MO-28509_47761_CA_IAR_20210428_Initial Abatement Action Report

ESP
April 28, 2021
Ms. Trudy Beverly, L.G.
North Carolina Department of Environmental Quality
UST Section
Mooresville Regional Office
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Reference: INITIAL ABATEMENT ACTION REPORT
Camp Stewart Road Site
Mecklenburg County Tax Parcel #11109204
Charlotte, North Carolina
NCDEQ Incident No. Pending
ESP Project No. E6-GP56.601
Dear Ms. Beverly:
On behalf of Professional Child Centers, Inc. (property owner) and Pulte Home Company, LLC
(prospective property purchaser), ESP Associates, Inc. is pleased to provide the attached Initial
Abatement Action Report documenting the removal of three residential heating oil underground
storage tanks (USTs) along with one above -ground storage tank, release detection soil sampling
and analysis, excavation of petroleum -impacted soil associated with a release from one on the
USTs, and subsequent confirmatory soil sampling and analysis associated with the subject site.
Thank you for your attention in this matter. If you should have any questions, please do not
hesitate to contact us at 704-583-4949.
Sincerely,
ESP Associates, Inc.
Nora A. Zirps, PE, RSM
Senior Project Engineer
NC License No. 023838
Christopher J. Ward, PG, RSM
Department Manager
NC License No. 1600
cc: Mr. Dean Davidson, Professional Child Centers, Inc. & Mr. Fred Matrulli, Pulte Home Company, LLC
Attachment - Initial Abatement Action Report

#�jESP
INITIAL ABATEMENT
ACTION REPORT
CAMP STEWART ROAD SITE
MECKLENBURG COUNTY TAX PARCEL #11109204
CHARLOTTE, NORTH CAROLINA
NCDEQ INCIDENT NO. PENDING
ESP PROJECT NO. E6-GP56.601
Prepared For:
North Carolina Department of Environmental Quality
UST Section
Mooresville Regional Office
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
On Behalf of:
Professional Child Centers, Inc.
505 Beachland Blvd., Suite #1
Vero Beach, Florida 32963
Prepared By:
ESP Associates, Inc.
P. 0. Box 7030
Charlotte, North Carolina 28241
April 28, 2021

Initial Abatement Action Report
Camp Stewart Road Site
Initial Abatement Action Report
SITE INFORMATION
1. Site Identification
O Date of Report: April 28, 2021
O Site Risk: Low
O Facility ID: N/A
ESP Project E6-GP56.601
April28, 2021
O UST Incident Number: Pending
O Site Name: Camp Stewart Road Site
O Site Street Address: Camp Stewart Road (Tax Parcel #11109204)
O City/County/Zip Code: Charlotte, Mecklenburg County, 28215
O Description of Geographical Data Point: Location of Removed UST-2 & UST-3
O Location Method: Survey
O Latitude: 35.24115
O Longitude:-80.66125
2. Information about Contacts Associated with the Leaking UST System
O
UST Owner:
Professional Child Centers, Inc.
O
UST Operator:
Professional Child Centers, Inc.
o
Property Owner:
Professional Child Centers, Inc.
Attn: Dean Davidson (772-913-1152)
505 Beachland Blvd, Suite #1
Vero Beach, FL 32963
O
Property Occupant:
Professional Child Centers, Inc.
O
Contractor:
A&D Environmental Services, Inc. —
Eric Brown (336-434-7750)
P.O. Box 484, High Point, NC 27261
O
Consultant:
ESP Associates, Inc. - Nora Zirps, PE (704-583-4949)
PO Box 7030, Charlotte, NC 28241
0
Analytical Laboratory:
Pace Analytical Services, Inc. (704-875-9092)
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
NC Certification No. 37706
3. Information about Release
O Date Discovered: February 9, 2021
0 Estimated Quantity of Release: Unknown
o Cause of Release: Apparent leak from UST-3
O Source of Release: UST-3
O Size and contents of UST system
from which release occurred: 550-gallon heating oil
4. Certification
I, Nora A. Zirps, a Professional Engineer for ESP Associates, Inc., do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
I A, J] ssociates, Inc. is licensed to practice both geology and engineering in North Carolina. ESP
aA so Inc.' certification numbers are: Geology: C-556 / Engineering: F-1407
2021.04.28 21:47:52-04'00'

Initial Abatement Action Report
Camp Stewart Road Site
TABLE OF CONTENTS
Section
ESP Project E6-GP56.601
April28, 2021
1.0 INTRODUCTION................................................................................................................................. I
2.0 SITE HISTORY AND CHARACTERIZATION.............................................................................1
2.1 Site Description/Setting.................................................................................................................1
2.2 Prior Site Ownership..................................................................................................................... 2
2.3 Previous Incidents.......................................................................................................................... 3
2.4 Potential Receptors........................................................................................................................ 3
3.0 CLOSURE OF USTs BY REMOVAL............................................................................................... 3
3.1 Preparatory Activities....................................................................................................................3
3.2 Removal of USTs and AST.......................................................................................................... 4
3.3 Collection and Analysis of Release Detection Soil Samples ...................................................... 5
3.4 Release Detection Soil Sample Analytical Results......................................................................6
3.5 24-Hour Release and UST Leak Reporting Form........................................................................ 6
4.0 INITIAL ABATEMENT ACTION ACTIVITIES........................................................................... 7
4.1 Excavation of Petroleum -Impacted Soil - February 9-10, 2021...........................................7
4.1.1 Collection and Analysis of Confirmatory Soil Samples ................................................... 7
4.1.2 Confirmatory Soil Sample Analytical Results................................................................... 8
4.2 Excavation of Petroleum -Impacted Soil - March 22, 2021...................................................9
4.2.1 Collection and Analysis of Confirmatory Soil Samples.................................................10
4.2.2 Confirmatory Soil Sample Analytical Results.................................................................10
5.0 OFF -SITE DISPOSAL OF PETROLEUM -IMPACTED SOIL..................................................10
6.0 BACKFILLING OF THE UST-2 and UST-3 EXCAVATION.................................................... I I
7.0 SUMMARY AND CONCLUSIONS.................................................................................................11
8.0 NEXT STEPS.......................................................................................................................................13
9.0 REFERENCES.....................................................................................................................................13
FIGURES
Figure 1 USGS Topographic Site Location Map
Figure 2 UST Location Map
Figure 3 150-Foot Radius Receptors Map
Figure 4 UST-1 Release Detection Soil Sample Locations and Results
Figure 5 UST-2 & UST-3 Release Detection Soil Sample Locations and Results
Figure 6 UST-2 & UST-3 Confirmatory Soil Sample Locations and Results
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Initial Abatement Action Report
Camp Stewart Road Site
TABLE OF CONTENTS (Continued)
TABLES
ESP Project E6-GP56.601
April28, 2021
Table 13-1 Site History - UST/AST System and Other Release Information
Table B-2 Site History - UST/AST Owner/Operator and Other Responsible
Party Information
Table B-3 Summary of Soil Sampling Results
APPENDICES
Appendix A Field Documentation
Appendix B Site Photographs
Appendix C UST-213, Site Investigation Report for Permanent Closure or
Change -in -Service of Un-registered UST
Appendix D Disposal Documentation
Appendix E UST-61, 24-Hour Release and UST Leak Reporting Form
Appendix F Laboratory Analytical Reports
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Initial Abatement Action Report
Camp Stewart Road Site
1. INTRODUCTION
ESP Project E6-GP56.601
April28, 2021
Pulte Home Company, LLC (Pulte) is considering the purchase of the property identified as
Mecklenburg County Tax Parcel ID No. 11109204, which is located off and south of Camp
Stewart Road in Charlotte, North Carolina (see location of the subject site on Figures 1 and 2).
The property is currently owned by Professional Child Centers, Inc. As part of their
pre -purchase due diligence, Pulte, on behalf of the property owner, procured the services of ESP
Associates, Inc. (ESP) to close by removal three existing approximate 550- to 600-gallon heating
oil underground storage tanks (USTs), identified as UST-1 through UST-3, and one approximate
550-gallon heating oil above -ground storage tank (AST). During removal, a release was found to
have occurred from UST-3.
ESP documented the removal of the three USTs and the AST, collected release detection soil
samples for laboratory analysis, excavated petroleum -impacted soil in the vicinity of UST-3
(along with UST-2 which was located in the same tank pit), and collected confirmatory soil
samples for laboratory analysis. The locations of the removed USTs within the subject site are
depicted on Figures 1 and 2. Table B-1 provides an overview of the removed USTs and AST
and associated release from UST-3.
2. SITE HISTORY AND CHARACTERIZATION
2.1 Site Description/Setting
The approximate 53.27-acre heavily wooded subject site, comprised of Tax Parcel ID No.
11109204, is located off and south of Camp Stewart Road, east of its intersection with
Harrisburg Road in Charlotte, North Carolina. The site, which is accessed through a locked gate,
has a listed street address of 5501 Camp Stewart Road and includes remnants of structures
associated with the closed Camp Stewart summer camp facility. An approximate two -acre pond
is located on the southern portion of the site with several streams flowing throughout the site. A
concrete in -ground swimming pool is located on the eastern portion of the site. The surrounding
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Initial Abatement Action Report
Camp Stewart Road Site
ESP Project E6-GP56.601
April28, 2021
area consists of residential subdivisions, single-family residences, commercial/retail properties, a
fire station, and undeveloped woods and fields.
The Mecklenburg County Soil Survey indicates that soils beneath the portion of the site where
UST-1 was located are classified as Appling sandy loam, 2 to 8 percent slopes, well drained
(ApB), while soils beneath the portion of the site where UST-2 & UST-3 were located are
classified as Cecil sandy clay loam, 2 to 8 percent slopes, moderately eroded and well drained
(Ce132). Based on our review of the Geologic Map of North Carolina (1985), the subject site is
located within the Charlotte Belt, comprised locally of metamorphosed quartz diorite, foliated to
massive. The soils encountered in this area are the residual product of chemical weathering of
rock presently underlying the site. The soil weathering is more advanced near the surface
grading with depth to less weathered rock and finally bedrock.
2.2 Prior Site Ownership
The following information regarding past ownership of the site was gleaned from deeds that are
readily available in the Mecklenburg County Polaris GIS Website:
• June 9, 1975: Professional Child Care Centers, Inc. purchased the property from HMC
Corporation.
• April 28, 1972, HMC Corporation purchased the property from the Trustees of
Mecklenburg Presbytery, Presbyterian Church in the United States.
• Trustees of Mecklenburg Presbytery, Presbyterian Church in the United States purchased
the property in three parts:
o November 21, 1945, from Ralph N. Miller and wife;
o June 8, 1946, from J. Todd Garrison and wife; and
o June 23, 1955, from V. H. Brawley and wife.
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Camp Stewart Road Site
2.3 Previous Incidents
ESP Project E6-GP56.601
April28, 2021
There have been no previous incidents reported to have occurred on the subject property (see
Table B-2).
2.5 Potential Receptors
On March 22, 2021, ESP performed a visual site reconnaissance to identify potential receptors
within an approximate 150-foot radius of the UST-3 release location (see Figure 3). No water
supply wells or surface water bodies were observed within 150 feet (ft) of the UST-3 release
location during the reconnaissance.
3. CLOSURE OF USTs BY REMOVAL
ESP procured the services of A&D Environmental Services, Inc. (A&D) of High Point, North
Carolina, to remove the three heating oil USTs and the one heating oil AST. Field
documentation and photographs documenting the removal of the three USTs and the AST are
provided in Appendices A and B, respectively. Table B-1 presents a summary regarding the
capacity, contents, construction details, dimensions, and removal date of the three USTs and the
one AST. A Site Investigation Report for Permanent Closure or Change -In -Service of
Un-registered UST (Form UST-2B) is provided in Appendix C.
3.1 Preparatory Activities
Prior to removal of the three heating oil USTs and the heating oil AST, the following preparatory
activities were completed:
• A&D contacted the Fire Prevention Bureau of the Charlotte Fire Department and
determined that a permit was not required for removal of the heating oil USTs; and
• A&D contacted NC811 to mark public underground utilities in the vicinity of the USTs.
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Initial Abatement Action Report
Camp Stewart Road Site
3.2 Removal of USTs and AST
ESP Project E6-GP56.601
April28, 2021
On February 8, 2021, A&D used a trackhoe to remove the overburden soils from above UST-2
and UST-3, which were located within the same tank pit. The approximate 600-gallon UST-2
was full and contained heating oil, while the approximate 550-gallon UST-3 appeared to be
empty with some petroleum residue. Once the overburden soils were removed, A&D tilted
UST-3 with the trackhoe and propped the tank up to be left overnight in an effort to allow the
residue to migrate to the spout end to be pumped out the following day. A&D used the trackhoe
to remove the overburden soils from above the approximate 550-gallon UST-1 that contained
approximately 4 inches of heating oil. The approximate 550-gallon AST appeared to be about a
quarter full and contained heating oil.
On February 9, 2021, A&D pumped out the contents from the three USTs and the AST into a
vacuum truck. Only approximately 1 gallon of residue was removed from UST-3. After
pumping was completed, A&D removed the three USTs (UST-1 through UST-3) from the
ground, and then washed out the three USTs and the AST by pressure washing and pumping out
the fluids into the vacuum truck. A total of 1,135 gallons of petroleum -contaminated fluid were
transported off -site under non -hazardous waste manifest (see copy of manifest in Appendix D) to
A&D's facility located at 2718 Uwharrie Road, Archdale, NC, where the oil and water were
separated. The oil was subsequently transported to Ross Incineration Services, Inc. located at
36790 Giles Road, Grafton, Ohio, for incineration. The water was subsequently transported to
HOH Corporation location at 1701 Vargrave Street, Winston-Salem, North Carolina for
treatment.
On February 9, 2021, A&D transported the three removed USTs and the AST off -site to its
facility located at 2718 Uwharrie Road, Archdale, NC, where the tanks were cleaned, crushed,
and then transported to D.H. Griffin Companies located at 4716 Hilltop Road, Greensboro, North
Carolina, for recycling (see copy of tank disposal manifest in Appendix D).
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Initial Abatement Action Report ESP Project E6-GP56.601
Camp Stewart Road Site April 28, 2021
3.3 Collection and Analysis of Release Detection Soil Samples
On February 9 and 10, 2021, in support of the UST-1, UST-2, and UST-3 closure activities,
release detection soil samples were collected according to procedures outlined in the North
Carolina Department of Environmental Quality's (NCDEQ's) Underground Storage Tank
Section Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement.
On February 10, 2021, two release detection soil samples were collected from native soils at the
base of the UST-1 tank pit (see Figure 4 for sample locations) at a depth of approximately 5.5 ft
below ground surface (BGS). Photoionization detector (PID) readings at the sampled locations
were as follows:
#1 NS - 0.0 parts per million (ppm)
#1 SS-0.0ppm
Following collection of the release detection soil samples, the UST-1 tank pit was backflled.
On February 9, 2021, two release detection soil samples were collected from native soils at the
base of each of the adjacent UST-2 and UST-3 tank pits (see Figure 5 for sample locations) at a
depth of approximately 4 to 4.5 ft BGS. PID readings at the sampled locations were as follows:
#2 NS - 11.9 ppm
#2 SS - 2.2 ppm
#3 NS - 34.9 ppm
#3 SS - 37.2 ppm
The release detection soil samples were placed in laboratory -provided containers, labeled, stored
on ice in a cooler, and hand delivered under standard chain -of -custody procedures to Pace
Analytical Laboratories' (Pace's) North Carolina -certified laboratory located in Huntersville,
North Carolina, for laboratory analysis. The laboratory analyzed the release detection soil
samples for total petroleum hydrocarbons (TPH) diesel range organics (DRO) by EPA Method
8015, TPH gasoline range organics (GRO) by EPA Method 8015, and BTEX (benzene, toluene,
ethylbenzene, and xylene) by EPA Method 8260.
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Initial Abatement Action Report ESP Project E6-GP56.601
Camp Stewart Road Site April 28, 2021
3.4 Release Detection Soil Sample Analytical Results
The laboratory analytical results for the release detection soil samples collected from the three
UST pits (#1 NS, #1 SS, #2 NS, #2 SS, #3 NS, and #3 SS) are presented in Table B-3, and
Figures 4 and 5. The laboratory analytical report is provided in Appendix F.
The release detection soil sample results for UST-1 (samples #1 NS and #1 SS) revealed that
TPH DRO and BTEX were non -detect in both of the soil samples. TPH GRO was non -detect in
soil sample #1 SS and detected at 5.8 milligrams per kilogram (mg/kg) in soil sample #1 NS,
which was below NCDEQ's soil screening level for TPH GRO of 50 mg/kg.
The release detection soil sample results from the UST-2 and UST-3 tank pit (samples #2 NS,
#2 SS, #3 NS, and #3 SS) revealed that both TPH DRO and TPH GRO were detected in all four
soil samples. TPH DRO results ranged from 2,040 to 10,500 mg/kg, which were all above
NCDEQ's soil screening level for TPH DRO of 100 mg/kg. TPH GRO results ranged from 4.9
to 75 mg/kg, which were all below NCDEQ's soil screening level for TPH GRO of 50 mg/kg
with the exception of #2 NS. BTEX results were non -detect except for trace levels of xylene in
#2 NS and #3 NS, which were below the soil -to -groundwater Maximum Soil Contaminant
Concentration (MSCC) for xylene. Although the highest TPH DRO and TPH GRO detections
were observed in sample #2 NS, UST-2 is not believed to have been the source of the release
since UST-2 was full of heating oil at the time of removal. UST-3 is believed to have been the
source of the release since it was empty at the time of removal. UST-2 and UST-3 were located
in the same tank pit.
3.5 24-Hour Release and UST Leak Reporting Form
On March 9, 2021, ESP submitted Form UST-61: 24-Hour Release and UST Leak Reporting
Form to Ms. Trudy Beverly of NCDEQ's Mooresville Regional Office UST Section via email to
report the release from UST-3 based on the laboratory analytical results for release detection soil
samples. A copy of the Form UST-61 (minus the laboratory analytical report) is provided in
Appendix E.
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Initial Abatement Action Report
Camp Stewart Road Site
ESP Project E6-GP56.601
April28, 2021
4. INITIAL ABATEMENT ACTION ACTIVITIES
Because of the elevated PID readings at the base of the UST-2 and UST-3 tank pit measured on
February 9, 2021, petroleum -impacted soil was excavated for off -site disposal. Excavation of
petroleum -impacted soil from the UST-2 and UST-3 location occurred during two separate
events. During each excavation event, a PID was used to field screen soils to direct the
excavation laterally and vertically. Field documentation and photographs documenting the initial
abatement action excavation activities and confirmatory soil sampling are provided in
Appendices A and B, respectively.
4.1 Excavation of Petroleum -Impacted Soil - February 9-10, 2021
On February 9 and 10, 2021, A&D excavated petroleum -impacted soil from the UST-2 and
UST-3 location. The lateral extent of the February 9-10, 2021, excavation is depicted on
Figure 6. As shown on Figure 6, the footprint of the February 9-10, 2021, excavation was
approximately 15.6 ft by 13.5 ft in size (based on the average of the side lengths). At 15 ft BGS,
excavation activities were terminated because the excavation had reached the depth limitations of
the trackhoe. The excavation did not encounter groundwater or bedrock. Excavated petroleum -
impacted soil was placed on and covered by plastic sheeting for off -site disposal at a later date
(see Section 5).
4.1.1 Collection and Analysis of Confirmatory Soil Samples
On February 10, 2021, five confirmatory soil samples were collected from the sidewalls
(designated #2 NW, #2 EW, #2 SW, and #2 WW) of the excavation at a depth of approximately
6.5 to 7 ft BGS and from the base (designated #2 BASE) of the excavation at a depth of
approximately 15 ft BGS (see Figure 6 for sample locations). PID readings at the sampled
locations were as follows:
#2 NW - 31.2 ppm
#2EW-2.3ppm
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Initial Abatement Action Report
Camp Stewart Road Site
#2 SW - 1.1 ppm
#2WW-8.3ppm
#2 BASE - 70.4 ppm
ESP Project E6-GP56.601
April28, 2021
The confirmatory soil samples were placed in laboratory -provided containers, labeled, stored on
ice in a cooler, and hand delivered under standard chain -of -custody procedures to Pace's North
Carolina -certified laboratory located in Huntersville, North Carolina, for laboratory analysis.
The laboratory analyzed the confirmatory soil samples for MADEP volatile petroleum
hydrocarbons (VPH), MADEP extractable petroleum hydrocarbons (EPH), semi -volatile organic
compounds (SVOCs) by EPA Method 8270, and volatile organic compounds (VOCs) by EPA
Method 8260.
4.1.2 Confirmatory Soil Sample Analytical Results
The analytical results for confirmatory soil samples #2 NW, #2 EW, #2 SW, #2 WW, and
#2 BASE are presented in Table B-3 and on Figure 6. The laboratory analytical report is
provided in Appendix F. As noted in Table B-3, the analytical results for the eastern and western
sidewall samples (#2 EW and #2 WW) were either non -detect or less than both soil -to -
groundwater and residential MSCCs. Soil -to -groundwater and/or residential MSCCs were
exceeded on the other two sidewalls (#2 NW and #2 SW) and the base (#2 BASE) of the
excavation as follows:
• #2 NW - Aromatics C9-C22, 1-methylnaphthalene, 2-methylnaphthlene,
p-isopropyltoluene, and naphthalene exceeded their corresponding soil -to -groundwater
MSCCs, while only 1-methylnaphthalene and naphthalene also slightly exceeded their
residential MSCCs. 1-Methylnaphthalene at 27.5 mg/kg exceeded its residential MSCC
of 22.8 mg/kg, and naphthalene at 7.76 mg/kg exceeded its residential MSCC of
5.5 mg/kg.
• #2 SW - Aromatics C9-C22 at 2,804.6 mg/kg exceeded both the soil -to -groundwater
MSCC of 31 mg/kg and the residential MSCC of 469 mg/kg, and Aliphatics C9-C 18 at
4,919.3 mg/kg exceeded both the soil -to -groundwater MSCC of 540 mg/kg and the
residential MSCC of 1,560 mg/kg.

Initial Abatement Action Report
Camp Stewart Road Site
ESP Project E6-GP56.601
April28, 2021
• #2 BASE - Aromatics C9-C22, Aliphatics C9-C 18, 1-methylnaphthalene,
2-methylnaphthlene, p-isopropyltoluene, and naphthalene exceeded their corresponding
soil -to -groundwater MSCCs, while only Aromatics C9-C22 and Aliphatics C9-C 18
exceeded their residential MSCCs. Aromatics C9-C22 at 2,277.2 mg/kg exceeded its
residential MSCC of 469 mg/kg, and Aliphatics C9-C18 at 10,194 mg/kg exceeded its
residential MSCC of 1,560 mg/kg.
4.2 Excavation of Petroleum -Impacted Soil - March 22, 2021
ESP procured the services of CCI Environmental Services (CCI) of Salisbury, North Carolina, to
excavate additional petroleum -impacted soil at the UST-2 and UST-3 location. On March 22,
2021, CCI extended the original excavation to the north and the south in an attempt to delineate
the lateral area of petroleum -impacted soil above residential MSCCs. The lateral extent of the
March 22, 2021, excavation area is depicted on Figure 6. The additional lateral excavation did
not encounter groundwater or bedrock. Due to the limitations of the trackhoe, the base of the
central portion of the excavation was not advanced deeper than its original 15-foot depth.
The northern end of the excavation, where 1-methylnaphthalene and naphthalene exceeded
residential MSCCs in the prior sidewall soil sample, was extended laterally approximately 17 ft
to the north because of continued trace PID readings (3 ppm and below). The depth of the
extended excavation was limited to approximately 7 ft BGS to align with the prior sidewall soil
sample depth.
The southern end of the excavation, where Aromatics C9-C22 and Aliphatics C9-C18 exceeded
residential MSCCs in the prior sidewall soil sample, was extended laterally approximately 10 ft
to the south. The depth of the extended excavation was limited to approximately 8 ft BGS to
align with the prior sidewall soil sample depth.
Excavated petroleum -impacted soil was placed directly into dump trucks for off -site transport
and disposal (see Section 5).
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Initial Abatement Action Report ESP Project E6-GP56.601
Camp Stewart Road Site April 28, 2021
4.2.1 Collection and Analysis of Confirmatory Soil Samples
On March 22, 2021, two confirmatory soil samples were collected from the sidewalls
(designated #2 NW-2 and #2 SW-2) of the extended excavation at a depth of approximately 6.5
to 7 ft BGS (see Figure 6 for sample locations). PID readings at the sampled locations were as
follows:
#2 NW-2 - 0.5 ppm
#2 SW-2 - 0.0 ppm
The confirmatory soil samples were placed in laboratory -provided containers, labeled, stored on
ice in a cooler, and hand delivered under standard chain -of -custody procedures to Pace's North
Carolina -certified laboratory located in Huntersville, North Carolina, for laboratory analysis.
Confirmatory soil samples were analyzed for the compounds that exceeded residential MSCCs in
the February 10, 2021, sidewall samples. Confirmatory soil sample #2 NW-2 was analyzed for
1-methylnaphthalene by EPA Method 8270 and naphthalene by EPA Method 8260.
Confirmatory soil sample #2 SW-2 was analyzed for MADEP VPH and MADEP EPH. All
parameters were analyzed by Pace's Huntersville, North Carolina, laboratory except for MADEP
EPH which was analyzed by Pace's West Columbia, South Carolina, laboratory, which is also
North Carolina -certified.
4.2.2 Confirmatory Soil Sample Analytical Results
The analytical results for confirmatory soil samples #2 NW-2 and #2 SW-2 are presented in
Table B-3 and on Figure 6. The laboratory analytical report is provided in Appendix F. As
noted in Table B-3, the concentrations of analyzed parameters were all below reporting limits.
5. OFF -SITE DISPOSAL OF PETROLEUM -IMPACTED SOIL
On March 22, 2021, the excavated petroleum -impacted soil from both the February 9-10, 2021,
and March 22, 2021, excavation events were loaded into dump trucks for off -site transport under
non -hazardous waste manifests to Alternative Energy Solutions of NC, LLC (AES) located at
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Initial Abatement Action Report
Camp Stewart Road Site
3841 Cunningham Road, Thomasville, NC
ESP Project E6-GP56.601
April28, 2021
AES is a permitted land farm (Permit #
SRU400014) where petroleum -impacted soils are treated by spreading and aeration. Copies of
the non -hazardous manifests/weigh tickets are provided in Appendix D. A total of 109.9 tons of
petroleum -impacted soil associated with the UST-3 release were transported off -site for disposal.
6. BACKFILLING OF THE UST-2 AND UST-3 EXCAVATION
Final backfilling of the UST-2 and UST-3 excavation occurred on March 22, 2021, following
collection of the second set of confirmatory soil samples. Field documentation and photographs
documenting backfilling of the UST-2 and UST-3 excavation are provided in Appendices A and
B, respectively.
The bottom of the excavation was demarcated with either plastic sheeting or orange safety
fencing material prior to backfilling. Unimpacted overburden material removed from above the
USTs was used as initial backfill material following by imported fill material supplied by Keller
Mining Inc. located in Kannapolis, North Carolina (copies of the material receipts are provided
in Appendix A). Backfill soil was placed in approximately one -foot lifts, and the trackhoe
bucket was used to tamp down the soils between lifts.
7. SUMMARY AND CONCLUSIONS
The following bullets summarize our findings based on completion of removal and initial
abatement action activities along with associated soil sample laboratory analytical results:
• On February 9, 2021, three 550- to 600-gallon heating oil USTs (UST-1 through UST-3)
and one approximate 550-gallon heating oil AST were removed from the subject site and
transported off -site where they were recycled. UST-2 and UST-3 were located adjacent
to each other within the same tank pit.
• Based on release detection soil sample laboratory analytical results, a release had not
occurred from UST-1.
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Initial Abatement Action Report
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ESP Project E6-GP56.601
April28, 2021
• Based on laboratory analytical results for the release detection soil samples collected
from the UST-2 and UST-3 tank pit, a release had occurred. NCDEQ's soil screening
level for TPH DRO of 100 mg/kg was exceeded in all four of the release detection soil
samples, with detected concentrations ranging from 2,040 to 10,500 mg/kg. Although
TPH GRO was detected in all four release detection soil samples, only the sample at the
north end of UST-2 (#2 NS) with a concentration of 75 mg/kg exceeded NCDEQ's soil
screening level for TPH GRO of 50 mg/kg. Although the highest TPH DRO and TPH
GRO detections were observed in sample #2 NS, UST-2 is not believed to have been the
source of the release since UST-2 was full of heating oil at the time of removal. UST-3
is believed to have been the source of the release since it was empty at the time of
removal.
• On March 9, 2021, ESP submitted a 24-Hour Release and UST Leak Reporting Form to
NCDEQ via email.
• 109.9 Tons of petroleum -impacted soil were excavated for off -site permitted disposal
from the UST-2 and UST-3 location during two events (February 9-10, 2021, and
March 22, 2021). The final surface footprint of the excavation was approximately 42.5 ft
long and ranged from 7 to 14.2 ft in width. The center section of the excavation extended
to 15 ft BGS (the trackhoe's excavation depth limit), while the extended excavations to
the north and south extended to 7 ft BGS and 8 ft BGS, respectively. The excavation did
not encounter groundwater or bedrock.
• Based on confirmatory soil sample results #2 NW-2, #2 EW, #2 SW-2, and #2 WW, all
compounds along the sidewalls at the final March 22, 2021, excavation extent were less
than residential MSCCs. Note that confirmatory soil sample locations #2 NW and
#2 SW, where there were residential MSCC exceedances, were subsequently removed
during the March 22, 2021, excavation activities.
• Confirmatory soil sample results at the center of the excavation's base exceeded
residential MSCCs for Aromatics C9-C22 (2,277.2 mg/kg compared to the residential
MSCC of 469 mg/kg) and Aliphatics C9-C18 (10,194 mg/kg compared to the residential
MSCC of 1,560 mg/kg). Aromatics C9-C22, Aliphatics C9-C18, 1-methylnaphthalene,
12

Initial Abatement Action Report
Camp Stewart Road Site
ESP Project E6-GP56.601
April28, 2021
2-methylnaphthlene, p-isopropyltoluene, and naphthalene exceed their corresponding
soil -to -groundwater MSCCs at the center of the base of the excavation.
• On March 22, 2021, the excavation was backfilled with unimpacted overburden soil and
imported backfill material.
• There are no water supply wells or surface water bodies within 150 ft of the UST-3
release location.
Based on the above findings, ESP requests that the UST-3 release be classified as low risk.
8. NEXT STEPS
As a result of soil -to -groundwater MSCC exceedances at the base of the UST-2 and UST-3
excavation, a Limited Site Assessment (LSA) will be performed, and the results submitted to
NCDEQ. During performance of the LSA, additional soil samples will be collected within the
area defined by the March 22, 2021, excavation to the north and south to better delineate the
extent of residential soil MSCC exceedances at the base of the excavation in those directions.
9. REFERENCES
1985 Geologic Map of North Carolina, The North Carolina Geological Survey, Phillip M.
Brown.
Mecklenburg County, North Carolina GIS website. https://polaris3g.mecklenburgcountync.govl
Mecklenburg County Health Dept./LUESA-GIS Well Information System 4.0, accessed on
March 3, 2021. https://edmsmapserver.mecklenburgcountync.govlwis4l
United States Department of Agriculture, Natural Resources Conservation Service. Sol] Survey
of Mecklenburg County, North Carolina. http://Websoilsurvey.nres.usda.govl
13

FIGURES

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KEY.All locations are approximate.
PROJECT NO. GP56.601
SHEET TITLE FIGURE 1
ESP Associates, Inc.
PARCEL BOUNDARY N
SCALE As Shown
USGS TOPOGRAPHIC SITE LOCATION MAP
P.O. Box 7030
ESP Charlotte, NC 28241
DRAWN BY CD
PROJECT CAMP STEWART ROAD SITE
0 440 880 w -�
UST LOCATION Feet s .
phone [phone]
CHECKED BY NZ
DATE 313112021
CHARLOTTE, NORTH CAROLINA
www.cspassociates.com

10810117
/\
11103601
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11103607
11103609
11103113
11103120
11103114
11103119
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\v/ 11109119 11109113
11131101 11109118
11132138
11109133
11109132 11132137
11109121
11109117
11109107 11109138
11109135 11132136
11109134
11132115
11109110
11109109 11132114
11109127
11132113
11109205
11109204
AA J.:
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11109719
11144127 �J
11153110
11144106
11144128 11152138
11144126
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1�11321]06 Cl:11:32�31:0
11109396
11109304
11109305
11109306
11109307
11109308
11109309
KEY.All locations are approximate.
PROJECT NO. GP56.601
SHEET TITLE
ESP Associates, Inc.
FIGURE 2
PARCEL BOUNDARY N
SCALE As Shown
UST LOCATION MAP
P.O. Box 7030
ESP Charlotte, NC 28241
0 175 350 w -, E
UST LOCATION Feet s .
DRAWN BY CD
PROJECT CAMP STEWART ROAD SITE
phone [phone]
CHECKED BY NZ
DATE 313112021
CHARLOTTE, NORTH CAROLINA
www.cspassociatcs.com

ASEM
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KEY: All locations are approximate.
PROJECT NO. GP56.601
SHEETTITLE
ESP Associates, Inc.
FIGURE 3
PARCEL BOUNDARY N
SCALE As Shown
150-FOOT RADIUS RECEPTORS MAP
P.O. Box 7030
A
Charlotte, NC 28241
150-FT RECEPTOR BOUNDARY o 220 440 w
AA —
Feet
s
DRAWN BY CD
PROJECT
phone [phone]
CAMP STEWART ROAD SITE
CHECKED BY NZ
DATE 313112021
CHARLOTTE, NORTH CAROLINA
www.espassociates.com

Key
8.G'
6.0'
#1 NS
#1 SS
PROJECT NUMBER: GP56.601 TITLE:
FIGURE 4 ESP Associates, Inc.
LIST SCALE: UST-1 RELEASE DETECTION SOIL SAMPLE LOCATIONS
NOT TO SCALE P.O. Box 7030
11 Charlotte, NC 28241
� ' DRAWN BY: CD PROJECT: CAMP STEWART ROAD SITE
ESP • SOIL SAMPLE LOCATION phone [phone]
FE:7777
3/11/2021 REVIEWED BY: NZ
CHARLOTTE, NORTH CAROLINAI www.esnassociates.cotr

Key:
O UST
• SOIL SAMPLE LOCATION
8.2'
#3 NS #2 NS
#3 SS #2 SS
1y PROJECT NUMBER
SCALE:
N� 0, �
c DRAWN BY:
DATE: 3/11/2021 REVIEWED BY:
GP56.601 TITLE: FIGURE 5
UST-2 & UST-3 RELEASE DETECTION
NOT TO SCALE SOIL SAMPLE LOCATIONS
CD PROJECT:
CAMP STEWART ROAD SITE ESP
NZ CHARLOTTE, NORTH CAROLINA
ESP Associates, Inc.
P.O. Box 7030
Charlotte, NC 28241
phone [phone]
WWW.espassociates.con

Key
14'
• SOIL SAMPLE LOCATION
.... FEBRUARY 9-10, 2021 EXCAVATION
MARCH 22, 2021 EXCAVATION
#2 SW-2
10' 15.6'
-----
(8' DEEP)
14.2'
12.8'
(15' DEEP)
#2 EW
OOR= +�
go= am
PROJECT NUMBER
SCALE:
n
DRAWN BY:
DATE: 3/23/2021 REVIEWED BY:
15.5'
7'
GP56.601 TITLE: FIGURE 6
UST-2 & UST-3 CONFIRMATORY
NOT TO SCALE SOIL SAMPLE LOCATIONS
CD PROJECT:
CAMP STEWART ROAD SITE ESP
NZ CHARLOTTE, NORTH CAROLINA
ESP Associates, Inc.
P.O. Box 7030
Charlotte, NC 28241
phone [phone]
WWW.espassoclates.con

