:36
02/11/2116:05
1330-20-7
97
%
70-130
1
02/11/2111:36
02/11/2116:05
2037-26-5
98
%
69-134
1
02/11/2111:36
02/11/2116:05
460-00-4
102
%
70-130
1
02/11/2111:36
02/11/2116:05
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
22.6 % 0.10 0.10 1 02/11/2114:13
N2
Sample: #1 SS (5.5) Lab ID: 92521577006 Collected: 02/10/21 09:50 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
ND mg/kg 7.0 3.2 1 02/11/21 15:01 02/12/21 16:34
C28)
Surrogates
n-Pentacosane (S)
84 % 32-130 1 02/11/21 15:01 02/12/21 16:34 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
ND mg/kg 14.1 2.7 1 02/12/21 11:17 02/12/21 12:40
Surrogates
4-Bromofluorobenzene (S)
83 % 66-131 1 02/12/21 11:17 02/12/21 12:40 460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM
without the written consent of Pace Analytical Services, LLC.
Page 9 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #1 SS (5.5) Lab ID: 92521577006 Collected: 02/10/21 09:50 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
9.7
3.9
1
02/11/2111:36
02/11/2116:23
71-43-2
ND
ug/kg
9.7
4.5
1
02/11/2111:36
02/11/2116:23
100-41-4
ND
ug/kg
9.7
2.7
1
02/11/2111:36
02/11/2116:23
108-88-3
ND
ug/kg
19.4
5.5
1
02/11/2111:36
02/11/2116:23
1330-20-7
101
%
70-130
1
02/11/2111:36
02/11/2116:23
2037-26-5
101
%
69-134
1
02/11/2111:36
02/11/2116:23
460-00-4
105
%
70-130
1
02/11/2111:36
02/11/2116:23
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
28.8 % 0.10 0.10 1 02/11/2114:13
N2
Sample: #2 NW (6.5-7) Lab ID: 92521577007 Collected: 02/10/21 17:25 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services
- Charlotte
Aliphatic (C09-C18)
ND
mg/kg
12.5
12.5
1
02/15/21 11:54
02/16/21 21:36
Aliphatic (C19-C36)
ND
mg/kg
12.5
12.5
1
02/15/21 11:54
02/16/21 21:36
Aromatic (C11-C22)
ND
mg/kg
12.5
12.5
1
02/15/21 11:54
02/16/21 21:36
Surrogates
1-Chlorooctadecane (S)
44
%
40-140
1
02/15/21 11:54
02/16/21 21:36
3386-33-2
o-Terphenyl (S)
64
%
40-140
1
02/15/21 11:54
02/16/21 21:36
84-15-1
2-Fluorobiphenyl (S)
97
%
40-140
1
02/15/21 11:54
02/16/21 21:36
321-60-8
2-Bromonaphthalene (S)
101
%
40-140
1
02/15/21 11:54
02/16/21 21:36
580-13-2
MADEPV
Analytical
Method: MADEP VPH Preparation Method:
MADEPV
Pace National - Mt. Juliet
Aliphatic (C05-CO8)
17.9J
mg/kg
43.7
14.5
6
02/10/21 17:25
02/21/21 22:31
Aliphatic (C09-C12)
304
mg/kg
43.7
14.5
6
02/10/21 17:25
02/21/21 22:31
Aromatic (C09-C10),Unadjusted
328
mg/kg
43.7
14.5
6
02/10/21 17:25
02/21/21 22:31
TPHC9C10A
Total VPH
649
mg/kg
43.7
14.5
6
02/10/21 17:25
02/21/21 22:31
VPH
Surrogates
2,5-Dibromotoluene (FID)
106
%
70.0-130
6
02/10/21 17:25
02/21/21 22:31
615-59-8FID
2,5-Dibromotoluene (PID)
117
%
70.0-130
6
02/10/21 17:25
02/21/21 22:31
615-59-8PID
8270E MSSV Microwave
Analytical
Method: EPA 8270E
Preparation Method: EPA 3546
Pace Analytical Services
- Charlotte
Acenaphthene
4970
ug/kg
4120
1060
10
02/15/21 10:39
02/17/2109:44
83-32-9
Acenaphthylene
ND
ug/kg
4120
974
10
02/15/2110:39
02/17/2109:44
208-96-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
N2
N2
N2
J
Page 10 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 NW (6.5-7) Lab ID: 92521577007 Collected: 02/10/21 17:25 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services
- Charlotte
Aniline
ND
ug/kg
4120
924
10
02/15/21 10:39
02/17/21 09:44
62-53-3
Anthracene
ND
ug/kg
4120
1070
10
02/15/21 10:39
02/17/21 09:44
120-12-7
Benzo(a)anthracene
ND
ug/kg
4120
1310
10
02/15/21 10:39
02/17/21 09:44
56-55-3
Benzo(a)pyrene
ND
ug/kg
4120
1780
10
02/15/21 10:39
02/17/21 09:44
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
4120
1660
10
02/15/21 10:39
02/17/21 09:44
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
4120
1610
10
02/15/21 10:39
02/17/21 09:44
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
4120
1730
10
02/15/21 10:39
02/17/21 09:44
207-08-9
Benzoic Acid
ND
ug/kg
20600
4440
10
02/15/21 10:39
02/17/21 09:44
65-85-0
Benzyl alcohol
ND
ug/kg
8230
2180
10
02/15/21 10:39
02/17/21 09:44
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
4120
1080
10
02/15/21 10:39
02/17/21 09:44
101-55-3
Butylbenzylphthalate
ND
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 09:44
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
8230
2510
10
02/15/21 10:39
02/17/21 09:44
59-50-7
4-Chloroaniline
ND
ug/kg
8230
2520
10
02/15/21 10:39
02/17/21 09:44
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 09:44
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
4120
874
10
02/15/21 10:39
02/17/21 09:44
111-44-4
2-Chloronaphthalene
ND
ug/kg
4120
917
10
02/15/21 10:39
02/17/21 09:44
91-58-7
2-Chlorophenol
ND
ug/kg
4120
958
10
02/15/21 10:39
02/17/21 09:44
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
4120
1070
10
02/15/21 10:39
02/17/21 09:44
7005-72-3
Chrysene
ND
ug/kg
4120
1200
10
02/15/21 10:39
02/17/21 09:44
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
4120
1650
10
02/15/21 10:39
02/17/21 09:44
53-70-3
Dibenzofuran
ND
ug/kg
4120
1030
10
02/15/21 10:39
02/17/21 09:44
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
4120
891
10
02/15/21 10:39
02/17/21 09:44
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
4120
927
10
02/15/21 10:39
02/17/21 09:44
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
4120
906
10
02/15/21 10:39
02/17/21 09:44
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
8230
2870
10
02/15/21 10:39
02/17/21 09:44
91-94-1
2,4-Dichlorophenol
ND
ug/kg
4120
1360
10
02/15/21 10:39
02/17/21 09:44
120-83-2
Diethylphthalate
ND
ug/kg
4120
893
10
02/15/21 10:39
02/17/21 09:44
84-66-2
2,4-Dimethylphenol
ND
ug/kg
4120
1030
10
02/15/21 10:39
02/17/21 09:44
105-67-9
Dimethylphthalate
ND
ug/kg
4120
931
10
02/15/21 10:39
02/17/21 09:44
131-11-3
Di-n-butylphthalate
ND
ug/kg
4120
1020
10
02/15/21 10:39
02/17/21 09:44
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
8230
6640
10
02/15/21 10:39
02/17/21 09:44
534-52-1
2,4-Dinitrophenol
ND
ug/kg
20600
13100
10
02/15/21 10:39
02/17/21 09:44
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
4120
1090
10
02/15/21 10:39
02/17/21 09:44
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
4120
1080
10
02/15/21 10:39
02/17/21 09:44
606-20-2
Di-n-octylphthalate
ND
ug/kg
4120
2350
10
02/15/21 10:39
02/17/21 09:44
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
4120
1350
10
02/15/21 10:39
02/17/21 09:44
117-81-7
Fluoranthene
ND
ug/kg
4120
1240
10
02/15/21 10:39
02/17/21 09:44
206-44-0
Fluorene
2280J
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 09:44
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
4120
1000
10
02/15/21 10:39
02/17/21 09:44
87-68-3
Hexachlorobenzene
ND
ug/kg
4120
1050
10
02/15/21 10:39
02/17/21 09:44
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
4120
1650
10
02/15/21 10:39
02/17/21 09:44
77-47-4
Hexachloroethane
ND
ug/kg
4120
938
10
02/15/21 10:39
02/17/21 09:44
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
4120
1880
10
02/15/21 10:39
02/17/21 09:44
193-39-5
Isophorone
ND
ug/kg
4120
894
10
02/15/21 10:39
02/17/21 09:44
78-59-1
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 NW (6.5-7)
Lab ID:
92521577007
Collected:
02/10/21
17:25
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are
adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services
- Charlotte
1-Methylnaphthalene
27500
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 09:44
90-12-0
2-Methylnaphthalene
39100
ug/kg
4120
1050
10
02/15/21 10:39
02/17/21 09:44
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
4120
912
10
02/15/21 10:39
02/17/21 09:44
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
4120
1040
10
02/15/21 10:39
02/17/21 09:44
15831-10-4
Naphthalene
4520
ug/kg
4120
985
10
02/15/21 10:39
02/17/21 09:44
91-20-3
2-Nitroaniline
ND
ug/kg
20600
2070
10
02/15/21 10:39
02/17/21 09:44
88-74-4
3-Nitroaniline
ND
ug/kg
20600
2180
10
02/15/21 10:39
02/17/21 09:44
99-09-2
IL
4-Nitroaniline
ND
ug/kg
8230
2030
10
02/15/21 10:39
02/17/21 09:44
100-01-6
Nitrobenzene
ND
ug/kg
4120
983
10
02/15/21 10:39
02/17/21 09:44
98-95-3
2-Nitrophenol
ND
ug/kg
4120
1270
10
02/15/21 10:39
02/17/21 09:44
88-75-5
4-Nitrophenol
ND
ug/kg
20600
6560
10
02/15/21 10:39
02/17/21 09:44
100-02-7
v1
N-Nitrosodimethylamine
ND
ug/kg
4120
1160
10
02/15/21 10:39
02/17/21 09:44
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
4120
1150
10
02/15/21 10:39
02/17/21 09:44
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
4120
1050
10
02/15/21 10:39
02/17/21 09:44
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
4120
1140
10
02/15/21 10:39
02/17/21 09:44
108-60-1
Pentachlorophenol
ND
ug/kg
8230
1880
10
02/15/21 10:39
02/17/21 09:44
87-86-5
Phenanthrene
9250
ug/kg
4120
1040
10
02/15/21 10:39
02/17/21 09:44
85-01-8
Phenol
ND
ug/kg
4120
983
10
02/15/21 10:39
02/17/21 09:44
108-95-2
Pyrene
ND
ug/kg
4120
1130
10
02/15/21 10:39
02/17/21 09:44
129-00-0
Pyridine
ND
ug/kg
4120
1040
10
02/15/21 10:39
02/17/21 09:44
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
4120
943
10
02/15/21 10:39
02/17/21 09:44
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
4120
1070
10
02/15/21 10:39
02/17/21 09:44
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
4120
1030
10
02/15/21 10:39
02/17/21 09:44
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
21-130
10
02/15/21 10:39
02/17/21 09:44
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
19-130
10
02/15/21 10:39
02/17/21 09:44
321-60-8
S4
Terphenyl-d14 (S)
0
%
15-130
10
02/15/21 10:39
02/17/21 09:44
1718-51-0
S4
Phenol-d6 (S)
0
%
18-130
10
02/15/21 10:39
02/17/21 09:44
13127-88-3
S4
2-Fluorophenol (S)
0
%
18-130
10
02/15/21 10:39
02/17/21 09:44
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
18-130
10
02/15/21 10:39
02/17/21 09:44
118-79-6
S4
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D
Preparation Method: EPA 5035A/5030B
Pace Analytical Services
- Charlotte
Acetone
ND
ug/kg
671
215
4
02/11/2111:36
02/11/2117:18
67-64-1
Benzene
ND
ug/kg
33.5
13.4
4
02/11/2111:36
02/11/2117:18
71-43-2
Bromobenzene
ND
ug/kg
33.5
10.9
4
02/11/2111:36
02/11/2117:18
108-86-1
Bromochloromethane
ND
ug/kg
33.5
9.9
4
02/11/2111:36
02/11/2117:18
74-97-5
Bromodichloromethane
ND
ug/kg
33.5
12.9
4
02/11/2111:36
02/11/2117:18
75-27-4
Bromoform
ND
ug/kg
33.5
11.8
4
02/11/2111:36
02/11/2117:18
75-25-2
Bromomethane
ND
ug/kg
67.1
53.0
4
02/11/2111:36
02/11/2117:18
74-83-9
2-Butanone (MEK)
ND
ug/kg
671
161
4
02/11/21 11:36
02/11/21 17:18
78-93-3
n-Butylbenzene
1680
ug/kg
33.5
15.8
4
02/11/2111:36
02/11/2117:18
104-51-8
sec-Butylbenzene
ND
ug/kg
33.5
14.8
4
02/11/2111:36
02/11/2117:18
135-98-8
tert-Butyl benzene
224
ug/kg
33.5
11.9
4
02/11/2111:36
02/11/2117:18
98-06-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 NW (6.5-7) Lab ID: 92521577007 Collected: 02/10/21 17:25 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Carbon tetrachloride
ND
ug/kg
33.5
12.5
4
02/11/21 11:36
02/11/21 17:18
56-23-5
Chlorobenzene
ND
ug/kg
33.5
6.4
4
02/11/21 11:36
02/11/21 17:18
108-90-7
Chloroethane
ND
ug/kg
67.1
25.9
4
02/11/21 11:36
02/11/21 17:18
75-00-3
Chloroform
ND
ug/kg
33.5
20.4
4
02/11/21 11:36
02/11/21 17:18
67-66-3
Chloromethane
ND
ug/kg
67.1
28.2
4
02/11/21 11:36
02/11/21 17:18
74-87-3
2-Chlorotoluene
ND
ug/kg
33.5
11.9
4
02/11/21 11:36
02/11/21 17:18
95-49-8
4-Chlorotoluene
ND
ug/kg
33.5
5.9
4
02/11/21 11:36
02/11/21 17:18
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
33.5
13.0
4
02/11/21 11:36
02/11/21 17:18
96-12-8
Dibromochloromethane
ND
ug/kg
33.5
18.9
4
02/11/21 11:36
02/11/21 17:18
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
33.5
14.8
4
02/11/21 11:36
02/11/21 17:18
106-93-4
Dibromomethane
ND
ug/kg
33.5
7.2
4
02/11/21 11:36
02/11/21 17:18
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
33.5
12.1
4
02/11/21 11:36
02/11/21 17:18
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
33.5
10.4
4
02/11/21 11:36
02/11/21 17:18
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
33.5
8.7
4
02/11/21 11:36
02/11/21 17:18
106-46-7
Dichlorodifluoromethane
ND
ug/kg
67.1
14.6
4
02/11/21 11:36
02/11/21 17:18
75-71-8
1,1-Dichloroethane
ND
ug/kg
33.5
13.8
4
02/11/21 11:36
02/11/21 17:18
75-34-3
1,2-Dichloroethane
ND
ug/kg
33.5
22.2
4
02/11/21 11:36
02/11/21 17:18
107-06-2
1,1-Dichloroethene
ND
ug/kg
33.5
13.8
4
02/11/21 11:36
02/11/21 17:18
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
33.5
11.5
4
02/11/21 11:36
02/11/21 17:18
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
33.5
11.7
4
02/11/21 11:36
02/11/21 17:18
156-60-5
1,2-Dichloropropane
ND
ug/kg
33.5
10.1
4
02/11/21 11:36
02/11/21 17:18
78-87-5
1,3-Dichloropropane
ND
ug/kg
33.5
10.5
4
02/11/21 11:36
02/11/21 17:18
142-28-9
2,2-Dichloropropane
ND
ug/kg
33.5
10.9
4
02/11/21 11:36
02/11/21 17:18
594-20-7
1,1-Dichloropropene
ND
ug/kg
33.5
16.1
4
02/11/21 11:36
02/11/21 17:18
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
33.5
9.1
4
02/11/21 11:36
02/11/21 17:18
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
33.5
11.5
4
02/11/21 11:36
02/11/21 17:18
10061-02-6
Diisopropyl ether
ND
ug/kg
33.5
9.1
4
02/11/21 11:36
02/11/21 17:18
108-20-3
Ethylbenzene
287
ug/kg
33.5
15.6
4
02/11/21 11:36
02/11/21 17:18
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
67.1
54.9
4
02/11/21 11:36
02/11/21 17:18
87-68-3
2-Hexanone
ND
ug/kg
335
32.3
4
02/11/21 11:36
02/11/21 17:18
591-78-6
Isopropylbenzene (Cumene)
326
ug/kg
33.5
11.4
4
02/11/21 11:36
02/11/21 17:18
98-82-8
p-Isopropyltoluene
6550
ug/kg
33.5
16.5
4
02/11/21 11:36
02/11/21 17:18
99-87-6
Methylene Chloride
ND
ug/kg
134
91.9
4
02/11/21 11:36
02/11/21 17:18
75-09-2
4-Methyl-2-pentanone (MIBK)
371
ug/kg
335
32.3
4
02/11/21 11:36
02/11/21 17:18
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
33.5
12.5
4
02/11/21 11:36
02/11/21 17:18
1634-04-4
Naphthalene
7760
ug/kg
33.5
17.6
4
02/11/21 11:36
02/11/21 17:18
91-20-3
n-Propylbenzene
595
ug/kg
33.5
11.9
4
02/11/21 11:36
02/11/21 17:18
103-65-1
Styrene
ND
ug/kg
33.5
8.9
4
02/11/21 11:36
02/11/21 17:18
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
33.5
12.9
4
02/11/21 11:36
02/11/21 17:18
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
33.5
8.9
4
02/11/21 11:36
02/11/21 17:18
79-34-5
Tetrachloroethene
ND
ug/kg
33.5
10.6
4
02/11/21 11:36
02/11/21 17:18
127-18-4
Toluene
ND
ug/kg
33.5
9.5
4
02/11/21 11:36
02/11/21 17:18
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
33.5
27.1
4
02/11/21 11:36
02/11/21 17:18
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
33.5
28.2
4
02/11/21 11:36
02/11/21 17:18
120-82-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 NW (6.5-7) Lab ID: 92521577007 Collected: 02/10/21 17:25 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
33.5
17.4
4
02/11/2111:36
02/11/2117:18
71-55-6
ND
ug/kg
33.5
11.1
4
02/11/2111:36
02/11/2117:18
79-00-5
ND
ug/kg
33.5
8.7
4
02/11/2111:36
02/11/2117:18
79-01-6
ND
ug/kg
33.5
18.5
4
02/11/2111:36
02/11/2117:18
75-69-4
ND
ug/kg
33.5
17.0
4
02/11/2111:36
02/11/2117:18
96-18-4
ND
ug/kg
33.5
9.2
4
02/11/2111:36
02/11/2117:18
95-63-6
4980
ug/kg
33.5
11.3
4
02/11/2111:36
02/11/2117:18
108-67-8
ND
ug/kg
335
24.4
4
02/11/2111:36
02/11/2117:18
108-05-4
ND
ug/kg
67.1
17.0
4
02/11/2111:36
02/11/2117:18
75-01-4
1790
ug/kg
67.1
19.1
4
02/11/2111:36
02/11/2117:18
1330-20-7
ND
ug/kg
67.1
22.9
4
02/11/2111:36
02/11/2117:18
179601-23-1
1790
ug/kg
33.5
14.8
4
02/11/2111:36
02/11/2117:18
95-47-6
101
%
70-130
4
02/11/2111:36
02/11/2117:18
2037-26-5 D3
115
%
69-134
4
02/11/2111:36
02/11/2117:18
460-00-4
103
%
70-130
4
02/11/2111:36
02/11/2117:18
17060-07-0
Analytical
Method: SW-846
Pace Analytical Services - Charlotte
19.6
%
0.10
0.10
1
02/11/2114:13
N2
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 80.1 % 1 02/22/21 11:28 02/22/21 11:36
Sample: #2 SW (6.5-7) Lab ID: 92521577008 Collected: 02/10/21 17:37 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
1-Chlorooctadecane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
Date: 02/24/2021 01:57 PM
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
4890
mg/kg
2560
2560 200
02/15/21 11:54
02/18/2109:08
N2
ND
mg/kg
2560
2560 200
02/15/21 11:54
02/18/2109:08
N2
2790
mg/kg
512
512 40
02/15/21 11:54
02/18/2109:08
N2
0
%
40-140
200
02/15/21 11:54
02/18/2109:08
3386-33-2
S4
0
%
40-140
40
02/15/21 11:54
02/18/2109:08
84-15-1
S4
0
%
40-140
40
02/15/21 11:54
02/18/2109:08
321-60-8
S4
0
%
40-140
40
02/15/21 11:54
02/18/2109:08
580-13-2
S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 SW (6.5-7)
Lab ID:
92521577008
Collected:
02/10/21 17:37
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are
adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
MADEPV
Analytical Method: MADEP VPH Preparation Method:
MADEPV
Pace National - Mt. Juliet
Aliphatic (C05-CO8)
10.6
mg/kg
8.26
2.75
1.05
02/10/21 17:37
02/14/21 22:05
B
Aliphatic (C09-C12)
29.3
mg/kg
8.26
2.75
1.05
02/10/21 17:37
02/14/21 22:05
Aromatic (C09-C10),Unadjusted
14.6
mg/kg
8.26
2.75
1.05
02/10/21 17:37
02/14/21 22:05
TPHC9C10A
Total VPH
54.4
mg/kg
8.26
2.75
1.05
02/10/21 17:37
02/14/21 22:05
VPH
Surrogates
2,5-Dibromotoluene (FID)
110
%
70.0-130
1.05
02/10/21 17:37
02/14/21 22:05
615-59-8FID
2,5-Dibromotoluene (PID)
84.6
%
70.0-130
1.05
02/10/21 17:37
02/14/21 22:05
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Pace Analytical Services
- Charlotte
Acenaphthene
ND
ug/kg
420
108
1
02/15/21 10:39
02/17/21 14:39
83-32-9
Acenaphthylene
ND
ug/kg
420
99.4
1
02/15/21 10:39
02/17/21 14:39
208-96-8
Aniline
ND
ug/kg
420
94.3
1
02/15/21 10:39
02/17/21 14:39
62-53-3
Anthracene
ND
ug/kg
420
109
1
02/15/21 10:39
02/17/21 14:39
120-12-7
Benzo(a)anthracene
ND
ug/kg
420
134
1
02/15/21 10:39
02/17/21 14:39
56-55-3
Benzo(a)pyrene
ND
ug/kg
420
182
1
02/15/21 10:39
02/17/21 14:39
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
420
169
1
02/15/21 10:39
02/17/21 14:39
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
420
164
1
02/15/21 10:39
02/17/21 14:39
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
420
177
1
02/15/21 10:39
02/17/21 14:39
207-08-9
Benzoic Acid
ND
ug/kg
2100
453
1
02/15/21 10:39
02/17/21 14:39
65-85-0
Benzyl alcohol
ND
ug/kg
840
223
1
02/15/21 10:39
02/17/21 14:39
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
420
110
1
02/15/21 10:39
02/17/21 14:39
101-55-3
Butylbenzylphthalate
ND
ug/kg
420
112
1
02/15/21 10:39
02/17/21 14:39
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
840
256
1
02/15/21 10:39
02/17/21 14:39
59-50-7
4-Chloroaniline
ND
ug/kg
840
257
1
02/15/21 10:39
02/17/21 14:39
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
420
112
1
02/15/21 10:39
02/17/21 14:39
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
420
89.2
1
02/15/21 10:39
02/17/21 14:39
111-44-4
2-Chloronaphthalene
ND
ug/kg
420
93.5
1
02/15/21 10:39
02/17/21 14:39
91-58-7
2-Chlorophenol
ND
ug/kg
420
97.7
1
02/15/21 10:39
02/17/21 14:39
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
420
109
1
02/15/21 10:39
02/17/21 14:39
7005-72-3
Chrysene
ND
ug/kg
420
122
1
02/15/21 10:39
02/17/21 14:39
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
420
168
1
02/15/21 10:39
02/17/21 14:39
53-70-3
Dibenzofuran
ND
ug/kg
420
105
1
02/15/21 10:39
02/17/21 14:39
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
420
90.8
1
02/15/21 10:39
02/17/21 14:39
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
420
94.5
1
02/15/21 10:39
02/17/21 14:39
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
420
92.4
1
02/15/21 10:39
02/17/21 14:39
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
840
293
1
02/15/21 10:39
02/17/21 14:39
91-94-1
2,4-Dichlorophenol
ND
ug/kg
420
139
1
02/15/21 10:39
02/17/21 14:39
120-83-2
Diethylphthalate
ND
ug/kg
420
91.1
1
02/15/21 10:39
02/17/21 14:39
84-66-2 v1
2,4-Dimethylphenol
ND
ug/kg
420
105
1
02/15/21 10:39
02/17/21 14:39
105-67-9
Dimethylphthalate
ND
ug/kg
420
94.9
1
02/15/21 10:39
02/17/21 14:39
131-11-3
Di-n-butylphthalate
ND
ug/kg
420
104
1
02/15/21 10:39
02/17/21 14:39
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
840
677
1
02/15/21 10:39
02/17/21 14:39
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2100
1340
1
02/15/21 10:39
02/17/21 14:39
51-28-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 SW (6.5-7) Lab ID: 92521577008 Collected: 02/10/21 17:37 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,4-Dinitrotoluene
ND
ug/kg
420
ill
1
02/15/21 10:39
02/17/21 14:39
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
420
110
1
02/15/21 10:39
02/17/21 14:39
606-20-2
Di-n-octylphthalate
ND
ug/kg
420
239
1
02/15/21 10:39
02/17/21 14:39
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
420
137
1
02/15/21 10:39
02/17/21 14:39
117-81-7
Fluoranthene
ND
ug/kg
420
127
1
02/15/21 10:39
02/17/21 14:39
206-44-0
Fluorene
ND
ug/kg
420
112
1
02/15/21 10:39
02/17/21 14:39
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
420
102
1
02/15/21 10:39
02/17/21 14:39
87-68-3
Hexachlorobenzene
ND
ug/kg
420
107
1
02/15/21 10:39
02/17/21 14:39
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
420
168
1
02/15/21 10:39
02/17/21 14:39
77-47-4
Hexachloroethane
ND
ug/kg
420
95.7
1
02/15/21 10:39
02/17/21 14:39
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
420
192
1
02/15/21 10:39
02/17/21 14:39
193-39-5
Isophorone
ND
ug/kg
420
91.2
1
02/15/21 10:39
02/17/21 14:39
78-59-1
1-Methylnaphthalene
ND
ug/kg
420
112
1
02/15/21 10:39
02/17/21 14:39
90-12-0
2-Methylnaphthalene
ND
ug/kg
420
107
1
02/15/21 10:39
02/17/21 14:39
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
420
93.0
1
02/15/21 10:39
02/17/21 14:39
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
420
106
1
02/15/21 10:39
02/17/21 14:39
15831-10-4
Naphthalene
ND
ug/kg
420
101
1
02/15/21 10:39
02/17/21 14:39
91-20-3
2-Nitroaniline
ND
ug/kg
2100
211
1
02/15/21 10:39
02/17/21 14:39
88-74-4
3-Nitroaniline
ND
ug/kg
2100
223
1
02/15/21 10:39
02/17/21 14:39
99-09-2
4-Nitroaniline
ND
ug/kg
840
207
1
02/15/21 10:39
02/17/21 14:39
100-01-6
Nitrobenzene
ND
ug/kg
420
100
1
02/15/21 10:39
02/17/21 14:39
98-95-3
2-Nitrophenol
ND
ug/kg
420
130
1
02/15/21 10:39
02/17/21 14:39
88-75-5
4-Nitrophenol
ND
ug/kg
2100
669
1
02/15/21 10:39
02/17/21 14:39
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
420
118
1
02/15/21 10:39
02/17/21 14:39
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
420
118
1
02/15/21 10:39
02/17/21 14:39
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
420
107
1
02/15/21 10:39
02/17/21 14:39
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
420
117
1
02/15/21 10:39
02/17/21 14:39
108-60-1
Pentachlorophenol
ND
ug/kg
840
192
1
02/15/21 10:39
02/17/21 14:39
87-86-5
Phenanthrene
ND
ug/kg
420
106
1
02/15/21 10:39
02/17/21 14:39
85-01-8
Phenol
ND
ug/kg
420
100
1
02/15/21 10:39
02/17/21 14:39
108-95-2
Pyrene
ND
ug/kg
420
116
1
02/15/21 10:39
02/17/21 14:39
129-00-0
Pyridine
ND
ug/kg
420
106
1
02/15/21 10:39
02/17/21 14:39
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
420
96.2
1
02/15/21 10:39
02/17/21 14:39
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
420
109
1
02/15/21 10:39
02/17/21 14:39
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
420
105
1
02/15/21 10:39
02/17/21 14:39
88-06-2
Surrogates
Nitrobenzene-d5 (S)
66
%
21-130
1
02/15/21 10:39
02/17/21 14:39
4165-60-0
2-Fluorobiphenyl (S)
62
%
19-130
1
02/15/21 10:39
02/17/21 14:39
321-60-8
Terphenyl-dl4 (S)
84
%
15-130
1
02/15/21 10:39
02/17/21 14:39
1718-51-0
Phenol-d6 (S)
54
%
18-130
1
02/15/21 10:39
02/17/21 14:39
13127-88-3
2-Fluorophenol (S)
55
%
18-130
1
02/15/21 10:39
02/17/21 14:39
367-12-4
2,4,6-Tribromophenol (S)
75
%
18-130
1
02/15/21 10:39
02/17/21 14:39
118-79-6
REPORT OF LABORATORY ANALYSIS
IL
vl
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 SW (6.5-7) Lab ID: 92521577008 Collected: 02/10/21 17:37 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
162
52.0
1
02/11/21 11:36
02/11/21 16:41
67-64-1
Benzene
ND
ug/kg
8.1
3.2
1
02/11/21 11:36
02/11/21 16:41
71-43-2
Bromobenzene
ND
ug/kg
8.1
2.6
1
02/11/21 11:36
02/11/21 16:41
108-86-1
Bromochloromethane
ND
ug/kg
8.1
2.4
1
02/11/21 11:36
02/11/21 16:41
74-97-5
Bromodichloromethane
ND
ug/kg
8.1
3.1
1
02/11/21 11:36
02/11/21 16:41
75-27-4
Bromoform
ND
ug/kg
8.1
2.8
1
02/11/21 11:36
02/11/21 16:41
75-25-2
Bromomethane
ND
ug/kg
16.2
12.8
1
02/11/21 11:36
02/11/21 16:41
74-83-9
2-Butanone (MEK)
ND
ug/kg
162
38.9
1
02/11/21 11:36
02/11/21 16:41
78-93-3
n-Butylbenzene
ND
ug/kg
8.1
3.8
1
02/11/21 11:36
02/11/21 16:41
104-51-8
sec-Butylbenzene
ND
ug/kg
8.1
3.6
1
02/11/21 11:36
02/11/21 16:41
135-98-8
tert-Butyl benzene
ND
ug/kg
8.1
2.9
1
02/11/21 11:36
02/11/21 16:41
98-06-6
Carbon tetrachloride
ND
ug/kg
8.1
3.0
1
02/11/21 11:36
02/11/21 16:41
56-23-5
Chlorobenzene
ND
ug/kg
8.1
1.6
1
02/11/21 11:36
02/11/21 16:41
108-90-7
Chloroethane
ND
ug/kg
16.2
6.2
1
02/11/21 11:36
02/11/21 16:41
75-00-3
Chloroform
ND
ug/kg
8.1
4.9
1
02/11/21 11:36
02/11/21 16:41
67-66-3
Chloromethane
ND
ug/kg
16.2
6.8
1
02/11/21 11:36
02/11/21 16:41
74-87-3
2-Chlorotoluene
ND
ug/kg
8.1
2.9
1
02/11/21 11:36
02/11/21 16:41
95-49-8
4-Chlorotoluene
ND
ug/kg
8.1
1.4
1
02/11/21 11:36
02/11/21 16:41
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
8.1
3.1
1
02/11/21 11:36
02/11/21 16:41
96-12-8
Dibromochloromethane
ND
ug/kg
8.1
4.5
1
02/11/21 11:36
02/11/21 16:41
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
8.1
3.6
1
02/11/21 11:36
02/11/21 16:41
106-93-4
Dibromomethane
ND
ug/kg
8.1
1.7
1
02/11/21 11:36
02/11/21 16:41
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
8.1
2.9
1
02/11/21 11:36
02/11/21 16:41
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
8.1
2.5
1
02/11/21 11:36
02/11/21 16:41
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
8.1
2.1
1
02/11/21 11:36
02/11/21 16:41
106-46-7
Dichlorodifluoromethane
ND
ug/kg
16.2
3.5
1
02/11/21 11:36
02/11/21 16:41
75-71-8
1,1-Dichloroethane
ND
ug/kg
8.1
3.3
1
02/11/21 11:36
02/11/21 16:41
75-34-3
1,2-Dichloroethane
ND
ug/kg
8.1
5.4
1
02/11/21 11:36
02/11/21 16:41
107-06-2
1,1-Dichloroethene
ND
ug/kg
8.1
3.3
1
02/11/21 11:36
02/11/21 16:41
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
8.1
2.8
1
02/11/21 11:36
02/11/21 16:41
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
8.1
2.8
1
02/11/21 11:36
02/11/21 16:41
156-60-5
1,2-Dichloropropane
ND
ug/kg
8.1
2.4
1
02/11/21 11:36
02/11/21 16:41
78-87-5
1,3-Dichloropropane
ND
ug/kg
8.1
2.5
1
02/11/21 11:36
02/11/21 16:41
142-28-9
2,2-Dichloropropane
ND
ug/kg
8.1
2.6
1
02/11/21 11:36
02/11/21 16:41
594-20-7
1,1-Dichloropropene
ND
ug/kg
8.1
3.9
1
02/11/21 11:36
02/11/21 16:41
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
8.1
2.2
1
02/11/21 11:36
02/11/21 16:41
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
8.1
2.8
1
02/11/21 11:36
02/11/21 16:41
10061-02-6
Diisopropyl ether
ND
ug/kg
8.1
2.2
1
02/11/21 11:36
02/11/21 16:41
108-20-3
Ethylbenzene
ND
ug/kg
8.1
3.8
1
02/11/21 11:36
02/11/21 16:41
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
16.2
13.2
1
02/11/21 11:36
02/11/21 16:41
87-68-3
2-Hexanone
ND
ug/kg
81.0
7.8
1
02/11/21 11:36
02/11/21 16:41
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
8.1
2.8
1
02/11/21 11:36
02/11/21 16:41
98-82-8
p-Isopropyltoluene
ND
ug/kg
8.1
4.0
1
02/11/21 11:36
02/11/21 16:41
99-87-6
Methylene Chloride
ND
ug/kg
32.4
22.2
1
02/11/21 11:36
02/11/21 16:41
75-09-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 SW (6.5-7) Lab ID: 92521577008 Collected: 02/10/21 17:37 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
81.0
7.8
1
02/11/2111:36
02/11/2116:41
108-10-1
ND
ug/kg
8.1
3.0
1
02/11/2111:36
02/11/2116:41
1634-04-4
ND
ug/kg
8.1
4.3
1
02/11/2111:36
02/11/2116:41
91-20-3
ND
ug/kg
8.1
2.9
1
02/11/2111:36
02/11/2116:41
103-65-1
ND
ug/kg
8.1
2.1
1
02/11/2111:36
02/11/2116:41
100-42-5
ND
ug/kg
8.1
3.1
1
02/11/2111:36
02/11/2116:41
630-20-6
ND
ug/kg
8.1
2.1
1
02/11/2111:36
02/11/2116:41
79-34-5
ND
ug/kg
8.1
2.6
1
02/11/2111:36
02/11/2116:41
127-18-4
ND
ug/kg
8.1
2.3
1
02/11/2111:36
02/11/2116:41
108-88-3
ND
ug/kg
8.1
6.5
1
02/11/2111:36
02/11/2116:41
87-61-6
ND
ug/kg
8.1
6.8
1
02/11/2111:36
02/11/2116:41
120-82-1
ND
ug/kg
8.1
4.2
1
02/11/2111:36
02/11/2116:41
71-55-6
ND
ug/kg
8.1
2.7
1
02/11/2111:36
02/11/2116:41
79-00-5
ND
ug/kg
8.1
2.1
1
02/11/2111:36
02/11/2116:41
79-01-6
ND
ug/kg
8.1
4.5
1
02/11/2111:36
02/11/2116:41
75-69-4
ND
ug/kg
8.1
4.1
1
02/11/2111:36
02/11/2116:41
96-18-4
ND
ug/kg
8.1
2.2
1
02/11/2111:36
02/11/2116:41
95-63-6
ND
ug/kg
8.1
2.7
1
02/11/2111:36
02/11/2116:41
108-67-8
ND
ug/kg
81.0
5.9
1
02/11/2111:36
02/11/2116:41
108-05-4
ND
ug/kg
16.2
4.1
1
02/11/2111:36
02/11/2116:41
75-01-4
ND
ug/kg
16.2
4.6
1
02/11/2111:36
02/11/2116:41
1330-20-7
ND
ug/kg
16.2
5.5
1
02/11/2111:36
02/11/2116:41
179601-23-1
ND
ug/kg
8.1
3.6
1
02/11/2111:36
02/11/2116:41
95-47-6
102
%
70-130
1
02/11/2111:36
02/11/2116:41
2037-26-5
97
%
69-134
1
02/11/2111:36
02/11/2116:41
460-00-4
102
%
70-130
1
02/11/2111:36
02/11/2116:41
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
22.7 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
77.3 %
02/11/21 14:13
1 02/22/2111:28 02/22/2111:36
REPORT OF LABORATORY ANALYSIS
N2
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 EW (6.5-7)
Lab ID:
92521577009
Collected:
02/10/21
17:05
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are
adjusted for percent moisture, sample size and any dilutions.