TABLES

Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: March 28, 2021 Incident Number and Name: Pending / Camp Stewart Road Site
UST ID
Current /
Previous
Capacity
Construction
Tank
Description
Date Tank
Status of
Release
Number
Most -Recent
Contents*
(in
Details**
Dimensions
of Piping
Installed
UST***
associated
Contents*
gallons)
and Pumps
with this USTS
stem?
UST-1
Heating Oil
Unknown
550
S-walled
4.2 ft diameter
N/A
Unknown
Removed
No
Steel
5.2 ft lon
2/9/2021
UST-2
Heating Oil
Unknown
600
S-walled
4 ft diameter
N/A
Unknown
Removed
No
Steel
6.3 ft long
2/9/2021
UST-3
Heating Oil
Unknown
550
S-walled
3.75 ft diameter
N/A
Unknown
Removed
Yes
Steel
6.3 ft long
2/9/2021
Add additional records as necessary
AST ID
Current /
Previous
Capacity
Construction
Tank
Description
Date Tank
Status of
Release
Number
Most -Recent
Contents*
(in
Details**
Dimensions
of Piping
Installed
AST***
associated
Contents*
gallons)
and Pumps
with this ASTS
stem?
AST-1
Heating Oil
Unknown
550
S-walled
3.5 ft diameter
N/A
Unknown
Removed
No
Steel
7.5 ft lon
2/9/2021
Add additional records as necessary
Incident
Number
F
Material
Released
Date of
Release
Description of Release
Pending
Heating
Oil
2/9/2021
During closure by removal of co -located UST-2 & UST-3, a release was detected based on
photoionization detector (PID) field screening measurements at base of tank pit.
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
* * * Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)

Table B-2: Site History - UST/AST Owner/Operator and Other Responsible
Party Information (Page 1 of 1)
Revision Date: March 28, 2021 Incident Number and Name: Pending/ Camp Stewart Road Site
UST ID
Number
N/A
Facility ID
Number
N/A
Owner Name (and Contact)
Dates of Operation
mm/dd/ to mm/dd/
Professional Child Centers, Inc.
Unknown
Street Address
505 Beachland Blvd, Suite #1
City
State
Zip
Telephone Number
Vero Beach
I FL
32963
772-913-1152
Operator Name (and contact)
Dates of Operation
mm/dd/ to mm/dd/
Same as Owner
Unknown
Street Address
City
State
Zip
Telephone Number
Other Incidents Onsite or Commingled/In
Close Proximity
Incident
Number
N/A
Date Incident
Occurred
N/A
Name of Responsible Parry
for Other Incident
Date Incident
Reported
N/A
N/A
Date Incident
Closed (i/a)
N/A
Street Address
N/A
City
State
Zip
Telephone Number
N/A
N/A
N/A
N/A

Table B-3: Summary of Soil Sampling Results (Page 1 of 4)
Revision Date: 3/28/2021 Incident Number: Pending — Camp Stewart Road Site, Charlotte, NC Facility ID#: N/A
Analytical Method (e.g., VOC by EPA 8260)
8015
8015
8260
8260
8260
8260
Contaminant of Concern
o
Date
Source Area
Sample
Incident
Sample ID
Collected
(eg. Tank
Depth
Phase
a
a
'
(Closure,
w
(m/dd/yy)
pit 1)
(ft BGS)
etc
Tank Pit 1
#1 NS (5.5)
2/9/2021
5.5
Closure
BRL
5.8 J
BRL
BRL
BRL
BRL
Base
Tank Pit 1
#1 SS (5.5)
2/9/2021
5.5
Closure
BRL
BRL
BRL
BRL
BRL
BRL
Base
Tank Pit 2
42 NS (4-4.5)
2/9/2021
4.5
Closure
10,500
75.0
BRL
BRL
BRL
0.528
Base
Tank Pit 2
#2 SS (4-4.5)
2/9/2021
4.5
Closure
4,720
4.9 J
BRL
BRL
BRL
BRL
Base
Tank Pit 3
#3 NS (4-4.5)
2/9/2021
4.5
Closure
3,040
19.1
BRL
BRL
BRL
0.0342
Base
Tank Pit 3
#3 SS (4-4.5)
2/9/2021
4.5
Closure
2,040
25.3
BRL
BRL
BRL
BRL
Base
Soil -to -Groundwater MSCC (mg/kg)
NE
NE
0.0072
8
5.4
6
esidential MSCC (mg/kg)
NE
NE
12
60.3
1,250
3,120
industrial/Commercial MSCC (mg/kg)
r
NE
NE
59.4
297
18,600
46,700
Bold values exceed lowest MSCC. TPH DRO and TPH GRO screening levels are 100 mg/kg and 50 mg/kg, respectively.
BRL = below reporting limits
ft BGS = feet below ground surface
J = Analyte was positively identified but the value is estimated below the reporting limit.
mg/kg = milligrams per kilogram
MSCC = maximum soil contaminant concentration
NE = not established

Table B-3: Summary of Soil Sampling Results (Page 2 of 4)
Revision Date: 3/28/2021 Incident Number: Pending — Camp Stewart Road Site, Charlotte, NC Facility ID#: N/A
Analytical Method (e.g., VOC by EPA 8260) 4
MADEP
MADEP
MADEP
8270
8270
8270
8270
8270
8270
VPH/EPH
VPH
VPH/EPH
Contaminant of Concern 4
.4 L?
¢
�°
o
Incident
Date
Source Area
Sample
phase
° 0,
P
Sample ID
Collected
(eg. Tank
Depth
w
a
(m/dd/yy)
pit 1)
(ft BGS)
(Closure,
d
A
LSA, etc.)
Over -Excavated
#2 NW (6.5 -7)
2/10/2021
Tank Pit 2&3
7
Closure
328
17.9
304
4.97
BRL
2.28 J
27.5
39.1
9.25
Sidewall
Over -Excavated
#2 SW (6.5 -7)
2/10/2021
Tank Pit 2&3
7
Closure
2,804.6
10.6
4,919.3
BRL
BRL
BRL
BRL
BRL
BRL
Sidewall
Over -Excavated
#2 EW (6.5 -7)
2/10/2021
Tank Pit 2&3
7
Closure
26.3
7.76
18.8
BRL
BRL
BRL
BRL
BRL
BRL
Sidewall
Over -Excavated
#2 WW (6.5 -7)
2/10/2021
Tank Pit 2&3
7
Closure
6.27 J
BRL
30.1 J
BRL
BRL
BRL
BRL
BRL
BRL
Sidewall
Over -Excavated
#2 BASE (15.0)
2/10/2021
15
Closure
2,277.2 J
44.7
10,194
BRL
1.38 J
1.37 J
20.2
29.8
9.27
Tank Pit 2&3 Base
Soil -to -Groundwater MSCC (mg/kg)
31
68
540
8.3
5.2
55
0.054
1.5
64
Residential MSCC (mg/kg)
469
625
1,560
930
15.6
625
22.8
62.5
469
Industrial/Commercial MSCC (mg/kg)
7,000
9,340
1 23,300
14,000
233
9,340
112
934
7,000
Bold values exceed lowest MSCC.
BRL = below reporting limits
ft BGS = feet below ground surface
J = Analyte was positively identified but the value is estimated below the reporting limit.
mg/kg = milligrams per kilogram
MSCC = maximum soil contaminant concentration
NE = not established

Table B-3: Summary of Soil Sampling Results (Page 3 of 4)
Revision Date: 3/28/2021 Incident Number: Pending — Camp Stewart Road Site, Charlotte, NC Facility ID#: N/A
Analytical Method (e.g., VOC by EPA 8260) 4
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
Contaminant of Concern 4
c
o
a
F
nt
c
°NN
v A
„
y0
0
d '�'
N
y
❑
>+
o
a
r
Date
Source Area
Sample
Incident
A
>
p
>
a s
A
o
9
O
E
r
a
Sample ID
Collected
(eg. Tank
Depth
Phase
Fq
oa
W
° U
G
a
o
L
,z
o
a
F
F
T
23
0
(m/dd/yy)
pit 1)
(ft BGS)
(Closure,
c
LSA, etc.)
Over -Excavated
#2 NW (6.5 -7)
2/10/2021
Tank Pit 2&3
7
Closure
1.68
0.224
0.287
0.326
6.55
0.371
7.76
0.595
BRL
4.98
1.79
BRL
1.79
Sidewall
Over -Excavated
#2 SW (6.5 -7)
2/10/2021
Tank Pit 2&3
7
Closure
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
Sidewall
Over -Excavated
#2 EW (6.5 -7)
2/10/2021
Tank Pit 2&3
7
Closure
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
Sidewall
Over -Excavated
#2 WW (6.5 -7)
2/10/2021
Tank Pit2&3
7
Closure
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
0.0051 J
BRL
BRL
BRL
Sidewall
Over -Excavated
#2 BASE (15.0)
2/10/2021
Tank Pit 2&3
15
Closure
BRL
BRL
0.823
0.777
8.17
0.404
5.45
BRL
0.161
6.14
4.15
0.521
3.63
Base
Soil -to -Groundwater MSCC (mg/kg)
2.4
1.7
8
1.3
0.12
0.42
0.2
1.4
5.4
6.6
6
6
6
Residential MSCC (mg/kg)
782
1,560
60.3
1,560
1,560
1,250
5.5
1,560
1,250
156
3,120
3,120
3,120
Industrial/Commercial MSCC (mg/kg)
11,600
23,300
297
23,300
23,300
18,600
27
23,300
18,600
2,330
46,700
46,700
1 46,700
Bold values exceed lowest MSCC.
BRL = below reporting limits
ft BGS = feet below ground surface
J = Analyte was positively identified but the value is estimated below the reporting limit.
mg/kg = milligrams per kilogram
MSCC = maximum soil contaminant concentration
NE = not established

Table B-3: Summary of Soil Sampling Results (Page 4 of 4)
Revision Date: 3/28/2021 Incident Number: Pending — Camp Stewart Road Site, Charlotte, NC Facility ID#: N/A
Analytical Method (e.g., VOC by EPA 8260) 4
MADEP
MADEP
MADEP
8270
8260
VPH/EPH
VPH
VPH/EPH
Contaminant of Concern 4
Incident
�?
Ed
d U
y
Date
Source Area
Sample
phase
o �
U
U
? �
U
Sample ID
Collected
(eg. Tank
1)
Depth
BGS)
(Closure,
Z
(m/dd/yy)
pit
(ft
LSA, etc.)
Additional
Over -Excavated
#2 NW-2 (6.5 -7)
3/22/2021
7
Closure
--
--
--
BRL
BRL
Tank Pit 2&3
Sidewall
Additional
Over -Excavated
#2 SW-2 (6.5-7)
3/22/2021
7
Closure
BRL
BRL
BRL
--
--
Tank Pit 2&3
Sidewall
Soil -to -Groundwater MSCC (mg/kg)
31
68
540
0.054
0.2
Residential MSCC (mg/kg)
469
625
1,560
22.8
5.5
Industrial/Commercial MSCC (mg/kg)
7,000
9,340
23,300
112
27
Bold values exceed lowest MSCC.
BRL = below reporting limits
ft BGS = feet below ground surface
J = Analyte was positively identified but the value is estimated below the reporting limit.
mg/kg = milligrams per kilogram
MSCC = maximum soil contaminant concentration
NE = not established
-- - Not Analyzed

APPENDIX A
FIELD DOCUMENTATION

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via!
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&A -all �WJL

26

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[e-mail]
�( E L L E R'5830 Wright Road
■�.. k.II.m,Iningxom M I N I N G i.o Kannapolis, NC 28081
DIRT & GRAVEL 704.699.9312
INVOICE
Customer C4-1
Address mid l r►LA 57`r4 f K
Phone
Truck QS 3 ❑ TAN ❑ TRI W-WAD
OTY
DESCRIPTION
PRICE
YDS STONE
TONS SAND
TONS SAND
YDS DIRT ASPHALT
LOADS DIRT IN
LOADS DIRT OUT
TRASH & DEBRIS
DATE: 7-2- '-zoz
Past due balances are subject to a 7Y2% service charge
TRUCK RENTAL TIME
START
STOP
LUNCH
N° 13491
Received By:
'NOT RESPONSIBLE OR LIABLE FOR DAMAGE TO
ANYONE'S PROPERTY PAST THE CURB LINE
�_; [e-mail]
INE L LE R 5830 Wright Road
kellermining.com M I N I N G i..
Kannapolis, NC 28081
DIRT & GRAVEL 704.699.9312
INVOICE
Customer lec;
Address .57 5-VI 6,2e, P Gc.r�r e3
Phone
Truck _tom' 3 ❑ TAN U TRI a WAD
OTY
DESCRIPTION
PRICE
YDS STONE
TONS SAND
TONS SAND
YDS DIRT ASPHALT
LOADS DIRT IN
LOADS DIRT OUT
TRASH & DEBRIS
DATE:
Past due balances are subject to a 71h% service charge
TRUCK RENTAL TIME
START
STOP
LUNCH
N° 13238
Received By: —':�
`NOT RE NS►BLE OR LIABLE FOR DAMAGE TO
ANYONE'S PROPERTY PAST THE CURB LINE

ELLER / %- " dirt5830WrightRoad
ffikellemini-el-- M I N I N G I n
Kannapolis, NC 28081
DIRT & GRAVEL 704.699.9312
INVOICE
Customer Af c r
Address S-rC1 r�ptlK� S�t�fGe.r9''—
Phone
Truck ❑ TAN J TRI 4-66AD
QTY
DESCRIPTION
PRICE
YDS STONE
TONS SAND
TONS SAND
YDS DIRT ASPHALT
LOADS DIRT IN
LOADS DIRT OUT
TRASH & DEBRIS
DATE:
Past due balances are subject to a 7Y2% service charge
TRUCK RENTAL TIME
START
STOP
LUNCH
N° 13499
Received BY:1
*NOT RESPONSIBLE OR LIABLE FOR DAMAGE TO
ANYONE'S PROPERTY PAST THE CURB LINE
�, ; [e-mail]
E L L E R� 5830 Wright Road
T% kellermining.com M I N I N G inc Kannapolis, NC 28081
DIRT & GRAVEL 704.699.9312
INVOICE
Customer 6a
Address &Sol &Mp
Phone
Truck Ll TAN ❑ TRI V6UAD
QTY
DESCRIPTION
PRICE
YDS STONE
TONS SAND
TONS SAND
YDS DIRT ASPHALT
LOADS DIRT IN
LOADS DIRT OUT
TRASH & DEBRIS
DATE: 3 22 /20Z
Past due balances are subject to a 7Yz% service charge
TRUCK RENTAL TIME
START
STOP
LUNCH
N° 13490
Received Bv:Al Le- �--
*NOT RESPONSIBLE OR LIABLE FOR DAMAGE TO
ANYONE'S PROPERTY PAST THE CURB LINE

� [e-mail]
EILLER MINING��� 5830 Wright Road
DIRT & GRAVEL Kannapolis, NC 28081
704.699.9312
INVOICE
Customer C
Address
Phone
Truck ❑ TAN ❑ TRI AD
O'
DESCRIPTION
PRICE
YDS STONE
TONS SAND
TONS SAND
YDS DIRT ASPHALT
LOADS DIRT IN
LOADS DIRT OUT
TRASH & DEBRIS
DATE: -z ;7-
Past due balancelf are subject to a 71h% service charge
I HUUK RENTAL TIME
START
STOP
LUNCH
N? 13498
Received By: Am J M
*NOT RESPONSIBLE OR LIABLE FOR DAMAGE TO
ANYONE'S PROPERTY PAST THE CURB LINE
dirt5
ELLER /— 5830 Wright RoadKellemining.eomMININGino
Kannapolis, NC 28081
DIRT & GRAVEL 704.699.9312
INVOICE
Customer cr.)�-
Address G'r1Jrtf gllffl �l,I
Phone
Truck ❑ TAN ❑ TRI Q<rAD
QTi
DESCRIPTION
PRICE
YDS STONE
TONS SAND
TONS SAND
YDS DIRT ASPHALT
LOADS DIRT IN
LOADS DIRT OUT
TRASH & D BRIS
DATE: 3 -
Past due bala/es are subj t to a 71h% service charge
TRUCK RENTAL THE
START
STOP
LUNCH
NO& 1.3492
Received By: 7
*NOT RESPONSIBLE OR LIABLE FOR DAMAGE TO
ANYONE'S PROPERTY PAST THE CURB LINE

APPENDIX B
SITE PHOTOGRAPHS

CAMP STEWART ROAD SITE
(FEBRUARY 8 - 10, 2021)
VIEW OF UST-2 & UST-3 LOCATION PRIOR TO CLEARING/EXCAVATING I VIEW OF UST-2 & UST-3 LOCATION FOLLOWING CLEARING
ACTIVITIES
VIEW OF EXCAVATION OF OVERBURDEN AT UST-2 LOCATION WITH TOP OF I VIEW OF EXCAVATION OF OVERBURDEN AT UST-3 LOCATION WITH TOP OF
UST-2 IN FOREGROUND UST-3 IN FOREGROUND

CAMP STEWART ROAD SITE
(FEBRUARY 8 - 10, 2021)
VIEW OF FULL UST-2 & APPARENT EMPTY UST-3, WITH UST-3 TILTED SO
ANY RESIDUAL PRODUCT COULD BE PUMPED OUT PRIOR TO REMOVAL
VIEW OF UST-2 REMOVED FROM LOCATION — NO PITTING OR HOLES
OBSERVED
VIEW OF PRODUCT BEING PUMPED FROM UST-2
VIEW OF BASE OF UST-2 TANK PIT AREA WITH STAINED SOILS AND
PETROLEUM ODOR

CAMP STEWART ROAD SITE
(FEBRUARY 8 - 10, 2021)
A 1G
VIEW OF UST-3 AFTER REMOVAL FROM LOCATION - NO PITTING OR HOLES
OBSERVED
VIEW OF #2 NS AND #2 SS RELEASE DETECTION SOIL SAMPLE LOCATIONS
VIEW OF #3 NS AND #3 SS RELEASE DETECTION SOIL SAMPLE LOCATIONS
r.
VIEW OF UST-2 & UST-3 OVER -EXCAVATED PIT LOCATION PRIOR TO
CONFIRMATORY SOIL SAMPLING WITH BASE DEPTH OF 15 FEET

CAMP STEWART ROAD SITE
(FEBRUARY 8 - 10, 2021)
VIEW OF UST-1 LOCATION PRIOR TO CLEARING/EXCAVATING ACTIVITIES I VIEW OF EXCAVATION OF OVERBURDEN AT UST-1 LOCATION
VIEW OF PRODUCT BEING PUMPED FROM UST -I I VIEW OF REMOVAL OF UST-1 FROM TANK PIT

CAMP STEWART ROAD SITE
(FEBRUARY 8 - 10, 2021)
AFT
ti
VIEW OF #1 NS AND #1 SS RELEASE DETECTION SOIL SAMPLE LOCATIONS
VIEW OF UST-1 AFTER REMOVAL FROM LOCATION —NO PITTING OR HOLES
OBSERVED
3
VIEW OF UST-1 LOCATION AFTER BACKFILLING OF PIT AREA
VIEW OF LOADING OF USTs FOR OFF -SITE DISPOSAL

CAMP STEWART ROAD SITE
(MARCH 22, 2021)
VIEW OF UST-2 & UST-3 PARTIALLY-BACKFILLED EXCAVATION LOCATION
PRIOR TO ADDITIONAL EXCAVATION ON MARCH 22, 2021
VIEW OF THE SOUTH WALL OVER -EXCAVATION AFTER COLLECTION OF
CONFIRMATORY SOIL SAMPLE #2 SW-2
VIEW OF PETROLEUM -IMPACTED SOIL BEING LOADED INTO DUMP TRUCK
FOR OFF -SITE TRANSPORT
VIEW OF THE NORTH WALL OVER -EXCAVATION AFTER COLLECTION OF
CONFIRMATORY SOIL SAMPLE #2 NW-2 AND DURING PLACEMENT OF
UNIMPACTED OVERBURDEN SOIL

CAMP STEWART ROAD SITE
(MARCH 22, 2021)
VIEW OF THE SOUTH OVER -EXCAVATION AREA AFTER THE UNIMPACTED VIEW OF THE NORTH OVER -EXCAVATION AREA AFTER THE UNIMPACTED
OVERBURDEN SOIL WAS PLACED AND COVERED WITH ORANGE FENCING I OVERBURDEN SOIL WAS PLACED AND COVERED WITH ORANGE FENCING
klm
Eta
\.
VIEW OF THE IMPORTED BACKFILL SOIL BEING PLACED WITHIN THE VIEW OF THE UST-2 & UST-3 EXCAVATION LOCATION AT THE CONCLUSION
EXCAVATION ON TOP OF THE ORANGE FENCING I OF THE FILL PLACEMENT

APPENDIX C
UST-2B, SITE INVESTIGATION REPORT FOR PERMANENT CLOSURE OR
CHANGE -IN-SERVICE OF UN -REGISTERED UST

UST-2B
Return completed form to:
Site Investigation Report for Permanent Closure or Change -in -
Service of
L1N-REGISTERED LIST
NC DEQ / DSNM ! UST SECTION
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN. REGISTRATION & PERMITTING
phone [phone] fax [phone] httpi//vvww.wastetiotnc.oroi
Facility ID #
Date Received
STATE USE ONLY:
INSTRUCTIONS (READ THIS FIRST) _
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at httipJ/deq.nc. ov/about/divisions/waste-manag ement/waste-
mana ement- ermi uidance.iunder round -story e-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change -in-service: Where UST systems wi11 be converted from storing a regulated substance to a non -regulated substance, complete sections I,
11, 111, IV, and VI.
4. For more than 5 un-registered UST systems, attach additional forms as needed.
5. Un-Re gistered USTs may be subject to unpaid fees and late penalties.
6. REGISTERED USTs use Form UST-2A.
I. OWNERSHIP OF TANKS
11. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)
Facility Name or Company
Professional Child Centers, Inc.
Professional Child Centers, Inc.
Street Address
Facility ID # (If known)
505 Beachland Blvd, Suite 41
NIA
City
County
street Address
Vero Beach
Indian River
Camp Stewart Road, Tax PIN 11 109204
State
Zip Code
City County Zip Code
FL
32963
Charlotte Mecklenburg 28215
Phone Number
Phone Number
772-913-1152
NIA
m r-nkt r h i-,' m=DQnAiki=i
Contact for Facility:
Job Title:
Phone #:
Dean Davidson
Property Ow-ner
772-913-1152
Closure Contractor Name:
Closure Contractor Company_
Address:
Phone #
Eric Brown
A&D Environnlental Services,Inc
P.O. Box 494
336-434-7750
high Point, NC 27261
Primary Consultant Name:
Primary Consultant Company:
Address:
Phone #
Nora Zirps. PE, RSM
ESP Associates, Inc.
P.O. Box 7030,
704-583-4949
Charlotte, NC 28241
IV. UST INFORMATION
FOR UN -REGISTERED UST SYSTEMS
V. EXCAVATION CONDITION
REGISTERED USTs use Form UST-2A.
Tank ID
Size in
Last
Last
Permanent
Method of Permanent Closure:
Change -in-
NctaMs-
No.
Gallons
Contents
Use
Close Date
Indicate REMOVED or enter fill
Service
Water in
Free product
adar
visible
or
soil
Date
material, such as foam/
Date
excavation
contaminatio
concrete/ sand
R
Yes
I No
Yes
No
Yes
No
UST-1
550
Heating Oi
NK
2/9/2021
REMOVED
NIA
❑
®
❑
®
❑
UST-2
600
Heating Oil
NK
2/9/2021
REMOVED
NIA
❑
®
❑
®
®
❑
UST-3
550
Heating Oil
NK
2/9/2021
REMOVED
NIA
❑
®
❑
®
®
❑
❑
I ❑
❑
❑
❑
❑
VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate
and complete.
Print name and official title of owner or owner's authorized representative
Nora Zirps, PE, RSM - Agent for Professional Child Centers, Inc.
Signature Date Signed
9
.rl. 1 3/28/2021
( NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL [QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION k

APPENDIX D
DISPOSAL DOCUMENTATION

&Environmental ServicesBill Lading- r I
A&D Job No:
Generator ID Number
Page 1 of
Emergency Response Phone
Tracking Number
Generator's Name and Mailing Address I Generator's site address (if different from mailing address)
3 p VIS
Generator's Phone
Transporter 1 W2Lj Company Name A D Environmental Services, Inc.
US EPA ID No: NCD986232221
Transporter 1 020 Company Name A&D Environmental Services (SC), LLC
US EPA ID No: SCD98 5598331
Transporter 1 2 Company Name
US EPA ID No:
Designated Facility
VAD Environmental Services, Inc.
2718 Uwharrie Road
Archdale, NC 27263
336-434-7750
NCD986232221
Designated Facility
A&D Environmental Services, Inc.
3149 Lear Drive
Burlington, NC 27215
336-229-0058
NCR000138628
Designated Facility (Please insed facility information below) -
I
HM
Hazardous Materials Shipping Name and (if applicable)
No.
Type
QTY.
WUVol
Profile Number
,
'Description
i
r � f'•.� t'�I� -,+ .. !`r t'tl��'�_ 1. (..h ..k. V t' ._% �-�� I \-,'_., 7 '< �J `i...�'.�..6
-'�i'�".-..-_� -_
„'F` �.thy
�,,,.� C..
? v�� r..-.-
i . �.r � �-✓ � 7 gr3
t
I
Petroleum Products for Recycle
No.
Type
QTY
WWol
Profile Number
X
NA1993, Diesel fuel, 3, Ill EGR# 128
X
NA 1993, Fuel oil No, 1,2,4,5 or 6), 3, 111 EGR# 128
X
UN1203, Gasoline, 3, II EGR# 128
USED OIL (Not a USDOT Hazardous Material)
Petroleum Contact Water (Not a USDOT Hazardous Material
_ Universal Waste Lamps, Batteries, Ballasts, and Electronics for Recycle
HM Ne. Type Est. Wt.
Count
Shipping Name and Description (if applicable)
Common Name
Discrepancy
X
RQ, UN3506. Mercury contained in manufactured articles, 8 (6.1), RQ ERG# 172
Mercury Devices
X
RQ, UN3432, Polychlorinated biphenyls, solid. 9, If EGR# 171
T'SCA Exempt PCB Lamp Ballasts
X
UN2800, Batteries, wet nonspillable, 8 EGR# 154
Sealed Lead Acid Batteries
X
UN2794, Batteries, wet, filled with acid, 8 EGR# 154
Lead Acid Batteries
X
UN2795, Batteries, wet, filled with alkali, 8 EGR# 154
Wet NiCad Batteries
X
UN3090, Lithium metal batteries, 9 EGR# 138
Lithium Metal Batteries
X
UN3480, Lithium ion batteries, 9 EGR# 147
Lithium Ion Batteries
X
Batteries, dry, sealed n.o.s.
Alkaline Batteries
X
Batteries, dry, sealed n.o.s.
Dry NiCad Batteries
Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173-164 (a) Florescent
famps (4-Ft and Under)
Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164 (a)
Florescent lamps (Over 4-FL)
Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164 (a)
Circular/U-tube lamps
Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173,164 (a) I
Compact Lamps
Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164 (e)
Shielded Lamps
Universal Waste Lamps (Not DOT -Regulated per 49 CFR 171164 (a)
HID/NiViUV Lamps
Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164 (e)
Incandescent Lamps
Non -PCB Light Ballasts for Recycle (Not DOT -Regulated) Non
-PCB Light BallastsrCapacilors
Electronic Equipment for Recycle Not DOT -Regulated)
a -Waste
Generator's Certification: This is to certify that the above -named materials are properly classified, described, packaged, marked, and labeled, and are in proper condition for transport according to iho
applicable regulations of the Department of Transportation. I further certify That none of the materials described above are hazardous waste as defined by EPA 40CFR Pad 261 or any applicablo slab law, and
unless specifically identified above the materials contain less than 1,000 prim total halogens and do not contain quantifiable le prim f PCBs as defined by EPA40 CFR Pads 279 and 761,
3enerator's/ Offeror's Printed/Typed Name Sign re Month Day Year
ansporier 1 Printed/Typed Name Signature Month Day Year
ransporter 2 Printed/Typed Name re Month Day Year
nsc[epancy indication r r+aaiuonaf information:.
fesignaled Facility Certification: I hereby acknowledge receipt of the materials covered by this manifest except for any discrepancy indicated above.
rinted/Typed Name ----� � I Signature Month Day Year

A Environmental Services, Inc.
P.O. Box 484 • High Point, NC • Phone [phone] • FAX [phone]
TANK DISPOSAL MANIFEST
1)
Tank Owner/Authorized Representative: Name and Mailing Address
Ae 9d)( Z,2-To
2)
Tank Owner/Authorized Representative: Contact -r
Phone#: 74LI
3)
Description Of Tanks:
Tank No, Capacity Previous Contents Comments
Smp
i 9
S CCY
3 l ®OC7 t 1
25 r
4)
Tank Owner/Authorized Representative Certification: The undersigned certifies that the above listed storage
tanks have been removed from the premises of the tank owner.
PrintedlTyped Name Signature Month/DaylYear
5)
Transporter: The undersigned certifies that the above listed storage tanks have been transported to A&D
Environmental and Industrial Services, 2718 U harrie Road, Archdale, N.C. 27263.
ALl i✓ l3eattl
PrintedlTyped Name Signature Monrh/DaylYear
6)
Disposal Certification: The undersigned certifies that the above named storage tank(s) have been cut
into scrap pieces and accepted by the metal recycling facility.
Recycling Facility: VA'_ _
PrintedlTyped Name Signature Month/DdylYear

.2' 10, Nor.
NORTH CAROLINA
OLIO WI=iGHMASTEP
Alternative Emel-gy Soltttioas of NCI LI,C' 'LICENSEE V ES 4 - 30, 2l}iq
Lost Office Box 310 �� 42672
�
Sanford, N(' 2733 t dOE F. HOWE
Phone #: [phone] IQdt•?1�t..lt3 I�AlI : SICN�iI
Fax #: [phone]
NON HAZARDOUS wASI•L; MANWES'1'
Project Number Load Number-
0 -44 .`
('ollsultattt: G _...
GAS Contact:
Phone: 334- �10 6474
Generator: ., 1-AJ( Contact:
I'Irone:
Transporter: PC !n r n contact:
g}trVk�e
Phone:
IIlatlOil; ACS C'ontflet: Scott Keller
3841 ('uurlirtgh:tnt Itoacl
'1'hontasyille, NC 27360 Phone:
Fe DetiCl•ipti0li: flSte i
4 Origination:
It #: ! 5 (o Gross Weight:
7`a re weight: ID. 1I0,
21,134"D ill TR
I
(6.--�L-1 .("_!
L'erucrator's Certif ention: I certify that the materials described about oil this manifest flee not
subject to Feder' ulations for' 1'epo"6119 Proper• dispposal of HAZARDOUS WASTE,,
Generator / Agent Signatut'e
Achnowledgrnent of Receipt of Material
Ic tt[c
3 22 2-az
crs Si ,natture I)aie
Noted Discrepancies:
Inspected & Accepted (except as anted above By: Larthtec I' snvironatental, 1rla)
Accepted By: t bate:
0 - ;:-�,O z-,(

Alternative Energy Solutions of NC, LLC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
Fax #: [phone]
W1W II A.r A n■v—
14 10. NO.
614156t0 ib OR
.NQRTFI CAROLINA
PUSLRCA' CIGHI< ASTER
LCCP.Ny : �`. JUNE 30, 201R
Jog F: I� 42fir�?
11 Vl9 i UNI. A+CfP'ii rg
-
Project Number:
��
ars�a.rnia
load Ntimber:
Consultant: 5
Colthict: Nor-,
Ph(►ne: g
Tenerntor. CGc iNt
Colttact:
Na �n *sue
Phone:
I'rausporter: 1�s���r Cis
i/
Contact: _ _w
Phone:
Destination: AF,S --
('ontact:
Scott Keller�_— —
3841 Cnoviingham Itnacl
Thomasville, Nf' 27360
Phone:
Waste Descrii)tioli: —
Waste a j y�• ��111° -
Origination:
—
Truck Ih
S
C1•o5S Weight:
`" °, /2,021
tore weight:-
-
Net Weight:
—
3,1560 lb HT
Gernerator's ['ertification: I certify that the materials described above olr this n)ai)ifest arc not
sub,iecl eder'a ous for I-epor•6119 proper disposal of tIAZARDOl1ti WAS'i E-
Generator / Ageut Signature
Acknowledgmeat of Receipt of Material: _
Drivers Signature � Dale
Noted Discrepancies.
luspeeted & Accepted (except as noted above By: I?artlltec I,uvironn3eutal, Inc.)
Accepted By:
m
r.�

NOhTj4 CARdLWA
_ > UBLIC Yilrt7GHMASTER 01
Alternative IsllerPA•Y Slilutiolls of NC', 1,I,C' L.ICF.N� ! glal 4 B JIiA1L 3D,
I'nsl Office Box 310 'JOE
42672
fianFOrd, NC27331 s
Phone #: [phone] '° P ? :'� ! S •�sl �' ' '
r
Fax #: [phone] ,
NON 11A%ARU()lIS WA8'1'i? MANII.1';5'1`
1'rlsjccl Nunthcr:
J Lond Number
oilt:1Ct: -Z �P 3
icurratur: Cc rl
'randlorter:
DCv,LGIwe*— v!e-e
3841 C unninl;hllill Road
' hopilasville, NC27361i
c i)chcription: ~—
�'. A- it-+ - S D r
pS -.:I,
C'on tact;
Phone:
t'r►ntuct: Scoti
licller
1'hauc:
(h•igiu:lticnl:
(:toss Weil;h
61s22v�
!'are Weight;
•--�—__.—_�� � ii
Net Weight:
~'
34220 lb NT
Cerneratol•'s ('ertificatioll: 1 c•ertiFv that the materials described :11)ove oil this 11-llifest are nol suhjecl In fede 11 r Lions tt►r rclsur"1114 proper dispasal of HAZARDO(IS WASTE.
Gellel•itor / Akc11 Sigilaturc
Acknowledgrneill of Receipt of MAte1•iat: 1 i t:ilr1
ers Signature I a L
Nutcrl Uisrrcp:lucies:
111sisecletl & Accepted (except As noted Above lly: 1sArthtec Environmer►tul, Inc.)
Accepter! 13y:•-

Alternative I:ne)-gY Solutions of NC, 1,I,C'
Post Office Box 310
yanli►rd, NC 27331
I'llone M. 336-302-0889
FAX #: [phone]
NORTH CAROLINAEi ..
PUBLIC WtIMASTER -
L10EN.SE. EXNikt JUKE 30, 2019
JOE F. HOLDER M72
IN ALID UNLE SIGNED
L .
NON 11AZARI)0115 WASTE MANIFEST
lll'o,�ert �lllillll•1':—^-,--~
bv8
1,0a(I N11111I)er �"-
('ontillu:►Ilt:
,S 1
C'onhlct: N -
welerator
1.1'fllltill()1'tl`{':
�CY+ fr arsGr✓lGei
✓
C•alit.lCt.�._�.—~---J—__.-�_—._...- .�
IDcsrinatiun: Ares
Pholle:
t ,lnrart:
38.11 ('nnnina;halll tic►.{d
_ Thomasville, N(' 2736Q
Phone:
Wasle Uesc•r'illtil►11: -��—_
5S o f �. ` �' �c.� •.r� iL�
(h•igillatiun:
ps „
Gross Weight. { 0 ` +y 0 q
-- —�_�
69200 1b GAR
Ne! Wl•I�llt: {
F-
1�+l7'
J
(rL'1'Ilel'1{t{/l''ti ('e1'tlfil`:Itlllll: 'Y t11at the nlaterials
dcscrihe(I above oil this Malllfest are n{)t
sub,�rc'I to fccicrl{I rc ons to cllortin}� proper clisllos111 of IIAI,kRU()114 WASTE.
(:e /
razor Al;rnt �ignailn'e
��.--�-
ACIi11UtiVIe(Il!n11,`{II of RL'rellll 1)1' M;lterlal:
1 S;IIi'
Drivers .'I"ll8t111'l'
Nmed
11181)rctld & Accel)(ed (excellt a8 noted above By: 1',al-tllter 1'.I1Wirolllllelltal, 111C.) •� _---� ���--��
Accepted 13y:
_ __ Dale: �j— - �(