Comments: • Volatile Petroleum Hydrocarbons by
Method MADEPV
- Surrogate
failure due to matrix interference.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services
- Charlotte
Aliphatic (C09-C18)
ND
mg/kg
12.8
12.8
1
02/15/21 11:54
02/16/21 22:30
N2
Aliphatic (C19-C36)
ND
mg/kg
12.8
12.8
1
02/15/21 11:54
02/16/21 22:30
N2
Aromatic (C11-C22)
ND
mg/kg
12.8
12.8
1
02/15/21 11:54
02/16/21 22:30
N2
Surrogates
1-Chlorooctadecane (S)
50
%
40-140
1
02/15/21 11:54
02/16/21 22:30
3386-33-2
o-Terphenyl (S)
60
%
40-140
1
02/15/21 11:54
02/16/21 22:30
84-15-1
2-Fluorobiphenyl (S)
93
%
40-140
1
02/15/21 11:54
02/16/21 22:30
321-60-8
2-Bromonaphthalene (S)
96
%
40-140
1
02/15/21 11:54
02/16/21 22:30
580-13-2
MADEPV
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
Aliphatic (C05-CO8)
7.76
mg/kg
7.59
2.54
1
02/10/21 17:15
02/14/21 22:38
B
Aliphatic (C09-C12)
18.8
mg/kg
7.59
2.54
1
02/10/21 17:15
02/14/21 22:38
Aromatic (C09-C10),Unadjusted
26.3
mg/kg
7.59
2.54
1
02/10/21 17:15
02/14/21 22:38
TPHC9C10A
Total VPH
52.9
mg/kg
7.59
2.54
1
02/10/21 17:15
02/14/21 22:38
VPH
Surrogates
2,5-Dibromotoluene (FID)
139
%
70.0-130
1
02/10/21 17:15
02/14/21 22:38
615-59-8FID
ST
2,5-Dibromotoluene (PID)
116
%
70.0-130
1
02/10/21 17:15
02/14/21 22:38
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method: EPA 3546
Pace Analytical Services
- Charlotte
Acenaphthene
ND
ug/kg
423
109
1
02/15/21 10:39
02/16/21 11:36
83-32-9
Acenaphthylene
ND
ug/kg
423
100
1
02/15/21 10:39
02/16/21 11:36
208-96-8
Aniline
ND
ug/kg
423
95.0
1
02/15/21 10:39
02/16/21 11:36
62-53-3
Anthracene
ND
ug/kg
423
110
1
02/15/21 10:39
02/16/21 11:36
120-12-7
Benzo(a)anthracene
ND
ug/kg
423
135
1
02/15/21 10:39
02/16/21 11:36
56-55-3
Benzo(a)pyrene
ND
ug/kg
423
183
1
02/15/21 10:39
02/16/21 11:36
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
423
170
1
02/15/21 10:39
02/16/21 11:36
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
423
165
1
02/15/21 10:39
02/16/21 11:36
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
423
178
1
02/15/21 10:39
02/16/21 11:36
207-08-9
Benzoic Acid
ND
ug/kg
2110
456
1
02/15/21 10:39
02/16/21 11:36
65-85-0
Benzyl alcohol
ND
ug/kg
846
224
1
02/15/21 10:39
02/16/21 11:36
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
423
ill
1
02/15/21 10:39
02/16/21 11:36
101-55-3
Butylbenzylphthalate
ND
ug/kg
423
113
1
02/15/21 10:39
02/16/21 11:36
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
846
258
1
02/15/21 10:39
02/16/21 11:36
59-50-7
4-Chloroaniline
ND
ug/kg
846
259
1
02/15/21 10:39
02/16/21 11:36
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
423
113
1
02/15/21 10:39
02/16/21 11:36
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
423
89.8
1
02/15/21 10:39
02/16/21 11:36
111-44-4
2-Chloronaphthalene
ND
ug/kg
423
94.2
1
02/15/21 10:39
02/16/21 11:36
91-58-7
2-Chlorophenol
ND
ug/kg
423
98.4
1
02/15/21 10:39
02/16/21 11:36
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
423
110
1
02/15/21 10:39
02/16/21 11:36
7005-72-3
Chrysene
ND
ug/kg
423
123
1
02/15/21 10:39
02/16/21 11:36
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
423
169
1
02/15/21 10:39
02/16/21 11:36
53-70-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 EW (6.5-7) Lab ID: 92521577009 Collected: 02/10/21 17:05 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Comments: • Volatile Petroleum Hydrocarbons by Method MADEPV - Surrogate failure due to matrix interference.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dibenzofuran
ND
ug/kg
423
106
1
02/15/2110:39
02/16/2111:36
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
423
91.5
1
02/15/2110:39
02/16/2111:36
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
423
95.2
1
02/15/2110:39
02/16/2111:36
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
423
93.0
1
02/15/2110:39
02/16/2111:36
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
846
295
1
02/15/2110:39
02/16/2111:36
91-94-1
2,4-Dichlorophenol
ND
ug/kg
423
140
1
02/15/2110:39
02/16/2111:36
120-83-2
Diethylphthalate
ND
ug/kg
423
91.8
1
02/15/2110:39
02/16/2111:36
84-66-2
2,4-Dimethylphenol
ND
ug/kg
423
105
1
02/15/2110:39
02/16/2111:36
105-67-9
Dimethylphthalate
ND
ug/kg
423
95.6
1
02/15/2110:39
02/16/2111:36
131-11-3
Di-n-butylphthalate
ND
ug/kg
423
104
1
02/15/2110:39
02/16/2111:36
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
846
682
1
02/15/2110:39
02/16/2111:36
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2110
1350
1
02/15/2110:39
02/16/2111:36
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
423
112
1
02/15/2110:39
02/16/2111:36
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
423
ill
1
02/15/2110:39
02/16/2111:36
606-20-2
Di-n-octylphthalate
ND
ug/kg
423
241
1
02/15/2110:39
02/16/2111:36
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
423
138
1
02/15/2110:39
02/16/2111:36
117-81-7
Fluoranthene
ND
ug/kg
423
128
1
02/15/2110:39
02/16/2111:36
206-44-0
Fluorene
ND
ug/kg
423
113
1
02/15/2110:39
02/16/2111:36
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
423
103
1
02/15/2110:39
02/16/2111:36
87-68-3
Hexachlorobenzene
ND
ug/kg
423
107
1
02/15/2110:39
02/16/2111:36
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
423
169
1
02/15/2110:39
02/16/2111:36
77-47-4
Hexachloroethane
ND
ug/kg
423
96.4
1
02/15/2110:39
02/16/2111:36
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
423
194
1
02/15/2110:39
02/16/2111:36
193-39-5
Isophorone
ND
ug/kg
423
91.9
1
02/15/2110:39
02/16/2111:36
78-59-1
1-Methylnaphthalene
ND
ug/kg
423
113
1
02/15/2110:39
02/16/2111:36
90-12-0
2-Methylnaphthalene
ND
ug/kg
423
108
1
02/15/2110:39
02/16/2111:36
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
423
93.7
1
02/15/2110:39
02/16/2111:36
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
423
106
1
02/15/21 10:39
02/16/21 11:36
15831-10-4
Naphthalene
ND
ug/kg
423
101
1
02/15/2110:39
02/16/2111:36
91-20-3
2-Nitroaniline
ND
ug/kg
2110
213
1
02/15/2110:39
02/16/2111:36
88-74-4
3-Nitroaniline
ND
ug/kg
2110
224
1
02/15/2110:39
02/16/2111:36
99-09-2
4-Nitroaniline
ND
ug/kg
846
209
1
02/15/2110:39
02/16/2111:36
100-01-6
Nitrobenzene
ND
ug/kg
423
101
1
02/15/2110:39
02/16/2111:36
98-95-3
2-Nitrophenol
ND
ug/kg
423
131
1
02/15/2110:39
02/16/2111:36
88-75-5
4-Nitrophenol
ND
ug/kg
2110
674
1
02/15/2110:39
02/16/2111:36
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
423
119
1
02/15/2110:39
02/16/2111:36
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
423
118
1
02/15/2110:39
02/16/2111:36
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
423
108
1
02/15/2110:39
02/16/2111:36
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
423
118
1
02/15/2110:39
02/16/2111:36
108-60-1
Pentachlorophenol
ND
ug/kg
846
194
1
02/15/2110:39
02/16/2111:36
87-86-5
Phenanthrene
ND
ug/kg
423
107
1
02/15/2110:39
02/16/2111:36
85-01-8
Phenol
ND
ug/kg
423
101
1
02/15/2110:39
02/16/2111:36
108-95-2
Pyrene
ND
ug/kg
423
116
1
02/15/2110:39
02/16/2111:36
129-00-0
REPORT OF LABORATORY ANALYSIS
IL
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 EW (6.5-7) Lab ID: 92521577009 Collected: 02/10/21 17:05 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Comments: • Volatile Petroleum Hydrocarbons by Method MADEPV - Surrogate failure due to matrix interference.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Pyridine
ND
ug/kg
423
107
1
02/15/21 10:39
02/16/21 11:36
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
423
96.9
1
02/15/21 10:39
02/16/21 11:36
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
423
110
1
02/15/21 10:39
02/16/21 11:36
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
423
106
1
02/15/21 10:39
02/16/21 11:36
88-06-2
Surrogates
Nitrobenzene-d5 (S)
60
%
21-130
1
02/15/21 10:39
02/16/21 11:36
4165-60-0
2-Fluorobiphenyl (S)
56
%
19-130
1
02/15/21 10:39
02/16/21 11:36
321-60-8
Terphenyl-dl4 (S)
74
%
15-130
1
02/15/21 10:39
02/16/21 11:36
1718-51-0
Phenol-d6 (S)
52
%
18-130
1
02/15/21 10:39
02/16/21 11:36
13127-88-3
2-Fluorophenol (S)
51
%
18-130
1
02/15/21 10:39
02/16/21 11:36
367-12-4
2,4,6-Tribromophenol (S)
76
%
18-130
1
02/15/21 10:39
02/16/21 11:36
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method:
EPA
5035A/5030B
Pace Analytical Services
- Charlotte
Acetone
ND
ug/kg
141
45.4
1
02/11/21 11:36
02/11/21 17:00
67-64-1
Benzene
ND
ug/kg
7.1
2.8
1
02/11/21 11:36
02/11/21 17:00
71-43-2
Bromobenzene
ND
ug/kg
7.1
2.3
1
02/11/21 11:36
02/11/21 17:00
108-86-1
Bromochloromethane
ND
ug/kg
7.1
2.1
1
02/11/21 11:36
02/11/21 17:00
74-97-5
Bromodichloromethane
ND
ug/kg
7.1
2.7
1
02/11/21 11:36
02/11/21 17:00
75-27-4
Bromoform
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
75-25-2
Bromomethane
ND
ug/kg
14.1
11.2
1
02/11/21 11:36
02/11/21 17:00
74-83-9
2-Butanone (MEK)
ND
ug/kg
141
33.9
1
02/11/21 11:36
02/11/21 17:00
78-93-3
n-Butylbenzene
ND
ug/kg
7.1
3.3
1
02/11/21 11:36
02/11/21 17:00
104-51-8
sec-Butylbenzene
ND
ug/kg
7.1
3.1
1
02/11/21 11:36
02/11/21 17:00
135-98-8
tert-Butyl benzene
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
98-06-6
Carbon tetrachloride
ND
ug/kg
7.1
2.6
1
02/11/21 11:36
02/11/21 17:00
56-23-5
Chlorobenzene
ND
ug/kg
7.1
1.4
1
02/11/21 11:36
02/11/21 17:00
108-90-7
Chloroethane
ND
ug/kg
14.1
5.5
1
02/11/21 11:36
02/11/21 17:00
75-00-3
Chloroform
ND
ug/kg
7.1
4.3
1
02/11/21 11:36
02/11/21 17:00
67-66-3
Chloromethane
ND
ug/kg
14.1
5.9
1
02/11/21 11:36
02/11/21 17:00
74-87-3
2-Chlorotoluene
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
95-49-8
4-Chlorotoluene
ND
ug/kg
7.1
1.3
1
02/11/21 11:36
02/11/21 17:00
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.1
2.7
1
02/11/21 11:36
02/11/21 17:00
96-12-8
Dibromochloromethane
ND
ug/kg
7.1
4.0
1
02/11/21 11:36
02/11/21 17:00
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.1
3.1
1
02/11/21 11:36
02/11/21 17:00
106-93-4
Dibromomethane
ND
ug/kg
7.1
1.5
1
02/11/21 11:36
02/11/21 17:00
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.1
2.2
1
02/11/21 11:36
02/11/21 17:00
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.1
1.8
1
02/11/21 11:36
02/11/21 17:00
106-46-7
Dichlorodifluoromethane
ND
ug/kg
14.1
3.1
1
02/11/21 11:36
02/11/21 17:00
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.1
2.9
1
02/11/21 11:36
02/11/21 17:00
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.1
4.7
1
02/11/21 11:36
02/11/21 17:00
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.1
2.9
1
02/11/21 11:36
02/11/21 17:00
75-35-4
REPORT OF LABORATORY ANALYSIS
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Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 EW (6.5-7) Lab ID: 92521577009 Collected: 02/10/21 17:05 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Comments: • Volatile Petroleum Hydrocarbons by Method MADEPV - Surrogate failure due to matrix interference.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/kg
7.1
2.4
1
02/11/21 11:36
02/11/21 17:00
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.1
2.1
1
02/11/21 11:36
02/11/21 17:00
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.1
2.2
1
02/11/21 11:36
02/11/21 17:00
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.1
2.3
1
02/11/21 11:36
02/11/21 17:00
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.1
3.4
1
02/11/21 11:36
02/11/21 17:00
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
7.1
1.9
1
02/11/21 11:36
02/11/21 17:00
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
7.1
2.4
1
02/11/21 11:36
02/11/21 17:00
10061-02-6
Diisopropyl ether
ND
ug/kg
7.1
1.9
1
02/11/21 11:36
02/11/21 17:00
108-20-3
Ethylbenzene
ND
ug/kg
7.1
3.3
1
02/11/21 11:36
02/11/21 17:00
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
14.1
11.6
1
02/11/21 11:36
02/11/21 17:00
87-68-3
2-Hexanone
ND
ug/kg
70.7
6.8
1
02/11/21 11:36
02/11/21 17:00
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
7.1
2.4
1
02/11/21 11:36
02/11/21 17:00
98-82-8
p-Isopropyltoluene
ND
ug/kg
7.1
3.5
1
02/11/21 11:36
02/11/21 17:00
99-87-6
Methylene Chloride
ND
ug/kg
28.3
19.4
1
02/11/21 11:36
02/11/21 17:00
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
70.7
6.8
1
02/11/21 11:36
02/11/21 17:00
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
7.1
2.6
1
02/11/21 11:36
02/11/21 17:00
1634-04-4
Naphthalene
ND
ug/kg
7.1
3.7
1
02/11/21 11:36
02/11/21 17:00
91-20-3
n-Propylbenzene
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
103-65-1
Styrene
ND
ug/kg
7.1
1.9
1
02/11/21 11:36
02/11/21 17:00
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
7.1
2.7
1
02/11/21 11:36
02/11/21 17:00
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
7.1
1.9
1
02/11/21 11:36
02/11/21 17:00
79-34-5
Tetrachloroethene
ND
ug/kg
7.1
2.2
1
02/11/21 11:36
02/11/21 17:00
127-18-4
Toluene
ND
ug/kg
7.1
2.0
1
02/11/21 11:36
02/11/21 17:00
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
7.1
5.7
1
02/11/21 11:36
02/11/21 17:00
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
7.1
5.9
1
02/11/21 11:36
02/11/21 17:00
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
7.1
3.7
1
02/11/21 11:36
02/11/21 17:00
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
7.1
2.3
1
02/11/21 11:36
02/11/21 17:00
79-00-5
Trichloroethene
ND
ug/kg
7.1
1.8
1
02/11/21 11:36
02/11/21 17:00
79-01-6
Trichlorofluoromethane
ND
ug/kg
7.1
3.9
1
02/11/21 11:36
02/11/21 17:00
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
7.1
3.6
1
02/11/21 11:36
02/11/21 17:00
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
7.1
1.9
1
02/11/21 11:36
02/11/21 17:00
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
7.1
2.4
1
02/11/21 11:36
02/11/21 17:00
108-67-8
Vinyl acetate
ND
ug/kg
70.7
5.1
1
02/11/21 11:36
02/11/21 17:00
108-05-4
Vinyl chloride
ND
ug/kg
14.1
3.6
1
02/11/21 11:36
02/11/21 17:00
75-01-4
Xylene (Total)
ND
ug/kg
14.1
4.0
1
02/11/21 11:36
02/11/21 17:00
1330-20-7
m&p-Xylene
ND
ug/kg
14.1
4.8
1
02/11/21 11:36
02/11/21 17:00
179601-23-1
o-Xylene
ND
ug/kg
7.1
3.1
1
02/11/21 11:36
02/11/21 17:00
95-47-6
Surrogates
Toluene-d8 (S)
101
%
70-130
1
02/11/21 11:36
02/11/21 17:00
2037-26-5
4-Bromofluorobenzene (S)
93
%
69-134
1
02/11/21 11:36
02/11/21 17:00
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
02/11/21 11:36
02/11/21 17:00
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 65

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 EW (6.5-7)
Lab ID: 92521577009 Collected:
02/10/21 17:05
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Comments: • Volatile Petroleum Hydrocarbons by Method MADEPV - Surrogate
failure due to matrix interference.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
20.7 % 0.10
0.10 1
02/11/21 14:13
N2
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM
2540 G
Pace National - Mt. Juliet
Total Solids
79.6 %
1
02/22/21 11:28
02/22/21 11:36
Sample: #2 WW (6.5-7)
Lab ID: 92521577010 Collected:
02/10/21 17:15
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
Aliphatic (C09-C18)
24.4 mg/kg 12.8
12.8 1
02/15/21 11:54
02/16/21 22:57
N2
Aliphatic (C19-C36)
ND mg/kg 12.8
12.8 1
02/15/21 11:54
02/16/21 22:57
N2
Aromatic (C11-C22)
ND mg/kg 12.8
12.8 1
02/15/21 11:54
02/16/21 22:57
N2
Surrogates
1-Chlorooctadecane (S)
50 % 40-140
1
02/15/21 11:54
02/16/21 22:57
3386-33-2
o-Terphenyl (S)
71 % 40-140
1
02/15/21 11:54
02/16/21 22:57
84-15-1
2-Fluorobiphenyl (S)
108 % 40-140
1
02/15/21 11:54
02/16/21 22:57
321-60-8
2-Bromonaphthalene (S)
114 % 40-140
1
02/15/21 11:54
02/16/21 22:57
580-13-2
MADEPV
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
Aliphatic (C05-CO8)
ND mg/kg 7.63
2.55 1
02/10/21 17:15
02/21/21 21:57
Aliphatic (C09-C12)
5.70J mg/kg 7.63
2.55 1
02/10/21 17:15
02/21/21 21:57
J
Aromatic (C09-C10),Unadjusted
6.27J mg/kg 7.63
2.55 1
02/10/21 17:15
02/21/21 21:57
TPHC9C10A J
Total VPH
12.0 mg/kg 7.63
2.55 1
02/10/21 17:15
02/21/21 21:57
VPH
Surrogates
2,5-Dibromotoluene (FID)
113 % 70.0-130
1
02/10/21 17:15
02/21/21 21:57
615-59-8FID
2,5-Dibromotoluene (PID)
117 % 70.0-130
1
02/10/21 17:15
02/21/21 21:57
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Acenaphthene
ND ug/kg 414
106 1
02/15/2110:39
02/16/2112:03
83-32-9
Acenaphthylene
ND ug/kg 414
98.0 1
02/15/2110:39
02/16/2112:03
208-96-8
Aniline
ND ug/kg 414
92.9 1
02/15/2110:39
02/16/2112:03
62-53-3
Anthracene
ND ug/kg 414
107 1
02/15/2110:39
02/16/2112:03
120-12-7
Benzo(a)anthracene
ND ug/kg 414
132 1
02/15/2110:39
02/16/2112:03
56-55-3
Benzo(a)pyrene
ND ug/kg 414
179 1
02/15/2110:39
02/16/2112:03
50-32-8
Benzo(b)fluoranthene
ND ug/kg 414
167 1
02/15/2110:39
02/16/2112:03
205-99-2
Benzo(g,h,i)perylene
ND ug/kg 414
162 1
02/15/2110:39
02/16/2112:03
191-24-2
Date: 02/24/2021 01:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 WW (6.5-7) Lab ID: 92521577010 Collected: 02/10/21 17:15 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Benzo(k)fluoranthene
ND
ug/kg
414
174
1
02/15/21 10:39
02/16/21 12:03
207-08-9
Benzoic Acid
ND
ug/kg
2070
446
1
02/15/21 10:39
02/16/21 12:03
65-85-0
Benzyl alcohol
ND
ug/kg
828
219
1
02/15/21 10:39
02/16/21 12:03
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
414
109
1
02/15/21 10:39
02/16/21 12:03
101-55-3
Butylbenzylphthalate
ND
ug/kg
414
110
1
02/15/21 10:39
02/16/21 12:03
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
828
252
1
02/15/21 10:39
02/16/21 12:03
59-50-7
4-Chloroaniline
ND
ug/kg
828
253
1
02/15/21 10:39
02/16/21 12:03
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
414
110
1
02/15/21 10:39
02/16/21 12:03
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
414
87.9
1
02/15/21 10:39
02/16/21 12:03
111-44-4
2-Chloronaphthalene
ND
ug/kg
414
92.2
1
02/15/21 10:39
02/16/21 12:03
91-58-7
2-Chlorophenol
ND
ug/kg
414
96.3
1
02/15/21 10:39
02/16/21 12:03
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
414
107
1
02/15/21 10:39
02/16/21 12:03
7005-72-3
Chrysene
ND
ug/kg
414
120
1
02/15/21 10:39
02/16/21 12:03
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
414
166
1
02/15/21 10:39
02/16/21 12:03
53-70-3
Dibenzofuran
ND
ug/kg
414
103
1
02/15/21 10:39
02/16/21 12:03
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
414
89.5
1
02/15/21 10:39
02/16/21 12:03
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
414
93.2
1
02/15/21 10:39
02/16/21 12:03
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
414
91.1
1
02/15/21 10:39
02/16/21 12:03
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
828
288
1
02/15/21 10:39
02/16/21 12:03
91-94-1
2,4-Dichlorophenol
ND
ug/kg
414
137
1
02/15/21 10:39
02/16/21 12:03
120-83-2
Diethylphthalate
ND
ug/kg
414
89.8
1
02/15/21 10:39
02/16/21 12:03
84-66-2
2,4-Dimethylphenol
ND
ug/kg
414
103
1
02/15/21 10:39
02/16/21 12:03
105-67-9
Dimethylphthalate
ND
ug/kg
414
93.6
1
02/15/21 10:39
02/16/21 12:03
131-11-3
Di-n-butylphthalate
ND
ug/kg
414
102
1
02/15/21 10:39
02/16/21 12:03
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
828
667
1
02/15/21 10:39
02/16/21 12:03
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2070
1320
1
02/15/21 10:39
02/16/21 12:03
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
414
110
1
02/15/21 10:39
02/16/21 12:03
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
414
108
1
02/15/21 10:39
02/16/21 12:03
606-20-2
Di-n-octylphthalate
ND
ug/kg
414
236
1
02/15/21 10:39
02/16/21 12:03
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
414
135
1
02/15/21 10:39
02/16/21 12:03
117-81-7
Fluoranthene
ND
ug/kg
414
125
1
02/15/21 10:39
02/16/21 12:03
206-44-0
Fluorene
ND
ug/kg
414
ill
1
02/15/21 10:39
02/16/21 12:03
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
414
101
1
02/15/21 10:39
02/16/21 12:03
87-68-3
Hexachlorobenzene
ND
ug/kg
414
105
1
02/15/21 10:39
02/16/21 12:03
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
414
166
1
02/15/21 10:39
02/16/21 12:03
77-47-4
Hexachloroethane
ND
ug/kg
414
94.3
1
02/15/21 10:39
02/16/21 12:03
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
414
189
1
02/15/21 10:39
02/16/21 12:03
193-39-5
Isophorone
ND
ug/kg
414
89.9
1
02/15/21 10:39
02/16/21 12:03
78-59-1
1-Methylnaphthalene
ND
ug/kg
414
110
1
02/15/21 10:39
02/16/21 12:03
90-12-0
2-Methylnaphthalene
ND
ug/kg
414
105
1
02/15/21 10:39
02/16/21 12:03
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
414
91.7
1
02/15/21 10:39
02/16/21 12:03
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
414
104
1
02/15/21 10:39
02/16/21 12:03
15831-10-4
Naphthalene
ND
ug/kg
414
99.1
1
02/15/21 10:39
02/16/21 12:03
91-20-3
2-Nitroaniline
ND
ug/kg
2070
208
1
02/15/21 10:39
02/16/21 12:03
88-74-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 WW (6.5-7)
Lab ID:
92521577010
Collected:
02/10/21 17:15
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are
adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Pace Analytical Services
- Charlotte
3-Nitroaniline
ND
ug/kg
2070
219
1
02/15/21 10:39
02/16/21 12:03
99-09-2 IL
4-Nitroaniline
ND
ug/kg
828
204
1
02/15/21 10:39
02/16/21 12:03
100-01-6
Nitrobenzene
ND
ug/kg
414
98.8
1
02/15/21 10:39
02/16/21 12:03
98-95-3
2-Nitrophenol
ND
ug/kg
414
128
1
02/15/21 10:39
02/16/21 12:03
88-75-5
4-Nitrophenol
ND
ug/kg
2070
660
1
02/15/21 10:39
02/16/21 12:03
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
414
116
1
02/15/21 10:39
02/16/21 12:03
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
414
116
1
02/15/21 10:39
02/16/21 12:03
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
414
106
1
02/15/21 10:39
02/16/21 12:03
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
414
115
1
02/15/21 10:39
02/16/21 12:03
108-60-1
Pentachlorophenol
ND
ug/kg
828
189
1
02/15/21 10:39
02/16/21 12:03
87-86-5
Phenanthrene
ND
ug/kg
414
104
1
02/15/21 10:39
02/16/21 12:03
85-01-8
Phenol
ND
ug/kg
414
98.8
1
02/15/21 10:39
02/16/21 12:03
108-95-2
Pyrene
ND
ug/kg
414
114
1
02/15/21 10:39
02/16/21 12:03
129-00-0
Pyridine
ND
ug/kg
414
105
1
02/15/21 10:39
02/16/21 12:03
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
414
94.8
1
02/15/21 10:39
02/16/21 12:03
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
414
107
1
02/15/21 10:39
02/16/21 12:03
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
414
104
1
02/15/21 10:39
02/16/21 12:03
88-06-2
Surrogates
Nitrobenzene-d5 (S)
77
%
21-130
1
02/15/21 10:39
02/16/21 12:03
4165-60-0
2-Fluorobiphenyl (S)
75
%
19-130
1
02/15/21 10:39
02/16/21 12:03
321-60-8
Terphenyl-d14 (S)
84
%
15-130
1
02/15/21 10:39
02/16/21 12:03
1718-51-0
Phenol-d6 (S)
64
%
18-130
1
02/15/21 10:39
02/16/21 12:03
13127-88-3
2-Fluorophenol (S)
64
%
18-130
1
02/15/21 10:39
02/16/21 12:03
367-12-4
2,4,6-Tribromophenol (S)
86
%
18-130
1
02/15/21 10:39
02/16/21 12:03
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D
Preparation Method: EPA 5035A/5030B
Pace Analytical Services
- Charlotte
Acetone
ND
ug/kg
151
48.5
1
02/11/21 14:01
02/15/21 17:11
67-64-1
Benzene
ND
ug/kg
7.6
3.0
1
02/11/21 14:01
02/15/21 17:11
71-43-2
Bromobenzene
ND
ug/kg
7.6
2.5
1
02/11/21 14:01
02/15/21 17:11
108-86-1
Bromochloromethane
ND
ug/kg
7.6
2.2
1
02/11/21 14:01
02/15/21 17:11
74-97-5
Bromodichloromethane
ND
ug/kg
7.6
2.9
1
02/11/21 14:01
02/15/21 17:11
75-27-4
Bromoform
ND
ug/kg
7.6
2.7
1
02/11/21 14:01
02/15/21 17:11
75-25-2
Bromomethane
ND
ug/kg
15.1
11.9
1
02/11/21 14:01
02/15/21 17:11
74-83-9 v1
2-Butanone (MEK)
ND
ug/kg
151
36.3
1
02/11/21 14:01
02/15/21 17:11
78-93-3
n-Butylbenzene
ND
ug/kg
7.6
3.6
1
02/11/21 14:01
02/15/21 17:11
104-51-8
sec-Butylbenzene
ND
ug/kg
7.6
3.3
1
02/11/21 14:01
02/15/21 17:11
135-98-8
tert-Butyl benzene
ND
ug/kg
7.6
2.7
1
02/11/21 14:01
02/15/21 17:11
98-06-6
Carbon tetrachloride
ND
ug/kg
7.6
2.8
1
02/11/21 14:01
02/15/21 17:11
56-23-5
Chlorobenzene
ND
ug/kg
7.6
1.5
1
02/11/21 14:01
02/15/21 17:11
108-90-7
Chloroethane
ND
ug/kg
15.1
5.8
1
02/11/21 14:01
02/15/21 17:11
75-00-3
Chloroform
ND
ug/kg
7.6
4.6
1
02/11/21 14:01
02/15/21 17:11
67-66-3
Chloromethane
ND
ug/kg
15.1
6.3
1
02/11/21 14:01
02/15/21 17:11
74-87-3
2-Chlorotoluene
ND
ug/kg
7.6
2.7
1
02/11/21 14:01
02/15/21 17:11
95-49-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 WW (6.5-7) Lab ID: 92521577010 Collected: 02/10/21 17:15 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
4-Chlorotoluene
ND
ug/kg
7.6
1.3
1
02/11/21 14:01
02/15/21 17:11
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.6
2.9
1
02/11/21 14:01
02/15/21 17:11
96-12-8
Dibromochloromethane
ND
ug/kg
7.6
4.2
1
02/11/21 14:01
02/15/21 17:11
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.6
3.3
1
02/11/21 14:01
02/15/21 17:11
106-93-4
Dibromomethane
ND
ug/kg
7.6
1.6
1
02/11/21 14:01
02/15/21 17:11
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.6
2.7
1
02/11/21 14:01
02/15/21 17:11
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.6
2.3
1
02/11/21 14:01
02/15/21 17:11
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.6
2.0
1
02/11/21 14:01
02/15/21 17:11
106-46-7
Dichlorodifluoromethane
ND
ug/kg
15.1
3.3
1
02/11/21 14:01
02/15/21 17:11
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.6
3.1
1
02/11/21 14:01
02/15/21 17:11
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.6
5.0
1
02/11/21 14:01
02/15/21 17:11
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.6
3.1
1
02/11/21 14:01
02/15/21 17:11
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
7.6
2.6
1
02/11/21 14:01
02/15/21 17:11
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.6
2.6
1
02/11/21 14:01
02/15/21 17:11
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.6
2.3
1
02/11/21 14:01
02/15/21 17:11
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.6
2.4
1
02/11/21 14:01
02/15/21 17:11
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.6
2.5
1
02/11/21 14:01
02/15/21 17:11
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.6
3.6
1
02/11/21 14:01
02/15/21 17:11
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
7.6
2.1
1
02/11/21 14:01
02/15/21 17:11
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
7.6
2.6
1
02/11/21 14:01
02/15/21 17:11
10061-02-6
Diisopropyl ether
ND
ug/kg
7.6
2.0
1
02/11/21 14:01
02/15/21 17:11
108-20-3
Ethylbenzene
ND
ug/kg
7.6
3.5
1
02/11/21 14:01
02/15/21 17:11
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
15.1
12.4
1
02/11/21 14:01
02/15/21 17:11
87-68-3
2-Hexanone
ND
ug/kg
75.5
7.3
1
02/11/21 14:01
02/15/21 17:11
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
7.6
2.6
1
02/11/21 14:01
02/15/21 17:11
98-82-8
p-Isopropyltoluene
ND
ug/kg
7.6
3.7
1
02/11/21 14:01
02/15/21 17:11
99-87-6
Methylene Chloride
ND
ug/kg
30.2
20.7
1
02/11/21 14:01
02/15/21 17:11
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
75.5
7.3
1
02/11/21 14:01
02/15/21 17:11
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
7.6
2.8
1
02/11/21 14:01
02/15/21 17:11
1634-04-4
Naphthalene
ND
ug/kg
7.6
4.0
1
02/11/21 14:01
02/15/21 17:11
91-20-3
n-Propylbenzene
ND
ug/kg
7.6
2.7
1
02/11/21 14:01
02/15/21 17:11
103-65-1
Styrene
ND
ug/kg
7.6
2.0
1
02/11/21 14:01
02/15/21 17:11
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
7.6
2.9
1
02/11/21 14:01
02/15/21 17:11
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
7.6
2.0
1
02/11/21 14:01
02/15/21 17:11
79-34-5
Tetrachloroethene
ND
ug/kg
7.6
2.4
1
02/11/21 14:01
02/15/21 17:11
127-18-4
Toluene
ND
ug/kg
7.6
2.1
1
02/11/21 14:01
02/15/21 17:11
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
7.6
6.1
1
02/11/21 14:01
02/15/21 17:11
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
7.6
6.3
1
02/11/21 14:01
02/15/21 17:11
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
7.6
3.9
1
02/11/21 14:01
02/15/21 17:11
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
7.6
2.5
1
02/11/21 14:01
02/15/21 17:11
79-00-5
Trichloroethene
ND
ug/kg
7.6
1.9
1
02/11/21 14:01
02/15/21 17:11
79-01-6
Trichlorofluoromethane
ND
ug/kg
7.6
4.2
1
02/11/21 14:01
02/15/21 17:11
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
7.6
3.8
1
02/11/21 14:01
02/15/21 17:11
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
7.6
2.1
1
02/11/21 14:01
02/15/21 17:11
95-63-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 WW (6.5-7)
Lab ID: 92521577010 Collected:
02/10/21 17:15
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
1,3,5-Trimethylbenzene
5.11 ug/kg 7.6
2.5 1
02/11/21 14:01
02/15/21 17:11
108-67-8
Vinyl acetate
ND ug/kg 75.5
5.5 1
02/11/21 14:01
02/15/21 17:11
108-05-4
Vinyl chloride
ND ug/kg 15.1
3.8 1
02/11/21 14:01
02/15/21 17:11
75-01-4
Xylene (Total)
ND ug/kg 15.1
4.3 1
02/11/21 14:01
02/15/21 17:11
1330-20-7
m&p-Xylene
ND ug/kg 15.1
5.2 1
02/11/21 14:01
02/15/21 17:11
179601-23-1
o-Xylene
ND ug/kg 7.6
3.3 1
02/11/21 14:01
02/15/21 17:11
95-47-6
Surrogates
Toluene-d8 (S)
102 % 70-130
1
02/11/21 14:01
02/15/21 17:11
2037-26-5
4-Bromofluorobenzene (S)
103 % 69-134
1
02/11/21 14:01
02/15/21 17:11
460-00-4
1,2-Dichloroethane-d4 (S)
106 % 70-130
1
02/11/21 14:01
02/15/21 17:11
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
21.3 % 0.10
0.10 1
02/11/21 14:13
N2
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM
2540 G
Pace National - Mt. Juliet
Total Solids
79.5 %
1
02/22/21 11:28
02/22/21 11:36
Sample: #2 BASE (15.0)
Lab ID: 92521577011 Collected:
02/10/21 16:55
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
Aliphatic (C09-C18)
9270 mg/kg 2460
2460 200
02/15/21 11:54
02/17/21 20:01
N2
Aliphatic (C19-C36)
ND mg/kg 2460
2460 200
02/15/21 11:54
02/17/21 20:01
N2
Aromatic (C11-C22)
2210 mg/kg 307
307 25
02/15/21 11:54
02/17/21 20:01
N2
Surrogates
1-Chlorooctadecane (S)
0 % 40-140
200
02/15/21 11:54
02/17/21 20:01
3386-33-2 S4
o-Terphenyl (S)
0 % 40-140
25
02/15/21 11:54
02/17/21 20:01
84-15-1 S4
2-Fluorobiphenyl (S)
0 % 40-140
25
02/15/21 11:54
02/17/21 20:01
321-60-8 S4
2-Bromonaphthalene (S)
0 % 40-140
25
02/15/21 11:54
02/17/21 20:01
580-13-2 S4
MADEPV
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
Aliphatic (C05-CO8)
44.7 mg/kg 36.5
12.2 5
02/10/21 16:55
02/21/21 23:03
Aliphatic (C09-C12)
924 mg/kg 36.5
12.2 5
02/10/21 16:55
02/21/21 23:03
Aromatic (C09-C10),Unadjusted
67.2J mg/kg 73.1
24.3 10
02/10/21 16:55
02/23/21 16:17
TPHC9C10A J
Total VPH
969 mg/kg 36.5
12.2 5
02/10/21 16:55
02/21/21 23:03
VPH
Surrogates
2,5-Dibromotoluene (FID)
106 % 70.0-130
5
02/10/21 16:55
02/21/21 23:03
615-59-8FID
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM
without the written consent of Pace Analytical Services, LLC.
Page 27 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 BASE (15.0)
Lab ID:
92521577011
Collected:
02/10/21
16:55
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are
adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
MADEPV
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
Surrogates
2,5-Dibromotoluene (FID)
100
%
70.0-130
10
02/10/21 16:55
02/23/21 16:17
615-59-8FID
2,5-Dibromotoluene (PID)
116
%
70.0-130
5
02/10/21 16:55
02/21/21 23:03
615-59-8PID
2,5-Dibromotoluene (PID)
102
%
70.0-130
10
02/10/21 16:55
02/23/21 16:17
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method: EPA 3546
Pace Analytical Services
- Charlotte
Acenaphthene
ND
ug/kg
4120
1060
10
02/15/21 10:39
02/17/21 10:11
83-32-9
Acenaphthylene
ND
ug/kg
4120
976
10
02/15/21 10:39
02/17/21 10:11
208-96-8
Aniline
ND
ug/kg
4120
926
10
02/15/21 10:39
02/17/21 10:11
62-53-3
Anthracene
ND
ug/kg
4120
1070
10
02/15/21 10:39
02/17/21 10:11
120-12-7
Benzo(a)anthracene
ND
ug/kg
4120
1310
10
02/15/21 10:39
02/17/21 10:11
56-55-3
Benzo(a)pyrene
ND
ug/kg
4120
1790
10
02/15/21 10:39
02/17/21 10:11
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
4120
1660
10
02/15/21 10:39
02/17/21 10:11
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
4120
1610
10
02/15/21 10:39
02/17/21 10:11
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
4120
1740
10
02/15/21 10:39
02/17/21 10:11
207-08-9
Benzoic Acid
ND
ug/kg
20600
4450
10
02/15/21 10:39
02/17/21 10:11
65-85-0
Benzyl alcohol
ND
ug/kg
8250
2190
10
02/15/21 10:39
02/17/21 10:11
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
4120
1080
10
02/15/21 10:39
02/17/21 10:11
101-55-3
Butylbenzylphthalate
ND
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 10:11
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
8250
2510
10
02/15/21 10:39
02/17/21 10:11
59-50-7
4-Chloroaniline
ND
ug/kg
8250
2520
10
02/15/21 10:39
02/17/21 10:11
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 10:11
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
4120
876
10
02/15/21 10:39
02/17/21 10:11
111-44-4
2-Chloronaphthalene
ND
ug/kg
4120
918
10
02/15/21 10:39
02/17/21 10:11
91-58-7
2-Chlorophenol
ND
ug/kg
4120
959
10
02/15/21 10:39
02/17/21 10:11
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
4120
1070
10
02/15/21 10:39
02/17/21 10:11
7005-72-3
Chrysene
ND
ug/kg
4120
1200
10
02/15/21 10:39
02/17/21 10:11
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
4120
1650
10
02/15/21 10:39
02/17/21 10:11
53-70-3
Dibenzofuran
1380J
ug/kg
4120
1030
10
02/15/21 10:39
02/17/21 10:11