Alternative Energy SoIntions of NC, I,I,C "
Post Office [lox 311)
Sanford, NC 27331
Phouc P: 336r392-0889
Fm #: 704-973-9573
NoItik( CAR47LINA '
pUK.,IC WEIG.jjI4R9''tli.
U1 FN5t EXP RE 4 1001-267
JQE F. HOL
INVA D S-SIGNED
NON HAZARDOUS WASTE, MA,NIFES'Y
I't•o.Iect IVunthcr'' -��- Load Numhet•:
Who
{'cnitact-
Z.f'fS
Phone: 3 3 L- 1L%a0�(o el 7 et
C.encrafu:: I�Grr �µe {'ontact: _.. -
I ransportcr;
lmfiolt:
3841 ('utill ingliant Bond
Thomasville, NC 273611
ut DDcsvrilttiolt: --
TY 4 1 6ff lS vv�
DJ
Phone:
{'(in l a ct:
Phone:
Contact: Scutt Feller
.Phone:
Origination:
�al'11titi Well;lll:
�y y+�
2 IDS fe
I ell a WCi�ltt:
21340 I�b FR lT EQ
Net Weight:
Cer-ner'alorY ('ertific ' )n I certify that the maMrials described above on this mmn!Ng sure nol
sub•jecl s fede - Sul: ons for reptn•tillg proper disposal of HAZARDOUS WAS'11,_
:euersttor / Agent !iignatnrc-
Acknowledglnenl of Receipt of 1lhsllerissk:
)rivers signature
!Voted Discrepancies:
Inspected & Acreptecl (except as noted strove By: Isartlttec 1?Itvironmental, Inc.)
Accepted By: Dole: ��

2019
Fri
Ip..1C69w8E E 4i02
.90E 5. HOL E
l)
Allernative Emergy Nolutions ofNC, I,l,C
Post Office Box 310 V,
Sanford, N(' 27331
Phone #- 336-302•-0889
Fa x #: 7114-973-95'13
NVIN ItAOA1)ndr1l1C \1fAU,ru ma
Project Number —�
Load Number:
�— --- ----
gs
--
I'llone; 33
_ Y;I.0 4,1 7
---__
-y-•
---
Contact'
-- -----..��_'----'_------------
Rj
Transporter: 1�
YC✓�y' Cl, � S4F'✓r i '� i
Contact:
— - — - -
Ph<nre:
Destination: AES — � `��
Contact: "S
olt"Kehler `—`--
3841 Cunningham Road
'Thomasville, N(' 273G{I
I'hone:
w is(e Description: - . ----
ame
Origination:
_
C-1-oss Wei TIrt:
jj }yam 0 fµl2y
21321
Tare Weight:
t:.yr
h 4I � ' i'��•_ -_
rA�
i�l04 lb wR
\�
YY/
Net Wight:
h. ✓'f 'J. -��� 1�Ar��
40680 lb
nH
Gerneralor's Cer'tifi r cer'til',y that the rma(erials described above on this manifest are nol
subject to 1'cdcra gelation fur reporting proper disposal of 11AZARDOtIS WAST F,.
� c
.ellerator / Agent Signatm- a ------ --p 11aftl
Adwowledgment of Receipt of Mlajerial: -- —� 1, 2?• nazi
1 r i v
r 4ignalure
Noted Discrepancies:
Inspeded & Accepted (except as noted above 13y: P;al'thtec I?nviroll file ut.)1, Inc.) — --
Accepted By:

APPENDIX E
UST-61, 24-HOUR RELEASE AND UST LEAK REPORTING FORM

UST-61
I 24-Hour Release and UST Leak Reporting Form
For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release
in NC from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a
known or suspected release
(DWM USE ONLY)
Suspected Contamination? (Y/N) Y
Facility ID # N/A
Y
Incident # Risk (H,I,L,U)
Confirmed GW Contamination? (Y/N) N
Received On Received By
Confirmed Soil Contamination? (Y/N) Y
Date Leak Discovered 2/9/2021
Region
/ ? k T Samples Taken? YN
Sam p ( ) Y
Comm/Non-Commercial. Non -Comm
Reported by (circle one): Phone, Email or Report
NAPL? (Y/N) N
Reg/Non-regulated? Non -regulated
If Yes, State Greatest Thickness N/A
INCIDENT DESCRIPTION
Incident Camp Stewart Road Site
Name:
Address: Camp Stewart Road, Tax PIN 11109204
County: Mecklenburg
City/Town: Charlotte
Zip Code: 28215
Regional Office (circle one): Asheville, Fayetteville, Mooresville,
Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): 35.241186
Longitude (decimal degrees):-80.661215
Location Obtained by:
El GPS
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount of
release, amount of NAPL present and recovery efforts, initial responses conducted, impacts to receptors)
❑ Topographic map
As part of Pulte Home Company, LLC's due diligence in advance of purchasing the subject property, two approximate
adjacent 550- allon heating oil USTs, designated UST-2 and UST-3, were removed. Upon removal of the two USTs,
V GIS Address matching
two leak detection soil samples were collected from the base of each of the two UST pits for laboratory analysis of
TPH-DRO and TPH-GRO see Table B-3 attached). All 4 release detection samples exceeded NCDEQ's TPH-DRO
✓ Other — Google Earth
❑ Unknown
screening level of 100 ppm, with levels ranging from 2,040 to 10,500 ppm. One release detection sample exceeded
NCDEQ's TPH-GRO screening level of 50 ppm, with a level of 75 ppm. An attempt was made to excavate all
Describe location:
petroleum -impacted soil, confirmatory soil samples were collected for laboratory analysis, and an Initial Abatement
Action Report is under preparation. The confirmatory soil sample analytical results at the base and two sidewalls
of the excavation show exceedances of residential MSCCs; therefore, a Limited Site Assessment is being planned.
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
❑ Release Detection Equipment or Methods ❑ Visual/Odor ❑ Groundwater Contamination
✓ During UST Closure/Removal ❑ Water in Tank ❑ Surface Water Contamination
❑ Property Transfer ❑ Water Supply Well Contamination ❑ Other (specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release Product Type Released
(Check one to indicate primary source) (Check one to indicate primary cause) (Check one) (Check one to indicate primary product type released)
✓ Tank ❑ Spill ✓ Petroleum ❑ Gasoline/Diesel/ ❑ Diesel/Veg.Oil
❑ Piping ❑ Overfill ❑ Non -Petroleum Kerosene Blend
❑ Dispenser ✓ Corrosion ❑ Both `/ Heating Oil ❑ Veg. Oil 100%
❑ Submersible Turbine Pump ❑ Physical/Mechanical Damage Location ❑ Other Petroleum ❑ E10 — E20
(Check one) Products ❑ E21 — E84
❑ Delivery Problem ❑ Install Problem
❑ Metals
❑ Facility ❑ E85 — E99
❑ Other (specify) ❑Other (specify) ❑ Other Inorganics
❑ Unknown ❑ Unknown ❑ Residence ❑ Ethanol 100%
❑ Other Organics
Definitions printed on reverse Definitions printed on reverse ✓ Other Summer ❑ E1 — E9
camp office
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig 5. Industrial 6. Commercial 7. Mining
(Recreational)
UST Form 61 (05/17) Page 1 of 2

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 12. No 3. Unknown
Number of Water Supply Wells Affected: N/A
Water Supply Wells Contaminated: (Include Users' Names, Addresses, and Phone Numbers. Attach additional sheet if necessary.)
1. N/A
2.
3.
UST SYSTEM OWNER
UST Owner / Company:
Professional Child Centers, Inc.
Point of Contact:
Address:
Dean Davidson
505 Beachland Blvd, Suite #1
City:
State:
Zip Code:
Telephone Number:
Vero Beach
FL
32963
772-913-1152
UST SYSTEM OPERATOR
UST Owner / Company:
Same as UST System Owner
Point of Contact:
Address:
City:
State:
Zip Code:
Telephone Number:
LANDOWNER AT LOCATION OF UST INCIDENT
UST Owner / Company:
Same as UST System Owner
Point of Contact:
Address:
City:
State:
Zip Code:
Telephone Number:
Draw Sketch of Area (showing two major road intersections) or Attach Map
See attached map
Person Reporting Incident
Company
Telephone Number
Nora Zirps, PE, RSM
ESP Associates, Inc.
704-583-4949
Title
Address
Date
Senior Project Engineer
P.O. Box 7030, Charlotte, NC 28241
March 9, 2021
UST Form 61 (05/17)
Page 2 of 2
Definitions of Sources:
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP): Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes:
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined

KINGBIRD CT ..
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w i 'V i L+ �R -
��-
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- 'P�� _ � i � � - -r - - _ - - - - _ _ - •for. � L WIG~CT
it C T
60
-
-- DRAWBR10Gf p� �P 4 - 3Tf�q�,TR.4CE�ipn4
-� Cr,
CELLO
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o
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p hJ
�J VfR ICA ORHARPLEY Cr
0 SERENADE ej
�a �E C i
EET P16 } 't O I Lr
^� kTs C pSSING.22
OR -
7R
f;--
ydea AC'Ro
�. EASTLAKE-RD
Site
All locations are approximate.
PROJECT NO.
GP56.600
SHEET TITLE
FIGURE 1
ESP Associates, Inc.
N
SCALE
As Shown
USGS TOPOGRAPHIC SITE LOCATION MAP
P.O. Box 7030
Charlotte, NC 28241
0 330 660 w+-E
FeetDRAWN
S
BY
FN
PROJECT
CAMP STEWART ROAD SITE
phone [phone]
CHECKED BY
Cw
DATE 512312018
CHARLOTTE, NORTH CAROLINA
www.espassociates.com

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/9/2021 Incident Number: Pending — Camp Stewart Road Site, Charlotte, NC Facility ID#: N/A
Analytical Method (e.g., VOC by EPA 8260) 4
8015
8015
8260
8260
8260
8260
Contaminant of Concern 4
°
Q
°
Date
Source Area
Sample
Incident
Sample ID
Collected
(eg. Tank
Depth
phase
a
a
(Cl
(Cl
(Closure,
w
(m/dd/yy)
pit 1)
(ft BGS)
etc
Tank Pit 2
42 NS (4-4.5)
2/9/2021
4.5
Closure
10,500
75.0
BRL
BRL
BRL
0.528
Base
Tank Pit 2
#2 SS (4-4.5)
2/9/2021
4.5
Closure
4,720
4.9 J
BRL
BRL
BRL
BRL
Base
Tank Pit 3
#3 NS (4-4.5)
2/9/2021
4.5
Closure
3,040
19.1
BRL
BRL
BRL
0.0342
Base
Tank Pit 3
#3 SS (4-4.5)
2/9/2021
4.5
Closure
2,040
25.3
BRL
BRL
BRL
BRL
Base
Soil -to -Groundwater MSCC (mg/kg)
NE
NE
0.0072
8
5.4
6
Residential MSCC (mg/kg)
NE
NE
12
60.3
1,250
3,120
Industrial/Commercial MSCC (mg/kg)
NE
NE
59.4
297
18,600
46,700
Bold values exceed lowest MSCC. TPH-DRO and TPH-GRO screening levels are 100 mg/kg and 50 mg/kg, respectively.
BRL = below reporting limits
ft BGS = feet below ground surface
J = Analyte was positively identified but the value is estimated below the reporting limit.
mg/kg = milligrams per kilogram
MSCC = maximum soil contaminant concentration
NE = not established

APPENDIX F
LABORATORY ANALYTICAL REPORTS

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
February 24, 2021
Chris Ward
ESP Associates
3475 Lakemont Boulevard
Fort Mill, SC 29708
RE: Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Dear Chris Ward:
Enclosed are the analytical results for sample(s) received by the laboratory on February 11, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
-�)GUA,
Bonnie Vang
[e-mail]
[phone]
Project Manager
Enclosures
cc: Account Payable, ESP Associates
REPORT OF LABORATORY ANALYSIS
r
e
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 65

laneAnalytical
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21LA 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92521577001
#3 NS (4-4.5)
Solid
02/09/21 14:10
02/11/21 08:00
92521577002
#3 SS (4-4.5)
Solid
02/09/21 14:15
02/11/21 08:00
92521577003
#2 NS (4-4.5)
Solid
02/09/21 14:20
02/11/21 08:00
92521577004
#2 SS (4-4.5)
Solid
02/09/21 14:25
02/11/21 08:00
92521577005
#1 NS (5.5)
Solid
02/10/21 09:45
02/11/21 08:00
92521577006
#1 SS (5.5)
Solid
02/10/21 09:50
02/11/21 08:00
92521577007
#2 NW (6.5-7)
Solid
02/10/21 17:25
02/11/21 08:00
92521577008
#2 SW (6.5-7)
Solid
02/10/21 17:37
02/11/21 08:00
92521577009
#2 EW (6.5-7)
Solid
02/10/21 17:05
02/11/21 08:00
92521577010
#2 WW (6.5-7)
Solid
02/10/21 17:15
02/11/21 08:00
92521577011
#2 BASE (15.0)
Solid
02/10/21 16:55
02/11/21 08:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
CAMP STEWARD ROAD SITE
92521577
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92521577001
#3 NS (4-4.5)
EPA 8015C Modified
SEM
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577002
#3 SS (4-4.5)
EPA 8015C Modified
SEM
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577003
#2 NS (4-4.5)
EPA 8015C Modified
JMS1
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577004
#2 SS (4-4.5)
EPA 8015C Modified
JMS1
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577005
#1 NS (5.5)
EPA 8015C Modified
JMS1
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577006
#1 SS (5.5)
EPA 8015C Modified
JMS1
2
PASI-C
EPA 8015C Modified
MAD
2
PASI-C
EPA 8260D
SAS
7
PASI-C
SW-846
KDF
1
PASI-C
92521577007
#2 NW (6.5-7)
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
ACG
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
92521577008
#2 SW (6.5-7)
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
JHH
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
92521577009
#2 EW (6.5-7)
MADEP EPH
BAJ
7
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Lab ID Sample ID
Method
Analysts
Analytes
Reported
Laboratory
MADEP VPH
JHH
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
92521577010 #2 WW (6.5-7)
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
ACG
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
92521577011 #2 BASE (15.0)
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
ACG, BMB
6
PAN
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #3 NS (4-4.5)
Lab ID: 92521577001 Collected:
02/09/21 14:10
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
3040 mg/kg 66.3
30.5 10
02/11/21 15:01
02/12/21 12:47
M1
C28)
Surrogates
n-Pentacosane (S)
92 % 32-130
10
02/11/21 15:01
02/12/21 12:47
629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
19.1 mg/kg 12.4
2.4 1
02/11/21 13:54
02/12/21 00:25
Surrogates
4-Bromofluorobenzene (S)
121 % 66-131
1
02/11/21 13:54
02/12/21 00:25
460-00-4
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Benzene
ND ug/kg 7.7
3.1 1
02/11/21 11:36
02/11/21 14:53
71-43-2
Ethylbenzene
ND ug/kg 7.7
3.6 1
02/11/21 11:36
02/11/21 14:53
100-41-4
Toluene
ND ug/kg 7.7
2.2 1
02/11/21 11:36
02/11/21 14:53
108-88-3
Xylene (Total)
34.2 ug/kg 15.4
4.4 1
02/11/21 11:36
02/11/21 14:53
1330-20-7
Surrogates
Toluene-d8 (S)
101 % 70-130
1
02/11/21 11:36
02/11/21 14:53
2037-26-5
4-Bromofluorobenzene (S)
125 % 69-134
1
02/11/21 11:36
02/11/21 14:53
460-00-4
1,2-Dichloroethane-d4 (S)
104 % 70-130
1
02/11/21 11:36
02/11/21 14:53
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
24.6 % 0.10
0.10 1
02/11/21 14:12
N2
Sample: #3 SS (4-4.5)
Lab ID: 92521577002 Collected:
02/09/21 14:15
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
2040 mg/kg 64.3
29.6 10
02/11/21 15:01
02/12/21 13:11
C28)
Surrogates
n-Pentacosane (S)
0 % 32-130
10
02/11/21 15:01
02/12/21 13:11
629-99-2 S4
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
25.3 mg/kg 10.8
2.1 1
02/12/21 11:17
02/13/21 00:21
Surrogates
4-Bromofluorobenzene (S)
110 % 66-131
1
02/12/21 11:17
02/13/21 00:21
460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #3 SS (4-4.5)
Lab ID: 92521577002 Collected:
02/09/21 14:15
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Benzene
ND ug/kg 7.8
3.1 1
02/11/21 11:36
02/11/21 15:11
71-43-2
Ethylbenzene
ND ug/kg 7.8
3.6 1
02/11/21 11:36
02/11/21 15:11
100-41-4
Toluene
ND ug/kg 7.8
2.2 1
02/11/21 11:36
02/11/21 15:11
108-88-3
Xylene (Total)
ND ug/kg 15.6
4.4 1
02/11/21 11:36
02/11/21 15:11
1330-20-7
Surrogates
Toluene-d8 (S)
96 % 70-130
1
02/11/21 11:36
02/11/21 15:11
2037-26-5
4-Bromofluorobenzene (S)
132 % 69-134
1
02/11/21 11:36
02/11/21 15:11
460-00-4
1,2-Dichloroethane-d4 (S)
102 % 70-130
1
02/11/21 11:36
02/11/21 15:11
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
21.7 % 0.10
0.10 1
02/11/21 14:13
N2
Sample: #2 NS (4-4.5) Lab ID: 92521577003 Collected: 02/09/21 14:20 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
10500 mg/kg 332
153 50
02/11/21 15:01
02/15/21 10:16
C28)
Surrogates
n-Pentacosane (S)
0 % 32-130
50
02/11/21 15:01
02/15/21 10:16
629-99-2 S4
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
75.0 mg/kg 11.2
2.1 1
02/12/21 11:17
02/13/21 01:45
Surrogates
4-Bromofluorobenzene (S)
141 % 66-131
1
02/12/21 11:17
02/13/21 01:45
460-00-4 S2
8260D/5035AI5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Benzene
ND ug/kg 9.4
3.7 1
02/11/21 11:36
02/11/21 15:29
71-43-2
Ethylbenzene
ND ug/kg 9.4
4.4 1
02/11/21 11:36
02/11/21 15:29
100-41-4
Toluene
ND ug/kg 9.4
2.7 1
02/11/21 11:36
02/11/21 15:29
108-88-3
Xylene (Total)
528 ug/kg 18.8
5.4 1
02/11/21 11:36
02/11/21 15:29
1330-20-7
Surrogates
Toluene-d8 (S)
97 % 70-130
1
02/11/21 11:36
02/11/21 15:29
2037-26-5
4-Bromofluorobenzene (S)
208 % 69-134
1
02/11/21 11:36
02/11/21 15:29
460-00-4 S5
1,2-Dichloroethane-d4 (S)
104 % 70-130
1
02/11/21 11:36
02/11/21 15:29
17060-07-0
Date: 02/24/2021 01:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 NS (4-4.5) Lab ID: 92521577003 Collected: 02/09/21 14:20 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture 24.6 % 0.10 0.10 1 02/11/21 14:13 N2
Sample: #2 SS (4-4.5) Lab ID: 92521577004 Collected: 02/09/21 14:25 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
C28)
Surrogates
n-Pentacosane(S)
Gasoline Range Organics
Gas Range Organics (C6-C10)
Surrogates
4-Bromofluorobenzene (S)
8260D/5035AI5030B Volatiles
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/24/2021 01:57 PM
4720 mg/kg 165
75.9
25
02/11/2115:01
02/15/2110:40
0 % 32-130
25
02/11/2115:01
02/15/2110:40
629-99-2 S4
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
4.9J mg/kg 10.6
2.0
1
02/12/2111:17
02/13/2103:10
98 % 66-131
1
02/12/21 11:17
02/13/2103:10
460-00-4
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND ug/kg 7.7
3.1
1
02/11/2111:36
02/11/2115:47
71-43-2
ND ug/kg 7.7
3.6
1
02/11/2111:36
02/11/2115:47
100-41-4
ND ug/kg 7.7
2.2
1
02/11/2111:36
02/11/2115:47
108-88-3
ND ug/kg 15.3
4.4
1
02/11/2111:36
02/11/2115:47
1330-20-7
102 % 70-130
1
02/11/2111:36
02/11/2115:47
2037-26-5
111 % 69-134
1
02/11/2111:36
02/11/2115:47
460-00-4
104 % 70-130
1
02/11/2111:36
02/11/2115:47
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
23.5 % 0.10
0.10
1
02/11/2114:13
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #1 NS (5.5) Lab ID: 92521577005 Collected: 02/10/21 09:45 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)
Surrogates
n-Pentacosane(S)
Gasoline Range Organics
Gas Range Organics (C6-C10)
Surrogates
4-Bromofluorobenzene (S)
8260D/5035A/5030B Volatiles
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND mg/kg 6.5 3.0 1 02/11/21 15:01 02/12/21 16:34
78 % 32-130 1 02/11/21 15:01 02/12/21 16:34 629-99-2
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
5.8J mg/kg 11.9 2.3 1 02/12/21 11:17 02/13/2104:34
100
%
66-131
1
02/12/21 11:17
02/13/2104:34
460-00-4
Analytical
Method: EPA 8260D Preparation Method:
EPA
5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
7.0
2.8
1
02/11/2111:36
02/11/2116:05
71-43-2
ND
ug/kg
7.0
3.3
1
02/11/2111:36
02/11/2116:05
100-41-4
ND
ug/kg
7.0
2.0
1
02/11/2111:36
02/11/2116:05
108-88-3
ND
ug/kg
14.1
4.0
1
02/11/2111:36
02/11/2116:05
1330-20-7
97
%
70-130
1
02/11/2111:36
02/11/2116:05
2037-26-5
98
%
69-134
1
02/11/2111:36
02/11/2116:05
460-00-4
102
%
70-130
1
02/11/2111:36
02/11/2116:05
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
22.6 % 0.10 0.10 1 02/11/2114:13
N2
Sample: #1 SS (5.5) Lab ID: 92521577006 Collected: 02/10/21 09:50 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-
ND mg/kg 7.0 3.2 1 02/11/21 15:01 02/12/21 16:34
C28)
Surrogates
n-Pentacosane (S)
84 % 32-130 1 02/11/21 15:01 02/12/21 16:34 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
ND mg/kg 14.1 2.7 1 02/12/21 11:17 02/12/21 12:40
Surrogates
4-Bromofluorobenzene (S)
83 % 66-131 1 02/12/21 11:17 02/12/21 12:40 460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM
without the written consent of Pace Analytical Services, LLC.
Page 9 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #1 SS (5.5) Lab ID: 92521577006 Collected: 02/10/21 09:50 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Benzene
Ethylbenzene
Toluene
Xylene (Total)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
9.7
3.9
1
02/11/2111:36
02/11/2116:23
71-43-2
ND
ug/kg
9.7
4.5
1
02/11/2111:36
02/11/2116:23
100-41-4
ND
ug/kg
9.7
2.7
1
02/11/2111:36
02/11/2116:23
108-88-3
ND
ug/kg
19.4
5.5
1
02/11/2111:36
02/11/2116:23
1330-20-7
101
%
70-130
1
02/11/2111:36
02/11/2116:23
2037-26-5
101
%
69-134
1
02/11/2111:36
02/11/2116:23
460-00-4
105
%
70-130
1
02/11/2111:36
02/11/2116:23
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
28.8 % 0.10 0.10 1 02/11/2114:13
N2
Sample: #2 NW (6.5-7) Lab ID: 92521577007 Collected: 02/10/21 17:25 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services
- Charlotte
Aliphatic (C09-C18)
ND
mg/kg
12.5
12.5
1
02/15/21 11:54
02/16/21 21:36
Aliphatic (C19-C36)
ND
mg/kg
12.5
12.5
1
02/15/21 11:54
02/16/21 21:36
Aromatic (C11-C22)
ND
mg/kg
12.5
12.5
1
02/15/21 11:54
02/16/21 21:36
Surrogates
1-Chlorooctadecane (S)
44
%
40-140
1
02/15/21 11:54
02/16/21 21:36
3386-33-2
o-Terphenyl (S)
64
%
40-140
1
02/15/21 11:54
02/16/21 21:36
84-15-1
2-Fluorobiphenyl (S)
97
%
40-140
1
02/15/21 11:54
02/16/21 21:36
321-60-8
2-Bromonaphthalene (S)
101
%
40-140
1
02/15/21 11:54
02/16/21 21:36
580-13-2
MADEPV
Analytical
Method: MADEP VPH Preparation Method:
MADEPV
Pace National - Mt. Juliet
Aliphatic (C05-CO8)
17.9J
mg/kg
43.7
14.5
6
02/10/21 17:25
02/21/21 22:31
Aliphatic (C09-C12)
304
mg/kg
43.7
14.5
6
02/10/21 17:25
02/21/21 22:31
Aromatic (C09-C10),Unadjusted
328
mg/kg
43.7
14.5
6
02/10/21 17:25
02/21/21 22:31
TPHC9C10A
Total VPH
649
mg/kg
43.7
14.5
6
02/10/21 17:25
02/21/21 22:31
VPH
Surrogates
2,5-Dibromotoluene (FID)
106
%
70.0-130
6
02/10/21 17:25
02/21/21 22:31
615-59-8FID
2,5-Dibromotoluene (PID)
117
%
70.0-130
6
02/10/21 17:25
02/21/21 22:31
615-59-8PID
8270E MSSV Microwave
Analytical
Method: EPA 8270E
Preparation Method: EPA 3546
Pace Analytical Services
- Charlotte
Acenaphthene
4970
ug/kg
4120
1060
10
02/15/21 10:39
02/17/2109:44
83-32-9
Acenaphthylene
ND
ug/kg
4120
974
10
02/15/2110:39
02/17/2109:44
208-96-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
N2
N2
N2
J
Page 10 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 NW (6.5-7) Lab ID: 92521577007 Collected: 02/10/21 17:25 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services
- Charlotte
Aniline
ND
ug/kg
4120
924
10
02/15/21 10:39
02/17/21 09:44
62-53-3
Anthracene
ND
ug/kg
4120
1070
10
02/15/21 10:39
02/17/21 09:44
120-12-7
Benzo(a)anthracene
ND
ug/kg
4120
1310
10
02/15/21 10:39
02/17/21 09:44
56-55-3
Benzo(a)pyrene
ND
ug/kg
4120
1780
10
02/15/21 10:39
02/17/21 09:44
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
4120
1660
10
02/15/21 10:39
02/17/21 09:44
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
4120
1610
10
02/15/21 10:39
02/17/21 09:44
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
4120
1730
10
02/15/21 10:39
02/17/21 09:44
207-08-9
Benzoic Acid
ND
ug/kg
20600
4440
10
02/15/21 10:39
02/17/21 09:44
65-85-0
Benzyl alcohol
ND
ug/kg
8230
2180
10
02/15/21 10:39
02/17/21 09:44
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
4120
1080
10
02/15/21 10:39
02/17/21 09:44
101-55-3
Butylbenzylphthalate
ND
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 09:44
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
8230
2510
10
02/15/21 10:39
02/17/21 09:44
59-50-7
4-Chloroaniline
ND
ug/kg
8230
2520
10
02/15/21 10:39
02/17/21 09:44
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 09:44
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
4120
874
10
02/15/21 10:39
02/17/21 09:44
111-44-4
2-Chloronaphthalene
ND
ug/kg
4120
917
10
02/15/21 10:39
02/17/21 09:44
91-58-7
2-Chlorophenol
ND
ug/kg
4120
958
10
02/15/21 10:39
02/17/21 09:44
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
4120
1070
10
02/15/21 10:39
02/17/21 09:44
7005-72-3
Chrysene
ND
ug/kg
4120
1200
10
02/15/21 10:39
02/17/21 09:44
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
4120
1650
10
02/15/21 10:39
02/17/21 09:44
53-70-3
Dibenzofuran
ND
ug/kg
4120
1030
10
02/15/21 10:39
02/17/21 09:44
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
4120
891
10
02/15/21 10:39
02/17/21 09:44
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
4120
927
10
02/15/21 10:39
02/17/21 09:44
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
4120
906
10
02/15/21 10:39
02/17/21 09:44
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
8230
2870
10
02/15/21 10:39
02/17/21 09:44
91-94-1
2,4-Dichlorophenol
ND
ug/kg
4120
1360
10
02/15/21 10:39
02/17/21 09:44
120-83-2
Diethylphthalate
ND
ug/kg
4120
893
10
02/15/21 10:39
02/17/21 09:44
84-66-2
2,4-Dimethylphenol
ND
ug/kg
4120
1030
10
02/15/21 10:39
02/17/21 09:44
105-67-9
Dimethylphthalate
ND
ug/kg
4120
931
10
02/15/21 10:39
02/17/21 09:44
131-11-3
Di-n-butylphthalate
ND
ug/kg
4120
1020
10
02/15/21 10:39
02/17/21 09:44
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
8230
6640
10
02/15/21 10:39
02/17/21 09:44
534-52-1
2,4-Dinitrophenol
ND
ug/kg
20600
13100
10
02/15/21 10:39
02/17/21 09:44
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
4120
1090
10
02/15/21 10:39
02/17/21 09:44
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
4120
1080
10
02/15/21 10:39
02/17/21 09:44
606-20-2
Di-n-octylphthalate
ND
ug/kg
4120
2350
10
02/15/21 10:39
02/17/21 09:44
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
4120
1350
10
02/15/21 10:39
02/17/21 09:44
117-81-7
Fluoranthene
ND
ug/kg
4120
1240
10
02/15/21 10:39
02/17/21 09:44
206-44-0
Fluorene
2280J
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 09:44
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
4120
1000
10
02/15/21 10:39
02/17/21 09:44
87-68-3
Hexachlorobenzene
ND
ug/kg
4120
1050
10
02/15/21 10:39
02/17/21 09:44
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
4120
1650
10
02/15/21 10:39
02/17/21 09:44
77-47-4
Hexachloroethane
ND
ug/kg
4120
938
10
02/15/21 10:39
02/17/21 09:44
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
4120
1880
10
02/15/21 10:39
02/17/21 09:44
193-39-5
Isophorone
ND
ug/kg
4120
894
10
02/15/21 10:39
02/17/21 09:44
78-59-1
REPORT OF LABORATORY ANALYSIS
v1
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 NW (6.5-7)
Lab ID:
92521577007
Collected:
02/10/21
17:25
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are
adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services
- Charlotte
1-Methylnaphthalene
27500
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 09:44
90-12-0
2-Methylnaphthalene
39100
ug/kg
4120
1050
10
02/15/21 10:39
02/17/21 09:44
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
4120
912
10
02/15/21 10:39
02/17/21 09:44
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
4120
1040
10
02/15/21 10:39
02/17/21 09:44
15831-10-4
Naphthalene
4520
ug/kg
4120
985
10
02/15/21 10:39
02/17/21 09:44
91-20-3
2-Nitroaniline
ND
ug/kg
20600
2070
10
02/15/21 10:39
02/17/21 09:44
88-74-4
3-Nitroaniline
ND
ug/kg
20600
2180
10
02/15/21 10:39
02/17/21 09:44
99-09-2
IL
4-Nitroaniline
ND
ug/kg
8230
2030
10
02/15/21 10:39
02/17/21 09:44
100-01-6
Nitrobenzene
ND
ug/kg
4120
983
10
02/15/21 10:39
02/17/21 09:44
98-95-3
2-Nitrophenol
ND
ug/kg
4120
1270
10
02/15/21 10:39
02/17/21 09:44
88-75-5
4-Nitrophenol
ND
ug/kg
20600
6560
10
02/15/21 10:39
02/17/21 09:44
100-02-7
v1
N-Nitrosodimethylamine
ND
ug/kg
4120
1160
10
02/15/21 10:39
02/17/21 09:44
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
4120
1150
10
02/15/21 10:39
02/17/21 09:44
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
4120
1050
10
02/15/21 10:39
02/17/21 09:44
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
4120
1140
10
02/15/21 10:39
02/17/21 09:44
108-60-1
Pentachlorophenol
ND
ug/kg
8230
1880
10
02/15/21 10:39
02/17/21 09:44
87-86-5
Phenanthrene
9250
ug/kg
4120
1040
10
02/15/21 10:39
02/17/21 09:44
85-01-8
Phenol
ND
ug/kg
4120
983
10
02/15/21 10:39
02/17/21 09:44
108-95-2
Pyrene
ND
ug/kg
4120
1130
10
02/15/21 10:39
02/17/21 09:44
129-00-0
Pyridine
ND
ug/kg
4120
1040
10
02/15/21 10:39
02/17/21 09:44
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
4120
943
10
02/15/21 10:39
02/17/21 09:44
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
4120
1070
10
02/15/21 10:39
02/17/21 09:44
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
4120
1030
10
02/15/21 10:39
02/17/21 09:44
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
21-130
10
02/15/21 10:39
02/17/21 09:44
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
19-130
10
02/15/21 10:39
02/17/21 09:44
321-60-8
S4
Terphenyl-d14 (S)
0
%
15-130
10
02/15/21 10:39
02/17/21 09:44
1718-51-0
S4
Phenol-d6 (S)
0
%
18-130
10
02/15/21 10:39
02/17/21 09:44
13127-88-3
S4
2-Fluorophenol (S)
0
%
18-130
10
02/15/21 10:39
02/17/21 09:44
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
18-130
10
02/15/21 10:39
02/17/21 09:44
118-79-6
S4
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D
Preparation Method: EPA 5035A/5030B
Pace Analytical Services
- Charlotte
Acetone
ND
ug/kg
671
215
4
02/11/2111:36
02/11/2117:18
67-64-1
Benzene
ND
ug/kg
33.5
13.4
4
02/11/2111:36
02/11/2117:18
71-43-2
Bromobenzene
ND
ug/kg
33.5
10.9
4
02/11/2111:36
02/11/2117:18
108-86-1
Bromochloromethane
ND
ug/kg
33.5
9.9
4
02/11/2111:36
02/11/2117:18
74-97-5
Bromodichloromethane
ND
ug/kg
33.5
12.9
4
02/11/2111:36
02/11/2117:18
75-27-4
Bromoform
ND
ug/kg
33.5
11.8
4
02/11/2111:36
02/11/2117:18
75-25-2
Bromomethane
ND
ug/kg
67.1
53.0
4
02/11/2111:36
02/11/2117:18
74-83-9
2-Butanone (MEK)
ND
ug/kg
671
161
4
02/11/21 11:36
02/11/21 17:18
78-93-3
n-Butylbenzene
1680
ug/kg
33.5
15.8
4
02/11/2111:36
02/11/2117:18
104-51-8
sec-Butylbenzene
ND
ug/kg
33.5
14.8
4
02/11/2111:36
02/11/2117:18
135-98-8
tert-Butyl benzene
224
ug/kg
33.5
11.9
4
02/11/2111:36
02/11/2117:18
98-06-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 NW (6.5-7) Lab ID: 92521577007 Collected: 02/10/21 17:25 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Carbon tetrachloride
ND
ug/kg
33.5
12.5
4
02/11/21 11:36
02/11/21 17:18
56-23-5
Chlorobenzene
ND
ug/kg
33.5
6.4
4
02/11/21 11:36
02/11/21 17:18
108-90-7
Chloroethane
ND
ug/kg
67.1
25.9
4
02/11/21 11:36
02/11/21 17:18
75-00-3
Chloroform
ND
ug/kg
33.5
20.4
4
02/11/21 11:36
02/11/21 17:18
67-66-3
Chloromethane
ND
ug/kg
67.1
28.2
4
02/11/21 11:36
02/11/21 17:18
74-87-3
2-Chlorotoluene
ND
ug/kg
33.5
11.9
4
02/11/21 11:36
02/11/21 17:18
95-49-8
4-Chlorotoluene
ND
ug/kg
33.5
5.9
4
02/11/21 11:36
02/11/21 17:18
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
33.5
13.0
4
02/11/21 11:36
02/11/21 17:18
96-12-8
Dibromochloromethane
ND
ug/kg
33.5
18.9
4
02/11/21 11:36
02/11/21 17:18
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
33.5
14.8
4
02/11/21 11:36
02/11/21 17:18
106-93-4
Dibromomethane
ND
ug/kg
33.5
7.2
4
02/11/21 11:36
02/11/21 17:18
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
33.5
12.1
4
02/11/21 11:36
02/11/21 17:18
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
33.5
10.4
4
02/11/21 11:36
02/11/21 17:18
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
33.5
8.7
4
02/11/21 11:36
02/11/21 17:18
106-46-7
Dichlorodifluoromethane
ND
ug/kg
67.1
14.6
4
02/11/21 11:36
02/11/21 17:18
75-71-8
1,1-Dichloroethane
ND
ug/kg
33.5
13.8
4
02/11/21 11:36
02/11/21 17:18
75-34-3
1,2-Dichloroethane
ND
ug/kg
33.5
22.2
4
02/11/21 11:36
02/11/21 17:18
107-06-2
1,1-Dichloroethene
ND
ug/kg
33.5
13.8
4
02/11/21 11:36
02/11/21 17:18
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
33.5
11.5
4
02/11/21 11:36
02/11/21 17:18
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
33.5
11.7
4
02/11/21 11:36
02/11/21 17:18
156-60-5
1,2-Dichloropropane
ND
ug/kg
33.5
10.1
4
02/11/21 11:36
02/11/21 17:18
78-87-5
1,3-Dichloropropane
ND
ug/kg
33.5
10.5
4
02/11/21 11:36
02/11/21 17:18
142-28-9
2,2-Dichloropropane
ND
ug/kg
33.5
10.9
4
02/11/21 11:36
02/11/21 17:18
594-20-7
1,1-Dichloropropene
ND
ug/kg
33.5
16.1
4
02/11/21 11:36
02/11/21 17:18
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
33.5
9.1
4
02/11/21 11:36
02/11/21 17:18
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
33.5
11.5
4
02/11/21 11:36
02/11/21 17:18
10061-02-6
Diisopropyl ether
ND
ug/kg
33.5
9.1
4
02/11/21 11:36
02/11/21 17:18
108-20-3
Ethylbenzene
287
ug/kg
33.5
15.6
4
02/11/21 11:36
02/11/21 17:18
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
67.1
54.9
4
02/11/21 11:36
02/11/21 17:18
87-68-3
2-Hexanone
ND
ug/kg
335
32.3
4
02/11/21 11:36
02/11/21 17:18
591-78-6
Isopropylbenzene (Cumene)
326
ug/kg
33.5
11.4
4
02/11/21 11:36
02/11/21 17:18
98-82-8
p-Isopropyltoluene
6550
ug/kg
33.5
16.5
4
02/11/21 11:36
02/11/21 17:18
99-87-6
Methylene Chloride
ND
ug/kg
134
91.9
4
02/11/21 11:36
02/11/21 17:18
75-09-2
4-Methyl-2-pentanone (MIBK)
371
ug/kg
335
32.3
4
02/11/21 11:36
02/11/21 17:18
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
33.5
12.5
4
02/11/21 11:36
02/11/21 17:18
1634-04-4
Naphthalene
7760
ug/kg
33.5
17.6
4
02/11/21 11:36
02/11/21 17:18
91-20-3
n-Propylbenzene
595
ug/kg
33.5
11.9
4
02/11/21 11:36
02/11/21 17:18
103-65-1
Styrene
ND
ug/kg
33.5
8.9
4
02/11/21 11:36
02/11/21 17:18
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
33.5
12.9
4
02/11/21 11:36
02/11/21 17:18
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
33.5
8.9
4
02/11/21 11:36
02/11/21 17:18
79-34-5
Tetrachloroethene
ND
ug/kg
33.5
10.6
4
02/11/21 11:36
02/11/21 17:18
127-18-4
Toluene
ND
ug/kg
33.5
9.5
4
02/11/21 11:36
02/11/21 17:18
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
33.5
27.1
4
02/11/21 11:36
02/11/21 17:18
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
33.5
28.2
4
02/11/21 11:36
02/11/21 17:18
120-82-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 NW (6.5-7) Lab ID: 92521577007 Collected: 02/10/21 17:25 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
33.5
17.4
4
02/11/2111:36
02/11/2117:18
71-55-6
ND
ug/kg
33.5
11.1
4
02/11/2111:36
02/11/2117:18
79-00-5
ND
ug/kg
33.5
8.7
4
02/11/2111:36
02/11/2117:18
79-01-6
ND
ug/kg
33.5
18.5
4
02/11/2111:36
02/11/2117:18
75-69-4
ND
ug/kg
33.5
17.0
4
02/11/2111:36
02/11/2117:18
96-18-4
ND
ug/kg
33.5
9.2
4
02/11/2111:36
02/11/2117:18
95-63-6
4980
ug/kg
33.5
11.3
4
02/11/2111:36
02/11/2117:18
108-67-8
ND
ug/kg
335
24.4
4
02/11/2111:36
02/11/2117:18
108-05-4
ND
ug/kg
67.1
17.0
4
02/11/2111:36
02/11/2117:18
75-01-4
1790
ug/kg
67.1
19.1
4
02/11/2111:36
02/11/2117:18
1330-20-7
ND
ug/kg
67.1
22.9
4
02/11/2111:36
02/11/2117:18
179601-23-1
1790
ug/kg
33.5
14.8
4
02/11/2111:36
02/11/2117:18
95-47-6
101
%
70-130
4
02/11/2111:36
02/11/2117:18
2037-26-5 D3
115
%
69-134
4
02/11/2111:36
02/11/2117:18
460-00-4
103
%
70-130
4
02/11/2111:36
02/11/2117:18
17060-07-0
Analytical
Method: SW-846
Pace Analytical Services - Charlotte
19.6
%
0.10
0.10
1
02/11/2114:13
N2
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 80.1 % 1 02/22/21 11:28 02/22/21 11:36
Sample: #2 SW (6.5-7) Lab ID: 92521577008 Collected: 02/10/21 17:37 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
1-Chlorooctadecane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
Date: 02/24/2021 01:57 PM
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical
Services - Charlotte
4890
mg/kg
2560
2560 200
02/15/21 11:54
02/18/2109:08
N2
ND
mg/kg
2560
2560 200
02/15/21 11:54
02/18/2109:08
N2
2790
mg/kg
512
512 40
02/15/21 11:54
02/18/2109:08
N2
0
%
40-140
200
02/15/21 11:54
02/18/2109:08
3386-33-2
S4
0
%
40-140
40
02/15/21 11:54
02/18/2109:08
84-15-1
S4
0
%
40-140
40
02/15/21 11:54
02/18/2109:08
321-60-8
S4
0
%
40-140
40
02/15/21 11:54
02/18/2109:08
580-13-2
S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 65