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
4120
892
10
02/15/21 10:39
02/17/21 10:11
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
4120
928
10
02/15/21 10:39
02/17/21 10:11
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
4120
907
10
02/15/21 10:39
02/17/21 10:11
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
8250
2870
10
02/15/21 10:39
02/17/21 10:11
91-94-1
2,4-Dichlorophenol
ND
ug/kg
4120
1360
10
02/15/21 10:39
02/17/21 10:11
120-83-2
Diethylphthalate
ND
ug/kg
4120
894
10
02/15/21 10:39
02/17/21 10:11
84-66-2 v1
2,4-Dimethylphenol
ND
ug/kg
4120
1030
10
02/15/21 10:39
02/17/21 10:11
105-67-9
Dimethylphthalate
ND
ug/kg
4120
932
10
02/15/21 10:39
02/17/21 10:11
131-11-3
Di-n-butylphthalate
ND
ug/kg
4120
1020
10
02/15/21 10:39
02/17/21 10:11
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
8250
6650
10
02/15/21 10:39
02/17/21 10:11
534-52-1
2,4-Dinitrophenol
ND
ug/kg
20600
13200
10
02/15/21 10:39
02/17/21 10:11
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
4120
1090
10
02/15/21 10:39
02/17/21 10:11
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
4120
1080
10
02/15/21 10:39
02/17/21 10:11
606-20-2
Di-n-octylphthalate
ND
ug/kg
4120
2350
10
02/15/21 10:39
02/17/21 10:11
117-84-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 BASE (15.0) Lab ID: 92521577011 Collected: 02/10/21 16:55 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
bis(2- Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D/5035A/5030B Volatiles
Acetone
Benzene
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
4120
1350
10
02/15/2110:39
02/17/2110:11
117-81-7
ND
ug/kg
4120
1250
10
02/15/2110:39
02/17/2110:11
206-44-0
1370J
ug/kg
4120
1100
10
02/15/2110:39
02/17/2110:11
86-73-7
ND
ug/kg
4120
1000
10
02/15/2110:39
02/17/2110:11
87-68-3
ND
ug/kg
4120
1050
10
02/15/2110:39
02/17/2110:11
118-74-1
ND
ug/kg
4120
1650
10
02/15/2110:39
02/17/2110:11
77-47-4
ND
ug/kg
4120
939
10
02/15/2110:39
02/17/2110:11
67-72-1
ND
ug/kg
4120
1890
10
02/15/2110:39
02/17/2110:11
193-39-5
ND
ug/kg
4120
896
10
02/15/2110:39
02/17/2110:11
78-59-1
20200
ug/kg
4120
1100
10
02/15/2110:39
02/17/2110:11
90-12-0
29800
ug/kg
4120
1050
10
02/15/2110:39
02/17/2110:11
91-57-6
ND
ug/kg
4120
913
10
02/15/2110:39
02/17/2110:11
95-48-7
ND
ug/kg
4120
1040
10
02/15/2110:39
02/17/2110:11
15831-10-4
3120J
ug/kg
4120
987
10
02/15/2110:39
02/17/2110:11
91-20-3
ND
ug/kg
20600
2070
10
02/15/2110:39
02/17/2110:11
88-74-4
ND
ug/kg
20600
2190
10
02/15/2110:39
02/17/2110:11
99-09-2
IL
ND
ug/kg
8250
2040
10
02/15/2110:39
02/17/2110:11
100-01-6
ND
ug/kg
4120
984
10
02/15/2110:39
02/17/2110:11
98-95-3
ND
ug/kg
4120
1270
10
02/15/2110:39
02/17/2110:11
88-75-5
ND
ug/kg
20600
6570
10
02/15/2110:39
02/17/2110:11
100-02-7
v1
ND
ug/kg
4120
1160
10
02/15/2110:39
02/17/2110:11
62-75-9
ND
ug/kg
4120
1150
10
02/15/2110:39
02/17/2110:11
621-64-7
ND
ug/kg
4120
1050
10
02/15/2110:39
02/17/2110:11
86-30-6
ND
ug/kg
4120
1150
10
02/15/2110:39
02/17/2110:11
108-60-1
ND
ug/kg
8250
1890
10
02/15/2110:39
02/17/2110:11
87-86-5
9270
ug/kg
4120
1040
10
02/15/2110:39
02/17/2110:11
85-01-8
ND
ug/kg
4120
984
10
02/15/2110:39
02/17/2110:11
108-95-2
ND
ug/kg
4120
1130
10
02/15/2110:39
02/17/2110:11
129-00-0
ND
ug/kg
4120
1040
10
02/15/2110:39
02/17/2110:11
110-86-1
ND
ug/kg
4120
944
10
02/15/2110:39
02/17/2110:11
120-82-1
ND
ug/kg
4120
1070
10
02/15/2110:39
02/17/2110:11
95-95-4
ND
ug/kg
4120
1040
10
02/15/2110:39
02/17/2110:11
88-06-2
0
%
21-130
10
02/15/2110:39
02/17/2110:11
4165-60-0
D3,S4
0
%
19-130
10
02/15/2110:39
02/17/2110:11
321-60-8
S4
0
%
15-130
10
02/15/2110:39
02/17/2110:11
1718-51-0
S4
0
%
18-130
10
02/15/2110:39
02/17/2110:11
13127-88-3
S4
0
%
18-130
10
02/15/2110:39
02/17/2110:11
367-12-4
S4
0
%
18-130
10
02/15/2110:39
02/17/2110:11
118-79-6
S4
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND ug/kg 628 202 4 02/11/2114:01 02/15/2119:54 67-64-1
ND ug/kg 31.4 12.5 4 02/11/2114:01 02/15/2119:54 71-43-2
REPORT OF LABORATORY ANALYSIS
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Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 65

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 BASE (15.0) Lab ID: 92521577011 Collected: 02/10/21 16:55 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Bromobenzene
ND
ug/kg
31.4
10.2
4
02/11/21 14:01
02/15/21 19:54
108-86-1
Bromochloromethane
ND
ug/kg
31.4
9.3
4
02/11/21 14:01
02/15/21 19:54
74-97-5
Bromodichloromethane
ND
ug/kg
31.4
12.1
4
02/11/21 14:01
02/15/21 19:54
75-27-4
Bromoform
ND
ug/kg
31.4
11.0
4
02/11/21 14:01
02/15/21 19:54
75-25-2
Bromomethane
ND
ug/kg
62.8
49.6
4
02/11/21 14:01
02/15/21 19:54
74-83-9 v1
2-Butanone (MEK)
ND
ug/kg
628
151
4
02/11/21 14:01
02/15/21 19:54
78-93-3
n-Butylbenzene
ND
ug/kg
31.4
14.8
4
02/11/21 14:01
02/15/21 19:54
104-51-8
sec-Butylbenzene
ND
ug/kg
31.4
13.8
4
02/11/21 14:01
02/15/21 19:54
135-98-8
tert-Butyl benzene
ND
ug/kg
31.4
11.2
4
02/11/21 14:01
02/15/21 19:54
98-06-6
Carbon tetrachloride
ND
ug/kg
31.4
11.7
4
02/11/21 14:01
02/15/21 19:54
56-23-5
Chlorobenzene
ND
ug/kg
31.4
6.0
4
02/11/21 14:01
02/15/21 19:54
108-90-7
Chloroethane
ND
ug/kg
62.8
24.2
4
02/11/21 14:01
02/15/21 19:54
75-00-3
Chloroform
ND
ug/kg
31.4
19.1
4
02/11/21 14:01
02/15/21 19:54
67-66-3
Chloromethane
ND
ug/kg
62.8
26.4
4
02/11/21 14:01
02/15/21 19:54
74-87-3
2-Chlorotoluene
ND
ug/kg
31.4
11.1
4
02/11/21 14:01
02/15/21 19:54
95-49-8
4-Chlorotoluene
ND
ug/kg
31.4
5.6
4
02/11/21 14:01
02/15/21 19:54
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
31.4
12.2
4
02/11/21 14:01
02/15/21 19:54
96-12-8
Dibromochloromethane
ND
ug/kg
31.4
17.6
4
02/11/21 14:01
02/15/21 19:54
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
31.4
13.8
4
02/11/21 14:01
02/15/21 19:54
106-93-4
Dibromomethane
ND
ug/kg
31.4
6.7
4
02/11/21 14:01
02/15/21 19:54
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
31.4
11.3
4
02/11/21 14:01
02/15/21 19:54
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
31.4
9.7
4
02/11/21 14:01
02/15/21 19:54
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
31.4
8.2
4
02/11/21 14:01
02/15/21 19:54
106-46-7
Dichlorodifluoromethane
ND
ug/kg
62.8
13.6
4
02/11/21 14:01
02/15/21 19:54
75-71-8
1,1-Dichloroethane
ND
ug/kg
31.4
12.9
4
02/11/21 14:01
02/15/21 19:54
75-34-3
1,2-Dichloroethane
ND
ug/kg
31.4
20.8
4
02/11/21 14:01
02/15/21 19:54
107-06-2
1,1-Dichloroethene
ND
ug/kg
31.4
12.9
4
02/11/21 14:01
02/15/21 19:54
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
31.4
10.7
4
02/11/21 14:01
02/15/21 19:54
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
31.4
11.0
4
02/11/21 14:01
02/15/21 19:54
156-60-5
1,2-Dichloropropane
ND
ug/kg
31.4
9.4
4
02/11/21 14:01
02/15/21 19:54
78-87-5
1,3-Dichloropropane
ND
ug/kg
31.4
9.8
4
02/11/21 14:01
02/15/21 19:54
142-28-9
2,2-Dichloropropane
ND
ug/kg
31.4
10.2
4
02/11/21 14:01
02/15/21 19:54
594-20-7
1,1-Dichloropropene
ND
ug/kg
31.4
15.1
4
02/11/21 14:01
02/15/21 19:54
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
31.4
8.5
4
02/11/21 14:01
02/15/21 19:54
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
31.4
10.8
4
02/11/21 14:01
02/15/21 19:54
10061-02-6
Diisopropyl ether
ND
ug/kg
31.4
8.5
4
02/11/21 14:01
02/15/21 19:54
108-20-3
Ethylbenzene
823
ug/kg
31.4
14.6
4
02/11/21 14:01
02/15/21 19:54
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
62.8
51.4
4
02/11/21 14:01
02/15/21 19:54
87-68-3
2-Hexanone
ND
ug/kg
314
30.3
4
02/11/21 14:01
02/15/21 19:54
591-78-6
Isopropylbenzene (Cumene)
777
ug/kg
31.4
10.7
4
02/11/21 14:01
02/15/21 19:54
98-82-8
p-Isopropyltoluene
8170
ug/kg
31.4
15.4
4
02/11/21 14:01
02/15/21 19:54
99-87-6
Methylene Chloride
ND
ug/kg
126
86.0
4
02/11/21 14:01
02/15/21 19:54
75-09-2
4-Methyl-2-pentanone (MIBK)
404
ug/kg
314
30.3
4
02/11/21 14:01
02/15/21 19:54
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
31.4
11.7
4
02/11/21 14:01
02/15/21 19:54
1634-04-4
REPORT OF LABORATORY ANALYSIS
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Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 65

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[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 BASE (15.0) Lab ID: 92521577011 Collected: 02/10/21 16:55 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Date: 02/24/2021 01:57 PM
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
5450
ug/kg
31.4
16.5
4
02/11/2114:01
02/15/2119:54
91-20-3
ND
ug/kg
31.4
11.2
4
02/11/2114:01
02/15/2119:54
103-65-1
ND
ug/kg
31.4
8.3
4
02/11/2114:01
02/15/2119:54
100-42-5
ND
ug/kg
31.4
12.1
4
02/11/2114:01
02/15/2119:54
630-20-6
ND
ug/kg
31.4
8.3
4
02/11/2114:01
02/15/2119:54
79-34-5
ND
ug/kg
31.4
9.9
4
02/11/2114:01
02/15/2119:54
127-18-4
161
ug/kg
31.4
8.9
4
02/11/2114:01
02/15/2119:54
108-88-3
ND
ug/kg
31.4
25.4
4
02/11/2114:01
02/15/2119:54
87-61-6
ND
ug/kg
31.4
26.4
4
02/11/2114:01
02/15/2119:54
120-82-1
ND
ug/kg
31.4
16.3
4
02/11/2114:01
02/15/2119:54
71-55-6
ND
ug/kg
31.4
10.4
4
02/11/2114:01
02/15/2119:54
79-00-5
ND
ug/kg
31.4
8.1
4
02/11/2114:01
02/15/2119:54
79-01-6
ND
ug/kg
31.4
17.3
4
02/11/2114:01
02/15/2119:54
75-69-4
ND
ug/kg
31.4
15.9
4
02/11/2114:01
02/15/2119:54
96-18-4
ND
ug/kg
31.4
8.6
4
02/11/2114:01
02/15/2119:54
95-63-6
6140
ug/kg
31.4
10.5
4
02/11/2114:01
02/15/2119:54
108-67-8
ND
ug/kg
314
22.9
4
02/11/2114:01
02/15/2119:54
108-05-4
ND
ug/kg
62.8
15.9
4
02/11/2114:01
02/15/2119:54
75-01-4
4150
ug/kg
62.8
17.9
4
02/11/2114:01
02/15/2119:54
1330-20-7
521
ug/kg
62.8
21.5
4
02/11/2114:01
02/15/2119:54
179601-23-1
3630
ug/kg
31.4
13.9
4
02/11/2114:01
02/15/2119:54
95-47-6
103
%
70-130
4
02/11/2114:01
02/15/2119:54
2037-26-5 D3
108
%
69-134
4
02/11/2114:01
02/15/2119:54
460-00-4
105
%
70-130
4
02/11/2114:01
02/15/2119:54
17060-07-0
Analytical
Method: SW-846
Pace Analytical Services - Charlotte
19.4
%
0.10
0.10
1
02/11/2114:13
N2
Analytical
Method: SM 2540G Preparation Method:
SM 2540 G
Pace National - Mt. Juliet
82.0
%
1
02/22/2111:28
02/22/2111:36
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 31 of 65

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9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 1621454 Analysis Method: MADEP VPH
QC Batch Method: MADEPV Analysis Description: MADEPV
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92521577008, 92521577009
METHOD BLANK: R3622828-3
Matrix:
Solid
Associated Lab Samples: 92521577008, 92521577009
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Aliphatic (C05-CO8)
mg/kg
1.70J
5.00
1.67
02/14/21 19:50 J
Aliphatic (C09-C12)
mg/kg
ND
5.00
1.67
02/14/21 19:50
Aromatic (C09-C10),Unadjusted
mg/kg
ND
5.00
1.67
02/14/21 19:50
Total VPH
mg/kg
1.70J
5.00
1.67
02/14/21 19:50 J
2,5-Dibromotoluene (FID)
%
85.7
70.0-130
02/14/21 19:50
2,5-Dibromotoluene (PID)
%
71.9
70.0-130
02/14/21 19:50
LABORATORY CONTROL SAMPLE & LCSD:
R3622828-1
R3622828-2
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
60.0
60.1
57.9
100
96.5
70.0-130
3.73
25
Aliphatic (C09-C12)
mg/kg
70.0
83.8
80.0
120
114
70.0-130
4.64
25
Aromatic (C09-C10),Unadjusted
mg/kg
10.0
9.82
9.35
98.2
93.5
70.0-130
4.90
25
Total VPH
mg/kg
140
154
147
110
105
70.0-130
4.65
25
2,5-Dibromotoluene (FID)
%
97.9
93.9
70.0-130
2,5-Dibromotoluene (PID)
%
83.0
80.7
70.0-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 1621956 Analysis Method: MADEP VPH
QC Batch Method: MADEPV Analysis Description: MADEPV
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92521577007, 92521577010, 92521577011
METHOD BLANK: R3623854-3
Matrix:
Solid
Associated Lab Samples: 92521577007, 92521577010,
92521577011
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Aliphatic (C05-CO8)
mg/kg
ND
5.00
1.67
02/21/21 17:00
Aliphatic (C09-C12)
mg/kg
ND
5.00
1.67
02/21/21 17:00
Aromatic (C09-C10),Unadjusted
mg/kg
ND
5.00
1.67
02/21/21 17:00
Total VPH
mg/kg
ND
5.00
1.67
02/21/21 17:00
2,5-Dibromotoluene (FID)
%
96.2
70.0-130
02/21/21 17:00
2,5-Dibromotoluene (PID)
%
99.3
70.0-130
02/21/21 17:00
LABORATORY CONTROL SAMPLE & LCSD:
R3623854-1
R3623854-2
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
60.0
57.9
58.7
96.5
97.8
70.0-130
1.37
25
Aliphatic (C09-C12)
mg/kg
70.0
79.1
79.9
113
114
70.0-130
1.01
25
Aromatic (C09-C10),Unadjusted
mg/kg
10.0
11.9
11.9
119
119
70.0-130
0.00
25
Total VPH
mg/kg
140
149
151
106
108
70.0-130
1.33
25
2,5-Dibromotoluene (FID)
%
110
111
70.0-130
2,5-Dibromotoluene (PID)
%
114
116
70.0-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 33 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 1623520 Analysis Method: MADEP VPH
QC Batch Method: MADEPV Analysis Description: MADEPV
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92521577011
METHOD BLANK: R3624414-3
Matrix:
Solid
Associated Lab Samples: 92521577011
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Aromatic (C09-C10),Unadjusted
mg/kg
ND
5.00
1.67 02/23/21 13:05
2,5-Dibromotoluene (FID)
%
86.8
70.0-130
02/23/21 13:05
2,5-Dibromotoluene (PID)
%
87.4
70.0-130
02/23/21 13:05
LABORATORY CONTROL SAMPLE & LCSD:
R3624414-1
R3624414-2
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aromatic (C09-C10),Unadjusted
mg/kg 10.0
12.6 12.3
126
123
70.0-130 2.41 25
2,5-Dibromotoluene (FID)
%
106
102
70.0-130
2,5-Dibromotoluene (PID)
%
109
105
70.0-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 34 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599422
Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E
Analysis Description: Gasoline Range Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577001
METHOD BLANK: 3160191
Matrix: Solid
Associated Lab Samples: 92521577001
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 6.0 1.1
02/11/21 22:04
4-Bromofluorobenzene (S)
%
87 66-131
02/11/21 22:04
LABORATORY CONTROL SAMPLE:
3160192
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
50 45.3 91
70-130
4-Bromofluorobenzene (S)
%
90
66-131
MATRIX SPIKE SAMPLE:
3160194
92521234002 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 70.2 75.8
98
70-145
4-Bromofluorobenzene (S)
%
100
66-131
SAMPLE DUPLICATE: 3160193
92521234003 Dup
Max
Parameter
Units
Result Result RPD
RPD
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 2.3J
30
4-Bromofluorobenzene (S)
%
93 90
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599699
Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E
Analysis Description: Gasoline Range Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577002, 92521577003,
92521577004, 92521577005, 92521577006
METHOD BLANK: 3161455
Matrix: Solid
Associated Lab Samples: 92521577002, 92521577003,
92521577004, 92521577005, 92521577006
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 6.0 1.1
02/12/21 12:12
4-Bromofluorobenzene (S)
%
86 66-131
02/12/21 12:12
LABORATORY CONTROL SAMPLE:
3161456
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
50.4 49.8 99
70-130
4-Bromofluorobenzene (S)
%
89
66-131
MATRIX SPIKE SAMPLE:
3161458
92521622002 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 68.5 68.4
98
70-145
4-Bromofluorobenzene (S)
%
89
66-131
SAMPLE DUPLICATE: 3161457
92521577006 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Gas Range Organics (C6-C10) mg/kg ND ND 30
4-Bromofluorobenzene (S) % 83 82
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599326 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577001, 92521577002, 92521577003, 92521577004, 92521577005, 92521577006, 92521577007,
92521577008,92521577009
METHOD BLANK: 3159501
Matrix: Solid
Associated Lab Samples: 92521577001, 92521577002, 92521577003, 92521577004, 92521577005, 92521577006, 92521577007,
92521577008,92521577009
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
1.9
02/11/21 10:58
1,1,1-Trichloroethane
ug/kg
ND
5.0
2.6
02/11/21 10:58
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
1.3
02/11/21 10:58
1,1,2-Trichloroethane
ug/kg
ND
5.0
1.7
02/11/21 10:58
1,1-Dichloroethane
ug/kg
ND
5.0
2.1
02/11/21 10:58
1,1-Dichloroethene
ug/kg
ND
5.0
2.1
02/11/21 10:58
1,1-Dichloropropene
ug/kg
ND
5.0
2.4
02/11/21 10:58
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
4.0
02/11/21 10:58
1,2,3-Trichloropropane
ug/kg
ND
5.0
2.5
02/11/21 10:58
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
4.2
02/11/21 10:58
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
1.4
02/11/21 10:58
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
1.9
02/11/21 10:58
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
2.2
02/11/21 10:58
1,2-Dichlorobenzene
ug/kg
ND
5.0
1.8
02/11/21 10:58
1,2-Dichloroethane
ug/kg
ND
5.0
3.3
02/11/21 10:58
1,2-Dichloropropane
ug/kg
ND
5.0
1.5
02/11/21 10:58
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
1.7
02/11/21 10:58
1,3-Dichlorobenzene
ug/kg
ND
5.0
1.6
02/11/21 10:58
1,3-Dichloropropane
ug/kg
ND
5.0
1.6
02/11/21 10:58
1,4-Dichlorobenzene
ug/kg
ND
5.0
1.3
02/11/21 10:58
2,2-Dichloropropane
ug/kg
ND
5.0
1.6
02/11/21 10:58
2-Butanone (MEK)
ug/kg
ND
100
24.0
02/11/21 10:58
2-Chlorotoluene
ug/kg
ND
5.0
1.8
02/11/21 10:58
2-Hexanone
ug/kg
ND
50.0
4.8
02/11/21 10:58
4-Chlorotoluene
ug/kg
ND
5.0
0.88
02/11/21 10:58
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
4.8
02/11/21 10:58
Acetone
ug/kg
ND
100
32.1
02/11/21 10:58
Benzene
ug/kg
ND
5.0
2.0
02/11/21 10:58
Bromobenzene
ug/kg
ND
5.0
1.6
02/11/21 10:58
Bromochloromethane
ug/kg
ND
5.0
1.5
02/11/21 10:58
Bromodichloromethane
ug/kg
ND
5.0
1.9
02/11/21 10:58
Bromoform
ug/kg
ND
5.0
1.8
02/11/21 10:58
Bromomethane
ug/kg
ND
10.0
7.9
02/11/21 10:58
Carbon tetrachloride
ug/kg
ND
5.0
1.9
02/11/21 10:58
Chlorobenzene
ug/kg
ND
5.0
0.96
02/11/21 10:58
Chloroethane
ug/kg
ND
10.0
3.9
02/11/21 10:58
Chloroform
ug/kg
ND
5.0
3.0
02/11/21 10:58
Chloromethane
ug/kg
ND
10.0
4.2
02/11/21 10:58
cis-1,2-Dichloroethene
ug/kg
ND
5.0
1.7
02/11/21 10:58
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
METHOD BLANK: 3159501 Matrix: Solid
Associated Lab Samples: 92521577001, 92521577002, 92521577003, 92521577004, 92521577005, 92521577006, 92521577007,
92521577008,92521577009
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
cis-1,3-Dichloropropene
ug/kg
ND
5.0
1.4
02/11/21 10:58
Dibromochloromethane
ug/kg
ND
5.0
2.8
02/11/21 10:58
Dibromomethane
ug/kg
ND
5.0
1.1
02/11/21 10:58
Dichlorodifluoromethane
ug/kg
ND
10.0
2.2
02/11/21 10:58
Diisopropyl ether
ug/kg
ND
5.0
1.4
02/11/21 10:58
Ethylbenzene
ug/kg
ND
5.0
2.3
02/11/21 10:58
Hexachloro-1,3-butadiene
ug/kg
ND
10.0
8.2
02/11/21 10:58
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
1.7
02/11/21 10:58
m&p-Xylene
ug/kg
ND
10.0
3.4
02/11/21 10:58
Methyl-tert-butyl ether
ug/kg
ND
5.0
1.9
02/11/21 10:58
Methylene Chloride
ug/kg
ND
20.0
13.7
02/11/21 10:58
n-Butylbenzene
ug/kg
ND
5.0
2.4
02/11/21 10:58
n-Propylbenzene
ug/kg
ND
5.0
1.8
02/11/21 10:58
Naphthalene
ug/kg
ND
5.0
2.6
02/11/21 10:58
o-Xylene
ug/kg
ND
5.0
2.2
02/11/21 10:58
p-Isopropyltoluene
ug/kg
ND
5.0
2.5
02/11/21 10:58
sec-Butylbenzene
ug/kg
ND
5.0
2.2
02/11/21 10:58
Styrene
ug/kg
ND
5.0
1.3
02/11/21 10:58
tert-Butyl benzene
ug/kg
ND
5.0
1.8
02/11/21 10:58
Tetrachloroethene
ug/kg
ND
5.0
1.6
02/11/21 10:58
Toluene
ug/kg
ND
5.0
1.4
02/11/21 10:58
trans-1,2-Dichloroethene
ug/kg
ND
5.0
1.8
02/11/21 10:58
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
1.7
02/11/21 10:58
Trichloroethene
ug/kg
ND
5.0
1.3
02/11/21 10:58
Trichlorofluoromethane
ug/kg
ND
5.0
2.8
02/11/21 10:58
Vinyl acetate
ug/kg
ND
50.0
3.6
02/11/21 10:58
Vinyl chloride
ug/kg
ND
10.0
2.5
02/11/21 10:58
Xylene (Total)
ug/kg
ND
10.0
2.8
02/11/21 10:58
1,2-Dichloroethane-d4 (S)
%
103
70-130
02/11/21 10:58
4-Bromofluorobenzene (S)
%
99
69-134
02/11/21 10:58
Toluene-d8 (S)
%
101
70-130
02/11/21 10:58
LABORATORY CONTROL SAMPLE:
3159502
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
1250
1260
101
70-130
1,1,1-Trichloroethane
ug/kg
1250
1290
104
70-130
1,1,2,2-Tetrachloroethane
ug/kg
1250
1240
99
70-130
1,1,2-Trichloroethane
ug/kg
1250
1280
102
70-130
1,1-Dichloroethane
ug/kg
1250
1270
102
70-130
1,1-Dichloroethene
ug/kg
1250
1390
111
70-130
1,1-Dichloropropene
ug/kg
1250
1310
105
70-130
1,2,3-Trichlorobenzene
ug/kg
1250
1240
99
65-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
Parameter
3159502
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,3-Trichloropropane
ug/kg
1250
1210
97
70-130
1,2,4-Trichlorobenzene
ug/kg
1250
1280
102
68-130
1,2,4-Trimethylbenzene
ug/kg
1250
1270
102
70-130
1,2-Dibromo-3-chloropropane
ug/kg
1250
1170
94
70-130
1,2-Dibromoethane (EDB)
ug/kg
1250
1270
101
70-130
1,2-Dichlorobenzene
ug/kg
1250
1240
99
70-130
1,2-Dichloroethane
ug/kg
1250
1200
96
63-130
1,2-Dichloropropane
ug/kg
1250
1260
101
70-130
1,3,5-Trimethylbenzene
ug/kg
1250
1250
100
70-130
1,3-Dichlorobenzene
ug/kg
1250
1220
97
70-130
1,3-Dichloropropane
ug/kg
1250
1260
101
70-130
1,4-Dichlorobenzene
ug/kg
1250
1230
98
70-130
2,2-Dichloropropane
ug/kg
1250
1290
103
66-130
2-Butanone (MEK)
ug/kg
2500
2550
102
70-130
2-Chlorotoluene
ug/kg
1250
1290
103
70-130
2-Hexanone
ug/kg
2500
2480
99
70-130
4-Chlorotoluene
ug/kg
1250
1260
101
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
2500
2490
100
70-130
Acetone
ug/kg
2500
2440
98
69-130
Benzene
ug/kg
1250
1190
95
70-130
Bromobenzene
ug/kg
1250
1270
102
70-130
Bromochloromethane
ug/kg
1250
1140
91
70-130
Bromodichloromethane
ug/kg
1250
1280
102
69-130
Bromoform
ug/kg
1250
1320
105
70-130
Bromomethane
ug/kg
1250
1350
108
52-130
Carbon tetrachloride
ug/kg
1250
1320
106
70-130
Chlorobenzene
ug/kg
1250
1240
99
70-130
Chloroethane
ug/kg
1250
1270
101
65-130
Chloroform
ug/kg
1250
1220
98
70-130
Chloromethane
ug/kg
1250
1150
92
55-130
cis-1,2-Dichloroethene
ug/kg
1250
1240
99
70-130
cis-1,3-Dichloropropene
ug/kg
1250
1290
104
70-130
Dibromochloromethane
ug/kg
1250
1300
104
70-130
Dibromomethane
ug/kg
1250
1190
95
70-130
Dichlorodifluoromethane
ug/kg
1250
1380
111
45-156
Diisopropyl ether
ug/kg
1250
1190
95
70-130
Ethylbenzene
ug/kg
1250
1190
95
70-130
Hexachloro-1,3-butadiene
ug/kg
1250
1170
93
66-130
Isopropylbenzene (Cumene)
ug/kg
1250
1250
100
70-130
m&p-Xylene
ug/kg
2500
2450
98
70-130
Methyl-tert-butyl ether
ug/kg
1250
1240
99
70-130
Methylene Chloride
ug/kg
1250
1100
88
65-130
n-Butylbenzene
ug/kg
1250
1300
104
67-130
n-Propylbenzene
ug/kg
1250
1260
101
70-130
Naphthalene
ug/kg
1250
1280
102
70-130
o-Xylene
ug/kg
1250
1240
99
70-130
p-Isopropyltoluene
ug/kg
1250
1280
102
67-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
3159502
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
sec-Butylbenzene
ug/kg
1250
1240
99
69-130
Styrene
ug/kg
1250
1310
105
70-130
tert-Butyl benzene
ug/kg
1250
1160
92
67-130
Tetrachloroethene
ug/kg
1250
1220
98
70-130
Toluene
ug/kg
1250
1230
99
70-130
trans-1,2-Dichloroethene
ug/kg
1250
1260
101
70-130
trans- 1,3-Dichloropropene
ug/kg
1250
1300
104
68-130
Trichloroethene
ug/kg
1250
1310
105
70-130
Trichlorofluoromethane
ug/kg
1250
1280
102
70-130
Vinyl acetate
ug/kg
2500
2730
109
70-130
Vinyl chloride
ug/kg
1250
1240
99
61-130
Xylene (Total)
ug/kg
3750
3690
98
70-130
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
99
69-134
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3159503
3159504
MS
MSD
92521080001
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
1, 1, 1,2-Tetrachloroethane
ug/kg
ND
10100
10100
10900
11100
108
110
70-131
2
30
1,1,1-Trichloroethane
ug/kg
ND
10100
10100
11100
11600
110
114
65-133
4
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
10100
10100
10100
10400
100
103
66-130
3
30
1,1,2-Trichloroethane
ug/kg
ND
10100
10100
10800
11500
106
113
66-133
6
30
1,1-Dichloroethane
ug/kg
ND
10100
10100
10700
11000
106
109
65-130
3
30
1,1-Dichloroethene
ug/kg
ND
10100
10100
12000
12100
118
119
10-158
1
30
1,1-Dichloropropene
ug/kg
ND
10100
10100
11200
11600
110
114
68-133
3
30
1,2,3-Trichlorobenzene
ug/kg
ND
10100
10100
10500
10900
103
108
27-138
4
30
1,2,3-Trichloropropane
ug/kg
ND
10100
10100
9680
9740
96
96
67-130
1
30
1,2,4-Trichlorobenzene
ug/kg
ND
10100
10100
11100
11500
109
113
51-134
3
30
1,2,4-Trimethyl benzene
ug/kg
90700
10100
10100
112000
114000
206
235
63-136
3
30 E,M1
1,2-Dibromo-3-
ug/kg
ND
10100
10100
9580
9600
95
95
32-130
0
30
chloropropane
1,2-Dibromoethane (EDB)
ug/kg
ND
10100
10100
10700
10800
105
107
70-130
1
30
1,2-Dichlorobenzene
ug/kg
ND
10100
10100
10300
10700
102
106
69-130
4
30
1,2-Dichloroethane
ug/kg
ND
10100
10100
9960
10300
98
102
59-130
3
30
1,2-Dichloropropane
ug/kg
ND
10100
10100
10900
11200
108
111
70-130
3
30
1,3,5-Trimethyl benzene
ug/kg
29400
10100
10100
37000
37100
75
76
65-137
0
30
1,3-Dichlorobenzene
ug/kg
ND
10100
10100
10600
10800
105
107
70-130
2
30
1,3-Dichloropropane
ug/kg
ND
10100
10100
10400
10500
103
103
70-130
1
30
1,4-Dichlorobenzene
ug/kg
ND
10100
10100
10500
10800
104
107
68-130
2
30
2,2-Dichloropropane
ug/kg
ND
10100
10100
10100
10700
100
106
32-130
6
30
2-Butanone (MEK)
ug/kg
ND
20200
20200
20000
20700
92
95
10-136
3
30
2-Chlorotoluene
ug/kg
ND
10100
10100
13300
13400
131
132
69-141
1
30
2-Hexanone
ug/kg
ND
20200
20200
26500
29900
131
147
10-144
12
30 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3159503
3159504
MS
MSD
92521080001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
4-Chlorotoluene
ug/kg
ND
10100
10100
10800
11900
106
117
70-132
10
30
4-Methyl-2-pentanone
ug/kg
ND
20200
20200
26700
36500
130
179
25-143
31
30 M1,R1
(MIBK)
Acetone
ug/kg
153000
20200
20200
165000
171000
57
85
10-130
3
30
Benzene
ug/kg
9030
10100
10100
19900
19900
107
108
67-130
0
30
Bromobenzene
ug/kg
ND
10100
10100
10800
11000
106
109
70-130
2
30
Bromochloromethane
ug/kg
ND
10100
10100
9790
9990
97
99
69-134
2
30
Bromodichloromethane
ug/kg
ND
10100
10100
10800
10900
107
108
64-130
1
30
Bromoform
ug/kg
ND
10100
10100
10600
10800
104
107
62-130
3
30
Bromomethane
ug/kg
ND
10100
10100
12000
11600
118
115
20-176
3
30
Carbon tetrachloride
ug/kg
ND
10100
10100
11600
11600
114
115
65-140
1
30
Chlorobenzene
ug/kg
ND
10100
10100
10700
10900
105
108
70-130
2
30
Chloroethane
ug/kg
ND
10100
10100
9930
10200
98
100
10-130
2
30
Chloroform
ug/kg
ND
10100
10100
10100
10600
100
105
63-130
5
30
Chloromethane
ug/kg
ND
10100
10100
9970
10400
98
102
58-130
4
30
cis-1,2-Dichloroethene
ug/kg
ND
10100
10100
10400
10800
103
106
66-130
4
30
cis-1,3-Dichloropropene
ug/kg
ND
10100
10100
10800
10800
106
106
67-130
0
30
Dibromochloromethane
ug/kg
ND
10100
10100
11000
11400
109
113
67-130
4
30
Dibromomethane
ug/kg
ND
10100
10100
10000
10400
99
103
63-131
4
30
Dichlorodifluoromethane
ug/kg
ND
10100
10100
12500
12500
124
124
44-180
0
30
Diisopropyl ether
ug/kg
ND
10100
10100
9520
9830
94
97
63-130
3
30
Ethylbenzene
ug/kg
214
10100
10100
10500
10600
101
103
66-130
1
30
Hexachloro-1,3-butadiene
ug/kg
ND
10100
10100
14400
14500
142
143
64-150
0
30
Isopropylbenzene
ug/kg
1450
10100
10100
12400
12500
108
110
69-135
2
30
(Cumene)
m&p-Xylene
ug/kg
633
20200
20200
21700
21900
104
105
60-133
1
30
Methyl-tert-butyl ether
ug/kg
ND
10100
10100
9890
10300
98
102
65-130
4
30
Methylene Chloride
ug/kg
ND
10100
10100
9080
9490
87
91
61-130
4
30
n-Butylbenzene
ug/kg
3980
10100
10100
17200
17700
131
136
65-140
3
30
n-Propylbenzene
ug/kg
12400
10100
10100
23200
23700
106
111
67-140
2
30
Naphthalene
ug/kg
82000
10100
10100
95100
97700
129
155
15-145
3
30 M1
o-Xylene
ug/kg
1410
10100
10100
12100
12500
106
110
66-133
3
30
p-Isopropyltoluene
ug/kg
3820
10100
10100
15300
15400
114
114
56-147
0
30
sec-Butylbenzene
ug/kg
ND
10100
10100
12500
13500
123
133
65-139
8
30
Styrene
ug/kg
314
10100
10100
11800
11700
113
113
70-132
0
30
tert-Butylbenzene
ug/kg
ND
10100
10100
11500
11600
113
115
62-135
1
30
Tetrachloroethene
ug/kg
ND
10100
10100
10700
10800
106
106
70-135
0
30
Toluene
ug/kg
579
10100
10100
11400
11300
107
106
67-130
1
30
trans-1,2-Dichloroethene
ug/kg
ND
10100
10100
10900
11200
107
110
69-130
3
30
trans-1,3-Dichloropropene
ug/kg
ND
10100
10100
11000
11300
108
111
62-130
3
30
Trichloroethene
ug/kg
ND
10100
10100
11700
11800
116
116
70-135
1
30
Trichlorofluoromethane
ug/kg
ND
10100
10100
11600
12100
114
120
10-130
5
30
Vinyl acetate
ug/kg
ND
20200
20200
21100
22100
104
109
53-130
5
30
Vinyl chloride
ug/kg
ND
10100
10100
11200
11600
110
114
61-148
4
30
Xylene (Total)
ug/kg
2040
30300
30300
33900
34400
105
107
63-132
2
30
1,2-Dichloroethane-d4 (S)
%
94
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 41 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3159503 3159504
MS MSD
92521080001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
4-Bromofluorobenzene (S) % 98 98 69-134
Toluene-d8 (S) % 100 100 70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 42 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599428 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577010, 92521577011
METHOD BLANK: 3160220
Associated Lab Samples: 92521577010, 92521577011
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
1.9
02/15/21 12:22
1,1,1-Trichloroethane
ug/kg
ND
5.0
2.6
02/15/21 12:22
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
1.3
02/15/21 12:22
1,1,2-Trichloroethane
ug/kg
ND
5.0
1.7
02/15/21 12:22
1,1-Dichloroethane
ug/kg
ND
5.0
2.1
02/15/21 12:22
1,1-Dichloroethene
ug/kg
ND
5.0
2.1
02/15/21 12:22
1,1-Dichloropropene
ug/kg
ND
5.0
2.4
02/15/21 12:22
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
4.0
02/15/21 12:22
1,2,3-Trichloropropane
ug/kg
ND
5.0
2.5
02/15/21 12:22
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
4.2
02/15/21 12:22
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
1.4
02/15/21 12:22
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
1.9
02/15/21 12:22
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
2.2
02/15/21 12:22
1,2-Dichlorobenzene
ug/kg
ND
5.0
1.8
02/15/21 12:22
1,2-Dichloroethane
ug/kg
ND
5.0
3.3
02/15/21 12:22
1,2-Dichloropropane
ug/kg
ND
5.0
1.5
02/15/21 12:22
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
1.7
02/15/21 12:22
1,3-Dichlorobenzene
ug/kg
ND
5.0
1.6
02/15/21 12:22
1,3-Dichloropropane
ug/kg
ND
5.0
1.6
02/15/21 12:22
1,4-Dichlorobenzene
ug/kg
ND
5.0
1.3
02/15/21 12:22
2,2-Dichloropropane
ug/kg
ND
5.0
1.6
02/15/21 12:22
2-Butanone (MEK)
ug/kg
ND
100
24.0
02/15/21 12:22
2-Chlorotoluene
ug/kg
ND
5.0
1.8
02/15/21 12:22
2-Hexanone
ug/kg
ND
50.0
4.8
02/15/21 12:22
4-Chlorotoluene
ug/kg
ND
5.0
0.88
02/15/21 12:22
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
4.8
02/15/21 12:22
Acetone
ug/kg
ND
100
32.1
02/15/21 12:22
Benzene
ug/kg
ND
5.0
2.0
02/15/21 12:22
Bromobenzene
ug/kg
ND
5.0
1.6
02/15/21 12:22
Bromochloromethane
ug/kg
ND
5.0
1.5
02/15/21 12:22
Bromodichloromethane
ug/kg
ND
5.0
1.9
02/15/21 12:22
Bromoform
ug/kg
ND
5.0
1.8
02/15/21 12:22
Bromomethane
ug/kg
ND
10.0
7.9
02/15/21 12:22 v1
Carbon tetrachloride
ug/kg
ND
5.0
1.9
02/15/21 12:22
Chlorobenzene
ug/kg
ND
5.0
0.96
02/15/21 12:22
Chloroethane
ug/kg
ND
10.0
3.9
02/15/21 12:22
Chloroform
ug/kg
ND
5.0
3.0
02/15/21 12:22
Chloromethane
ug/kg
ND
10.0
4.2
02/15/21 12:22
cis-1,2-Dichloroethene
ug/kg
ND
5.0
1.7
02/15/21 12:22
cis-1,3-Dichloropropene
ug/kg
ND
5.0
1.4
02/15/21 12:22
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
METHOD BLANK: 3160220
Associated Lab Samples: 92521577010, 92521577011
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromochloromethane
ug/kg
ND
5.0
2.8
02/15/21 12:22
Dibromomethane
ug/kg
ND
5.0
1.1
02/15/21 12:22
Dichlorodifluoromethane
ug/kg
ND
10.0
2.2
02/15/21 12:22
Diisopropyl ether
ug/kg
ND
5.0
1.4
02/15/21 12:22
Ethylbenzene
ug/kg
ND
5.0
2.3
02/15/21 12:22
Hexachloro-1,3-butadiene
ug/kg
ND
10.0
8.2
02/15/21 12:22
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
1.7
02/15/21 12:22
m&p-Xylene
ug/kg
ND
10.0
3.4
02/15/21 12:22
Methyl-tert-butyl ether
ug/kg
ND
5.0
1.9
02/15/21 12:22
Methylene Chloride
ug/kg
ND
20.0
13.7
02/15/21 12:22
n-Butylbenzene
ug/kg
ND
5.0
2.4
02/15/21 12:22
n-Propylbenzene
ug/kg
ND
5.0
1.8
02/15/21 12:22
Naphthalene
ug/kg
ND
5.0
2.6
02/15/21 12:22
o-Xylene
ug/kg
ND
5.0
2.2
02/15/21 12:22
p-Isopropyltoluene
ug/kg
ND
5.0
2.5
02/15/21 12:22
sec-Butylbenzene
ug/kg
ND
5.0
2.2
02/15/21 12:22
Styrene
ug/kg
ND
5.0
1.3
02/15/21 12:22
tert-Butyl benzene
ug/kg
ND
5.0
1.8
02/15/21 12:22
Tetrachloroethene
ug/kg
ND
5.0
1.6
02/15/21 12:22
Toluene
ug/kg
ND
5.0
1.4
02/15/21 12:22
trans-1,2-Dichloroethene
ug/kg
ND
5.0
1.8
02/15/21 12:22
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
1.7
02/15/21 12:22
Trichloroethene
ug/kg
ND
5.0
1.3
02/15/21 12:22
Trichlorofluoromethane
ug/kg
ND
5.0
2.8
02/15/21 12:22
Vinyl acetate
ug/kg
ND
50.0
3.6
02/15/21 12:22
Vinyl chloride
ug/kg
ND
10.0
2.5
02/15/21 12:22
Xylene (Total)
ug/kg
ND
10.0
2.8
02/15/21 12:22
1,2-Dichloroethane-d4 (S)
%
108
70-130
02/15/21 12:22
4-Bromofluorobenzene (S)
%
100
69-134
02/15/21 12:22
Toluene-d8 (S)
%
99
70-130
02/15/21 12:22
Qualifiers
LABORATORY CONTROL SAMPLE:
3160221
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
1250
1210
97
70-130
1,1,1-Trichloroethane
ug/kg
1250
1240
99
70-130
1,1,2,2-Tetrachloroethane
ug/kg
1250
1140
91
70-130
1,1,2-Trichloroethane