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 SW (6.5-7)
Lab ID:
92521577008
Collected:
02/10/21 17:37
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are
adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
MADEPV
Analytical Method: MADEP VPH Preparation Method:
MADEPV
Pace National - Mt. Juliet
Aliphatic (C05-CO8)
10.6
mg/kg
8.26
2.75
1.05
02/10/21 17:37
02/14/21 22:05
B
Aliphatic (C09-C12)
29.3
mg/kg
8.26
2.75
1.05
02/10/21 17:37
02/14/21 22:05
Aromatic (C09-C10),Unadjusted
14.6
mg/kg
8.26
2.75
1.05
02/10/21 17:37
02/14/21 22:05
TPHC9C10A
Total VPH
54.4
mg/kg
8.26
2.75
1.05
02/10/21 17:37
02/14/21 22:05
VPH
Surrogates
2,5-Dibromotoluene (FID)
110
%
70.0-130
1.05
02/10/21 17:37
02/14/21 22:05
615-59-8FID
2,5-Dibromotoluene (PID)
84.6
%
70.0-130
1.05
02/10/21 17:37
02/14/21 22:05
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Pace Analytical Services
- Charlotte
Acenaphthene
ND
ug/kg
420
108
1
02/15/21 10:39
02/17/21 14:39
83-32-9
Acenaphthylene
ND
ug/kg
420
99.4
1
02/15/21 10:39
02/17/21 14:39
208-96-8
Aniline
ND
ug/kg
420
94.3
1
02/15/21 10:39
02/17/21 14:39
62-53-3
Anthracene
ND
ug/kg
420
109
1
02/15/21 10:39
02/17/21 14:39
120-12-7
Benzo(a)anthracene
ND
ug/kg
420
134
1
02/15/21 10:39
02/17/21 14:39
56-55-3
Benzo(a)pyrene
ND
ug/kg
420
182
1
02/15/21 10:39
02/17/21 14:39
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
420
169
1
02/15/21 10:39
02/17/21 14:39
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
420
164
1
02/15/21 10:39
02/17/21 14:39
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
420
177
1
02/15/21 10:39
02/17/21 14:39
207-08-9
Benzoic Acid
ND
ug/kg
2100
453
1
02/15/21 10:39
02/17/21 14:39
65-85-0
Benzyl alcohol
ND
ug/kg
840
223
1
02/15/21 10:39
02/17/21 14:39
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
420
110
1
02/15/21 10:39
02/17/21 14:39
101-55-3
Butylbenzylphthalate
ND
ug/kg
420
112
1
02/15/21 10:39
02/17/21 14:39
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
840
256
1
02/15/21 10:39
02/17/21 14:39
59-50-7
4-Chloroaniline
ND
ug/kg
840
257
1
02/15/21 10:39
02/17/21 14:39
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
420
112
1
02/15/21 10:39
02/17/21 14:39
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
420
89.2
1
02/15/21 10:39
02/17/21 14:39
111-44-4
2-Chloronaphthalene
ND
ug/kg
420
93.5
1
02/15/21 10:39
02/17/21 14:39
91-58-7
2-Chlorophenol
ND
ug/kg
420
97.7
1
02/15/21 10:39
02/17/21 14:39
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
420
109
1
02/15/21 10:39
02/17/21 14:39
7005-72-3
Chrysene
ND
ug/kg
420
122
1
02/15/21 10:39
02/17/21 14:39
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
420
168
1
02/15/21 10:39
02/17/21 14:39
53-70-3
Dibenzofuran
ND
ug/kg
420
105
1
02/15/21 10:39
02/17/21 14:39
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
420
90.8
1
02/15/21 10:39
02/17/21 14:39
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
420
94.5
1
02/15/21 10:39
02/17/21 14:39
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
420
92.4
1
02/15/21 10:39
02/17/21 14:39
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
840
293
1
02/15/21 10:39
02/17/21 14:39
91-94-1
2,4-Dichlorophenol
ND
ug/kg
420
139
1
02/15/21 10:39
02/17/21 14:39
120-83-2
Diethylphthalate
ND
ug/kg
420
91.1
1
02/15/21 10:39
02/17/21 14:39
84-66-2 v1
2,4-Dimethylphenol
ND
ug/kg
420
105
1
02/15/21 10:39
02/17/21 14:39
105-67-9
Dimethylphthalate
ND
ug/kg
420
94.9
1
02/15/21 10:39
02/17/21 14:39
131-11-3
Di-n-butylphthalate
ND
ug/kg
420
104
1
02/15/21 10:39
02/17/21 14:39
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
840
677
1
02/15/21 10:39
02/17/21 14:39
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2100
1340
1
02/15/21 10:39
02/17/21 14:39
51-28-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 65

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 SW (6.5-7) Lab ID: 92521577008 Collected: 02/10/21 17:37 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
2,4-Dinitrotoluene
ND
ug/kg
420
ill
1
02/15/21 10:39
02/17/21 14:39
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
420
110
1
02/15/21 10:39
02/17/21 14:39
606-20-2
Di-n-octylphthalate
ND
ug/kg
420
239
1
02/15/21 10:39
02/17/21 14:39
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
420
137
1
02/15/21 10:39
02/17/21 14:39
117-81-7
Fluoranthene
ND
ug/kg
420
127
1
02/15/21 10:39
02/17/21 14:39
206-44-0
Fluorene
ND
ug/kg
420
112
1
02/15/21 10:39
02/17/21 14:39
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
420
102
1
02/15/21 10:39
02/17/21 14:39
87-68-3
Hexachlorobenzene
ND
ug/kg
420
107
1
02/15/21 10:39
02/17/21 14:39
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
420
168
1
02/15/21 10:39
02/17/21 14:39
77-47-4
Hexachloroethane
ND
ug/kg
420
95.7
1
02/15/21 10:39
02/17/21 14:39
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
420
192
1
02/15/21 10:39
02/17/21 14:39
193-39-5
Isophorone
ND
ug/kg
420
91.2
1
02/15/21 10:39
02/17/21 14:39
78-59-1
1-Methylnaphthalene
ND
ug/kg
420
112
1
02/15/21 10:39
02/17/21 14:39
90-12-0
2-Methylnaphthalene
ND
ug/kg
420
107
1
02/15/21 10:39
02/17/21 14:39
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
420
93.0
1
02/15/21 10:39
02/17/21 14:39
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
420
106
1
02/15/21 10:39
02/17/21 14:39
15831-10-4
Naphthalene
ND
ug/kg
420
101
1
02/15/21 10:39
02/17/21 14:39
91-20-3
2-Nitroaniline
ND
ug/kg
2100
211
1
02/15/21 10:39
02/17/21 14:39
88-74-4
3-Nitroaniline
ND
ug/kg
2100
223
1
02/15/21 10:39
02/17/21 14:39
99-09-2
4-Nitroaniline
ND
ug/kg
840
207
1
02/15/21 10:39
02/17/21 14:39
100-01-6
Nitrobenzene
ND
ug/kg
420
100
1
02/15/21 10:39
02/17/21 14:39
98-95-3
2-Nitrophenol
ND
ug/kg
420
130
1
02/15/21 10:39
02/17/21 14:39
88-75-5
4-Nitrophenol
ND
ug/kg
2100
669
1
02/15/21 10:39
02/17/21 14:39
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
420
118
1
02/15/21 10:39
02/17/21 14:39
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
420
118
1
02/15/21 10:39
02/17/21 14:39
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
420
107
1
02/15/21 10:39
02/17/21 14:39
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
420
117
1
02/15/21 10:39
02/17/21 14:39
108-60-1
Pentachlorophenol
ND
ug/kg
840
192
1
02/15/21 10:39
02/17/21 14:39
87-86-5
Phenanthrene
ND
ug/kg
420
106
1
02/15/21 10:39
02/17/21 14:39
85-01-8
Phenol
ND
ug/kg
420
100
1
02/15/21 10:39
02/17/21 14:39
108-95-2
Pyrene
ND
ug/kg
420
116
1
02/15/21 10:39
02/17/21 14:39
129-00-0
Pyridine
ND
ug/kg
420
106
1
02/15/21 10:39
02/17/21 14:39
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
420
96.2
1
02/15/21 10:39
02/17/21 14:39
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
420
109
1
02/15/21 10:39
02/17/21 14:39
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
420
105
1
02/15/21 10:39
02/17/21 14:39
88-06-2
Surrogates
Nitrobenzene-d5 (S)
66
%
21-130
1
02/15/21 10:39
02/17/21 14:39
4165-60-0
2-Fluorobiphenyl (S)
62
%
19-130
1
02/15/21 10:39
02/17/21 14:39
321-60-8
Terphenyl-dl4 (S)
84
%
15-130
1
02/15/21 10:39
02/17/21 14:39
1718-51-0
Phenol-d6 (S)
54
%
18-130
1
02/15/21 10:39
02/17/21 14:39
13127-88-3
2-Fluorophenol (S)
55
%
18-130
1
02/15/21 10:39
02/17/21 14:39
367-12-4
2,4,6-Tribromophenol (S)
75
%
18-130
1
02/15/21 10:39
02/17/21 14:39
118-79-6
REPORT OF LABORATORY ANALYSIS
IL
vl
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 65

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 SW (6.5-7) Lab ID: 92521577008 Collected: 02/10/21 17:37 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Acetone
ND
ug/kg
162
52.0
1
02/11/21 11:36
02/11/21 16:41
67-64-1
Benzene
ND
ug/kg
8.1
3.2
1
02/11/21 11:36
02/11/21 16:41
71-43-2
Bromobenzene
ND
ug/kg
8.1
2.6
1
02/11/21 11:36
02/11/21 16:41
108-86-1
Bromochloromethane
ND
ug/kg
8.1
2.4
1
02/11/21 11:36
02/11/21 16:41
74-97-5
Bromodichloromethane
ND
ug/kg
8.1
3.1
1
02/11/21 11:36
02/11/21 16:41
75-27-4
Bromoform
ND
ug/kg
8.1
2.8
1
02/11/21 11:36
02/11/21 16:41
75-25-2
Bromomethane
ND
ug/kg
16.2
12.8
1
02/11/21 11:36
02/11/21 16:41
74-83-9
2-Butanone (MEK)
ND
ug/kg
162
38.9
1
02/11/21 11:36
02/11/21 16:41
78-93-3
n-Butylbenzene
ND
ug/kg
8.1
3.8
1
02/11/21 11:36
02/11/21 16:41
104-51-8
sec-Butylbenzene
ND
ug/kg
8.1
3.6
1
02/11/21 11:36
02/11/21 16:41
135-98-8
tert-Butyl benzene
ND
ug/kg
8.1
2.9
1
02/11/21 11:36
02/11/21 16:41
98-06-6
Carbon tetrachloride
ND
ug/kg
8.1
3.0
1
02/11/21 11:36
02/11/21 16:41
56-23-5
Chlorobenzene
ND
ug/kg
8.1
1.6
1
02/11/21 11:36
02/11/21 16:41
108-90-7
Chloroethane
ND
ug/kg
16.2
6.2
1
02/11/21 11:36
02/11/21 16:41
75-00-3
Chloroform
ND
ug/kg
8.1
4.9
1
02/11/21 11:36
02/11/21 16:41
67-66-3
Chloromethane
ND
ug/kg
16.2
6.8
1
02/11/21 11:36
02/11/21 16:41
74-87-3
2-Chlorotoluene
ND
ug/kg
8.1
2.9
1
02/11/21 11:36
02/11/21 16:41
95-49-8
4-Chlorotoluene
ND
ug/kg
8.1
1.4
1
02/11/21 11:36
02/11/21 16:41
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
8.1
3.1
1
02/11/21 11:36
02/11/21 16:41
96-12-8
Dibromochloromethane
ND
ug/kg
8.1
4.5
1
02/11/21 11:36
02/11/21 16:41
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
8.1
3.6
1
02/11/21 11:36
02/11/21 16:41
106-93-4
Dibromomethane
ND
ug/kg
8.1
1.7
1
02/11/21 11:36
02/11/21 16:41
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
8.1
2.9
1
02/11/21 11:36
02/11/21 16:41
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
8.1
2.5
1
02/11/21 11:36
02/11/21 16:41
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
8.1
2.1
1
02/11/21 11:36
02/11/21 16:41
106-46-7
Dichlorodifluoromethane
ND
ug/kg
16.2
3.5
1
02/11/21 11:36
02/11/21 16:41
75-71-8
1,1-Dichloroethane
ND
ug/kg
8.1
3.3
1
02/11/21 11:36
02/11/21 16:41
75-34-3
1,2-Dichloroethane
ND
ug/kg
8.1
5.4
1
02/11/21 11:36
02/11/21 16:41
107-06-2
1,1-Dichloroethene
ND
ug/kg
8.1
3.3
1
02/11/21 11:36
02/11/21 16:41
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
8.1
2.8
1
02/11/21 11:36
02/11/21 16:41
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
8.1
2.8
1
02/11/21 11:36
02/11/21 16:41
156-60-5
1,2-Dichloropropane
ND
ug/kg
8.1
2.4
1
02/11/21 11:36
02/11/21 16:41
78-87-5
1,3-Dichloropropane
ND
ug/kg
8.1
2.5
1
02/11/21 11:36
02/11/21 16:41
142-28-9
2,2-Dichloropropane
ND
ug/kg
8.1
2.6
1
02/11/21 11:36
02/11/21 16:41
594-20-7
1,1-Dichloropropene
ND
ug/kg
8.1
3.9
1
02/11/21 11:36
02/11/21 16:41
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
8.1
2.2
1
02/11/21 11:36
02/11/21 16:41
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
8.1
2.8
1
02/11/21 11:36
02/11/21 16:41
10061-02-6
Diisopropyl ether
ND
ug/kg
8.1
2.2
1
02/11/21 11:36
02/11/21 16:41
108-20-3
Ethylbenzene
ND
ug/kg
8.1
3.8
1
02/11/21 11:36
02/11/21 16:41
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
16.2
13.2
1
02/11/21 11:36
02/11/21 16:41
87-68-3
2-Hexanone
ND
ug/kg
81.0
7.8
1
02/11/21 11:36
02/11/21 16:41
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
8.1
2.8
1
02/11/21 11:36
02/11/21 16:41
98-82-8
p-Isopropyltoluene
ND
ug/kg
8.1
4.0
1
02/11/21 11:36
02/11/21 16:41
99-87-6
Methylene Chloride
ND
ug/kg
32.4
22.2
1
02/11/21 11:36
02/11/21 16:41
75-09-2
REPORT OF LABORATORY ANALYSIS
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Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 65

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 SW (6.5-7) Lab ID: 92521577008 Collected: 02/10/21 17:37 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND
ug/kg
81.0
7.8
1
02/11/2111:36
02/11/2116:41
108-10-1
ND
ug/kg
8.1
3.0
1
02/11/2111:36
02/11/2116:41
1634-04-4
ND
ug/kg
8.1
4.3
1
02/11/2111:36
02/11/2116:41
91-20-3
ND
ug/kg
8.1
2.9
1
02/11/2111:36
02/11/2116:41
103-65-1
ND
ug/kg
8.1
2.1
1
02/11/2111:36
02/11/2116:41
100-42-5
ND
ug/kg
8.1
3.1
1
02/11/2111:36
02/11/2116:41
630-20-6
ND
ug/kg
8.1
2.1
1
02/11/2111:36
02/11/2116:41
79-34-5
ND
ug/kg
8.1
2.6
1
02/11/2111:36
02/11/2116:41
127-18-4
ND
ug/kg
8.1
2.3
1
02/11/2111:36
02/11/2116:41
108-88-3
ND
ug/kg
8.1
6.5
1
02/11/2111:36
02/11/2116:41
87-61-6
ND
ug/kg
8.1
6.8
1
02/11/2111:36
02/11/2116:41
120-82-1
ND
ug/kg
8.1
4.2
1
02/11/2111:36
02/11/2116:41
71-55-6
ND
ug/kg
8.1
2.7
1
02/11/2111:36
02/11/2116:41
79-00-5
ND
ug/kg
8.1
2.1
1
02/11/2111:36
02/11/2116:41
79-01-6
ND
ug/kg
8.1
4.5
1
02/11/2111:36
02/11/2116:41
75-69-4
ND
ug/kg
8.1
4.1
1
02/11/2111:36
02/11/2116:41
96-18-4
ND
ug/kg
8.1
2.2
1
02/11/2111:36
02/11/2116:41
95-63-6
ND
ug/kg
8.1
2.7
1
02/11/2111:36
02/11/2116:41
108-67-8
ND
ug/kg
81.0
5.9
1
02/11/2111:36
02/11/2116:41
108-05-4
ND
ug/kg
16.2
4.1
1
02/11/2111:36
02/11/2116:41
75-01-4
ND
ug/kg
16.2
4.6
1
02/11/2111:36
02/11/2116:41
1330-20-7
ND
ug/kg
16.2
5.5
1
02/11/2111:36
02/11/2116:41
179601-23-1
ND
ug/kg
8.1
3.6
1
02/11/2111:36
02/11/2116:41
95-47-6
102
%
70-130
1
02/11/2111:36
02/11/2116:41
2037-26-5
97
%
69-134
1
02/11/2111:36
02/11/2116:41
460-00-4
102
%
70-130
1
02/11/2111:36
02/11/2116:41
17060-07-0
Analytical Method: SW-846
Pace Analytical Services - Charlotte
22.7 % 0.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
77.3 %
02/11/21 14:13
1 02/22/2111:28 02/22/2111:36
REPORT OF LABORATORY ANALYSIS
N2
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 EW (6.5-7)
Lab ID:
92521577009
Collected:
02/10/21
17:05
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are
adjusted for percent moisture, sample size and any dilutions.
Comments: • Volatile Petroleum Hydrocarbons by
Method MADEPV
- Surrogate
failure due to matrix interference.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services
- Charlotte
Aliphatic (C09-C18)
ND
mg/kg
12.8
12.8
1
02/15/21 11:54
02/16/21 22:30
N2
Aliphatic (C19-C36)
ND
mg/kg
12.8
12.8
1
02/15/21 11:54
02/16/21 22:30
N2
Aromatic (C11-C22)
ND
mg/kg
12.8
12.8
1
02/15/21 11:54
02/16/21 22:30
N2
Surrogates
1-Chlorooctadecane (S)
50
%
40-140
1
02/15/21 11:54
02/16/21 22:30
3386-33-2
o-Terphenyl (S)
60
%
40-140
1
02/15/21 11:54
02/16/21 22:30
84-15-1
2-Fluorobiphenyl (S)
93
%
40-140
1
02/15/21 11:54
02/16/21 22:30
321-60-8
2-Bromonaphthalene (S)
96
%
40-140
1
02/15/21 11:54
02/16/21 22:30
580-13-2
MADEPV
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
Aliphatic (C05-CO8)
7.76
mg/kg
7.59
2.54
1
02/10/21 17:15
02/14/21 22:38
B
Aliphatic (C09-C12)
18.8
mg/kg
7.59
2.54
1
02/10/21 17:15
02/14/21 22:38
Aromatic (C09-C10),Unadjusted
26.3
mg/kg
7.59
2.54
1
02/10/21 17:15
02/14/21 22:38
TPHC9C10A
Total VPH
52.9
mg/kg
7.59
2.54
1
02/10/21 17:15
02/14/21 22:38
VPH
Surrogates
2,5-Dibromotoluene (FID)
139
%
70.0-130
1
02/10/21 17:15
02/14/21 22:38
615-59-8FID
ST
2,5-Dibromotoluene (PID)
116
%
70.0-130
1
02/10/21 17:15
02/14/21 22:38
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method: EPA 3546
Pace Analytical Services
- Charlotte
Acenaphthene
ND
ug/kg
423
109
1
02/15/21 10:39
02/16/21 11:36
83-32-9
Acenaphthylene
ND
ug/kg
423
100
1
02/15/21 10:39
02/16/21 11:36
208-96-8
Aniline
ND
ug/kg
423
95.0
1
02/15/21 10:39
02/16/21 11:36
62-53-3
Anthracene
ND
ug/kg
423
110
1
02/15/21 10:39
02/16/21 11:36
120-12-7
Benzo(a)anthracene
ND
ug/kg
423
135
1
02/15/21 10:39
02/16/21 11:36
56-55-3
Benzo(a)pyrene
ND
ug/kg
423
183
1
02/15/21 10:39
02/16/21 11:36
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
423
170
1
02/15/21 10:39
02/16/21 11:36
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
423
165
1
02/15/21 10:39
02/16/21 11:36
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
423
178
1
02/15/21 10:39
02/16/21 11:36
207-08-9
Benzoic Acid
ND
ug/kg
2110
456
1
02/15/21 10:39
02/16/21 11:36
65-85-0
Benzyl alcohol
ND
ug/kg
846
224
1
02/15/21 10:39
02/16/21 11:36
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
423
ill
1
02/15/21 10:39
02/16/21 11:36
101-55-3
Butylbenzylphthalate
ND
ug/kg
423
113
1
02/15/21 10:39
02/16/21 11:36
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
846
258
1
02/15/21 10:39
02/16/21 11:36
59-50-7
4-Chloroaniline
ND
ug/kg
846
259
1
02/15/21 10:39
02/16/21 11:36
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
423
113
1
02/15/21 10:39
02/16/21 11:36
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
423
89.8
1
02/15/21 10:39
02/16/21 11:36
111-44-4
2-Chloronaphthalene
ND
ug/kg
423
94.2
1
02/15/21 10:39
02/16/21 11:36
91-58-7
2-Chlorophenol
ND
ug/kg
423
98.4
1
02/15/21 10:39
02/16/21 11:36
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
423
110
1
02/15/21 10:39
02/16/21 11:36
7005-72-3
Chrysene
ND
ug/kg
423
123
1
02/15/21 10:39
02/16/21 11:36
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
423
169
1
02/15/21 10:39
02/16/21 11:36
53-70-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 EW (6.5-7) Lab ID: 92521577009 Collected: 02/10/21 17:05 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Comments: • Volatile Petroleum Hydrocarbons by Method MADEPV - Surrogate failure due to matrix interference.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Dibenzofuran
ND
ug/kg
423
106
1
02/15/2110:39
02/16/2111:36
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
423
91.5
1
02/15/2110:39
02/16/2111:36
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
423
95.2
1
02/15/2110:39
02/16/2111:36
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
423
93.0
1
02/15/2110:39
02/16/2111:36
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
846
295
1
02/15/2110:39
02/16/2111:36
91-94-1
2,4-Dichlorophenol
ND
ug/kg
423
140
1
02/15/2110:39
02/16/2111:36
120-83-2
Diethylphthalate
ND
ug/kg
423
91.8
1
02/15/2110:39
02/16/2111:36
84-66-2
2,4-Dimethylphenol
ND
ug/kg
423
105
1
02/15/2110:39
02/16/2111:36
105-67-9
Dimethylphthalate
ND
ug/kg
423
95.6
1
02/15/2110:39
02/16/2111:36
131-11-3
Di-n-butylphthalate
ND
ug/kg
423
104
1
02/15/2110:39
02/16/2111:36
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
846
682
1
02/15/2110:39
02/16/2111:36
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2110
1350
1
02/15/2110:39
02/16/2111:36
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
423
112
1
02/15/2110:39
02/16/2111:36
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
423
ill
1
02/15/2110:39
02/16/2111:36
606-20-2
Di-n-octylphthalate
ND
ug/kg
423
241
1
02/15/2110:39
02/16/2111:36
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
423
138
1
02/15/2110:39
02/16/2111:36
117-81-7
Fluoranthene
ND
ug/kg
423
128
1
02/15/2110:39
02/16/2111:36
206-44-0
Fluorene
ND
ug/kg
423
113
1
02/15/2110:39
02/16/2111:36
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
423
103
1
02/15/2110:39
02/16/2111:36
87-68-3
Hexachlorobenzene
ND
ug/kg
423
107
1
02/15/2110:39
02/16/2111:36
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
423
169
1
02/15/2110:39
02/16/2111:36
77-47-4
Hexachloroethane
ND
ug/kg
423
96.4
1
02/15/2110:39
02/16/2111:36
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
423
194
1
02/15/2110:39
02/16/2111:36
193-39-5
Isophorone
ND
ug/kg
423
91.9
1
02/15/2110:39
02/16/2111:36
78-59-1
1-Methylnaphthalene
ND
ug/kg
423
113
1
02/15/2110:39
02/16/2111:36
90-12-0
2-Methylnaphthalene
ND
ug/kg
423
108
1
02/15/2110:39
02/16/2111:36
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
423
93.7
1
02/15/2110:39
02/16/2111:36
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
423
106
1
02/15/21 10:39
02/16/21 11:36
15831-10-4
Naphthalene
ND
ug/kg
423
101
1
02/15/2110:39
02/16/2111:36
91-20-3
2-Nitroaniline
ND
ug/kg
2110
213
1
02/15/2110:39
02/16/2111:36
88-74-4
3-Nitroaniline
ND
ug/kg
2110
224
1
02/15/2110:39
02/16/2111:36
99-09-2
4-Nitroaniline
ND
ug/kg
846
209
1
02/15/2110:39
02/16/2111:36
100-01-6
Nitrobenzene
ND
ug/kg
423
101
1
02/15/2110:39
02/16/2111:36
98-95-3
2-Nitrophenol
ND
ug/kg
423
131
1
02/15/2110:39
02/16/2111:36
88-75-5
4-Nitrophenol
ND
ug/kg
2110
674
1
02/15/2110:39
02/16/2111:36
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
423
119
1
02/15/2110:39
02/16/2111:36
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
423
118
1
02/15/2110:39
02/16/2111:36
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
423
108
1
02/15/2110:39
02/16/2111:36
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
423
118
1
02/15/2110:39
02/16/2111:36
108-60-1
Pentachlorophenol
ND
ug/kg
846
194
1
02/15/2110:39
02/16/2111:36
87-86-5
Phenanthrene
ND
ug/kg
423
107
1
02/15/2110:39
02/16/2111:36
85-01-8
Phenol
ND
ug/kg
423
101
1
02/15/2110:39
02/16/2111:36
108-95-2
Pyrene
ND
ug/kg
423
116
1
02/15/2110:39
02/16/2111:36
129-00-0
REPORT OF LABORATORY ANALYSIS
IL
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 EW (6.5-7) Lab ID: 92521577009 Collected: 02/10/21 17:05 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Comments: • Volatile Petroleum Hydrocarbons by Method MADEPV - Surrogate failure due to matrix interference.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Pyridine
ND
ug/kg
423
107
1
02/15/21 10:39
02/16/21 11:36
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
423
96.9
1
02/15/21 10:39
02/16/21 11:36
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
423
110
1
02/15/21 10:39
02/16/21 11:36
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
423
106
1
02/15/21 10:39
02/16/21 11:36
88-06-2
Surrogates
Nitrobenzene-d5 (S)
60
%
21-130
1
02/15/21 10:39
02/16/21 11:36
4165-60-0
2-Fluorobiphenyl (S)
56
%
19-130
1
02/15/21 10:39
02/16/21 11:36
321-60-8
Terphenyl-dl4 (S)
74
%
15-130
1
02/15/21 10:39
02/16/21 11:36
1718-51-0
Phenol-d6 (S)
52
%
18-130
1
02/15/21 10:39
02/16/21 11:36
13127-88-3
2-Fluorophenol (S)
51
%
18-130
1
02/15/21 10:39
02/16/21 11:36
367-12-4
2,4,6-Tribromophenol (S)
76
%
18-130
1
02/15/21 10:39
02/16/21 11:36
118-79-6
8260D/5035A/5030B Volatiles
Analytical
Method: EPA 8260D Preparation Method:
EPA
5035A/5030B
Pace Analytical Services
- Charlotte
Acetone
ND
ug/kg
141
45.4
1
02/11/21 11:36
02/11/21 17:00
67-64-1
Benzene
ND
ug/kg
7.1
2.8
1
02/11/21 11:36
02/11/21 17:00
71-43-2
Bromobenzene
ND
ug/kg
7.1
2.3
1
02/11/21 11:36
02/11/21 17:00
108-86-1
Bromochloromethane
ND
ug/kg
7.1
2.1
1
02/11/21 11:36
02/11/21 17:00
74-97-5
Bromodichloromethane
ND
ug/kg
7.1
2.7
1
02/11/21 11:36
02/11/21 17:00
75-27-4
Bromoform
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
75-25-2
Bromomethane
ND
ug/kg
14.1
11.2
1
02/11/21 11:36
02/11/21 17:00
74-83-9
2-Butanone (MEK)
ND
ug/kg
141
33.9
1
02/11/21 11:36
02/11/21 17:00
78-93-3
n-Butylbenzene
ND
ug/kg
7.1
3.3
1
02/11/21 11:36
02/11/21 17:00
104-51-8
sec-Butylbenzene
ND
ug/kg
7.1
3.1
1
02/11/21 11:36
02/11/21 17:00
135-98-8
tert-Butyl benzene
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
98-06-6
Carbon tetrachloride
ND
ug/kg
7.1
2.6
1
02/11/21 11:36
02/11/21 17:00
56-23-5
Chlorobenzene
ND
ug/kg
7.1
1.4
1
02/11/21 11:36
02/11/21 17:00
108-90-7
Chloroethane
ND
ug/kg
14.1
5.5
1
02/11/21 11:36
02/11/21 17:00
75-00-3
Chloroform
ND
ug/kg
7.1
4.3
1
02/11/21 11:36
02/11/21 17:00
67-66-3
Chloromethane
ND
ug/kg
14.1
5.9
1
02/11/21 11:36
02/11/21 17:00
74-87-3
2-Chlorotoluene
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
95-49-8
4-Chlorotoluene
ND
ug/kg
7.1
1.3
1
02/11/21 11:36
02/11/21 17:00
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.1
2.7
1
02/11/21 11:36
02/11/21 17:00
96-12-8
Dibromochloromethane
ND
ug/kg
7.1
4.0
1
02/11/21 11:36
02/11/21 17:00
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.1
3.1
1
02/11/21 11:36
02/11/21 17:00
106-93-4
Dibromomethane
ND
ug/kg
7.1
1.5
1
02/11/21 11:36
02/11/21 17:00
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.1
2.2
1
02/11/21 11:36
02/11/21 17:00
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.1
1.8
1
02/11/21 11:36
02/11/21 17:00
106-46-7
Dichlorodifluoromethane
ND
ug/kg
14.1
3.1
1
02/11/21 11:36
02/11/21 17:00
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.1
2.9
1
02/11/21 11:36
02/11/21 17:00
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.1
4.7
1
02/11/21 11:36
02/11/21 17:00
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.1
2.9
1
02/11/21 11:36
02/11/21 17:00
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 65