ug/kg
1250
1170
93
70-130
1,1-Dichloroethane
ug/kg
1250
1190
95
70-130
1,1-Dichloroethene
ug/kg
1250
1270
102
70-130
1,1-Dichloropropene
ug/kg
1250
1220
97
70-130
1,2,3-Trichlorobenzene
ug/kg
1250
1150
92
65-130
1,2,3-Trichloropropane
ug/kg
1250
1110
89
70-130
1,2,4-Trichlorobenzene
ug/kg
1250
1170
94
68-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
Parameter
3160221
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trimethylbenzene
ug/kg
1250
1150
92
70-130
1,2-Dibromo-3-chloropropane
ug/kg
1250
1110
89
70-130
1,2-Dibromoethane (EDB)
ug/kg
1250
1190
95
70-130
1,2-Dichlorobenzene
ug/kg
1250
1130
91
70-130
1,2-Dichloroethane
ug/kg
1250
1150
92
63-130
1,2-Dichloropropane
ug/kg
1250
1150
92
70-130
1,3,5-Trimethylbenzene
ug/kg
1250
1140
91
70-130
1,3-Dichlorobenzene
ug/kg
1250
1140
91
70-130
1,3-Dichloropropane
ug/kg
1250
1150
92
70-130
1,4-Dichlorobenzene
ug/kg
1250
1150
92
70-130
2,2-Dichloropropane
ug/kg
1250
1230
98
66-130
2-Butanone (MEK)
ug/kg
2500
2330
93
70-130
2-Chlorotoluene
ug/kg
1250
1190
95
70-130
2-Hexanone
ug/kg
2500
2240
89
70-130
4-Chlorotoluene
ug/kg
1250
1160
93
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
2500
2220
89
70-130
Acetone
ug/kg
2500
2220
89
69-130
Benzene
ug/kg
1250
1090
87
70-130
Bromobenzene
ug/kg
1250
1190
95
70-130
Bromochloromethane
ug/kg
1250
1090
87
70-130
Bromodichloromethane
ug/kg
1250
1200
96
69-130
Bromoform
ug/kg
1250
1290
103
70-130
Bromomethane
ug/kg
1250
1490
119
52-130 v1
Carbon tetrachloride
ug/kg
1250
1240
99
70-130
Chlorobenzene
ug/kg
1250
1160
93
70-130
Chloroethane
ug/kg
1250
1160
93
65-130
Chloroform
ug/kg
1250
1130
91
70-130
Chloromethane
ug/kg
1250
1060
84
55-130
cis-1,2-Dichloroethene
ug/kg
1250
1150
92
70-130
cis-1,3-Dichloropropene
ug/kg
1250
1170
94
70-130
Dibromochloromethane
ug/kg
1250
1260
101
70-130
Dibromomethane
ug/kg
1250
1140
91
70-130
Dichlorodifluoromethane
ug/kg
1250
1240
99
45-156
Diisopropyl ether
ug/kg
1250
1100
88
70-130
Ethylbenzene
ug/kg
1250
1100
88
70-130
Hexachloro-1,3-butadiene
ug/kg
1250
1070
86
66-130
Isopropylbenzene (Cumene)
ug/kg
1250
1150
92
70-130
m&p-Xylene
ug/kg
2500
2250
90
70-130
Methyl-tert-butyl ether
ug/kg
1250
1140
91
70-130
Methylene Chloride
ug/kg
1250
1010
81
65-130
n-Butylbenzene
ug/kg
1250
1150
92
67-130
n-Propylbenzene
ug/kg
1250
1120
90
70-130
Naphthalene
ug/kg
1250
1170
93
70-130
o-Xylene
ug/kg
1250
1150
92
70-130
p-Isopropyltoluene
ug/kg
1250
1160
93
67-130
sec-Butylbenzene
ug/kg
1250
1110
89
69-130
Styrene
ug/kg
1250
1230
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
Parameter
3160221
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
tert-Butyl benzene
ug/kg
1250
1100
88
67-130
Tetrachloroethene
ug/kg
1250
1150
92
70-130
Toluene
ug/kg
1250
1120
90
70-130
trans-1,2-Dichloroethene
ug/kg
1250
1160
93
70-130
trans- 1,3-Dichloropropene
ug/kg
1250
1190
96
68-130
Trichloroethene
ug/kg
1250
1220
98
70-130
Trichlorofluoromethane
ug/kg
1250
1260
101
70-130
Vinyl acetate
ug/kg
2500
2450
98
70-130
Vinyl chloride
ug/kg
1250
1120
90
61-130
Xylene (Total)
ug/kg
3750
3400
91
70-130
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
100
69-134
Toluene-d8 (S)
%
99
70-130
MATRIX SPIKE SAMPLE:
Parameter
3160223
Units
92521639001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
637
788
124
70-131
1,1,1-Trichloroethane
ug/kg
ND
637
747
117
65-133
1,1,2,2-Tetrachloroethane
ug/kg
ND
637
657
103
66-130
1,1,2-Trichloroethane
ug/kg
ND
637
683
107
66-133
1,1-Dichloroethane
ug/kg
ND
637
688
108
65-130
1,1-Dichloroethene
ug/kg
ND
637
747
117
10-158
1,1-Dichloropropene
ug/kg
ND
637
691
109
68-133
1,2,3-Trichlorobenzene
ug/kg
ND
637
634
100
27-138
1,2,3-Trichloropropane
ug/kg
ND
637
539
85
67-130
1,2,4-Trichlorobenzene
ug/kg
ND
637
625
98
51-134
1,2,4-Trimethylbenzene
ug/kg
ND
637
643
101
63-136
1,2-Dibromo-3-chloropropane
ug/kg
ND
637
611
96
32-130
1,2-Dibromoethane (EDB)
ug/kg
ND
637
687
108
70-130
1,2-Dichlorobenzene
ug/kg
ND
637
635
100
69-130
1,2-Dichloroethane
ug/kg
ND
637
674
106
59-130
1,2-Dichloropropane
ug/kg
ND
637
700
110
70-130
1,3,5-Trimethylbenzene
ug/kg
ND
637
638
100
65-137
1,3-Dichlorobenzene
ug/kg
ND
637
624
98
70-130
1,3-Dichloropropane
ug/kg
ND
637
671
105
70-130
1,4-Dichlorobenzene
ug/kg
ND
637
612
96
68-130
2,2-Dichloropropane
ug/kg
ND
637
224
35
32-130
2-Butanone (MEK)
ug/kg
ND
1270
1170
92
10-136
2-Chlorotoluene
ug/kg
ND
637
647
102
69-141
2-Hexanone
ug/kg
ND
1270
1160
91
10-144
4-Chlorotoluene
ug/kg
ND
637
607
95
70-132
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
1270
1230
96
25-143
Acetone
ug/kg
ND
1270
1250
98
10-130
Benzene
ug/kg
ND
637
658
103
67-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
MATRIX SPIKE SAMPLE:
3160223
92521639001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromobenzene
ug/kg
ND
637
655
103
70-130
Bromochloromethane
ug/kg
ND
637
636
100
69-134
Bromodichloromethane
ug/kg
ND
637
691
109
64-130
Bromoform
ug/kg
ND
637
661
104
62-130
Bromomethane
ug/kg
ND
637
768
121
20-176 v1
Carbon tetrachloride
ug/kg
ND
637
704
111
65-140
Chlorobenzene
ug/kg
ND
637
661
104
70-130
Chloroethane
ug/kg
ND
637
186
29
10-130
Chloroform
ug/kg
ND
637
671
105
63-130
Chloromethane
ug/kg
ND
637
671
105
58-130
cis-1,2-Dichloroethene
ug/kg
ND
637
674
106
66-130
cis-1,3-Dichloropropene
ug/kg
ND
637
534
84
67-130
Dibromochloromethane
ug/kg
ND
637
721
113
67-130
Dibromomethane
ug/kg
ND
637
648
102
63-131
Dichlorodifluoromethane
ug/kg
ND
637
700
110
44-180
Diisopropyl ether
ug/kg
ND
637
635
100
63-130
Ethylbenzene
ug/kg
ND
637
644
101
66-130
Hexachloro-1,3-butadiene
ug/kg
ND
637
529
83
64-150
Isopropylbenzene (Cumene)
ug/kg
ND
637
695
109
69-135
m&p-Xylene
ug/kg
ND
1270
1330
105
60-133
Methyl-tert-butyl ether
ug/kg
47.1
637
697
102
65-130
Methylene Chloride
ug/kg
ND
637
616
97
61-130
n-Butylbenzene
ug/kg
ND
637
590
93
65-140
n-Propylbenzene
ug/kg
ND
637
630
99
67-140
Naphthalene
ug/kg
ND
637
699
110
15-145
o-Xylene
ug/kg
ND
637
708
111
66-133
p-Isopropyltoluene
ug/kg
ND
637
636
100
56-147
sec-Butylbenzene
ug/kg
ND
637
631
99
65-139
Styrene
ug/kg
ND
637
720
113
70-132
tert-Butyl benzene
ug/kg
ND
637
628
99
62-135
Tetrachloroethene
ug/kg
ND
637
618
97
70-135
Toluene
ug/kg
ND
637
702
110
67-130
trans-1,2-Dichloroethene
ug/kg
ND
637
633
99
69-130
trans- 1,3-Dichloropropene
ug/kg
ND
637
787
124
62-130
Trichloroethene
ug/kg
ND
637
711
112
70-135
Trichlorofluoromethane
ug/kg
ND
637
267
42
10-130
Vinyl acetate
ug/kg
ND
1270
1070
84
53-130
Vinyl chloride
ug/kg
ND
637
698
110
61-148
Xylene (Total)
ug/kg
ND
1910
2040
107
63-132
1,2-Dichloroethane-d4 (S)
%
104
70-130
4-Bromofluorobenzene (S)
%
101
69-134
Toluene-d8 (S)
%
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 65

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
SAMPLE DUPLICATE: 3160222
Parameter
Units
92521577010
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,1-Trichloroethane
ug/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,2-Trichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethene
ug/kg
ND
ND
30
1,1-Dichloropropene
ug/kg
ND
ND
30
1,2,3-Trichlorobenzene
ug/kg
ND
ND
30
1,2,3-Trichloropropane
ug/kg
ND
ND
30
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2,4-Trimethylbenzene
ug/kg
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
30
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,2-Dichloroethane
ug/kg
ND
ND
30
1,2-Dichloropropane
ug/kg
ND
ND
30
1,3,5-Trimethylbenzene
ug/kg
5.1J
5.9J
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichloropropane
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
2,2-Dichloropropane
ug/kg
ND
ND
30
2-Butanone (MEK)
ug/kg
ND
ND
30
2-Chlorotoluene
ug/kg
ND
ND
30
2-Hexanone
ug/kg
ND
ND
30
4-Chlorotoluene
ug/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
30
Acetone
ug/kg
ND
ND
30
Benzene
ug/kg
ND
ND
30
Bromobenzene
ug/kg
ND
ND
30
Bromochloromethane
ug/kg
ND
ND
30
Bromodichloromethane
ug/kg
ND
ND
30
Bromoform
ug/kg
ND
ND
30
Bromomethane
ug/kg
ND
ND
30 v1
Carbon tetrachloride
ug/kg
ND
ND
30
Chlorobenzene
ug/kg
ND
ND
30
Chloroethane
ug/kg
ND
ND
30
Chloroform
ug/kg
ND
ND
30
Chloromethane
ug/kg
ND
ND
30
cis-1,2-Dichloroethene
ug/kg
ND
ND
30
cis-1,3-Dichloropropene
ug/kg
ND
ND
30
Dibromochloromethane
ug/kg
ND
ND
30
Dibromomethane
ug/kg
ND
ND
30
Dichlorodifluoromethane
ug/kg
ND
ND
30
Diisopropyl ether
ug/kg
ND
ND
30
Ethylbenzene
ug/kg
ND
ND
30
Hexachloro-1,3-butadiene
ug/kg
ND
ND
30
Isopropylbenzene (Cumene)
ug/kg
ND
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
SAMPLE DUPLICATE: 3160222
Parameter
Units
92521577010
Result
Dup
Result
m&p-Xylene
ug/kg
ND
ND
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
ND
ND
p-Isopropyltoluene
ug/kg
ND
ND
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
ND
ND
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
106
106
4-Bromofluorobenzene (S)
%
103
102
Toluene-d8(S)
%
102
101
Max
RPD RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 49 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599380
Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546
Analysis Description: 8015 Solid GCSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577001, 92521577002,
92521577003, 92521577004, 92521577005, 92521577006
METHOD BLANK: 3159913
Matrix: Solid
Associated Lab Samples: 92521577001, 92521577002,
92521577003, 92521577004, 92521577005, 92521577006
Blank Reporting
Parameter
Units
Result Limit MDL Analyzed
Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND 4.9 2.3 02/12/21 11:09
n-Pentacosane (S)
%
79 32-130 02/12/21 11:09
LABORATORY CONTROL SAMPLE:
3159914
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
67.1 41.7 62 47-130
n-Pentacosane (S)
%
100 32-130
MATRIX SPIKE SAMPLE:
3159915
92521577001 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
3040 87.2 3260 259
10-133 M1
n-Pentacosane(S)
%
96
32-130
SAMPLE DUPLICATE: 3159916
92521577002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Diesel Range Organics(C10-C28) mg/kg 2040 1500 30 30
n-Pentacosane (S) % 0 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 50 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599953 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
METHOD BLANK: 3162680 Matrix: Solid
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
328
75.1
02/16/21 08:54
1,2-Dichlorobenzene
ug/kg
ND
328
70.9
02/16/21 08:54
1,3-Dichlorobenzene
ug/kg
ND
328
73.8
02/16/21 08:54
1,4-Dichlorobenzene
ug/kg
ND
328
72.1
02/16/21 08:54
1-Methylnaphthalene
ug/kg
ND
328
87.3
02/16/21 08:54
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
328
91.1
02/16/21 08:54
2,4,5-Trichlorophenol
ug/kg
ND
328
85.1
02/16/21 08:54
2,4,6-Trichlorophenol
ug/kg
ND
328
82.4
02/16/21 08:54
2,4-Dichlorophenol
ug/kg
ND
328
108
02/16/21 08:54
2,4-Dimethylphenol
ug/kg
ND
328
81.7
02/16/21 08:54
2,4-Dinitrophenol
ug/kg
ND
1640
1050
02/16/21 08:54
2,4-Dinitrotoluene
ug/kg
ND
328
86.8
02/16/21 08:54
2,6-Dinitrotoluene
ug/kg
ND
328
85.7
02/16/21 08:54
2-Chloronaphthalene
ug/kg
ND
328
73.0
02/16/21 08:54
2-Chlorophenol
ug/kg
ND
328
76.3
02/16/21 08:54
2-Methylnaphthalene
ug/kg
ND
328
83.4
02/16/21 08:54
2-Methylphenol(o-Cresol)
ug/kg
ND
328
72.6
02/16/21 08:54
2-Nitroaniline
ug/kg
ND
1640
165
02/16/21 08:54
2-Nitrophenol
ug/kg
ND
328
101
02/16/21 08:54
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
328
82.5
02/16/21 08:54
3,3'-Dichlorobenzidine
ug/kg
ND
656
228
02/16/21 08:54
3-Nitroaniline
ug/kg
ND
1640
174
02/16/21 08:54
4,6-Dinitro-2-methyl phenol
ug/kg
ND
656
528
02/16/21 08:54
4-Bromophenylphenyl ether
ug/kg
ND
328
86.0
02/16/21 08:54
4-ChIoro-3-methyl phenol
ug/kg
ND
656
200
02/16/21 08:54
4-Chloroaniline
ug/kg
ND
656
201
02/16/21 08:54
4-Chlorophenylphenyl ether
ug/kg
ND
328
85.1
02/16/21 08:54
4-Nitroaniline
ug/kg
ND
656
162
02/16/21 08:54
4-Nitrophenol
ug/kg
ND
1640
523
02/16/21 08:54
Acenaphthene
ug/kg
ND
328
84.3
02/16/21 08:54
Acenaphthylene
ug/kg
ND
328
77.6
02/16/21 08:54
Aniline
ug/kg
ND
328
73.6
02/16/21 08:54
Anthracene
ug/kg
ND
328
85.0
02/16/21 08:54
Benzo(a)anthracene
ug/kg
ND
328
104
02/16/21 08:54
Benzo(a)pyrene
ug/kg
ND
328
142
02/16/21 08:54
Benzo(b)fluoranthene
ug/kg
ND
328
132
02/16/21 08:54
Benzo(g,h,i)perylene
ug/kg
ND
328
128
02/16/21 08:54
Benzo(k)fluoranthene
ug/kg
ND
328
138
02/16/21 08:54
Benzoic Acid
ug/kg
ND
1640
354
02/16/21 08:54
Benzyl alcohol
ug/kg
ND
656
174
02/16/21 08:54
IL
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
METHOD BLANK: 3162680 Matrix: Solid
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
bis(2-Chloroethoxy)methane
ug/kg
ND
328
87.5
02/16/21 08:54
bis(2-Chloroethyl) ether
ug/kg
ND
328
69.6
02/16/21 08:54
bis(2-Ethylhexyl)phthalate
ug/kg
ND
328
107
02/16/21 08:54
Butylbenzylphthalate
ug/kg
ND
328
87.3
02/16/21 08:54
Chrysene
ug/kg
ND
328
95.2
02/16/21 08:54
Di-n-butylphthalate
ug/kg
ND
328
80.9
02/16/21 08:54
Di-n-octylphthalate
ug/kg
ND
328
187
02/16/21 08:54
Dibenz(a,h)anthracene
ug/kg
ND
328
131
02/16/21 08:54
Dibenzofuran
ug/kg
ND
328
82.0
02/16/21 08:54
Diethylphthalate
ug/kg
ND
328
71.1
02/16/21 08:54
Dimethylphthalate
ug/kg
ND
328
74.1
02/16/21 08:54
Fluoranthene
ug/kg
ND
328
99.0
02/16/21 08:54
Fluorene
ug/kg
ND
328
87.7
02/16/21 08:54
Hexachloro-1,3-butadiene
ug/kg
ND
328
79.7
02/16/21 08:54
Hexachlorobenzene
ug/kg
ND
328
83.2
02/16/21 08:54
Hexachlorocyclopentadiene
ug/kg
ND
328
131
02/16/21 08:54
Hexachloroethane
ug/kg
ND
328
74.7
02/16/21 08:54
Indeno(1,2,3-cd)pyrene
ug/kg
ND
328
150
02/16/21 08:54
Isophorone
ug/kg
ND
328
71.2
02/16/21 08:54
N-Nitroso-di-n-propylamine
ug/kg
ND
328
91.8
02/16/21 08:54
N-Nitrosodimethylamine
ug/kg
ND
328
92.2
02/16/21 08:54
N-Nitrosodiphenylamine
ug/kg
ND
328
83.6
02/16/21 08:54
Naphthalene
ug/kg
ND
328
78.5
02/16/21 08:54
Nitrobenzene
ug/kg
ND
328
78.3
02/16/21 08:54
Pentachlorophenol
ug/kg
ND
656
150
02/16/21 08:54
Phenanthrene
ug/kg
ND
328
82.5
02/16/21 08:54
Phenol
ug/kg
ND
328
78.3
02/16/21 08:54
Pyrene
ug/kg
ND
328
90.2
02/16/21 08:54
Pyridine
ug/kg
ND
328
82.9
02/16/21 08:54
2,4,6-Tribromophenol (S)
%
85
18-130
02/16/21 08:54
2-Fluorobiphenyl (S)
%
73
19-130
02/16/21 08:54
2-Fluorophenol (S)
%
69
18-130
02/16/21 08:54
Nitrobenzene-d5 (S)
%
80
21-130
02/16/21 08:54
Phenol-d6 (S)
%
71
18-130
02/16/21 08:54
Terphenyl-d14 (S)
%
102
15-130
02/16/21 08:54
Qualifiers
LABORATORY CONTROL SAMPLE:
3162681
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1640
1470
89
47-130
1,2-Dichlorobenzene
ug/kg
1640
1380
84
49-130
1,3-Dichlorobenzene
ug/kg
1640
1350
82
48-130
1,4-Dichlorobenzene
ug/kg
1640
1370
84
49-130
1-Methylnaphthalene
ug/kg
1640
1380
84
54-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
Parameter
3162681
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,2'-Oxybis(1-chloropropane)
ug/kg
1640
1440
87
38-130
2,4,5-Trichlorophenol
ug/kg
1640
1400
85
49-130
2,4,6-Trichlorophenol
ug/kg
1640
1430
87
50-130
2,4-Dichlorophenol
ug/kg
1640
1480
90
51-130
2,4-Dimethylphenol
ug/kg
1640
1550
94
53-130
2,4-Dinitrophenol
ug/kg
8220
6530
79
39-130
2,4-Dinitrotoluene
ug/kg
1640
1470
89
53-130
2,6-Dinitrotoluene
ug/kg
1640
1470
89
55-130
2-Chloronaphthalene
ug/kg
1640
1360
83
48-130
2-Chlorophenol
ug/kg
1640
1350
82
54-130
2-Methylnaphthalene
ug/kg
1640
1410
86
57-130
2-Methylphenol(o-Cresol)
ug/kg
1640
1290
78
50-130
2-Nitroaniline
ug/kg
3290
2860
87
49-130
2-Nitrophenol
ug/kg
1640
1420
86
50-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1640
1440
88
50-130
3,3'-Dichlorobenzidine
ug/kg
3290
2550
77
47-130
3-Nitroaniline
ug/kg
3290
2370
72
45-130IL
4,6-Dinitro-2-methyl phenol
ug/kg
3290
2900
88
50-142
4-Bromophenylphenyl ether
ug/kg
1640
1540
94
55-130
4-ChIoro-3-methyl phenol
ug/kg
3290
3070
93
52-130
4-Chloroaniline
ug/kg
3290
2630
80
49-130
4-Chlorophenylphenyl ether
ug/kg
1640
1510
92
53-130
4-Nitroaniline
ug/kg
3290
2540
77
51-130
4-Nitrophenol
ug/kg
8220
8670
105
40-130
Acenaphthene
ug/kg
1640
1390
84
56-130
Acenaphthylene
ug/kg
1640
1370
83
58-130
Aniline
ug/kg
1640
1240
75
44-130
Anthracene
ug/kg
1640
1420
86
60-130
Benzo(a)anthracene
ug/kg
1640
1500
91
59-130
Benzo(a)pyrene
ug/kg
1640
1520
92
57-130
Benzo(b)fluoranthene
ug/kg
1640
1520
92
54-130
Benzo(g,h,i)perylene
ug/kg
1640
1480
90
59-130
Benzo(k)fluoranthene
ug/kg
1640
1450
88
54-130
Benzoic Acid
ug/kg
8220
4550
55
19-130
Benzyl alcohol
ug/kg
3290
2780
84
50-130
bis(2-Chloroethoxy)methane
ug/kg
1640
1340
81
55-130
bis(2-Chloroethyl) ether
ug/kg
1640
1360
82
53-130
bis(2-Ethylhexyl)phthalate
ug/kg
1640