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 EW (6.5-7) Lab ID: 92521577009 Collected: 02/10/21 17:05 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Comments: • Volatile Petroleum Hydrocarbons by Method MADEPV - Surrogate failure due to matrix interference.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/kg
7.1
2.4
1
02/11/21 11:36
02/11/21 17:00
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.1
2.1
1
02/11/21 11:36
02/11/21 17:00
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.1
2.2
1
02/11/21 11:36
02/11/21 17:00
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.1
2.3
1
02/11/21 11:36
02/11/21 17:00
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.1
3.4
1
02/11/21 11:36
02/11/21 17:00
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
7.1
1.9
1
02/11/21 11:36
02/11/21 17:00
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
7.1
2.4
1
02/11/21 11:36
02/11/21 17:00
10061-02-6
Diisopropyl ether
ND
ug/kg
7.1
1.9
1
02/11/21 11:36
02/11/21 17:00
108-20-3
Ethylbenzene
ND
ug/kg
7.1
3.3
1
02/11/21 11:36
02/11/21 17:00
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
14.1
11.6
1
02/11/21 11:36
02/11/21 17:00
87-68-3
2-Hexanone
ND
ug/kg
70.7
6.8
1
02/11/21 11:36
02/11/21 17:00
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
7.1
2.4
1
02/11/21 11:36
02/11/21 17:00
98-82-8
p-Isopropyltoluene
ND
ug/kg
7.1
3.5
1
02/11/21 11:36
02/11/21 17:00
99-87-6
Methylene Chloride
ND
ug/kg
28.3
19.4
1
02/11/21 11:36
02/11/21 17:00
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
70.7
6.8
1
02/11/21 11:36
02/11/21 17:00
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
7.1
2.6
1
02/11/21 11:36
02/11/21 17:00
1634-04-4
Naphthalene
ND
ug/kg
7.1
3.7
1
02/11/21 11:36
02/11/21 17:00
91-20-3
n-Propylbenzene
ND
ug/kg
7.1
2.5
1
02/11/21 11:36
02/11/21 17:00
103-65-1
Styrene
ND
ug/kg
7.1
1.9
1
02/11/21 11:36
02/11/21 17:00
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
7.1
2.7
1
02/11/21 11:36
02/11/21 17:00
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
7.1
1.9
1
02/11/21 11:36
02/11/21 17:00
79-34-5
Tetrachloroethene
ND
ug/kg
7.1
2.2
1
02/11/21 11:36
02/11/21 17:00
127-18-4
Toluene
ND
ug/kg
7.1
2.0
1
02/11/21 11:36
02/11/21 17:00
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
7.1
5.7
1
02/11/21 11:36
02/11/21 17:00
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
7.1
5.9
1
02/11/21 11:36
02/11/21 17:00
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
7.1
3.7
1
02/11/21 11:36
02/11/21 17:00
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
7.1
2.3
1
02/11/21 11:36
02/11/21 17:00
79-00-5
Trichloroethene
ND
ug/kg
7.1
1.8
1
02/11/21 11:36
02/11/21 17:00
79-01-6
Trichlorofluoromethane
ND
ug/kg
7.1
3.9
1
02/11/21 11:36
02/11/21 17:00
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
7.1
3.6
1
02/11/21 11:36
02/11/21 17:00
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
7.1
1.9
1
02/11/21 11:36
02/11/21 17:00
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
7.1
2.4
1
02/11/21 11:36
02/11/21 17:00
108-67-8
Vinyl acetate
ND
ug/kg
70.7
5.1
1
02/11/21 11:36
02/11/21 17:00
108-05-4
Vinyl chloride
ND
ug/kg
14.1
3.6
1
02/11/21 11:36
02/11/21 17:00
75-01-4
Xylene (Total)
ND
ug/kg
14.1
4.0
1
02/11/21 11:36
02/11/21 17:00
1330-20-7
m&p-Xylene
ND
ug/kg
14.1
4.8
1
02/11/21 11:36
02/11/21 17:00
179601-23-1
o-Xylene
ND
ug/kg
7.1
3.1
1
02/11/21 11:36
02/11/21 17:00
95-47-6
Surrogates
Toluene-d8 (S)
101
%
70-130
1
02/11/21 11:36
02/11/21 17:00
2037-26-5
4-Bromofluorobenzene (S)
93
%
69-134
1
02/11/21 11:36
02/11/21 17:00
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
02/11/21 11:36
02/11/21 17:00
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 65

lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 EW (6.5-7)
Lab ID: 92521577009 Collected:
02/10/21 17:05
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Comments: • Volatile Petroleum Hydrocarbons by Method MADEPV - Surrogate
failure due to matrix interference.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
20.7 % 0.10
0.10 1
02/11/21 14:13
N2
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM
2540 G
Pace National - Mt. Juliet
Total Solids
79.6 %
1
02/22/21 11:28
02/22/21 11:36
Sample: #2 WW (6.5-7)
Lab ID: 92521577010 Collected:
02/10/21 17:15
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
Aliphatic (C09-C18)
24.4 mg/kg 12.8
12.8 1
02/15/21 11:54
02/16/21 22:57
N2
Aliphatic (C19-C36)
ND mg/kg 12.8
12.8 1
02/15/21 11:54
02/16/21 22:57
N2
Aromatic (C11-C22)
ND mg/kg 12.8
12.8 1
02/15/21 11:54
02/16/21 22:57
N2
Surrogates
1-Chlorooctadecane (S)
50 % 40-140
1
02/15/21 11:54
02/16/21 22:57
3386-33-2
o-Terphenyl (S)
71 % 40-140
1
02/15/21 11:54
02/16/21 22:57
84-15-1
2-Fluorobiphenyl (S)
108 % 40-140
1
02/15/21 11:54
02/16/21 22:57
321-60-8
2-Bromonaphthalene (S)
114 % 40-140
1
02/15/21 11:54
02/16/21 22:57
580-13-2
MADEPV
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
Aliphatic (C05-CO8)
ND mg/kg 7.63
2.55 1
02/10/21 17:15
02/21/21 21:57
Aliphatic (C09-C12)
5.70J mg/kg 7.63
2.55 1
02/10/21 17:15
02/21/21 21:57
J
Aromatic (C09-C10),Unadjusted
6.27J mg/kg 7.63
2.55 1
02/10/21 17:15
02/21/21 21:57
TPHC9C10A J
Total VPH
12.0 mg/kg 7.63
2.55 1
02/10/21 17:15
02/21/21 21:57
VPH
Surrogates
2,5-Dibromotoluene (FID)
113 % 70.0-130
1
02/10/21 17:15
02/21/21 21:57
615-59-8FID
2,5-Dibromotoluene (PID)
117 % 70.0-130
1
02/10/21 17:15
02/21/21 21:57
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Acenaphthene
ND ug/kg 414
106 1
02/15/2110:39
02/16/2112:03
83-32-9
Acenaphthylene
ND ug/kg 414
98.0 1
02/15/2110:39
02/16/2112:03
208-96-8
Aniline
ND ug/kg 414
92.9 1
02/15/2110:39
02/16/2112:03
62-53-3
Anthracene
ND ug/kg 414
107 1
02/15/2110:39
02/16/2112:03
120-12-7
Benzo(a)anthracene
ND ug/kg 414
132 1
02/15/2110:39
02/16/2112:03
56-55-3
Benzo(a)pyrene
ND ug/kg 414
179 1
02/15/2110:39
02/16/2112:03
50-32-8
Benzo(b)fluoranthene
ND ug/kg 414
167 1
02/15/2110:39
02/16/2112:03
205-99-2
Benzo(g,h,i)perylene
ND ug/kg 414
162 1
02/15/2110:39
02/16/2112:03
191-24-2
Date: 02/24/2021 01:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 WW (6.5-7) Lab ID: 92521577010 Collected: 02/10/21 17:15 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Benzo(k)fluoranthene
ND
ug/kg
414
174
1
02/15/21 10:39
02/16/21 12:03
207-08-9
Benzoic Acid
ND
ug/kg
2070
446
1
02/15/21 10:39
02/16/21 12:03
65-85-0
Benzyl alcohol
ND
ug/kg
828
219
1
02/15/21 10:39
02/16/21 12:03
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
414
109
1
02/15/21 10:39
02/16/21 12:03
101-55-3
Butylbenzylphthalate
ND
ug/kg
414
110
1
02/15/21 10:39
02/16/21 12:03
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
828
252
1
02/15/21 10:39
02/16/21 12:03
59-50-7
4-Chloroaniline
ND
ug/kg
828
253
1
02/15/21 10:39
02/16/21 12:03
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
414
110
1
02/15/21 10:39
02/16/21 12:03
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
414
87.9
1
02/15/21 10:39
02/16/21 12:03
111-44-4
2-Chloronaphthalene
ND
ug/kg
414
92.2
1
02/15/21 10:39
02/16/21 12:03
91-58-7
2-Chlorophenol
ND
ug/kg
414
96.3
1
02/15/21 10:39
02/16/21 12:03
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
414
107
1
02/15/21 10:39
02/16/21 12:03
7005-72-3
Chrysene
ND
ug/kg
414
120
1
02/15/21 10:39
02/16/21 12:03
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
414
166
1
02/15/21 10:39
02/16/21 12:03
53-70-3
Dibenzofuran
ND
ug/kg
414
103
1
02/15/21 10:39
02/16/21 12:03
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
414
89.5
1
02/15/21 10:39
02/16/21 12:03
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
414
93.2
1
02/15/21 10:39
02/16/21 12:03
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
414
91.1
1
02/15/21 10:39
02/16/21 12:03
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
828
288
1
02/15/21 10:39
02/16/21 12:03
91-94-1
2,4-Dichlorophenol
ND
ug/kg
414
137
1
02/15/21 10:39
02/16/21 12:03
120-83-2
Diethylphthalate
ND
ug/kg
414
89.8
1
02/15/21 10:39
02/16/21 12:03
84-66-2
2,4-Dimethylphenol
ND
ug/kg
414
103
1
02/15/21 10:39
02/16/21 12:03
105-67-9
Dimethylphthalate
ND
ug/kg
414
93.6
1
02/15/21 10:39
02/16/21 12:03
131-11-3
Di-n-butylphthalate
ND
ug/kg
414
102
1
02/15/21 10:39
02/16/21 12:03
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
828
667
1
02/15/21 10:39
02/16/21 12:03
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2070
1320
1
02/15/21 10:39
02/16/21 12:03
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
414
110
1
02/15/21 10:39
02/16/21 12:03
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
414
108
1
02/15/21 10:39
02/16/21 12:03
606-20-2
Di-n-octylphthalate
ND
ug/kg
414
236
1
02/15/21 10:39
02/16/21 12:03
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
414
135
1
02/15/21 10:39
02/16/21 12:03
117-81-7
Fluoranthene
ND
ug/kg
414
125
1
02/15/21 10:39
02/16/21 12:03
206-44-0
Fluorene
ND
ug/kg
414
ill
1
02/15/21 10:39
02/16/21 12:03
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
414
101
1
02/15/21 10:39
02/16/21 12:03
87-68-3
Hexachlorobenzene
ND
ug/kg
414
105
1
02/15/21 10:39
02/16/21 12:03
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
414
166
1
02/15/21 10:39
02/16/21 12:03
77-47-4
Hexachloroethane
ND
ug/kg
414
94.3
1
02/15/21 10:39
02/16/21 12:03
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
414
189
1
02/15/21 10:39
02/16/21 12:03
193-39-5
Isophorone
ND
ug/kg
414
89.9
1
02/15/21 10:39
02/16/21 12:03
78-59-1
1-Methylnaphthalene
ND
ug/kg
414
110
1
02/15/21 10:39
02/16/21 12:03
90-12-0
2-Methylnaphthalene
ND
ug/kg
414
105
1
02/15/21 10:39
02/16/21 12:03
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
414
91.7
1
02/15/21 10:39
02/16/21 12:03
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
414
104
1
02/15/21 10:39
02/16/21 12:03
15831-10-4
Naphthalene
ND
ug/kg
414
99.1
1
02/15/21 10:39
02/16/21 12:03
91-20-3
2-Nitroaniline
ND
ug/kg
2070
208
1
02/15/21 10:39
02/16/21 12:03
88-74-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 WW (6.5-7)
Lab ID:
92521577010
Collected:
02/10/21 17:15
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are
adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Pace Analytical Services
- Charlotte
3-Nitroaniline
ND
ug/kg
2070
219
1
02/15/21 10:39
02/16/21 12:03
99-09-2 IL
4-Nitroaniline
ND
ug/kg
828
204
1
02/15/21 10:39
02/16/21 12:03
100-01-6
Nitrobenzene
ND
ug/kg
414
98.8
1
02/15/21 10:39
02/16/21 12:03
98-95-3
2-Nitrophenol
ND
ug/kg
414
128
1
02/15/21 10:39
02/16/21 12:03
88-75-5
4-Nitrophenol
ND
ug/kg
2070
660
1
02/15/21 10:39
02/16/21 12:03
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
414
116
1
02/15/21 10:39
02/16/21 12:03
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
414
116
1
02/15/21 10:39
02/16/21 12:03
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
414
106
1
02/15/21 10:39
02/16/21 12:03
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
414
115
1
02/15/21 10:39
02/16/21 12:03
108-60-1
Pentachlorophenol
ND
ug/kg
828
189
1
02/15/21 10:39
02/16/21 12:03
87-86-5
Phenanthrene
ND
ug/kg
414
104
1
02/15/21 10:39
02/16/21 12:03
85-01-8
Phenol
ND
ug/kg
414
98.8
1
02/15/21 10:39
02/16/21 12:03
108-95-2
Pyrene
ND
ug/kg
414
114
1
02/15/21 10:39
02/16/21 12:03
129-00-0
Pyridine
ND
ug/kg
414
105
1
02/15/21 10:39
02/16/21 12:03
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
414
94.8
1
02/15/21 10:39
02/16/21 12:03
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
414
107
1
02/15/21 10:39
02/16/21 12:03
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
414
104
1
02/15/21 10:39
02/16/21 12:03
88-06-2
Surrogates
Nitrobenzene-d5 (S)
77
%
21-130
1
02/15/21 10:39
02/16/21 12:03
4165-60-0
2-Fluorobiphenyl (S)
75
%
19-130
1
02/15/21 10:39
02/16/21 12:03
321-60-8
Terphenyl-d14 (S)
84
%
15-130
1
02/15/21 10:39
02/16/21 12:03
1718-51-0
Phenol-d6 (S)
64
%
18-130
1
02/15/21 10:39
02/16/21 12:03
13127-88-3
2-Fluorophenol (S)
64
%
18-130
1
02/15/21 10:39
02/16/21 12:03
367-12-4
2,4,6-Tribromophenol (S)
86
%
18-130
1
02/15/21 10:39
02/16/21 12:03
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D
Preparation Method: EPA 5035A/5030B
Pace Analytical Services
- Charlotte
Acetone
ND
ug/kg
151
48.5
1
02/11/21 14:01
02/15/21 17:11
67-64-1
Benzene
ND
ug/kg
7.6
3.0
1
02/11/21 14:01
02/15/21 17:11
71-43-2
Bromobenzene
ND
ug/kg
7.6
2.5
1
02/11/21 14:01
02/15/21 17:11
108-86-1
Bromochloromethane
ND
ug/kg
7.6
2.2
1
02/11/21 14:01
02/15/21 17:11
74-97-5
Bromodichloromethane
ND
ug/kg
7.6
2.9
1
02/11/21 14:01
02/15/21 17:11
75-27-4
Bromoform
ND
ug/kg
7.6
2.7
1
02/11/21 14:01
02/15/21 17:11
75-25-2
Bromomethane
ND
ug/kg
15.1
11.9
1
02/11/21 14:01
02/15/21 17:11
74-83-9 v1
2-Butanone (MEK)
ND
ug/kg
151
36.3
1
02/11/21 14:01
02/15/21 17:11
78-93-3
n-Butylbenzene
ND
ug/kg
7.6
3.6
1
02/11/21 14:01
02/15/21 17:11
104-51-8
sec-Butylbenzene
ND
ug/kg
7.6
3.3
1
02/11/21 14:01
02/15/21 17:11
135-98-8
tert-Butyl benzene
ND
ug/kg
7.6
2.7
1
02/11/21 14:01
02/15/21 17:11
98-06-6
Carbon tetrachloride
ND
ug/kg
7.6
2.8
1
02/11/21 14:01
02/15/21 17:11
56-23-5
Chlorobenzene
ND
ug/kg
7.6
1.5
1
02/11/21 14:01
02/15/21 17:11
108-90-7
Chloroethane
ND
ug/kg
15.1
5.8
1
02/11/21 14:01
02/15/21 17:11
75-00-3
Chloroform
ND
ug/kg
7.6
4.6
1
02/11/21 14:01
02/15/21 17:11
67-66-3
Chloromethane
ND
ug/kg
15.1
6.3
1
02/11/21 14:01
02/15/21 17:11
74-87-3
2-Chlorotoluene
ND
ug/kg
7.6
2.7
1
02/11/21 14:01
02/15/21 17:11
95-49-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 WW (6.5-7) Lab ID: 92521577010 Collected: 02/10/21 17:15 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
4-Chlorotoluene
ND
ug/kg
7.6
1.3
1
02/11/21 14:01
02/15/21 17:11
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.6
2.9
1
02/11/21 14:01
02/15/21 17:11
96-12-8
Dibromochloromethane
ND
ug/kg
7.6
4.2
1
02/11/21 14:01
02/15/21 17:11
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.6
3.3
1
02/11/21 14:01
02/15/21 17:11
106-93-4
Dibromomethane
ND
ug/kg
7.6
1.6
1
02/11/21 14:01
02/15/21 17:11
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.6
2.7
1
02/11/21 14:01
02/15/21 17:11
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.6
2.3
1
02/11/21 14:01
02/15/21 17:11
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.6
2.0
1
02/11/21 14:01
02/15/21 17:11
106-46-7
Dichlorodifluoromethane
ND
ug/kg
15.1
3.3
1
02/11/21 14:01
02/15/21 17:11
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.6
3.1
1
02/11/21 14:01
02/15/21 17:11
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.6
5.0
1
02/11/21 14:01
02/15/21 17:11
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.6
3.1
1
02/11/21 14:01
02/15/21 17:11
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
7.6
2.6
1
02/11/21 14:01
02/15/21 17:11
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.6
2.6
1
02/11/21 14:01
02/15/21 17:11
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.6
2.3
1
02/11/21 14:01
02/15/21 17:11
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.6
2.4
1
02/11/21 14:01
02/15/21 17:11
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.6
2.5
1
02/11/21 14:01
02/15/21 17:11
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.6
3.6
1
02/11/21 14:01
02/15/21 17:11
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
7.6
2.1
1
02/11/21 14:01
02/15/21 17:11
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
7.6
2.6
1
02/11/21 14:01
02/15/21 17:11
10061-02-6
Diisopropyl ether
ND
ug/kg
7.6
2.0
1
02/11/21 14:01
02/15/21 17:11
108-20-3
Ethylbenzene
ND
ug/kg
7.6
3.5
1
02/11/21 14:01
02/15/21 17:11
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
15.1
12.4
1
02/11/21 14:01
02/15/21 17:11
87-68-3
2-Hexanone
ND
ug/kg
75.5
7.3
1
02/11/21 14:01
02/15/21 17:11
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
7.6
2.6
1
02/11/21 14:01
02/15/21 17:11
98-82-8
p-Isopropyltoluene
ND
ug/kg
7.6
3.7
1
02/11/21 14:01
02/15/21 17:11
99-87-6
Methylene Chloride
ND
ug/kg
30.2
20.7
1
02/11/21 14:01
02/15/21 17:11
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
75.5
7.3
1
02/11/21 14:01
02/15/21 17:11
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
7.6
2.8
1
02/11/21 14:01
02/15/21 17:11
1634-04-4
Naphthalene
ND
ug/kg
7.6
4.0
1
02/11/21 14:01
02/15/21 17:11
91-20-3
n-Propylbenzene
ND
ug/kg
7.6
2.7
1
02/11/21 14:01
02/15/21 17:11
103-65-1
Styrene
ND
ug/kg
7.6
2.0
1
02/11/21 14:01
02/15/21 17:11
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
7.6
2.9
1
02/11/21 14:01
02/15/21 17:11
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
7.6
2.0
1
02/11/21 14:01
02/15/21 17:11
79-34-5
Tetrachloroethene
ND
ug/kg
7.6
2.4
1
02/11/21 14:01
02/15/21 17:11
127-18-4
Toluene
ND
ug/kg
7.6
2.1
1
02/11/21 14:01
02/15/21 17:11
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
7.6
6.1
1
02/11/21 14:01
02/15/21 17:11
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
7.6
6.3
1
02/11/21 14:01
02/15/21 17:11
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
7.6
3.9
1
02/11/21 14:01
02/15/21 17:11
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
7.6
2.5
1
02/11/21 14:01
02/15/21 17:11
79-00-5
Trichloroethene
ND
ug/kg
7.6
1.9
1
02/11/21 14:01
02/15/21 17:11
79-01-6
Trichlorofluoromethane
ND
ug/kg
7.6
4.2
1
02/11/21 14:01
02/15/21 17:11
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
7.6
3.8
1
02/11/21 14:01
02/15/21 17:11
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
7.6
2.1
1
02/11/21 14:01
02/15/21 17:11
95-63-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 WW (6.5-7)
Lab ID: 92521577010 Collected:
02/10/21 17:15
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
1,3,5-Trimethylbenzene
5.11 ug/kg 7.6
2.5 1
02/11/21 14:01
02/15/21 17:11
108-67-8
Vinyl acetate
ND ug/kg 75.5
5.5 1
02/11/21 14:01
02/15/21 17:11
108-05-4
Vinyl chloride
ND ug/kg 15.1
3.8 1
02/11/21 14:01
02/15/21 17:11
75-01-4
Xylene (Total)
ND ug/kg 15.1
4.3 1
02/11/21 14:01
02/15/21 17:11
1330-20-7
m&p-Xylene
ND ug/kg 15.1
5.2 1
02/11/21 14:01
02/15/21 17:11
179601-23-1
o-Xylene
ND ug/kg 7.6
3.3 1
02/11/21 14:01
02/15/21 17:11
95-47-6
Surrogates
Toluene-d8 (S)
102 % 70-130
1
02/11/21 14:01
02/15/21 17:11
2037-26-5
4-Bromofluorobenzene (S)
103 % 69-134
1
02/11/21 14:01
02/15/21 17:11
460-00-4
1,2-Dichloroethane-d4 (S)
106 % 70-130
1
02/11/21 14:01
02/15/21 17:11
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
21.3 % 0.10
0.10 1
02/11/21 14:13
N2
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation Method: SM
2540 G
Pace National - Mt. Juliet
Total Solids
79.5 %
1
02/22/21 11:28
02/22/21 11:36
Sample: #2 BASE (15.0)
Lab ID: 92521577011 Collected:
02/10/21 16:55
Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
Aliphatic (C09-C18)
9270 mg/kg 2460
2460 200
02/15/21 11:54
02/17/21 20:01
N2
Aliphatic (C19-C36)
ND mg/kg 2460
2460 200
02/15/21 11:54
02/17/21 20:01
N2
Aromatic (C11-C22)
2210 mg/kg 307
307 25
02/15/21 11:54
02/17/21 20:01
N2
Surrogates
1-Chlorooctadecane (S)
0 % 40-140
200
02/15/21 11:54
02/17/21 20:01
3386-33-2 S4
o-Terphenyl (S)
0 % 40-140
25
02/15/21 11:54
02/17/21 20:01
84-15-1 S4
2-Fluorobiphenyl (S)
0 % 40-140
25
02/15/21 11:54
02/17/21 20:01
321-60-8 S4
2-Bromonaphthalene (S)
0 % 40-140
25
02/15/21 11:54
02/17/21 20:01
580-13-2 S4
MADEPV
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
Aliphatic (C05-CO8)
44.7 mg/kg 36.5
12.2 5
02/10/21 16:55
02/21/21 23:03
Aliphatic (C09-C12)
924 mg/kg 36.5
12.2 5
02/10/21 16:55
02/21/21 23:03
Aromatic (C09-C10),Unadjusted
67.2J mg/kg 73.1
24.3 10
02/10/21 16:55
02/23/21 16:17
TPHC9C10A J
Total VPH
969 mg/kg 36.5
12.2 5
02/10/21 16:55
02/21/21 23:03
VPH
Surrogates
2,5-Dibromotoluene (FID)
106 % 70.0-130
5
02/10/21 16:55
02/21/21 23:03
615-59-8FID
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM
without the written consent of Pace Analytical Services, LLC.
Page 27 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 BASE (15.0)
Lab ID:
92521577011
Collected:
02/10/21
16:55
Received: 02/11/21
08:00 Matrix: Solid
Results reported on a "dry weight"
basis and are
adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
MADEPV
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
Surrogates
2,5-Dibromotoluene (FID)
100
%
70.0-130
10
02/10/21 16:55
02/23/21 16:17
615-59-8FID
2,5-Dibromotoluene (PID)
116
%
70.0-130
5
02/10/21 16:55
02/21/21 23:03
615-59-8PID
2,5-Dibromotoluene (PID)
102
%
70.0-130
10
02/10/21 16:55
02/23/21 16:17
615-59-8PID
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method: EPA 3546
Pace Analytical Services
- Charlotte
Acenaphthene
ND
ug/kg
4120
1060
10
02/15/21 10:39
02/17/21 10:11
83-32-9
Acenaphthylene
ND
ug/kg
4120
976
10
02/15/21 10:39
02/17/21 10:11
208-96-8
Aniline
ND
ug/kg
4120
926
10
02/15/21 10:39
02/17/21 10:11
62-53-3
Anthracene
ND
ug/kg
4120
1070
10
02/15/21 10:39
02/17/21 10:11
120-12-7
Benzo(a)anthracene
ND
ug/kg
4120
1310
10
02/15/21 10:39
02/17/21 10:11
56-55-3
Benzo(a)pyrene
ND
ug/kg
4120
1790
10
02/15/21 10:39
02/17/21 10:11
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
4120
1660
10
02/15/21 10:39
02/17/21 10:11
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
4120
1610
10
02/15/21 10:39
02/17/21 10:11
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
4120
1740
10
02/15/21 10:39
02/17/21 10:11
207-08-9
Benzoic Acid
ND
ug/kg
20600
4450
10
02/15/21 10:39
02/17/21 10:11
65-85-0
Benzyl alcohol
ND
ug/kg
8250
2190
10
02/15/21 10:39
02/17/21 10:11
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
4120
1080
10
02/15/21 10:39
02/17/21 10:11
101-55-3
Butylbenzylphthalate
ND
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 10:11
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
8250
2510
10
02/15/21 10:39
02/17/21 10:11
59-50-7
4-Chloroaniline
ND
ug/kg
8250
2520
10
02/15/21 10:39
02/17/21 10:11
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
4120
1100
10
02/15/21 10:39
02/17/21 10:11
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
4120
876
10
02/15/21 10:39
02/17/21 10:11
111-44-4
2-Chloronaphthalene
ND
ug/kg
4120
918
10
02/15/21 10:39
02/17/21 10:11
91-58-7
2-Chlorophenol
ND
ug/kg
4120
959
10
02/15/21 10:39
02/17/21 10:11
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
4120
1070
10
02/15/21 10:39
02/17/21 10:11
7005-72-3
Chrysene
ND
ug/kg
4120
1200
10
02/15/21 10:39
02/17/21 10:11
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
4120
1650
10
02/15/21 10:39
02/17/21 10:11
53-70-3
Dibenzofuran
1380J
ug/kg
4120
1030
10
02/15/21 10:39
02/17/21 10:11
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
4120
892
10
02/15/21 10:39
02/17/21 10:11
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
4120
928
10
02/15/21 10:39
02/17/21 10:11
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
4120
907
10
02/15/21 10:39
02/17/21 10:11
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
8250
2870
10
02/15/21 10:39
02/17/21 10:11
91-94-1
2,4-Dichlorophenol
ND
ug/kg
4120
1360
10
02/15/21 10:39
02/17/21 10:11
120-83-2
Diethylphthalate
ND
ug/kg
4120
894
10
02/15/21 10:39
02/17/21 10:11
84-66-2 v1
2,4-Dimethylphenol
ND
ug/kg
4120
1030
10
02/15/21 10:39
02/17/21 10:11
105-67-9
Dimethylphthalate
ND
ug/kg
4120
932
10
02/15/21 10:39
02/17/21 10:11
131-11-3
Di-n-butylphthalate
ND
ug/kg
4120
1020
10
02/15/21 10:39
02/17/21 10:11
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
8250
6650
10
02/15/21 10:39
02/17/21 10:11
534-52-1
2,4-Dinitrophenol
ND
ug/kg
20600
13200
10
02/15/21 10:39
02/17/21 10:11
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
4120
1090
10
02/15/21 10:39
02/17/21 10:11
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
4120
1080
10
02/15/21 10:39
02/17/21 10:11
606-20-2
Di-n-octylphthalate
ND
ug/kg
4120
2350
10
02/15/21 10:39
02/17/21 10:11
117-84-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 BASE (15.0) Lab ID: 92521577011 Collected: 02/10/21 16:55 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
bis(2- Ethyl hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Pyridine
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D/5035A/5030B Volatiles
Acetone
Benzene
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
ND
ug/kg
4120
1350
10
02/15/2110:39
02/17/2110:11
117-81-7
ND
ug/kg
4120
1250
10
02/15/2110:39
02/17/2110:11
206-44-0
1370J
ug/kg
4120
1100
10
02/15/2110:39
02/17/2110:11
86-73-7
ND
ug/kg
4120
1000
10
02/15/2110:39
02/17/2110:11
87-68-3
ND
ug/kg
4120
1050
10
02/15/2110:39
02/17/2110:11
118-74-1
ND
ug/kg
4120
1650
10
02/15/2110:39
02/17/2110:11
77-47-4
ND
ug/kg
4120
939
10
02/15/2110:39
02/17/2110:11
67-72-1
ND
ug/kg
4120
1890
10
02/15/2110:39
02/17/2110:11
193-39-5
ND
ug/kg
4120
896
10
02/15/2110:39
02/17/2110:11
78-59-1
20200
ug/kg
4120
1100
10
02/15/2110:39
02/17/2110:11
90-12-0
29800
ug/kg
4120
1050
10
02/15/2110:39
02/17/2110:11
91-57-6
ND
ug/kg
4120
913
10
02/15/2110:39
02/17/2110:11
95-48-7
ND
ug/kg
4120
1040
10
02/15/2110:39
02/17/2110:11
15831-10-4
3120J
ug/kg
4120
987
10
02/15/2110:39
02/17/2110:11
91-20-3
ND
ug/kg
20600
2070
10
02/15/2110:39
02/17/2110:11
88-74-4
ND
ug/kg
20600
2190
10
02/15/2110:39
02/17/2110:11
99-09-2
IL
ND
ug/kg
8250
2040
10
02/15/2110:39
02/17/2110:11
100-01-6
ND
ug/kg
4120
984
10
02/15/2110:39
02/17/2110:11
98-95-3
ND
ug/kg
4120
1270
10
02/15/2110:39
02/17/2110:11
88-75-5
ND
ug/kg
20600
6570
10
02/15/2110:39
02/17/2110:11
100-02-7
v1
ND
ug/kg
4120
1160
10
02/15/2110:39
02/17/2110:11
62-75-9
ND
ug/kg
4120
1150
10
02/15/2110:39
02/17/2110:11
621-64-7
ND
ug/kg
4120
1050
10
02/15/2110:39
02/17/2110:11
86-30-6
ND
ug/kg
4120
1150
10
02/15/2110:39
02/17/2110:11
108-60-1
ND
ug/kg
8250
1890
10
02/15/2110:39
02/17/2110:11
87-86-5
9270
ug/kg
4120
1040
10
02/15/2110:39
02/17/2110:11
85-01-8
ND
ug/kg
4120
984
10
02/15/2110:39
02/17/2110:11
108-95-2
ND
ug/kg
4120
1130
10
02/15/2110:39
02/17/2110:11
129-00-0
ND
ug/kg
4120
1040
10
02/15/2110:39
02/17/2110:11
110-86-1
ND
ug/kg
4120
944
10
02/15/2110:39
02/17/2110:11
120-82-1
ND
ug/kg
4120
1070
10
02/15/2110:39
02/17/2110:11
95-95-4
ND
ug/kg
4120
1040
10
02/15/2110:39
02/17/2110:11
88-06-2
0
%
21-130
10
02/15/2110:39
02/17/2110:11
4165-60-0
D3,S4
0
%
19-130
10
02/15/2110:39
02/17/2110:11
321-60-8
S4
0
%
15-130
10
02/15/2110:39
02/17/2110:11
1718-51-0
S4
0
%
18-130
10
02/15/2110:39
02/17/2110:11
13127-88-3
S4
0
%
18-130
10
02/15/2110:39
02/17/2110:11
367-12-4
S4
0
%
18-130
10
02/15/2110:39
02/17/2110:11
118-79-6
S4
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
ND ug/kg 628 202 4 02/11/2114:01 02/15/2119:54 67-64-1
ND ug/kg 31.4 12.5 4 02/11/2114:01 02/15/2119:54 71-43-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 BASE (15.0) Lab ID: 92521577011 Collected: 02/10/21 16:55 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Bromobenzene
ND
ug/kg
31.4
10.2
4
02/11/21 14:01
02/15/21 19:54
108-86-1
Bromochloromethane
ND
ug/kg
31.4
9.3
4
02/11/21 14:01
02/15/21 19:54
74-97-5
Bromodichloromethane
ND
ug/kg
31.4
12.1
4
02/11/21 14:01
02/15/21 19:54
75-27-4
Bromoform
ND
ug/kg
31.4
11.0
4
02/11/21 14:01
02/15/21 19:54
75-25-2
Bromomethane
ND
ug/kg
62.8
49.6
4
02/11/21 14:01
02/15/21 19:54
74-83-9 v1
2-Butanone (MEK)
ND
ug/kg
628
151
4
02/11/21 14:01
02/15/21 19:54
78-93-3
n-Butylbenzene
ND
ug/kg
31.4
14.8
4
02/11/21 14:01
02/15/21 19:54
104-51-8
sec-Butylbenzene
ND
ug/kg
31.4
13.8
4
02/11/21 14:01
02/15/21 19:54
135-98-8
tert-Butyl benzene
ND
ug/kg
31.4
11.2
4
02/11/21 14:01
02/15/21 19:54
98-06-6
Carbon tetrachloride
ND
ug/kg
31.4
11.7
4
02/11/21 14:01
02/15/21 19:54
56-23-5
Chlorobenzene
ND
ug/kg
31.4
6.0
4
02/11/21 14:01
02/15/21 19:54
108-90-7
Chloroethane
ND
ug/kg
62.8
24.2
4
02/11/21 14:01
02/15/21 19:54
75-00-3
Chloroform
ND
ug/kg
31.4
19.1
4
02/11/21 14:01
02/15/21 19:54
67-66-3
Chloromethane
ND
ug/kg
62.8
26.4
4
02/11/21 14:01
02/15/21 19:54
74-87-3
2-Chlorotoluene
ND
ug/kg
31.4
11.1
4
02/11/21 14:01
02/15/21 19:54
95-49-8
4-Chlorotoluene
ND
ug/kg
31.4
5.6
4
02/11/21 14:01
02/15/21 19:54
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
31.4
12.2
4
02/11/21 14:01
02/15/21 19:54
96-12-8
Dibromochloromethane
ND
ug/kg
31.4
17.6
4
02/11/21 14:01
02/15/21 19:54
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
31.4
13.8
4
02/11/21 14:01
02/15/21 19:54
106-93-4
Dibromomethane
ND
ug/kg
31.4
6.7
4
02/11/21 14:01
02/15/21 19:54
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
31.4
11.3
4
02/11/21 14:01
02/15/21 19:54
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
31.4
9.7
4
02/11/21 14:01
02/15/21 19:54
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
31.4
8.2
4
02/11/21 14:01
02/15/21 19:54
106-46-7
Dichlorodifluoromethane
ND
ug/kg
62.8
13.6
4
02/11/21 14:01
02/15/21 19:54
75-71-8
1,1-Dichloroethane
ND
ug/kg
31.4
12.9
4
02/11/21 14:01
02/15/21 19:54
75-34-3
1,2-Dichloroethane
ND
ug/kg
31.4
20.8
4
02/11/21 14:01
02/15/21 19:54
107-06-2
1,1-Dichloroethene
ND
ug/kg
31.4
12.9
4
02/11/21 14:01
02/15/21 19:54
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
31.4
10.7
4
02/11/21 14:01
02/15/21 19:54
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
31.4
11.0
4
02/11/21 14:01
02/15/21 19:54
156-60-5
1,2-Dichloropropane
ND
ug/kg
31.4
9.4
4
02/11/21 14:01
02/15/21 19:54
78-87-5
1,3-Dichloropropane
ND
ug/kg
31.4
9.8
4
02/11/21 14:01
02/15/21 19:54
142-28-9
2,2-Dichloropropane
ND
ug/kg
31.4
10.2
4
02/11/21 14:01
02/15/21 19:54
594-20-7
1,1-Dichloropropene
ND
ug/kg
31.4
15.1
4
02/11/21 14:01
02/15/21 19:54
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
31.4
8.5
4
02/11/21 14:01
02/15/21 19:54
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
31.4
10.8
4
02/11/21 14:01
02/15/21 19:54
10061-02-6
Diisopropyl ether
ND
ug/kg
31.4
8.5
4
02/11/21 14:01
02/15/21 19:54
108-20-3
Ethylbenzene
823
ug/kg
31.4
14.6
4
02/11/21 14:01
02/15/21 19:54
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
62.8
51.4
4
02/11/21 14:01
02/15/21 19:54
87-68-3
2-Hexanone
ND
ug/kg
314
30.3
4
02/11/21 14:01
02/15/21 19:54
591-78-6
Isopropylbenzene (Cumene)
777
ug/kg
31.4
10.7
4
02/11/21 14:01
02/15/21 19:54
98-82-8
p-Isopropyltoluene
8170
ug/kg
31.4
15.4
4
02/11/21 14:01
02/15/21 19:54
99-87-6
Methylene Chloride
ND
ug/kg
126
86.0
4
02/11/21 14:01
02/15/21 19:54
75-09-2
4-Methyl-2-pentanone (MIBK)
404
ug/kg
314
30.3
4
02/11/21 14:01
02/15/21 19:54
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
31.4
11.7
4
02/11/21 14:01
02/15/21 19:54
1634-04-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
Sample: #2 BASE (15.0) Lab ID: 92521577011 Collected: 02/10/21 16:55 Received: 02/11/21 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A/5030B Volatiles
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Date: 02/24/2021 01:57 PM
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
5450
ug/kg
31.4
16.5
4
02/11/2114:01
02/15/2119:54
91-20-3
ND
ug/kg
31.4
11.2
4
02/11/2114:01
02/15/2119:54
103-65-1
ND
ug/kg
31.4
8.3
4
02/11/2114:01
02/15/2119:54
100-42-5
ND
ug/kg
31.4
12.1
4
02/11/2114:01
02/15/2119:54
630-20-6
ND
ug/kg
31.4
8.3
4
02/11/2114:01
02/15/2119:54
79-34-5
ND
ug/kg
31.4
9.9
4
02/11/2114:01
02/15/2119:54
127-18-4
161
ug/kg
31.4
8.9
4
02/11/2114:01
02/15/2119:54
108-88-3
ND
ug/kg
31.4
25.4
4
02/11/2114:01
02/15/2119:54
87-61-6
ND
ug/kg
31.4
26.4
4
02/11/2114:01
02/15/2119:54
120-82-1
ND
ug/kg
31.4
16.3
4
02/11/2114:01
02/15/2119:54
71-55-6
ND
ug/kg
31.4
10.4
4
02/11/2114:01
02/15/2119:54
79-00-5
ND
ug/kg
31.4
8.1
4
02/11/2114:01
02/15/2119:54
79-01-6
ND
ug/kg
31.4
17.3
4
02/11/2114:01
02/15/2119:54
75-69-4
ND
ug/kg
31.4
15.9
4
02/11/2114:01
02/15/2119:54
96-18-4
ND
ug/kg
31.4
8.6
4
02/11/2114:01
02/15/2119:54
95-63-6
6140
ug/kg
31.4
10.5
4
02/11/2114:01
02/15/2119:54
108-67-8
ND
ug/kg
314
22.9
4
02/11/2114:01
02/15/2119:54
108-05-4
ND
ug/kg
62.8
15.9
4
02/11/2114:01
02/15/2119:54
75-01-4
4150
ug/kg
62.8
17.9
4
02/11/2114:01
02/15/2119:54
1330-20-7
521
ug/kg
62.8
21.5
4
02/11/2114:01
02/15/2119:54
179601-23-1
3630
ug/kg
31.4
13.9
4
02/11/2114:01
02/15/2119:54
95-47-6
103
%
70-130
4
02/11/2114:01
02/15/2119:54
2037-26-5 D3
108
%
69-134
4
02/11/2114:01
02/15/2119:54
460-00-4
105
%
70-130
4
02/11/2114:01
02/15/2119:54
17060-07-0
Analytical
Method: SW-846
Pace Analytical Services - Charlotte
19.4
%
0.10
0.10
1
02/11/2114:13
N2
Analytical
Method: SM 2540G Preparation Method:
SM 2540 G
Pace National - Mt. Juliet
82.0
%
1
02/22/2111:28
02/22/2111:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 1621454 Analysis Method: MADEP VPH
QC Batch Method: MADEPV Analysis Description: MADEPV
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92521577008, 92521577009
METHOD BLANK: R3622828-3
Matrix:
Solid
Associated Lab Samples: 92521577008, 92521577009
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Aliphatic (C05-CO8)
mg/kg
1.70J
5.00
1.67
02/14/21 19:50 J
Aliphatic (C09-C12)
mg/kg
ND
5.00
1.67
02/14/21 19:50
Aromatic (C09-C10),Unadjusted
mg/kg
ND
5.00
1.67
02/14/21 19:50
Total VPH
mg/kg
1.70J
5.00
1.67
02/14/21 19:50 J
2,5-Dibromotoluene (FID)
%
85.7
70.0-130
02/14/21 19:50
2,5-Dibromotoluene (PID)
%
71.9
70.0-130
02/14/21 19:50
LABORATORY CONTROL SAMPLE & LCSD:
R3622828-1
R3622828-2
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
60.0
60.1
57.9
100
96.5
70.0-130
3.73
25
Aliphatic (C09-C12)
mg/kg
70.0
83.8
80.0
120
114
70.0-130
4.64
25
Aromatic (C09-C10),Unadjusted
mg/kg
10.0
9.82
9.35
98.2
93.5
70.0-130
4.90
25
Total VPH
mg/kg
140
154
147
110
105
70.0-130
4.65
25
2,5-Dibromotoluene (FID)
%
97.9
93.9
70.0-130
2,5-Dibromotoluene (PID)
%
83.0
80.7
70.0-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 1621956 Analysis Method: MADEP VPH
QC Batch Method: MADEPV Analysis Description: MADEPV
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92521577007, 92521577010, 92521577011
METHOD BLANK: R3623854-3
Matrix:
Solid
Associated Lab Samples: 92521577007, 92521577010,
92521577011
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Aliphatic (C05-CO8)
mg/kg
ND
5.00
1.67
02/21/21 17:00
Aliphatic (C09-C12)
mg/kg
ND
5.00
1.67
02/21/21 17:00
Aromatic (C09-C10),Unadjusted
mg/kg
ND
5.00
1.67
02/21/21 17:00
Total VPH
mg/kg
ND
5.00
1.67
02/21/21 17:00
2,5-Dibromotoluene (FID)
%
96.2
70.0-130
02/21/21 17:00
2,5-Dibromotoluene (PID)
%
99.3
70.0-130
02/21/21 17:00
LABORATORY CONTROL SAMPLE & LCSD:
R3623854-1
R3623854-2
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
60.0
57.9
58.7
96.5
97.8
70.0-130
1.37
25
Aliphatic (C09-C12)
mg/kg
70.0
79.1
79.9
113
114
70.0-130
1.01
25
Aromatic (C09-C10),Unadjusted
mg/kg
10.0
11.9
11.9
119
119
70.0-130
0.00
25
Total VPH
mg/kg
140
149
151
106
108
70.0-130
1.33
25
2,5-Dibromotoluene (FID)
%
110
111
70.0-130
2,5-Dibromotoluene (PID)
%
114
116
70.0-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 33 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 1623520 Analysis Method: MADEP VPH
QC Batch Method: MADEPV Analysis Description: MADEPV
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92521577011
METHOD BLANK: R3624414-3
Matrix:
Solid
Associated Lab Samples: 92521577011
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Aromatic (C09-C10),Unadjusted
mg/kg
ND
5.00
1.67 02/23/21 13:05
2,5-Dibromotoluene (FID)
%
86.8
70.0-130
02/23/21 13:05
2,5-Dibromotoluene (PID)
%
87.4
70.0-130
02/23/21 13:05
LABORATORY CONTROL SAMPLE & LCSD:
R3624414-1
R3624414-2
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aromatic (C09-C10),Unadjusted
mg/kg 10.0
12.6 12.3
126
123
70.0-130 2.41 25
2,5-Dibromotoluene (FID)
%
106
102
70.0-130
2,5-Dibromotoluene (PID)
%
109
105
70.0-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 34 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599422
Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E
Analysis Description: Gasoline Range Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577001
METHOD BLANK: 3160191
Matrix: Solid
Associated Lab Samples: 92521577001
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 6.0 1.1
02/11/21 22:04
4-Bromofluorobenzene (S)
%
87 66-131
02/11/21 22:04
LABORATORY CONTROL SAMPLE:
3160192
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
50 45.3 91
70-130
4-Bromofluorobenzene (S)
%
90
66-131
MATRIX SPIKE SAMPLE:
3160194
92521234002 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 70.2 75.8
98
70-145
4-Bromofluorobenzene (S)
%
100
66-131
SAMPLE DUPLICATE: 3160193
92521234003 Dup
Max
Parameter
Units
Result Result RPD
RPD
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 2.3J
30
4-Bromofluorobenzene (S)
%
93 90
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599699
Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E
Analysis Description: Gasoline Range Organics
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577002, 92521577003,
92521577004, 92521577005, 92521577006
METHOD BLANK: 3161455
Matrix: Solid
Associated Lab Samples: 92521577002, 92521577003,
92521577004, 92521577005, 92521577006
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 6.0 1.1
02/12/21 12:12
4-Bromofluorobenzene (S)
%
86 66-131
02/12/21 12:12
LABORATORY CONTROL SAMPLE:
3161456
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
50.4 49.8 99
70-130
4-Bromofluorobenzene (S)
%
89
66-131
MATRIX SPIKE SAMPLE:
3161458
92521622002 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 68.5 68.4
98
70-145
4-Bromofluorobenzene (S)
%
89
66-131
SAMPLE DUPLICATE: 3161457
92521577006 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Gas Range Organics (C6-C10) mg/kg ND ND 30
4-Bromofluorobenzene (S) % 83 82
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599326 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577001, 92521577002, 92521577003, 92521577004, 92521577005, 92521577006, 92521577007,
92521577008,92521577009
METHOD BLANK: 3159501
Matrix: Solid
Associated Lab Samples: 92521577001, 92521577002, 92521577003, 92521577004, 92521577005, 92521577006, 92521577007,
92521577008,92521577009
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
1.9
02/11/21 10:58
1,1,1-Trichloroethane
ug/kg
ND
5.0
2.6
02/11/21 10:58
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
1.3
02/11/21 10:58
1,1,2-Trichloroethane
ug/kg
ND
5.0
1.7
02/11/21 10:58
1,1-Dichloroethane
ug/kg
ND
5.0
2.1
02/11/21 10:58
1,1-Dichloroethene
ug/kg
ND
5.0
2.1
02/11/21 10:58
1,1-Dichloropropene
ug/kg
ND
5.0
2.4
02/11/21 10:58
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
4.0
02/11/21 10:58
1,2,3-Trichloropropane
ug/kg
ND
5.0
2.5
02/11/21 10:58
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
4.2
02/11/21 10:58
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
1.4
02/11/21 10:58
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
1.9
02/11/21 10:58
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
2.2
02/11/21 10:58
1,2-Dichlorobenzene
ug/kg
ND
5.0
1.8
02/11/21 10:58
1,2-Dichloroethane
ug/kg
ND
5.0
3.3
02/11/21 10:58
1,2-Dichloropropane
ug/kg
ND
5.0
1.5
02/11/21 10:58
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
1.7
02/11/21 10:58
1,3-Dichlorobenzene
ug/kg
ND
5.0
1.6
02/11/21 10:58
1,3-Dichloropropane
ug/kg
ND
5.0
1.6
02/11/21 10:58
1,4-Dichlorobenzene
ug/kg
ND
5.0
1.3
02/11/21 10:58
2,2-Dichloropropane
ug/kg
ND
5.0
1.6
02/11/21 10:58
2-Butanone (MEK)
ug/kg
ND
100
24.0
02/11/21 10:58
2-Chlorotoluene
ug/kg
ND
5.0
1.8
02/11/21 10:58
2-Hexanone
ug/kg
ND
50.0
4.8
02/11/21 10:58
4-Chlorotoluene
ug/kg
ND
5.0
0.88
02/11/21 10:58
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
4.8
02/11/21 10:58
Acetone
ug/kg
ND
100
32.1
02/11/21 10:58
Benzene
ug/kg
ND
5.0
2.0
02/11/21 10:58
Bromobenzene
ug/kg
ND
5.0
1.6
02/11/21 10:58
Bromochloromethane
ug/kg
ND
5.0
1.5
02/11/21 10:58
Bromodichloromethane
ug/kg
ND
5.0
1.9
02/11/21 10:58
Bromoform
ug/kg
ND
5.0
1.8
02/11/21 10:58
Bromomethane
ug/kg
ND
10.0
7.9
02/11/21 10:58
Carbon tetrachloride
ug/kg
ND
5.0
1.9
02/11/21 10:58
Chlorobenzene
ug/kg
ND
5.0
0.96
02/11/21 10:58
Chloroethane
ug/kg
ND
10.0
3.9
02/11/21 10:58
Chloroform
ug/kg
ND
5.0
3.0
02/11/21 10:58
Chloromethane
ug/kg
ND
10.0
4.2
02/11/21 10:58
cis-1,2-Dichloroethene
ug/kg
ND
5.0
1.7
02/11/21 10:58
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
METHOD BLANK: 3159501 Matrix: Solid
Associated Lab Samples: 92521577001, 92521577002, 92521577003, 92521577004, 92521577005, 92521577006, 92521577007,
92521577008,92521577009
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
cis-1,3-Dichloropropene
ug/kg
ND
5.0
1.4
02/11/21 10:58
Dibromochloromethane
ug/kg
ND
5.0
2.8
02/11/21 10:58
Dibromomethane
ug/kg
ND
5.0
1.1
02/11/21 10:58
Dichlorodifluoromethane
ug/kg
ND
10.0
2.2
02/11/21 10:58
Diisopropyl ether
ug/kg
ND
5.0
1.4
02/11/21 10:58
Ethylbenzene
ug/kg
ND
5.0
2.3
02/11/21 10:58
Hexachloro-1,3-butadiene
ug/kg
ND
10.0
8.2
02/11/21 10:58
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
1.7
02/11/21 10:58
m&p-Xylene
ug/kg
ND
10.0
3.4
02/11/21 10:58
Methyl-tert-butyl ether
ug/kg
ND
5.0
1.9
02/11/21 10:58
Methylene Chloride
ug/kg
ND
20.0
13.7
02/11/21 10:58
n-Butylbenzene
ug/kg
ND
5.0
2.4
02/11/21 10:58
n-Propylbenzene
ug/kg
ND
5.0
1.8
02/11/21 10:58
Naphthalene
ug/kg
ND
5.0
2.6
02/11/21 10:58
o-Xylene
ug/kg
ND
5.0
2.2
02/11/21 10:58
p-Isopropyltoluene
ug/kg
ND
5.0
2.5
02/11/21 10:58
sec-Butylbenzene
ug/kg
ND
5.0
2.2
02/11/21 10:58
Styrene
ug/kg
ND
5.0
1.3
02/11/21 10:58
tert-Butyl benzene
ug/kg
ND
5.0
1.8
02/11/21 10:58
Tetrachloroethene
ug/kg
ND
5.0
1.6
02/11/21 10:58
Toluene
ug/kg
ND
5.0
1.4
02/11/21 10:58
trans-1,2-Dichloroethene
ug/kg
ND
5.0
1.8
02/11/21 10:58
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
1.7
02/11/21 10:58
Trichloroethene
ug/kg
ND
5.0
1.3
02/11/21 10:58
Trichlorofluoromethane
ug/kg
ND
5.0
2.8
02/11/21 10:58
Vinyl acetate
ug/kg
ND
50.0
3.6
02/11/21 10:58
Vinyl chloride
ug/kg
ND
10.0
2.5
02/11/21 10:58
Xylene (Total)
ug/kg
ND
10.0
2.8
02/11/21 10:58
1,2-Dichloroethane-d4 (S)
%
103
70-130
02/11/21 10:58
4-Bromofluorobenzene (S)
%
99
69-134
02/11/21 10:58
Toluene-d8 (S)
%
101
70-130
02/11/21 10:58
LABORATORY CONTROL SAMPLE:
3159502
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
1250
1260
101
70-130
1,1,1-Trichloroethane
ug/kg
1250
1290
104
70-130
1,1,2,2-Tetrachloroethane
ug/kg
1250
1240
99
70-130
1,1,2-Trichloroethane
ug/kg
1250
1280
102
70-130
1,1-Dichloroethane
ug/kg
1250
1270
102
70-130
1,1-Dichloroethene
ug/kg
1250
1390
111
70-130
1,1-Dichloropropene
ug/kg
1250
1310
105
70-130
1,2,3-Trichlorobenzene
ug/kg
1250
1240
99
65-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
Parameter
3159502
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,3-Trichloropropane
ug/kg
1250
1210
97
70-130
1,2,4-Trichlorobenzene
ug/kg
1250
1280
102
68-130
1,2,4-Trimethylbenzene
ug/kg
1250
1270
102
70-130
1,2-Dibromo-3-chloropropane
ug/kg
1250
1170
94
70-130
1,2-Dibromoethane (EDB)
ug/kg
1250
1270
101
70-130
1,2-Dichlorobenzene
ug/kg
1250
1240
99
70-130
1,2-Dichloroethane
ug/kg
1250
1200
96
63-130
1,2-Dichloropropane
ug/kg
1250
1260
101
70-130
1,3,5-Trimethylbenzene
ug/kg
1250
1250
100
70-130
1,3-Dichlorobenzene
ug/kg
1250
1220
97
70-130
1,3-Dichloropropane
ug/kg
1250
1260
101
70-130
1,4-Dichlorobenzene
ug/kg
1250
1230
98
70-130
2,2-Dichloropropane
ug/kg
1250
1290
103
66-130
2-Butanone (MEK)
ug/kg
2500
2550
102
70-130
2-Chlorotoluene
ug/kg
1250
1290
103
70-130
2-Hexanone
ug/kg
2500
2480
99
70-130
4-Chlorotoluene
ug/kg
1250
1260
101
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
2500
2490
100
70-130
Acetone
ug/kg
2500
2440
98
69-130
Benzene
ug/kg
1250
1190
95
70-130
Bromobenzene
ug/kg
1250
1270
102
70-130
Bromochloromethane
ug/kg
1250
1140
91
70-130
Bromodichloromethane
ug/kg
1250
1280
102
69-130
Bromoform
ug/kg
1250
1320
105
70-130
Bromomethane
ug/kg
1250
1350
108
52-130
Carbon tetrachloride
ug/kg
1250
1320
106
70-130
Chlorobenzene
ug/kg
1250
1240
99
70-130
Chloroethane
ug/kg
1250
1270
101
65-130
Chloroform
ug/kg
1250
1220
98
70-130
Chloromethane
ug/kg
1250
1150
92
55-130
cis-1,2-Dichloroethene
ug/kg
1250
1240
99
70-130
cis-1,3-Dichloropropene
ug/kg
1250
1290
104
70-130
Dibromochloromethane
ug/kg
1250
1300
104
70-130
Dibromomethane
ug/kg
1250
1190
95
70-130
Dichlorodifluoromethane
ug/kg
1250
1380
111
45-156
Diisopropyl ether
ug/kg
1250
1190
95
70-130
Ethylbenzene
ug/kg
1250
1190
95
70-130
Hexachloro-1,3-butadiene
ug/kg
1250
1170
93
66-130
Isopropylbenzene (Cumene)
ug/kg
1250
1250
100
70-130
m&p-Xylene
ug/kg
2500
2450
98
70-130
Methyl-tert-butyl ether
ug/kg
1250
1240
99
70-130
Methylene Chloride
ug/kg
1250
1100
88
65-130
n-Butylbenzene
ug/kg
1250
1300
104
67-130
n-Propylbenzene
ug/kg
1250
1260
101
70-130
Naphthalene
ug/kg
1250
1280
102
70-130
o-Xylene
ug/kg
1250
1240
99
70-130
p-Isopropyltoluene
ug/kg
1250
1280
102
67-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
3159502
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
sec-Butylbenzene
ug/kg
1250
1240
99
69-130
Styrene
ug/kg
1250
1310
105
70-130
tert-Butyl benzene
ug/kg
1250
1160
92
67-130
Tetrachloroethene
ug/kg
1250
1220
98
70-130
Toluene
ug/kg
1250
1230
99
70-130
trans-1,2-Dichloroethene
ug/kg
1250
1260
101
70-130
trans- 1,3-Dichloropropene
ug/kg
1250
1300
104
68-130
Trichloroethene
ug/kg
1250
1310
105
70-130
Trichlorofluoromethane
ug/kg
1250
1280
102
70-130
Vinyl acetate
ug/kg
2500
2730
109
70-130
Vinyl chloride
ug/kg
1250
1240
99
61-130
Xylene (Total)
ug/kg
3750
3690
98
70-130
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
99
69-134
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3159503
3159504
MS
MSD
92521080001
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
1, 1, 1,2-Tetrachloroethane
ug/kg
ND
10100
10100
10900
11100
108
110
70-131
2
30
1,1,1-Trichloroethane
ug/kg
ND
10100
10100
11100
11600
110
114
65-133
4
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
10100
10100
10100
10400
100
103
66-130
3
30
1,1,2-Trichloroethane
ug/kg
ND
10100
10100
10800
11500
106
113
66-133
6
30
1,1-Dichloroethane
ug/kg
ND
10100
10100
10700
11000
106
109
65-130
3
30
1,1-Dichloroethene
ug/kg
ND
10100
10100
12000
12100
118
119
10-158
1
30
1,1-Dichloropropene
ug/kg
ND
10100
10100
11200
11600
110
114
68-133
3
30
1,2,3-Trichlorobenzene
ug/kg
ND
10100
10100
10500
10900
103
108
27-138
4
30
1,2,3-Trichloropropane
ug/kg
ND
10100
10100
9680
9740
96
96
67-130
1
30
1,2,4-Trichlorobenzene
ug/kg
ND
10100
10100
11100
11500
109
113
51-134
3
30
1,2,4-Trimethyl benzene
ug/kg
90700
10100
10100
112000
114000
206
235
63-136
3
30 E,M1
1,2-Dibromo-3-
ug/kg
ND
10100
10100
9580
9600
95
95
32-130
0
30
chloropropane
1,2-Dibromoethane (EDB)
ug/kg
ND
10100
10100
10700
10800
105
107
70-130
1
30
1,2-Dichlorobenzene
ug/kg
ND
10100
10100
10300
10700
102
106
69-130
4
30
1,2-Dichloroethane
ug/kg
ND
10100
10100
9960
10300
98
102
59-130
3
30
1,2-Dichloropropane
ug/kg
ND
10100
10100
10900
11200
108
111
70-130
3
30
1,3,5-Trimethyl benzene
ug/kg
29400
10100
10100
37000
37100
75
76
65-137
0
30
1,3-Dichlorobenzene
ug/kg
ND
10100
10100
10600
10800
105
107
70-130
2
30
1,3-Dichloropropane
ug/kg
ND
10100
10100
10400
10500
103
103
70-130
1
30
1,4-Dichlorobenzene
ug/kg
ND
10100
10100
10500
10800
104
107
68-130
2
30
2,2-Dichloropropane
ug/kg
ND
10100
10100
10100
10700
100
106
32-130
6
30
2-Butanone (MEK)
ug/kg
ND
20200
20200
20000
20700
92
95
10-136
3
30
2-Chlorotoluene
ug/kg
ND
10100
10100
13300
13400
131
132
69-141
1
30
2-Hexanone
ug/kg
ND
20200
20200
26500
29900
131
147
10-144
12
30 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3159503
3159504
MS
MSD
92521080001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
4-Chlorotoluene
ug/kg
ND
10100
10100
10800
11900
106
117
70-132
10
30
4-Methyl-2-pentanone
ug/kg
ND
20200
20200
26700
36500
130
179
25-143
31
30 M1,R1
(MIBK)
Acetone
ug/kg
153000
20200
20200
165000
171000
57
85
10-130
3
30
Benzene
ug/kg
9030
10100
10100
19900
19900
107
108
67-130
0
30
Bromobenzene
ug/kg
ND
10100
10100
10800
11000
106
109
70-130
2
30
Bromochloromethane
ug/kg
ND
10100
10100
9790
9990
97
99
69-134
2
30
Bromodichloromethane
ug/kg
ND
10100
10100
10800
10900
107
108
64-130
1
30
Bromoform
ug/kg
ND
10100
10100
10600
10800
104
107
62-130
3
30
Bromomethane
ug/kg
ND
10100
10100
12000
11600
118
115
20-176
3
30
Carbon tetrachloride
ug/kg
ND
10100
10100
11600
11600
114
115
65-140
1
30
Chlorobenzene
ug/kg
ND
10100
10100
10700
10900
105
108
70-130
2
30
Chloroethane
ug/kg
ND
10100
10100
9930
10200
98
100
10-130
2
30
Chloroform
ug/kg
ND
10100
10100
10100
10600
100
105
63-130
5
30
Chloromethane
ug/kg
ND
10100
10100
9970
10400
98
102
58-130
4
30
cis-1,2-Dichloroethene
ug/kg
ND
10100
10100
10400
10800
103
106
66-130
4
30
cis-1,3-Dichloropropene
ug/kg
ND
10100
10100
10800
10800
106
106
67-130
0
30
Dibromochloromethane
ug/kg
ND
10100
10100
11000
11400
109
113
67-130
4
30
Dibromomethane
ug/kg
ND
10100
10100
10000
10400
99
103
63-131
4
30
Dichlorodifluoromethane
ug/kg
ND
10100
10100
12500
12500
124
124
44-180
0
30
Diisopropyl ether
ug/kg
ND
10100
10100
9520
9830
94
97
63-130
3
30
Ethylbenzene
ug/kg
214
10100
10100
10500
10600
101
103
66-130
1
30
Hexachloro-1,3-butadiene
ug/kg
ND
10100
10100
14400
14500
142
143
64-150
0
30
Isopropylbenzene
ug/kg
1450
10100
10100
12400
12500
108
110
69-135
2
30
(Cumene)
m&p-Xylene
ug/kg
633
20200
20200
21700
21900
104
105
60-133
1
30
Methyl-tert-butyl ether
ug/kg
ND
10100
10100
9890
10300
98
102
65-130
4
30
Methylene Chloride
ug/kg
ND
10100
10100
9080
9490
87
91
61-130
4
30
n-Butylbenzene
ug/kg
3980
10100
10100
17200
17700
131
136
65-140
3
30
n-Propylbenzene
ug/kg
12400
10100
10100
23200
23700
106
111
67-140
2
30
Naphthalene
ug/kg
82000
10100
10100
95100
97700
129
155
15-145
3
30 M1
o-Xylene
ug/kg
1410
10100
10100
12100
12500
106
110
66-133
3
30
p-Isopropyltoluene
ug/kg
3820
10100
10100
15300
15400
114
114
56-147
0
30
sec-Butylbenzene
ug/kg
ND
10100
10100
12500
13500
123
133
65-139
8
30
Styrene
ug/kg
314
10100
10100
11800
11700
113
113
70-132
0
30
tert-Butylbenzene
ug/kg
ND
10100
10100
11500
11600
113
115
62-135
1
30
Tetrachloroethene
ug/kg
ND
10100
10100
10700
10800
106
106
70-135
0
30
Toluene
ug/kg
579
10100
10100
11400
11300
107
106
67-130
1
30
trans-1,2-Dichloroethene
ug/kg
ND
10100
10100
10900
11200
107
110
69-130
3
30
trans-1,3-Dichloropropene
ug/kg
ND
10100
10100
11000
11300
108
111
62-130
3
30
Trichloroethene
ug/kg
ND
10100
10100
11700
11800
116
116
70-135
1
30
Trichlorofluoromethane
ug/kg
ND
10100
10100
11600
12100
114
120
10-130
5
30
Vinyl acetate
ug/kg
ND
20200
20200
21100
22100
104
109
53-130
5
30
Vinyl chloride
ug/kg
ND
10100
10100
11200
11600
110
114
61-148
4
30
Xylene (Total)
ug/kg
2040
30300
30300
33900
34400
105
107
63-132
2
30
1,2-Dichloroethane-d4 (S)
%
94
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 41 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3159503 3159504
MS MSD
92521080001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
4-Bromofluorobenzene (S) % 98 98 69-134
Toluene-d8 (S) % 100 100 70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 42 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599428 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577010, 92521577011
METHOD BLANK: 3160220
Associated Lab Samples: 92521577010, 92521577011
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
1.9
02/15/21 12:22
1,1,1-Trichloroethane
ug/kg
ND
5.0
2.6
02/15/21 12:22
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
1.3
02/15/21 12:22
1,1,2-Trichloroethane
ug/kg
ND
5.0
1.7
02/15/21 12:22
1,1-Dichloroethane
ug/kg
ND
5.0
2.1
02/15/21 12:22
1,1-Dichloroethene
ug/kg
ND
5.0
2.1
02/15/21 12:22
1,1-Dichloropropene
ug/kg
ND
5.0
2.4
02/15/21 12:22
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
4.0
02/15/21 12:22
1,2,3-Trichloropropane
ug/kg
ND
5.0
2.5
02/15/21 12:22
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
4.2
02/15/21 12:22
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
1.4
02/15/21 12:22
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
1.9
02/15/21 12:22
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
2.2
02/15/21 12:22
1,2-Dichlorobenzene
ug/kg
ND
5.0
1.8
02/15/21 12:22
1,2-Dichloroethane
ug/kg
ND
5.0
3.3
02/15/21 12:22
1,2-Dichloropropane
ug/kg
ND
5.0
1.5
02/15/21 12:22
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
1.7
02/15/21 12:22
1,3-Dichlorobenzene
ug/kg
ND
5.0
1.6
02/15/21 12:22
1,3-Dichloropropane
ug/kg
ND
5.0
1.6
02/15/21 12:22
1,4-Dichlorobenzene
ug/kg
ND
5.0
1.3
02/15/21 12:22
2,2-Dichloropropane
ug/kg
ND
5.0
1.6
02/15/21 12:22
2-Butanone (MEK)
ug/kg
ND
100
24.0
02/15/21 12:22
2-Chlorotoluene
ug/kg
ND
5.0
1.8
02/15/21 12:22
2-Hexanone
ug/kg
ND
50.0
4.8
02/15/21 12:22
4-Chlorotoluene
ug/kg
ND
5.0
0.88
02/15/21 12:22
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
4.8
02/15/21 12:22
Acetone
ug/kg
ND
100
32.1
02/15/21 12:22
Benzene
ug/kg
ND
5.0
2.0
02/15/21 12:22
Bromobenzene
ug/kg
ND
5.0
1.6
02/15/21 12:22
Bromochloromethane
ug/kg
ND
5.0
1.5
02/15/21 12:22
Bromodichloromethane
ug/kg
ND
5.0
1.9
02/15/21 12:22
Bromoform
ug/kg
ND
5.0
1.8
02/15/21 12:22
Bromomethane
ug/kg
ND
10.0
7.9
02/15/21 12:22 v1
Carbon tetrachloride
ug/kg
ND
5.0
1.9
02/15/21 12:22
Chlorobenzene
ug/kg
ND
5.0
0.96
02/15/21 12:22
Chloroethane
ug/kg
ND
10.0
3.9
02/15/21 12:22
Chloroform
ug/kg
ND
5.0
3.0
02/15/21 12:22
Chloromethane
ug/kg
ND
10.0
4.2
02/15/21 12:22
cis-1,2-Dichloroethene
ug/kg
ND
5.0
1.7
02/15/21 12:22
cis-1,3-Dichloropropene
ug/kg
ND
5.0
1.4
02/15/21 12:22
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
METHOD BLANK: 3160220
Associated Lab Samples: 92521577010, 92521577011
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromochloromethane
ug/kg
ND
5.0
2.8
02/15/21 12:22
Dibromomethane
ug/kg
ND
5.0
1.1
02/15/21 12:22
Dichlorodifluoromethane
ug/kg
ND
10.0
2.2
02/15/21 12:22
Diisopropyl ether
ug/kg
ND
5.0
1.4
02/15/21 12:22
Ethylbenzene
ug/kg
ND
5.0
2.3
02/15/21 12:22
Hexachloro-1,3-butadiene
ug/kg
ND
10.0
8.2
02/15/21 12:22
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
1.7
02/15/21 12:22
m&p-Xylene
ug/kg
ND
10.0
3.4
02/15/21 12:22
Methyl-tert-butyl ether
ug/kg
ND
5.0
1.9
02/15/21 12:22
Methylene Chloride
ug/kg
ND
20.0
13.7
02/15/21 12:22
n-Butylbenzene
ug/kg
ND
5.0
2.4
02/15/21 12:22
n-Propylbenzene
ug/kg
ND
5.0
1.8
02/15/21 12:22
Naphthalene
ug/kg
ND
5.0
2.6
02/15/21 12:22
o-Xylene
ug/kg
ND
5.0
2.2
02/15/21 12:22
p-Isopropyltoluene
ug/kg
ND
5.0
2.5
02/15/21 12:22
sec-Butylbenzene
ug/kg
ND
5.0
2.2
02/15/21 12:22
Styrene
ug/kg
ND
5.0
1.3
02/15/21 12:22
tert-Butyl benzene
ug/kg
ND
5.0
1.8
02/15/21 12:22
Tetrachloroethene
ug/kg
ND
5.0
1.6
02/15/21 12:22
Toluene
ug/kg
ND
5.0
1.4
02/15/21 12:22
trans-1,2-Dichloroethene
ug/kg
ND
5.0
1.8
02/15/21 12:22
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
1.7
02/15/21 12:22
Trichloroethene
ug/kg
ND
5.0
1.3
02/15/21 12:22
Trichlorofluoromethane
ug/kg
ND
5.0
2.8
02/15/21 12:22
Vinyl acetate
ug/kg
ND
50.0
3.6
02/15/21 12:22
Vinyl chloride
ug/kg
ND
10.0
2.5
02/15/21 12:22
Xylene (Total)
ug/kg
ND
10.0
2.8
02/15/21 12:22
1,2-Dichloroethane-d4 (S)
%
108
70-130
02/15/21 12:22
4-Bromofluorobenzene (S)
%
100
69-134
02/15/21 12:22
Toluene-d8 (S)
%
99
70-130
02/15/21 12:22
Qualifiers
LABORATORY CONTROL SAMPLE:
3160221
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
1250
1210
97
70-130
1,1,1-Trichloroethane
ug/kg
1250
1240
99
70-130
1,1,2,2-Tetrachloroethane
ug/kg
1250
1140
91
70-130
1,1,2-Trichloroethane
ug/kg
1250
1170
93
70-130
1,1-Dichloroethane
ug/kg
1250
1190
95
70-130
1,1-Dichloroethene
ug/kg
1250
1270
102
70-130
1,1-Dichloropropene
ug/kg
1250
1220
97
70-130
1,2,3-Trichlorobenzene
ug/kg
1250
1150
92
65-130
1,2,3-Trichloropropane
ug/kg
1250
1110
89
70-130
1,2,4-Trichlorobenzene
ug/kg
1250
1170
94
68-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
Parameter
3160221
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trimethylbenzene
ug/kg
1250
1150
92
70-130
1,2-Dibromo-3-chloropropane
ug/kg
1250
1110
89
70-130
1,2-Dibromoethane (EDB)
ug/kg
1250
1190
95
70-130
1,2-Dichlorobenzene
ug/kg
1250
1130
91
70-130
1,2-Dichloroethane
ug/kg
1250
1150
92
63-130
1,2-Dichloropropane
ug/kg
1250
1150
92
70-130
1,3,5-Trimethylbenzene
ug/kg
1250
1140
91
70-130
1,3-Dichlorobenzene
ug/kg
1250
1140
91
70-130
1,3-Dichloropropane
ug/kg
1250
1150
92
70-130
1,4-Dichlorobenzene
ug/kg
1250
1150
92
70-130
2,2-Dichloropropane
ug/kg
1250
1230
98
66-130
2-Butanone (MEK)
ug/kg
2500
2330
93
70-130
2-Chlorotoluene
ug/kg
1250
1190
95
70-130
2-Hexanone
ug/kg
2500
2240
89
70-130
4-Chlorotoluene
ug/kg
1250
1160
93
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
2500
2220
89
70-130
Acetone
ug/kg
2500
2220
89
69-130
Benzene
ug/kg
1250
1090
87
70-130
Bromobenzene
ug/kg
1250
1190
95
70-130
Bromochloromethane
ug/kg
1250
1090
87
70-130
Bromodichloromethane
ug/kg
1250
1200
96
69-130
Bromoform
ug/kg
1250
1290
103
70-130
Bromomethane
ug/kg
1250
1490
119
52-130 v1
Carbon tetrachloride
ug/kg
1250
1240
99
70-130
Chlorobenzene
ug/kg
1250
1160
93
70-130
Chloroethane
ug/kg
1250
1160
93
65-130
Chloroform
ug/kg
1250
1130
91
70-130
Chloromethane
ug/kg
1250
1060
84
55-130
cis-1,2-Dichloroethene
ug/kg
1250
1150
92
70-130
cis-1,3-Dichloropropene
ug/kg
1250
1170
94
70-130
Dibromochloromethane
ug/kg
1250
1260
101
70-130
Dibromomethane
ug/kg
1250
1140
91
70-130
Dichlorodifluoromethane
ug/kg
1250
1240
99
45-156
Diisopropyl ether
ug/kg
1250
1100
88
70-130
Ethylbenzene
ug/kg
1250
1100
88
70-130
Hexachloro-1,3-butadiene
ug/kg
1250
1070
86
66-130
Isopropylbenzene (Cumene)
ug/kg
1250
1150
92
70-130
m&p-Xylene
ug/kg
2500
2250
90
70-130
Methyl-tert-butyl ether
ug/kg
1250
1140
91
70-130
Methylene Chloride
ug/kg
1250
1010
81
65-130
n-Butylbenzene
ug/kg
1250
1150
92
67-130
n-Propylbenzene
ug/kg
1250
1120
90
70-130
Naphthalene
ug/kg
1250
1170
93
70-130
o-Xylene
ug/kg
1250
1150
92
70-130
p-Isopropyltoluene
ug/kg
1250
1160
93
67-130
sec-Butylbenzene
ug/kg
1250
1110
89
69-130
Styrene
ug/kg
1250
1230
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
Parameter
3160221
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
tert-Butyl benzene
ug/kg
1250
1100
88
67-130
Tetrachloroethene
ug/kg
1250
1150
92
70-130
Toluene
ug/kg
1250
1120
90
70-130
trans-1,2-Dichloroethene
ug/kg
1250
1160
93
70-130
trans- 1,3-Dichloropropene
ug/kg
1250
1190
96
68-130
Trichloroethene
ug/kg
1250
1220
98
70-130
Trichlorofluoromethane
ug/kg
1250
1260
101
70-130
Vinyl acetate
ug/kg
2500
2450
98
70-130
Vinyl chloride
ug/kg
1250
1120
90
61-130
Xylene (Total)
ug/kg
3750
3400
91
70-130
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
100
69-134
Toluene-d8 (S)
%
99
70-130
MATRIX SPIKE SAMPLE:
Parameter
3160223
Units
92521639001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
637
788
124
70-131
1,1,1-Trichloroethane
ug/kg
ND
637
747
117
65-133
1,1,2,2-Tetrachloroethane
ug/kg
ND
637
657
103
66-130
1,1,2-Trichloroethane
ug/kg
ND
637
683
107
66-133
1,1-Dichloroethane
ug/kg
ND
637
688
108
65-130
1,1-Dichloroethene
ug/kg
ND
637
747
117
10-158
1,1-Dichloropropene
ug/kg
ND
637
691
109
68-133
1,2,3-Trichlorobenzene
ug/kg
ND
637
634
100
27-138
1,2,3-Trichloropropane
ug/kg
ND
637
539
85
67-130
1,2,4-Trichlorobenzene
ug/kg
ND
637
625
98
51-134
1,2,4-Trimethylbenzene
ug/kg
ND
637
643
101
63-136
1,2-Dibromo-3-chloropropane
ug/kg
ND
637
611
96
32-130
1,2-Dibromoethane (EDB)
ug/kg
ND
637
687
108
70-130
1,2-Dichlorobenzene
ug/kg
ND
637
635
100
69-130
1,2-Dichloroethane
ug/kg
ND
637
674
106
59-130
1,2-Dichloropropane
ug/kg
ND
637
700
110
70-130
1,3,5-Trimethylbenzene
ug/kg
ND
637
638
100
65-137
1,3-Dichlorobenzene
ug/kg
ND
637
624
98
70-130
1,3-Dichloropropane
ug/kg
ND
637
671
105
70-130
1,4-Dichlorobenzene
ug/kg
ND
637
612
96
68-130
2,2-Dichloropropane
ug/kg
ND
637
224
35
32-130
2-Butanone (MEK)
ug/kg
ND
1270
1170
92
10-136
2-Chlorotoluene
ug/kg
ND
637
647
102
69-141
2-Hexanone
ug/kg
ND
1270
1160
91
10-144
4-Chlorotoluene
ug/kg
ND
637
607
95
70-132
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
1270
1230
96
25-143
Acetone
ug/kg
ND
1270
1250
98
10-130
Benzene
ug/kg
ND
637
658
103
67-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
MATRIX SPIKE SAMPLE:
3160223
92521639001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromobenzene
ug/kg
ND
637
655
103
70-130
Bromochloromethane
ug/kg
ND
637
636
100
69-134
Bromodichloromethane
ug/kg
ND
637
691
109
64-130
Bromoform
ug/kg
ND
637
661
104
62-130
Bromomethane
ug/kg
ND
637
768
121
20-176 v1
Carbon tetrachloride
ug/kg
ND
637
704
111
65-140
Chlorobenzene
ug/kg
ND
637
661
104
70-130
Chloroethane
ug/kg
ND
637
186
29
10-130
Chloroform
ug/kg
ND
637
671
105
63-130
Chloromethane
ug/kg
ND
637
671
105
58-130
cis-1,2-Dichloroethene
ug/kg
ND
637
674
106
66-130
cis-1,3-Dichloropropene
ug/kg
ND
637
534
84
67-130
Dibromochloromethane
ug/kg
ND
637
721
113
67-130
Dibromomethane
ug/kg
ND
637
648
102
63-131
Dichlorodifluoromethane
ug/kg
ND
637
700
110
44-180
Diisopropyl ether
ug/kg
ND
637
635
100
63-130
Ethylbenzene
ug/kg
ND
637
644
101
66-130
Hexachloro-1,3-butadiene
ug/kg
ND
637
529
83
64-150
Isopropylbenzene (Cumene)
ug/kg
ND
637
695
109
69-135
m&p-Xylene
ug/kg
ND
1270
1330
105
60-133
Methyl-tert-butyl ether
ug/kg
47.1
637
697
102
65-130
Methylene Chloride
ug/kg
ND
637
616
97
61-130
n-Butylbenzene
ug/kg
ND
637
590
93
65-140
n-Propylbenzene
ug/kg
ND
637
630
99
67-140
Naphthalene
ug/kg
ND
637
699
110
15-145
o-Xylene
ug/kg
ND
637
708
111
66-133
p-Isopropyltoluene
ug/kg
ND
637
636
100
56-147
sec-Butylbenzene
ug/kg
ND
637
631
99
65-139
Styrene
ug/kg
ND
637
720
113
70-132
tert-Butyl benzene
ug/kg
ND
637
628
99
62-135
Tetrachloroethene
ug/kg
ND
637
618
97
70-135
Toluene
ug/kg
ND
637
702
110
67-130
trans-1,2-Dichloroethene
ug/kg
ND
637
633
99
69-130
trans- 1,3-Dichloropropene
ug/kg
ND
637
787
124
62-130
Trichloroethene
ug/kg
ND
637
711
112
70-135
Trichlorofluoromethane
ug/kg
ND
637
267
42
10-130
Vinyl acetate
ug/kg
ND
1270
1070
84
53-130
Vinyl chloride
ug/kg
ND
637
698
110
61-148
Xylene (Total)
ug/kg
ND
1910
2040
107
63-132
1,2-Dichloroethane-d4 (S)
%
104
70-130
4-Bromofluorobenzene (S)
%
101
69-134
Toluene-d8 (S)
%
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 65