1460
89
58-130
Butylbenzylphthalate
ug/kg
1640
1510
92
46-138
Chrysene
ug/kg
1640
1370
83
57-130
Di-n-butylphthalate
ug/kg
1640
1480
90
57-130
Di-n-octylphthalate
ug/kg
1640
1570
95
57-130
Dibenz(a,h)anthracene
ug/kg
1640
1530
93
60-130
Dibenzofuran
ug/kg
1640
1400
85
54-130
Diethylphthalate
ug/kg
1640
1470
89
55-130
Dimethylphthalate
ug/kg
1640
1430
87
57-130
Fluoranthene
ug/kg
1640
1520
92
57-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
Parameter
3162681
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Fluorene
ug/kg
1640
1440
88
56-130
Hexachloro-1,3-butadiene
ug/kg
1640
1610
98
41-130
Hexachlorobenzene
ug/kg
1640
1560
95
53-130
Hexachlorocyclopentadiene
ug/kg
1640
1210
74
23-130
Hexachloroethane
ug/kg
1640
1430
87
48-130
Indeno(1,2,3-cd)pyrene
ug/kg
1640
1550
94
61-130
Isophorone
ug/kg
1640
1470
90
49-130
N-Nitroso-di-n-propylamine
ug/kg
1640
1520
92
52-130
N-Nitrosodimethylamine
ug/kg
1640
1320
80
45-130
N-Nitrosodiphenylamine
ug/kg
1640
1420
86
56-130
Naphthalene
ug/kg
1640
1390
84
56-130
Nitrobenzene
ug/kg
1640
1500
91
50-130
Pentachlorophenol
ug/kg
3290
2750
84
33-130
Phenanthrene
ug/kg
1640
1440
88
60-130
Phenol
ug/kg
1640
1430
87
54-130
Pyrene
ug/kg
1640
1470
89
61-130
Pyridine
ug/kg
1640
1030
63
35-130
2,4,6-Tribromophenol (S)
%
98
18-130
2-Fluorobiphenyl (S)
%
83
19-130
2-Fluorophenol (S)
%
82
18-130
Nitrobenzene-d5(S)
%
91
21-130
Phenol-d6 (S)
%
84
18-130
Terphenyl-d14(S)
%
106
15-130
Qualifiers
SAMPLE DUPLICATE: 3162683
Parameter
Units
92522099001
Result
Dup
Result RPD
Max
RPD
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
1-Methylnaphthalene
ug/kg
ND
ND
30
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
30
2,4,5-Trichlorophenol
ug/kg
ND
ND
30
2,4,6-Trichlorophenol
ug/kg
ND
ND
30
2,4-Dichlorophenol
ug/kg
ND
ND
30
2,4-Dimethylphenol
ug/kg
ND
ND
30
2,4-Dinitrophenol
ug/kg
ND
ND
30
2,4-Dinitrotoluene
ug/kg
ND
ND
30
2,6-Dinitrotoluene
ug/kg
ND
ND
30
2-Chloronaphthalene
ug/kg
ND
ND
30
2-Chlorophenol
ug/kg
ND
ND
30
2-Methylnaphthalene
ug/kg
0.11J mg/kg
ND
30
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
30
2-Nitroaniline
ug/kg
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 65

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
SAMPLE DUPLICATE: 3162683
Parameter
Units
92522099001
Result
Dup
Result RPD
Max
RPD Qualifiers
2-Nitrophenol
ug/kg
ND
ND
30
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
30
3,3'-Dichlorobenzidine
ug/kg
ND
ND
30
3-Nitroaniline
ug/kg
ND
ND
30 IL
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
30
4-Bromophenylphenyl ether
ug/kg
ND
ND
30
4-Chloro-3-methylphenol
ug/kg
ND
ND
30
4-Chloroaniline
ug/kg
ND
ND
30
4-Chlorophenylphenyl ether
ug/kg
ND
ND
30
4-Nitroaniline
ug/kg
ND
ND
30
4-Nitrophenol
ug/kg
ND
ND
30
Acenaphthene
ug/kg
ND
ND
30
Acenaphthylene
ug/kg
ND
ND
30
Aniline
ug/kg
ND
ND
30
Anthracene
ug/kg
ND
ND
30
Benzo(a)anthracene
ug/kg
ND
ND
30
Benzo(a)pyrene
ug/kg
ND
ND
30
Benzo(b)fluoranthene
ug/kg
ND
ND
30
Benzo(g,h,i)perylene
ug/kg
ND
ND
30
Benzo(k)fluoranthene
ug/kg
ND
ND
30
Benzoic Acid
ug/kg
ND
ND
30
Benzyl alcohol
ug/kg
ND
ND
30
bis(2-Chloroethoxy)methane
ug/kg
ND
ND
30
bis(2-Chloroethyl) ether
ug/kg
ND
ND
30
bis(2-Ethylhexyl)phthalate
ug/kg
ND
ND
30
Butylbenzylphthalate
ug/kg
ND
ND
30
Chrysene
ug/kg
ND
ND
30
Di-n-butylphthalate
ug/kg
ND
ND
30
Di-n-octylphthalate
ug/kg
ND
ND
30
Dibenz(a,h)anthracene
ug/kg
ND
ND
30
Dibenzofuran
ug/kg
ND
ND
30
Diethylphthalate
ug/kg
ND
ND
30
Dimethylphthalate
ug/kg
ND
ND
30
Fluoranthene
ug/kg
ND
ND
30
Fluorene
ug/kg
ND
ND
30
Hexachloro-1,3-butadiene
ug/kg
ND
ND
30
Hexachlorobenzene
ug/kg
ND
ND
30
Hexachlorocyclopentadiene
ug/kg
ND
ND
30
Hexachloroethane
ug/kg
ND
ND
30
Indeno(1,2,3-cd)pyrene
ug/kg
ND
ND
30
Isophorone
ug/kg
ND
ND
30
N-Nitroso-di-n-propylamine
ug/kg
ND
ND
30
N-Nitrosodimethylamine
ug/kg
ND
ND
30 v1
N-Nitrosodiphenylamine
ug/kg
ND
ND
30
Naphthalene
ug/kg
ND
ND
30
Nitrobenzene
ug/kg
ND
ND
30
Pentachlorophenol
ug/kg
ND
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
SAMPLE DUPLICATE: 3162683
Parameter
Phenanthrene
Phenol
Pyrene
Pyridine
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
Units
92522099001
Result
Dup
Result
ug/kg
ND
ND
ug/kg
ND
ND
ug/kg
ND
ND
ug/kg
ND
ND
%
82
96
%
65
78
63
66
%
70
80
%
61
67
%
84
99
Max
RPD RPD Qualifiers
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 56 of 65

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599982 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
METHOD BLANK: 3162933
Matrix:
Solid
Associated Lab Samples:
92521577007, 92521577008,
92521577009, 92521577010, 92521577011
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
10.1 10.1
02/16/21 09:22 N2
Aliphatic (C19-C36)
mg/kg
ND
10.1 10.1
02/16/21 09:22 N2
Aromatic (C11-C22)
mg/kg
ND
10.1 10.1
02/16/21 09:22 N2
1-Chlorooctadecane (S)
%
54
40-140
02/16/21 09:22
2-Bromonaphthalene (S)
%
93
40-140
02/16/21 09:22
2-Fluorobiphenyl (S)
%
93
40-140
02/16/21 09:22
o-Terphenyl (S)
%
73
40-140
02/16/21 09:22
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
3162934
Units
Spike
Conc.
3162935
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec Max
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
9.9
ND ND
68
68
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.2
ND 10.1
74
76
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28.1
17.1 18.5
61
66
40-140 8 50 N2
1-Chlorooctadecane (S)
%
67
71
40-140
2-Bromonaphthalene (S)
%
90
98
40-140
2-Fluorobiphenyl (S)
%
90
98
40-140
o-Terphenyl(S)
%
66
76
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 57 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599437 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577001, 92521577002, 92521577003, 92521577004, 92521577005, 92521577006, 92521577007,
92521577008,92521577009,92521577010,92521577011
SAMPLE DUPLICATE: 3160252
92521440001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 25.2 25.0 1 25 N2
SAMPLE DUPLICATE: 3160253
92521628001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 13.0 12.8 1 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 58 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 1622568 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
METHOD BLANK: R3624121-1 Matrix: Solid
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Solids % 0.00100 02/22/21 11:36
LABORATORY CONTROL SAMPLE: R3624121-2
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Solids % 50.0 50.0 100 85.0-115
SAMPLE DUPLICATE: R3624121-3
L1317135-05 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Solids % 78.3 77.1 1.52 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
J Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
ST Surrogate recovery was above laboratory control limits. Results may be biased high.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
CAMP STEWARD ROAD SITE
92521577
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92521577001
#3 NS (4-4.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577002
#3 SS (4-4.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577003
#2 NS (4-4.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577004
#2 SS (4-4.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577005
#1 NS (5.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577006
#1 SS (5.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577007
#2 NW (6.5-7)
MADEP EPH
599982
MADEP EPH
600346
92521577008
#2 SW (6.5-7)
MADEP EPH
599982
MADEP EPH
600346
92521577009
#2 EW (6.5-7)
MADEP EPH
599982
MADEP EPH
600346
92521577010
#2 WW (6.5-7)
MADEP EPH
599982
MADEP EPH
600346
92521577011
#2 BASE (15.0)
MADEP EPH
599982
MADEP EPH
600346
92521577007
#2 NW (6.5-7)
MADEPV
1621956
MADEP VPH
1621956
92521577008
#2 SW (6.5-7)
MADEPV
1621454
MADEP VPH
1621454
92521577009
#2 EW (6.5-7)
MADEPV
1621454
MADEP VPH
1621454
92521577010
#2 WW (6.5-7)
MADEPV
1621956
MADEP VPH
1621956
92521577011
#2 BASE (15.0)
MADEPV
1621956
MADEP VPH
1621956
92521577011
#2 BASE (15.0)
MADEPV
1623520
MADEP VPH
1623520
92521577001
#3 NS (4-4.5)
EPA 5030B
599422
EPA 8015C Modified
599467
92521577002
#3 SS (4-4.5)
EPA 5030B
599699
EPA 8015C Modified
599714
92521577003
#2 NS (4-4.5)
EPA 5030B
599699
EPA 8015C Modified
599714
92521577004
#2 SS (4-4.5)
EPA 5030B
599699
EPA 8015C Modified
599714
92521577005
#1 NS (5.5)
EPA 5030B
599699
EPA 8015C Modified
599714
92521577006
#1 SS (5.5)
EPA 5030B
599699
EPA 8015C Modified
599714
92521577007
#2 NW (6.5-7)
EPA 3546
599953
EPA 8270E
600218
92521577008
#2 SW (6.5-7)
EPA 3546
599953
EPA 8270E
600218
92521577009
#2 EW (6.5-7)
EPA 3546
599953
EPA 8270E
600218
92521577010
#2 WW (6.5-7)
EPA 3546
599953
EPA 8270E
600218
92521577011
#2 BASE (15.0)
EPA 3546
599953
EPA 8270E
600218
92521577001
#3 NS (4-4.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577002
#3 SS (4-4.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577003
#2 NS (4-4.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577004
#2 SS (4-4.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577005
#1 NS (5.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577006
#1 SS (5.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577007
#2 NW (6.5-7)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577008
#2 SW (6.5-7)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577009
#2 EW (6.5-7)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577010
#2 WW (6.5-7)
EPA 5035A/5030B
599428
EPA 8260D
599439
92521577011
#2 BASE (15.0)
EPA 5035A/5030B
599428
EPA 8260D
599439
92521577001
#3 NS (4-4.5)
SW-846
599437
92521577002
#3 SS (4-4.5)
SW-846
599437
92521577003
#2 NS (4-4.5)
SW-846
599437
92521577004
#2 SS (4-4.5)
SW-846
599437
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 02/24/2021 01:57 PM
without the written consent of Pace Analytical Services, LLC.
Page 61 of 65

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
CAMP STEWARD ROAD SITE
92521577
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92521577005
#1 NS (5.5)
SW-846
599437
92521577006
#1 SS (5.5)
SW-846
599437
92521577007
#2 NW (6.5-7)
SW-846
599437
92521577008
#2 SW (6.5-7)
SW-846
599437
92521577009
#2 EW (6.5-7)
SW-846
599437
92521577010
#2 WW (6.5-7)
SW-846
599437
92521577011
#2 BASE (15.0)
SW-846
599437
92521577007
#2 NW (6.5-7)
SM 2540 G
1622568
SM 254OG
1622568
92521577008
#2 SW (6.5-7)
SM 2540 G
1622568
SM 254OG
1622568
92521577009
#2 EW (6.5-7)
SM 2540 G
1622568
SM 254OG
1622568
92521577010
#2 WW (6.5-7)
SM 2540 G
1622568
SM 254OG
1622568
92521577011
#2 BASE (15.0)
SM 2540 G
1622568
SM 254OG
1622568
Date: 02/24/2021 01:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 62 of 65

Document Name: Document Revised: October 28, 2020
1!
Sample Condition Upon Receipt(SCUR) Page 1 of 2
2eAnalyfical r Document No.: Issuing Authority:
F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
. r Client Name: on Receipt Project i#: Wad : 92521577
Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client 1111111111111111111111
❑ Commercial ❑Pace []Other:
92521577
Custody Seal Present? ❑Yes ❑No Seals Intact? ❑Yes ❑No
Packing Material; ❑Bubble Wrap []Bubble Bags ❑None ❑ Other
Thermometer: ❑wet ❑Blue
❑ IR Gun ID: 92TO64 Type of Ice:
Correction Factor:
Cooler Temp: i Add/Subtract (°C) -0.1
Cooler Temp Corrected (*Cl: L4 . S .
USDA Regulated Soil{-aI1i/rA: water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
nYes Fiw- a 1' . I ,
Date/Initials Person Examining Contents:
Biological Tissue Frozen?
❑N4ne [-]Yes❑No ON/A
Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
inrlurfinv Wnwaii nnrl Punrtn Rirn11 F-lVnc C'7Mn
Comments/Discrepancy:
Chain of Custody Present?
`]Yes
❑No
[]N/A
1,
Samples Arrived within Hold Time?
[]yes
[-]No
❑N/A
2.
Short Hold Time Analysis (c72 hr.)?
❑Yes
❑No
❑N/A
3.
aush Turn Around Time Requested?
Dyes
❑No
El N/A
4,
Sufficient Volume?
Llyes
[—]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
E]Yes
Des
❑No
❑No
❑N/A
N/A
6.
Containers Intact?
. !es
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
ON/A
81
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
❑Yes
❑No
❑N/A
9,
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑No
E N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Dyes
❑No
❑No
❑�/A
' N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Persorr-contaz ted. — --Oate/Time:
Project Manager SCURF Review:
Lot ID of split containers:
Date;
Field Data Required? ❑Yes [:]No
Project Manager SRF Review:
Date;
Page 63 of 65

Document Name:
Sample Condition Upon Recei
Analytical x document No.:
F-CAR-CS-033-Rev•07
Document Revised: October 28, 2020
Page 2 of 2
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
EKceptI0ns: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Project 7-?
92
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot H
Note: Whenever there Is a discrepancy affeatrig Nor[trCarotirraTompttance samptes, it copy of Tms fornr w,r,
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 64 of 65

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Beverly, Trudy
From: Beverly, Trudy
Sent: Thursday, March 11, 2021 7:04 AM
To: Nora Zirps
Subject: RE: [External] Camp Stewart Road Site - 24-Hour Release and UST Leak Notification
Thank you Nora.
Trudy
Trudy Beverly, L.G.
D
IE �1
Hydrogeologist, Division of Waste Management
_ North Carolina Department of Environmental Quality
Q� Ue parlren[oi Lnnron men�LGmY�R� UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: ht_pt s://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: hgps:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deu.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-mans
File Review Procedures:
ht_pt s://deq.nc.gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
htt2s://deg.nc.gov/about/divisions/waste-mana2ement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.eov/nedea/Waste%2OMana2ement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policy.odf
https:Hfiles.nc.gov/ncdeg/Waste%2OManagement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Nora Zirps [ma iIto: [e-mail]]
Sent: Thursday, March 11, 2021 6:48 AM
To: Beverly, Trudy <[e-mail]>
Subject: RE: [External] Camp Stewart Road Site - 24-Hour Release and UST Leak Notification
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Trudy,
The 24-hour notification was not attached to Dan's email. He may have forwarded it to you in a separate email. Just in
case, I am sending it to you directly.
Nora
Nora A. Zirps, PE, RSM
ESP Associates, Inc.
7011 Albert Pick Road, Suite E
Greensboro, NC 27409
www.espassociates.com

[e-mail]
336.232.5213 Direct
336.334.7724 Office
336.420.6979 Cell
From: Bowser, Daniel P <[e-mail]>
Sent: Wednesday, March 10, 2021 1:17 PM
To: Nora Zirps <[e-mail]>
Cc: Beverly, Trudy <[e-mail]>
Subject: RE: [External] Camp Stewart Road Site - 24-Hour Release and UST Leak Notification
THIS MESSAGE ORIGINATED OUTSIDE OF ESP ASSOCIATES, INC. USE CAUTION WHEN OPENING ATTACHMENTS, CLICKING LINKS, OR
RESPONDING TO REQUESTS FOR INFORMATION.
Trudy Beverly handles Non -Regulated USTs in Mecklenburg county I have forwarded her the notice.
Thank you,
Daniel P. Bowser, PG
Hydrogeologist
North Carolina Department of Environmental Quality
Underground Storage Tank Section - Corrective Action Branch
[phone]
dan.bowserancdenr.aov
610 East Center Ave
Suite 301
Mooresville, North Carolina 28115
Q >E
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
From: Nora Zirps <[e-mail]>
Sent: Tuesday, March 09, 2021 9:14 PM
To: Bowser, Daniel P <[e-mail]>
Cc: Chris Ward <[e-mail]>; Fred Matrulli <[e-mail]>; Jeremy Huntsman
<[e-mail]>; Cameron Caudle, Jr. ([e-mail])
<[e-mail]>; Danis Simmons <[e-mail]>; Brian F. Welch
<[e-mail]>
Subject: [External] Camp Stewart Road Site - 24-Hour Release and UST Leak Notification

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Dan,
Attached please find a 24-Hour Release Notification for two adjacent approximate 550-
gallon heating oil USTs at the Camp Stewart Road Site discovered during UST removal. Contaminated soil has been
removed to the extent practicable and additional soil samples collected. We are currently preparing an Initial
Abatement Action report and planning a Limited Site Assessment. Please call if you have any questions.
Nora
Nora A. Zirps, PE, RSM
ESP Associates, Inc.
7011 Albert Pick Road, Suite E
Greensboro, NC 27409
www.espassociates.com
[e-mail]
336.232.5213 Direct
336.334.7724 Office
336.420.6979 Cell