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
SAMPLE DUPLICATE: 3160222
Parameter
Units
92521577010
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,1-Trichloroethane
ug/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,2-Trichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethene
ug/kg
ND
ND
30
1,1-Dichloropropene
ug/kg
ND
ND
30
1,2,3-Trichlorobenzene
ug/kg
ND
ND
30
1,2,3-Trichloropropane
ug/kg
ND
ND
30
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2,4-Trimethylbenzene
ug/kg
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
30
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,2-Dichloroethane
ug/kg
ND
ND
30
1,2-Dichloropropane
ug/kg
ND
ND
30
1,3,5-Trimethylbenzene
ug/kg
5.1J
5.9J
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichloropropane
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
2,2-Dichloropropane
ug/kg
ND
ND
30
2-Butanone (MEK)
ug/kg
ND
ND
30
2-Chlorotoluene
ug/kg
ND
ND
30
2-Hexanone
ug/kg
ND
ND
30
4-Chlorotoluene
ug/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
30
Acetone
ug/kg
ND
ND
30
Benzene
ug/kg
ND
ND
30
Bromobenzene
ug/kg
ND
ND
30
Bromochloromethane
ug/kg
ND
ND
30
Bromodichloromethane
ug/kg
ND
ND
30
Bromoform
ug/kg
ND
ND
30
Bromomethane
ug/kg
ND
ND
30 v1
Carbon tetrachloride
ug/kg
ND
ND
30
Chlorobenzene
ug/kg
ND
ND
30
Chloroethane
ug/kg
ND
ND
30
Chloroform
ug/kg
ND
ND
30
Chloromethane
ug/kg
ND
ND
30
cis-1,2-Dichloroethene
ug/kg
ND
ND
30
cis-1,3-Dichloropropene
ug/kg
ND
ND
30
Dibromochloromethane
ug/kg
ND
ND
30
Dibromomethane
ug/kg
ND
ND
30
Dichlorodifluoromethane
ug/kg
ND
ND
30
Diisopropyl ether
ug/kg
ND
ND
30
Ethylbenzene
ug/kg
ND
ND
30
Hexachloro-1,3-butadiene
ug/kg
ND
ND
30
Isopropylbenzene (Cumene)
ug/kg
ND
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
SAMPLE DUPLICATE: 3160222
Parameter
Units
92521577010
Result
Dup
Result
m&p-Xylene
ug/kg
ND
ND
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
ND
ND
p-Isopropyltoluene
ug/kg
ND
ND
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
ND
ND
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
106
106
4-Bromofluorobenzene (S)
%
103
102
Toluene-d8(S)
%
102
101
Max
RPD RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 49 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599380
Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546
Analysis Description: 8015 Solid GCSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577001, 92521577002,
92521577003, 92521577004, 92521577005, 92521577006
METHOD BLANK: 3159913
Matrix: Solid
Associated Lab Samples: 92521577001, 92521577002,
92521577003, 92521577004, 92521577005, 92521577006
Blank Reporting
Parameter
Units
Result Limit MDL Analyzed
Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND 4.9 2.3 02/12/21 11:09
n-Pentacosane (S)
%
79 32-130 02/12/21 11:09
LABORATORY CONTROL SAMPLE:
3159914
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
67.1 41.7 62 47-130
n-Pentacosane (S)
%
100 32-130
MATRIX SPIKE SAMPLE:
3159915
92521577001 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
3040 87.2 3260 259
10-133 M1
n-Pentacosane (S)
%
96
32-130
SAMPLE DUPLICATE: 3159916
92521577002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Diesel Range Organics(C10-C28) mg/kg 2040 1500 30 30
n-Pentacosane (S) % 0 66
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 50 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599953 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
METHOD BLANK: 3162680 Matrix: Solid
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
328
75.1
02/16/21 08:54
1,2-Dichlorobenzene
ug/kg
ND
328
70.9
02/16/21 08:54
1,3-Dichlorobenzene
ug/kg
ND
328
73.8
02/16/21 08:54
1,4-Dichlorobenzene
ug/kg
ND
328
72.1
02/16/21 08:54
1-Methylnaphthalene
ug/kg
ND
328
87.3
02/16/21 08:54
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
328
91.1
02/16/21 08:54
2,4,5-Trichlorophenol
ug/kg
ND
328
85.1
02/16/21 08:54
2,4,6-Trichlorophenol
ug/kg
ND
328
82.4
02/16/21 08:54
2,4-Dichlorophenol
ug/kg
ND
328
108
02/16/21 08:54
2,4-Dimethylphenol
ug/kg
ND
328
81.7
02/16/21 08:54
2,4-Dinitrophenol
ug/kg
ND
1640
1050
02/16/21 08:54
2,4-Dinitrotoluene
ug/kg
ND
328
86.8
02/16/21 08:54
2,6-Dinitrotoluene
ug/kg
ND
328
85.7
02/16/21 08:54
2-Chloronaphthalene
ug/kg
ND
328
73.0
02/16/21 08:54
2-Chlorophenol
ug/kg
ND
328
76.3
02/16/21 08:54
2-Methylnaphthalene
ug/kg
ND
328
83.4
02/16/21 08:54
2-Methylphenol(o-Cresol)
ug/kg
ND
328
72.6
02/16/21 08:54
2-Nitroaniline
ug/kg
ND
1640
165
02/16/21 08:54
2-Nitrophenol
ug/kg
ND
328
101
02/16/21 08:54
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
328
82.5
02/16/21 08:54
3,3'-Dichlorobenzidine
ug/kg
ND
656
228
02/16/21 08:54
3-Nitroaniline
ug/kg
ND
1640
174
02/16/21 08:54
4,6-Dinitro-2-methyl phenol
ug/kg
ND
656
528
02/16/21 08:54
4-Bromophenylphenyl ether
ug/kg
ND
328
86.0
02/16/21 08:54
4-ChIoro-3-methyl phenol
ug/kg
ND
656
200
02/16/21 08:54
4-Chloroaniline
ug/kg
ND
656
201
02/16/21 08:54
4-Chlorophenylphenyl ether
ug/kg
ND
328
85.1
02/16/21 08:54
4-Nitroaniline
ug/kg
ND
656
162
02/16/21 08:54
4-Nitrophenol
ug/kg
ND
1640
523
02/16/21 08:54
Acenaphthene
ug/kg
ND
328
84.3
02/16/21 08:54
Acenaphthylene
ug/kg
ND
328
77.6
02/16/21 08:54
Aniline
ug/kg
ND
328
73.6
02/16/21 08:54
Anthracene
ug/kg
ND
328
85.0
02/16/21 08:54
Benzo(a)anthracene
ug/kg
ND
328
104
02/16/21 08:54
Benzo(a)pyrene
ug/kg
ND
328
142
02/16/21 08:54
Benzo(b)fluoranthene
ug/kg
ND
328
132
02/16/21 08:54
Benzo(g,h,i)perylene
ug/kg
ND
328
128
02/16/21 08:54
Benzo(k)fluoranthene
ug/kg
ND
328
138
02/16/21 08:54
Benzoic Acid
ug/kg
ND
1640
354
02/16/21 08:54
Benzyl alcohol
ug/kg
ND
656
174
02/16/21 08:54
IL
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
METHOD BLANK: 3162680 Matrix: Solid
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
bis(2-Chloroethoxy)methane
ug/kg
ND
328
87.5
02/16/21 08:54
bis(2-Chloroethyl) ether
ug/kg
ND
328
69.6
02/16/21 08:54
bis(2-Ethylhexyl)phthalate
ug/kg
ND
328
107
02/16/21 08:54
Butylbenzylphthalate
ug/kg
ND
328
87.3
02/16/21 08:54
Chrysene
ug/kg
ND
328
95.2
02/16/21 08:54
Di-n-butylphthalate
ug/kg
ND
328
80.9
02/16/21 08:54
Di-n-octylphthalate
ug/kg
ND
328
187
02/16/21 08:54
Dibenz(a,h)anthracene
ug/kg
ND
328
131
02/16/21 08:54
Dibenzofuran
ug/kg
ND
328
82.0
02/16/21 08:54
Diethylphthalate
ug/kg
ND
328
71.1
02/16/21 08:54
Dimethylphthalate
ug/kg
ND
328
74.1
02/16/21 08:54
Fluoranthene
ug/kg
ND
328
99.0
02/16/21 08:54
Fluorene
ug/kg
ND
328
87.7
02/16/21 08:54
Hexachloro-1,3-butadiene
ug/kg
ND
328
79.7
02/16/21 08:54
Hexachlorobenzene
ug/kg
ND
328
83.2
02/16/21 08:54
Hexachlorocyclopentadiene
ug/kg
ND
328
131
02/16/21 08:54
Hexachloroethane
ug/kg
ND
328
74.7
02/16/21 08:54
Indeno(1,2,3-cd)pyrene
ug/kg
ND
328
150
02/16/21 08:54
Isophorone
ug/kg
ND
328
71.2
02/16/21 08:54
N-Nitroso-di-n-propylamine
ug/kg
ND
328
91.8
02/16/21 08:54
N-Nitrosodimethylamine
ug/kg
ND
328
92.2
02/16/21 08:54
N-Nitrosodiphenylamine
ug/kg
ND
328
83.6
02/16/21 08:54
Naphthalene
ug/kg
ND
328
78.5
02/16/21 08:54
Nitrobenzene
ug/kg
ND
328
78.3
02/16/21 08:54
Pentachlorophenol
ug/kg
ND
656
150
02/16/21 08:54
Phenanthrene
ug/kg
ND
328
82.5
02/16/21 08:54
Phenol
ug/kg
ND
328
78.3
02/16/21 08:54
Pyrene
ug/kg
ND
328
90.2
02/16/21 08:54
Pyridine
ug/kg
ND
328
82.9
02/16/21 08:54
2,4,6-Tribromophenol (S)
%
85
18-130
02/16/21 08:54
2-Fluorobiphenyl (S)
%
73
19-130
02/16/21 08:54
2-Fluorophenol (S)
%
69
18-130
02/16/21 08:54
Nitrobenzene-d5 (S)
%
80
21-130
02/16/21 08:54
Phenol-d6 (S)
%
71
18-130
02/16/21 08:54
Terphenyl-d14 (S)
%
102
15-130
02/16/21 08:54
Qualifiers
LABORATORY CONTROL SAMPLE:
3162681
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1640
1470
89
47-130
1,2-Dichlorobenzene
ug/kg
1640
1380
84
49-130
1,3-Dichlorobenzene
ug/kg
1640
1350
82
48-130
1,4-Dichlorobenzene
ug/kg
1640
1370
84
49-130
1-Methylnaphthalene
ug/kg
1640
1380
84
54-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
Parameter
3162681
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,2'-Oxybis(1-chloropropane)
ug/kg
1640
1440
87
38-130
2,4,5-Trichlorophenol
ug/kg
1640
1400
85
49-130
2,4,6-Trichlorophenol
ug/kg
1640
1430
87
50-130
2,4-Dichlorophenol
ug/kg
1640
1480
90
51-130
2,4-Dimethylphenol
ug/kg
1640
1550
94
53-130
2,4-Dinitrophenol
ug/kg
8220
6530
79
39-130
2,4-Dinitrotoluene
ug/kg
1640
1470
89
53-130
2,6-Dinitrotoluene
ug/kg
1640
1470
89
55-130
2-Chloronaphthalene
ug/kg
1640
1360
83
48-130
2-Chlorophenol
ug/kg
1640
1350
82
54-130
2-Methylnaphthalene
ug/kg
1640
1410
86
57-130
2-Methylphenol(o-Cresol)
ug/kg
1640
1290
78
50-130
2-Nitroaniline
ug/kg
3290
2860
87
49-130
2-Nitrophenol
ug/kg
1640
1420
86
50-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1640
1440
88
50-130
3,3'-Dichlorobenzidine
ug/kg
3290
2550
77
47-130
3-Nitroaniline
ug/kg
3290
2370
72
45-130IL
4,6-Dinitro-2-methyl phenol
ug/kg
3290
2900
88
50-142
4-Bromophenylphenyl ether
ug/kg
1640
1540
94
55-130
4-ChIoro-3-methyl phenol
ug/kg
3290
3070
93
52-130
4-Chloroaniline
ug/kg
3290
2630
80
49-130
4-Chlorophenylphenyl ether
ug/kg
1640
1510
92
53-130
4-Nitroaniline
ug/kg
3290
2540
77
51-130
4-Nitrophenol
ug/kg
8220
8670
105
40-130
Acenaphthene
ug/kg
1640
1390
84
56-130
Acenaphthylene
ug/kg
1640
1370
83
58-130
Aniline
ug/kg
1640
1240
75
44-130
Anthracene
ug/kg
1640
1420
86
60-130
Benzo(a)anthracene
ug/kg
1640
1500
91
59-130
Benzo(a)pyrene
ug/kg
1640
1520
92
57-130
Benzo(b)fluoranthene
ug/kg
1640
1520
92
54-130
Benzo(g,h,i)perylene
ug/kg
1640
1480
90
59-130
Benzo(k)fluoranthene
ug/kg
1640
1450
88
54-130
Benzoic Acid
ug/kg
8220
4550
55
19-130
Benzyl alcohol
ug/kg
3290
2780
84
50-130
bis(2-Chloroethoxy)methane
ug/kg
1640
1340
81
55-130
bis(2-Chloroethyl) ether
ug/kg
1640
1360
82
53-130
bis(2-Ethylhexyl)phthalate
ug/kg
1640
1460
89
58-130
Butylbenzylphthalate
ug/kg
1640
1510
92
46-138
Chrysene
ug/kg
1640
1370
83
57-130
Di-n-butylphthalate
ug/kg
1640
1480
90
57-130
Di-n-octylphthalate
ug/kg
1640
1570
95
57-130
Dibenz(a,h)anthracene
ug/kg
1640
1530
93
60-130
Dibenzofuran
ug/kg
1640
1400
85
54-130
Diethylphthalate
ug/kg
1640
1470
89
55-130
Dimethylphthalate
ug/kg
1640
1430
87
57-130
Fluoranthene
ug/kg
1640
1520
92
57-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
LABORATORY CONTROL SAMPLE:
Parameter
3162681
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Fluorene
ug/kg
1640
1440
88
56-130
Hexachloro-1,3-butadiene
ug/kg
1640
1610
98
41-130
Hexachlorobenzene
ug/kg
1640
1560
95
53-130
Hexachlorocyclopentadiene
ug/kg
1640
1210
74
23-130
Hexachloroethane
ug/kg
1640
1430
87
48-130
Indeno(1,2,3-cd)pyrene
ug/kg
1640
1550
94
61-130
Isophorone
ug/kg
1640
1470
90
49-130
N-Nitroso-di-n-propylamine
ug/kg
1640
1520
92
52-130
N-Nitrosodimethylamine
ug/kg
1640
1320
80
45-130
N-Nitrosodiphenylamine
ug/kg
1640
1420
86
56-130
Naphthalene
ug/kg
1640
1390
84
56-130
Nitrobenzene
ug/kg
1640
1500
91
50-130
Pentachlorophenol
ug/kg
3290
2750
84
33-130
Phenanthrene
ug/kg
1640
1440
88
60-130
Phenol
ug/kg
1640
1430
87
54-130
Pyrene
ug/kg
1640
1470
89
61-130
Pyridine
ug/kg
1640
1030
63
35-130
2,4,6-Tribromophenol (S)
%
98
18-130
2-Fluorobiphenyl (S)
%
83
19-130
2-Fluorophenol (S)
%
82
18-130
Nitrobenzene-d5 (S)
%
91
21-130
Phenol-d6 (S)
%
84
18-130
Terphenyl-d14(S)
%
106
15-130
Qualifiers
SAMPLE DUPLICATE: 3162683
Parameter
Units
92522099001
Result
Dup
Result RPD
Max
RPD
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
1-Methylnaphthalene
ug/kg
ND
ND
30
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
30
2,4,5-Trichlorophenol
ug/kg
ND
ND
30
2,4,6-Trichlorophenol
ug/kg
ND
ND
30
2,4-Dichlorophenol
ug/kg
ND
ND
30
2,4-Dimethylphenol
ug/kg
ND
ND
30
2,4-Dinitrophenol
ug/kg
ND
ND
30
2,4-Dinitrotoluene
ug/kg
ND
ND
30
2,6-Dinitrotoluene
ug/kg
ND
ND
30
2-Chloronaphthalene
ug/kg
ND
ND
30
2-Chlorophenol
ug/kg
ND
ND
30
2-Methylnaphthalene
ug/kg
0.11J mg/kg
ND
30
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
30
2-Nitroaniline
ug/kg
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 65

Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
SAMPLE DUPLICATE: 3162683
Parameter
Units
92522099001
Result
Dup
Result RPD
Max
RPD Qualifiers
2-Nitrophenol
ug/kg
ND
ND
30
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
30
3,3'-Dichlorobenzidine
ug/kg
ND
ND
30
3-Nitroaniline
ug/kg
ND
ND
30 IL
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
30
4-Bromophenylphenyl ether
ug/kg
ND
ND
30
4-Chloro-3-methylphenol
ug/kg
ND
ND
30
4-Chloroaniline
ug/kg
ND
ND
30
4-Chlorophenylphenyl ether
ug/kg
ND
ND
30
4-Nitroaniline
ug/kg
ND
ND
30
4-Nitrophenol
ug/kg
ND
ND
30
Acenaphthene
ug/kg
ND
ND
30
Acenaphthylene
ug/kg
ND
ND
30
Aniline
ug/kg
ND
ND
30
Anthracene
ug/kg
ND
ND
30
Benzo(a)anthracene
ug/kg
ND
ND
30
Benzo(a)pyrene
ug/kg
ND
ND
30
Benzo(b)fluoranthene
ug/kg
ND
ND
30
Benzo(g,h,i)perylene
ug/kg
ND
ND
30
Benzo(k)fluoranthene
ug/kg
ND
ND
30
Benzoic Acid
ug/kg
ND
ND
30
Benzyl alcohol
ug/kg
ND
ND
30
bis(2-Chloroethoxy)methane
ug/kg
ND
ND
30
bis(2-Chloroethyl) ether
ug/kg
ND
ND
30
bis(2-Ethylhexyl)phthalate
ug/kg
ND
ND
30
Butylbenzylphthalate
ug/kg
ND
ND
30
Chrysene
ug/kg
ND
ND
30
Di-n-butylphthalate
ug/kg
ND
ND
30
Di-n-octylphthalate
ug/kg
ND
ND
30
Dibenz(a,h)anthracene
ug/kg
ND
ND
30
Dibenzofuran
ug/kg
ND
ND
30
Diethylphthalate
ug/kg
ND
ND
30
Dimethylphthalate
ug/kg
ND
ND
30
Fluoranthene
ug/kg
ND
ND
30
Fluorene
ug/kg
ND
ND
30
Hexachloro-1,3-butadiene
ug/kg
ND
ND
30
Hexachlorobenzene
ug/kg
ND
ND
30
Hexachlorocyclopentadiene
ug/kg
ND
ND
30
Hexachloroethane
ug/kg
ND
ND
30
Indeno(1,2,3-cd)pyrene
ug/kg
ND
ND
30
Isophorone
ug/kg
ND
ND
30
N-Nitroso-di-n-propylamine
ug/kg
ND
ND
30
N-Nitrosodimethylamine
ug/kg
ND
ND
30 v1
N-Nitrosodiphenylamine
ug/kg
ND
ND
30
Naphthalene
ug/kg
ND
ND
30
Nitrobenzene
ug/kg
ND
ND
30
Pentachlorophenol
ug/kg
ND
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
SAMPLE DUPLICATE: 3162683
Parameter
Phenanthrene
Phenol
Pyrene
Pyridine
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
Units
92522099001
Result
Dup
Result
ug/kg
ND
ND
ug/kg
ND
ND
ug/kg
ND
ND
ug/kg
ND
ND
%
82
96
%
65
78
63
66
%
70
80
%
61
67
%
84
99
Max
RPD RPD Qualifiers
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 56 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599982 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
METHOD BLANK: 3162933
Matrix:
Solid
Associated Lab Samples:
92521577007, 92521577008,
92521577009, 92521577010, 92521577011
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
10.1 10.1
02/16/21 09:22 N2
Aliphatic (C19-C36)
mg/kg
ND
10.1 10.1
02/16/21 09:22 N2
Aromatic (C11-C22)
mg/kg
ND
10.1 10.1
02/16/21 09:22 N2
1-Chlorooctadecane (S)
%
54
40-140
02/16/21 09:22
2-Bromonaphthalene (S)
%
93
40-140
02/16/21 09:22
2-Fluorobiphenyl (S)
%
93
40-140
02/16/21 09:22
o-Terphenyl (S)
%
73
40-140
02/16/21 09:22
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
3162934
Units
Spike
Conc.
3162935
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec Max
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
9.9
ND ND
68
68
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.2
ND 10.1
74
76
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28.1
17.1 18.5
61
66
40-140 8 50 N2
1-Chlorooctadecane (S)
%
67
71
40-140
2-Bromonaphthalene (S)
%
90
98
40-140
2-Fluorobiphenyl (S)
%
90
98
40-140
o-Terphenyl(S)
%
66
76
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 57 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 599437 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92521577001, 92521577002, 92521577003, 92521577004, 92521577005, 92521577006, 92521577007,
92521577008,92521577009,92521577010,92521577011
SAMPLE DUPLICATE: 3160252
92521440001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 25.2 25.0 1 25 N2
SAMPLE DUPLICATE: 3160253
92521628001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 13.0 12.8 1 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC.
Page 58 of 65

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
QC Batch: 1622568 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
METHOD BLANK: R3624121-1 Matrix: Solid
Associated Lab Samples: 92521577007, 92521577008, 92521577009, 92521577010, 92521577011
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Solids % 0.00100 02/22/21 11:36
LABORATORY CONTROL SAMPLE: R3624121-2
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Solids % 50.0 50.0 100 85.0-115
SAMPLE DUPLICATE: R3624121-3
L1317135-05 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Solids % 78.3 77.1 1.52 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: CAMP STEWARD ROAD SITE
Pace Project No.: 92521577
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
J Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
ST Surrogate recovery was above laboratory control limits. Results may be biased high.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/24/2021 01:57 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
CAMP STEWARD ROAD SITE
92521577
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92521577001
#3 NS (4-4.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577002
#3 SS (4-4.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577003
#2 NS (4-4.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577004
#2 SS (4-4.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577005
#1 NS (5.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577006
#1 SS (5.5)
EPA 3546
599380
EPA 8015C Modified
599611
92521577007
#2 NW (6.5-7)
MADEP EPH
599982
MADEP EPH
600346
92521577008
#2 SW (6.5-7)
MADEP EPH
599982
MADEP EPH
600346
92521577009
#2 EW (6.5-7)
MADEP EPH
599982
MADEP EPH
600346
92521577010
#2 WW (6.5-7)
MADEP EPH
599982
MADEP EPH
600346
92521577011
#2 BASE (15.0)
MADEP EPH
599982
MADEP EPH
600346
92521577007
#2 NW (6.5-7)
MADEPV
1621956
MADEP VPH
1621956
92521577008
#2 SW (6.5-7)
MADEPV
1621454
MADEP VPH
1621454
92521577009
#2 EW (6.5-7)
MADEPV
1621454
MADEP VPH
1621454
92521577010
#2 WW (6.5-7)
MADEPV
1621956
MADEP VPH
1621956
92521577011
#2 BASE (15.0)
MADEPV
1621956
MADEP VPH
1621956
92521577011
#2 BASE (15.0)
MADEPV
1623520
MADEP VPH
1623520
92521577001
#3 NS (4-4.5)
EPA 5030B
599422
EPA 8015C Modified
599467
92521577002
#3 SS (4-4.5)
EPA 5030B
599699
EPA 8015C Modified
599714
92521577003
#2 NS (4-4.5)
EPA 5030B
599699
EPA 8015C Modified
599714
92521577004
#2 SS (4-4.5)
EPA 5030B
599699
EPA 8015C Modified
599714
92521577005
#1 NS (5.5)
EPA 5030B
599699
EPA 8015C Modified
599714
92521577006
#1 SS (5.5)
EPA 5030B
599699
EPA 8015C Modified
599714
92521577007
#2 NW (6.5-7)
EPA 3546
599953
EPA 8270E
600218
92521577008
#2 SW (6.5-7)
EPA 3546
599953
EPA 8270E
600218
92521577009
#2 EW (6.5-7)
EPA 3546
599953
EPA 8270E
600218
92521577010
#2 WW (6.5-7)
EPA 3546
599953
EPA 8270E
600218
92521577011
#2 BASE (15.0)
EPA 3546
599953
EPA 8270E
600218
92521577001
#3 NS (4-4.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577002
#3 SS (4-4.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577003
#2 NS (4-4.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577004
#2 SS (4-4.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577005
#1 NS (5.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577006
#1 SS (5.5)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577007
#2 NW (6.5-7)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577008
#2 SW (6.5-7)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577009
#2 EW (6.5-7)
EPA 5035A/5030B
599326
EPA 8260D
599327
92521577010
#2 WW (6.5-7)
EPA 5035A/5030B
599428
EPA 8260D
599439
92521577011
#2 BASE (15.0)
EPA 5035A/5030B
599428
EPA 8260D
599439
92521577001
#3 NS (4-4.5)
SW-846
599437
92521577002
#3 SS (4-4.5)
SW-846
599437
92521577003
#2 NS (4-4.5)
SW-846
599437
92521577004
#2 SS (4-4.5)
SW-846
599437
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 02/24/2021 01:57 PM
without the written consent of Pace Analytical Services, LLC.
Page 61 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
CAMP STEWARD ROAD SITE
92521577
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92521577005
#1 NS (5.5)
SW-846
599437
92521577006
#1 SS (5.5)
SW-846
599437
92521577007
#2 NW (6.5-7)
SW-846
599437
92521577008
#2 SW (6.5-7)
SW-846
599437
92521577009
#2 EW (6.5-7)
SW-846
599437
92521577010
#2 WW (6.5-7)
SW-846
599437
92521577011
#2 BASE (15.0)
SW-846
599437
92521577007
#2 NW (6.5-7)
SM 2540 G
1622568
SM 254OG
1622568
92521577008
#2 SW (6.5-7)
SM 2540 G
1622568
SM 254OG
1622568
92521577009
#2 EW (6.5-7)
SM 2540 G
1622568
SM 254OG
1622568
92521577010
#2 WW (6.5-7)
SM 2540 G
1622568
SM 254OG
1622568
92521577011
#2 BASE (15.0)
SM 2540 G
1622568
SM 254OG
1622568
Date: 02/24/2021 01:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 62 of 65

Document Name: Document Revised: October 28, 2020
f Sample Condition Upon Receipt(SCUR) Page 1 of 2
�AceAnalyfical Document No.: Issuing Authority:
F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [] Raleigh❑ Mechanicsville[] Atlanta[] Kernersville❑
• . r Client Name: on Receipt Project #: Wa# : 92521577
Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client IIII 11111III�IIIII�I�
❑ Commercial []Pace ❑Other:7
Custody Seal Present? ❑Yes []No Seals Intact? ❑Yes ❑No
Packing Material: ❑Bubble Wrap .❑Bubble Bags ❑None ❑ Other
Thermometer: ❑Wet ❑Blue
IR Gun ID: 92TO64 Type of Ice:
Correction Factor:
Cooler Temp: «ti Add/Subtract (°C) -0.1
Cooler Temp Corrected (*Cl: lae ` 1)
USDA Regulated Soil�BVAr, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check mapsl?
F�l'Yes R
Date/Initials Person Examining Contents:
Biological Tissue Frozen?
[-]None
❑Yes ❑No ❑N/A
Temp should be above freezing to 6°C
❑Samples out or temp criteria. Samples an ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
inrluriina Hawaii nnri Pi —In nirni� I�Vac - I mI
Comments/Discrepancy:
Chairi of Custody Present?
[]Yes
❑No
❑N/A
1,
Sample$ Arrived within Hold Time?
[]Yes
❑No
❑N/A
2.
Short Hold Time Analysis (c72 hr.)?
❑Yes
[]No
❑NIA
3.
Aush Turn Around Time Requested!
Des
nNo
❑N/A
4,
Sufficient Volume?
•.r yes
[-]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
❑Yes
Elves
[:]No
❑No
[]N/A
[-]N/A
6,
Containers intact?
. ves
[:]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
[]Yes
[-]No
❑N/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
❑Yes
[—]No
[—]N/A
9,
Heads ace in VOA Vials (>5-6mm)?
[]Yes
No
, N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Yes
ONO
No
❑N/A
,N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Pers'arrc .
Project Manager SCURF Review:
Date/Time:
Date:
Field Data Required? Dyes ❑No
Project Manager SRF Review: Date:
Page 63 of 65

Oocument Name:
Sample Condition Upon Recei
Analytical Document No.:
F-CAR-CS-033-Rev.07
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
EKceptlons: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
Document Revised: October 28, 2020
t(SCUR) Page 2 of 2
Issuing Authority:
Pace Carolinas Quality Office
Project # ��
5215 02I la
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Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Loth
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Note, Whenever there Is a digcre. hTarotina-camptiance Samples, a copy of -this form will be5ent-te4he- t a-6af4aa DE4 A f ertif Cation CMG84a
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 64 of 65

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Page 65 of 65

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 26, 2021
Nora Zirps
ESP Associates
7011 Albert Pick Rd.
Suite E
Greensboro, NC 27409
RE: Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
Dear Nora Zirps:
Enclosed are the analytical results for sample(s) received by the laboratory on March 22, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
[phone]
Project Manager
Enclosures
cc: Account Payable, ESP Associates
REPORT OF LABORATORY ANALYSIS
r
e
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 31

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 31

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92528956001
92528956002
#2 NW-2 (6.5-7)
#2 SW-2 (6.5-7)
Solid
Solid
03/22/21 11:07
03/22/21 11:14
03/22/21 11:20
03/22/21 11:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 31

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92528956001 #2 NW-2 (6.5-7)
EPA 8270E
Bpi
4
PASI-C
EPA 8260D
CL
4
PASI-C
SW-846
KDF
1
PASI-C
92528956002 #2 SW-2 (6.5-7)
MADEP VPH
LMB
6
PASI-C
SW-846
KDF
1
PASI-C
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 31

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
Sample: #2 NW-2 (6.5-7)
Lab ID: 92528956001 Collected:
03/22/21 11:07
Received: 03/22/21 11:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
1-Methylnaphthalene
ND ug/kg 391
138 1
03/23/21 12:46
03/24/21 20:43
90-12-0
Surrogates
Nitrobenzene-d5 (S)
34 % 21-130
1
03/23/21 12:46
03/24/21 20:43
4165-60-0
2-Fluorobiphenyl (S)
33 % 19-130
1
03/23/21 12:46
03/24/21 20:43
321-60-8
Terphenyl-d14 (S)
43 % 15-130
1
03/23/21 12:46
03/24/21 20:43
1718-51-0
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
Naphthalene
ND ug/kg 6.8
3.6 1
03/23/21 15:23
03/23/21 20:29
91-20-3
Surrogates
Toluene-d8 (S)
100 % 70-130
1
03/23/21 15:23
03/23/21 20:29
2037-26-5
4-Bromofluorobenzene (S)
95 % 69-134
1
03/23/21 15:23
03/23/21 20:29
460-00-4
1,2-Dichloroethane-d4 (S)
108 % 70-130
1
03/23/21 15:23
03/23/21 20:29
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
14.8 % 0.10
0.10 1
03/22/21 16:14
N2
Sample: #2 SW-2 (6.5-7)
Lab ID: 92528956002 Collected:
03/22/21 11:14
Received: 03/22/21 11:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
Aliphatic (C05-008)
ND mg/kg 3.9
3.9 1
03/22/21 16:18
03/23/21 06:51
N2
Aliphatic (C09-C12)
ND mg/kg 3.9
3.9 1
03/22/21 16:18
03/23/21 06:51
N2
Aliphatic(C09-C12)Adjusted
ND mg/kg 3.9
3.9 1
03/22/21 16:18
03/23/21 06:51
N2
Aromatic (C09-C10)
ND mg/kg 3.9
3.9 1
03/22/21 16:18
03/23/21 06:51
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
107 % 70-130
1
03/22/21 16:18
03/23/21 06:51
460-00-4
4-Bromofluorobenzene (PID) (S)
98 % 70-130
1
03/22/21 16:18
03/23/21 06:51
460-00-4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
20.2 % 0.10
0.10 1
03/23/21 16:10
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 31

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
QC Batch: 608307 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92528956002
METHOD BLANK: 3204575
Matrix:
Solid
Associated Lab Samples: 92528956002
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Aliphatic (C05-CO8)
mg/kg
ND
2.5
2.5 03/23/21 04:00 N2
Aliphatic (C09-C12)
mg/kg
ND
2.5
2.5 03/23/21 04:00 N2
Aromatic (C09-C10)
mg/kg
ND
2.5
2.5 03/23/21 04:00 N2
4-Bromofluorobenzene (FID) (S)
%
100
70-130
03/23/21 04:00
4-Bromofluorobenzene (PID) (S)
%
93
70-130
03/23/21 04:00
LABORATORY CONTROL SAMPLE & LCSD:
3204576
3204577
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg 15
13.4 13.8
89
92
70-130 3 25 N2
Aliphatic (C09-C12)
mg/kg 15
14.3 14.6
95
97
70-130 2 25 N2
Aromatic (C09-C10)
mg/kg 5
5.0 5.0
99
100
70-130 1 25 N2
4-Bromofluorobenzene (FID) (S)
%
97
99
70-130
4-Bromofluorobenzene (PID) (S)
%
88
89
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2021 02:18 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 31

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
QC Batch: 608617
Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B
Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92528956001
METHOD BLANK: 3205892
Matrix: Solid
Associated Lab Samples: 92528956001
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
Qualifiers
Naphthalene
ug/kg
ND 5.0 2.6
03/23/21 10:44
1,2-Dichloroethane-d4 (S)
%
116 70-130
03/23/21 10:44
4-Bromofluorobenzene (S)
%
95 69-134
03/23/21 10:44
Toluene-d8 (S)
%
103 70-130
03/23/21 10:44
LABORATORY CONTROL SAMPLE: 3205893
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Naphthalene
ug/kg
1250 1260 100
70-130
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
99
69-134
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE: 3206804
92528794002 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Naphthalene
ug/kg
ND 797 528
66
15-145
1,2-Dichloroethane-d4 (S)
%
119
70-130
4-Bromofluorobenzene (S)
%
96
69-134
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 3205894
92528942001 Dup
Max
Parameter
Units
Result Result RPD
RPD
Qualifiers
Naphthalene
ug/kg
ND ND
30
1,2-Dichloroethane-d4 (S)
%
106 105
4-Bromofluorobenzene (S)
%
98 96
Toluene-d8 (S)
%
101 102
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 31

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
QC Batch: 608527 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92528956001
METHOD BLANK: 3205418
Matrix:
Solid
Associated Lab Samples: 92528956001
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
1-Methylnaphthalene
ug/kg
ND
336
118 03/24/21 10:11
2,4,6-Tribromophenol (S)
%
75
18-130
03/24/21 10:11
2-Fluorobiphenyl (S)
%
72
19-130
03/24/21 10:11
2-Fluorophenol (S)
%
70
18-130
03/24/21 10:11
Nitrobenzene-d5 (S)
%
82
21-130
03/24/21 10:11
Phenol-d6 (S)
%
72
18-130
03/24/21 10:11
Terphenyl-d14 (S)
%
102
15-130
03/24/21 10:11
LABORATORY CONTROL SAMPLE:
3205419
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
1-Methylnaphthalene
ug/kg
1660 1400
84
54-130
2,4,6-Tribromophenol (S)
%
89
18-130
2-Fluorobiphenyl (S)
%
83
19-130
2-Fluorophenol (S)
%
76
18-130
Nitrobenzene-d5 (S)
%
89
21-130
Phenol-d6 (S)
%
79
18-130
Terphenyl-d14 (S)
%
112
15-130
MATRIX SPIKE SAMPLE:
3205420
92528874009 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
1-Methylnaphthalene
ug/kg
ND 2110
1330
63
30-130
2,4,6-Tribromophenol (S)
%
39
18-130
2-Fluorobiphenyl (S)
%
34
19-130
2-Fluorophenol (S)
%
50
18-130
Nitrobenzene-d5 (S)
%
53
21-130
Phenol-d6 (S)
%
50
18-130
Terphenyl-d14 (S)
%
42
15-130
SAMPLE DUPLICATE: 3205421
92528874010 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
1-Methylnaphthalene ug/kg ND ND 30
2,4,6-Tribromophenol (S) % 48 61
2-Fluorobiphenyl (S) % 28 52
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 31

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
SAMPLE DUPLICATE: 3205421
92528874010
Dup Max
Parameter
Units
Result
Result RPD RPD
2-Fluorophenol(S)
%
44
61
Nitrobenzene-d5 (S)
%
49
68
Phenol-d6 (S)
%
44
59
Terphenyl-d14 (S)
%
25
23
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2021 02:18 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 31

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
QC Batch: 608259 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92528956001
SAMPLE DUPLICATE: 3204619
Parameter
Percent Moisture
SAMPLE DUPLICATE: 3204622
Parameter
Percent Moisture
92528956001 Dup
Units Result Result
14.8 14.3
92528851010 Dup
Units Result Result
% 21.8 23.0
Max
RPD RPD Qualifiers
4 25 N2
Max
RPD RPD Qualifiers
5 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 31

lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
QC Batch: 608646 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92528956002
SAMPLE DUPLICATE: 3206100
Parameter
Percent Moisture
SAMPLE DUPLICATE: 3206101
Parameter
Percent Moisture
92528941001 Dup
Units Result Result
18.6 17.8
92529212003 Dup
Units Result Result
% 9.6 9.1
Max
RPD RPD Qualifiers
5 25 N2
Max
RPD RPD Qualifiers
5 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 31

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2021 02:18 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 31

lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Camp Stewart Road Site / GP56.
Pace Project No.: 92528956
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92528956002
#2 SW-2 (6.5-7)
MADEP VPH
608307
MADEP VPH
608319
92528956001
#2 NW-2 (6.5-7)
EPA 3546
608527
EPA 8270E
608787
92528956001
#2 NW-2 (6.5-7)
EPA 5035A/5030B
608617
EPA 8260D
608652
92528956001
#2 NW-2 (6.5-7)
SW-846
608259
92528956002
#2 SW-2 (6.5-7)
SW-846
608646
Date: 03/26/2021 02:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 31

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Page 15 of 31

aceAnalytical
Report of Analysis
Pace Analytical Services, LLC
9800 Kincey Avenue
Suite 100
Huntersville, NC 28078
Attention: Bonnie Vang
Project Name: Camp Steward Road Site / GP56.
Project Number: 92528956
Lot Number:WC24013
Date Completed:03/26/2021
Project Manager:Blaire M. Gagne
03/26/2021 1:24 PM
Approved and released by:
Project Manager I: Hannah K. Lucas
JA
A CC A E O[ 7 E O
YESiIHG LABORA70MI
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 16 of 31
Page 1 of 16

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Pace Analytical Services, LLC
Lot Number: WC24013
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
MA EPH
A reduced initial volume was used for sample -001 due to the sample matrix. The reporting limits have
been raised accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 31
Page 2 of 16

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical Services, LLC
Lot Number: WC24013
Project Name: Camp Steward Road Site / GP56.
Project Number: 92528956
Sample Number Sample ID Matrix Date Sampled Date Received
001 #2 SW-2 (6.5-7) Solid 03/22/2021 1114 03/24/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 31
Page 3 of 16

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Pace Analytical Services, LLC
Lot Number: WC24013
Project Name: Camp Steward Road Site / GP56.
Project Number: 92528956
Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 16
Page 19 of 31

MA EPH (aromatics)
Client: Pace Analytical Services, LLC Laboratory ID: WC24013-001
Description: #2 SW-2 (6.5-7) Matrix: Solid
Date Sampled:03/22/2021 1114 Project Name: Camp Steward Road Site / % Solids: 80.1 03/24/2021 2312
Date Received: 03/24/2021 Project Number: 92528956
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 03/25/2021 2035 NCM 03/24/2021 1344 86726
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 4.1 4.1 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2)
2-Fluorobiphenyl (fractionation 1)
o - Terphenyl (aromatic)
90 40-140
97 40-140
79 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 31
Page 5 of 16

MA EPH (aliphatics)
Client: Pace Analytical Services, LLC Laboratory ID: WC24013-001
Description: #2 SW-2 (6.5-7) Matrix: Solid
Date Sampled:03/22/2021 1114 Project Name: Camp Steward Road Site / % Solids: 80.1 03/24/2021 2312
Date Received: 03/24/2021 Project Number: 92528956
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 03/25/2021 1832 NCM 03/24/2021 1344 86725
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND 4.1 4.1 mg/kg 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 4.1 4.1 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
97 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 31
Page 6 of 16

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WC24013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 22 of 31
Page 7 of 16

MA EPH (aliphatics) - MB
Sample ID: WQ86725-001 Matrix: Solid
Batch: 86725 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 03/24/2021 1344
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C18 Aliphatics ND 1 10 10 mg/kg 03/25/2021 1701
C19 - C36 Aliphatics ND 1 10 10 mg/kg 03/25/2021 1701
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 102 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 16
QC Data for Lot Number: WC24013
Page 23 of 31

MA EPH (aliphatics) - LCS
Sample ID: WQ86725-002 Matrix: Solid
Batch: 86725 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 03/24/2021 1344
Spike
Amount Result %Rec
Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date
C9 - C18 Aliphatics 10 6.1 1 61 40-140 03/25/2021 1731
C19 - C36 Aliphatics 13 12 1 91 40-140 03/25/2021 1731
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 106 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 16
QC Data for Lot Number: WC24013
Page 24 of 31

MA EPH (aliphatics) - LCSD
Sample ID: WQ86725-003 Matrix: Solid
Batch: 86725 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 03/24/2021 1344
Spike
Amount
Result
%Rec
% RPD
Parameter (mg/kg)
(mg/kg) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics 10
6.0
1 60 1.7 40-140
25 03/25/2021 1802
C19 - C36 Aliphatics 13
13
1 94 2.9 40-140
25 03/25/2021 1802
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 107 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
= RSD is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 16
QC Data for Lot Number: WC24013
Page 25 of 31

MA EPH (aromatics) - MB
Sample ID: WQ86726-001 Matrix: Solid
Batch: 86726 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 03/24/2021 1344
Parameter Result Q Dil LOQ DL Units Analysis Date
C11 - C22 Aromatics ND 1 10 10 mg/kg 03/25/2021 1903
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 86 40-140
2-Fluorobiphenyl (fractionation 1) 95 40-140
o - Terphenyl (aromatic) 82 40-140
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WC24013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 26 of 31
Page 11 of 16

MA EPH (aromatics) - LCS
Sample ID: WQ86726-002
Matrix:
Solid
Batch: 86726
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
03/24/2021 1344
Spike
Amount
Result
%Rec
Parameter
(mg/kg)
(mg/kg) Q
Dil
% Rec Limit Analysis Date
C11 - C22 Aromatics
28
18
1
62 40-140 03/25/2021 1934
Surrogate
Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2) 88 40-140
2-Fluorobiphenyl (fractionation 1) 94 40-140
o - Terphenyl (aromatic) 81 40-140
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WC24013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 27 of 31
Page 12 of 16

MA EPH (aromatics) - LCSD
Sample ID: WQ86726-003 Matrix: Solid
Batch: 86726 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 03/24/2021 1344
Spike
Amount Result %Rec % RPD
Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics 28 19 1 67 8.1 40-140 25 03/25/2021 2004
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 96 40-140
2-Fluorobiphenyl (fractionation 1) 103 40-140
o - Terphenyl (aromatic) 86 40-140
LOQ = Limit of Quantitation ND = Not detected at or above the DL N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL P = The RPD between two GC columns exceeds 40 %
= RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WC24013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 28 of 31
Page 13 of 16

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 31
Page 14 of 16

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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 16
Page 30 of 31

PACE ANALYTICAL SERVICES, LLC
Samples Pecarpt Cherklkt ISRQ (MEDOISC: 15I ReMtssc_9
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Sample Receipt Cbeckl6t (SRC)
Client: PACE Echaler Jnsnected b}',ldwc: M111.1 i fkl�).f21 Lit P: %%rc 4013
Means of receipt: Pace I rNtl3l. I f TQIhCr=
Yes I L!NOJ1, Were cmtady leaks present on titre co-: Iel'?
PCs ..LJNaJ [4 MA 12. Iftimtody Sea€twar- prwrtl. wcr0y intact and wibrok'50
pH Strip TIS= K.4 Chlodnc drip 17); Wr. .,.._ -- Tested by` 31A
Ori'�i-aar L,Nolre3nture upon rreoipt! l riVW (CM-yxwd) t4mpeMture UPO-n receipt 'f.So id Snap -Cup JD: 21443
4.L ?4A OC NA INA uC NA INA ;PC NA jNA VC
Mcrhod. ❑-FCMPeMtLLre I)JRrLk iest �trttics I Gkirt I1}: ° 1R Cilul Correction Factor: a °C
MCChOd of COAM L: ❑, VVcL lcc ILc PA&H ❑ Dr4 rae L] Nonce
[� Yes
❑ No
❑ NA
" t t tcmParamra or ally cooler eMeeWa tx LrU, was MJCCt MLlnug:r QUID
PM was Notif od b}, phow f ernail) face -to •f4ce (circle one).
Yes
I LiNu
U NA4
4, 1s dfa rurune .ai eaurier's ruck irgsl=l,rdiinahed to Leis fhirn7
Ytx:
' No
5. Wero IrnIFr p s:LN L tdu P"IL t, ffe.c (rt,kin uished,lrecei-%Fed) foil#wed?
d
Yo5
L No
6, Wero sampk: ids IiAW on the C:OC'P
Yes
❑ No
17, Were sample IDs Iisteel an all saippla 4altt#ih3elP
l 'r-es
7 Yes
Nu
N
8_ Was eollt�Uitui dyLr & lime Iistod on the COC7
9_ Was call tti0ri date & time iistcd ona:l sa epic colt incas4
Yes
i ❑'N0
10_ Did all ufntain(tT 49b61 inforr tat:on (1D, date, time) oaree with 11,e co ?
Yusi
LJ No
11. Wore tcsts to Ill: paeormed Itsted nn Ehe CCC?
YJ'femI LL tta
lv'lYes
u rat}
,r Yes li—-❑-
o
C
❑ Yet
'J N o
❑ No
QWA
EYcs
Nu
A
Ye€,
LJWtLl
L7JNA
❑ Yes
❑ N
❑,{ ; A
IL Did all �.,mn,nlms arrive in the proper containers far eftCh test anJo'pr iat +Sovd 4:wLdititm
("brukcn, lids 0n4 atc. j'r'
13. Wwv, adaluatc sample valunle available'r
14. Were nil Sam plo rcccivcd within Vz the holding tirr_e 0r 4 hntirs, whichever comes FCst7
15. Wpm any swnp:es rontafnerR miSwinVgxceSS (ci~tile 03te) t,4li5tad on COC7
16. Rv VOA and F,8K-1?5 swaiples, wu'ra hubb€cs Prescnt -,Jea-size" ('/."or45mm io diaatctcr)
in any of die VOA vials?
17. Wtee all I?RCVn-rfaiF;,rrutrieLn sate ]as l ecel veJ aL a trH UP< m" H. k4eni a1' t.yard *.. sale Ales received at a }rH > 12 yard slefide sainpilea received of et PH 9?
19. Wem u1: uppl.'-Mblc NN r.t7 1cyaltidt;' ltenn167.r, I i601S3 f{ 0.T—L) same es free of
❑ Yes ONO d�A 20. Were client rernarksimquests (i.::. rrglt=M dilutions, his .MSD desigrtptions,
�oi:wuutlly lransriibM f1om Cte COO i-lli the comluvnc mctiolt 311 r. M;5?
L—JyQ1 A Na 121. Was the quote numbor Iistod on the cantainer label? It yCs, QucAc # "*
SOu PIC Prmrvation ([dust be caLnpleted for any samples) in47orcectly pewee, d or wkth hcadspFce.) i
'Sample(s) MR wc:rc reccpved h3cofrBCtty preserved wed we:-e adjusted ecco_-dirt;ly
Sul sample reee:v:rg with 1`A mL of:.inr.1t on= WS04, FNO3, HU, NaolI usdq SR ft —
T`me of pipeservatlon NA , If mare llitkii Cute pm"L-Yalrivc is hooded_ please tiote itl the Cumrncncsbclavr_
ampte(s) NA _ were received with bubbly:: =d mrr_. ill diamnicr,
p;nplcs(s) �^ -- .-- _ wem reu:ivLt1 wi-h TKC > 0,5 mg/L (If ri 19 is wv ) and were
djaster accordingly in sample Teceivhigwidl sodium Lhiiw0fatc (NVsS203) with Shealy ID; A
R lxartodlo labels applieity: rnols ry Date: 03124nMl
Corninetits:
1oF1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 16
Page 31 of 31

Beverly, Trudy
From: Nora Zirps <[e-mail]>
Sent: Thursday, May 13, 2021 10:48 AM
To: Beverly, Trudy
Subject: RE: [External] Camp Stewart Road Site - Residential Heating Oil UST Release - Submittal
of IAA and LSA Reports
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Will do. It will likely be tomorrow.
Nora A. Zirps, PE, RSM
ESP Associates, Inc.
7011 Albert Pick Road, Suite E
Greensboro, NC 27409
www.espassociates.com
[e-mail]
336.232.5213 Direct
336.334.7724 Office
336.420.6979 Cell
From: Beverly, Trudy <[e-mail]>
Sent: Thursday, May 13, 2021 10:36 AM
To: Nora Zirps <[e-mail]>
Subject: RE: [External] Camp Stewart Road Site - Residential Heating Oil UST Release - Submittal of IAA and LSA Reports
Nora,
I didn't see a statement in the IAA nor LSA about the AST, aside from it being removed. If there was no evidence of
contamination, sent me a signed/seal short statement for the file.
Thanks,
Trudy
From: Beverly, Trudy
Sent: Thursday, May 13, 2021 10:20 AM
To: Nora Zirps <[e-mail]>
Subject: RE: [External] Camp Stewart Road Site - Residential Heating Oil UST Release - Submittal of IAA and LSA Reports
Hey Nora,
I named the site Camp Stewart Property in the RUST database (Incident #47761, UST Number MO-28509). See link
below for the Alternate Land Use Restriction NORP. Add a 5' buffer in the soil restriction area. Do you have an email
address for Dean Davidson with Professional Child Care Centers, Inc.?
Instructions and Form for Notice of Residual Petroleum with Alternate Land Use Restriction
https://deg.nc.gov/about/divisions/waste-management/ust/forms

Let me know if you have questions.
Trudy
4
fH '�FdCAl
F's
rla4 DL
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.l3everlykncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https:Hdeg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httDs://deo.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-mans
File Review Procedures:
hns://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hitps://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
htti)s:Hfiles.nc.¢ov/ncdeg/Waste%2OManaizement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policv.adf
https:Hfiles.nc. gov/ncdeq/Waste%2OManagement/DWM/UST/Corrective%2OAction/UST%20file%20names%2Ofor%2OLaserfiche.docx
From: Nora Zirps [mailto:[e-mail]]
Sent: Tuesday, May 11, 20218:33 AM
To: Beverly, Trudy <[e-mail]>
Subject: RE: [External] Camp Stewart Road Site - Residential Heating Oil UST Release - Submittal of IAA and LSA Reports
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Trudy,
Just a quick note ... the rectangular area will not be situated due north to south. The area slants more like northeast to
southwest. The north -south terminology was used for simplicity.
Talk to you later this week.
Nora
Nora A. Zirps, PE, RSM
ESP Associates, Inc.
7011 Albert Pick Road, Suite E
Greensboro, NC 27409
www.espassociates.com
[e-mail]
336.232.5213 Direct
336.334.7724 Office
336.420.6979 Cell

From: Nora Zirps
Sent: Monday, May 10, 2021 5:42 PM
To: Beverly, Trudy <[e-mail]>
Subject: RE: [External] Camp Stewart Road Site - Residential Heating Oil UST Release - Submittal of IAA and LSA Reports
I understand. Thank you, Trudy.
Nora A. Zirps, PE, RSM
ESP Associates, Inc.
7011 Albert Pick Road, Suite E
Greensboro, NC 27409
www.espassociates.com
[e-mail]
336.232.5213 Direct
336.334.7724 Office
336.420.6979 Cell
From: Beverly, Trudy <[e-mail]>
Sent: Monday, May 10, 2021 3:48 PM
To: Nora Zirps <[e-mail]>
Subject: RE: [External] Camp Stewart Road Site - Residential Heating Oil UST Release - Submittal of IAA and LSA Reports
Hey Nora,
It may be later in the week before I can review the information. I'll get back with you as soon as it's reviewed.
Have a great day,
Trudy
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
I�r
704.235.2182 (Office)
Trudy.13everlykncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-manaaement/ust
Branch's Above Ground Storage Tanks Website Address: https:Hdeg.nc.gov/about/divisions/waste-mana2ement/ust/ast-proeram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hit 2s://deg.nc.gov/about/divisions/waste-manaaement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
httys:Hfiles.nc.eov/nedeci/Waste%2OManaeement/DWM/UST/W hatsNew/Final-Electronic-Document-Submittal-Policy.odf
https:Hfiles.nc.gov/ncdeq/Waste%20Management/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx

From: Nora Zirps [ma iIto: [e-mail]]
Sent: Monday, May 10, 2021 12:31 PM
To: Beverly, Trudy <[e-mail]>
Subject: RE: [External] Camp Stewart Road Site - Residential Heating Oil UST Release - Submittal of IAA and LSA Reports
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Trudy,
I hope your husband's surgery went well, and he is recovering quickly.
I imagine today is a busy day for you playing catch-up, but I did want to reach out to you since I would like to discuss the
soil deed restriction for the subject site with you this week. It would be helpful to know if what we are proposing is
acceptable prior to us preparing the plat to avoid iterations. We feel it is necessary to record a plat to define the
location since the parcel is over 50 acres.
As you will see when you review the submitted IAA and LSA reports, we have completed a good bit of sample
analysis. Based on that, we would like to suggested using the following points to define a "rectangular" area
(approximately 14 ft x 25.5 ft) for the soil deed restriction bounded by the following points:
TMW-1 to the north
#2 EW to the east
B-1 to the south
#2 WW to the west
Soil sample results were below residential MSCCs at each of these locations, plus all but the TMW-1 location were also
below soil -to -groundwater MSCCs. The soil sample collected from the base of the approximate center of the area
exceeded residential MSCCs, resulting in the need for the soil deed restriction. Groundwater is below NC 2L
groundwater standards, so we do not plan to include a groundwater deed restriction.
I look forward to your response as to the acceptability of our proposed soil deed restricted area. If a telephone call is
warranted, please let me know what time would work for you.
Thank you.
Nora
Nora A. Zirps, PE, RSM
ESP Associates, Inc.
7011 Albert Pick Road, Suite E
Greensboro, NC 27409
www.espassociates.com
[e-mail]
336.232.5213 Direct
336.334.7724 Office
336.420.6979 Cell
From: Nora Zirps
Sent: Thursday, April 29, 2021 12:34 PM

To: Beverly, Trudy <[e-mail]>
Cc: Fred Matrulli <Fred.MatruIli @PulteGroup.com>; Cameron Caudle, Jr. ([e-mail])
<[e-mail]>; Chris Ward <[e-mail]>
Subject: RE: [External] Camp Stewart Road Site - Residential Heating Oil UST Release - Submittal of IAA and LSA Reports
Trudy,
I hope all goes well with your husband's surgery.
I look forward to speaking with you the week of May 10.
Nora
Nora A. Zirps, PE, RSM
ESP Associates, Inc.
7011 Albert Pick Road, Suite E
Greensboro, NC 27409
www.espassociates.com
[e-mail]
336.232.5213 Direct
336.334.7724 Office
336.420.6979 Cell
From: Beverly, Trudy <[e-mail]>
Sent: Thursday, April 29, 2021 12:32 PM
To: Nora Zirps <[e-mail]>
Cc: Fred Matrulli <Fred.MatruIli @PulteGroup.com>; Cameron Caudle, Jr. ([e-mail])
<[e-mail]>; Chris Ward <[e-mail]>
Subject: RE: [External] Camp Stewart Road Site - Residential Heating Oil UST Release - Submittal of IAA and LSA Reports
THIS MESSAGE ORIGINATED OUTSIDE OF ESP ASSOCIATES, INC. USE CAUTION WHEN OPENING ATTACHMENTS, CLICKING LINKS, OR RESPONDING
TO REQUESTS FOR INFORMATION.
Hey Nora,
Document received. No need to mail a paper copy. I have meetings this afternoon and will be on leave tomorrow
through May 7t". I'll be back to working remotely on May 10th. Unfortunately, a discussion will have to wait until that
week. My husband is having surgery.
Have a wonderful day,
Trudy
Trudy Beverly, L.G.
D- I E Q Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: hitps://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-proeram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httDs:Hdeu.ne. aov/about/divisions/waste-manaeement/waste-manaeement-rules-data/waste-manaaement-eis-mans
File Review Procedures:
https:Hdcq.nc. gov/about/divisions/waste-manaaement/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
httns://deo.nc. aov/about/divisions/waste-manaeement/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https:Hfiles.nc.gov/ncdeg[Waste%20Manatiement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policv.pdf
https:Hfiles.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%20filc%20names%20for%2OLaserfiche.docx
From: Nora Zirps [mailto:[e-mail]]
Sent: Thursday, April 29, 2021 10:12 AM
To: Beverly, Trudy <[e-mail]>
Cc: Fred Matrulli <[e-mail]>; Cameron Caudle, Jr. ([e-mail])
<[e-mail]>; Chris Ward <[e-mail]>
Subject: [External] Camp Stewart Road Site - Residential Heating Oil UST Release - Submittal of IAA and LSA Reports
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Trudy,
Attached please find the Initial Abatement Action (IAA) Report and the Limited Site Assessment (LSA) Report for the
approximate 550-gallon residential heating oil UST (designated UST-3) removed from the Camp Stewart Road Site located within
Mecklenburg County Tax Parcel No.11109204 in Charlotte, NC. You had indicated prior that electronic submittal of these reports was
sufficient.
These reports relate to the release reported to you on March 9, 2021, that we have discussed on several occasions.
Our next step in the process is to submit a draft Notice of Residual Petroleum and associated plat to you for
review. Based on the data that have been collected, I would like to discuss the proposed area for the soil deed
restriction with you. Please let me know a time that would be convenient for you.
Regards,
Nora
Nora A. Zirps, PE, RSM
ESP Associates, Inc.
7011 Albert Pick Road, Suite E
Greensboro, NC 27409
www.espassociates.com
[e-mail]
336.232.5213 Direct
336.334.7724 Office
336.420.6979 Cell